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HomeMy WebLinkAboutWQ0001817_Monitoring (2) - 11-2020_20201221Monitoring Report Submittal ............................................................................................................................................ Permit Number #* WQ0001817 Name of Facility:* Albemarle Utility Company Month:* November Year:* 2020 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR November MR's.pdf 5.72MB PDF Only GW-59 November MW Reports.pdf 20.21 MB FLJF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* danny.perry@albemarleplantation.com Name of Submitter:* danny s perry Signature: Date of submittal: 12/21/2020 This will be filled in autocratically Initial Review Reviewer: Williams, Kendall Is the project number correct?* WQ0001817 Is the monitoring report Yes r No accepted?* Regional Office* Washington Accepted Date: 12/21/2020 SUBMIT FORM ON YELLOW PAPER ONLY , • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Comapany Non -Discharge W00001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island RD TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford N.0 27944 County Perqimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: North of Holding Lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -1 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 6.12 units Temp. 000lo: 17.9 °C DRY at Depth to Water Level 82546: 12.2 ft. below measuring point Screened Interval: -5 ft. to -20 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Turbid here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 ' / 2-C`s` a o,N 0 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 362 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 6.12 units Ba - Barium 01007 ug/L TOC 00680 4.4 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 17 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type Agent) LJ (Date) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY , • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Comapany Non -Discharge W00001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island RD TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford N.0 27944 County Perqimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: North of Holding Lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -1 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 6.12 units Temp. 000lo: 17.9 °C DRY at Depth to Water Level 82546: 12.2 ft. below measuring point Screened Interval: -5 ft. to -20 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Turbid here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 ' / 2-C`s` a o,N 0 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 362 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 6.12 units Ba - Barium 01007 ug/L TOC 00680 4.4 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 17 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type Agent) LJ (Date) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY , • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Comapany Non -Discharge W00001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island RD TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford N.0 27944 County Perqimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: North of Holding Lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -1 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 6.12 units Temp. 000lo: 17.9 °C DRY at Depth to Water Level 82546: 12.2 ft. below measuring point Screened Interval: -5 ft. to -20 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Turbid here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 ' / 2-C`s` a o,N 0 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 362 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 6.12 units Ba - Barium 01007 ug/L TOC 00680 4.4 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 17 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type Agent) LJ (Date) GW-59 Rev.06-07-2018 6envirochem ANALYTICAL $ CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmiil Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4,;."1 l 710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax 255-A Wilmington Highway Jacksonville, NC 28540 " 910.347.5843 Lab/> nx infoLenvironmentalchemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50364 Site: MW-1 11/19/2020 10:30 AM Water Jay Baker Test Method Results Date Analyzed Color cow Tan/Turbid 11/19/2020 Depth to water, ft. Depth to Water, Ft 12.2 feet 11/19/2020 Ammonia Nitrogen EPA350.1 <200pg/L 11/25/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2020 Odor Qualitative Slight Sulfur 11/19/2020 Total Dissolved Solids (TDS) SM 2540 C 362 mg/L 11 /20/2020 Temperature SM 2550 B 17.9 C 11/19/2020 Chloride SM 4500 Cl E 17 mg/L 11 /27/2020 pH SM 4500 H B 6.12 units 11/19/2020 Total Organic Carbon (TOC) sM 5310 B 4.4 mg/L 11/23/2020 1,1,1, 2-Tetrachloroethane SM 6200B <0.5 lag/L 11/25/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 lag/L 11/25/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/25/2020 1,1,2-Trichloroethane SM 62008 <0.5 lag/L 11/25/2020 1,1-Dich loroethane SM 62008 <0.5 lag/L 11/25/2020 1, 1 -Dichloroethene SM 62008 <0.5 lag/L 11/25/2020 1, 1 -Dichloropropene SM 6200B <0.5 lag/L 11/25/2020 1,2, 3-Trichlorobenzene SM 6200B <0.5 lag/L 11/25/2020 1,2,3-Trichloropropane SM 6200B <0.5 lag/L 11/25/2020 1,2,4-Trichlorobenzene SM 62008 <0.5 lag/L 11/25/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 lag/L 11/25/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/25/2020 1,2-Dibromoethane SM 6200B <0.5 lag/L 11/25/2020 1,2-Dichlorobenzene SM 6200B <0.5 lag/L 11/25/2020 1,2-Dichloroethane SM 6200E <0.5 lag/L 11/25/2020 1,2-Dichloropropane SM 6200E <0.5 lag/L 11/25/2020 Report *: 2020-19783 Page 1 of 30 SM ANALYTICAL & CONSULTING CHEMIST: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910,392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info @envirot) men talchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 05, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/25/2020 1,3-Dichlorobenzene SM 62008 <0.5 pg/L 11/25/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/25/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/25/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/25/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/25/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/25/2020 Benzene SM 6200B <0.5 pg/L 11/25/2020 Bromobenzene SM 6200B <0.5 pg/L 11/25/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/25/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/25/2020 B romoform SM 62008 <0.5 pg/L 11/25/2020 Bromomethane SM e2008 <0.5 pg/L 11/25/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/25/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/25/2020 Chloroethane SM 6200B <0.5 pg/L 11/25/2020 Chloroform SM 5200B <0.5 pg/L 11/25/2020 Chloromethane SM 6200B <0.5 pg/L 11/25/2020 cis- 1,2-Dichloroethene SM 62006 <0.5 pg/L '11/25/2020 cis- 1,3-Dichloropropene SM 8200B <0.5 pg/L 11/25/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/25/2020 Dibromomethane SM 62008 <0.5 pg/L 11/25/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/25/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/25/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/25/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/25/2020 M+P Xylene SM 6200B <1.0 pg/L 11/25/2020 Methylene chloride SM 6200B <0.5 pg/L 11/25/2020 Naphthalene SM 6200B <0.5 pg/L 11/25/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/25/2020 [?eport #:: 2020-19783 Page 2 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/i ax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemises.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM 6200B <0.5 µg/L 11/25/2020 ortho-Xylene SM 6200B <0.5 µg/L 11/25/2020 p-Isopropyltoluene SM 6200B <0.5 µg/L 11/25/2020 sec -Butyl benzene SM 6200B <0.5 µg/L 11/25/2020 Styrene SM 6200B <0.5 µg/L 11/25/2020 tert-Butyl benzene SM 6200E <0.5 µg/L 11/25/2020 Tetrachloroethene SM 6200B <0.5 µg/L 11/25/2020 Toluene SM 6200B <0.5 µg/L 11/25/2020 Trans-1,2-Dichloroethene SM 6200B <0.5µg/L 11/25/2020 Trans-1, 3-dichloropropene SM 6200B <0.5 µg/L 11/25/2020 Trichloroethene SM 62008 <0.5 µg/L 11/25/2020 Trichlorofluoromethane SM 62006 <0.5 µg/L 11/25/2020 Vinyl chloride SM 6200E <0.5 µg/L 11/25/2020 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 11/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 < 0.02 mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.03mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method 0.03 mg/L 12/05/2020 Report #, 2020-19783 Page 3 of ; SUBMIT FORM ON YELLOW PAPER ONLY ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC Pnnt Clearly or Type 27944 County Perquimans Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Well Location/Site Name: East of Baffle Lagoon No. of wells to be sampled: 10 LL ID NUMBER (from Permit): MW-2 Date sample collected: 11/19/2020 I Depth: 12 ft. Well Diameter: 2 in. tth to Water Level 82546: 3.6 ft. below measuring point Screened Interval: -2 ft. isuring Point is 3 ft. above land surface Relative M.P. Elevation: ime of water pumped/bailed before sampling: 4.0 gallons nples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified. ❑ YES DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 ERMIT Number: Expiration Date: 05-31-2025 on -Discharge WQ0001817 UIC PDES Other YPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: to -12 ft. ft. NO FIELD ANALYSES: pH 00400: 5.45 units Spec. Cond. 00094: Odor 00085: Sulfur Appearance Tan Temp. 0oolo:17•8 °C uMhos Date sample analyzed:11/19/2020 — / -pS -J.yc u Laboratory Name: Environment Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 51 colonies /100mL Nitrate (NO3) as N 00620 0.14 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 340 mg/L Al - Aluminum o1105 mg/L pH (Lab) 00403 5.45 units Ba - Barium 01007 ug/L TOC 00680 23.4 mg/L Ca - Calcium 00916 mg/L Chloride 00940 31 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 719oo ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VDUs: mg/L vut, Kemoval7o If WELL DRY at time of sampling, check here:❑ GW-59 Rev.06-07-2018 SR' ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott Lab ID Sample ID: 20-50365 Site: Mw-2 Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 F r: 710 13owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax infor environrnentak iieniists.com Date of Report: Dec 05, 2020 Customer PO #: 27944 Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) 1,1,1,2-Tetrachloroethane 1, 1, 1 -Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1, 1 -Dichloroethane 1, 1 -Dichloroethene 1, 1 -Dichloropropene 1, 2, 3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1, 2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane Collect Date/Time Matrix 11/19/2020 10:45 AM Water Method Color Depth to Water, Ft EPA 350.1 Gallons Bailed before sampling Qualitative SM 2540 C SM 2550 B SM 4500 CI E SM 4500 H B SM 5310 B SM 62008 SM 62008 SM 6200B SM 6200E SM 62008 SM 62008 SM 6200B SM 62008 SM 6200B SM 6200B SM 62008 SM 6200B SM 6200B SM 6200B SM 6200B SM 62008 Results Sampled by Jay Baker Date Analyzed Tan 11/19/2020 3.6 feet 11/19/2020 < 200pg/L 11/30/2020 4 (dry)gallons 11/19/2020 Sulfur 11 /19/2020 340mg/L 11/20/2020 17.8 C 11/19/2020 31 mg/L 11 /27/2020 5.45units 11/19/2020 23.4 mg/L 11/23/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 Report #:: 2020-19783 Page 4 of 30 pp"105' _. ""7 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 rix 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax ca 255-A Wilmington liignway, Jacksonville, NC 28540 • 910.347.5843 Lab/flax ANALYTICAL & CONSULTING CHEMISTS info teenvironmentalchemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/25/2020 1,3-Dichlorobenzene SM 6200E <0.5 pg/L 11/25/2020 1,3-Dichloropropane SM 62DOB <0.5 pg/L 11/25/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/25/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/25/2020 2-Ch lorotoluene SM 6200B <0.5 pg/L 11/25/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/25/2020 Benzene SM 6200B <0.5 pg/L 11/25/2020 Bromobenzene SM 6200B <0.5 pg/L 11/25/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/25/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/25/2020 Bromoform SM 62008 <0.5 pg/L 11/25/2020 Bromomethane SM 6200B <0.5 pg/L 11/25/2020 Carbon tetrachloride SM 62008 <0.5pg/L 11/25/2020 Chlorobenzene SM 62008 <0.5 pg/L 11/25/2020 Chloroethane SM 62008 <0.5 pg/L 11/25/2020 Chloroform SM 6200B <0.5 pg/L 11/25/2020 Chloromethane SM 6200B <0.5 pg/L 11/25/2020 cis- 1,2-Dichloroethene SM 6200B <0.5 pg/L 11/25/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 11/25/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/25/2020 Dibromomethane SM 6200B <0.5 pg/L 11/25/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/25/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/25/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/25/2020 Isopropylbenzene SM 62008 <0.5 pg/L 11/25/2020 M+P Xylene SM 62DOB <1.0 pg/L 11/25/2020 Methylene chloride SM 62000 <0.5 pg/L 11/25/2020 Naphthalene SM 8200B <0.5 pg/L 11/25/2020 n-Butylbenzene SM 62006 <0.5 pg/L 11/25/2020 Report #: 2020-19703 Page 5 of 30 r 4M ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott Environmental Chemists, Inc;. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab i 110.3142,442.1 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab , Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fa> info,ti environmentalchemists.com Date of Report: Dec 05, 2020 Customer PO #: 27944 Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM 6200B <0.5 Ng/L 11/25/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/25/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/25/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/25/2020 Styrene SM 6200B <0.5 pg/L 11/25/2020 tert-Butyl benzene SM 6200B <0.5 pg/L 11/25/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/25/2020 Toluene SM 6200B <0.5 pg/L 11/25/2020 Trans- l ,2-Dichloroethene SM 6200B <0.5 pg/L 11/25/2020 Trans- 1,3-dichloropropene SM 6200B <0.5►Jg/L 11/25/2020 Trichloroethene SM 6200B <0.5 pg/L 11/25/2020 Trichlorofluoromethane SM 6200B <0.5 fag/L 11125/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/25/2020 Fecal Coliform SM 9222D MF 51 Colonies/100mL 11/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 < 0.02mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.14 mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method 0.14 mg/L 12/05/2020 Reportk 2020-19783 Page 5o`:[KK� „�XA� SUBMIT FORM ON YELLOW PAPER ONLY . • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge W00001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans RK Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South East of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 3 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.05 units Temp. 000lo: 17.6 °C DRY at Depth to Water Level 82546: 3 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 3 gallons Appearance Tan/Turbid here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 — j� -ps -,���o Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 5600 colonies /100mL Nitrate (NO3) as N 00620 .024 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 1140 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 6.05 units Ba - Barium 01007 ug/L TOC 00680 21.2 mg/L Ca - Calcium 00916 mg/L Chloride 00940 19 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.374 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type ittee (ollAtfthorized Aqent) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab , 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 9 910.347.5843 Lab /Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 07, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-50366 Site: MW-3 11/19/2020 11:00 AM Water Jay Baker Test Method Results Date Analyzed Color color Tan/Turbid 11/19/2020 Depth to water, ft. Depth to water, Ft 7.1 feet 11/19/2020 Ammonia Nitrogen EPA 350.1 374 pg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 3 (dry) gallons 11/19/2020 Odor Qualitative None 11/19/2020 Total Dissolved Solids (TDS) SM 2540 C 1140 mg/L 11/20/2020 Temperature SM 2550 B 17.6 C 11/19/2020 Chloride SM 4500 Cl E 19 mg/L 11 /27/2020 pH SM 4500 H B 6.05 units 11/19/2020 Total Organic Carbon (TOC) SM 5310 B 21.2 mg/L 11/23/2020 1, 1, 1,2-Tetrach loroethane SM 6200B <0.5 pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11 /26/2020 1,1,2-Trichloroethane SM 8200E <0.5 pg/L 11/26/2020 1,1-Dich loroethane SM 5200B <0.5 pg/L 11/26/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 62008 <0.5 pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane sM8200B <0.5pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/26/2020 1,2-Dichiorobenzene SM 62008 <0.5 pg/L 11 /26/2020 1,2-Dichloroethane SM 5200B <0.5 pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 Report # 2020.19783 Page 7 of 30 F"7— Environmental Chemists, Inc. envirochem A 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab * 910.392.442-4 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 t ab, Fax ANALYTICAL & CONSULTING CHEMISTS info@environinentatcheniists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200E <0.5 pg/L 11/26/2020 1,3-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11 /26/2020 Benzene SM e200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM e200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 62008 <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 C hloroethane SM 6200B <0. 5 pg/L 11/26/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SM 6200B <0.5 pg/L 11/26/2020 cis- 1,2-Dichloroethene SM 6200B <0.5 pg/L 11/26/2020 cis-1, 3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM e200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 8200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM e200B <0.5 pg/L 11/26/2020 Report #:: 2020-19783 Page 8 of 30 �- envirochem ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 91.0.,347.5843 Lab /Fax in fo(a?envi rorimenta Ichem ists. coin Date of Report: Dec 05, 2020 Customer PO #: 27944 Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM 62008 <0.5 pg/L 11/26/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 62008 <0.5 pg/L 11/26/2020 sec -Butyl benzene SM 6200B <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-B utyl benzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/26/2020 Toluene SM 6200B 18.8 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans- 1,3-dichloropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/26/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/26/2020 Fecal Coliform SM 9222D MF 5600 Colon ies/100mL 11/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 0.02mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0,26mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method 0.24 mg/L 12/05/2020 Report #:: 2020-19783 Page 9 o` 3Q SUBMIT FORM ON YELLOW PAPER ONLY • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Pnnt Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County. Perquimans N Lagoon ❑ Remediation: Infiltration Gallery 0 Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South West of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 4 Date sample collected: 11 /19/2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.38 units Temp. 000lo. 18.2 °C DRY at Depth to Water Level e2546: 6.8 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 000sa: µMhos time ofsampling, 3 Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 4.0 gallons Appearance Tan/Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES NNO LABORATORY INFORMATION Date sample analyzed:11/19/2020 - �,� -Q �' "-jC-A—n Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 22 colonies /100ml- Nitrate (NO3) as N 00620 0.42 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 224 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 6.38 units Ba - Barium 01007 ug/L TOC 00680 24.0 mg/L Ca - Calcium 00916 mg/L Chloride oos4o 6 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71soo ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.713 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type (or gthbrized Agent) GW-59 Rev.06-07-2018 g:virochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 279% • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infotaenvironmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 07, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50367 Site: MW-4 11/19/2020 11:15 AM Water Jay Baker Test Method Results Date Analyzea Color Color Tan/Clear 11 /19/2020 Depth to water, ft. Depth to Water, Ft 6.8 feet 11 /19/2020 Ammonia Nitrogen EPA350.1 713pg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 4 (dry) gallons 11 /19/2020 Odor Qualitative None 11 /19/2020 Total Dissolved Solids (TDS) SM 2540 c 224 mg/L 11 /20/2020 Temperature SM 2550 8 18.2 C 11 /19/2020 Chloride SM 4500 Cl E 6 mg/L 11 /27/2020 pH SM 4500 H B 6.38 units 11 /19/2020 Total Organic Carbon (TOC) SM 5310 8 24.0 mg/L 11/23/2020 1, 1,1,2-Tetrachloroethane SM 62008 <0.5 pg/L 11 /26/2020 1, 1, 1 -Trichloroethane SM 62008 <0.5 pg/L 11 /26/2020 1,1,2,2-Tetrachloroethane SM 62008 <0.5 pg/L 11 /26/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11 /26/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 11 /26/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11 /26/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11 /2612020 1,2,3-Trichlorobenzene SM 62008 <0.5 pg/L 11 /26/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11 /26/2020 1,2,4-Trichlorobenzene SM 62008 <0.5 pg/L 11 /26/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 11 /26/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11 /26/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L '11 /26/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11 /26/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11 /26/2020 Report # 2020-19783 Page 10 of 30 :envirochem ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com environmentalchemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells 1,3,5-Trimethyl benzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 6200B <0.5 pg/L 11/26/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SM 6200B <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM 6200E <0.5 pg/L 11/26/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 62006 <0.5 pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 6200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Report # 2020-19783 Page 11 of 30L..,a.. Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab / Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 05, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 62DOB <0.5 pg/L 11 /26/2020 p-isopropyltoluene SM 62008 <0.5 pg/L 11/26/2020 sec -Butyl benzene SM 6200B <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-B utyl benzene SM 62008 <0.5 pg/L 11/26/2020 Tetrachloroethene SM 6200e <0.5 pg/L 11/26/2020 Toluene SM 6200B <0.5 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans- 1,3-dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Trichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/26/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/26/2020 Fecal Coliform SM 9222D MF 22 Colonies/100mL 11/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 0.05 mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.47mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method 0.42 mg/L 12/05/2020 Report #t 2020-19783 Page 12 cf K SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: • • • • INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED H Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South West of Sprayfield No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 5 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.50 units Temp. 000io: 1 9.0 °C DRY at time of Depth to Water Level 82546: 7.1 ft. below measuring point Screened Interval: 12 ft. to 2 ft. Spec. Cond. 00094: µMhos sampling, 9. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here: El Samples for metals were collected unfiltered: ❑ YES N NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed: 11/19/2020 —/ 2 _C j"-,2 ijk Z; Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 rng/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 2 colonies /100mL Nitrate (NO3) as N 00620 0.04 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 250 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 6.50 units Ba - Barium 01007 ug/L TOC 00680 16.1 mg/L Ca - Calcium oo916 mg/L Chloride 00940 45 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel o1o67 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.06-07-2018 SM ANALYTICAL & CONSULTING CHEMISTS Environmental. Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392,E424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab /Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax i nfo@aenvironmen talchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 05, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50368 Site: MW-5 11/19/2020 11:30 AM Water Jay Baker Test Method Results Date Analyzed Color color Tan/Clear 11/19/2020 Depth to water, ft. Depth to Water, Ft. 7.1 feet 11/19/2020 Ammonia Nitrogen EPA 350.1 < 200 pg/L 11 /30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2020 Odor Qualitative None 11/19/2020 Total Dissolved Solids (TDS) SM 2540 C 250 mg/L 11 /20/2020 Temperature SM 2560 B 19.0 C 11/19/2020 Chloride SM 4500 Cl E 45 mg/L 11 /27/2020 pH SM 4500 H B 6.50 units 11/19/2020 Total Organic Carbon (TOC) SM 5310 B 16.1 mg/L 11 /23/2020 1,1,1,2-Tetrachloroethane SM 62008 <0.5 pg/L 11/26/2020 1,1,1-Trichloroethane SM 6200B <0.5 pg/L 11 /2612020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/26/2020 1,1,2-Trichloroethane SM 62006 <0.5 pg/L 11/26/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloroethene SM 8200B <0.5 pg/L 11/26/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11 /2612020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 62008 <0.5 pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0. 5 pg/L 11/26/2020 1,2-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 1,2-Dichloroethane SM 6200E <0.5 pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 Report #.. 2020-19783 Page 13 of 30 [envi7rochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab/ Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax into@environnlentolcheniists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 5200B <0.5 pg/L 11126/2020 6romochloromethane SM 6200E <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromoform SM 8200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 6200B <0.5 pg/L 11/26/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SM 6200B <0.5 pg/L 11/26/2020 cis- 1,2-Dichloroethene SM 62008 <0.5 pg/L 11/26/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200E <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 1sopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Methylene chloride SM 5200B <0.5 pg/L 11/26/2020 Naphthalene SM 6200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Report # 2020-19763 Page 14 of 30 u - 77"1 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 L.ab; Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM 6200B <0.5 µg/L 11/26/2020 ortho-Xylene SM 6200B <0.5 µg/L 11/26/2020 p-Isopropyltoluene SM 6200B <0.5 µg/L 11/26/2020 sec -Butyl benzene SM 6200B <0.5 µg/L 11/26/2020 Styrene SM 6200B <0.5 µg/L 11/26/2020 tert-Butyl benzene SM 62008 <0.5 µg/L 11/26/2020 Tetrachloroethene SM 62008 <0.5 µg/L 11/26/2020 Toluene SM 6200B <0.5 µg/L 11/26/2020 Trans- 1,2-Dichloroethene SM 6200B <0.5 µg/L 11/26/2020 Trans-1, 3-d ich loropropene SM 6200B <0.5 µg/L 11/26/2020 Trichloroethene SM 6200B <0.5 µg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5 µg/L 11/26/2020 Vinyl chloride SM 62008 <0.5 µg/L 11/26/2020 Fecal Coliform SM 9222D MF 2 Colonies/100mL 11/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 <0.02mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.04 mg/L 11 /27/2020 Nitrate Nitrogen Subtraction Method 0.04 mg/L 12/05/2020 Report #:: 2020-19783 Page 15 of 3 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-25-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans N Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West Of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 6 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.39 units Temp. 000lo: 18.8 °C DRY at Depth to Water Level 82546: 9.1 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 -!), -cs- a; Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 4 colonies /100mL Nitrate (NO.) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 615 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.39 units Ba - Barium 01007 ug/L TOC 00680 4.3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 189 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Secretary - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type ittee for/Authorized Aqent) 2 GW-59 Rev.06-07-2018 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.3475843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmelltalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 05, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50369 Site: MW-6 11/19/2020 11:42 AM Water Jay Baker Test Method Results Date Analyzed Color color Tan/Clear 11/19/2020 Depth to water, ft. Depth to Water, Ft 9.1 feet 11/19/2020 Ammonia Nitrogen EPA 350.1 < 200 pg/L 11 /30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2020 Odor Qualitative Sulfur 11/19/2020 Total Dissolved Solids (TDS) SM 2540 C 615 mg/L 11 /20/2020 Temperature SM 2550 B 18.8 C 11/19/2020 Chloride SM 4500 Cl E 189 mg/L 11 /27/2020 pH SM 4500 H B 6.39 units 11/19/2020 Total Organic Carbon (TOC) SM 5310 B 4.3 mg/L 11 /23/2020 1,1,1,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11 /26/2020 1, 1, 2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11 /26/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11 /26/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 11 /26/2020 1, 1 -Dich loroethene SM 6200B <0.5 pg/L 11 /26/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11 /26/2020 1,2, 3-Trichlorobenzene SM 6200B <0.5 pg/L 11 /26/2020 1,2, 3-Trichloropropane SM 6200B <0.5 pg/L 11 /26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11 /26/2020 1,2,4-Trimethyl benzene SM 6200B <0.5 pg/L 11 /26/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 11 /26/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/26/2020 1,2-Dichlorobenzene SM 82008 <0.5 pg/L 11 /26/2020 1,2-Dichloroethane SM 62008 <0.5 pg/L 11 /26/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11 /26/2020 Report #:: 2020-19783 Page 16 of 30 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc, 6602 Windmill Wav, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392,4424 Fax 710 Bowsertovvii Road, Manteo, NC 27954 • 252,473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC. 28540 • 910.347.5843 Lab/'Fax info ci-environmentalchemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells 1, 3, 5-Trimethylbenzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dich lorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 2-Chlorotoluene sM e200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochloromethane SM e2008 <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM e200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 62006 <0.5 pg/L 11/26/2020 Chlorobenzene SM e20013 <0.5 ug/L 11/26/2020 Chloroethane SM 6200B <0.5 pg/L 11 /26/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SM 6200B <0.5 pg/L 11/26/2020 cis- 1,2-Dichloroethene SM 62008 <0.5 pg/L 11/26/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 8200B <0.5 pg/L 11/26/2020 Dibromomethane SM e200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 62008 <0.5 pg/L 11/26/2020 Ethylbenzene SM e200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 i sopropyl benzene SM e200B <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Methylene chloride SM e200B <0.5 pg/L 11/26/2020 Naphthalene SM 6200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Report # 2020-19783 Page 17 of 30 [envi7rochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(aenvironmentalchemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 6200B <0. 5 pg/L 11/26/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11126/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Styrene SM 8200E <0.5 pg/L 11/26/2020 tert-Butyl benzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/26/2020 Toluene SM 6200B <0.5 µg/L 11/26/2020 Trans- 1,2-Dichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trans- 1,3-dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Trichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 8200B <0.5 pg/L 11/26/2020 Vinyl chloride SM 62008 <0.5 pg/L 11/26/2020 Fecal Coliform SM 9222D MF 4 Colonies/100ml- 11/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 0.05mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/05/2020 Report # . 2020-19783 Page 11 8 of ?,' SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM - . ,... 1 ... -..- . T.- Please Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC 27944 act Person: Danny Shelton Perry ORC Location/Site Name: West of Baffle lagoon or County Perquimans Telephone#: 252-426-1007 No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED N Lagoon ❑ Remediation: Infiltration Gallery 0 Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 7 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 16.9 ft. Well Diameter: 2 in. pH 00400: 6.86 units Temp. 0001o: 17.8 °C DRY at time of Depth to Water Level 82546: 4.3 ft. below measuring point Screened Interval: 11.9 ft. to 16.9 ft. Spec. Cond. 00094: µMhos sampling, g, Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Red/Tan here: El Samples for metals were collected unfiltered: ❑ YES (] NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 ,• Laboratory Name: Environmental Chemists, Inc Certification No. 94 - PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 rrlg/L Nitrite (NO2) as N 00615 <0.02 Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.10 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 )issolved Solids:Total 70300 232 mg/L Al - Aluminum 01105 pH (Lab) 00403 6.86 units Ba - Barium 01007 TOC 00680 13.5 mg/L Ca - Calcium 00916 Chloride 00940 35 mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total 01034 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate 00945 mg/L Hg - Mercury 71900 Specific Conductance 00095 µMhos K - Potassium 00937 Total Ammonia 00610 0.401 mg/L Mg - Magnesium 00927 (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn -Manganese 01055 TKN as N 00625 mg/L Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L Pb - Lead o1o51 Zn - Zinc 01092 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev. U6-01-2U16 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax s.: 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 07, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50370 Site: MW-7 11/19/2020 10:15 AM Water Jay Baker Test Method Results Date Analyzed Color Color Red/Tan 11 /19/2020 Depth to water, ft. Depth to Water, Ft 4.3 feet 11/19/2020 Ammonia Nitrogen EPA350A 401 pg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11 /19/2020 Odor Qualitative Slight Sulfur 11 /19/2020 Total Dissolved Solids (TDS) SM 2540 C 232 mg/L 11 /20/2020 Temperature SM 2550 B 17.8 C 11 /19/2020 Chloride SM 4500 Cl E 35 mg/L 11 /27/2020 pH SM 4500 H B 6.86 units 11/19/2020 Total Organic Carbon (TOC) SM 5310 B 13.5 mg/L 11 /23/2020 1, 1, 1,2-Tetrachloroethane SM 620013 <0.5 pg/L. 11 /26/2020 1, 1, 1 -Trichloroethane SM 62006 <0.5 pg/L 11 /26/2020 1, 1, 2,2-Tetrachloroethane SM 6200B <0.5 pg/L. 11/261.2..020 1,1, 2-Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1, 1 -Dichloroethane SM 62008 <0.5 pg/L 11 /26/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11 /26/2020 1,1-Dichioropropene SM 6200B <0.5 pg/L 11 /26/2020 1, 2, 3-Trichlorobenzene SM 6200B <0. 5 pg/L 11 /26/2020 1,2,3-Trichloropropane SM 62006 <0.5 pg/L 11 /26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11 /26/2020 1,2,4-Trimethylbenzene SM 6200E <0.5 pg/L 11 /2612020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 pq/L 11 /26/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11 /26/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11 /26/2020 1,2-Dichloropropane SM 62008 <0.5 pg/L 11 /26/2020 Report #: 2020-197B3 Page 19 of 30 :envirochemn] ANALYTICAL & CONSULTING CHEMISTS Environmental. Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.44 !4 Fix 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info envi ronntentalcllemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11 /26/20?0 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200E <0.5 pg/L 11/26/2020 Bromoform SM 62008 <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0, 5 pg/L 11/26/2020 Carbon tetrachloride SM 62008 <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 6200B <0.5 pg/L 11/26/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SM 62006 <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM 8200B <0.5 pg/L 11/26/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 62008 <0.5 pg/L 11 /26/2020 Isop ropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 62008 <1.0 pg/L 11/26/2020 Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 6200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Report # 2020-19783 Page 20 of 30 roop"-.— -,-"7 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Far sM 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab!Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/26/2020 sec -Butyl benzene SM 6200B <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 {Jg/L 11/26/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/26/2020 Toluene SM 62008 <0.5 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 62008 <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/26/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/26/2020 Fecal Coliform SM9222DMF <1 Colonies/100mL 11/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 < 0.02 mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.10mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method 0.10 mg/L 12/05/2020 Report # 2020-19783 Page 21 of 3C SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: East of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 8 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.43 units Temp. 000lo: 19.8 °C DRY at Depth to Water Level 82546: 4.8 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Lt Tan/Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 -� /2-C S -1.Q,i� Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 < 0.02 mg/L Pb - Lead 01051 ug/L Coliform: IMF Fecal 31616 4400 colonies /100mL Nitrate (1103) as N 00620 0.27 ni Zn - Zinc 01092 ni Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 349 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.43 units Ba - Barium 01007 11 TOC 00680 12.9 mg/L Ca - Calcium 00916 mg/L Chloride 00940 107 ni Cd - Cadmium 01027 11 Arsenic 01002 111 Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 ni ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 11 Fe - Iron 01045 111 (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 719oo iii Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 ni VOC 7873 method # Total Ammonia 00610 0.446 mg/L Mg - Magnesium 00927 ni method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese o1o55 iii , method # TKN as N 00625 ni Ni - Nickel 01067 ug/L method # For Remediation Systems Only Total• certify that. to the best of my knowledge and belief. the information submitted in this report is true. aca DWR-certified laboratory. I am aware that there are significant penalties for submitting false information Corporate Secetary ni Effluent Total VOCs: Permittee (or Authorized Aqent) Name and Title - Please print or type Signature of Pf.Xitteo/ thorized Agent) GW-59 Rev.06-07-2018 f mg/L VOC Removal% _"107 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392A223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists_com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 07, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50371 Site: MW-8 11/19/2020 11.58 AM Water Jay Baker Test Method Results Date Analyzed Color Color Lt Tan/Clear 11/19/2020 Depth to water, ft. Depth to water, Ft. 4.8 feet 11 /19/2020 Ammonia Nitrogen EPA 350.1 446 pg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11 /19/2020 Odor Qualitative Sulfur 11 /19/2020 Total Dissolved Solids (TDS) SM 2540 C 349 mg/L 11 /20/2020 Temperature SM 2550 B 19.8 C 11 /19/2020 Chloride SM 4500 Cl E 107 mg/L 11 /27/2020 pH SM 4500 H B 6.43 units 11 /19/2020 Total Organic Carbon (TOC) SM 5310 B 12.9 mg/L 11/23/2020 1,1,1,2-Tetrachloroethane SM 8200E <0.5 uglL 11/25/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/25/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/25/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/25/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 11/25/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11/25/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11/25/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/25/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11/25/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/25/2020 1,2,4-Trimethyl benzene SM 6200B <0.5 pg/L 11 /25/2020 1,2-Dibromo-3-Chloropropane SM62008 <0.5pg/L 11/25/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/25/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/25/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/25/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/25/2020 Report 9 2020.19783 Page 22 of 30 011�- envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax info -it environmen talchemists.coni Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/25/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/25/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/25/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/25/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/25/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/25/2020 4-Chlorotoluene SM 52008 <0.5 pg/L 11/25/2020 Benzene SM 6200B <0.5 pg/L 11/25/2020 Bromobenzene SM 5200B <0.5 pg/L 11/25/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/25/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/25/2020 Bromoform SM 6200B <0.5 pg/L 11/25/2020 Bromomethane SM 6200B <0.5 pg/L 11/25/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11 /25/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/25/2020 Chloroethane SM 6200B <0.5 pg/L 11/25/2020 Chloroform SM 62008 <0.5 pg/L 11/25/2020 Chloromethane SM 6200B <0.5 pg/L 11/25/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/25/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 11/25/2020 Dibromochloromethane SM 62008 <0.5 pg/L 11/25/2020 Dibromomethane SM 62008 <0.5 pg/L 11/25/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/25/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/25/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/25/2020 lsopropylbenzene SM 6200B <0.5 pg/L 11/25/2020 M+P Xylene SM 6200B <1.0 pg/L 11/25/2020 Methylene chloride SM 6200B <0.5 pg/L 11/25/2020 Naphthalene SM 6200B <0.5 pg/L 11/25/2020 n-Buhylbenzene SM 6200B <0.5 pg/L 11/25/2020 Report #.. 2020-19763 Page 23 of 30 FFPW"-.- "I $M ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 La'b/F"ax iiifo@environmentalcheniists.cc.,rn Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM 6200B <0.5 pg/L 11 /2512020 ortho-Xylene SM 6200B <0.5 pg/L 11/25/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/25/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/25/2020 Styrene SM 6200B <0.5 pg/L 11/25/2020 tert-Butyibenzene SM 62006 <0.5 pg/L 11/25/2020 Tetrachloroethene SM 8200B <0.5 pg/L 11/25/2020 Toluene SM 8200B <0.5 pg/L 11/25/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/25/2020 Trans- 1,3-dichloropropene SM6200B <0.5pg/L 11/25/2020 Trichloroethene SM 6200B <0.5 pg/L 11/25/2020 Trichiorofluoromethane SM 6200E <0.5 pg/L 11/25/2020 Vinyl chloride SM 62008 <0.5 pg/L 11/25/2020 Fecal Coliform SM 9222D MF 4400 Colonies/100nnL 11 /19/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.27mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method 0.27 mg/L 12/05/2020 Report #:. 2020-19783 Oage 24 :,)" G SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 9 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 0040o: 5.81 units Temp. 000lo: 1 9.4 °C DRY at Depth to Water Level 82546: 7.6 ft. below measuring point Screened Interval: 4 ft. to 14 ft. Spec. Cond. 000sa: µ time ofMhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 - �,L -�� S` - z c� Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 >6000 colonies /100mL Nitrate (NO3) as N 00620 0.14 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids -.Total 70300 55 mg/L Al - Aluminum ol1o5 mg/L pH (Lab) 00403 5.81 units Ba - Barium 01007 ug/L TOC 00680 1.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 6 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance oo095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type Aqent) GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 16602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 B 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info,tr,environmentalchennists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 05, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50372 Site: MW-9 11/19/2020 12:25 PM Water Jay Baker Test Method Results Date Analyzed Color Color Clear 11/19/2020 Depth to water, ft. Depth to water, Ft 7.6 feet 11/19/2020 Ammonia Nitrogen EPA 350.1 < 200 pg/L 11 /30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/19/2020 Odor Qualitative None 11/19/2020 Total Dissolved Solids (TDS) SM 2540 c 55 mg/L 11/20/2020 Temperature SM 2550 B 19.4 C 11/19/2020 Chloride SM 4500 Cl E 6 mg/L 11/27/2020 Did SM 4500 H B 5.81 units 11/19/2020 Total Organic Carbon (TOC) SM 5310 B 1.1 mg/L 11 /23/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 11126/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 11/26/2020 1, 1 -Dichloroethene SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloropropene SM 6200B <0, 5 pg/L 11/26/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200E <0.5 pg/L 11/26/2020 1,2,4-TrimethyIbenzene SM 6200B <0.5 pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/26/2020 1,2-Dibromoethane SM 62008 <0.5 pg/L 11/26/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 Report # 2020-19783 Page 25 of 30 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmuigtor, NC 28405 Y 910.392.0223 Lab " 910.392.4424 Fax 710 Bowsertown Road. Manteo, NC 27954 ' 252.473.5702 Lab/Fax s" 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@emvironmentalchemists.conl Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 05, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells 1, 3,5-Trimethylbenzene SM 62005 <0.5 pg/L 11/26/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1, 3-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 62006 <0.5 pg/L 11/26/2020 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochlorom ethane SM 6200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 620DB <0.5 pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 62008 <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Ch loroethane SM 6200B <0.5 pg/L 11 /26/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SM 62008 <0.5 pg/L 11/26/2020 cis- 1,2-Dichloroethene SM 6200B <0.5 pg/L 11/26/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Dibromomethane SM 62008 <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 62008 <1.0 pg/L 11/26/2020 Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 6200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Report # 2020-19783 Page 26 of 30 �„ Lenvirochem SN ANALYTICAL & CONSULTING CHEMISTS Environmental. Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.442" i;ax 710 BoNvsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,,, Fax 255-A Wilmington Highway, Jacksonville, NC 28540 n 910.347.5843 Lab/Fax info ,tenvironnientalchemists.com Albemarle Utility Date of Report: Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells n-Propyibenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 620CB <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/26/2020 sec-B utyl benzene SM 6200B <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-B utyl benzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/26/2020 Toluene SM 6200B <0.5 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans- 1,3-dichloropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/26/2020 Vinyl chloride SM 6200E <0.5 pg/L 11/26/2020 Fecal Coliform SM 9222D MF >6000 Colonies/100mL 11/19/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 < 0.02mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.14 mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method 0.14 mg/L 12/05/2020 Report #:: 2020-19763 Page 27 of 3;J SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery Hertford N.C. 27944 County Perquimans A Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Weil Location/Site Name: South of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 11/19/2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.23 units Temp. 000lo: 19.4 °C DRY at Depth to Water Level 82546: 9.4 ft. below measuring point Screened Interval: 5 ft. to 14 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES © NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed:11/19/2020 - /�-p S -?-G�. �; Laboratory Name: Environmental Chemists„ Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.29 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 207 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.23 units Ba - Barium 01007 ug/L TOC 00680 1.0 mg/L Ca - Calcium 00916 mg/L Chloride 00940 71 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH, as N. Ammonia Nitrogen. Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type (or Ayih( ized Aqent) 2 GW-59 Rev.06-07-2018 Foop"'.— --- —1 7 -7 SM ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott Lab ID Sample ID: 20-50373 Site: MW-10 Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo; NC 27954 • 252.473.5702 I.ab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 1.,ab/Pax infow environnientalchemists.com Date of Report: Dec 05, 2020 Customer PO #: 27944 Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) 1,1,1,2-Tetrachloroethane 1, 1, 1 -Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1, 1 -Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane Collect Date/Time Matrix 11/19/2020 12:13 PM Water Method Color Depth to Water, Ft. EPA 350.1 Gallons Bailed before sampling Qualitative SM 2540 C SM 2550 B SM 4500 CI E SM 4500 H B SM 5310 B SM 6200B SM 6200B SM 6200B SM 6200B SM 62008 SM 6200B SM 6200B SM 8200B SM 6200B SM 6200B SM 62008 SM 6200B SM 62008 SM 6200B SM 6200B SM 62008 Results Sampled by Jay Baker Date Analyzed Clear 11/19/2020 9.4 feet 11/19/2020 < 200 pg/L 11 /30/2020 5.0gallons 11/19/2020 None 11/19/2020 207 mg/L 11/20/2020 19.4 C 11/19/2020 71 mg/L 11 /27/2020 6.23units 11/19/2020 1.0 mg/L 11/23/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 µg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 <0.5 pg/L 11/25/2020 Report #:: 2020-19783 Page 28 of 30 :enviriochemn] ANALYTICAL 8 CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab ^ 910.392.4424 ==a\ 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax. 255-A Wilmington Highwav, Jacksonville, NC 28540 • 910.347.5843 Lab%Fax infow cnvironmentalchemists.corn Date of Report: Dec 05, 2020 Customer PO #: 27944 Customer ID: 09110024 Report #: 2020-19783 Project ID: Monitoring Wells 1,3, 5-Trimethylbenzene SM 6200B <0.5 pg/L 11/25/2020 1,3-Dichlorobenzene SM 6200E <0.5 pg/L 11/25/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11 /25/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/25/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11 /25/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/25/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/25/2020 Benzene SM 6200B <0.5 pg/L 11/25/2020 Bromobenzene SM 6200E <0.5 pg/L 11/25/2020 Bromochloromethane SM 62008 <0.5 pg/L 11/25/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/25/2020 Bromoform SM 6200B <0.5 pg/L 11/25/2020 Bromomethane SM 6200B <0.5 pg/L 11/25/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/25/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/25/2020 Chloroethane SM 6200B <0.5 pg/L 11/25/2020 Chloroform SM 6200B <0.5 pg/L 11/25/2020 Chloromethane SM 6200B <0.5 pg/L 11/25/2020 cis- 1,2-Dichloroethene SM 6200B <0.5 pg/L 11/25/2020 cis-1, 3-Dichloropropene SM 6200B <0.5 pg/L 11/25/2020 Dibromochloromethane SM 62008 <0.5 pg/L 11/25/2020 Dibromomethane SM 6200B <0.5 pg/L 11/25/2020 Dichlorodifluoromethane SM 5200B <0.5 pg/L 11/25/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/25/2020 Hexachlorobutadiene SM 620DB <0.5 pg/L 11 /25/2020 1sopropylbenzene SM 6200B <0.5 pg/L 11/25/2020 M+P Xylene SM 6200B <1.0 pg/L 11/25/2020 Methylene chloride SM 6200B <0.5 pg/L 11/25/2020 Naphthalene SM 6200B <0.5 pg/L 11/25/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/25/2020 Report # 2020-19783 Page 29 of 30 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4421 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Leib/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Vax info@environmentalchemists.com Albemarle Utility Date of Report, Dec 05, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-19783 Project ID: Monitoring Wells n-Propylbenzene SM e200B <0.5 pg/L 11 /2512020 ortho-Xylene SM 62006 <0.5 µg/L 11/25/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/25/2020 sec -Butyl benzene SM 6200B <0.5 pg/L 11/25/2020 Styrene SM e200B <0.5 pg/L 11/25/2020 tert- B utyl benzene SM 82006 <0.5 pg/L 11/25/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/25/2020 Toluene SM 62008 <0.5 pg/L 11/25/2020 Trans-1,2-Dichloroethene SM 62008 <0.5 pg/L 11/25/2020 Trans- 1,3-dichloropropene SM 6200B <0.5 pg/L 11/25/2020 Trichloroethene SM 6200B <0.5 pg/L 11/25/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/25/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/25/2020 Fecal Coliform SM 9222D MF <1 Colonies/100mL 11/19/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 3532 < 0.02 mg/L 11/20/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.29 mg/L 11/27/2020 Nitrate Nitrogen Subtraction Method 0.29 mg/L 12/05/2020 Comment: Reviewed by: Report #:: 2020-19783 Page 30 of 30 1 GW-59A COMPLIANCE REPORT FORM Permit #�( (Submit one each monitoring period with GW-59 forms.) I Enter date monitoring results were due. (i.2-5 j'i=) Will this monitoring report (GW-59 and GW-59A) YES 0144 be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES O identification plate, area overgrown, etc.)? ff the answer is "Yes ", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? ES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: �� .. P.t4 � , (9 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, annd- sample collection date for each occurrence (for the last two years). Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES O If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. g The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. 1 hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. 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