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NCG200514_2020 DMR_20201230
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ANALYTICAL BlueSky Solutions -Charlotte Amy Anderson 5019 Hovis Rd., Suite G Charlotte, NC 28208 INC Certification No. 402 INC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Stormwater Project No.: NCG020000 Lab Submittal Date: 07/01/2020 Work Order: 0070017 Case Narrative 7/16/20 15:08 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL Terri W. Cole Project Manager Data Qualifiers Key Reference: BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 13 (2) Waypoint. ANALYTICAL Sample Receipt Summary 07/16/2020 Work Order: 0070017 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received Outfall 001 0070017-01 Water 07/01/20 15:34 07/01/20 16:00 Samples were received in good condition at 6.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 13 Laboratory Report Waypoint 07/16/2020 ANALYTICAL BlueSky Solutions -Charlotte Project: Stormwater Client Sample ID: Outfall 001 Attn: Amy Anderson Sample ID: 0070017-01 5019 Hovis Rd., Suite G Project No.: NCG020000 Work Order: 0070017 Charlotte, NC 28208 Sample Matrix: Water Time Collected: 07/01/20 15:34 Time Submitted: 07/01/20 16:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Chemical Oxygen Demand 74 mg/L 50 11 1 *SM5220 D 7/6/20 11:51 SLS POG0067 Total Suspended Solids 88 mg/L 11 0.75 1 *SM2540 D 7/7/20 14:20 ENM POG0107 Total Metals Copper 0.055 mg/L 0.020 0.0033 1 *200.7 7/8/20 16:17 JAB POG0075 Lead 0.012 mg/L 0.010 0.0025 1 *200.7 7/8/20 16:17 JAB POG0075 Zinc 0.40 mg/L 0.050 0.015 1 *200.7 7/8/20 16:17 JAB POG0075 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 13 Way po 0nt,. ANALYTICAL BlueSky Solutions -Charlotte Attn: Amy Anderson 5019 Hovis Rd., Suite G Charlotte, NC 28208 Total Metals - Quality Control Analyte Batch POG0075 - 200.7 Project: Stormwater Project No: NCG020000 Level II QC Report 7/16/20 Work Order: 0070017 Time Submitted: 7/1/2020 4:00:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (POG0075-BLK1) Prepared &Analyzed: 07/08/20 Copper BRL 0.020 mg/L Lead BRL 0.010 mg/L Zinc BRL 0.050 mg/L Blank (POG0075-BLK2) Prepared &Analyzed: 07/08/20 Copper BRL 0.020 mg/L Lead BRL 0.010 mg/L Zinc BRL 0.050 mg/L LCS (POG0075-BS1) Prepared &Analyzed: 07/08/20 Copper 0.485 0.020 mg/L 0.5001 97 85-115 Lead 0.501 0.010 mg/L 0.5001 100 85-115 Zinc 0.490 0.050 mg/L 0.5001 98 85-115 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 13 Level II QC Report Way po Int. 7/16/20 ANALYTICAL BlueSky Solutions -Charlotte Project: Stormwater Work Order: 0070017 Attn: Amy Anderson Time Submitted: 7/1/2020 4:00:OOPM 5019 Hovis Rd., Suite G Project No: NCG020000 Charlotte, NC 28208 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POG0067 - NO PREP Blank (POG0067-BLK1) Prepared &Analyzed: 07/06/20 Chemical Oxygen Demand BRL 50 mg/L LCS (POG0067-BS1) Prepared &Analyzed: 07/06/20 Chemical Oxygen Demand 494 50 mg/L 500.0 99 90-110 Batch POG0107 - NO PREP Blank (POG0107-BLK1) Prepared &Analyzed: 07/07/20 Total Suspended Solids BRL 5.0 mg/L LCS (POG0107-BS1) Prepared &Analyzed: 07/07/20 Total Suspended Solids 430 5.0 mg/L 477.0 91 90-110 Sample Extraction Data Prep Method: 200.7 Lab Number Batch Initial Final Date/Time 0070017-01 POG0075 50 mL 50 mL 07/08/20 8:06 Subcontracted Analyses The following analyses were subcontracted to Waypoint Analytical Lab Number Analysis 0070017-01 O & G - TPH (SGT-HEM) This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 13 8 O G) z D r ❑❑z0 3 ANC CR s >- Q w � � mp m z o m z o 3 m 8 �, a-3� v 3 p °1• rr�=N rL co o m m m a �+ n c �c cn o r ym o o F� �� o O❑C m Z m j. -0z-y 'm o�i • 3 O DNDzO 2 c c SIC S G1 �] i o=i 3 -� 6 — 0 y ID mD E;N ELK 0 co n m D r 50 � D m rL OOG] z3 o� a zoo om o Ir nm y x O � a 5 ❑ z,� m0 D� m G H = co) : B• m ^� m o a �m >x eN x�o a ❑❑D?! mo �� (D y,y0 �o zTa rm n z In o� .�S` i�. a 3$ cl) yL]$ zN Nm 0 0 a O� Ay5 (D CDya pm0� m� m �c� W mX x SS z 3. N d c m W C N m m �D :, ❑❑ �� m in in = C. " m W 'm 9 O c n m m m s n m fc Q 7 z m y Om y m 7 N N N ID 0 < nD 3 3 zm no w p o mm ❑ E± m r n mpmr m_ ° Q momw� m co N = d ' N— — C 0 Oopngi m z m'I 111 ��I 'yam° 1 D j A m O❑ A DmOA a� W • ON �O ❑Z0 r m 03 ' O �m N 1' to X z z — o n <� 'a m >omm i7 I(D zzyra a V Imp Q N F, �/ fA 8d n m m o hN6 I >r @ a❑ m m an F lz:) C� , m m�§ as m o 6 y� ®� yC 8opc" y z s ° N ❑ TI NO W D o z m, rn r0CD ❑ cA© m; n CD zmCD�p m m pZD ° yn p❑ Z m o 0 0 omm n m m •Q 0 @ o a� 8 u0i y co < 0r a D C) a CD ° d z rn s► o O U2 AIL. m 9 CD CD r C' �' r D Q G CL m Q" 0 CAm z a o� O 'C ❑ 3 N O r m .00. _ rn z ' X r 3 O a a X m- 3 y 3 y N CAz r m i v z n s O z a m y O 3 ° z m o r Sa z cN a� 0 v O. < O :or a o < � Gaf m � N• Im/l ID 0 x .n•' N D C en41 Q O m cu a0 Ds G x N nl< N C O O .'0 a DID O N m Z 3 n. O I y m n n IUD p 01 ro X co) IO —1 r 'U n E7 r m r� ID SfA r 0 m�o� mo `m m � a � n N `"kss�N=m �v O > V[p c n < m m m G) c) d a 0 n ^� Q (n m N m n a n m a n ^a ° I O z ci Page 6 of 13 n 2 z D on '0 V/ D X 0 v Waypoint ANALYTICAL 7/10/2020 Waypoint Analytical Charlotte Ms. Terri Cole P.O. Box 240543 Charlotte, NC, 28224-0543 Ref: Analytical Testing Lab Report Number: 20-189-0073 Client Project Description: Subcontract #0070017 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Ms. Terri Cole: Waypoint Analytical, LLC. received sample(s) on 7/7/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Andrea R Brownfield Project manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 7 of 13 Page 1 of 7 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arizona State Program AZ0816 08/30/2020 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 05/10/2020 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2020 Illinois State Program - NELAP 200078 10/10/2020 Kentucky State Program 80215 06/30/2020 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2020 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31/2020 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2020 Tennessee State Program 02027 02/11/2023 Tennessee A21LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2020 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2020 Washington State Program C1018 07/31/2020 Page 1 of 1 00 Page 8 of 13 Page 2 of 7 • 2790 Whitten Road, Memphis, TN 38133 Waypoint'- Main 901.213.2400 ° fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 20-189-0073 Client Project Description: Subcontract #0070017 Lab No Client Sample ID Matrix Date Collected Date Received 86935 Outfall001 Aqueous 07/01/202015:34 07/07/2020 Page 9 of 13 Page 3 of 7 Waypointo ANALYTICAL Project Subcontract #0070017 Information: Waypoint Analytical Charlotte Ms. Terri Cole P.O. Box 240543 Charlotte, NC 28224-0543 Report Number: 20-189-0073 Report Date: 7/10/2020 Sample Results Outfall 001 Date Collected 07/01/2020 15:34 WPA Lab No 86935 Date Received 07/07/2020 Matrix Aqueous 1664B-SGT Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 1 7/9/202012:50:00 CxC L500416 CAS# Parameter SGT HEM: Non -Polar Material Qualifiers/ MQL Method Quantitation Limit Definitions Result MQL Units ND 5.6 mg/L Page 4 of 7 Page 10 of 13 r Waypoint 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Quality Control Data Client ID: Waypoint Analytical Charlotte Project Description: Subcontract #0070017 Report No: 20-189-0073 QC Analytical Batch: L500416 Analysis Method: 1664B-SGT Analysis Description: Oil and Grease - TPH Lab Reagent Blank LRB Matrix: AQU Associated Lab Samples: 86935 Blank MQL Analyzed Parameter Units Result SGT HEM: Non -Polar Material mg/L < 5.0 5.0 07/09/20 12:50 Ongoing Precision and Recovery OPR Spike OPR % Analyzed %Rec Qualifie Parameter Units Conc. Result Recovery Limits SGT HEM: Non -Polar Material mg/L 20.0 14.7 74.0 07/09/20 12:50 64-132 Ongoing Precision and Recovery OPR2 Spike OPR % Analyzed %Rec Qualifie Parameter Units Conc. Result Recovery Limits SGT HEM: Non -Polar Material mg/L 20.0 13.9 70.0 07/09/20 12:50 64-132 Matrix Spike L 86004-MS MS Spike MSD MS Result MSD MS %Rec Max Parameter Units Result Conc. Spike Result %Rec Limits RPD Conc. SGT HEM: Non -Polar Material mg/L < 5.1 40.8 26.5 65.0 64-132 Date: 07/10/2020 10:35 AM Page 11 of 13 Page 5 of 7 (2) WayPoint .279p Whitten Road, Memphis, 3$133 Main 901.213.2400 °Fax 901.21213.2440 A N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 25657 Customer Name: Waypoint Analytical Charlotte Report Number: 20-189-0073 Shipping Method ® Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: T99 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: Summer Harrison Date & Time: 07/07/2020 14:16:55 Page 12 of 13 Page 6 of 7 ANALYTICAL SUBCONTRACT ORDER C citificabari � NELAC USACI WaypointAnalytical �C }r SC Other -- 0070037 N-,A SENDLNG LABORATORY: RECEIVING LABORATORY-. Waypoint Analytical Waypoim Analytical P. 0. Box 2,10543 2790 Whitten Road Charlotte, NC 28224-0543 Memphis,'FN 38133 Phone: 900-529-6364 Phone :(901) 2;3-2400 Fax_ 704-525-0409 Fax: (901) 213-2440 Project Manager. Terri W. Cole Analysis Due Expires Laboratory ID Comments Sample ID: 0070017-01 Water Sampled: D7101120 15:34 U & G - TPH (SGT-HE4i) 07129i2(1 15-34 Containers Supplied.• 4 /1 ( 6-_ /-fc L le4v IIIIII I II W I��AII I�I���II�I �I 111111111111 INIlfl I1 25657 002073 Wavuoint AnalvlicaI Charlotte 14:16 38 SuhconIract NOD 7DD17 N ► � TJ 0 .� Page 7 of 7 f Page13of13 • (2) Waypofnt. ANALYTICAL BlueSky Solutions -Charlotte Amy Anderson 5019 Hovis Rd., Suite G Charlotte, NC 28208 NO Certification No. 402 NO Drinking water Cert No. 37735 SC Certirication No. 99012 Project: Stormwater Project No.: NCG020000 Lab Submittal Date: 11/12/2020 Work Order: 0110169 Case Narrative 11/23/20 16:06 G�- This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL Terri W. Cole Project Manager Data Qualifiers Key Reference: E,,,,k , E-14, 919 5-7A- 5-3a9 OG HEM O&G is less than the reporting limit, therefore TPH (SGT-HEM) is less than the reporting limit. Sample not extracted for TPH (SGT-HEM). BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 6 Sample Receipt Summary Waypoint. ANALYTICAL 11/23/2020 Work Order: 0110169 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received Outfall001 0110169-01 Water 11/12/20 8:52 11/12/20 9:24 Samples were received in good condition at 1.6 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - CharloHe, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-800152"364 - Fax: 704152"409 Page 2 0f 6 • 0 Waypoint. ANALYTICAL BlueSky Solutions -Charlotte Attn: Amy Anderson 5019 Hods Rd., Suite G Charlotte, NC 28208 Project: Stormwater Project NO.: NCG020000 Sample Matrix: Water Laboratory Report 11/2312020 Client Sample ID: Outfall 001 Sample ID: 0 110 169-01 Work Order: 0110169 Time Collected: 11/12/20 08:52 Time Submitted: 11/12/20 09:24 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelrme ID General Chemistry Parameters Chemical Oxygen Demand BRL mglL 50 11 1 "SM5220 D 11/16/20 11c18 SLS POK0281 Oil & Grease (SGT•HEM) 4tRLOG mglL 5.0 3.4 1 '1664B 11/17/20 9:44 SLS POK0307 Total Suspended Solids ' 10 mglL 2.5 0.75 1 "SM2540 D 11116/20 14:45 ENM POK0283 Total Metals Copper ,BRL mglL 0.020 0.0033 1 '200.7 11/16/20 1C40 JAB POK0236 Lead /BRL mglL 0.010 0.0025 1 200.7 11/16/20 1C40 JAB POK0236 Zinc BRL mglL 0.050 0.015 1 200.7 11/16/20 14:40 JAB POK0236 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525.0409 Page 3 of E7 Waypoint-0 ANALYTICAL BlueSky Solutions -Charlotte Attn: Amy Anderson 5019 Hovis Rd., Suite G Charlotte, NC 28208 Total Metals - Quality Control Analyte Batch POK0236 - 200.7 Project: Stormwater Project No: NCG020000 Level II QC Report 11 /23/20 Work Order: 0110169 Time Submitted: 11/12/2020 9:24:00AM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (POK0236-BLK1) u _ Prepared: 11/13/20 Analyzed: 11/16/20 _ Copper BRL 0.020 MA Lead BRL 0.010 mg/L Zinc BRL 0.050 mg1L Blank (POK0236-BLK2) Prepared: 11/13/20 Analyzed: 11/16/20 Copper BRL 0.020 mglL Lead BRL 0.010 mg& Zinc BRL 0.050 mg)L LCS (POK0236-B51) Prepared: 11/13/20 Analyzed: 11/16/20 Copper 0.501 0.020 mg1L 0.5001 100 85-115 Lead 0.490 0.010 mglL 0.5001 98 85-115 Zinc 0.495 0.050 mg1L 0.5001 99 85-115 This report should not be reproduced, except in its entirety, without the written consent of WaypointAnalyticaI. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Tell Free Number: 1-800/529.6364 - Fax: 704/525-0409 Page 4 o16 Waypoint(2) ANALYTICAL BlueSky Solutions -Charlotte Attn: Amy Anderson 5019 Hovis Rd., Suite G Charlotte, NC 28208 General Chemistry Parameters - Quality Control Analyte Batch POK0281 - NO PREP Project: Stormwater Project No: NCG020000 Reporting Result Limit Units Level II QC Report 11123I20 Work Order: 0110169 Time Submitted: 11/12/2020 9:24:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank(POK0281-BLK1) Prepared &Analyzed: 11/16/20 Chemical Oxygen Demand BRL 50 mg/L LCS (POK0281-BS1) Prepared &Analyzed: 11/16/20 Chemical Oxygen Demand 504 50 mg/L 500.0 101 90-110 Matrix Spike (POK0281-MS2) Source: 011016"'! Prepared & Analyzed: 11/16/20 Chemical Oxygen Demand 489 50 mg1L 500.0 BRL 98 80-120 Matrix Spike Dup (POK0281-MSD2) Source: 0110169-01 Prepared & Analyzed: 11/16/20 Chemical Oxygen Demand 486 50 mglL 500.0 BRL 97 80-120 0.5 20 Batch POK0283 - NO PREP Blank (POK0283-BLK1) Prepared & Analyzed: 11/16/20 Total Suspended Solids BRL 5.0 mgll Batch POK0307 - NO PREP Blank (POK0307-B_LK1) Prepared & Analyzed: 11/17/20 Oil & Grease (SGT-HEM) BRL 5.0 mg1L OG LCS (POK0307-BSI) Prepared & Analyzed: 11/17/20 Oil & Grease (SGT-HEM) 17.8 5.0 mglL 20.00 89 64-132 Sample Extraction Data Prep Method: 200.7 Lab Number Batch Initial Final Daternme 0110169-01 POK0236 50 mL 50 mL 11/13/20 &30 This report should not be reproduced, except in its ent+rety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 6 10 T CHAIN OF CUSTODY RECORD -: YES NO WA Waypoint- PAGE OF QUOTE // TOENSURE pROPFTi e1L4N6= �r..(1 Samples INTACT upon arrival? ANALYTICAL 449 SpNngbrook Road • Charlotte, NC Z8217 �nf1 Project Name: S CJ1 � r lk f l Received IN ICE? Phone 7114! .636T Ram: 7 52Sg4a5 Short Hold Analysis es NO UST Project: eE NO !Y (Yes) { )(Yes) { ) 'Piease PROPER PRESERVATIVES Intliratetl7 / — Reoelved WITHIN HOLDING TIMES? ++`` Client Company Namo V ATTACH any project specific reporting (QC LEVEL I It III IV) Report TolCoatact Name: prmrlsions and/or QC Requirements Invoice To: CUSTODY SEALS INTACT? _ VOLATILES reed Wlou r HEADSPACE? —� Reporting Add g Address: PROPER CONTAIl4 S u 7 }yam tt TEMP: Therm IO: I]5servedC !Corr, /+aC phone. Fax (Ytts No}: purchase Order Na1Bllling Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address Requested Due Do* 0 1 Day ❑ 2 Days Q 3 Days 0 4 USA ❑ 5 Days Certification: NO Be EDO Type: PDF— XceliOther "Working Days" Q M Days 0 Standard 10 days 0 Rush Work Must Be Site Location Name: Samples received after 15:00 will be processed next twsil>eu da�d`sdl Other_ NIA Site Location Physical Addr¢Ss• Turnaround same is based on business days, excluding weekends and holidays, Water Chlorinated: YES NO_ (SEE REVERSE FORTEAMS a CONDmMe OREGANmNG SERVICES EiENDER _ 9Y WAYPOINT AkALYTICAL, LLC TO CLIENT] Samples Iced Upon Collection: YES_NO TIME MATRIX SAMPLE CONTAINER I ANAJYS4Sji[EQUEffiUD CLIENT DATE COLLECTED (SOIL, PRESERVA- (Y REMARKS ID NO. 'TYPE NO. 912E SAMPLE DESCRlP'iIOM COLLECTED MILITAttY WATER, OR 7IVE$ HOURS SLUDGE) SEEBELOW 11 DDI1 ►� �o =5P J L NtXl� D I P I 2'5DMI 92SO4 Or Z 1L G room, 3 Samplers Signatu Sampled By (Pont Name) hw Affillation Upon relinquishing, this ch44 of Custody Is your authorisation for Waypoint Analytical to pp6ceed with the analyses as requested above. Any angel must be Sitepr Time: submitted in writing to the WV/point AnaVical Project Manager. There will be charges for any changes after ana"es have been Initialized. R irw4hee w-lslgrre ) Received By (sk -kn) Dare Mimry/H r Additlanal Comments: Site Deparhae Time: I7e5rquisMd ey (Slgrucae( 8y (Sw lure) Dam Field Tech Fee: Relhqugdmd . [ Ig.W.) 'ntAaly" By. Dam - Mileage: Methotl Sltipmen[ MOri: ALLsaawlE COOLERS S7fOULb SE TAPEb SHUr H CII9TDDY SFALS FOR TRAHSPORTAMNTO THE LABORATORY.wJU IAOMtin SAMPLES ARE NUT ACCEPTED AND VER:RED AGAINST COc UNTIL RECFJVED AT THE LA$OfiATDRi: t y� j iJ F,r Ee O UPS D Hand-ddvwwI 01Wrpoi Anelyti®I Fmld r& OOlher tW/ I 11193MM M. NP E : usr GROUNDWATER DRINKING WATER: ID WASTE: RCRA: BRWNFLI3 LAND LL HER: ❑ NC O SC ZINC 0 SC Q NC © SC ❑ NC ZI SC ❑ NC ❑ SC '] INC Q SC LI NC ❑ SC � I NC I] SC 10 Q ILi NC U SC Page 6 of 6 ❑_ ❑ .❑ ___ ❑ Cl 1 M.ONTaeuco �vse rnnFa• a _ .��._ .. _ ^,__.. .... ..,___ ^- m...w^. n ., n..w r r__� .._ �. _....�„_..__� ._�r...r,. ram..._ .,_-� ^---_'