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Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, December 21, 2020 EI Group, Inc. (TH005) Attn: Parker Alvis 2101 Gateway Center Blvd., Suite 200 Morrisville, NC 27560 RE: Laboratory Results for Project Number: [none], Project Name/Desc: DATA-DCTC ENCO Workorder(s): CD20029 Dear Parker Alvis, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, December 7, 2020. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, A40 Bill Scott Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of S (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfall -01 Lab ID: CD20029-01 Sampled: 12/07/20 10:06 Received: 12/07/20 13:12 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B EPA 1664B 01/04/21 12/15/20 08:15 12/15/20 13:11 SM 254OD-2011 NO PREP 12/14/20 12/08/20 17:21 12/08/20 17:21 SM 4500H +B-2011 NO PREP 12/07/20 10:20 12/09/20 17:45 12/09/20 18:03 Client ID: Outfall -02 Lab ID: CD20029-02 Sampled: 12/07/20 09:54 Received: 12/07/20 13:12 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1664B EPA 1664B 01/04/21 12/15/20 08:15 12/15/20 13:11 SM 254OD-2011 NO PREP 12/14/20 12/08/20 17:21 12/08/20 17:21 SM 4500H +B-2011 NO PREP 12/07/20 10:08 12/09/20 17:45 12/09/20 18:03 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 8 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Outfall -01 Lab ID: CD20029-01 Analvte Results Flag MDL 2 Units Method Notes pH 7.1 1.0 1.0 pH SM 4500H+B-2011 Q-01 Temperature for pH (deg. Q 7.4 pH SM 4500H+B-2011 Q-01 Total Suspended Solids 8.7 4.2 4.2 mg/L SM 254OD-2011 Client ID: Outfall -02 Lab ID: CD20029-02 Analvte Results Flag MDL 2 Units Method Notes pH 7.0 1.0 1.0 pH SM 4500H+B-2011 Q-01 Temperature for pH (deg. Q Total Suspended Solids 7.5 pH 6.5 2.9 2.9 mg/L SM 4500H+B-2011 Q-01 SM 254OD-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 8 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: Outfall -01 Lab Sample ID: CD20029-01 Received: 12/07/20 13:12 Matrix: Water Sampled: 12/07/20 10:06 Work Order: CD20029 Project: DATA-DCTC Sampled By: Parker Alvis Classical Chemistry Parameters I ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes pH^ 7.1 pH 1 1.0 1.0 OL09016 SM 4500H+B-2011 12/09/20 18:03 DMJ Q-01 Temperature for pH (deg. Q 7.4 pH 1 OL09016 SM 4500H+B-2011 12/09/20 18:03 DM] Q-01 Total Suspended Solids^ 8.7 mg/L 1.67 4.2 4.2 OL08006 SM 2540D-2011 12/08/20 17:21 DM] Classical Chemistry Parameters ^ - ENCO Jacksonw1le certified analyte [NC 442] Analyte rCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes Oil & Grease (HEM) [C-0007]^ ND mg/1- 1 1.50 5.00 OL14007 EPA 1664B 12/15/20 13:11 LTS Description: Outfall -02 Lab Sample ID: CD20029-02 Received: 12/07/20 13:12 Matrix: Water Sampled: 12/07/20 09:54 Work Order: CD20029 Project: DATA-DCTC Sampled By: Parker Alvis Classical Chemistry Parameters I ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes pH^ 7.0 pH 1 1.0 1.0 OL09016 SM 4500H+B-2011 12/09/20 18:03 DMJ Q-01 Temperature for pH (deg. Q 7.5 pH 1 OL09016 SM 4500H+B-2011 12/09/20 18:03 DM] Q-01 Total Suspended Solids^ 6.5 mg/L 1.18 2.9 2.9 OL08006 SM 2540D-2011 12/08/20 17:21 DM] Classical Chemistry Parameters ^ - ENCO Jacksonw1le certified analyte [NC 442] Analyte rCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes Oil & Grease (HEM) [C-0007]^ ND mg/L 1 1.50 5.00 OL14007 EPA 1664B 12/15/20 13:11 LTS FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 8 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 0L08006 - NO PREP Blank (OL08006-BLKI) Prepared & Analyzed: 12/08/2020 17:21 Spike Source %REC RPD Anala Result Flag Q Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (OL08006-BSI) Prepared & Analyzed: 12/08/2020 17:21 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 110 2.5 mg/L 100 113 80-120 Duplicate (OL08006-DUP1) Prepared & Analyzed: 12/08/2020 17:21 Source: CD19528-01 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 320 50 mg/L 310 2 20 Duplicate (OL08006-DUP2) Prepared & Analyzed: 12/08/2020 17:21 Source: CD19905-03 Spike Source %REC RPD Analvte Result Flag 2 Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 120 25 mg/L 110 16 20 Batch 0L09016 - NO PREP LCS (OL09016-BSI) Prepared: 12/09/2020 17:45 Analyzed: 12/09/2020 18:03 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes pH 7.0 1.0 pH 7.00 100 99-101 Duplicate (OL09016-DUP1) Prepared: 12/09/2020 17:45 Analyzed: 12/09/2020 18:03 Source: CD20029-01 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes pH 6.9 1.0 pH 7.1 4 25 Classical Chemistry Parameters - Quality Control Batch 0L14007 - EPA 1664E Blank (OL14007-BLKI) Prepared: 12/15/2020 08:15 Analyzed: 12/15/2020 13:11 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 1.50 U 5.00 mg/L LCS (OL14007-BSI) Prepared: 12/15/2020 08:15 Analyzed: 12/15/2020 13:11 Spike Source %REC RPD Anala Result Flag Q Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 133 5.00 mg/L 162 82 78-114 LCS Dup (OL14007-BSDI) Prepared: 12/15/2020 08:15 Analyzed: 12/15/2020 13:11 Spike Source %REC RPD Anala Result Flag Q Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 138 5.00 mg/L 163 85 78-114 4 18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 Of 8 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 0L14007 - EPA 1664E - Continued Matrix Spike (OL14007-MSI) Prepared: 12/15/2020 08:15 Analyzed: 12/15/2020 13:11 Source: BD03941-01 Spike Source %REC RPD Analvte Result Flag 2 Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 121 5.00 mg/L 153 1.50 u 79 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of S (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. Q-01 Analysis performed outside of method - specified holding time. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 of 8 , »>I � 2 \ 7 E( 2 a \ ~ ` _ CD ID / ° O k% § a 2 � m & :3 7.-; pa k Page 8y8