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NC0030210_Renewal Application_20180601
NPDES DOCUMENT SCANNING COVER SHEET NPDES Permit: NC0030210 Charlotte / Mallard Creek WWTP Document Type: Permit Issuance Wasteload Allocation Authorization to Construct (AtC) Permit Modification Complete File - Historical Engineering Alternatives (EAA) Renewal Application Instream Assessment (67b) Speculative Limits Environmental Assessment (EA) Document Date: June 1, 2018 This documeaat is printed oa reuse paper - igazore any coateat oa the reYerse side /'\ CHARLOTTEeld W6T E R June 1,2018 ATTN: Julie Grzyb NC DENR/DWR RECEIVEDIDENRIDWR NPDES Permitting Unit JUN 0 7 2018 1617 Mail Service Center Raleigh, NC 27699-1617 Water Resources Permitting Section Re: Mallard Creek WRF Permit Renewal Application Mallard Creek WRF— NPDES Permit #NC0030210 Ms. Grzyb, Please find the enclosed NPDES permit renewal application for Mallard Creek WRF. Per our conversation on February 26, Charlotte Water (CLTWater) intends to apply for an expansion of Mallard Creek WRF in April of 2019. CLTWater will amend this renewal application as needed at that time. Please note that Part G of this application, Combined Sewer Systems, is not applicable to Mallard Creek WRF. This application includes Attachments #1-9. The following is a summary of the attachments submitted with this application: 1. Attachment #1 summarizes the receiving stream total hardness and addresses Part A.10.e. 2. Attachment #2 is a description of the treatment process and solids management plan that address Part A.11.a. and Part B.3. 3. Attachment #3 addresses Part B.1. and explains the steps underway to minimize inflow and infiltration. 4. Attachment #4 includes the topographical map required in Part B.2. S. Attachment #5 includes the flow schematic required in Part B.3. 6. Attachment #6 includes a summary of scheduled improvements and the implementation schedule. 7. Attachment #7 includes the Priority Pollutants Analysis with organics results that are summarized in Part D. 8. Attachment #8 includes copies of the second species toxicity tests completed at Mallard WRF since the last permit renewal. This information is required in Part E.2. 9. Attachment #9 is the Significant Industrial User Information required in Part F.3. The analytical data summary information reported in Part A.12. — Effluent Testing Information, Part B.6. - Effluent Testing Data, and Part D. - Expanded Effluent Testing Data include all the effluent testing results at Mallard Creek WRF from January 1, 2016 through March 31, 2018. In addition to emailing you an electronic submittal today, CLTWater is mailing an original and two copies hardcopies for your review. Charlotte Water 5100 Brookshire Blvd, Charlotte, NC 28216 charlottewater.org cmt Operated by the City or Charlotte /0' Please let us know if you have any questions or if you need any further information. If you do, please call Shannon Sypolt, Water Quality Program Administrator, at 704/634-6984 or Henry Eudy, Mallard Cr ek WRF ORC, at 704/336-1024. You may also call me at 704/336-5433. Thank you for your assist nce with the renewal process. Respectfully, Ja q Yeline A. Jarr li P.E. perations Chief, Environmental Management Division Charlotte Water Cc: H. EI dy, S. Sypolt Charlotte Water 5100 Brookshire Blvd, Charlotte, NC 28216 charlottewater.org O Operated by the City of Charlotte 50 FACILITY NAME AND PERMIT NUMBER: Mallard Creek WRF, NCO030210 FORM 2A NPDES APPLICATION OVERVIEW PERMIT ACTION REQUESTED: RIVER BASIN: Renewal Yadkin - PeeDee Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet and a "Supplemental Application Information" packet. The Basic Application Information packet is divided into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental Application Information packet. The following items explain which parts of Form 2A you must complete. BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.S. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B. Additional Application Information for Applicants with a Design Flow z 0.1 mgd. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions B.1 through 6.6. C. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D (Expanded Effluent Testing Data): Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to provide the information. E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing Data): Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. F. Industrial User Discharges and RCRAICERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges and RCRAICERCLA Wastes). SIUs are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or c. Is designated as an SIU by the control authority. G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION) EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 1 of 22 r l FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee BASIC APPLICATION INFORMATION PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS: All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet A.I. Facility Information. Facility Name Mallard Creek Water Reclamation Facility Mailing Address 12400 US Hwy 29 North Charlotte NC 28262 Contact Person Henry Eudv Title Plant Supervisor Telephone Number 1 704 1 547-0680 Facility Address 12400 US Hwy 29 North (not P.O. Box) Charlotte NC 28262 A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name Charlotte Water Mailing Address 5100 Brookshire BLVD. . Charlotte NC 28216 Contact Person Jacqueline A Jarrell P.E. Title Operations Chief Telephone Number 1 704 ) 336-5433 Is the applicant the owner or operator (or both) of the treatment works? X owner X operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. ❑ facility X applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -issued permits). NPDES NCO030210 PSD UIC Other RCRA Other W00013252 - Reclaimed Water Permit A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type of Collection System Ownership Chadotte NC Separate Sanitary Sewer System Charlotte Water Total population served 195,951 EPA Form 3510-2A (Rev. 1-99). Replaces EPA fortes 7550-6 $ 7550-22, Page 2 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 I Renewal I Yadkin - PeeDee A.5. Indian Country. a. Is the treatment works located in Indian Country? ❑ Yes X No b. Does the treatment works discharge to a receiving water that is either in Indian Countryor that is upstream from (and eventually flows through) Indian Country? ❑ Yes X No A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12" month of -this year' occurring no more than three months prior to this application submittal. a. Design flow rate 12.0 mgd Two Years Aoo b. Annual average daily flow rate 2016 ava - 8.96 Last Year 2017 avg. - 9.54 This Year 1" Q 2018 avg. - 9:48 C. Maximum daily flow rate 14.5 20.1 12.6 A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. X Separate sanitary sewer 100 % ❑ Combined storm and sanitary sewer A.B. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? X Yes ❑ No If yes, list how many of each of the following types of discharge points the treatment works uses: I. Discharges of treated effluent ii. Discharges of untreated or partially treated effluent III. Combined sewer overflow points iv. Constructed emergency overflows (prior to the headworks) V. Other b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the U.S.? ❑ Yes If yes, provide the following for each surface impoundment: X No Location: Annual average daily volume discharge to surface impoundments) mgd Is discharge ❑ continuous or ❑ intermittent? C. Does the treatment works land -apply treated wastewater? ❑ Yes X No If yes, provide the following for each land application site: Locator: d. Number of acres: Annual average daily volume applied to site: Is land application ❑ continuous or ❑ intermittent? Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? mgd ❑ Yes X No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 3 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). If transport is by a party other than the applicant, provide: Transporter Name Mailing Address Contact Person Title Telephone Number I 1 For each treatment works that receives this discharge, provide the following: Name Mailing Address Contact Person Title Telephone Number ( ) If known, provide the NPDES permit number of the treatment works that receives this discharge Provide the average daily How rate from the treatment works into the receiving facility, mgd e. Does the treatment works discharge or dispose of its wastewater in a manner not included in A.8. through A.8.d above (e.g., underground percolation, well injection): ❑ Yes X No If yes, provide the following for each disposal method: Description of method (including location and size of site(s) if applicable): Annual daily volume disposed by this method: Is disposal through this method ❑ continuous or ❑ intermittent? EPA Farm 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 4 of 22 A#"N r7 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee WASTEWATER DISCHARGES: If you answered "Yes" to question A.8.acomplete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question A.8.a, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Ouffall. a. Outfell number 001 b. Location Charlotte NC 28262 (City or town, if applicable) (Zip Code) (County) 35°19'52" (State) 80°41'54" (Latitude) (Longftude) C. Distance from shore (if applicable) 1' ft. d. Depth below surface (if applicable) n/a ft. e. Average daily flow rate 9.28 mgd f. Does this outfall have either an intermittent or a periodic discharge? ❑ Yes X No (go to A.9.g.) If yes, provide the following information: Number f times per year discharge ocwrs: Average duration of each discharge: Average flow per discharge: mgd Months in which discharge occurs: g. Is outfall equipped with a diffuser? ❑ Yes X No A.10. Description of Receiving Waters. a. Name of receiving water Mallard Creek b. Name of watershed (if known) Rocky River to Yadkin PeeDee Basin United States Soil Conservation Service 14-digit watershed code (if known): C. Name of State Management/River Basin (if known): Yadkin PeeDee United States Geological Survey 8-digit hydrologic cataloging unit code (if known): HUC: 03040105 Sub - basin 03-07-11 d. Critical low flow of receiving stream (if applicable) acute 0.35 cfs chronic cfs e. Total hardness of receiving stream at critical low flow (if applicable): 86 mgfl of CaCO3 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 8 7550-22. Page 5 of 22 0� AI\ FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - Pee Dee A.11. Description of Treatment a. What level of treatment are provided? Check all that apply. X Primary X Secondary X Advanced ❑ Other. Describe: Please see Attachment #2 b. Indicate the following removal rates (as applicable): Design BOD5 removal or Design CBOD5 removal 97 Design SS removal 97 % Design P removal n/a % Design N removal 40 % Other % C. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe: UV If disinfection is by chlorination is dechlorination used for this outfall? ❑ Yes ❑ No Does the treatment plant have post aeration? ❑ Yes X No A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All Information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart Outfall number: 001 MAXIMUM DAILY VALUE AVERAGE DAILY VALUE PARAMETER Value Units Value Units Number of Samples pH (Minimum) 6.5 SM. pH (Maximum) 7.4 s.u. Flow Rate 20.1 MGD 9.28 MGD 821 Temperature winter) 24.0 °C 18.8 °C 264 Temperature (Summer) 27.7 °C 24.4 °C 297 ' For pH please report a minimum and a maximum daily value MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANTS ANALYTICAL MLIMDL Cone. Units Conc. Units Numberof METHODSamples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN BOD5 DEMAND (Report one) CBOD5 9.8 m IL 1.03 m IL 356 SM 5210B 2.0 FECAL COLIFORM 62 CFU/100 1 CFU/100 561 SM 9222D 10 ml ml MF) TOTAL SUSPENDED SOLIDS (TSS) 8.2 m IL 1.23 m /L 356 SM 2540D 2.5 END OF PART A. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7650-6 & 7550-22. Page 6 of 22 0OWN `\ FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee BASIC APPLICATION INFORMATION PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR EQUAL TO 0.1 MGD (100,000 gallons per day). All applicants with a design flow rate 2 0.1 mgd must answer questions BA through B.6. All others go to Part C (Certification). B.I. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration. 152,000 gpd Briefly explain any steps underway or planned to minimize inflow and infiltration. Charlotte Water has been smoke testing and Nina collection system lines to determine sources of I and I. When sources are identified we are rehabilitating pipelines by lining the existing infrastructure rebuilding manholes, and in some areas building relief sewer lines. Please see Attachment #3 for additional information. B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) a. The area surrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable. c. Each well where wastewater from the treatment plant is injected underground. d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within % mile of the property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. I. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redunancy in the system. Also provide a ureter balance showing all treatment units, including disinfection (e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. Please see Attachments #2 and #5 BA. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? ❑ Yes X No If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional pages if necessary). Name: Mailing Address: Telephone Number: ( ) Responsibilities of Contractor: B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfali number (assigned In question A.9) for each outfall that is covered by this implementation schedule. 001 b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. ❑ Yes X No EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 7 of 22 �0 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee C. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable). d. Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as applicable. For improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates, as applicable. Indicate dates as accurately as possible. Schedule Actual Completion Implementation Stage MM/DD/YYYY MN1/DD/YYYY - Begin Construction - End Construction / / I / - Begin Discharge I l I l - Attain Operational Level / / / / e. Have appropriate permits/clearances concerning other Federal/State requirements been obtained? X Yes ❑ No Describe briefly: Please see Attachment k6 B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY). Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not Include information on combine sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be based on at least three pollutant scans and must be no more than four and on -half years old. Outfall Number: 001 MAXIMUM DAILY AVERAGE DAILY DISCHARGE POLLUTANT DISCHARGE ANALYTICAL MLIMDL Conc. Units Conc. Units Number of METHOD Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA(as N) 1.9 mg/L 0.03 mg/L 356 SM 4500-NH3-H-97 0.1 CHLORINE (TOTAL RESIDUAL, TRC) 0 mg/L 0 mg/L 4 SM 4500-CL-G-00 10/15 DISSOLVED OXYGEN 9.9 mg/L 8.53 mg/L 561 SM 4500-OG - 01 0.1 TOTAL KJELDAHL 1.6 mg/L 0.786 mglL 28 EPA 351.2-93 0.25 NITROGEN (TKN) NITRATE PLUS NITRITE 21 mg/L 16.2 mg1L 30 EPA 353.2-93 0.75 NITROGEN OIL and GREASE 0 mg/L 0 mg1L 29 EPA 1664B 5.0 PHOSPHORUS (Total) 4.7 mg/L 3.61 mg/L 29 EPA 4500-H-99 0.1 TOTAL DISSOLVED SOLIDS (TDS) 320 mg/L 289 mg/L 4 SM 2540 C .97 25 OTHER END OF PART B. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 87550-22, Page 8 of 22 I'M%, FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee BASIC APPLICATION INFORMATION PART C. CERTIFICATION All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application Is submitted. Indicate which parts of Form 2A you have completed and are submitting: X Basic Application Information packet Supplemental Application Information packet: X Part D (Expanded Effluent Testing Data) X Part E (Toxicity Testing: Biomonitonng Data) X Part F (Industrial User Discharges and RCRAICERCLA Wastes) ❑ Part G (Combined Sewer Systems) ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name and official title Jac ueline A. Jarrell O erations Chef Signature 4 113 r Telephone number 17 41 336-5433 Date signed 7 ' 3 1- 19 Upon request of the permitting authority, you must submit any other intonation necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. SEND COMPLETED FORMS TO: NCDENR/ DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 9 of 22 Aw,' FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NC0030210 Renewal Yadkin - PeeDee SUPPLEMENTAL APPLICATION INFORMATION PART D. EXPANDED EFFLUENT TESTING DATA Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is dischareed. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one -Ralf years old. Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MLIMDL POLLUTANT Number Cone. Unit Mass Units Con�UnitsMass Units of s Samples METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 200.8 5.0 ARSENIC 0 ug/L 0 #/day 0 ug/L 0 #/tlay 123 EPA 200.8 5.0 BERYLLIUM 0 ug/L 0 #/tlay 0 ug/L 0 #/tlay 4 EPA 200.8 2.015.0 CADMIUM 0 ug/L 0 #/day 0 ug/L 0 #/day 123 EPA 200.8 1.0 CHROMIUM 0 ug/L 0 #/day 0 ug/L 0 #/day 123 EPA 200.8 5.0 COPPER 8.8 ug/L 0.681 #Iday 2.71 ug/L 0.209 #Iday 123 EPA 200.8 2.0 LEAD 0 ug/L 0 #Iday 0 ug/L 0 #Iday 123 EPA 200.8 5.0 MERCURY 0.002 ug/L 0.00015 #/day 0.00063 ug/L 0.000D48 #/day 29 EPA 1631 E 0.001 NICKEL 2.8 ug/L 0.216 #/day 0.95 ug/L 0.073 #/day 123 EPA 200.8 2.0 SELENIUM 0 ug/L 0 #/day 0 ug/L 0 #Iday 123 EPA 200.8 6.0 SILVER 0 ug/L 0 #/day 0 ug/L 0 #Iday 123 EPA 200.8 5.0 THALLIUM 0 uglL 0 #Iday 0 ug/L 0 #/day 4 EPA 200.8 1.015.0 ZINC 53 ug/L 4.10 #/day 38 ug/L 2.94 #Iday 123 EPA 200.8 10 CYANIDE 0 uglL 0 #/day 0 ug/L 0 #/day 64 HACH 10-204 00.1-x 10 TOTAL PHENOLIC 0.039 mg/L 3.01 #/day 0.009 mglL 0.696 #Iday 4 EPA 420.2 0.00510.0 COMPOUNDS 5 SM 2340B or HARDNESS (as CeCO3) 150 mglL 11,609 #Iday 125 mglL 9,674 #Iday 28 5.0 & 1.0 EPA 200.7 Use this space (or a separate sheet) to provide information on other metals requested by the permit writer EPA Form 3510-2A (Rev. 1-99). Replaces EPA fors 7550-6 8 7550-22. Page 10 of 22 �1 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Number Conc. Units Mass Units Conc. Units Mass Units of METHOD Samples VOLATILE ORGANIC COMPOUNDS ACROLEIN 0 ug/L 0 #/day 0 ug/L 0 ##day 4 EPA 624 100 ACRYLONITRILE 0 ug/L 0 111 0 ug/L 0 #/day 4 EPA 624 100 BENZENE 0 ug/L 0 #/day 0 uglL 0 #/day 4 EPA 624 5 BROMOFORM 0 ugll- 0 #/clay 0 uglL 0 #/day 4 EPA 624 5 CARBON TETRACHLORIDE 0 ug/L 0 #/day 0 uglL 0 #/day 4 EPA 624 5 CHLOROBENZENE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 5 CHLORODIBROMO- METHANE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 5 CHLOROETHANE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 10 2-CHLOROETHYLVINYL ETHER 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 10 CHLOROFORM 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 5 DICHLOROBROMO- METHANE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 5 1,1-DICHLOROETHANE 0 ug/L 0 #/day 0 uglL 0 #/day 4 EPA 624 5 1,2-DICHLOROETHANE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 5 TRANS-I,2-DICHLORO- ETHYLENE 0 ug/L 0 #Ida Y 0 ug/L 0 #/da Y 4 EPA 624 5 1,1-DICHLORO- ETHYLENE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 5 1,2-DICHLOROPROPANE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 5 1,3-DICHLORO- PROPYLENE 0 ug/L 9 0 #Ida Y 0 ug/L 9 0 #Idey 4 EPA 624 5 ETHYLBENZENE 0 ug/L 0 ##day 0 ug/L 0 #/day 4 EPA 624 5 METHYL BROMIDE 0 ug/L 0 #/day 0 ug/L 0 #/clay 4 EPA 624 10 METHYL CHLORIDE 0 uglL 0 #/day 0 ug/L 0 #/day 4 EPA 624 10 METHYLENE CHLORIDE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 624 5 1,TETRA- CHLORHLOROETHANE 0 ug/L 0 #/da Y 0 ug/L 0 #/da Y 4 EPA 624 5 TETRACHLORO- ETHYLENE 0 ug/L 0 #/da Y 0 u /L 9 0 #/da Y 4 EPA 624 5 TOLUENE 0 ug/L 0 #/day 0 1 ug/L 0 #/day 4 EPA 624 5 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 11 of 22 .WN A01%k FACILITY NAME AND PERMIT NUMBER: Mallard Creek WRF, NCO030210 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Yadkin - PeeDee Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) I POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MLIMDL Cone. Units Mass Units Cone. Units Mass Units Number of Samples 1,1,1 TRICHLOROETHANE 0 ug/L 0 #/day 0 ug/L 0 Afday 4 EPA 624 5 1,1,2 TRICHLOROETHANE 0 ug/L 0 #/day 0 uglL 0 #)day 4 EPA 624 5 TRICHLOROETHYLENE 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 624 5 VINYL CHLORIDE 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 624 10 Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL 0 ug/L 0 #Iday 0 ug/L 0 Wday 4 EPA 625 10 2-CHLOROPHENOL 0 uglL 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 2,4-DICHLOROPHENOL 0 ug/L 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 2,4-DIMETHYLPHENOL 0 ug/L 0 #Iday 0 ug/L 0 #/day 4 EPA 625 10 4,6-DINITRO-0-CRESOL 0 ug/L 0 *day 0 uglL 0 #Iday 4 EPA 625 20 2,4-DINITROPHENOL 0 ug/L 0 #Iday 0 ug/L 0 #/day 4 EPA 625 50 2-NITROPHENOL 0 ug/L 0 #Iday 0 ug/L 0 #/day 4 EPA 625 10 4-NITROPHENOL 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 PENTACHLOROPHENOL 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 20 PHENOL 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 2,4,6- TRICHLOROPHENOL 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 Use this space (or a separate sheet) to provide information on other acid -extractable compounds requested by the permit writer I BASE -NEUTRAL COMPOUNDS ACENAPHTHENE I 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 ACENAPHTHYLENE 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 625 10 ANTHRACENE 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 625 10 BENZIDINE 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 625 50 BENZO(A)ANTHRACENE 0 ug/L 0 #Iday 0 ug/L 0 #/day 4 EPA 625 10 BENZO(A)PYRENE 0 ug/L 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 12 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT I ANALYTICAL ML1MDL Number i. Cone. Units Mass Units Cone. Units Mass Units of METHOD Samples FLUORANTHENE RANT 0 ug/L 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 BENZO(GHI)PERYLENE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA625 10 BENZO( FLUORANTHENE g ugll- 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 BIS (2-CHLOROETHOXY) METHANE 0 uglL 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 BIS (2-CHLOROETHYL} 0 ug/L 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 ETHER BIS (2-CHL 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 625 10 PROPVL)EETHER THER BIS (2-ETHYLHEXYL) PHTHALATE 0 ug/L 0 #/day 0 ug/L 0 #Itlay 4 EPA 625 10 HE PHENYL E PHENYL ETHERR 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 625 10 BUTYL BENZYL PHTHALATE 0 ug/L 0 #Iday 0 uglL 0 #Iday 4 EPA 625 10 H NAPHTTHALHAL ENE NA 0 ug/L 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 PHENYL ETHER PHENYL ETHERL 0 uglL 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 CHRYSENE 0 uglL 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 DI-N-BUTYL PHTHALATE 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 625 10 DI-N-OCTYL PHTHALATE 0 ug/L 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 DIBENZO(A,H) ANTHRACENE 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 625 10 1,2-DICHLOROBENZENE 0 ug/L 0 #Iday 0 ug/L 0 #/day 4 EPA 625 10 1,3-DICHLOROBENZENE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 1,4-DICHLOROBENZENE 0 ug/L 0 #Iday 0 ug/L 0 #Iday 4 EPA 625 10 3,3-DICHLORO- BENZIDINE 0 ug/L 0 #Iday 0 ug/L 0 #/day 4 EPA 625 10 DIETHYL PHTHALATE 0 ug/L 0 #Itlay 0 ug/L 0 #Iday 4 EPA 625 10 DIMETHYL PHTHALATE 0 ug/L 0 #Iday 0 ug/L 0 #/day 4 EPA 625 10 2,4-DINITROTOLUENE 0 uglL 0 #Iday 0 ug/L 0 #/day 4 EPA 625 10 2,6-DINITROTOLUENE 0 uglL 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 1,2-DIPHENYL- HYDRAZINE 0 ug/L 0 #/da y 0 ug/L 0 #/da y 4 EPA 625 10 EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 13 of 22 .-"N I — FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin - PeeDee Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Number Conc. Units Mass Units Conc. Units Mass Units of METHOD Samples FLUORANTHENE 0 ug/L 0 #/day 0 ug/L 0 Nclay 4 EPA 625 10 FLUORENE 0 uglL 0 #/day 0 ug/L 0 i#day 4 EPA 625 10 HEXACHLOROBENZENE 0 uglL 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 HEXA- 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 BUTADIENE DIENE HEROCYCLO- 0 ug/L 0 #/day 0 ug/L 0 #Iday 4 EPA 625 10 PENTADIENE NTADIE HEXACHLOROETHANE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 INDENO(1,2,3-CD) 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 PYRENE ISOPHORONE 0 ug/L 0 #/day 0 uglL 0 #/day 4 EPA 625 10 NAPHTHALENE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 NITROBENZENE 0 ug/L 0 #/day 0 uglL 0 #/day 4 EPA 625 10 N-NITROSODI-N- 0 ug/L 0 #/day 0 uglL 0 #/day 4 EPA 625 10 PROPYLAMINE N-NITROSODI- 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 METHYLAMINE N-NITROSODI- PHENYLAMINE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 PHENANTHRENE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 PYRENE 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 1.RIOHLOROBENZENE TRIC 0 ug/L 0 #/day 0 ug/L 0 #/day 4 EPA 625 10 Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer Use this space (or a separate sheet) to provide information on other pollutants (e.g. pesticides) requested by the permit writer END OF PART D. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22, Page 14 022 rsk Go FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: Mallard Creek WRF, NCO030210 JWIV�ERASIN: Renewal Yadkin - PeeDee SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity, tests for acute or chronic toxicity for each of the factlitys discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information requested in question EA for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.I. Required Tests. Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. x chronic See Attachment # 8 for all second species (Fat Head Minnow) Toxicity test data collected since Jan 1, 2014, the effective date of our current permit. E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one column per test (where each species constitutes a test). Copy this page if more than three tests are being reported. Test number: Test number: Test number. a. Test information. Test Species & test method number Age at initiation of test Outfall number Dates sample collected Date test started Duration b. Give toxicity test methods followed. Manual tifle Edition number and year of publication Page number(s) c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hourcomposite Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection EPA Form 3510-2A (Rev. 1-99). Replaces EPA forms 7550-6 & 7550-22. Page 15 of 22 Attachment #1 Mallard Creek WRF - Receiving Stream Hardness Calculation MCA - Upstream of Mallard MCB - Downstream of Mallard 1/14/2016 75 1/14/2016 100 2/18/2016 �70 2/18/2016 74 3/14/2016 1!98 3/14/2016 100 4/11/2016 77 4/11/2016 110 5/10/2016 179 5/10/2016 110 6/13/2016 �77 6/13/2016 110 7/11/2016 56 7/11/2016 110 8/15/2016 86 8/15/2016 120 9/19/2016 90 9/19/2016 100 10/10/2016 58 10/10/2016 58 11/21/2016 J00 11/21/2016 130 12/21/2016 184 12/21/2016 120 1/18/2017 ,83 1/18/2017 93 2/14/2017 '82 2/14/2017 110 3/16/2017 '66 3/16/2017 98 4/11/2017 77 4/11/2017 100 5/17/2017 77 5/17/2017 100 6/14/2017 29 6/14/20 17 39 7/18/2017 67 7/18/2017 87 8/22/2017 60 8/22/2017 99 9/11/2017 64 9/11/2017 100 10/18/2017 99 10/18/2017 100 11/15/2017 63 11/15/2017 110 12/12/2017 64 12/12/2017 94 1/16/2018 76 1/16/2018 100 2/14/2018 69 2/14/2018 95 3/19/2018 38 3/19/2018 98 Average: 73 99 Count: 27 27 Receiving Stream Hardness: 86 Attachment #2 Charlotte Water Mallard Creek WRF NPDES # NC0030210 Process Flow Description Attachment #3 — Description of Treatment — Additional Information OUTFALL NUMBER: 001 A.11.a I Description of Treatment Treatment consists of coarse and fine mechanical bar screens; grit removal; day tanks; storm flow equalization; five primary clarifiers; three trains in parallel of activated sludge treatment; four final clarifiers; effluent traveling bridge filters; ultraviolet disinfection; reuse distribution; sludge thickening; anaerobic digesters; and sludge dewatering. B.3. ii Process Flow Diagram or Schematic I The attached flow schematic SC-1 (Attachment 2) shows the processes of the treatment facility along with bypasses. The plant is currently permitted to treat 12.0 MGD of wastewater. Preliminary Treatment: Wastewater enters the plant through a 36-inch gravity sewer line to enter the headworks and influent pumping station. The flow entering the headworks flows through two mechanical screens where the screenings are compacted and conveyed to a dumpster. Flow from the screens is sent to two vortex grit removal basins of 30 MGD capacity. Primary Treatment: Following preliminary treatment, the wastewater splits between two cells of the flow equalization day tanks. From here, it is pumped to the distribution boxes (DB), DB-1, DB-1A, and DB-2A and is distributed to the five existing primary clarifiers (PC-1 through PC-5). After primary treatment the flow from all of the operating clarifiers is collected and discharged into DB-5 where it is combined with the collected RAS flow from all three treatment trains and then is �'1Q1 distributed to the aeration basins. Secondary Treatment: The combined flow is combined with RAS and split equally between biological treatment trains 1, 2 and 3. It goes through anoxic zone and aeration zone with internal recycle. The activated sludge process is carried out in a series of rectangular aeration basins and, in trains 1 and 2, is followed by additional round aeration basins. Following the aeration basin, flow from the round oxic basins of trains 1 and 2 are combined in DB-9 and split to final clarifiers (FC) FC-1, FC-2 and FC-5. Flow from train 3 aeration basin is sent to FC-3 at DB-18. A portion of the flow at DB- 18 can be directed to DB-9 to mix with the flows from trains 1 and 2 and feed to FC-1, FC-2 and FC-5. This portion is determined by a modulating pinch valve that calculates an input percentage to divert. i Tertiary Treatment: Combined secondary effluent from all the final clarifiers is sent to filter distribution structure (FDS) FDS-1 and FDS-2 for filtration. Filtered effluent is I� ! sent for UV disinfection and re -aeration structure where aeration takes place. The effluent is discharged through a 42" line into Mallard Creek. it Solids Processing and Biosolids Management Plan at Mallard Creek WRF I Mallard Creek WRF is currently operating one 1.0 MG and two .48MG primary digesters with an average detention time of 40-50 days. The average total solids of raw sludge to the primary digesters is 3.0-4.0%. Average sludge flow to the primary digesters is between 50-60k gallons/day. Mallard is currently operating one secondary digester with a volume of 480k gallons. The' average total percent solids of digested sludge at Mallard is 1.5%. For thickening and dewater,i ng purposes, Mallard uses three Humboldt/Bird and one GEA/Westfalia centrifuges —'two for thickening and two for dewatering. Dewatered solids are belt conveyed out of the dewatering building into a 24 cu. yard dump truck and taken to a cover storage pad onsite where they are stored in batches and tested. The average ercent solids of Mallard's cake is 20%. All biosolids produced at Mallard Creek WRF are Clan B biosolids and they are land applied in both North and South Carolina per our contract with Synagro provided that they pass all required testing and are conforming solids according to 40 CFR Part 503. All non -conforming solids are hauled by Synagro and landfilled. Attachment #3 (Om*� Mallard Basin Inflow and Infiltration (W) Reduction Practices Charlotte Water (CLTWater) has maintained an established evaluation and rehabilitation program since the early 1990's. The purpose of this program is to restore and preserve hydraulic ci pacity, structural integrity, and to reduce corrective maintenance costs by addressing i, sues that cause SSOs. This includes maintaining and implementing an on -going 1/1 reduction pl', n. Multiple construction contracts are continually in place to address these issues. Through comprehens've SSES efforts, including manhole inspections, smoke testing, CCTV, flow monitoring, etc., areas are identified for rehabilitation and work orders assigned to a contractor. The work may include manhole rehabilitation, point repairs, pipe lining and pipe replacement. Since July 2 q03, CLTWater's Rehabilitation Team has inspected in excess of 4,700 manholes, smoke tested at least 137,000 ft. of pipe, and performed CCTV inspection on more than 15,600 ft. of pipe, r sulting in the following...... 670 manholes rehabbed/repaired, 750 inflow dishes installed and 3,150 ft. of pipe rehabbed/replaced throughout the collection system. This does not include similar work performed by CLTWater's Field Operation Division. CLTWater also implemented a chemical root control program in March 2005 and we continue to maintain and expand that program. CLTWater uses flow monitoring extensively to support engineering analyses, to prioritize sewer improvements, and to evaluate capacity issues and 1/1 loadings in the major trunk lines in the system. CLTWater currently has 52 permanent flow meters installed throughout the service area (4 permanent meters in the Mallard Creek basin) and utilizes temporary flow metering on an as-neededi basis. eo*) Attachment #4 Date: 5/31/2018 N Project: Mallard Creek WWTP cHnaLorre Scale-1 inch =1,786 feet One Mile Radius W TER N Created By'. sclontz Map Number. 1 CHARLOTTE WATER ENGINEERING DIVISION A_1 5100 BROOKSHIRL BLVD CIIARLOTIti, NC 9,8216 Page 1 of 1 Mallard Parcel ® Mallard WWTP Two Mile Radius • Well / Drinking Water • Biosolids Storage Biosolids a Wastewater Mains ForceMain Gravity LowPressure Sludge Streams North Date: 5/31/2018 N Map Number: 1 Project: Mallard Creek VNNiP CHARLOTTE WATER CHARLOTTE Scale: Two Mile Radius 1 inch =3,573 feet ' / 'u�„lo� WOTER W oar d .,m `° ENGINEERING DIVISION 5100 BROOKSWRE BLVD A _2 ~ v o.���•em.c wm°...o+r wrna.nw�. Created BY: scbntz S ..00�.op.�..s m... wr.ama CFiARLO'I7E.NC 28216 Page 1 of 1 Attachment #5 OBIT BwalY - xcueYarY. anx sswtoa / PRIMARY / FUTURE •1 \ SLUOGE FINAL FUTURE PUMPING Blcrsaass I CLARIFIER CLARIFIER PRIMARY ' CLARIFIER SIN rrII_ _ - FUTURE eonlvlr`+mExm�"'� NO 4 R RS/WP.S PUMPING NO. 6 NO IJ AERATION BASIN 1- °1" 0 STRTIDN . 2 DB 0. OB ND. 1 FUTURE res - - PRIMARY CLARIFIER IE9� ' B AERATION BASIN 4.1 -a,�~ NO_4 SCUM "'-• N AERATION BASIN NELL uv e4 nBsxo x"•nl` 3.2 •°P 1 OB NO. t ° DO NO. 19 - ANOXIC BABE N0. 3.2 ssso IB _a _ xu.-. x s PRIMARY ANOXIC BASIN NO. 3.1 RERRTLON BREIN 3.1 DB NO 2 CLARIFIER zB� FINAL + NO_5 CLARIFIER - - PRIM R -Na. 3 R sraB NO_3 Q MH NO 3 PRFIIMINRRY TREATMENT 6L (OUT OF SERVICE) s O OB NO, 10 MH NO, 2 MH NO. 5 MH NO. 6 , - - - - 0B NO, 3 �' as- uL n - _ MH NO, I ;k 4 n �a MH N 7 MH NO. 13 MH N0. 4 F. PRiMARY TRICKLING FILTER - AERATTON 'S AERATION 11 F NR CLRIER _ CLRRTFIER N0. 2 _ BRSIN BASIN a NO. N N0. 2 N0. 1. c"esxr wnu J o°s:sn'"ws' 0 MH NO.DB , 3 NO, z RIN PLANT DRAIN �3 4 ti y'F - = - �r 08 NO, 12 v j 1� .--L-.'r•„ q� �eY0nnax •`m s� M1� wr-+.x s'; `ram ^T DX IC RECYCLE PUMPING �: 3 _J,� OXIC R• RECYCLE r RRS/W $• PUM INTERMEDIATE - FLOW ED ION SP ,� f i`Q = - s•r �PUMPIN z '^. STRTIi PUMPING STATION c-n-ryz BASIN (B MGD CAP. ERCH PUMP) TOTAL tc.Bn:.B� ❑B N0. 1R OB N0. 4 -' °'s•'c'°. L.,.� o + �J132NGp BN STATION -` - N0. 1 OB N0. 6-+.I F 'a�" jti ti - I AERATION G ❑B NO-�p wras N0. 2 rscTusv C xw • se-r CAP.) '•• d'P a "a +s ➢B - a RERRT DN g wiis s R IN N0. ,�°�� �T?-, '°0°B .B ""uwr oun°I" B • BRSIN 0. 1.1 DB NO, 15 e 3 `ID00 = `+-= - TR I G IL-T - _ y FINAL Ilro- / ll PRIMARY CLARIFIER TRICKLING T N FI TER _ z U• - s� AERATION MH N0. 35 BRSIN ss-xs �' Q AERATION BRS7 CLA_ R Ie.oni�_ as N0. 1 ,1/[ + �x-x H N0. 1.3 t O3 0� 0 O MH N0. 33 _ ___1 _ ac ++ , ��� , FLOW FLOW H NO34 M. IMCp BASINRNOXIC NO . 2.1 1 EGURLIZRTION EOUALIZATIO DRY DRY PLANT DRAIN PUMPING trla• gpAr,NIONX 1.1ET a•sa+ u,en.B++I"-`-" 08 N0. 14v u,seH,ur u.on,w TANK TANK STATION co.sa J x I.• .. + s CELL N0. 1 CELL NO. 2 !' B• pion seou on DB N0. 13 ns"Ts� nxx "BI "..YxwrB, TO INFLUENT I xx ssnrlts xx rB..a .z• st Ic.al:.Bl PUMP[NG STATION � QQ CHLORINE "a CONTACT FILTER FILTER CHAM ER DISTRIBUTION TR �TID ImmsunYBl STRUCTURE TRU T PARS ALL - NO. 1 Its MCD -EFFLUENT O CAP. EACH) s z - - FILTERS O O GRIT � FLOW l I REMOVAL BASINS x se n.B"c tt n.n '° ac•sc n. EQUALIZATION / \ 130 MODD' CHAP. EACH] LEGEND _� _ "E�°' BASIN xQ-a L=J LINE S1ZE SERVICE '}i _ o 0 35" RS (12/24) E;FF I NI T FT T R $ y $ DESIGN FLOW-- 1. PEAK FLOW I FUTURE FUTURE FLOW EFFLUENT I I EQUALIZATION EOUCPME(1T,flBBREVI AL[DH L_F CEND $ - 3 = FILTERS BASIN K REP-X FLOATING SURFACE flERATOR 5� Iz rB lar xlu [MP-X INTERMEDIATE PUMP W E f I J IP-X INFLUENT PUMP _ A F A ox rl sus ORP-X OXIC RECYCLE PUMP mxuBr L y I GENERAL NOTE M xB�wY+UL PD-X PLANT DRAIN PUMP JB No, 1 - sc�-.o "�"' - - - - J SCREENED (LIGHT) DELINEATION SHOWN ON THE DRAWINGS INDICATES EXISTING FACILITIES. SCREENED INFORMATION aqE-^ P.oY s.Be I PSP-X PRIMARY SLUOGE/SC IM PUMP �'le UV WAS TAKEN FROM PREVtOUS CONSTRUCTION DRAWINGS, AND SHALL BE FIELD VERIFIED. RASP-X RAS PUMP .x• ex Ie.Brre.ol gi"eaExnnBx Q " IS FOR REFERENCE ONLY BOLD (DARKI DELINEATION IS NEW WORK OR LOCATION OF TO MODIFIED UNDER THIS '- SCUM-X SCUM PUMP i,°vcr�lusnw w UV NEW UV DISINFECTIOk EXISTING CONSTRUCTION BE CONTRACT UNLESS OTHERWISE NOTED. e°wa'"1F•ns"'.aY,"` IAtlue(f c ���uu Ix'iicB uB.s Rc-X BLurcE cPrE UV ➢TSINFECTION ANO s. - .c I: AND RE -AERATION STRUCTURE RECORD DRAWING INFLUENT PUMPING STRTIDN SLG-X SLIDE GATE RE-RER TION STRUCTURE w.n`si's Rr� a NRSP-X WAS PUMP t01p" mxisF.woganv a�x sisi°N THIS DRAWING HAS.BEEN MOTAU IEO TO REFLECT CHANGER MADE DURING CONTRUCTION BASED sTssa UPON INFORMATION AS MAYS BE PROVIDE BY TI CONTRACTOR RND CONSTRUCTION OBSERVATION .B.a.B. -� .T •x.c+ M,� "B BY THE ENGINEER'S AUTHORIZED REPRESENTRTI BY............... ............... ENGINEER DATE d CHARLOTTE-MECKLENBURG UTILITIES so���� u � .Wil¢sB�innBY MALLARD CREEK HATER RECLAMATION FACILITY THIS DOCUMENT - ORIGINALLY a ORIANDGINALLY ISSUED I' ` DESI GNEO RWB DETAILED RLC,M00 �� ,A //��jj��// Q, a /[ ^ �7�,e��.di6 '.7. ii �S��.J�Tan PROJECT NO. EXPANSION TO 12 MGD PRN.By i DAVIOSNPpRKER CBRRECI STRATIDNIDNAL EN� RED l� B6D4 Cliff Cameron Delve N0. 18516 ON 02/10/9B SHEET CHECKED Cie 164 259252 LIQUIDS SCHEMATIC 1 q 1 APPROVED Chorloffe, N-th Carolina 1 OF 1 I nnrc REVISIONS AND RECORD nF TAAIIF N0_ PY !'V. RPP nRIF- _ 2B26Q k GENERAL NOTES: 1. PROCESS SCHEMATIC PROVIDED FOR REFERENCE ONLY. NOT ALL EXISTING OR NEW VALVES, PIPING, EQUIPMENTOR INSTRUMENTS ARE SHOWN. FUTURE 1 _—�T--_--..— FUTURE I PRIMARY I -- � — i FUTURE AERATION I I CLARIFICLARIFER R No. 6 I r . - — BASIN W No. 42 '•\ No. a DIVIDER -I------------------•- / - i• WALL --- %. -\�.. RASIWAS FUTURE AERATION f� DB.1s ,(� PUMPING BASIN No.4., � /? 5TATlON No.2 I f PRIMARY V( CLARIFIER DB.17 No 4 AERATION DB-19 - BASIN No. 32 I 1 AERATION � DR-2 I I CLARIFIER �,�. I BASIN No.3.7 ff� FINAL ` No.S I _ L CLARIFIER g `..... -.. No.3 DBAU CONTFLOW \ ! \ SCUM PUMPS OL STRUCTURE PRIMARY MH-51 CLARIFIER I MH.57 FINAL No.3 30• A1C - 6�SC CLARIFIER No. 5 1r RAS TO 3• SPD f O 750D 3a•PE ,� � 36' SI MH54 k MHSB (' Dli3 24•RAS OB-10 MF1$ ` O ll \\\\ RAS PUMPS MH-3 16' RAS 3D' ML MHO f�\ PRIMARY MH-1 �•'�� i M MH-5 }, FINAL CIARIF�R WSJ No.2 MF152 AERAWN �J L� .. - ,' - AERATION CLARIFIER \ BASIN MH-4 \ No 2 96'PE WIN DS-5 MH33 _ - No. 12 o.22 ��•\ \\\ No. 22 h AERATION { AERATION BASIN No. 1.1 ♦ DB-t5 ff WIN 1N No.2, DBE f ue 1q: L— �k�- !MH-50 MH-a fff i DO + / 4B'PE _ AERATION 1 AERATION t f\ BASIN 6ac RECYCLE I BASIN ! PRIMARY No. 12 !! CLARIFIER PUMPING STATION OXIC RECYCLE 1 No. 2.3 DIM) P No.1 BASIN No. 1.1 NO. ANOXIC PUMPINGSTATION RASIWAS FINAL _1 BASIN No. 21 NO.2 �� PUMPING CLARIFER 2a' OR MH-35 - L 2 STATION No.1 No.1 MH33 1 0 a MH34 - CXIC RECYCLE _.. PUMPING STATION i 'T-1 08-11 N0. 7A TO FILTER DISTROtUION J 7300 - STRUCTURES No. 1 & 2 ! I ,S'pR DB-14 r� E DB-13 OXIC RECYCLEPUMPING ,�---� STATtCN NO.2A 7400 I DRAWN eF ° ne �,j�� CMU -MALLARD CREEK WATER RECLAMATION FACILITY E�kFvsca�s a a 0 BAR IS ONE MOt1 ON DRAWING _ a�cKm O L' '�+: 8115 HARMS CORNERS PARKWAY. suss aaD M ■ ' ■ ■ nTT�.�� FINAL CLARIFIER AND RELATED IMPROVEMENTS ORIGNAL 0 ®�' NO. 00-G09 w_ EPP w CHARLOTTE, NC28269 iL.R.J!■. !R■. O 1■ sM GENERAL DATE DATE - rp + n PHONE: (704)598-0918 FAx:pDt)5ssas7B PROCESS SCHEMATIC IFNOTONEINOHOIN SHEETNO. I - DESCPoPPON 1172D70 _ NR i<1fnB10 NE R 11:a2-j0 LICENSE No. G2119 TM SHEET, AWUbT SG9LESACWROBIGLY FILENAME: B"IB7B70-00.G419.tlWg PLOT 7IME: SIMES 9 OF 103! Attachment #6 e"*� Filter The purpose of this project is to provide updated and more reliable equipment for the filtration of final clari Iler effluent and for UV disinfection of plant discharge flow. Additionally with this project, impt,ovements will be made to FC-1.. FC-2 and FC-3. The existing raveling bridge sand filters will be replaced with rotating disc filters with a total peak flow ca' 3acity of 32mgd. These filters will be placed in the footprint of the existing filters with modifications to the flow routing. Along with the filters the existing UV disinfection system will be repla ed with an updated system also capable of flows of 32mgd. The UV system will be moved into t e footprint previously used by the existing filters with flow modifications. Along with this project the interior metal structure and operating parts of FC-1, FC-2 and FC-3 will be replaced and upgraded with stainless steel structure and mechanisms to protect against corrosion and updates will be made to the drive and scum collection systems. Notice to Proceed Date /10� July 2019 Final Complet'on Date March 2021 Operational Date March 2021 Generator and Power Distribution Improvements The purpose of this project is to improve reliability of power and backup generator feed to the Mallard Creek plant. A new generator building will be constructed with two 3000kW generators and related switchgear along with a new electrical substation. The new generators will replace the single active backup generator currently onsite and the new electrical',, substation will consolidate the existing power distribution system and make it more reliable., Notice to Proc ed Date November 201 Final Completion Date June 2020 Operational June 2020 Expansion Proiect The purpose bf this project is to expand the Mallard Creek plant in order to stay ahead of increased flow projections in the service basin of the treatment plant. This project is still in its early stages but may include the expansion or replacement of the influent lift station, screening removal, primary clarifiers, aeration basins, blowers, final clarifiers and equalization basin. Notice to Pro�eed Date Undetermined Final Completion Date Undetermined Operational Date Undetermined! look1 Attachment #7 EFFLUENT Annual Monitoring and Pollutant Scan Permit No. NC0030210 Month August Outfall 001 Year 2014 i Facility Name Mallard Creek WWTP ORC Mr. Darrell Dewitt Date of EFFLUENTI Sampling: 8/6/2014. low level mercury 8/ 114 Phone (704) 547-0680 Analytical Laboratory:) CMUD Environmental Lab NC 192.Prism Lab NC 402, Access Lab NC 618 i �M i{Aii r : re er; L ;sampie Type . Analytical } Method Quan on :Lev 1 k amp e Result i o ,r ;11�easuremeuu�es� um er4p "' .t. `•1{, Ammonia (as N) Composite SM 4500-NH3-H-97 0.1 Less than mg/L 2 Dissolved oxygen Grab SM4500-0-G-01 1.0 7.9 mg/L 1 Nitrate/Nitrite Composite EPA 353.2-93 1.0 18 mg/L 1 Total Kjeldahl nitrogen Composite EPA 351.2-93 0.25 0.48 mg/L 1 Total Phosphorus I Composite SM 4500P-G-99 0.1 4.2 mg/L 1 Total dissolved solids Composite SM 254OC-97 25 314 mg/L 1 Hardness Composite SM 234OB-97 0.5 130 mg/L 1 Chlorine (total residua}, TRC) Grab SM 4500C1-G-00 10 Less than ug/L 1 OR and grease j Grab EPA 1664B 5 Less than mg/L 1 �rx ' ^.6' : r:. .'s•.4. .r Metalsk.lfo_tal zecooe 1e1;:rcvariide t - and.tofal{oi '♦ ��} - _ _ ,!' �.. '� _ .s. t. 7- •n__i.•,i"Y7.�.`T->. t:yiA enols: •, _ } _. _ ' . 4 ,. �k::. s. +...t � - _ , . r .:� .r i Antimony Composite 200.8 5.0 Less than ug/L 1 Arsenic Composite 200.8 5.0 Less than ug/L 2 Beryllium Composite 200.8 5.0 Less than ug/L 1 Cadmium ! Composite 200.8 1.0 Less than ug/L 2 Chromium j Composite 200.8 5.0 Less than ug/L 2 Copper Composite 200.8 2.0 6.1 ug/L 2 Lead j Composite 200.8 5.0 Less than ug/L 2 Mercury Grab EPA 1631E 1.0 Less than ng/L 1 Nickel Composite 200.8 2.0 2.3 ug/L 1 Selenium Composite 200.8 5.0 Less than ug/L 2 Silver Composite 200.8 5.0 Less than ug/L 2 Thallium Composite 200.9 1.0 Less than ug/L 1 Zinc Composite 200.8 10 41 ug/L 2 Cyanide Grab 10-204-00-i-X 10 Less than ug/L 1 Total phenolic compounds Grab EPA 420.2 0.005 0.039 mg/L 1 Volatile oilganicaomp/'�/uads c" r..s.i +tr+.: r..1Y. :1i". •� Y. .k i�.. .4�� -. N.iG_ 2v CI.�.2' L.�. .inr'..! Acrolein Grab EPA 624 100 Less than ug/L 1 Acrylonitrile ( Grab EPA 624 100 Less than ug/L 1 Benzene I Grab EPA 624 5 Less than ug/L 1 Bromoform Grab EPA 624 5 Less than ug/L 1 Carbon tetrachloride i Grab EPA 624 5 Less than ug/L 1 Chlorobenzene i i Grab EPA 624 5 Less than ug/ L 1 Chlorodibromomethane' Dibromochloromethane I Grab EPA 624 5 Less than ug/ L 1 Chloroethane E Grab EPA 624 10 Less than ug/L 1 2-chloroethylvinyl ether! Grab EPA 624 10 Less than ug/L 1 Chloroform Grab EPA 624 5 Less than ug/L 1 Dichlorobromomethane Bromodichloromethane Grab EPA 624 5 Less than ug/L 1 1,1-dichloroethane Grab EPA 624 5 Less than ug/L 1 1,2-dichloroethane Grab EPA 624 5 1 Less than lug/L ug/L 1 Trans- l,2-dichloroethyl; ne Grab EPA 624 5 Less than 1 Form - DMR- PPA-1 Page 1 EFFLUENT Annual Monitoring and Pollutant Scan ,001K Permit No. NCO030210 Outfall 001 Month August Year 2014 _ Paa3eter:: r _i�. t .+f� .�..'..w. -.l ; Type •? s 1Viethod t.. ..i l.. . 1, Level iai,. .: J. :i.: %tesult ' : ni o l�Ieasw�elment f.� :�ituAl.e e,'�l^.tiie : --,er;o '" sam�es .Sb:.i..'g. W i�..4. ♦.; `Y oa{iierganr►'lCoy" 9--. 77�.?5=•1t Dua�$ t�/{lnti', ' .!,d t YS-,tp, 1,1-dichloroethylene Grab EPA 624 ' S Less than ug/L 1 1,2-dichloropropane Grab EPA 624 5 Less than ug/L 1 1,3-dichloropropylenel Grab EPA 624 5 Less than ug/L 1 Ethylbenzene Grab EPA 624 5 Less than ug/ L 1 Methyl bromide(Bromomethane) Grab EPA 624 10 Less than ug/ L 1 Methyl chloride(Chloromethane) Grab EPA 624 10 Less than ug/L 1 Methylene chloride ( Grab EPA 624 5 Less than ug/L 1 1,1,2,2-tetrachloroethane Grab EPA 624 5 Less than ug/L 1 Tetrachloroethylene Grab EPA 624 5 Less than ug/L 1 Toluene Grab EPA 624 5 Less than ug/L 1 1, 1, 1 -trichloroethane Grab EPA 624 5 Less than ug/L 1 1,1,2-trichloroethane I Grab EPA 624 5 Less than ug/L 1 Trichloroethylene i Grab EPA 624 5 1 Less than ug/L 1 Vinyl chloride Grab EPA 624 10 Less than ug/L 1 Aci�.�extractalale coounds �, , r -: � �; ,, , �; , , , ,; „ , ;�,.� ># • � , �� � P-chloro-m-creso 4-chloro-3-meth 1 heno Composite EPA 625 10 Less than ug/L 1 2-chlorophenol Composite EPA 625 10 Less than ug/ L 1 2,4-dichlorophenol Composite EPA 625 10 Less than ug/L 1 2,4-dimethylphenol Composite EPA 625 10 Less than ug/L 1 4,6-dinitro-o-cresol (4,6 Dinitro-2-methvIrphenoll Composite EPA 625 20 Less than ug/L 1 2,4-dinitrophenol f Composite EPA 625 50 Less than ug/L 1 2-nitrophenol j Composite EPA 625 10 Less than ug/L 1 4-nitrophenol Composite EPA 625 10 Less than ug/L 1 Pentachlorophenol Composite EPA 625 20 Less than ug/L 1 Phenol Composite EPA 625 10 Less than ug/L 1 2,4,6-trichlorophenol j Composite EPA 625 10 Less than ug/L 1 Base-nential y_7 z Acenaphthene i Composite EPA 625 10 Less than ug/L 1 Acenaphthylene Composite EPA 625 10 Less than ug/ L 1 Anthracene Composite EPA 625 10 Less than ug/L 1 Benzidine Composite EPA 625 50 Less than ug/L 1 Benzo(a)anthracene Composite EPA 625 10 Less than ug/L 1 Benzo(a)pyrene Composite EPA 625 10 Less than ug/L 1 3,4 benzofluoranthene Benzo fluoranthene { Composite EPA 625 10 Less than ug/L 1 Benzo(ghi)perylene ! Composite EPA 625 10 Less than ug/L 1 Benzo(k)fluoranthene Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethoxy) methane Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethyl) ether Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroisopropyl) �ther Composite EPA 625 10 Less than ug/L 1 Bis (2-ethylhexyl) phthalate Composite EPA 625 10 Less than ug/L 1 4-bromophenyl phenyl �ther Composite EPA 625 10 Less than ug/L 1 Butyl benzyl phthalate 'I Composite EPA 625 10 Less than ug/L 1 2-chloronaphthalene Composite EPA 625 10 Less than ug/L 1 4-chlorophenyl phenyl ether Composite EPA 625 10 Less than lug/L 1 Form - DMR- PPA-1 Page 2 /MI' EFFLUENT Annual Monitoring and Pollutant Scan Permit No. NC0030210 Month August Outfall 001 Year 2014 P,arameter _� amp a 'Type F t,• i:'' Method uan a on Leven mp a Result x io Measu�emeat�i c un erM ,� f'� �sara�plesi` !Base aeus' �al�com ds' �contj Chrysene Composite EPA 625 10 Less than ug/L 1 Di-n-butyl phthalate Composite EPA 625 10 Less than ug/L 1 Di-n-octyl phthalate ! Composite EPA 625 10 Less than ug/L 1 Dibenzo(a,h)anthracerie Composite EPA 625 10 Less than ug/L 1 1,2-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 1,3-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 1,4-dichlorobenzene Composite EPA 625 10 Less than ug/L I 3,3-dichlorobenzidine Composite EPA 625 10 Less than ug/L i Diethyl phthalate i Composite EPA 625 10 Less than ug/L 1 Dimethyl phthalate Composite EPA 625 10 Less than ug/L 1 2,4-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 2,6-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 1,2-dipheny1hydrazinei Composite EPA 625 10 Less than ug/L 1 Fluoranthene I Composite EPA 625 10 Less than ug/ L 1 Fluorene Composite EPA 625 10 Less than ug/L 1 Hexachlorobenzene Composite EPA 625 10 Less than ug/L 1 Hexachlorobutadiene Composite EPA 625 10 Less than ug/L 1 Hexachlorocyclo-penta 'ene Composite EPA 625 10 Less than ug/L 1 Hexachloroethane Composite EPA 625 10 Less than ug/L 1 Indeno(1,2,3-cd)pyrene! Composite EPA 625 10 Less than ug/L 1 Isophorone i Composite EPA 625 10 Less than ug/L 1 Naphthalene Composite EPA 625 10 Less than ug/L 1 Nitrobenzene Composite EPA 625 10 Less than ug/L 1 N-nitrosodi-n-propylamEine Composite EPA 625 10 Less than ug/L 1 N-nitrosodimethylammp Composite EPA 625 10 Less than ug/L 1 N-nitrosodiphenylamine Composite EPA 625 10 Less than ug/L 1 Phenanthrene i Composite EPA 625 10 Less than ug/L 1 Pyrene i Composite EPA 625 1 10 Less than ug/L I1 1,2,4,-trichlorobenzene Composite EPA 625 10 Less than ug/L I1 I certify under penalty and supervision in a gather and evaluat manage the system, information submitte aware that there are possibility of fines an of law that this document and all attachments were prepared under my direction cordance with a system to design to assure that qualified perdonnel properly a information submitted. Based on my inquiry of the person or persons that 4++r those persons directly responsibel for gathering the information, the I is, to the best of my knowledge and belief, true, accurate and complete. I am significant penalties for submitting false information, including the imprisonment for knowing violations. Authorized Representative name S' ature Date ` Form - DMR- PPA-1 Page 3 INFLUENT Annual Monitoring and Pollutant Scan Permit No. NCO030210 Outfall 001 ` Facility Name MallardlICreek WWTP ORC Mr. Darrell Dewitt Date of INFLUENT ampling: 8 5 14 Phone (704) 547-0680 Analytical Laboratory:! CMUD Environmental Lab NC 192 Prism Lab NC 402 Access Lab NC 618 Month Aug zst Year 2014 Paraiie"ter � ' �ampie . r fiype taalycal .Method � Quantttation ; ,_ .:Level sample : ° .. Result . � Units;tiof ., Me�asuremwent'� Nnmbero � pl���: Ammonia (as N) Composite SM 4500-NH3-H-97 1.0 31 mg/L 2 Dissolved oxygen Grab SM4500-0-G-01 n/a n/a mg/L 0 Nitrate/Nitrite Composite EPA 353.2-93 0.05 Less than mg/L 1 Total Kjeldahl nitrogen, Composite EPA 351.2-93 2.5 46 mg/L 1 Total Phosphorus Composite SM 4500P-G-99 0.2 5.7 mg/L 1 Total dissolved solids Composite SM 254OC-97 n/a n/a mg/L 0 Hardness Composite SM 2340C-97 n/a n/a mg/L 0 Chlorine (total residual TRC) Grab SM 4500C1-G-00 n/a n/a ug/L 0 OR and grease i Grab EPA 1664B 5.01 19 mg/ L 1 ,,-ter rtotacov.T-n, 1Vietials l er le ;c aide aad,,totat., Y N Antimony Composite EPA 200.8 5.0 Less than ug/L 1 Arsenic Composite EPA 200.8 5.0 Less than ug/L 1 Beryllium Composite EPA 200.8 5.0 Less than ug/L 1 Cadmium Composite EPA 200.8 1.0 Less than ug/L 1 Chromium Composite EPA 200.8 5.0 Less than ug/L 1 Copper i Composite EPA 200.8 2.0 24 ug/L 1 Lead Composite EPA 200.8 5.0 Less than ug/L 1 Mercury ( Composite EPA 245.2 0.2 Less than ug/L 1 Nickel Composite EPA 200.8 2.0 2.9 ug/L 1 Selenium Composite EPA 200.8 5.0 Less than ug/L 1 Silver j Composite EPA 200.8 5.0 Less than ug/ L 1 Thallium G Composite EPA 200.9 1.0 Less than ug/L 1 Zinc j Composite EPA 200.8 20 130 ug/L 1 Cyanide Grab 10-204-00-1-X 10 Less than ug/L 1 Total phenolic compou4ds Grab EPA 420.2 0.005 0.033 mg/L 1 tl ;Nola ..' Acrolein Grab EPA 624 100 Less than ug/L 1 Acrylonitrile Grab EPA 624 100 Less than ug/L 1 Benzene Grab EPA 624 5 Less than ug/L 1 Bromoform ! Grab EPA 624 5 Less than ug/L 1 Carbon tetrachloride j Grab EPA 624 5 Less than ug/L 1 Chlorobenzene j Grab EPA 624 5 Less than ug/L 1 Chlorodibromomethane ibromochlorome ane i Grab EPA 624 5 Less than ug/L 1 Chloroethane Grab EPA 624 10 Less than ug/L lug/L 1 2-chloroethylvinyl ether Grab EPA 624 10 Less than 1 Chloroform j Grab EPA 624 5 Less than ug/L 1 Dichlorobromomethane Bmmodichloromethane j Grab EPA 624 5 Less than ug/L 1 1,1-dichloroethane Grab EPA 624 5 Less than ug/L 1 1,2-dichloroethane Grab EPA 624 5 Less than ug/L 1 7`rans-1,2-dichloroethyl�ne Grab EPA 624 5 Less than ug/L 1 Form - DMR- PPA-1 Page 1 INFLUENT Annual Monitoring and Pollutant Scan Qi Permit No. NCO030210 Outfall 001 Month A Year 2014 -i -r e Paraai�ter :•J RAY a'.i f}v! - r ..c.. i. _ Type 1� .. - c. -.., t,. '! Method i - :1 i t c�, � �,i T'.-, , Level ls. .S F_ .d.y. t i rY7'r t;qk Result .aJ i �'•�'._� yu.K �ry.:ti..�'S, Measeme� Y �1 rL .r-i\'+r«:AL .�.-.I `�::nyo... +:.iC.; k�l t samp es, . :�•. +17� .-v:L�:«.:aNa ..P.a .s r...aL-)'.r.- ....-.-r...._ ...s. .-..... ._... ... :..4..._... -.. :" .-. ... .1:, .. _!. ..Ym-...)..._ 1,1-dichloroethylene Grab EPA 624 5 Less than ug/L 1 1,2-dichloropropane Grab EPA 624 5 Less than ug/L 1 1,3-dichloropropylenq Grab EPA 624 5 Less than ug/L 1 Ethylbenzene Grab EPA 624 5 Less than ug/L 1 Methyl bromide(Brom methane) Grab EPA 624 10 Less than ug/L 1 Methyl chloride(Chlor methane) Grab EPA 624 10 Less than ug/L 1 Methylene chloride Grab EPA 624 5 Less than ug/L 1 1,1,2,2-tetrachloroeth a Grab EPA 624 5 Less than ug/L 1 Tetrachloroethylene Grab EPA 624 5 Less than ug/L 1 Toluene Grab EPA 624 5 Less than ug/L 1 1, 1, 1-trichloroethane Grab EPA 624 5 Less than ug/L 1 1,1,2-trichloroethane Grab EPA 624 5 Less than ug/L 1 Trichloroethylene Grab EPA 624 1 5 Less than ug/L 1 Vinyl chloride Grab EPA 624 10 Less than ug/L 1 AC�d-eRtl'8C'�Sb�e NCO Oill'td8 � - f - _ - _ '"'�� "•' �_ '� P-chloro-m-creso 4-chloro-3-meth 1 henoll Composite EPA 625 10 Less than ug/L 1 2-chlorophenol Composite EPA 625 10 Less than ug/L 1 2,4-dichlorophenol Composite EPA 625 10 Less than ug/L 1 2,4-dimethylphenol Composite EPA 625 10 Less than ug/L 1 4,6-dinitro-o-cresol 4 &Dinitro-2-meth 1 he of Composite EPA 625 20 Less than ug/L 1 2,4-dinitrophenol Composite EPA 625 50 Less than ug/L 1 2-nitrophenol Composite EPA 625 10 Less than ug/L 1 4-nitrophenol Composite EPA 625 10 Less than ug/L 1 Pentachlorophenol Composite EPA 625 20 Less than ug/L 1 Phenol I Composite EPA 625 10 Less than ug/L 1 2,4,6-trichlorophenol Composite EPA 625 10 Less than ug/L 1 Base4aentracompo ds t Acenaphthene� I Composite EPA 625 10 Less than ug/L 1 Acenaphthylene Composite EPA 625 10 Less than ug/L 1 Anthracene Composite EPA 625 10 Less than ug/L 1 Benzidine Composite EPA 625 50 Less than ug/L 1 Benzo(a)anthracene Composite EPA 625 10 Less than ug/L 1 Benzo(a)pyrene Composite EPA 625 10 Less than ug/L 1 3,4 benzofluoranthene ffienzoffilfluonanthenel Composite EPA 625 10 Less than ug/L 1 Benzo(ghi)perylene ` Composite EPA 625 10 Less than ug/L 1 Benzo(k)Iluoranthene Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethoxy) m thane Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethyl) ethek Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroisopropyl) Other Composite EPA 625 10 Less than ug/L 1 Bis (2-ethylhexyl) phth ' ate Composite EPA 625 10 Less than ug/L 1 4-bromophenyl phenyl 4ther Composite EPA 625 10 Less than ug/L 1 Butyl benzyl phthalate Composite EPA 625 10 Less than ug/L 1 2-chloronaphthalene Composite EPA 625 10 Less than ug/L 1 4-chlorophenyl phenyl ether Composite EPA 625 10 Less than ug/L 1 Form - DMR- PPA-1 Page 2 r INFLUENT Annual Monitoring and Pollutant Scan Permit No. NC6030210 Month August Outfall 001 Year 2014 fit. Paxaameter: � , :. _ - ,. p e Type, - a Method uan on= Level amp e: Result _ o �lieasurement wm ergo sam�p�es�.� '�ppp�'ut�aiaas C�o�Y14 ands:/Ciont•j � s s Chrysene Composite EPA 625 10 Less than ug/L 1 Di-n-butyl phthalate Composite EPA 625 10 Less than ug/L 1 Di-n-octyl phthalate Composite EPA 625 10 Less than ug/L 1 Dibenzo(a,h)anthracene Composite EPA 625 10 Less than ug/L 1 1,2-dichlorobenzene j Composite EPA 625 10 Less than ug/L 1 1,3-dichlorobenzene ! Composite EPA 625 10 Less than ug/L 1 1,4-dichlorobenzene ; Composite EPA 625 10 Less than ug/L 1 3,3-dichlorobenzidine,l Composite EPA 625 10 Less than ug/L 1 Diethyl phthalate Composite EPA 625 10 Less than ug/L 1 Dimethyl phthalate 1 Composite EPA 625 10 Less than ug/L 1 2,4-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 2,6-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 1,2-dipheny1hydrazine! Composite EPA 625 10 Less than ug/L 1 Fluoranthene Composite EPA 625 10 Less than ug/L 1 Fluorene Composite EPA 625 10 Less than ug/L 1 Hexachlorobenzene Composite EPA 625 10 Less than ug/L 1 Hexachlorobutadiene Composite EPA 625 10 Less than ug/L 1 Hexachlorocyclo-pentadiene Composite EPA 625 10 Less than ug/L 1 Hexachloroethane I Composite EPA 625 10 Less than ug/L 1 Indeno(1,2,3-cd)pyrenO Composite EPA 625 10 Less than ug/L I Isophorone I Composite EPA 625 10 Less than ug/L 1 Naphthalene Composite EPA 625 10 Less than ug/L 1 Nitrobenzene Composite EPA 625 10 Less than ug/L 1 N-nitrosodi-n-propyl ine Composite EPA 625 10 Less than ug/L 1 N-nitrosodimethylamir a Composite EPA 625 10 Less than ug/L 1 N-nitrosodiphenylamin6 Composite EPA 625 10 Less than ug/L 1 Phenanthrene Composite EPA 625 10 Less than ug/L 1 Pyrene { Composite 1 EPA 625 1 10 Less than ug/ L I1 1,2,4,-trichlorobenzene Composite I EPA 625 1 10 1 Less than ug/L 1 1 I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified perdonnel properly gather and evaluat the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibel for gathering the information, the information submitt d is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Adthorized Representative name Signature /Oft\ 4llg/;wl4 Date Form - DMR- PPA-1 Page 3 EFFLUENT Annual Monitoring and Pollutant Scan Permit No. NCO030210 Month November Outfall 001 Year 2015 f �Pacility Name Mallard Creek WWTP ORC Mr. Darrell Dewitt Date of EFFLUENT Sampling: 11 / 11 / 2015, low level mercury 11 / 10 / 15 Phone (7041 547-0680 1 Analytical Laboratory: CHARLOTTE WATER Environmental Lab NC 192. Prism Lab NC 402 Parameter sample Type Analytical Method QnanUtaUon Level sample Result unita o Measurement. umber o samples Ammonia (as N) Composite SM 4500-NH3-H-97 0.1 Less than mg/ L 2 Dissolved oxygen Grab ASTM D888-09C 1.0 8.6 mg/L 1 Nitrate/Nitrite Composite EPA 353.2-93 1.0 12 mg/L 1 Total Kjeldahl nitrogen Composite EPA 351.2-93 0.25 1.2 mg/L 1 Total Phosphorus Composite SM 4500P-H-99 0.1 1.7 mg/L 1 Total dissolved solids Composite SM 2540C-11 25 220 mg/ L 1 Hardness Composite SM 2340B-11 1.0 110 mg/L 1 Chlorine (total residual,! TRC) Grab ISM 4500C1-G-00 151 Less than ug/L 1 Oil and grease Grab EPA 1664B 5 1 Less than I mg/L 1 Metals (total reoovera le), cyanide and total phenols Antimony Composite EPA 200.8 5.0 Less than ug/L 1 Arsenic Composite EPA 200.8 5.0 Less than ug/ L 2 Beryllium Composite EPA 200.8 5.0 Less than ug/L 1 Cadmium Composite EPA 200.8 1.0 Less than ug/L 2 Chromium Composite EPA 200.8 5.0 Less than ug/L 2 Copper Composite EPA 200.8 2.0 2.1 ug/L 2 Lead Composite EPA 200.8 5.0 Less than ug/L 2 ercury Grab EPA 1631E 1.0 Less than ng/ L 1 Nickel Composite EPA 200.8 2.0 Less than ug/L 2 Selenium Composite EPA 200.8 5.0 Less than ug/L 2 Silver Composite EPA 200.8 5.0 Less than ug/L 2 Thallium Composite EPA 200.8 5.0 Less than ug/L 1 Zinc I Composite EPA 200.8 10 22 ug/ L 2 Cyanide Grab 10-204-00-1-X 10 Less than ug/L 1 Total phenolic compounds Grab EPA 420.2 0.005 Less than mg/ L 1 o Volatile n c comP ' _ ram. rands Acrolein Grab EPA 624 100 Less than ug/L 1 Acrylonitrile Grab EPA 624 100 Less than ug/L 1 Benzene Grab EPA 624 5 Less than ug/L 1 Bromoform ' Grab EPA 624 5 Less than ug/L 1 Carbon tetrachloride Grab EPA 624 5 Less than ug/ L 1 Chlorobenzene ; Grab EPA 624 5 Less than ug/ L 1 Chlorodibromomethane Dibromochlorometha.ne Grab EPA 624 5 Less than ug/L 1 Chloroethane Grab EPA 624 10 Less than ug/L 1 2-chloroethylvinyl ether Grab EPA 624 10 Less than ug/L 1 Chloroform Grab EPA 624 5 Less than ug/L 1 Dichlorobromomethane Bromod' hloromet Grab EPA 624 5 Less than ug/L 1 1,1-dichloroethane Grab EPA 624 5 Less than ug/L 1 1,2-dichloroethane Grab EPA 624 5 Less than ug/L 1 Trans-1,2-dichloroethyl ,ne Grab EPA 624 5 Less than lug/ L 1 Form - DMR- PPA-1 Page 1 EFFLUENT Annual Monitoring and Pollutant Scan /" F Permit No. NCO030210 Outfall 001 7- Month November Year 2015 eter Sample Type Analytical Method quantionSample Level Result Units of Measurement Number o saamples Volatile organic compounds (Cont.) 1,1-dichloroethylene Grab EPA 624 5 Less than ug/L 1 1,2-dichloropropane Grab EPA 624 5 Less than ug/L 1 1,3-dichloropropylene Grab EPA 624 5 Less than ug/L 1 Ethylbenzene Grab EPA 624 5 Less than ug/L 1 Methyl bromide(Bromomethane) Grab EPA 624 10 Less than ug/L 1 Methyl chloride(Chloro$nethane) Grab EPA 624 10 Less than ug/L 1 Methylene chloride I Grab EPA 624 5 Less than ug/L 1 1,1,2,2-tetrachloroeth a Grab EPA 624 5 Less than ug/L 1 Tetrachloroethylene Grab EPA 624 5 Less than ug/ L 1 Toluene Grab EPA 624 5 Less than ug/L 1 1,1,1-trichloroethane Grab EPA 624 5 Less than ug/ L 1 1,1,2-trichloroethane Grab EPA 624 5 Less than ug/L 1 Trichloroethylene Grab EPA 624 1 5 Less than ug/ 1 1 Vinyl chloride Grab EPA 624 10 Less than ug/L 1 Acid-6ztraaable co=n founds P-chloro-m-creso 4-chloro-3-methyl henol Composite EPA 625 10 Less than ug/L 1 2-chlorophenol j Composite EPA 625 10 Less than ug/L 1 2,4-dichlorophenol Composite EPA 625 10 Less than ug/L 1 2,4-dimethylphenol Composite EPA 625 10 Less than ug/L 1 4,6-dinitro-o-cresol (4,6- ginitro-2-methylphenoll Composite EPA 625 20 Less than ug/L 1 2,4-dinitrophenol Composite EPA 625 50 Less than ug/L 1 2-nitrophenol Composite EPA 625 10 Less than ug/L 1 4-nitrophenol I Composite EPA 625 10 Less than ug/ L 1 Pentachlorophenol Composite EPA 625 20 Less than ug/L 1 Phenol Composite EPA 625 10 Less than ug/L 1 2,4,6-trichlorophenol Composite EPA 625 10 Less than ug/L 1 Base neutral compouujds Acenaphthene Composite EPA 625 10 Less than ug/L 1 Acenaphthylene I Composite EPA 625 10 Less than ug/L 1 Anthracene Composite EPA 625 10 Less than ug/L 1 Benzidine Composite EPA 625 50 Less than ug/L 1 Benzo(a)anthracene Composite EPA 625 10 Less than ug/L 1 Benzo(a)pyrene Composite EPA 625 10 Less than ug/L 1 3,4 benzofluoranthene Ben.zo b fluoranthene Composite EPA 625 10 Less than ug/L 1 Benzo(ghi)perylene Composite EPA 625 10 Less than ug/L 1 Benzo(k)fluoranthene Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethoxy) met aane Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethyl) ether, Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroisopropyl) a her Composite EPA 625 10 Less than ug/L 1 Bis (2-ethylhexyl) phth4 ate Composite EPA 625 10 Less than ug/L 1 4-bromophenyl phenyl ether Composite EPA 625 10 Less than ug/L 1 Butyl benzyl phthalate Composite EPA 625 10 Less than ug/L 1 2-chloronaphthalene Composite EPA 625 10 Less than ug/L 1 4-chlorophenyl phenyl e. er Composite EPA 625 10 Less than ug/L 1 Form - DMR- PPA-1 Page 2 EFFLUENT Annual Monitoring and Pollutant Scan Permit No. NC0030210 Outfall 001 Month November Year 2015 Parameter ;�. sample 1"e Calnan Method on Level p Result ni o Meaauremeat umper o samples , Base -neutral compo , ds (cunt.) Chrysene Composite EPA 625 10 Less than ug/ L 1 Di-n-butyl phthalate Composite EPA 625 10 Less than ug/ L 1 Di-n-octyl phthalate Composite EPA 625 10 Less than ug/ L 1 Dibenzo(a,h)anthracen Composite EPA 625 10 Less than ug/L 1 1,2-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 1,3-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 1,4-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 3,3-dichlorobenzidine Composite EPA 625 10 Less than ug/L 1 Diethyl phthalate Composite EPA 625 10 Less than ug/L 1 Dimethyl phthalate Composite EPA 625 10 Less than ug/L 1 2,4-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 2,6-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 1,2-diphenylhydrazine ; Composite EPA 625 10 Less than ug/L 1 Fluoranthene Composite EPA 625 10 Less than ug/L 1 Fluorene Composite EPA 625 10 Less than ug/L 1 Hexachlorobenzene Composite EPA 625 10 Less than ug/L 1 Hexachlorobutadiene Composite EPA 625 10 Less than ug/L 1 Hexachlorocyclo-pentadiene Composite EPA 625 10 Less than ug/L 1 Hexachloroethane Composite EPA 625 10 Less than ug/L 1 Indeno(1,2,3-cd)pyrene Composite EPA 625 10 Less than ug/L 1 Isophorone Composite EPA 625 10 Less than ug/L 1 Naphthalene Composite EPA 625 10 Less than ug/L 1 Nitrobenzene Composite EPA 625 10 Less than ug/L 1 N-nitrosodi-n-propyl a Composite EPA 625 10 Less than ug/L 1 N-nitrosodimethylamin' Composite EPA 625 10 Less than ug/L 1 N-nitrosodiphenylamine Composite EPA 625 10 Less than ug/L 1 Phenanthrene Composite EPA 625 10 Less than ug/L 1 Pyrene Composite EPA 625 10 Less than ug/L 1 1,2,4,-trichlorobenzene Composite EPA 625 10 Less than ug/L 1 I certify under penal of law that this document and all attachments were prepared under my direction and supervision in ac ordance with a system to design to assure that qualified perdonnel properly gather and evaluat the information submitted. Based on my inquiry of the person or persons that manage the system, cr those persons directly responsibel for gathering the information, the information submitted is , to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Au orized Representative name Aigan"re / 0 -// 7A/ Date Form - DM R- PPA-1 Page 3 INFLUENT Annual Monitoring and Pollutant Scan Permit No. NCO030210 Month November Outfa11001 Year 2015 Facility Name Mallard reek WWTP ORC Mr. Darrell Dewitt Date of INFLUENT S` pling: 11110 / 2015, additional Phenol 11 / 11 / 15 Phone j7041 547-0680 Analytical Laboratory: CHARLOTTE WATER Environmental Lab NC 192, Prism Lab NC 402 Parameter Type Mhod catanLeveluo n Result Measurement umurox . �sd*ples j Ammonia (as N) Composite SM 4500-NH3-H-97 1.0 14 mg/L 2 Dissolved oxygen Grab ASTM D888-09C n/a n/a mg/L 0 Nitrate/Nitrite Composite EPA 353.2-93 0.05 0.27 mg/L 1 Total Kjeldahl nitrogen Composite EPA 351.2-93 2.5 23 mg/ L 1 Total Phosphorus Composite SM 4500P-H-99 0.2 2.7 mg/L 1 Total dissolved solids Composite SM 2540C-11 n/a n/a mg/L 0 Hardness I Composite SM 2340B-11 n/a n/a mg/L 0 Chlorine (total residual,iTRC) Grab SM 4500C1-G-00 n/a n/a ug/L 0 Oil and grease Grab EPA 1664B 5.01 12 mg/L 1 Metals (total recoverable), cyanide and total phenols Antimony Composite EPA 200.8 5.0 Less than ug/L 1 Arsenic Composite EPA 200.8 5.0 Less than ug/L 1 Beryllium Composite EPA 200.8 5.0 Less than ug/L 1 Cadmium Composite EPA 200.8 1.0 Less than ug/L 1 Chromium Composite EPA 200.8 5.0 Less than ug/L 1 Copper Composite EPA 200.8 2.0 15 ug/L 1 Lead Composite EPA 200.8 5.0 Less than ug/L 1 Mercury Composite EPA 245.1 0.2 Less than ug/L 1 Nickel Composite EPA 200.8 2.0 3.3 ug/ L 1 Selenium Composite EPA 200.8 5.0 Less than ug/L 1 Silver Composite EPA 200.8 5.0 Less than ug/L 1 Thallium Composite EPA 200.8 5.0 Less than ug/L 1 Zinc Composite EPA 200.8 10 60 ug/L 1 Cyanide Grab 10-204-00-1-X 10 Less than ug/L 1 Total phenolic compounos Grab EPA 420.2 0.050 Less than mg/ L 2 Volatile' organic comp . unds AcroIein Grab EPA 624 100 Less than ug/L 1 Acrylonitrile Grab EPA 624 100 Less than ug/L 1 Benzene Grab EPA 624 5 Less than ug/L 1 Bromoform Grab EPA 624 5 Less than ug/L 1 Carbon tetrachloride Grab EPA 624 5 Less than ug/L 1 Chlorobenzene Grab EPA 624 5 Less than ug/L 1 Chlorodibromomethane Dibromochloromethane Grab EPA 624 5 Less than ug/L 1 Chloroethane Grab EPA 624 10 Less than ug/ L 1 2-chloroethylvinyl ether Grab EPA 624 10 Less than ug/ L 1 Chloroform Grab EPA 624 5 Less than ug/ L 1 Dichlorobromomethane ro di hloromethan Grab EPA 624 5 Less than ug/L 1 1, 1 -dichloroethane Grab EPA 624 5 Less than ug/L 1 1,2-dichloroethane Grab EPA 624 5 Less than ug/L 1 Trans-1,2-dichloroethyl' ne Grab EPA 624 5 Less than ug/L 1 Form - DMR- PPA-1 Page 1 INFLUENT Annual Monitoring and Pollutant Scan Permit No. NCO030210 Month November Outfall 001 Year 2015 Parameter ample Type Analytical Method quanutaubn Level Sample Result Units o Measurement uia er o samples'. Volatile organic com ' unds (Cont.) 1,1-dichloroethylene Grab EPA 624 5 Less than ug/L 1 1,2-dichloropropane Grab EPA 624 5 Less than ug/L 1 1,3-dichloropropylene Grab EPA 624 5 Less than ug/L 1 Ethylbenzene Grab EPA 624 5 Less than ug/L 1 Methyl bromide(Bromo ethane) Grab EPA 624 10 Less than ug/L 1 Methyl chloride(Chloro ethane) Grab EPA 624 10 Less than ug/L 1 Methylene chloride Grab EPA 624 5 Less than ug/L 1 1, 1,2,2-tetrachloroethane Grab EPA 624 5 Less than ug/L 1 Tetrachloroethylene Grab EPA 624 5 Less than ug/ L 1 Toluene Grab EPA 624 5 Less than ug/L 1 1, 1, 1-trichloroethane ! Grab EPA 624 5 Less than ug/L 1 1,1,2-trichloroethane Grab EPA 624 5 Less than ug/L 1 Trichloroethylene Grab EPA 624 5 Less than ug/L I1 Vinyl chloride i Grab EPA 624 10 Less than ug/ L 1 Add -extractable com uads P-chloro-m-creso 4-chloro-3-meth 1 henol Composite EPA 625 10 Less than ug/L 1 2-chlorophenol Composite EPA 625 10 Less than ug/L 1 2,4-dichlorophenol ! Composite EPA 625 10 Less than ug/L 1 2,4-dimethylphenol Composite EPA 625 10 Less than ug/L 1 4,6-dinitro-o-cresol 4 6-Dinitro-2-methvl hen I Composite EPA 625 20 Less than ug/L 1 2,4-dinitrophenol Composite EPA 625 50 Less than ug/L 1 2-nitrophenol Composite EPA 625 10 Less than ug/L 1 4-nitrophenol Composite EPA 625 10 Less than ug/L 1 Pentachlorophenol Composite EPA 625 20 Less than ug/L 1 Phenol Composite EPA 625 10 Less than ug/L 1 2,4,6-trichlorophenol Composite EPA 625 10 Less than ug/L 1 Base,-neutra!_compoun s--. Acenaphthene Composite EPA 625 10 Less than ug/L 1 Acenaphthylene Composite EPA 625 10 Less than ug/L 1 Anthracene Composite EPA 625 10 Less than ug/L 1 Benzidine Composite EPA 625 50 Less than ug/L 1 Benzo(a)anthracene Composite EPA 625 10 Less than ug/L 1 Benzo(a)pyrene , Composite EPA 625 10 Less than ug/L 1 3,4 benzofluoranthene Benno fl oranthene Composite EPA 625 10 Less than ug/L 1 Benzo(ghi)perylene Composite EPA 625 10 Less than ug/L 1 Benzo(k)fluoranthene Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethoxy) methane Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethyl) ether! Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroisopropyl) ether Composite EPA 625 10 Less than ug/L 1 Bis (2-ethylhexyl) ph ate Composite EPA 625 10 Less than ug/L 1 4-bromophenyl phenyl ether Composite EPA 625 10 Less than ug/L 1 Butyl benzyl phthalate Composite EPA 625 10 Less than ug/L 1 2-chloronaphthalene Composite EPA 625 10 Less than ug/ L 1 4-chlorophenyl phenyl ether Composite EPA 625 10 Less than ug/L 1 Form - DMR- PPA-1 Page 2 r INFLUENT Annual Monitoring and Pollutant Scan Permit No. NC0030210 Month November Outfall 001 Year 2015 Parameter sample Zype c Method uaa on Level amp a Result s o. Measurement um er o samples Base -neutral compo;; s (cont.) Chrysene Composite EPA 625 10 Less than ug/L 1 Di-n-butyl phthalate Composite EPA 625 10 Less than ug/L 1 Di-n-octyl phthalate Composite EPA 625 10 Less than ug/L 1 Dibenzo(a,h)anthracen Composite EPA 625 10 Less than ug/L 1 1,2-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 1,3-dichlorobenzene ! Composite EPA 625 10 Less than ug/L 1 1,4-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 3,3-dichlorobenzidine Composite EPA 625 10 Less than ug/L 1 Diethyl phthalate Composite EPA 625 10 Less than ug/L 1 Dimethyl phthalate Composite EPA 625 10 Less than ug/L 1 2,4-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 2,6-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 1,2-diphenylhydrazine j Composite EPA 625 10 Less than ug/L 1 Fluoranthene Composite EPA 625 10 Less than ug/ L 1 Fluorene Composite EPA 625 10 Less than ug/L 1 Hexachlorobenzene Composite EPA 625 10 Less than ug/L 1 Hexachlorobutadiene Composite EPA 625 10 Less than ug/L 1 Hexachlorocyclo-pent "ene Composite EPA 625 10 Less than ug/L 1 Hexachloroethane Composite EPA 625 10 Less than ug/L 1 Indeno(1,2,3-cdjpyrene Composite EPA 625 10 Less than ug/L 1 Isophorone Composite EPA 625 10 Less than ug/L 1 Naphthalene Composite EPA 625 10 Less than ug/L 1 Nitrobenzene Composite EPA 625 10 Less than ug/L 1 N-nitrosodi-n-propylan*e Composite EPA 625 10 Less than ug/ L 1 N-nitrosodimethylamine Composite EPA 625 10 Less than ug/L 1 N-nitrosodiphenylamine Composite EPA 625 10 Less than ug/L I Phenanthrene Composite EPA 625 10 Less than ug/L 1 Pyrene Composite EPA 625 10 Less than ug/L 1 1,2,4,-trichlorobenzene Composite EPA 625 10 1 Less than ug/L 1 I certify under penalty and supervision in accordance gather and evaluat th manage the system, or information submitte aware that there are possibility of fines an of law that this document and all attachments were prepared under my direction with a system to design to assure that qualified perdonnel properly information submitted. Based on my inquiry of the person or persons that those persons directly responsibel for gathering the information, the is , to the best of my knowledge and belief, true, accurate and complete. I am ignificant penalties for submitting false information, including the imprisonment for knowing violations. "o AutHorized Representative name ' f _ qSigna re Date Form - DMR- PPA-1 Page 3 Permit No. NCO030210 . Outm 001 j onk1 Facility Name Mallard Date of EFFLUENT Analytical Laboratory EFFLUENT Annual Monitoring and Pollutant Scan Month February Year 2016 TP ORC Mr. Darrell Dewitt 2 / 10/ 16, low level mercu 2219 /2016 Phone L704) 547-0680 ,: ti amp erg ,IC...sd_'.�+Y'.� is : t .-« rJit -�„��..iA"ss� .fi.�wri.�u`ir.^.-ra.ect'•�.+.1•!�:aY:sk" si cetn a ont r'� =3'r �+ %` .�'` Yh=���'.it��'_F[�'F: :' l+"1S � ��'�� ;Rwxdrvy �iY�i!�vi�� k.i•,"' ,' rc eas sement� 3 �'w1 ^-. .. �:" � .�sam �L: Ammonia (as N) Composite SM 4500-NH3-H-11 0.1 Less than mg/L 2 Dissolved oxygen Grab ASTM D888-09C 1.0 9.5 mg/L 1 Nitrate/Nitrite Composite EPA 353.2-93 1.0 15 mg/L 1 Total Kjeldahl nitrogept Composite EPA 351.2-93 0.25 1.1 mg/L 1 Total Phosphorus Composite SM 4500P-G-11 0.1 2.9 mg/L 1 Total'dissolved solids Composite SM 2540C-11 25 300 mg/L 1 Hardness Composite EPA 200.7 1.0 150 mg/L 1 Chlorine (total residual, TRC) Grab SM 4500C1-G-00 15 Less than ug/L 1 Oil and grease Grab EPA 1664B 5 Less than mg/L 1 ��i r_ • to " eCOVear w.alsatal+.ru �i�Y P• f le 'l' „f�ii~i�iae Z+t.. No.«+.wa..ta_r� _ Y C T.. F �►d/�ophendl� w.w.� .7 a- S A. • r / t '17 �r �`�. '1�., r �.'.' R ..te^-i .m+.wsecaawL..T.•,•`e..h.::=2��w�.s�.�.?�v:.'r},>1F�+-.'t�e�L.,. w��.�r;v-w:�,ta r . N _ ! * cv"�'� :rrf3;:��_�• �'�;.,,, -i: sr c .JF. tpq�Isp�': . . ��w'.� �f'y �i Y.` Ct,- �' �. Antimony Composite EPA 200.8 5.0 Less than ug/L 1 Arsenic Composite EPA 200.8 5.0 Less than ug/L 2 Beryllium Composite EPA 200.8 5.0 Less than ug/L 1 Cadmium Composite EPA 200.8 1.0 Less than ug/L 2 Chromium Composite EPA 200.8 5.0 Less than ug/L 2 Copper Composite EPA 200.8 2.0 2.5 ug/L 2 Lead Composite EPA 200.8 5.0 Less than ug/L 2 Mercury Grab EPA 1631E 1.0 Less than ng/L 1 Nickel Composite EPA 200.8 2.0 Less than ug/L 2 Selenium Composite EPA 200.8 5.0 Less than ug/L 2 Silver Composite EPA 200.8 5.0 Less than ug/L 2 Thallium Composite EPA 200.8 5.0 Less than ug/L 1 Zinc 1 Composite EPA 200.8 10 44 ug/L 2 Cyanide Grab 10-204-00-1-X 10 Less than ug/L 1 Total phenolic comp o s Grab EPA 420.2 0.05 Less than mg/L 1 U�t�eO�i'��y�YV� ��if"'--^ i..C...1`i•.......M.'A F-w "V .'; r T ��. �dwi r .. t 1z1- ' i "• s ' j 4.iay�. 4.J. .,.tN,•,: .J.'1 \c.,.•f..,1.Ya(I.I.::a+l`. �,: , Y ; ,: . V .vl d } n J x .r �v� o.+t! Sr jj-may- �rLlli Sl.a.{i;.w.-:F{�1 iL'G."1�:. T�� L;` �r ` 1 1, � �F i? ''�«e' +.-.a..T'L='..'.J....s'•r..�".ULNr..%'.Jl.N1�3a 1 � 7`YC � Y-��"-•.i �: -� * �' , �. t vl;�tl_t t�' �,_ x�. � -r t�, f' .f.,.�a:�'tY1.�.::J:.'C�.:�k' Acrolein Grab EPA 624 100 Less than ug/L 1 Acrylonitrile Grab EPA 624 100 Less than ug/L 1 Benzene Grab EPA 624 5 Less than ug/L 1 Bromoform Grab EPA 624 5 Less than ug/L 1 Carbon tetrachloride Grab EPA 624 5 Less than ug/L 1 Chlorobenzene Grab EPA 624 5 Less than ug/L 1 Chlorodibromomethane ibromochlo ethane Grab EPA 624 5 Less than ug/L 1 Chloroethane Grab EPA 624 10 Less than ug/L 1 2-chloroethylvinyl ether Grab EPA 624 10 Less than ug/L 1 Chloroform ) Grab EPA 624 5 Less than ug/L 1 Dichlorobromomethane romodichloromethane i Grab EPA 624 5 Less than ug/ L 1 1,1-dichloroethane Grab EPA 624 5 Less than ug/L 1 1,2-dichloroethane Grab EPA 624 5 Less than ' ug/L�rr 1 ans-1,2-dichloroethyl a Grab EPA 624 5 Less than ug/L 1 Form - DMR- PPA-� 1 Page 1 EFFLUENT Annual Monitoring and Pollutant Scan MWi Permit No. NCO030210 Outfall001 j Month February Year 2016 •.Y ..r..� }'...: LLFrameeTri.i.w. .._-.-.-. r,J'Y.vi�i._dr.�.. -. T T�Y...rL�.e. .t._. •.,.-+�� -.. ''S • 'f. Y. i ""tfi.:� 3 _ 4 Di .dj.e.. ._ th_._To• adir.7-roa��:.M..:+. UtaUon.11 ' h 1`Y� ti�.'';. Y ,L' emotvf. - ._�e.'."tii1"i :1'. �.a� l %gMie,ni l i' � t�el.sr, al�t o� cs: yd •:......,. •Ji SS. f. ^_ st..M-+Mi e- �"..a• '9 �Mt`s'1 ,�...�; uY r7, e1.ms;T..1"e um e_ro ��•c' .'�.i..�.V�ixor.t VIM'tW.o9Y +,�Qr 1�,� �UmL "n�' f:` Y_ s rv1z. �':� • 1_� .; �.. +.^t3 ' } ~fl i rI1�f . ' (.1'.d' ' �Y•+.Y✓Ki, .�1.. a. ..I.. •� ` .I .+ ..s•'... .+..a G. al/A�... I.HJwiT.� eL:1�..KLL.tR 'i.�'I• 1,1-dichloroethylene ; Grab EPA 624 5 Less thanc ug/L 1 1,2-dichloropropane Grab EPA 624 5 Less than ug/L 1 1,3-dichloropropylene Grab EPA 624 5 Less than ug/L 1 Ethylbenzene j Grab EPA 624 5 Less than ug/L 1 Methyl bromide(Bromo ethane) Grab EPA 624 10 Less than ug/L 1 Methyl chloride(Chloro*ethane) Grab EPA 624 10 Less than ug/L 1 Methylene chloride I Grab EPA 624 5 Less than ug/L 1 1, 1,2,2-tetrachloroethei ie Grab EPA 624 5 Less than ug/L 1 Tetrachloroethylene Grab EPA 624 5 Less than ug/L 1 Toluene Grab EPA 624 5 Less than ug/L 1 1, 1, 1-trichloroethane, Grab EPA 624 5 Less than ug/L 1 1,1,2-tdchloroethane Grab EPA 624 5 Less than ug/L 1 Trichloroethylene Grab EPA 624 5 Less than ug/L 1 Vinyl chloride Grab EPA 624 10 Less than lug/L 1 Ce"�-�'��"���•>rY ""+�p'�T']/� w ,Sf � r-'Gi:�r•iT_t` i r $^ '�k"7"�ti =;s `S� { i�.'.- VfVG��s..(�.� '..t f,� y i 1 r '","c r -,• } '. . •r ..nc • i �e d.v... +�r+►:.i,C...... .. 1.'. .th.'i..,.r.wv4.�::.;Syt'...7,�Y'nl`nw�:w�:...+:�x�..r.:tiara.iia±_.-..�Y.._.`...T,:ski-.'.:Cf•`,:a>��r:.:'Yid+7fiw .r. ta�,-.4t1' Y3� 3r'-�.:''�'•ti4 'y.�T.4F4'^ 1 . aL J•,.,, KU`.'.'�.,, Y1-�', cYb-'`°=L'tFitry�•- �F.a; i � .•'�3:�41 P-chloro-m-creso G (4-chloru-3-methylphenoll Composite EPA 625 10 Less than ug/L 1 2-chloropheriol Composite EPA 625 10 Less than ug/L 1 2,4-dichlorophenol ( Composite EPA 625 10 Less than ug/L 1 2,4-dimethylphenol Composite EPA 625 10 Less than ug/L 1 4,6-dinitro-o-cresol (4,6 Dfti itro-2-meth l henol) i Composite EPA 625 20 Less than ug/L 1 2,4-dinitrophenol Composite EPA 625 50 Less than ug/L 1 2-nitrophenol Composite EPA 625 10 Less than ug/L 1 4-nitrophenol Composite EPA 625 10 Less than ug/L 1 Pentachlorophenol Composite EPA 625 20 Less than ug/L 1 Phenol I Composite EPA 625 10 Less than ug/L 1 2,4,6-trichlorophenol i I Composite JEPA 625 10 Less than ug/L 1 1 .�.:..�+.'?a'+1iOT?RI.�..:�in.w7» '• -r ''.Y'F.s• n '^"'�` :^Y, ..ram '.;^v A - ;`:,r••7.�- rn.Y. ,wA._ S `�? r-W Base�enW. ' coin oun s -- _ --- "-- —�...r..� A�..l i .'Z� .:1... - �: +. c.::&•ia.•.:'„v.tie........':..k:,k�`:,r�.r'L+�o:.:�Z..ei�.r'iir,'.i,�v�ijJ3dri:�,�[%.t<.CL1.',d'�tSYL'3�,��R�.--ti.a'�7 t. y.i .!'.vP f .'.ra-,r. Acenaphthene Composite EPA 625 10 Less than ug/L 1 Acenaphthylene Composite EPA 625 10 Less than ug/L• 1 Anthracene j Composite EPA 625 10 Less than ug/L 1 Benzidine Composite EPA 625 50 Less than ug/L 1 Benzo(a)anthracene Composite EPA 625 10 Less than ug/L 1 Benzo(a)pyrene Composite EPA 625 10 Less than ug/L 1 3,4 benzofluoranthene enzo fluoran ene j !! Composite EPA 625 10 Less than ug/L 1 Benzo(ghi)perylene Composite EPA 625 10 Less than ug/L 1 Benzo(k)fluoranthene ' Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethoxy) mean Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethyl) ether's Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroisopropyl)her Composite EPA 625 10 Less than ug/L 1 Bis (2-ethylhexyl) phthalate Composite EPA 625 10 Less than ug/L 1 4-bromophenyl phenyl efher Composite EPA 625 10 Less than ug/L 1 Butyl benzyl phthalate ') Composite EPA 625 10 Less than ug/L 1, 2-chloronaphthalene ! Composite EPA 625 10 Less than ug/L 1 4-chlorophenyl phenyl elder Composite EPA 625 10 Less than ug/L 1 . i Form - DMR- PPX-1 Page 2 EFFLUENT Annual Monitoring and Pollutant Scan /Ift Permit No. NCO030210 Outfall001 j Month February Year 2016 Paraideter +tt'�—•tl. _•. i..1d_7.. amp a 1pe .i _. Method l_ uaa a oa Level a ..1r .�,•I. .L� 1 am a-= Result \-• ,.e. ..3..•.. �F o ,° 'L Mea oremeat, i.,'.a�rif�t4.+t``i.'•�..4r+�.. um eVo •. ;sa�mIes, .3, _ .r .•tea .. ..��p. i�t "f .Y �ht.wL.,'; ,,r '1rr.P �`}:,L•W.rery. t ase-neutral" rrom7a;,+ o } .w.Yy IG>+.=I j./rr .s.11�`1�3+.. B •., 4-•. r. .. ,4 1+1 A \i(4 ( .11 !rh- '1f M1.- .'^'.•i. �tAS +•+.——w�Li:.^I^^.. 1 � r (. ",4 rLf� � 1 � � is 1 •. 4� it -i\ kl ! i `h.t 4 S � yi ' 1•— •'. d8' Moat. 1 i k ; t yy• 1 } .� �1 .r r Ya t , � raF� r • H.�yyy����' `�� 3T � �`�+ •h x`i��i��'a; �� —.S. 1. f..a.1.1-.: ..j.. ..�,i.. .1.V- ..r.:l'.3, iXt. at.. .••,0i+!'.J.rNi.t.fW'L'i�j :.. %as:r,1�1._.rk Chrysene I Composite EPA 625 10 Less than ug/L 1 Di-n-butyl phthalate ) Composite EPA 625 10 Less than ug/L 1 Di-n-octyl phthalate Composite EPA 625 10 Less than ug/L 1 Dibenzo(a,h)anthracen Composite EPA 625 10 Less than ug/L 1 1,2-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 1,3-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 1,4-dichlorobenzene j Composite EPA 625 10 Less than ug/L 1 3,3-dichlorobenzidine Composite EPA 625 10 Less than ug/L 1 Diethyl phthalate Composite EPA 625 10 Less than ug/L 1 Dimethyl phthalate Composite EPA 625 10 Less than ug/L 1 2,4-dinitrotoluene I Composite EPA 625 10 Less than ug/L 1 2,6-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 1,2-diphenylhydrazine Composite EPA 625 10 Less than ug/L 1 Fluoranthene Composite EPA 625 10 Less than ug/L 1 Fluorene Composite EPA 625 10 Less than ug/L 1 Hexachlorobenzene ) Composite EPA 625 10 Less than ug/L 1 Hexachlorobutadiene G Composite EPA 625 10 Less than ug/L 1 Hexachlorocyclo-penta*ene Composite EPA 625 10 Less than ug/L 1 Hexachloroethane Composite EPA 625 10 Less than ug/L 1 Indeno(1,2,3-cd)pyrene j Composite EPA 625 10 Less than ug/L 1 Isophorone Composite EPA 625 10 Less than ug/L 1 Naphthalene Composite EPA 625 10 Less than ug/L 1 Nitrobenzene ` Composite EPA 625 10 Less than ug/L 1 N-nitrosodi-n-propyla*e Composite EPA 625 10 Less than ug/L 1 N-nitrosodimethylamin' Composite EPA 625 10 Less than ug/L 1 N-nitrosodiphenylamin� Composite EPA 625 10 Less than ug/L 1 Phenanthrene Composite EPA 625 10 Less than ug/L 1 Pyrene Composite EPA 625 10 Less than g/L 1 1,2,4,-trichlorobenzene Composite EPA 625 10 Less than +ug/L 1 I certify under penalty and supervision in acTordance gather and evaluat tht manage the system, o1r information submitted aware that there are possibility of fines an of law that this document and all attachments were prepared under my direction with a system to design to assure that qualified perdonnel properly information submitted. Based on my inquiry of the person or persons that those persons directly responsibel for gathering the information, the is , to the best of my knowledge and belief, true, accurate and complete. I am gnificant penalties for submitting false information, including the imprisonment for knowing violations. Au orized Representative name gli6aaiure / 31A(-)/ Late Form - DMR- PPA41 i i Page 3 INFLUENT Annual Monitoring and Pollutant Scan Permit No. NCO030210 Month February Outfall 001 Year 2016 Facility Name Mallard Creek WWTP ORC Mr. Darrell Dewitt Date of INFLUENT Sampling 2 /9/ 16 Phone (704) 547-0680 Analytical Laboratory: _ HARLOTTE WATER Environmental Lab NC 192, Prism Lab NC 402 Ammonia (as N) Composite SM 4500-NH3-H-11 1.0 30 mg/L 2 Dissolved oxygen Grab ASTM D888-09C n/a n/a mg/L 0 Nitrate/Nitrite Composite EPA 353.2-93 0.05 Less than mg/L 1 Total Kjeldahl nitrogen Composite EPA 351.2-93 2.5 40 mg/L 1 Total Phosphorus Composite SM 4500P-G-11 0.1 5.2 mg/L 1 Total dissolved solids Composite SM 254OC-11 n/a n/a mg/L 0 Hardness Composite EPA 200.7 n/a n/a mg/L 0 Chlorine (total residual,E TRC) Grab SM 4500C1-G-00 n/a n/a ug/L 0 Oil and grease Grab EPA 1664B 5.0 28 mg/L 1 Antimony Composite EPA 200.8 5.0 Less than ug/L 1 Arsenic Composite EPA 200.8 5.0 Less than ug/L 1 Beryllium Composite EPA 200.8 5.0 Less than ug/L 1 Cadmium j Composite EPA 200.8 1.0 Less than ug/L 1 Chromium { Composite EPA 200.8 5.0 Less than ug/L 1 Copper Composite EPA 200.8 2.0 18 ug/L 1 Lead Composite EPA 200.8 5.0 Less than ug/L' 1 Mercury Composite EPA 245.1 0.2 Less than ug/L 1 Nickel Composite EPA 200.8 2.0 3.0 ug/L I Selenium Composite EPA 200.8 5.0 Less than ug/L 1 Silver Composite EPA 200.8 5.0 Less than ug/L 1 Thallium ! Composite EPA 200.8 5.0 Less than ug/L 1 Zinc Composite EPA 200.8 10 110 ug/L 1 Cyanide Grab 10-204-00-1-X 10 Less than ug/L 1 Total phenolic compouri s Grab EPA 420.2 0.050 0.064 mg/L 1 Tp' •G' f^ '4.1.• x 7.. i. iy^: .`t.'V. '2e+R •eZ.sa \"V i fL i l.- r w �� ■�� 'Yt y- J,,� y°'.i: 5'•+t"�=f' y'T! 3.. `"4 0. �_e o'Oga%cf�c In Yi•��}• : , i.l..rfr t.3�..._. .fnil+l i i' k 1T �� ,fi r'+ ki{ter } . t�tAA�K � idCWS. I.M� ca 5 . �'. .•.yi y Tti' °�°'�`.- �.�^�s� } }��!* Od 1r"Nvw G3tlL¢;:L4 ��-i�.�i.T��V+'hiiirit Acrolein Grab EPA 624 100 Less than ug/L 1 Acrylonitrile Grab EPA 624 100 Less than ug/L 1 Benzene Grab EPA 624 5 Less than ug/L 1 Bromoform Grab EPA 624 5 Less than ug/L 1 Carbon tetrachloride Grab EPA 624 5 Less than ug/L 1 Chlorobenzene Grab EPA 624 5 Less than ug/L 1 Chlorodibromomethane ibmmochloromethane Grab EPA 624 5 Less than ug/L 1 Chloroethane Grab EPA 624 10 Less than ug/L 1 2-chloroethylvinyl ether Grab EPA 624 10 Less than ug/L 1 Chloroform j Grab EPA 624 5 Less than ug/L 1 Dichlorobromomethane (Bromodichloromethanel Grab EPA 624 5 Less than ug/L 1 1,1-dichloroethane Grab EPA 624 5 Less than ug/L 1 1,2-dichloroethane '; Grab EPA 624 5 Less than ug/L 1 ans-1,2-dichloroethylOne Grab EPA 624 5 Less than ug/L 1 Form - DMR- PPA-1 Page 1 INFLUENT Annual Monitoring and Pollutant Scan Permit No. NCO030210 Outfa a 001 Month February Year 2016 r i er, �Pn •a.�r»�a+tm';i^.�.fie' tc? rt' _ t 3? _y}.z,.�: i - r_E ' �1 _ :tp 8" , uaa a on ?,CEE►p,es�,,.�yt,, Y, ..r'4_�MMr"e; : ��ao�j.'d, Sir�} `t �s�, d Yi3? w`�'.YSi�'l`r�'-�.e'-v`e.yTj�"'1 srr F� ist� .:est•++�i�:.oa.ic .:i 4 ' "' ,� �i t .t .i.. ��i ii�'c r..'.� ::.SRL�a�,i�m"`�s,..up_ 4l2ta�n ., i �.7 .....�:.�r.,:,.t�i" t'9-oZi w yP1+Y- :.rn�.sc?+Ft }:G:�.b: V .. oo.wa.^c+.y«� �Gf.SrLn ..w f,. . r..v.:'�i"T.�Y.'k,Li. i s_.h. �T�-hi t4' n...Gi�.l �: J< '7' •[f �' P,yY 1,1-dichloroethylene Grab EPA 624 5 Less than ug/L 1 1,2-dichloropropane Grab EPA 624 5 Less than ug/L I 1,3-dichloropropylene' Grab EPA 624 5 Less than ug/L 1 Ethylbenzene Grab EPA 624 5 Less than ug/L 1 Methyl bromide(Brom methane) Grab EPA 624 10 Less than ug/L 1 Methyl chloride(Chlor methane) Grab EPA 624 10 Less than ug/L 1 Methylene chloride { Grab EPA 624 5 Less than ug/L 1 1,1,2,2-tetrachloroethi6ie Grab EPA 624 5 Less than ug/L 1 Tetrachloroethylene Grab EPA 624 5 Less than ug/L 1 Toluene j Grab EPA 624 5 Less than ug/L 1 1, 1, 1-trichloroethane Grab EPA 624 5 Less than ug/L 1 1,1,2-trichloroethane { Grab EPA 624 5 Less than ug/L 1 Trichloroethylene j Grab EPA 624 5 Less than ug/L 1 Vinyl chloride Grab JEPA 624 10 Less than ug/L 1 iT!•IJ�'�i�i �.K��.l1R� o�d.Jl�o u,':Ld-.r.Y.�t �_ idnr.Qra. � w.�S....7tia�3: 3„�, .L- Y.:!tyt+.s'1�t.,.J.�13::T���.L'Jlt.3..��1FW$n:.��d_'7L'S�i�YJ:.r .,�tS�`"_'..S !�:`ai:ASI'S .'^'�•x" . P-chloro-m-creso Wcbloro-3-methylbhenoll Composite EPA 625 10 Less than ug/L 1 2-chlorophenol Composite EPA 625 10 Less than ug/L 1 2,4-dichlorophenol Composite EPA 625 10 Less than ug/L 1 2,4-dimethylphenol Composite EPA 625 10 Less than ug/L 1 4,6-dinitro-o-cresol 4 6-Dinitro-2-meth 1phenol) Composite EPA 625 20 Less than ug/L 1 2,4-dinitrophenol j Composite EPA 625 50 Less than ug/L 1 2-nitrophenol Composite EPA 625 10 Less than. ug/L 1 4-niirophenol Composite EPA 625 10 Less than ug/L 1 Pentachlorophenol Composite EPA 625 20 Less than ug/L 1 Phenol Composite EPA 625 10 15 ug/L 1 2,4,6-trichlorophenol Composite EPA 625 10 Less than I ug/L 1 s c `_. 1' r+.., cT ,�5"T�'a i w'^7' `- t r 'R-`�sr-3!o•r� Bas a 'bAO [t N+J is3::fi:4 yiC.�'��l�`%':.Sr�'����.�r�.�1:C::13y4{il �.��i...13-�t.rR "7if , fin. •-.-.^ .i"i.AwY�+.ii+3f..1'ti:+.75� l (x `� �'q,`.'.' rh''it .., w.S�. �'�'�!�.iM •`�' �3+C����'.. Acenaphthene Composite EPA 625 10 Less than ug/L 1 Acenaphthylene i Composite EPA 625 10 Less than ug/L 1 Anthracene Composite EPA 625 10 Less than ug/L 1 Benzidine Composite EPA 625 50 Less than ug/L 1 Benzo(a)anthracene Composite EPA 625 10 Less than ug/L 1 Benzo(a)pyrene Composite EPA 625 10 Less than ug/L 1 3,4 benzofluoranthene enzo fluoranthene Composite EPA 625 10 Less than ug/L 1 Benzo(ghi)perylene j Composite EPA 625 *10 Less than ug/L 1 Benzo(k)fluoranthene Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethoxy) metihane Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroethyl) ether, Composite EPA 625 10 Less than ug/L 1 Bis (2-chloroisopropyl) e, er Composite EPA 625 10 Less than ug/L 1 Bis (2-ethylhexyl) phthalate Composite EPA 625 10 Less than ug/L 1 4-bromophenyl phenyl ether Composite EPA 625 10 Less than ug/L 1 Butyl benzyl phthalate Composite EPA 625 10 Less than ug/L 1 2-chloronaphthalene Composite EPA 625 10 Less than ug/L 1 4-chlorophenyl phenyl ether Composite EPA 625 10 1 Less than ug/L 1 Form - DMR- PPA 1 Page 2 INFLUENT Annual Monitoring and Pollutant Scan Permit No. NCO030210 Month February Outfall 001 Year 2016 Pasaaie ei, s .1, : i� Bas"�aeii$ial com p s a ont ztb a r -� >�. �! .,, Method ,b j �TYP � Level�Menienieat u�§dsi �:-�.�'�. .tF'l�i.�i� t•'t}•'T��� i'Y-i!t g/L.•�'Y ►...w•.n..�w.+... J. .:,:! i- .. t. i. . t. �t +,-- :•.i+.i.. ", ....1..Y.� > 4. rho ; 'Y..H ,+' azples �� sn 1 . Chrysene Composite EPA 625 10 Less than ug/L 1 Di-n-butyl phtMate:1 Composite EPA 625 10 Less than ug/L 1 Di-n-octyl phthalate Composite EPA 625 10 Less than ug/L 1 Dibenzo(a,h)anthracei a Composite EPA 625 10 Less than ug/L 1 1,2-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 13-6chlorobenzene Composite EPA 625 10 Less than ug/L 1 1,4-dichlorobenzene Composite EPA 625 10 Less than ug/L 1 3,3-dichlorobenzidine Composite EPA 625 10 Less than ug/L 1 Diethyl phthalate Composite EPA 625 10 Less than ug/L 1 Dimethyl phthalate Composite EPA 625 10 Less than ug/L 1 2,4-dinitrotoluene Composite EPA 625 10 Less than ug/L 1 2,6-dinitrotoluene ' Composite EPA 625 10 Less than ug/L 1 1,2-dipheny1hydrazine! Composite EPA 625 10 Less than ug/L 1 Fluoranthene Composite EPA 625 10 Less than ug/L 1 Muorene Composite EPA 625 10 Less than ug/L 1 Hexachlorobenzene I Composite EPA 625 10 Less than ug/L 1 Hexachlorobutadiene Composite EPA 625 10 Less than ug/L 1 Hexachlorocyclo-pentaoiene Composite EPA 625 10 Less than ug/L 1 Hexacbloroethane Composite EPA 625 10 Less than ug/L 1 Indeno(1,2,3-cd)pyrene; Composite EPA 625 10 Less than ug/L 1 Isophorone Composite EPA 625 10 Less than ug/L Naphthalene i Composite EPA 625 10 Less than ug/L 1 Nitrobenzene Composite EPA 625 10 Less than ug/L 1 N-nitrosodi-n-propylanone Composite EPA 625 10 Less than ug/L 1 N-nitrosodimethylaminl Composite EPA 625 10 Less than ug/L 1 N-nitrosodiphenylamine Composite EPA 625 10 Less than ug/L 1 Phenanthrene Composite EPA 625 10 Less than ug/L 1 Pyrene Composite EPA 625 1 10 Less than ug/L 1 1,2,4,-trichlorobenzene Composite EPA 625 10 Less thanlug/L 1 i I certify under penaltv' of law that this document and all attachments were prepared under my direction and supervision in accordance with a system to design to assure that qualified perdonnel properly gather and evaluat the information submitted. Based on my inquiry of the person or persons that manage the system, or those persons directly responsibel for gathering the information, the information submitted is , to the best of my knowledge and belief, true, accurate and complete. I am aware that there are 11gnificant penalties for submitting false information, including the -issibility of fines and imprisonment for knowing violations. Authorized Representative name i S' re Date Page 3 %w- Annual Monitoring and Pollutant Scan Permit No. NCO030210 Outfall 001 FaciUty Name: Mallard Creek WWTP ORC Mr. Darrell Dewitt Date of EFFLUENT sa�I npling : 511012017, 519 Low level mercury Phone (704) 547-0680 Analytical Laboratory.- CHARLOTTE WATER Environmental Lab --NC 192: and Prism Lab NC 402 Month May Year 2017 arameter OP M -- 4MPI 17 x e Ammonia (as N) C0610 Composite SM 4500-NH3-H-1 1 0.10 Less than mg/L Chlorine (total residual, TRC) 50060 Grab Hach 10014ULR 15 Less than ug/L Dissolved Oxygen 00300 Grab ASTM D888-09C 1.0 8.5 mg/L Nitrite plus Nitrate Total (as N) 00630 Composite EPA 353.2-93 1 13 mg/L Total Kjeldahl Nitroge 00625 Composite EPA 351.2-93 0.25 0.6 mg/L Oil and Grease 00556 Grab EPA 1664B 5 Less than mg/L Total Phosphorus C0665 Composite SM 4500P-H- 11 0.10 2.20 mg/L Total Dissolved Solids 70295 Composite SM 2540C- 11 25 320 jmg/L Hardness 00900 Composite EPA 200.7 1.0 130 ;nr .6 mg/L Antimony 01097 Composite EPA 200.8 5.0 Less than ug/L Arsenic 01002 Composite EPA 200.8 5.0 Less than ug/L Beryllium 01012 Composite EPA 200.7 2.0 Less than ug/L Cadmium 01027 Composite EPA 200.8 1.0 Less than ug/L IChromium 01034 Composite EPA 200.8 5.0 Less than ug/L Copper 01042 Composite EPA 200.8 2.0 3.8 ug/L Lead 01051 Composite EPA 200.8 5.0 Less than ug/L Mercury (Method 16310) COMER Grab EPA 1631E 1.0 Less than. ng/L Nickel 01067 Composite EPA 200.8 2.0 Less than ug/L Selenium 01147 Composite EPA 200.8 5.0 Less than ug/L Silver 01077 Composite EPA 200.8 5.0 Less than ug/L Thallium, 01059 Composite EPA 200.8 5.0 Less than ug/L Zinc 01092 Composite EPA 200.8 10 40 ug/L Cyanide 00720 Grab 10-204-00-I-X 10 Less than lug/L Total phenolic compounds 32730 Grab EPA 420.2 0.050 Less than mg/L organic-, Acrolein 34210 Grab EPA 624 100 Less than ug/L Acrylonitrile 34215 Grab EPA 624 100 Less than ug/L Benzene 34030 Grab EPA 624 5 Less than ug/L Bromoform 32104 Grab EPA 624 5 Less than ug/L Carbon Tetrachloride j 32.102 Grab EPA 624 5 Less than ug/L Chlorobenzene 34301 Grab EPA 624 5 Less than ug/L Chlorodibromomethane 34306 Grab EPA 624 5 Less than ug/L Chloroethane 85811 Grab EPA 624 10 Less than ug/L 2-chloroethyl vinyl ethex 34576 Grab EPA 624 10 Less than ug/L Chloroform i 32106 Grab EPA 624 5 Less than ug/L ichlorobromomethane 32101 Grab EPA 624 5 Less than ug/L I 1-dichloroethane 34496 Grab EPA 624 5 Less than ug/L 1 12.- d.ichloro eth ane 32103 Grab EPA 624 5 Less than ug/L Trans- 1,2-dichloroethylene 34546 Grab EPA 624 5 Less than ug/L Form - DMR- PPA-1 Page 1 r Q� Annual Monitoring and Pollutant Scan Permit No. NCO0302 10 Outfall 001 Month May Year 2017 Awk we" Parameter Sample ' y Afiid" d6dl t h"0A. Qi1aldtibitiOW, �-,S ample Units of 77 1, 1-dichloroethylene 34501 Grab EPA 624 5 Less than ug/L 1,2-dichloropropane 34541 Grab EPA 624 5 Less than ug/L 1,3-dichloropropylene, 77163 Grab EPA 624 5 Less than ug/L Ethylbenzene 34371 Grab EPA 624 5 Less than ug/L Methyl Bromide 34413 Grab EPA 624 10 Less than ug/L Methyl Chloride 34418 Grab EPA 624 10 Less than ug/L Methylene Chloride j 34423 Grab EPA 624 5 Less than ug/L 1, 1,2,2-tetrachloroethane 81549 Grab EPA 624 5 Less than ug/L Tetrachloroethylene 34475 Grab EPA 624 5 Less than ug/L Toluene 34010 Grab EPA 624 5 Less than ug/L 1, 1, 1 -trichloroethane 34506 Grab EPA 624 5 Less than ug/L 11 1,2-trichloroethane 34511 Grab EPA 624 5 Less than ug/L Trichloroethylene 39180 Grab EPA 624 5 Less than ug/L Vinyl Chloride 39175 Grab EPA 624 10 Less than ug/L g 5" P-chloro-m-creso 34452 Composite EPA 625 10 Less than ug/L 2-chlorophenol 34586 Composite EPA 625 10 Less than ug/L 2,4-dichlorophenol 34601 Composite EPA 625 10 Less than ug/L 2,4-dhnethylphenol 34606 Composite EPA 625 10 Less than ug/L 44,6-dinitro-o-cresol 34657 Composite EPA 625 20 Less than ug/L 2,4-dinitrophenol 34616 Composite EPA 625 50 Less than ug/L 2-nitrophenol 34591 Composite EPA 625 10 Less than ug/L 4-nitrophenol 34646 Composite EPA 625 10 Less than ug/L Pentachlorophenol j 39032 Composite EPA 625 20 Less than ug/L Phenol 34694 Composite EPA 625 10 Less than_Lug/L 2,4,6-tdchlorophenol 34621 Composite EPA 625 10 Less than lug/L POMPm; Acenaphthene 34205 Composite EPA 625 10 Less than ug/L Acenaphthylene 34200 Composite EPA 625 10 Less than ug/L Anthracene J CO220 Composite EPA 625 10 Less than ug/L Benzidine j 39120 Composite EPA 625 so Less than ug/L Benzo(a)anthracene 34526 Composite EPA 625 10 Less than ug/L Benzo(a)pyrene 34247 Composite EPA 625 10 Less than ug/L 3,4 benzofluoranthene 34230 Composite EPA 625 10 Less than ug/L Benzo(ghi)perylene 34521 Composite EPA 625 10 Less than ug/L Benzo(k)fluoranthene i 34242 Composite EPA 625 10 Less than ug/L Bis (2-chloroethoxy) methane 34278 Composite EPA 625 10 Less than ug/L Bis (2-chloroethyl) ether, 34273 Composite EPA 625 10 Less than ug/L Bis (2-chloroisopropyl) ether 34283 Composite EPA 625 10 Less than ug/L Bis (2-ethylhexyl) phIh!Vte 39100 Composite EPA 625 10 Less than ug/L 4,-bromophenyl phenyl er 34636 Composite EPA 625 10 Less than ug/L utyl benzyl phthalate 34292 Composite EPA 625 10 Less than ug/L 2-chloronaphthalene 34581 Composite EPA 625 .10 Less than ug/L 4-chlorophenyl phenyl ether 34641 Composite EPA 625 10 Less than ug/L Chrysene 34320 Composite EPA 625 10 1 Less than jug/L Form - DMR- PPA-1 Page 2 W Permit No. NCO030210 Outfall 001 Annual Monitoring and Pollutant Scan Month May Year 2017 _ Parameter i ' Parameter Code Sample Ty 'e P Amid tidal Metiod Quantitatioa Lapel '.Sample Result Units?of leasur meal ' Di-n-butyl phthalate i 39110 Composite EPA 625 10 Less than ug/L Di-n-octyl phthalate ' 34596 Composite EPA 625 10 Less than ug/L Dibenzo(a,h)anthrac a 34556 Composite EPA 625 10 Less than ug/L 1,2-dichlorobenzene 34536 Composite EPA 625 10 Less than ug/L 1,3-dichlorobenzene 34566 Composite EPA 625 10 Less than ug/L 1,4-dichlorobenzene ! 34571 Composite EPA 625 10 Less than ug/L 3,3-dichlorobenzidine 34631 Composite EPA 625 10 Less than ug/L Diethyl phthalate 34336 Composite EPA 625 10 Less than ug/L Dimethyl phthalate 34341 Composite EPA 625 10 Less than ug/L 2,4-dinitrotoluene 34611 Composite EPA 625 10 Less than ug/L 2,6-dinitrotoluene C0626 Composite EPA 625 10 Less than ug/L 1,2-diphenylhydrazine 34346 Composite EPA 625 10 Less than ug/L Fluoranthene C0376 Composite EPA 625 10 Less than ug/L Fluorene 34381 Composite EPA 625 10 Less than ug/L Hexachlorobenzene C0700 Composite EPA 625 10 Less than ug/L Hexachlorobutadiene j 39702 Composite EPA 625 10 Less than ug/L Hexachlorocyclo-pentadiene 34386 Composite EPA 625 10 Less than ug/L Hexachloroethane 34396 Composite EPA 625 10 Less than ug/L Indeno(1,2,3-cd)pyrene 34403 Composite EPA 625 10 Less than ug/L Isophorone 34408 Composite EPA 625 10 Less than ug/L Naphthalene 34696 Composite EPA 625 10 Less than ug/L Nitrobenzene , 34447 Composite EPA 625 10 Less than ug/L N-nitrosodi-n-propylmx4ne 34428 Composite EPA 625 10 Less than ug/L N-nitrosodimethylaminp 34438 Composite EPA 625 10 Less than ug/L N-nitrosodiphenylaxnine 34433 Composite EPA 625 10 Less than ug/L Phenanthrene 34461 Composite EPA 625 10 Less than ug/L Pyrene 34469 Composite EPA 625 10 Less than ug/L 1,2,4,-trichlorobenzene; 34551 Composite EPA 625 10 Less than ug/L "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Authorized Representative name SignaVure 6o // t,!5�4-01 s-7 - Date Form - DMR- PPA 1 Page 3 Annual Monitoring and Pollutant Scan Permit No. NCO030210 Month May /Vtl� Outfall 001 Year 2017 Facility Name: Mallar Creek WWTP ORC Mr. Darrell Dewitt Date of INFLUENT s pling: 5/9/2017 Phone (704) 547-0680 Analytical Laborato CHARLOTTE WATER Environmental Lab --NC 192: and Prism Lab NC 402 Gi r -� P rame : r u�T-.zan.r....::..+.as_. '...?..:k.ac.'`t. i ..>T Paraete, _"'Code; ..a.1::,4:e�.�hsc�:r..e: r•,a Sample . , ;-r' "i�.:.a4s•�``,e MEW - scr.>..nc.,.iwKa..:aa± %I:aa>_+.. TMAnatytical «..;.'�'"`b:'.#L.� �. ri«r. ..ra:.r.. ,Qgarititatioa t... mz..., 1+i. :GC. .w1 SampleIIaits,o7 tr:..:,.. �` :z as ement., s Ammonia (as N) C0610 Composite SM 4500-NH3-H-11 1.0 33 mg/L Chlorine (total residual, TRC) 50060 Grab HgLch 10014ULR 15 N/A ug/L Dissolved Oxygen 1 00300 Grab ASTM D888-09C 1.0 N/A mg/L Nitrite plus Nitrate To (as N) 00630 Composite EPA 353.2-93 0.05 Less than mg/L Total Kjeldahl Nitroge 00625 Composite EPA 351.2-93 2.5 46 mg/L Oil and Grease 00556 Grab EPA 1664B 5.0 21 mg/L Total Phosphorus C0665 Composite SM 4500P-H-11 0.10 5.40 mg/L Total Dissolved Solids 70295 Composite SM 2540C-11 25 N/A mg/L Hardness 00900 Composite EPA 200.7 1.0 N/A mg/L '.T :: ur+'1•. w'MS.''✓=-s�K.` - '"v1'•ssc<: �otalzrecove1..:r--.e) yanidandtotalpheuo c '.: y+.'tA ;a,+.If. $j'Ya$•Y. y�u.+:sF,!' _ 14 3fi �.,-cf"k. G t T T 7 t _ _:'Grt' 7Y..=k k_.ii 3 t d r �::.`3�� rj �Y? ti.Jy?•'' 3` at '.1i.2::-k:.i;.-�+'.�'� �.�. Antimony j 01097 Composite EPA 200.8 5.0 Less than ug/L Arsenic 01002 Composite EPA 200.8 5.0 Less than ug/L Beryllium 01012 Composite EPA 200.7 5.0 Less than ug/L Cadmium 01027 Composite EPA 200.8 1.0. Less than ug/L Chromium 01034 Composite EPA 200.8 5.0 Less than ug/L Copper 01042 Composite EPA 200.8 2.0 17 ug/L Lead 01051 Composite EPA 200.8 5.0 Less than ug/L Mercury COMER Composite EPA 245.1 0.2 Less than ug/L Nickel 01067 Composite EPA 200.8 2.0 3.4 ug/L Selenium 01147 Composite EPA 200.8 5.0 Less than ug/L Silver 01077 Composite EPA 200.8 5.0 Less than ug/L Thallium 01059 Composite EPA 200.8 5.0 Less than ug/L Zinc 01092 Composite EPA 200.8 50 93 ug/L Cyanide l 00720 Grab 10-204-00-i-X 10 Less than ug/L Total phenolic compounds 32730 Grab EPA 420.2 0.050 0.060 mg/L � i•'t .>.-_ Sy 1 ..{ IY . - +.. t. a c Y � i ?. +r. +.�: .�'t �k :j_,'.,tirr '-,7 ..'�`� 1}. .�i?`?• .X.�I''+s �.::. 4 } t1 1.,. T.. J '! ? . 2 �i� � U i 1 .� Y•�,' .sNaA'.CiopxMr.1..I. ). L• .0 :' <.4v. V�,tiieosganc compuads Acrolein 34210 Grab EPA 624 100 Less than ug/L Acrylonitrile 34215 Grab EPA 624 100 Less than ug/L Benzene 34030 Grab EPA 624 5 Less than ug/L Bromofonn 32104 Grab EPA 624 5 Less than ug/L Carbon Tetrachloride 32102 Grab EPA 624 5 Less than ug/L Chlorobenzene ! 34301 Grab EPA 624 5 Less than ug/L Chlorodibromomethane 34306 Grab EPA 624 5 Less than ug/L Chloroethane 85811 Grab EPA 624 10 Less than ug/L 2-chloroethyl vinyl ether 34576 Grab EPA 624 10 Less than ug/L Chloroform 32106 Grab EPA 624 5 Less than ug/L ichlorobromomethane ., 32101 Grab EPA 624 5 Less than ug/L 1, 1 -dichloroethane 34496 Grab EPA 624 5 Less than ug/L 1,2-dichloroethane 32103 Grab EPA 624 5 Less than ug/L Trans-1,2-dichloroethylene 34546 Grab EPA 624 5 Less than ug/L Form - DMR- PPA-1 Page 1 W GO - Annual Monitoring and Pollutant Scan Permit No. NCO030210 Outfall 001 Month May Year 2017 ' = Parameter z w72- Paameter r Code Saar -1e tL`ype Ana ical t jMeod uaniritatio Levelesu Sample Unifs'of�, _ to r.:gy�rn,�� Measurement 1,1-dichloroethylene 34501 Grab EPA 624 5 Less than ug/L 1,2-dichloropropane 34541 Grab EPA 624 5 Less than ug/L 1,3-dichloropropylene 77163 Grab EPA 624 5 Less than ug/L Ethylbenzene ' 34371 Grab EPA 624 5 Less than ug/L Methyl Bromide 34413 Grab EPA 624 10 Less than. ug/L Methyl Chloride 34418 Grab EPA 624 10- Less than ug/L Methylene Chloride 34423 Grab EPA 624 5 Less than ug/L 1,1,2,2-tetrachloroethane 81549 Grab EPA 624 5 Less than ug/L Tetrachloroethylene I 34475 Grab EPA 624 5 Less than ug/L Toluene ! 34010 Grab EPA 624 5 Less than ug/L 1, 1, 1-trichloroethane 34506 Grab EPA 624 5 Less than ug/L 1,1,2-trichloroethane 34511 Grab EPA 624 5 Less than ug/L Trichloroethylene 39180 Grab EPA 624 5 Less than ug/L Vinyl Chloride I -39175 Grab EPA 624 10 Less than ug/L a-�� ��.� - ::ti�:rk..�c'�� c: .;. r . :4 '� ` - ' .7 `� i . i `�,. �•��a�i : iF�� "Y 3 � e,� ra ���.eS�'','L.,. } cad etractatile.4compouiids�...wr.....�... P-chloro-m-creso j 34452 Composite EPA 625 10 Less than ug/L 2-chlorophenol 34586 Composite EPA 625 10 Less than ug/L 2,4-dichlorophenol 34601 Composite EPA 625 10 Less than ug/L 2,4-dimethylphenol 34606 Composite EPA 625 10 Less than ug/L 4,6-dinitro-o-cresol 34657 Composite EPA 625 20 Less than ug/L 2,4-dinitrophenol 34616 Composite EPA 625 50 Less than ug/L 2-nitrophenol 34591 Composite EPA 625 10 Less than ug/L 4-nitrophenol 34646 Composite EPA 625 10 Less than ug/L Pentachlorophenol J 39032 Composite EPA 625 20 Less than ug/L Phenol 34694 Composite EPA 625 10 12 ug/L 2,4,6-trichlorophenol 34621 Composite EPA 625 10 Less than ug/L . Yu Sase-neutral .aM.�-tw:�.�.-�r�.4msa,:. �,-s.i.. .<. .cw-r...a--..w ...,,,.. �.. a w....,..: .... .... ,.... il.. ,.' .. '.'.x. ... ..:+ r ... : ....L:...��.b..1`:t•'.��` .-.i..,ii. -..+$an �,:,c . _i Acenaphthene 34205 Composite EPA 625 10 Less than ug/L Acenaphthylene I 34200 Composite EPA 625 10 Less than ug/L Anthracene CO220 Composite EPA 625 10 Less than ug/L Benzidine 39120 Composite EPA 625 50 Less than ug/L Benzo(a)anthracene 34526 Composite EPA 625 10 Less than ug/L Benzo(a)pyrene 34247 Composite EPA 625 10 Less than ug/L 3,4 benzofluoranthene 34230 Composite EPA 625 10 Less than ug/L Benzo(ghi)perylene 34521 Composite EPA 625 10 Less than ug/L Benzo(k)fluoranthene 34242 Composite EPA 625 10 Less than ug/L Bis (2-chloroethoxy) methane 34278 Composite EPA 625 10 Less than ug/L Bis (2-chloroethyl) etherl 34273 Composite EPA 625 10 Less than ug/L Bis (2-chloroisopropyl) ether 34283 Composite EPA 625 10 Less than ug/L Bis (2-ethylhexyl) phthalate 39100 Composite . EPA 625 10 Less than ug/L 4-bromophenyl phenyl either 34636 Composite EPA 625 10 Less than ug/L utyl benzyl phthalate 34292 Composite EPA 625 10 Less than ug/L 2-chloronaphthalene 34581 Composite EPA 625 10 Less than ug/L 4-chlorophenyl phenyl ether 34641 Composite EPA 625 10 Less than ug/L Chrysene 34320 Composite EPA 625 10 Less than lug/L Form - DMR- PPA-1 Page 2 Annual Monitoring and Pollutant Scan Permit No. NCO030210 Outfall 001 Month May Year 2017 - esamete Paaiieter, : r: :Code Sam le a Pr Ty'"e Ana ical: ` lyt s Metfiod Q uaniita#ioa Level =,Sam' le �Reeult -° wuE;._ - ;Unity of a� 4& 1Vteasurement _ ;�- _ Di-n-butyl phthalate 39110 Composite EPA 625 10 Less than ug/L Di-n-octyl phthalate 34596 Composite EPA 625 10 Less than ug/L Dibenzo(a,h)anthrace a 34556 Composite EPA 625 10 Less than ug/L 1,2-dichlorobenzene 34536 Composite EPA 625 10 Less than ug/L 1,3-dichlorobenzene 34566 Composite EPA 625 10 Less than ug/L 1,4-dichlorobenzene 34571 Composite EPA 625 10 Less than ug/L 3,3-dichlorobenzidine 34631 Composite EPA 625 10 Less than ug/L Diethyl phthalate 34336 Composite EPA 625 10 Less than ug/L Dimethyl phthalate ) 34341 Composite EPA 625 10 Less than ug/L 2,4-dinitrotoluene 34611 Composite EPA 625 10 Less than ug/L 2,6-dinitrotoluene C0626 Composite EPA 625 10 Less than ug/L 1,2-diphenylhydrazinej 34346 Composite EPA 625 10 Less than ug/L Fluoranthene C0376 Composite EPA 625 10 Less than ug/L Fluorene 34381 Composite EPA 625 10 Less than ug/L Hexachlorobenzene C0700 Composite EPA 625 10 Less than ug/L Hexachlorobutadiene 39702 Composite EPA 625 10 Less than ug/L Hexachlorocyclo-pentadiene 34386 Composite EPA 625 10 Less than ug/L Hexachloroethane 34396 Composite EPA 625 10 Less than ug/L Indeno(1,2,3-cd)pyrene 34403 Composite EPA 625 10 Less than ug/L Isophorone 34408 Composite EPA 625 10 Less than ug/L Naphthalene 34696 Composite EPA 625 10 Less than ug/L Nitrobenzene i 34447 Composite EPA 625 10 Less than ug/L N-nitrosodi-n-propylamine 34428 Composite EPA 625 10 Less than ug/L N-nitrosodimethylamine 34438 Composite EPA 625 10 Less than ug/L N-nitrosodiphenylamine 34433 Composite EPA 625 10 Less than ug/L Phenanthrene 34461 Composite EPA 625 10 Less than ug/L Pyrene 34469 Composite EPA 625 10 Less than ug/L 1,2,4,-trichlorobenzene'I 34551 Composite EPA 625 10 Less than ug/L 44 1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Authorized Representative name Qi ture J.'av— &/,-� 6 /o° 0/ Date Form - DMR- PPA-1 Page 3 Attachment #8 PA Rnx 18414, (imAnvllle, SC YB11116 (864) 877-6942 a Fa (884) B77-6998 4 Craftsman Court, Greer, SC 29650 Fathead Minnow Survival and Growth Test EPA-821-R-02-013 Method 1000 Client: CHARLOTTE MECKLENBURG UTILITIES DEPT Facility: MALLARD CREEK WRF NPDES #: NCO030210 Test Date: 28-May-14 Laboratory ID#: T43460 P.PROMELAS 5-28 Test Reviewed and Approved By: 4/ Robert W. Kelley, Ph.D. QA/QC Officer Certillcatlon 087819 /^ Testmsultspresented in this reportcooform to all requirements of NELAC, conducted cad"NBLAC CerttEcatiooNumber B87819 Florida Dept. of health. Included resultspcnain only to provided sareples. Page 1 of 8 Farhad Rostampour laboratory Director SCDHEC CertlBestlan #23104 NCDENR certification a 022 A Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date: 6/9/2014 Facility: CMUD Mallarld Creek WRF NPDES# NCO030210 Pipe#: 001 County: Mecklenburg Laboratory: 1=1T Environmental, Inc. Comments x Signature of Operator In �tesp har ORC Phone/Email x Signature of Laboratory Supervisor Test Initiation Date/11me % Eff. Repl. control I Surviving # Original # Wt/original (mg) 23% 1 Surviving # Original # Wt/original (mg) 45% 1 Surviving # Original # Wt/orlgtnal (mg) 609'o 11 Surviving # Original # Wt/orlgtnal (mg) 90% 1 Surviving # Original # Wt/origlnai (mg) 100% 11 Surviving # Original If Wt/original (mg) nvironmental Sciences Sect on Division of Water Resources NC DENR 1621 Mail Sservice Center Raleigh, NC 27699-1621 /2014 1435 Avg Wt/Surv. Control 0.9245 1 2 3 4 9 9 9 9 10 10 1 10 10 i 1.0090 0.7890 0.7160 1 0.8140 9 10 10 9 10 10 10 10 0.7900 0.9520 1 0.7700 1 0.8370 1 9 8 9 8 1 10 10 10 10 10.8400 0.6760 0.9460 0.9580 8 9 9 10 ', 10 10 1 10 10 0.8140 0.8470 0.9380 1 0.8920 8 9 9 9 1 10 10 10 10 7 7 $ 8 10 10 1 10 10 0.5870 0.7900 1 0.8550 1 0.9170 % Survival 90% Avg Wt (mg) 0.8320 % Survival 95% Avg Wt (mg) 0.8373 % Survival 85% Avg Wt (mg) 0.8550 % Survival 90% Avg Wt (mg) 0.8728 % Survival 87.5% Avg Wt (mg) 0.8173 % Survival 75.0% Avg Wt (mg) 1 0.7873 Water Quality Data I Day Control ! 0 1 2 3 4 5 6 pH (SU) [nit/Fin DO (mg/L) init/Fln Temp m Init/Fin High Concentration 1 1 0 1 2 3 4 5 6 8.0/ 7.6 8.0/ 7.9 8.1/ 7.5 7.9/ T.9 8.0/ 7S 7.9/ 7S P24".124.6 7.9/ 6S7.8/ 7.77.7/ 6.77.7/ 7.18.3/ 6.0 8.27S 24.3 24.9 24.9 / 24.8 24.8 / 24.6 24.2 / 24.7 24.7 / 24.9 24.9 / 24.8 Test Organisms RCultured in -House Outside Supplier Hatch Date: 5/27/2014 Hatch Time: 1100-1300 pH (SU) Init/Fin DO (mg/L) [nit/Fin Temp© Init/F[n Sample 1 2 3 SurvivalGrowth Overall Result Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine (mg/L) Temp. at Receipt (C) OS 2 14 OS 28 14 OS 9 1 24 hour 24 hour 24 hour 125.4 125.4 125.4 78.2 71.7 65.4 1495 501 507 i 0.11 <0.05 <0.05 3.4 3.3 2.6 Normal yes ChV 94 g% Hom. Var. na M NOEC 90% Ol 0% LOEC 100% >100% ChV 94.9% >100% Method Steels RS Steels RS stats Survival Growth Conc. Critical Calculated Critical Calculated Dilution H2O I Hardness (mg/L) 49.9 23% 10 22 10 I9 Alkalinity (mg/L) 41.5 45% t4_ 14 100 19 Conductivity (umhos/cm) 205 60% 10 18 _ 10 22 90% _10 16 10 19 1005'0 10 10 10 18 DWQform AT-5 revised Page 2 of 8 7.9/ 7.9 7.9 8.0 8.0/ 8.0 8.0/ 7.8 8.1 8.0 7.9 7.9 7.8/ 7.9 1/ 6.3 8.3/ 7.1 8.4 fi.8 8.2/ 6.5 8.1 6.5 8.4/ 6.8 8.1 7.3 E241 24.6 24.3 24.9 25.0 / 24.8 24.8 / 24.6 24.2 / 24.7 24.9 / 24.9 25.0 / 24.8 CHRONIC ;DEFINITIVE SURVIVAL AND REPRODUCTION/GROWTH TEST Statistical Analyses Client: Charlotte Mecklenburg/Mallard Creek Sample Identificati n: MALLARD Test Date: 28 May-2014 for Normality and Heterogeneity of Variance Sample Use Teter Test U d Result Sample Dato Sample Used rlity NIA NIA Sample A 26-May-14 28-May-14 29-May614 xe NIA N/A Sample B 28-May-14 30-May-14 31-May-14 Sample C 30-May44 01-Jun-14 02-Jun-14 03-Jun-14 �►1SO [Efst Type Used: Linear Interpolation% Effluent fect Control 23.0% 45.0% 60.0% 90.0% 100.0% 90.0% 95.0% 85.0% 90.0% 87.5% 75.0% % reduction 0.0% 0.0% 0.0% 0.0% 18.9% i Growth 0.832 0.837 0.855 0.873 0.817 0.787 % reduction(smoothed) 0.0% 0.0% 0.0% 3.8% 7.3% Variance 0.064 0.007 0.017 0.003 0.075 0.021 Acceptability Criteria Value Upper Limit Lower Limit CV:Coeff. of Variation 26.4% 42.0% 8.9°% PMSD: % MSD 29.2% 30.0% 12.0% MSD:Min. Si . Diff. 0.280 Accpytability criteria limits not exceeded C25 Point Estimates Survival 105=> 100.0% Growth IC25-> 100.0% TEST RESULTS %Reduction per Linear Interpolation @CTC of 0.0% ypothesis Testing OEC Growth ChV Gmwth > 100.0% 100.0% Survival effect NA Growth effect NA PASS Page 3 of 8 Concentration -Response: Survival 100% Oevsot =0% "a% W.0% 900% 100.0% Test Concentration"�'r''�"'° � su„�r Concentral lon.Responlsw.. Roproduation t Growth l� om t$ 0.60 a' 10.40 h' 0.ro r 0 aWMI :1.0% esoq 60.0% 904% 1000% Test Concentration famm vu Man z7o 43460 P.PROME Client CMUD Sample 10 MALLARD op- NCCO030210 0 & fed Date8-Ma I 14 4 fed Time436 ed A fed BO Orgenlarn lme hates iumelaorgantam ap48 HOURS ce RO HATCH 5.27-1 1400 Type CCD Dliution Water C H2O 5-15-14 Emits for Conc. Mid BROOD aatvasssts ml eatvolums 60 Ml cubators aht Irlemin MUM ltlal Tam 'C 25 .159 X2 PER DAY eat method EPAe21-R-02-012:1000 Au reps tlave 7 u Mgantsms unless noted otherwise. 'JON TEMP; INITIAL - 24.1 MY 1 - 24.3 MY 2- 24.9 MY 3- 24.8 MY 4 - 24.2 MY 5- 24.7 MY 8- 24.9 4 - NC H2O 5-29-14 0 i Day 1 Devi Day 3 ow DMY5 Da Rnal New pH Sal Old pH DO Sol 6, W. .. d ' 1 _ "MI" a` ' "u "W 4aaa Z. �l� i5:, �W _ r�1 11* A EIWO '. "e` R815MMa "s"�«°.51 . 3ir.M... l' 04k New DO Old pH DO Sal 8.0 8.1 i 82 7.9 &0 8.5 8.1 7.8 I7.7 7.8 7.8 7.9a 7.9 8.5 8.8 6.6 6.5 6.9 7.9 New 00 Old PH 00 Sal 8.2 8.1 8.5 8.1 7.9=&4 7.9 7.8 7.9 7.6 7.9 6.4 0.8 6.7 6.6 6.2 s Haw DO Old pH 00 Ssl 8.2 8.2 i 8.8 7.9 8.1 8.4 8.1 7.9 7.9 7.9 7.6 7.9 7.8 7.8 8.2 16.9 6.9 6.3 6.4 7.1 7.3 MM MOM New 00 Old pH DO Sal 8.3 0.3 .8 8.0 8.2 8.3 8.2 7.9 .8 8.0 7.7 8.1 7.7 7.9 5.6 .7 6.0 6.1 6.2 0.2 7.1 New DO Sal Old PH DO Sal 8.1 8.3 6.4 8.2 6.1 8.4 8.1 7.0 tol 8.0 7.8 8.0 7.9 7.0 6.3 4.1 0.8 6.5 0.6 6.8 7.3 _ 00 Sal Old pH 00 Sal _ •Naw pH 7.91 7.91 6.0 8.01 6.11 7.91 7.8 pn or the nignest surviving luenuauan Page 5 of 8 .v T-i- CIUW OF CUSTODY RECORD NO— 964H, GletssWra, SC 2580E-74f4 .' PBge (M) 877-6M (8as1j S8t•23P•S Faac(fl84? 877 as Sldpptng Addtew.4 Cm4smaa Cl. Gma. SC 28850 ETTif PO Svx t6414. Greenvale, SC ]98n6-T414 (664) 27M942, (600) 691.2325 Fac(664) 677 6936 ShIPPIng Address 4 Craftsman C, Greer, SC 29 Sn'/ W. RRN V IOONN C)KALCON CHAIN OF CUSTODY RECORD Page _of_ Client C / n t% Q y7" ��)) Facility: 11lajjcirWCPed< W -- Prog ram Containers Prctenvtn•c Parameters nbateamomersah. - tate• V C NPDLS r: fv c.. U U 3 8 a JAD zaare araam rm o = ca U (CamPasne puny) (Gab or CvmPadte) Q T 12 _ g e Z cSiw, and Printbeiaw the dotted Ime 3 c > c = '- m c U c o• aa+ oos _ j a H _ z - ' m _ .-`?• SAMPLE ID rmPmuesvn vne Time samP¢Cmmra mm Time COIIMetl by CJ w ti, Z o H a� 6�ZOAc - < - - - _ - ` - x = ` =III ='-• O >° - �pav <' C1 U :J c- in = u = 3 i Chemical Anahrsis e. other 31 X �tw, m ------------- m------------- ------------- Special Instructions: Sample Custody Transfer Record Secure Receipt Sample Date Time Relinquished By /AOrsuatization ReoeivedB00raanizati.. Area Team °C Preserved? d9�[ � U l/1 f�✓ � rye /h �! f�7JL�rf� L,t /- e1 A- ^ a l3Dc I~l,,/ /7 TI I COMPOS/TESAMPLING AOCEDURES TEd41ER477JRE MONITORING PROCEDURES HOLD TMEPROCEDURES Composite samples must be collected over a 24 hourperiod. Sample temperature during collection and transport must be between for tprschy testing the sample must fast be used within 36 horns Time Proportional: 1 sample each hour 1or24 hours. Equal volm 0.0 and 6.0 -C. Samples must not be frozen. Use water ice in sealed bags. of sample collection (completion of composite sample). or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used afmr72 hours Sam sample collection. Flow Proportional: As per instructions in NPDES permit ETT CHAIN OF CUSTODY RECORD PO am 16474. 6R=Nwu . Be 29606-" .41t 1864) 8"-6942. 9SOM 8$1-2929 IrA=9064) 877 6928 634=3W= ADD==. 4. CRArTSMAN Or. GRrXR. Be 29550 arwtsox (D m -4 C) I esk, . ETnvrO hto. (884) 877.6942 + FAx (8e4) 67•fi988 P.Q Rate IFAT 0. SC 296M 4 CZWMM COM Greer. SC 288W Fa&ead. Ifannow Survival and Growth Test . EPA -821-R-02-013 Method 1000 Mut: CHA►RLOM OMMURG UI i I j i &S D]EPT Feeft.- CFJM V NPDES t. KC0030210 Test Dato: 10-Fcb-1S Laboratory W#: T4W2 F.FR©MELU ZAS TegRadowcd and Appravcd k.- Rob W cUq. Pb.n. Fa&a Rostampour QA/QC OMGW Labaratwv Dhamr Tostsestt pracccCd?nab =portcce9=toall=q of M AC UWWMACCmWdcnX=bcrEM19 Ftoiula t a4'Fica[tb.Iaaiadod rc v1%paign a* to provided sampks. Page I of 7 SWPBD 6111114 aILLEDMI4 SCDREC Cart eadon #23104 NCDFNR ccrttfcation r� Wuent TadclW Report arm -Chrome Fathead Minnow Multi-Concenuation Test Facay. CMUD Creek NPDR$ # NCCO 003=0 PIpe IA 0 � Ceu113r. Envirortme x t� 7An i - slgnattu e of to ResporsWe Charge x W.YZA r - Test laidaft Oate/ita�� %E. ff. Control Surwvtn origl met1W i Qni odglnal Wtlortginal (m C.. =•t swvtftg Odglnal Wtiorwlasl (rr ® s CrWnal W009olnal (mt Surviving olai Woorlgirtat (ml 1fl4 SurvivMg OrtoinaE WVodolhal A Water cluRdi;y Data Down pH (SU) trdtlF1 00 (msq InitlFi Temp(C)InWFl High Concentration PH (5U)10Fi DO (MB44 InNs Temp (C) MR sampl Collection Start Dal Ora Composite (Dtuatbl Nantes (moll Atltatl» W (mo GWUctl * (ti hoslon Chiodne(mglt Temp at Receipt(0) NOW Hardness (molt ASWhttY (msn Conductivity (umhoslcn DWQ FormAT-s (f1" 1KAX ORIGMAL TO: 2aviraA=t2t Sd=ca 8rancb Divts£oa cf WatcrrQaality BIC pEi�iR Isu Mallso &eCaatar Rddgb,NC 2709-101 10-Feb-18 1 16447 - Avg V1 UUrv. Contra]O�B4$�v Z 2 S 4 %sunrhral 1aoa� Avg Wt (mg) 0.8465 °� survival 100.fl'9'o Avg Wt (gag) a76a5 46 Survww 100.0% Avg Wt(nrg) 0.7388 9U Smvhw 1QOA96 Avg Wt (mg) %srmriM 1aofl% 9b surv�1W 97.it36 Avg Wt (mg) Q.$2 Daar - 10 1fl 10 �fl 10 1fl 10 1fl 0.7140 fl.9450 fl.SO4fl O.S230 10 10 10 1fl 1Q 1a 1a 1a 4.7i77fl a7820 Q81?A 0.7110 i0 is '!fl 9 10 10 40 D o�67sfl aT$sfl a sst~fl fl.t3fla0 10 10 9 1Q 1fl 10 9 10 0.6Ts0 0 87T0 0.8419 aTlb'0 8 1fl 10 9 s 1a 10 s 0.8T3fl 0.9210 .• fl.7S8T 1 7.0 8.0 J 7.7 8.1 ! 73 8.0 ! 7.1 8.2 ! T.9 8.1 ! 7.4 8.1 / T.S 7.8 l &.a 7.9 1 8.2 8.0 l 52 7.7 ! 8.3 7.9 1 $.? 7.2 1 8.2 TA ! 68 24A ! t5.o 25A r 2S.! SSA ! 2s0 2a•T r 2s1 2U ! 2A.7 2C7 r ?d.8 t0.ci ! AS.i 16D 10 le 2AI IV 6 78 ! 7.8 77 ! 7.6 7.3 l 7.6 7.7 1 7.2 7.2 / 7.8 7.8 / 7.5 Tsl' 1 7.8 7.8 ! 8.? 8.0 ! 0.0 8.0 i 6►1 7.9 ! 8.2 8.4 ! t3.3 80 / S.4 8.4 ! a.3 es o r aS.o zso r xs .7 ur r 25.4 zos r zsA ZS.a r seo z%s r zaa 243 r 24.5 ?rS45 2.11-15 ?r1,'tr19 24 hr 24 hr 24 hr 76.0 82.3 63.8 498 483 494 <flos 4*.0s aoT 0.$ 1.? 2fl 60.0 53.80 213 rest organstns Qcwtured tn-tiouso qx orrbwesupptier Hatch Dabs 2ti9_�_ Hatch Tune: fl�T3fl-O800 Survival Gt+ovutit t3sreralt Result Nannal Ono Qyrs City Norri.11ar. [:]no dyes NOW 100-0% 100.03's I.OEC y1�% >10�0°�6 ChV >�^ MO45 M.... Method Stasis Dtmnetb Stab Survhrgl Growth torso, adtical Catautsrta0 CdBcat Catcutatod 23 10 18 2.41 1.3$ 10 � .r... Paget af? Claiest: Sample AW Test Data: IBC DEFDdTIVE. SURVIVAL AND REPRODUCTION/GR®''Q nU TEST Static cal Analyses Charlotte Mec1denburW3LaU d Creek Pimephales promelas MALLARD Second Species Yana afvarleaoc �� ?bsr Rs�lt SsraAkDatc kUsvd WIA NIA Smr*A 09-Fcb-I$ 10•Fcb-15 11 ftb-]$ WA WA Samples 11-Fcb-15 12-Feb••1S Mfbb.IS &=*c MM-15 1446-15 ls-Fe AS 164WO.15 Fha umc. T,tacmrlatezlsolaaon E�tu=t cc 1 23.Wo 450! 60 0% 90A 6AWAY,. 10 io 100.0% I130.Wa 160Ag6 100.0�Yo PQ*aOECGh'*w& 1 = >100%1 = >100% CTcof 90.0% k raft sumva! excct 0.0% 100.0% &Owthcm= 0.0% Page $ 0 7 ConceWafion-Revonsec Smvka Em i z � z t& . T&%Co-nc%Tmllori A I t$ O.W On 0LD Om T�C�naeattlal�a � �� 6 tim L�i3E11Ly7nCls]1�1�1�1�t�i7iltliiLI�1♦�', �ilEln�7nC1�]<Iit]itiltls3�Ilt] 'lm��� C��n�l•Il■ iiiiiiiiirir��� -- ©1.1•Si1��1•�ii�i�=n�n��n�� Km tlJti mu lllo noon < WTE—I 1 liffS7 � 1t miff iLI I!iiS3ilinmm won mmimmAliwn nMi L�wwooll[]tliiitJi�]it1/���1•Uwl witloll[1inGlilr9n[]i�71<9n[Iil�r,�il��� �Iri�n�>•iii>•iiisn�i•���� ©iti�>•iiiiiiiirl•�r��3 ©iii����lti�il•i�i��l• ', E1��)�Aldl��l���)��1�1��1�i•ASKO I��l�l[]�no�]nlata■n��:Tii�im�■�i<II �it7�:i11t1�1�]�il<]t�=]t3.iin®���I ©il■[ rlul� w i il■■ IAIt i � ii 1�■■I�■�I/�Ir� r�l�ll�l�/itn�lrin■.�rn■ �■tn�t>•1� �� ����� r � � n� s 1■� n� I■■ � n■� � n/ i l�r � �� � n■�n r�l�ll �lal�u i� u>o.ir�.�.ia.ni■�.a salilir� �» Ili l_iii�i>•Im ��■ra�nelot��nnnnnr��nl���noll��l��.a t�r�l■n�ano ■nl�ralc�nd�nnrr�nolo®1•■��n� n■��nr��nar�Irtnnn�annlrla�nr��r��.�-- �■�I�sa �r �rllri �7 ®io sa ll�a ilia �ia�>� ]Ir��o �1�l�im�� i�■i �I �i�Iral� ■nnolnar� c�nln�al��rs�znn��■�I�r■illl� ca■r � nrs � na � lea � � s� � is � r� �n � n�■/� � �■m Ci�t7t7�Qil�tJt]�7ti�l�]i1�L•-r•• I��� ' 7 ©�i �®��■■In�l� i■1�11■�iil��l�rinl�l�� _.._.....1�)� l�ii�n>ti�i��ii�i�n��l•�7 � »] �[�)� � ICt t1 t7 C7�7 ICI �i � XY �11�)♦ l�l Citli 'nt:�ll�i�It7Elit7s7r1i�1���] �3lIit]nt�ttl�liin<71t7ii]�i :� ��� C��]i Clnt] �il71t1 �7�11[I �7l1 i m� �iEfl � � I�ii'a�■fit/il•iiinrii•r�� i�■Illrli ■� ®/ lull i lrll i mil l■Il il/ti � � � C�ii�®/�iii �rii1•ii�!•� E�il•�■/n■iti�iiiii��i� € : �ii�■■�rri�iirii���>t] 4aG42 PPRCemu E NC00302t0 Comm 0 Womb stztafedData IQ!Fab45 s caa ma 1w stmadawft jr, astaraae�aat Alta tts Noo. bom aato :, 48 HOUIM wmbm tkao AW H&TCH !M-Tng NOW Daauoa W4*r NO HM 2" %: rd BROOD Tbatvowmo 250ta4 uctstt MISUM Md Ta * 25 AMOCO 1.1 2xUy TbstMoMod lemala4somoco =isms LW40WDo w cam. ONTO: Rau.: 24.6 1Y 1- 25 kY2- 24.7 1Y 3- 24.5 1Y 4- 24S lYS- 24.6 lY 6 - 24.6 I CITAM OF CUSTODY RECORD ' pa gao� fee asae, sc a.� a � 87T•8�42. {emo)a3txs25 �0(88�}jBTT 6938 �-.- t X'r0$i2tit Cbitts;tttarS Frosor�►IItiYa 11'hafa A Acato Chrodc s {Coa>pa�lcaaty) (QmborCompasita) sign,P " and riot below zoxct. v the dotted line g�S _ �'MID $%�Vi� .s S 04000ftSMit Data lime S=Vo CcoWsa aato The CWtactod by r3 sn y z n�• } ?i 2►�ta , t -------------- rrr..•-r rr...rr-- �rr•.ww rrr� MMUMAP a -?fb+ Custody M%ns#'er lteeord . i'M%wohra $otter 1 � Receipt I Sample "Gad t 1tfPCJIYlTI�S�lPLiNG ROCRD TEkiPFRd? URSII�ON1!'ORlNG P1iOCRDURF.s /low TIASPROMUMS Contpasita samples must be collected overa 24 hour period Sample temparature during collection and transport must be between For toxichy tas tg the sample must *9 be used within 36 haws 'f3ma Propartionax 1 sample eaali Itaur far24 hour. Equal volui 0.0 and &0 I*Q Samples must not b$ ifczem Use wafer ire In scaled tags. of sample collection (completion of composite. sample). oratmlnimum t sample overy4bours over 24ltours. Sample may not be used atker72 hours from sample collection. l WEP ottiona]:As ggr inatrmtions in NPDES eermlL E CRAM (W CUSTODY RECORD �o ea c 4, Stu8011%SO =9 M414 P"07-M& (80o)89t•2325 FWc(8s4) 87t 6M ShVft Adtlssss:4 Craiisraaa Ch Greer, SC 28880 client: �,� Program GbntaMora Preser►�atit►o Pstramwters �aCitfty: �ia1 �f Uj PIE r 1YbolotaraLTosidly ppp in Statta: �,, i Di3S#: Acnta lande I Tes! Orgftums s - (Wrapesitooaty} (GraborCatapasita) � � � � � � � Slga, and Prlat baltnv tlta dolled I#oe s� MUM " 'g , � S ro MOLE ID � C9mge:ttosm�i a�:s 7im8 SamaSoCoQeataa asta 7isna G�k�ea 6y' � � � z :$ ,.°1.0 � oftax � �-raa�to � -� Q S. '" � Its -' A a � � I � �- �' E ii � � � onarr�lzat Artatyala 809tor �i d ial Inswotiaas: s~ `a ea rqg a• 0 - Q.- Sample Custody Trawfar Reeord Seom Receipt Sample Date 'MaeM x n ftcd l3! oi► - ACCo • Byl-010nization Area TWO T Pre Wed? ,1r r �✓ ��J Zle MW Ir Yir1/ U I 11lP 1?'�SrdMPl.ING RDCRDURES TSUPERATIM& MO]V17ONNO PR4CEDV40 HOLD 71ME PROMURM Campasitesamples must be collected overs 24 how period. Sample tompsrature dwbg collecKflu and trauspoii must be betwen For toxhAy testing the sample must first be used vAdiin 36 hours T,me Wep Wench I sarnpla each hour for 24 haws. &teal Bolin 0.0 and 62 °G. Samplas must not be fmwn. Use water Ir+e in scaled bag. oFsampie aoliectien (completion oFrompasit$ sample). or at etialiti m I sample every 4 hours over24 hours. Sample may not ba used after ?x ltm iMM sample con Cagan. lloY+r Fro orlioani: As instsuations is I+IPD$S wrrnit. CHAIN OR C"[J'S'i'ODY RECORD POBOXIMI4. Witt 0,SG2sso8-74id 044)877.6442, (800)091-2MFeX4684) 817$938 GJ*PU 3 AddtasS:4 Crftme Ct, Greer, SC 2WO 1WJLAM79"WICaMMOCCA LTM Program i Centafnars %•ac#lity: Al. _ 11 _ I fi I /_ � {Catispaulaoaly) {GrabarCa�+pas,'ic) ftan mid hint bclmv the dotted line M lco�tS:AdDssa Time �aR'e�l412004101TIM Caiimcetbv Custody Transfer word Time -. Rellanchhed Bv! Dzo SGi � 3•tW03 40A%08 M f 'R ; 05 R' • l- 0 a*o S�tJ�lPIM Mlv 9''EhfPRR+I?7i18AnviroNmaPROMDUMM Coutposltesamples must ba collected over a 24 hour period. Sampla temperature during collection and transport must be hctrvean Time Proportional: I samplp each hour for 24 howl. Eslual volur 0.0 and 6.0 °Q StuPles mast not bo frozen. Use water fee in scaled bags. oratmin alum l sansplc ovcry4hours over20lionx. Pstrnmet�ers A Page_Of q w coo ,4 G Secure Receipt I Sample I f 1� 1�tl OLD TWEPROMDURES rr toxicity testing the sample must first be used Ivftitlu X hours •snmpla Collection (Compladon of cempoells sample). wipIa may not be used after 72 hours from sample colleodon. .-. P.O. BOX 1 E414,'GreenYlle. SC 29505 (694) B77.6942 . FAX (864) 877.683B 4 Craftsman Courl, Greer, SC 29650 Fathead Minnow Survival and Growth Test EPA-821-R-02-013 Method 1000 Client: CHARLOTTE WATER Facility: MALLARD CREEK NPDES #: NC0030210 Test Date: 02-Aug-16 Laboratory ID#: T47451 P PROMELAS Test Reviewed and Approved By: pig Robert W. Kelley, PhD. QA/QC Officer A404h, Certification 087819 Test results presented in dds report conform to an requiremc ce of NBLAC, conducted =derNB1.AC CertiOcation Number E87819 Florida Dept. ofBeabh Included results rertnin only to provided..Vle.. Farhed Rostampour laboratory Director SCDHEC Cernrrcatien 423104 NCDEINR Certification # 022 Page 1 of 7 Effluent Toxicity Report Facility., Charlotte 1 Laboratory: Signature of x Signature of In Test Initiation Rateft % Elf. R I Control Surviving # Original # WUodglnal (mg) 23 Surviving Orignna( W t/otigtnel ( ) 476 Surviving Original WUorlglnal (rn' ) 60Surviving Original WUortglnal (m ) 80 Surviving Original, Wtioriginal (m' ) 100 Survivingl� Orlglnall WUcrlginal (m ) Water Quality Date PH (SU) DO (mglL) Temp (C) High Concentration PH (SU) RO (mglL) Temp (C) Collection Start RE or Composite (Duratic Hardness (mg� Alkalinity (mg Conductivity (umhostci Chlorine(mgi Temp at Receipt ( C) Dilution H7 Hardness (mg! Alkalinity (mgl Conductivity (umhoslct -Chronic Fathead Minnow Multi -Concentration Test Mallard Creek NPDES # NC0030210 At= ORIGINAL TOt Environmental Sciences Branch Division of Water Quality NC DENS ' 1621 Mail Service Center Raleigh, NC 27699-1621 Pipe #: 001 County. Mecklenburg 812f18 1 1637 Avg WUSurv. Control 0.661 1 2 3 4 !0 10 10 10 10 10 9 10 10 10 10 0.8330 0.8440 0.7060 0,6810 Test Organisms QCURUred In -House 0 X Dotards supplier Hatch Rate: 811-2l16 % 8urvival 97.65E Hatch Ttme: 1600 -1000 Avg Wt (mg) 1 0.6810 %Survival 100.0% 10 10 10 10 Avg Wt (mg) 0.7C83 ' A7.S% Avg Wt (mg) 0.7195 %Survival SSA% Avg Wt (Mg) 0.8540 % Survival 100.0% Avg Wt (mg) 0.7Q88 Ray n 7 2 A d R R 10 10 10 10 0.8320 0.7080 0,8840 0.7810 10 10 8 10 8 10 10 10 10 10 10 !0 0,5480 0.8T40 0.7130 a.8810 10 10 10 10 70 10 10 10 0.7220 0.6710 0.7180 0.7260 7.7 / 7.4 7.7 1 7.6 7.8 ! 7.4 7.7 ! 7.4 7.6 1 7.5 7.8 1 7.8 7.8 ! 7.3 8.1 ! 7.2 8.3 / 8.5 8.0 ! 8.7 7.8 / 6.8 7.8 ! 7.0 7.8 / 8.4 8.1 ! 8.1 24A ! 26.2 24.8 1 26.2 24.7 1 26.0 24.0 ! 26.6 24.7 1 26.2 24.ti / 26.1 24.0 1 26.0 7.0 1 7.7 7.8 I 7.7 7.8 ! 7.8 7.8 I 7.6 7.6 ! 7.8 7.7 1 7.8 7.8 ! 7.6 8.0 1 8.8 8.4 I 82 8.2 / 6.1 7.7 ! 8.2 8.8 ! 6A 7.8 / 6.8 8.3 ! 6.2 26.0 1 2S.2 24.6 ! 262 243 / 26A 24.B / 26.6 24.7 / 262 24A I 26.1 24.4 1 26A ! 2 3 8-1-18 6-3-18 8-4-18 24 hr 24 hr 24 hr 124.6 124.5 124.0 77.7 76.6 80.6 6a8 488 Sao <o.as <o.ot; <o.08 0.1 0.1 1.7 46.0 31.8 188 Survival Growth Overall Result Normal 1:1 no []yes ChV >700% Hem. var. ❑yes ❑yea iYOEC 100% 100% LOEC >10a% >100% ChV >10a% >100% Methcd Steels DUnnetts Stets SurvlVef Growth Cone. Crrttoel Calculated Critical Calculated 23 10 16 2.41 -0.01 45 10 18 2.41 -1.08 60 10 18 2.41 -1A0 80 10 18 2.41 0.18 100 10 18 2.41 -1.15 DWq Farm AT-6 (1/04) j Page 2 of 7 CHROMIC 4 Client: Sample Identificat Test Date: for Normality and i poet Tact Uzi tuty NIA uxi NIA EFINITIVE SURVIVAL AND REPRODUCTION/GROWTH TEST Statistical Analyses Charlotte Meeklenburg/Mallard Creek Pimephales promelas MALLARD CREEK Second Species 02Aug Z016 of Varlance 8amplo Use Result SamplaDate SamploUscd NIA Swi*cA 01-Aug-16 02Aug 16 03-Aug 16 NIA Samplo H 03-Aug-16 04-Aug 16 05 Aug-16 Sample C 04-Aug-16 06-Aug-16 07 Aug•15 08-Ang-16 est 7jpo Used: I Linear Interpolation %B$luent Effect CanN11236,0% 45.0% 60.0% 90.0% 100.0% rvival 10 IOOA% 97.5% 95.0% 100.0% reduction1.2q/o 2.5°% Z.5°� 2.5% th 0. 0.7063 0.7195 0.6540 0,7088 uction smooth r 0.0% 0.0% 0.0% 0.8% 0.8% aance O.Q 0.0010 0.0043 0.0058 0.0053 0.0007 tability CYiteria I Value Upsuer Limit Lower Limi 'oeff of Variation 9.6% D: %MSD 14.2% ►:Min. Sign. Diff. ':. 0.094 'PointBstlmates lval IC2 5= > 100.0% All 1 - > 100.0% rthcsis Tasting C Growth 100.0% Growth > i oax% eon 12.0% Aria limits not exceeded RESULTS action per Linear Interpolation C of 90.0010 al effect 2.5% i affect 0.9% Concenba ior-Respnse: Survival a �aaPON- tea tq1 raa COMMI - 'M'-' M0% MUS e°apra Test Concentmban 52Z%ad "" �� Coetoltt�ifiomRt�otisas• Reprod�lcli�n l Gra�Wb O.flO 0.70 �. 0.80 0.�10 0.30 0:30 Calttrw 23.0% 0.0% to,0ti 14.04 Test Cancentretian fcma Page 3 of 7 e f. -- G'1•moon NONE] MONO mom tpW-Edfiffoomb •� ®©®® I® l.abt T47451 P PROMELA Chant CHARLOTTE WATE Sample ID MALLARD CREEK UPON# NCODS0210 County 0 Mouth 8 start 8j fad Date 02Aug-18 StartB fad Thae 1637 Started & fed By JG Test Orpaatsm Pone ales romala Nee. born date -c48 HOURS Nao. born time ADS HATCH I-AUG- TealType NCCD Dilutlon Water SSP 7-21-18 URtta for Conn. yi %3rd BROOD Teatvesaals 400 ml Testvolumb 260 ml tneubatart 1 t.t ht J161118ft InitlatTem •e 26 Moral& IGPA JS X 2 PER DAY Testmethod 633-114n-012:10W Comments Anzapshave 10 rganlsms unless noted otherwtse. ON TEMPS .INITIAL 24A DAY 1 24.e DAY 2 24.7 DAY 3 24.9 DAY 4 24.7 DAY S- 24.5 DAY 6 - 24.6 Page 4 of 7 ET'jL FC Box 16414, GeerM9e, SC 29806 7414 (864) W-eM. (980) B91-2325 F=(864) M 6938 Shipping Add...4 man.•'man Ct Gmar ,, SC egaso W VIW.LlT6NVIRCNNpfigL.CpM CAATN Of CUSTODY RECORD Page _Laf� Client: i'1� ( Prop Containers - --- W Facility: am Prrscrvatnx Parameters (�ik� 1asGY Ct rr c�-F 11Ro1e F111vev[Tasidll• Statnn er NPDPS �e d l Aate Chmvt. lest Orgavlsvu c U (Comtwsite oNy) (Grab or Cmvpmite) ^ = ii t O U c = Z ' Sign, and Print belmr 3 c m = mxaa = _ ,n — _ ' W o - the dotted as E c — c U' a y `m _ s-xws c = o = r2 _ < SANTLEID g C=moeraesevtlm Twe S�[evmi®mm 'time C.edW ln• Uo °rnZ � >' = >._ U= et i - 2 1Chemical An yeaso her � w 1(� —EegL mL hI Al I I v d ------------- 0 ------------- ------------- — ` Speciallasnuctions: Ce.siocA Sample Custody Transfer Record - Secure Receipt I Sample Date Time Rebuquisdied H / Organiation RecenrR By / Organization Area T=D °C PrwemTd? �o C b OSIT ,VIAj, L'T OCEDURES TE �ERATURE MONITORRJGPROCEDURES OL£I TIME PROCEDUP.ES Composite samples most wllectedovera24hourperiod. Sample tcmpemmre dams colleution and txanspoR mast bebcnveen Fortoaichy restine the sample must ficYbe wed within 36 hours Tune Pmpwtional: I sample each hour for24 boors. Equalwlm 0.0 and 6.0 °G Samples mustnotbe fi men. Use seater ice in sealed bags. of sample collection (completion of composite samplej or at minimum 1=ple everv4 hours over24 hours. Sample may not be used after? boors from sample collection - Flow Proportional: As per instructions inNPDFS perniit. ETT PO Box 16414. Greewft SC Z98p6-]414 (854) 8Tl-6942, (86B) 691-2626 Fac(864) M 6966 s1r9ping PAtlres 4 Cmesman Ct, Greer, SC a666 �Mw'W CrfBNVIRONnC13rq�.CAm CHAIN uF CUSTODY RECORD Client: Progam I Caaminers Presenatirc Parameters Facility: F 1 t�tn-� < 3 = U U i .. c h t '• E — o ,fl c U s-tueor Y1tinlf ScZ1lC Nhvic PlnvmrTovritp : 3 � = L Chemical Analysis e.Other — e _ < L Z f State: l NPDPS Am¢ Chrnvie xce Orpvums SAMPLE 1D o n u' o (ComPvs6e Doty) Cempuiksmn+.N. Time (Caab are CongwsiR) 5svpk Gllmion Dom it Sign, and Privtbelow the dotted line Cvnecem br - °- E V C) m O jr = = U C _c = :s c h rn 2 U rn-f 8 -1 g 4- b -=CAL&IW- - ------------- ------------- ------------- ------ Special Immrctions: Sample Custody Transfer Record DateTime elin fished Bv 1 -91. Receiv /Oreanizatioo ?-� UOV0 Secure Area Receipt Temp °C Sample I Presen-ed? 1 1 4 13 ' 0. 1 COhfPOSfTE SAMPLIN PROCED Composite sample must a cuHacrxd over a 24 horn' period. Time Proportional: 1 sample each hour for 24 hours. Equalvolm or at minimum I sample every hours over 24 hours. Flow ProortionaL-As erinsbuctionsin NPDES ermit EAPERATUREMON/TOArVGPROCEDURES Sample temperature during collection and transport must be betvveen 0.0 and 6.0 -C. Samples must not be ficuen. Use water ice in sealed bags. LDTIMEPP.00EDUP,PS For toxicity testing the sample mast first be used vwthia 36hours of sample collection (compledon ofcomposite sample). Sample may not be used after ? hours from sample collection. ET'*jL" POBae IW4, Gm -Mlf% SC 29808-7414 (854) 877-6942, (000) 891-2325 Faz(BB4) 877 8938 Shipping Addm 4 Cansrnan CL Greer. SC nSM VNItV.CTTCI VIYONMFNI'ALGOM CHAIN OF CUSTODY RECORD Page client C r% J 1O e W 44 K, aplity: M •A c -Q W 9 r � Pmarem cantainam Preservative Parameters n•sai�sma�ero:;�b. State: N NFDES rot t4C 3 Aeutw Chmuie reto SAMPLED) (J _ 4. (Cmnp"•^•oNJ') C.mposuestmt m Time (Grebar Co.,wie) sma eeeu vmAm Time Sift and Ptirtbelmw the dotted line C.11 C by U — m = n m Z - = O >' = t-xtsou 1.xco n ¢ _ = � = U U _ c m O c _ i = m - 'e U r = 3 = L Chemica Analyss&O her ¢ !,a )ao }� I I I I ------------- ------------- ------------- ~ ------------- Specialasanctions: ertl„ �C SPS r1y l �`:�lbu/S Sample Custody Transfer Record Secure Receipt Sample Date Time PAlimmished /Ornan¢abon Rec ed By/Organ®tion Area Temp'C Preseted? is-)Qwq toff$ I I I I COMPOSITE S.619PLlNG PROCEDURES Composite samples must be collected m er a24 hour period. Time Proportional: I sample each hour fur24 hours Equal volm or at minimum I sample every4 hours ov 24 hours. Flow Proortionah"As per instructions inNPDES permiL TEMPERATURE MONPTORMIG PROCEDURES Sample temperamte during collection and ttansport must be between 0.0 and 6.0'C. Samples must ant he frozen. Use water ice in sealed bass. HOLD TIME PROCEDURES For toxicity testing the sample must fast be used nidtin 36 haars of Sample oallectioa (completion of composite sample). Sample may pat be used afrerV2 hours than sample collection. i^ ET,,v=,T.,u,.,. Ad"\ ^\ P.O. Box 1E414,:Greenvile, SC 266ob (E64) B77.6942 . FAX (964) 677-6938 4 Craftsman Court, Graer, SC 29650 Fathead Minnow Survival and Growth Test EPA-821-R-02-013 Method 1000 Client: CHARLOTTE WATER Facility: Mallard Creek NPDES #: NCO030210 Test Date: 14-Nov-17 Laboratory Sample ID #: T50422 P PROMELAS Test Reviewed and Approved By: .err% 41 Robert W. Kelley, Pb.D. QA/QC Officer CertiBcaaon #E87819 Tut resellsm pevmd'm this rcpad covform to e0 roquaemevis of N"C, conducted under NEIAC CeniBcation Number E87819 Flod da Dept. of Health. Included results pertain only to provided samples. Farhad Rostampour Laboratory Director SCDHEC Cer86catlont123104 NCDENRCer0ficadon# 022 Page 1 of 6 Facility: Charlotte Laboratory: x Signature of Open of Test lnlbgon Datelli % Eff. Rep Control Survlving Original Wt/odgtnal (m } 25.0 Surviving Original WUoriginal (m 45.0 Survlving Original WUodginal (m 60.0 Surviving Original WUorlginal (m 90.0 Surviving Original Wtloriglnal (mg 100.0 Surviving Original Wcrlglnal (mg Water Quality Data C1 pH (SU) I DO (mg1L) li Temp (C) I High Concentration pH (SU) li DO (mg/L) li Temp (C) h Collection Start Composite (Duratic Han#ness (mgl Alkalinity (mgl Conductivity (umhos/ci Chlorine(mg! Temp at Receipt ( C) DIlution H2 Hardness (mg/ Alkalinity (mg/ Conductivity (umhoslcr DWQ Form A T 5 (1/04) NPDES # NCO030210 MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Servtee Center Raleigh, NC 27699-1621 Pipe #: 001 County: 11/14/17 / 05:06 PM Avg WUSurv. Control 0.6599 4 9 d d 9 10 110 10 10 10 1 10 1 10 0.5640 0.6400 0.7350 1 0.6380 10 9 7 10 10 10 9 10 1 0.5400 0.5710 0.5578 0.6500 9 10 1 10 9 10 10 1 110 9 0.5930 0.8190 1 0.6640 0.7011 10 9 9 10 10 1 10 10 10 0.6390 0.6800 0.6420 1 0.7030 10 8 9 10 10 9 1 10 10 0.5720 0.8100 0.7380 1 0.5550 10 10 10 10 10 10 10 10 0.5210 0.6080 0.7910 1 0.8190 % Survival 1 97.5% Avg Wt (mg) 0.6443 % Survival 92.3% Avg Wt (mg) 0.5797 % Survival 97.4% Avg Wt (mg) 1 0.6943 % Survival 95.0% Avg Wt (mg) 0.6660 % Survival 94.9% Avg Wt (mg) 0.6688 % Survival 100.00/c Avg Wt (mg) 0.6848 Test Organisms Cultured In -House X Outside Supplier Hatch Date: 11113/17 Hatch Time. 1030-1130 l Day n 4 9 a d 9; R 7 7.9 1 - 7.9 / 7.6 7.7 1 7.3 17.9 / 7.4 17.6 / 7.1 17.7 1 7.3 7.7 1 7.3 ---1 7.8 7.0 /- 7.8 1 6.4 17.6 / 5.6 17.3 / 5.5 8.1 1 5.0 16.6 / 6.5 7.7 1 1 5.8 -1 6.2 24.7 1 - 24.6 / 24.8 124.6 1 24.7 124.5 / 24.5 124.4 I 24.5 24.5 1 25.1 24.6 1 26.0 -/ 25.4 n 4 9 9 c a 7 7.9 / - 7.7 / 7.6 7.9 1 7.5 7.8 1 7.7 7.4 / 7.5 7.5 1 7.6 7.5 / 7.6 -/ 7.9 9.1 1 - 7.8 / 5.9 7.6 1243 1 5.9 7.7 / 6.2 1 8.8 I 5.7 8.7 / 6.8 8.6 / 5.5 -/ 5.7 25.0 / - 24.6 / 24.8 1 24.7 24.8 1 24.5 24.7 1 24.6 24.9 / 25.1 243 1 25.0 - / 25.4 1 •2 not frozen not frozen 46.0 29.2 178 Survival Growth Overall Result Normal yes yes ChV >100A0 Mom. Var, yes NOEC 100.0% 100.0% LOEC >100.00% >100.00% CW 2100.00% >100.00% Method T Test T Test State Survival Growth Conc. Critical Calculated Critical Calculated 25%� 2AI 1.20 2.41 0.97 45% 2A1 0.00 2AII -0.75 60% 2A1 0.59 2AI -0.33 90% 2.41 0.66 2.41 -0.37 100% 2.41 -0.69 2.41 -0.61 Page 2 of 6 Day 1 0812 L Day 3 Day 4! Day 6 L Day 6 b Day? lad Losl asd ast sad Losl sad Lost Deed Lost ead Lost asd La LabS 50422 P PROMELP Client HARLOTTE WATE sample ro aQard Creek fmsoldenburg "pass# CC030210 Coon Month 11 start A fed Date 14-NOV-17 Start A fed Time 06:06 PM Started A fed By JO Test Organism Phaphalas promcfai Rea. born data 13-NOV-17 HBO. born time 1030-1130 MDT TestType NCCD Oltntlon Water 83F 11-1-17 Units for Cono. % 'lard BROOD Testvassals 400ml Teal volume 250 ml laaubatore 1 Llpht IISPJBdk lattlsl Temp 'C 6 Anemia 5 X 2 PER DAY I.-FA Testmathod a21-141402-60.N060 6.72 �MIU, mul mul mul =11MU, M MINE Renew JG JC. JGi I JC AM JO End Data Fed JQ JC JC AM JO ride fed i nesw 01�3 PM 0434 P M 0e:10 AM 10:4a AM 03�a PM t w� 1 2 `-NOV-17 FJ affeentNow temp. -0 24.6 2 .7.$ i24 24.7 24.9 24.7 o4:3oPM am temp. •0 2 .8 2 .7.6 24.5 26.1 26 25.4 cewelltewwmo.•o 24.8 2 6. 24.41 24.5 24_B Page 3 of 6 ET':i' PO Hox 16414, Grnenu9le. SC 29606]414 (864) 87`ea42 (Sao) 891-2325 Falc(864) 81-7 6938 Snipping AddreS n 4 Craftsman Ct. Greer, SC Man —+Trettnnanrnxru.cor CHAIN OF CUSTODY RECORD Page of Client: A /C CI, i Facility: ,1. Pmemm Containers Prtscrtatiae Pammeren /4l-cl 9 r-. whom Effluent Tosldh State: G NPDEMS +'..-.V CU �'� Acvte Chrome TestOranums o� = U (Cooryos'rte 0*) (Grab w Ccmpuite) G ?' r o t o P Z Sign, and Print below = � -'a v - v c 1-lesal a.xo, - = y � _ �Z ==>_ the dotted line - c-' U o = s-xnvv - ? = = 3 _ - __ _ - SAMPLEID O CamposaeStart Oaa 'time ivye Cun®mnvle Time GIIm1eA b, V o i7 in Z � ^ O > = y,n� 4 f U V [) � L E rn = J = 3 2 Chemi�alAVlvsisSOrhar ------------- ------------- pecial Instructions_ �e iz 3:�C S„�ieTa�,6i`e Ta"^e �r'rk�w�: e��dtt d° �°•' s e� j9ek iN e Sample Custody Transfer Record Secure Recefor S-mole Date Time Relim ished Bvj oneviLmort. RepehedB /Omar cation Area -I Mn'C Preserved? /] -t"J- pp1' i 9 /I C A/POSlT£SAA9PL: PROCEDURES TEWERATURE.NONJTORMO PROCEDURES HOLD 7hfE PRO CEDU_RS Composite samples m e collected wet a 24 hourperiod. Semple temperature during collection and transport must be between For tosiciry testing the sample mtrm firm be used within 36 hours Time Proportional: 1 sample each bour for 24 hours. Equal volm 0.0 and 6.0'C. Samples most not be frozen. Use hater ice in sealed bags. ofsample collection (completion of composite sample). or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 horns from sample collection. Flow Pro ortional: As net instructions in NPDES permit ETT `Box 16414, Greenvale, SC 2960G7414 (864) 3 7-6942. (800) 891-= Fax(864) 877 8938 ShiPPing Addm r.. 4 Craftsman CC Gm ,, SC 29660 MW W.CrlS,uvIYONry!'H�Y4COry CHAIN OF CUSTODY RECORD Page _of_ 1 Iienr-. ` hAc 10 \ N e.r Facility: Program Conmincrs Presenari.•c Paramettrs n — R'hotc FJlloeu ioxidr_r State;- t>'PDFiSR Ante Cbroeie Tes[O riuvrx (Camposik m8y) (Grab or Cmoposik) C '`'-' = ii c U e ? Z ✓ — Sign, and Print below V y a y �w c o ..mow — U - � - E aE = y i s SAIvQ1LElD r? CvAoova6mm ram Time Smple eelkvian o,,.. Time the dotted line CallerlN q• = U 'e y E h c Z U o .2 � U = > `—' IWM_ yoVc Q E V 2 TU 3 — U J C n := 2 Chem)eal AnzlysisLOthar (�l��f-F C i�t)s�r� »%6)t7 _ �a�(� - 3 � Sd42•�.B sPe iallnstructiom: T 1 Sample Custody Transfer Record Secure Receipt Sample Date Time Rel' uahed8 / Orpnization -Received By/Oreanimtion .Area Temn'C Presen•ed9 �� fit6� :2� •ern ' - n H 9-"T ,t� � o.0110 -fibzo C OS/TES.4A4PLlN PROCEOU S rEAPERATUREMONfrOR/NCPROCEDURES Y U V HOLD rLhgPP,OCEDURES Composite Samples must collected over a 24 hour period. Sample temperature during collection and transport must be between Far mxicic resdns the sample must fast be used within 36 hours Time Proportional: ) sample each hour for 24 hours. Equal vol 0.0 and 6.0'C. Samples must not be Frozen- Use weer ice in sealed bags. ofsample collection (completion of composite sample). oraz minimwn 1 sample every 4 hoursover M hours. Sample may not be vied after? hours kom;-ample colic ion. Flory Pro ottionah As r instructions in NPDES on ^nit 14 0 ETPL' - PO our lusm. CreenMfle, SG 2a9aF]414 (8e4) sn-9942 (eoo) 891- 325 Fa(e64) en Base ShIPPin9 Addles 4 Craftsman Ct, Greer, SC 2MM CHAIN OF CUSTODY RECORD Page _�of client / /� Yl ( Facility: 97 _ 1 P-Mngnm Con Hers p arname Pa ame�ers � c� vt jCr, n'6olc [nlvmt Tavrin - I fate• IrrDFs 00302 Arnte Cbravic Tett Oryiisms 22 U (Compntiie onW) (Gab or Compasite) < �` '-' = U = V Z Sign, and Print below the dotted line 3 = > c e; o u 2 v = nHaa a-wms = � _ o - ' " _ _ � � " - 2 w SAMPLE ID �?rimeo mia5mn o.m Times 5®plet"mevtm no¢ Col4seedM - U rn y Z = O > - s•gvu Q ' G - _ •" _ O = - > - "_ - -� - ' _ - ._ a. qyQ J iJ i) c � ;� = V _ 3 L Chemical Analysts LONer M-Cry ------------- Special Instructions: Sample Custody Transfer Record Secure Receipt Sample Drattet Tit ed Bv/ Ord.,anirrtion Received By/Orr2tt®tion Arta Temo'C nt Preseed? '� 7 l bv+ q I I ' S'C] l 1 (' . 2 1 1 '3Z at f I ct ' J l l 0 t l 121 tl 1'l t� i3`i� i( 7 Isz3 F COMPOSITESAMPUNGPROCEDURES TEMPERATURE MONITORING PROCEDURES W HOLD TIME PROCEDURES Composite samples most be collected over a 24 how period. Sample temperature during, colection and tramport most be bemet For to ciciry testing, the sample a = fam be wed nithin 36 hours Time Frapo[tional: 1 sample each how for 24 how. Equal Nralui 0.0 and 6.01C. Samples must not be frozen. Use nester ice in sealed bags of sample collection (completion of composite sample). or at minimum I sample every 4 hours over 24 hours. Sample may not be wed after M how. firm saaole collection. Flow Proportional: As per instructions in NPDES permit. sNON, P.O. box 1F4J4. Greellvlie. 5C 29606 (964) 977Z942 . FAX (864) 877-6938 4 Craftsman Court, Greer, SC 29650 Fathead Minnow Survival and Growth Test EPA-821-R-02-013 Method 1000 Client: CHARLOTTE WATER Facility: Mallard Creek NPDES #: NC0030210 Test Date: 13-Feb-18 Laboratory Sample ID #: T50955 P promelas Test Reviewed and Approved By: Robot W. Kellcy, Ph.D. QA/QC Ofcm Certification M7819 Test msvhs pmscomd inthis mpod cv f.. to a➢rcquamcats of NELAC, ccoducmd node NHAC Ctn fiadon Nu ber E87819 Florida Dept ofElmlt l udcd mauls penam only to prmidcd samples. Page 1 of 6 Forbad Rostampour Laboratory Director SCDHEC Certification #23104 NCDENR Certification # 022 EtiiuentTaA Reps FacTrty: Chariot Laboratory: x Signature of Op x Test Initiation Da me % Eff. pl. Control Survi g # Origl, al # Wticriginal I mg) i 25.0 SurvivI ig # Orig al # Wt(orlglnal mg) 45.0 SurvIv1 ig # Origli ial # , Wt/original ! mg) 60.01 Survivl ig # Origli ial # Wtlodginal mg) 90.0 Survi g # Orlgl' a # Wt/originaI i mg) 100-01 Surviv, 19 # Origi 1183, # Wtlortginai mg) Water Quality Data Cal frol pH (SU) Inf lFn DO (mg/L) In n Temp (C) Ind Win High Concentration pH (SU) Ini 1FIn DO (mglL) In In Temp (C) In ffin Collection Start Composite (Duce Hardness (n Alkalinity (n Conductivity (umhos Chlodne(q Temp at Receipt Dilution Hardness (rti Alkalinity Conductivity (umh DWQ Form AT-S ;hmnic Fathead 141anow Multl-Cancentration Test Mallard Creek NPDES # NCO030210 MAIL ORIGVUL TO: Envirenanental Sciences Branch Division Of Water Quality NC DENR 1621 Mao Service Center ltaleigh, NC 27699-1621 Pipe #. 001 County. Comments 02/13/18 1 04:50 PM Avg Wt/Surv. Control 0.7483 1 9 Z A 10 10 9 10 10 10 1 10 10 0.6650 0.7626 0.6930 0.7860 10 10 10 10 10 1 10 10 10 0.6530 0.7010 0.7230 0.7160 10 10 10 10 10 10 10 10 0.5300 0.6490 0.8010 0.7640 10 10 1 10 10 10 10 10 10 0.7560 0.7910 0.81010 0.7960 9 10 10 10 9 10 10 10 0.7222 0.7640 0.6260 0.8590 10 10 10 ff 10 10 10 0.9430 0.8300 0.8490 % Survival 97.5% Avg Wt (mg) 0.7290 % Survival 100.0% Avg Wt (mg) 0.6983 % Survival 100.0% Avg Wt (mg) 0.6860 % Survival 100.0% Avg Wt (mg) 0.7860 % Survival 100.0% Avg Wt (mg) 0.7403 % Survival 100.0% Avg Wt (mg) 0.8575 Test Organisms P Cultured In-House Outside Supplier Hatch Date: 02/12118 Hatch Mme: 1000-1130h Day n 1 9 A A G a � 7 7.4 1 - 7.6 / 7.4 17.9 / 7.6 7.6 1 7.7 17.8 I 7Aa 17.7 / 7.4 1 7.6 1 7.4 -1 8.0 8.6 / -- 8.3 / 6.7 1 7.7 1 6.2 7.7 1 6.3 17.6 / 5.5 7.7 I 5.2 5.6 1 6.4 1-1 6.2 24.7 I - 24.7 1 24.8 24.6 / 25.4 124.9 1 252 124.7 1 252 24.8 1 25.1 24.6 / 252 -1 24.8 n 1 9 '4 A r% a 7 7.1 1 -- 7.6 1 7.6 7.6 1 7.9 7.8 1 7.6 7.7 1 7.7 7.5 1 7.6 7.8 / 7.7 --- I 7.9 92 1 - 8.0 1 6.5 8.1 1 6.8 7.5 1 5.7 7.7 / 6.4 7.4 / 5.7 7.2 / 6.1 -1 5.9 25.0 I - 24.7 / 24.8 24.9 1 25A 25.0 I 25.2 24.8 / 252 24.8 / 25.1 24.7 / 252 - I 24.8 1 2 46.0 28A 179 not frozen not frozen Survival Growth Overall Result Normal no yes ChV >100.000/ Ham. Var. yes yes NOEC 100.0% 100.0% LOEC >100.00% >100.00% Cw >100.00% >100.00% Method Steel's Test T Test Stats Survival Growth Cana Critical Calculated Critical 25% 10.00 20.00 2AI 45% 10.00 20.00 2.41 60% 10.00 20.00 2AI 90% 10.00 20.00 2.41 100% 10.00 20.00 2.41 Page 2 of 8 Calculated 0.69 0.82 -2AS 1 r 4 Day 5 Day 6 1 Day 7 Lost Lead Lost Load Los! lboad Lo 01 01 01 01 01 o a 7.54 0 0 0 0 0 0 0 6.26 o�0 01 o 0 0 8.59 V V V 21251 V V V V .7.+IO O gig! 0 0 0 0 0 8.3 JC I JJG JC I FJ JC JG JC IJG JC FJ JC JG 1 i Weer 00:54 PY Pi/ *till PM COW PM 10AIAM 03al i Now tmp.'c 24.7 24.9 25.0 24.8 24.8 Z We 24.8 125.4 25.2 25.2 25.1 21, Fecundity Page 3 of 6 rz 10 10 0 0 0 0 10 10 10 10 0 0 0 0 Labs T50955 P promelas client CHARLOTTE WATE Sample to Makard Creak NFDESS NCCO30210 County Mecklenburg Month 2 Start a. tad Date 13-Feb-18 Start i led Time 04:50 PM Stsrtod b 4od By JC TostCrpset:tn PIME PHALES PRO Moo. bom date 12-Feb-18 Neo.bom time 1000-113OMST ostType NCCD Motion Water SSF 212M8 uttrts for Cam % 1i3rd BROOD Testvessols 400 ml Testvolume 250 ml rrtcubstort 1 Light 16It18dk 25 Metals .15g WAY method SPA eZt-n ots:taao Comments AEE reps have 10 organisms unless noted otherwise. ABS PJ13118 i48HRS OLD or riot Err PG aea 16414, Greenvllla, Be aa8ge-7614 (854) 877-6942, (000) 891-2325 Fax(884) 877 6938 shipping Addrems:4 cattleman Ct, Greer, SC 29M VFW W.RTCNVIPONMCNTPLAGM CHAIN OF CUSTODY RECORD Page of 7-7 Client: .r, • ,l�t��d Fj Program Containers Preservative Pnrametcrc Facility: /q CC2C- k ,g f Whole Gmuent Tesicrry• X, State: 1 NPDRS Acute Chreak Tor orgaetsms O (Campmire W,) (Gob ar Compmilvl < O o t2 = rj U ' o a i '- O C a Signeand Priatbelom Ole dotted line 'u 'u = = ° ` �. g — to SA[vII'LE ID Cempadmsunone Time 5empiecellr,fl.. 1 mm Collecmd by U h m z c i O > — s-z°n° s=Doer f< U U U i_ `m >`. = U !— 3 - 2 Chemical Anelysls&Other >--"-`O 5'04ss ------------- ------------- ------------- ------------- Special Instructions: eGs 7 \s Sample Custody Transfer Record Secure Receipt Sample Date Time Relin uished BY /Organization Rec ived By Area Tem °C Preserved? 293-15 , 1 C A OS/TR SAd4PL/N PROCEDURE EAMERATURE A40NTOR/NG PROCEDURES HOLD TIME PROCEDURES Compositesariplesmus ecollectedovera 24 hour period. V. Smmile temperature during collection and transport must be belmveen For toxicity testing die sample must first be used within 36 hour Time Proportional: 1 sa each hour for 24 )hors. Equal voitn 0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags. of sample collection (completion of composite sample). or at minimum I sample every 4 hours ovor 24 hours. Sample may not be used afrer72 hours from sample collection. Flow proportional: As per instructions in WDES permit I ET'll PO Box 16414, Greenville, SC 2aBO&7414 (964) 8774942, (800) 891-2325 Fat(664) 677 6938 Shipping Address:'4'Creftarm n to;Guar; SC29B50 Ww W.6TlENVmoNMENi<LCV M CHAIN OF CUSTODY RECORD Page of Client: I 1�/ _ 1,, � Program Cnnmincrs Prascn•etiec Parameters LI'acil(ty: / �� `NPDPS:: GmaaT 0 � State: VG Acute Chronic h,.nT st 0. Test Organisms — e C y 0 u (Cemposileanly) (Gmbor Composite) 6 c t2 > J Sign, and Print below 3 e m o z-x0L tt s6s _ `o s �s ? v cn > F ` the dotted lint Eta,' U •_ E o $ s-xxoa s-awH it u o o_ o u_ r SAMPLE ID Camnmiw aNn aae rime eemple aolleNan Dim nma Callectad br U h y Z o >° — a-ou,.r < a u u ei d �, i Cmemieal AnalyslsSONer Special Instructions: ) Sample Custody Transfer Record Secure Receipt Sample Date Time Relin uished By/Or ni ' n Received By/Oreanization Area Tem `C Preserved? 3 4 k G/R "� , C10 LA IF-X ahrr 9 sa �� I lo.ono C ATPOSITESAMPL/ PROCEDURE TEMPERATURE MONITORING PROCEDURES HOLD TIME PROCEDURES Composite samples mus be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing the sample most first be used within 36 hours Time Proportional: 1 sample cacti hourfor 24 boors. Equal A•olw 0.0 and 6.0'C. Samples must not be frozen. Use Avatar ice in scaled bags. ofsample collection (completion of composite sample). or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Plow Proportional: As Der instructions in NPDES permit ETI It , PO eox 16414, Cmeweg, a 29605-7414 (864)877-6942. (BBB)081-2325 Fax(084) 8776938 ShlppiV Mdresa:4 Craftsman Ct, Groat, SC 2050 WM'W.6TfENV IHONMCIT.LL.COM CHAIN OF CUSTODY RECORD Page of Client: O '�-t° I'm.,.. Cnntelecre PresenativG Parameters ¢` ` Facility: i�6b)It�tcl� f"t q, �! \YholaLmuantToxtdry� l State: N NPDLS$: yK Jo Acute Chroelc I Txet Craanfsms a (C-nrutetcenly) (tomb or Camposlte) Q $ U (yZy o n E 2 E a Sign, and Print below i3 y'- ca n o bxss01 2-xtx ; l' _ 2 ° � _ 5 `— 9 E c m z 0tiiG dotted 1111E e E E U y M C•kaox =C o C13 SANIPLEtti V Camana<alenane Time hnplCCeatdentrnm Time Ukdedby UW o21 y Z C V j a•ZvAc < o — — _ >,- Ci Chemlal Analysis 80Ner My `, C PIl�l9 _r•�II a �^ Y �`t X I. YJ.1 -'N,S�//''++ - ------------- ------------- Special Instructions: sty gale ��M� . TV Sample Custody Transfer Record Secure Receipt I Sample Date Time Relinquished BY/Organization eceiv dBy/Ora niation Fuca Tema C Preserved? 2116 f -Ib• :3 - c I 77 Fl I 10.0 I U� C0"O5T7ESAA1PLIHGPROCE S TEALPE•24TURE A40NPTORIHG PROCEDURES HOLD TIME PROCEDURES Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be behveen For toxicity testing the sample must first be used within 36 hours Time Proportional: I sample each huurfor 24 hours. Equal value 0.0 and 6.0 eC. Samples must not be frozen. Use water ice in sealed bag ofsample collection (completion ofcomposite sample). or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample collection. Flaw Pra orfional: As per instrucliens in NPDES permit. Attachment #9 ,. /\ FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin Pee Dee SUIPPLEIIII APPLICATION INFORMATION PART F.INDUSTRI L USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. a. Number of non -categorical SIUs. 0 b. Number of CIUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: i See following pages for answers to F3—F8. Mailing Address: FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. F.5. Principal Produ I s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product( ): Raw material(s): F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge Into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. gpd ( continuous or intermittent) b. Non-procewastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons p ur day (gpd) and whether the discharge is continuous or Intermittent. gpd ( continuous or intermittent) F.7. Pretreatment Sta idards. Indicate whether the SIU is subject to the following: a. Local limits ❑ Yes ❑ No b. Categorical pretreatment standards ❑ Yes ❑ No If subject to categ ncal pretreatment standards, which category and subcategory? n eoft1 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following "' nation for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the informatlo requested for each SIU. F.3. Significant IndusFrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Avago Technologies Wireless (USA) Manufacturing Inc Mailing Address: 9815 David Taylor Drive Charlotte NC 28262 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Metal Finishing — Etching of Quartz Wafer with a metal film F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Quartz Wafers Raw matedal(s): Quartz or silicon wafers cleaning solvents Etchants and addatives ohotoresist coatings. polymer coating for silicon wafers Thin film metal mating F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) a d whether the discharge is continuous or intermittent. 7544 gpd ( continuous or X intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons pit day (gpd) and whether the discharge is continuous or intermittent. 1879' gpd (X continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Loral limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categ I cal pretreatment standards, which category and subcategory? 40 CFR 433.17 F.B. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. 1 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the Information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. i Name: Cartier Corporation Mailing Address: 9701 Old Statesville Road Charlotte NC 28269 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Operation includes various metal working activities such as plasma -arc cutting, rolling, shothlasting, welding, brazing, machine, assembly, washing, insulation adhesive operation, testing (leak testing and final testing) and painting heavy and light chillers. Prior to painting, Cartier will operate two phosphating operations, which discharges continuously. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Large Capacity Chillers Raw materal(s): Rinse Waters F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 10000 gpd (x continuous or intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system In gallons per day (gpd) and whether the discharge is continuous or intermittent. 1900( gpd (X continuous or intermittent) F.7. Pretreatment Sta dards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categolrical pretreatment standards, which category and subcategory? 433.17 Metal Finisher F.B. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works In the past three years? ❑ Yes ® No If yes, describe each episode. A SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Mallard Creek Polymers Mailing Address: 2800 Morehead Road Charlotte. NC 28262 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Produce tlIroanic chemicals mostly styrene and butadiene polymers F.6. Principal Produc s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SI U's discharge. Principal product( ): Styrene/butadiene polymers Raw material(s): styrene butadiene various other chemicals F.6. Flow Rate. a. Process we day (gpd) and lewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per whether the discharge is continuous or intermittent. I 52,833 gpd ( X continuous or intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons p r day (gpd) and whether the discharge is continuous or Intermittent. 1,400 gpd ( X continuous or intermittent) F.7. Pretreatment Stajtdards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 40 CFR 414 suboart D F.B. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. /'A r�l FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mallard Creek WRF, NCO030210 Renewal Yadkin Pee Dee RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck, rail or dedicated pipe? ❑ Yes ® No (go to FA 2) F.10. Waste transport. Method by which RCRA waste is received (check all that apply): ❑ Truck ❑ Rail ❑ Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount (volume or mass, specify units). EPA Hazardous Waste Number Amount Units CERCLA (SUPERFOND) WASTEWATER, RCRA REMEDIATIONICORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remedlation Wasie. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? ❑ Yes (compl ete FA 3 through F.15.) ® No F.13. Waste Origin. De cribe the site and type of facility at which the CERCLAIRCRA/or other remedial waste originates (or is excepted to origniate in the next five years),I iI FA4. Pollutants. List lhd hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach add I tional sheets if necessary.) F.16. Waste Treatment a. Is this waste treated (or will be treated) prior to entering the treatment works? ❑ Yes ❑ No If yes, descri 1 the treatment (provide information about the removal efficiency): b. Is the discha a (or will the discharge be) continuous or intermittent? ❑ Conlin ous ❑ Intermittent If intermittent, describe discharge schedule. END OF PART F. REFER TO TH APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE