Yancey Co. Complaints 2019

GLEN AVEN°
April 3, 2019
Mr. G. Landon Davidson, P.G.
Regional Supervisor
NCDEQ Division of Water Resources
Asheville Regional Office
2090 US 70 Highway
Swannanoa, North Carolina 28778
Subject: Notice of Violation
Incident No. 201900630
Glen Raven Custom Fabrics, LLC
Burnsville, Yancey County, North Carolina
Dear Mr. Davidson:
DMIslon OY Walar KOsOOluv
APR 4 2019
Water Qusl". R 'glonal operadons
1 r 1 1(?fce
Glen Raven Custom Fabrics, LLC is submitting this letter to provide information related to the
above referenced Notice of Violation dated March 26, 2019. Upon discovery that extrusion
cooling water was discharging to the on site stormwater collection pit, Glen Raven Custom Fabrics
Burnsville Plant immediately initiated the following actions:
Glen Raven Custom Fabrics — Burnsville Plant maintenance personnel removed the pumps
from the stormwater collection pit;
The NCDEQ Division of Water Resources was notified of the incident;
Glen Raven Custom Fabrics — Burnsville Plant maintenance personnel rerouted extrusion
cooling water discharge to the sanitary sewer;
A third party environmental firm collected a grab sample of water in the stormwater pit
and a grab sample of extrusion process cooling water and submitted both by chain -of -
custody protocol to a drinking water certified laboratory for analysis of the following
parameters (one week turn -around requested);
COD pH EPA Method 8270 (semi-volatiles)
BOD TSS EPA Method 8260 (volatiles)
A third party laboratory scheduled additional certified field analysis for total residual
chlorine (TRC) for week ending April 6, 2019.
The Glen Raven Custom Fabrics — Burnsville Plant is currently developing the following
additional activities in response to the incident:
Glen Raven Custom Fabrics — Burnsville Plant will review potential environmental
permitting issues related to the local sewer use ordinance and pretreatment requirements;
Glen Raven Custom Fabrics — Burnsville Plant will address potential training issues with
all engineering, production and maintenance personnel, which will include enhanced
GLEN RAVEN, INC. 1831 NORTH PARK AVENUE, GLEN RAVEN, NC 27217-1 100 T. (001( 336-227-621 1 WWW.GLENRAVEN.COM
GLENRAVEN" general
stormwater permit annual training, a detailed review of allowable stormwater discharges
and a general review of the Clean Water Act; Glen
Raven Custom Fabrics — Burnsville Plant will review and modify, as necessary, the current
policy of environmental review and approval of all projects in an effort to capture potential
environmental issues that may arise as a result of the proposed scope of work; Glen
Raven Custom Fabrics — Burnsville Plant will submit a subsequent letter report of analytical
results to the NCDEQ Division of Water Resources within one week of receiving analytical
reports. The
Glen Raven Custom Fabrics — Burnsville Plant takes pride in its environmental and safety records
and understands that targeted actions are needed to prevent any similar occurrence in the future.
Glen Raven Custom Fabrics, LLC will treat this incident as an opportunity to improve existing
programs, including enhanced training of employees and management throughout the company.
Should you have any questions of require additional information, please call me at (828) 682-
2142. Sincerely,
GLEN
RAVEN CUSTON FABRICS, LLC Wendell
Wilson Plant
Manager CC:
Kelsey Herring — Glen Raven Custom Fabrics - Environmental Coordinator Charles
Walser — Glen Raven Corporate Manager — Safety, Security & Environmental Affairs GLEN
RAVEN, INC. 1831 NORTH PARK AVENUE, GLEN RAVEN, NC 27217-1100 T. (001( 336-227-6211 WWW.GLENRAVEN.COM
Apr118, 2019
Mr. G. Landon Davidson, P.G.
Regnal Supervisor
NCOEQ Division of Water Resources
Ashville Regional Office
209OUS 70 Highway
Swadnanoa, North Carolina 28778
Subject: Notice of Violation
Incident No. 201900630
Glen Raven Custom Fabrics, LLC
Burnsville, Yancey County, North Carolina
DearMr. Davidson:
eh ti a4ll mrFlos ev
APR 14 2019
Wgter [],on.a i°
As promised, Glen Raven Custom Fabrics, LLC is submitting the results pertaining to the above
referenced Notice of Violation dated March 26, 2019.
Should you have any questions of require additional information, please call me at [phone].
Sincerely,.
GLEN RAVEN CUSTON FABRICS, LLC
Wendell Wilson
Plant Manager
CC.' Kelsey Herring —Glen Raven Custom Fabrics - Environmental Coordinator
Charles Walser —Glen Raven Corporate Manager — Safety, Security & Environmental Affairs
GLEN RAVEN, INC. 1831 NORTH PARK AVENUE, GLEN RAVEN, NC 272TTt 100 T.1001I33622T6211 N EGLENRAVFN.COM
ace Analytical
mvn,parslebe..
April 15, 2019
Steven Gerrald
Leaf Environmental & Engineering, P.C.
1426 NC-54
Durham, NC 27713
RE: Project: Glen Raven 4/2
Pace Project No.: 92423737
Pace Analytical Services, LLC
9800 K'ow, Ave. Suite 100
HunteraMle, NC 28078
p047875-9092
Dear Steven Gerrald:
Enclosed are the analytical results for sample(s) received by the laboratory on April 02, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
828)254-7176
Project Manager
Enclosures
cc: Tim Monroe, Leaf Environmental & Engineering, PC.
REPORT OF LABORATORY ANALYSIS
rhia report ahau not be reprodccad, except to full,
without the written consent of Pace Analytical Services, LLC.
U4,
APR 2 A 2019
Water fi r l
Page 1 of 6
aceAnalytical
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CERTIFICATIONS
Pace Analytical Services, LLC
9800KIncey Ave. suibarea
Huntarsvllle, NC 28078
704)875-9092
Project: Glen Raven 412
Pace Project No.: 92423737
Charlotte Certification M.
9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001
LouisianalNELAP Certification#L l70028 FloridaMELAP Certification #: E87627
North Carollna Drinking Water Certification#: 37706 Kentucky UST Certification #:84
North Carolina Field Services Certifcadon #: 5342 VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be repmduoad, except in full
without the written consent m Pace Analytical Services, LLC. Page 2 of 6
Pace Analytical Services, LLC
aceAna6tical' 9800 Klncey Ave. Suite 100
Munteraville, NC 28e78
awrvpxNabamm
e4)e]5-9092
ANALYTICAL RESULTS
Project: Glen Raven 4/2
Pace Project No.: 92423737
Sample: RAINCATCHMENT Lab ID: OU23737001 Collected: 04/0211913:30 Received: 04/02/1915:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data Analytical Method
Collected By Thomas 1 04102/1913:30
O'Shea
Collected Date 412119 1 04/02119 13:30
Collected Time 13:30 1 04/0211913'.30
Chlorine, Total Residual c220 Tel [phone]:30 ]]82-50-5
Sample: LINE Lab ID: 92423737002 Collected : 04102/1914:00 Received: 0410211915:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data Analytical Method
Collected By Thomas O 1 04102/1914:00
Shea
Collected Date 412119 1 04/02/1914:00
Collected Time 14:00 1 0410211914:00
Chlorine, Total Residual <220 mg/L 0.050 1 0410211914'.00 ]]82-50-5
REPORT OF LABORATORY ANALYSIS
Thicreportshall not bereproduced, exceptin full,
Date: 041151201909:39 AM Wuhout the Wnttsn con.ant.f Pacennelytlwl services, LLC. Page 3 of 6
aceAnalytical
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QUALIFIERS
Project: Glen Raven 4/2
Pace Project No.: 92423737
DEFINITIONS
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntermville, NC 28078
704)875-e092
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
MDL-AdjustedMethod Detection Limit.
POL - Practical Commutation Limit.
RL- Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S- Surrogate
1,2-Dipheny1hydrezine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unmunded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate fort Chloroethylvinyl ether
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofArmlein and AcryloniUile by EPA
Method 8260.
N-Nitroso liphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyses.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services -Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date'. 04/161201909:39 AM without the wants consent of Pace Analytical Services,LLG. Page 4 of 6
Pace Analytical SONIC as, LLC
9800 Kincey Ave. Suite 100aceAnalyticaluntereville, NC 28078
amvpecsabact. (]04)8]5- 9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Glen Raven 4l2
Pace Project No.: 92423737
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92423737001 RAIN CATCHMENT
92423737002 LINE
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in for
Date: 04115/201909:39 AM wil the sell consent of Pars anaytical Services,LLC, Page 5 of
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ENCO Laboratories
lcGnrate. Timely. Responsive, Innovative.
102-A Woodwinds Industrial court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Wednesday, April 10, 2019
Leaf Environmental, Inc. (BE012)
Attn: Tim Monroe
PO BOX 14609
RTP, NC 27709-
RE: Laboratory Results for
Project Number: 203796, Project Name/Desc: 103796
ENCO Workorder(s): CCO5007
Dear Tim Monroe,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, March 29, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
LWrlAPR 24 2019
Chuck Smith
fauFlgy, I•iProjectManager
P=n oerntlona
Enclosure(s) -----
FINAL This report Nadal only to the wmple s:,xmved by No labamrory, and may only No repmdddJ In Nil. Pope 1 or 22
www.encolabs.cos,
SAMPLE SUMMARY/LABORATORY CHRONICLE
CllentID: Wastewater Lab ID: CCO5007-01 Sampled: 03/29/19 10:15 Ruaaaa 0: 03/29/19 15:00
P3Ci35£ Ba gamed_ Holtl Oare/Time(s) Preo Date/Time(s) Analysis DatelTimelsl
EPA 8260D EPA 5030B_PC C4/12/19 04/02/19 15A2 04/02/19 20.10
EPA 8270E EPA 3510C_MS 04/05/19 05/11/19 04/01/19 11:33 04/02/l9 01:03
SM 2540D-2011 NO PREP 04/05/19 04/04/19 12:45 04/04/19 1245
SM 5210 0,2011 NO PREP 03/31/19 MIS 03/30/19 13'.43 03/30/19 1343
SM 5220D-2011 Same 04/26/19 041OV19 13:50 04/02/19 1631
Client ID: Sump Lab ID: CCO5007-02 Sampled: 03/29/19 10:30 Recelvetl: 03/29/19 15:00
Pare,, P1YpeL3D Held Date/r'mehl Pre, Datelrmerel Analves Date/rme(s)
EPA 8260D EPA 5030B_ME 04/12/19 04JR/19 15:42 04/02/19 20:42
EPA 9270E EPA 3510CM5 04/05/19 05/11/19 04/01/19 11:33 04/02/19 01:33
SM 2540D-2011 NO PREP 04/05/19 04/04/19 12A5 04/04/19 12:45
SM 5210 B-2011 NO PREP 03/31/19 10:30 03/3/19 1143 OW30/19 13:43
SM 522OD-2011 a 04/26/19 04/02/19 13:50 N10419 1631
Client ID: Trip Blank Lab ID: CC05007-03 Sampled: 03/29/19 30:15 Revived: 03/29/19 15:00
Pd[SD1454[prepared, Hold Date/Time(s) pass Date/Time(sl Analysis Gate/Time(sl
EPA 8260D EPA 5030B MS 04/12/19 04/02/19 15:42 041GO19 21:13
APR 2 4 2019
Water qv I
A _._ raharrtT
FINAL mismport relate—lym the sample a::e¢rvM by leemborzta,, and may per be mpmeu[el m Nu. Page 2 of 2
ENCO
www.enmlabs.com
SAMPLE DETECTION SUMMARY
client lo: wartewafer Labro: CCO5007-01
Aea lWe Real Mae MPL M Ul Method N210
2,4,&Trl[hJ,mo enol 47 2.6 10 ug/L EPA 8270E
2,4-Dichlarophenol 15 2.6 10 ug/L EPA 8270E
2-Chloropbeno1 3.4 1 2.2 10 ug/L EPA 8270E
Anal 24 10 20 ug/L EPA 82WD
Blahemical Orygem Demand 3.7 2.0 2.0 mg/L SM 5210&2011
BIS(2-NbyEegl)phtm1ate 9.0 1.9 5.0 bad. EPA 8270E
Chemical Oxygen Demand 21 30 10 mg/L SM 5220D-2011
ISoorawlbenrelle 1.0 1.14 10 m/L EPA 8260D
Acetone 12 1 30 20 ug/L EPA 8260D
Bi.m.ital Chat Demand 3.9 2.0 2.0 mg/L SM 5210 B-2011
Bls(2-e@ylheryl)phthalate 4.5 1 1.9 5.0 ug/L EPA 8270E
ChemiGl Onygen Demand 28 10 10 mg/L SM 5220D-2011
1Ill Thb report relates only to the sample ae rerelved by de labo eem, and may only be romll In full. vage3 of 23
Www.encolaba.com
ANALYTICAL RESULTS
Descrlptient Wastewater Lab Sample ID:C105007-01 Received: 03/29/19 15:00
Matrix: Waste Water Sampled: 03/29/1910:15 Work Order: CCA5007
project: 103796 Sampled By: Steven Gerrald
Anal 1CAS Numberl sneaks FJgq 1.IBlt6 PE MDL POLL Batch Method Analysed y Notec
1,1,1,2-Teba alvacthane[630-20 6]A 0.17 D u9IL 1 0.17 1.0 9D02040 EPA B260D 04102/19 20:10 MRK
1, 1,1-TriCM1lometlane[71-55-6]1 0.12 U u9IL 1 0.12 1.0 9D02040 EPA 8260D D4/@/19 20a0 MRK
1,1,2,2-TNrachlotoHM1ane[79345]1 0.28 a u9IL 1 0.28 1.0 9D02040 EPA 8260D O4/02/19 20:10 MRK
1,1,2-Trkh1PPceOhane[79-00 or 0.14 ll u9IL 1 0.14 1.0 9D02040 EPA 8260D 04/02/19 20:10 MRK
1,1-Dichlaraethes,[75 343]1 O,13 a ug/L I 0.13 LO oral EPA 8260D 04/02/19 20:10 MRK
1,1-DiCM1IOraMM1ene[2535-4]1 0.21 U ug/L 1 0.21 1.0 9DOd040 EPA 8260D 04/02/19 20:10 MRK
1,1-1schitrapropene[563-58 6]A 0.15 U u9IL 1 0.15 1.0 9D02040 EPA 8260D 04/02/19 20a0 MRK
1,2,3-TtlUlorabenzene(87 61-6]A 0.012 U ug/L 1 0.012 1.0 9D02040 EPA 8260D 04/02/19 20:10 MRK
1,2,3-Trahlompmpane[96-104]A 0.23 U ug/L 1 0.23 1.0 9D020Q EPA 8260D 04/02/19 20:10 MRK
1,2,4Tricblombenzene[120 82-1]A 0.14 U u9IL 1 0.14 LD 9002040 EPA 0260D 04/02/19 20:10 MRK
1,2,4Trimethylbenzene[95-6M]A 0.10 U u9IL 1 0.10 1.0 9ool EPA 8260D 04/02/19 20:10 MRK
1,2-Dlbromo-3-chbropmpane[96-12-8]A 0.48 U og/L 1 0.48 1.0 9DW040 EPA 8260D 04/02/19 20:10 MRK
1,2-Dibromoethane[106-934]A 0.66 U ug1L 1 0.66 1.0 9DD2040 EPA 8260D 04/02/19 20:10 MRK
1,2-Dichlorobenzene[95-50l 0.19 U u9IL 1 0.19 1.0 gD02D40 EPA 8260D 04/02119 20:10 MRK
1,2-Dichlomethane[102-06-2]A 0.21 D u9IL 1 0.21 1.0 9002040 EPA 8260D 04/02/19 20:10 MRK
1,2-DlcMompropane [78-87-5]1 0.10 D ug/L 1 0.10 1.0 9D02040 EPA 0260D 04/02/19 20:10 MRK
1,3,5-Trlmethylbenzene(108-62-8]A 030 U u9/L 1 0.30 1.0 9D02090 EPA 8260D W/lR/l9 20:10 MRK
1,3-Dichlorobenzene[541-71lr 0.15 U u9IL 1 0.15 1.0 9D02040 EPA 8260D 04/02/19 20:10 MRK
1,3-Dich1ompropane[142-28-971 0.16 U u9IL 1 0.16 1.0 9DO204D EPA 8260D 04/02/19 20:10 MRK
1,4-Dichlombenzene[10E4&7]A 0.19 U ugh 1 0.19 1.0 9D02090 EPA 8260D 04/02/19 20:10 MRK
21-Dichloropropene[594-20l 0.28 U ug/L 1 0.28 1.0 9D02D40 EPA 8260D 04/IID119 20;10 MRK
2-Butanone[76-93-31A 1.3 U u9IL 1 1.3 5.0 9DOl EPA 8260D 04/02/19 20:10 MRK
2-Chlerachyl ethyl Ether[ 110 75-B]A 1.1 a ug/L 1 1.1 5.0 oral EPA 8260D 04/02/19 20:10 MRK
2-Chlorotoluene[95-49-8]A 0.081 U ug/L 1 0.081 1.0 9D02040 EPA 8260D W/02/19 20:10 Max
2-Hexanone[591-78-6]A 0.88 U u9IL 1 0.88 5.0 9DD2040 EPA 8260D W/02/l9 20:10 MRK
4LhlorotDluene[106-43-4]A 0.068 U u9IL 1 0.068 1.0 9D02040 EPA 9260D 04/02/19 20:10 MRK
4-Isopmpy1taluene[99-87-6]A 0.085 U u9IL 1 0.085 1.0 9D020Q EPA 8260D 04/02/19 20:10 MRK
4Pkrhy1-2-pentarwne[108-10-17A 1.1 U, up/L 1 1.1 5.0 9D02040 EPA 8260D 04/02/19 20;10 MRK
Acetone [67-64-11A 2A ug/L 1 10 20 9D02040 EPA 8260D D4/02/19 20:10 MRK
Benzene[21-43-2]A 0,15 a u9IL 1 0.15 1.0 9D02040 EPA 8260D 04/02/19 20:10 MRK
Bramabenzene[106-86-1]A 0.16 U u9IL 1 0.16 1.0 9D02040 EPA 8260D W/02/19 20:10 MRK
BmmochlDromal[24W-51A 0.48 U u9IL 1 0.48 IA 9D02040 EPA 8260D 04/0419 20:10 MRK
Bromedichloromethane[75-274]A 0.17 U ug/L I 0.17 1.0 9002040 EPA 8260D 04/0211920: 30 MRK
Bromoform[75-25-2]A 0.22 U u9IL t 0.22 1.0 9D0200 EPA 8260D 04/02/1920: 10 MRK
Bmmomethane[74-83-9]A 0.14 U u9/L 1 0.14 1.0 9Dl EPA 8260D 04/02/19 20:10 MRK
Carbon diulflne[T5-15.01A 1.5 a u9IL 1 1E 5.0 9D112W0 EPA 8260D 04/02/19 Ell MRK
Cartoon tet2chlorid,[56-23-5]A 0.17 D ug/L 1 0.17 1.0 9D112040 EPA 8260D 04/02/19 20'.10 MRK
Chlorobenzene[108-90-71A 0.17 U ug/L 1 0.17 1.0 9DO2040 EPA 0260D 04/02/19 20:10 MRK
Chlomethene[75-DD-31A 0.23 U ug/L 1 0.23 1.0 9DD2040 EPA 8260D 04/02/l9 20:10 MRK
CM1lorolam[67-663]A 0.18 D u9/L I 0.18 1.0 9002040 EPA 82690 W/@/19 20:10 MRK
Chiberandeane[749-3]A 0.13 U u9IL 1 0.13 1.0 9D0200 EPA 81601) 04/02/19 20:10 MRK
cis-1,2-Dichlmoethal[156-59-2]1 0.15 U ug/L 1 0.15 1.0 9D02040 EPA 82601) 04/02/19 20:10 MRK
the-1,3-DicNoropzopene[1006101-5]A 0.20 U u9IL 1 0.20 1.0 9D02040 EPA 8260D A102119 20:10 MRK
DlbmmocM1lommethane[12,-Q-t]A 0.17 U ug/L 1 0.17 1.0 9D02040 EPA 8260D 04/02/19 20.10 MRK
Dinarromethane[74-95-3]A 0.27 U ugh 1 0.27 1.0 9D02040 EPA 8260D 04/02/19 20:10 MRK
Dichlmorll0uoromethane[75-71-8]A 0.20 D u9IL 1 0.20 1.0 9D02040 EPA 0260D W/02/19 2010 MRK
Ethylbenzene[10041-4]A 0.13 U u9IL 1 0.13 1.0 9D02040 EPA 82600 0402/19 20:10 MRK
FINAL Thla re Pon relates only to the Ample a5 reel by the laboratory, aM may only be reprWwetan At Page 4 of 32
ENCO
www.encolabe.com
ANALYTICALPESULTS
Description: Wastewater Lab Sample ID:000500-01 sessional 03/29/1915:00
Matrix: Waste Water Sampled:03/29/19 10:15 Work Orders CCO5007
Project: 103796 Sampled 6y:5teven Gerald
GCMS
Appal ICASNumberl FroulI6 BAR Made a MOL PPOL each Method Analysed Re fbi
HexacM1bmbutanlene[82-68-3]^ 0.22 U ug/L 1 0.22 1.0 9D02W0 EPA 3260D 04/02/1920:10 MRK
Ieopre"lbenxene[911.1 ^ 1.0 ug/L 1 0.14 1.0 9002040 EPA 8260D 0410211920.10 MRK
m, Xylenes[108-38-3/10642-3]^ 0.17 U Ir9/L 1 0.17 2.0 9DO204D EPA 8260D 04/02/1920: 10 MRK
Matt chlollde[75-09-21A 0.23 U ugh 1 0.23 1.0 9D4ID40 EPA 8260D 04/02/1920: 10 MRK
MMhyl-tart-Butyl Mer[I63 04-41^ 0.16 U ug/L 1 0.16 1.0 91,02040 EPA 8260D M/02/1920: 10 MRK
all alene[91-203]A 0.11 U ml 1 0.11 1.0 9D02040 EPA 3260D 04/02/1920: 10 MRK
n-Butyl Become[304-51-8]^ 0.059 U til 1 0.058 1.0 9DO2040 EPA 8260D 04J0211920: 10 MRK
n-Pmpyl Bermene[ID365-11^ 0.12 U ug/L 1 0.12 1.0 9D02090 EPA 8260D 04/0211920:10 MRK
o-Xylene(95-47-6]A 0A65 U u9/L 1 0.065 LD 9DO2040 EPA8260D 04/02/1920: 10 MRK
secButylbenune[135-98-87A 0.10 U ug/L 1 0.10 1.0 9002040 EPA 8260D D4/02/1920: 30 MRK
Styrene[10042-5]A 0.11 U ug/L 1 0.11 1.0 9002040 EPA 8260D 09/02/1920: 30 MRK
teR-Burylben2ene[98-a6-6]A 0.17 U ug/L 1 0.17 1.0 9DO2040 EPA 8260D 04/02/1920:10 MRK
Tetrachloroethene[122-18-4]A 0.17 U ogh 1 0.17 LO 9DO2040 EPA 8260D 04/02/1920:10 ARK
Tell[30B-BB-3]A 0.14 U u9/L 1 0.14 1.0 94,02040 EPA 8260D all 20: 10 MRK
trans-1,2-DI&I.emethene[156-605]A 0.21 U ml 1 0.21 1.0 9002040 EPA 8260D D4/02/1920: 10 MRK
t2na1,3-0ICMoroprapene[10061-112-6]^ 0.15 U ug/L I 0.15 1.0 9002040 EPA 8260D 04/02/I920: 10 MRK
Trent, 0.15 U ugh 1 0.15 1.0 9DO2040 EPA 8260D 04/02/1920:10 MRK
Trichlorofiuomme0tane[75-69411 0.24 U ug/L 1 0.24 1.0 9Do20W EPA 8260D 04/02/1920:10 MRK
Vinyl chloride[75-01-4]A 0.32 U ug/L 1 0.32 1.0 9DO2040 EPA 8260D 04/02/1920:10 MRK
ylenes[Totep[3330-2077A 0.95 U ug/L 1 0.45 3.0 9DO2040 EPA 8260D 09/e2/1920. 10 MRK
SM_".1sor. Resu/M DF pjka,4 Roc so, Roc[/m/[s Bp(pQ meiL2p AoalrzeC Rye Net,
9-8m benzprM 50 1 50.0 101 % 53-136 90@010 EnA 8260D 09/@/1920, 10 MRK
OlDroma/luommeth3ne 50 1 500 100% 67129 90OX40 EPA 82600 OVAOL1920.'10 MRK
Ta/cece48 51 1 50.0 102% 5A134 9002040 EPA 82600 WrrOel920. 10 Al
Semivolatile Organic Compounds by GCMS
A-- cay rn88eoana4*a re" ell
AnalVtt PEAS Nomberl Relates" Fla. Union DF NDS R" 3[d2 Method spoliate @y N429F
1,2,4Tr1<hlorabenune[120-82-1]1 2.5 U ug/L 1 2.5 10 9DO1013 EPA 8220E 04/02/190103 DFM
1,2-Dlchboasynzene[95-501]A 2.5 U ug/L I 2.5 10 9DO1013 EPA 8220E 04/02/1901:03 DFM
1,YOichlorobeazena[541-731]A 2.5 U u9/L 1 2.5 10 9DO1013 EPA 8220E 04/02/190103 DFM
1,4-01chlambenzens[106467]A 2.4 U ug/L 1 2.4 IO 9DO1013 EPA 8220E M/02/19 D3:03 DEM
1-Methylnaphthelene[9012-07A 2.7 U IL 1 2.7 10 9DO1013 EPA 8220E 04/02/1901:03 DFM
2,4,5-Trichlompherlol[95-95-4]1 2.5 U u9/L 1 2.5 30 9001013 EPA 8270E 09/02/1901:03 DFM
2,4,6-Tricblorophem1 E80-o6-2]A 47 meT 1 2.6 10 9Do1013 EPA 8270E 04104190103 DFM
2p-Dlchloapphenol[120-ill 15 ug/L 1, 2.6 10 9DO1013 EPA 8270E 04/02/190103 DFM
2,rDlmethylphenol[105-67-9]A 2.3 U ugh 1 2.3 10 9DO1013 EPA 8270E 04/02/1901'.03 DFM
2,4-Dirn[mphenol 151-285]A 2.6 U ugh 1 2.6 10 9DO1013 EPA 8279E 04/02/1901:03 DFM
2,4DiniVotoluene[121-14-2]A 2.6 U ug/L 1 2.6 10 9DO1013 EPA 8270E Call 01:03 OFM
2,6 Dinibotluene[606-20-2]A 2.5 U ug/L 1 2.5 10 9DOID13 EPA 8270E 09/02/1901:03 DEM
2 Chloronapinhalena[91-5B-7]A 2.8 U ug/L t 2.8 10 9DO1013 EPA 6270E 04102/1901:03 DFM
2-onloropheno1[95-57-0]A 3.4 3 ug/L 1 2.2 10 9DO1013 EPA 8270E 04/02/1901:03 OFM
2-M¢Uryl-0,6-dinitmphenal[534-52-1]A 3.3 U ug/L 1 3.3 10 9DO1013 EPA 8270E 04/02/1901:03 DFM
2-Methylnaphthalene[91-57-6]A 2,8 U til 1 2.8 10 9DDID13 EPA 8270E 04/02/19 01:03 DFM QV-01
2-Methylphdhol[95 48-7]A 2.0 U Ug/L 1 2.0 10 9DO1013 EPA 8270E 04/02/1901:03 DFM
2-Nltrcani8na[88-74-4]A 2.5 U u9/L I 2.5 10 9DO1013 EPA 8270E 09/02/190103 DFM
2-Nitrophenol[88-75-5]A 1.1 U ug,L 1 1.1 10 9DO1013 EPA 8270E Pal 0103 DFM
NNAL mannerism relates only tothe sample as,eseived by the Lboral and may only ce reprodyientoll. Page 5 of 11
wwvi.encolaba.com
ANALYTICAL RESULTS
Description: Wastewater Lab Sample IMCC05007-01 Recall 03/29/1915:00
Matrix: Waste Water Sampletl:03/29/19 10:15 Work Omer: CCO5007
Project: 103796 Sampled By:Steven Gerreld
Organic Compounds
Ana1Ne ]CA5Numbarl
3 8i-Methylphenal[108-394/106 945]^
3,T-Dichloraberophe[91-94-]]^
3 Nitmaniline[99 09-21^
4Boarell adyl-phenylether.[101-55-3]^
4-Chlom-3-methNphenol[5950-7]^
4{hl0manillne[06-47-B1A
4Chroophenyl-portylether[7005-72-3]^
4-Niboanilin,[100-01-6]A
4-NBmphenol[10 lal^
Acensphthene [83 32-911
Acenaphthylene[208-96-8]^
Arlthrecene[120-12-0]^
Ben2itline[92-87-5]^
Benm(a)anthracene[56 55-311
Benzo(a)pyrene[50-32-81A
Benzo(b)Barreadene[205-942]A
Benm(g,h,hperyare[191-24-2]1
Benm(k)euoranthene[207-08.9]^
Benzoic add[65-85-0]^
cannot alcohol[100.51-6]^
8iA2chlomsthmdy)mErpmA[111-91-1]1
Bis(2-chlamemypether [111444]^
Bls(2-chromiampre,a4eWer [108-60-171
Ble(2-etaylaexynPbthalats
117-8141ABadylbenzylphtha W[85-68-21^
Chrysene[218-01-9]^
Dlbenzo(ANanMramens[53-70-3]1
Dibendefoan[132-649]^
Diethylphthalate [84-66-27^
Dlmethylphablete[131-11-3]^
Di-a-butylphoorte[84 74-2]1
be naMlphthalate 1117-84011
Flmranthene[20644-0]^
Hundreds [86-73-7]^
Hessaderebenzene[118-74-1]A
Haxachnableatedline[87-581
Hexachandayclopenfatllens 177-42-4]1
HevachlorOeNane[67-72-1]^
Inheno(1,2,3-W)pyrene[193-39-5]^
Isophor0ne[7859-1]^
Naphthalene [91-20-3]A
Parmberaene[98-95-31^
N-NitrosOLimethylamine[62-05-91A
N Nitrom-bl-n-propylamine [621-647]1
N-nitrosWtphenylamine/Olphenylamine
86-30-6/122-39-4]^
PeniacMOmphearl[87-86-51A
RSanffi F9 Wits DIP MDL EQy Ea b Methutl Abafyed B Disks
2.1 a u9/L 1 2.1 10 9DO1013 EPA 8220E 04/D2/19 01:03 DFM
3.5 U dark 1 3.5 10 901013 EPA 8223E 04/02/19 01:03 DFM
2.6 D 111 1 2.6 10 9001013 EPA 8220E 04/021190103 DFM
2.4 0 ug/L 1 2.4 10 9DO1013 EPA 827CE 04/02/19 01:03 DFM
2.4 U ug/L 1 2.4 10 9DO1013 EPA 8220E 04/02]19 01:03 DFM
2.0 U ug/L 1 2.0 10 9MID13 EPA 8220E hall 01 03 DFM
2.6 U ug/L 1 2.6 10 9DO1013 EPA 8220E 04/021190103 DFM
3.2 U u9/L 1 3.2 10 9DO1013 EPA 8220E o4/02/19 01:03 DFM
2.8 U u9/1. 1 2.8 10 9DO1013 EPA 8270E 04/02/1901:03 DFM 2.
7 U u9/L 1 2.7 10 9MI013 EPA 8220E 04102/1901:03 DFM 2.
6 U uglL 1 2.6 10 9VO1013 EPA 8220E 04/02/19 01:03 DFM 2.
4 U ug/L 1 2.4 10 9DO1013 EPA 8270E 04/02/19 0103 DFM 1.
6 U ug/L 1 1.6 10 9DO1013 EPA 8270E 09/02/1901:03 DFM QV -al 2.
4 U ug/L 1 2.4 10 9001013 EPA 8270E 04/02/19 0103 DFM 2.
2 U ug/L 1 2.2 10 9DO1013 EPA 8270E 04/02/19 01:03 DFM 2.
8 U up/L 1 2.8 l0 9DO1013 EPA 8270E 04/02/19 0103 DEEM 2.
4 a ug/L 1 2.4 10 9DO1013 EPA 8220E 04/02/1901:03 DFM 2.
4 U ug/L 1 2.4 10 9MI013 EPA 8270E 04/04190103 DFM 1.
0 U ug/L 1 1.0 50 9DO1013 EPA 8220E 04/02/19 01:03 DFM 2.
4 U ug/L - 1 2.4 10 9DO1013 EPA 827CE 04/02/19 0103 DFM 2.
4 U deal 1 2.4 10 9DO1013 EPA 8270E 04/02/19 0103 DFM 2.
6 U u9/L 1 2.6 30 9MI013 EPA 8270E 04/02/19 01:03 DFM 2.
5 U dI 1 2.5 30 9DO1013 EPA 8270E 04/02/1901:03 OEM 9.
0 ug/L 1 1.9 5.0 9DO1013 EPA 8270E 04/02/19 01:03 DFM 3.
8 U ug/L 1 3.8 10 9DO1013 EPA 8270E 04/02/19 OL03 DFM 2.
2 U ug/L 1 2.2 10 9DO1013 EPA 8270E 04/02/190103 DFM 2.3
U u9/L 1 2.3 10 9DO1013 EPA 8270E 04/02/19 0103 DFM 2.6
U p9/L 1 2.6 10 9DO1013 EPA 8270E 04/02/19 01:03 DFM 2.4
U ug/L 1 2.4 10 9DOID13 EPA 8270E 04/02/19 0103 DFM 2.5
U al 1 2.5 10 9DO1013 EPA 8220E MJ02/1901:03 DFM 2.8
U ug/L 1 2.8 10 9DO1013 EPA 8220E 04/02/19 01:03 DFM 3.1
U ug/L 1 3.1 10 9DO1013 EPA 8220E 04/02/19 01:03 DFM 3.1
a ug/L 1 3.1 10 9001013 EPA 8270E 04/02/19 0193 DFM 2.5
U lot 1 2.5 10 9DO1013 EPA 8270E 04/02/19 0103 DFM 2.3
U u9/L 1 2.3 10 9DO1013 EPA 8270E a4/02/19 0103 DFM 2.8
U u9/L 1 2.8 10 9DO1013 EPA 8270E 04/02/19 01:03 11 QV-01 2.7
U ug/L 1 2.7 10 9DO1013 EPA 8270E 04/02/19 01:03 DFM QV-01 2.6
U M/L 1 2.6 10 9DO1013 EPA 8270E 04/02/19 01.03 DFM 2.2
U ugh 1 2.2 10 9DO1013 EPA 8220E 04/02/1901:03 DFM 2.5
U ug/L 1 2.5 10 9DOI EPA 8270E 0410103 DFM 2.8
U ug/L 1 2.8 10 9DO1013 EPA 8270E 04/02/19 01:03 DFM 2.5
U ug/L 1 2.5 10 9DO1013 EPA 8270E W/02/19)l DFM 1.9
U ug/L 1 1.9 10 9DO1013 EPA 8270E 09/02/19 0103 DFM 2.3
U ug/L 1 2.3 10 911 EPA 8270E 04/@/1901:03 DFM 2.5
U ug/L 1 2.5 10 9DO1013 EPA 8270E 04/02/19 0103 DFM 2.1
U u9/L 1 2.1 10 9DO1013 EPA 8270E 04/02/19 01:03 DFM FINAL Its
mPort Mates only to the sample as rttelven by he laWpen,, and may only be repmEuretl In 011. Page 1 o122
www.encolabs.com
ANALYTICAL RESULTS
Description: Wastewater Lab Sample ID: CCO5007-01 Received: 03/29/19 15:00
Matrix: Waste Water Sampled:03/29/19 10:15 Work Order: CC05007
Project: 103796 Sampled ey:5teven Gerald
GCMS
Analvre LOS NumherJ Results FIaa YAOM DF Mob POOL lotch Memand Anal etl B Nors,
Phellanhoone[85 01-8], 2.6 u u9/L 1 2.6 SO 9DO1013 EPA 8279E 04/02/19 01:03 DFM
Phenol 1108-95-2]1 1.7 0 ug/L 1 1.7 30 9DO1013 EPA 8270E 04/02/1901:03 DFM
Pyrene[129 00 Oil 3.5 D u9/L 1 3.5 10 9DO1013 EPA 8270E 04/02/19 0103 DFM
Pyridine [110-86-1]' 2.2 u ug/L 1 2.2 10 9DO1013 EPA 8270E 04/02/19 0103 DFM synneyeat.$
Ciy(6f DF Snike LN ygeL Nx (!m/fs 1 Aha(IIpQ Analaep BY Notes 2$
6-Tnbromopherrol 90 1 100 90 % I0.119 9MI013 EPA 8210E 04/02/190103 eFM z-
FiwroaPhenN 39 I 50.0 76 % 10-149 9MI013 EPA 8220E 04/0211901.'03 DFM 2-
puwophendl 51 I 100 51 % 1P110 9NIO13 EPA 8270E 04/02/1901,03 DFM Nrfrober
zened5 32 1 50.0 65% 16149 MOM EPA 8220E O4/02/1901.03 DFM PhenWJS
42 1 100 47% IOdB 9MO13 EPA 8220E 0410/190103 DFM 75eryhmy/
614 42 1 50.0 85% 19-10 9MI013 EPA 8220E 04/OL190103 DFM Classical
Chemistry Parameters enro
can amreaawrm trot s9r1 sedate
ICAS Numberl Results Else IL DS DF MDL POL 1 Method Analyzed B R¢t.. BiocM1emical
Oxygen comedy- 3.7 mg/L 1 2.0 2.0 900091 SM 5210 B-2011 0313011913:43 JOE Onemical
Ool barred' 11 not. 1 10 10 9DO2023 SM 5220D-2011 04/02/19 16:31 JOE Total
SuVarded Salida^ 2.5 u mg/L 1 2.5 2.5 9DO1009 SM 2540D-2011 04/04/19 12:45 ASC FINAL
This rent 21ah5 any to the sample a$ dlyyed by the laboratory( and may only be reeddu[M N NII. sage 1112
www.encolaba.com
ANALYTICAL RESULTS
Description: Sump Lab Sample I0:CC05OD7-02 Received: 03/29/1915:00
Matrix: Waste Water Sampled)O3/29/1910:30 Work Order: CC05007
Project: 103796 Sampled BV:Stewn Genald
Volatile Organic Compounds by GCMS
Anahete MASNumberl Results EM9 un"a DE MOL E" Baron Method AJy etl BY Ngtgg
1,1,1,2-Tdm,h1oroetbane[630-20-6]1 0.17 U ug/L 1 0.17 1.0 9D01040 EPA 8260D 04/02/3920:42 MRK
1,1,1-Tuichlorae8tane[71-55-6]A 0.12 U ug/L 1 0.12 1.0 900204E EPA 8260D 04/02/1920:42 MRK
1,1,2,2-Tetmm1.Pethane[79-345]1 0.28 U ug/L 1 0.28 1.0 9DO2040 EPA 8260D 0410211920'.42 MRK
1,1,2-Triahlouxthane[79-005]A 0.14 U ug/L 1 0.14 1.0 9D02090 EPA 8260D 04/02/1920:42 MRK
1,1-Di chlmoethane[Ad43]^ 0.13 U u9/L 1 0.13 1.0 9D02040 EPA B260D M/02/1920:42 MRK
1,1-DichlorOethene 175-35-41A 0.21 U u9/L I 0.21 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
1,1-Dichloropmpene 1563-58611 0.15 U u9/L 1 0.15 1.0 9D02040 EPA 8260D 04102/19 20 42 MRK
1,2,3-Trich1arabenzene[87-61-611 0.012 U u9/L 1 0.012 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
1,2,3-Trithlompmpane [96-184]^ 0.23 U u9/L 1 0.23 1.0 9002040 EPA 8260D D4/02/1920:42 MRK
1,2,4Trlchlorobenune[I20-82-1]A O.14 U ug/L t 0.14 1.0 9002040 EPA 8260D 04/02/1920:42 MRK
I,2,4Tbmethylbenzene[95-63-6]^ 0.10 U ug/L 1 0.10 1.0 9D02090 EPA 8260D 04/02/1920:42 MRK
1,2-Dibmmo-3-chlompmpane[96-12-8]A 0.48 U ug/L 1 0.48 1.0 9D02040 EPA 8260D 04/02/1920,42 MRK
1,2-Olbramoethene[306-934]1 0.66 U u9/L 1 0.66 1.0 9M2MO EPA 8260D W/02/1920:42 MIRK
1,2-Oich1oroben.ne[95-50 fl^ O.19 U ug/L 1 0.19 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
1,2-Dichlomethane[502-06-2]^ 0.21 U U9/L 1 0.21 LD 9DO2040 EPA 8260D 04/02/1920:42 MRK
1,2-Dichlompropane pe-87-SA 0.10 U ug/L 1 0.10 1.0 9D02040 EPA 8260D 04/02/1920'42 MRK
1,3,5-Trimethylbenzene[108E7-8]A 0.30 U ug/L t 0.30 1.0 900204E EPA 8260D M/02/1920:42 MRK
l,3-0ICMoroben2ene[541-23-1]^ 0.15 U ug/L 1 0.15 1.0 9D020Q EPA 8260D 04/02/1920:42 MRK
1,3-DichlomprOpane[142-28-9]^ 0.16 U ug/L 1 0.16 1.0 002040 EPA 8260E 04/02/1920:42 MRK
1,4Dlchlombeuzene[106-467]1 0.19 U ug/L 1 0.19 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
2,2-0Ich1oropmpane[594-20.7]A 0.28 U ug/L I 0.28 1.0 9D02040 EPA 8260D M/02/1920:42 MRK
2-Butanone[78-93-3]1 1.3 U ug/L 1 1.3 5.0 9D02040 EPA 8260D 04/02/1920:42 MRK
2-Chloraethyl Vinyl Ether [110-25-8]^ 1.1 U x/L 1 1.1 5.0 9D02040 EPA 8260D 04/02/1920:42 MRK
2-ChlorpWluene [95a9d]^ 0.081 U ug/L 1 0.081 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
2-H.urre1591-08-67A 0.88 a ug/L 1 0.88 5.0 9D02040 EPA 8260D 04/02/1920.42 MRK
4-CM1lomtoluene[106-43-4]^ 0.068 U ug/L 1 0.069 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
9-Ie0pmu,[Wluene[99d7-6]1 0.085 U ug/L 1 0.085 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
4-Methyl-2-pentenone[108-30-1]^ 1.1 U ug/L 1 1.1 5.0 9D02M0 EPA 8260D 04/0211920:42 MIRK
Acetone[57-6Y1]A 12 3 u9/L 1 30 20 9142040 EPA 8260D 04/0211920:42 MRK
Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9D02040 EPA 8260D 04/0271920:42 MRK
Bromobenzene[109-861]A 0.16 U ug/L 1 0.16 1.0 9D02040 EPA 82600 O4/92/1920:42 MRK
Bromochlommethane[74-9]-5]^ 0.48 U ug/L 1 0.48 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
Bromotlibhloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1A 9D0R040 EPA 8260D 04/02/1920A2 MRK
BmmotorM[75-25-2]^ 0.22 U ug/L 1 0.22 LD 9D02040 EPA 8260D W/02/1920:42 MRK
Bmmomethane[24d3-9]^ 0,14 U ug/L 1 0.14 1.0 9DD20,10 EPA 8260D 04/ll2/1920:42 MRK
Carbon dlsdflde[25-15-0]^ 1.5 U ug/L 1 1.5 5.0 91D0MD EPA 8260D 04/02/1920:42 MRK
Carbon tetraehloritle[56-23-5]^ 0.17 U u9/L 1 0.17 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
Chlmabenzene(108-90-2]^ 0.17 U ug/L 1 0.17 1.0 9D0200 EPA 8260D 04/02/1920'.42 MRK
Chloroe[hane[75-90-3]A 0.23 U ug/L 1 0.23 1.0 9DD2040 EPA 8260D 04/92/1920:42 MRK
Chlorotorm[67-663]^ 0.18 U ug/L 1 0.18 1.0 9D0204D EPA 8260E MJ02/1920:42 MRK
CHloromathane[74b7-3]A 0.13 U ug/L 1 0.13 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
tls1,2-0I[hl0methene[156-59-2]1 0.15 U ug/L 1 0.15 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK
c1e-1,3-Dich1ompmpene[10061-01-5]A 0.20 U ug/L 1 0.20 1.0 9D02040 EPA 8260D D4/02/1920:42 MRK Dibmmo:hbmmerhane[
124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK Dlbromomethane[74A5-
3]^ 0.27 U ug/L 1 0.27 1.0 9002W0 EPA 8260D 04/02/1920:42 MRK OichlomtlifluommMhane[75-
71-8]^ 0.20 U ug/L 1 0.20 1.0 9D02040 EPA 8260D 04/02/1920:42 MRK Ethylbenzene[100-
01-4]^ O.13 U ug/L 1 0.13 1.0 9DD2040 EPA 0260D D4/02/1920'.42 MRK FlNAL ThIS
ro[he Sampleasp.. EV ma labwarory, ann may only be repmLucM,n all. Page 8112
vrvrW.encolabs.cem
ANALYTICAL RESULTS
Description: Sump Lab Sample ID:0005007-02 Received: 03/29/1915:00
Matrix: Waste Water Sampled: 03/29/1910:30 Work Order: CCO5007
Project: 103796 Sampled By:Steven Gapped
Compounds by GCMS
Annemarie ICASNumberl Results Elan Dnitl OF Not POL 9 hh Method Aral, AB Notgg
HeAchlorobuta0leme[8768-3]^ 0.22 U ug/L 1 0.22 1.0 9DO2040 EPA 3260D 04/02/19 20:42 MRK
Isopmpolpsrsene[98-82-8]^ 0.14 U ug/L I 0.14 1.0 900204o EPA 8260D 04/02/19 20:42 MRK
mp-Xylenec[108-38-3/10642-3]^ 0.17 U u9/L 1 0.17 2.0 9DO20Q EPA 8260D 04/02/19 20:42 MRK
Merhylenechlorids[75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9D02040 EPA 8260D 04/02/19 20:42 MRK
Metmryl-@R-Butyl ENer[1634044]^ 0.16 U ug/L 1 0.16 lA 9002040 EPA 8260D 04/02/19 20:42 MRK
NapM1thelene[91-20-3]^ 0.11 U ug/L 1 0.11 1.0 9D020,10 EPA 9260D 04/02/19 20:42 MRK
n-Butyl Benzene[104-51-8]^ 0.058 U ug/L 1 0.058 LD 9DO2040 EPA 8260D o4/02/19 20:42 MRK
n-Propyl demesne [103 65-1]1 0.12 U ug/L 1 0.12 1.0 9DO2040 EPA 8260D 04/02/19 20:42 MRK
Xy]ene[95-4I-6]A 0.065 U ug/L I 0.065 1.0 902040 EPA 8260D 04/02/1920:42 MRK
sec-Butylbarsene[135-98-Sr 0.10 U ug/L 1 0.10 1.0 9002040 EPA 8260D 04/02/19 S)A2 MRK
Styrene []09-02-5]^ 0.11 U ug/L 1 0.11 1.0 9DO2040 EPA 8260D 04/02/19 20:42 MRK
ten-Butylbenzene[98-06-Ely 0.17 U ug/L 1 0.17 1.0 9D02040 EPA 8260D 04/02/19 20:42 MRK
Tetrxhloroethene[122-18-4]A 0.17 U ug/L 1 0.17 1.0 9DO2040 EPA 8260D 04/02/19 20:42 MRK
Toluene[10888-31A 0.14 U u9/L 1 0.14 1.0 91)02040 EPA 8260D 04J02/1920:42 MRK
vans-1,2-oicMornothene[156-60-5]1 0.21 U ug/L 1 0.21 LC 9DD20Q EPA 82600 04/02/19 20.42 MRK
trant-1,3-1)icM1lompropene[10061-02-6]1 0,15 U ug/L 1 0.15 1.0 9DO2040 EPA 8260D 04/02/19 20:42 MRK
TrichlorceMene[29-01-6]A 0.15 U ug/L I 0.15 1.0 91FUND EPA 8260D 04/02/19 20:42 MRK
Tn[M1lomflurnmandane[25-694]A 0.24 U ug/L 1 0.24 1.0 9DO20,10 EPA 8260D 04/02/1920:42 MRK
Vinyl oulorlJe[25-014]A 0.32 U ug/L 1 0.32 1.0 9DO2040 EPA 8260D 04/02/19 20:42 MRK
Xylenes QMal)[1330-20-2]A 045 U ug/L 1 0.45 3.0 9DO2040 EPA 8260D FSSS19 20:42 MRK
Sh.hurs, Re(s r/}' Pe opo Lsoof pq@9 Rec(imib Ral Mf-[hyQ gpa(ygof f{gtge
4-eromoAinmbenzene 54 1 50.0 LOB % 53-136 9001040 EPA 8260D 0 10L1920.42 MRK
0/Mwno9uoraneMax 49 1 50.0 96% 67-129 9S?M EPA 8260D 6,FVW1920.42 MRK
To/udM-08 50 1 5SO 100 % 59134 9WE2 EPA 8260D 0102/192042 MRK
Semivolatile Organic Compounds by GCMS
crvcD ary nmAeJanaly[e(A'C sse]
Anoints ICAS Numberl Results Fla. Matt, a Not Q Hatch Method AR;IVZnd a NNow$
1,2,4-TricMombenrene[120-82-1]1 2.5 U ug/L 1 2.5 10 9DO1013 EPA 8270E 04/02/19 01:33 mal
1,2-DlchlorobnF.ne[95-50-t]A 25 U ug/L 1 2.5 10 9DO1013 EPA 8270E 04/02/1901:33 DFM 1,
3-Djohlorobenzene[541-73-1]A 2.5 U ug/L 1 2.5 10 9DO1013 EPA 8220E 04/02/19 01:33 DFM 1,
4-Dilulorobennene[106-469]A 2.4 U ug/L 1 2.4 30 9DO1013 EPA 8270E 04/02/19 01:33 DFM 1-
McMylnaphthelene[90 12-CIA 2.7 U ug/L 1 2.7 10 90D1013 EPA 8270E 04/02/19 0133 DFM 2,
4,5-TricMoraphenol[95-95-4]1 2.5 U ug/L 1 2.5 10 9DO1013 EPA 0270E M/02/190133 DFM 2,
4,6-Thrul.opherml[SS06-2]A 2.6 U ug/L 1 2.6 10 9DO1013 EPA 8270E 04/02/1901:33 DFM A, Dichlomphenol[
120-93-2]A 2.6 U ug/L 1 2.6 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM 2,4-
Dimstmelphenol[105-67-9]1 2.3 U ug/L I 2.3 10 9DO1013 EPA 8220E 04/02/19 01:33 DFM 2,4Dlnibophenol[
51-28 5]A 2.6 U ug/L 1 2.6 10 9DO1013 EPA 8270E M102119 01,33 DFM 2,4-
0initmt0luene[121-14-2]A 2.6 U ug/L 1 2.6 10 9DO1013 EPA 827DE 04/02/19 DP33 DFM 2,6-
Dlnikotoluene[606-20-2]1 2.5 U ug/L 1 2.5 10 9DO1013 EPA 0220E 04/02/19 01:33 DFM 2-Chicemsphthakne191-
58-71^ 2.8 U ug/L 1 2.8 10 9DD1013 EPA 8270E 04102/190133 DFM 2-CM1lorapheml[
95-52-B]^ 2.2 U ug/L 1 2.2 l0 9DO1013 EPA 8220E 04/02/19 01:33 DFM 2-Methyl-
1,6-elnitmphenal[534-52-Ito 33 U ug/L 1 3.3 10 9DO1013 EPA 8270E M/02/19 01:33 DFM 2-Methy1napMhalene[
91-57-6]1 2.8 U ug/L 1 2.8 10 9DO1013 EPA 8270E 04/02219 01:33 DFM QV-01 2-Memhylphena1[
95-48-2]A 2.0 a ug/L 1 2.0 10 9DO1013 EPA 8270E M102/1901:33 DFM 2-Nitrwn0ne[
88-74-0]A2.5 U Uyll 1 2.5 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM 2-Ninophenol[
8875-5]A 1.1 U ug/L 1 1.1 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM FINAL Lay
moon relso-nly to theaamPle as rxelval by the labmmory, and may only W repm0uceb In roll. Pape 9.1R
APR 2 4 m19Ap L
vmw.encolabs.rom
Description: Sump Received; 03/29/1915:00
Matrix: Waste Water Sampled:03/29119 10:30 Work Order: CC05007 IProject: 103796 Sampled By:Stenn Germid
Ana Me MAS Number]
3 & 4MeNylphenol [10&394/106 445]1
3,3-DI<hlaroincrodlne[91-94-1]^
3-Nltmenllln,[99 09-2]^
4-BromaphenyFphenyl,ther[101-55-3]A
4-CM1lam3-mMhylpherel EtE50l
4{hloroanlhme [106-47-8]^
4Erharaphenyl-phenylether[7005 723]A
4-Nlnoanlllne[10001-6]A
4-Nlhophenol[1l 7JA
Acenaphtltene[83-32-9]A
Acenaphthylene[208-96-8]^
Anthracene[120-12-7]A
Benzidine[92-87-5]A
Benotyp anthlatene[56-55-3]A
Benm(a)pyrene [50-32-8]A
Benro(b)flusnothene[205-99-2]A
Benza(9AAperylene[191-24-2]^
henzo(k)fluensthhne[207-OB-9]^
demote Art [65-850]A
E l all [100-51-6)A
Bis(2<MoroMhwy)melfane
Ble(2-ChloroMhyl)Mher[111-44411
Bis(2-CHloralsopropypether(1o8fi0-1]A
Blc(2-ethylNeryl)p1dlhall
1ll-81-y]A
Burylberizylphthalate[85 68-711
Chrysene[218-01-9]A
Dibenzo(a,h)andlracene[53-70-3]A
Dibercofuran[132-649]A
Dlethylphlhalate[E466-2]A
DlmMhylph[halate[131-11-3]A
Di-n-butylphthalabe[84 74-211
Di-n-oCTylph[halafE 1117-84-O]A
Fluaranthene (206 440]1
Flwrene [86-73-7]A
Hex hl.beruene[118-74-1]A
Hatacblorobutadiene[67-68-3]^
Herzchlorocydopentediene []7-47-4]^
HexallrbIdethane[67-72-t]A
1Meno(1,A3<d)Pyrene[193-39-5]A
Imphomne [28-59-1]A
Naphthalene[91-203]A
Nlhabenzene[98-95-3]A
N-1,11[rosadimethylamine[62-75-91^
N-Nihose-di-n-propylamine [621.647]1
N-nllrosadiphenylamine/Olphenylamine
86-30-6/122-39-4]A
Pentachlomphen0l[87-86-5]A
Fall Elm malls DF MIL Q Batch Method 9ppVyd n jhtes
2.1 U u9/L 1 2.1 10 9MID13 EPA 8270E 04/02/19 01:33 DFM
3.5 U u9/L 1 3.5 10 9DO1013 EPA 8220E 04/02/19 01:33 DFM
2.6 U u9/L I 2.6 ld 9D01013 EPA 8220E 04/02/19 01:33 DFM
2.4 U u9/L 1 2.4 10 9DO1013 EPA 8270E 04/02/1901:33 DFM
2.4 U u9/L 1 2.4 10 9DO1013 EPA 8220E 04/02/19 OL33 DFM
2.0 U ug/L 1 2.0 10 9DO1013 EPA 8270E 0410211901:33 DFM
2.6 U ug/L 1 2.6 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM
3.2 U ug/L 1 3.2 IO 9DO1013 EPA 8270E M/02/1901:33 DFM
2.8 U ug/L 1 2.8 10 9MI013 EPA 8270E 04/041901:33 DFM
2.7 U ug/L 1 2.7 30 9DO1013 EPA 8210E 04/02/19 0133 DFM
2.6 U u9IL I 2.6 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM
2.4 U u9/L 1 2.4 IC 9DDI%3 EPA 8270E 04/02/19 01:33 DFM
1.6 U Ug/L 1 1.6 10 9DO1013 EPA 8210E M/02/1901:33 DFM QV-01
2.4 U ug/L 1 2.4 30 9DO1013 EPA 8270E M/02/190133 DFM
2.2 U ug/L 1 2.2 30 9DO1013 EPA 8210E W/02/19 0133 DEN
2.8 U til 1 2.8 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM
2.4 U u9/L 1 2.4 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM
2.4 U ug/L 1 2.4 10 9001013 EPA 8270E M/02/1901:33 DFM
1.0 U u9IL 1 1.0 50 9DO1013 EPA 8270E 04/02/19 01:33 DFM
2.4 U ug/L 1 2.4 10 9DO1013 EPA 8270E p4/02/19 0133 DFM
2.4 U Ug/L 1 2.4 10 9DO1013 EPA 8270E 04/02/19 0133 DFM
2.6 U u9/L 1 2.6 10 9DO1013 EPA 8270E 04/02/19 0133 DFM
2.5 U ug/L 1 2.5 10 9DO1013 EPA 8270E Col l9 0133 DFM
4.5 3 u9IL 1 1.9 5.0 9DO1013 EPA 8270E 04/02/19 0133 UFM
3.8 U ug/L 1 3.8 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM
2.2 U ug/L 1 2.2 30 9DO1013 EPA 8270E 04/02/19 01,33 DFM
2.3 U u9IL 1 2.3 10 9DO1013 EPA 8270E 04/02/19 0133 DFM
2.6 U u9IL I 2.6 10 9DO1013 EPA 8270E M/02/19 0133 DFM
2.4 U ug/L 1 2.4 10 9DO1013 EPA 8270E 09/02/19 0133 OEM
2.5 U ug/L 1 2.5 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM
2.8 U ug/L 1 2.8 10 9DOID13 EPA 8270E 04/02/19 01:33 DFM
3.1 U u9/L 1 3.1 30 9DO1013 EPA 8270E 04/02/19 OL33 DFM
3.1 U ug/L 1 3.1 10 9DO1013 EPA 8270E M/02/19 01:33 DFM
2,5 U Ug/L 1 2.5 10 9DO1013 EPA 8210E M/02/19 0133 DFM
2.3 U u9/L 1 2.3 10 9DO1013 EPA 8270E 04/02/19 0133 DFM
2.8 U ug/L I 2.8 10 9DO1013 EPA 8270E W/02/190133 DFM QV -al
2.7 U u9/L 1 2.7 IO 9DO1013 EPA 827DE 04/02/19 01:33 OEM QV-01 -
2.6 U ug/L 1 2.6 10 9DO1013 EPA 9270E M/02/19 01:33 DFM
2.2 U upL 1 2.2 10 9DOI013 EPA 8270E hall 01:33 DFM
2.5 U ug/L 1 2.5 10 9DO1013 EPA 8270E M/02/19 01:33 DFM
2.8 U u9IL 1 2.8 10 9DO1013 EPA 8270E 04/02/19 0133 DFM
2.5 U ug/L 1 2.5 10 9DO1013 EPA 0220E 04/02/19 01'.33 DFM
1.9 U ug/L 1 1.9 10 9DO1013 EPA 8270E 04/02/19 0133 DFM
2.3 U ug/L 1 2.3 10 9DO1013 EPA 8270E 04/02/19 0133 DFM
2.5 U ug/L I 2.5 10 9DO1013 EPA 8270E 04/02/19 0133 DFM
2.1 U ug/L 1 2.1 10 9DO1013 EPA 8270E 04/02/19 01:33 DFM
FlNAL Thla repot relates only to the temple ad reamed by the laboratory, and may only be reprWucN in Nil. Pate to of 22
wwvi.encolabs.com
ANALYTICAL RESULTS
Description: Sump Lab Sample lD:0005007-02 Received: 03/29/1915:00
Matrix: Waste Water Sampled; 03/29/1910:30 Work Order: CCO5007
Project: 103796 Sampled By:Steven Gerreld
Semivolatue Organic Compounds by GCMS
Ansiste FCASDumherl Itesulls Eia Lot DF MIDL EI Batch Method. Abandoned By holes
Phounnthrene[8501-83^ 2.6 U ug/L 1 2.6 l0 9D01013 EPA 8270E 04104190133 DFM
Phend[108-95-27^ 1.7 U ug/L 1 13 10 9DO1013 EPA 8270E 04/02/190133 DFM
there[329-00<- 3.5 U uvi- 1 3.5 10 9DO1013 EPA 8270E 04/@/190133 DFM
PIT dine [110-86-1]A 2.2 U ug/L 1 2.2 10 9MI013 EPA 8270E 04/0211901:33 DFM
8exr/(s OF 75kse LW s deRess, Be((ff MBCBPg 90d(gCd adds.
4,6-TnOromophend 96 1 100 96% 10-179 M1013 EPA 8270E 04/0L1901.33 DFM
2-Fl.,volshesty/ 35 1 500 69% 10149 9001013 EPA 8270E 04/07/1901,3 DFM
2-F/uWyeves./ 49 1 100 49% 10-110 9001013 FPA 8270E 04/02/190133 OM
N/frobenzenPdS 18 1 50.0 57% 10-149 9D01013 EPA 8270E 04/02/190133 OFN
PMde, 44 1 100 44% IG88 9001013 EPA 8270E 04/0L1901..33 DFM 7eryhenyFd14
44 1 50.0 00% 1P188 9001013 EPA 8270E Oei4y/1901.'33 OM Classical
Chemistry Parameters ENcoon
nne4aaameLNC s4L AnalvFe
PEAS numbed Factiltg Nd0 lJoila RE I_DL POL Batch Method a lded @y Not,f Biochemical
Oxygen Demand' 3.9 mg/L 1 2.0 2.0 9C30001 SM52103-2011 03130/1913:43 30C chemical
published Demand' 28 mg/L 1 10 10 91302023 SM 5220D-2011 04/02/1916: 31 30C Tons
Suspended Safid$A 2.5 U Tel 1 2.5 2.5 9D04009 SM 2540D-2011 04/04/1912:45 ASC Le"
J 1.1LrGnD APR
2 4 2019 - FINAL
This reaNnnates only A the ii at mreNM W the laboundo, and may only be,eomduwA In I Fate ll o1R
www.encolabs.mm
ANALYTICAL RESULTS
Description: Trip Blank Lab Sample ID:0005007-03 Received: 03/29/1915:00
Matrix: Water Sampled: 03/29/1910:15 Work Order: CCO5007
project 103796 Sampled By: ENCO
Volatile Organic Compounds by GCMS
Analvte ICASaumberl Reel lt¢ fw Units DF MIL pQy Inach Method Anshess, AM Nnre
1,1,3,2-TaAmsh1oroethyne[630-2P6]^ 0.17 U ug/L 1 0.12 1.0 9002040 EPA 8260D 04/02/192113 MRK
1,1,1-Trichloraethane[7155-6]^ 0.12 U u9/L 1 0.12 1.0 9DO2040 EPA 8260D 04/02/1921:13 MRK
1,1,2,2-Tetach1orcethane[79-34-5]^ 0.28 U ug/L 1 0.28 1.0 900204E EPA 8260D 04/02/1921:13 MRK
1,1,2-Trichloroethane[79-00-51A 0.14 U ug/L 1 0.14 1.0 9D0204D EPA 8260D 04/02/1921:13 MRK
1,1-Dichlemethone[75343]1 0.13 U ug/L 1 0.13 1.0 900204E EPA 8260D 04102/1921:13 MRK
1,1-D'ichlozaethudo [75-35-4]A 0.21 U ug/L 1 0.21 1.0 9DO2040 EPA 3260D D4/02/1921:13 MIRK
1,1-DiMlarapropene[563-58-6]A 0.15 U ug/L 1 0.15 1.0 9102040 EPA 8260D 04/02/1921:13 MRK
1,2,3-Trich1.m1a,.rc l87-61-67A 0.012 U ug/L 1 0.012 1.0 9DO2040 EPA 8260D 04/02/1921:13 MRK
1,2,3-Trichioropmpane[96-104]A • 0.23 U pg/L 1 0.23 1.0 9DO20C EPA 8260D 04/02/1921:13 MRK
1,2,4-Tnch1orobenzene[320-82-1]A 0.14 U del 1 0.14 1.0 9002040 EPA 82600 M/02/1921.13 MRK
1,2,4-Trimetbylbenune[95-63-6]A 0.10 U ug/L I 0.10 1.0 DD02M0 EPA 8260D M/D2/1921:13 MRK
1,2-Dlbmmo-3chbmpsmpane[96-12-B]A 0.48 U ug/L 1 0.4E 1.0 9D02040 EPA 8260D 04/02/1921:13 MRK
1,2-0Ibmmoethane[306-93-4]A 0.66 U ug/L 1 0.66 1.0 900204E EPA 8260D 04102119 21 13 MRK
1,2-0lcMombenzene[95-5U3]A 0.19 U u9IL 1 0.19 1.0 9DO2040 EPA 8260D 04/02/192113 MRK
1,2-Dichloroethane[307-06-2]1 0.21 U u9IL 1 0.21 1.0 9DD2040 EPA 8260D W/02/1921:13 MRK
1,2-DicM11.,,nbane[7&82-5]A 0.10 U PyL 1 0.10 1.0 9DO2040 EPA 8260D M/02/1921:13 MIRK
1,3,5-Trimenrylbenzene[108-674PA 0.30 U ug/L 1 0.30 1.0 9DD20W EPA 8260D 04/0211921:13 MRK
1,3-Dichlherobenzene[541-73-1]A 0.15 U ug/L 1 0.15 1.0 9D02040 EPA 8260D 04/02/192113 MRK
1,3-Dichlompmpane[142-28-9]A 0.16 U ug/L 1 0.16 1.0 9D02090 EPA 8260D N10211921,13 MRK
1,4D'ichiombenrene[106-46-271 0.19 U u9/L 1 0.19 1.0 9DO2040 EPA 8260D M/02/1921:13 MRK
2,2-DiCM1lomprop re,[594-20-2]A 0.28 U ug/L 1 0.28 1.0 9DO2040 EPA 8260D 04/02/1921:13 MRK
2-Butenone[78-93-3]A 1.3 U u9/L 1 1.3 5.0 9002040 EPA 8260D 04102/19 21 13 MRK
2-Chlmaethyl Vlnyl Ether[110-25-8]A 1.1 U ug/L 1 1.1 5.0 900209E EPA 8260D 04/02/1921:13 MRK
2-0iorotniuene 195-49-8]A 0.081 U ug/L 1 0.081 LO 9DO2040 EPA 8260D M/02/1921:13 MRK
2-H.none[591-28-6]A 0.88 U del 1 0.88 5.0 9D02040 EPA 8260D 09/02/1921:13 MRK
4{hlomtaluene[106-4,4JA 0.068 U ug/L 1 0.068 1.0 9W2040 EPA 8260D 04102/1921: 13 MRK
4-ISopmpyltaluene[99-87L1^ dent U ug/L 1 0.085 1.0 9D02040 EPA 8260D 04/02/192113 MRK
4Methyl-2-pentamne[106-10-1]A 1.1 U ug/L 1 1.1 5.0 90020E EPA 8260D 04/02/1921:13 MRK
AceMne[62-64-1]A 30 U ug/L 1 10 20 9DD2040 EPA 8260D 04/02/1921:13 MRK
Benzene [71-43-2]A 0.15 U u9IL 1 0.15 1.0 9DO2090 EPA 8260D M/02/1921:13 MRK
BrOmabenzene[108-86-1]A 0.16 U ug/L 1 0.16 1.0 9D02040 EPA 8260D 04/02/1921:13 MRK
Bromochloromethane p492-5]A 0.4E U ug/L 1 0.48 1.0 9D02040 EPA 8260D 04/02/1921:13 MRK
Bmmotlichlommeders[75-224r 0.12 U ug/L 1 0.17 1.0 9DO2040 EPA 8260D M/02/1921:13 MRK
BramOfazm[75-2S2]A 0.22 U ug/L 1 0.22 1.0 9DO2040 EPA 8260D 04/02/1921:13 MRK
Bromomethane[2403-9]A 0.14 U ug/L 1 0.14 1.0 9002W0 EPA SZ60D 04/041921:13 MRK
Carbon tlisulfide[75-15-CIA 1.5 U u9/L 1 1.5 5.0 9D02M0 EPA 8260D 04102119 21 13 MRK
Carbon hOrachlobde[56-23-5]A 0.12 U ug/L 1 0.12 1.0 9D02040 EPA 8260D M/02/192113 MRK
Chlmabenzene[100-90d]A 0.17 U ug/L 1 0.17 1.0 9DO2040 EPA 8260D 04/02/1921:13 MRK
ChloyeeMane[7500-3]A 0.23 U ug/L 1 0.23 1.0 9002040 EPA 8260D 04/02/1921:13 MRK
Chloroform 167-66-3]A 0.18 U ug/L 1 0.18 LO 002040 EPA 8260D 04/02/1921:13 MRK
Chloromethane [7482-3]A 0.13 U u9IL 1 0.13 1.0 9DOZM0 EPA 8260D 04/02/1921:13 MRK
cisl,2-Dichlaraethene[156-59-2]A 0.15 U ug/L 1 0.15 1.0 9DD2040 EPA 8260D M/02/1921:13 MRK
ds-1,3-DiCM1laraprOpene[30061-01-57A 0.20 U ug/L 1 0.20 1.0 9DD20M EPA 8260D 0,1/02/1921:13 MRK DlbromOchler.mohane[12448-1]A
0.17 U ug/L 1 0.17 LD 9D02040 EPA 8260D 04/02/1921:13 MRK Dlbromomethane [74A5-3]^ 0.22
U del 1 0.27 1.0 9DOl EPA 8260D 04/0/1921:13 MRK D¢M1loradl0uomme6ane p5-21-811
0.20 U ug/L 1 0.20 1.0 900204E EPA 8260D 04102/19 21 13 MRK ENylbenzens[10041-4]A 0.
13 U uyL 1 0.13 1.0 9DD2040 EPA 8260D 04/0211921:13 MRK r1NAL The rePorc relaMs mlytothe
sample as revived by the labarabery, and mayonly be rryraduced in All. 1111 of 21
orapha.encolabs.com
ANALYTICAL RESULTS
Description: Trip Blank Lab Sample lD:C005007-03 Received: 03/29/1915:00
Mai Water Si mpled:03/29/1910:15 Work Order. CCO5007
Project: 103796 Sampled By: ENM
Volatile Organic Compounds by GCMS
AnaMe I[AS Numbed Books Be. Unit[ ME ML PQL Bi Method gp31YSQ BB basal
theachlmdbumtliene[eb68-3]A 0.22 U ug/L 1 0.22 1.0 9002090 EPA 8260D W/02/1921:13 MRK
Imprapylbemene[98-82-87^ 0.14 U ug/L 1 0.14 1.0 9[ai EPA 8260D 04102/1921:13 MRK
mpXylanes[108-38-3/10642-3]A 0.12 U ri 1 0.1I 2.0 9002040 EPA 8260D 0410211921:13 MRK
Methylene chloride p5-09-21A 0.23 U ug/L I 0.23 1.0 9002040 EPA 8260D 04/02/1921L13 MRK
Methyl-Nrt-Butyl Ether[163404-4]^ 0.16 U hi 1 0.16 1.0 9D02040 EPA 8260D 04/02/1921: 13 MRK
Naphthalene [91-20-3]A 0.11 U ug/L 1 0.11 1.0 9D0204D EPA 826ED 04102/1921: 13 MRK
hi Bemmre[104-51-B]A 0.058 U ug/L 1 0.058 1.0 900209 EPA 8260D 04/02/1921:13 MRK
0-0mpyl Berseeme[10365-1]A 0.12 U hei- 1 0.12 1.0 91)02040 EPA 8260D 04/02/1921: 13 MRK
o-Xyleme[95-42-6]A 0.065 U u9/L 1 0.065 1.0 91 EPA 8260D 04/02/1921: 13 MRK
SeCButylbenzene[I35A8-81A 0.10 U u9/L 1 0.10 1.0 9DO204D EPA 8260D 04102/1921: 13 MRK
Styrene[100-02-51^ 0.11 U u9/L 1 0.11 1.0 9DO20Q EPA 8260D 04102/192113 MRK
tart-Butylbenune[98-0b61A 0.17 U ug/L 1 0.17 1.0 9DO2040 EPA 8260D 04/02/1921:13 ARK
Tehachl0methene[127-18-4]A 0.12 U ug/L 1 0.17 1.0 9Di EPA 8260D M/02/1921: 13 MRK
TPluene(108-88-3]A 0.14 U hi 1 0.14 LO 9DO2040 EPA 8260D 04/W/1921: 13 MRK
transl,2-Dichlomethene[15660-5]A 0.21 U ug/L I 0.21 1.0 9D02040 EPA 8260D 04102/1921: 13 MRK
here -1,3-Mchlompropene[10061-Pd-6]A 0.15 U hi 1 0.15 1.0 9D02040 EPA 8260D 04/02/1921:13 MRK
Tnchlomethene[29-0161 0.15 U Ali 1 0.15 1.0 9DD2040 EPA 8260D 04/02/1921: 13 MRK
Trichlomfluommethane(75-69-0]^ 0.24 U u9/L 1 0.24 1.0 9D02040 EPA 826ED 04/02/1921:13 MRK
Vinyl chloride[7501-4]A 0.32 U u9/L I 0.32 1.0 9MZ040 EPA 826ED 04102/1921:13 MRK
Xylenes(Teri [1330-20-]]A OAS U ug/L 1 0.45 3.0 9002NO EPA 8260D M/02/1921:13 MRK
FY2tdlee, gagd(r F 5S r R_A As Fec Limih Mbo Mph[ And Bye NOW
4-/Imrno{/rpiobeuex 53 1 50.0 105A 53-136 9002MO EPA 82600 04/02/I921.'13 MRK
Olbrom09u0rnmethax 49 I 50.0 by' Sy 67-129 9001040 EPA 8260D 04/02/1921:13 MRK
To/uene-00 51 1 500 101 % 53134 9D02040 EPA 8260D 0IW1921.13 MRK
P., This report relates onlytothe sample as husband W the la threat,, and may only be repmi In Nil. vage t3 at"
uco
www.encolebs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Bath 9DO2O4O-EPA 503OL M5
Blank(9002040-6LK1) Prepared 04/O RDS 15:42 Analyrea: 04/02/2019 18:04
Anal Rte Result Raga, IFFIN. u" fo
1,1,1,2-Tet2Cllayethane 0.17 U 1.0 ug/L
1,I,1-Trichioroethane 0.12 U 1.0 ug/L
1,1,2,2-Tetrachl0roethane 0.28 U 1.0 ug/L
1,1,2-Trl<hloroethane N14 U 1.0 ug/L
1,1-Dlchlomethans 0.13 U 1.0 ug/L
1,1-Mchloreethen, 0.21 U 1.0 ug/L
1,1-DicM1bmpmpene 0.15 U 1.0 ug/L
1,2,3-TricM1lombenune 0.012 U 1.0 ug/L
b2,3-Trich1oropr0pane 0.23 U 1.0 ug/L
1,2,4-Tricb1o.1,enaene 0.14 U 1.0 ug/L
1,2,arTrimethylbenzene 0.10 U 1.0 ug/L
1,2-Dibromo-3-chlympmpane 0.48 U LO ug/L
1,2-Dlbromoetbane 0.66 U 1.0 ug/L
1,2-Dichlorobenaene 0.19 U 1.0 ug/L
1,2-Dichlom ra 0.21 U 1.0 ug/L
1,2-Dikhlor0pr0pane 0.10 U I.0 ug/L
1,3,5-Ttimethyfler¢ene 0.30 U 1.0 ug/L
1,3-Dichlorobenttne 0.15 a 1.0 ug/L
1,3-Dichloropmpane 0.16 U 1.0 ug/L
Ib4DIch1ombenzens 0.19 U LO ug/L
2,2-Dlchbm,ropane 0.28 U 1.0 ug/L
2-Bufanone 1.3 U 5.0 ug/L
2-Chlomethyl Vinyl Ether 1.1 U 5.0 ug/L
2-CFloratoluene 0.081 U 1.0 ug/L
2-Hexanone 0.88 U 5.0 ug/L
4-Chlombdrene 0.068 U 1.0 ug/L
4-Impropyltoluene 0.085 U 1.0 ug/L
4kMeMy1-2-pentanone 1.1 U 5.0 ug/L
Acetone 10 U 20 ug/L
Benzene 0.15 U 1.0 ug/L
Bmmobenzene 0.16 U 1.0 ug/L
BromochlommathErs 0.4a U 1.0 ug/L
Bromoblchloromethane 0.17 U 1.0 ug/L
Bromaform 0.22 U 1.0 ug/L
Bmmoma[hane 0.14 U 1.0 ug/L
Carbon dgulFltle 1.5 U 5.0 ug/L
Carbon tetraghlontle 0.32 U 1.0 ug/L
Chlomben2ene 0.12 U 1.0 ug/L
Chlomethane 0.23 U 1.0 ug/L
Chloroform 0.18 U 1.0 ug/L
Chloromethane 0.13 U 1.0 ug/L
cis-1,2-Dichloraethen, 0.15 U 1.0 ug/L
cis1,3-Dkhlorepmpene 0.20 U 1.0 ug/L
Dlbromochlorome0lane 0.12 U 1.0 ug/L
Dibmmomethane 0.22 U 1.0 ug/L
DahlorollOuoromelhane 0.20 U 1.0 ug/L
Ethylbenzare 0.13 U 1.0 ug/L
Hexachlombutablene 0.22 U 1.0 ug/L
hoprapylbenune 0.14 U 1.0 uu/L
Spike Sources WeREC
Level Result %REC I.I.He RPD RPDLimit ague,
FINAL his report reletee Mly to the eample aS heelved by the labarueL, end may only be repreaucerf In hell. Pape 14 of 22
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QUALITY CONTROL DATA
VDlatlle Organic Compounds by GCMS - Quality Control
Batch 9001040-EPA 5030E MS -Continued
Blank (SD02040-BLK1)CanOnuetl Prepa2tl: 04/02/2019 15:42 Malyzcd: M/02/2019 18:04
Spike Saurte el RPD
9oR1Yd0 Batch Flap P0. u" u Level Reach[ % REC 1-1106£ Ron YMR Nobel -
m,p-Xylsne5 0.12 U 2.0 Ug/L
Methylene chloride 0.23 U 1.0 ug/L
Methyl-tert-Butyl Ether 0.16 U 1.0 thl
Naphthalene 0.11 U 1.0 hi
n-Butyl Benzene 0.058 U 1.0 ug/L
n-ph lBenzene 0.12 U LO ug/L
o-Xylene 0.065 U 1.0 ug/L
ses-Butylberuene 0.10 U 1.0 ug/L
Stimming, 0.11 U 1.0 ug/L
tM-BnMbenzere 0.17 u 1.0 ug/L
TetracMoroethene 0.17 U 1.0 u9/L
Toluene 0.14 U 1.0 hi
trans-1,2-Dishimmothene 0.21 U 1.0 u9/L
trans-1,3-Dichlompropene 0.15 U 1.0 ug/L
TricMorocul 0.15 U 1.0 u9/L
TrichlomOUoromethane 0.24 U 1.0 ul
Vinyl chloride 0.32 U 1.0 hi
Xylenee(Total) 0.45 U 3.0 ug/L
4-8mmolluorobenzeru 55 ug/L 50.0 110 53-136
O/bromiveysom /nefbane 50 o9/4 50.0 101 61-129
ToloexJB 52 W/L 50.0 104 B-134
LCS (91020,10-1151) Prepared: 09/02/2019 15:42 Amilyze[L W/02/2019 15:57
Spike Source REC RPO
AnalVd0 Raise Fla. P9L unity Level Result %REC Larral RPD Limit N4d96-
1,1-MicMomethene 22 1.0 ug/L 20.0 112 25-133
Benzene 22 1.0 u9/L 20.0 ill 80-13l
Chloroberuene 20 1.0 u9/L 20.0 100 80420
Toluene 20 1.0 ug/L 20.0 100 71-120
Thmd.merhene 24 1.0 hi 20.0 119 24-120
4-Brumo9uombemene 53 c¢L Solo 10 53-136
OlGromaHuommefha/u 51 W/L 50.0 1" 67129
TOGK atlB 51 u9/L 50.0 102 59134
MaMZ Spike (91XV2040-M51) oral 04/02/2019 15:42 Agra 1 04/02/2019 16:29
Source: CC05281-02
Spike Source REC RPI)
BnS1Yi€ Real t Nap P01. 1WLa Level Ross REC L.mle RPID Unit RPSEE
1,1-Dlchlmoethene 24 1.0 hi 20.0 0.21 U 119 25-133
Beruene 23 1.0 u9/L 20.0 0.15 U 116 80-134
ChItrobelpene 21 1.0 ug/L 20.0 0.12 U 103 80-120
Toluene 20 1.0 ug/L 20.0 0.14 U 102 71-120
Tnd9omerheoe 26 1.0 111 20.0 0.15 U 129 7+120 QM-02
4-emmpNcaro15. 53 u9/2 Soto I06 53136
sodgy.Auammeybne 51 191L 50.0 101 67129 4
To/uenetlB 51 U91L 50.0 102 54134
FINPL This report mantes only rnthe sample as reaelvM by the laboratory, and may only ee rMmdhood In fins. Gage 15 Of
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Bath 9001040-EPA 50308 MS -Continued
Matrix Spike Dup(9D02040-MSDI) Prepared: M/02/2019 15:42 smalyze4: 04/02/2019 17'.00
Source: cc05281-02
Spike Source REC man
9nAIY10 Real Ens POL IlNLi Level all oral Lol RPD Llmll Names
1,1-MCManaetbene 23 1.0 u9/L 20.0 0.21 U 116 75-133 3 20
0enzene 24 1.0 ug/L 20.0 0.15 U 118 80134 1 17
Chlorobelaene 20 1.0 ugh 20.0 0.12 U 100 90-120 4 16
Toluene 21 1.0 ug/L 20.0 0.14 U 106 21-120 3 17
Trlchlomaethene 26 1.0 ug/L 20.0 0.15 U 130 24-120 0.3 22 QM -a]
4-8rompevapbenzane 54 L 50.0 108 53-136
OlbronMflWromethax 48 151L 50.0 96 67129
Toluene-08 52 WIL 500 104 5 134
Semivolatlle Organic Compounds by GCMS - Quality Control
BaKh 9DO1013 - EPA 3510C MS
Blank (9D03013-BLRI) prepared: 04/01/2019 11:33 Malyutl: 04/01/2019 16:M
Spike Source %REC RPD
Anal Real Nay P41 Leib Loyal Real ^/DREG Linni RPD k[MR None,
1,2,4-Trichlomobensne 2.5 U 10 ug/L
1,2-31chicrobenzene 2.5 U 10 ug/L
1,3-Mohlombenzene 2.5 U 30 ugh
1,4 Ducblembenune 2.4 U 10 u9/L
1-M¢Myindpbthalen, 2] U 10 ug/L
2,4,5-Tricllmophenal 2.5 U 10 ug/L
2,4,6-Trichlarophena1 2.6 U 30 ug/L
2,4Diehlorophenol 2.6 U 10 opl-
2,4-DimeRrylphenal 2.3 U l0 ug/L
2,4DIn sephenal 2.6 U 10 ug/L
2,4Dininata1vene 2.6 U 10 u9/L
2,6-Dmitookikere 2.5 U 10 ug/L
2-ChloronapilMaiene 2.8 U 10 ug/L
2-Chlemplia l 2.2 U 10 ug/L
2-Melhyl-4,6-0ini0rophenal 3.3 U 10 ug/L
2-Menyliephtubsone 2.8 U 10 ug/L QV -OS
2-Methylphenol 2.0 U 30 ug/L
2-Nitroaniliue 2.5 U 10 ug/L
2-Nitrophenol 1.1 U 10 It
3&4-Methylphenol 2.1 U 30 u9/L
3,3'-Dichlmabenzinme 3.5 U 10 ug/L
3-Nitmoanlllme 2.6 U 10 ug/L
48mmephenyl-phenylether 2.4 U m ug/L
4Chlama-3-methylphenal 2.4 U 10 ug/L
4CMoraaniline 2.0 U 10 It
4-Chirrophenyl-phenyleMer 2.6 U 10 ug/L
4-NlFroanilln, 3.2 U 10 ug/L
4Nibephemol 2.8 U 10 ug/L
ACenaphthene 2.7 U 10 ug/L
Acenaphuylene 2.6 U 30 ug/L
Andineene 2.4 U ID ug/L
Benzltme, 1.6 U 10 ug/L QV-01
Some(a)anthoseco, 2.4 U 10 ug/L
FINAL Thma report relates only lobe sample as racelval bythelaboratory, not may only be Rpropufetl in sill. Pal bi.121
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QUALITY CONTROL DATA
Semivolefile Organic Compounds by GCMS - Quality Control
Batch 9D01013-EPA 3510C MS -Continued
Blank (1)O01013-Ell Continued Prepare; 04/01/2019 11:33 Analyzed: 04/01/7019 I6:34
Spike Source REC RPD
Ane vte Steel flan pOl gnkE Level Result AREC turn" RPD Limit Notes
Benzo(a)pyrene 2.2 U 10 ug/L
eenzo(b)(luenothene 2.8 U l0 ug/L
Beresheh,i)penene 2.4 U 10 ml
Benao(k)fluoranthene 2.4 U 10 ug/L
Benzolt ode 1.0 U 50 ug/L
Beo,l alcohol 2.4 U 10 ug/L
Bb(2-chlomethory)methane 2.4 U t0 ug/L
Bis(2LMoroMhypemer 2.6 U Io ug/L
Bls(2-chioroimpropypelher 2.5 U 10 ug/L
Bis(2-ethylhexypphthelate 1.9 U 5.0 ug/L
Butylbenrylphthalate 3.8 U to u,L
chrysene 2.2 U 10 ml
Diumseon,h)anthecene 2.3 U 10 og/L
Dlbenzon.P 2.6 U to ug/L
Diethylphtleste 2.4 U 10 ug/L
Dimethylphtleate 2.5 U 10 ug/L
Di-a-butylpMhalate 2.8 U 10 ug/L
Di-n-waylphthalate 3.1 U to ugh
Fluoranthene 3.1 U 10 ug/L
I'll 2.5 U 10 ug/L
lopachlorobentene 2.3 U 10 ug/L
Ho,achlorobuledlene 2.8 U 10 ugh QV-01
Hexachlorogdopentsdlene 2.7 U 10 ug/L QV-b1
Heanchlorcethane 2.6 U l0 ug/L
Inmema(1,2,3-cd)pyrene 2.2 U 10 ug/L
Ieophorane 2.5 U 30 ug/L
Naphthalene 2.8 U 10 ug/L
Ninobereene 2.5 U 10 ml
N-NitrosWimethylamine, 1.9 U 10 ug/L
N-Nitroso-tlFn-poe,lamine 2.3 U 10 ug/L
N-nitrosMiphenylalnlne/Dlphenylamins, 2.5 U 10 ug/L
Pentochlorophenel 2.1 U 10 ug/L
PhementMene 2.6 U 10 ug/L
Phenol 1.7 U 10 ug/L
Pyrene 3.5 U 10 ug/L
F}vlmine 2.2 U 10 ug/L
2,4,6-Tnbromaphems 89 WIL 100 89 10-1]9
2-FlWrob nyl 38 WL 50.0 76 10-149
2-F/wmphenpl 46 w I00 4s 10110
Nitrobenzene 0e 32 Wlt 500 64 10149
Gh 1r536WILto361088
7erplenyl414 49 WA 50.0 98 10-188
Les (9001013.551) Prepare; 04/01/2019 11:33 Analyz N', 04/01/2019 12:04
Spike Spuren DREG RPD
AralVte kneels Ran POL 4ni4 Level Reault REC Und RPD LIMl note5-
1,2,4Trichlarabemene 37 10 ug/L 50.0 23 27-90
1,4-Dichlorobenzene 35 10 ugh Solo 69 23-84
2,4Dlninatoluene 45 10 ug/L 50.0 89 62-132
Fl NPL Ihls mpan rtlMes only to the sample as realvM by the labo2bry, and may only be mpromeea In Nll. Paget] efl2
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QUALITY CONTROL DATA
Semivalatile Organic Compounds by GCMS - Quality Control
Batch YD0IC13 - EPA 35101- Coatiousen
LCS (9)01013-1 51) Continued Perri 04/01/2019 1133 Analyse@ 04/01/2019 17:04
Spike Source Asi RPD
Anaete R..RR Flan not Um'ta Level Result REC Li Thus RPD Limit None
2{hlmephemol 35 10 mi 50.0 70 40-109
4Chlaro-3-mathylphenol 44 10 ug/L 50.0 82 58-121
4-Nitmphenol 30 30 ug/L 50.0 60 33-105
Acenaphthene 42 30 ug/L 50.0 83 39-125
N-NRroso-dl-n-propylamine 41 10 ug/L 50.0 83 41
PeMachlorophenol 46 10 ug/L 50.0 93 51-135
Phenol 22 10 sai 50.0 43 19-28
he 47 10 ug/L 50.0 95 4 132
2,4,6-Trvbro x,,h, l 92 WIL 100 97 10-119
2-Fluorodphenyl 43 191L 500 85 10149
2-Flabad / 47 WL 100 47 10110
Nif tAsh,en,d5 35 u9/L 50.0 69 10199
Phe ,5 36 191L 100 38 1088
7eyhmN'd14 45 WL 50.0 90 10138
Matrix Spike(9D03013-M51) Prepared: 04/01/2019 11:33 Analyret1: 04/01/201917:34
Source: CC045(ii
Spike Source REC RPD
Analv[e load Flag FIX Bahl Level Ransil[ REC Limits RPD Limit N9Le6-
1,2,4Trichlombenzene 36 10 ug/L 50.0 2.5 U 23 27-90
1,4Dich1orobem ane 35 10 ug/L 50.0 2.4 U 20 23-84
2,,-O nitmtoluene 42 10 Fi 50.0 2.6 U 85 62-132
2-Chlorophenol 35 10 Lg/L 50.0 2.2U 20 90109
4-Chime-3-methylphenel 42 10 Lg/L 50.0 2.4U 85 50-121
4-Nitrophenol 31 30 mi 50.0 2.8 U 61 33-105
Acenaphthene 42 10 m/L 50.0 2.2 U 83 34125
N-Nltrow-di-b-propyWmine 40 10 u9/L 50.0 2.3 U 81 48-126
Penlechlorophenol 40 1D Lg/L 50.0 2.1 U 9 51-135
Phenol 29 10 Lai 50.0 IJ U 58 1978
Pyrene 44 10 ug/L 50.0 3.5 U 87 44-137
2,4,6-Ti/5mmophena/ 93 WL 100 93 11
2-Flwmbi 42 u¢L 50.0 83 10149
Fla/ovbe0ol 51 WIN 100 51 10-110
Niaobemm e-d5 34 Alt 50.0 61 10-149
Phe/ro/-05 51 WIL 100 51 lOdO
Teryheny/-019 41 Ii 50.0 83 10188
Matrix Spike Dup (9001013-MSD1) Prepared: 04/01/2019 11:33 Analyeel 04/01/2019 18:04
Source: CC04569-08
Spike Source xiuc RPD
9aA1YfR Result Flag pull. LI lta Level Rego t AAREC Linalum RPO L1m11 N9W-
1,2,4-Tnehlorobenzene 38 10 uglL 50.0 2.5 U 25 2IA0 3 43
1,aDlchorobaZeOa 36 10 ug/L 50.0 2.4U IS 23,M 1 39
2,4-Dinitrotoluene 41 10 ug/L 50.0 2.6 U 82 62-132 3 17
2-Chlorophenal 36 10 Lg/L 50.0 2,2 U 22 40-109 3 22
4-Chloro-3-meihylphdool 41 10 Lg/L 50.0 2.4 U 02 58 121 3 22
4-NAraphenol 28 10 ug/L 50.0 2.8 U 55 33-105 11 22
Acenaphthene 43 10 ug/L 50.0 23 U 65 3A125 3 25
N-Mioaso-dir,mepylamix, 41 10 Lg/L 50.0 2.3 U 82 40-126 0.2 23
Pentachlorophenol 46 10 Lg/L 50.0 2.1 U 93 51-135 4 it
FINAL This report mass anlV to mi ample of salved by[he labehiss, and may only be reproduce N Nil. Page 18 o121 -
ENCO
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Balch 9DO1O13 -EPA 351OC MS-ConOnuetl
Matrix$Pike Due(9D010I3-M9D3) Continued Prepacat 04/01/201911:33 Analyzed 0110:04
Source: CC04569.08
Spike curt, REC RFD
Ami Resed Nan FQ_L 4nIL4 Level Result BREC Ll,t RFD Omit Notes
Phi29 10 ug/L 50.0 1.7U 58 19-78 0.3 IB
Pyrene 47 10 ug/L 50.0 3.5U 93 4 137 6 24
246-Tiicmmophmd 92 10 100 92 10 -IN
2-R bph ,4 45 WIL 50.0 89 10-149
2-Hdomphera/ 52 WIL 100 52 1Lh110
Nlhodenz mi 35 191 50.0 70 10-149
Phenold5 51 WIL 100 51 10-BB
Te phenNdl4 45 IWL 50.0 91 16188
Classical Chemistry parameters - Quality Control
Batch 900001-NO PREP
Blank (901 Prtpa d & AnaMetl', 031301201913:43
Spike Saamax %REC RFD
9n31Y1n R4flllS flan FIX LWM Level Result IAREC Lord RFD limit Rome
Blechemlral Oxygen Demand 2.0 U 2.0 mg/L
LCS (901 Prepared & Analyzed 03/30/201913:43
Spike Source %REC RFD
Prelims Basis Man poll. LIDIt9 Level Result -AREC Undle RFD LDDI[ None
Rechemical Oxygen Demand 210 2.0 nai 198 105 85-115
Duplicate (9C30001-DUPI) Prepared & AmPeac: 03/30/201913:43
Source: CCO3002-01
Spike Source %REC RFD
Anent Rame.1 M9 2 U.I. Level Result %REC Limit@ RFD yjmjt N,.s
Biochemical Cagan Demand 3.8 2.0 mg/L 3.7 3 30
Batch 9D01O23-Same
Blank (9002023-BLK3) Prepared 04/02/201913:50 AnalyzN: 09/@/201916:31
Spike Source %REC RFD
Paul 9ts Recut Man FDA. units Level Result %REC L.nite RFD Limit Not,
Chemical O gan Demand 10 U 10 mg/L
Les (gD02023-BSI) Prepared 04/02/201913:50 Analyzed 04102/201916:31 Spike Source %REC
Rp0 9D%ISR4 B9
MBR 246 Halts Level Result %REC Limits RFD Limit Room Chemical Oxygen Demand
480 10 mg/L 500 96 9N110 Matrix Spike (9D02023-
MS3) Prepared'. 04/02/201913:50 Analyzed 04/02/201916:31 Source: CC01621-01
Spike Source %REC
RFD Anaryte Be,,[ Mon
CDL Imuor Died Raoul t %REC Limits RFD 6Im11 Rates Chemical Oxygen Demand
680 10 mg/L 526 160 99 90-110 Matrix Spike Dup (
9D020231 Prepared: 04/02/201913:5D Analyred 04/02/201916:31 Source: CC01621-01
Spike Source °bREC
RFD AmoIVIa Racal[ Mon
29L Chits Level ReeylL V.REC Ll RFD L)ID11 NS9i FINAL 11i rePon
clax only M[he sampleac..I,. ey the lai Intl may only be rin a. In 111. o, mof 11
knoxa.encolalrs.com
QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Bath 9002023-Same -ConNnae0
Matrix Spike Dup(9D02023-MSD3)Continued Prepared:N/02/201913:50 AnalyleU: 04/0212019 16 31
Source: CCO1621-01
Spike Source -/eREC RPD
9pAlwal purot Firm PILL Ithlb, Level Result %REC Lt.[ RPD LImR IN ter_
Chemical Oxygen Demand 670 10 mg/L 526 160 96 90-110 2 10
Beth 9D0 W9 -NO PREP
Blank (9D04009-BLR3) Prepares & Analyted'. 04/N/201912:45
Spike Source riaREC RPD
An31Yt9 Road t NewC2 UOtiIF Level Result DeREC Lund g RPD Limit IN Wa
Total Suspended Solids 2.5 O 2.5 mg/L
LCS (9004001 Praparad &Analyse@ 04/04/201912:45
Spike Saurce WeREC RPD
Anal l'LC Beau[ NSfl P41 Smite Level Resu[ %aREC Unalla WIND Unlit Naten Total
Suspended Solids 100 2.5 mg/L 100 100 8U320 DupliW
W (9D04009-DUPS) Depend & Analyzed. 04104/201912:45 Source:
CC04s24-01 Spike
Source WeREC RPD Anal
Ke B48n1[ Nan P01, SlDltat, Level Result °/eREC L'm"b RPD Limit Name_ Total
Suspendetl Sol do 120 2.5 mg/L 160 4 20 Duplicate (
9004009-DUP2) Prepared &Analyzed C4/C4/201912:45 Source:
CC04359-01 Spike
Source °uREC RPD Amid
4 R43p15 flaA E2 llnita Level Result -/eREC Limits RPD Limit Not 1N
I Suspended Solids 230 2.5 m9/L 230 0 20 FlUPL
Thlo reprt relate only to me sample as moved by the [a seats, and may nnly be oproaurM In Nil. Psso to o112
ENCO
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDQ and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, In the case of soil samples, moisture content.
PQL PQL: Practical Quantitating Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85 % or greater
confidence) to make a -tentative identifcation".
P Greater than 25 %concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
CALC] Calculated analyte- MDL/MRL reported to the highest reporting limit of the component analyses.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QV-01 The associated continuing calibration verification standard exhibited high blas; since the result is ND, there
is no impact.
FINN. ielz not Meng on,.Ire sample es—,er,to Woe., and mw rely bi iniiIn 111. Page 21 of 22
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Sample Preservation Verification
ENCO Cary
Work Order: CCO5007 Project: 103796
Client: Leaf Environmental, Inc. (BE012) Project 103796
Logged In 29-Mar-19 15:00 Logged By: John C King
Preservation Check Performed By: Date/Time:
CCO5007-01
font Type Rres p); eulrementp ebke InCentro) ted' DateTme pHAdjus Ad,ustetl Reagent Used/Comments G
250mLP+H28O4 2 Y N / NA V / NA CCO5007-
02 Cont
I Type Rres eq (PH)a)nt p In Control PH Adjusted ` gtlryatede':, Reegeht Used/Comments G
250ml-P+112504 1 <2 J& / N / NA Y /W / NA Rea
ent Name ID 1
2
Reagent
Name ID 3
4
Reagent
Name ID 5
6
pH
Strip ID:Cc(, C:
IELMNT\Printlwko_PreservatlonCheck.rpt Page 1