WQ0001863_Regional Office Historical File Pre 2018 (15)

435 Williams Court, Suite 100
40 Baltimore, N1D 21220 SYNAGRO"'O
www.synagro.com zcr--i ;711 nts /DWR
FEBRUARY 26, 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2018 Annual Report for Permit No. WQ0001863
Dear NCDEQ:
WQROS
MOORESVILLE REGIONAL OFFICE
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Mount Holly, NC.
If you have any questions or need additional information, please do not hesitate to contact
Danny Jackson at [phone] or Adam Brigman at [phone].
Sincerely,
k�'
Derrick Shivar
Environmental- Compliance Manager
Enclosures .
cc: Danny Jackson, City of Mount Holly
Adam Brigman, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

City of Mount Holly, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0001863
2018 ANNUAL REPORT

City of Mount Holly, NC
Residuals Land Application Program
2018 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00001863 County Gaston Year 2018
Facility Name (as shown on permit) Mount Holly WWTP & WTP NPDES No. NCO021156 & 01-36-020
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 22
Total number of fields utilized for land application during the year: 14
Total amount of dry tons applied during the year for all application sites: 207.03
Total number of acres utilized for land application during the year: 218.65
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including th possi i ity of fines and imprisonment for
knowing violations."
Danny Jackson, City Manager 113— 1q
Permittee Name d Title ( pe or print) Signat re Pe Date
7,0 �I�u)I
ignatu • of Preparer* Date Signa e and Appl e Date
(if different from Permittee) (if different from ermittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
MOUNT HOLLY, NC
■IOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
MONTHNEAR
March 2018
May 2018
June 2018
August 2018
December 2018
YEARLY TOTAL
AMOUNT UNIT
892,800.00
G
117, 800.00
G
409,200.00
G
787,400.00
G
688,200.00
G
2,895,400.00
G
DRY TONS
UNIT
71.85
D
7.66
D
26.62
D
60.72
D
40.18
D
207.03
D
DRY METRIC
TONS
65.17
6.95
24.14
55.09
36.45
187.80
1 /28/2019

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001863
Facility Name: MOUNT HOLLY, NC
NPDES# : NCO021156
or WQ# (residual only)
WWTP Name: MOUNT HOLLY WWTP
Residuals Analysis Data
Product Type
Date Sampled (grab) or
Date Composited
Percent Solids
AEDLIQ
01/15/18
AEDLIQ
AEDLIQ.
03/21/18
06/19/18
1.93 1.56 1.85
Laboratory
Waypoint Analytical Virginia Inc.
SHEALY ENVIRONMENTAL SERVICES INC.
AEDLIQ
10/01/18
1.40
PARAMETERS (mg/kg dry weight)
Arsenic
<3
18 <5
<5
Cadmium
<2
P
/ <-15—7 <1
J<0.4
<1
Mercury
<0.4
/ <116 ITV
0.0149
Chromium
154
120 J 169
4.78
Copper
359
390 487
11.2
Lead
10.8
« 0� a 9.99
�
<3
Molybdenum
Nickel
<5
12.6
<42� 5.02
<120 16.1
<2.5
<2.5
Selenium
<5
� J
<6�<5
<5
Zinc
650
620 769
18.7
Total Phosphorus
12000
14000 14200
269
TKN
73200
69000 71500
176000
Ammonia -Nitrogen
10800
6100 28000
22100
Nitrate and Nitrite
<23
38 <2. 42
573
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURV DF PREPARER)
Date Z - 2- Z%
DENR FORM RSSF (5/2003) Printed: Wednesday - February 6, 2019 at 08:55:38 for: 1701 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
WQ0001863
Facility Name:
MOUNT HOLLY, NC
NPDES# :
NCO021156
or WQ# (residual only)
WWTP Name:
MOUNT HOLLY WWTP
Residuals Analysis Data r/
Product Type
AEDLIQ
AEDLIQ
Date Sampled (grab) or
01/15/18
03/21/18
Date Composited
Percent Solids
1.93
1.56
PARAMETERS (mg/kg dry weight)
Laboratory
Waypoint Analytical Virginia Inc.
SHEALY ENVIRONMENTAL SERVICES INC.
AEDLIQ AE LIQ
06/19/18 10/01/18
1.85 1.40
Aluminum
9390
9600
8530
231
Calcium
8180
7100
9330
224
Magnesium
2340
2900
3130
55.7
pH
7.38
7.14
7.40
7.50
Potassium
2940
4800
3070
<50
Sodium
5150
8100
5320
<250
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date 2 /2"/ �
(SIGNATURE
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Wednesday - February 6, 2019 at 08:59:57 for: 1701 01

Page: 1 of 2
Report Number: 18-016-0202
Account Number: 00015
Submitted By: Adam Brigman
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 58078
Sample Id : Mt Holly 1 of
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Total Phosphorus
Total Potassium
Total Sulfur
Total Calcium
Total Magnesium
Total Sodium
Total Iron
Total Aluminum
Total Manganese
Total Copper
Total Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
(D 7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalyttcal.com
Project: Mt Holly
REPORT OF ANALYSIS
Date Sampled: 1/16/2018 06:30:00
Date Received: 01/16/2018 00:00
Date Reported: 01/23/2018
RESULT
RESULT
QUANTITATION
METHOD
1.93
19300
100.0
JM
01/16/201815:00
SM-254OG
98.06
100.0
JM
01116/201815:00
SM-2540G
7.32
73200
50.0
R D
01/17/2018 08:15
SM-4500-NH3C-TKN
1.20
12000
100
MOS
01/17/201816:07
6010C
0.29
2940
100
MOS
01117/201815:07
6010C
1.20
12000____
_100—__
MOS
01/17/201815:07—
6010C-
0.82
8180
100
MOS
01/17/201815:07
6010C
0.23
2340
100
MOS
01/17/201815:07
6010C
0.52
5150
100
MOS
01/17/201815:07
6010C
6110
100
MOS
01/17/201815:07
6010C
9390
100
MOS
01/17/201815:07
6010C
210
5.00
MOS
01/17/201815:07
6010C
359
5.00
MOS
.01/17/201815:07
6010C
650
5.00
MOS
01/17/201815:07
6010C
1.08
10800
50.0
R D
01/17/2018 08:.15
SM-4500-NH3C
6.24
62400
50.0
01/17/2018 08:15
CALCULATION
<23.0
23.0
MMT
01/18/2018 08:53
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
�« imp G�
t)trrreporls and tellers are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or olber public announcements without obtaininrd our prior written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 18-016-0202
Account Number: 00015
Submitted By: Adam Brigman
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Waypoint 0 (D
ANALYTICAL
Project: Mt Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Lab Number: 58078 REPORT OFANALYSIS Date Sampled: 1/15/2018 06:30:00
Date Received: 01/16/2018 00:00
Sample Id : Mt Holly 1 of 4 Date Reported: 01/23/2018
---------
«.uu
z.uu
MOS
01/17/2018 15:07
6010C
Total Chromium
154
5.00
MOS
01/17/2018 15:07
6010C
Total Nickel
12.6
5.00
MOS
01/17/2018 15:07
6010C
Total Lead
10.8
5.00
MOS
01/17/2018 15:07
6010C
Total Arsenic
<3.00
3.00
MOS
01/17/2018 15:07
6010C
Total Mercury
<0.400
0.400
MOS
01/22/2018 15:35
SW-7471 B
Total Selenium
<5.00
5.00
MOS
01/17/2018 15:07
6010C
pH *
7.38
1.00
R D
01/17/2018 08:15
9045D
Total Molybdenum
<5,00
5.00
MOS
01/17/2018 15:07
6010C
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis,
Our reports andletters are forthe exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made
how« m` 610wr
to the work, the results, or the company in any advertising, news release, orother public announcements without obtaining ourpdor wrilten authorizafion.
Pauric McGroary
Agronomist

WASTEWATER SAMPLE: TkAAN
Way pohit
7621 Wlutepiuc Road Richmond VA 23237 Tcl: 804-743-9,1011
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Account tE
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Svnanro Central LLC/ MT Holly 14:18:01
Mr Hnllv
MSitofner+lnf
Sub'mItted, BY
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�. _. �- • - ) �uPY: l o
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127ol l qa c ,
CAI ,� . �leu, P; :11� AVG 28134
Prdject, LQ -)7U I Phone: 70 �- G b O- `i 3 Z'l I Fax: E-mail: Cp b
Sample Information
Lab Number Collection Information Container Information Please Write in Desired Tests
Sample ID (Lab Use
Only) Type Date Time Number �'�Z 5Q3 N'l'�dl
of Bottles Type Volume
rl
I
mt, No If Me Seri d
t� Glass So oz
�( �(
U.� I y l� Composite I�l�/f 6 ('3o"r its 'Plastic —p it x x
61r
qt < y
_ Grab _ Glass _ oL
_ Composite Plastic --Pint
— t.
— Grab
Composite
_ Glass
Plastic
o`
pint
t
_ Grab
Composite
_ Glass
Plastic
_ o7
—pint
t
Relinquished By: (Signature)
Date
Time
Received By:
Date
Time
(Signature)
1b
Test Available
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate &Organic Nitrogen,
Special Instructions or Remarks
Phosphorus (total, orthor), POMSSILim, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
�/ �n
C /' `GJt[���✓Yk
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen
_/�
Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)

Sodium Absorption Ratio Calculation (SAR) /
I
a
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 1/15/2018 1/1/2018-3/31/2018 1.7900
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (5150 x 1.9300) _ 100 = 99.395
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (8180 x 1.9300) + 100 = 157.874
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2340 x 1.9300) _ 100 = 45.162
Na meq = Na mg/1 _ Molec.Wgt.Na = 99.395 _ 23 = 4.32152
Ca meq = Ca mg/1 _ Molec.Wgt.Ca = 157.874 _ 20 = 7.8937
Mg meq = Mg mg/1 _ Molec.Wgt.Mg = 45.162 _ 12 = 3.7635
SAR = Na meq - SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.32152 _ SgrRoot[0.5(7.8937+3.7635)] = 1.79001
Printed: 2/6/2019
Page 1 10:14

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mount Holly
Project Number: 50-1701
Lot Number:TC21067
Date Completed:06/06/2018
Revision Date: 06/05/2018
NEW
06/06/2018 9:40 AM
Approved and released by:
Project Manager: Lucas Odom
4
MiAM
TNI
ACCREDITED
`AeORAY��J
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: TC21067
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case
Narrative. The sample receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC
standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating
procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the
results page or discussed below.
Where applicable, all solid sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding
time.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 7

Client:Synagro
Description: MOUNT HOLLY 2 OF 4
Date Sampled:03/21/2018 0730
Date Received:03121/2018
Laboratory ID:TC21
Matrix: Solk
% Solids: 1.56t
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Solids) SM 2540G
1
03/21/2018 2118 HRJ
67593
1 350.1
(Ammonia - N ) 350.1
5
03/28/2018 1318 DMA
68028
1
(Nitrate - N ) 9056A
1
03/28/2018 0629 HKL
68009
1
(Nitrite - N ) 9056A
1
03/28/2018 0629 HKL
68010
1
(pH) 9045D
1
03/22/2018 1439 KNF
67673
1
(Phosphorus) 365.1
2
03/22/2018 1639 DMA
03/22/2018 1130 67619
2 351.4
(TKN) 351.2
1
03/30/2018 1610 DMA
03/30/2018 1037 68335
CAS Analytical
Parameter Number Method Result Q LOCI Units Run
% Solids SM 254OG 1.56 % 1
Ammonia - N (gas diffusion) 350.1 6100 320 mg/kg 1
Nitrate - N (soluble) 9056A 38 13 mg/kg 1
Nitrite - N (soluble) 9056A 310 13 mg/kg 1
pH 9045D 7.14 su 1
Phosphorus 7723-14-0 365.1 14000 640 mg/kg 1
TKN 351.2 69000 1600 mg/kg 2
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 03/27/2018 1519 CJZ 03/24/2018 1212 67745
2 3050B 6010D 1 04/26/2018 1657 CJZ 04/24/2018 1140 70177
CAS Analytical
-Parameter Number Method Result Q LOQ DL �� Units Run
luminum 7429-90-5 6010D 9600 % 1200 450 ` mg/kg 1
Arsenic 7440-38-2 6010D 18 J ! 45 15 mg/kg 1
Cadmium 7440-43-9 6010D ND ! 15 3.8 mg/kg 1
Calcium 7440-70-2 6010D 7100 J l 15000 1900 1 mg/kg 1
Chromium 7440-47-3 6010D 120 ' 30 7.5 j mg/kg 1
Copper 7440-50-8 6010D 390 30 13 mg/kg 1
Iron 7439-89-6 6010D 5600 300 140 mg/kg 1
Lead 7439-92-1 601OD ND f 30 13 mg/kg 1
Magnesium 7439-95-4 6010D 2900 J 'i 15000 1900 // mg/kg 1
Manganese 7439-96-5 6010D 120 y 45 18 /{ mg/kg 1
Molybdenum 7439-98-7 6010D ND i 42 11 / mg/kg 2
Nickel 7440-02-0 6010D ND 1 120 31 mg/kg 1
Potassium 7440-09-7 6010D 4800 J 15000 1900, mg/kg 1
Selenium 7782-49-2 6010D ND 60 24 mg/kg 1
Sodium 7440-23-5 6010D 8100 J \15000 190p mg/kg 1
Zinc 7440-66-6 6010D 620 \ 150 37 mg/kg 1
0
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
:aly Environmental Services, Inc.
i Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 7

Client: Synagro
Description: MOUNT HOLLY 2 OF 4
Date Sampled:03/21/2018 0730
Date Received:03/21/2018
Run Prep Method
1 7471 B
CVAA
Analytical Method Dilution Analysis Date Analyst
7471 B 1 03/27/2018 2108 SLS
Laboratory ID:TC21067
Matrix: Solid /
% Solids: 1.56i
Prep Date Batch
03/27/2018 1849 67978
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GG columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
aaly Environmental Services, Inc.
':I Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 7

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NOW Pali sarnpdes ara ret ned for six weeks from receipt uroless other IA5 USE OWI.Y P0C-- 'I nn—t-O
arran ements are made Race:.'ad nn Ivs i :h=.k} 2fY El N F1I-Peat/ 1 f . (,a a
Blank
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m
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SHEALY ENVIRONMENTAL SERVICES, INC.
Slmnly����cu-sm:atal5crrices, fv,G
Pkt�men; N�snhr 61 LdUe! BL'- ] 2
Nr. 1 nrt
EiRcti v e Unit 12-KIWN l8
Sample Receipt Cheddist {S.R ')
Client: Cuulor 111spectcd b};'dt;tG; C-OL'.: ! -Z"- i ' I ,�� Lot. 0:
Meatlsofreceip(: JZ 51;�51 IUClicnt ❑ UPS ❑FedF.s LICfther:_ -
D YcS1 -1 1. t' me ctxslody Seals present or tho woler?
E]Yesl
DiNa
7NIA
2. Ifolrstcd m-lix Yitnv P3'L:s :nt. were they intactandunbmil, ?
{?II Strip ID: Chlorine Strip TD-
Cooler ID r 0r{gtlal tenipcmttlrc upon rccsript r 1Derived (Caerected) temperature upon receipt:
h'tettiod: QTetnpelraiure thank []Against 1 oulcs 1R Gxrtl ID: j- tit Gun C.-tirr cdcu Faotor: (::'a °C
h4cthod ofcoalunt; I -wet Icu 0 Iee Packs C) DTy Tcc J None _
U Yes
I� Nu
Nel
-- if ienipc'awrc of any cooler exceeded 6.0°C_, was Prc jest Nf naser Notificd?
PM leas Kirtificd by: phone r email , fase-to-facie (circl-e one).
❑ Yes
u Nc,
,n
4. Is the commcrcial courier s packing slip attached to this form?
,Yes
CI No
J5. V,rerz {?ralx.rcustcr iy pmce.lvte, (relinquishcdfrcecitictid} Colluacd
Yes
J No
G. Were sample ILTS list--d rri the COC?
r
Z YtS
E] No
7. Wurx; sarnpk 113a Iht-:d on a4] sample container-57
❑ YoR
Z Non
3. Nils wilm-d-an date its [tine Iis" on the COC?
EI VeR
D'tvn
Clare & time listed on all SWLnple (ontainers^
Ycs
1-1 No
10. 1)id all container lobe] information (11), date, tine) agree with the ('()C'.
OYes
❑ Na
I1, Werc tests w 1.� perfortned listed on tha(.:i'1C:?
Yc s
©No
'
12. Did all samples anivc in the proper w,tlainets for each test and.'or in good condition
(unbroken; ]ids on, ctc,)?
Yes
n No
13, Was adctlua{estuaple vulucleavailablc?
172'Yes
U No
14. Were all samplas rccaivcd within 3,4 thelmlding time or-48 hitun, whichevea-comrs fret?
Yes
21 No
15-'Were any sampt,x5 c;fntainern rrlissin 'e,;ccss (circle orte) s x:nples 14ur 115tcd prt C.()C:?
Ej Yes
i-1 Nu
A
16. Far V 6A and KSK-175 samples, weTe habit l05 rrr:: Lot >" 11ea-size" (!4 'ar &0In in did meter) in
ally of the VIDA vials?
Yes
No
`NA
17, Wm all DR0ime;als+ttutrient samplcR rev eival al a pH of-. 3?
Q Yes
❑ Nu
A
I S. Were all cyanide swples'r;:eived tit a p-H : 13 and ulfide sarnpl rccciced at a piT - 92
Ycs
❑ No
L XNI
119. wcm all xlpplicable. 25 (< C',Jmg�) SurrliWs t1EY-. C rk� t(11J 01
chlorine?
L[ Yes
'D No
21NA
i
20- Were client rornarkslrc-quests (i.e. aegncstcd diimiuns, NiSgUSE) dzsignation i, etc...}
1-oiTt%1ly cranscribcd fronn the COC into the comment wulion in LI64S"
n
I C Yes �x'T140 l V: ag t-he nunte number itscd ll;kcra front the container lab.`1?
5rxnple Preservation {Must he : i�rnple[ial for a �y satuplc(G} ircorrec-tly pn~scrrd nr wit1� ne ulsg�ace.)
5amplc�s} __ tiverz rctuivetl ircorrectl}' ()resor:cd and a'zrc adjnstcXl itcc[trdingly
in "mplt rir:uiving tyith (ITaSt];, INU_, Eel, Nit(011) using SR k
Time 017perservatton.
Sum{rle(s} I vverc., rcccivod with bubbles:-6 mix in diamctrr.
auiples(f l were received wide TRC> 0.5 mglT. (Tf# I9 is no j and was
cjusted aG.^ordingl f�ieT sample receiving'�'ith sodiust� lhio-slilt'atc (7VazS�41� i with 5lxealy IL'1: _
1 _
SR barcode iaiiots applied by:
conlincilts:
I f'� 6 czi l Q. c E; :^. -4-1 Jyt,-ri_ t,, CC., C . C i- 1 '
i
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 3/21/2018 411/2018-6/30/2018 2.5466
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (8100 x 1.5600) = 100 = 126.36
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (7100 x 1.5600) _ 100 = 110.76
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2900 x 1.5600) + 100 = 45.24
Na meq = Na mg/1 _ Molec.Wgt.Na = 126.36 _ 23 = 5.49391
Ca meq = Ca mg/I = Molec.Wgt.Ca = 110.76 = 20 = 5.538
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 45.24 _ 12 = 3.77
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.49391 - SgrRoot[0.5(5.538+3.77)] = 2.54665
Page 1
Printed: 2/6/2019
10:14

(2)
WayPA®intN
NALYTICAL
6/29/2018
Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC, 28134
Ref: Analytical Testing
Report Number: 18-171-0206
Project Description: CITY OF MT. HOLLY
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Wayne Brady:
Waypoint Analytical Virginia, Inc. received sample(s) on 6/20/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam. X 6'_J-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
"ec
Me.
11 t
Page 1 of 7

(2)
WayPAc�intN
NALYTICAL
Client: Synagro Central LLC/ MT Holly
Project: CITY OF MT. HOLLY
Lab Report Number: 18-171-0206
Date: 6/29/2018
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
TKN (Titration) Method SM-4500-NHXJKN
Analyte: TKN
QC Batch No: E64653
Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual
result was
XXJ which calculates to a recovery of XX%.
Analyte was flagged for 0% recovery in the LCS and/or LCSD . The actual result was
.928 which calculates to a recovery of 93%.
Sample 61265 (MT. HOLLY 3 OF 4 N+M)
QC Batch No: E64653
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Nitrate + Nitrite Nitrogen Method SM-4500NO3F
Analyte: NO3+NO2-N
QC Batch No: E64694/E64656
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Solids Total Mercury Analysis - CVAA Method SW-7471 B
Sample 61264
Analyte: Hg
QC Batch No: E64699
MS/MSD Recovery failed, PDS confirmed matrix interference
Page 2 of 7

(2)
Waypoint
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-171-0206
Client Project Description: CITY OF MT. HOLLY
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61265
MT. HOLLY 3 OF 4 N+M
Solids
06/19/2018 06:30
06/20/2018
61265
MT. HOLLY 3 OF 4 N+M
Solids
06/19/2018 06:30
06/20/2018 6010D WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 3 of 7

Report Number: 18-171-0206
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 61265
Sample Id : MT HOLLY 3 OF 4 N+M
Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: CITY OF MT. HOLLY
REPORT OF ANALYSIS Date Sampled: 6/19/2018 06:30:00
Date Received: 06/20/2018 00:00
Date Reported: 06/29/2018
Total Solids *
1.85
18500
100.0
JM
06/20/2018 15:15
SM-2540G
Moisture *
98.14
100.0
JM
06/20/2018 15:15
SM-2540G
Total Kjeldahl Nitrogen
7.15
71500
50.0
R D
06/21/2018-09:00
SM-4500-NH3C-TKN
Phosphorus
1.42
14200
50.0
KKM
06/27/201813:44
601OD
Potassium
0.31
3070
50.0
KKM
06/27/201813:44
601OD
Sulfur
1.15
11500
50.0
KKM
06/27/201813:44
601OD
Calcium
0.93
9330
50.0
KKM
06/27/201813:44
601OD
Magnesium
0.31
3130
50.0
KKM
06/27/201813:44
601OD
Sodium
0.53
5320
250
KKM
06/27/201813:44
601OD
Iron
5930
50.0
KKM
06/27/201813:44
601OD
Aluminum
8530
50.0
KKM
06/27/201813:44
601OD
Manganese
160
5.00
KKM
06/27/201813:44
6010D
Copper
487,
2.50
KKM
06/27/2018 13:44
6010D
Zinc
769
5.00
KKM
06/27/201813:44
6010D
Ammonia Nitrogen
2.80
28000
50.0
JM
06/21/2018 09:00
SM-4500-NH3C
Organic N
4.35
43500
50.0
06/21/2018 09:00
CALCULATION
Nitrate+Nitrite-N
<2.42
2.42
MMT
06/22/2018 09:48
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk.
Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Page 4of7

Report Number: 18-171-0206
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 61265
Sample Id : MT. HOLLY 3 OF 4 N+M
Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: CITY OF MT HOLLY
REPORT OF ANALYSIS Date Sampled: 6/19/2018 06:30:00
Date Received: 06/20/2018 00:00
Date Reported: 06/29/2018
Cadmium
<1.00
Chromium
169
Nickel
16.1
Lead
9.99
Arsenic
<5.00
Mercury
<0.400
Selenium
<5.00
pH *
7.4
Molybdenum
5.02
Comments:
NC CERT#257
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
1.00
KKM
06/27/201813:44
601OD
2.50
KKM
06/27/201813:44
601OD
2.50
KKM
06/27/201813:44
601OD
3.00
KKM
06/27/201813:44
6010D
5.00
KKM
06/27/201813:44
6010D
0.400
MMT
06/22/2018 15:14
SW-7471 B
5.00
KKM
06/27/201813:44
6010D
1.0
R D
06/21/2018 09:00
9045D
2.50
KKM
06/27/201813:44
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
?We, r- #1 C 10*4r,
Pauric McGroary
Agronomist
Page 5 of 7

Waypoint-Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 00015
Customer Name: Synagro Central LLC/ MT Holly
Report Number: 18-171-0206
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
• Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
• Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
• Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
® N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature: lBrandi Watson Date & Time: 06/20/2018 13:45:33
Page 6 of 7

m
cQ
ro
--It
0
-J
'WASTEWATER sAp�,E TRANSMITTAL r IIIIIIIilllllilllllllilllllllllllllllllllllllllllllllllllllllllll18 "' °206
� �- 000ls
Waypolllt AnalytrCal Svnanro Central LLC! MT Holly 06-20-2018
7621 Whitepine Road Richmond VA 23237 Tel.: [phone] Fax: [phone] CITY OF MT. HOLLY 13:44:21
Account #
Customer Information
Submitted By Charge To t;opy I o
/�
� I iGt Wl Q 1-s k7116i!P7
%/jQL 2 GL
12-701 �a2, q_ F1 cv`
C4 v orlAq 1/4
1 Fbne v ,'Il i Al 2-9134
Project
SO-17®9
Phone: 70`1 — 650 — t-1 5 4
Fax
E-mail: 0—kJ
Sample Information
Lab Number
Collection Information
Container Information
Please Write In Desired Tests
Sample ID
(Lab Use
Only)
Type
Date
Time
Number
Type
Volume
SL2
H
of Bottles
M� •l�'Sect
n ,1
AM, fLC Il' �
�n
_Grab
�
011tz
��'1
lass
dPlastic
�j�
� oz
int
—qt
�/
L\
�/
/v
Y
�(
�f_Composite
-
_ Grab
_ Glass
oz
pint
— Composite
— Plastic
t
Grab
_ Glass
Oz
Pint
— Composite
— Plastic
t
_ Grab
_ Glass
oz
pint
FT
— Composite
— Plastic
t
P,plin uished By: (Signature)
Date
Time
Received By: (Signature)
Date
Time
/y /.
r
p
Test Available
Special Instructions or Remarks
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
Phosphorus(total, orthcr), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 6/19/2018 711/2018-9130/2018 1.6497
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (5320 x 1.8500) = 100 = 98.42
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (9330 x 1.8500) = 100 = 172.605
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3130 x 1.8500) _ 100 = 57.905
Na meq = Na mg/I = Molec.Wgt.Na = 98.42 + 23 = 4.27913
Ca meq = Ca mg/I = Molec.Wgt.Ca = 172.605 = 20 = 8.63025
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 57.905 + 12 = 4.82542
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.27913 _ SgrRoot[0.5(8.63025+4.82542)] = 1.64975
Printed: 2/6/2019
Page 1 10:15

Waypoint(D
ANALYTICAL
10/11/2018
Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC, 28134
Ref: Analytical Testing
Report Number: 18-275-0202
Project Description: City of Mt Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Wayne Brady:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/2/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P� IV 6&7,-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
O i t
�s
Page 1 of 6

(D
Waypoint
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 ° Fax [phone].
ANALYTICAL
www.waypointanalytical.com
Sample Summary Table
Report Number:
18-275-0202
Client Project Description:
City of Mt Holly
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
62940
Mt Holly 4 of 4 N&M
Solids
10/01/2018 13:00
10/02/2018
62940
Mt Holly 4 of 4 N&M
Solids
10/O1/2018 13:00
10/02/2018
SM-4500-NH3C
WTN
62940
Mt Holly 4 of 4 N&M
Solids
10/01/2018 13:00
10/02/2018
9045D
WTN
62940
Mt Holly 4 of 4 N&M
Solids
10/O1/2018 13:00
10/02/2018
4500NO3F-2011
WTN
62940
Mt Holly 4 of 4 N&M
Solids
10/O1/2018 13:00
10/02/2018
6010D
WTN
62940
Mt Holly 4 of 4 N&M
Solids
10/01/2018 13:00
10/02/2018
SW-7471B
WTN
62940
Mt Holly 4 of 4 N&M
Solids
10/01/2018 13:00
10/02/2018
SM-4500-NH3C-TKN
WTN
62940
Mt Holly 4 of 4 N&M
Solids
10/01/2018 13:00
10/02/2018
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Report Number: 18-275-0202
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 62940
Sample Id : Mt Holly 4 of 4 N&M
Waypoint.(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: City of Mt Holly
REPORT OF ANALYSIS Date Sampled: 10/1/2018 13:00:00
Date Received: 10/02/2018 00:00
Date Reported: 10/11/2018
Total Solids *
1.40
14000
100.0
CJR
10/04/2018 13:45
SM-2540G
Moisture *
98.60
100.0
CJR
10/04/2018 13:45
SM-2540G
Total Kjeldahl Nitrogen
17.60
176000
120
CLIP
10/09/2018 13:30
SM-4500-NH3C-TKN
Phosphorus
0.03
269
50.0
BKN
10/09/201814:23
601OD
Potassium
<50.0
50.0
BKN
10/09/201814:23
601OD
Sulfur
0.02
232
50.0
BKN
10/09/201814:23
601OD
Calcium
0.02
224
100
JTR
10/10/201816:31
601OD
Magnesium
55.7
50.0
BKN
10/09/201814:23
601OD
Sodium
<0.03
<250
250
BKN
10/09/201814:23
601OD
Iron
218
50.0
BKN
10/09/201814:23
601OD
Aluminum
231
50.0
BKN
10/09/201814:23
601OD
Manganese
5.26
5.00
BKN
10/09/201814:23
6010D
Copper
11.2
2.50
BKN
10/09/201814:23
6010D
Zinc
18.7
5.00
BKN
10/091201814:23
6010D
Ammonia Nitrogen
2.21
22100
50.0
ZBD
10/08/2018 14:00
SM-4500-NH3C
Organic N
15.39
153900
120
10/08/2018 14:00
CALCULATION
Nitrate+Nitrite-N
573
4.72
ZBD
10/09/201815:40
4500NO317-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding
Time
Pow«
- /
P 60w
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist
Page 3 of 6

Report Number: 18-275-0202
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 62940
Sample Id : Mt Holly 4 of 4 N&M
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Molybdenum
Comments:
Waypoint(D
ANALYTICAL
Project : City of Mt Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OF ANALYSIS Date Sampled: 10/1/2018 13:00:00
Date Received: 10/02/2018 00:00
Date Reported: 10/11/2018
<1.00
1.00
BKN
10/09/201814:23
6010D
4.78
2.50
BKN
10/09/201814:23
6010D
<2.50
2.50
BKN
10/09/201814:23
6010D
<3.00
3.00
BKN
10/09/201814:23
6010D
<5.00
5.00
BKN
10/09/201814:23
6010D
0.0149
0.0144
KKM
10/05/2018 12:52
SW-7471 B
<5.00
5.00
BKN
10/09/201814:23
6010D
7.5
JSL
10/08/2018 08:50
9045D
<2.50
2.50
BKN
10/09/201814:23
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
?We, C. X C 110*4r,
Pauric McGroary
Agronomist
Page 4 of 6

Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 00015
Customer Name: Synagro Central LLC/ MT Holly
Report Number: 18-275-0202
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
• Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
® N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
• N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lBrandi Watson Date & Time: 10/02/2018 12:37:21
Page 5 of 6

.WASTEWATER SA 1111111111111111111111111111111111111111111111111111II11111111111as 02 2018Z
Svnaaro Central LLC/ MT Holly
City of MI Holly 12:34:09
7621 Whitepine Road Richmond VA
TN
-customer inlu1.1.I,aU —
/� J (? Submitted By Charge To
/ IU rvl 13n MaP7 r0 (-QA-4reL�
12701 Gac �� Fly l
dF pf'n e ;1 Le All— 2-191311
roject. 5O'I1oi Phone: /Qq _ �i.5©_'q5Ll I Fax:
Q PS
vccount #
�� C��®D� A
ypointanalyticaI.com
Copy To
E-mail: l� h !�,` � , � r•�„_,. ,
Sample Information
Lab Number
Collection Information
Container Information
Please Write in Desired Tests
Sample ID
(Lab Use
Only)
Type
Date
Time
Number
Type
Volume
�I
L 2
�� 5
/(/ try,
Jr
—7—
of Bottles
M4' Hcllt
1/Crab
/
Glass
oz
I°''N v
—Composite
I �( /%�
I'U�P""
tit Plastic
�fnt
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X,
Grab
Glass
— oz
— Composite
_
— Plastic
pint
t
_ Grab
Glass
— oz
— Composite
_
Plastic
—pin`
t
_ Grab
Glass
— oz
— Composite
_
Plastic
—pint
— I
qt
Received
%/ //y t � �> I `V
Test Available
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Pheriol, Solids (Dissolved, Suspended, Total, Volatile)
Date Time
Special Instructions or

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 10/1/2018 10/1/2018-12/31/2018 0.4570
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (250 x 1.4000) = 100 = 3.5
Ca mg/1 = (Ca mg/kg x % Solids) _ 100 = (224 x 1.4000) _ 100 = 3.136
Mg mg/1 = (mg mg/kg x % Solids) _ 100 = (55.7 x 1.4000) = 100 = 0.7798
Na meq = Na mg/I _ Molec.Wgt.Na = 3.5 _ 23 = 0.152174
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 3.136 _ 20 = 0.1568
Mg meq = Mg mg/1 _ Molec.Wgt.Mg = 0.7798 _ 12 = 0.0649833
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.152174 _ SgrRoot[0.5(0.1568+0.0649833)] = 0.456973
Printed: 2/6/2019
Page 1 10:15

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: HULETT
OWNER: RIVER TAW FARMS PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 34.28
SITE #: NC CL 00012 FIELD# : CL 00012 0001 OPERATOR: TRAVIS JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 51.20 ACRES PERMITTED: 51.20
Page
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
5/23/18
117,800.00 (G)
2300.7811
1.56
0.150
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
69,000. p
6,100.00 p
38.00 p
21958
FESCUE
May-18
117,800.00 (G)
2,300.781
6/5/18
99,200.00 (G)
1937.500
1.56
0.126
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
69,000. p
6,100.00 p
38.00 p
21958
I FESCUE
6/6/18
93,000.00 (G)
1816.406
1.56
0.118
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
69,000. p
6,100.00 p
38.00 p
21958
I FESCUE
6/7/18
93,000.00 (G)
1816.406
1.56
0.118
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
69,000. p
6,100.00 p
38.00 p
21958
I FESCUE
6/8/18
86,800.00 (G)
1695.313
1.56
0.110
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
69,000.p
6,100.00 p
38.00 p
21958
li FESCUE
6/9/18
37,200.00 (G)
726.563
1.56
0.047
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
69,000.p
6,100.00 p
38.00 p
21958
FESCUE
Jun-18 1
409,200.00 (G)
7,992.188
1 oun uanons/AC: lU,LYZ.Y /
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
29
0.024
0.020
0.161
0.522
0.040
0.002
0.056
0.161
0.080
0.83Q 18.75
Cumulative Ibs/acre
0.024
0.020
0.161
0.522
0.040
0.002
0.056
0.161
0.080
0.830
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
141
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 k
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
g
(SIGNATURE OfLAND APPL DATE
I
V p..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified persor
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields v

FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: MADISON
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 3.49
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 3.40 ACRES PERMITTED: 3.40
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
��"
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acre
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
3/15/18
43,400.00 (G)
12764.706
1.93
1.027
MHAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
73,200. p
10,800.00 p7�1
24143
FESCUE
Mar-18
43,400.00 (G)
12,764.706
1 Mal Va11[1nJ/1AE;_.
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 50
0.006 0.004 0.316 0.738 0.022 <.001 0.010 0.026 0.010 1.336 24.66
Cumulative Ibs/acre 0.015 0.010 0.954 2.267 0.091 0.002 0.026 0.069 0.026 3.715
Permit PAN Limit (]bs/acre) 1st Crop/2nd Crop
;
149
FD Cumulative Pollutant Loading Rate Limit Ibs/acre
g ( )
36.6
34 8
\
1339.0
267.9
15.0
375.0
89.0
2500.0 v
�'
r
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
11�,_ -
x G
- -
( NAT F LAN LIER) DATE
"I certi , under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0006
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 14.47
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or
or Wet Tons (WT) (specify)
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
3/15/18
179,800.00 (G)
20202.247
1.93
1.626
MHAEDL
MOIST
0-<1/2"
SUR
0.5
03F17T7.
10,800.00 p
23.00 p
24143
FESCUE
Mar-18
179,800.00 (G)
20,202.247
1
Total Gallons/Ac: 20,202.25
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 79
0.010 0.007 0.501 1.167 0.035 0.001 0.016 0.041 0.016 2.114 39.02
Cumulative lbs/acre 0.071 0.045 5.887 11.895 0.688 0.024 0.161 0.571 0.120 17.995
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
'�
183
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
(SIGNATURE O AND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE M NC GA 00041 FIELD# : GA 00041 0010
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 12.97
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90
Page : 1
Lime Applied ***
Date::T
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oYO
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pprn)
Crop
MONTH
Total
Per Acre
Solids
3/15/18
68,200.00 (G)
8632.911
1.93
0.695
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
FESCUE
3/16/18
93,000.00 (G)
11772.152
1.93
0.947
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
FESCUE
Mar-18
1 161,200.00 (G)
1 20,405.063
Total Gallons/Ac: 20,405.06
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 79
0.010 0.007 0.506 1.179 0.035 0.001 0.016 0.041 0.016 2.135 39.41
Cumulative lbs/acre
0.043 0.028 3.845 7.683 0.439 0.016 0.108 0.377 0.075 11.532
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
�"
04
q
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
TT
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
X 2 ��
(SIGNATU F LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0014
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 12.48
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.80 ACRES PERMITTED: 6.80
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
3/16/18
155,000.00 (G)
22794.118
1.93
1.834
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
FESCUE
Mar-18
155,000.00 (G)
22,794.118
1
1
Total Gallons/Ac: 22,794.12
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg M6 Ni Se Zn P PAN
Annual Ibs/acre 89
0.011 0.007 0.565 1.317 0.040 0.001 0.018 0.046 0.018 2.385 44.03
Cumulative Ibs/acre 0.056 0.037 4.911 9.885 0.556 0.019 0.134 0.460 0.097 15.136
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
,
185
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X 2A� / 9
(SIGN URE OF APPLI DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: LLOYD
OWNER: DAVID ALLEN PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 18.18
SITE #: NC GA 00045 FIELD# : GA 00045 0001 OPERATOR: DAVID ALLEN CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pprn)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate **
Rate
Nitrite
8/27/18
93,000.00 (G)
5470.588
1.85
0.422
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE HAY
8/28/18
74,400.00 (G)
4376.471
1.85
0.338
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE HAY
8/29/18
68,200.00 (G)
4011.765
1.85
0.309
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE HAY
Aug-18
235,600.00 (G)
13,858.824
I VLa ij,000.oc
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual lbs/acre
-
5 g
0.011
0.002
0.361
1.041
0.021
<.001
0,011
0.034
0.011
1.644 30.36
Cumulative lbs/acre
0.045
0.025
3.055
6.953
0.360
0.010
0.072
0.257
0.068
10.889
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
176
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
W._._.. m
1339.0
267.9
15.0 1
#_..... #
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
(SIGNA-rURE OF J PA PLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: JENNY SHANK PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 16.74
SITE #: NC LT 00044 FIELD# : LT 00044 0001 OPERATOR: LEE SHANK CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 15.65 ACRES PERMITTED: 15.65
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/18/18
62,000.00 (G)
3961.661
1.85
0.306
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE PASTURE
8/20/18
99,200.00 (G)
6338,658
1.85
0.489
MHAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE PASTURE
8/21/18
55,800.00 (G)
3565.495
1.85
0.275
MHAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE PASTURE
Aug-18
217,000.00 (G)
13,865.814
1 'A -al Mallullb/11C. 1J,003.01
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
5 g
0.011
0.002
0.362
1.042
0.021
<.001
0.011
0.034
0.011
1.645
30.38
Cumulative lbs/acre
0.011
0.002
0.362
1.042
0.021
<.001
0.011
0.034
0.011
1.645
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
209
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 €
375.0
89.0
2500.0
MHAEDL= MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
(SIGNATURE O APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

S
FACILITY NAME: MOUNT HOLLY, NC
OWNER: TONY JONES
SITE #: NC LT 00046 FIELD# : LT 00046 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 12.97
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80
Page: 1
Lime Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
3/19/18
24,800.00 (G)
2101.695
1.93
0.169
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
I FESCUE
3/23/18
31,000.00 (G)
2627.119
1.93
0.211
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
I FESCUE
3/24/18
105,400.00 (G)
8932.203
1.93
0.719
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
FESCUE
Mar-18
161,200.00 (G)
13,661.017
Total Gallons/Ac: 13,661.02
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 53
0.007 0.004 0.339 0.789 0.024 <.001 0.011 0.028 0.011 1.429 26.39
Cumulative lbs/acre 0.069 0.042 5.174 9.423 0.637 0.019 0.108 0.440 0.107 14.709
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
1
",
a
Y
167
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
(SIGNATU AND APPLIER) DATE
"I certify, un er penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 23.53
SITE #: NC LT 00046 FIELD# : LT 00046 0002 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 45.20 ACRES PERMITTED: 45.20
Page: 1
Lime Applied ***
Date
Lbs Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
I
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
12/7/18
179,800.00 (G)
3977.876
1.40
0.232
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
176,00(p
22,100.00 p
573.00 p
57793
FESCUE PASTURE
12/8/18
161,200.00 (G)
3566.372
1.40
0.208
MHAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
176,00(p
22,100.00 p
573.00 p
57793
FESCUE PASTURE
12/27/18
62,000.00 (G)
1371.681
1.40
0.080
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
176,00(p
22,100.00 p
573.00 p
57793
FESCUE PASTURE
Dec-18
1 403,000.00 (G)
8,915.929
Total Gallons/Ac: 8,915.93
TOTALS
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
60
0.005
0.001
0.005
0.012
0.003
<.001
0.003
0.003
0.005
0.019 0.28
Cumulative lbs/acre
0.367
0.075
6.021
30.640
2.071
0.065
0.344
1.386
0.167
37.562 1 . ___,
7 - 711
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
149
FD Cumulative Pollutant LoadingRate Limit Ibs/acre
( )
36.6
34.8
1339.0
267.9
' '
15.0 �
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X.
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: MOUNT HOLLY, NC
OWNER: TONY JONES
SITE #: NC LT 00046 FIELD# : LT 00046 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 9.98
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90
Page: 1
Lime Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm )
Crop
p
Total
Per Acre
MONTH
3/19/18
86,800.00 (G)
8767.677
1.93
0.706
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
FESCUE
3/23/18
18,600.00 (G)
1878.788
1.93
0.151
MHAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
I FESCUE
3/24/18
18,600.00 (G)
1878.788
1.93
0.151
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
FESCUE
Mar-18
124,000.00 (G)
12,525.253
1 otal Gallons/Ac: 12,525.25
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.006 0.004 0.310 0.724 0.022 <.001 0.010 0.025 0.010 1.310 24.19 49
Cumulative lbs/acre 0.075 0.046 5.626 10.242 0.691 0.021 0.119 0.489 0.117 15.838
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
3
167
„I
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
f'
1339.0
267.9
15.0
375.0
89.0 2500.0
a.
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
(SIGNATUR&OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: MOUNT HOLLY, NC
OWNER: TONY JONES
SITE #: NC LT 00046 FIELD# : LT 00046 0004
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 16.65
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 19.40 ACRES PERMITTED: 19.40
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
12/26/18
161,200.00 (G)
8309.278
1.40
0.485
MHAEDL
MOIST
0-<1/2"
SUR
0.5
22,100.00 p
573.00 p
57793
FESCUE PASTURE
12/27/18
124,000.00 (G)
6391.753
1.40
0.373
MHAEDL
MOIST
0-<1/2"SUR
0.5
T3176,00(p
6,00(p
22,100.00 p
573.00 p
57793
FESCUE PASTURE
Dec-18
285,200.00 (G)
14,701.031
rotal Gallons/Ac: 14,701.03
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs/acre
99
0.009
0.002
0.008
0.019
0.005
<.001
0.004
0.004
0.009
0.032
0.46
Cumulative lbs/acre
0.145
0.074
4.587
40.531
1.672
0.085
0.461
1.555
0.167
37.068
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
i
148
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 r
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
Xx;v / 0 ,2111117
(SIG ATU O D APPLIER) DATE
"I certi under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: LLOYD
OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 15.31
SITE #: NC LT 00046 FIELD# : LT 00046 0005 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90
Page
Lime Applied ***
Date
+_Ibs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/14/18
99,200.00 (G)
12556.962
1.85
0.969
MIIAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE PASTURE
8/15/18
99,200.00 (G)
12556.962
1.85
0.969
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE PASTURE
Aug-18
1 198,400.00 (G)
25,113.924
I otal Gallons/Ac: 25,11392
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
105
0.019
0.004
0.655
1.887
0.039
0.002
0.019
0.062
0.019
2.980
55.02
Cumulative Ibs/acre
0.056
0.023
3.042
5.987
0.320
0.009
0.068
0.254
0.068
9.149
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
139
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500,0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
(SIGNAT�UOF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: MOUNT HOLLY, NC
OWNER: TONY JONES
SITE #: NC LT 00046 FIELD# : LT 00046 0007
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: PACOLET
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 10.52
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.00 ACRES PERMITTED: 7.00
Page
Lime Applied ***
Date
Lbs/Ae
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/15/18
6,200.00 (G)
885.714
1.85
0.068
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE HAY
8/16/18
49,600.00 (G)
7085.714
1.85
0.547
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE HAY
8/17/18
55,800.00 (G)
7971.429
1.85
0.615
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE HAY
8/18/18
24,800.00 (G)
3542.857
1.85
0.273
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
71,500. p
28,000.00 p
2.42 p
27052
FESCUE HAY
Aug-18
1 136,400.00 (G)
19,485.714
Total Gallons/Ac: 19,485.71
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
81
0.015
0.003
0.508
1.464
0.030
0.001
0.015
0.048
0.015
2.312 42.69
Cumulative lbs/acre
0.045
0.023
2.944
5.828
0.339
0.011
0.065
0.277
0.065
8.569 _.
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
182
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X ll c
(SlGNATI,RE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

FACILITY NAME: MOUNT HOLLY, NC
OWNER: TONY JONES
SITE #: NC LT 00046 FIELD# : LT 00046 0008
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 5.49
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60
Page: 1
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
or Wet Tons (WT) (specify)
0
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
TP7rAcre
Solids
3/23/18
68,200.00 (G)
10333.333
1.93
0.832
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
73,200. p
10,800.00 p
23.00 p
24143
FESCUE PASTURE
Mar-18
68,200.00 (G)
10,333.333
r
total Gallons/Ac: 1U,333.33
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual Ibs/acre 40
0.005 0.003 0.256 0.597 0.018 <.001 0.008 0.021 0.008 1.081 19.96
Cumulative Ibs/acre
0.071 0.045 5.425 9.866 0.670 0.021 0.114 0.476 0.112 15.164 l; ••,•„
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
36.6
34.8
1339.0
267.9
15.0 375.0
a
89.0
171
2500.0
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X/2��7 __, /I
(SIGNATU OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

SECTION 4

MSU101mor
M-41WROtdhiENf>AL TLCf1N0.LQG1f!5, Inc
Aresfb,tiral L.sbara ashes
February 01, 2018
Adam Brigman
Synagro, NC 28134
12701 Lancaster Hwy
Pineville, NC 28134
TEL: [phone]
FAX: [phone]
RE: Mt Holly
Dear Adam Brigman:
Sununit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Order No.: 18010671
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/16/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
#, f MI-11
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 26

Summit Environmental Technologies, Inc. Case Narrative
fTS-10MMIT 3310 Win St.
5hdirlRt7tlh1EN7'r1L u4:Cd®LQGI , tic_ Cuyahoga Falls, Ohio 44223 ` O#: 18010671
,fir,_aiytrssl Lffharafories TEL: [phone] FAX: [phone]
Website: httv:llwww.settek.com Date: 2/1/2018
CLIENT: Synagro, NC 28134
Project: Mt Holly
WorkOrder Narrative:
18010671: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Notes:
mb-30518 tclp-svoc-cpest_tclp(8081): The TCLP Pesticide Method Blank (Batch 30518) exhibited
high recovery for Surrogates: DCB and TCMX: the MB was ND for all analytes of interest.
lcs-30518 telp-svoc-cpest_tclp(8081): The TCLP Pesticide LCS (Batch 30518) exhibited high recovery
for Surrogates: DCB and TCMX: The LCS Exhibited recoveries within the acceptance limits for all
analytes of interest.
Original
Page 2 of 26

Summit Environmental Technologies, In Qualifiers and Acronyms
fm SugWraff 3310 Win 6
FrWIRONhIENTAL 1'f-"tJOLCMES, INN Cuyahoga Falls, Ohio 4421 WO#: 18010671
itr3iytic'31%h�a'att%{fie. TEL: [phone] FAX.' (330) 253-446
Website: htty://www.settek.co Date: 2/1/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLv1
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximmn Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualiflers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 26

Summit Environmental Technologies, Inc. Workorder
asumpArt 3310 Win St.
t VIRONPa7Et•,�AL#9P30LG'1_5, t aG Cuyahoga Falls, Ohio 44223 Sample Summary
dnwryff of Ls borain de t TEL: [phone] FAX.- [phone] WO#: 18010671
Website: http://Www.settek.com 01-Feb-18
CLIENT: Synagro, NC 28134
Project: Mt Holly
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
18010671-001 Mt Holly TCLP 2018 1/15/2018 6:30:00 AM 1/16/2018 10:05:00 AM Sludge
Page 4 of 26

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENV190NIIENT L TSvWJOLOGISS, III.._
Cuyahoga Falls, Ohio 44223
'
tltTitt{rPtcat #:,�ut7rt3fot-iPs TEL: [phone] FAX.- [phone]
WO#: 18010671
Website: http://www.settek.com
01-Feb-18
Client:
Synagro, NC 28134
Project:
Mt Holly
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
18010671-OOIA Mt Holly TCLP 2018 1/15/2018 6:30:00 AM Sludge Ignitability of Solids (SW-846: 1030)
1/25/2018 1:00:00 PM
pH (SW9045D)
1/17/2018 3:19:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
1/19/2018 4:48:00 PM
Reactive Sulfide (9034)/7.3.4.2
1/19/2018 4:48:00 PM
TCLP Herbicides Analysis (SW1311/81/22/2018 6:00:00 PM
1/23/2018 11:30:00 A 1/26/2018 5:33:00 PM
TCLP Mercury Analysis (SW1311/7471/22/2018 6:00:00 PM
1/23/2018 11:10:00 A 1/23/2018 2:13:00 PM
TCLP Metals Analysis (SW1311/601011/22/2018 6:00:00 PM
1/23/2018 12:00:27 PM 1/23/2018 8:40:48 PM
TCLP Pesticides Analysis (SW1311/8(1/22/2018 6:00:00 PM
1/26/2018 4:11:00 PM
TCLP Semi-Volatiles Analysis 1/22/2018 6:00:00 PM
1/24/2018 7:00:00 AM 1/24/2018 7:33:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
1/22/2018 4:00:00 PM 1/23/2018 4:16:00 PM
Original
Page 5 of 26

Summit Environmental Technologies, Inc.
qt 3310 Win St.
+FUVIRt3NMEN` ALTECI-1 OLi3GIES, VIC Cuyahoga Falls, Ohio 44223
raiyrti a3 ? x arsi rle= TEL: [phone] FAX: [phone]
Website: httD://www.settekcom
Analytical Report
(base report)
WO#: 18010671
Date Reported: 2/1/2018
CLIENT:
Synagro, NC 28134 Tag Number:
Matrix:
SLUDGE Collection Date: 1/15/2018 6:30:00 AM
Lab ID:
18010671-001A
Project:
Mt Holly
Client Sample ED Mt Holly TCLP 2018
Analyses Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: EAM
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND
0.00500
mg/L
1
1/23/2018 2:13:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW3010A
Analyst: KMS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
1.25
mg/L
1
1/23/2018 8:40:48 PM
TCLP Badum(Ba)
ND
12.5
mg/L
1
1/23/2018 8:40:48 PM
TCLP Cadmium(Cd)
ND
0.250
mg/L
1
1/23/2018 8:40:48 PM
TCLP Chromium(Cr)
ND
0.500
mg/L
1
1/23/2018 8:40:48 PM
TCLP Lead(Pb)
ND
1.25
mg/L
1
1/23/2018 8:40:48 PM
TCLP Selenium(Se)
ND
0.125
mg/L
1
1/23/2018 8:40:48 PM
TCLP Silver(Ag)
ND
1.25
mg/L
1
1/23/2018 8:40:48 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND
0.0800
mg/L
2
1/24/2018 7:33:00 PM
2,4,5-Trichlorophenol ND
0.200
mg/L
2
1/24/2018 7:33:00 PM
2,4,6-Trichlorophenol ND
0.200
mg/L
2
1/24/2018 7:33:00 PM
2,4-Dinitrotoluene ND
0.0400
mg/L
2
1/24/2018 7:33:00 PM
o-Cresol ND
0.200
mg/L
2
1/24/2018 7:33:00 PM
m/p-Cresol(s) ND
0.200
mg/L
2
1/24/2018 7:33:00 PM
Cresols, Total ND
4.00
mg/L
2
1/24/2018 7:33:00 PM
Hexachloro-1,3-butadiene ND
0.0160
mg/L
2
1/24/2018 7:33:00 PM
Hexachlorobenzene ND
0.0400
mg/L
2
1/24/2018 7:33:00 PM
Hexachloroethane ND
0.0800
mg/L
2
1/24/2018 7:33:00 PM
Nitrobenzene ND
0.0800
mg/L
2
1/24/2018 7:33:00 PM
Pentachlorophenol ND
0.200
mg/L
2
1/24/2018 7:33:00 PM
Pyridine ND
0.200
mg/L
2
1/24/2018 7:33:00 PM
Surr: 2-Fluorophenol 38.7
10 - 109
%Rec
2
1/24/2018 7:33:00 PM
Surr: PhenoW6 19.2
10 - 109
%Rec
2
1/24/2018 7:33:00 PM
Surr: Nitrobenzene-d5 75.4
19 - 120
%Rec
2
1/24/2018 7:33:00 PM
Surr: 2,4,6-Tribromophenol 46.2
10 - 120
%Rec
2
1/24/2018 7:33:00 PM
Surr: 2-Fluorobiphenyl 67.2
22 - 117
%Rec
2
1/24/2018 7:33:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 6 of 26

Summit Environmental Technologies, Inc. Analytical Report
SUSK10iffit 3310 Win St.
lStfliiQhlhiEN'I',1L�_Ctt€dr]Lr��Jrs,Wr, Cuyahoga Falls, Ohio44223 (base report)
ra.};tics l f_r xat��rl TEL: [phone] FAX: [phone] WO#: 18010671
Website: httn.•//www.settek.com Date Reported: 2/1/2018
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 1/15/2018 6:30:00 AM
Lab ID: 18010671-OOIA
Project: Mt Holly
Client Sample ID Mt Holly TCLP 2018
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14 73.9
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
87.9
Surr: DCB
73.7
SW8270D SW351OC Analyst: BJH
34 - 116 %Rec 2 1 /24/2018 7:33:00 PM
SW8081 Analyst: JBN
0.0100
mg/L
1
1/26/2018 4:11:00 PM
0.0200
mg/L
1
1/26/2018 4:11:00 PM
0.00100
mg/L
1
1/26/2018 4:11:00 PM
0.00100
mg/L
1
1/26/2018 4:11:00 PM
0.00100
mg/L
1
1/26/2018 4:11:00 PM
0.00100
mg/L
1
1/26/2018 4:11:00 PM
0.00100
mg/L
1
1/26/2018 4:11:00 PM
10 - 119
%Rec
1
1/26/2018 4:11:00 PM
10 - 119
%Rec
1
1/26/2018 4:11:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)
2,4-D ND 1.00
2,4,5-TP ND 0.500 d
Surr: DCAA 69.2 20 - 140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
SW8151A SW8151A Analyst: JBN
mg/L 1 1/26/2018 5:33:00 PM
mg/L 1 1/26/2018 5:33:00 PM
%Rec 1 1/26/2018 5:33:00 PM
SW8260B SW1311M Analyst: MES
0.0500
mg/L
10
1/23/2018 4:16:00 PM
0.0500
mg/L
10
1/23/2018 4:16:00 PM
0.250
mg/L
10
1/23/2018 4:16:00 PM
0.0500
mg/L
10
1/23/2018 4:16:00 PM
0.0500
mg/L
10
1/23/2018 4:16:00 PM
0.0500
mg/L
10
1/23/2018 4:16:00 PM
0.0500
mg/L
10
1/23/2018 4:16:00 PM
0.0500
mg/L
10
1/23/2018 4:16:00 PM
0.0500
mg/L
10
1/23/2018 4:16:00 PM
0.0200
mg/L
10
1/23/2018 4:16:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds �-� Permit Limft=:5 Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 26

Summit Environmental Technologies, Inc. 3310 Win St. Analytical Report
t:tb4rIFi0R0ett=,WrALTEtJ*J0Lrt1F5,tnc Cuyahoga Falls, Ohio44223 (base report)
in iytir<al L IaAr sd 5 TEL: [phone] FAX: [phone] WO#: 18010671
Website: htto://www.settek.com Date Reported: 2/1/2018
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 1/15/2018 6:30:00 AM
Lab ID: 18010671-001A
Project: Mt Holly
Client Sample ID Mt Holly TCLP 2018
Analyses Result RL Qual Units D>F' Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Sum 4-Bromofluorobenzene
96.3
Sum Dibromofluoromethane
99.3
Surr: Toluene-d8
98.0
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
RCI-SOLID-W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
RCI-SOLID-W/ IGNITABILITY1030
PH (SW9045D)
pH
7.2
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
SW8260B SW1311M Analyst: MES
70 - 130 %Rec 10 1/23/2018 4:16:00 PM
70 - 130 %Rec 10 1/23/2018 4:16:00 PM
70 - 130 %Rec 10 1/23/2018 4:16:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
SW9014 Analyst: MS
0.500 mg/Kg 1 1/19/2018 4:48:00 PM
SW1030 Analyst: AJT
1 1/25/2018 1:00:00 PM
SW9045D Analyst: DHC
s.u.@18.9C 1 1/17/2018 3:19:00 PM
SW9034 Analyst: MS
25.0 mg1Kg 1 1/19/20184:48:00 PM
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 26

Summit Environmental Technologies, Inc. Accredltatic
sumfArr 3310 Win St.
FS�IRONi,9�kJi'AL3�t t edr9Lt;i, i t4 Cuyahoga Falls, Ohio 44223 Analyten-t --g-
.drraitntral Lzborfiot'fer: TEL: [phone] FAX.- [phone] WO#: 1E
Website: http://N ww.settek.com 01-Feb-18
Client: Synagro, NC 28134 State: NW
Project: Mt Holly Program Name: NC WW SCM
Sample ID Matrix Test Name Analyte Status
18010671-OOIA
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
NC WW SCM A Accredited
Ignitability of Solids (SW-846: 1030)
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
Reactive Sulfide (9034)/7.3.4.2
TCLP Herbicides Analysis (SW 1311/8151)
TCLP Herbicides Analysis (SW1311/8151)
TCLP Herbicides Analysis (SW1311/8151)
TCLP Mercury Analysis (SW1311/7470)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Senu-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Senu-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
NC WW SCM U Unavailable
Ignitability
Hydrogen Ion (pH)
Cyanide, Reactive
Sulfide, Reactive
2,4,5-TP
2,4-D
DCAA
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
2,2',3,3',4,4',5,5',6,6'-
Decachlorobiphenyl
Chlordane, total
Endrin
gamma-BHC
Heptachlor
Heptachlor epoxide
Methoxychlor
Tetrachloro-m-xylene
Toxaphene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Tribromophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
2-Fluorobiphenyl
2-Fluorophenol
A
A
U
U
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
Original 41.
Page 9 of 26

Summit Environmental Technologies, Inc. Accreditation Program
Stsmiolut 3310 Win St. Anal teS Report
i
R-WIRONid1ENMILTIEEC €dv6L,QnIE5, IRC, Cuyahoga Falls, Ohio 44223 Y P
R3nHa vtlNaf Lsboxalorie,- TEL: [phone] FAX.- [phone] WO#: 18010671
Website: http://www.settek.com 01-Feb-18
Client: Synagro, NC 28134 State: NW
Project: Mt Holly Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
18010671-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
3,4-Metlrylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene-d5
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Phenol-d6
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
p-Terphenyl-d14
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
4-Bromofluorobenzene
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Dibromofluoromethane
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Toluene-d8
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original # 1
Page 10 of 26

Summit Environmental Technologies, Inc. QC SUMMARY
/fly /f A 7� �7 REPORT
y T PO T
TdSummmor 3310 Win St. 1. U 1V11� 1L yld I R �`� It 1
E'dVAROW1 04TAI ar--CW4GL0GI=_w, iNIC Cuyahoga Falls, Ohio 44223 WO#: 18010671
nail tfcr� La �zreAacar2es TEL: [phone] FAX: [phone]
Website: http://www.settek.com 01-Feb-18
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 30508
Sample ID Ics 6111 20PPB
SampType: LCS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79763
-lient ID: LCSS
Batch ID: 30508
TestNo: SW8260B SW1311M
Analysis Date: 1/23/2018
SegNo: 1387689
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.0226
0.00500
0.0200
0
113
79.4
131
1,2-Dichloroethane
0.0190
0.00500
0.0200
0
95.1
73.6
137
MEK
0.0919
0.0250
0.100
0
91.9
55.1
163
Benzene
0.0197
0.00500
0.0200
0
98.7
73.1
132
Carbon tetrachloride
0.0195
0.00500
0.0200
0
97.3
63.7
139
Chlorobenzene
0.0183
0.00500
0.0200
0
91.7
72.3
139
Chloroform
0.0200
0.00500
0.0200
0
99.9
79.3
129
Tetrachloroethene
0.0189
0.00500
0.0200
0
94.3
56.2
187
Trichloroethene
0.0191
0.00500
0.0200
0
95.3
64.1
138
Vinyl chloride
0.0211
0.00200
0.0200
0
106
22.1
147
Surr: 4-Bromofluorobenzene
51.6
50.00
103
80.4
126
Surr: Dibromofluoromethane
50.6
50.00
101
70.3
125
Surr: Toluene-d8
48.7
50.00
97.3
82
117
Sample ID mb-30508
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 1/22/2018
RunNo: 79763
client ID: PBS
Batch ID: 30508
TestNo: SW8260B SW1311M
Analysis Date: 1/23/2018
SegNo: 1387696
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected
O RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
Page 11 of 26

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summlar 3310 Win St.
ENIVIROWAGNTAL TECI— MOLOGIES; AINC Cuyahoga Falls, Ohio 44223
WO#: 18010671
AnuTlrPtc.�1' Larp!'Atot-It: TEL: [phone] FAX.- [phone]
Website: ham://Www.settek.com 01-Feb-18
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 30508
Sample ID mb-30508
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 1/22/2018
RunNo: 79763
client ID: PBS
Batch ID: 30508
TestNo: SW8260B SW1311M
Analysis Date: 1/23/2018
SegNo: 1387696
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
497
Surr: Dibromofl uorom ethane
498
Surr: Toluene-d8
494
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
500.0 99.3 70 130
500.0 99.6 70 130
500.0 98.8 70 130
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 12 of 26

�� Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
'Es
EPZVIRC WAZ-:NTA1. TICWJOLOGILS, WC Cuyahoga Falls, Ohio 44223
.1wr,,rlyG'r.-ai L3boraavra€ TEL: [phone] FAX.- [phone]
WO#: 18010671
Website: http.Ilwww.settek.com 01-Feb-18
Client: Synagro, NC 28134
Project: Mt Holly BatchED: 30508
Sample ID 18010656-00laMS
SampType: MS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79761
'lient ID: BatchQC
Batch ID: 30508
TestNo: SW8260B SW1311M
Analysis Date: 1/23/2018
SegNo: 1387669
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.188
0.0500
0.200
0
94.0
39.9
160
1,2-Dichloroethane
0.204
0.0500
0.200
0
102
42.5
157
MEK
1.26
0.250
1.00
0.401
86.0
16.6
227
Benzene
0.184
0.0500
0.200
0
92.1
38.1
155
Carbon tetrachloride
0.197
0.0500
0.200
0
98.4
40.8
162
Chlorobenzene
0.190
0.0500
0.200
0
95.2
35.7
168
Chloroform
0.194
0.0500
0.200
0
97.2
18.3
199
Tetrachloroethene
0.190
0.0500
0.200
0
94.8
10
261
Trichloroethene
0,195
0.0500
0.200
0
97.4
23.8
175
Vinyl chloride
0.189
0.0200
0.200
0
94.3
10
165
Surr:4-Bromofluorobenzene
467
500.0
93.5
84.6
130
Surr: Dibromofl uorom ethane
517
500.0
103
71.4
127
Surr: Toluene-d8
479
500.0
95.9
74.6
127
Sample ID 18010656-00laMSD
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79761
'lient ID: BatchQC
Batch ID: 30508
TestNo: SW8260B SW1311M
Analysis Date: 1/23/2018
SegNo: 1387670
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.186
0.0500
0.200 0 93.0
39.9
160
0.188 1.07
25
1,2-Dichloroethane
0.209
0.0500
0.200 0 105
42.5
157
0.204 2.66
25
MEK
1.35
0.250
1.00 0.401 94.4
16.6
227
1.26 6.41
25
Benzene
0.181
0.0500
0.200 0 90.4
38.1
155
0.184 1.81
25
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 13 of 26

Summit Environmental Technologies, Inc.
summogr 3310 Win St.
eWlR0WPoIZMTAl-TECHNOLOGITSS,WC Cuyahoga Falls, Ohio44223
�ri1•t11 Laa'atct'ie TEL: [phone] FAX.- [phone]
Website: http://Www.settek.com
QC SUMMARY REPORT
WO#: 18010671
01-Feb-I8
Client: Synagro, NC 28134
Project: Mt Holly BatchlD: 30508
Sample ID 18010656-00laMSD
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79761
client ID: BatchQC
Batch ID: 30508
TestNo: SW8260B SW1311M
Analysis Date: 1/23/2018
SegNo: 1387670
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Carbon tetrachloride
0.194
0.0500
0.200
0
97.2
40.8
162
0.197
1.12
25
Chlorobenzene
0.189
0.0500
0.200
0
94.6
35.7
168
0.190
0.685
25
Chloroform
0.198
0.0500
0.200
0
99.0
18.3
199
0.194
1.73
25
Tetrachloroethene
0.187
0.0500
0.200
0
93.6
10
261
0.190
1.22
25
Trichloroethene
0.194
0.0500
0.200
0
97.0
23.8
175
0.195
0.360
25
Vinyl chloride
0.187
0.0200
0.200
0
93.4
10
165
0.189
1.01
25
Surr:4-Bromofluorobenzene
464
500.0
92.8
84.6
130
0
25
Surr: Dibromofluorom ethane
521
500.0
104
71.4
127
0
25
Surr: Toluene-d8
484
500.0
96.9
74.6
127
0
25
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 14 of 26

Summit Environmental Technologies, Inc.sug—AMIT
3310 Wig: St.
QC SUMMARY REPORT
'.�Iret�tarlratT�L#+rJt fkasiF., 3itt
Cuyahoga Falls, Ohio 44223
WO#: 18010671
TEL:
[phone] FAX.- [phone]
Website: http://www.settek.com
01-Feb-18
Client:
Synagro, NC 28134
Project:
Mt Holly
BatchID: 30522
TCLP Mercury ND 0.00200
TCLP Mercury 0.00411 0.00200 0.00400 0 103 80 120
TCLP Mercury 0.00539 0.00200 0.00400 0 135 75 125 S
TCLP Mercury 0.00511 0.00200
0.00400 0 128 75
125
0.00539 5.33 20 S
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit Original
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 15 of 26

MSUMMIT
Summit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
EN%alFtOWACNTAI TE"?JCL GIES, ift�C Cuyahoga Falls, Ohio 44223
•'lrtrrlPttcnf Laboratoaae:� TEL: [phone] FAX.- [phone]
WO#: 18010671
Website: htta.//www.settek.com
01-Feb-18
Client:
Synagro, NC 28134
Project:
Mt Holly
BatchID: 30522
Sample ID 18010789-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/23/2018
RunNo: 79771
Client ID: Batch=
Batch ID: 30522
TestNo: SW7470A SW7470A
Analysis Date: 1/23/2018
SegNo: 1387928
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected Original
P O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 16 of 26

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
r*tVIR0t0.1FWTA1. TEC9 NOLOGIES, fmc. Cuyahoga Falls, Ohio 44223
m9'summior
3310 Win St.
WO#: 18010671
04l�rrf�Plcn.f L'shciratot'It�{ TEL: [phone] FAX.- [phone]
Website: http://Www.settek.com 01-Feb-18
Client: Synagro, NC 28134
Project: Mt Holly BatchID• 30543
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0 d
Surr: DCAA 363 500.0 72.6 20 140
2,4-D
ND 1.00
0.500
0 81.1
62.6
125
2,4,5-TP
ND 0.500
0.500
0 83.6
52.5
128
Surr: DCAA
432
500.0
86.3
20
140
2,4-D
ND 1.00
0.500 0 81.5 37
105
2,4,5-TP
ND 0.500
0.500 0 81.5 38
106
Sum DCAA
399
500.0 79.8 20
140
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 17 of 26

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
slitamlir 3310 Win St.
EP,"0,730WF,1ZWTAL iSCW40L0G4ES: INIC Cuyahoga Falls, Ohio 44223 WOM 18010671
.ratytlea,i Catapraiarle TEL: [phone] FAX- [phone]
Website: http://www.settek.com 01-Feb-18
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 30543
Sample ID 18010671-001amsd
SampType: msd
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/23/2018
RunNo: 79954
Client ID: Mt Holly TCLP 2018
Batch ID: 30543
TestNo: SW8151A SW8151A
Analysis Date: 1/26/2018
SegNo: 1393405
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D ND 1.00 0.500 0 83.3 37 105 0 0 30
2,4,5-TP ND 0.500 0.500 0 85.0 38 106 0 0 30
Surr: DCAA 423 500.0 84.5 20 140 0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 18 of 26

SUMMITSummit Environmental Technologies, vie. 3310 Win St. QC SUMMARY REPORT
ENVIRON&IFNTALTEC+e 40LOG iES, iN'C Cuyahoga Falls, Ohio44223 WOM 18010671
Irra'(lIticaf CaborafuOeiF TEL: [phone] FAX.- [phone]
Website: htto.•Ilwww.settek.com 01-Feb-18
Client: Synagro, NC 28134
Project: Mt Holly BatchID: R79S62
Sample ID LCS-R79562
SampType: LCS
TestCode: pH_011(9045 Units: s.u.@19.7C
Prep Date:
RunNo: 79562
-lient ID: LCSW
Batch ID: R79562
TestNo: SW9045D
Analysis Date: 1/17/2018
SegNo: 1381356
4nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
7.0 0 101 90 110
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 19 of 26

SUMMINt
Summit Envir•onrnental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
ENVIRROW IENTA TEC€HWLOG1E-5,]NC
1:nalyi,'cai L3ooratc+,rie� TEL:
Cuyahoga Falls, Ohio44223
[phone] FAX.- [phone]
WO#: 18010671
Website: http.Ilwww.settek.com
01-Feb-18
Client:
Synagro, NC 28134
Project:
Mt Holly
BatchID: R79728
Sample ID MB-R79728
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 79728
Client ID: PBW
Batch ID: R79728
TestNo: SW9014
Analysis Date: 1/1912018
SegNo: 1386705
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID LCS-R79728
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 79728
Client ID: LCSW
Batch ID: R79728
TestNo: SW9014
Analysis Date: 1/1912018
SegNo: 1386707
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 0.997 0.500 1.000 0 99.7 85 115
Sample ID 18010675-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 79728
Client ID: BatchQC
Batch ID: R79728
TestNo: SW9014
Analysis Date: 1/1912018
SegNo: 1386710
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.10 0.500 1.000 0 110 81.3 118 QMR
Sample ID 18010675-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 79728
Client ID: Batch=
Batch ID: R79728
TestNo: SW9014
Analysis Date: 1/19/2018
SegNo: 1386711
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive
1.03 0.500
1.000 0 103 81.3
118
1.103 7.23
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
5 R
Original
Page 20 of 26

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffJ summur 3310 Wig: St.
ENVIRM-PAENTAI. TECHUCLOGIES: imc Cuyahoga Falls, Ohio 44223 WO#: 18010671
ArrafIffIvaX Laboratories TEL: [phone] FAX: [phone]
Website: htto://www.settek.com 01-Feb-I8
Client: Synagro, NC 28134
Project: Mt Holly BatchID: R79728
Sample ID 18010675-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 79728
client ID: BatchQC
Batch ID: R79728
TestNo: SW9014
Analysis Date: 111912018
SegNo: 1386711
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
NOTES:
The Sample MS and MSD exhibited a high RPD; The MS and MSD exhibited passing recoveries individually; The parent sample is ND.
QualiFers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 21 of 26

M'SUHM111
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
r=NVIRONNIGNTAL TpC9N0LGG4E9, N.0
Cuyahoga Falls, Ohio 44223
WO#: 18010671
.Kr;fiilrriCar Lrrcorrmtw'Ita�" TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
01-Feb-18
Client:
Synagro, NC 28134
Project:
Mt Holly
BatchID: R79777
Sulfide, Reactive ND 25.0
Sulfide, Reactive 4620 25.0 4800 0 96.2 85 115
Sulfide, Reactive 4660 25.0 4800 0 97.1 75 125
Sulfide, Reactive
4560 25.0
4800 0 95.0 75
125
4660 2.17 30
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 22 of 26

Summit Environmental Technologies, Inc.MQC SUMMARY REPORT
SUMIWIT3310 Win St.
ENVIROtdFAEItTAL TrjClitJOLGGirS, !NC Cuyahoga Falls, Ohio 44223
.J;r4aflrL'caf taSarAtraTle5: TEL: [phone] FAX: [phone]
WO#: 18010671
Website: http://www.settek.com 01-Feb-18
Client: Synagro, NC 28134
Project: Mt Holly BatchID: R79777
Sample ID 18010675-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 79777
client ID: BatchQC
Batch ID: R79777
TestNo: SW9034
Analysis Date: 1/19/2018
SegNo: 1388151
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 23 of 26

Summit Environmental Technologies, Inc.PE sumfort 3310 Win St. QC SUMMARY REPORT
ENVIRONNICNTAI. ifCW40L461SS, !O C Cuyahoga Falls, Ohio 44223
Ar;afyUctal Lsboratar e,� TEL: [phone] FAX.• [phone] WO#: 18010671
Website: http•//www.settek.com 01-Feb-18
Client: Synagro, NC 28134
Project: Mt Holly BatchID: R79884
Sample ID LCS-R79884
SampType: LCS
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 79884
;lient ID: LCSS
Batch ID: R79884
TestNo: SW1030
Analysis Date: 1/25/2018
SegNo: 1391034
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability
6.22
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
7.240 0 85.9 70
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
130
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 24 of 26

i
i
190MMIT
ENVIRONMENTAL -TECHNOLOGIES, INC.
3310 iHin Sxrsi
�InitOs,�Ohb 44223
DC�QACOC338 Ray.6.
Effaa i?. Dato:121
28115
Analysis Request /.Chain of Custody
For Summit Environmental Technologies, Inc. use only
Page 1 df 1
Page 25 of 26

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
f. 1�IR6-t1PdEN'fA.L''r='�#:hiFJLdG1E5, ihG- Cuyahoga Falls, Ohio 44223 Sample Log -In Check List
IrrrA-Paryrtiral LabayaiorJes TEL: [phone] FAX: [phone]
Website: http://www.settekeom
Client Name: SYN-NC-28134 Work Order Number: 18010671 RcptNo: 1
Logged by: Christopher Livengood 1/16/2018 10:05:00 AM
Completed By: Christopher Livengood 1/16/2018 3:10:22 PM
Reviewed By: Jennifer Woolf 1/26/2018 6:37:55 PM '^
Chain of Custody
1. Is Chain of Custody complete? Yes d❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Loq In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4, Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes 91 No ❑ NA ❑
7. Sample(s) in proper container(s)?
Yes
❑d
No ❑
8. Sufficient sample volume for indicated test(s)?
Yes
❑d
No ❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
d❑
No ❑
10. Was preservative added to bottles?
Yes
❑
No ❑
NA ❑d
NA
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑
No VOA Vials
12. Were any sample containers received broken?
Yes
❑
No ]
13. Does paperwork match bottle labels?
Yes
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
0
No ❑
15. Is it clear what analyses were requested?
Yes
0
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑
NA ❑d
Person Notified: �� Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions: j
18. Additional remarks:
Cooler Information
Cooler No
I Temp °C
I Condition
I Seal Intact
I Seal No
I Seal Date
Signed By
1
12.6
Page 26 of 26

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: WQ0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 01/01/2018 To 03/31/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirnhle +n niternn+ive nerfnrmerl !(7ncc A nr Clace Rl rmmnlr+n +hP fnllnwina mnni+nrina Aa+a-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6eh
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221C
of total solids
CFU
510,000
519,919
540,000
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Mt. 3 Option/Mt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Mt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
DotrK-Shoudt Division Manager Wastewater
Prepa ame an Title (ty or print)
2-rZ�i 9
gnature f Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

4
y
`i- NC Certification No. 402 Case Narrative ,
1"1MIFull Service Analytical & NC Drinking Water Cert No. 37735 01/15/2018 C'
Environmental Solutions SC Certification No. 99012
���3�s�' LABORATORIES INC.
k'
Synagro
Adam Brigman
12701 Lancaster Hwy.
Pineville, NC 28134
Project: 2018 Production
Project No.: Mt. Holly
Lab Submittal Date: 01/11/2018
Prism Work Order: 8010142
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This report contains a total of 4 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Cara C. Rusmisell
Project Manager
Data Qualifiers Key Reference:
Reviewed By Cara C. Rusmisell
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 26224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 Of 1

®marm..:
Sample Receipt Summary
Full-SeMce
R
x I
Environmental Solutions
al Solutions
01/15/2018
Ft;
�� L460RATORIEg ING
((44
C
Prism Work Order: 8010142
r13
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Mt Holly 1 of 4
8010142-01
Solid
01/11/18
01/11/18
Mt Holly 1 of
8010142-02
Solid
01/11/18
01/11/18
Mt Holly 1 of 4
8010142-03
Solid
01/11/18
01/11/18
Mt Holly 1 of 4
8010142-04
Solid
01/11/18
01/11/18
Mt Holly 1 of 4
8010142-05
Solid
01/11/18
01/11/18
Mt Holly 1 of 4
8010142-06
Solid
01/11/18
01/11/18
Mt Holly 1 of 4
8010142-07
Solid
01/11/18
01/11/18
Samples were received in good condition at 4.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 10

f,�'Nfi r .
to
BORATORIES, INC.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Client Name: Synagr0
Sample Date/Time Collected:
Sample Date/Time Submitted:
Full -Service Analytical &
Environmental Solutions
449 Springbrook Rd.
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
Fax: [phone]
Project Name: City of Mt. Holly
1-11-18 07:15 Project ID: Mt. Holly 1 of 4
1-11-18 09:50 C®C Group: 8010142
�msmFecal
Sample
ID
Client
Sample ID
o m ormra In
Solids(cfu/g)
SM9222 D
Reporting
Limit
% Solids SM2540 G
Analysis Date/Time
8010142-01
Mt. Holly 1 of 4
510000 A
510000
1.96
1-11-18 11:17
8010142-02
Mt. Holly 1 of 4
520000 A
520000
1.93
1-11-18 11:17
8010142-03
Mt. Holly 1 of 4
540000 A
540000
1.85
1-11-18 1117
8010142-04
Mt. Holly 1 of 4
520000 A
520000
1.94
1-11-18 11:17
8010142-05
Mt. Holly 1 of
520000 A
520000
1.93
1-11-18 11:17
8010142-06
Mt. Holly 1 of
520000 A
520000
1.94
1-11-18 11:17
8010142-07
Mt. Holly 1 of
510000 A
510000
1.97
1-11-18 11:17
Geometric Mean Calculation: -
Prism Sample ID: 8010142 Geometric Mean: 519919 A cfu/g
Reporting Limit: 519919
Note: All results are reported on a dry -weight basis.
A: The result is less than the reporting limit. At the request of the client, the value reported equals the value of the reporting
limit. /
Data Reviewed By: Pr jict Manager: C. RUsmisell
Review Date: 1-15-18 Approval Date: 1-15-18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

CHAIN OF CUSTODY RECORD •
y ' Full -Service Analytical & y t rry
y'f Environmental Solutions PAGE ` OF QUOTE # TO ENSURE PROPER BIILL�L�9G: ^'r_ J
�0''• -'.`• YEG NO ,'•N/A
`✓ ,- ,.. rSamples INTACT upon arrival? :`, ;_ • � �-
LABORATORIES, INC.
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] Fax: [phone]
Client Company Name: _5 J/a,-r-c
Report To/Contact Name: r p /d elo
Re r; c,.W+ c 11
Reporting Address: 12, 701 -4n —crsA-14c.,,�:
�rnPtrille: APc � 1B)'3�i
Project fume: 64` - G"r 1 Kq-• H0/ f
Short Hold Analysts: ( (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL I II III IV)
provisions and/or OC Requirements
Invoice To: f�tgOf
r
Address:
Phone: Al Fax (Yes){N�):
Purchase Order No./Billing Reference
TO DE FILLED IN BY CLIENT/SABIiiPLING PERSONNEL
�—
Emali Address: ' t r c; ,n�a•� Syr . cc.,
r. Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF I/ Excel Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days El Rush
Work Must BePre-
Site Location Name: (t (y Ur /r ni
pproved
Samples received after 14:00 will be processed next business day.
SC OTHER
N/A
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
NO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
REMARKS
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
*TYPE
NO.
SIZE
TIVES///////
ID NO.
HOURS
SLUDGE)
SEE BELOW
IvWqa)( FvP1
i I l �
`� '
S L
I
vz
C)
Fea,
I
cyz
1; i
(
Z
=t'o r,1r�
rt
cry
d L
A Zr
I
u,��
G�
7 ,, 2 -
S
0_5
77
6
0�
7
07
Sampler's Signature /
Sampled By (Print Name) A r) i'FG Irt-i. Affiliation
Upon relinquishing, this Chain of Custody is your authorization
for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
.
Relinquished By: (Signature),
�'-
Received By: (Signature) Date Military/Hours Additional Comments
;SRe Arrrval� Ti n -
f
Relinquished By: (Signature)
Received By: (Signature) Date
- •Sf(e,Departure) I mnO:,.
Relinquished By: (Signature)
Received For Prism Laboratories By: D t
-
•. _
�•�4111cage ,
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. .rp `.,� R oll 1 �
tj
❑ Fed Ex ❑ UPS ❑ Hand -delivered ❑ Prism Field Service O Other
NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: R❑CRA: CERCLA LANDFILL OTHER:
❑NC❑SC El NC ®SC El NC ❑SC ❑NC ❑SC Ea NC ❑SC NC®SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC
*CONTAINI PE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Car = Volatile Organics Analysis (Zero Head Space)
IKIA.I_

Im
PA
PROM PT•ACCLI RATE -RELIABLE
LABORATORIES, INC
WWN%'.P:%RLABS.CUNI
REPORT OF ANALYSES
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: JAN 18
DATE: 02/22/18
SAMPLE NUMBER- 130324 SAMPLE ID- MT HOLLY 1 OF 4 SAMPLE MATRIX- SO
DATE SAMPLED- 01/11/18 TIME SAMPLED- 0715
DATE RECEIVED-- 01/11/18 SAMPLER- AB RECEIVED BY- DJ
TIME RECEIVED- 0910 DELIVERED BY- AB TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 01/11/18 1230 RE ATTACHED
LABORATORY DIRECTOR
P.U. Box 411483 • Charlotte, NC' 25241-1453
Phone: [phone] • Fax: [phone]i

PLLF;Z
PROM PT•ACCU RATE- RELIABLE
LABORATORIES, INC
WWW.PARLAS.S.COM
30 ®ay Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
• s MT HOLLY 1 OF 4
130324
• 01 /11118
o 02/09/18
Start: End:
TS O
0.1603
0.1505
TS%
1.53%
1.55%
VS ()
0.1294
0.1190
VS%
80.72%
79.07%
I N
0.00372
OUT
0.00342184
FSVR (Mass Balance)
8.01%
FSVR (Van Kleeck
9.77%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 * Charlotte, NC 28241-1483
Phone: [phone] Fax: [phone]'

PLIR
PROMPT'
ACCURATE- RELIABLER LA-BOATORIES, INC
W W W.PARLABS.COM
Collected
D.O.
Crucible
Tare Wt (g)
Sample(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Wt(g)
Furnace Temp "C
Date/Time In
Date/Time Out
Burned Wt(g)
TS%
VS%
30 ®ay Bench Scale Extended Aeration Teat
VAK option 3, rercent voiame aouas Keouction
SYNAGRO
MT HOLLY 1 OF 4
130324
01/11/18
02/09/18
As Received Day 0 Day 7 Day 14 Day 21 Day 28
01/11/18 01/12/18 01/19/18 01/26/18 02/02/18 02/09/18
5.98
6.14
6.31
7.01
7.08
X2
X6
X1
X24
X1
X2
25.0673
24.3094
20.5154
21.2200
20.5157
25.0680
35.9189
34.7867
38.6312
31.7722
33.0179
34.7766
105
106
105
106
106
105
01/11/18 12:50
01/12/18 15:45
01/19/18 16:00
01/26/18 16:15
02/02/18 15:40
02/09/18 11:00
01/12/18 11:00
01/15/18 09:00
01/22/18 08:50
01/29/18 09:30
02/05/18 10:00
02/12/18 08:45
25.2874
24.4697
20.7908
21.3814
20.7120
25.2185
550
550
550
550
550
01/15/18 14:40
01/22/18 13:00
01/29/18 14:00
02/05/18 16:00
02/12/18 11:50
01/15/18 15:15
01/22/18 14:25
01/29/18 15:15
02/05/18 17:20
02/12/18 13:10
24.3403
20.5705
21.2532
20.5566
25.0995
2.03%
1.53%
1.52%
1.53%
1.57%
1.55%
80.72%
79.99%
79.43%
79.16%
79.07%
y
0.003719812
x
0.000888271
TS ()
0.1603
VS (g)
1 0.1294
Volatile Fraction In: 1 0.52758
P.O. Box 411483 a Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]
0.003421841
x
0.000905781
TS ()
0.1505
VS g)
0.119
Volatile Fraction Out: 1 0.5 0013

aLASORAR CHAIN OF CUSTODY
TORrEs.INc. PAR Laboratories, Inc
Phone [phone]
www.pariabs.com Fax [phone]
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
r-,..,r— no—t—f of nnri Nnhval Racni ir—c
Company Name (billing)
Comments/ Special Instructions
Clarifier Effluent provided in the event that
SYNAGRO CENTRAL
Address
the sample needs to be reduced to below
12701 LANCASTER HWY
2% solids.
City, State 8 zip code
PINEVILLE NC 28134
Point of Contact 8 Telephone Number
ADAM BRIGMAN 704-650-4341
Sample
Taken By: SIGNATURE PRINTED NAME k1g17l rf. � k?
ARE SAMPLES FOR STATE or EPA REPORTING? YES t// NO
*Sample Type: DW WW GWMW HW Soil other r/
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
**Field Preserved: Yes V No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (Y/N):
Client Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date/Time
Collection
Date/Time
Analyses
Requested
30 - Dq y
n
Relinquished by' Date/Time Receive Mb t atei I Ime
Relinquished by: Date/Time Received by: Date/Time
' C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: WQ0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 04/01/2018 To 06/30/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahle to alternative nerformed (Class A nr Class Rl romnlete the following mnnitnrinu data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61h
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221C
of total solids
CFU
670,000
706,727
750,000
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Doug Shoudt Division Manager Wastewater
Prep ame and itle (typ or print)
2-�Z-rq
Signature of reparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

f'[P R, ISM
- N7 LA001WORIES WG
Synagro
Adam Brigman
12701 Lancaster Hwy.
Pineville, NC 28134
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cart No. 37735
Environmental Solutlons SC Certification No. 99012
Project: 2018 Production
Lab Submittal Date: 03/21/2018
Prism Work Order: 8030318
Case Narrative
03/23/2018
This data package contains the analytical results for the project Identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This report contains a total of 4 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Cara C. Rusmisell
Project Manager
Data Qualifiers Key Reference:
Reviewed By Cara C. Rusmisell
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

r :p\//�' Full-Sorvlce Analytical8
�''h'• IS
, V , I Environmental Solutions
'�-��-•'- �uli�n4mat b rr:c
Sample Receipt Summary
03/23/2018
Prism Work Order: 8030318
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Mt. Holly 2 of 4 -1
8030318-01
Solid
03/21/18
03/21/18
Mt. Holly 2 of 4 - 2
8030318-02
Solid
03/21/18
03/21/18
Mt. Holly 2 of 4 - 3
8030318-03
Solid
03/21/18
03/21/18
Mt. Holly 2 of 4 - 4
8030318-04
Solid
03/21/18
03/21/18
Mt. Holly 2 of 4 - 5
8030318-05
Solid
03/21/18
03/21/18
Mt. Holly 2 of 4 - 6
8030318-06
Solid
03/21/18
03/21/18
Mt. Holly 2 of 4 - 7
8030318-07
Solid
03/21/18
03/21/18
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

tiiLABORATORIES,.INC.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Client Name: Synagro
Sample Date/Time Collected:
Sample Date/Time Submitted:
Full -Service Analytical &
Environmental Solutions
449 Springbrook Rd.
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
Fax: [phone]
Project Name: Mount Holly
3-21-18 07:30 Project ID: Mount Holly 2 of 4
3-21-18 09:20 COC Group: 8030318
rism
Sample
ID
Client
Sample ID
Fecal Coliform in
Solids(cfu/g)
SM9222 D
Reporting
Limit
% Solids SM2540 G
Analysis Date/Time
8030318-01
Mt. Holly 2 of 4
730000 A
730000
1.37
3-21-18 10:27
8030318-02
Mt. Holly 2 of 4
710000 A
710000
1.40
3-21-18 10:27
8030318-03
Mt. Holly 2 of 4
690000 A
690000
1.44
3-21-18 10:27
8030318-04
Mt. Holly 2 of 4
700000 A
700000
1.43
3-21-18 10:27
8030318-05
Mt. Holly 2 of 4
670000 A
670000
1.49
3-21-18 10:27
8030318-06
Mt. Holly 2 of 4
750000 A
750000
1.34
3-21-1810:27
8030318-07
Mt. Holly 2 of 4
700000 A
700000
1.43
3-21-18 10:27
Geometric Mean Calculation:
Prism Sample ID: 8030318 Geometric Mean: 706727 A cfu/g
Reporting. Limit: 706727
Note: All results are reported on a dry -weight basis.
A: The result is less than the reporting limit. At the request of the client, the value reported equals the value of the reporting
limit.
I�
Data Reviewed By: . (I� Project Manager: C. Rusmisell
Review Date: 3-23-18 Approval Date: 3-23-18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

Full -Service Analytical & CHAIN OF CUSTODY RECORD
PiR
1ISM I Environmental Solutions PAGE OF(— QUOTE # TO ENSURE PROPER BILLING:
noonnrorties Inc /�f r-
449 Springbrook Road - Charlotte, NC 28217 Project Name: , ' L6�hl
Phone [phone] • Fax: [phone] Short Hold Analysis: a (No) UST Project: (Yes) (NO)
`Please ATTACH any prod ct specific reporting (QC LEVEL 1 11 111 IV)
Client Company Name: S ?nG 'r
Report To/Contact Name: _�'� ttfh provisions and/nnorhhQ��,,C--Requi�em,ents
�p��� Invoice To: Ar-ear
Reporting Address: � �� i1.L1 A;
Address:
Samples INTACT upon arrival?
Received ON WET ICE?
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS -INTACT?
VOLATILES reed WIOUT HEADSPACE?
PROPER CONTAINERS used?
TEMP: Therm ID:I&-Z- Observed:
�YENO NIA
°C 1 Corr:
Phone: Zul L ' /U S �f Fax (Yes),( o}/:s
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: n ?
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
q
Certification: NELAC DoD
FL NC
EDD Type. PDF_Excel Other
yp
"Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ Rush work Must Be
` Pre -Approved
Site Location Name:. C f k ? JM &%s.T /-zt7 ' � Samples received after 14:00 will be processed next business day.
SC OTHER
N/A
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
NO
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
/ ANALYSIS REQUESTED
✓ f
REMARKS
PRISM
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
/ID
//////
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
�1
NO.
tGfe�% zo t
3 1- l d
7; 30
a
Pf
I
b?
1 C�
>°c
r`
rV7
7.3 2
2
w
��►
�.
'
y
Ts.
7r 7
I
7:
6
I
'eS_
7'y2
I
,�
%:`'f
7
VJ
I
I
I
PRESS DOWN
I yN `-f
FI
Sampler's Signature
Sampled By (Print Name) 1 Affiliation
Upon relinquishing, t1�1h of Custody is your authorization
for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing e mProject Manager. There will be charges for any changes after analyses have been initialized.
Relinquis o By: (Signature) - o
Received By: (Signature) Date Military! ours Additional Comments:
{Site Arrival Time:
Relinquished By: (Signature)
Received By: (Signature) Date
Site Departure Time:
Relinquished By: (Signature)
Receive rPnsm Latmratodos Br, Dal ,} ��
v� /V 3—G - 7 iXJ
Field Tech Fee:
Mileage:
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED AT THE LABORATORY. /y�� n
❑ Fed Ex ❑ UPS ❑ Hand -delivered O Prism Field Service ❑ Other Qt/ i/Jq
DRINKNG SOLID CERCLA LANDILL
1❑
NC
•�
CI NC ❑ S01 ❑ NC El SC ElNOCU ❑ SCTER: ❑
NC SCATER: ❑ NC DASC'E I O ❑ SC ❑ NC ❑ SC I ❑ NCFCISC El NC ❑ SC
❑ El ❑
❑
't^t^i
'CONTAIN 'PE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cal A = Volatile Organics Analysis (Zero Head Space)

A&
P
PROM PT- A CC U RATE -RE LIABLE
LABORATORIES, INC
WWWPARLABS.COiNi
REPORT OF ANALYSES
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: MAR 18
DATE: 05/07/18
SAMPLE NUMBER- 131040 SAMPLE ID- MOUNT HOLLY SAMPLE MATRIX- SO
DATE SAMPLED- 03/21/18
DATE RECEIVED- 03/21/18 SAMPLER- AB RECEIVED BY- DJ
TIME RECEIVED- 0940 DELIVERED BY- AB TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 03/21/18 1330 RE ATTACHED
LABORATORY DIRECTOR
P.O. Box =411483 • Charlotte, NC 28241-1=483
Phonc: [phone] • Fax: [phone]

PA
CCIJRATE•RELIABLE
LABOR-ATORIES, INC
WWW. PARLABS. COM
30 ®ay Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
Start: End:
TS (g)
0.1466
0.1202
TS%
1.54%
1.53%
VS (g)
0.1235
0.0954
VS%
84.24%
79.37%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0129941
0.0121397
x Mass Fraction of Fixed Solids in Liquid Sludge
0.00243051
0.0031558
FSVR (Mass Balance)
6.59%
FSVR (Van Kleeck)
6.56%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box411483 • Charlotte, NC 28241-1483
Phone: [phone] Far: [phone]

PiIR
PRO h1PT• ACCURATE - RELIAS LE
LABORATORIES, INC
W W W.PARLABS.COM
30 Day Bench Scale Extended Aeration Test
VAR Ontinn 3 Percent Volatile Solids Reduction
CUENT'NAMEs I ' •
,SAMPLE. ID:
ISAMPLE'#:
.START DATE.
'END DATE:
As Received Day 0 Day 7 Day 14 Day 21 Day 28
Collected 03/21/18 03/21/18 03/28/18 04104/18 04/11118 04/18/18
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge W1
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample Wi
+ Tare Wt (g)
Dried Sludge Wt (g)
Fixed Solids Wt (g)
Furnace Temp °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
2.88
2.97
3.15
3.26
3.69
X6
X6
X11
X16
X2
X6
24.3069
24.3069
21.0369
23.1836
25.0626
24.3065
33.8112
33.8112
31.4934
33.6861
35.1581
32.1650
9.5043
9.5043
10.4565
10.5025
10.0955
7.8585
106
106
105
106
106
105
03/21/18 13:50
03/21/18 13:50
03/28/18
04/04/18
04/11/18
04/18/18
03/22/18 14:00
03/22/18 14:00
03/29/18
04/05/18
04/12/18
04/19/18
24.4535
24.4535
21.1937
23.3401
25.2150
24.4267
0.1466
0.1466
0.1568
.0.1565
0.1524
0.1202
0.0231
0.0248
0.0269
0.0288
0.0248
550
550
550
550
550
03/22/18 00:00
03/29/18
04/05/18
04/12/18
04/19/18
03/22/18 00:00
03/29/18
04/05/18
04/12/18
04/19/18
24.3300
21.0617
23.2105
25.0914
24.3313
0.1235
0.1320
0.1296
0.1236
0.0954
1.54%
1.54%
1.50%
1.49%
1.51 %
1.53%
84.24%
84.18%
82.81 %
81.10%
79.37%
yf Mass Fraction of Volatile Solids in Liquid (Feed)
Sludge at Start of Test
0.0129941
yb Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at End of Test
0.0121397
xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
at Start of Test
0.0024305
xb Mass Fraction of Fixed Solids in Liquid (Bottom)
Sludge at End of Test
0.0031558
TS (g)1
0.1466
TS ()
0.1202
VS (g)
1 0.1235
VS (g)
1 0.0954
Volatile Fraction In: 0.54701 Volatile Fraction Out: 0.51876
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: (704) W-8335
1 ,r

LLABORR CHAIN ®F CUSTODY
ATORIES.hvc. PAR Laboratories, Inc
Phone [phone]
www.par/abs.com Fax [phone]
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that ail information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North
Carolina Department of Environmental and Natural Resources,
Company Name (billing) Comments/ Special Instructions
SYNAGRO CENTRAL
Clarifier Effluent provided in the event that
Address the sample needs to be reduced to below
12701 LANCASTER HWY 2% solids.
City, State It zip code
PINEVILLE NC 28134
Point of Contact & Telephone Number
ADAM BRIGMAN 704-650-4 41
Sample ,Q,
Taken By: SIGNATURE PRINTED NAME / (F" &:�'-`W`7
ARE SAMPLES FOR STATE or EPA REPORTING? YES NO
'Sample Type: DW WW GWMW HW soil other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
Client Sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date/Time
Collection
DateTme
nalyses
Requested
��cunyuwncv may. aver rnie necery oy uate/ 1 lme
Relinquished bgy% Datemme Received by: / Date/Time I
' C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: WQ0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 07/01/2018 To 09/30/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 31C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlicahle to alternative nerformed (Class A or Class R) cmmnlete the fallowinu mnnitorinp data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6th
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221 C
of total solids
CFU
89,000
161,837
1,000,000
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Mt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Doug Shoudt Division Manager Wastewater
Pnrepareame "Titlepe or print)
Z-f2-1 e�
Signature (' Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mt. Holly Biosolids
Project Number: 50-1701
Lot Number:TF19052
Date Completed:06/27/2018
s
06/27/2018 1:52 PM
Approved and released by:
Project Manager: Lucas Odom
d
M
ACCREDITED
DOD ELAP
`geOflA'[0�—
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: TF19052
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Geometric Mean
161,837
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyiab.com,
Page 2 of 12

Client:Synagro Laboratory ID:TF19052-001
Description: MT HOLLY 3 OF 4 FECAL Matrix: Solid
Date Sampled:06/19/2018 0645 % Solids: 1.96 06/20/2018 1821
Date Received:06/1912018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9221 C E-2006 1 06/22/2018 2218 SA1 06/19/2018 2250
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform (Class B MPN)
SM 9221C E- 100000
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Daly Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
20 MPN/g 1
Page 3 of 12

Client:Synagro Laboratory ID:TF19052-002
Description: MT HOLLY 3 OF 4 FECAL Matrix: Solid
Date Sampled:06/19/2018 0645 % Solids: 1.93 06/20/2018 1821
Date Received:06/19/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9221C E-2006 1 06/22/2018 2218 SA1 06/19/2018 2250
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform (Class B MPN) SM 9221C E- 300000 20 MPN/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
ialy Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of f 2

Client:Synagro Laboratory ID:TF19052-003
Description: MT HOLLY 3 OF 4 FECAL Matrix: Solid
Date Sampled:06/19/2018 0645 % Solids: 2.25 06/20/2018 1821
Date Received:06/19/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9221 C E-2006 4450 06/22/2018 2218 SA1 06/19/2018 2250
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform (Class B MPN)
SM 9221C E-20 ND
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
:aly Environmental Services, Inc.
i Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
89000 MPN/g 1
Page 5 of 12

Client:Synagro Laboratory ID: TF1 9052-004
Description: MT HOLLY 3 OF 4 FECAL Matrix: Solid
Date Sampled:06/19/2018 0645 % Solids: 2.23 06/20/2018 1821
Date Received: 06119/2018
Inorganic non-metals
-Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9221 C E-2006 4500 06/22/2018 2218 SA1 06/19/2018 2250
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform (Class B MPN)
SM 9221C E-20 ND
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
90000 MPN/g 1
Page 6 of 12

Client:Synagro Laboratory ID:TF19052-005
Description: MT HOLLY 3 OF 4 FECAL Matrix: Solid
Date Sampled:06/19/2018 0645 % Solids: 1.88 06/20/2018 1821
Date Received: 0611912018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9221 C E-2006 1 06/22/2018 2218 SA1 06/19/2018 2250
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform (Class B MPN)
SM 9221C E- 1000000
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantilation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Daly Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
20 MPN/g 1
Page 7 of 12

Client:Synagro Laboratory ID: TF19052-006
Description: MT HOLLY 3 OF 4 FECAL Matrix: Solid
Date Sampled:06/19/2018 0645 % Solids: 1.82 06/20/2018 1821
Date Received:06/19/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9221 C E-2006 5400 06/22/2018 2218 SA1 06/19/2018 2250
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform (Class B MPN) SM 9221C E-20 ND 110000 MPN/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantilation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 12

Client:Synagro Laboratory ID: TF19052-007
Description: MT HOLLY 3 OF 4 FECAL Matrix: Solid
Date Sampled:06/19/2018 0645 % Solids: 1.97 06/20/2018 1821
Date Received:06119/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9221C E-2006 5400 06/22/2018 2218 SA1 06/19/2018 2250
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform (Class B MPN) SM 9221C E-20 ND 110000 MPN/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

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SHEALY ENVIRONMENTAL SERVICES, INC.
3h; r 17 Eak-kcnmenial 5ervi:*3, [no. Rqc i of
rJ: cu [ Nunel-w- UF710190-11 i I11R-; ,, D'aec: 4iv:•�ti l
Sample Receipt C'hec4�->.<st (S'R(j �r �
Client: XaL i )-_... Cooler Inspected by,'date_ L �.�'+�'
h•IeHrts of rccei Sl2sl OClieitt ❑ ITS 0FcdF-K !]Ottller.
-VWc—rcciistodv
❑ Yes
I FD\1
1, seals present on tht: cooler?
I7 Yes
I ❑ No I El NA
12, If custody seats were pi-esetd, ,vwv chi;� is tact and ut.broken?
rH Strip ID: _ Chlorine Strip 1D.-
Coca] cr II) r igir I temperature upon receipt ,•• Derived (Corrected) t: rnperaturc upon receipt: --
r �= —
I4 crhrxl: [TI'emperature airk ❑Against ]Bottles IR Cruri Ti3: M riot) Corroction F&tor. — °C
J+letlicd of caoJ antr t_` tii`et Ir ❑ Ia c Packs ❑ Dn� Ice ❑ Node
❑ Yc`
❑ No
`
_;. If teiriperat❑mr of any cooler exceeded 6.11T, %vas Projcct Manager N6titied?
PNI t�;as Notified by: phone ; entail I face -to -dice (circle urat).
❑ Yes
ID No
::
4. is the colnmeacial courier's pocking slip attached to t]lis form.? j
Yrs
EJ No
5. Were propea• custody prr)"dun:s (.Clinquisliedrieceive(1) Jolloned? i
A Yes
_I No
�
6. Were samp]c IDs listed on the COC`?
Yes
❑ No
V
7. Wem s�"plt: IDs listed on all sain- le cnntainca-s?
F. es
❑ No
S. W:s cullcetion date & time listed on the CDC?
as
❑ leer
9. Was e:arllcctim dr:tc & time listed on all sample containers"
Yr;s
❑ No
10. Did all cortainer label information (7D, date, tir.ie) �rt:c Mth the COC7
cs
❑ No
11. l& ere tests to be performed Iistcd an the CO'
Laf5r'cs
❑Teo
12. Did all samples arrivr in the proper containei5 ii)r mQh test andiar in'Ig d eaindition
(unbroken, lids nn, es,-.)? _
Yea
0 Na
13. Vti'as adequate sample vnh me available.'?
�— CCa
❑ No
14, Were all sarnples received within 14 the holding tierce or 48 hours, whichever corner first?
Yes
_ e n
I5. WerC any samples contains; migningeoxcm foirci,: olio) Samples Nei: listed on C+ C'?
❑ Yes
n No
16. )For 1'{}q and RSIs-1 5 samples_ vver�e bubbles prescnl>"pea-sine" (° "rig 6mrn in di an7 ACT) in
any of lho VOA .dals?
-re
Y cs
Ll No
1 NA
17. We all DRCIImetalsr'ntrtricnt sainples teceiver3 at sa pN of
❑ 'Yes
El -No
'A
18, Wt;re all cyanide samples received aL a pK > 121 and sulfide samples received at a pH = 97
J 'Yes
❑ No
p_<A
13, W= all applicable �iH_r TICNicyanidc,phenolr£r25 t;-� 0.5mg.1) satnptcs free, of residual
chlorine? '
Yes
Elr' No
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20. R'ere clieait retnrar•ks?reyue:;t5 (i.c, r--quesred dilutions,1k4SeNJSD designations, etc...)
wrrectly transcribed fi-on3 die CUC irrtt) a1v comment section in I.TVS? i i
❑ Yes
.' IjI41
121.
WQS the gLkUtc number used Taken from the oontaii)er label? i
ruple Preservation (Must be C❑mpl it-41 for any sample) incoriee(iy F•rc:scrvcd or with
arnple(s)
i ,ample rcm. iving with
line of pmsery 4ion —
wcn,'receitied incorrectly presuT-ecd rind
HNO3, IICI, NaQi1) using Siff Ai
adjusted accordin-ly
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were aecoi,--ed ,.vith TRC - UJ nig/J
sodium thiosulfate(Na,S,03) with Shealy ID:
5
Date:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
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Page 12 of 12

Im
PLL
PROMPT•ACCU RATE -RE LIABLE
LABORATORIES, INC
WWW.PARL ABS.COl
REPORT OF ANALYSES
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: JUN 18
DATE: 07/18/18
SAMPLE NUMBER- 131868 SAMPLE ID- MT. HOLLY 3RD EVENT SAMPLE MATRIX- SO
DATE SAMPLED- 06/05/18 TIME SAMPLED- 0600
DATE RECEIVED- 06/05/18 SAMPLER- AB RECEIVED BY- CT
TIME RECEIVED- 0650 DELIVERED BY- AB TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 06/05/18 1315 RE 5.48
LABORATORY DIRECTOR`-`—
P.O. Box =411483 • Charlotte. NC 252=41-1453
Phone: (70 4)5SS-S333 • 1-:ix: [phone]

Mh
PbkF;Z
PROMPT -ACCURATE -RE LIABLE
LABORATORIES, INC
WWW.PARLABS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
MOUNT HOLLY 3RD EVENT
131868
06/05118
07/03/18
Start: End:
TS )
0.1514
0.1413
TS%
1.44%
1.38%
VS
0.1234
0.1134
VS%
81.51 %
80.25%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0117171
0.0110737
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0026587
0.0027245
FSVR Mass Balance
5.55%
FSVR (Van Kleeck)
5.48%
FSVR Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]
• fi

PLIR
PROMPT.
ACCURATE• RELIABLER LABOATORIES, INC
W W W.PARLASS.COM
Collected
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge Wi
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample Wi
+ Tare Wt (g)
Dried Sludge Wt (g)
Fixed Solids Wt (g)
Furnace Temp °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
30 ®ay Bench Scale Extended Aeration Test
VAR nntinn 3 Parcant Vnlatile Solids Reduction
SYNAGRO
r
MOUNT HOLLY 3RD EVENT
iSTART,DATE:06106/18
131868
jwlsMlP
07/03/18
As Received Day 0 Day 7 Day 14 Day 21 Day 28
narnariR nafnrtiR nrmwiR nwiwiA 06/26/18 07/03/18
3.08
3.37
4.09
4.33
5.10
X17
X17
X16
X8
X17
X28
21.2169
21.2169
22.6938
24.7188
21.2182
21.0968
31.7485
31.7485
32.9089
34.6988
31.4018
31.3373
10.5316
10.5316
10.2151
9.9800
10.1836
10.2405
106
106
105
106
106
107
06/05/18 13:15
06/05/18 13:15
06/12/18 08:45
06/19/18 09:00
06/26/18 09:15
07/03/18 09:00
06/06/18 12:50
06/06/18 12:50
06/13/18 09:00
06/20/18 08:50
06/27/18 09:30
07/04/18 09:30
21.3683
21.3683
22.8348
24.8545
21.3557
21.2381
0.1514
0.1514
0.1410
0.1357
0.1375
0.1413
0.0280
0.0273
0.0263
0.0268
0.0279
550
550
550
550
550
06/06/18 14:00
06/13/18 11:50
06/20/18 13:40
06/27/18 15:00
107/05/18 08:45
06/06/18 15:15
06/13/18 12:10
06/20/18 14:50
06/27/18 16:00
07/05/18 09:05
21.2449
22.7211
24.7451
21.2450
21.1247
0.1234
0.1137
0.1094
0.1107
0.1134
1.44%
1.44%
1.38%
1.36%
1.35%
1.38%
81.51 %
80.64%
80.62%
80.51 %
80.25%
yf Mass Fraction of Volatile Solids in Liquid (Feed)
yb Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at Start of Test
0.01 17171
Sludge at End of Test
0.0110737
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
Xb Mass Fraction o1 Fixed Solids in Liquid (Bottom)
at Start of Test
0.0026587
Sludge at End of Test
0.0027245
TS )
0.1514
TS
0.1413
VS (g
0.1234
VS (g)
0.1134
Volatile Fraction In: 1 0.56 1 Volatile Fraction Out: 1 0.58152
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] Fax: [phone]

PAR
LABORATORIES, INC.
www.partabs.com
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
1�.....1:.... n.......i.......1 of 0n.4.nn.. --1 -4 kl. #... �I 0-
--
Company Name (baling)
Comments/ Special Instructions
Clarifier Effluent provided in the event that
SYNAGRO CENTRAL
Address
the sample needs to be reduced to below
12701 LANCASTER HWY
2% solids.
City, State Et:zip code
PINEVILLE NC 28134
Point of Contact E* Telephone Number
ADAM BRIGMAN 7047650-4341
Sample
Taken By:
SIGNATURE
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES V NO
'Sample Type: DW WW tl GWMW HW soil other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No nla
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
I(®tit Sample l 0
Sample Location /Number) -
Comp
Grab
Presery
Set Up: '
17aterrlme
Collection
Datemriie
Anajysbs,
equested `_ -
n rr ! f
/,��• 1 (�I11 �rCl ��%EJ
G b/
�'(7Q
�V CI�V1�
� o l2j %326f c'1
Relinquished, y:
Da err'me
5 �;3�
Receiv try:
Dater ime
-S- a6-0
Relin b .
at /Time
Received by:
Daterrime
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number:
WWTP Name: Mt Holly WWTP NPDES Number:
Monitoring Period: From 10/01/2018 To 12/31/2018
WQ0001863
NCO021156
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if annlicahle to alternative nerfnrmed (Class A or Class R) emmnlete the follnwina mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 61h
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221 C
of total solids
CFU
50,335
218,572
8,822,323
CFU/g
1
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Doua Shoudt Division Manaeer Wastewater
Preparer e and 'tle (typ 'br print)
k
ignature Q P parer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mt. Holly Biosolids
Project Number: 50-1701
Lot Number:T126040
Date Completed:10/02/2018
10/02/2018 4:12 PM
Approved and released by:
Project Manager: Lucas Odom
TNt A C C A ED IT ED
I�eORATO� oa—CD�_
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: T126040
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Geometric Mean
218,572
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

Client:Synagro Laboratory ID:T126040-001
Description: Mt. Holly 4 of 4 Fecal Matrix: Solid
Date Sampled:09/26/2018 0700 % Solids: 1.71 09/27/2018 2242
Date Received: 09126/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 09/27/2018 2033 SA1 09/26/2018 1940
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 8822323 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
aaly Environmental Services, Inc.
i Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

Client:Synagro Laboratory ID:TI26040-002
Description: Mt. Holly 4 of 4 Fecal Matrix: Solid
Date Sampled:09/26/2018 0700 % Solids: 1.99 09/27/2018 0312
Date Received: 09126/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 09/27/2018 2033 SA1 09/26/2018 1940
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <50335 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
ialy Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Synagro Laboratory ID:TI26040-003
Description: Mt. Holly 4 of 4 Fecal Matrix: Solid
Date Sampled:09/2612018 0700 % Solids: 1.71 09/27/2018 0312
Date Received:09/26/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 09/27/2018 2033 SA1 09/26/2018 1940
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 175583 * 20 col/g 1
Footnote(s): * SM 9222D-2006 (MF) 24 hr 503 NC - Fecal Coliform (MF): result is considered estimated
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
ialy Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Synagro Laboratory ID:T126040-004
Description: Mt. Holly 4 of 4 Fecal Matrix: Solid
Date Sampled:09/26/2018 0700 % Solids: 0.634 09/27/2018 2242
Date Received:09/26/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 09/27/2018 2033 SA1 09/26/2018 1940
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 157729 * 20 col/g 1
Footnote(s): * SM 9222D-2006 (MF) 24 hr 503 NC - Fecal Coliform (MF): result is considered estimated
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holdina time W = Reoorted on wet weight basis
.aly Environmental Services, Inc.
i Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Synagro Laboratory ID:T126040-005
Description: Mt. Holly 4 of 4 Fecal Matrix: Solid
Date Sampled:09/26/2018 0700 % Solids: 0.924 09/27/2018 2242
Date Received:09/26/2018
Inorganic non-metals
"Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 09/27/2018 2033 SA1 09/26/2018 1940
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <108225 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 12

Client:Synagro Laboratory ID:T126040-006
Description: Mt. Holly 4 of 4 Fecal Matrix: Solid
Date Sampled:09/26/2018 0700 % Solids: 0.939 09/27/2018 2242
Date Received:09/26/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 09/27/2018 2033 SA1 09/26/2018 1940
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <106485 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
.aly Environmental Services, Inc.
i Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 12

Client:Synagro Laboratory ID:T126040-007
Description: Mt. Holly 4 of 4 Fecal Matrix: Solid
Date Sampled:09/26/2018 0700 % Solids: 1.19 09127/2018 0312
Date Received:09/26/2018
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 09/27/2018 2033 SA1 09/26/2018 1940
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 168152 * 20 col/g 1
Footnote(s): * SM 9222D-2006 (MF) 24 hr 503 NC - Fecal Coliform (MF): result is considered estimated
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
mly Environmental Services, Inc.
I Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

�c)
CD
os
m
m M
ro <
- EnviroJ7merii:af Servtcp,s,
t Cl301r1 of CustodV fiecorrf10E3 `/Qrtage Poirt Drive
o d l�rest Ca urnsaie, Sou-,h Csr�ifna 20972
CD < m T�tlei pane Nn. (3!3j 79-1.97,10 F_x ha. {BC;s; 791-Ji I
* R. Iab.cant
E eporr Eo'. ontecl
CD m `}'It metro Sampler { rfed PJ11htj
ridalr. A ratan Ir',darr rlipm-,r,
o p Addltts 5 -ttl°phone No, i Fa.Y No. i F.Ci6J�
1270; L-acnforMVy waybill No.
3 ;-70tip tti1r 1) :2b nrnr_nt'Tjsynaprc,CA,II
Cliy Sfata Zip ^ode PfLSeIVatIVR
ca Pinevillu h1C 73t 1, U=r a. 4. FAQs 7. NoOF
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srAad �.°5h � i m 8 ec [JhJGrnHa= rcl ` FlwrnmrthL;
�� e p `Yr ❑ I atom to i:I Cnf �' Q15r b?I.1k' Lab Julc;. Irri :nt
5linnrule,k;I bft'esnjrp%r (�C°loan I ttrkncs�'rn
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Date T rnr, r �, kece?/oi b• nu; l f G
ar•_11slt�Abq rt* irUl_r J /lfi:!3� _ ��1 �.1n�
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SHEALY ENVIRONMENTAL SERVICES, INC.
Shay I3JJVi1Q11U)UJILJI SCraLMS, Inc Page 1 rr I
Uacpm, w Numbun IErm-c Zi Sllml.-yu D ::, 9?1f3i18
Sample Receipt Checklist (,SRC)
Client: gt•jM'aA.-ro. __— Cu,lcrJnspcetedby.(}ate:J-IILl , _d.,-j J.ot0;77_r,)((_,gb
deans crCleceipl: SESI Gj Client L-t UPS I] FedRv f] Othei
C Yes
No
1. 5; lei e Custody s '118 presrmt on the cooler'?
Yes
❑ No
NA
2. IT clistudy ssals wctz preserlt, were they intact mid unbroken?
'pl-i Sttip 113: Ctrheriru: Strip TD; _..... Te:,wd by:^
Ori+inal temperature upon rcccipt? D;:rivcd (Corrected) umperawre upnn rectipl: %Solid Snap -Cup ID!
�4ethad:. Trmprrrrrturc. Inn:; ❑.gams: Bottles IR C'rurt ID: � IR Oin Correction Factor: n- °C
',4erhod of coolant: ZJ We-t Ice ❑ kv Pucks ❑ Dl • lcc ❑ done
❑
S. If li;mperawre of tiny cooler exceeded 60''C, was Project Nluougcr Notified?
PNJ was Notified by: phone:.+ email .+ ftiee-to-face (61vie (wo),
LI Yes
❑ No
VNA
4. Is the commercial courier's packing slip attached to this fora,?
V.)cs
❑ Nn
s- %I/em proper custody pr°c-4CIU S (re]inyui�hrrb'rcx civcd) folloi�'cd'?
ff Ycs
❑ t%,o
6, We= .-ample Ills listed on the COC?
Y,5s
❑ NO
7. WeJ)e sample lUs listed on all sample, c..olltalllus ?
Il Yesf
G No
S. Was coll"fion date & time listed on the C OC T
I -vcs
Cr No
9. Was collect,on date & timc listed un all sample containers?
Yes
I� No
16. Did all container label hifoinnadon (Ii7r date, time) anpree with the COC2
j Yes
No
11. 'r>lrLrd lL$Is In be performed listed on The COC?
tr 3'e5
L Nu
l2' Did all samplestrr-i ve in the prnpce ccrnn,incr for caell test :tntL'4C ing oo d candition
(Iln 7roken, fads oil, 00.)?
t YL•;
J No
13, Wes udzc1tlatc sample volume available?
Yes
I] No
14. Were all sarnllles T=viv::d 'milhin Vi tha holding time. or 48 hours, whichever conies first?
❑ Yes
15. Were uny =triples conwiners missingfexcess (circle orie) samples Not listed on COC?
I }':s
❑ <Jo
P�lrl
16. For VOA and RSK-175 swnples, were bubbles pre-sent=�"pc�I-size°` (W'or 6mm in diameter) in
any of [he VOA ,pia ]s?
71 Yes
Nu
N
17. Wem , it DROAnc_lalsrnutrient sAlllPles received at a P1I of <: 2?
Yes
❑ No
l�1NA
IS. Weree all cvaalde samples rr�.ivtd w n pH ­ 12 and sulfide samples received at,, pH > 9?
❑ Yes
f_-9 Na
�NA
19. IXere a a licable NTAyril-MIc hnidol hmol,'625 (-. 4.5ing'Li s"i io' frvu of res]dual
Pl' }'P P
r;hlorine?
Yes
ida
'L NA
2 0. Were client ren,arkstrcglresm (i.e. reVested diluticum M3,citi4SD dcsiLma ions, etc..,)
correctly irwscribed from the COC uito the comment seLdUn in UNIS?
U Yes
No
21. Was the quote number listed on the Lnnudner lobi]? tf }yes, Quote;
Sample Prescrvation (.Must
be completed tar may sarnple(s) incorrc;:tly preserved 4r w-th headspace.)
Sample(,) ____were rece7a•ed incorrectly prescrved and wem; adju%Md acr:ordin xly
in sample receiving With in of circle one: H2SO4, 14NO.;, NCI, Nn014 u:;ing SR 0
Time of presermi]on _.- If More the r ant' preserva[iti c is nr~cdc•l, plwase riots in The curry rents helativ.
Samples) were r&,eiyed with bubbles >6 niLit In di: peter.
s
.E; Ples,$) _. wcm received with TRC> 0.5 m&'L (Iftt19 is no) and were
adjusted accordingly in sample r=Uiving with sodium thiosnloate (Na2S,01 ) with Slrealp lla:
SR Lai -rode laheN applied by, _ �-.� � - — Dale:
Comments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

pil
PROM PT•ACCU RATE -RE LIABLE
LABORATORIES, INC
WWNV.PARLABS.00M1I
REPORT OF ANALYSES
A t, 1, n : ADAM BRI GMAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: SEP 18
DATE: 11/28/18
SAMPLE NUMBER- 133504 SA14PLE 7D- MT. HOLLY SAMPLE MATRIX- SO
DATE SAMPLED- 09/26/18
DATE RECEIVED- 09/26/18 SAMPLEI:- AB RECEIVED BY- DJ
TIME RECEIVED- 1255 DELIVERED THY- AB TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 09/26/18 1445 RE 2.54 %
LI>50RATORY DIRECTOR ' ` - - r_:: �•�•--�
P.O. Box 411483 ^ Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]

PbLF;Z
PROMPT- ACCURATE• RELIA9LE
LA�BOR.ATORIES' INC
WWW. PARLABS. COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
CLIENT'NAME: -___--
'SAMPLE ID: ' •
'SAMPLE#:
,START DATE: '
END DATE_ _
Start: End:
TS ()
0.1569
0.1531
TS%
1.54%
1.54%
VS (g)
0.1243
0.1184
VS%
79.22%
77.34%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0122365
0.0119238
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0032093
0.0034946
FSVR Mass Balance)
2.56%
FSVR Van Kleeck)
2.54%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: (704) SSS-8333 • Pax: [phone]

PiIR
PRO MPT•ACCU RATE RELIABLE
LABORATORIES, INC
WWW.PARLABS.COM
Collected
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge WI
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample Wi
+ Tare Wt (g)
Dried Sludge Wt (g)
Fixed Solids Wt (g)
Furnace Temp °C
DatelTime In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
30 ®ay Bench Scale Extended Aeration Test
VAR C)ntinn 3 Percent Volatile Solids Reduction
;CLIENT NAME: ' •
SAMPLE IDs _ •
'SAMPLE # T J
START DATE-
ENA DATE ��
As Received Day 0 Day 7 Day 14 Day 21 Day 28
ng/2a/1R ng12s/18 10/03/18 10/10/18 10117/18 10/24/18
4.06
5.18
5.55
6.07
6.13
X16
X16
X25
18
X31
X28
22.6936
22.6936
21.4460
23.0238
22.0992
21.0970
32.8517
32.8517
31.5266
33.1753
32.0940
31.0267
10.1581
10.1581
10.0806
10.1515
9.9948
9.9297
107
107
105
106
105
106
09/26/18 14:45
09/26/18 14:45
10/03/18 09:15
10/10/18 08:50
10/17/18 09:50
10/24/18 10:40
09/27/18 13:50
09/27118 13:50
10/04/18 09:00
10/11/18 08:45
10/18/18 10:00
10/25/18 11:00
22.8505
22.8505
21.5975
23.1744
22.2500
21.2501
0.1569
0.1569
0.1515
0.1506
0.1508
0.1531
0.0326
0.0318
0.0320
0.0324
0.0347
550
550
550
550
550
09/27/ 18 16:00
10/04/18 12:10
10/11 /18 11:20
10/18/18 13:15
10/25/18 15:00
771
09/27/18 17:05
10/04/18 13:15
10/11 /18 13:00
10/18/18 14:20
10/25/18 16:15
22.7262
21.4778
23.0558
22.1316
21.1317
0.1243
0.1197
0.1185
0.1184
0.1184
1.54%
1.54%
1.50%
1 1.48%
1.51 %
1.54%
79.22%
79.01 %
78.75%
78.51 %
77.34%
yf Mass Fraction of Volatile Solids in Liquid (Feed)
yb Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at Start of Test
0.0122365
Sludge at End of Test
0.0119238
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
Xb Mass Fraction of Fixed Solids in Liquid (Bottom)
at Start of Test
0.0032093
Sludge at End of Test
0.0034946
TS (9)1
0.1569
TS ()
0.1531
VS ()
0.1243
VS (g)
0.1184
Volatile Fraction In: 1 0.51442
P.O. Box 411483 • Charlotte, NC28241.1483
Phone: [phone] • Fax; [phone]
a z
Volatile Fraction Out: 1 0.50221

PAIR
CHAIN OF CUSTODY
LABORATORIES. INC.
PAR Laboratories, Inc
Phone [phone]
www.partabs.com
Fax (704)•588.8335
Shipping:
Mailing:
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28273
Charlotte, NC 28241-1483
It is essential that all information be recorded on Nis
Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North
Carolina Department of Environmental and Natural Resources
Company Name (billing)
Comments/ Special Instructions
SYNAGRO CENTRAL
Clarifier Effluent provided in the event that
Address
the sample needs to be reduced to below
2% solids.
12701 LANCASTER HWY
City, State & zip code
PINEVILLE NC 28134
Point of Contact ti Telephone Number
ADAM BRIGMAN 704-650-4341
Sample �j�;
Taken By: SIGNATURE 7 )c PRINTED NAME 14 Ct1!'CC�C)177 `
ARE SAMPLES FOR STATEfor EPA REPORTING? YES NO
"Sample Type: DW Ww GWMW HW soil other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: o C
"Field Preserved: Yes /No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
Bent sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date/Time
Collection
Daterrime
nalyses
equested
/b'l`l. Noll 30 -�r�h
,/
r�ennqursneo uy�� �/ water r rmi
e.
Relinquished
Date/Time
meceivea o}r
Received by:
uarer I Ime _
Date/Time
' C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

SECTION 6

Agricultural Lime Application Log
Year: 2018
Project: Mount Holly 50-1701
Field
Grower
Soil
Lime Require
Tons/Acre
Date
Total
(state -county -site -field)
�H
from soil anal sis
A lied
A lied
Acres
NC-CL-12-01
RiverTaw
5.7
0.7 Ton/Acre
NC-GA-41-01
Greg S rin
F 5.9
0.5 Ton/Acre
1.0
®
3.4
NC-GA-41-06
Greg Springs
6.9
0 Ton/Acre 10.0
0
8.9
NC-GA-41-10 11
Greg S rin s
6.7
0 Ton/Acre I0.0
0
7.9
NC-GA-41-14 11
Greg S rin s
6.8
0 Ton/Acre I0.0
0
6.8
NC-GA-45-01
David Allen
6.2
0 Ton/Acre
0.0
0
17.0
NC-LT-44-01 11
Lee Shank
6.2
0 Ton/Acre
0.0
15.7
NC-LT-46-01 11
Tony Jones
6.5
0 Ton/Acre 10.0
0
11.8
NC-LT-46-02 11
Tony Jones
6.2
0 Ton/Acre
0.0
45.2
NC-LT-46-03 11
Tony Jones
5.7
0.5 Ton/Acre
NC-LT-46-04 11
Tony Jones
6.2
0 Ton/Acre 10.0
19.4
NC-LT-46-05
Tony Jones
5.4
1.3 Ton/Acre
NC-LT-46-07
Tony Jones
=J
1.0 Ton/Acre
1.5
®
7.0
NC-LT-46-08 11
Tony Jones
6.3
0 Ton/Acre
# lime has been ordered but not spread

SECTION 7

NCDA&CS comic Division Phone: [phone] Website: www.nca...,-,v/agronomi/
Report No. F _ __ 3L037057
Yaco2 Predictive Client:
Synagro
Advisor:
�4PG¢��u�ruae
e
12701 Lancaster Hwy
S F
Soil Report Mehlich-3 Extraction
Pineville, NC 28134
M
Sampled County :Cleveland
t� ��,• Links to Helpful Information Sampled: Not Provided
Received: 06/12/2018
Farm: NC-CL-12 Completed: 06/18/2018
Client ID: 449334
Advisor ID:
Sample ID: 12-01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P205
K20 Mg S
Mn Zn Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.7 120-200 70
30 0 0
0 0 0 0
Note: 12
2-
Test Results [units - WN in g/cnr ; CEC and�la•in m\eq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH 1 P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.46 1.06 6.7 71 2.0 5.7 r 30 57 46 21
30 98 76
47 47 44 0.1 1
1
_North Carolina
.;;.2
1'17 t3l
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS r,u -comic Division Phone: [phone] Website: www.ncL-..„,)v/aaronomi/
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at o
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full ra
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
neagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/acrronomi/obpart4.hLn-7 fsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizes
Test Results
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/aaronomi/uvrst.htm
Report No. F _ _ _ 5L037057
Page 2 of 2
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
WN
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

Page 1 of 1
Report No: 18-072-8665
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
WaypointCW
ANALYTICAL
Client: David Allen
NC-GA-44
City of Mount Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone] ..
www.waypointanalytical.com
Farm: NC-GA-45
Date Received: 03/13/2018
Date of Report: 02/08/2019
Lab No Field /D Sample ID
Soil Class HM% W1.V pH
Ae
P-1
K-1
S-I
Mn-1
Zn-1
Zn-Al
Cu-1
CEC
BS% Ca% Mg% ESP Na SS-1 NO3 N
24369 45-01
MIN 6.2
0.9
6
16
37
2000
- 70
70
100
714
88 63 21 2.3 0.2
Crop Recommendations:
Rec Uom Lime (t/acre)
N
W P2O5
K2
S
Mn
Mn-A/
Zn
Cu
B
Mg Last Crop
1- Fescue. Hay
lb/acre , 0:0
150
131
109
20
0
1214.
0
0
0
0
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis

Page 1 of 1
Report No: 18-072-9664
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypoint.
ANALYTICAL
Client: Greg Springs
NC-GA-41
City of Mount Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-GA-41
Date Received: 03/13/2018
Date of Report: 12/31/2018
Lab No Field ID
Sample ID
Soil Class HM% W/V pH
Ac
P-1
K-1
S-1
Mn-/
Zn-1
Zn-Al
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
24365
41-01
MIN
5.9
1.7
113
117
31
138
475
475
210
10.0
83
57
18
1.2 0.1
Crop Recommendations:
1- Fescue Hay
_
Rec Uom
Ib/acre
Lime (f/acre)
0.5
N
150
P205
0
K20
0
S
20
Mn
0
Mn-Al
101
Zn'
0
Cu
0
B-
0
- Mg
0
Last Crop
24366
41-06
MIN
6.9
0.1
87
17
40
81
380
380
330
9.7
99
71
26
1.6 0.2
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
150
P205
0
K20
107
S
20
Mn
0
Mn-Al
52
Zn
0
Cu
0
B
0
Mg
0
Last Crop
24367
41-10
MIN
6.7
0.5
75
18
40
156
395
395
320
10.1
96
67
26
1.6 0.2
- -- — - - - --- -
Crop Recommendations:
1- Fescue Hay
-
_ Rec Uom
lb/acre
Lime (t(acre)
0.0
N
150
P205
0
K20
104
S-
20
Mn
0
Mn-AI
100
Zn
0
Cu
0
B
0
Mg
0
—
-
--
Last Crop
24368
41-14
MIN
6.8
0.3
70
18
33
156
383
383
305
10.2
97
71
25
1.2 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (t/acre)
0.0
N
150
P205
0
K20
104
S
20
Mn
0
Mn-Al
98
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 18-354-0572
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypoint.0 a
ANALYTICAL
Client: Lee Shank
Mt Holly
Synagro
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm:
Date Received:12/20/2018
Date of Report: 12/31/2018
ab No Field ID
Sample ID
Soil Class
HM% WN
pH
Ac
P-1
K-1
S-1
Mn-I
Zn-I
Zn-Al
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na
SS-1 NO3 N
?9761
LT-44-01
MIN
6.2
0.7
44
65
29
119
65
65
115
5.7
87
63
17
1.9
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 18-073-9915
Account.No: 00015
Advisor: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville NC 28134
Waypoint.
ANALYTICAL
Client: Toney Jones
NC-LT-46
Mt Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-LT-46
Date Received: 03/14/2018
Date of Report: 12/31/2018
Lab No Field ID
Sample ID
Soil Class HM% W/V pH
Ac
P-1
K I
S-1
Mn-/
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
25764
46-01
MIN
6.5
0.4
15
15
50
231
55
55
200
5.5
93
75
14
2.5 0.1
_______ _.___ _
Crop Recommendations:
1- Fescue Hay
____
Rec Uom
lb/acre
Lime (t/acre)
0.0
_ _
N
150
_
PZ 05
105
KZ D
Ill
____
S
20
_
Mn
0
Mn AI
148
Zn
0
Cu
0
B
0
Mg
0
—
----- ---- ---
Last Crop
25765
46-03
MIN
5.7
0.9
4
14
100
581
35
35
100
4.3
80
55
21
2.8 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (t/acre)
0.5
N
150
P205
137
K2
114
S
20
Mn
0
Mn-AI
370
Zn
0
Cu
0
B
0
Mg
0
Last Crop
25766
46-08
MIN
6.3
0.6
37
12
29
150
93
93
205
5.3
90
72
14
2.1 0.1
Crop Recommendations:
1- Fescue Hay
-
Rec Uom
Ib/acre
Lime (t/ecre)
0.0
N _^PZOs
150
51
K20
119
S
20
Mn
0
Mn-AI
102
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 18-354-0576
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypointal-
ANALYTICAL
Client: Tony Jones
Mt Holly
Synagro
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-LT-46
Date Received: 12/20/2018
Date of Report: 12/31/2018
Lab No Field ID
Sample ID
Soil Class HM%
W/V pH
Ac
P-I
K-1
S-1
Mn-1
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO3 N
09767
LT-46-05
MIN
5.4
2.5
26
130
166
69
200
200
255
8.9
72
44
20
1.2
0.1
09768
LT-46-07
MIN
5.5
2.3
38
149
73
113
203
203
345
8.9
74
45
19
1.4
0.1
09769
LT-46-02
MIN
6.2
0.5
21
16
35
463
68
68
155
3.8
88
62
22
2.3
0.1
09770
LT-46-04
MIN
6.2
0.5
21
15
27
506
68
68
160
3.9
86
60
22
2.2
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

435 Williams Court, Suite 100
Baltimore, MD 21220 SYNAr-nRO
www.synagro.com
REeEivebmc
FEBRUARY 20, 2020
WQROS
MOORESVILLE REGIONAL OFFICE
NCDEQ
Division of Water Resources(�1C��C�
Information Processing Unit `\iI rC�lr�C�
1617 Mail Service Center p`c� 2.o
Raleigh, NC 27699-1617 F�8 e
Re: 2019 Annual Report for Permit No. WQ0001863
Dear NCDEQ:
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Mount Holly, NC.
If you have any questions or need additional information, please do not hesitate to contact
Danny Jackson at [phone] or Adam Brigman at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Danny Jackson, City of Mount Holly
Adam Brigman, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

City of Mount Holly, NC
RESIDUALS LAN® APPLICATION PROGRAM
Permit No. WQ0001863
2019 ANNUAL REPORT

City of Mount Holly, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WO0001863 County Gaston Year 2019
Facility Name (as shown on permit) Mount Holly WWTP & WTP NPDES No. NC0021156 & 01-36-020
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 16
Total number of fields utilized for land application during the year: I 1
Total amount of dry tons applied during the year for all application sites: 328.82
Total number of acres utilized for land application during the year: 191.30
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and be 'ef, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including th possi lity of fines and imprisonment for
knowing violations." � /j
Danny Jackson, City Manager / \& „VVV / .4 t ,1—Z '.V t
Permittee__Name and Title (type or print) Signa e e Data
'Si re o eparer Date Signa of Land Appli Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
MOUNT HOLLY, NC
MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
DRY METRIC
MONTHNEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
February 2019
235,600.00
G
15.72
D
14.25
March 2019
489,800.00
G
32.67
D
29.64
April 2019
967,200.00
G
55.64
D
50.48
June 2019
539,400.00
G
31.03
D
28.15
July 2019
241,800.00
G
25.91
D
23.51
September 2019
731,600.00
G
78.42
D
71.14
November 2019
1,165,600.00
G
89.43
D
81.11
YEARLY TOTAL
4,371,000.00
G
328.82
D
298.28
1/30/2020

SECTION 2

V
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001863
Facility Name: MOUNT HOLLY, NC
NPDES# : NCO021156
or WQ# (residual only)
WWTP Name: MOUNT HOLLY WWTP
Residuals Analysis Data
Product Type
Date Sampled (grab) or
Date Composited
Percent Solids
AEDLIQ AEDLIQ
01/03/19 04/30/19
PARAMETERS (mg/kg dry weight)
Laboratory
PACE ANALYTICAL SERVICE INC.
SHEALY ENVIRONMENTAL SERVICES INC.
AEDLIQ AEDLIQ
07/10/19 10/09/19
1.60 1.38 2.57
Arsenic
<30
<4.4
<9.6
Cadmium
<3
1.1
<2.4
Mercury
<0.31
<1.3
<0.72
Chromium
255
150
140
Copper
540
440
370
Lead
<15
11
<8.6
Molybdenum
<15
<8.8
<19
Nickel
18.5
14
<20
Selenium
<30
<7.2
<16
Zinc
731
780
670
Total Phosphorus
12200
24000
13000
TKN
59100
82000
46000
Ammonia -Nitrogen
8090
7500
11000
Nitrate and Nitrite
<121
<19n
39ti
-5-3 ,
1.84
<5.3
<1.1
<1
250
660
15
<9
22
<8.2
1200
15000
77000
9700
110 t37D
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
DENR FORM RSSF (5/2003)
Date

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001863
Facility Name: MOUNT HOLLY, NC
NPDES# : NCO021156
or WQ# (residual only)
WWTP Name: MOUNT HOLLY WWTP
Residuals Analysis Data
Laboratory
PACE ANALYTICAL SERVICE INC.
SHEALY ENVIRONMENTAL SERVICES INC.
Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ
Date Sampled (grab) or 01/03/19 04/30/19 07/10/19 10/09/19
Date Composited
Percent Solids 1.60 1.38 2.57 1.84
PARAMETERS (mg/kg dry weight)
Aluminum
14500
20000
15000
20000
Calcium-
11400
10000
9000
14000
Magnesium
3070
3700
2600
3300
pH
7.30
7.20
7.50
7.50
Potassium
<15000
4800
3300
2700
Sodium
<15000
8300
5400
8500
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system -
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIG
OF PREPARER)
NR - Data Not Reported or Data Not Required
Date
DENR FORM RSSF-B (7/2002) Printed: Saturday - February 1, 2020 at 13:56:30 for: 1701 01

(�IaneAnalyfical"
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5
January 22, 2019
Adam Brigman
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
RE: Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DearAdam Brigman:
Enclosed are the analytical results for sample(s) received by the laboratory on January 03, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Revised Report. The sample was redigested and reanalyzed for metals.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
64 -
Lord Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
PICCRF��
s�
`9e ,RAZO�J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

(�71acieAnalytical"
wmpacelabs.com
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
Lab ID Sample ID
92412758001 MT. HOLLY 1OF4 N+M
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 601OD
SH1
14
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
MFO
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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lacmnalyticalo
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
Sample: MT. HOLLY 10F4 N+M
Lab ID: 92412758001 Collected:
01/03/19
08:30
Received: 01/03/19
12:56 Matrix: Solid
Results reported on a "dry weight'
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Aluminum
14500 mg/kg
300
1
01/17/19 08:28
01/18/19 11:19
7429-90-5 M1
Arsenic
ND mg/kg
30.0
1
01/17/19 08:28
01/18/19 11:19
7440-38-2
Cadmium
ND mg/kg
3.0
1
01/17/19 08:28
01/18/19 11:19
7440-43-9
Calcium
11400 mg/kg
300
1
01/17/19 08:28
01/18/19 11:19
7440-70-2
Chromium
255 mg/kg
15.0
1
01/17/19 08:28
01/18/19 11:19
7440-47-3
Copper
540 mg/kg
15.0
1
01/17/19 08:28
01/18/19 11:19
7440-50-8
Lead
ND mg/kg
15.0
1
01/17/19 08:28
01/18/19 11:19
7439-92-1
Magnesium
3070 mg/kg
300
1
01/17/19 08:28
01/18/19 11:19
7439-95-4
Molybdenum
ND mg/kg
15.0
1
01/17/19 08:28
01/18/19 11:19
7439-98-7
Nickel
18.5 mg/kg
15.0
1
01/17/19 08:28
01/18/19 11:19
7440-02-0
Potassium
ND mg/kg
15000
1
01/17/19 08:28
01/18/19 11:19
7440-09-7
Selenium
ND mg/kg
30.0
1
01/17/19 08:28
01/18/19 11:19
7782-49-2
Sodium
ND mg/kg
15000
1
01/17/19 08:28
01/18/19 11:19
7440-23-5
Zinc
731 mg/kg
30.0
1
01/17/19 08:28
01/18/19 11:19
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
lercury
ND mg/kg
0.31
1
01/04/1919:56
01/07/1911:02
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
1.6 % 0.000010
1
01/03/19 17:14
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.4 %
0.10
1
01/03/19 17:05
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
7.3 Std. Units
0.10
1
01/07/19 15:09
H3
Plant Available Nitrogen
Analytical Method: SM 271 OB-2011
PlantAvailable Nitrogen
19300 mg/kg
0.12
1
01/08/19 11:27
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation
Method:
EPA 350.1 Rev 2.0
1993 Mod.
Nitrogen, Ammonia
8090 mg/kg
518
1
01/05/19 09:48
01/05/19 13:14
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
59100 mg/kg
1970
1
01/07/19 11:53
01/08/19 01:30
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0
1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND mg/kg
121
1
01/04/19 00:02
01/04/19 02:46
Nitrogen, Nitrate
ND mg/kg
121
1
01/04/19 00:02
01/04/19 02:46
14797-55-8
Nitrogen, Nitrite
ND mg/kg
60.3
1
01/04/19 00:02
01/04/19 02:46
14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0
1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Dl,,)sphorus
12200 mg/kg
470
5
01/04/19 18:56
01/05/19 04:32
7723-14-0
REPORT OF LABORATORY ANALYSIS
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Date: 01 /22/2019 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 16

5aceAnalytical"
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QUALITY CONTROL DATA
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
QC Batch: 450852 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Associated Lab Samples: 92412758001
METHOD BLANK: 2466307 Matrix: Solid
Associated Lab Samples: 92412758001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 01/07/1910:16
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2466308
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.068 82 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2466309 2466310
MS MSD
92412774001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
.Aercury mg/kg ND 0.053 0.053 0.021 0.016 40 30 75-125 27 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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(�5a'cmnalydca(
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QUALITY CONTROL DATA
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
QC Batch: 452988 Analysis Method: EPA6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92412758001
METHOD BLANK: 2475518
Associated Lab Samples: 92412758001
Parameter
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Aluminum
mg/kg
ND
10.0
01/18/1911:12
Arsenic
mg/kg
ND
1.0
01118/1911:12
Cadmium
mg/kg
ND
0.10
01/18/1911:12
Calcium
mg/kg
ND
10.0
01/18/1911:12
Chromium
mg/kg
ND
0.50
01/18/1911:12
Copper
mg/kg
ND
0.50
01/18/1911:12
Lead
mg/kg
ND
0.50
01/18/1911:12
Magnesium
mg/kg
ND
10.0
01/18/1911:12
Molybdenum
mg/kg
ND
0.50
01/18/1911:12
Nickel
mg/kg
ND
0.50
01/18/1911:12
Potassium
mg/kg
ND
500
01/18/1911:12
Selenium
mg/kg
ND
1.0
01/18/1911:12
Sodium
mg/kg
ND
500
01/18/1911:12
inc
mg/kg
ND
1.0
01/18/1911:12
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2475519
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mg/kg
500
489
98
80-120
Arsenic
mg/kg
50
42.9
86
80-120
Cadmium
mg/kg
50
45.6
91
80-120
Calcium
mg/kg
500
486
97
80-120
Chromium
mg/kg
50
48.5
97
80-120
Copper
mg/kg
50
48.6
97
80-120
Lead
mg/kg
50
44.7
89
80-120
Magnesium
mg/kg
500
457
91
80-120
Molybdenum
mg/kg
50
49.2
98
80-120
Nickel
mg/kg
50
46.5
93
80-120
Potassium
mg/kg
500
ND
96
80-120
Selenium
mg/kg
50
41.2
82
80-120
Sodium
mg/kg
500
478J
96
80-120
Zinc
mg/kg
50
43.6
87
80-120
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2475520 2475521
MS MSD
92412758001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Aluminum mg/kg 14500 14500 15300 35700 36200 145 142 75-125 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 01 /22/2019 03:06 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 16

5aceAnalyfical
(�www.pacelabs.com
QUALITY CONTROL DATA
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2475520
MS
92412758001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2475521
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
1450
1530
1240
1310
85
85
75-125
5
Cadmium
mg/kg
ND
1450
1530
1330
1400
91
91
75-125
5
Calcium
mg/kg
11400
14500
15300
26000
26600
100
100
75-125
2
Chromium
mg/kg
255
1450
1530
1670
1740
97
97
75-125
4
Copper
mg/kg
540,
1450
1530
2000
2090
101
101
75-125
4
Lead
mg/kg
ND
1450
1530
1310
1370
89
89
75-125
5
Magnesium
mg/kg
3070
14500
15300
16700
17300
93
93
75-125
4
Molybdenum
mg/kg
ND
1450
1530
1430
1510
98
98
75-125
5
Nickel
mg/kg
18.5
1450
1530
1370
1430
93
93
75-125
5
Potassium
mg/kg
ND
14500
15300
18100
18700
99
98
75-125
4
Selenium
mg/kg
ND
1450
1530
1180
1240
80
81
75-125
5
Sodium
mg/kg
ND
14500
15300
22300
22800
97
96
75-125
2
Zinc
mg/kg
731
1450
1530
2000
2100
87
89
75-125
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /22/2019 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16

(�5a'cmnalytkalo
www.pacelabs.com
QUALITY CONTROL DATA
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
QC Batch: 450688 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92412758001
SAMPLE DUPLICATE: 2465713
92412623001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 24.5 24.7 1
SAMPLE DUPLICATE: 2465714
92412474001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 80.4 80.4 0
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /22/2019 03:06 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 16

aceAnalytical
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QUALITY CONTROL DATA
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
QC Batch: 450994 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92412758001
SAMPLE DUPLICATE: 2466932
92412757001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.8 5.8 1 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /22/2019 03:06 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 16

IeAnalytical
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QUALITY CONTROL DATA
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
QC Batch: 450952 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92412758001
METHOD BLANK: 2466776
Associated Lab Samples: 92412758001
Parameter Units
Nitrogen, Ammonia mg/kg
LABORATORY CONTROL SAMPLE: 2466777
Parameter Units
Nitrogen, Ammonia mg/kg
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 01/05/1913:00
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 503 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2466778 2466779
MS MSD
92412682001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec .Limits RPD Qual
litrogen, Ammonia mg/kg 2720 1840 1840 4440 4510 93 97 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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lacmnalydcalo
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Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
QC Batch: 451040
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92412758001
METHOD BLANK: 2467104
Associated Lab Samples: 92412758001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 01/08/19 01:17
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2467105
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 926 93 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2467106 2467107
MS MSD
92409974001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. . Conc. Result Result % Rec % Rec Limits RPD Qua]
litrogen, Kjeldahl, Total mg/kg 241 768 848 942 983 91 88 90-110 4 H1,M1
Results presented on this page are in the units indicated by the "Units" column except where an aItem ate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
QC Batch: 450721
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92412758001
METHOD BLANK: 2465789
Associated Lab Samples: 92412758001
Parameter
Units
Nitrogen, Nitrate
mg/kg
Nitrogen, Nitrite
mg/kg
Nitrogen, NO2 plus NO3
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 01/04/19 02:33
ND 0.99 01/04/19 02:33
ND 2.0 01/04/19 02:33
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2465790
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.6
14.6 100 90-110
Nitrogen, Nitrite
mg/kg
9.7
9.7 100 90-110
Nitrogen, NO2 plus NO3
mg/kg
24.4
24.3 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2465791
2465792
MS
MSD
92412476001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
123
27.1
27.3
272
283
175
213
90-110
4 M1
Nitrogen, Nitrite
mg/kg
15.8
18.1
18.3
58.1
54.7
162
141
90-110
6 M6
Nitrogen, NO2 plus NO3
mg/kg
138
45.3
45.6
330
338
169
184
90-110
2 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
QC Batch: 450867
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92412758001
METHOD BLANK: 2466387
Associated Lab Samples: 92412758001
Parameter Units
Phosphorus mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.9 01/05/19 03:36
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2466388
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 48.1 44.5 93 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2466389 2466390
MS MSD
92412682001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
'hosphorus mg/kg 13000 205 205 12800 12400 -77 -289 90-110 3 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
laneMalXicalo Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: City of Mt.Holly 50-1701 1/3
Pace Project No.: 92412758
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG —Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accred itatio ns/ce rtifi cations is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/22/2019 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 16

leAnalytical o
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
City of Mt.Holly 50-1701 1/3
92412758
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92412758001
MT. HOLLY 10174 N+M
EPA 3050E
452988
EPA 601 OD
453121
92412758001
MT. HOLLY 1OF4 N+M
EPA 7471 B
450852
EPA 7471 B
450907
92412758001
MT. HOLLY 1OF4 N+M
SM 2540G-2011
450819
92412758001
MT. HOLLY 1OF4 N+M
ASTM D2974-87
450688
92412758001
MT. HOLLY 10174 N+M
EPA 9045D
450994
92412758001
MT. HOLLY 1OF4 N+M
SM 2710E-2011
451237
92412768001
MT. HOLLY 1OF4 N+M
EPA 350.1 Rev 2.0 1993
450952
EPA 350.1 Rev 2.0 1993
450956
Mod.
Mod.
92412758001
MT. HOLLY 1OF4 N+M
EPA 351.2 Rev 2.0 1993
451040
EPA 351.2 Rev 2.0 1993
451164
92412758001
MT. HOLLY 10174 N+M
EPA 353.2 Rev 2.0 1993
450721
EPA 353.2 Rev 2.0 1993
450728
92412758001
MT. HOLLY 1OF4 N+M
EPA 365.1 Rev 2.0 1993
450867
EPA 365.1 Rev 2.0 1993
450908
Date: 01/22/2019 03:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 16

CHAIN -OF -CUSTODY
Analytical Request Document
Analj4icalo
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relavent fields
92412755
Company: SYNAGRO
Billing Information; Mary Brewer: 284 Boger rd, Macksville
NC27028
Address: 12701 Lancaster HW, Pineville NC, 28134
ContalnerPreserva
ReportTo: Adam Brigman ([e-mail])
EmaIlTo: [e-mail]
I.. A L....
11 Preservative Types: (1) nitric acid, (2) sulfuric add, (3) hydrochloric add, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) socilum bisulfate, (8) sodium thlosultate, (9) hixane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (0) TSP, (U) UnpreservEd, (a) Other
Copy To: Lysa Finnerty ([e-mail])
Site Collection Info/Address:
Analyses
n J.-
Customer Project Narhe/Numbe
State: county/City: Time 7cne Collected:
1701
6A 1 /VC )PT I ]MT [ ]CT ]ET
�i "A CUIVe X=: ilqnbLt�u7x p3apsen. Wit
Phone.'704-650-4341
Site/Facility ID 4:
Compliance Monitoring?
Email:[e-mail]
IX Yes No NC I Sc
Y.
N: Ilk"
N
.R
Collected By (print): Adam Brigman
Purchase Order #:
DW PWS 10 9:
Quote H:
DW Location Code:
V
-
Co II aturI.'rum
­dDate Re ulmd:
Immedlatel Packed cnIce :
4
7— VAYJ
ix ]Yes I IN.
N
sample [RS06hK.'_
Rush:
Field Filtered (if applicable):
JX] Dlspose as appropriate I Retum
Same Day Next Day
Yes ]No
Z
(n
]Archive:
2 Day 3 Day [ ]4Day [ ]SDay
Z
a)
—6
I ]Hold:
(Expedite Charges Apply)
Analysis:
J—
Z
C/5
CU.
Matrix Codes (insert in Matrix box below): Drinking Water [DW), Ground Water (GM, Wastewater (WW),
Product (P), Soil/Solid (SQ, Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (VI, Other (OT)
:_P
CT
0
Matrix •
Comp/
Grab
Collected (or
Composite Start)
Composite End
Res
Cl
R of
Ctns
Customer Sample ID
Date
Time
Date
Time
:D
(D
IV+M
SL
A16
X
X
X
X
Customer Remarks I Special Conditions)
. /V oz"9h ca", I i—n k
by/Company:
Hazards: 'N.6lne
Radchem )icrqiin O.-N50 Y
IReceive ICOMPW (Sign e) 1/s/N hx% 1. 2
JDate/nme: ' lReciilved by/Company: (Signature)
Relinquished by/Company: (Signature) IDate/nme: I I Received by/Company: (Signature)
T�_' R I
Date/nme:
Date/Tlme:
able
X N.
esiBUal -h-1
-P
. . .........
r A`BStrn0Ii1Xempdraiurd.1nfo:-..
e Y v
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ecdhf6&`.Y, NX
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.:JPage
of.
Page 16 f 16

Sodium Absorption Ratio Calculation (SAR)
all
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 1/3/2019 1/1/2019-3/31/2019 4.0697
DIGESTED LIQUID
Na mg/1= (Na mg/kg x % Solids) _ 100 = (15000 x 1.6000) _ 100 = 240
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (11400 x 1.6000) _ 100 = 182.4
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3070 x 1.6000) _ 100 = 49.12
Na meq = Na mg/I _ Molec.Wgt.Na = 240 + 23 = 10.4348
Ca meq = Ca mg/I + Molec.Wgt.Ca = 182.4 = 20 = 9.12
Mg meq = Mg mg/I + Molec.Wgt.Mg = 49.12 + 12 = 4.09333
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 10.4348 _ SgrRoot[0.5(9.12+4.09333)] = 4.05968
Page 1
Printed: 2/1 /2020
13:57

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mt. Holly
Project Number: 50-1701
Lot Number:UD30072
Date Completed:05/10/2019
05/10/2019 3:40 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
R�
pCCAWAB
19e0RA1��,
A C CA C fl
oo—�—
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UD30072
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported.on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure: UD30072-001,due to low % solids the initial amount of these samples were 4 times the
standard procedure. The LOQ has been adjusted accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 7

Client:Synagro
Description: Mt. Holly 2 of 4 N&M
Date Sampled:04/30/2019 0730
Date Received:04/30/2019
Laboratory ID:UD30072-0
Matrix: Solid
% Solids: 1.38 05/f
j
Inorganic
i
non-metals
un Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
2
(% Solids) SM 2540G
1
05/02/2019 0027
KFE
15395
1 350.1
(Ammonia - N ) 350.1
5
05/01/2019 1419
DMA
15286
1
(Nitrate - N) 9056A
1
05/06/2019 2243
HKL
15882
2
(Nitrite - N) 9056A
1
05/08/2019 0924
HKL
16168
1
(pH) 9045D
1
05/02/2019 2251
HET
15537
1
(Phosphorus) 365.1
10
05/02/2019 1013
DMA
05/01/2019 1217 15297
1 351.4
(TKN) 351.2
1
05/02/2019 1151
DMA
05/01/2019 1721 15334
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
1.38
%
2
Ammonia - N (gas diffusion)
350.1
7500,
360
190
mg/kg
1
Nitrate - N (soluble)
9056A
30
(11,500
14
1.8
mg/kg
1
Nitrite - N (soluble)
9056A
14
1.4
mg/kg
2
pH @ 21.7 ° C
9045D
7.2
su
1
Phosphorus
7723-14-0 365.1
24000
3600
720
mg/kg
1
TKN
351.2
82000
1800
1800
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 05/02/2019 1701 JMH
05/02/2019 1353
15424
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
^^ercury
7439-97-6 7471E
ND
5.5
1.3
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 05/09/20191316 JCF
05/06/2019 1057
15558
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 601OD
20000
350
130
mg/kg
1
Arsenic
7440-38-2 6010D
ND
13
4.4
mg/kg
1
Cadmium
7440-43-9 6010D
1.1 J
4.4
1.1
mg/kg
1
Calcium
7440-70-2 6010D
10000
4400
550
mg/kg
1
Chromium
7440-47-3 601OD
150
8.8
2.2
mg/kg
1
Copper
7440-50-8 601OD
440
8.8
4.0
mg/kg
1
Iron
7439-89-6 6010D
9600
88
40
mg/kg
1
Lead
7439-92-1 6010D
11
8.8
4.0
mg/kg
1
Magnesium
7439-95-4 6010D
3700 J
4400
550
mg/kg
1
Manganese
7439-96-5 6010D
170
13
5.2
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
35
8.8
mg/kg
1
Nickel
7440-02-0 6010D
14 J
35
9.3
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Dut of holding time W = Reported on wet weight basis
My Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 7

Client:Synagro Laboratory ID:UD30072-001
Description: Mt. Holly 2 of 4 N&M Matrix: Solid
Date Sampled:04/30/2019 0730 % Solids: 1.38 05/02/2019 0027
Date Received:04/30/2019
ICP-AES
Jun Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD 1 05/09/20191316 JCF
05/06/2019 1057
15558
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
4800
4400
550
mg/kg
1
Selenium
7782-49-2 601OD
ND
18
7.2
mg/kg
1
Sodium
7440-23-5 6010D
8300
4400
550
mg/kg
1
Zinc
7440-66-6 6010D
780
44
11
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
(j=\Out of holding time W = Reported on wet weight basis
1 —,aaly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 7

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SHEALY ENVIRONMENTAL SERVICES, INC.
Sim- Envimnsncutal sm vires, roc
Fkull cm NL-n6;- Mit1}71 SC-14 Paz* I or i
'4RMPle RCCCII7t 1[':heck1l iist (SRi_irecr:tic¢l�ce:5;�118
Client: 5pliagro
- cooler ras ecterl h JHtc: M62 it,1GJ] }Ltt 9: UM0071
--�
N tvns of receipt: ® SFtiI j] Client jl UJ'S-
❑ Vcs
0 NR
?. �;i4'1'C custad}' :v 8Js')rrscnt on the Cooley? —
Yes
Nu
11r12. IfcusrorlV seals were resent, weae lhcv int: ct and ienbrokcn?
pH Strip
TT?: NA
Chlorine Ntl-jp ID; NA Tested by, NA
Driginal
remNrattu'e upon rc%xipt /Derived (Corrected) Golttrierniure uliou receipt °�,,5r�]id Snag. Cup 1D.- 19-611
3.6 13.f rC
NA ,'NA '-C NA ,INA oC NA ,1iA ::t. —
111cthod;
�Ternperature- Bltink []Against BoUlus JR C�tln Ib: _3 I12 Gun C or€ectinn Facwr_ 0 °
[w1, thnd oc)laat: 0 W'ct Ice. Q Jce P;mk-s ❑ Dry Ice
Yes
❑ No
® 1A 3. If tcinperaturc of any cooler excccdcd (j.f?"(;, was Project manaro Noti fed?
- PINT was Nkitifacd by_ Phone.," email l face-to-flx-z (circI a onc).
Q Ycs
-
QNo
ON.A 4. Is the rOrnmercial courier's packing slip attached to Ehis fc. 1?
I� 'rk,
M ltiu
ere proper cusuidy proccdurm (rolingrnWwdireanived) fatlowc:V
Yesa
No
6. W'ere sumplc IDs. listed ore Lho COC9
® Yess
Q N-0
7. Wi,.re sample. lD.i lis#cd on tll sample c--antairlera7
Yes
Q No
S. Was orrlreetion daLu & time listed oil ths. (:Or?
Yes
El Nu
9. Was collection date& titre lis#cd On all salirPl[ 4antatnels7
i Yr:s
Q N(l
ifi- Did all container lrlbe•1 ir,$rmat+on (10, date, l[me) agree witlt ncc C:(1C?
® Y
Q Nn
] I . 'dNcre l rs tri be pc-Tl!bmled liaced on the CC)C?
0
12. Did all samples alrivc In t11e proper e4intniners fbr cacti test and/or in goad condition
(unbroken, lids on, ctc.),? _
Yes
C1 No
13. bras adeg(eate sample volume amailablc7
I� Yes
Q NO
ZNo
14- Were. all sampi:-4 reaeiVed vrjthin °6 t[ze lialiring tinge ur 18 hnlres, whichcv:r eomes f;rsC`,
Q Yes
] 5. let'(.re anV .."—Iles conOliuers missfn&Y'excess (circle onc) samples, Nni listed on (,,()(_?
F-1 Yes,
QNu
ZqA ,16. For V0.1 and RSK-175 sainitles, were bubbles present -"pca-size"r)r l$ITLn1 It diatTleter)
3n an}' Of the V0 A vials?
0 Ye$
No
NA 17. Were all DTZ0.-'rnctHJs,: iutrieLr:t sarnplcs reccivcd :K a pH or-: 27
Q tires
0 No
NA t R. Were all cymliAQ sa1Ti l:s receivr d at a aE) ? 12 and sulf'jdc sain lCs received a> a 9?
Y r
❑ No
pH .-
O NA 19_ W'cle all applicaolc tN11V'TK.Nicyani chew, G25 - 6.3mn+7.) sael0r?lr s tl'ee of residual
El
Yes Q Nsi ®lar4 20. e,'ere client rernarjc5ij';tlLt-;sts (l.c. requestcd •:1rPutians, NT&-MSD dcsig,Iations, etc...)
camolly transcribed from the CoC inm the corl1mcnt seal on in LIMS 7
El Yes No: 2 ]. 14"a5the aa6L nutttbcr listosi nn 111e contaialcr lahal? If yes, C)utite r NA
Sample Freservolion (Must be completed for any sar>Itple(s) inco- rrcct� Iv preserved or with hcadspacc:,)
Sariple(s)yi ,vera received inoo:rc�r1}• preserved and .vPre a�jusied ac:cordin�r}• in samplc ret ivi11g with `try uiL of circle or1c; H2SC74, HNO3,1.1C1, N-101-1 usuie, SR 9 NA
Tien: of pre;vmti(iri NA If More than One prescrvative is riumled_ plewc ino(c in the 4omment$ faelot�'.
Swuplr(s) NA r5ceivcd wilh bubbles >6 mitt in digrnelor.
SarnRlcs(s) NA _ were lviceiVed with TRC: ? 0.5 m� C -gr , {
1Fr19 isrrv) and were
acliustrd ac trrc[ingiy' in plc rC i:ing wilt sadiarn IhioSu. l HtC (Na,S 0,z) with Mealy JD: NA
SR barcocde lnbeLs applied, tiv: ETD Date. 4130119
C=LTLen Ls:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 4/30/2019 4/1/2019-6/30/2019 2.1087
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (8300 x 1.3800) = 100 = 114.54
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (10000 x 1.3800) = 100 = 138
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3700 x 1.3800) _ 100 = 51.06
Na meq = Na mg/I = Molec.Wgt.Na = 114.54 _ 23 = 4.98
Ca meq = Ca mg/I + Molec.Wgt.Ca = 138 = 20 = 6.9
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 51.06 — 12 = 4.255
SAR = Na meq -= SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.98 _ SgrRoot[0.5(6.9+4.255)] = 2.10867
Printed: 2/1/2020
Page 1 13:57

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mt. Holly
Project Number: 50-1701
Lot Number:UG10025
Date Completed:07/25/2019
07/25/2019 3:48 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
�a
A
ACCREDITED
9eORPf� oa�—
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UG10025
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 7

Client:Synagro
Description: Mt Holly 3 of 4 N&M
Date Sampled:07/10/2019 0815
Date Received:07110/2019
Laboratory ID:U
Matrix: S,
% Solids: 2
Inorganic
non-metals
un Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Solids) SM 2540G
1
07/11/2019 0054 KFE
22171
1 350.1
(Ammonia - N ) 350.1
10
07/15/2019 1322 DMA
22538
1
(Nitrate - N ) 9056A
1
07/18/2019 1615 SLU
23173
2
(Nitrite - N ) 9056A
1
07/25/2019 0618 GMH
23699
1
(pH) 9045D
1
07/14/2019 1519 HET
22490
1
(Phosphorus) 365.1
10
07/11/2019 1830 DMA
07/09/2019 1315 21965
1 351.4
(TKN) 351.2
1
07/18/2019 1446 DMA
07/16/2019 1821 22774
Parameter
CAS Analytical
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
2.57
%
1
Ammonia - N (gas diffusion)
350.1
11000,
390
200
mg/kg
1
Nitrate - N (soluble)
9056A
� '3
7.8
0.95
mg/kg
1
Nitrite - N (soluble)
9056A
f 14,
7.8
0.75
mg/kg
2
pH @ 21.7 ° C
9045D
�7:5
su
1
Phosphorus
7723-14-0 365.1
13000
1900
390
mg/kg
1
TKN
351.2
46000
970
970
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 07/16/2019 1218 TJW
07/15/2019 1835 22366
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Uercury
7439-97-6 7471E
ND
3.0
0.72
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 07/11/2019 2310 KSH2
07/11/2019 1220 22233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 601OD
15000
770
290
mg/kg
1
Arsenic
7440-38-2 6010D
ND
29
9.6
mg/kg
1
Cadmium
7440-43-9 6010D
ND
9.6
2.4
mg/kg
1
Calcium
7440-70-2 6010D
9000 J
9600
1200
mg/kg
1
Chromium
7440-47-3 6010D
140
19
4.8
mg/kg
1
Copper
7440-50-8 6010D
370
19
8.6
mg/kg
1
Iron
7439-89-6 6010D
8100
190
87
mg/kg
1
Lead
7439-92-1 601OD
ND
19
8.6
mg/kg
1
Magnesium
7439-95-4 6010D
2600 J
9600
1200
mg/kg
1
Manganese
7439-96-5 6010D
160
29
11
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
77
19
mg/kg
1
Nickel
7440-02-0 6010D
ND
77
20
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
Out of holding time
W = Reported on wet weight basis
!aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 7

Client:Synagro Laboratory I D: UG1 0025-001
Description: Mt Holly 3 of 4 N&M Matrix: Solid
Date Sampled:07/10/2019 0815 % Solids: 2.57 07/11/2019 0054
Date Received:07/10/2019
ICP-AES
un Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD 1 07/11/2019 2310 KSH2
07/11/2019 1220
22233
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 6010D
3300 J
9600
1200
mg/kg
1
Selenium
7782-49-2 6010D
ND
38
16
mg/kg
1
Sodium
7440-23-5 6010D
5400 J
9600
1200
mg/kg
1
Zinc
7440-66-6 6010D
670
96
24
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Dut of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheaiylab.com
Page 4 of 7

Chain I Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 7

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SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy t n irccrolenla9 S� ices_ foe. ; Pub I ai I
L�cu:nai;Nainbcr.hlL�ri7BC-I� 7•:I140?e bI ie: 812.+2gis
Sample Receipt ChUldist (SRC)
ClieriL SLr r. r'
� -- _ C:c�alc�r [n� eotad by. dale• 0'rn ; 711tJ.+'l9 Lat Y: UG 10035
mcons ofrccci t: iEsl
d C1[cnt ❑ UPS ®FedEx C7cdicr:
yes rj 'Jo 1. Wem custody seal-, present on 11j4 uodcf?
I A If cus[od • coals -were lomsunt, were the intacr and unhroke n?
pI-I Strip ID: NA i lllarinc Strip 10; NA- _ Tessin b _
Urigicta[ tcniperature upon rr..ceipt J Dtor]vcd (ColreCt2d) tolliperatum upon tvceipt. %Soli;1 Snap -Cur ID: 11-1070 1
3.7 i3.7 -C NA ,Nk "C NA ,+i\A °C NA iNA cC
A6clttod: ®'Cetriperllttu•e Blank E1A9ailtst 1'otdes IR Our] ID.- (I IR (3un Correction Factor: 0 1C:.
A4etliod orcooln t: 0 -14et Ice ❑ 0� ' ke 0 Nona i
r Q' Icyl i"ac[cs
'do O NA ' l.f tcmpea�tuln_ of any confer exceeded 5.0°C, was Projuct;vlw)apr Nlot[fierl?
FE] Yr, El !
P141 8•� '
N'o
.S NUtlllf*d by. p,:atle, urnnll } f'rIOC-CU-face (Ci'Cle:0118).
NA 4- Tv tale commercial couriers packing sl[pat:Rcil.ed to lhia forts?
Q]' Yes
_ (] Nn
S. Were pro}a�r auslnriy' pra:.edasres (rululquishcd•�i•ceAived) fullotiectl°
® Yes
❑ No
G. Wcra sample ]D3s listed ou. ON COC?
7. Were sample IDs listcd on all sam le aantasincrs?
ffYesE
8- +,t'as collection date &. tittle [aAcd on the COC'?
9. Was coltectiorr daa,Q &time listcd on all sartiple c6nluirtcrs?
10. Did all comalacr IaLel info,ranatioa5 ID dote time) ) agree with (he CO4'.
0 Yes
E No
I I _ M--rc mso; to bo performed listed on, do COC?
IZI Yes
ha
12. D[ri ;,ill samples arrive iu the proper cortluincts for each test alldlor in good rmlitioil
j
(unbroken, lids ott, etc)?
'I cs
❑ No
13. `may adequate Sample volume flat [lable?
ye�,
T'o
I4. Vs'e1-c all sanlpies received wi[hin Y: the holding time or 4-9 hours, whichever comes first
Yea
ho
] 5. V" era any sans iCy coniaine± tttissit>g1e,' uss (circle tint.) sans les Not fisted on coc?
El Yes
® ND
13 NA 16. For V4 A and RSK-1?$ Kinples, were bubbles prasenl > `lac, -size" ('1'°or 61nin in dianu
�jn
any of lite. VOA vials'
❑ YeN
Na
VJ NA 17. DR0 ,'mctals/n utri=I: slant;[es rcceiv ed at a pH of < 2?
1'cs
❑ 1sPa
GZI ]sPA ! S. 'eta all cyaoidc sErutp[cs rece[tiOd at a pF[ � 1? and Sull'idc sans .les received at a pH r 9
❑ Yars
® No
Z NA 19.1Ta'ero a 1 applicab e Nllz,"[ IGI�I/t +aniderla euolit �5 (< 0.5M tB) same?L!,q rr7c- of residual
Chlorine?
Ycs
®-No
[, j NA �0. )Were client »anuks,-'reque;;l.-1 (i.C. mquestcd diluliuns, MS/NTSD dkigrlations, etc...)
Carree dy trau-wrtbed froin did COC. 111to IElr; goTrjment 5CGI i011 I[t ] I rIS'?
EEI Yee
- a
�i. 'a4'aS the quote number listed un the Cianitaincr Inbel? If yes, Chime: 4 NTA
;am PIE! Preservation ([Must be cotrlplcted for any satnplefs'r incorrectly preserved car with ltaadspace.)
,amplc(s) NA _wrm received incorrectly preset ved Hid ware adjusted Eamordh
1 Sample teeei4•inewillt NA m.Lofcircle rant:: IP2S0�I, HwCl3, Ht�l, �laC3T[ ca33rg Sty Nil
imc ofltre5crvaiinrt NA , If1ttrra: lh,-n one pta3C1Na1ive is needed, please note in the comrjIonts below,
Satnplc(s) NA %were recuJvcd wirh bubbles--6 ram in diameter.
Shn1UlPS(S) NA
vvere received with "l Kc > 0.5 ing L (If A'l9 is Ito and V,•ere
ldjusted agcordingly in sarlaplz racciving �vitla sodiurn lbiostllt'a[e ( a;!520j) with Sbcnly ID, KA
SR bar-code labels atomic+ by: MIN Dare: 7il0119 —
CcsmrtbznJ s; -
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 7/10/2019 711/2019-9/30/2019 2.0615
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (5400 x 2.5700) + 100 = 138.78
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (9000 x 2.5700) _ 100 = 231.3
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2600 x 2.5700) + 100 = 66.82
Na meq = Na mg/I _ Molec.Wgt.Na = 138.78 _ 23 = 6.03391
Ca meq = Ca mg/I = Molec.Wgt.Ca = 231.3 + 20 = 11.565
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 66.82 = 12 = 5.56833
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.03391 _ SgrRoot[0.5(11.565+5.56833)] = 2.06155
Printed: 2/1 /2020
Page 1 13:57

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mt. Holly
Project Number: 50-1701
Lot Number:UJ09103
Date Completed:10/22/2019
w
10/23/2019 1:32 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
PCCRFO���G
2"SQ
ARAB
N
ACCREDITED
`AeORAiO�DDDELAP
—
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UJ09103
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure: UJ09103-001. Due to low % solids, the initial amount of these samples were 3 times the
standard procedure amount. The LOQ has been adjusted accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 7

I
Client:Synagro
t
Laboratory ID:Ii
Description: 4 of 4 N+M
Matrix: S,
Date Sampled:10/09/2019 0900
% Solids: 11
Date Received:1010912019
Inorganic
non-metals
un Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
2
(% Solids) SM 2540G
1
10/11/2019 0117
MOM
31713
1 350.1
(Ammonia - N ) 350.1
10
10/18/2019 1617
DMA
32376
1
(Nitrate - N) 9056A
1
10/16/2019 1831
SLU
32380
2
(Nitrite - N) 9056A
1
10/17/2019 2107
SLU
32509
1
(Phosphorus) 365.1
10
10/14/2019 1841
DMA
10/14/201.9 1302 31918
1
(Soil pH meas) 9045D
1
10/15/2019 2036
HET
32128
2 351.4
(TKN) 351.2
1
10/22/2019 1438
HKL
10/18/2019 1654 32537
CAS Analytical
Parameter
Number Method
Result Q
LOCI
DL
Units
Run
% Solids
SM 2540G
1.84
%
2
Ammonia - N (gas diffusion)
350.1
9 -0D
540
280
mg/kg
1
Nitrate - N (soluble)
9056A
11 a-
27
1.3
mg/kg
1
Nitrite - N (soluble)
9056A
�
11
1.0
mg/kg
2
Phosphorus
7723-14-0 365.1
15000
2700
540
mg/kg
1
Soil pH measured in water @ 19.1 ° C
9045D
7.5
su
1
TKN
351.2
77000
1400
1400
mg/kg
2
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 10/15/2019 1002 KSH2
10/14/2019 1440 31613
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
4.2
1.0
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 10/16/2019 1757 LLL
10/11/2019 1019 31612
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
20000
360
140
nrl
1
Arsenic
7440-38-2 601OD
ND
14
5.3
mg/kg
1
Cadmium
7440-43-9 601OD
ND
4.5
1.1
mg/kg
1
Calcium
7440-70-2 6010D
14000
4500
560
mg/kg
1
Chromium
7440-47-3 601OD
250
9.0
2.3
mg/kg
1
Copper
7440-50-8 601OD
660
9.0
4.1
mg/kg
1
Iron
7439-89-6 6010D
13000
90
41
mg/kg
1
Lead
7439-92-1 6010D
15
9.0
4.1
mg/kg
1
Magnesium
7439-95-4 6010D
3300 J
4500
560
mg/kg
1
Manganese
7439-96-5 6010D
360
14
5.3
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
36
9.0
mg/kg
1
Nickel
7440-02-0 6010D
22 J
36
9.5
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
-- Out of holding time
W = Reported on wet weight basis
:aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 7

Client:Synagro Laboratory ID:UJ09103-001
Description: 4 of 4 N+M Matrix: Solid
Date Sampled:10/09/2019 0900 % Solids: 1.84 10/11/2019 0117
Date Received:10/09/2019
ICP-AES
un Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD 1 10/16/2019 1757 LLL
10/11/2019 1019
31612
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 601OD
2700 J
4500
560
mg/kg
1
Selenium
7782-49-2 6010D
ND
18
8.2
mg/kg
1
Sodium
7440-23-5 601OD
8500
4500
560
mg/kg
1
Zinc
7440-66-6 6010D
1200
45
11
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 7

Chain Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 7

c)
0
c
3
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S11-1HEALY Chain Of Custody Record
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"p,
Pprrak"M Ly fl%ft $dvb vwte rcr-106.1 al
SHEALY ENVIRONMENTAL SERVICES, INC,
106 Van age Paint Drivo a West Columbia, sc 219172
Telephone No, 1303-791-970re Pwrl\lo.803-791,9111
vAv,v.shc,4r1ab,coni
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a Hejx'xFtdhF)Uw I;y DWO 7k?19
RL
Voft?: Ail __.�._
samples are rata4tied for four gregkjq FforjT rece{vt
yRfess other armng*rnerifa am made.
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LAB USE QVI.Y
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SHEALY ENVIRONMENTAL SERVICES, INC.
$h�181:lkt•iaonnunrzlSul Yicrs,ir,_•. Ynac ;61'i
D--1 NumbcvMEN 15U,1'I F.I.rxltt'vL'ah:R•:f.?QI.�
Sill pt,la Receipt Checklist ('SRC`}
lic,r— S`n,. -��-- Cooler IrLipectcd byl€late u47h+ ,' ]0?U�J,'!g i.or-t: UAY-fl!03
gleans ofrcccipt: S-rSI [j Clietlt U UPS 0 h'udEx D (1rbcT
Ej YesML]NO
!. wera ratstod}+ seal~ pr-acnt on iliv cooler^r
Yes e ley 2_ Ff custody r uuls a c;e prernt, •trttz dery inf.3Cr altd urtbztaktill? -
pH 5 trip ILo_ NA Chroritte Strip ID: NA _ Tested by; Nil —
:rit irtai telnperiturn, Upon n=vipt ? Derived ((-:or Fettled) tCMP8ratu7rc upon nut:ipt %golid Crlap-Cult ir): 14-161
2_5 12.5 rC NA ''N- A, cC NA ; NA_°C NA ;NA tte
�1ethntl: Z Tetlireraturc l3Esn11; [1Againsl BmIes IR CTun !D_ ? II; Gun Conwtion 1-actor, 0 0c
iethr d €tt CUU1anl: ®ZT4r't Tc`. Ll is Packs ❑ DIV Iou None
N®
L teanp�r3tnra , fan-Y wore,t;rdcd 6.0C, was PFoct�1. nag sd?°es
N.A "1g
PM eras Iti od Eetl hy^ Phone i en -jail ! rac"U-ice (circle ow.
Yes
❑' No
® NA 4- Is the c miunercial uciwji r°s packing slip attarbcsl to tllis farm?
Vj Ycs
C] K1n
S.[�l7ctcpropeecnstieUlyPrarCc�luFs (ruliltgnislleLG`rereir�d} fr�llnuci"?
1 'sr�+
❑ No
6, 1t.•'ese sample IL't, listcd on the COC 9
® 5'es
0 No
?. I''Vere s implc 1Dn 3istesr1 on all surnplr. ccnitainm?
Yes
❑ Ni o
S. Was r llcodon date & ihne. listed on tliti mc,,?
lees
11 No
9. Was collection datc & tine listcd M1 all samp[c OMIAinrss?
Yes
No
tG. Did tsll cott[ainer label hifa Tmattion (1D: date,, tisnep al,rcc with Lha C:()C;'
Yes
No
11 ° Were tests to be parfornted listed on fit (.0t.7?
21 ire
❑ No
[2, Did fill s:t11ple;5 arrive- in dw proper coFatainors for eauh test andiar in goad oundition
(unbrnkou, lids on, cic,l°
0 'tis
CJ
13- Vtius adegaulo sample t•nh,mo availilble?
Yc:
ri o
14. L; = all satnples received vrithin :� the Holding tinta or 49 hdxFTM, t�liiuher er lirsR,
L7 1'cs
J ldo
comes
1S. Were amp saniFdes containers nti.sitlg?excu�.s (circle fiaca satuples Not listed ttn C C?
`os
No
NA 16. I'Dr �.0 L uml RSK-175 samples, werr. babbles present:x"p a -size" 4,,"cr tjm[Y4 in clisstri[�tei
ill ariw° of the V0A i�ial3'�
L-1 it 3
4
R'A 17, 'v rl,3 uEl l_)R(y1raVl BI81`[llDC37e rt[ SaDYpI Fr?t rived at pH of ?? L
11 y"
fir
®-NA 18., Werc 911 C. �ndu sate l' 11�CC1Yt3Cl rtt 9 ? 1? and sulfitit-
Yteti
ON.1
pH mmples recol cd at a �Ti >
0 NA 1$. 1Verc rill applicable NIfI-;� KN.�c}�nidelpllcno '6?S (_: {l.5utg,'I,) s�rnples Crc4 of'r�,idlustl
�,,,' ❑ N¢ ®JINI.,kl2tt.1'r'crt: elicru. rcmt r12s."rtcllrests (i-a- rxlnested CUtions, N+ISMSD de�ignatiotts: etc,.corrt:ctty [rancGa;bcd li-oul the COC into the corrrmcr,t sectidirl in 1LIIv V
Yes b.To2.1 ° 'Was the note rttiml,cr listcd on the containur label? if yes, LFu�[e 1F Net
�arnple P,"cssa'Yatit,n (Aiusl be comp[eiyrll'or any �amplc(sj inr:rrirectl�; prtscxt�cd or'x�th [tea;lsl�etce.l
sr�gtle(s) NA wcrc receivtxl in^orrectly prescrved3 and were adj�js(cd &cc,
7'Mmple recoiviFlt; with N'A mL of Cir:le tmo: H2SO4, HNO3, IICI, NaGlli LvjinE 31t,1 NA
lens• of presctvatialt NA . If more than one preservative is needed, plense now: in the r.oawicwsbelt-w.
NA
v,ern J)&: ive;i vdtEi bubbles .•6 Fnm :n diatt_etcr.
`'' ' we_a rertfv, 1 mvith TRC = 0.5 n3grL (1f. 19 t.s fgo ) arlcl were
accordingly in sample rcxmriving with sodlium Lbiosulfate (Na 5,03) i0h Shealy ID, NA
b;Lrrode labels applied t }y: JSR
CVerlmcnts_
Dale: l [L•'Ug! t 9
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 10/9/2019 101112019-12131/2019 2.2705
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (8500 x 1.8400) + 100 = 156.4
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (14000 x 1.8400) = 100 = 257.6
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3300 x 1.8400) t- 100 = 60.72
Na meq = Na mg/I _ Molec.Wgt.Na = 156.4 = 23 = 6.8
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 257.6 + 20 = 12.88
Mg meq = Mg mg/I = Molec.Wgt.Mg = 60.72 = 12 = 5.06
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.8 _ SgrRoot[0.5(12.88+5.06)] = 2.27045
Printed: 2/1 /2020
Page 1 13:57

SECTION 3

Q
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: HULETT
OWNER: CEDAR LAKE FARMS PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 135.36
SITE #: NC CL 00012 FIELD# : CL 00012 0001 OPERATOR: CHARLIE JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 51.20 ACRES PERMITTED: 51.20
Page
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Ni items
6/20/19
86,800.00 (G)
1695.313
1.38
0.098
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
530.00\p
26630
FESCUE PASTURE
6/21/19
86,800.00 (G)
1695.313
1.38
0.098
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
530.00 p
26630
FESCUE PASTURE
6/24/19
105,400.00 (G)
2058.594
1.38
0.118
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
530.00 p
26630
FESCUE PASTURE
6/26/19
99,200.00 (G)
1937.500
1.38
0.112
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
530.00 p
26630
FESCUE PASTURE
6/27/19
68,200.00 (G)
1332.031
1.38
0.077
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
p
26630
FESCUE PASTURE
6/28/19
93,000.00 (G)
1816.406
1.38
0.105
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
'530.00
530.00 p
26630
FESCUE PASTURE
Jun-19
539,400.00 (G)
10,535.157
7/1/19
130,200.00 (G)
2542.969I
2.57
0.273
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
9.00 p
16139
FESCUE PASTURE
7/2/19
111,600.00 (G)
2179.688
2.57
0.234
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
39.00 p
16039
FESCUE PASTURE
Jul-19
241,800.00 (G)
4,722.657
5 . �
9/3/19
37,200.00 (G)
726.563
2.57
0.078
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
16039
FESCUE PASTURE
9/4/19
105,400.00 (G)
2058.594
2.57
0.221
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
/10,'-00
39.00 p
16039
FESCUE PASTURE
9/5/19
136,400.00 (G)
2664.063
2.57
0.286
MI-IAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
39.00 p
16039
FESCUE PASTURE
9/6/19
130,200.00 (G)
2542.969
2.57
0.273
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
39.00 p
16039
FESCUE PASTURE
9/9/19
105,400.00 (G)
2058.594
2.57
0.221
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
39.00 p
16039
FESCUE PASTURE
9/10/19
49,600.00 (G)
968.750
2.57
0.104
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
39.00 p
16039
FESCUE PASTURE
9/11/19
105,400.00 (G)
2058.594
2.57
0.221
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
39.00 p
16039
FESCUE PASTURE
9/12/19
62,000.00 (G)
1210.938
2.57
0.130
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
46,000. p
11,000.00 p
.00
16039
FESCUE PASTURE
Sep-19
731,600.00 (G)
14,289.065
42),�J

FACILITY NAME: MOUNT HOLLY, NC
OWNER: CEDAR LAKE FARMS
SITE #: NC CL 00012 FIELD# : CL 00012 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HULETT
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 135.36
OPERATOR: CHARLIE JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 51.20 ACRES PERMITTED: 51.20
Page : 2
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1 otal UalIons/Ac: 29,546.8N
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
98
0.044
0.011
0.752
2.041
0.048
0.005
0.088
0.098
0.074
3.676
82.07
Cumulative Ibs/acre
0.069
0.031
0.913
2.564
0.089
0.007
0.144
0.259
0.154
4.506
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
132
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
;
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X 120
(SIGNATURE AND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: MADISON
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 6.54
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 3.40 ACRES PERMITTED: 3.40
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
N
4/1/19
55,800.00 (G)
16411.7651
1.38
0.944
MIIAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
530.00 p/
26630
FESCUE HAY
Apr-19
55,800.00 (G)
16,411.765
11/7/19
43,400.00 (G)
12764.7061
1.84
0.979
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
(110`.00 p,-)
21150
FESCUE HAY
Nov-19
1 43,400.00 (G)
12,764.706
1
q
Total Gallons/Ac:
Total Wet Tons/Ac:
29,176.47
v.w
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
100
0.019
0.004
0.773
2.124
0.050
0.004
0.034
0.070
0.030
3.824
74.71
Cumulative lbs/acre
0.034
0.015
1.727
4.391
0.141
0.007
0.060
0.139
0.055
7.539
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
r
146
a
q
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
1
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
xx;�2
(SIGNATURE O AND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: MOUNT HOLLY. NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 22.00
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90
Page
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite��
4/1/19
167,400.00 (G)
18808.989
1.38
1.082
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
SC 30.00T")26630
FESCUE HAY
Apr-19
167,400.00 (G)
1 18,808.989�-p
-�
11/7/19
136,400.00 (G)
15325.8431
1.84
1.176
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
J"10- 0 p
25150
I FESCUE HAY
11/11/19
24,800.00 (G)
2786.517
1.84
0.214
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
; 110.00,"p "r
21150
FESCUE HAY
Nov-19
161,200.00 (G)
18,112.360
Total Gallons/Ac:
Total Wet Tons/Ac:
Total Cubic Yds/Acm
36,921.35
0 00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
128
0.024
0.005
1.020
2.787
0.066
0.006
0.044
0.091
0.038
5.024 �93.65
Cumulative lbs/acre
0.095
0.051
6.907
14.682
0.753
0.030
0.205
0.662
0.158
--
23.018 r
-
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
I
179
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 I
i
375.0
89.0
2500.0
9
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
DATE
is document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
ed %=percent p=ppm ormg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
n, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

SUMMARYANNUAL LAND APPLICATION FIELD FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: GREG SPRINGS PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 9.28
SITE #: NC GA 00041 FIELD# : GA 00041 0010 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or'Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/1/19
24,800.00 (G)
3139.241
1.38
0.181
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
530:00 p
26630
FESCUE HAY
4/2/19
86,800.00 (G)
10987.342
1.38
0.632
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
t 530.00 p
26630
FESCUE HAY
4/3/19
49,600.00 (G)
6278.481
1.38
0.361
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
\530.00j;
26630
FESCUE HAY
Apr-19
1 161,200.00 (G)
20,405.064
i orai vauons/Ac:
Total Wet Tons/Ac:
2U,4U.-J.Ub
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual lbs/acre
63
0.010
0.003
0.352
1.033
0.026
0.003
0.021
0.033
0.017
1.832 56.36
Cumulative lbs/acre
0.053
0.031
4.197
8.716
0.465
0.019
0.129
0.410
0.092
13.364
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
187
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
15.0 � �
375.0
89.0
1
2500.0 ,
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
x
(SIGNATURE OF L ER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0014
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 15.46
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.80 ACRES PERMITTED: 6.80
Page
Lime Applied ***
Date
LbsAc
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I
DATE or
Solids
Per
Residual
Dry, Wet,
Past24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/1/19
24,800.00 (G)
3647.059
1.38
0.210
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
p
26630
FESCUE HAY
4/2/19
62,000.00 (G)
9117.647
1.38
0.525
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
t/530.00
1� 530.00 p
26630
FESCUE HAY
4/3/19
49,600.00 (G)
7294.118
1.38
0.420
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
''530.0_0_p
26630
FESCUE HAY
Apr-19
136,400.00 (G)
20,058.824
I1/7/19
99,200.00 (G)
14588.2351
1.84
1.119
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
; 110.0d p
25150
FESCUE HAY
Nov-19
99,200.00 (G)
14,588.235
1
I
Total Gallons/Ac: 34,647.06
Total Wet Tons/Ac:
Total Pubic Vds/Ar- n nn
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
118
0.022
0.005
0.906
2.493
0.059
0.005
0.040
0.082
0.035
4.487
88.99
Cumulative ]bs/acre
0.078
0.042
5.817
12.378
0.614
0.024
0.174
0.542
0.132
19.623
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
;
177
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
s
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
x
(SIGNATURE OF LAND R) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 10.35
SITE #: NC LT 00046 FIELD# : LT 00046 0001 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/11/19
86,800.00 (G)
7355.932
1.38
0.423
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
/530.00 p�
26630
FESCUE HAY
4/17/19
93,000.00 (G)
7881.356
1.38
0.454
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
530.00 p
26630
FESCUE HAY
Ap,19
1 179,800.00 (G)
15,237.288
'
Total (gallons/Ac:
Total Wet Tons/Ac:
15,237.29
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
47
0.008
0.002
0.263
0.772
0.019
0.002
0.015
0.025
0.013
1.368
42.09
Cumulative Ibs/acre
0.076
0.044
5.437
10.195
0.656
0.022
0.123
0.465
0.119
16.077
J
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
182
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
(SIGNATURE OF L APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME : MOUNT HOLLY, NC
OWNER: TONY JONES
SITE #: NC LT 00046 FIELD# : LT 00046 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 64.24
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 45.20 ACRES PERMITTED: 45.20
Page
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp )
Crom p
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
2/14/19
99,200.00 (G)
2194.690
1.60
0.146
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
59,100. p
8,090.00 p
121.00 p
19469
FESCUE PASTURE
2/15/19
136,400.00 (G)
3017.699
1.60
0.201
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
59,100. p
8,090.00 p
121.00 p
19469
FESCUE PASTURE
Feb-19
1 235,600.00 (G)
5,212.389
_
11/11/19
155,000.00 (G)
3429.204
1.84
0.263
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
0.00 p
25150
I FESCUE PASTURE
11/18/19
55,800.00 (G)
1234.513
1.84
0.095
MHAEDL
MOIST
"0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
0.00 p
21110
FESCUE PASTURE
11/19/19
117,800.00 (G)
2606.195
1.84
0.200
MHAEDL
MOIST
"0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
0.00 p
25150
FESCUE PASTURE
11/20/19
173,600.00 (G)
3840.708
1.84
0.295
MHAEDL
MOIST
"0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
.00 p
(ov,
25150
FESCUE PASTURE
11/21/19 .
130,200.00 (G)
2880.531
1.84
0.221
MHAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p000
21150
FESCUE PASTURE
Nov-19
632,400.00 (G)
13,991.151

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME : MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LTJ PROPERTIES LLC PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 64.24
SITE #: NC LT 00046 FIELD# : LT 00046 0002 OPERATOR: LTJ PROPERTIES LLC CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 45.20 ACRES PERMITTED: 45.20
Page: 2
Lime Applied ***
Date
Lb,/A,
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1 Mal Uauuus�t-�c:
Total Wet Tons/Ac:
m,.«..1 �..L:.. V.1../A ...
1 Y,LUJ.J4
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
68
0.032
0.004
0.714
1.793
0.043
0.002
0.030
0.060
0.038
3.085 40.69
Cumulative lbs/acre
0.400
0.079
6.735
32.432
2.114
0.067
0.373
1.446
0.205
40.647
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
!
137
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
T z Lwi z�
X
(SIGNATURE OF LAND 4PLI R) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: MOUNT HOLLY, NC
OWNER: TONY JONES
SITE #: NC LT 00046 FIELD# : LT 00046 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 9.28
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90
Page
Lime Applied ***
Date
Lbs Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrpte�..^
4/3/19
31,000.00 (G)
3131.313
1.38
0.180
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
f�530.00 p�
26630
FESCUE HAY
4/4/19
62,000.00 (G)
6262.626
1.38
0.360
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
i 530.00 P k
26630
FESCUE HAY
4/11/19
43,400.00 (G)
4383.838
1.38
0.252
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
", 530.00 p ,-
26630
FESCUE HAY
4/17/19
24,800.00 (G)
2505.051
1.38
0.144
MHAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
530.00 Xp
26630
FESCUE HAY
Apr-19
161,200.00 (G)
16,282.828
-I-U5b
i otai liattons/AC:
Total Wet Tons/Ac:
16,282.N:5
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
50
0.008
0.002
0.281
0.825
0.021
0.002
0.016
0.026
0.013
1.462
44.98
Cumulative ]bs/acre
0.083
0.049
5.907
11.066
0.712
0.024
0.135
0.515
0.130
17.300
j
—
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
183
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
IS 0 €
_ s
375.0
89.0
2500.0�—
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X 21,1126�1
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or m&g ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LTJ PROPERTIES LLC PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 17.60
SITE #: NC LT 00046 FIELD# : LT 00046 0004 OPERATOR: LTJ PROPERTIES LLC CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 19.40 ACRES PERMITTED: 19.40
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm )
crop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite��
11/21/19
43,400.00 (G)
2237.113
1.84
0.172
MHAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
g 110'00 p
ri
25150
FESCUE PASTURE
11/22/19
186,000.00 (G)
9587.629
1.84
0.736
MHAEDL
DRY
"0-<1/2"
SUR
0.5
0.30
77,000. p
9,700.00 p
110.00 p�
25150
FESCUE PASTURE
Nov-19
229,400.00 (G)
119824.742
t,
Total Gallons/Ac:
Total Wet Tons/Ac:
11,824.74
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
46
0.010
0.002
0.454
1.198
0.027
0.002
0.016
0.040
0.015
2.177
27.22
Cumulative lbs/acre
0.155
0.076
5.041
41.728
1.700
0.087
0.477
1.595
0.181
39.246
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
126
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0—
375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 6.07
SITE #: NC LT 00046 FIELD# : LT 00046 0008 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or%
Wet Tons (WT) (specify)
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite__\
4/3/19
31,000.00 (G)
4696.970
1.38
0.270
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
/530.00 p \
26630
FESCUE HAY
4/4/19
49,600.00 (G)
7515.152
1.38
0.432
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
{ 530.00 p
26630
FESCUE HAY
4/11/19
24,800.00 (G)
3757.576
1.38
0.216
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
82,000. p
7,500.00 p
�53, 0 00 pfr
26630
FESCUE HAY
Apr-19
1 105,400.00 (G)
15,969.698
Total Gallons/Ac:
Total Wet Tons/Ac:
15,969.70
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
49
0.008
0.002
0.276
0.809
0.020
0.002
0.016
0.026
0.013
1.434
44.11
Cumulative lbs/acre
0.079
0.047
5.701
10.675
0.690
0.023
0.130
0.502
0.125
16.598
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
187
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
C
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X � zo
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DEAN S. CONNELL PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 32.68
SITE #: NC MG 00037 FIELD# : MG 00037 0001 OPERATOR: DEAN S. CONNELL CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 20.20 ACRES PERMITTED: 20.20
Page
Lime Applied ***
Date .
Lbs Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
00
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
3/8/19
124,000.00 (G)
6138.614
1.60
0.410
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
59,100. p
8,090.00 p
121.00 p
19469
FESCUE PASTURE
3/18/19
223,200.00 (G)
11049.505
1.60
0.737
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
59,100. p
8,090.00 p
121.00 p
19469
FESCUE PASTURE
3/19/19
142,600.00 (G)
7059.406
1.60
0.471
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
59,100. p
8,090.00 p
121.00 p
19469
FESCUE PASTURE
Mar-19
1 489,800.00 (G)
24,247.525
Total Gallons/Ac:
Total Wet Tons/Ac:
24,247.52
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs/acre
63
0.097
0.010
0.825
1.747
0.049
0.001
0.049
0.060
0.097
2.365
39.47
Cumulative lbs/acre
0.202
0.046
5.349
10.419
0.587
0.020
0.154
0.483
0.187
14.957
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
I
f
,
145
FD Cumulative Pollutant Loading Rate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0 1
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
X 2/lam/moo
(SIGNATURE OF L APPLI DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

SECTION 4

P Stll?f?tiPalcilT 1L'$d C1ub*1€}1 ii ^i, INC
Arli-ity0cal Laboraroneg
January 21, 2019
Adam Brigman
Synagro, NC 28134
12701 Lancaster Hwy
Pineville, NC 28134
TEL: [phone]
FAX: [phone]
RE: Mt Holly
Dear Adam Brigman:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Order No.: 19010438
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/9/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 28

Summit Environmental Technologies, Inc. Case Narrative
native
SUMMIT 3310 Win St.
ERV11101 eIrENTAL TEC4iN0LQC:,lF , INC, Cuyahoga Falls, Ohio 44223 WO#: 19010438
Amai vtical Labonvort&r TEL: [phone] FAX: [phone]
Website: http://Www.settek.com Date: 1/21/2019
DENT: Synagro, NC 28134
Project: Mt Holly
WorkOrder Narrative:
19010438: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
-'mes and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
_Dr use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19010438-OOIA SVOC-BNA_TCLP(8270d): Possible low bias for Pyridine due to low recovery in
CCV; Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
19010438-OOIA SVOC-BNA TCLP(8270d): Sample exhibited low recovery of Surrogates: 2-
Fluorophenol, Phenol-d6 possibly due to matrix effect.
Analytical Sequence QC Notes:
ccv 250 18712 re svoc-cPEST_npw(8081): CCV exhibits high recovery for endrin. All samples are ND
CCV 40ng 14287 SVOC-MSTR S(8270): The CCV (Batch R93442) exhibited high recovery for
Hexachlorobutadiene and Pentachlorophenol. The associated samples are ND for the analytes with high
Original
Page 2 of 28

Summit Environmental Technologies, Inc. 3310 Win St. Case Narrative
mS+lt?0NMl 5-MTAL'rEC J0I- 47, s, INC, Cuyahoga Falls, Ohio 44223 w04: 19010438
- 417.-T'yilcal LaboralorioG TEL: [phone] FAX.- [phone]
Website: httn:11www.settek.com Date: 1/21/2019
LIENT: Synagro, NC 28134
Project: Mt Holly
recoveries.
CCV 40ng 14287 SVOC-MSTR_S(8270): The CCV (Batch R93442) exhibited low recovery for
Pyridine. Possible low bias for Pyridine due to low recovery in CCV; Reporting Limit Check shows
adequate instrument sensitivity for reporting purposes.
MB-35513 SVOC-BNA_TCLP(8270): MB-35513 exhibited low recovery of Surrogate: 2-Fluorophenol.
MB-35513 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
LCS-35513 SVOC-BNA_TCLP(8270): LCS-35513 exhibited low recovery of Surrogate: 2-
Fluorophenol.
LCS-35513 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
Original
Page 3 of 28

Sununit Environmental Technologies, In Qualifiers and Acronyms
summ1mr 3310 Win S
�tlrlt?O T L iLG71&VOLCyG3;S INC Cuyahoga Falls, Ohio 442�
WO#: 19010438
4-,Tafytlaal Laboratarf& TEL: [phone] FAX.- (330) 253-445
11www.settek.co11Www.settek.co Date: 1/21/2019
Website: hqp.-
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded. Not Clean Water Act compliant.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+). .
S The spike result was outside of accepted recovery limits.
W Samples were received outside temperature limits (0' — 6° C). Not Clean Water Act compliant.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 28

Summit Environmental Technologies, Inc. Workorder
m9summrr 3310 Win St.
NVIR0Nra wTALTLC 11.N0LQGIES, IN 0 Cuyahoga Falls, Ohio 44223 Sample Summary
t IMIlIff"cal L,?b ratar{as TEL: [phone] FAX.- [phone] WO#: 19010438
Website: http://www.settek.com 21-Jan-19
CLIENT: Synagro, NC 28134
Project: Mt Holly
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
19010438-001 Mt Holly 1/7/2019 10:02:00 AM 1/9/2019 10:20:00 AM Sludge
Page 5 of 28

SuinrnitEnvironnsentalTechnologies,Inc DATES F 'ORT
SUMMIT3310 Win Si
1�4rlbtt7Nd1+1� •�T�L Pc�tti a, PICA Cuyahoga Falls, Ohio 44223
eIngfytienP Laborasonos TEL: [phone] FAX.- [phone] WO#: 19010438
Wehsite: hto.-Ilwww.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
19010438-OOIA Mt Holly 1/7/2019 10:02:00 AM Sludge Ignitability of Solids (SW-846: 1030) 1/11/2019 11:00:00 AM
Paint Filter Free Liquids Test (SW-846 1/9/2019 3:15:00 PM
9095)
pH (SW9045D) 1/10/2019 3:52:16 PM
Reactive Cyanide (9014/7.3.3.2)-Solid 1/14/2019 11:38:00 AM
Reactive Sulfide (9034)/7.3.4.2 1/14/2019 11:08:00 AM
SVOC PCB (8082) 7-Arochlors 1/10/2019 9:30:00 AM 1/14/2019 12:28:00 PM
TCLP Herbicides Analysis (SW1311/81/9/2019 6:00:00 PM 1/11/2019 5:00:00 PM 1/18/2019 4:18:00 PM
TCLP Mercury Analysis (SW1311/7471/9/2019 6:00:00 PM 1/10/2019 12:45:00 PM 1/10/2019 5:42:00 PM
TCLP Metals Analysis (SW1311/6010:1/9/2019 6:00:00 PM 1/10/2019 11:45:00 A 1/11/2019 3:05:24 PM
17
TCLP Pesticides Analysis (SW1311/8(1/9/2019 6:00:00 PM 1/11/2019 11:45:00 A 1/16/2019 11:04:00 AM
r7
TCLP Semi-Volatiles Analysis 1/9/2019 6:00:00 PM 1/14/2019 10:45:00 A 1/15/2019 11:03:00 PM
(SW1311/8270) Td
TCLP Volatiles Analysis 1/9/2019 6:00:00 PM 1/10/2019 2:42:00 PM
Original
Page 6 of 28

Summit Environmental Technologies, Inc. Analytical Report
summilt 3310 Win St.
Cka�lt?t7tJh1} tJl',4L��c?�r9c]4etIS, t`, Cuyahoga Falls, Ohio 44223 (base report)
A mtti11'tical TEL: [phone] FAX: [phone] WO#: 19010438
Website: http://`vwiv.settek.com Date Reported: 1/21/2019
'LIENT:
Synagro, NC 28134 Tag Number:
Matrix:
SLUDGE Collection Date: 1/7/2019 10:02:00 AM
Lab ID:
19010438-001A
Project:
Mt Holly
Client Sample ID Mt Holly
Analyses Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
0.00500
mg/L
1
1/10/2019 5:42:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW601OD
SW3010A
Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND
0.500
mg/L
1
1/11/2019 3:05:24 PM
TCLP Barium(Ba) ND
5.00
mg/L
1
1/11/2019 3:05:24 PM
TCLP Cadmium(Cd) ND
0.100
mg/L
1
1/11/2019 3:05:24 PM
TCLP Chromium(Cr) ND
0.200
mg/L
1
1/11/2019 3:05:24 PM
TCLP Lead(Pb) ND
0.500
mg/L
1
1/11/2019 3:05:24 PM
TCLP Selenium(Se) ND
0.0500
mg/L
1
1/11/2019 3:05:24 PM
TCLP Silver(Ag) ND
0.500
mg/L
1
1/11/2019 3:05:24 PM
CLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW3510C Analyst: BJH
i CLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND
0.0800
mg/L
2
1/15/2019 11:03:00 PM
2,4,5-Trichlorophenol ND
0.200
mg/L
2
1/15/2019 11:03:00 PM
2,4,6-Trichlorophenol ND
0.200
mg/L
2
1/15/2019 11:03:00 PM
2,4-Dinitrotoluene ND
0.0400
mg/L
2
1/15/2019 11:03:00 PM
o-Cresol ND
0.200
mg/L
2
1/15/2019 11:03:00 PM
m/p-Cresol(s) ND
0.200
mg/L
2
1/15/2019 11:03:00 PM
Cresols, Total ND
4.00
mg/L
2
1/15/2019 11:03:00 PM
Hexachloro-1,3-butadiene ND
0.0160
QC+
mg/L
2
1/15/2019 11:03:00 PM
Hexachlorobenzene ND
0.0400
mg/L
2
1/15/2019 11:03:00 PM
Hexachloroethane ND
0.0800
mg/L
2
1/15/2019 11:03:00 PM
Nitrobenzene ND
0.0800
mg/L
2
1/15/2019 11:03:00 PM
Pentachlorophenol ND
0.200
QC+
mg/L
2
1/15/2019 11:03:00 PM
Pyridine ND
0.200
QC-
mg/L
2
1/15/2019 11:03:00 PM
Surr: 2-Fluorophenol 7.60
10 - 109
S
%Rec
2
1/15/2019 11:03:00 PM
Surr: Phenol-d6 8.76
10 - 109
S
%Rec
2
1/15/2019 11:03:00 PM
Surr: Nitrobenzene-d5 64.5
19 - 120
%Rec
2
1/15/2019 11:03:00 PM
Surr: 2,4,6-Tribromophenol 15.3
10 - 120
%Rec
2
1/15/2019 11:03:00 PM
Surr: 2-Fluorobiphenyl 65.1
22 - 117
%Rec
2
1/15/2019 11:03:00 PM
Qualifiers: Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
0 RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 7 of 28

Summit Environmental Technologies, Inc. Analytical Report
m9summmor 3310 Win St.
ef§t4+Ifs�tJi�11�1T,�Lzt?tccatic;��.,,r,4c. Cuyahoga Falls, Ohio44223 (base report)
Af7dr(YUC12/ LaboraxoH&e TEL: [phone] FAX: [phone] WO#: 19010438
Website: http:/hviviv.settek.com Date Reported: 1/21/2019
'LIENT:
Synagro, NC 28134
Matrix:
SLUDGE
Lab ID:
19010438-OOIA
Project:
Mt Holly
Client Sample ID Mt Holly
Tag Number:
Collection Date: 1/7/2019 10:02:00 AM
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
SW8270D SW3510C Analyst: BJH
Surr: p-Terphenyl-d14 99.8 34 - 116 %Rec 2 1/15/2019 11:03:00 PM
NOTES:
Possible low bias for Pyridine due to low recovery in CCV; Reporting Limit Check shows adequate instrument sensitivity for reporting
purposes.
Sample exhibited low recovery of Surrogates: 2-Fluorophenol, Phenol-d6 possibly due to matrix effect.
SVOC PCB (8082) 7-AROCHLORS
SW8082 SW3550C Analyst: PGP
Aroclor 1016
ND
0.00600
mg/Kg
1
1/14/2019 12:28:00 PM
Aroclor 1260
ND
0.00600
mg/Kg
1
1/14/2019 12:28:00 PM
Aroclor 1221
ND
0.00600
mg/Kg
1
1/14/2019 12:28:00 PM
Aroclor 1232
ND
0.00600
mg/Kg
1
1/14/2019 12:28:00 PM
Aroclor 1242
ND
0.00600
mg/Kg
1
1/14/2019 12:28:00 PM
Aroclor 1248
ND
0.00600
mg/Kg
1
1/14/2019 12:28:00 PM
Aroclor 1254
ND
0.00600
mg/Kg
1
1/14/2019 12:28:00 PM
Total PCBs
ND
0.00600
mg/Kg
1
1/14/2019 12:28.-00 PM
Surr: DCB
100
10 - 165
%Rec
1
1/14/2019 12:28:00 PM
Surr: TCMX
72.5
10 - 139
%Rec
1
1/14/2019 12:28:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C Analyst: MES
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
10
1/16/2019 11:04:00 AM
Toxaphene
ND
0.0500
mg/L
10
1/16/2019 11:04:00 AM
Endrin
ND
0.00500
QC+ mg/L
10
1/16/2019 11:04:00 AM
gamma-BHC
ND
0.00500
mg/L
10
1/16/2019 11:04:00 AM
Heptachlor
ND
0.00500
mg/L
10
1/16/2019 11:04:00 AM
Heptachlor epoxide
ND
0.00500
mg/L
10
1/16/2019 11:04:00 AM
Methoxychlor
ND
0.00500
mg/L
10
1/16/2019 11:04:00 AM
Surr: TCMX
22.6
10 - 119
%Rec
10
1/16/2019 11:04:00 AM
Surr: DCB
35.3
10 - 119
%Rec
10
1/16/2019 11:04:00 AM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND
Not Detected
0 RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
Original
R
RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 8 of 28

Summit Environmental Technologies, Inc. Analytical Report
SUMMINt 3310 Win St.
�A l'IRONh1@idTAL3EC%fS<!O!_CPf;I�$, wC, Cuyahoga Falls, Ohio 44223 (base report)
Arrfi .rMcal Latioralows TEL: [phone] FAX.- [phone] WO#: 19010438
Website: http://www.settelc.com Date Reported: 1/21/2019
:LIENT:
Synagro, NC 28134
Matrix:
SLUDGE
Lab ID:
19010438-001A
Project:
Mt Holly
Client Sample ID Mt Holly
Tag Number:
Collection Date: 1/7/2019 10:02:00 AM
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)
2,4-D ND 1.00
2,4,5-TP ND 0.500
Surr: DCAA 72.6 20 - 140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
99.3
Surr: Di brom ofluorom ethane
95.2
Surr: Toluene-d8
100
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
PAINT FILTER FREE LIQUIDS TEST (SW-846: 9095)
Free Liquid fail
RCI-SOLID-W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
SW8151A SW8151A Analyst: MES
mg/L 1 1/18/2019 4:18:00 PM
mg/L 1 1/18/2019 4:18:00 PM
%Rec 1 1/18/2019 4:18:00 PM
SW8260B SW1311 M Analyst: RMT
0.0500
mg/L
10
1/10/2019 2:42:00 PM
0.0500
mg/L
10
1/10/2019 2:42:00 PM
0.250
mg/L
10
1/10/2019 2:42:00 PM
0.0500
mg/L
10
1/10/2019 2:42:00 PM
0.0500
mg/L
10
1/10/2019 2:42:00 PM
0.0500
mg/L
10
1/10/2019 2:42:00 PM
0.0500
m mg/L
10
1/10/2019 2:42:00 PM
0.0500
mg/L
10
1/10/2019 2:42:00 PM
0.0500
mg/L
10
1/10/2019 2:42:00 PM
0.0200
mg/L
10
1/10/2019 2:42:00 PM
70 - 130
%Rec
10
1/10/2019 2:42:00 PM
70 - 130
%Rec
10
1/10/2019 2:42:00 PM
70 - 130
%Rec
10
1/10/2019 2:42:00 PM
SW9014
Analyst: MS
0.495
mg/Kg
1
1/14/2019 11:38:00 AM
SW9095
Analyst: DHC
1
1/9/2019 3:15:00 PM
SW1030
Analyst: AJT
1
1/11/2019 11:00:00 AM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
0 RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 28

Summit Environmental Technologies, Inc. Analytical Report
summlar 3310 Win St.
1fi1'II}t�IVIYt>i•ITA.L€C±��+o4ctc;�zS,th1�. Cuyahoga Falls, Ohio44223 (base report)
AnrityYlcal Laborworics. TEL: [phone] FAX.• [phone] WO#: 19010438
Website: http://www.settek.com Date Reported: 1/21/2019
'LIENT:
Synagro, NC 28134
Matrix:
SLUDGE
Lab ID:
19010438-001A
Project:
Mt Holly
Client Sample ID Mt Holly
Tag Number:
Collection Date: 1/7/2019 10:02:00 AM
Analyses Result RL Qual Units DF Date Analyzed
RCI-SOLID-W/ IGNITABILITY1030 SW9045D Analyst: VVK
PH (SW9045D)
pH 6.9 s.u.@20.00 1 1/10/2019 3:52:16 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 1/14/2019 11:08:00 AM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
0 RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 10 of 28

Summit Environmental Technologies, Inc. Accreditation Program
MSUMMIT 3310 Win St. Anal teS Report
¢ 1rIRC�NPe1> T•1Tr�L$z 9 i�C56Ci4aiZ5,IrIC Cuyahoga Falls, Ohio44223 Y p
ARrifytkt?! Laborawt'w TEL: [phone] FAX- [phone] WO#: 19010438
Website: http://Wivw.settek.cont 21-Jan-19
Client:
Synagro, NC 28134
State:
NW
Project:
Mt Holly
Program Name:
NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
1901043 8-001 A
Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Paint Filter Free Liquids Test (SW-846: 9095)
Free Liquid
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
SVOC PCB (8082) 7-Arochlors
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1016
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1221
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1232
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1242
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1248
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1254
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1260
A
Sludge
SVOC PCB (8082) 7-Arochlors
Tetrachloro-m-xylene
A
Sludge
SVOC PCB (8082) 7-Arochlors
Total PCBs
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4,5-TP
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4-D
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
DCAA
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Original # 1
Page 11 of 28

Summit Environmental Technologies, Inc. Accreditation Program
m9
SUMMIT3310 Win St. Analp tes Report
_NRIIf?L�Nh.1Et-ITAL �iFC9��t(31-i?C�lGS, 1r-4 Cuyahoga Falls, Ohio 44223 J p
rinalj Irtica} Ldborator/&s TEL: [phone] FAX: [phone] WO#: 19010438
Website: http://www.settek.coni 21-Jan-19
Client: Synagro, NC 28134 State: NW
Project: Mt Holly Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19010438-001A Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Tetrachloro-m-xylene
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Tribromophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
3,4-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene-d5
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Phenol-d6
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
p-Terphenyl-dl4
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane A
Sludge
TCLP Volatiles Analysis
2-Butanone A
Sludge
TCLP Volatiles Analysis
4-Bromofluorobenzene A
Sludge
TCLP Volatiles Analysis
Benzene A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride A
Sludge
TCLP Volatiles Analysis
Chlorobenzene A
Sludge
TCLP Volatiles Analysis
Chloroform A
Sludge
TCLP Volatiles Analysis
Dibromofluoromethane A
Original # 1
Page 12 of 28

Summit Environmental Technologies, Inc. Accreditation Program
Oro. - UMMIffir3310 Win St. Anal teS Report
ENrVI T0fJMr-I,JTAL �icr[.t Gt S, fP 4 Cuyahoga Falls, Ohio 44223 y p
AgaJytJ J Laboratories TEL: [phone] FAX [phone] WO#: 19010438
Website: http://Www.settek.com 21-Jan-19
Client: Synagro, NC 28134 State: NW
Project: Mt Holly Program Name: NC_WW SCM
Sample ID Matrix
Test Name
Analyte
Status
19010438-001A Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Toluene-d8
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
Original # 1
Page 13 of 28

1Ar Summit Environmental Technologies, Inc. QC SUMMARY Rl,JL)ORT
ffJ:&UMM3310 Win St.
E Mr1i10 J1.1EITML TEECTINO4oGtZS, ItIC Cuyahoga Falls, Ohio 44223
,�kr7�Ft;�'.f/e�1 LtllatxJ�tt�rd�+s WO#: 19010438
TEL: [phone] FAX.- [phone]
Website: htW.-Ilwww.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 35455
Sample ID MB-35455
SampType: MBLK
TestCode:
TCLP-voc-ms Units: mg/L
Prep Date: 1/9/2019
RunNo: 93248
Client ID: PBS
Batch ID: 35455
TestNo:
SW8260B SW1311M
Analysis Date: 1/10/2019
SegNo: 1902259
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
48.0
Surr: Di brom ofl uorom ethane
48.0
Sum Toluene-d8
48.0
50.00 95.9 70 130
50.00 95.9 70 130
50.00 95.9 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 14 of 28
Original

Summit Environmental Technologies, Inc. QC SUMMARY 7� l)ORT
L&UNkMIT 3310 Win St. 11.. �7 i i11� 1
��t�liiU:tJP.1rSJ7�L'>riCtrt�cat t3 :� , J11J:C Cuyahoga Falls, Ohio 44223
Aj7vidcaf LaLi ra,forio TEL: [phone] FAX.- [phone] WO#: 19010438
;,
Website: htto://www.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 35458
Sample ID MB-35458
SampType: MBLK
TestCode:
SVOC-PCB_ Units: mg/Kg
Prep Date: 1/10/2019
RunNo: 93274
Client ID: PBS
Batch ID: 35458
TestNo:
SW8082 SW3550C
Analysis Date: 1/10/2019
SegNo: 1902113
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Aroclor 1016
ND
0.00600
0
0
Aroclor 1260
ND
0.00600
0
0
Aroclor 1221
ND
0.00600
0
0
Aroclor 1232
ND
0.00600
0
0
Aroclor 1242
ND
0.00600
0
0
Aroclor 1248
ND
0.00600
0
0
Aroclor 1254
ND
0.00600
0
0
Total PCBs
ND
0.00600
0
0
Surr: DCB
35.2
33.40
105 10 165
Surr: TCMX
24.1
33.40
72.1 10 139
m
Sample ID LCS-35458
SampType: LCS
TestCode:
SVOC-PCB_ Units: mg/Kg
Prep Date: 1/10/2019
RunNo: 93274
;lient ID: LCSS
Batch ID: 35458
TestNo:
SW8082 SW3550C
Analysis Date: 1/10/2019
SegNo: 1902114
analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Aroclor 1016
0.140 0.00600
0.165
0 84.7
31.1
130
Aroclor 1260
0.174 0.00600
0.165
0 105
38.4
130
Total PCBs
0.314 0.00600
0.330
0 95.1
36
130
Surr: DCB
34.9
33.40
104
40.6
130
Surr: TCMX
23.9
33.40
71.5
28.2
130
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 15 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
m
Original

UMSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY Fri A OR
nsa
PN.4rl`Z014NIEWAL 7c m Bt C cb � ,.]t` Cuyahoga Falls, Ohio 44223
Anj.iydcaf L,aberrotarlos TEL: [phone] FAX.- [phone] WO#: 19010438
Website: htW:Ilwww.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 35458
Sample ID 19010442-001AMS
SampType: MS
TestCode:
SVOC-PCB_ Units: mg/Kg
Prep Date: 1/10/2019
RunNo: 93274
Client ID: Batch=
Batch ID: 35458
TestNo:
SW8082 SW3550C
Analysis Date: 1/1012019
SegNo: 1903335
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Aroclor 1016
0.931
0.898 0.988
0 94.2
1
165
Aroclor 1260
1.09
0.898 0.988
0 110
1
158
Total PCBs
2.02
0.898 1.98
0 102
1
153
Surr: DCB
120
200.0
59.9
11.9
124
Surr: TCMX
59.9
200.0
29.9
32.6
105 S
Sample ID 19010442-001AMSD
SampType: MSD
TestCode:
SVOC-PCB_ Units: mg/Kg
Prep Date: 1/10/2019
RunNo: 93274
Client ID: BatchQC
Batch ID: 35458
TestNo:
SW8082 SW3550C
Analysis Date: 1/10/2019
SegNo: 1903336
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Aroclor 1016
1.04
0.898 0.988
0 105
1
165 0.931
11.1
30
Aroclor 1260
1.19
0.898 0.988
0 120
1
158 1.09
8.87
30
Total PCBs
2.23
0.898 1.98
0 113
1
153 2.02
9.92
30
Surr: DCB
120
200.0
59.9
11.9
124
0
0
Surr: TCMX
79.8
200.0
39.9
32.6
105
0
0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 16 of 28
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY iWx'ORT
um M-i it 3310 Win St.
ENVIR4J4JM5NTALTZdIENOC2[ GMS,.iao Cuyahoga Falls, Ohio 44223
Are .tyl/ �I:L stat tiles TEL: [phone] FAX: [phone] WO#: 19010438
Website: hQ://www.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 35459
Sample ID MB-35459
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID: PBS
Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 1/10/2019
SegNo: 1903301
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
CLP Mercury
ND 0.00200
Sample ID LCS-35459
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID: LCSS
Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 1/10/2019
SegNo: 1903302
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00439 0.00200 0.00400 0 110 80 120
Sample ID 19010394-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID: BatchQC
Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 1/10/2019
SegNo: 1903305
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00445 0.00200 0.00400 0.0000500 110 75 125
Sample ID
19010394-001AMSD SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID:
BatchQC Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 1/10/2019
SegNo: 1903306
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00441 0.00200 0.00400 0.0000500 109 75 125 0.00445 0.903 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 17 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY iLui�ORT
3310 Win St.
ERVIltOUtolENTAL MCHN It i'� :i ,.ING Cuyahoga Falls, Ohio 44223
Aia.d'ytlt ai ioraTEL: [phone] FAX.• [phone]
WO#: 19010438
Website: http://www.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly Patch)m: 35459
Sample ID 19010394-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID: BatchQC
Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 1/10/2019
SegNo: 1903306
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 18 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY RiL JL ORT
Lwummllr 3310 Win St. �c
ENWIi OWAII':NTAL Ti:.MIN01.051 ;, 114C Cuyahoga Falls, Ohio 44223 WO#: 19010438
i1i7�1, [deg 1.L�1ar��rt�c�� TEL: [phone] FAX.- [phone]
Website: htW.-Ilwww.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 35523
2,4-D
ND
1.00 0.500
0 78.4
43.8
130
2,4,5-TP
ND
0.500 0.500
0 62.9
51.5
ill
Surr: DCAA
357
500.0
71.4
34.2
150
2,4-D ND 1.00 0 0 d
2,4,5-TP ND 0.500 0 0
Surr: DCAA 320 500.0 64.0 20 140
2,4-D
ND
1.00 0.500
0 100
37
105
W
2,4,5-TP
ND
0.500 0.500
0 89.8
38
106
W
Surr: DCAA
567
500.0
113
20
140
W
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 19 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC
SUMMARY
7�ZT T l)Ol�Z
it 3310 Win St. tQ S V 1�11V1AR i i`L i�
�ITihJPa1;ri1r�L cce�Wr4[�ta.�,, its' Cuyahoga Falls, Ohio 44223
Aia�zt';� 6cal' LabaraS00'es TEL: [phone] FAX.- [phone] WO#: 19010438
Website: hitp://www.settelc.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: 35523
Sample ID 19010307-001amsd
SampType: MSD
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
Client ID: BatchQC
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914646
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 83.7
37
105 0
0
30 W
2,4,5-TP
ND
0.500 0.500
0 71.5
38
106 0
0
30 W
Surr: DCAA
453
500.0
90.6
20
140
0
W
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 20 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. Q!�'� SUMMARY A 17 �T T. 1�07�'�'
LWumm-11 3310 Win St. 1. S7 V lrll- R i itL R
EN%(l120t•11o1r-MTAL E c�&N�°•1€7t Ch+�l��$, ;ttC. Cuyahoga Falls, Ohio 44223
�r+.tf [1:e�1' Lrrfacr�lc�tlns TEL: [phone] FAX.- [phone] WO#: 19010438
Website: hto:llwww.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchlD: R93258
Sample ID LCS-R93258
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@21.9C
Prep Date:
RunNo: 93258
Client ID: LCSW
Batch ID: R93258
TestNo: SW9045D
Analysis Date: 1/10/2019
SegNo: 1901827
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.7 90 110
Sample ID CHECK 7
SampType: LCS
TestCode:
pH_Oil(9045 Units: s.u.@21.9C
Prep Date:
RunNo: 93258
Client ID: LCSW
Batch ID: R93258
TestNo:
SW9045D
Analysis Date: 1/10/2019
SegNo: 1901844
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH 7.0 7.0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
0 100 90 110
J
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 21 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

g'i M Sunsmit Environmental Technologies, Inc.ILI, ', M". �� SUMMARY �i'®RT
3310 Win St.
t�14Pti�OtJPttsTL'cINe�t,cts, la Cuyahoga Falls, Ohio 44223
��,i`;,°tlel Ltriyrdast3t+�, TEL: [phone] FAX [phone] WO#: 19010438
Website: hQ.-Ilwww.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: R93297
Sample ID LCS-R93297
SampType: LCS
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: LCSS
Batch ID: R93297
TestNo:
SWI030
Analysis Date: 1/11/2019
SegNo: 1902691
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
7.240 0 112 70 130
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 22 of 28
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

+ Summit Environmental Technologies, Inc. QC SUMMARY Tt�-JL'®RT
frLD-Umm-lor 3310 Win St.
C�w4+I C5tJtdCt1T,4L �'�.Ctaii4l [sGI S, IpZG Cuyahoga Falls, Ohio 44223
Anrr }ytic,af L aborolo6es TEL: [phone] FAX.- [phone] WO#: 19010438
Website: httl2:llwww.settelc.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly Batchll): R93390
Sample ID 19010535-01AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunN-o: 93390
Client ID: Batch=
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906045
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 8.98 0.490 10.00 0 89.8 81.6 122
Sample ID
19010535-001AMSD SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
Client ID:
Batch= Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906046
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.09 0.495 10.00 0 90.9 81.6 122
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page.23 of 28
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc.M"Dum_ QC SUMMARY T��'ORT
Mw1mr, 3310 Win St.
Etgti7,U.tdh9�:17T�L1f3%1eL+rlra.11 Cuyahoga Falls, Ohio 44223 WO#: 19010438
�n.:lyL'�Lr�tadtd�e TEL: [phone] FAX.- [phone]
Website: hgp.•Ilwww.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: R.93390
Sample ID LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 93390
Client ID: LCSW
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906029
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive 9.57 0.490 10.00 0 95.7 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 24 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY %X ORT
Laummist 3310 Win St.
Eh^4+l TOIVAENTAL �—ECH OLOGIZS, WC Cuyahoga Falls, Ohio 44223 WO#: 19010438
Ar7tt.?y0caf-aboraisartr+� TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: R93465
Sample ID 19010535-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
Client ID: BatchQC
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908916
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4210 25.0 4800 0 87.7 80 120
Sample ID 19010535-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
Client ID: BatchQC
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908917
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4320 25.0 4800 0 90.0 80 120 4210 2.58 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 25 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY Kiu,20RT
ffJ:&UJVkM11t 3310 Win St.
PW112[ N&IENTAL T-ECTIN .Lco-,IE_5,-llae Cuyahoga Falls, Ohio 44223
Aj7ja y0cn.?.Labcrosari as TEL: [phone] FAX- [phone] WO#: 19010438
Website: http:llwww.settelc.com 21-Jan-19
Client: Synagro, NC 28134
Project: Mt Holly BatchID: R93465
Sample ID MB-R93465
SampType: MBLK
TestCode:
Sulfide,React Units: mg/L
Prep Date:
RunNo: 93465
Client ID: PBW
Batch ID: R93465
TestNo:
SW9034
Analysis Date: 1/14/2019
SegNo: 1908902
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
ND 25.0
Sample ID LCS-R93465
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 93465
Client ID: LCSW
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908903
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4620 25.0 4800 0 - 96.2 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 26 of 28
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

OC-QACOC338 Rev.4.1
Ellwlive Dote: I I/17U2018
ffq S U &I &%IV
Analysis Request / Chain of Custody
ENVIRONMENTAL TECHNOLOGIES, INC. Far Summit Environmental Technol
3210 YA. S '—' ogles, Inc, use only
oo�o VF11lio ON- 44223 Find us at; wwwsettek.eo>n
SET WO No.: ,,, III
L � 0 (ti i 2
Client Name E h PO
Pro]eMldenttMntton,my
y
f
65
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e a
„a IF�
d
= G
p°
a
a
M
rt
p
o
AnalytiestParemete]sandUMetfhodsJ
Client Address
Cricai rnone IReport
70 �-1 - 6 E - '13"11
ProjectAddress
W
f-
C
—
1
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3
U
a.
To
A Clam Bc mel l)
Cont i Person
({ e-, �'IEf.h
PO q
QuolaNamber
Cllcat li snn l Address
o-b rjgmQkAr0 . Lon1
PWS m
Facility ID
- i 70)
Sampled ffrfnlNameand ide Ibnotrrrc)
A440f
Reportlag/AteredltationRequlrement!
jOhloVAP Q OEPA Pb, Cu
Prinking Water Compliance
Other Complionce(List Slatdprogram):
For D W only, results have
o
by the Lb. If yes, lab tee may apply
ed to state
Y ❑ N
0
Sample PointTD
Sampietdentllleatian
Date
CelUded
Time
Collected
>M� Moil 20!qcy
R
ed by:
Date
Time
Received by:
Date
Time
Notes / Comments:
5�5
Was sutiicicsu vahone provided to run QC: YES / NO Cooler YES / NO Othcr,
p
ReF Temp: Ice: ES NO / melted
Received In Lab by:
late
Time
Carrier
Rush Requested: Day(s)
Must be approved by Lab Manager
Legend: PrestMlrves: I-13NO3, 2-I-g04, 3-}ICI, 4-Zinc Acetate, 5-NaOH, 6-EDA, 7-nonc, 8-other (spcci$od in comments) Refer to lab's terms and conditions at WWw.scitek.com
Pagel of 1:
Page 1 of 1
Page 27 of 28

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENIVIROtIMENTAL S[�9ttuc�I x�G�M�, iNC, Cuyahoga Falls, Ohio 44223 Sample Log -In Check List
AIJVtkrt/c:;l C°ab0ra10F16s TEL: [phone] FAX: [phone]
Website: htto://www.settek.com
Client Name: SYN-NC-28134 Work Order Number: 19010438 RcptNo: 1
Logged by: Rachel Thomas 1/9/2019 10:20:00 AM
Completed By: Christopher Livengood 1/9/2019 2:09:02 PM
Reviewed By: Jennifer Woolf 1/9/2019 6:10:34 PM
Chain of Custody
1. Is Chain of Custody complete? Yes No ❑ Not Present ❑
2. How was the sample delivered? UPS
Log In
3.
Coolers are present?
Yes
0
No
❑
NA ❑
4,
Shipping container/cooler in good condition?
Yes
❑d
No
❑
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present �/❑
No. Seal Date:
Signed By:
5.
Was an attempt made to cool the samples?
Yes
V
No
❑
NA ❑
6.
Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No
❑
NA ❑
7,
Sample(s) in proper container(s)?
Yes
0
No
❑
8,
Sufficient sample volume for indicated test(s)?
Yes
d❑
No
❑
g,
Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No
❑
10.
Was preservative added to bottles?
Yes
❑
No
❑
NA d❑
NA
11.
Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑
No VOA Vials d❑
12.
Were any sample containers received broken?
Yes
❑
No
d❑
13.
Does paperwork match bottle labels?
Yes
d❑
No
❑
(Note discrepancies on chain of custody)
14.
Are matrices correctly identified on Chain of Custody?
Yes
W
No
❑
15.
Is it clear what analyses were requested?
Yes
W
No
❑
16.
Were all holding times able to be met?
Yes
d❑
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17.
Was client notified of all discrepancies with this order?
Yes
❑
No
❑
NA d❑
Person Notified: �— Date r—
By Whom: p Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
I Temp °C
I Condition
Seal Intact
I Seal No
Seal Date
Signed B
1
15.5
1 Good
Not Present
Page 28 of 28

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: WQ0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 01/01/2019 To 03/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 31C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if annlienhle to alternative nerfnrmed Wlass A nr C'lass Rl emmnlete the fnllnwina mnnitnrina rinfn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 611
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221C
of total solids
CFU
61,671
88,049
316,336
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Mt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying— Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Doug Shoudt Division Manager Wastewater
Prepar me rtd Title (type or print)
nature reparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mt. Holly Biosolids
Project Number: 50-1301
Lot Number:UA03048
Date Completed:01/08/2019
.�;
01 /09/2019 10:51 AM
Approved and released by:
Lab Director - Greenville: Lucas Odom
P«R�
Ili
A V RB
ACCREDITED
`geORAro
—�—
oon DAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UA03048
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Geometric Mean
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

Client:Synagro Laboratory ID:UA03048-001
Description: Mt. Holly 1 of 4 Fecal Matrix: Solid
Date Sampled:01/03/2019 0815 % Solids: 1.55 01/03/2019 2342
Date Received:0110312019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/04/2019 2304 AMR 01/03/2019 2157
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <64433 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = DetectionLimit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
Daly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

Client:Synagro Laboratory ID:UA03048-002
Description: Mt. Holly 1 of 4 Fecal Matrix: Solid
Date Sampled:01/03/2019 0815 % Solids: 1.55 01/03/2019 2342
Date Received:01103/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/04/2019 2304 AMR 01/03/2019 2157
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <64725 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GG columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
Daly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Synagro Laboratory I D: UA03048-003
Description: Mt. Holly 1 of 4 Fecal Matrix: Solid
Date Sampled:01/03/2019 0815 % Solids: 1.59 01/03/2019 2342
)ate Received:01/03/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/04/2019 2304 AMR 01/03/2019 2157
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- <62869 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
Daly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Synagro Laboratory ID:UA03048-004
Description: Mt. Holly 1 of 4 Fecal Matrix: Solid
Date Sampled:01/03/2019 0815 % Solids: 1.58 01/03/2019 2342
Date Received:01103/2019
Inorganic non-metals
'un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/04/2019 2304 AMR 01/03/2019 2157
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <63239 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
'- — Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
105 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Synagro Laboratory ID:UA03048-005
Description: Mt. Holly 1 of 4 Fecal Matrix: Solid
Date Sampled:01/03/2019 0815 % Solids: 1.58 01/03/2019 2342
Date Received: 01 /03/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/04/2019 2304 AMR 01/03/2019 2157
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 126831 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
= Out of holding time W = Reported on wet weight basis
_.iealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 12

Client:Synagro Laboratory ID:UA03048-006
Description: Mt. Holly 1 of 4 Fecal Matrix: Solid
Date Sampled:01/03/2019 0815 % Solids: 1.58 01/03/2019 2342
Date Received: 01/03/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/04/2019 2304 AMR 01/03/2019 2157
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 316336
0
20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quanlilation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
= Out of holding time W = Reported on wet weight basis
_.:ealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8of12

Client:Synagro Laboratory ID:UA03048-007
Description: Mt. Holly 1 of 4 Fecal Matrix: Solid
Date Sampled:01/03/2019 0815 % Solids: 1.62 01/03/2019 2342
Date Received:01103/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/04/2019 2304 AMR 01/03/2019 2157
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <61671 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

Chain c: ,Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

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SHEALY ENVIRONMENTAL SERVICES, INC.
Sh:aly FRNIWnrilwal 3ccvlee4, In•.4 Pee I of t
Documtat Nurnbor. hAF.YJUI ipc:- 11 ELYceLI Ve i�ox &•�P?0 L's
Sample Receipt Checklist (SRQ
Client-_ l kr- Cwler Inspecicd byrdate; ip 1 � Lo> _ ��ti'�?
Means of eipt: FzSESI M �1 Client ❑ 4'PS ❑ FcdEx ❑ other_
❑ Yes
No I
I.'a1,= custody seats present on trae cooler?
rl Yes
Ea Ito r4
2. If custody scgls were prescLLt, were ffit-y intact, kind unbroken?
ti Strip ID; _-_ C31loritaa Strip ID; _ .__ "Tested by:
Origioul. to upon receipt +' Derived (Correvted) terlllaC iuru upon raccipt: %Solid Snap -.Cup ID:
{mperature
f'-i114t� -1 eail}rL'C81rarG )�Q 71: ❑ i TilnSt J Oit1PS IR C'ruai IJ�: �' IR Gun Cormctirm factor: j'C:'
-- --
h-Ictilodort"coclant; IT %IIau ❑ 1cePacks ❑ DrvIce+ El None
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3. If bemperuLure of jinn cooler exceeded 6.43C, was Nof ece Iwlaayage'r Nr[M'LG l^
Phf ivas; Notified by: phone.f email; + face-to-face (circie. one).
I❑II
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4. Is the countrenial cots jex,s p3ckbig slip ajjUG114d t4] this form? -
es
U Into
5. Were propQr custody procedures (rel nquishede'received) followed?
`r:s
❑ Na
6. Were sample IDs listed on the coc?
I,r. Yos
❑ No
17. 'Wert samp[o IDs listed on all sample containers?
es
n N- o
8. Wir; cellcction d:te. & time l.istgcl on the coc?
V-a
❑.No,
9. Was Collection dalu k. time listed on all sample contaitten?
k� s
❑ h'o
10. Did all container label illronriation (U), Llate, tine) a -6e wllh the C4C
yes
❑ No
11. Were tests to be pertplmt4 list ,, on the Co(:?
5 r Y es
❑ Nt�
12. Did all sarrgalcs alTivc in the proper eontaincls fbr each test ana-'or in }rood ce?nditiotl
(unbroken, lids on, etc.)?
Yes
❑ No
13. Was adequane sampic voltune avaitable?
cs
L� NT.
14. Were all samples received wiLI)irL V2 the hotding tirne or4it hours, whichever cr7Lr1Cs. Cirsl?
Yes
I � c,
15. Viicrc alu}-.swn Ie;.s containers missing'excess (eircl-ono) samples pq t listed D7 CSC"
Yes
:-1 No
2-NA
16- For VOA and RSI -115 sampin- wcr: babbles present >"pea -size'' (Vi"oC 6atlnl in tllart UfCr-) in
any of the VOA ,IaM
[] Yes
. No
NA
17, Wt= all mples received at a pH of < 2?
El 'Yes
❑ No
.
.........-..
18, %Vea a all cynnidc st nPIes receivM at s p"ai > 12 and su.Lri lt� sllmpks received. at V1-I -3 9?
0 Yes
r No
19. Were all app ica a 1 k1.j'TKMvyuTiidcrphvnnll625 (<0 Srn6E:) samples free r]IFrLnitltlsel
chlorine'?
❑ Yos
❑ No
[gyp,
20, W'cro client remarkVmquwt-s (Le. requested dilutions, NIS." ISD designations, etc...j'
currectly transcribed frpm the COC i11to th+; comment section ELI LINTS?
'las
Ve
21. IWI.5 tiic quotes numl]er lisLccl r)n the coattainer label? _Ifyes, Quote 4
Sample Preser nation (h f1I.4t he wilapl"atd for arty stlrnpic(s) incerreerly prrsc-rwed or with heudsplcc j
rEtP1eks) _- were received incomctlyllrzwaved andwer: adjtustcd accol-dingly
s,ampic rcoeiving vvidl rnL of circle oire:11-290 1, RN03, IICI, Na0H using SR 9
nle of pruscnration , if inure tharl onr; preservative i-5 Deeded, plena note hi lice comments 1,210 w.
were received wiib babbles ,6 min is attuncter,
tsJ _-.- -- were receiver] with TRC? 0.5 rtln}I. (If #19 is real) a»cf wa�a;
aGLCl'a iDol}` iq 5iS711}IUr CCl4ina14'lCilsodillm t111Osulft7BC (l�la2S O � WIt11 Silea1y ED_
Nimode labels zpplied by:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

p AM
PROM PT•ACCL.I RATE- RELIABLE
LABORATORIES., INC
www.P.XRLABS.CONI
r'.EPc1RT OF AN1-.1_•Y:-E:-
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER. HWY
PINEVILLE, NC 28134-
P30j' CT NAME: J Ai`1 19
DhTE: 'J2; i 3/19
SAMPLE NUMBER- 1 3,150 1 SAMPLE ID- CI'r'r ,_F i'fii'. HOLLY i OF' 4
DATE SAMPLED-
DATE RECEIVED- 01 /03/ 19 SAMPLER AB
TIME RECEIVED-" 1340 DELIVERED BY- AF",
Page 1 of 1
ANALYSIS
30 DAY BENCH SCALE TEST
SAMPLE MATRIX- SO
TIME SAMPLED- 0830
RECEIVED BY- DJ
TYPE SAMPLE- Grab
ANALYSIS
METHOD DATE 'TIME BY RESULT UNITS
VAR 01/n/19 1E;10 RE 3.39
LABORATOR`_ DIRECTOR
2217 Graham Park Drive • Charlotte. NC 28273
Phone: [phone] • Pax: [phone]

PA
PROM PT•ACCU RATE- RELIABLE
LABORATORIES INC
WWW.PARLASS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
CITY OF MT HOLLY 1 OF 4
134501
� s 01/31/19
Start: End:
TS ()
0.1625
0.1638
TS%
1.67%
1.63%
VS (
0.1275
0.1270
VS%
78.46%
77.53%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0130870
0.0126411
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0035925
0.0036629
FSVR Mass Balance)
3.44%
FSVR (Van Kleeck)
3.39%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] Fax: [phone]

PAR
PROMPT- ACCURATE• R ELIAS LE
LABORATORIES, INC
W W W.PARLABS.COM
Collected
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge Wt
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample Wt
+ Tare Wt (g)
Dried Sludge Wt (g)
Fixed Solids Wt (g)
Furnace Temp °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
30 Day Bench Scale Extended Aeration Test
vHK upuon 3, Percent volatile JOilas rceauctlon
SYNAGRO
m CITY OF MT HOLLY 1 OF 4
134501
a 01/03/19
0 0 01/31/19
As Received Day 0 Day 7 Day 14 Day 21 Day 28
nafnarlq n41na11q n111n11q n1/17119 M/24/19 01131119
.;F
4.68
5.10
5.93
6.11
6.69
X29
X29
X31
X32
X2
X7
20.1060
20.1060
22.1002
24.4284
25.0654
19.2827
29.8485
29.8485
31.8701
34.3355
35.1293
29.3293
9.7425
9.7425
9.7699
9.9071
10.0639
10.0466
106
106
106
105
106
106
01/03/19 16:00
01/03/19 16:00
01/10/19 09:30
01/17/19 08:50
01/24/19 10:00
01/31/19 11:20
01/04/19 14:50
01/04/19 14:50
01/11/19 10:00
01/18/19 09:10
01/25/19 10:00
02/01/19 11:00
20.2685
20.2685
22.2626
24.5940
25.2325
19.4465
0.1625
0.1625
0.1624
0.1656
0.1671
0.1638
_
0.0350
0.0361
0.0370
0.0374
0.0368
550
550
550
550
550
01/04/19 16:30
01/11/19 13:40
01/18/19 12:30
01/25/19 12:15
02/01/19 14:00
01/04/19 17:20
01/11/19 14:45
01/18/19 13:50
01/25/19 13:10
02/01/19 15:05
20.1410
22.1363
24.4654
25.1028
19.3195
0.1275
0.1263
0.1286
0.1297
0.1270
1.67%
1.67%
1.66%
1.67%
1.66%
1.63%
78.46%
77.77%
77.66%
77.62%
77.53%
yf Mass Fraction of Volatile Solids in Liquid (Feed)
yb Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at Start of Test
0.0130870
Sludge at End of rest
0.0126411
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
Xb Mass Fraction of Fixed Solids in Liquid (Bottom)
at Start of Test
0.0035925
Sludge at End of Test
0.0036629
TS ()
0.1625
TS ()
0.1638
VS (g)
0.1275
VS (g)
1 0.127
Volatile Fraction In: 0.46982
P.O. Box 411483 o Charlotte, NC 28241-1483
Phone: [phone] • Fax:[phone]
Volatile Fraction Out: 1 0.47564

PAR CHAIN OF CUSTODY
LA6oRATORIES,INC. PAR Laboratories, Inc
Phone [phone]
www.pariabs.com Fax [phone]
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North
('-- i. rlena —f nF C—i--m I.I —H Mn1,—I Racni—
Company Name (billing)
Comments/ Special Instructions
Clarifier Effluent provided in the event that
SYNAGRO CENTRAL
Address
the sample needs to be reduced to below
12701 LANCASTER HWY
2% solids..
City, State rx zip code
PINEVILLE NC 28134
Point of Contact t3 Telephone Number
ADAM BRIGMAN 704-650-4341
Sample
Taken By: SIGNATURE / C PRINTED NAME Ala Q< r-'Gm�,r
ARE SAMPLES FOR STATE or EPAREPORTINNG? YES NO
*Sample Type: DW WW GWMW HW Soil other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
**Field Preserved: Yes 'Ao 4/Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN):
Client Sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Daterrime
Collection
DateMme
Analyses
Requested
�-1 a l' so FO,
t/
13� 9 �:30
30 �%./ Oe,17 7? � Q�
Ketln Ua[er I Ime RCI:eIVCO y vafcr r uuc
/</ vI03'� 3 d
Res d by: DateMme Received by: DateMme
li i
C=Composite G=Grab DW=-Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: WQ0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 04/01/2019 To 06/30/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying ' Composting Aerobic Digestion
Anaerobic Digestion
If Anniienhi P. to alternative nerfnrm Pd Wince A nr ('lace R) rum nla4a *h. fnllm.,— —4-- — .7..4—
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6th
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221 C
of total solids
CFU
72,005
97,746
146,103
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
Doug Shoudt Division Manager Wastewater
Prepar a e and Title (type or rint)
i
Signa re of reparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mt. Holly
Project Number: 50-1701
Lot Number:UD30045
Date Completed:05/07/2019
05/07/2019 4:23 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
PC
ARAB
`e0RAS0
ACCREDITED
oo—�—
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UD30045
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Geometric Mean
97,746
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

Client:Synagro Laboratory ID:UD30045-001
Description: Mt. Holly 2 of 4 Fecal Matrix: Solid
Date Sampled:04/30/2019 0730 % Solids: 1.38 05/01/2019 0118
Date Received:04130/2019
Inorganic non-metals
tun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 05/01/2019 2330 MDD 04/30/2019 1954
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 145180 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
mly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

Client: Synagro Laboratory ID: UD30045-002
Description: Mt. Holly 2 of 4 Fecal Matrix: Solid
Date Sampled:04/30/2019 0730 % Solids: 1.39 05/01/2019 0118
Date Received:04/3012019
Inorganic non-metals
tun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 05/01/2019 2330 MDD 04/30/2019 1954
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <72005 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
: Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Synagro Laboratory I D: UD30045-003
Description: Mt. Holly 2 of 4 Fecal Matrix: Solid
Date Sampled:04/30/2019 0730 % Solids: 1.37 05/01/2019 0118
Date Received:04/30/2019
Inorganic non-metals
;un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 05/01/2019 2330 MDD 04/30/2019 1954
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 73105 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
: Out of holding time W = Reported on wet weight basis
saly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Synagro Laboratory ID:UD30045-004
Description: Mt. Holly 2 of 4 Fecal Matrix: Solid
Date Sampled:04/30/2019 0730 % Solids: 1.37 05/01/2019 0118
Date Received:04/30/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 05/01/2019 2330 MDD 04/30/2019 1954
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 146103 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
?aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Synagro Laboratory ID:UD30045-005
Description: Mt. Holly 2 of 4 Fecal Matrix: Solid
Date Sampled:04/30/2019 0730 % Solids: 1.36 05/01/2019 0118
Date Received:0413012019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 05/01/2019 2330 MDD 04/30/2019 1954
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 73314 20 col/g 1
LOQ = Limit of Quantitation 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
!aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7of12

Client:Synagro Laboratory ID: UD30045-006
Description: Mt. Holly 2 of 4 Fecal Matrix: Solid
Date Sampled:04/30/2019 0730 % Solids: 1.38 05/01/2019 0118
Date Received:04/30/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 05/01/2019 2330 MDD 04/30/2019 1954
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 72727 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 12

Client: Synagro Laboratory ID: UD30045-007
Description: Mt. Holly 2 of 4 Fecal Matrix: Solid
Date Sampled:04/30/2019 0730 % Solids: 1.40 05/01/2019 0118
Date Received:04130/2019
Inorganic non-metals
tun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 05/01/2019 2330 MDD 04/30/2019 1954
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 143195 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
= Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

Chain i Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

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SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Envif n.11c11r81 szrACc$ lnc". 1':CgU I Or L
Do:.umcmt Numtcr w11;DO I BC-.4 C;i:cctivc Tait : 8P2o201 S
Sample Receipt checklist (SR
Cliem: SYNAGRO Cooler hispectEA byldate: LKH / 04-3020l9 Lot ir: UD30045
Mcarts ofrcccipt: `,j SESI 0 Client E] UPS ❑ FcdEx ® Other:
❑ ye"4
0 NO
I
11. Were custody seals present on the cooleO
Yes
Np
0 NA
12, If csustody suaal3 were prusuni, weru LhLy intact and unbrok n?
pH Strip ID: NA Chlorilic Strip ID; NA Tested 1ry: NA
OTi heal temperacilr� upon l9a eiPt+' Deri.ye�3 (Correure;t) lemp:a�rture 1ljt7ra receipt %Solid Snap -Cup ID: 19-61 L
3,6 t3,61 =C NA INA c NA ; NA 'C Nil ;NA °C
Method: jITemperature Blank []Agains" Botdes 1R (hurl iD- a I.R Cur+ Cormclian ra tor: 0' =C
[ letliod of coolant: 0 Wet lee 0 Ice Packs El Dry Mt; ® Naiie
_._
❑
if temneratllrr: arany C04.11er vw.P Rvd 6A°C, was Prnicct Manngcr 'Notified?
PIVI vas Notified b}r_ phone.+'email,+face-ta-facel'circ_leanel.
❑ Ycs
0 No
O NA
4. is the cammnicrcial courier's packing slip attached to hits for1117
Yes
❑ Nu
5_ Were proper custody prmvdulr frefinaltiislleu`reCeivcd} Iblluwt d?
I71 Yes
No
6. Wetc sample 1Ds listed on the COC?
® Ycsj
❑ No
7. Wert�sornplu ID3i Lisicd on all samptocontaincr3?
0 Yes
❑ Nn
S. Was collection date & time listed on the CQC?
® Yes
❑ No
9. Wus collection date & time listed on all sample containers?
® Y6.5
El 'No
10. Did all writaiour label informti Jur; (1D, date, lime) a with the COC?
Yes
D No
11, we[%e tent., to lie 1lerfnriried listed nri tha CAC:?
� Yes
®Na
12, Did all samples arrive in the proper containem for each Le,t UFLdi >r in gosul condilion
(unbroken, lids on, etc.)?
r ® Yes
❑ No
13. was adequate sample volume availab] c?
9 Yes
Q No
1-1. Wore all samplers receiver) within Vi the holding (illle or 49 hours. tvhidic!yer comes first)
❑ Yes
No
P5. Wgle any samples eonminets rnis9in&xcess (circle. ant~) samples Not Usled on COC?
® Yei!
® NO
0 NA lin
16. Fcm VOA nn,I RSh-175 sa.mplcs, �Arrc. Bubbles present }"pea -size" ('•d*'or fimm in diai�ictcr)
aLnyofdie VDA vkAs"
® Yes
No
ONTA
17_ Were all ata p Ot'<22
❑ fires
0 No
® NA
;IS- Weie all cyanide swipk:; mct:ivc(J tit a pHl 3 124 and sulfide gamplec received at a 1,11 _} 9"
❑ YesNn
®�A
19. ))Were ail applicableNf%;, TKN1cyanide�pheno1!625 (<:0.5mtr}I.) s;impls_s fray? of residual
Chlorine?
1:1 es
No
®NA
2f)- Were client mnarksarequestsfi.e. requested dilutions, WSAISD itesignalious, etc:..,}
correctly transcribed from the COC into the curnment section in LiMS7
❑
Yr
No
? I, NVas he quote number listed on the container labol? If vcs Qaotc ' NA
Sample )?'reservation (i w5t be complotael for any salliple(s) incorrectly paesertoa or %vitl'i ficu lspam.)
Sampic(s) NL A were received hicorrectly Imserved ar d wur a pLl3'eCd 8CC�71'dCn�IV
in sarnplo mocjving with NA mL of c jicle olte: W/.SO4, HN'03, HCI, NaOH usinG Slt # NA
isle cif presorvtlliUrr NA If more than one preserw.ive. is needed. please note in the cam.-nent5 help►+-,
Sample(S) NA _ were rrccivL 1 with bubbJes >6 tarn in diameter,
Samples(s) NA 1vare received ►vith TRC - 0.5 rnEjL (if in 9 is na) and wee m
atlJusted acoxdhigly in sample mewing willL sodium thiasulfate with Shealy 1D; NA
SR harcodc labels applied by: JSH Dam_ 04-10-2019
Comments,
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

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PROM PT•ACCU RATE -RELIABLE
LABORATORIES, INC
WWW.1'A Rt.ABS.00i1,1
REPORT OF ANALYSES
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 2$134-
PROJECT NAME: APR 19
DATE: 06/07/19
SAMPLE NUMBER- 135690 SAMPLE ID- MT HOLLY 30 DAYBENCH SAMPLE MATRIX- SO
DATE SAMPLED- 04/30/19
DATE RECEIVED- 04/30/19 SAMPLER- AB RECEIVED BY- RE
TIME RECEIVED- 1006 DELIVERED BY- AB TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 04/30/19 1310 RE 1.08 %
LABORATORY DIRECTOR
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fax: [phone]

PA&R
PROM PT -ACCURATE- RELIABLE
LABORATORIES, INC
WWW. PARLAE3S. COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
MOUNT HOLLY
135690
o • 04/30/19
Start: End:
TS
0.1387
0.1479
TS%
1.43%
1.44%
VS ()
0.1062
0.1112
VS%
76.57%
75.19%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0109482
0.0108289
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0033504
0.0035739
FSVR Mass Balance
1.08%
FSVR Van Kleeck)
1.08%
FSVR Mass Balance <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1433
Phone:[phone] • Fax: [phone]
I

PLkR
PROMPT • ACCURATE- RELIABLE
LABORATORIES, INC
W W W.PARLABS.COM
30 Day Bench Scale Extended Aeration Test
VAN upuon 3, l-ercem voiame aoiias Keaucuon
SYNAGRO
® MOUNT HOLLY
135690
04/30/19
a 05/28/19
As Received Day 0 Day 7 Day 14 Day 21 Day 28
Collected 04/30/19 04/30/19 05/07/19 05/14/19 05/21/19 05/28/19
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge W1
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample Wt
+ Tare Wt (g)
Dried Sludge-Wt (g)
Fixed Solids Wt (g)
Furnace Temp °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
4.38
4.60
4.81
5.07
5.36
X10
X10
X15
X31
X13
X11
22.7074
22.7074
23.1830
.20.1017
21.8732
21.0376
32.4076
32.4076
33.5650
32.4876
32.2210
31.3064
9.7002
9.7002
10.3820
12.3859
10.3478
10.2688
105
105
106
105
106
106
04/30/19. 13:10
04/30/19 13:10
05/07/19 10:00
05/14/19 09:40
05/21/19 10:00
05/28/19 09:00
05/01/19 13:05
05/01/19 13:05
05/08/19 10:10
05/15/19 09:50
05/22/19 10:15
05/29/19 09:15
22.8461
22.8461
23.3304
20.2788
22.0191
21.1855
0.1387
0.1387
0.1474
0,1771
0.1459
0.1479
0.0325
0.0353
0.0428
0.0355
0.0367
550
550
550
550
550
05/01/19 15:55
05/08/19 13:50
05/15/19 13:40
05/22/19 14:00
05/29/19 12:50
05/01/19 17:00
05/08/19 14:10
05/15/19 14:50
05/22/19 15:10
05/29/19 13:05
22.7399
23.2183
20.1445
21.9087
21.0743
0.1062
0.1121
0.1343
0.1104
0.1112
1.43%
1.43%
1.42%
1.43% 1
1.41% 1
1.44%
76.57%
76.05%
75.83%
75.67%
75.19%
yf Mass Fraction of Volatile Solids in Liquid (Feed)
yb Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at Start of Test
0.0109482
Sludge at End of Test
0.0108289
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
Xb Mass Fraction of Fixed Solids in Liquid (Bottom)
at Stan of Test
0.0033504
Sludge at End of Test
0.0035739
TS (9).0.1387
TS (
0.1479
- VS ()
1 0.1062
VS ()
1 0,1112
Volatile Fraction In: 0.53545 Volatile Fraction Out: 0.52215
P.O. Box 411483 • Chulotte, NC 28241.1483
Phone: [phone] Fax:[phone]

L
R
LABORATORIES.
. INC.
www.pariabs.com
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax (704) -588-8335
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North
CMrnli— rinnnrf—nf of P—immmantni and Nnhi-I P—ir—
Company Name (billing)
Comments/ Special Instructions
Clarifier Effluent provided in the event that
SYNAGRO CENTRAL
Address
the sample needs to be reduced to below
12701 LANCASTER HWY
2% solids.
City, State Ft zip code
PINEVILLE NC 28134
Point of Contact li Telephone Number
ADAM BRIGMAN 704-650-4341
Sample
Taken By: SIGNATURE
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES _VNO
'Sample Type: DW vVW _l GWMW HW soil Other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No ✓Teflon Liner/Zero Headspace: Yes _No _ n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (Y/N):
Client Sample I.D.
Sample Location ! Number)
Comp
Grab
Preserv.
Set Up
Dateffime
Collection
Daterrime
Analyses
Requested
All , f -(o 0(1 30 OCA &-Pic h
✓
y �0//9
�0 �� s� I �1�1�t Sc��e
Relinquished b uate/ l Ime Keceivea p . .r,_;- water i lme
qbo'd6
RelinquiSAW I Date Ime Received by: Daterrime
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: WQ0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 07/01/2019 To 09/30/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlienhle to alternative nerfnrmed (Class A nr Class R) rmmnlete the fnllnwina mnnitnrinv dntac
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 61h
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221 C
of total solids
CFU
57,767
58,874
62,520
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives
were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Doug Shoudt Division Manager Wastewater
Prepar a e and Ti (type or print)
i
v
Si ature o reparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: City of Mt. Holly
Project Number: 50-1301
Lot Number:UG10023
Date Completed:07/18/2019
07/18/2019 3:28 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
2� pCCff�c�' O
A
ACCREDITED
�9e0R,---IDODELAP--
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UG10023
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Geometric Mean
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

Client:Synagro Laboratory ID: UG10023-001
Description: 3 of 4 Fecal Mt Holly Matrix: Solid
Date Sampled:07/10/2019 0810 % Solids: 1.60 07/11/2019 0054
Date Received:07/10/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/12/2019 0110 MDD 07/10/2019 2121
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <62520 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
Daly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

Client: Synagro Laboratory ID: UG10023-002
Description: 3 of 4 Fecal Mt Holly Matrix: Solid
Date Sampled:07/10/2019 0810 % Solids: 1.71 07/11/2019 0054
Date Received:07/1012019
Inorganic non-metals
tun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/12/2019 0110 MDD 07/10/2019 2121
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <58394 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Synagro Laboratory ID: UG10023-003
Description: 3 of 4 Fecal Mt Holly Matrix: Solid
Date Sampled:07/10/2019 0810 % Solids: 1.72 07/11/2019 0054
Date Received:0711012019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/12/2019 0110 MDD 07/10/2019 2121
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <57984 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Synagro Laboratory ID: UG10023-004
Description: 3 of 4 Fecal Mt Holly Matrix: Solid
Date Sampled:07/10/2019 0810 % Solids: 1.71 07/11/2019 0054
Date Received:07110/2019
Inorganic non-metals
Win Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/12/2019 0110 MDD 07/10/2019 2121
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <58620 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Synagro Laboratory ID: UG10023-005
Description: 3 of 4 Fecal Mt Holly Matrix: Solid
Date Sampled:07/10/2019 0810 % Solids: 1.70 07/11/2019 0054
Date Received:07110/2019
Inorganic non-metals
;un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/12/2019 0110 MDD 07/10/2019 2121
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <58734
20 col/g 1
LOCI = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
!aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 12

Client: Synagro Laboratory ID: UG10023-006
Description: 3 of 4 Fecal Mt Holly Matrix: Solid
Date Sampled:07/10/2019 0810 % Solids: 1.72 07/11/2019 0054
Date Received:07110/2019
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/12/2019 0110 MDD 07/10/2019 2121
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <58234
20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 12

Client:Synagro Laboratory ID:UG10023-007
Description: 3 of 4 Fecal Mt Holly Matrix: Solid
Date Sampled:07/10/2019 0810 % Solids: 1.73 07/11/2019 0054
Date Received:07/1012019
Inorganic non-metals
tun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/12/2019 0110 MDD 07/10/2019 2121
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- <57767 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9of12

Chain i Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

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SHEALY ENVIRONMENTAL SERVICES, INC.
Sheulr Fnvlronlro=:l I Ssrn:ca, ji�a
DocumaTA NimUkT_ riGOpIAC-F-
i Ps�r. I •�i' I
rrroctiLnn IL: N")jiDIS
Saimple Receipt Checklist (SRC5
t;l3ert: ynas;ro Coiner ln5 ected by,datc: LTD i 7110119 Lot tom: LICsIOD?;
MuHns nfreceipt, SESI ❑ Client Q UPS 0 laedF.x Q Othtr; —
Yes Nn t_ Wcna custody seals present. on the cooky?
Yes r10 f4rA 2_ If etrstadv seals were pt-esea4 w'cre t[leY intact and urlbrnkell7
H Strip [D: ttiA Chlorine Strip 1173; NA TmCd by:7tiA
101ij-,Inal temperature ❑por receipt J D;rived (Cnmcud) temperature upnn receipt %Solid Snap-t71tp ID; 19-1020
17 �`a.7 IC NA 'o'NA °C NA DNA oC 14A ,NA :{
14?eC6od: J Tempiranu Blank ®A ainst f Ottles ift tiun ID, 6 _ Ik c Jan Correction Factor: 0 :]c i
twiethni of coolcut1: ® 'et Ice ❑ [rzu I'aam Q Dr.. Iti-- El None
❑ Yes ❑ o . It temperanire of:tny cooler excccded 6.01C. was Proiect. hlana;er lwot[tied? '
I'M was T�otified by: phone 1 etreo-iil face-t(,-fagc (circle Ono).
❑ Yes Q Na d\lA q. is lhuminmercial c.ollder's pl;cking.slip attached to [his form?
Ye, +y ry
No S. Were a proper cu.,Iody procedures (ralin.luishedh-recived) fol lowed`i
Yes 7~Tir 6,Jerc sample if].s listed un tits CQC? i
® y; Q N4r 7. Were santiple IDy listed on all sample enntainees? I
i YM 'WL."; eollectian date & tir[1e l istcd on the C OC?
Y Nn 9. ' as collection rlate Ac rime listed tIn Hil samP[e wlntainerw?
YUS Q iJo 10_ Did all co,tlaincr laher information (11), date, time) aegr•ee ,With the COC°
® Y651 Q No 11. Wurc tests ro L,c ero�rrmcc[ lisred nn the L'QC ; —
Yes Ll n 12. Did rll samples urivc in the. Propea• curanincrs fet' each test mza('ar in t:r(f ronditiart
(unhalkcn, lids on, etc.)?
®Yas EI No 13. V�'a ; adn�uaie samp le vL`Iurnc avaiJalb[o?
Yes ❑ No 14. Wer,e,,,ll sainplesreceivail s.•ithin'r'a the. holriing tulle or43 hours, uvhichcuercomas first?!
Yes No IS. Were any ma—'— enntainers n�issiar� taccss (circJt• orle) sarnocs Not listed on CC)(}?
® Yes Q lti°v O NA 16. T'orV0A and RSK-]?.5 samples; wope bubbles prefiurtt'},pea-siz-0" ('r'W%ar 6mni in (fiainct; )
in 2TlY of the VOA; vials?
® Yes El Na N—A 17. tiWere kill 131104accals4lulrimit 5111e to received ata pH L)F--2?
Q Yes �NL 0 ®N.q 1 s. ti4'erc all cyanide samples received nt a l-1 :: 12 and sWftdc samples received nt a Id > 9?
0 Yes MNo [DNA Iy We're all ap�,lical,le. H,TI{jyfclratSidr�`[,lienolr'ti'?5 {�� 0.5m'WLi salnfiles Urce ofresi ul
chlorine?
Yes [] hie ] NA 20. tVere client rctm:Rrksrreque5ts (i.e. mquested dilution.g, h4S+[�9SD tlrsignadens, etc...) '
correctly trail wribcd ti'o:tr the CDC into the comment section in LFINIS7
Q Yes NO 3 J . 'Jr'as titre note awnbcr listed ca the conlniner label? If ties, Quote # NA
ir¢ple Pt-eatiation (Must be completed for any sample(,;) incorrer;lly preservesi (jr witli ttc•adspsceQ
Sarnplr (s) 1`dfi. were received incormctly pr+escrvied atttd were aijusrW acco;clin ' y
in samplo receiving -.with NA ML of circle one; 112SO4, H O:-'P, HC'J, NaOEJ usiiro SKr NA Titrtn of trae,ervation h[!t If moit Ihnn one preservative is needed, Please notr in the comments_ below,
i
Sample(,) HA ware e�x Ned with blffblus>6 mm in diameter.
Satttp:esj ac 1�1A were received with `Fit s -x 0.5 mkjl. (If t 19 is ►to j and avr-m
justetl accotYlinglp• in sample receiving.witb sodiurtl thic�ullaW(N-,L2320D'-With ShCaly ID_ NA _
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Cnm Wiest ls;
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

PLI
PRO MPT- ACCU RATE- RELIABLE
LAB 0P-A'r0P,IES.7 INC
WW%V.PARLABS.00M
REPORT OF ANALYSES
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER HWY
PINEVTLLE, NC 28134-
PROJECT NAME: JUL 19
DATE: 08/30/19
SAMPLE NUMBER- 136518 SAMPLE !D- HOLLY "I OF 4
DATE SAMPLED- 07/17/19
DATE RECEIVED- 0'7/18/19 SAMPLER- AB
TIME RECEIVED- 0845 DELIVERED BY- AB
Page I of 1
ANALYSIS
30 DAY BENCH SCALE TEST
A N A T,'--'S 1 S
MIE 11-10D DATE TIME BY
SAMPLE MATRIX- SO
TIME SAMPLED- 1000
RECEIVED BY- RE
TYPE SAMPLE- Grab
RESULT UNITS
VAR 07/18/19 RE 3.87 %-
T,ASOR.7,'rORY D T R "-CTC','R
2217 Graham Park Drive - Charlotte, NC 28273
Phone: [phone] - Fax: [phone]

PLLF;Z
PROM PT•ACCU RATE• RELI A BLE
LABORATORIES, INC
WWW.PARLASS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
MT HOLLY 3 OF 4
136518
• 07/18/19
r � • 08/15/19
Start: End:
TS ()
0.1849
0.1854
TS%
1.92%
1.91 %
VS )
0.1414
0.1370
VS%
76.47%
73.89%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0146819
0.0141100
x Mass Fraction of Fixed Solids in Liquid Sludge
0.00451671
0.0049849
FSVR (Mass Balance)
3.91 %
FSVR Van Kleeck
3.87%
FSVR Mass Balance <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: (704) S88-8333 0 Fax: [phone]

PAR
PROMPT' ACCURATE- RELIABLE
LABORATORIES,
INC
W W W. PARLABS.COM
30 Day Bench Scale Extended Aeration Test
VAR Ontinn 3 Percant Volatile Snlids Reduction
CLIENT NAME: ' •
SAMPLE 10 _ IVIT HOLLYOF 4
START DATE*
LEND D6TE:
As Received Day 0 Day 7 Day 14 Day 21 Day 28
Collected 07/18/19 07118119 07126/19 08/01/19 08108119 08/15119
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge Wt
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample Wt
+ Tare Wt (g)
Dried Sludge Wt (g)
Fixed Solids Wt (g)
Furnace Temp °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
2.18
3.34
3.57
3.72
4.30
X23
X23
X29
X27
X5
X14
21.9000
21.9000
20.1068
17.4229
20.5168
20.9054
31.5309
31.5309
30.5067
27.0493
30.3203
30.6148
9.6309
9.6309
10.3999
9.6264
9.8035
9.7094
106
106
107
105
106
106
07/18/19 10:50
07/18/19 10:50
07/25/19 09:15
08/01/19 10:00
08/08/19 08:50
08/15/19 08:45
07/19/19 11:00
07/19/19 11:00
07/26/19 09:00
08/02/19 09:45
08/09/19 09:00
08/16/19 09:10
22.0849
22.0849
20.3034
17.6068
20.7040
21.0908
0.1849
0.1849
0.1966
0.1839
0.1872
0.1854
0.0435
0.0478
0.0449
0.0468
0.0484
550
550
550
550
550
07/19/19 16:10
07/26/19 14:50
08/02/19 13:45
08/09/19 14:00
08/16/19 14:20
07/19/19 17:05
07/26/19 16:00
08/02/19 14:50
08/09/19 15:05
08/16/19 15:30
21.9435
20.1546
17.4678
20.5636
20.9538
0.1414
0.1488
0.1390
0.1404
0.1370
1.92%
1.92%
1.89%
1.91%
1.91%
1.91%
76.47%
75.69%
75.58%
75.00%
73.89%
yf Mass Fraction of Volatile Solids in Liquid (Feed)
yb Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at Start of Test
0.0146819
Sludge at End of Test
0.0141100
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
Xb Mass Fraction of Fixed Solids in Liquid (Bottom)
at Start of Test
0.0045167
Sludge at End of Test
0.0049849
TS ()
0.1849
TS ()
0.1854
VS ()
0.1414
VS ()
1 0.137
Volatile Fraction In: 0.39828 Volatile Fraction Out: 0.38686
P.O. Box 411483 • Charlotte. NC 28241-1483
Phone: [phone] Fax: [phone]

q
CHAIN ®F CUSTODY
ATORIES.INC.
L
PAR Laboratories, Inc
Phone [phone]
www.parlabs.com
Fax [phone]
Shipping:
Mailing:
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28273
Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North
Carolina Department of Environmental and Natural Resources.
C N b'II.-
ompany ame (t tng) Comments/ Special Instructions
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State It zip code
PINEVILLE NC 28134
Point of Contact t-s Telephone Number
ADAM BRIGMAN 704-650-4341
Sample
Taken By: SIGNATURE --
Clarifier Effluent provided in the event that
the sample needs to be reduced to below
2% solids.
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTINCy? YES 1/ NO
"Sample Type: DW WW GWMW HW Soil Other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
Client Sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date/Time
Collection
Date/Time
Analyses
Requested
/%'li, I le lj� 3aFN 30 Gat 9&0
Vtv;�
7ly
�o Cyy
r�cuuyuiancu u uarel l lrne by: Dated" e
71.tte etlE IN - �� 07 r-�) f) �
Relinquishe y DateTme Received by: Da e/Time
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

6
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly
WQ Permit Number: WQ0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 010/01/2019 To 12/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A•
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative per (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
- --- - -
Parameter
- -
Allowable Level in Sludge
— a1 " GUiu .- hue lUllUW1R momrorin
Pathogen Density
aara:
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61h
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221C
of total solids
X..
CFU
53,014
60,122
109,836
CFU/g
0
Quarterly
Grab
SM9222D
1900 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
e
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107)
- Please indicate option/alternative performed:
0ption/Alt. 1
(VS reduction)
Option/Mt. 2
(40-day bench)
Option/Alt. 3 Option/Mt. 4
(30-day bench) X (Spec. 02 uptake)
Option.Wt. 5
(14-Day Aerobic)
Option/Mt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Doug Shoudt Division Manager Wastewater
Prepar ame and Title (type or print) Land Applier Name and Title (if applicable) (type or print)
.0
Signature o reparer* Date Signature of Land Applier (if applicable)
*Prep4eris• ea. fia%0,CFR Part 503.9(r) and 15ANCAC 2T.1102 (26)
Date

'_J _ * �I �•, i � )-'A dJ . L! !— Ar 'tea .
Synalglro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Mt Holly 50-1701
Project Number: 50-1701
Lot Number:UJ09071
Date Completed:10/11/2019
10/16/2019 2:54 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
�pCCRE���A
AMAB
:#.
C4BORA'[
ACCREDITED
DOD VAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 13

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Loft Number: UJ09071
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary "
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Geometric Mean
60,122
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 13

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Synagro
Lot Number: UJ09071
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
4 of 4 Fecal
Solid
10/09/2019 0900
10/09/2019
002
4 of 4 Fecal
Solid
10/09/2019 0900
10/09/2019
003
4 of 4 Fecal
Solid
10/09/2019 0900
10/09/2019
004
4 of 4 Fecal
Solid
10/09/2019 0900
10/09/2019
005
4 of 4 Fecal
Solid
10/09/2019 0900
10/09/2019
006
4 of 4 Fecal
Solid
10/09/2019 0900
10/09/2019
007
4 of 4 Fecal
Solid
10/09/2019 0900
10/09/2019
(7 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 13

Inorganic non-metals
Client:Synagro Laboratory ID: UJ09071-001
Description: 4 of 4 Fecal Matrix: Solid
Date Sampled:10/09/2019 0900 % Solids: 1.83 10/10/2019 0042
Date Received:10/09/2019
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 10/10/2019 2051 AMR 10/09/2019 2103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- <54600 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 13

Inorganic non-metals
Client:Synagro Laboratory ID:UJ09071-002
Description: 4 of 4 Fecal Matrix: Solid
ite Sampled:1010912019 0900 % Solids: 1.81 10/10/2019 0042
e Received:1010912019
in Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 10/10/2019 2051 AMR 10/09/2019 2103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 55203 20 col/g 1
wu = Limit of Uuantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
it of holding time W = Reported on wet weight basis
, y Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 13

Inorganic non-metals
Client:Synagro Laboratory ID: UJ09071-003
Description: 4 of 4 Fecal Matrix: Solid
Date Sampled:10109/2019 0900 % Solids: 1.87 10/10/2019 0042
-,te Received:10109/2019
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 10/10/2019 2051 AMR 10/09/2019 2103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- <53573 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
_..__., ...... ...... ...... _-...-- ..._.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 13

Inorganic non-metals
Client:Synagro Laboratory ID: UJ09071-004
Description: 4 of 4 Fecal Matrix: Solid
Date Sampled:10/09/2019 0900 % Solids: 1.89 10/10/2019 0042
)ate Received:1010912019
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 10/10/2019 2051 AMR 10/09/2019 2103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- <53014 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
" - Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
i ub Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 13

Inorganic non-metals
Client:Synagro Laboratory ID:UJ09071-005
Description: 4 of 4 Fecal Matrix: Solid
ate Sampled:10/09/2019 0900 % Solids: 1.82 10/10/2019 0042
ite Received:1010912019
in Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 10/10/2019 2051 AMR 10/09/2019 2103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 109836 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Jut of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 13

Inorganic non-metals
Client:Synagro Laboratory ID: UJO9071-006
Description: 4 of 4 Fecal Matrix: Solid
)ate Sampled:10/09/2019 0900 % Solids: 1.84 10/10/2019 0042
ate Received: 10109/2019
Lin Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
I (Fecal Colifo) SM 9222 D-2006 1 10/10/2019 2051 AMR 10/09/2019 2103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 54463 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
" - Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
1ot3 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 13

Inorganic non-metals
Client: Synagro Laboratory ID: UJ09071-007
Description: 4 of 4 Fecal Matrix: Solid -
ate Sampled:10/09/2019 0900 % Solids: 1.80 10/10/2019 0042
to Received:10109/2019
Lin Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 10/10/2019 2051 AMR 10/09/2019 2103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 55451 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and> DL
Out of holding time W = Reported on wet weight basis
oiicaly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 10 of 13

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 o_ --

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106 Vantago Polfft Bravo - 'Afest C-blumbila, sc .25i772
Telephone No. SM791-0,700 r7ax No. B03-791-9111
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 13 of 13

P AEL
UR
PROM PT•AC CURATE -RE LIABLE
J_,A_B®P_A-F0FUF".S, IWC
\VWlV.PARLABS.00M
REPORT OF ANALYSES
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: OCT 19
DATE: 12/09/19
SAMPLE NUMBER- 137485 SAMPLE ID- MT. HOLLY 4 OF 4 SAMPLE MATRIX- SO
DATE SAMPLED- 10/28/19 TIME SAMPLED- 1000
DATE RECEIVED- 10/30/19 SAMPLER- AB RECEIVED BY- DJ
TIME RECEIVED- 1025 DELIVERED BY- AB TYPE SAMPLE- Grab
Page. 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 10/30/19 RE 1.04 o
LABORATORY DIRECTOR - - ' =•-' _
2217 Graham Park Drive Charlotte, NC 28273
Phone: [phone] = Fax: [phone]
a

PA
PROMPT- ACCU RATE- RELIABLE
WWW.PARLABS.COM
Solids30 Day Bench Scale Extended Aeration Test
Percent Volatile Reduction
Start: End:
TS O
0.1598
0.1855
TS%
1.82%
1.82%
VS )
0.1223
0.1405
VS%
76.53%
75.74%
y Mass Fraction of Volatile Solids in Liquid Sludge
0-01392951
0.0137814
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0042711
0.0044140
FSVR Mass Balance)
1.06%
FSVR Van Kleeck)
1.04%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 * Charlotte, NC 28241-1483
Phone: [phone] i Fax: [phone]
r

PLIR
PRO MPT• ACCU RATE, R ELIAS LE
LABORATORIES, INC
W W W. PARLABS.COM
Collected
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge W
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample W
+ Tare Wt (g)
Dried Sludge Wt (g,
Fixed Solids Wt (g;
Furnace Temp °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
30 ®ay Bench Scale Extended Aeration Test
VAN uption 3, Nercent Volatile jowl Keauction
SYNAGRO
MT HOLLY 4 OF 4
137485
10/30/19
11/27/19
As Received Day 0 Day 7 Day 14 Day 21 Day 28
10/30/19 10/30/19 11 /06/19 11/13119 11 /20/19 11127/19
3.60
4.93
5.41
5.71
5.89
X28
X28
X11
X9
X16
X20
21.0987
21.0987
21.0367
21,5208
23.1838
15.0166
29.8786
29.8786
30.3560
31.2021
32.0543
25.2115
8.7799
8.7799
9.3183
9.6813
8.8705
10.1949
105
105
107
106
106
107
10/30/19 14:50
10/30/19 14:50
11/06/19 08:40
11/13/19 09:00
11/20/19 08:50
11/27/19 08:25
10/31/19 14:30
10/31/19 14:30
11/07/19 08:30
11/14/19 09:05
11/21/19 08:55
11/28/19 08:30
21.2585
21.2585
21.2091
21.6970
23.3461
15.2021
0.1598
0.1598
0.1724
0.1762
0.1623
0.1855
0.0375
0.0407
0.0419
0.0389
0.0450
550
550
550
550
550
10/31/19 16:20
11/07/19 09:55
11/14/19 14:30
11/21/19 15:00
12/02/19 15:50
10/31/19 17:25
11/07/19 11:00
11/14/19 15:40
11121 / 19 16:05
12/02/19 17:00
21.1362
21.0774
21.5627
23,2227
15.0616
0.1223
0.1317
0.1343
0.1234
0.1405
1.82%
1.82%
1.85%
1.82%
1.83%
1.82%
76.53%
76.39%
76.22%
76.03%
75.74%
yf Mass Fraction of Volatile Solids in Liquid (Feed)
Sludge at Start of Test
0.0139295
A Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at End of Test
0.0137814
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
at Start of Test
0.0042711
Xb Mass FraLton of Fixed Solids in Liquid (Bottom)
Sludge at End of Test
0.0044140
TS (g)
0.1598
TS (g)
0.1855
VS (g)
0.1223
VS (g)
0.1405
Volatile Fraction In: 0.42049 Volatile Fraction Out: 0.41615
P.O. Box 411483 a Charlotte, NIZ 28241-1483
Phone: [phone]Fax: [phone]
a a'. -

PAR CHAIN OF CUSTODY
L4 SOR4 TORIES. INC- PAR Laboratories, Inc
Phone [phone]
www.parlabs.com Fax [phone]
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
!•...,.i:..., fl.....,.A...nn, of Cn..irnnmcn Fir anA Rl�t, ir�l rJncnirnec
Company Name (billing)
Comments/ Special Instructions
Clarifier Effluent provided in the event that
SYNAGRO CENTRAL
Address
the sample needs to be reduced to below
12701 LANCASTER H1NY
2% solids.
City, State rt zip code
PINEVILLE NC 28134
Point of Contact ti Telephone Number
ADAM BRIGMAN 704-650-4341
Sample '`' yy��
Taken By: SIGNATURE PRINTED NAME /�-(JCl1'1
ARE SAMPLES FOR STATE or EPA REPORTING? YES NO
*Sample Type: DW WW GWMW HW soil Other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
**Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n1a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
Client Sample I.D.
(Sample Location ! Number)
Comp
Grab
Preserv.
Set Up
DateTme
Collection
DateTme
Analyses
Requested
��1 ��o<< 3� r�
n A ���1P 16-
tieunqursnea by: �/ � Z�r e• rcecervpaoy. - vare�rme�
Relinquished v �DatefFime Received by: DatefRme
C=Composite G=Grab DW=Drinking Water UWV=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste
C

SECTION 6

Agricultural Lime Application Log
2019
Project: Mount Holly 50-1701
Field 11
Grower =SoilJ
Lime Requirement
Tons/Acre
Date
Total
(state -county -site -field) 11
®H
from soil anal sis
A lied
A lied
Acres
NC-CL-12-01 11
RiverTaw
6.4
0 Ton/Acre
0.0
0
51.2
NC-GA-41-01
I Greg S rin s
5.61
0.3 Ton/Acre
NC-GA-41-06 11
Greg S rin s
5.7
0.2 Ton/Acre
NC-GA-41-10 11
Greg S rin s
5.6
0.3 Ton/Acre
1.0
®
7.9
NC-GA-41-14 11
Greg S rin
F-5-5--11
0.3 Ton/Acre
NC-LT-46-01
Tonv Jones
6.6
0 Ton/Acre
0.0
0
11.8
NC-LT-46-02
Tony Jones
6.5
0 Ton/Acre I0.0
45.2
NC-LT-46-03
Tony Jones--]6.51
0 Ton/Acre
0.0
0
9.9
NC-LT-46-04
Ton Jones I6.41
0 Ton/Acre
0.0
19.4
NC-LT-46-08
Ton Jones
6.5
0 Ton/Acre I0.0
0
6.6
NC-MG-37-01 11
Dean Connell
6.1
0 Ton/Acre
0.0
0
20.2
# lime has been ordered but not spread

SECTION 7

Page 1 of 1
Report No: 20-017-1175
Account No: 11010
Advisor: Synagro-LEWA (52-0174)
Adam Brigman.
12701 Lancaster Hwy
Pineville NC 28134
Waypo'16
ANALYTICAL
Client: Rivertow
Mt. Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-CL-12
Date Received: 01/17/2020
Date of Report: 01/20/2020
Lab No Field ID
Sample ID
Soil Class
HM%
WIV pH
Ac
P-1
K-1
S-1
Mn-1
Zn-1
Zn-AI
Cu-1
GEC
BS%
Ca%
Mg%
ESP
Na
SS-1 NO3 N
25214
12-01
MIN
1.2
6.4
0.5
21
131
37
213
80
80
120
5.8
91
48
30
1.3
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines. Analvsis oreoared bv: Wavooint Analytical Virginia. Inn.

Page 1 of 1
Report No: 20-021-1028
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypoeint.
ANALYTICAL
Client: Greg Springs
Mt Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-GA-41
Date Received: 01/21/2020
Date of Report: 01/24/2020
Lab No Field ID
Sample ID
Soil Class
HM% W/V
pH
Ac
P-I
K-1
S-1
Mn-I
Zn-1
Zn-AI Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO3 N
03201
41-01
MIN
1.0
5.6
0.7
66
11
46
75
78
70
2.9
76
49
24
1.3
0
03202
41-06
MIN
1.0
5.7
0.6
66
10
40
63
83
60
2.9
78
52
23
1.6
0
03203
41-10
MIN
0.8
5.6
0.7
92
12
.35
69
123
80
2.9
75
50
22
1.2
0
03205
41-14
MIN
0.9
5.5
0.7
45
12
35
63
50
35
2.6
75
49
22
2.2
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint A

Page 1 of 1
Report NW 20-021-1020
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypoi t
ANALYTICAL
Client: Toney James
Mt. Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytica I.com
Farm: NC-LT-46
Date Received: 01/21/2020
Date of Report: 01/22/2020
Lab No Field ID
Sample ID
Soil Class
HM% W/V
pH
Ac
P-1
K-1
S-1
Mn-I
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO3 N
03179
46-01
MIN
2.1
6.6
0.4
15
27
64
106
98
98
240
7.0
95
72
20
1.4
0.1
03180
46-02
MIN
2.3
6.5
0.3
16
17
87
150
75
75
130
4.5
94
59
32
1.3
0.1
03181
46-03
MIN
2.2
6.5
0.4
11
18
96
144
68
68
130
4.9
92
58
31
1.2
0.1
03183
46-04
MIN
2.3
6.4
0.4
24
17
85
200
95
95
125
4.7
92
59
30
1.4
0.1
03184
46-08
MIN
1.9
6.5
0.5
17
25
62
113
100
100
235
7.0
92
71
18
1.4
0.1
Comment:
/I
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
•
Report No: 20-017-1173 Waypoint
7621 Whitepine Road, Richmond, VA 23237
Account No: 11010 Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: Synagro-LEWA (52-0174) Client: Dean Connell Farm: NC-MG-37
Adam Brigman Mt. Holly
12701 Lancaster Hwy
Pineville NC 28134 Date Received: 01/17/2020
Date of Report: 01/20/2020
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 1fin-1 Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO3 N
25211 37-01 MIN 1.3 6.1 0.6 26 76 29 194 93 93 80 4.4 87 53 24 1.7 0.1
Comment:
Test result units =. CEC and Na in meq/1000m3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.