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NCG030234_DMR_20200403
704.596.5112 office 866.596.5112 toll-free ENDEL 704.5 704.597.5069 fax TANK & HEAT EXCHANGER A TransTech Company 4823 North Graham Street Charlotte, NC 28269 April 3, 2020 NCDEQ Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh,NC 27699-1617 Subject: Monthly Discharge Monitoring Report Submittal for 2020 REc `\/F,D Bendel Tank& Heat Exchanger, LLC APR 2 0 2020 4823 N. Graham Street, CEN T Charlotte, Mecklenburg County CWR SE 711E`� Stormwater Permit COC Number NCG030234 ON Dear Division of Water Quality, As required by the referenced Stormwater Permit Certificate of Coverage, please find enclosed an original and one copy of the monthly Discharge Monitoring Report (DMR)for the referenced facility. These DMRs are being submitted as the following sample designated in the Tier III section of the permit: As required in Tier III of the Stormwater Plan, Bendel will continue to monitor for all required parameters until such time as the site can demonstrate three consecutive samples that are below the benchmark value for all parameters in a Tier response. Based on the new general stormwater permit,this should be attainable for copper. Once attainment has been reached for copper, Bendel may seek a variance from the Department of Environmental Quality for zinc. Additionally,Bendel has triggered a Tier I response in March for TSS. As designated in the Tier I section of the Permit, Bendel will: • Conduct a stormwater management inspection of the facility within two weeks of receiving results. • Identify and evaluate possible causes of the benchmark value exceedance. • Identify potential,and select the specific feasible: source controls, operational controls,or physical improvements to reduce concentrations of the parameters of concern,and/or to bring concentrations within the benchmark range. • Implement the selected feasible actions within two months of the inspection; and • Record each instance of a Tier One response in the SPPP, including the date and value of the benchmark exceedance,the inspection date,the personnel conducting the inspection,the selected actions,and the date the selected actions were implemented. Please call me at(704) 596-5112 if you have any questions or if you require any additional information. Sincere , im Rozsa Vice President, Operations Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 04/03/2020 CERTIFICATE OF COVERAGE NO. NCGO3 O 2 3 4 SAMPLE COLLECTION YEAR 2020 FACILITY NAME Bendel Tank&Heat Exchanger SAMPLE PERIOD •Jan-June ❑July-Dec COUNTY Mecklenburg or Monthly'March (month) PERSON COLLECTING SAMPLES Coleman Marchin/AECOM DISCHARGING TO CLASS nORW ❑HQW ❑Trout ❑PNA LABORATORY Pace Analytical Lab Cert.# 12,5342,37706 *Zero-flow ❑Water Supply ❑SA Comments on sample collection or analysis: •Other C PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results 1•I No discharge this period?2 Date Sample ' 24-hour rainfall H, Non-Polar O&G/ p Total Toxic Outfall No. Collected) amount, Total Suspended Solids Standard units Copper Lead Zinc Total Petroleum Organicss (mo/dd/yr) Inches3 Hydrocarbons Benchmarks===> - - 100 mg/L or 50 mg/L4 6.0—9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L SW-001 3/3/2020 0.66 377 8.7 0.0523 <0.005 0.218 <0.005 N/A 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall,you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit,Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11;for semiconductor manufacture use the definition as found in 40 CFR 469.12;for electronic crystal manufacture use the definition as found in 40 CFR 469.22;and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-5/31/2021 SWU-245,last revised 2/1/2019 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver,the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO),I certify that to the best of my knowledge and belief,no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Jim Rozsa Name(Print name) Vice President, Operations Title(Print ti ) -Y-2 ao (S. ture) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL,<PQL, Non-detect, ND, or other similar non-numerical format. When results are below the applicable limits,they must be reported in the format,"<XX mg/L",where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this period?2 Date Sample 24-hour rainfall Outfall No. 1 Collected amount, Non-polar O&G/TPH by (mo/dd/yr) Inches3 EPA 1664(SGT-HEM) Total Suspended Solids pH Benchmarks===> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0—9.0 SU NA NA NA NA NA NA Footnotes from Part A also apply to this Part B *See General Permit text,Table 5,identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Page 2 of 3 Note: If you report a sample value in excess of the benchmark,you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑■ NO❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑■ NO❑ REGIONAL OFFICE CONTACT NAME: Samar Bou-Ghazale Mail an original and one copy of this DMR,including all"No Discharge"reports, within 30 days of receipt of the lab results(or at end of monitoring period in the case of"No Discharge"reports)to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for:athering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete. I am aware that there are signifi .nt pen.(ties for submitting false information,including the possibility of fines and imprisonment for knowing violations." (Signatur Permittee) (Date) Page 3 of 3 Pace Analytical Services,LLC • aceAnalytical 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 wwr.pealsbs.con (704)875-9092 March 26, 2020 Mr. Jim Rozsa Bendel Corp. 4823 North Graham St. Charlotte, NC 28269 RE: Project: Bendel-Revised Report Pace Project No.: 92467938 Dear Mr. Rozsa: Enclosed are the analytical results for sample(s) received by the laboratory on March 04, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. This revision was issued on 3/26/20 to include the correct client Chain-of-Custody, and to report the reanalysis result for lead, per client request. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Coleman Marchin,AECOM Jennifer Wheat,AECOM :.0 t ` REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, r without the written consent of Pace Analytical Services,LLC. Page 1 of 12 Pace Analytical Services,LLC e aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.eom (704)875-9092 CERTIFICATIONS Project: Bendel-Revised Report Pace Project No.: 92467938 Pace Analytical Services Charlotte 9800 Kincey Ave.Ste 100, Huntersville,NC 28078 South Carolina Certification#:99006001 Louisiana/NELAP Certification#LA170028 Florida/NELAP Certification#: E87627 North Carolina Drinking Water Certification#:37706 Kentucky UST Certification#:84 North Carolina Field Services Certification#:5342 VirginiaNELAP Certification#:460221 North Carolina Wastewater Certification#: 12 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40 Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001 Massachusetts Certification#:M-NC030 VirginiaNELAP Certification#:460222 North Carolina Drinking Water Certification#:37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 12 Pace Analytical Services,LLC aceAnalytical 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pacNabs.coA (704)875-9092 SAMPLE ANALYTE COUNT Project: Bendel-Revised Report Pace Project No.: 92467938 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92467938001 SW-1 EPA 1664E HH 1 PASI-C EPA 200.7 Rev 4.4 1994 DS 3 PASI-A SM 2540D-2011 CJL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 12 Pace Analytical Services,LLC Ea aceAnalytical 9800 I<incey Ave. Suite100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Bendel-Revised Report Pace Project No.: 92467938 Sample: SW-1 Lab ID: 92467938001 Collected: 03/03/20 11:30 Received: 03/04/20 14:05 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM,TPH Analytical Method:EPA 1664E Total Petroleum Hydrocarbons ND mg/L 4.8 1 03/12/20 09:46 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Copper 52.3 ug/L 5.0 1 03/24/20 00:31 03/24/20 16:56 7440-50-8 Lead ND ug/L 5.0 1 03/24/20 00:31 03/24/20 16:56 7439-92-1 Zinc 218 ug/L 10.0 1 03/24/20 00:31 03/24/20 16:56 7440-66-6 2540D Total Suspended Solids Analytical Method:SM 2540D-2011 Total Suspended Solids 337 mg/L 41.7 1 03/09/20 18:33 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 12 Pace Analytical Services,LLC 9800 Kincey Ave. Suite100 aceAnalytical Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Bendel-Revised Report Pace Project No.: 92467938 QC Batch: 530031 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM,TPH Associated Lab Samples: 92467938001 METHOD BLANK: 2830510 Matrix: Water Associated Lab Samples: 92467938001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 03/12/20 09:34 LABORATORY CONTROL SAMPLE: 2830511 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 15.1 76 64-132 MATRIX SPIKE SAMPLE: 2830512 92467808002 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 7.4 19.2 9.8 13 64-132 M1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 12 Pace Analytical Services,LLC aceAnalytical 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pacelaba.coro (704)875-9092 QUALITY CONTROL DATA Project: Bendel-Revised Report Pace Project No.: 92467938 QC Batch: 532080 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92467938001 METHOD BLANK: 2840569 Matrix: Water Associated Lab Samples: 92467938001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 03/24/20 16:49 Lead ug/L ND 5.0 03/24/20 16:49 Zinc ug/L ND 10.0 03/24/20 16:49 LABORATORY CONTROL SAMPLE: 2840570 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Copper ug/L 500 496 99 85-115 Lead ug/L 500 492 98 85-115 Zinc ug/L 500 479 96 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2840571 2840572 MS MSD 92467938001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 52.3 500 500 586 570 107 104 70-130 3 Lead ug/L ND 500 500 507 496 101 99 70-130 2 Zinc ug/L 218 500 500 724 709 101 98 70-130 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 12 Pace Analytical Services,LLC ea 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.core (704)875-9092 QUALITY CONTROL DATA Project: Bendel-Revised Report Pace Project No.: 92467938 QC Batch: 529343 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92467938001 METHOD BLANK: 2827355 Matrix: Water Associated Lab Samples: 92467938001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/09/20 18:31 LABORATORY CONTROL SAMPLE: 2827356 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 251 236 94 90-110 SAMPLE DUPLICATE: 2827520 92467938001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 337 355 5 SAMPLE DUPLICATE: 2827521 92467984001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 9000 8270 8 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 12 Pace Analytical Services,LLC i ®aceAnalytcal 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pacelabs.cem (704)875-9092 QUALIFIERS Project: Bendel-Revised Report Pace Project No.: 92467938 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. LABORATORIES PAST-A Pace Analytical Services-Asheville PASI-C Pace Analytical Services-Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 12 Pace Analytical Services,LLC 9800 Kincey Ave. Suite100 aceAnalytical Huntersville,NC 28078078 www.paeslabs.con (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bendel-Revised Report Pace Project No.: 92467938 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92467938001 SW-1 EPA 1664E 530031 92467938001 SW-1 EPA 200.7 Rev 4.4 1994 532080 EPA 200.7 Rev 4.4 1994 532104 92467938001 SW-1 SM 2540D-2011 529343 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 12 Document Name: Document Revised:February 7,2018 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 aceAnalytieal y Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville❑ EdenE Greenwood❑ Huntersville❑ Raleigh❑ MechanicsvilleLl Sample Condition-- Client Name: W0# : 92467938 Upon Receipt t It ,, Project#: E Courier: ❑Fed Ex CUPS ❑LISPS ❑ClienttiiI''I'II'I"I� ❑Commercial ❑Pace ❑Other:_ l 82 467938 I Custody Seal Present? ❑Yes ~❑No Seals Intact? ❑Yes ❑No ( "� r) Date/Initials Person Examining Contents: )- 7 -((1 Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer: ❑Yes ❑No ON/A ❑IR Gun ID: 92T060 Type of Ice: :Met ['Blue Duane Cooler Temp('C): O 'II Correction Factor:Add/Subtract(°C) 0.0 Temp should be above freezing to 6°C Cooler Temp Corrected('C): • ❑Samples out of temp criteria.Samples on ice,cooling process has begun USDA Regulated Soil (a N/A,water sample) Did samples originate in a quarantine zone within the United States:CA,NY,or SC(check maps)? Old samples originate from a foreign source(internationally, ❑Yes Duo Including Hawaii and Puerto Rico)?❑Yes Duo Comments/Discrepancy: Chain of Custody Present?' • [(Yes ❑No ON/A 1. Samples Arrived within Hold Time? ❑Yes ❑No ON/A 2. Short Hold Time Analysis(<72 hr.)? Oyes Duo ON/A 3. 'Rush Turn Around Time Requested? Oyes Duo ❑N/A 4. Sufficient Volume? • Oyes Duo ❑N/A 5. Correct Containers Used? Oyes Ono ON/A 6. -Pace Containers Used? fives Duo EN/A Containers Intact? Oyes Duo ❑N/A 7. Dissolved analysis:Samples Field Filtered? Dyes Duo ON/A 8. Sample Labels Match COC? ❑Yes Duo ON/A 9. -Includes Date/Time/ID/Analysts Matrix: Headspace in VOA Vials(>5-6mm)? Oyes Duo ❑N/A 10. Trip Blank Present? Oyes Duo ON/A 11. Trip Blank Custody Seals Present? Dyes Duo ON/A COMMENTS/SAMPLE DISCREPANCY field Data Required? Dyes Ohio Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Ai (Il6 Date: 5 iLf 1-z:0(r l� Project Manager SRF Review: f5i\AR(.> Date: �jl Li/1) v Page 10 of 12 Document Name: Document Revised:February J,2018 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 ( ceAnalicar Document No.: Issuing Authority: F-CAR CS-033-Rev,06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project fi WO# 92467938 verified and within the acceptance range for preservation 03/13/20 samples. PM: NMG Due Date Exceptions:VOA,Coliform,TOC,Oil and Grease,DRO/8015(water)DOC,LLHg CLIENT: 92-AECOM CHA **Bottom half of box is to list number of bottle i 1 n a " v u 2 ¢ a a a vou aZt- a zN �,z m z z m m „Z Z Z a Z _ C Q Zn m S •_¢z7-7 -R .-, V _ _ ta> 2 2 2 2 = v c,, T = Cl N e v x x ¢ _ ? ¢ Z ? a,i r w w N e a n n "— a y v n n Z z ¢ '° z — ,n d 7 m W N `1 at 99 m Ql N I N y g CJ Q fn = Z N T V N .2 n a a n O Z ¢ O n •a j O r� E 2 2 0 o ii =ri c c a n D c = T. N Z a c tJ ry x ¢ vi —o 0 ., > i0 — z D 0 c u _ , u u u r I v = y V c ran .ti v «VI , = 7• u r u '- 2-, C ,n W l] E I z = I Jr 1,1 .92 - .Q Cl Cl 3 aa m 2 m m n p a -n E a E 0 a a a 4 d y u A E E a c. F. n a n a a E C Q ¢ E ¢ y 0 o 0 O g. n N ,n ¢ -, E E E a yg E E E D a`, a`i E v E g(;J E E E rO .3 E E E E E E N gi F. N N N N N 3 - - O - O Q OO O O O v > N O „a O O O rl .•1 N I q q •�•• N N nc 6 6 > > at N v 2 , i 6 vl yr a 2 H 7 S Y g > > > V, rr en .4 M f�5 or or Cr ci U' to f�i of O O� 61 a 6 0. a a a rL n In L.? t7 t7 t7 t7 t7 U' t7 t7 O \ d 0. n to t7 \m m m m m. m as \\m\ 3 a `\'a a ¢ a ¢ c > > o > > v+ \m a > o 1 \ ♦ _ r l� \\ 2 \ ,. . , \ _ . . 3 _ \ _ , 4 5 l _ } _ 6 \ , , \ „ 7 \ .— — — —— 8 \ 9 \ _ 10 \ \ \ l 11 \ \ '\ 12 \ \\1.\\ \\ , - — _ — - \ \-- - pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot ii adjusted added Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina DEHNR Certification Office(i.e. Out of hold,Incorrect preservative,out of temp,incorrect containers. Page 11 of 12 N � CHAIN-OF-CUSTODY ! Analytical Request Document N PdceAr>alyticai The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed accurately. CV .wr.¢uus cow m r0 Section A Section B Section C D_ Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1 Company AECOM,Charlotte Report To. Wheat,Jennifer Attention. Address: 6000 Fairview Rd Copy To: , _ - -, •,tly._r.t,�;,q, Company Name Suite 200,Charlotte,NC 28210 Address: Regulatory Agency Email: jennifer.wheat@aecom min Purchase Order#: Paco Quote, Phone: Fax Project Name: Bendel Pace Project Manager: rncole pasiorowski r@i pacelabs corn. State I Location Requested Due Date Project#: Pace Profile#: 6012-1 NC Requested Analysis Filtered(YIN) Z MATRIX cone — o COLLECTED Preservatives >- - Dunking Wale, OW 3 WOO WT W _ Wale WaIrt WW - m Z Plodanl P 9 o a SAMPLE ID C°°a j START END m Z c CM OL T a w CO N • One Character per box. W!Ve We _ EC -IS q All An o a com IA-t,O-BI,-) O rr,- m �. cJ st 0.0i OT U ,., O m g "' Sample Ids must be unique r,:,.°. T;: x w w p lil ¢ a a O d O Z c c :1:, —7/ i( . . 1— w DATE TIME DATE TIME rn ar D _ _ = z co 2. 0 Q i-- $ I-- tt ~I"` • `j�( rt t 2 I 3 ■ 4 5 6 7 8 9 10 11 -, - 12 - 1 ADDITIONAL COMMENTS RELINQUISHED 11'/,AFFILIATION DATE TIME ACCEPTED BY/AF=ILIATION DATE TIME SAMPLE CONDITIONS .S. SAMPLER NAME AND SIGNATURE U o PRINT(dame of P ER: ' .S e, (-- *vi,t A ill k oi--C 1 T/ a V n P. r i n SIGNATU = L R: _ D ,E,S gned: rw- v— U p1 g> w c-• Pace Analytical Services,LLC aceAnalytical© 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 March 26, 2020 Mr. Jim Rozsa Bendel Corp. 4823 North Graham St. Charlotte, NC 28269 RE: Project: Bendel-Revised Report Pace Project No.: 92467938 Dear Mr. Rozsa: Enclosed are the analytical results for sample(s) received by the laboratory on March 04, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. This revision was issued on 3/26/20 to include the correct client Chain-of-Custody, and to report the reanalysis result for lead, per client request. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Coleman Marchin,AECOM Jennifer Wheat,AECOM I...i�;.' REPORT OF LABORATORY ANALYSIS 1. This report shall not be reproduced,except in full, ' _raj without the written consent of Pace Analytical Services,LLC. Page 1 of 12 Pace Analytical Services,LLC 0 9800 Kincey Ave. Suite 100 _ aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 CERTIFICATIONS Project: Bendel-Revised Report Pace Project No.: 92467938 Pace Analytical Services Charlotte 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Certification#:99006001 Louisiana/NELAP Certification#LA170028 Florida/NELAP Certification#:E87627 North Carolina Drinking Water Certification#:37706 Kentucky UST Certification#:84 North Carolina Field Services Certification#:5342 VirginiaNELAP Certification#:460221 North Carolina Wastewater Certification#:12 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40 Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001 Massachusetts Certification#:M-NC030 VirginiaNELAP Certification#:460222 North Carolina Drinking Water Certification#:37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 12 Pace Analytical Services,LLC aceAnalytical 9800 Kinsey Ave. Suite100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: Bendel-Revised Report Pace Project No.: 92467938 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92467938001 SW-1 EPA 1664E HH 1 PASI-C EPA 200.7 Rev 4.4 1994 DS 3 PASI-A SM 2540D-2011 CJL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 12 (." Pace Analytical Services,LLC 0 9800 aceAnalyticalHulntersvlte,NC128078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Bendel-Revised Report Pace Project No.: 92467938 Sample: SW-1 Lab ID: 92467938001 Collected: 03/03/20 11:30 Received: 03/04/20 14:05 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM,TPH Analytical Method:EPA 1664E Total Petroleum Hydrocarbons ND mg/L 4.8 1 03/12/20 09:46 200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994 Copper 52.3 ug/L 5.0 1 03/24/20 00:31 03/24/20 16:56 7440-50-8 Lead ND ug/L 5.0 1 03/24/20 00:31 03/24/20 16:56 7439-92-1 Zinc 218 ug/L 10.0 1 03/24/20 00:31 03/24/20 16:56 7440-66-6 2540D Total Suspended Solids Analytical Method:SM 2540D-2011 Total Suspended Solids 337 mg/L 41.7 1 03/09/20 18:33 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 12 Pace Analytical Services,LLC aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Bendel-Revised Report Pace Project No.: 92467938 QC Batch: 530031 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM,TPH Associated Lab Samples: 92467938001 METHOD BLANK: 2830510 Matrix: Water Associated Lab Samples: 92467938001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 03/12/20 09:34 LABORATORY CONTROL SAMPLE: 2830511 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 15.1 76 64-132 MATRIX SPIKE SAMPLE: 2830512 92467808002 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 7.4 19.2 9.8 13 64-132 M1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 12 (11( ' Pace Analytical Services,LLC © 9800 Kincey Ave. Suite 100 aceAnalytical® Huntersville,NC 28078 www.pacelabs.cam (704)875-9092 QUALITY CONTROL DATA Project: Bendel-Revised Report Pace Project No.: 92467938 QC Batch: 532080 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92467938001 METHOD BLANK: 2840569 Matrix: Water Associated Lab Samples: 92467938001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 03/24/20 16:49 Lead ug/L ND 5.0 03/24/20 16:49 Zinc ug/L ND 10.0 03/24/20 16:49 LABORATORY CONTROL SAMPLE: 2840570 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Copper ug/L 500 496 99 85-115 Lead ug/L 500 492 98 85-115 Zinc ug/L 500 479 96 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2840571 2840572 MS MSD 92467938001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Copper ug/L 52.3 500 500 586 570 107 104 70-130 3 Lead ug/L ND 500 500 507 496 101 99 70-130 2 Zinc ug/L 218 500 500 724 709 101 98 70-130 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 12 Pace Analytical Services,LLC a aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Bendel-Revised Report Pace Project No.: 92467938 QC Batch: 529343 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92467938001 METHOD BLANK: 2827355 Matrix: Water Associated Lab Samples: 92467938001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 03/09/20 18:31 LABORATORY CONTROL SAMPLE: 2827356 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 251 236 94 90-110 SAMPLE DUPLICATE: 2827520 92467938001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 337 355 5 SAMPLE DUPLICATE: 2827521 92467984001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 9000 8270 8 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 12 Pace Analytical Services,LLC i ®aceAnalytcal 9800 Kincey Ave. Suite100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Bendel-Revised Report Pace Project No.: 92467938 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services-Asheville PASI-C Pace Analytical Services-Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 12 Pace Analytical Services,LLC aceAnalytical© 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.corn (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bendel-Revised Report Pace Project No.: 92467938 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92467938001 SW-1 EPA 1664B 530031 92467938001 SW-1 EPA 200.7 Rev 4.4 1994 532080 EPA 200.7 Rev 4.4 1994 532104 92467938001 SW-1 SM 2540D-2011 529343 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/26/2020 02:30 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 12 Document Name: Document Revised:February 7,2018 b Sample Condition Upon Recelpt(SCUR) Page 1 of 2 (e!2eAnalylicar Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville❑ Eden❑ Greenwood❑ Huntersville❑.-.'f Raleigh❑ MechanicsvilleD Sample Condition- Client Name: WO# •x 92 467938 Upon Receipt / } rr , ; 1/ 1 Project#: Courier: Ora Ex ❑UPS DUSPS _ ['Client I 11141111141E ❑Commercial ❑Pace ❑Other: t 92467938 Custody Seal Present? DYes -0No Seals Intact? Dyes LINo • ' it Date/Initials Person Examining Contents: 'i -" Packing Material: ['Bubble Wrap ['Bubble Bags ['None ❑ Other Biological Tissue Frozen? Thermometer -" Dyes ONo ❑N/A QIAGun ID: 92TO60 Type of Ice: ©Wet ❑Blue ❑None Cooler Temp('C): ( ; -i Correction Factor:Add/Subtract(°C) 0.0 .i Temp should be above freezing to 6°C Cooler Temp Corrected('C)i ' 0 ❑Samples out of temp criteria.Samples on ice,cooling process has begun USDA Regulated Sall (IN/A,water sample) Did samples originate in a quarantine zone within the United States:CA,NY,or SC(check maps)? Did samples originate from a foreign source(internationally, Oyes QNo •: Including Hawaii and Puerto Rico)?Dyes DNo i Comments/Discrepancy: 6hainofCustoilyPresent?`�'° El es ❑No ON/A 1. Samples Arrived within Hold Time? (]Yes ONo ON/A 2. ;Short Hold Time Analysis(<72:1r:)? Dyes [NO ON/A ' 3. (Rush Turn Around Time Requested? ❑Yes ONO.- ON/A 4. .• :Sufficient Volume? 1 Oy ❑No ON/A S. Correct Containers Used? Des ONo ON/A 6. -Pace Containers Used? DY s Do ❑N/A , Containers Intact? Mes DNo ID N/A 7. Dissolved analysis:Samples Field Filtered? Dyes DNo []N/A 8. Sample Labels Match COG? Dig; ❑No ON/A 9. I-Includes Date/ Time/ID/Analysis Matrix: I,,,•' 1 . Headspace In VOA Vials(>5-6mm)? Dyes ❑No []N/A 10. Trip Blank Present?, ❑Yes ONO ON/A 11. Trip Blank Custody Seals Present? Dyes Ono ON/A- • COMMENTS/SAMPLE DISCREPANCY Field Data Required? Oyes DNo Lot ID of spilt containers: 'CLIENTNOTIFICATION/RESOLUTION • Person contacted: Date/Time: Project Manager SCURF Review: N`rJ e Date: J- jL//Z21) Project Manager SRF Review: ,- G Date: Zjl P 1 J Page 10 of 12 Document Name: Document Revised:February 7,2018 J Sample Condition Upon Recelpt(SCUR) Page 1 of 2 __, aceAnalytical Document No.: Issuing Authority: F-CAR-05-033-Rev.O6 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project# ' Wo# : 92467938 verified and within the.acceptance range for preservation samples. PM: NMG Due Date: 03/13/20 Exceptions:VOA,Coliform,TOC,Oil and Grease,DRO/801S(water)DOC,LLHg CLIENT: 92-AECOM CHA **Bottom half of box is to list number of bottle I i b ZZ 7 2S a a — - -0. z _ 7, ` ` z Z z z Q uNN a- z z M 'j AZ N .-i = z -0 Cz I Q > d V ^ vS2 Q « y , 2z -0 FA w n a a ,a a ". a ei .a. z ct .1_ : -i- ? gel'O m E a. m O ¢ O a = O E 2 N z v o E. " t ry c v S > a . = Z N Z 7 y L., = 2 Q U ,.,2, 0. 0 > a 2 2 c9. uuu uu. uL v v D y a E x D M L Y a _ a A ,4 Y A 2 % 2 o -g .n E '° E 2 E a a C mhvv ,o E c c a o m a 0. EQ44CQ yO p 0 O a E, J — 4 n 6E g E a` E E J J -CI ..1-?, w E 5 a E EE 0 9 E E E E Eg 2 8 ,v 6 e o _ c 0 q uti o 0 moan '' N � - ' N -/ rri r1 '7' Ny N `f 7 ¶ - r-ry N Q a E a m N .s a a e a rl m ." m cs m 4T) 0 la !n 7v r� of 8m m m m m m m m 3 a a a a a a o a > o > > °u, . a > o I. \ i \ \ \2 \ , . : . \ \ 3 \ \ 4 \ _ . 5 \ \ . \ \\\\*\ _ _ . 6 \ \ \\2 _ \ --— - \ -- \ ---_ -- -- -- 8 \ . \ _ _ 9 \ 10 \ — 11 \ ': \ \ ' 12 \ i \ \ pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot 8 adjusted added Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina DEHNR Certification Office(i.e. Out of hold,Incorrect preservative,out of temp,incorrect containers. Page 11 of 12 N � CHAIN-OF-CUSTODY/Analytical Request Document N -PaceAnalytical The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed accurately. m NW..nrtOS we CIS CO Section A Section B Section C Q- Required Client Information: Required Project Information: Invoice Information: Page 1 Of 1 Company. AECOM,Charlotte Report To: Wheat,Jennifer Attention: Address: 6000 Fairview Rd Copy To: {.-,� ,t{..:,t :K d.-,Z.f,t,.i i q; Company Name: Suite 200,Charlotte,NC 28210 Address: Regulatory Agency Email: jennifer.wheat©aecom.com Purchase Order#: Pace Quote: Phone: IFax. Project Name: Bendel Pace Project Manager: nicole.gasiorowskicpacetabs.com, State FLocation Requested Due Date: Project#: Pace Profile*: 6012-1 NC Requested Analysis Filtered(YIN) a' Z ° `o COLLECTED Preservatives >- MATRIX CODE re V Dunking Water OW 61 O Water WT S m U Wa;fe Warc, W —W Q-ca cc j 2- Puttied SAMPLE ID O'' m DL .ill. C? START END co 2 One Character per box. wive WP w ul a = v m w i° . (A•Z.0.91 r-) Au AR p 0}. F -. m to o U Other OT I- t G a # Sample Ids must be unique Tree. Ta x 5 a7 = m o 0 N w% oN 51 W � � � o a � Z m aagN � C6-0 7 �( i- - w DATE TIME DATE TIME N .e D 2 S X Z Z 2 O I- m r i T��2' i ljj //' �� tip ` * co/ , 2 , r 3 4 5 6 7 8 , 9 10 11 12 , ADDmONAL COMMENTS RELINQUISHED 4ll(hFFILIATION • DATA TIME ACCEPTED BY IAF ILIATION DATE TIME SAMPLE CONDITIONS _..-5e9 a l l 51 ,>I ,j y`.12/-1 f i/( / i- _ i ,z � /',,7- i SAMPLER NAME AND SIGNATURE o PRINT Name of P ER: A i� w m / C.OG Vtlti4 i..: / 0/6 l�'1,y(r a o v `m n z SIGNATU = R .�.- .--,DlJfAligned: rw- CC m} t i rn.U> co c-..