WQ0039053_Regional Office Historical File Pre 2018

P,OY COOPER
Govemor
MICHAEL S. REGAN
Secretary
S. DANIEL SMITH
Dfrector
VAUGHN STEVENSON — VICE PRESIDENT
BIO-NOMIC SERVICES, INC.
530 WOODLAWN STREET
BELMONT, NORTH CAROLINA 28012-2130
Dear Mr. Stevenson:
NORTH CAROLINA
i:nvtransnental Quality
March 9, 2020
�t .ss.. a. • ks� .
Subject: Permit No. WQ0039053
Bio-Nomic Services DCAR
Attachment A Certification
Gaston County
In accordance with your permit major modification request received December 3, 2019, and
subsequent additional information received January 31, 2020, we are forwarding herewith a modified
Attachment A certified March 9, 2020, to Bio-Nomic Services, Inc. for the subject residuals management
program.
Modifications to the subject Attachment are as follows: Addition of 2,000 dry tons/year from
George L. Bernhardt, Sr. Lake Rhodhiss WTP (Permit No. NCO114010) located in Caldwell County.
The modified Attachment A shall be effective from the date of certification until February 28, 2022
(i.e., expiration date of the current permit), shall void Attachment A of Permit No. WQ0030953 issued
March 22, 2017 that was previously certified on April 16, 2019, and shall be subject to the conditions and
limitations as specified therein, as well as those specified in the above -referenced permit. Please replace
Attachment A of Permit No. WQ0039053 that was certified on April 16, 2019 with the modified
Attachment A. Please note that the Permittee shall submit a renewal application no later than
September 1, 2021.
If any parts, requirements or limitations contained in this certification are unacceptable, the
Permittee has the right to request an adjudicatory hearing upon written request within 30 days following
receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B
of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail
Service Center, Raleigh, NC 27699-6714. Otherwise, this certification shall be final and binding.
If you need any additional information concerning this matter, please contact Poonam Giri at (919)
707-3656 or Coonam.giri(r_0ncdenr.gov.
Sincerely, tt��
Daniel Smith, Director
Division of Water Resources
North Car ollna Department of Environmental Quality I Dlvislon of Water Resources
C_ �S S12 Norih Salisbury Street 11617 mail Service Center I Raleigh, North Carolina 27699-1617
-�.. 4v+
� �=�.1— 919,707.9000

State of North Carolina
Department of Environmental Quality
Division of Water Resources
WATER QUALITY REGIONAL OPERATIONS SECTION
Division of Water Resources NON -DISCHARGE APPLICATION REVIEW REQUEST FORM
't-1k' UlNCDENR/DWIt
December 4, 2019
DEC - 9 2019
To: �WQR®S:_A ndrew.Ptfner / Corey Basinger ._.;�
--- IwQROS
From: Poonam Giri, Water Quality Permitting Section -Non-Discharge Branch "00RE=SVILLE RF_(3I011dAL OFFPCF
Permit Number: WQ0039053 Permit Type: Distribution of Residual Solids (503 Exempt)
Applicant: Bio-Nomic Services, Inc.
Owner Type: Organization
Facility Name: Bio-Nomic Services DCAR
Signature Authority: Vaughn Stevenson
Address: 530 Woodlawn St., Belmont, NC 28012
Fee Category: Non -Discharge Major
Project Type: Major Modification
Owner in BIMS? Yes
Facility in RIMS? Yes
Title: Vice President
County: Gaston
Fee Amount: $395 - Major Modification
Comments/Other Information: Copy of the application is on Laserfiche - Residuals source is in Lenoir County
(WaRO). of
IIJ
Attached, you will find all information submitted in support of the above -referenced application for your review,
comment, and/or action. Within 45 calendar days, please take the following actions:
® Return this form completed. ® Return a completed staff report.
❑ Attach an Attachment B for Certification. ❑ Issue an Attachment B Certification.
When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and
return it to the appropriate Central Office Water Quality Permitting Section contact person listed above.
RO-WQROS Reviewer:
Date: /2f�✓//
FORM: WQROSNDARR 09-15 Page 1 of 1

k 4
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
LINDA CULPEPPER
Director
VAUGHN STEVENSON —VICE PRESIDENT
BIO-NOMIC SERVICES, INC.
530 WOODLAWN ST.
BELMONT, NORTH CAROLINA 28012
Dear Mr. Stevenson:
NORTH CAROLINA
Environmental Quality
December 5, 2019
Subject: Acknowledgement of
Application No. WQ0039053
Bio-Nomic Services DCAR
Residuals Management System
Gaston County
The Water Quality Permitting Section acknowledges receipt of your permit application and
supporting documentation received on December 3, 2019. Your application package has been assigned the
number listed above, and the primary reviewer is Poonam Giri.
Central and Regional Office staff will perform a detailed review of the provided application, and
may contact you with a request for additional information. To ensure maximum efficiency in processing
permit applications, the Division of Water Resources requests your assistance in providing a timely and
complete response to any additional information requests.
Please note that processing standard review permit applications may take as long as 60 to 90 days
after receipt of a complete application. If you have any questions, please contact
Poonam Giri at [phone] or [e-mail].
Sincerely,
Nathaniel D. Thornburg, Supervisor
Division of Water Resources
cc:ii:Qn
Permit File WQ0039053
®— North Carolina Department of Environmental Quality I Division of Water Resources
512 North Salisbury Street 1 1617 Mail Service Center I Raleigh, North Carolina 27699-1617
N0111 +caaa DNA
Depvrlment al Emimnmen4•I Quality 919.707.9000

DW_R-­_._
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
WATER QUALITY REGIONAL OPERATIONS SECTION
NON -DISCHARGE APPLICATION REVIEW REQUEST FORM
March 21, 2019
To: ` :z®L-i7+ROaicruva CareA Basinger
RECEIVED/NCbCNR/DbVji
tV��A R 2 0 2,919
From: Troy Doby, Water Quality Permitting Section - Non -Discharge Branch �J'00R1 w� PEGI
Q ty g g SVILLE RECIpNtiL CFFfCJ�
Permit Number: WQ0039053 Permit Type: Distribution of Residual Solids (503 Exempt)
Applicant: Bio-Nomic Services, Inc.
Owner Type: Organization
Facility Name: Bio-Nomic Services DCAR
Signature Authority: Vaughn Stevenson
Address: 530 Woodlawn St., Belmont, NC 28012
Fee Category: Non -Discharge Major
Project Type: Major Modification
Owner in BIMS? Yes
Facility in BIMS? Yes
Title: Assistant Vice President
County: Gaston
Fee Amount: $395 - Major Modification
Comments/Other Information. Regional copy of the application is on I a'ser� 1che
Attached, you will find all information submitted in support of the above -referenced application for your review,
comment, and/or action. Within 45 calendar days, please take the following actions:
® Return this form completed. ® Return a completed staff report.
❑ Attach an Attachment B for Certification. ❑ Issue an Attachment B Certification.
When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and
return it to the appropriate Central Office Water Quality Permitting Section contact person listed above.
RO-WQROS Reviewer:
Date:
FORM: WQROSNDARR 09-15 Page 1 of I

W
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
LINDA CULPEPPER
Director
NORTH CAROLINA
Environmental Quality
March 22, 2019
VAUGHN STEVENSON —ASSISTANT VICE PRESIDENT
BIO-NOMIC SERVICES, INC.
530 WOODLAWN ST.
BELMONT, NORTH CAROLINA 28012
Subject: Acknowledgement of
Application No. WQ0039053
Bio-Nomic Services DCAR
Residuals Management System
Gaston County
Dear Applicant:
The Water Quality Permitting Section acknowledges receipt of your permit application and
supporting documentation received on March 21, 2019. Your application package has been assigned the
number listed above, and the primary reviewer is Troy Doby.
Central and Regional Office staff will perform a detailed review of the provided application, and
may contact you with a request for additional information. To ensure maximum efficiency in processing
permit applications, the Division of Water Resources requests your assistance in providing a timely and
complete response to any additional information requests.
Please note that processing standard review permit applications may take as long as 60 to 90 days
after receipt of a complete application. If you have any questions, please contact
Troy Doby at (919) 707-3 65 5 or [e-mail].
Sincerely,
Nathaniel D. Thornburg, Supervisor
Division of Water Resources
cc: Mooresville Regonal`Office, WateraQuality Regional Operations Section'
Permit File WQ0039053
North Carolina Department of Environmental Quality I Division of Water Resources
512 North Salisbury Street 1 1617 Mail Service Center I Raleigh, North Carolina 27699-1617
NORTH CAROL INA
oupanmemmEnviron anmlmuulp 919.707.9000

a � �
f R ,
DW-R-
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
WATER QUALITY REGIONAL OPERATIONS SECTION
NON -DISCHARGE APPLICATION REVIEW REQUEST FORM
December 12, 2018
To:/IRuQR'OS.;izdr w Prfner oreyABasing
RECEIVED/NCDENR/Dl14 R
DEC 17 2018
WQP,OS
From: Troy Doby, Water Quality Permitting Section - Non -Discharge Branch MOORESVILLE REGIONAL OFFICE
Permit Number: WQ0039053 Permit Type: Distribution of Residual Solids (503 Exempt)
Applicant: Bio-Nomic Services, Inc.
Owner Type: Organization
Facility Name: Bio-Nomic Services DCAR
Signature Authority: Pete Fleetwood
Address: 530 Woodlawn St., Belmont, NC 28012
Fee Category: Non -Discharge Minef /f!A_�WZ
Project Type: Major Modification
Owner in BIMS? Yes
Facility in BIMS? Yes
Title: President
County: Mecklenburg
Fee Amount: 6-- meet
34- M r &4Q
Comments/Other Information: RegionallOffice �opyofathesapp'lcationxts2ori Lass
Attached, you will find all information submitted in support of the above -referenced application for your review,
comment, and/or action. Within 45 calendar days, please take the following actions:
® Return this form completed. ® Return a completed staff report.
❑ Attach an Attachment B for Certification. ❑ Issue an Attachment B Certification.
When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and
return it to the appropriate Central Office Water Quality Permitting Section contact person listed above.
RO-WQROS Reviewer:
Date:
FORM: WQROSNDARR 09-15 Page 1 of 1

NORTH CAROLINA
Environmentaf Quality
December 13, 2018
PETE FLEETWOOD — PRESIDENT
BIO-NOMIC SERVICES, INC.
530 WOODLAWN ST.
BELMONT, NORTH CAROLINA 28012
Dear Mr. Fleetwood:
ROY COOPER
ove"fa
MICHAEL S. REGAN
ecri tore
LIN A CULPEPPER
Director
Subject: Acknowledgement of
Application No. WQ0039053
Bio-Nomic Services DCAR
Residuals Management System
Mecklenburg County
The Water Quality Permitting Section acknowledges receipt of your permit application and
supporting documentation received on December 12, 2018. Your application package has been assigned
the number listed above, and the primary reviewer is Troy Doby.
Central and Regional Office staff will perform a detailed review of the provided application, and
may contact you with a request for additional information. To ensure maximum efficiency in processing
permit applications, the Division of Water Resources requests your assistance in providing a timely and
complete response to any additional information requests.
Please note that processing standard review permit applications may take as long as 60 to 90 days
after receipt of a complete application. If you have any questions, please contact
Troy Doby at [phone] or [e-mail].
Sincerely,
l
Nathaniel D. Thornburg, Supervisor
Division of Water Resources
cc: LMoolesv lle Regional Office ^Water. uali , �Re anal O eratiotts_Sectiogf
__ _ Q �ty g .p
Permit File WQ0039053
North Carolina Department of Environmental Quality I Division of Water Resources I Non -Discharge Branch
512 North Salisbury Street 11617 Mail Service Center I Raleigh, North Carolina 27699-1617
919.707.3654

APPLICATION FOR
DISTRIBUTION! OF CLASS A RESIDUALS
PERMIT MODIFICATION
BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
Willcox & Mabe Soil Solutions, PLLC Project No. l 5-1 8
Prepared for:
Bio-Nomic Services, Inc.
530 Woodlawn Street.
Belmont, North Carolina 28012
Prepared by:
Willcox & Mabe Soil Solutions, PLLC
7231 B Summerfield Road
Greensboro, North Carolina 27358
willcax&mate
SOIL. S 0 L U T 1 0 N S
December, 2018

Martin Mabe
From:
Sent:
To:
Subject:
Attachments:
Excellent news. Thank you.
Zac Lake <[e-mail]>
Friday, November'30, 2018 5:04 PM
Martin Mabe
Re: Landowner Agreement
McCallFarmsBruceFoods_Fina(ClosureLetter_2.0180ctOl.pdf
Below is what we sent to the state and attached is their reply. Please let me know if you need more info.
Dear Rick,
As discussed during a phone. conference call held on August 7, 2018, between the North Carolina Department
of Environmental Quality (NCDEQ), Geosyntec Consultants (Geosyntec), and Mr. Zac Lake, who, serves as a
consultant to McCall Farms (McCall), the following plan has been agreed upon between McCall and the City of
Wilson (the City) to finalize the closure of the lagoon system at the former Bruce Foods Facility. The first part
of this email summarizes the background information that led to the teleconference, and the second part of the
email Iays out the concrete steps planned, to finalize the closure process.
Geosyntec respectfully requests that NCDEQ review the proposed steps forward summarized below and
provide concurrence (via reply to this email) with the plan. Following execution of the steps below, Geosyntec
will compile documentation in a "Closure Report Addendum" to be submitted to NCDEQ for final approval of
the lagoon closure process.
Background:
* In June 2016, McCall and the City of Wilson entered into an Agreement in which McCall donated the
former Bruce Foods Facility located in Wilson, NC, to the City of Wilson. The property contains six inactive
wastewater lagoons that were part. of the former Bruce Foods wastewater treatment operations. As part of the
Agreement, McCall agreed to remove wastewater and biosolids from the lagoons, and the City agreed to be
responsible for the backfilling of four of the six lagoons (labeled 49 0, 1, 2, and 3), while keeping lagoons 44 4
and 5 open for future use by the City.
* Following the execution of the Agreement, McCall removed the remaining wastewater from the six lagoons
tluough land application onto nearby permitted land application fields. The land application attempted to
maximize the removal of biosolids from the lagoons, but residual biosolids remained at the bottom of the
lagoons. McCall sampled the biosolids, and since results were below the Preliminary Soil Remediation Goals
(PSRG) for -protection of groundwater and fecal coliform levels were below 1,000 MPN/g (i.e. Class A),
McCall proposed to leave the residuals in place.
* Following the completion of the landapplication efforts, Geosyntec, on behalf of McCall, submitted a
Lagoon Closure Report dated April 2018 to NCDEQ to document the lagoon closure activities at the former
Bruce Foods Facility.
* Subsequent to the submittal of the Closure Report, NCDEQ issued a letter to McCall dated May 21, 2018
indicating that the lagoon closure was incomplete given that the lagoons have not been fully decommissioned.
Given that the decommissioning will be the responsibility of the City of Wilson and that two lagoons will
remain open for future use, some of the retention berms will remain in place. This, in turn, means that the
lagoon system will only be "partially decommissioned" with respect to berms and retention structures.

In subsequent conversations between McCall and the City, McCall agreed to linaiicially suppoI•t the removal
of residual biosolids from the lagoons, with subsequent land application of the biosolids onto the permitted
nearby land application fields. In addition, if more acreage is needed, the City has available land to
accommodate the excess biosolids. In return for the financial support, the City will use its contractors and
equipment to remove and land apply the biosolids.
Steps Forward:
The City confirmed in a letter dated July 30, 2018 (attached to this email) that it intents to move forward
consistent with the Agreement and the steps laid out above.
* Preliminary calculations yielded a total area of 206 acres required to land apply the estimated volume of
biosolids. These calculations include the following assumptions:
* Biosolids can be applied at agronomic rates of 275 lbs of plant. available nitrogen (PAN) per acre;
* Lbs of PAN per ton of biosolids have been calculated based on the analytical results for TKN, NH3-N,
and NO2/NO3-N from composite samples of each lagoon using an EPA -generated spreadsheet that accounts for
inorganic nitrogen as well as mineralization of organic nitrogen in the biosolids;
* Sludge volumes and tonnages were calculated by McCaIl based on measured sludge thicknesses in each
lagoon; and
* Supporting spreadsheet calculations are attached to this email.
.4, A total of only 244 lbs of PAN has been land -applied to fields B and C during irrigation of the lagoon
wastewater over the past two years, which means that almost the entire acreage of the permitted areas is
available for land application.
x The City will use its contractors and equipment to remove the biosolids from the lagoons and to land apply
them onto Fields A, B, and C, with excess biosolids being applied to other City -owned land.
* The City has an existing, erosion and sedimentation control plan that it is going to implement during the
excavation of the biosolids as well as the regrading and reseeding of the disturbed areas.
* Given that the biosolids meet Class A requirements and are below PSRG levels for protection of
groundwater, they can be land applied to these proposed areas (including the City -owned land) without
restrictions.
* Subsequent to the excavation and land application activities, the City will backfill lagoons ## 0, 1, 2, and 3
and reseed the disturbed areas with grasses while leaving lagoons ## 4 and 5 open, consistent with the letter
attached to this email.
1= Following completion of these closure activities, McCall will subni t supporting documentation to
Geosyntec, and Geosyntec will compile a "Closure Report Addendum" that documents these activities for final
approval of the closure process by NCDEQ.
As indicated in the introduction, please review this information and conceptual plan and provide concurrency in
a reply to this email.
Best regards,
Herwig Goldemund, Ph.D.
Senior Scientist
Geosyntec Consultants
1255 Roberts Boulevard, NW

0 . , 11 A
Suite 200
Kennesaw, GA 30144
Phone: [phone]
Fax: [phone]
Mobile: 404.4,32.0499
WWV ieosy��tec.c_QgI<h 1) //www.gec�sya icc:cam/>
Thanks,
Zac
On Nov 30, 2018, at 3:29 PM, Martin Mabe <Martiiire WI1_J,QOXNIABESOII_.COM> wrote:
Zac,
I just received the TCLP results and they are good to go.
Thanks,
Martin Mabe,
<image0�0pp2.jpg> AID�"5.i_.3H 5,.�'71
PLEASE N011 OUR ADS S A7INIGiED
Willcox & Mabe Soil Solutions, PLLC
7231E Summerfield Road
Summerfield, N.C. 27358
Mobile No. 336-312-1396
martiLi,Pwillcoxmabesoil.cor-n
From: Martin Mabe
Sent: Friday, November 30, 2018 2:10 PM
To:'Zac Lake' <zaclake@indecendencewater_net>
Subject: RE: Landowner Agreement
i received the fecais this morning. They passed for Class A levels. Still waiting on TCLP and Nutirent &
Metal analyses form the lab.
Can you give me a call at 336-31.2-1396?
M.
3

-
Environntcnlal Quullty
October 1, 2018
Mr. Marion Swink
McCall Farms, Inc.
6615 South Irby St.
Effingham, SC 29541
Subject: Approval of Updated Lagoon Closure Plan for Former Bruce Foods Facility
Located in Wilson County (Wilson, NC)
McCall Farms, Inc. (Effingham, SC)
Dear Mr, Swink:
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
i..INDA CULPEPPER
Interim Director
The NC DEQ, Division of Water Resources (DWR), Water Quality Regional Operations Section
(WQROS), has reviewed the updated lagoon closure plan, received on August 28, 2018, for the Former
Bruce Foods Facility. The updated report was prepared by Geosyntec Consultants. We have recently
discussed with Geosyntec Consultants how the biosolids at the site are able to meet Class A requirements.
In summary, we have determined that the updated lagoon closure submittal is complete.
Be sure to contact us iflhere are any significant changes to tite current agreement Nvilh the City of Wilson
that impact the lagoon closure activities and compliance with permit WQ0003823, if you have any
questions regarding this letter, please contact me or Rick Bolich at [phone]..
Sincerely,
-i'
Thomas I-1. McKinney
Environmental Engineer
cc: DWR Central Files
RRO-WQROS Files
Zach Lake, McCall Farms, Inc., via email
Jeffrey M. Ahrens, P.E., Geosyntech Consultants, via email
Jimmy Pridgeu, City of Wilson WWTP, via email
'• �a r.; l 111:'? it l.. Ciir{� T;,; rC!i
Division of Water Resources, Raleigh Regional Otiice, Water Quality Ope,atiom Section luip: pore tt,ncdenr.oryhveb/�cetaps
1628 Mail Service Cenicr, Raleigh, NC 27699-1628 Phone: [phone]
Location: 3800 Barren Drive, Raleigh, NC 27609 Fax: [phone]
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Kf-1
a
Water Resources
ENVIRONMENTAL. QUALITY
F
March 22, 2017
PETER. P. FLEETWOOD —PRESIDENT
BIo-NOMIC SERVICES, INC.
516 ROUNTREE ROAD -
CHARLOTTE, NORTH CAROLINA 28217
Dear Mr. Fleetwood:
ROY COOPER
Governor
MICHAEL S. REGAN.
Secretary
S. JAY ZIMMERMAN.
Director
Subject: Permit No. WQ0039053
Bio-Nomic Services DCAR
Distribution of Class A Water
Treatment Plant Residuals
Mecklenburg County
In accordance with your permit -application request received February 7 2017, we are forwarding
herewith Permit No. WQ0039053. dated March 22, 2017, to Bio-Nomic Services, Inc. for the operation of
the subject residuals management program.
This permit shall be effective from the date of issuance until February 28, 2022, and shall be subject .
to the conditions and limitations as specified therein. Please pay particular attention to ,the .monitoring
requirements listed in Attachment A. Failure to establish an adequate system for collecting and maintaining
the required operational information shall result in future compliance problems.
If any parts, requirements or limitations contained- in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with -the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be -final and binding.
If you need additional information concerning this permit, please contact Troy Doby at .(919)
8076336 or tro- .doby-(&ncdenr.gov.
Sincerely,
S. Jay Zimmerman, P.G.; Director
Division of Water Resources
cc: Chatham County Health.Department:(Electronic Copy)
Durham County Health Department (Electronic Copy)
Raleigh Regional Office, Water Quality Regional Operations Section (Electronic Copy)
- := -- clothing Compzires _.,,...
State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non -Discharge Permitting
1617 Mail. Service Center I Raleigh,.North Carolina 27699-1617
919-807-6332

Mr. Peter P. Fleetwood
March 22, 2017
Page 2 of 2
Mooresville Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Martin Mabe, Rob Wilcox_- Wilcox & Mabe Soil Solutions (Electronic Copy)
Beth Buffington — Protection and Enforcement Branch (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files

NORTH CAROLINA
Lt �]�U 1�►(I II:� 1�►�'%\►`/_�11—�11� i �1►Y 1[K��t� f(.X�i]�I
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
DISTRIBUTION OF CLASS A WATER TREATMENT PLANT RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, *and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Bio-Nomic Services, Inc.
Mecklenburg County
FOR THE
operation of a residuals management program for Bio-Nomic Services, Inc. and consisting of the
distribution of Class A Water Treatment Plant residuals generated by the approved facilities listed in
Attachment A with no discharge of wastes to surface waters, pursuant to the application received February
7, 2017, and in conformity with other supporting data subsequently filed and approved by the Department
of Environmental Quality and considered a part of this permit. The use and disposal of residuals are
regulated under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Permittee
from complying with the federal regulations.
This permit shall be effective from the date of issuance until February 28, 2022, and shall be subject to the
following specified conditions and limitations:
I. SCHEDULES
No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application.
[15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109]
II. PERFORMANCE STANDARDS
The subject residuals management program shall be effectively maintained and operated at all times so
there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distribution of residuals, contact the Raleigh Regional Office supervisor, and take any immediate
corrective actions. [G.S. 143-215.1]
2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02B .0200,
02L .0100]
WQ0039053 Version 1.0 Shell Version 160210 Page 1 of 9

3. Only residuals generated by the facilities listed in Attachment A are approved for distribution in
accordance with this permit. [G.S. 143-215.1]
4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed
the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(milligrams per kilogram)
Monthly Average
Concentration
(milligrams per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[ 15A NCAC 02T .1105]
5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T
.1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC
02T .1106]
6. Setbacks for Class A land applied bulk residuals shall be as follows:
Setback by residual type
Setback Description
(feet)
Liquid
Cake'
Private or public water supply
100
100
Surface waters (streams — intermittent and perennial,
100
25
perennial waterbodies, and wetlands
Surface water diversions (ephemeral streams,
25
0
waterways, ditches)
Groundwater lowering ditches (where the bottom of
25
0
the ditch intersects the SHWT)
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported and
spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast spreader or
other equipment designed for handling solid materials) without leaving any significant liquid
fraction behind.
[15A NCAC 02T .1108]
WQ0039053 Version 1.0 Shell Version 160210 Page 2 of 9

7. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance
of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen
requirements based on the determined Realistic Yield Expectations (RYE) using any of the following
methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (http://nutrients.soil.ncsu.edu/yields/index.phQ). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter 1
(http://www.ncagr.gov/SWC/tech/documents/9th Guidance Doc 100109.pdf).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA NRCS 590 Nutrient Management
Standards(ftp:/±p-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590_pdf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[ 15A NCAC 02T . 1109(b)(1)(k)]
The Permittee shall not distribute Class A Water Treatment Plant residuals that have a sodium
adsorption ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may
seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high
SAR content; has agreed on proper residual application rates; and has agreed to operational
considerations to ensure that the high SAR content will not adversely impact the receiving sites.
Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a
mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained
from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services,
the Natural Resource Conservation Service, allorth Carolina Licensed Soil Scientist, or an agronomist.
[15ANCAC 02T .0108(b)(1)]
WQ0039053 Version 1.0 Shell Version 160210 Page 3 of 9

III. OPERATION AND MAINTENANCE REQUIREMENTS
The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards. [15A NCAC 02T .l 110]
2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications
to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan,
at the minimum, shall include:
a. Operational functions;
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
notification requirements under the monitoring and reporting section of the permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen reduction requirements (e.g. facilities that dispose multiple times per year but
have an annual sampling frequency, may need to sample during winter months when pathogen
reduction is most likely to be negatively affected by cold temperatures).
[15A NCAC 02T .1100]
3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in responsible
charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC
08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204,
or as specified in the most recently approved O&M plan (i.e., see Condition 111.2.), and shall comply
with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources' Protection and Enforcement
Branch.at [phone]. At the time of this permit issuance, a certified ORC is not required for the
subject Distribution of Class A Residuals program. [15A NCAC 02T .0117]
4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be
maintained at the land application sites during land application activities. [15A NCAC 02T
.0108(b)(1)]
5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles. [15A NCAC 02T .1110]
WQ0039053 Version 1.0 Shell Version 160210 Page 4 of 9

6. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G.S. 143-215.1]
7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land
application sites onto which residuals are applied, or application shall be in accordance with the crop
management plan outlined by the local Cooperative Extension Office, the Department of Agriculture
and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved
by the Division. [15A NCAC 02T .1109(b)(1)]
8. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
residuals would occur;
e. Within the ] 00-year flood elevation, unless the bulk residuals are injected or incorporated within a
24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18% for injected or incorporated bulk liquid residuals;
h. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in a
USDA no -till program shall be exempted from meeting this vegetative cover requirement;
i. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
j. If the vertical separation of bedrock and the depth of residuals application is less than one foot;
k.. Application exceeds agronomic rates.
[15A NCAC 02T. 1109]
9. The Permittee shall notify all third -party entities receiving bulk distributed Class A Water Treatment
Plant residuals that land application activities occurring on the third -parry's property shall meet the
requirements in 15A NCAC 02T .1108(b)(1) and 02T .1109(b) (i.e., Conditions I1.8. and 111.8.,
respectively). [15A NCAC 02T .1103(5)]
10. All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may
be placed on a concrete pad, placed under shelter or physically covered until it is distributed to a third -
party entity. If bulk residuals are to be applied, the residuals may be staged at the application site for
up to 30 days for biological residuals, and 60 days for non -biological residuals. If an alternate storage
site is used, approval must be obtained from the Division. [15A NCAC 02T .0108(b)(1)]
WQ0039053 Version 1.0 Shell Version 160210 Page 5 of 9

11. A label shall be affixed to the bag or other container in which residuals are sold or given away for land
application, or an information sheet shall be provided to the person who receives Class A residuals. At
a minimum, the label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet;
c. A statement identifying that this material shall be prevented from entering any public or private
water supply source (including wells) and any surface water (e.g., stream, lake; river, wetland, etc.);
d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[I 5A NCAC 02T .1109(a)]
12. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals
contrary to the conditions of this permit. The Permittee shall report to the Raleigh Regional Office as
per reporting conditions under Condition N.S. any person or entity known.to be applying residuals
contrary to the condition of this permit. [ 15A NCAC 02T .1103 (a)]
IV. MONITORING AND REPORTING REOUIREMENTS
1. Any Division -required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)]
2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40
CFR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability,
reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed at the
frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of
five years. Any exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1;4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene 100.0
( )
Heptachlor (and its hydroxide)
(0.008)
Toxaphene (0.5)
Chloroform (6.0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
WQ0039053 Version 1.0 Shell Version 160210 Page 6 of 9

Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15A NCAC 13A .0102(b), 02T .1101, 02T .1105]
3. An analysis shall be conducted on the Class A residuals at the frequency specified in Attachment A,
and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the
following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate=Nih•ite Nitrogen
Sodium Adsorption Ratio(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[I 5A NCAC 02T .1101 ]
4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency
specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the
approved O&M plan. The required data shall be specific to the stabilization process utilized, and
sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC
02T .1106 (a) and (b)(2) shall be met. Any exceptions from the requirements in this condition shall be
specified in Attachment A. [ 15A NCAC 02T .1106, 02T .1107, 02T .1111(c)]
5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be
in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B .0505]
6. The Permittee shall maintain records tracking all bulk residual distribution or land application events
performed by the Permittee. At a minimum, these records shall include the following:
a. Source of residuals;
b. Date of distribution/land application;
c. Name and address of recipient of residuals;
d. Volume of residuals distributed to each recipient;
e. Intended use of residuals;
f. If land application events performed by the Permittee - Nitrogen Application Rate based on RYEs
(if using data obtained from the North Carolina State University Department of Soil Science
Website, the printout page shall be kept on file and reprinted every five years).
[I 5A NCAC 02T .0109(a)]
WQ0039053 Version 1.0 Shell Version 160210 Page 7 of 9

7. Three copies of an annual report shall be submitted on or before March I". The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms.
Instructions for reporting and annual report forms are available at
http://portal.ncdenr.orWweb/M/Us/lau/reportina, or can be obtained by contacting the Land
Application Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[ 15A NCAC 02T . I I I I (a)]
8. Noncompliance Notification
The Permittee shall report by telephone to the Raleigh Regional Office, telephone number (919) 791-
4200, as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following:
a. Distribution of residuals abnormal in quantity or characteristic.
b. Any failure of the distribution program resulting in a release of material to surface waters.
c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone].Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b)(1)]
V. INSPECTIONS
1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T .0108(b)]
2. Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals
storage, transport and distribution facilities to identify malfunctions, facility deterioration and operator
errors that could result in discharges to the environment, a threat to human health or a public nuisance.
The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of
inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee
shall maintain this inspection log for a period of five years from the date of inspection, and this log
shall be made available to the Division upon request. [15A NCAC 02T .0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the land application sites or facilities permitted herein
at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy
any records required to be maintained under the terms and conditions of this permit; and may collect
groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)]
WQ0039053 Version 1.0 Shell Version 160210 Page 8 of 9

VI. GENERAL. CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to
143-215.6C. [G.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals distribution events are not carried out in accordance
with the conditions of this permit. [15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the permit
application and other supporting documentation. [G.S. 143-215.11
The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in
15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and
under the Division's General Permit NCGO 10000; any requirements pertaining to wetlands under 15A
NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [ 15A NCAC 02T .0105(c)(6)]
In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [ 15A NCAC 02T .0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b).
[I 5A NCAC 02T, 0 120]
8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T
.0105(e)(3)]
Permit issued this the 2211 day of March 2017
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
Jay Zimmerman, P.G., Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0039053
WQ0039053 Version 1.0 Shell Version 160210 Page 9 of 9

THIS PAGE BLANK

ATTACHMENT A - Approved Residual Sources
Dio-Nomic Services, Inc.
Certification Date: March 22, 2017
Permit Number: WQ0039053 Version: 1.0
Maximum
Monitoring
Monitoring
Monitoring
Frequency ffor
Approved
Owner
Facility Name
County
Permit
Biological
Dry Tons
Frequency for
for Frequency
Freqy
Pathogen &
Mineralization
Number
Residuals
Per Year r
Non -hazardous
Metals and
Vector Attraction
Rate
Characteristics 2
Nutrients' s
Reductions d, e, 6
City of Durham
Williams WTP
Durham
03-32-010(B)
No
4,000
Annually
See Table Below
None 6
-
Chatham County
Chatham County WTP
Chatham
NCO084093
No
500
Once per Permit
See Table Below
None 6
Cycle
Total
4,500
1. Maximum Dry Tons per Year is the amount of residuals approved for distribution from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2.
3. Testing of metals and nutrients as stipulated under permit Condition IV.3.
4_ Analyses of pathogen reductions as stipulated under permit Condition IVA.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Distributed
short tons per ear(Established
Monitoring Frequency
in 40 CFR 503 and 15A NCAC 02T .1111
<319
1/Year
=>319 - <1,650
l/ Quarter (4 times per year)
=>1,650 - <16,500
1/60 Days 6 times per year
=>16,500
1/month (12 times per year)
6. Class A Water Treatment Plant residuals are exempt from meeting the pathogen & vector attraction reduction requirements in Condition IVA., provided they are not mixed with residuals that have
been generated during the treatment of domestic wastewater, the treatment of animal processing wastewater, or the biological treatment of industrial wastewater. The Class A Water Treatment
Plant residuals must be treated and processed in a manner as to not meet the definition of "Biological Residuals" as defined in 15A NCAC 02T .1102(6).
If no distribution events occur during a required sampling period (e.g. no distribution occur during an entire year when annual monitoring is required), then no sampling
data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to
EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification.
WQ0039053 Version 1.0 Attachment A Page 1 of 1

2019 ANNUAL REPORT
LAND APPLICATION PROGRAM
BIO-NOMIC SERVICES, INC.
PERMIT #WQ0039053
RECEIVEIYNCDENRAWR
FEB 10 2020
WQROS
MOOR E�slhnE ,REa'am'-iuDI FF. .
�I -.nNC,DE-()l
*C10111
3 AN '2 9
perm► trig U9►
�c:r1= F
JA N 2 9 2020
�S VJR. J�v i I0N
Prepared For: 1� +FORpjiATION PROCESSING UNIT
Bio-Nomic Services
530 Woodlawn St
Belmont, NC 28012
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
January 2020

Willcox&mate
SOIL SOLUTIONS
January 28, 2020
NCDEQ-DWR Non -Discharge Branch
512 North Salisbury Street
9"' Floor, Office #942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitfing Unit
Reference: 2019 LAND APPLICATION ANNUAL REPORT
1f Bio-Nomic Services, Inc.
Permit No. WQ0039053
WMSS Project No. 15-18 Ph: 09
Non -Discharge Permitting Unit:
RECEIVEOINCDF-MRIDWR
FEB 10 2020
WQROS
` OORESVILLE REGIONAL OFFICE
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Bio-Nomic Services,
Inc. (Bio-Nomics) for the above referenced permit. WMSS compiled this report using data
gathered during the compliance year by Bio-Nomics. This data includes: 1) Class A Annual
Distribution and Marketing / Surface Disposal Certification and Summary Form(s)
(DMSDF), 2) Annual Residual Sampling Summary Form(s) (ARSS), 3) Annual Pathogen
and Vector Attraction Reduction Form (2T), and 4) Analytical Data.
Bio-Nomics distributed a total of 3,645.52 Dry Tons of residual solids during the 2019
calendar year.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact the Bio-Nomic Services, Inc. or WMSS for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosures
Shared\WMSS Projects\2015\15-18 Bio-Nomics\Phase 09 - Class A Permit\2018 Annual Report\2018 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, NC 27358 / Rob 336.339.9128 or Martin
336.312.1396/www.\ illcoxmabesoil.com

Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC .28012
NC PERMIT # WQ0039053
Vaughn "Buck" Stevenson, Vice President
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmond, NC 28012
2019 Greenville Utilities WTP (NC0082139) Dry Tons 1,356.3
2019 McCall Farms WWTP (WQ0003823) Dry Tons 2,289.22
2019 Total Dry Tons 3,645.52
Total Dry Metric Tons 3,306.49

TABLE OF CONTENTS
SECTION NO. TITLE
I DMSDF
H RSSF
III PVRF (2T)
IV Analytical Data

17J,RIofA

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039053 FACILITY NAME: Bio-Nomic Services, Inc.
PHONE: [phone] COUNTY: Gaston OPERATOR: Vaughn Stevenson - Vice President
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
C] Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes ENO [] —0� If No skip parts A, B, C and certify form below
Part A*
Part B*•
Month
Sources(s) (include NPDES # if
applicable)
Volume (drytons
Reci lent Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
Greenville Utilities WTP NCO082139
182.92
City of Greenville
182.92
Fertilizer
July
Greenville Utilities WTP NCO082139
233.67
City of Greenville
233.67
Fertilizer
August
Greenville Utilities WTP NCO082139
236.04
City of Greenville
236.04
Fertilizer
September
Greenville Utilities WTP NCO082139
223.35
City of Greenville
223.35
Fertilizer
October
Greenville Utilities WTP NCO082139
260.78
City of Greenville
260.78
Fertilizer
November
Greenville Utilities WTP NCO082139
137.87
City of Greenville
137.87
Fertilizer
December
Greenville Utilities WTP NCO082139
81.67
City of Greenville
81.67
Fertilizer
Total from FORM DMSDF (sup)
0
0
0
0
Totals: Annual (dry tons):
0
0
1356.3
................................
1356.3
....................
Amendment(s) used:
Bulking Agent(s) used:
* If mores ace is required, attach additional information sheets FORM DMSDF su Total Number of Form DMSDF Su 0
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit (including p Yes !:
but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No 10 If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached._,
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
V,/ -
Signature of Permittee
�- 4 2
Date Signature of Preparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039053 FACILITY NAME: Bio-Nomic Services, Inc.
PHONE: [phone] COUNTY: Gaston OPERATOR: Vaughn Stevenson - Vice President
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
p Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation durinE the past calendar near? Yes OVo ❑ ---► If No skip parts A, B, C and certify form below
Part A*•
Part B*•
Month
Sources(s) (include NPDES # if
applicable)
Volume (drytons
Reci lent Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
McCall Farms WWTP WQ0003823
752
752
City of Wilson
752
Fertilizer
May
McCall Farms WWTP WQ0003823
760
760
City of Wilson
760
Fertilizer
June
McCall Farms WWTP WQ0003823
777.22
777.22
City of Wilson
777.22
Fertilizer
Jul
August
September
October
November
December
Total from FORM DMSDF (sup)l
0
0
0
0
Totals: Annual (dry tons):
0
2289.22
2289.22
2289.22
......
Amendment(s) used: I
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Part C:
Total Number of Form DMSDF (Supp)l 0
Facility was compliant during the past calendar year with all conditions of the land application permit (including p Yes
but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Da e
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Permittee)
Date
wD
jr
DENR FORM DMSDF (12/2006)

RSSF

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or NPDES
WWTP Name:
Recidnal Analvsic nata
WQ0039053
Bio-Nomic Services, Inc.
NCO082139
Greenville Utilities WTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Cone. Limit
m k a
Sample or Composite Date ---
----
5/6/19
5/6/19
7/10/19
8/28/19
10/7/19
12/11/19
Percent Solids (%)
8.84
9.23
20
39.4
19.6
16.5
Arsenic
9.06
11.1
11.3
9.31
25.5
16.4
Cadmium
1
1
1
1
1 5.1
0.606
Copper
247
293
353
127
391
368
Lead
15.7
15.1
19.2
20.7
20.5
23.4
Mercury
0.304
0.439
0.252
0.117
0.561
0.51
Molybdenum
2.5
2.5
2.5
2.5
12.8
1.96
Nickel
9.41
11.4
13.3
38.1
1 13.8
12.4
Selenium
5
5
5
5
25.5
4.19
Zinc
53.1
55.5
61.6
50.2
70.9
61.8
TKN
_
11100
7390
100
46900
100
5130
305
12300
510
16200
606
Ammonia- N�+Y^��- 100
4.76
2090
n limits listed in this form are not annlicable.
4.7
5
4.56
25
30.3
2290
2390
1840
2910
3160
Reference the individual
hermit
for metals limits.
mment was prepared under my direction or supervision in accordance with a system designed to assure
nd evaluated the information submitted. I am aware that there are significant penalties for submitting
r fines and impriso ent for knowing violations."
Z� 1117 4/Lo
Date
CAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analvsis Data
WQ0039053
Bio-Nomic Services, Inc.
WQ0003823
McCall Farms WWTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Cone.
Limit
(mg/kg)'
Sample or Composite Date
02/20/19
2/20/19
4/1/19
4/1/19
4/1/19.
4/1/19
Percent Solids (%)
NA
32.1
42.5
43.1
44.8
32.1
45.8
Arsenic
75
5.00
5.00
5.00
5.00
5.00
5.00
Cadmium
85
1.00
1.00
1.00
1.00
1.00
1.00
Copper
4,300
95.70
71.70
50.50
54.10
70.70
50.50
Chromium
NA
182.00
161.00
124.00
120.00
125.00
122.00
Lead
840
23.90
20.30
15.20
16.20
19.60
15.40
Mercury
57
0.04
0.06
0.05
0.06
0.04
0.05
Molybdenum
75
2.74
2.50
2.50
2.50
2.50
2.50
Nickel
420
75.30
67.50
50.00
48.70
50.90
49.60
Selenium
100
5.00
5.00
5.00
5.00
1 5.00
5.00
Zinc
7,500
356
271
189
196
263
184
Total Phosphorus
NA
3,060
2,400
1,740
1,690
2,210
1,620
TKN
NA
17,400
9,980
11,000
12,200
17,000
13,300
Ammonia -Nitrogen
NA
2,430
1,530
696
1,580
1,180
1,200
Nitrate and Nitrite
NA
84
13
309
36
137
18
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties
for submitting false information, including the possibility of fines and imprisonment for knowing violations."
l zY 20
Signature of Preparer bate
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
WQ0039053
Bio-Nomic Services, Inc.
WQ0003823
McCall Farms WWTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter(mg/kg)--
Sampleor • •• Date
•11
11
•11
11
11
• 11
----_
• • 11
1 1
1 11
11
• 1 1
� 111
___--
'•
1
•11
' 1
:•1
1
1 1----
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fnes and imprisonment for knowing violations."
.7z ( �
Signature of Preparer * ate
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006)

PVRF 2T

Greenville Utilities WTP is not required by permit to perform Pathogen Reduction or Vector Attraction
Reduction Monitoring, therefore no PVRF 2T Form has been included in this report.
McCall Farms WWTP falls into the bi-monthly (or 6 times per year) sampling frequency. This project
was performed in accordance with a lagoon closure plan in order to close out all lagoons at the facility.
The residual solids were removed from the lagoons, co -mingled, and stockpiled on site prior to land
application activities beginning. The project only lasted for approximately three months. Therefore all
six pathogen reduction samples (six sets of 7 fecal coliform samples) were collected during the three
month window of actual land application activities from the stockpiles to best represent the actual
material being land applied. On the attached PVRF 2T forms the monitoring period is listed as the
actual date of each set of 7 fecal coliform samples and was not listed as a time period such as January 1,
2019 through February 28, 2019. This approach is the best representation of the actual analytical data
collected.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc. WQ Permit Number: WQ0039053
WWTP Name: McCall Farms WWTP NPDES Number: WQ0003823
Monitoring Period: From 2/26/2019 To
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test)
T Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ElGamma
Ray ElPasteurization
Class B:
JAIL (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
I Composting ❑
lAerobic Digestion ❑
Anaerobic Digestion
estion
_...... .._.................. ... .._...............
If applicable to alternative performed (Class A or Class B) complete the following monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g tY
Number o
Excee-
Excee-
Frequency
of Analysis
Sample
'Type
Analytical
Tech-nique
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
41
49
77
MPN/g
0
6 x Year
Grab
SM 9221 c
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
0
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
l] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met.one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn 'Buck" Stevenson, Vice President
Preparer Name and Title (type or print)
Signature of Preparer* D to
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
......................................
............................
..................
02/26/19
42
1.6232
02/26/19
41
1.6128
02/26/19
48
1.6812
02/26/19
59
1.7709
02/26/19
41
1.6128
02/26/19
77
1.8865
02/26/19
42
1.6232
Total 11.8107
Average 1.6872
Geometric Mean 4i€€€€ Fecal Coliform MPN /gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results
Bio-Nomic Service, INC
530 Woodlawn Street
Belmont, NC 28012
Receive Date: 02/26/2019
Reported: 03/15/2019
For: McCall Farms Group #2
Comments:
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190226-15-01
Fecal Coliforms
MF2-1
<42
MPN/g
SM92210E-2006
02/26/2019
WC
190226-15-01
Percent Solids
MF2-1
47.3
%
SM2540B-2011
02/26/2019
WC
190226-15-02
Fecal Coliforms
MF2-2
<41
MPN/g
SM92210E-2006
02/26/2019
WC
190226-15-02
Percent Solids
M172-2
49
%
SM254OB-2011
02/26/2019
WC
190226-15-03
Fecal Coliforms
MF2-3
<48
MPN/g
SM92210E-2006
02/26/2019
WC
190226-15-03
Percent Solids
MF2-3
42
%
SM254OB-2011
02/26/2019
WC
190226-15-04
Fecal Coliforms
MF2-4
<59
MPN/g
SM92210E-2006
02/26/2019
WC
190226-15-04
Percent Solids
MF2-4
34
%
sM254OB-2011
02/26/2019
WC
190226-15-05
Fecal Coliforms
MF2-5
<41
MPN/g
SM92210E-2006
02/26/2019
WC
190226-15-05
Percent Solids
MF2-5
49
%
SM254OB-2011
02/26/2019
WC
190226-15-06
Fecal Coliforms
MF2-6
<77
MPN/g
SM92210E-2006
02/26/2019
WC
190226-15-06
Percent Solids
MF2-6
26
%
SM2540B-2011
02/26/2019
WC
190226-15-07
Fecal Coliforms
MF2-7
<42
MPN/g
SM92210E-2006
02/26/2019
WC
190226-15-07
Percent Solids
MF2-7
47.4
%
SM2540B-2011
02/26/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190226-15-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-06 Temp on Arrival: 3.2
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-15-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Me.Wl Fauns 5arKPL Oro'ep=#-L fA F=Akf(,,li r?rm.S
Clienh ��,� NC�Mt �
STAUSVILLE ANALYTICAL
Add ress: �( O "aej S+
122 Court Street • P.O. Box 228
nn M / tZ.
IDe yrtOh.� C.
Statesville, NC 28687
(704)R72-0697
97
Chain of
Custody Record
Contact Person: A i a pr Phone q 704 _10 7-y 3 7 3 • FAX#
PO # lit 750 ! Requisitioned by: (Time Date)
1
custorner
Semple INLatYID
n
TimeSemplod /^�
(Grab Only) J'�
DaleSamplau
(Grab Only)
Matrix
s", W �v
Parameters rcqueatcd for analysis
Fe oas 5 ..
2
oz
s: Z 5
01
6
5.36
Relinquished by:
Time % YS am, pm Date LJ!L4J'!2
Sampled by:
Received by:
1�
Time 09[�/S am pm DateZ ��'
Transported by:
Relinquished by:
Time am, pm Date _/�_
Holding times met:
Received by:
Time am, pm Date —I_1_
Compliance work:
Composite Sampling 1#1:
Time begin am, pm Date _J_I—
Non-compliance work:
Time end am, pm Date ___f_/
Lab Comments: Samples Transported On Ice:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date /_J _ _
Initials:
n
00
W
00
N
U
Z
ci
i+
N
00
N
N
X
O
00
a

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc.
WWTP Name: McCall Farms WWTP
Monitoring Period: From 2/26/2019 To
WQ Permit Number:
NPDES Number:
WQ0039053
WQ0003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ I
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
AIt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermoplulic ❑
Beta Ray El
Y
Ray
Gamma RY ❑
aste ization
P ur ❑
Class B:
jAlt. (1)Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ®
Air Drying ❑
Composting
lAerobic Digestion ❑
estio n ❑
Anaerobic Digestion
..........................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech-ni ue
q
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
WN
CFU
1000 mpn per gram
of total solid (dry
weight)
32
47
77
MPN/g
0
6 x Year
Grab
SM 9221 c
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed:
Alt.l (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
El
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified .personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn 'Buck" Stevenson, Vice President
Preparer Name and 'tle (type or print) 11AX
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
-- . *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
...........
...................................................
'IteFeciliri.i
.............................
N 'eraz'
02/26/19
38
1.5798
02/26/19
54
1.7324
02/26/19
41
1.6128
02/26/19
32
1.5051
02/26/19
77
1.8865
02/26/19
1 38.5
1 1.5855
02/26/19
1 67
1 1.8261
Total 1 11:7281
Average 1 1.6754
Geometric Mean I Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results STATESVILLE
ANALYTICAL
Bio-Nomic Service, INC ;
530 Woodlawn Street
Belmont, NC 28012
Receive Date: 02/26/2019
Reported: 03/15/2019
For: McCall Farms Group #1
Comments:
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
190226-16-01
Fecal Coliforms
MF-1-1
<38
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-01
Percent Solids
MF-1-1
53
%
SM2540B-2011
02/26/2019
WC
190226-16-02
Fecal Coliforms
MF1-2
<54
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-02
Percent Solids
MF1-2
37.3
%
SM2540B-2011
02/26/2019
WC
190226-16-03
Fecal Coliforms
MF1-3
<41
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-03
Percent Solids
MF1-3
49
%
SM254OB-2011
02/26/2019
WC
190226-16-04
Fecal Coliforms
MF1 4
<32
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-04
Percent Solids
MF1 4
62.3
%
SM2540B-2011
02/26/2019
WC
190226-16-05
Fecal Coliforms
MF1-5
<77
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-05
Percent Solids
MF1-5
26
%
SM2540B-2011
02/26/2019
WC
190226-16-06
Fecal Coliforms
MF1-6
<38.5
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-06
Percent Solids
MF1-6
52
%
SM25406-2011
02/26/2019
WC
190226-16-07
Fecal Coliforms
MF1-7
<67
MPN/g
SM92210E-2006
02/26/2019
WC
190226-16-07
Percent Solids
MF1-7
30
%
SM2540B-2011
02/26/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190226-16-01
Temp on Arrival: 3.3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190226-16-02
Temp on Arrival: 3.3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190226-16-03
Temp on Arrival: 3.3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190226-16-04
Temp on Arrival: 3.3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190226-16-05
Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-16-06 Temp on Arrival: 3.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190226-16-07 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

M�- = M1,C,all FlrMS
Client: j 0- N r t
STA'[ESVILLE A IYALY77CAL
Address:
530 1 54
122 coon swot • P.O. Box 228
� wit
Statesville,lc, NC 28687
(704)872469797
.,(—
o,I l N L Z �Q Z
Contact Person: /t r Tay �Dr,
t
Phone #704_4a7- 7ela FAX#
Chain of
Custody Record
PO # Lt. g eo Requisitioned by: tTma Date)
7
Customer
ON
Lab -II) fJ
Time Sa"Plod /�
(Grab Only) >
Oale Sampled
(Grab Only)
Matrix
siwp w
p�mners requested for analysisSample
i
1 � .lI.QOI
5� n �
Z/Z6 Y
G Fey a L. ass t
Z
02
3
0
00
S.n7
5
0
S:Oy
6
S it
7
07-
5 : i
Relinquished by:
Time y5 am, pm Date 2. J?4/ff Sampled by:
Received by: AOO,—
TimeMOYT/aq pm Date 2> I--'i� Transported by:
Relinquished by:
Time am, pm Date —1—j— Holding times met:
Received by:
Time am, pm Date _/ /—
Compliance work:
Composite Sampling #1:
Time begin am, pm Date _! /
Non-compliance work:
Time end am, pm Date `/_/_
Lab Comments: Samples Transported On Ice:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date �_/_
Inldels:
r,
tb
LD
tb
N
U
Z
v
N
ice+
r0
Y
N
00
N
N
X
O
m
0

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc. WQ Permit Number: WQ0039053
WWTP Name: McCall Farms WWTP
Monitoring Period: From
3/4/2019 To
NPDES Number: WQ0003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta RayGamma
❑
Ray ❑
Y
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
I Composting ❑
jAerobic Digestion ❑
Anaerobic
aerob Digestion estion
g
........................................................................................................................................... .
If applicable to alternative performed (Class A or Class B) complete the following monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g Ty
Number o
Excee-
I dences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
NWN
CFU
1000 mpn per gram
of total solid (dry
weight)
37
46
61
MPN/g
0
6 x Year
Grab
SM 9221 c
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn "Buck" Stevenson, Vice President
Preparer Na e and Title (type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
........................................................
I to
............................
Fec oli of
..........................
.°
.................
03/04/19
48
1.6812
03/04/19
51.3
1.7101
03/04/19
43
1.6335
03/04/19
39
1.5911
03/04/19
44.2
1.6454
03/04/19
61
1.7853
03/04/19
37
1.5682
Total 1 11.6148
Average 1 1.6593
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results
Bio-Nomic Service, INC
530 Woodlawn Street
Belmont, NC 28012
Receive Date: 03/04/2019
Reported: 03/15/2019
For: McCall Farms Sample #3
Comments: Geometric Mean <46 MPN/g
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190304-12-01
Fecal Coliforms
1
<48
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-01
Percent Solids
1
42
%
SM2540B-2011
03/04/2019
WC
190304-12-02
Fecal Coliforms
2
<51.3
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-02
Percent Solids
2
39
%
SM2540B-2011
03/04/2019
WC
190304-12-03
Fecal Coliforms
3
<43
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-03
Percent Solids
3
47
%
SM254OB-2011
03/04/2019
WC
190304-12-04
Fecal Coliforms
4
<39
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-04
Percent Solids
4
51.4
%
SM254OB-2011
03/04/2019
WC
190304-12-05
Fecal Coliforms
5
<44.2
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-05
Percent Solids
5
45.2
%
SM2540B-2011
03/04/2019
WC
190304-12-06
Fecal Coliforms
6
<61
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-06
Percent Solids
6
33
%
SM2540B-2011
03/04/2019
WC
190304-12-07
Fecal Coliforms
7
<37
MPN/g
SM92210E-2006
03/04/2019
WC
190304-12-07
Percent Solids
7
54
%
sM254OB-2011
03/04/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190304-12-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-06 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-12-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

a i,; l &runs 54,ao% # :� (.Mr)
Client: p
STATESVILLEANALYTICAL
Address: 5 3 0 1 1�c ! f k� r} 5
l.� of ll T
122 Court Street P.O. Box 228
Statesville, NC 28687
v1MG�I ti L Z �� 1 Z
�..
(704) 8724697
Contact Person: r` u s 1 eve 't sir Phone # 1c�4 _ PAxN 71) Lf_ S ZY _ fb 4
t ll
Chain of
IMMM Custody Record
PO H 1 3 Z— Requisitioned by: (Time Dale)
Cuslomor
Sample IDA
_
Lab -ID 0@
Time Sampled
(Grob Only)
Date Sampled
(Grab 0 ly)
Matrix
swaw W ww
Pwemercrx«quesred for ¢n¢lysia
4.30
3
031
4 '• .�
r.t
0.qD
_
5Q5ti
11
(,
K '3
Relinquished by:
Time /0 jl; sn am, pm Date 3 /---LL
Sampled by:
Received by: e '
Time _��m, pm Date _l l
Transported by:
Relinquished by:
Time am, pm Date .—./_/
Holding times met:
Received by:
Time am, pm Date _/_/
Compliance work:
COMROsite Sam I�Ing##1:
Time begin am, pm Date _/�_
Non-compliance work:
Time end am, pm Date _/�_
Lab Comments: Samples Transported On Ice:
Composite So p-ling #2;
Time begin am, pm Date J_/
Time end am, pm Date _I^I
Inilfels:
N
00
lD
00
N
U
Z
dJ
41
to
V)
00
N
N
X
0
co

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc. WQ Permit Number: WQ0039053
WWTP Name: McCall Farms WWTP
Monitoring Period: From 3/4/2019 To
NPDES Number: WQ0003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (tune/temp) ❑
Alt B (Alk Treatment) ❑ TAlt.
C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thernioplulic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑ .
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
I Composting ❑
jAerobic Digestion ❑
Digestion ❑
........................................................::..
..................................................................................... .
.....:: . ... ::::Anaerobic
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech-ni ue
q
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
38
50
74
MPN/g
0
6 x Year
Grab
sM 9221 c
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑Alt.
4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
0
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn 'Buck" Stevenson, Vice President
Preparer Na e and Title (type or print).
Signature of Preparer* D to
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
........................................................
g.............
03/04/19
55
1.7404
03/04/19
49
1.6902
03/04/19
51
1.7076
03/04/19
74
1.8692
03/04/19
38
1.5798
03/04/19
45
1.6532
03/04/19
42
1.6232
Total 1 11.8636
Average 1.6948
Geometric Mean Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results
Bio-Nomic Service, INC
530 Woodlawn Street
Belmont, NC 28012
Receive Date: 03/04/2019
Reported: 03/15/2019
For: McCall Farms Sample #4
Comments: Geometric Mean <50 MPN/g
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190304-13-01
Fecal Coliforms
1
<55
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-01
Percent Solids
1
36.3
%
SM2540B-2011
03/04/2019
WC
190304-13-02
Fecal Coliforms
2
<49
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-02
Percent Solids
2
41
%
SM2540B-2011
03/04/2019
WC
190304-13-03
Fecal Coliforms
3
<51
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-03
Percent Solids
3
39
%
SM25QB-2011
03/04/2019
WC
190304-13-04
Fecal Coliforms
4
<74
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-04
Percent Solids
4
27
%
SM25QB-2011
03/04/2019
WC
190304-13-05
Fecal Coliforms
5
<38
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-05
Percent Solids
5
53
%
SM254OB-2011
03/04/2019
WC
190304-13-06
Fecal Coliforms
6
<45
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-06
Percent Solids
6
44
%
SM254OB-2011
03/04/2019
WC
190304-13-07
Fecal Coliforms
7
<42
MPN/g
SM92210E-2006
03/04/2019
WC
190304-13-07
Percent Solids
7
48
%
SM254OB-2011
03/04/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190304-13-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4
I
I

Parameter Schedule: Fecal Coliforms
I
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-06 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190304-13-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

/A, Lac! -Ful'rfi4-�Qikhie5 4-w /Mr)
Client; � N ,
0 1 - S of u tk e Ge ,j
S ANSVILLEANALYTICAL
Address: [ JD r lD� ! J� /(
122 Court ShCCt - P.O. Box 228
Statesville, NC 28687
(704) 8724697
Contact Person: V ,1 evetSem /'ri-5�'-WrO 70q-5L l P Phone �, e! FAX#. y
Chain Of
Custody Record
PO # L, `45 3 1 Requisitioned by: Crime Date)
t
Customer
Sample ION
Lab -ID M
Tlrtre SampleU /� p
(Grab Only) AM
Date Samplod
(Grab Only)
Matrix
swyp w w.v
Parametcrs rdtuesta for 0e31yS15
L F
4 C (wss B
z-
02
5
d
5: io
Relinquished by:
Time /C,' yQA am, pm Date /ftj q
Sampled by: ��
Received by: /
rr/`
Time I D YCam, pm Date
_
Transported
by:
Relinquished by:
Time am, pm Date �_/
Holding times met:�Wz
Received by:
Time am, pm Date �_/
Compliance work:
Composite Sampling #1:
Time begin am, pm Date _/�,
Non-compliance work:
Time end am, pm Date _I /_
Composite Sampling #2:
Lab Comments: Samples Transported On Ice:
Time begin am, pm Date
Time end am, pm Date
InlBals:
rn
LID
1�t "t
N O
00
'ztC
0 Co
n
00
LID
tb
N
U
Z
ai
V1
en
CU
•
lb
N
N
X
O
00
o_

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc.
WWTP Name: McCall Farms WWTP
Monitoring Period: From 3/5/2019 To
WQ Permit Number: WQ0039053
NPDES Number: WQ0003823
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (tune/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermoplulic ❑
Beta Ra Y ❑
Gamma Ra Y ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
1 Composting ❑
jAerobic Digestion ❑
Anaerobic Di es tion
g
............................................................................................................................................ .
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g Ty
Num er o
Excee-
dences
Frequency
of Analysis
Sample
'Type
Analytical
Tech-nique
Minimu
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
31
47
65
MPN/g
0
6 x Year
Grab
SM 9221 c
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
0
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn 'Buck" Stevenson, Vice President
Preparer Name and Title (type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
03/05/19
53
1.7243
03/05/19
33
1.5185
03/05/19
63
1.7993
03/05/19
45
1.6532
03/05/19
51.3
1.7101
03/05/19
31
1.4914
03/05/19
65
1.8129
Total 11.7097
Average 1.6728
Geometric Mean 4 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results
STATESVILLE
ANALYTICAL
Bio-Nomic service, INC
(to-~"�
530 Woodlawn Street
Belmont, NC 28012
Receive Date: 03/05/2019
Reported: 03/15/2019
For: McCall Farm
Comments: Geometric Mean: <47 MPN/g
Sample Number parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
190305-33-01 Fecal Coliforms
1
<53
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-01 Percent Solids
1
38
%
SM2540B-2011
03/05/2019
CL
190305-33-02 Fecal Coliforms
2
<33
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-02 Percent Solids
2
61.3
%
SM2540B-2011
03/05/2019
CL
190305-33-03 Fecal Coliforms
3
<63
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-03 Percent Solids
3
32
%
SM2540B-2011
03/05/2019
CL
190305-33-04 Fecal Coliforms
4
<45
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-04 Percent Solids
4
44
%
SM2540B-2011
03/05/2019
CL
190305-33-05 Fecal Coliforms
5
<51.3
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-05 Percent Solids
5
39
%
SM2540B-2011
03/05/2019
CL
190305-33-06 Fecal Coliforms
6
<31
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-06 Percent Solids
6
65
%
SM2540B-2011
03/05/2019
CL
190305-33-07 Fecal Coliforms
7
<65
MPN/g
SM92210E-2006
03/05/2019
CL
190305-33-07 Percent Solids
7
31
%
SM25408-2011
03/05/2019
CL
Respectfully submitted,
r�!' ' l✓Di� JT3)
Dena Myers
NC Cert #440,
NCDW Cert #37755,
—, EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190305-33-01 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-02 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-03 Temp on Arrival: 3.3
i
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-04 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-05 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-06 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190305-33-07 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

I" C,L/1 1 ' .. Ir, -�' r /vt I /
Client:
3
122 CourtStrcct 11.0. 13ux 228
Smtcsville, NC 29687
(7114) 872- 697
c, r
Address: 5 3G LI f. , (r I[ tti •v J� Ct t
V
Contact Person: �(t i
ur N't S 1C r", sya•i
Phone A
FAM
Chitin of
Custody Record
PO it <� �{ f . Requisitioned by: (Time Date)
Cuslomor
Sumplo to,
Lab -ID M
Time Sampled
(Grab Only)
p
/ 1 IA
Dale Sampled
(Grab Only)
sw,aa
Matrix
w
ww
Pommcrm myucsicd rer analysis
FL
02
0;
LI
; 1
--
— �J—
//o4
lG
-7 1 7
—
—
QlY
7 I 4�
0 q
7 z
I
Relinquished by: __>%
Time /� ,�9G9-Y
am, CID to ! 5 /
Sampled by: `/ S
Received by:
Time
am,jr Date
Transported by:
Relinquished by:
Time
am, pm Dale ,/_/_
Holding limes met:
Received by:
Time
am, pm Date —/_/_
Compliance work: V/
Composite Sam Ip ing #1:
Time begin am, pm Date _!—/—
Non-compliance work:
Time end am, pm Date _/—/_
Lab
Comments:
Samples Transported On Ico:
C_g posite Sampj g#22
Time begin am, pm Date
-ime end am, pm Date _/—/—
Initials:
r-
m
N O
00
� rn
o a
00
W
00
N
U
Z
t1J
v
N
N
X
O
on
O
d

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Bio-Nomic Services, Inc.
WWTP Name: McCall Farms WWTP
WQ0039053
WQ0003823
Monitoring Period: From 3/5/2019 To
Pathozen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
WQ Permit Number:
NPDES Number:
Class A:
Alt. A (time/temp) [IAlt
B (Alk Treatment) ❑
Alt. G (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermoplulic ❑
Beta Ra Y ❑
Gamma Ra Y ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAeroble Digestion ❑
Anaerobic Di estion Elg
.......................................................................................................................................... .
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number o
Excee-
deuces
Frequency
of Analysis
Sample
Type
Yp
Analytical
Tech-nique
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
27
32
36
MPN/g
0
6 x Year
Grab
SM 9221 c
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
0
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
[] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Vaughn 'Buck" Stevenson, Vice President
r Preparer
/Name and Title (type or print)
Signature of Preparer*
I Z j
Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

BIO-NOMIC SERVICES, INC.
WQ0039053
McCall Farms
......................................................
I fe
Fec bli o r
ti '
03/05/19
32
1.5051
03/05/19
27
1.4314
03/05/19
32
1.5051
03/05/19
36
1.5563
03/05/19
31
1.4914
03/05/19
34
1.5315
03/05/19
33
1.5185
Total 1 10.5393
Average 1.5056
Geometric Mean ii€i3 Fecal Coliform MPN / gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

0
Analytical Results STATESVILLE
��.-� AIeIALYTICAL
r
Bio-Nomic service, INC -
530 Woodlawn Street -'
Belmont, NC 28012
Receive Date: 03/05/2019
Reported: 03/15/2019
For:
Comments: Geometric Mean: <32 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190305-34-01
Fecal Coliforms
1
<32
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-01
Percent Solids
1
62
pro
SM2540B-2011
03/05/2019
CL
190305-34-02
Fecal Coliforms
2
<27
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-02
Percent Solids
2
74
pro
SM2540B-2011
03/05/2019
CL
190305-34-03
Fecal Coliforms
3
<32
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-03
Percent Solids
3
63
pro
SM2540B-2011
03/05/2019
CL
190305-34-04
Fecal Coliforms
4
<36
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-04
Percent Solids
4
55.3
pro
SM2540B-2011
03/05/2019
CL
190305-34-05
Fecal Coliforms
5
<31
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-05
Percent Solids
5
65
pro
SM2540B-2011
03/05/2019
CL
190305-34-06
Fecal Coliforms
6
<34
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-06
Percent Solids
6
59
%
SM2540B-2011
03/05/2019
CL
190305-34-07
Fecal Coliforms
7
<33
MPN/g
SM92210E-2006
03/05/2019
CL
190305-34-07
Percent Solids
7
61
%
SM2540B-2011
03/05/2019
CL
/Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190305-34-01 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190305-34-02
Temp on Arrival: 3.3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190305-34-03
Temp on Arrival: 3.3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190305-34-04
Temp on Arrival: 3.3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190305-34-05
Temp on Arrival: 3.3
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190305-34-06
Temp on Arrival: 3.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190305-34-07 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page,3 of 4

IV<- (_,.II
Client: n
—
STA77-SVILL@ANALYTICAI.
122 Court Strcet • P.O. [lox 228
Slmavillc, NC 28687
(70-1)872-1697
Address: C) l l/:
l 4 u..; j �'(c e.
Contact Person: Phone
�` <ua �t vi 5 ev� PI ,
.,
1) FAM
Chain of
Custody Record
PO M (1 �� Lf / _ Requisitioned by: (Tlma Date)
(
Customer
Sample IDtr
Lab-) M
Tin) Sampled
(Gmb Only)
/j N1
/ 1
Data Sumplud
(GrabOnly)
„
_
Matrix
I'mmou tinted fin :maly,is
soh^
w
ervr
}-
-�_
2
7 .7 17
-
-
-
Relinquished bar:—'
Time ),',,.2, am, dim Date / / ��
Sampled by: V
Received by:
Time ��'2_-6 am,Q Date
Transported by:
_I
Relinquished by:
Time am, pm Date
_/_/_
Holding times met:_
Received by:
Time am, pm Date
/
Composite Sampling #1:
_/_/_
Compliance work:
Time begin am, pm Date _/_/—
Non-compliance work:
Time end am, pm Dale
Composite Sampling #2:
Lab Comments: Samples Transported On Ice:
Time begin am, pm Date
Time end am, pm Date _/_/_
Initials:
r`
rn
N O
r- "r
00
It
o (L
n
00
LID
00
N
U
41
ai
tll
41

ANALYTICAL DATA

Greenville Utilities WTP is an ongoing dredge and dewatering project at the alum lagoon at the
respective plant. The project actually began in June of 2019. The sampling frequency is bi-monthly (or
6 times per year) which is determined by the amount of dry tons distributed in 2019. Six sets of nutrient
and metal analyses were performed during 2019 to satisfy the permit condition outlined in Attachment
A. One TCLP analysis has also been included.
McCall Farms WWTP falls into the bi-monthly (or 6 times per year) sampling frequency. This project
was performed in accordance with a lagoon closure plan in order to close out all lagoons at the facility.
The residual solids were removed from the lagoons and stockpiled on site prior to land application
activities beginning. The project only lasted for approximately three months. Therefore all six nutrient
and metal analyses were collected during the three month window of actual land application activities
from the stockpiles to best represent the actual material being land applied. One TCLP analysis has also
been included.

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: May 6, 2019
Greenville Utility Commision #1 Permit No. WQ0039053
8.84 % Solids
6.7 nH
Nitrogen (TKN)
1.110
11,100.000
22.200
Phosphorus
0.209
2,090.000
4.180
Potassium
0.037
368.000
0.736
PAN (injected)*
0.230
3,869.500
7.739
PAN (surface)*
0.225
3,777.000
7.554
Ammonia Nitrogen
0.010
100.000
0.200
Calcium
0.106
1,060.000
2.120
Calcium Carbonate E .
40.200
116,000.000
232.000
Magnesium
0.049
487.000
0.974
Sodium
0.025
250.000
0.500
Sulfur
---
4,830.000
9.660
Nitrate N / Nitrite N
---
4.760
0.010
Barium
---
--- ---
Chloride
---
537.000
1.074
Iron
---
31700.000
63.400 I Ce
Aluminum
---
117,000.00
234.000
Arsenic
---
9.06
0.018
Cadmium
---
1.000
0.002
Chromium
---
23.900
0.048
Copper
---
247.00
0.494
Lead
---
15.70
0.031
Mercury
---
0.3040
0.001
Molybdenum
---
2.50
0.005
Nickel
---
9.41
0.019
Selenium
---
5.00
0.010
Zinc
---
53.10
0.106
Waypoint Analytical 19-127-0214
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia
N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By: SO I L SO LUTI O N S
75
85
840
57
75
7

h
Waypoint I
ANALYTICAL
5/15/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-127-0214
Project Description: GUC #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/7/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P.,,,:• R° 6-7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

•
W, ��� ' �t 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-127-0214
Client Project Description: GUC #1
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
66255
I
GUC #1 Dewatered
66255
GUC #1 Dewatered
66255
GUC #1 Dewatered
i
66255
GUC #1 Dewatered
66255
GUC #1 Dewatered
66255
GUC #1 Dewatered
66255
GUC #1 Dewatered
66255
GUC #1 Dewatered
66255
GUC #1 Dewatered
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354
05/06/2019
15:30
05/07/2019
05/06/2019
15:30
05/07/2019
05/06/2019
15:30
05/07/2019
05/06/2019
15:30
05/07/2019
05/06/2019
15:30
05/07/2019
05/06/2019
15:30
05/07/2019
05/06/2019
15:30
05/07/2019
05/06/2019
15:30
05/07/2019
05/06/2019
15:30
05/07/2019
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
Page 2 of 6

Report Number: 19-127-0214
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 66255
Sample Id : GUC #1 Dewatered
Wavpoint
AW ANALYTICAL
Project: GUC #1
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 5/6/2019 15:30:00
Date Received: 05/07/2019 00:00
Date Reported: 05/15/2019
Total Solids
1
8.84
88400
100.0
CJR
05/08/2019 15:15
SM-2540G
Moisture'
91.20
100.0
CJR
05/08/201915:15
SM-254OG
Total Kjeldahl Nitrogen
1.11
11100
250
JPJ
05/14/2019 13:00
SM-4500-NH3C-TKN
Phosphorus
0.21
2090
50.0
BKN
05/10/201918:30
601OD
Potassium
0.04
368
50.0
BKN
05/10/201918:30
6010D
Sulfur
0.48
4830
50.0
BKN
05/10/201918:30
601OD
Calcium
0.11
1060
250
BKN
05/10/201918:30
6010D
Magnesium
0.05
487
50.0
BKN
05/10/201918:30
6010D
Sodium
<0.03
<250
250
BKN
05/10/201918:30
6010D
Iron
31700
50.0
BKN
05/10/201918:30
601OD
Aluminum
117000
500
KKM
05/13/201914:09
601OD
Manganese
413
5.00
BKN
05/10/201918:30
6010D
Copper
247
2.50
BKN
05/10/201918:30
6010D
Zinc
53.1
12.5
BKN
05/10/201918:30
6010D
Ammonia Nitrogen
<0.01
<100
100
JPJ
05/14/2019 13:00
SM-4500-NH3C
Organic N
1.11
11100
250
05/14/2019 13:00
CALCULATION
Nitrate+Nitrite-N
<4.76
4.76
ZBD
05/09/201912:50
4500NO317-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding
Time
CG
. /
p 6ew
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist
Page 3 of 6

Report Number: 19-127-0214
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 66255
Sample Id : GUC #1 Dewatered
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH*
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Chloride
Comments:
6.7
11.60
45.30
Waypoint
ANALYTICAL
Project : GUC #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OF ANALYSIS
RESULT -QUANTITATION'LIM11'r-
ANALYST
Date Sampled: 5/6/2019 15:30:00
Date Received: 05/07/2019 00:00
Date Reported: 05/15/2019
ANALYSIS
• f
<1.00
1.00
BKN
05/10/201918:30
601OD
23.9
2.50
BKN
05/10/201918:30
6010D
9.41
2.50
BKN
05/10/201918:30
6010D
15.7
3.00
BKN
05/10/201918:30
6010D
9.06
5.00
BKN
05/10/201918:30
601OD
0.304
0.0155
TJS
05/10/2019 12:51
SW-7471 B
<5.00
5.00
BKN
05/10/201918:30
6010D
JSL
05/14/2019 07:27
9045D
116000
1000
DXT
05/10/2019 15:01
AOAC 955.01
453000
100.0
CJR
05/08/201915:15
SM-2540G
<2.50
2.50
BKN
05/10/201918:30
601OD
537
200
JM
05/08/201916:22
SM-4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time ?Ift6 i1r�C GQON�
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McG roary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 4 of 6

(D
���®' ��� 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-127-0214
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample label(s)?
9 Yes
0 No
COC properly completed
• Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
! Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
* Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
9 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: lBrandi Watson Date & Time: 5/07/2019 14:56:07
Page 5 of 6

.A S TE WA TFR g ;
,
7621 kVhitepine Road Richmond'
i
..Subrnitted Byli
a lv- NOvniC Se,vtc,
3o WUOO! ! n L%lr1 STre.
Project
l
U C
Phone: 7orf ocon
Sample ID
Lab Number
(Lab Use
Collection Information
Only)
Type Date Th
wC
X
IiewatzR
d
Grab
_Composite
er�
eaj -__
X Grab
q
Composite / 3. 3G
— Grab
— Composite
—
Grab
—
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0
,�„Cs: t otal
^`---�--
Kjeldahl,Ammonium,
_ Nitn
Cocrt
Presider",
I$10-HOMIC SERVICES
A Curylon Cnu,pnny
The Enviranmeno,
530 l5`axllnn•n Str•e!
Proreclion Specat's,s
l3elnu1111• NC 28012
= It
Web Site
,•_,_
l'Itunr. [phone]
wvrn Boo Nomm com
Fax: (704) 529" 1()1K
gull Fred: 1-800-782-07%
A Carylo„ Company
Cell: (7(4) 90.1-970d
v^m-raryloncarp.con I
!:-Mail:
jcuraG='biu-❑ut12 tc.c, L"11
IN OE CUS7_ UDY_
—Account
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IIIIIIII�IIIIIIIIIIIIIIIOIIII�III�IIIIIIIIIIIIIIIflllll 0-0214
5-07� 019
Illll�llll waypointanalytical.coln
14:76
sio-Nomic Servics Inc
GUC#1
— Copy To
_
/
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7,y/%7G. �31(7—�oc')7iG 3erO'Ce-3, mr—
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=Fax':.o�t-S1q- 16h8
f dvto.m i c,[ ovrt
E-mail: Haar+;h®wrlfcox�vtabeso�/
/
copy, tf
Sample Information
Container Information
Please Write in Desired Tests
/�!
P✓
S, cal,
Fel r4 (
�h)
N('(
Nye
liNumbereof
Bottles
Type
Volume
4
D3-N
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pint
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t
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— Oz
pint
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gen.
V_,-gnesium, Sodium, Iron, Aluminum,
:IM-- Cobalt, Molybdenum, Mercury, Lead,
erg -. cal Oxygen Demand (5 days), Boron,
4� ----,ravalent Chromium, Oil and Grease (EPA),
i
I
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Special Instructions or
/,\JG C/ass A

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: May 6, 2019
Greenville Utility Commision #2 Permit No. WQ0039053
9.23 % Solids
(_1 nH
Parameter
\Y s
Mil-
MgiW
(l
dsDpTnryu
Nitrogen (TKN)
0.739
7,390.000
14.780
Phosphorus
0.229
2,290.000
4.580
Potassium
0.029
292.000
0.584
PAN (injected)*
0.156
3,869.500
7.739
PAN (surface)*
0.151
3,777.000
7.554
Ammonia Nitrogen
0.010
100.000
0.200
Calcium
0.178
1,780.000
3.560
Calcium Carbonate E .
40.200
145,000.000
290.000
Magnesium
0.042
417.000
0.834
Sodium
0.027
273.000
0.546
Sulfur
---
5,890.000
11.780
Nitrate N / Nitrite N
---
4.700
0.009
Barium
---
---
Chloride
---
606.000
1.212
Iron
---
31600.000
63.200
Aluminum
---
137,000.00
274.000
Arsenic
---
11.10
0.022
Cadmium
---
1.000
0.002
Chromium
---
43.700
0.087
Copper
---
293.00
0.586
Lead
---
15.10
0.030
Mercury
---
0.4390
0.001
Molybdenum
---
2.50
0.005
Nickel
---
11.40
0.023
Selenium
---
5.00
0.010
Zinc
---
55.50
0.111
Waypoint Analytical 19-127-0215
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
� e
Willcox&mabe
Prepared By:
SO I L SOLUTI O N S
75
85
840
57
75
420
100
7.501

(D
WayPA®ont..
NALYTICAL
5/15/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-127-0215
Project Description: GUC #2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/7/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
F ;� r 6.7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

� e
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-127-0215
Client Project Description: GUC #2
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
66256
GUC
#2
Dewatered
Solids
05/06/2019
15:30
05/07/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
Page 2 of 6

Report Number: 19-127-0215
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 66256
Sample Id : GUC #2 Dewatered
Waypoint0
ANALYTICAL
Project: GUC #2
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 5/6/2019 15:30:00
Date Received: 05/07/2019 00:00
Date Reported: 05/15/2019
Total Solids *
9.23
92300
100.0
CJR
05/08/2019 15:15
SM-2540G
Moisture *
90.80
100.0
CJR
05/08/2019 15:15
SM-2540G
Total Kjeldahl Nitrogen
0.74
7390
250
JPJ
05/14/2019 13:00
SM-4500-NH3C-TKN
Phosphorus
0.23
2290
50.0
BKN
05/10/201918:35
6010D
Potassium
0.03
292
50.0
BKN
05/10/201918:35
601OD
Sulfur
0.59
5890
50.0
BKN
05/10/201918:35
601OD
Calcium
0.18
1780
250
BKN
05/10/201918:35
6010D
Magnesium
0.04
417
50.0
BKN
05/10/201918:35
6010D
Sodium
0.03
273
250
BKN
05/10/201918:35
601OD
Iron
31600
50.0
BKN
05/10/201918:35
601OD
Aluminum
137000
500
KKM
05/13/201914:14
6010D
Manganese
719
5.00
BKN
05/10/201918:35
6010D
Copper
293
2.50
BKN
05/10/201918:35
6010D
Zinc
55.5
12.5
BKN
05/10/201918:35
6010D
Ammonia Nitrogen
<0.01
<100
100
JPJ
05/14/2019 13:00
SM-4500-NI3C
Organic N
0.74
7390
250
05/14/2019 13:00
CALCULATION
Nitrate+Nitrite-N
<4.70
4.70
ZBD
05/09/201912:50
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding
Time
rOZG
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
Pauric McG roary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number: 19-127-0215
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 66256
Sample Id : GUC #2 Dewatered
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Chloride
Comments:
Waypoint
ANALYTICAL
Project: GU #2
REPORT OFANALYS/S
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 5/6/2019 15:30:00
Date Received: 05/07/2019 00:00
Date Reported: 05/15/2019
<1.00
1.00
BKN
05/10/201918:35
601OD
43.7
2.50
BKN
05/10/201918:35
601OD
11.4
2.50
BKN
05/10/201918:35
601OD
15.1
3.00
BKN
05/10/201918:35
6010D
11.1
5.00
BKN
05/10/201918:35
601OD
0.439
0.0144
TJS
05/10/2019 12:52
SW-7471 B
<5.00
5.00
BKN
05/10/201918:35
601OD
6.1
JSL
05/14/2019 07:27
9045D
14.50 145000
1000
DXT
05/10/2019 15:01
AOAC 955.01
51.70 517000
100.0
CJR
05/08/201915:15
SM-2540G
<2.50
2.50
BKN
05/10/201918:35
601OD
606
200
JM
05/08/201916:22
SM-4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Page 4 of 6
Pam« imp 10"r
Pauric McGroary
Agronomist

Wavpoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-127-0215
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
• No
Comments:
Signature: lBrandi Watson Date & Time: 05/07/2019 15:00:29
Page 5 of 6

NT
19-127-0215
45671
05-07-2019
1. F; rx: 9 1) 1 - '7 1 + 111, 1
Bio-Nornic Servics Inc 14:59:07
GUC #2
cu%toutier Infortnation
Charge To
Copy TO
ii-011
Project', Phone.-
'A_
Sample Information
Please Write in Desired Tests
Lot) Number
Collection Information
_.oIII:I1Iv:f
11formarlon
-f
Sample ID
(Lab Use
Only)
Uo I
IIIw,
I YIW
Volume
volu
I
II
C
C
Y
"king
0Z
GoInposile
Grab
2 ell
Composite
I IlwAic
-Pint
Grab
tllmx
*1
0z
pint
Composite
I S c
q
115
oz
pint
.onpo.,Ie
Composite
1
III, sfic
I qt _I
Rejipquishedgy: (Si nature
Date
1 it I Iv
By. Si nature
Date
Time
Z
Special Instructions or Remarks
Nitrogen Series: '101;11 KJOIrl'.1111L Jvhlh:ilo Y. Otilanic
Nitrogen i'\J c A
Magnesium, Sodium, Iron, Aluminum,
jin. Cobalt, Molybdenum. Mercury, Lead
t,mical Oxygen Demand (5 days), Boron,
-
loxava lent Chromium, Oil and Grease 0-I W,
I B10-HOMIC SERWES
lilt, tll.
WHO
101 I—e

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: July 10, 2019
Greenville Utility Commision #3 Permit No. WQ0039053
20.00 % Solids
6.2 off
Parameter,
'2 %
Mg/Kg Dry WeYght
�oundslDry Tiro
Nitrogen (TKN)
4.690
46,900.000
93.800
Phosphorus
0.239
2,390.000
4.780
Potassium
0.035
352.000
0.704
PAN (injected)*
0.947
3,869.500
7.739
PAN (surface)*
0.942
3,777.000
7.554
Ammonia Nitrogen
0.010
100.000
0.200
Calcium
0.148
1,480.000
2.960
Calcium Carbonate E .
40.200
27,000.000
54.000
Magnesium
0.050
501.000
1.002
Sodium
0.025
250.000
0.500
Sulfur
---
6,470.000
12.940
Nitrate N / Nitrite N
---
5.000
0.010
Barium
---
---
---
Chloride
---
1190.000
2.380
Iron
---
29800.000
59.600
Aluminum
---
149,000.00
298.000
Arsenic
---
11.30
0.023
Cadmium
---
1.000
0.002
Chromium
---
40.200
0.080
Copper
---
353.00
0.706
Lead
---
19.20
0.038
Mercury
---
0.2520
0.001
Molybdenum
---
2.50
0.005
Nickel
---
13.30
0.027
Selenium
---
5.00
0.010
Zinc
---
61.60
0.123
Waypoint Analytical 19-192-0007
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
willcox&mate
Prepared By:
SO I L SOLUTI O N S
75
85
4,301
840
57
75
420
100
7.501

& Eft io
Wayp"It.
i
7/19/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-192-0007
Project Description: GUC-4-3
1621 Whitepine Road, Richmond, VA 23237
Main>804-743-9401 0 Fak8l.64471-6446
wwwMaypo'i itanalocal.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 7/11/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pia P c0-r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
M° y
Page 1 of 8

7522,Whitep nie Road, Ruhtnoi d, VA 23237
Nlaiii 804-74A'*O it Eax.804-271-60446
www.viaypoiitanalyticat.aar�i
Client: Bio-Nomic Servics Inc CASE NARRATIVE
Project: GUC$ 3 AWOK 7-22-19
Lab Report Number: 19-192-0007
Date: 7/19/2019
Metals Analysis Method 6010D
Sample 67321
Analyte: Aluminum
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Calcium
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Sulfur
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Selenium
Page 2 of 8

a a a
762I whitep ne Raa i Richmi nd, VA•Z3237
Main 804443-9401 ° Faxt804471-6446
was w.waypoir tanalytieal.co' '
QC Batch No: L445577
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 8

W...ay 7621 Wt tepine Road, Richmontl, VA 23237
point Main:8U4 74344U1 ° Fax8U4
271 6446
ANALYTICAL wwvs.",pointanalytical.com
Sample Summary Table
Report Number:
Client Project Description:
19-192-0007
GUC-+- 37 1"e"'L
7 -;1;1-1'7
Lab No Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
67317 GUC-3
Solids
07/10/201911:47
07/11/2019
67317 GUC-3
Solids
07/10/201911:47
07/11/2019
SM-2540G
WTN
67317 GUC-3
Solids
07/10/201911:47
07/11/2019
SW-7471B
WTN
67317 GUC-3
Solids
07/10/201911:47
07/11/2019
SM-4500-NH3C-TKN
WTN
67317 GUC-3
Solids
07/10/201911:47
07/11/2019
4500NO3F-2011
WTN
67317 GUC-3
Solids
07/10/201911:47
07/11/2019
6010D
WTN
67317 GUC-3
Solids
07/10/201911:47
07/11/2019
SM-4500-NH3C
WTN
67317 GUC-3
Solids
07/10/201911:47
07/11/2019
9045D
WTN
67317 GUC-3
Solids
07/10/2019 11:47
07/11/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 4 of 8

Report Number: 19-192-0007
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 67317
Sample Id: GUC-3
Wayo.oi
1 1 1
Project: GUC-1
REPORT OF ANALYSIS
7621 Whitepine RoLd, Richmond; VA 23237
MainI.404-743-9401 ° Fax; $trt4-271-6446
viww.waypointanalytical.com
Date Sampled: 7/10/2019 11:47:00
Date Received: 07/11/2019 00:00
Date Reported: 07/19/2019
Total Solids "
20.00
ADM
07/15/2019 16:01
SM-2540G
Moisture '
80.00
ADM
07/15/2019 16:01
SM-2540G
Total Kjeldahl Nitrogen
4.69
46900
250
JPJ
07/18/2019 10:00
SM-4500-NH3C-TKN
Phosphorus
0.24
2390
50.0
BKN
07/18/2019 02:32
6010D
Potassium
0.04
352
50.0
BKN
07/1812019 02:32
601 OD
Sulfur
0.65
6470
50.0
BKN
07/18/2019 02:32
6010D
Calcium
0.15
1480
250
BKN
07/18/2019 02:32
6010D
Magnesium
0.05
501
50.0
BKN
07/18/2019 02:32
6010D
Sodium
<0.03
<250
250
BKN
07/18/2019 02:32
6010D
Iron
29800
50.0
BKN
07/18/2019 02:32
6010D
Aluminum
149000
500
BKN
07/18/201911:41
6010D
Manganese
578
5.00
BKN
07/18/2019 02:32
6010D
Copper
353
2.50
BKN
07/18/2019 02:32
6010D
Zinc
61.6
12.5
BKN
07/18/2019 02:32
6010D
Ammonia Nitrogen
<0.01
<100
100
JPJ
07/18/2019 14:00
SM-4500-NH3C
Organic N
4.69
46900
250
07/18/2019 10:00
CALCULATION
Nitrate+Nitrite-N
<5.00
5.00
ZBD
07/17/201912:12
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist
Page 5 of 8

Report Number: 19-192-0007
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 67317
Sample Id : GUC-3
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Calcium Carbonate Equivalent
Molybdenum
Chloride
Comments:
WOY'
ANALYTICAL.
Project: GUC-1
REPORT OF ANALYSIS
76zI.lAtf �tepine:,Ro d, Nchmond� VA Z3 7
IVian$04-743-94QI°FaxSQ4275t146
www.waypoiritanalytical.com
Date Sampled: 7/10/2019 11:47:00
Date Received: 07/11/2019 00:00
Date Reported: 07/19/2019
<1.00
1.00
BKN
07/18/2019 02:32
6010D
40.2
2.50
BKN
07/18/2019 02:32
6010D
13.3
2.50
BKN
07/18/2019 02:32
6010D
19.2
3.00
BKN
07/18/2019 02:32
6010D
11.3
5.00
BKN
07/18/2019 02:32
6010D
0.252
0.0135
TJS
07/16/2019 11:06
SW-7471 B
<5.00
5.00
BKN
07/18/2019 02:32
6010D
6.2
JSL
07/15/2019 07:27
9045D
2.70 27000
1000
DXT
07/18/2019 12:13
AOAC 955.01
<2.50
2.50
BKN
07/18/2019 02:32
6010D.
1190
200
JCM
07/17/201916:14
SM-4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H -Beyond holding time oil
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric MCGroary
to the worts, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 6 of 8

s
Waypoint7621 Whitepine Road,. Richmond, VA 23237
Main 804-743-9401 "Fax [phone]
ANALYTICAL www.waypaintanaiyticai.corti
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-192-0007
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1'
Custody seals intact on shipping container/cooler?
0 Yes
0 No Not Required
Custody seals intact on sample bottles?
0 Yes
0 No Not Required
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample label(s)?
• Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
• Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No N/A
Water - VOA vials free of headspace
0 Yes
0 No N/A
Trip Blanks received with VOAs
0 Yes
0 No N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No N/A
F_ High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
No
Comments:
Signature: lBrandi Watson Date & Time: 7/11/2019 10:18:14
Page 7 of 8

Wood[;)
e i# 0A /V I
Phone: IFaX*
T,
Qate-o
Time:,,
T' Ype
. Y� �,
-volume
, . , "
"T,
J
file
.FO
_4
K"
4",
Composite
tir
Plastic-
OZ
—pitnt
/-q
Grab
G,
oz
Composite
Plastic
pint
Grab
composite
Glass
Plastic
oz
pint
Grab
Glass
oz
Composite
^ Plastic
pint
r0gen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen,
osph,orus(total, orthot), PoajsSiurn. SUlfate-Suffur,, Qalcium,. Magnq,5jum,Sodiumz, lror),.AIuhjihum,
nganese, ;Copper, Zinc, Arsenic, Baelum,,Cadrnium, Chromium, Ciobalt, Molybdenum, Mercury, Lead,
lenium, Silver. Nickel. Acidity (Total}, Alkalinity (Total), piochernical Oxygen Demand (5 days),.Boron,
emical Oxygen Demand, Chloride, Conductance (Spe(cific), Hexavaleht Chromium, Oil and.Grease (EPA),
Pbenol, Solids. (Dissolved, SuspeOded, Total, Volatile)

I
BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 28, 2019
Greenville Utility Commision #4 Permit No. WQ0039053
39.40 % Solids
5.9 pH
Nitrogen (TKN)
0.513
5,130.000
10.260
Phosphorus
0.184
1,840.000
3.680
Potassium
0.068
680.000
1.360
PAN (injected)*
0.127
3,869.500
7.739
PAN (surface)*
0.112
3,777.000
7.554
Ammonia Nitrogen
0.031
305.000
0.610
Calcium
0.191
1,910.000
3.820
Calcium Carbonate E .
0.100
1,000.000
2.000
Magnesium
0.096
961.000
1.922
Sodium
0.025
250.000
0.500
Sulfur
---
4,070.000
8.140
Nitrate N / Nitrite N
---
4.560
0.009
Barium
---
---
---
Chloride
---
16.200
0.032
0�7�
Iron
---
25,300.00
50.600
"Cerlmg,Goncen.
Aluminum
---
79,700.00
159.400
Arsenic
---
9.31
0.019
75
Cadmium
---
1.000
0.002
85
Chromium
---
102.000
0.204
---
Copper
---
127.00
0.254
4,300
Lead
---
20.70
0.041
840
Mercury
---
0.1170
0.000
57
Molybdenum
---
2.50
0.005
75
Nickel
---
38.10
0.076
420
Selenium
---
5.00
0.010
100
Zinc
---
50.20
0.100
7,500
Waypoint Analytical 19-241-0008
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
Willcox&make
Prepared By:
SOI L SOLUTIONS

I
1
I
0
1
Waypoint....
ANALYTICAL.
9/9/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-241-0008
Project Description: GUC-4
7621'Wi tepine Rdad, Richmond, VA 23237
Main 804-743-9461 * Fax 804=271-6446.
WWWr vaypo'tntanaiyticaI.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/29/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pau:< r Gcw-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

7621 WWitepihe Road, RichmondInt, VA 23237
'ay I Main804 743-9A01804-271-6446
OA N A:LYTI CA L vuwv�r:waypoiritanaljit;cal.corn
Sample Summary Table
Report Number: 19-241-0008
Client Project Description: GUC-4
Lab No Client Sample ID
Matrix Date Collected Date Received Method Lab ID
67998
GUC-4
Solids
67998
GUC-4
Solids
67998
GUC-4
Solids
67998
GUC-4
Solids
67998
GUC-4
Solids
67998
GUC-4
Solids
67998
GUC-4
Solids
67998
GUC-4
Solids
67998
GUC-4
Solids
67998
GUC-4
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
08/28/2019
10:47
08/29/2019
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
AWN
9056A
WTN
AOAC 955.01
WTN
Page 2 of 6

Report Number: 19-241-0008
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 67998
Sample Id: GUC-4
Waypowt...
ANALYTICAL
Project: GUC-4
REPORT OF ANALYSIS
7621.Whitepine' Road, Richmond. VA 23237
Main 80,043 9401 ° Fax [phone]A46
w:wvowaypointanalytical.com
Date Sampled: 8/28/2019 10:47:00
Date Received: 08/29/2019 00:00
Date Reported: 09/10/2019
Total Solids *
39.40
ADM
09/03/2019 16:16
SM-2540G
Moisture *
60.60
ADM
09/03/2019 16:16
SM-2540G
Total Kjeldahl Nitrogen
0.51
5130
250
JPJ
09/06/2019 09:00
SM-4500-NH3C-TKN
Phosphorus
0.18
1840
50.0
JTR
09/05/2019 21:43
6010D
Potassium
0.07
680
50.0
JTR
09/05/2019 21:43
6010D
Sulfur
0.41
4070
50.0
JTR
09/05/2019 21:43
6010D
Calcium
0.19
1910
250
JTR
09/05/2019 21:43
601 OD
Magnesium
0.10
961
50.0
JTR
09/05/2019 21:43
601 OD
Sodium
<0.03
<250
250
JTR
09/05/2019 21:43
6010D
Iron
25300
50.0
JTR
09/05/2019 21:43
6010D
Aluminum
79700
50.0
JTR
09/05/2019 21:43
6010D
Manganese
648
5.00
JTR
09/05/2019 21:43
6010D
Copper
127
2.50
JTR
09/05/2019 21:43
6010D
Zinc
50.2
12.5
JTR
09/05/2019 21:43
6010D
Ammonia Nitrogen
0.03
305
100
JPJ
09/06/2019 14:30
SM-4500-NH3C
Organic N
0.48
4825
250
09/06/2019 09:00
CALCULATION
Nitrate+Nitrite-N
<4.56
4.56
ZBD
09/04/201915:25
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B -Anal a detected in blank H - Beyond holding time t'rC
Yt Y 9
Our reports and fetters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work, the results, or the company in any advertising, news release, or ocher public announcements without obtaining our prior written authorization. Agronomist
Page 3 of 6

Report Number: 19-241-0008
Account Number: 45671 i vftpoint
►NMYT1CAL.
Send To: Bio-Nomic Servics Inc Project : GUC-4
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 67998
Sample Id: GUC-4
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH'
Calcium Carbonate Equivalent
Total Volatile Solids
Molybdenum
Chloride —
Silicon
Comments:
REPORT OF ANALYSIS
7621 Whitaptne;,Road, Richmond, VA 23237
Main 804-743 9401 ° Fax 804 2A1 6A46
www:wayp ointanatytleaLeiin
Date Sampled: 8/28/2019 10:47:00
Date Received: 08/29/2019 00:00
Date Reported: 09/10/2019
<1.00
1.00
JTR
09/05/2019 21:43
6010D
102
2.50
JTR
09/05/2019 21:43
6010D
38.1
2.50
JTR
09/05/2019 21:43
6010D
20.7
3.00
JTR
09/05/2019 21:43
6010D
9.31
5.00
JTR
09/05/2019 21:43
601 OD
0.117
0.0138
TJS
09/04/2019 13:57
SW-7471 B
<5.00
5.00
JTR
09/05/2019 21:43
601 OD
5.9
JSL
09/04/2019 06:13
9045D
<0.10 <1000
1000
DXT
09/05/2019 10:12
AOAC 955.01
21.80
ADM
09/03/201916:16
SM-2540G
<2.50
2.50
JTR
09/05/2019 21:43
6010D
16.2
4.00
CCR
09/09/201917:21
9056A
458
25.0
JTR
09/05/2019 21:43
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports crud letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric MCG roary
to the woik, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist
Page 4 of 6

7621 whitepine Road, Richmond, VA 23237 aypoinv.Main 804-74379401 'Fax [phone]
ANALYTICAL wwvi waypoiiitanalytical.coiri
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-241-0008
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Y1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample label(s)?
• Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
• Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
• Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) F_ Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
No
Comments:
Signature: jBrandi Watson Date & Time: 8/29/2019 14:18:16
Page 5 of 6

110111111111111111 I E1111111111111111 �'�°$
Siior Namic Seniica Inc 2019
GUC-4 14:17:20
7621 Whitepine'Road Richmond
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530 uort t.;wr1 a Free
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eaypointanalytical.com
l onaturet ,Gate
Test.:Available S cial insxructian ,or"13 marks-
Nitrogen "Series; Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver, Nickel Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand; Chloride, Conductance (Specific), HexavalentChromium., Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
Account": ,
Page 6 of 6

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 7, 2019
Greenville Utility Commision #5 Permit No. WQ0039053
19.60 % Solids
6.1 DH
Nitrogen (TKN)
1.230
12,300.000
24.600
Phosphorus
0.291
2,910.000
5.820
Potassium
0.039
391.000
0.782
PAN (injected)*
0.289
3,869.500
7.739
PAN surface)*
0.264
3,777.000
7.554
Ammonia Nitrogen
0.051
510.000
1.020
Calcium
0.239
2,390.000
4.780
Calcium Carbonate E .
7.400
74,000.000
148.000
Magnesium
0.061
607.000
1.214
Sodium
0.128
1,280.000
2.560
Sulfur
---
5,970.000
11.940
Nitrate N / Nitrite N
---
25.000
0.050
Barium
Chloride
---
---
---
53.600
0.107
Iron
Aluminum
---
---
32,200.00
128,000.00
64.400
256.000
Gee
Arsenic
---
25.50
0.051
Cadmium
---
5.100
0.010
Chromium
---
63.800
0.128
Copper
---
391.00
0.782
Lead
---
20.50
0.041
Mercury
---
0.5610
0.001
Molybdenum
---
12.80
0.026
Nickel
---
13.80
0.028
Selenium
---
25.50
0.051
Zinc
---
70.90
0.142
Waypoint Analytical 19-281-0002
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
willc®x&mabe
Prepared By: S O I L S O L U T I O N S
75
85
840
57
75
420
100
7.501

Way III
PMSTICAL.
10/17/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-281-0002
Project Description: GUC-5
7621'Whitepine Road, Richmond, VA 23237
Main 804'743.9461 * Fax [phone]
www.waypo ntanalyticbl.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/8/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

iWaypollit.:
1 ► i
Client: Bio-Nomic Servics Inc
Project: GUC-5
Lab Report Number: 19-281-0002
Date: 10/16/2019
7621 Whitepine Road, Richmond, VA23237
Main 804-143-9401 ° Fax [phone]
www.waypoiotanalyfica I,coi
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 68529
Analyte: Aluminum
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Calcium
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Potassium
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Sulfur
QC Batch No: L458430
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L458430
Page 2 of 8

WayRTICAL
7621 Whitepirie Road, Richmond, VA 23237
Main 804-743-940i 4 Fax [phone]
wW w.waypointa na lOca l.corh
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 8

e
Way, t7621 Whitepine Road, Richmond, VA 23237
Main 864-743-9401 ° Fax 804:471-6446
ANALYTICAL www.w6ypointanalytical.coni
Sample Summary Table
Report Number: 19-281-0002
Client Project Description: GUC-5
Lab No Client Sample ID
68526
GUC-5
68526
GUC-5
68526
GUC-5
68526
GUC-5
68526
GUC-5
68526
GUC-5
68526
GUC-5
68526
GUC-5
68526
GUC-5
68526
GUC-5
Matrix Date Collected Date Received Method Lab ID
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
10/07/2019
14:11
10/08/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
450dNO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
9056A
WTN
AOAC 955.01
WTN
Page 4 of 8

Waypoint
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Report Number:19-281-0002
Lab No : 68526
Sample ID: GUC-5
7621.tiNhrtepine Road; Richmond, VA 23?37
1Vlain 804-143-9401 ° Fax [phone],
wwvi:waypo intaiialyticai:com
Project GUC-5
Information :
REPORT OFANAL YSIS
Report Date : 10/17/2019
Received : 10/08/2019
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 10/7 / 2019 14:11
Moisture 80.4 H % 0.010 1 10/15/19 16:30 ADM SM-254OG
Selenium <25.5 mg/Kg - dry 25.5 10 10/10/19 23:00 BKN 6010D
Total Solids
19.6 H
%
0.010
1 10/15/19 16:30
ADM
SM-2540G
Total Kjeldahl Nitrogen
1.23
% - dry
0.127
1 10/15/19 09:00
JPJ
;M-4500-NH3C-TKP
Phosphorus
2910
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Potassium
391
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Sulfur
5970
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Calcium
2390
mg/Kg - dry
1280
10 10/10/19 23:00
BKN
6010D
Magnesium
607
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Iron
32200
mg/Kg - dry
255
10 10/10/19 23:00
BKN
6010D
Manganese
857
mg/Kg - dry
25.5
10 10/10/19 23:00
BKN
6010D
Copper
391
mg/Kg - dry
12.8
10 10/10/19 23:00
BKN
6010D
Organic N
1.23
% - dry
0.127
1 10/15/19 09:00
CALCULATION
Nitrate+Nitrite-N
<25.0
mg/Kg - dry
25.0
1 10/11/19 15:28
ZBD
4500NO3F-2011
Nickel
13.8
mg/Kg - dry
12.8
10 10/10/19 23:00
BKN
6010D
Mercury
0.561
mg/Kg - dry
0.0785
1 10/11/19 12:17
TJS
SW-7471B
pH
6.1
S.U.
1 10/14/19 08:04
JSL
9045D
Calcium Carbonate
Equivalent
7.4
%
0.1
1 10/15/19 14:55
DXT
AOAC 955.01
Total Volatile Solids
38.0 H
%
0.010
1 10/15/19 16:30
ADM
SM-254OG
Qualifiers/
*
Outside QC Limit
B
Analyte detected in blank
Definitions
C
GCMS Confirmation Analysis
E
Result above cal range
g
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
N
Refer to cover letter.
Page 5 of 8

t.. /� k
pWay
V� '
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert Project GUC-5
530 Woodlawn St Information
Belmont, NC 28012
Report Number :19-281-0002 REPORTOFA
Lab No : 68526
Sample ID: GUC-5
76�1.tiUhdepige Road, R�chmord, VA 23237
Win'>j04-7439461 ° Fax [phone]
www.waypo intanalyticaII 66iri
Report Date : 10/17/2019
Received : 10/08/2019
VAIYSIS Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 30/7/ 2019 14:11
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Ammonia Nitrogen
<0.051
% - dry
0.051
1
10/15/19 13:00
JPJ
SM-4500-NH3C
Chloride
53.6
mg/Kg - dry
20.4
1
10/14/19 17:23
CCR
9056A
Aluminum
128000
mg/Kg - dry
255
10
10/10/19 23:00
BKN
6010D
Arsenic
<25.5
mg/Kg - dry
25.5
10
10/10/19 23:00
BKN
6010D
Cadmium
<5.10
mg/Kg - dry
5.10
10
10/10/19 23:00
BKN
6010D
Chromium
63.8
mg/Kg - dry
12.8
10
10/10/19 23:00
BKN
6010D
Lead
20.5
mg/Kg - dry
15.3
10
10/10/19 23:00
BKN
6010D
Molybdenum
<12.8
mg/Kg - dry
12.8
10
10/10/19 23:00
BKN
6010D
Sodium
<1280
mg/Kg - dry
1280
10
10/10/19 23:00
BKN
6010D
Zinc
70.9
mg/Kg - dry
63.8
10
10/10/19 23:00
BKN
6010D
Qualifiers/ B Analyte detected in blank
Definitions
H Beyond holding time
Page 6 of 8

n3,¢
aypownt'­
i 1 l
7621 Whliepine Road, Richmond; VA 2323Z
Main 804-743-9401 ° Fax [phone]
wvi W.wayj ointanalyticai:com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-281-0002
Shipping Method
• Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
10 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
i
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
9 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
• No
Comments:
Signature: jBrandi Watson Date & Time: 10/08/2019 14:25:54
Page 7 of 8

VAST,', ATER S, A
..... . .....
Waypoint' 45671
7621 Whitepine Road Richmond VA M37 Tel: [phone](l, Seivirs Inc '10-0-2019
Account#:
570 54:7
777-7
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Phone: _7.C=oFax:
E-mail: khCoaTio blo-'nomm. CO =ni
SAmplay In rmation
Sample lb.
:tali *U rnb4at"
01,10
Gontainer,inforniallon,
Heqo6.
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'Date
Time-
umber
of 6bttles
Type
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Date
Time,
10 /0:;'1/19
f;?d ex
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Test-'Availablei - ',' r . . I I 1 1. . I I'll
ftecia[ Instructions orRamarks
Nitrogen Series, Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
15hosphorus(total, orthor), Poatsaium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum.,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt; Molybdenum,, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), AlWnity (Total), Bloohemical Oxygen Demand (6 days), Boron,.
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH. Phenol, Solids (Dissolved, Suspended, Total, Volatile)
N C,
f-
Page 8 of 8

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 11, 2019
Greenville Utility Commision #6 Permit No. WQ0039053
16.50 % Solids
6.5 DH
Parameter
%
Mg/Kg Dry Weightl
(% x 10,000)
Pounds/DryTon
1 (Mg/Kg x 0.002)
Nitrogen (TKN)
1.620
16,200.000
32.400
Phosphorus
0.316
3,160.000
6.320
Potassium
0.046
458.000
0.916
PAN (injected)*
0.376
3,755.100
7.510
PAN (surface)*
0.345
3,452.100
6.904
Ammonia Nitrogen
0.061
606.000
1.212
Calcium
0.192
1,920.000
3.840
Calcium Carbonate E .
8.400
84,000.000
168.000
Magnesium
0.056
559.000
1.118
Sodium
0.033
332.000
0.664
Sulfur
---
5,480.000
10.960
Nitrate N / Nitrite N
---
30.300
0.061
Barium
---
---
---
Chloride
---
89.700
0.179
Iron
---
35,400.00
70.800
Aluminum
---
139,000.00
278.000
Arsenic
---
16.40
0.033
Cadmium
---
0.606
0.001
Chromium
---
60.400
0.121
Copper
---
368.00
0.736
Lead
---
23.40
0.047
Mercury
---
0.5100
0.001
Molybdenum
---
1.96
0.004
Nickel
---
12.40
0.025
Selenium
---
4.19
0.008
Zinc
---
61.80
0.124
Waypoint Analytical 19-346-0005
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
0.69
Ceiling Concen.,
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By: S O I L S O L U T I O N S

,. a
Waypoll
®.•
ANALYTICAL,
12/20/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-346-0005
Project Description: GUC-6
762 1Whitepine Road, Richmond, VA.23237
Main 804443-8401 O' Fa)°8.04=271-6446
www.waypo iritanalyiita l.coni
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 12/12/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
Waypownt7621 Whitepine Road, Richmond, VA 23237
Main 804-743-001 0 Fax [phone]
ANALYTICAL www.waypointanalyt;cal.com
Sample Summary Table
Report Number: 19-346-0005
Client Project Description: GUC-6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
69881
GUC-6
Solids
WTN: Waypoint Analytical - TN, Memphis, TN
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
12/11/2019
07:44
12/12/2019
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
9056A
WTN
AOAC 955.01
WTN
Page 2 of 7

i
ay.
int.
7621,Whrtepfne
'804-`743
Road, Richmond, VA 232.37
Main 9401 ° Fax [phone]
A(VALYTICAL
wwvvw4p6intanal"Icat
cor i
45671
Bio-Nomic Servics Inc
Joel Coert
Project
GUC-6
Report Date : 12/20/2019
530 Woodlawn St
Information :
Received : 12/12/2019
Belmont , NC 28012
Pauric McGroary
Report Number: 19-346-0005
REPORTOFANALYSIS
Agronomist
Lab No : 69881
Matrix:
Solids
Sample ID: GUC-6
Sampled:
12/11/2019 7:44
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
83.5
%
0.010
1
12/16/19 18:11
ADM SM-2540G
Calcium Carbonate Equivalent 8.4
% - dry
0.1
1
12/17/19 09:33
DXT AOAC 955.01
Test
Results,
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
<606
mg/Kg - dry
606
1
12/18/19 09:00
JPJ SM-4500-NH3C
Chloride
89.7
mg/Kg - dry
24.2
1
12/18/19 17:47
CCR 9056A
Nitrate+Nitrite-N
<30.3
mg/Kg - dry
30.3
1
12/17/19 15:06
ZBD 4500NO3F-2011
Organic N
16200
mg/Kg - dry
1520
1
12/16/19 09:00
CALCULATION
pH
6.5
S.U.
1
12/16/19 07:16
JSL 9045D
Total Solids
16.5
%
0.010
1
12/16/19 18:11
ADM SM-2540G
Total Volatile Solids
45.5
%
0.010
1
12/16/19 18:11
ADM SM-2540G
__. Total Kjeldahl Nitrogen
16200
mg/Kg - dry
1520
1
12/16/19 09:00
JPJ SM-4500-NH3C-TKP
Phosphorus
3160
mg/Kg - dry
30.3
1
12/17/19 01:37
BKN 6010D
Aluminum
139000
mg/Kg - dry
303
10
12/17/19 13:49
KKM 6010D
Arsenic
16.4
mg/Kg - dry
3.03
1
12/17/19 01:37
BKN 6010D
Calcium
1920
mg/Kg - dry
152
1
12/17/19 01:37
BKN 6010D
Cadmium
<0.606
mg/Kg - dry
0.606
1
12/17/19 01:37
BKN 6010D
Chromium
60.4
mg/Kg - dry
1.52
1
12/17/19 01:37
BKN 6010D
Copper
368
mg/Kg - dry
1.52
1
12/17/19 01:37
BKN 6010D
Iron
35400
mg/Kg - dry
30.3
1
12/17/19 01:37
KKM 6010D
Qualifiers/ B
Analyte detected in blank
DF Dilution Factor
Definitions L
Limit Exceeded
MQL Method
Quantitation Limit
Page 3 of 7

Way tG
7621:tilUhitepine
Road, R�cf�mond,
VA 23ZW
Mziin 804=743-9401 ° Fax [phone]
ANALYT( AL
'"W.waypointa6al".caf.com
45671
Bio-Nomic Servics Inc
Joel Coert
Project
GUC-6
Report Date : 12/20/2019
530 Woodlawn St
Information :
Received : 12/12/2019
Belmont, NC 28012
-
Pauric McGroary
Report Number :19-346-0005
REPOR T OF A NA L YSIS
Agronomist
Lab No : 69881
Matrix: Solids
Sample ID : GUC-6
Sampled: 12/11/2019
7:44
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Method
Lead
23.4
mg/Kg - dry
1.82
1
12/17/19.01:37 BKN
6010D
Magnesium
559
mg/Kg - dry
30.3
1
12/17/19 01:37 BKN
6010D
Manganese
812
mg/Kg - dry
3.03
1
12/17/19 01:37 KKM
6010D
Mercury
0.510
mg/Kg - dry
0.0806
1
12/17/19 15:54 TJS
SW-7471B
Molybdenum
1.96
mg/Kg - dry
1.52
1
12/17/19 01:37 BKN
6010D
Nickel
12.4
mg/Kg - dry
1.52
1
12/17/19 01:37 BKN
6010D
Potassium
458 B
mg/Kg - dry
30.3
1
12/17/19 19:47 KKM
6010D
Selenium
4.19
mg/Kg - dry
3.03
1
12/17/19 01:37 BKN
6010D
Sodium
332
mg/Kg - dry
152
1
12/17/19 01:37 BKN
6010D
Zinc
61.8
mg/Kg - dry
7.58
1
12/19/19 14:51 KKM
6010D
Sulfur
5480
mg/Kg - dry
30.3
1
12/17/19 01:37 BKN
6010D
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 4 of 7

Client: Bio-Nomic Servics Inc
Project: GUC-6
Lab Report Number: 19-346-0005
Date: 12/19/2019
7621 Whitepicie'Roadf Richm ond, VA 0237
tVidii 804-743-94(ii ° R= i804=271-6446
wv,�w.iaypo inanalytical.corn
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 69881 (GUC-6)
Analyte: Potassium
QC Batch No: 1-469392/1-468801
Target analyte(s) was identified in the method blank associated with this project. Per laboratory protocol any
associated affected sample result is flagged "B" to indicate that it was detected in the method blank.
Page 5 of 7

7621 WFiitepine.Road, Richmond, VA 2323Z
Main 804-743-9401 ° Fax 804-271-G446
ANALYTICAL
wwv✓:waypointanalytical.com
Shipment
Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-346-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 Other: 1
0 UPS 0 Client 0 Courier
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No Not Present
Custody seals intact on sample bottles?
0 Yes
0 No Not Present
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
_ COC properly completed
• Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
• Yes
0 No
Cooler temperature in compliance?
• Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
0 Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No N/A
Water - VOA vials free of headspace
0 Yes
0 No N/A
Trip Blanks received with VOAs
0 Yes
0 No N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No N/A
F_ High concentration container (48 hr)
F_ Low concentration EnCore samplers (48 hr)
F High concentration pre -weighed (methanol -14 d) F Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No
Signature: lBrandi Watson Date & Time: 12/12/2019 14.20:19
Page 6 of 7

I 142
Inc
GUC-6 14:M32
submltf6d By
va,aca I awvi i�vt5?4
Phone: F;;
Sample Information
Lab Number
Callectio.6116formation
Cofflainer Information
Please;W*,In Deslred'Tesls
Sample 10
(Lab Use
Only)
tpe,
Data
Time
Number
N
Type
Wumell
Qv
fej 41)
?-"
cg
Pb
5
1�1-
00
070,
I
of BotttesX
AN, 9a
*k'�04
A
At
Grab
Composite
IAIM
0794
Glass
plastic
0z
____pinj
/
V
V
V/
_V
4 qt
Grab
Glass
— oz
Composite
Plastic
—Pint
Grab
Glass*
Composite
plastic .
Qt
Grab
Glass-
oz
Composite
Plastic
—pin
Date
-1,/ 1 V1.
— iesT,Avajl8Dle , IJ - V, ' .11 1 . 5p2clal Instructions or Remarks,
Nitrogen Series; Total Kjal.dahl, Ammonium, Nitrate & Organic Nitrogen,
Phosphorus(total, orthor), Poatsslum, Sullale-Sulfur, Calcium, Magnesium, Sod . ium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Cond uctance (Specifics: Hexavalent Chromium, Oil and: Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
Page 7 of 7

T
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-168891-1
Client Project/Site: Greenville WTP
Revision: 2
For:
Bio-Nomics Services., Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Vaughn Stevenson
Authorized for release by.
3/19/2019 12:40:16 PM
Ken Hayes, Project Manager II
[phone]
ken. [e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTI?
Table of Contents
TestAmerica Job ID: 490-168891-1
CoverPage ............................................... 1
Table of Contents ......................................... 2
Sample Summary ......................................... 3
Case Narrative ........................................... 4
Definitions ............................................... 5
Client Sample Results ...................................... 6
QC Sample Results ........................................ 8
QC Association ........................................... 20
Chronicle ................................................ 24
Method Summary ......................................... 25
Certification Summary ...................................... 26
Chain of Custody .......................................... 27
Receipt Checklists ......................................... 30
Page 2 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)
M1

Sample Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Lab Sample ID Client Sample ID
490-168891-1 GUC
TestAmerica Job ID: 490-168891-1
iTs
Matrix Collected Received L—E
Sludge 02/19/19 12:00 02/21/19 08:55
TestAmerica Nashville
Page 3 of 30 3/19/2019 (Rev. 2)

Case Narrative
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Job ID: 490-168891-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-168891-1
TestAmerica Job ID: 490-168891-1
REVISED REPORT: Revised to report Cyanide, Sulfide, and PCBs without dry weight conversion. This report replaces the one generated
on 03/08/19 @ 1653.
Comments
While TA Pittsburgh carries South Carolina certification for 8260D and 8270E, the referenced matrix "Sludge", is causing the report to
indicate the lab as not certified for these.
No additional comments.
Receipt
The sample was received on 2/21/2019 8:55 AM; the sample arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 3.01 C.
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-271299 was outside the method criteria for the
following analyte: 2-Butanone. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is
considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
GUMS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page
General Chemistry
Method 101 OA: Method 1010A is applicable only to liquid matrix. This method has been modified to incorporate soil/ solid matrices of the
following sample: GUC (490-168891-1).
Method 9034_Calc: Sample GUC (490-168891-1) was analyzed for Sulfide. Sulfide as H2S level is calculated at 1303.8 mg/Kg
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Geotechnical
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
Method 351OC: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271365.
Method 351OC: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271367.
Method 8151A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271391.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Nashville
Page 4 of 30 3/19/2019 (Rev. 2)

Definitions/Glossary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Qualifiers
GC/MS Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
GI®ssarV ---- —
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 30 3/19/2019 (Rev. 2)

Client Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Client Sample ID: GUC
Date Collected: 02/19/19 12:00
Date Received: 02/21/19 08:55
TestAmerica Job ID: 490-168891-1
Lab Sample ID: 490-168991-1
Matrix: Sludge
Method: EPA 8260D - Volatile Organic Compounds by GC/MS - TCLP
Analyte
Result Qualifier
RL MDL
Unit D
1,1-Dichloroethene
ND
0.200
mg/L
1,2-Dichloroethane
ND
0.200
mg/L
i
2-Butanone (MEK)
ND
0.200
mg/L
Benzene
ND
0.200
mg/L
Carbon tetrachloride
ND
0.200
mg/L
Chlorobenzene
ND
0.200
mg/L
Chloroform
ND
0.200
mg/L
Tetrachloroethene
ND
0.200
mg/L
Trichloroethene
ND
0.200
mg/L
Vinyl chloride
ND
0.200
mg/L
Surrogate %Recovery Qualifier
1,2-Dichloroethane-d4 (Surr) 89
4-Bromofluorobenzene (Surr) 81
Dibromofluoromethane (Surr) 106
Toluene-d8 (Surr) 100
Prepared Analyzed
Dil Fac
02/26/19 09:23
1
02/26/19 09:23
1
02/26/19 09:23
1
-M26/10 09:23
1
02/26/19 09:23
1
02/26/19 09:23
1
02/26/19 09:23
1
02/26/19 09:23
1
02/26/19 09:23
1
02/26/19 09:23
1
Limits
Prepared Analyzed
DH Fac
73 -143
02726/19 09:23
1
61-123
02/26/19 09:23
1
68 -128
02/26/19 09:23
1
75 -124
02/26/19 09:23
1
Method: 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL
1,4-Dichlorobenzene
ND
0.0500
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0500
Hexachlorobenzene
ND
0.0500
Hexachlorobutadiene
ND
0.0500
Hexachloroethane
ND
0.0500
Nitrobenzene
ND
0.0500
Pentachlorophenol
ND
0.250
Pyridine
ND
0.100
Cresols
ND
0.100
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
mg/L
02/26/19 12:10
02/27/1917:24
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
76
25-112
02/26/19 12:10
02/27/19 17:24
1
2-Fluorophenol (Surr)
91
61-105
02/26/19 12:10
02127119 17:24
1
2-Fluorobiphenyl
93
62-105
0212611912:10
02127119 17:24
1
Nitrobenzene-d5 (Surr)
94
64-105
02/26/19 12:10
02127119 17:24
1
Phenol-d5 (Surr)
85
47-105
02/26/19 12:10
02/27/19 17:24
1
Terphenyl-d14 (Surr)
84
45-130
02/26/19 12:10
02/27/19 17:24
1
Method: EPA 8081 D - Organochlorine Pesticides (GC) - TCLP
Analyte Result Qualifier RL
MDL Unit
D Prepared
Analyzed
Dil Fac
j Chlordane (technical)
ND
0.00500
mg/L
02/26/1 111:00
02/27/19 16.03
1
Endrin
ND
0.000500
mg/L
02/26/19 11:00
02/27/1916:03
1
gamma-BHC (Lindane)
ND
0,010500
mg/L
02/26/19 11:00
02/21/19 16:03
1
Heptachlor
ND
0.000500
mg/L
02/26/19 11:00
02/27/1916:03
1
Heptachlor epoxide
ND
0.000500
mg/L
02/26/19 11:00
02/27/19 16:03
1
Methoxychlor
ND
0.000500
mg/L
02/26/19 11:00
02/27/1916:03
1
Toxaphene
ND
0.0400
mg/L
02/26/19 11:00
02/27/1916:03
1
i
TestAmerica
Nashville
Page 6 of 30
3/19/2019
(Rev. 2)

Client Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Client Sample ID: GUC
Date Collected: 02/19/19 12:00
Date Received: 02/21/19 08:55
TestAmerica Job ID: 490-168891-1
Lab Sample ID: 490-166991-1
Matrix: Sludge
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl (Surr)
95
62 -150
02/26/19 11:00
02127119 16:03
1
Tetrachloro-m-xylene
91
54 -138
02/26/19 11:00
02127119 16:03
1
;
Method: EPA 8082A - Polychlorinated
Biphenyls (PCBs) by Gas
Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
PCB-1016
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB-1221
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB-1232
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB-1242
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB-1248
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB-1254
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB-1260
ND
16.4
ug/Kg
02/27/19 09:52
02/2$/19 15:46
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene (Surr)
81
51-116
02/27/19 09:52
02/28/19 15:46
1
DCB Decachlorobiphenyl (Surr)
87
44 -116
02/27/19 09:52
02128119 15:46
1
Method: EPA 8151A - Herbicides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
2,4-D
ND
0.0400
mg/L
02/26/19 14:30
02/28/19 01:14
20
Silvex (2,4,5-TP)
ND
0.0100
mg/L
02/26/19 14:30
02/28/19 01:14
20
2,4,5-T
ND
0.0100
mg/L
02/26/19 14:30
02/28/19 01:14
20
Surrogate %Recovery Qualifier
2,4-Dichlorophenylacetic acid 73
Method: EPA 6010D - Metals (ICP) - TCLP
Analyte Result Qualifier
Arsenic ND
Barium ND
Cadmium ND
Chromium ND
Lead ND
Selenium ND
Silver ND
Method: EPA 7470A - Mercury (CVAA) - TCLP
Analyte Result Qualifier
Mercury ND
General Chemistry
Analyte Result Qualifier
Cyanide, Total ND
Total Sulfide 31.7
Analyte Result Qualifier
Flashpoint >200
Percent Moisture 97.4
Percent Solids 2.6
pH 6.6 HF
Limits
Prepared
Analyzed
Dil Fac
20 -105
02/26/19 14:30
02128119 01:14
20
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.500
mg/L
02/26/19 12:20
02/27/19 09:13
1
2.00
mg/L
02/26/19 12:20
02/27/19 09:13
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:13
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:13
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:13
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:13
1
0.500
mg)L
02/26/19 12:20
02/27/19 69:13
1
RL
MDL
Unit
D
Prepared
Analyzed
oil Fac
0.000200
mg/L
02126/1911:05
02/26/1916:17
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.505
mg/Kg
03/01/1912:40
03/01/1919:32
1
30.0
mg/Kg
02/26/19 09:35
02/26/19 11:20
1
RL
RL
Unit
D
Prepared
Analyzed
Dil Fac
1.00
Degrees F
03/01/19 17:29
1
0.1
%
02/27/19 08:43
1
0.1
%
02/27/19 08A3
1
0.1
SU
02/2711912:00
1
TestAmerica Nashville
Page 7 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 8260D - Volatile Organic Compounds by GC/IDS
Lab Sample ID: LCS 180-271299/3
Matrix: Soled
Analysis Batch: 271299
TestAmerica Job ID: 490-168891-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
1,1-Dichloroethene
0.0400
0.04011
mg/L
100
57-135
1,2-Dichloroethane
0.0400
0.03331
mg/L
83
69 -127
2-Butanone (MEK)
0.0400
0.02829
mg/L
71
36 -150
Benzene
0.0400
0.04064
mg/L
102
66 -124
Carbon tetrachloride
0.0400
0.04205
mg/L
105
69 -130
Chlorobenzene
0.0400
0.04443
mg/L
111
72 -122
Chloroform
0.0400
0.03950
mg/L
99
69-119
Tetrachloroethene
0.0400
0.04642
mg/L
116
73-129
Trichloroethene
0.0400
0.04744
mg/L
119
75 -122
Vinyl chloride
0.0400
0.03919
mg/L
98
57 -132
LCS LCS
Surrogate %Recovery Qualifier Limits
1, 2-Dichloroethane-d4 (Surr) 80 73 -143
4-Bromofluorobenzene (Surr) 97 61-123
Dibromofluoromethane (Surr) 105 68-128
Toluene-d8 (Surr) 103 75-124
Lab Sample ID: LB 180-271312/1-A
Matrix: Solid
Analysis Batch: 271299
LB LB
Analyte Result Qualifier
1,1-Dichloroethene ND
1,2-Dichloroethane ND
2-Butanone (MEK) ND
Benzene ND
Carbon tetrachloride ND
Chlorobenzene ND
Chloroform ND
Tetrachloroethene ND
Trichloroethene ND
Vinyl chloride ND
LB LB
Surrogate %Recovery Qualifier
1,2-Dichloroethane-d4 (Surr) 85
4-Bromofluorobenzene (Surr) 82
Dibromofluoromethane (Surr) 102
L Toluene-d8 (Surr) 104
-Lab Sample ID: 490-168891-1 MS
Matrix: Sludge
Analysis Batch: 271299
Client Sample ID: Method Blank
Prep Type: TCLP
RL
MDL Unit
D Prepared Analyzed
Dil Fac
0.0500
mg/L
02/26/19 09:01
1
0.0500
mg/L
02/26/19 09:01
1
0.0500
mg/L
02/26/19 09:01
1
0.0500
mg)L
02/26/19 69:01
1
0.0500
mg/L
02/26/19 09:01
1
0.0500
mg/L
02/26/19 09:01
1
0.0500
m9/L
02/26/16 69:01
1
0.0500
mg/L
02/26/19 09:01
1
0.0500
mg/L
02/26/19 09:01
1
0.0500
mg/L
02/26/19 09:01
1
Limits
Prepared Analyzed
Dil Fac
73 -143
02/26/19 09:01
1
61-123
02/26/19 09:01
1
68 -128
02/26/19 09:01
1
75 -124
02/26%19 69:01
1
Client Sample ID: GUC
Prep Type: TCLP
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
1,1-Dichloroethene ND
1.60
1.556 mg/L
97 57-135
1,2-Dichloroethane ND
1.60
1.409 mg/L
88 69-127
i 2-Butanone(MEK) ND 1.60 0.8771 mg/L 55 36-150
TestAmerica Nashville
Page 8 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: 490-168891-1 MS Client Sample ID: GUC
Matrix: Sludge Prep Type: TCLP
Analysis Batch: 271299
Sample Sample
Analyte
Result Qualifier
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Spike
MS MS
Added
Result Qualifier
1.60
1.613
1.60
1.711
1.60
1.768
1.60
1.638
1.60
1.815
1.60
1.869
1.60
1.383
MS MS
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 85 73-143
4-Bromofluorobenzene (Surr) 98 61-123
Dibromofluoromethane (Surr) 104 68-128
Toluene-d8 (Surr) 101 75-124
Lab Sample ID: 490-168891-1 MSD
Matrix: Sludge
Analysis Batch: 271299
Sample Sample
Analyte
Result Qualifier
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
2-Butanone (MEK)
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
%Rec.
Unit
D %Rec
Limits
mg/L
101
66 -124
mg/L
107
69 -130
mg/L
Ill
72 -122
mg/L
102
69 -119
mg/L
113
73 -129
mg/L
117
75 -122
mg/L
86
57 -132
Client Sample ID: GUC
Prep Type: TCLP
Spike
Added
MSD MSD
Result Qualifier
Unit
D %Rec
%Rec.
Limits
RPD
RPD
Limit
1.60
1.702
mg/L
106
57 -135
9
35
1.60
1.434
mg/L
90
69 -127
2
16
1.60
0.9013
mg/L
56
36 -150
3
35
1.66
1.638
mg/L
1 U
66 -124
2
16
1.60
1.689
mg/L
106
69 -130
1
17
1.60
1.798
mg/L
112
72 -122
2
15
1.60
1.639
mg/L
102
69 -119
0
16
1.60
1.882
mg/L
118
73 -129
4
15
1.60
1.879
mg/L
117
75 -122
1
15
1.60
1.558
mg/L
97
57 -132
12
21
MSD MSD
Surrogate %Recovery Qualifier Limits
1, 2-Dichloroethane-d4 (Surr) 67 73 -143
4-Bromofluorobenzene (Surr) 99 61-123
Dibromofluoromethane (Surr) 106 68-128
Toluene-d8 (Surr) 105 75 -124
Method: 8270E - Semivolatile Organic Compounds (GC/IDS)
Lab Sample ID: NIB 180-271367/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
MB MB
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed Dil Fac
1,4-Dichlorobenzene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
2,4,5-Trichlorophenol
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
2,4,6-Trichlorophenol
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
2,4-Dinitrotoluene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
TestAmerica Nashville
Page 9 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: 8270E - Selv'livolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 180-271367/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
MB MB
Analyte Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed Dil Fac
Hexachlorobenzene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
Hexachlorobutadiene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
Hexachloroethane
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
Nitrobenzene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
Pentachlorophenol
ND
0.250
mg/L
02/26/19 12:10
02/27/19 09:11 1
Pyridine
ND
0.100
mg/L
02/26/19 12:10
02/27/19 09:11 1
Cresols
ND
0.100
mg/L
02/26/19 12:10
02/27/19 09:11 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4,6-Tribromophenol (Surr)
83
25-112
02/26/19 12:10
02/27/19 09:11 1
2-Fluorophenol (Surr)
87
61-105
02126119 12:10
02/27/19 09:11 1
2-Fluorobiphenyl
83
62 -105
02/26/19 12:10
02127119 09:11 1
Nitrobenzene-d5 (Surr)
83
64-166
02/26/19 12:10
62dXm 69:11 1
Phenol-d5 (Surr)
86
47-105
02/26/19 12:10
02/27/19 09:11 1
Terphenyl-d14 (Surr)
75
45-130
02/26/19 12:10
02127119 09:11 1
Lab Sample ID: LCS 180-27136712-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,4-Dichlorobenzene
0.250
0.2277
mg/L
91
57-100
2,4,5-Trichlorophenol
0.250
0.2157
mg/L
86
58 -100
2,4,6-Trichlorophenol
0.250
0.2096
mg/L
84
57-100
2,4-Dinitrotoluene
0.250
0.2023
mg/L
81
40-100
Hexachlorobenzene
0.250
0.1527
mg/L
61
38 -100
Hexachlorobutadiene
0.250
0.2146
mg/L
86
53 -105
Hexachloroethane
0.250
0.2352
mg/L
94
57 -100
Nitrobenzene
0.250
0.2299
mg/L
92
56 -103
Pentachlorophenol
0.250
0.1630 J
mg/L
65
16 -100
Pyridine
0.250
0.2391
mg)L
96
51 -107
Cresols
0.750
0.6754
mg/L
90
54 -103
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
2, 4, 6-Tribromophenol (Surr) 88
25 -112
2-Fluorophenol (Surr) 90
61-105
2-Fluorobiphenyl 86
62 -105
Nitrobenzene-d5 (Surr) 90
64-105
Phenol-d5 (Surr) 90
47-105
LTerphenyl-d14 (Surr) 69
45-130
r-
Lab Sample ID: LCSD 180-271367/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
1,4-Dichlorobenzene
0.250
0.2220
mg/L
89
57-100 3 16
2,4,5-Trichlorophenol
0.250
0.2095
mg/L
84
58-100 3 16
TestAmerica Nashville
Page 10 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 180-27136713-A
Matrix: Solid
Analysis Batch: 271438
Analyte
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Cresols
TestAmerica Job ID: 490-168891-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch:271367
Spike
LCSD LCSD
%Rec. RPD
Added
Result Qualifier Unit
D %Rec
Limits RPD Limit
0.250
0.2135
mg/L
85
57-100 2 15
0.250
0.1977
mg/L
79
40 -100 2 15
0.250
0.1553
mg/L
62
38 -100 2 16,
0.250
0.2085
mg/L
83
53 -105 3 15
0.250
0.2259
mg/L
90
57 -100 4 18
0.250
0.2141
mg/L
86
56 -103 7 15
0.250
0.1462 J
mg/L
58
16 -100 11 24
0.250
0.2257
mg/L
90
51 -107 6 18
0.750
0.6719
mg/L
90
54 -103 1 17
Surrogate
LCSD LCSD
%Recovery Qualifer
Limits
2,4,6-Tribromophenol (Surr)
86
25-112
2-Fluorophenol (Surr)
86
61-105
2-Fluorobiphenyl
86
62 -105
Nitrobenzene-d5 (Surr)
84
64 -105
Phenol-d5 (Surr)
86
47 -105
Terphenyl-d14 (Surr)
68
45-130
Lab Sample ID: LB 180-271274/1-D
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271438
Prep Batch: 271367
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
ND
0.0500
mg/L
02/26/1912:10
02/2711911:33
1
2,4,5-Trichlorophenol
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
2,4,6-Trichlorophenol
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
2,4-Dinitrotoluene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Hexachlorobenzene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Hexachlorobutadiene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Hexachloroethane
ND
0.0500
mg/L
02/26/1912:10
02127/1611:33
1
Nitrobenzene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Pentachlorophenol
ND
0.250
mg/L
02/26/1912:10
02/27/1911:33
1
Pyridine
ND
0.100
mg/L
02/26/1912:10
02/2711911:33
1
Cresols
ND
0.100
mg/L
02/26/1912:10
02127/1911:33
1
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol(Surr)
88
25-112
02/2611 112.10
02/27/191133
1
2-Fluorophenol (Surr)
85
61-105
02/26/19 12:10
02/27/19 11:33
1
2-Fluorobiphenyl
85
62-105
02/26/19 12:10
02/27/19 11:33
1
Nitrobenzene-d5 (Surr)
87
64 -105
02/26/19 12:10
02/am 11:33
1
Phenol-d5 (Surr)
87
47-105
02/26/19 12:10
02127119 11:33
1
Terphenyl-d14 (Surr)
74
45-130
02/26/19 12:10
02127119 11:33
1
TestAmerica Nashville
Page 11 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Method: EPA 8001 B - ®rganochlorine Pesticides (GC)
Lab Sample ID: MB 180-271365/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271475
Prep Batch: 271365
MB MB
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed Dil Fac
Chlordane (technical)
ND
0.00500
mg/L
02/26/19 11:00
02/27/19 13:14 1
Endrin
ND
0.000500
mg/L
02/2611911:00
02/27/1913:14 1
gamma-BHC (Lindane)
ND
0.000500
mg/L
02/26/19 11:00
02/27/19 13:14 1
Heptachlor
ND
0.000500
mg/L
02/26/1911:00
02/27/1913:14 1
Heptachlor epoxide
ND
0.000500
mg/L
02/26/1911:00
02/27/1913:14 1
Methoxychlor
ND
0.000500
mg/L
02/26/1911:00
02/27/1913:14 1
Toxaphene
ND
0.0400
mg/L
02/26/1911:00
02/27/1913:14 1
MB MB
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
,Surrogate
DCB Decachlorobiphenyl (Surr)
94
62-150
02/26/19 11:00
02127119 13:14 1
Tetrachloro-m-xylene
91
54-138
0212611911:00
0212711913:14 1
Lab Sample ID: LCS 180-271365/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271475
Prep Batch: 271365
Spike LCS LCS
%Rec.
Analyte
Added Result Qualifier
Unit
D %Rec
Limits
Endrin
0.0100 0.009924
mg/L
99
71 -134
gamma-BHC (Lindane)
0.0100 0.008481
mg/L
85
66 -127
Heptachlor
0.0100 0.009290
mg/L
93
66 -134
Heptachlor epoxide
0.0100 0.008870
mg/L
89
65 -141
Methoxychlor
0.0100 0.01001
mg/L
100
59 -131
LCS LCS
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surr)
95
62-150
Tetrachloro-m-xylene
96
54 -138
Lab Sample ID: LCSD 180-271365/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271475
Prep Batch: 271365
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier Unit
D %Rec
Limits RPD Limit
Endrin
0.0100
0.009900
mg/L
99
71 -134 0 18
gamma-BHC (Lindane)
0.0100
0.008743
mg/L
87
66 -127 3 15
Heptachlor
0.0100
0.009428
mg/L
94
66-134 1 15
Heptachlor epoxide
0.0100
0.008791
mg/L
88
65 -141 1 15
Methoxychlor
0.0100
0.009889
mg/L
99
59 -131 1 28
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surf)
95
62-150
Tetrachloro-m xylene
93
54 -138
TestAmerica Nashville
Page 12 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA 8081 B - ®rganochlorine Pesticides (GC) (Continued)
Lab Sample ID: LB 180-271274/16-E
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271475
Prep Batch: 271365
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Chlordane (technical)
ND
0.00500
mg/L
02/26/19 11:00
02/27/19 14:15 1
Endrin
ND
0.000500
mg/L
02/26/19 11:00
02/27/19 14:15 1
gamma-BHC (Lindane)
ND
0.000500
mg/L
02/26/19 11:00
02/27/19 14:15 1
Heptachlor
ND
0.000500
mg%L
0 2/26/19 1 1: 0 0
02/2 7 /19 14:15 1
Heptachlor epoxide
ND
0.000500
mg/L
02/26/19 11:00
02/27/19 14:15 1
Methoxychlor
ND
0.000500
mg/L
02/26/19 11:00
02/27/19 14:15 1
Toxaphene
ND
0.0400
mg/L
02/26/1911:00
02/27/1914:15 1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCB Decachlorobiphenyl (Surr)
98
62 -150
02/26/19 11:00
02/27/19 14:15 1
Tetrachloro-m-xylene
92
54 -138
02/26/19 11:00
02127119 14:15 1
Method: EPA 8082A - Polychlorinated
Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: MB 180-271476/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271567
Prep Batch: 271476
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
PCB-1016
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
PCB-1221
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
PCB-1232
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
PCB-1242
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
PCB-1248
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
PCB-1254
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
PCB-1260
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed DH Fac
Tetrachloro-m-xylene (Surr)
91
51-116
02/27/19 09.52
6212811 113.54 1
DCB Decachlorobiphenyl (Surr)
94
44-116
02127119 09:52
02/28/19 13:54 1
ILab Sample ID: LCS 180-271476/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271567
Prep Batch: 271476
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier Unit
D %Rec
Limits
PCB-1016
1330
1090 ug/Kg
82
57 -114
PCB-1260
1330
1059 ug/Kg
79
55-112
LCS LCS
Surrogate %Recovery Qualifier
Limits
Tetrachloro-m-xylene (Surr)
85
51-116
DCB Decachlorobiphenyl (Surr)
87
44 -116
TestAmerica Nashville
Page 13 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Lab Sample ID: 490-168890-B-1-J MS
Matrix: Solid
Analysis Batch: 271567
Sample Sample
Analyte Result Qualifier
PCB-1016 ND
PCB-1260 ND
Spike MS MS
Added Result Qualifier
1330 908.3
1330 933.1
MS MS
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene (Surr) 66 51-116
DCB Decachlorobiphenyl (Surr) 72 44 -116
Lab Sample ID: 490-168890-B-1-K MSD
Matrix: Solid
Analysis Batch: 271567
Sample Sample
Analyte Result Qualifier
PCB-1016 ND
PCB-1260 ND
Spike
MSD MSD
Added
Result Qualifier
1290
831.7
1290
837.2
MSD MSD
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene (Surr) 64 51-116
DCB Decachlorobiphenyl (Surr) 71 44 -116
Method: EPA 8151A - Herbicides (GC)
Lab Sample ID: MB 180-271391/1-A
Matrix: Solid
Analysis Batch: 271555
MB MB
Analyte
Result Qualifier
RL
2,4-D
ND
0.0400
Silvex (2,4,5-TP)
ND
0.0100
2,4,5-T
ND
0.0100
MB MB
Surrogate %Recovery
Qualifier
Limits
2,4-Dichlorophenylacetic acid
71
20-105
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 271476
%Rec.
Unit D %Rec Limits
ug/Kg 68 57-114
ug/Kg 70 55-112
e,
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 271476
%Rec. RPD
Unit
D %Rec Limits RPD Limit
ug/Kg
64 57-114 9 34
ug/Kg
65 55 -112 11 16
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271391
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/19 14:30
02/27/19 20:57
20
mg/L
02/26/19 14:30
02/27/19 20:57
20
mg/L
02/26/19 14:30
02/27/19 20:57
20
Prepared
Analyzed
DY Fac
02/26/19 14:30
02/27/19 20:57
20
Lab Sample ID: LCS 180-271391/2-A
Matrix: Solid
Analysis Batch: 271555
Spike
LCS LCS
Analyte
Added
Result Qualifier
2,4-D
0.200
0.1340
Silvex (2,4,5-TP)
0.0500
0.03454
2,4,5-T
0.0500
0.02981
LCS LCS
Surrogate %Recovery Qualifier
Limits
2,4-Dichlorophenylacetic acid 67
20-105
Client Sample I
Unit D %Rec
mg/L 67
mg/L 69
mg/L 60
D:
10-100
23-109
11-101
TestAmerica Nashville
Page 14 of 30
3/19/2019 (Rev. 2)

CSC Sample Results
1
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 6151A - Herbicides (GC) (Continued)
Lab Sample ID: LCSD 180-271391/3-A
Matrix: Solid
Analysis Batch: 271555
Analyte
2,4-D
Silvex (2,4,5-TP)
2,4,5-T
TestAmerica Job ID: 490-168891-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 271391
Spike
LCSD LCSD
%Rec. RPD
Added
Result Qualifier Unit
D %Rec
Limits RPD Limit
0.206
0.1578
mg/L
79
10 -100 16 35
0.0500
0.04003
mg/L
80
23 -109 15 35
0.0500
0.03558
mg/L
71
11 -101 18 35
LCSD LCSD
Surrogate %Recovery Qualifier Limits
2,4-Dichlorophenylacetic acid 78 20-105
Lab Sample ID: LB 180-271274/16-G
Matrix: Solid
Analysis Batch: 271555
LB LB
Analyte Result Qualifier RL
2,4-D ND 0.0400
Silvex (2,4,5-TP) ND 0.0100
2,4,5-T ND 0.0100
LB LB
Surrogate %Recovery Qualifier Limits
2,4-Dichlorophenylacetic acid 60 20-105
Method: EPA 6010D - Metals (ICP)
Lab Sample ID: MB 180-271355/1-A
Matrix: Solid
Analysis Batch: 271499
MB MB
Analyte
Result Qualifier
RL
Arsenic
ND
0.0500
Barium
ND
0.200
Cadmium
ND
0.0500
Chromium
ND
0.0500
Lead
ND
0.0500
Selenium
ND
0.0500
Silver
ND
0.0500
Lab Sample ID: LCS 180-271355/2-A
Matrix: Solid
Analysis Batch: 271499
Analyte
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 271391
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/19 14:30
02/27/19 22:24
20
mg/L
02/26/19 14:30
02/27/19 22:24
20
mg/L
02/26/19 14:30
02/27/19 22:24
20
Prepared
Analyzed
Dil Fac
62126 9 19 14:30
02/27/19 22:24
20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271355
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
Spike
Added
LCS LCS
Result Qualifier
0.500
0.5281
2.00
2.051
0.0500
0.05449
0.200
0.2054
0.500
0.5102
0.500
0.5558
0.0500
0.05381
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271355
%Rec.
Unit
D %Rec
Limits
mg/L
106
80 -120
mg/L
103
80 -120
mg/L
109
80 -120
mg/L
103
80 -120
mg/L
102
80-120
mg/L
111
80 -120
mg/L
108
80 -120
TestAmerica Nashville
Page 15 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 6010D - Metals (ICP) (Continued)
Lab Sample ID: LB 180-271274/1-C
Matrix: Solid
Analysis Batch: 271499
LB LB
Analyte
Result Qualifier
RL
Arsenic
ND
0.500
Barium
ND
2.00
Cadmium
ND
0.500
Chromium
ND
0.500
Lead
ND
0.500
Selenium
ND
0.500
Silver
ND
0.500
Method: EPA 7470A - Mercury (CVAA)
Lab Sample ID: MB 180-271342/1-A
Matrix: Solid
Analysis Batch: 271395
MB MB
Analyte Result Qualifier
Mercury ND
Lab Sample ID: LCS 180-271342/2-A
Matrix: Solid
Analysis Batch: 271395
Analyte
LMercury
Lab Sample ID: LB 180-271274/1-B
Matrix: Solid
Analysis Batch: 271395
LB LB
Analyte Result Qualifier
Mercury ND
Lab Sample ID: 180-86915-A-1-1 MS
Matrix: Solid
Analysis Batch: 271395
TestAmerica Job ID: 490-168891-1
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 271355
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/1912:20
02/27/1 008.00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
. .
mg/L
... ....
02/26/19 12:20
. ..
02/27/19 08:00
1
RL MDL Unit
0.000200 mg/L
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271342
D Prepared Analyzed Dil Fac
02/26/1911:05 02/26/1916:00 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271342
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
0.00 550 0.002605 mg/L 104 80 -120
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 271342
RL MDL Unit D Prepared Analyzed Dil Fac
0.000200 mg/L 02/26/1911:05 02/26/1916:02 1
Client Sample ID: Matrix Spike
Prep Type: TCLP
Prep Batch: 271342
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Mercury
ND
0.00500
0.005020
mg/L
100
75 -125
Lab Sample ID: 180-86915-A-1-J MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Mercury
ND
0.00500
0.005026
mg/L
101
75-125 0 20
TestAmerica Nashville
Page 16 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: 1010A - Ignitability, pensky-Martens Closed -Cup Method
Lab Sample ID: MB 490-578372/1
Matrix: Solid
Analysis Batch: 578372
MB MB
Analyte Result Qualifier RL
Flashpoint >200 1.00
Lab Sample ID: LCS 490-578372/2
Matrix: Solid
Analysis Batch: 578372
TestAmerica Job ID: 490-168891-1
Client Sample ID: Method Blank
Prep Type: Total/NA
RL Unit D Prepared Analyzed Dil Fac
Degrees F 03/01/19 17:29 1
Client Sample ID: Lab Control Sample El
Prep Type: Total/NA
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Flashpoint 81.0 81.20 Degrees F 100 94 -106
Lab Sample ID: LCSD 490-578372/14
Matrix: Solid
Analysis Batch: 578372
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Flashpoint 81.0 83.40 Degrees F 103 94 -106 3 20
Lab Sample ID: 280-120182-A-1 DU
Matrix: Solid
Analysis Batch: 578372
Sample Sample
Analyte Result Qualifier
Flashpoint 128
DU DU
Result Qualifier Unit D
134.3 Degrees F
Client Sample ID: Duplicate
Prep Type: Total/NA
RPD
RPD Limit
5 10
Method: 2540G - SM 2540G
Lab Sample ID: 180-86358-B-20 DU Client Sample ID: Duplicate
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271450
Sample Sample DU DU RPD
Analyte Result Qualifier Result Qualifier Unit D RPD Limit
Percent Moisture 26.5 28.2 % 6 10
Percent Solids 73.5 71.8 % 2 10
Method: EPA 9012B - Cyanide, Total andor Amenable
Lab Sample ID: MB 180-271760/4-A
Matrix: Solid
Analysis Batch: 271809
MB MB
Analyte Result Qualifier_ _ RL
Cyanide, Total ND 0.500
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271760
MDL Unit D Prepared Analyzed Dil Fac
mg/Kg 03/01/1912:40 03/01/1919:23 1
Lab Sample ID: HLCS 180-27176012-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271809 Prep Batch: 271760
Spike HLCS HLCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Cyanide, Total 0.260 0.2479 mg/Kg 99 90 -110
TestAmerica Nashville
Page 17 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 9012B - Cyanide, Total andor Amenable (Continued)
Lab Sample ID: LCS 180-271760/3-A
Matrix: Solid
Analysis Batch: 271809
Analyte
LCyanide, Total
Lab Sample ID: LLCS 180-271760/1-A
Matrix: Solid
Analysis Batch: 271809
Analyte
Cyanide, Total
Lab Sample ID: 180-87076-D-1-B MS
Matrix: Solid
Analysis Batch: 271809
Sample Sample
Analyte Result Qualifier
Cyanide, Total 0.655
Lab Sample ID: 180-87076-D-1-C MSD
Matrix: Solid
Analysis Batch: 271809
Sample Sample
Analyte Result Qualifier
Cyanide, Total 0.655
TestAmerica Job ID: 490-168891-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271760
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
190 114.2 mg/Kg 60 26 -139
Client Sample ID: Lab Control Sample IM
Prep Type: Total/NA
Prep Batch: 271760
Spike LLCS LLCS %Rec.
Added Result Qualifier Unit D %Rec Limits
0.0500 0.04970 mg/Kg 99 90 -110
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 271760
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
5.05 5.182 mg/Kg 90 75 -125
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 271760
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
5.05 5.268 mg/Kg 91 75 -125 2 20
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 180-271319/1-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271334 Prep Batch: 271319
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
[-Total Sulfide ND 30.0 mg/Kg 02/26/19 09:35 02/26/19 11:15 1
Lab Sample ID: LCS 180-27131912-A
Matrix: Solid
Analysis Batch: 271334
1 Analyte
1 Total Sulfide
FLab Sample ID: 490-168890-B-1-C MS
Matrix: Solid
Analysis Batch: 271334
Sample Sample
Analyte Result Qualifier
Total Sulfide 57.0
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271319
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
150 144.3 mg/Kg 97 85 -115
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 271319
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
150 223.2 mg/Kg 111 75 -125
TestAmerica Nashville
Page 18 of 30
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: 490-168890-B-1-D MSD Client Sample ID: Matrix Spike Duplicate
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271334 Prep Batch: 271319
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Total Sulfide 57.0 149 209.1 mg/Kg 102 75.125 7 20
Method: EPA 9045D -
Lab Sample ID: LCS 180-271506/1
Matrix: Solid
Analysis Batch: 271506
Analyte
pH
r Lab Sample ID: 180-86977t1-1 DU
Matrix: Solid
Analysis Batch: 271506
Sample Sample
Analyte Result Qualifier
pH 3.6
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
7.00 7.0 SU 101 99-101
Client Sample ID: Duplicate
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
3.6 SU 0 2
TestAmerica Nashville
Page 19 of 30 3/19/2019 (Rev. 2)

QC Association Summary
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville V TP
GC/MS VOA
Analysis Batch: 271299
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 GUC
TCLP
Sludge
EPA 8260D
271312
LB 180-271312/1-A Method Blank
TCLP
Solid
EPA 8260D
271312
LCS 180-271299/3 Lab Control Sample
Total/NA
Solid
EPA 8260D
490-168891-1 MS GUC
TCLP
Sludge
EPA 8260D
271312
490-168891-1 MSD GUC
TCLP
Sludge
EPA 8260D
271312
Leach Batch: 271312
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch 11111110111111
490-168891-1 GUC
TCLP
Sludge
EPA 1311
LB 180-271312/1-A Method Blank
TCLP
Solid
EPA 1311
490-168891-1 MS GUC
TCLP
Sludge
EPA 1311
490-168891-1 MSD GUC
TCLP
Sludge
EPA 1311
GUMS Semi VOA
Leach Batch: 271274
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
EPA 1311
LB 180-271274/1-D
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 271367
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
3510C
271274
LB 180-271274/1-D
Method Blank
TCLP
Solid
3510C
271274
MB 180-271367/1-A
Method Blank
Total/NA
Solid
3510C
LCS 180-271367/2-A
Lab Control Sample
Total/NA
Solid
3510C
LCSD 180-271367/3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Analysis Batch: 271438
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
8270E
271367
LB 180-271274/1-D
Method Blank
TCLP
Solid
8270E
271367
180-271367/1-A
Method Blank
Total/NA
Solid
8270E
271367
1MB
LCS 180-271367/2-A
Lab Control Sample
Total/NA
Solid
8270E
271367
LCSD 180-271367/3-A
Lab Control Sample Dup
Total/NA
Solid
8270E
271367
GC Semi VOA
Leach Batch: 271274
FLab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
EPA 1311
LB 180-271274/16-E
Method Blank
TCLP
Solid
EPA 1311
LB 180-271274/16-G
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 271365
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
_
490-168891-1
GUC
_
TCLP
Sludge
3510C
271274
LB 180-271274/16-E
Method Blank
TCLP
Solid
3510C
271274
MB 180-271365/1-A
Method Blank
Total/NA
Solid
3510C
LCS 180-271365/2-A
Lab Control Sample
Total/NA
Solid
3510C
TestAmerica Nashville
Page 20 of 30 3/19/2019 (Rev. 2)

QC Association Summary
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
I
GC Semi VOA (Continued) —
—
Prep Batch: 271365 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LCSD 180-271365/3-A Lab Control Sample Dup
Total/NA
Solid
3510C
Prep Batch: 271391
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 GUC
TCLP
Sludge
8151A
271274
LB 180-271274/16-G Method Blank
TCLP
Solid
8151A
271274
MB 180-271391/1-A Method Blank
Total/NA
Solid
8151A
111011111111
LCS 180-271391/2-A Lab Control Sample
TotaVNA
Solid
8151A
WIN
LCSD 180-271391/3-A Lab Control Sample Dup
TotaVNA
Solid
8151A
Analysis Batch: 271475
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 GUC
TCLP
Sludge
EPA 80816
271365
LB 180-271274/16-E Method Blank
TCLP
Solid
EPA 8081 B
271365
MB 180-271365/1-A Method Blank
Total/NA
Solid
EPA 8081B
271365
LCS 180-271365/2-A Lab Control Sample
Total/NA
Solid
EPA 8081B
271365
LCSD 180-271365/3-A Lab Control Sample Dup
Total/NA
Solid
EPA 8081 B
271365
Prep Batch: 271476
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 GUC
Total/NA
Sludge
3541
MB 180-271476/1-A Method Blank
Total/NA
Solid
3541
LCS 180-271476/2-A Lab Control Sample
Total/NA
Solid
3541
490-168890-B-1-J MS Matrix Spike
TotaVNA
Solid
3541
490-168890-B-1-K MSD Matrix Spike Duplicate
Total/NA
Solid
3541
Analysis Batch: 271555
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 GUC
TCLP
Sludge
EPA 8151A
271391
LB 180-271274/16-G Method Blank
TCLP
Solid
EPA 8151A
271391
MB 180-271391/1-A Method Blank
TotaVNA
Solid
EPA 8151A
271391
LCS 180-271391/2-A Lab Control Sample
Total/NA
Solid
EPA 8151A
271391
LCSD 180-271391/3-A Lab Control Sample Dup
Total/NA
Solid
EPA 8151A
271391
Analysis Batch: 271567
r-
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
Total/NA
Sludge
EPA 8082A
271476
MB 180-271476/1-A
Method Blank
Total/NA
Solid
EPA 8082A
271476
LCS 180-271476/2-A
Lab Control Sample
TotaVNA
Solid
EPA 8082A
271476
490-168890-B-1-J MS
Matrix Spike
Total/NA
Solid
EPA 8082A
271476
490-168890-B-1-K MSD
Matrix Spike Duplicate
Total/NA
Solid
EPA 8082A
271476
Metals
Leach Batch: 271274
Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
,F-Lab
490-168891-1
GUC
TCLP
Sludge
EPA 1311
LB 180-271274/1-B
Method Blank
TCLP
Solid
EPA 1311
LB 180-271274/1-C
Method Blank
TCLP
Solid
EPA 1311
180-86915-A-1-1 MS
Matrix Spike
TCLP
Solid
EPA 1311
TestAmerica Nashville
Page 21 of 30 3/19/2019 (Rev. 2)

CSC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
(Metals (Continued
TestAmerica Job ID: 490-168891-1
Leach Batch: 271274 (Continued)
�Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
180-86915-A-1-J MSD Matrix Spike Duplicate TCLP Solid EPA 1311
Prep Batch: 271342
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-168891-1
GUC
TCLP
Sludge
7470A
LB 180-271274/1-B
Method Blank
TCLP
Solid
7470A
MB 180-271342/1-A
Method Blank
Total/NA
Solid
7470A
LCS 180-271342/2-A
Lab Control Sample
Total/NA
Solid
7470A
180-86915-A-1-1 MS
Matrix Spike
TCLP
Solid
7470A
180-86915-A-1-J MSD
Matrix Spike Duplicate
TCLP
Solid
7470A
Prep Batch: 271355
Lab Sample ID
490-168891-1
LB 180-271274/1-C
MB 180-271355/1-A
LCS 180-271355/2-A
Analysis Batch: 271395
Lab Sample ID
490-168891-1
LB 180-271274/1-B
MB 180-271342/1-A
LCS 180-271342%2-A
180-86915-A-1-1 MS
180-86915-A-1-J MSD
Prep Batch
271274
271274
271274
271274
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
GUC
TCLP
Sludge
3010A
271274
Method Blank
TCLP
Solid
3010A
271274
Method Blank
Total/NA
Solid
3010A
Lab Control Sample
Total/NA
Solid
3010A
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
GUC
TCLP
Sludge
EPA 7470A
271342
Method Blank
TCLP
Solid
EPA 7470A
271342
Method Blank
Total/NA
Solid
EPA 7470A
271342
Lab Control Sample
Total/NA
Solid
EPA 7470A
271342
Matrix Spike
TCLP
Solid
EPA 7470A
271342
Matrix Spike Duplicate
TCLP
Solid
EPA 7470A
271342
Analysis Batch: 271499
Lab Sample ID
Client Sample ID
490-168891-1
GUC
LB 180-271274/1-C
Method Blank
MB 180-271355/1-A
Method Blank
LCS 180-271355/2-A
Lab Control Sample
General Chemistry
Prep Type
Matrix
Method
Prep Batch
TCLP
Sludge
EPA 601 OD
271355
TCLP
Solid
EPA 601 OD
271355
Total/NA
Solid
EPA 601 OD
271355
Total/NA
Solid
EPA 601 OD
271355
Prep Batch: 271319
FLab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168891-1
GUC
Total/NA
Sludge
9030B
MB 180-271319/1-A
Method Blank
Total/NA
Solid
9030B
LCS 180-271319/2-A
Lab Control Sample
Total/NA
Solid
9030B
490-168890-B-1-C MS
Matrix Spike
Total/NA
Solid
9030B
L490-168890-B-1-D MSD
Matrix Spike Duplicate
Total/NA
Solid
9030B
Analysis Batch: 271334
F
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
Total/NA
Sludge
EPA 9034
271319
MB 180-271319/1-A
Method Blank
Total/NA
Solid
EPA 9034
271319
LCS 180-271319/2-A
Lab Control Sample
Total/NA
Solid
EPA 9034
271319
490-168890-B-1-C MS
Matrix Spike
Total/NA
Solid
EPA 9034
271319
TestAmerica Nashville
Page 22 of 30
3/19/2019 (Rev. 2)

CSC Association Summary
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
General Chemistry (Continued)
Analysis Batch: 271334 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-B-1-D MSD Matrix Spike Duplicate
Total/NA
Solid
EPA 9034
271319
Analysis Batch: 271450
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 GUC
Total/NA
Sludge
2540G
180-86358-B-20 DU Duplicate
Total/NA
Solid
2540G
Analysis Batch: 271506
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 GUC
Total/NA
Sludge
EPA 9045D
LCS 180-271506/1 Lab Control Sample
Total/NA
Solid
EPA 9045D
180-86977-J-1 DU Duplicate
Total/NA
Solid
EPA 9045D
Prep Batch: 271760
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 GUC
Total/NA
Sludge
9012B
MB 180-271760/4-A Method Blank
Total/NA
Solid
9012B
HLCS 180-271760/2-A Lab Control Sample
Total/NA
Solid
9012B
LCS 180-271760/3-A Lab Control Sample
Total/NA
Solid
9012E
LLCS 180-271760/1-A Lab Control Sample
Total/NA
Solid
9012B
180-87076-D-1-B MS Matrix Spike
Total/NA
Solid
9012E
180-87076-D-1-C MSD Matrix Spike Duplicate
Total/NA
Solid
9012E
Analysis Batch: 271809
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
Total/NA
Sludge
EPA 9012B
271760
MB 180-271760/4-A
Method Blank
Total/NA
Solid
EPA 9012B
271760
HLCS 180-271760/2-A
Lab Control Sample
Total/NA
Solid
EPA 9012B
271760
LCS 180-271760/3-A
Lab Control Sample
Total/NA
Solid
EPA 9012E
271760
LLCS 180-271760/1-A
Lab Control Sample
Total/NA
Solid
EPA 9012B
271760
180-87076-D-1-B MS
Matrix Spike
Total/NA
Solid
EPA 9012E
271760
180-87076-D-1-C MSD
Matrix Spike Duplicate
Total/NA
Solid
EPA 9012E
271760
Analysis Batch: 578372
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168891-1
GUC
Total/NA
Sludge
1010A
MB 490-578372/1
Method Blank
Total/NA
Solid
1010A
LCS 490-578372/2
Lab Control Sample
Total/NA
Solid
1010A
LCSD 490-578372/14
Lab Control Sample Dup
Total/NA
Solid
1010A
280-120182-A-1 DU
Duplicate
Total/NA
Solid
1010A
TestAmerica Nashville
Page 23 of 30 3/19/2019 (Rev. 2)

Lab Chronicle
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Client Sample ID: GUC
Date Collected: 02/19/19 12:00
Date Received: 02/21/19 08:55
Batch
Batch
Prep Type
Type
Method Run
TCLP
Leach
EPA 1311
TCLP
Analysis
EPA 8260D
TCLP
Leach
EPA 1311
TCLP
Prep
3510C
TCLP
Analysis
8270E
TCLP
Leach
EPA 1311
TCLP
Prep
3510C
TCLP
Analysis
EPA 8081B
Total/NA
Prep
3541
Total/NA
Analysis
EPA 8082A
TCLP
Leach
EPA 1311
TCLP
Prep
8151A
TCLP
Analysis
EPA 8151A
TCLP
Leach
EPA 1311
TCLP
Prep
3010A
TCLP
Analysis
EPA 601 OD
TCLP
Leach
EPA 1311
TCLP
Prep
7470A
TCLP
Analysis
EPA 7470A
Total/NA
Analysis
1010A
Total/NA
Analysis
2540G
Total/NA
Prep
9012B
Total/NA
Analysis
EPA 9012B
Total/NA
Prep
9030E
Total/NA
Analysis
EPA 9034
Total/NA
Analysis
EPA 9045D
TestAmerica Job ID: 490-168891-1
Lab Sample ID: 490-166691-1
Matrix: Sludge
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
25 g
500 mL
271312
02/26/19 08:16
TAH
TAL PIT
1
0.125 mL
5 mL
271299
02/26/19 09:23
KLG
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
200 mL
10.0 mL
271367
02/26/19 12:10
CBY
TAL PIT
1
1 mL
1 mL
271438
02/27/19 17:24
VVP
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
100 mL
40.0 mL
271365
02/26/19 11:00
CBY
TAL PIT
1
271475
02/27/19 16:03
DFE
TAL PIT
15.2 g
20.0 mL
271476
02/27/19 09:52
BAP
TAL PIT
1
271567
02/28/19 15:46
JMO
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
100 mL
10.0 mL
271391
02/26/19 14:30
CBY
TAL PIT
20
271555
02/28/19 01:14
JBF
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
5 mL
50 mL
271355
02/26/19 12:20
NAM
TAL PIT
1
271499
02/27/19 09:13
RJG
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
50 mL
50 mL
271342
02/26/19 11:05
RJR
TAL PIT
1
271395
02/26/19 16:17
KAK
TAL PIT
1
578372
03/01/19 17:29
VRP
TAL NSH
1
271450
02/27/19 08:43
JMS
TAL PIT
0.99 g
50 mL
271760
03/01/19 12:40
BSH
TAL PIT
1
271809
03/01/19 19:32
JAS
TAL PIT
5.00 g
50 mL
271319
02/26/19 09:35
SES
TAL PIT
1
271334
02/26/19 11:20
SES
TAL PIT
1
20 mL
20 mL
271506
02/27/19 12:00
JMS
TAL PIT
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
Page 24 of 30 3/19/2019 (Rev. 2)

Method Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Method
Method Description
Protocol
Laboratory
EPA 8260D
Volatile Organic Compounds by GC/MS
SW846
TAL PIT
8270E
Semivolatile Organic Compounds (GC/MS)
SW846
TAL PIT
EPA 8081B
Organochlorine Pesticides (GC)
SW846
TAL PIT
EPA 8082A
Polychlorinated Biphenyls (PCBs) by Gas Chromatography
SW846
TAL PIT
EPA 8151A
Herbicides (GC)
SW846
TAL PIT
EPA 6010D
Metals (ICP)
SW846
TAL PIT
EPA 7470A
Mercury (CVAA)
SW846
TAL PIT
1010A
Ignitability, Pensky-Martens Closed -Cup Method
SW846
TAL NSH
2540G
SM 2540G
SM22
TAL PIT
EPA 9012B
Cyanide, Total andor Amenable
SW846
TAL PIT
EPA 9034
Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL PIT
EPA 9045D
pH
SW846
TAL PIT
3010A
Preparation, Total Metals
SW846
TAL PIT
3510C
Liquid -Liquid Extraction Se arato Funnel
( P ry )
SW846
TAL PIT
3541
Automated Soxhlet Extraction
SW846
TAL PIT
5030C
Purge and Trap
SW846
TAL PIT
7470A
Preparation, Mercury
SW846
TAL PIT
8151A
Extraction (Herbicides)
SW846
TAL PIT
9012B
Cyanide, Total and/or Amenable, Distillation
SW846
TAL PIT
9030E
Sulfide, Distillation (Acid Soluble and Insoluble)
SW846
TAL PIT
EPA 1311
TCLP Extraction
SW846
TAL PIT
Protocol References:
SM22 = Standard Methods For The Examination Of Water And Wastewater, 22nd Edition
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
Page 25 of 30 3/19/2019 (Rev. 2)

Accreditation/Certification Summary
Client Bio-Nomics Services- Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville V TP
Laboratory: TestArnerica Nashville
The accreditations/certifications listed below are applicable
to this report.
Authority Program
EPA Region Identification Number
Expiration Date
South Carolina State Program
4 84009 ( 001)
02-28-19
Laboratory: TestAmerica Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under
each accreditation/certification below.
Authority Program
EPA Region Identification Number
Expiration Date
South Carolina State Program
4 89014
04-30-19
The following analytes are included in this report, but the laboratory is
not certified by the governing authority. This
list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method
Matrix
Analyte
254OG
Sludge
Percent Moisture
2540G
Sludge
Percent Solids
8270E 3510C
Sludge
1,4-Dichlorobenzene
8270E 3510C
Sludge
2,4,5-Trichlorophenol
8270E 3510C
Sludge
2,4,6-Trichlorophenol
8270E 3510C
Sludge
2,4-Dinitrotoluene
8270E 3510C
Sludge
Cresols
8270E 3510C
Sludge
Hexachlorobenzene
8270E 3510C
Sludge
Hexachlorobutadiene
8270E 3510C
Sludge
Hexachloroethane
8270E 3510C
Sludge
Nitrobenzene
8270E 3510C
Sludge
Pentachlorophenol
8270E 3510C
Sludge
Pyridine
EPA 8151A 8151A
Sludge
2,4,5-T
EPA 8151A 8151A
Sludge
2,4-D
EPA 8151A 8151A
Sludge
Silvex (2,4,5-TP)
EPA 8260D
Sludge
1,1-Dichloroethene
EPA 8260D
Sludge
1,2-Dichloroethane
EPA 8260D
Sludge
2-Butanone (MEK)
EPA 8260D
Sludge
Benzene
EPA 8260D
Sludge
Carbon tetrachloride
EPA 8260D
Sludge
Chlorobenzene
EPA 8260D
Sludge
Chloroform
EPA 8260D
Sludge
Tetrachloroethene
EPA 8260D
Sludge
Trichloroethene
EPA 8260D
Sludge
Vinyl chloride
EPA 9012B 9012B
Sludge
Cyanide, Total
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
TestAmerica Nashville
Page 26 of 30 3/19/2019 (Rev. 2)

L,—Al L44ek
TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN COOLER RECEIPT FORIII 490-168891 Chain of Custody
Cooler Received/Opened On 2/21/2019 @ 8:55
Time Samples Removed From CoolerTime Samples Placed In Storage �� (2 Hour Window)
1. Tracking # (last 4 digits, FedEx) Courier: FedEx
i
IR Gun ID 17960358 pH Strip Lot ChlorinneeStrip Lot
2. Temperature of rep. sample or temp blank when opened: Y19 Degrees Celsius
3. If Item #2 temperature is 0°C or less, was the representative sample or temp blank frozen? YES NO..6A�l
4. Were custody seals on outside of cooler? / ry , /,S...NO... NA
If yes, how many and where: l ° / `v✓
5. Were the seals intact, signed, and dated correctly? I ... NO ... NA
6. Were custody papers inside cooler? O...NO... NA
I certify that I opened the cooler and answered questions 1-6 (intial)
7. Were custody seals on containers: YES NO and Intact YES ... NO.. -NA
Were these signed and dated correctly? YES ... NO... A
8. Packing mat'I used? Bubblewrap Plastic bag Peanuts Vermiculite Foam Insert Paper Other None`
9. Cooling process: Ice Ice -pack Ice (direct contact) Dryice Other None
10. Did all containers arrive in good condition (unbroken)? S ..NO ... NA
11. Were all container labels complete (#, date, signed, pres., etc)?
ES ..NO ... NA
12. Did all container labels and tags agree with custody papers?
ES ..NO ... NA
13a. Were VOA vials received?
YES .I O..NA
b. Was there any observable headspace present in any VOA vial?
YES ... NO..�IA)
® #M
Larger than this.
14. Was there a Trip Blank in this cooler? YES. NO.. NA If multiple coolers, sequence #
I certify that I unloaded the cooler and answered questions 7-14 (intial)
15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level?
YES ... NO.NA
SO
b. Did the bottle labels indicate that the correct preservatives were used
ES
16. Was residual chlorine present?
YES ... NO.&
'D ,
I certify that I checked for chlorine and pH as per SOP and answered questions 15-16 (intial)
17. Were custody papers properly filled out (ink, signed, etc)?
E ... NO ... NA
18. Did you sign the custody papers in the appropriate place?
•YE ... NO ... NA
1 19. Were correct containers used for the analysis requested?
YE ...NO...NA
20. Was sufficient amount of sample sent in each container?
YE ... NO ... NA
I certify that I entered this project into LIMS and answered questions 17.20 (intial)
X
I certify that I attached a label with the unique LIMS number to each container (intial)•
21. Were there Non -Conformance issues at login? YE 1� Was a NCM generated? CES ..NO...#
BI5 = Broken in shipment
Cooler Receipt Folm.doc LF-I
End oPFolm
Page 27 of 30
Revised 8/23/17 i
3/19/2019 (Rev. 2)

Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
nhone 615.726 0177 fax [phone]
Chariot;
Chain of Custody Record
I
1613 91 TestAmenoca
THE LEADER IN ENVIRONMENTAL TESTING
TrctA mar;ra 7.ahnra}nrinc Tnr
Client Contact
Project Manager: Vaughn Stevenson
Site Contact:
Date: 2/20/19
COC No:
Bio-Nomic Services
Tel/Fax:
Lab Contact: Ken Hayes
Carrier: Feder
1 of 1 COCs
516 Rountree Road
U
a
a
F
U
v�i
1
F
>
°:
F
a
F
a
F
U
3
7
a
a
999
w
cU
Job No.
Charlotte, NO 28217
Calendar ( C ) or Work Days (W)
704-529-0000
TAT if different from Below
0 2 weeks
0 I week
0 2 days
l day
_r
q?
b:
SDG No.
Project Name: Greenville WTP
State: NC
P O# 48761
Sample Identification
Sample
Date
Sample
Time
Sample
Type
Matrix
our
Cont.'
Sample Specific Notes:
GUC
2/19/2019
1200
"solid
'solid
X
X
I X
X
X
X
X
X
X
'Use Alternate Matrix: Sludge
-l7
D)
(D
N
tb
D
W
0
Preservation Used: 1= Ice, 2-- HC1; 3= H2SO4; 4=H•NO3; rNaOH; 6= Other
Possible Hazard Identification
0 Non -Hazard 0 Flammable =Skin Irritant Poison B Unknown
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
0 Return To Client Disposal By Lab 0 Archive For Months
Special Instructions/QC Requirements & Comments: "Alternate Matrix: Sludee
1
Relinquished by:
Company:
Date/Time:
Reep*�ed'bv:
Company:
r
Date f ime:
(31 �It� 1 O'5-Yb
Relinquished by t\
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Client Information (Sub Contract Lab) Hayes. Ken 490=168B91 Chain of Custody 330.1
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TestArnerica Laboratories, Inc.
Slate Program -North Carolina (WWISW); Slate Program-...
490-168891-1
Address:
Do"Date Requested:
Pfusorvalion Codes:
301 Alpha Drive. RIDC Park,
212212019
Analysis Requested
A-l1CL M-Iie.ano
City
TAT Requested (days):
8-NaOH N-None
Pittsburgh
C-Zn A.celale 0-AsNaO2
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?4.te' Since laboratory actreddalioAs are subject to change, TeslArnenca Laboralones, Inc. places the owneiship of roomed. an a!yte R accredila Unti compliance upon Dui subcontract labour tones. This sample shipment is forvardod or:'r charn-of-cuslody If the laboratory does not
currently mamtam accreditation in the State of Origin used aoove for anaPpsl:Jtestymalnx being ana!yzod, the samples must be shipped back to the Tdsilvicenca lanoratoryDr other ,nsuucbons irdl oo prov,ded Any changus to attieditalwn status should bebrought to TestAmorlca
Labaa[or,es, Inc otienUon—enomly if av iequenied accreddabons are current tr, date, lelurn the signed Chain of Cuslody ahesting to said rornpLeance In TeslAntenca Laboratories, Inc
Possible Hazard Identification
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
Unconfirmed/
=1Refurn To Client =Disposal By LabArchive For Months
I
Deliverable Requested: I. II, III, IV, Other (specify) Primary Deliverable Rank: 2
Special Instructions/OC Requirements:
Empty Kit Relinquished by. Date: Time. Methai ul sn pment.
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Login Sample Receipt Checklist
Client: Bio-Nomics Services., Inc. Job Number: 490-168891-1
SDG Number:
Login Number: 168891 List Source: TestAmerica Pittsburgh
List Number: 2 List Creation: 02/23/19 11:33 AM
Creator: Say, Thomas C
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
TestAmerica Nashville
Page 30 of 30 3/19/2019 (Rev. 2)

BIO-NOMIC SERVICES, INC. - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: Most Restrictive Result of all samples
McCall Permit No. WQ0003823
Mineralization Rate 0.20 45.80 % Solids
8.4 off
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.740
17,400.000
34.800
Phosphorus
0.306
3,060.000
6.120
Potassium
0.293
2,930.000
5.860
PAN (incorporated)*
On
` P.M
PAN (surface)*
0.452
4,518.000
9.036
Ammonia Nitrogen
0.243
2,430.000
4.860
Calcium
2.850
28,500.000
57.000
Calcium Carbonate Eq.
9.100
91,000.000
182.000
Magnesium
---
4,750.000
9.500
Sodium
---
369.000
0.738
Sulfur
---
3,870.000
7.740
Nitrate N / Nitrite N
---
309.000
0.618
Barium
---
---
---
Chloride
---
---
---
Iron
---
12,200.000
24.400
Aluminum
---
18,900.00
37.800
Arsenic
---
5.000
0.010
Cadmium
---
1.000
0.002
Chromium
---
182.000
0.364
Copper
---
95.70
0.191
Lead
---
23.90
0.048
Mercury
---
0.063
0.000
Molybdenum
---
2.740
0.005
Nickel
---
75.30
0.151
Selenium
---
5.000
0.010
Zinc
---
356.00
0.712
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.36
Ceiling Concen.
75
85
840
57
75
420
100
7,50,

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 20, 2019
McCall Farms #1 Permit No. WQ0003823
Mineralization Rate 0.20 32.10 % Solids
8.4 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,001
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.740
17,400.000
34.800
Phosphorus
0.306
3,060.000
6.120
Potassium
0.293
2,930.000
5.860
PAN (incorporated)*
55€ €€
`:: ::
' ' : 6'•
PAN (surface)*
0.429
4,292.800
8.586
Ammonia Nitrogen
0.243
2,430.000
4.860
Calcium
1.690
16,900.000
33.800
Calcium Carbonate Eq.
3.500
35,000.000
70.000
Magnesium
---
4,750.000
9.500
Sodium
---
369.000
0.738
Sulfur
---
3,870.000
7.740
Nitrate N / Nitrite N
---
83.800
0.168
Barium
---
---
---
Chloride
---
---
---
Iron
---
11,700.000
23.400
Aluminum
---
17,600.00
35.200
Arsenic
---
5.000
0.010
Cadmium
---
1.000
0.002
Chromium
---
182.000
0.364
Copper
---
95.70
0.191
Lead
---
23.90
0.048
Mercury
---
0.042
0.000
Molybdenum
---
2.740
0.005
Nickel
---
75.30
0.151
Selenium
---
5.000
0.010
Zinc
---
356.00
0.712
Waypoint Analytical 19-052-0206
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.36
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

' o
Wa 0
nt,�
ANALYTICAL
3/1 /2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-052-0206
Project Description: McFar #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/21/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam• rr 6—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
Alt
Page 1 of 6

(2)
PARTICAL
��� 7621 Whitepine Road, Richmond, VA 23237
Way
Main 804-743-9401° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-052-0206
Client Project Description: McFar #1
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
64890
McFar #1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
64890
McFar #1
Solids
WTN: Waypoint Analyticai -TN, Memphis, TN, Certification: #1354
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
02/20/2019
07:30
02/21/2019
SM-254OG
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
Page 2 of 6

Report Number: 19-052-0206
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 64890
Sample Id : McFar #1
Waypoi nt(D
ANALYTICAL
Project: McFar #1
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 2/20/2019 07:30:00
Date Received: 02/21 /2019 00:00
Date Reported: 03/01/2019
Total Solids *
32.10
321000
100.0
CJR
02/26/2019 15:35
SM-2540G
Moisture "
67.90
100.0
CJR
02/26/2019 15:35
SM-254OG
Total Kjeldahl Nitrogen
1.74
17400
250
CLP
02/28/2019 11:30
SM-4500-NH3C-TKN
Phosphorus
0.31
3060
50.0
KKM
02/26/2019 21:45
6010D
Potassium
0.29
2930
50.0
KKM
02/26/2019 21:45
6010D
Sulfur
0.39
3870
50.0
KKM
02/26/2019 21:45
6010D
Calcium
1.69
16900
250
KKM
02/26/2019 21:45
601 OD
Magnesium
0.48
4750
50.0
KKM
02/26/2019 21:45
6010D
Sodium
0.04
369
250
KKM
02/27/201917:47
6010D
Iron
11700
50.0
KKM
02/26/2019 21:45
601 OD
Aluminum
17600
50.0
KKM
02/26/2019 21:45
6010D
Manganese
66.5
5.00
KKM
02/26/2019 21:45
6010D
Copper
95.7
2.50
KKM
02/26/2019 21:45
6010D
Zinc
356
12.5
KKM
02/27/201917:47
6010D
Ammonia Nitrogen
0.24
2430
100
ZBD
02/27/2019 14:00
SM-4500-NH3C
Organic N
1.50
14970
250
02/27/2019 14:00
CALCULATION
Nitrate+Nitrite-N
83.8
4.76
ZBD
02/26/201914:19
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. ' /
B-Analyte detected in blank H - Beyond Holding Time Wje. me 64W
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Paurlc• MCGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior- written authorization. Agronomist
Page 3 of 6

Report Number: 19-052-0206
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 64890
Sample Id : McFar #1
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH "
Calcium Carbonate Equivalent
Molybdenum
Chloride
Comments:
Waypoint0 (D
ANALYTICAL
Project : McFar #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OF ANALYSIS Date Sampled: 2/20/2019 07:30:00
Date Received: 02/21/2019 00:00
Date Reported: 03/01/2019
<1.00
1.00
KKM
02/26/2019 21:45
601 OD
182
2.50
KKM
02/26/2019 21:45
6010D
75.3
2.50
KKM
02/26/2019 21:45
6010D
23.9
3.00
KKM
02/26/2019 21:45
6010D
<5.00
5.00
KKM
02/26/2019 21:45
6010D
0.0419
0.0139
TJS
02/26/201911:09
SW-7471B
<5.00
5.00
KKM
02/26/2019 21:45
6010D
8.4
JSL
02/27/2019 08:36
9045D
3.50 35000
1000
DXT
02/26/2019 11:00
AOAC 955.01
2.74
2.50
KKM
02/26/2019 21:45
601 OD
436
200
JM
02/25/201910:25
SM-4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part; nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Page 4 of 6
pwi4 imp Gewr
Pauric McGroary
Agronomist

i Wayp®int-
Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]"6
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-052-0206
Shipping Method
• Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
I* Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
• Not Required
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
• Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
• Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: 113randi Watson Date & Time: 2/21/2019 14:09:52
Page 5 of 6

WASTEWATER SAMPLE TRANSMITTAL FC /C IN.Oft'UST'06' '.
Waypoint Analytical
7621 Whitcpinc Road Richmond VA 23237 Tel: [phone] fax: [phone] [mail: supportva«;waypointan alytical.com
'R"!
Customer Information
Account #
45671
submffted By Charge To Illllllllllllllllllllllillllllllllllllllllllllllllllllllllll p�j 20196
Bio-Nomic Services, Inc. Bio-Nomic Services, Inc.
Bio-Nomic Servics Inc 11:05:43
530 Woodlawn Street 530 Wo Al $ McFar#1
o awn treet
Belmont, NC 28012 Belmont, NC 28012
vstevenson bio-nomic.com
Project . ' Phone: [phone] Fax: E- mail:, ,,;_,�,_,;,,� _ „
Sample Information
Lab Number
Collection Information
Container information
Please Write in Decked Tests
Sample ID
p
Only)
Type
Date
Time
Number
Type
Volumed
Npqlf
PJ
�_L
i
1 `''fit
2A/
Nt�
�`�i;
!�°�
�`�'
rv"CO3ok W
of Bottles
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K
aV
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PA, -,.-
Sal
—N
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Grab
/% C�
ZJZalt
�' ��Ai�
Glass
oz
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t
roc FA
_ Grab
7 �{ y F
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—
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— Composite
i
_
-"Plastic
pint
✓ qt
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— Grab
— Composite
2�
—1 pa;�,,t
/ '
1
_ Glass
Plastic
— °Ini
�pt
_ Grab
_ Glass
— °Z
pint
— Composite
— Plastic
at
Date I Time
Test Available SPI
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate 8 Organic Nitrogen. n
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, 1 V C•
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
b; � �
ctions or Remarks

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
i'
Residual Type: Wastewater Treatment Plant
Date Sampled: February 20, 2019
'i
McCall Farms #2 Permit No. WQ0003823
Mineralization Rate 0.20 42.50 %.Solids
8.4 nH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
0.998
9,980.000
19.960
Phosphorus
0.240
2,400.000
4.800
Potassium
0.260
2,600.000
5.200
PAN (incorporated)*...3
........................3,3,i1..........,...........................
C 4f�.,..
PAN (surface)*
0.247
2,468.200
4.936
Ammonia Nitrogen
0.153
1,530.000
3.060
Calcium
2.850
28,500.000
57.000
Calcium Carbonate Eq.
0.100
1,000.000
2.000
Magnesium
---
4,270.000
8.540
Sodium
---
323.000
0.646
Sulfur
---
2,930.000
5.860
Nitrate N / Nitrite N
---
13.200
0.026
Barium
---
---
--- f
Chloride
---
---
--- 11
Iron
- -
11,500.000
23.000
Aluminum
---
17,100.00
34.200
Arsenic
---
5.000
0.010
Cadmium
---
1.000
0.002
Chromium
---
161.000
0.322
Copper
---
71.70
0.143
Lead
---
20.30
0.041
Mercury
---
0.060
0.000
Molybdenum
---
2.500
0.005
Nickel
---
67.50
0.135
Selenium
---
5.000
0.010
Zinc
---
271.00
0.542
Waypoint Analytical 19-052-0207
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.31
Ceiling Concen.
75
85
840
57
75
420
100
7.501

(D
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
3/1 /2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-052-0207
Project Description: McFar #2
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/21/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
l ' sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P":.'r&fi-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
`S s [Ct �Rds
a � Y
Page 1 of 6

0
•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-052-0207
rliant Prniart rlaerrintinne MrFar *7
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
SM-2540G
WTN
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
SW-7471B
WTN
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
SM-4500-NH3C-TKN
WTN
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
4500NO3F-2011
WTN
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
6010D
WTN
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
SM-4500-NH3C
WTN
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
9045D
WTN
64891
McFar #2
Solids
02/20/2019 07:45
02/21/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Report Number: 19-052-0207
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 64891
Sample Id : McFar #2
Waypoint(D
ANALYTICAL
Project : McFar #2
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 2/20/2019 07:45:00
Date Received: 02/21 /2019 00:00
Date Reported: 03/01/2019
Total Solids *
42.50
425000
100.0
CJR
02/26/2019 15:35
SM-2540G
Moisture *
57.50
100.0
CJR
02/26/2019 15:35
SM-2540G
Total Kjeldahl Nitrogen
1.00
9980
250
CLP
02/28/2019 11:30
SM-4500-NH3C-TKN
Phosphorus
0.24
2400
50.0
KKM
02/26/2019 21:15
601 OD
Potassium
0.26
2600
50.0
KKM
02/26/2019 21:15
6010D
Sulfur
0.29
2930
50.0
KKM
02/26/2019 21:15
6010D
Calcium
2.85
28500
250
KKM
02/26/2019 21:15
6010D
Magnesium
0.43
4270
50.0
KKM
02/26/2019 21:15
601 OD
Sodium
0.03
323
250
KKM
02/27/201917:52
601 OD
Iron
11500
50.0
KKM
02/26/2019 21:15
601 OD
Aluminum
17100
50.0
KKM
02/26/2019 21:15
601 OD
Manganese
58.3
5.00
KKM
02/26/2019 21:15
6010D
Copper
71.7
2.50
KKM
02/26/2019 21:15
6010D
Zinc
271
12.5
KKM
02/27/201917:52
6010D
Ammonia Nitrogen
0.15
1530
100
ZBD
02/27/2019 14:00
SM-4500-NH3C
Organic N
0.85
8450
250
02/27/2019 14:00
CALCULATION
Nitrate+Nitrite-N
13.2
4.78
ZBD
02/26/201914:19
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding
Time
I f��6
�'� ///
tic 6QON
Our reports and letters are for the exclusive and confidential use of our clients, and
may not be reproduced in whole or part, nor may any reference be made
Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public
announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number: 19-052-0207
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 64891
Sample Id : McFar #2
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH'
Calcium Carbonate Equivalent
Molybdenum
Chloride
Comments:
Waypoint(D
ANALYTICAL
Project: McFar #2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OF ANALYSIS Date Sampled: 2/20/2019.07:45:00
Date Received: 02/21/2019 00:00
Date Reported: 03/01/2019
<1.00
1.00
KKM
02/26/2019 21:15
6010D
161
2.50
KKM
02/26/2019 21:15
6010D
67.5
2.50
KKM
02/26/2019 21:15
6010D
20.3
3.00
KKM
02/26/2019 21:15
6010D
<5.00
5.00
KKM
02/26/2019 21:15
6010D
0.0603
0.0153
TJS
02/26/2019 11:11
SW-7471 B
<5.00
5.00
KKM
02/26/2019 21:15
6010D
8.4
JSL
02/27/2019 08:36
9045D
<0.10 <1000
1000
DXT
02/26/2019 11:00
AOAC 955.01
<2.50
2.50
KKM
02/26/2019 21:15
6010D
368
200
JM
02/25/201910:25
SM-4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Page 4 of 6
me GWr
Pauric McGroary
Agronomist

(D
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-052-0207
Shipping Method
• Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers received F 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
• Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
• N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
No
Comments:
Signature: 113randi Watson Date & Time: 2/21/2019 14:27:12
Page 5 of 6

WASTEWATER SA�/iPI'E TIC A 1SMITTAI
b 4 t Waypoint Analytical
7621 Whitepinc Road Richmond VA 23237 Tel: [phone] Fax: R04-371-f
19-052-0207
111111111111Jill 11111111111111111111111111111111111111111Jill Jill 45671-201 s
Bio-Nomic Servics Inc 14:16-00
Account #
45671
Customer Information
Submitted By Charge
Bio-Nomic Services, Inc.
Bio-Nomic Services, Inc.
530 Woodlawn Street
530 Woodlawn Street
Belmont, NC 28012 Belmont, NC 28012
Phone: [phone] Fax: Email: [e-mail]@willeoxmabesoil.com
Project
Sample Information
Lab Number
Collection Information
Container Information
Please Write in Desired Tests
Sample ID
(Lab Use
Only)
Type
Date
Time
Number
of Bottles
Type
volume
TkN
N14LI-9
A103_n!
p
K.
j, (
Na
r �ti
At. G
1.
CC!
C�
/J:
Apt
/L'
11
G.
n
L
l ,t
l L
;t• �?
,,'�`.{..`','
Grab
_Composite
_Grab
_Composite
/ {
L1 �G'I 14I
-1'JL' i
1 / Jj
/ �' ` I
7
l
i
Glass
Plastic
_Glass
✓Plastic
°a
— pint
n2
--
—pint
II
I
Grab
Composite
Zh
ft
Glass
I:/:Plastic
ainI
_p
(t
i
I
Grab
Composite
_ Glass
Plastic
—I
— o2
—pint
at '
I
F
I
Relinquished By: Signature
Date
Time
Received By: (Signature)
Date
Time
Test Available
Special Instructions or Remarks
Nitrogen Series: Total Kieldahl, Ammonium, Nitrate 8 Organic Nitrogen.
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver, Nickel, Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
J� � / J
r

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
i
Residual Type: Wastewater Treatment Plant
Date Sampled: April 1, 2019
McCall Farms #3 Permit No. WQ0003823
Mineralization Rate 0.20 43.10 % Solids
7.9 DH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.100
11,000.000
22.000
Phosphorus
0.174
1,740.000
3.480
Potassium
0.197
1,970.000
3.940
PAN (incorporated)*
............................................................
ii 3� 73
`©6i$L10
13
PAN (surface)*
0.272
2,717.800
5.436
Ammonia Nitrogen
0.070
696.000
1.392
Calcium
1.700
17,000.000
34.000
Calcium Carbonate Eq.
9.100
91,000.000
182.000
Magnesium
---
2,950.000
5.900
Sodium
---
250.000
0.500
Sulfur
---
2,060.000
4.120
Nitrate N / Nitrite N
---
309.000
0.618
Barium
---
---
---
Chloride
---
---
---
Iron
---
12,200.000
24.400
Aluminum
---
18,900.00
37.800
Arsenic
---
5.000
0.010
Cadmium
---
1.000
0.002
Chromium
---
124.000
0.248
Copper
---
50.50
0.101
Lead
---
15.20
0.030
Mercury
---
0.051
0.000
Molybdenum
---
2.500
0.005
Nickel
---
50.00
0.100
Selenium
---
5.000
0.010
Zinc
---
189.00
0.378
Waypoint Analytical 19-092-0211
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.30
Ceiling Concen.
(Mg/Kg)
75
85
840
57
75
420
100
7,50,

Waypoint(D
ANALYTICAL
4/10/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-092-0211
Project Description: Biosolid 3
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/2/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam. a, 6—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 Pennsylvania 68-03109 Virginia 460014
South Carolina 93007
New Jersey VA011
Florida E871087
North Carolina 257
Page 1 of 8

yPAnWat(D
NALYTICAL
Client: Bio-Nomic Servics Inc
Project: Biosolid 3
Lab Report Number: 19-092-0211
Date: 4/10/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 65680 (3)
Analyte: Aluminum
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Iron
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Sodium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate, (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Phosphorus
Page 2 of 8

WayPA��nty 0
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Lead
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L429733/L429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: 1-429733/1-429542
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 3 of 8

Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-092-0211
Client Project Description: Biosolid 3
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65680
3
Solids
04/01/2019
09:00
04/02/2019
65680
3
Solids
04/01/2019
09:00
04/02/2019
SM-2540G
WTN
65680
3
Solids
04/O1/2019
09:00
04/02/2019
SW-7471B
WTN
65680
3
Solids
04/O1/2019
09:00
04/02/2019
SM-4500-NH3C-TKN
WTN
65680
3
Solids
04/O1/2019
09:00
04/02/2019
4500NO3F-2011
WTN
65680
3
Solids
04/O1/2019
09:00
04/02/2019
6010D
WTN
65680
3
Solids
04/O1/2019
09:00
04/02/2019
SM-4500-NH3C
WTN
65680
3
Solids
04/O1/2019
09:00
04/02/2019
9045D
WTN
65680
3
Solids
04/O1/2019
09:00
04/02/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 4 of 8

Report Number: 19-092-0211
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 65680
Sample Id : 3
0 (D
Waypoint
ANALYTICAL
Project : Biosolid 3
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/1/2019 09:00:00
Date Received: 04/02/2019 00:00
Date Reported: 04/10/2019
Total Solids *
43.10
431000
100.0
CJR
04/04/2019 17:59
SM-2540G
Moisture *
56.90
100.0
CJR
04/04/2019 17:59
SM-2540G
Total Kjeldahl Nitrogen
1.10
11000
250
CLP
04/08/2019 13:30
SM-4500-NH3C-TKN
Phosphorus
0.17
1740
50.0
BKN
04/05/201918:43
6010D
Potassium
0.20
1970
50.0
BKN
04/05/201918:43
601OD
Sulfur
0.21
2060
50.0
BKN
04/05/201918:43
601OD
Calcium
1.70
17000
250
BKN
04/05/201918:43
601OD
Magnesium
0.30
2950
50.0
BKN
04/05/201918:43
601OD
Sodium
<0.03
<250
250
BKN
04/05/201918:43
601OD
Iron
12200
50.0
BKN
04/05/201918:43
601OD
Aluminum
18900
50.0
BKN
04/05/201918:43
6010D
Manganese
45.7
5.00
BKN
04/05/201918:43
6010D
Copper
50.5
2.50
BKN
04/05/201918:43
6010D
Zinc
189
12.5
BKN
04/05/201918:43
6010D
Ammonia Nitrogen
0.07
696
100
JPJ
04/08/2019 09:30
SM-4500-NI3C
Organic N
1.03
10304
250
04/08/2019 09:30
CALCULATION
Nitrate+Nitrite-N
309
4.97
ZBD
04/08/201915:45
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding
Time
I oft6
W 601w ' s
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 5 of 8

Report Number: 19-092-0211
•
Account Number: 45671 Wai ooi ■ ■t
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 65680
Sample Id : 3
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH "
Calcium Carbonate Equivalent
Molybdenum
Chloride
Comments:
ANALYTICAL
Project: Biosolid 3
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/1/2019 09:00:00
Date Received: 04/02/2019 00:00
Date Reported: 04/10/2019
<1.00
1.00
BKN
04/05/201918:43
601OD
124
2.50
BKN
04/05/201918:43
6010D
50.0
2.50
BKN
04/05/201918:43
6010D
15.2
3.00
BKN
04/05/201918:43
6010D
<5.00
5.00
BKN
04/05/201918:43
6010D
0.0506
0.0148
US
04/05/2019 13:35
SW-7471 B
<5.00
5.00
BKN
04/05/201918:43
6010D
7.9
JSL
04/08/2019 06:40
9045D
9.10 91000
1000
DXT
04/07/2019 12:01
AOAC 955.01
<2.50
2.50
BKN
04/05/201918:43
6010D
925
200
JM
04/04/201916:40
SM-4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time ?ate« me GQONy
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 6 of 8

• o
ayp®1 n - 7621 ain 8 4-7 Road, Richmond, 27 -6446
Main 804-743-9401 'Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-092-0211
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
• Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
• Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) 7 Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No
Signature: lBrandi Watson Date & Time: 4/02/2019 13:55:40
Page 7 of 8

WASTEWATER SAMPLE TR.
®` 'WaYP
a 7621 Whitcpine Road Richmond VA 23237 Tel: 80d-7t
IIIInIIIIIIIIIIIII a0920211 DDY Account#
llllllllllllllllllllllllllltlllllll1111111111 II oa oz 2019 45671
Bio-Nomic Servics Inc 13:55:18
Binsolid 3
Custom
... .......:...... .
Submitti=d By ,,.,.,.yam ,.. :....... .. ......... vuNy
Bio-Nomic Services, Inc.
Bio-Nomic Services, Inc.
530 Woodlawn Street 530 Woodlawn Street
Belmont, NC 28012 Belmont, NC 28012
E-mail: [e-mail]
Phone: [phone] Fax: [e-mail]
PrOj@Ct . :
Sample Information
Sample ID
Lab Number
(Lab Use
Only)
Collection Information
Type Date Time
Container Information
of Bolles Type Volume
P 11
�3 K
Please Write in De 'red Tests
0
Ca, QI Z„ N� �5 itO /v`�./ (Qr;%3
, 1JgN� S
rab
_Cc omposite
/
I f/ i
� • � � ��
I
Glass
�astic
-p lot
�t
j
j
--Plastic
oz
_- pint
t
,GrabGlass
✓ Composite
5
Grab�k'lastic
✓ Composite
n
Glass
_ oz
pent
t
6
Grab
Composite
Ij 1
I
ZOy
_ Glass
�Rlastic
— 02
pint
t
Date Time
Special Instructions or Remarks
NL d aS S "A„ 9;J 5 0 (r
Relinquished By: (Signature)
D to
Time
Received BY: (Signature)
Tes Available
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
v ke.,

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 1, 2019
McCall Farms #4 Permit No. WQ0003823
Mineralization Rate 0.20 44.80 % Solids
8.2 pH
Parameter
I %
I Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.220
12,200.000
24.400
Phosphorus
0.169
1,690.000
3.380
Potassium
0.189
PAN (incorporated)*
..................
.........3.7.4..€
.€.€....€.............1..,.8..49...0f.1..,.0...t0.).04... .
.....3.780
..............7..i.4.8. ..
PAN (surface)*
0.295
2,950.400
5.901
Ammonia Nitrogen
0.158
1,580.000
3.160
Calcium
1.270
12,700.000
25.400
Calcium Carbonate Eq.
7.100
71,000.000
142.000
Magnesium
---
2,830.000
5.660
Sodium
---
250.000
0.500
Sulfur
---
2,030.000
4.060
Nitrate N / Nitrite N
---
36.400
0.073
Barium
---
---
---
Chloride
---
---
---
Iron
---
9,950.000
19.900
Aluminum
---
15,200.00
30.400
Arsenic
---
5.000
0.010
Cadmium
---
1.000
0.002
Chromium
---
120.000
0.240
Copper
---
54.10
0.108
Lead
---
16.20
0.032
Mercury
---
0.063
0.000
Molybdenum
---
2.500
0.005
Nickel
---
48.70
0.097
Selenium
---
5.000
0.010
Zinc
---
196.00
0.392
Waypoint Analytical 19-092-0212
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.35
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

Waypoin(2)ty
ANALYTICAL
4/10/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-092-0212
Project Description: Biosolid 4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/2/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam. Iff cw-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
c
Page 1 of 6

Waypoint..(2)
ANALYTICAL
Report Number: 19-092-0212
Client Project Description: Biosolid 4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65681
4
Solids
04/01/2019 09:10
04/02/2019
65681
4
Solids
04/01/2019
09:10
04/02/2019
SM-2540G
WTN
65681
4
Solids
04/O1/2019
09:10
04/02/2019
SW-7471B
WTN
65681
4
Solids
04/O1/2019
09:10
04/02/2019
SM-4500-NH3C-TKN
WTN
65681
4
Solids
04/01/2019
09:10
04/02/2019
4500NO3F-2011
WTN
65681
4
Solids
04/01/2019
09:10
04/02/2019
6010D
WTN
65681
4
Solids
04/01/2019
09:10
04/02/2019
SM-4500-111-13C
WTN
65681
4
Solids
04/01/2019
09:10
04/02/2019
9045D
WTN
65681
4
Solids
04/01/2019
09:10
04/02/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Report Number: 19-092-0212
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 65681
Sample Id: 4
Waypoint(D
ANALYTICAL
Project: Biosolid 4
REPORT OFANALYSIS
7621 Whitepirie Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/1/2019 09:10:00
Date Received: 04/02/2019 00:00
Date Reported: 04/10/2019
Total Solids
44.80
448000
100.0
CJR
04/04/2019 17:59
SM-2540G
Moisture "
55.20
100.0
CJR
04/04/2019 17:59
SM-2540G
Total Kjeldahl Nitrogen
1.22
12200
250
CLP
04/08/2019 13:30
SM-4500-NH3C-TKN
Phosphorus
0.17
1690
50.0
BKN
04/06/2019 02:02
6010D
Potassium
0.19
1890
50.0
BKN
04/06/2019 02:02
6010D
Sulfur
0.20
2030
50.0
BKN
04/06/2019 02:02
6010D
Calcium
1.27
12700
250
BKN
04/06/2019 02:02
6010D
Magnesium
0.28
2830
50.0
BKN
04/06/2019 02:02
6010D
Sodium
<0.03
<250
250
BKN
04/06/2019 02:02
601 OD
Iron
9950
50.0
BKN
04/06/2019 02:02
601OD
Aluminum
15200
50.0
BKN
04/06/2019 02:02
601OD
Manganese
42.2
5.00
BKN
04/06/2019 02:02
6010D
Copper
54.1
2.50
BKN
04/06/2019 02:02
6010D
Zinc
196
12.5
BKN
04/06/2019 02:02
6010D
Ammonia Nitrogen
0.16
1580
100
JPJ
04/08/2019 09:30
SM-4500-NH3C
Organic N
1.06
10620
250
04/08/2019 09:30
CALCULATION
Nitrate+Nitrite-N
36.4
4.70
ZBD
04/08/201915:46
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding
Time
pw�&
' /
#1C 60W
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in
whole or part, nor may any reference
be made
Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public
announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number: 19-092-0212
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 65681
Sample Id: 4
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH'
Calcium Carbonate Equivalent
Molybdenum
Chloride
Comments:
Waypoint.(D
ANALYTICAL
Project: Biosolid 4
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/1/2019 09:10:00
Date Received: 04/02/2019 00:00
Date Reported: 04/10/2019
<1.00
1.00
BKN
04/06/2019 02:02
6010D
120
2.50
BKN
04/06/2019 02:02
6010D
48.7
2.50
BKN
04/06/2019 02:02
601OD
16.2
3.00
BKN
04/06/2019 02:02
601OD
<5.00
5.00
BKN
04/06/2019 02:02
6010D
0.0629
0.0145
TJS
04/05/2019 13:36
SW-7471 B
<5.00
5.00
BKN
04/06/2019 02:02
601 OD
8.2
JSL
04/08/2019 06:40
9045D
7.10 71000
1000
DXT
04/07/2019 12:01
AOAC 955.01
<2.50
2.50
BKN
04/06/2019 02:02
6010D
990
200
JM
04/04/201916:40
SM-4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Page 4 of 6
?W�C- #1C Gar`'
Pauric McGroary
Agronomist

(D
"llaypoint,u
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-092-0212
Shipping Method
• Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
• Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
w Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
• Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
• Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
• Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
I* N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
• N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
• N/A
High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature: jBrandi Watson Date & Time: 4/02/2019 14:01:25
Page 5 of 6

_ - 71
WASTEWATER SAMPLE TR
'ODY
r.-
7621 Whitcpinc Road Richmond VA 23237 TcW 0!, II�IIIIIIIIIIIIII�III�IIIIIIIIIIIIIIIIIIIIII�IIIIIIIIIIIIIIIII) o 02
Account #
45671 '
Custor Bio-Nomic Servics Inc
zo�s2
14:01:04
I
-Submitted By BiosoGd a
Bio-Nomic Services, Inc.
To..
oervices, Inc.
530 Woodlawn Street
530 Woodlawn Street
Belmont, NC 28012
Belmont, NC 28012
I
II
Project.'
Phone: [phone]
Fax:
vstevenson bio-nomic.com
E-mail: le-7—!enso�[e-mail]
I I
Sample ID
Lab Number
(Lab Use
Collection Information
ner Information
Please Write in Desired Tests
!
Only)
Type
Date
Time
Wm,,enformation
Type
Volume
T}tN
P��
/1z"
N
%9
l�
%`t�
(0.�3K
✓Composite
�I
, ��
_Glass
A.. C.,
U
�,Grab
— oZ
1
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mastic
—pint
1
—,,Grab
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�i
�' IG AM
—
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qqt
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I
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41
_Grab
✓ Composite
/
`/
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(
— Glass
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� "Composite
,t'
ZD! rr
_Glass
t
l l
— pint
(
_[Plastic
�t
I�
Relin uished B : Si nature)
D(to
Time
Received B : Si nature
Date
Time
ere k
QcF
Z
;
f
Test Available
I
Nitrogen Series: Total Kjeldahl, AmmoniumNitrate &Organic Nitrogen.
Secial Instructions or Remarks,
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium,
�t
Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel, Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
;
i
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
4
r
ll
�I
it
I
/

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 1, 2019
McCall Farms #5 Permit No. WQ0003823
Mineralization Rate 0.20 32.10 % Solids
isi PH
Parameter
Il
I %
I Mg/Kg Dry Weight
(% x 10,001
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.700
17,000.000
34.000
Phosphorus
0.221
2,210.000
4.420
Potassium
0.247
2,470.000
4.940
PAN (incorporated)*
.............
.....................
.......................
PAN (surface)*
0.389
3,891.000
7.782
Ammonia Nitrogen
0.118
1 1,180.000
2.360
Calcium
1.620
16,200.000
32.400
Calcium Carbonate Eq.
8.600
86,000.000
172.000
Magnesium
---
3,960.000
7.920
Sodium
---
289.000
0.578
Sulfur
---
3,130.000
6.260
Nitrate N / Nitrite N
---
137.000
0.274
Barium
---
---
Chloride
---
---
---
Iron
---
9,870.000
19.740
Aluminum
---
15,500.00
31.000
Arsenic
---
5.000
0.010
Cadmium
---
1.000
0.002
Chromium
---
125.000
0.250
Copper
---
70.70
0.141
Lead
---
19.60
0.039
Mercury
---
0.037
0.000
Molybdenum
---
2.500
0.005
Nickel
---
50.90
0.102
Selenium
---
5.000
0.010
Zinc
---
263.00
0.526
Waypoint Analytical 19-092-0213
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.30
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

0 (2)
Waypoint
ANALYTICAL
4/10/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-092-0213
Project Description: Biosolid 5
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/2/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam• of & r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
e ' i
Page 1 of 6

. 7621 Whitepine Road, Richmond, VA 23237
Waypoint Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-092-0213
Cliant Prniart nacrrintinne Rincnlirl 5
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
65682
5
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
04/01/2019
09:15
04/02/2019
SM-2540G
WTN
SW-74716.
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-111-13C
WTN
9045D
WTN
AOAC 955.01
WTN
Page 2 of 6

Report Number: 19-092-0213
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 65682
Sample Id : 5
0 (D
Waypoint
ANALYTICAL
Project : Biosolid 5
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/1/2019 09:15:00
Date Received: 04/02/2019 00:00
Date Reported: 04/10/2019
Total Solids *
32.10
321000
100.0
ADM
04/08/2019 15:25
SM-2540G
Moisture "
67.90
100.0
ADM
04/08/2019 15:25
SM-2540G
Total Kjeldahl Nitrogen
1.70
17000
250
CLP
04/08/2019 13:30
SM-4500-NH3C-TKN
Phosphorus
0.22
2210
50.0
BKN
04/06/2019 02:07
6010D
Potassium
0.25
2470
50.0
BKN
04/06/2019 02:07
6010D
Sulfur
0.31
3130
50.0
BKN
04/06/2019 02:07
601 OD
Calcium
1.62
16200
250
BKN
04/06/2019 02:07
601 OD
Magnesium
0.40
3960
50.0
BKN
04/06/2019 02:07
601 OD
Sodium
0.03
289
250
BKN
04/08/201915:30
601 OD
Iron
9870
50.0
BKN
04/06/2019 02:07
601 OD
Aluminum
15500
50.0
BKN
04/06/2019 02:07
6010D
Manganese
50.5
5.00
BKN
04/06/2019 02:07
6010D
Copper
70.7
2.50
BKN
04/06/2019 02:07
6010D
Zinc
263
12.5
BKN
04/06/2019 02:07
6010D
Ammonia Nitrogen
0.12
1180
100
JPJ
04/08/2019 09:30
SM-4500-NI3C
Organic N
1.58
15820
250
04/08/2019 09:30
CALCULATION
Nitrate+Nitrite-N
137
4.67
ZBD
04/08/201915:46
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. '''' ��/�
B-Analyte detected in blank H - Beyond Holding Time pt�« mC GQGIvr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number: 19-092-0213
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 65682
Sample Id : 5
0 (D
Waypoint
ANALYTICAL
Project : Biosolid 5
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/1/2019 09:15:00
Date Received: 04/02/2019 00:00
Date Reported: 04/10/2019
Cadmium
<1.00
1.00
BKN
04/06/2019 02:07
601 OD
Chromium
125
2.50
BKN
04/06/2019 02:07
6010D
Nickel
50.9
2.50
BKN
04/06/2019 02:07
601 OD
Lead
19.6
3.00
BKN
04/06/2019 02:07
6010D
Arsenic
<5.00
5.00
BKN
04/06/2019 02:07
601 OD
Mercury
0.0365
0.0157
TJS
04/05/2019 13:37
SW-7471 B
Selenium
<5.00
5.00
BKN
04/06/2019 02:07
601 OD
pH *
7.7
JSL
04/08/2019 06:40
9045D
Calcium Carbonate Equivalent
8.60 86000
1000
DXT
04/07/2019 12:01
AOAC 955.01
Molybdenum
<2.50
2.50
BKN
04/06/2019 02:07
6010D
Chloride
970
200
JM
04/04/201916:40
SM-4500CI-D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time I owf�G X GQ41dr
Our- reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist
Page 4 of 6

(D
r 1 aypofnt
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-092-0213
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
f 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample label(s)?
• Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
• Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
• No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
9 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No
Signature: Brandi Watson Date & Time: 4/02/2019 .03.21
Page 5 of 6

Project '
Lab Number
Sample ID (Lab Use
Only)
i
s
6
WASTEWATER SAMPLE TRAI
?Y
W aypo i I I
I
II��II
II��I
IIII
3
"2
7621 Whitepinc Road Richtnond VA 23237
Tel: [phone] Bio-Nomic Servics Inc
2019
14:02:35
Biosolid 5
Customer I
Subrri tied By
k.upy t o
Bio-Nomic Services, Inc.
Bio-Nomic Services, Inc.
530 Woodlawn Street
530 Woodlawn Street
Belmont, NC 28012
Belmont, NC 28012
Rhone: 704-529-0000
Fax:
E-mail: [e-mail]
r Ira tvillcoxmabesoil.com
Sam le Information
Collection Information
Container Information
Please Write in Desired Tests
Type
Date
Time
Number
Type
Volume
IN
P
� Q]
'2,
N
Pt
of Bottles
NO3�/
K
N
Jltw &
C-4
Ar-
_Grab
,,/Composite
I
9:oo !��
f
Glass
— °Z
pint
I
mastic
/qt
j
(�Plastic
v Combposite
I
pint
t
_ Grab
AM
Glass
_ 0z
✓ Composite
(
,=-Raslic
pint
t
_ Grab
�
Z�
_Glass
02
Composite
t'
(
Plastic
in
Re inguished By: (Signature) I Dote Time I Received By (Signature) I Date Time
r7 1Fede
Nitrogen tsenes: Iota] Kjeldahl, Ammonium, Nitrate & Organic Nitrogen. >VG Cl
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, l a5 S
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
Account #
45671
N

BIO-NOMIC SERVICES, INC - CLASS A
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 1, 2019
McCall Farms #6
Mineralization Rate 0.20
45.80 % Solids
8.2 pH
Permit No. WQ0003823
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg x 0.002)
Nitrogen (TKN)
1.330
13,300.000
26.600
Phosphorus
0.162
1,620.000
3.240
Potassium
0.205
2,050.000
4.100
PAN (incorporated)*
............................................................
.............
a364 €
.....................
;€63i(�Q?i5;
.......................
PAN (surface)*
0.304
3,038.200
6.076
Ammonia Nitrogen
0.120
1,200.000
2.400
Calcium
1.400
14,000.000
28.000
Calcium Carbonate Eq.
9.000
90,000.000
180.000
Magnesium
---
2,910.000
5 8820
Sodium
---
250.000
0.500
Sulfur
---
2,090.000
4.180
Nitrate N / Nitrite N
---
18.200
0.036
Barium
---
---
---
Chloride
---
---
---
Iron
---
10,900.000
21.800
Aluminum
---
16,100.00
32.200
Arsenic
---
5.000
0.010
Cadmium
---
1.000
0.002
Chromium
---
122.000
0.244
Copper
---
50.50
0.101
Lead
---
15.40
0.031
Mercury
---
0.045
0.000
Molybdenum
---
2.500
0.005
Nickel
---
49.60
0.099
Selenium
---
5.000
0.010
Zinc
---
184.00
0.368
Waypoint Analytical 19-092-0214
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
SAR
0.34
Ceiling Concen.
(Mg/Kg)
75
85
4,300
840
57
75
420
100
7,500

Waypoint
ANALYTICAL
4/10/2019
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-092-0214
Project Description: Biosolid 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/2/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam. [,-Obr
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
el
Page 1 of 6

Waypoint.(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-092-0214
Client Project Description: Biosolid 6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65683
6
Solids
04/01/2019
09:20
04/02/2019
65683
6
Solids
04/01/2019
09:20
04/02/2019
65683
6
Solids
04/01/2019
09:20
04/02/2019
65683
6
Solids
04/01/2019
09:20
04/02/2019
65683
6
Solids
04/01/2019
09:20
04/02/2019
65683
6
Solids
04/01/2019
09:20
04/02/2019
65683
6
Solids
04/01/2019
09:20
04/02/2019
65683
6
Solids
04/01/2019
09:20
04/02/2019
65683
6
Solids
04/01/2019
09:20
04/02/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
SM-2540G
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
4500NO3F-2011
WTN
6010D
WTN
SM-4500-NH3C
WTN
9045D
WTN
AOAC 955.01
WTN
Page 2 of 6

Report Number: 19-092-0214
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 65683
Sample Id : 6
D
Waypoin(t,.
ANALYTICAL
Project: Biosolid 6
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/1/2019 09:20:00
Date Received: 04/02/2019 00:00
Date Reported: 04/10/2019
Total Solids *
45.80
458000
100.0
ADM
04/08/2019 15:25
SM-2540G
Moisture *
54.20
100.0
ADM
04/08/2019 15:25
SM-2540G
Total Kjeldahl Nitrogen
1.33
13300
250
CLP
04/08/2019 13:30
SM-4500-NH3C-TKN
Phosphorus
0.16
1620
50.0
BKN
04/06/2019 02:13
6010D
Potassium
0.21
2050
50.0
BKN
04/06/2019 02:13
6010D
Sulfur
0.21
2090
50.0
BKN
04/06/2019 02:13
6010D
Calcium
1.40
14000
250
BKN
04/06/2019 02:13
6010D
Magnesium
0.29
2910
50.0
BKN
04/06/2019 02:13
6010D
Sodium
<0.03
<250
250
BKN
04/06/2019 02:13
6010D
Iron
10900
50.0
BKN
04/06/2019 02:13
6010D
Aluminum
16100
50.0
BKN
04/06/2019 02:13
6010D
Manganese
41.5
5.00
BKN
04/06/2019 02:13
6010D
Copper
50.5
2.50
BKN
04/06/2019 02:13
6010D
Zinc
184
12.5
BKN
04/06/2019 02:13
6010D
Ammonia Nitrogen
0.12
1200
100
JPJ
04/08/2019 09:30
SM-4500-NI3C
Organic N
1.21
12100
250
04/08/2019 09:30
CALCULATION
Nitrate+Nitrite-N
18.2
5.00
ZBD
04/08/201915:47
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding
Time
pofiG
mC 60Wr
Our reports and letters are for the exclusive and confidential use of our clients, and
may not be reproduced in
whole or part, nor may any reference be made
Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public
announcements without obtaining our prior written authorization.
Agronomist
Page 3 of 6

Report Number: 19-092-0214
Account Number: 45671
Send To: Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Lab Number: 65683
Sample Id : 6
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH'
Calcium Carbonate Equivalent
Molybdenum
Chloride
Comments:
Waypoint(z)
ANALYTICAL
Project: Biosolid 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° fax [phone]
www.waypointanalytical.com
REPORT OF ANALYSIS Date Sampled: 4/1/2019 09:20:00
Date Received: 04/02/2019 00:00
Date Reported: 04/10/2019
<1.00
1.00
BKN
04/06/2019 02:13
6010D
122
2.50
BKN
04/06/2019 02:13
6010D
49.6
2.50
BKN
04/06/2019 02:13
601 OD
15.4
3.00
BKN
04/06/2019 02:13
601 OD
<5.00
5.00
BKN
04/06/2019 02:13
6010D
0.0453
0.0145
TJS
04/05/2019 13:41
SW-7471 B
<5.00
5.00
BKN
04/06/2019 02:13
6010D
8.2
JSL
04/08/2019 06:40
9045D
9.00 90000
1000
DXT
04/07/2019 12:01
AOAC 955.01
<2.50
2.50
BKN
04/06/2019 02:13
6010D
955
200
JM
04/04/201916:40
SM-4500CI-D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Page 4 of 6
?W« mC Ger
Pauric McGroary
Agronomist

C
• s
Waypo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 19-092-0214
Shipping Method
• Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
0 No
Number of coolers received
r 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
I& Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
I& Not Required
Chain of Custody (COC) present?
• Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
• Yes
0 No
Samples in proper containers?
• Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
• Yes
0 No
Cooler temperature in compliance?
0 Yes
® No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 9 No
Comments:
Signature: Brandi Watson Date & Time: 4/02/2019 14:04:45
Page 5 of 6

i
WASTEWATER SAMPLE TR ODY Account #
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7021 Whitepinc Road Richmond VA 2323Bio-Nomic Serncs Inc Tel: SO4-' 14:04:24
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Bio-Nomic Services, Inc. Bio-Nomic Services, Inc.
530 Woodlawn Street 530 Woodlawn Street i
Belmont, NC 28012 Belmont, NC 28012
Project Phone: [phone] FaX: [e-mail]
E-mail:
[e-mail] w
Sample Information
Lab Number
Collection Information
Container Information
Please Write in Desired Tests
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(Lab Use
Only)
Type
Date
Time
Number
Type
Volume
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Test Available Special Instructions or Remarks ;
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen. v
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, rUL Ct u5 S ,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
- A
I

............ LINKS......
TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-168890-1
Client Project/Site: McCall Farms
For:
Bio-Nomics Services., Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Vaughn Stevenson
Authorized for release by.
31612019 1:53:59 PM
Ken Hayes, Project Manager II
[phone]
ken.hayes @testamericainc.com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory
C

Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Table of Contents
C P 1
over age ..............................................
Table of Contents .........................................
2
Sample Summary ..........................................
3
Case Narrative ...........................................
4
Definitions ...............................................
5
Client Sample Results ......................................
6
QC Sample Results ........................................
9
QC Association ...........................................
21
Chronicle................................................
25
Method Summary .........................................
26
Certification Summary ......................................
27
Chain of Custody ..........................................
28
Receipt Checklists .........................................
31
TestAmerica Nashville
Page 2 of 31 3/6/2019

Sample Summary
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Lab Sample ID Client Sample ID Matrix Collected Received
490-168890-1 McCall Farms Sludge 02/19/19 10:00 02/21/19 08:55
TestAmerica Nashville
L31
Page 3 of 31 3/6/2019

Case Narrative
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Job ID: 490-166890-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-168890-1
Comments
While TA Pittsburgh carries South Carolina certification for 8260D and 8270E, the referenced matrix "Sludge", is causing the report to
indicate the lab as not certified for these.
No additional comments.
Receipt
The sample was received on 2/21/2019 8:55 AM; the sample arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 3.00 C.
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-271299 was outside the method criteria for the
following analyte: 2-Butanone. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is
considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 101OA: Method 1010A is applicable only to liquid matrix. This method has been modified to incorporate soil/ solid matrices of the
following sample: McCall Farms (490-168890-1).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Geotechnical
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
Method 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271365.
Method 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271367.
Method 8151A: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-271274 and 180-271391.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Nashville
Page 4 of 31 3/6/2019

Definitions/Glossary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Qualifiers
GC/MS Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
NO Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 31 3/6/2019

Client Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Client Sample ID: McCall Farms Lab Sample ID: 490-168890-1
Date Collected: 02/19/19 10:00 Matrix: Sludge
Date Received: 02/21/19 08:56
Method: EPA 8260D - Volatile Organic Compounds by GC/MS - TCLP
Analyte
Result Qualifier
RL
MDL Unit
1,1-Dichloroethene
ND
0.200
mg/L
1,2-Dichloroethane
ND
0.200
mg/L
2-Butanone (MEK)
ND
0.200
mg/L
Benzene
ND
0.200
mg/L
Carbon tetrachloride
ND
0.200
mg/L
Chlorobenzene
ND
0.200
mg/L
Chloroform
ND
0.200
mg/L
Tetrachloroethene
ND
0.200
mg/L
Trichloroethene
ND
0.200
mg/L
Vinyl chloride
ND
0.200
mg/L
D Prepared Analyzed
Dil Fac
02/26/19 10:29
1
02/26/19 10:29
1
02/26/19 10:29
1
02/26/19 10:29
1
02/26/19 10:29
1
02/26/19 10:29
1
02/26/19 10:29
1
02/26/19 10:29
1
02/26/19 10:29
1
02/26/19 10:29
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
89
73-143
02/26/19 10:29
1
4-Bromofluorobenzene (Surr)
83
61-123
02/26/19 10:29
1
Dibromofluoromethene (Surr)
105
68-128
02/26/19 10:29
1
Toluene-d8 (Surr)
100
75-124
02/26/19 10:29
1
Method: 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL
1,4-Dichlorobenzene
ND
0.0500
2,4, 5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0500
Hexachlorobenzene
ND
0.0500
Hexachlorobutadiene
ND
0.0500
Hexachloroethane
ND
0.0500
Nitrobenzene
ND
0.0500
Pentachlorophenol
ND
0.250
Pyridine
ND
0.100
Cresols
ND
0.100
Surrogate
2,4,6-Tribromophenol (Surr)
2-Fluorophenol (Surr)
2-Fluorobiphenyl
Nitrobenzene-d5 (Surr)
Phenol-d5 (Surr)
Terphenyl-d14 (Surr)
%Recovery Qualifier
Limits
74
25- 112
89
61- 105
90
62 -105
88
64 - 105
86
47-105
79
45 -130
Method: EPA 8081 B - Organochlorine Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
Chlordane (technical)
ND
0.00500
Endrin
ND
0.000500
gamma-BHC (Lindane)
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500
Toxaphene
ND
0.0400
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
0212611912:10
02127/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
mg/L
02/26/1912:10
02/27/1916:57
1
Prepared
Analyzed
Dil Fac
02/ 6/19 12:10
02/27/19 16:57
1
0212611912:10
0212711916:57
1
0212611912:10
0212711916:57
1
OM/26/1912:10
0212711916:57
1
0212611912:10
0212711916:57
1
0212611912:10
0212711916:57
1
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/1911:00
02/27/1915:48
1
mg/L
02/26/1911:00
02/2711915:48
1
mg/L
02/26/1911:00
02/27/1915:48
1
mg/L
02/26/1911:00
02127/1915:48
1
mg/L
02/26/1911:00
02/27/1915:48
1
mg/L
02/26/1911:00
02/27/1915:48
1
mg/L
02/26/1911:00
02/27/1915:48
1
TestAmerica Nashville
Page 6 of 31 3/6/2019

Client Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Client Sample ID: McCall Farms Lab Sample ID: 490-168890-1
Date Collected: 02/19/19 10:00 Matrix: Sludge
Date Received: 02/21/19 08:55
Surrogate
%Recovery Qualifier
DCB Decachlorobiphenyl (Surr)
93
Tetrachloro-m-xylene
97
Method: EPA 8151A - Herbicides (GC) - TCLP
Analyte
Result Qualifier
2,4-D
ND
Silvex (2,4,5-TP)
ND
2,4,5-T
ND
Surrogate
%Recovery Qualifier
2,4-Dichlorophenylacetic acid
64
Method: EPA 6010D - Metals (ICP) - TCLP
Analyte
Result Qualifier
Arsenic
ND
Barium
ND
Cadmium
ND
Chromium
ND
Lead
ND
Selenium
ND
Silver
ND
Method: EPA 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
Mercury
ND
General Chemistry
Analyte
Result Qualifier
Flashpoint
>200
Percent Moisture
48.8
Percent Solids
51.2
pH
8.6 HF
Limits
Prepared
Analyzed
Dil Fac
62 -150
02/2611 111:00
02/27/19 15:48
1
54 -138
02/26/19 11:00
02127119 15:48
1
•
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
0.0400
mg/L
02/26/19 14:30
02/28/19 00:53
20
0.0100
mg/L
02/26/19 14:30
02/28/19 00:53
20
0.0100
mg/L
02/26/19 14:30
02/28/19 00:53
20
Limits
Prepared
Analyzed
Dil Fac
20-105
02/26/19 14:30
02/28/19 00:53
20
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
0.500
mg/L
02/26/19 12:20
02/27/19 09:08
1
2.00
mg/L
02/26/19 12:20
02/27/19 09:08
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:08
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:08
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:08
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:08
1
0.500
mg/L
02/26/19 12:20
02/27/19 09:08
1
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
0.000200
mg/L
02/26/1911:05
02/26/1916:16
1
RL
RL Unit
D
Prepared
Analyzed
Dil Fac
1.00
Degrees F
03/01/19 17:29
1
0.1
%
02/27/19 08:43
1
0.1
%
02/27/19 08:43
1
0.1
SU
02/27/1912:00
1
TestAmerica Nashville
Page 7 of 31
3/6/2019

Client Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Client Sample ID: McCall Farms Lab Sample ID: 490-168890-1
Date Collected: 02/19/19 10:00 Matrix: Sludge
Date Received: 02/21/19 08:56 Percent Solids: 51.2
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
PCB-1016
ND
32.4
ug/Kg
02/27/19 09:52
02/28/19 14:50
1
PCB-1221
ND
32.4
ug/Kg
02/27/19 09:52
02/28/19 14:50
1
13
PCB-1232
ND
32.4
ug/Kg
02/27/19 09:52
02/28/19 14:50
1
PCB-1242
ND
32.4
ug/Kg
02/27/19 09:52
02/28/19 14:50
1
PCB-1248
ND
32.4
ug/Kg
02/27/19 09:52
02/28/19 14:50
1
PCB-1254
ND
32.4
ug/Kg
02/27/19 09:52
02/28/19 14:50
1
PCB-1260
ND
32.4
ug/Kg
02/27/19 09:52
02/28/19 14:50
1
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene (Surr) 83 51-116
DCB Decachlorobiphenyl (Surr) 90 44 -116
General Chemistry.
Analyte Result Qualifier
Cyanide, Total ND
Sulfide 111
RL
0.940
58.3
Prepared
Analyzed
Dil Fac
27/19 09:52
28/19 14:50
1
02/27/19 09:52
02128119 14:50
1
MDL Unit D Prepared
Analyzed
Dil Fac
mg/Kg 03/01/1912:40
03/01/1919:30
1
mg/Kg 02/26/19 09:35
02/26/19 11:22
1
TestAmerica Nashville
Page 8 of 31
3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Method: EPA 8260D -Volatile Organic Compounds by GC/MS
Lab Sample ID: LCS 180-271299/3
Matrix: Solid
Analysis Batch: 271299
Analyte
1,1-Dichloroethene
1,2-Dichloroethane
2-Butanone (MEK)
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Spike
LCS LCS
Added
Result Qualifier
0.0400
0.04011
0.0400
0.03331
0.0400
0.02829
0.0400
0.04064
0.0400
0.04205
0.0400
0.04443
0.0400
0.03950
0.0400
0.04642
0.0400
0.04744
0.0400
0.03919
TestAmerica Job ID: 490-168890-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
Unit
D %Rec
Limits
mg/L
100
57 -135
mg/L
83
69 -127
mg/L
71
36 -150
mg/L
102
66 -124
mg/L
105
69 -130
mg/L
111
72 -122
mg/L
99
69 -119
mg/L
116
73 -129
mg/L
119
75 -122
mg/L
98
57-132
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
80
73- 143
4-Bromofluorobenzene (Surr)
97
61-123
Dibromofluoromethane (Surr)
105
68-128
Toluene-d8 (Surr)
103
75-124
Lab Sample ID: LB 180-271312/1-A
Client Sample ID: Method
Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271299
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
1, 1 -Dichloroethene
ND
0.0500
mg/L
02/26/19 09:01
1
1,2-Dichloroethane
ND
0.0500
mg/L
02/26/19 09:01
1
2-Butanone (MEK)
ND
0.0500
mg/L
02/26/19 09:01
1
Benzene
ND
0.0500
mg/L
02/26/19 09:01
1
Carbon tetrachloride
ND
0.0500
mg/L
02/26/19 09:01
1
Chlorobenzene
ND
0.0500
mg/L
02/26/19 09:01
1
Chloroform
ND
0.0500
mg/L
02/26/19 09:01
1
Tetrachloroethene
ND
0.0500
mg/L
02/26/19 09:01
1
Trichloroethene
ND
0.0500
mg/L
02/26/19 09:01
1
Vinyl chloride
ND
0.0500
mg/L
02/26/19 09:01
1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
85
73-143
02/26/19 09.01
1
4-Bromofluorobenzene (Surr)
82
61-123
02/26/19 09:01
1
Dibromofluoromethane (Surr)
102
68-128
02/26/19 09:01
1
Toluene-d8 (Surr)
104
75-124
02/26/19 09:01
1
Lab Sample ID: 490-168891-A-1-B MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271299
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
1,1-Dichloroethene
ND
1.60
1.556
mg/L
97
57-135
1,2-Dichloroethane
ND
1.60
1.409
mg/L
88
69-127
2-Butanone (MEK)
ND
1.60
0.8771
mg/L
55
36-150
TestAmerica Nashville
`7
Page 9 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: 490-168891-A-1-B
MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271299
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Benzene
ND
1.60
1.613
mg/L
101
66 -124
Carbon tetrachloride
ND
1.60
1.711
mg/L
107
69 -130
Chlorobenzene
ND
1.60
1.768
mg/L
111
72.122
Chloroform
ND
1.60
1.638
mg/L
102
69-119
Tetrachloroethene
ND
1.60
1.815
mg/L
113
73-129
Trichloroethene
ND
1.60
1.869
mg/L
117
75-122
Vinyl chloride
ND
1.60
1.383
mg/L
86
57 -132
MS MS
Surrogate
%Recovery Qualifier
Limits
1, 2-Dichloroethane-d4 (Surr)
85
73 -143
4-Bromofluorobenzene (Surr)
98
61-123
Dibromofluoromethane (Surr)
104
68-128
Toluene-d8 (Surr)
101
75-124
Lab Sample ID: 490-168891-A-1-C
MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271299
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
1,1-Dichloroethene
ND
1.60
1.702
mg/L
106
57-135 9 35
1,2-Dichloroethane
ND
1.60
1.434
mg/L
90
69.127 2 16
2-Butanone (MEK)
ND
1.60
0.9013
mg/L
56
36 -150 3 35
Benzene
ND
1.60
1.638
mg/L
102
66 -124 2 16
Carbon tetrachloride
ND
1.60
1.689
mg/L
106
69 -130 1 17
Chlorobenzene
ND
1.60
1.798
mg/L
112
72-122 2 15
Chloroform
ND
1.60
1.639
mg/L
102
69-119 0 16
Tetrachloroethene
ND
1.60
1.882
mg/L
118
73-129 4 15
Trichloroethene
ND
1.60
1.879
mg/L
117
75-122 1 15
Vinyl chloride
ND
1.60
1.558
mg/L
97
57-132 12 21
MSD MSD
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
87
73- 143
4-Bromofluorobenzene (Surr)
99
61- 123
Dibromofluoromethane (Surr)
106
68- 128
Toluene-d8 (Sun•)
105
75-124
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 180-271367/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dichlorobenzene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
2,4,5-Trichlorophenol
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
2,4,6-Trichlorophenol
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
2,4-Dinitrotoluene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11 1
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Page 10 of 31
3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 180-271367/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
MB MB
Analyte
Result Qualifier
RL
MDL Unit D
Prepared
Analyzed
Dil Fac
Hexachlorobenzene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11
1
Hexachlorobutadiene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11
1
Hexachloroethane
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11
1
Nitrobenzene
ND
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11
1
Pentachlorophenol
ND
0.250
mg/L
02/26/19 12:10
02/27/19 09:11
1
Pyridine
ND
0.100
mg/L
02/26/19 12:10
02/27/19 09:11
1
Cresols
ND
0.100
mg/L
02/26/19 12:10
02/27/19 09:11
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surf)
83
25-112
02/2611 112.10
02/27/19 09:11
1
2-Fluorophenol (Surr)
87
61-105
02/26/19 12:10
02/27/19 09:11
1
2-Fluorobiphenyl
83
62 -105
02/26/19 12:10
02/27/19 09:11
1
Nitrobenzene-d5 (Surr)
83
64 -105
02/26/19 12:10
02/27/19 09:11
1
Phenol-d5 (Surr)
86
47-105
02/26/19 12:10
02127119 09:11
1
Terphenyl-d14 (Surr)
75
45-130
02/26/19 12:10
02/27/19 09:11
1
Lab Sample ID: LCS 180-27136712-A
Matrix: Solid
Analysis Batch: 271438
Analyte
1,4-Dichlorobenzene
2,4, 5-Trichlorophenol
2,4, 6-Trichlorophenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Cresols
LCS LCS
Surrogate
%Recovery Qualifier
2,4,6-Tribromophenol (Surr)
88
2-Fluorophenol (Surr)
90
2-Fluorobiphenyl
86
Nitrobenzene-d5 (Surr)
90
Phenol-d5 (Surr)
90
Terphenyl-d14 (Surr)
69
Lab Sample ID: LCSD 180-271367/3-A
Matrix: Solid
Analysis Batch: 271438
Analyte
1,4-Dichlorobenzene
2,4, 5-Trichlorophenol
Spike
LCS LCS
Added
Result Qualifier
0.250
0.2277
0.250
0.2157
0.250
0.2096
0.250
0.2023
0.250
0.1527
0.250
0.2146
0.250
0.2352
0.250
0.2299
0.250
0.1630 J
0.250
0.2391
0.750
0.6754
Limits
25-112
61-105
62 -105
64-105
47-105
45-130
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271367
%Rec.
Unit
D %Rec
Limits
mg/L
91
57 -100
mg/L
86
58 -100
mg/L
84
57 -100
mg/L
81
40 -100
mg/L
61
38 -100
mg/L
86
53 -105
mg/L
94
57 -100
mg/L
92
56 -103
mg/L
65
16 -100
mg/L
96
51 - 107
mg/L
90
54 - 103
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 271367
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0.250 0.2220 mg/L 89 57 -100 '3 16
0.250 0.2095 mg/L 84 58 -100 3 16
TestAmerica Nashville
Page 11 of 31
3/6/2019

P,
0
QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 180-271367/3-A
Client Sample
ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier Unit
D %Rec
Limits RPD Limit
2,4,6-Trichlorophenol
0.250
0.2135
mg/L
85
57-100 2 15
2,4-Dinitrotoluene
0.250
0.1977
mg/L
79
40-100 2 15
Hexachlorobenzene
0.250
0.1553
mg/L
62
38-100 2 16
Hexachlorobutadiene
0.250
0.2085
mg/L
83
53 -105 3 15
Hexachloroethane
0.250
.0.2259
mg/L
90
57 -100 4 18
Nitrobenzene
0.250
0.2141
mg/L
86
56 -103 7 15
Pentachlorophenol
0.250
0.1462 J
mg/L
58
16 -100 11 24
Pyridine
0.250
0.2257
mg/L
90
51 -107 6 18
Cresols
0.750
0.6719
mg/L
90
54-103 1 17
Surrogate
LCSD LCSD
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
86
25-112
2-Fluorophenol (Surr)
86
61-105
2-Fluorobiphenyl
86
62-105
Nitrobenzene-d5 (Surr)
84
64-105
Phenol-d5 (Surr)
86
47-105
Terphenyl-d14 (Surr)
68
45-130
Lab Sample ID: LB 180-271274/1-D
Matrix: Solid
Analysis Batch: 271438
Analyte
LB LB
Result Qualifier
RL
MDL Unit
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 271367
D Prepared Analyzed Dil Fac
1,4-Dichlorobenzene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
2,4,5-Trichlorophenol
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
2,4,6-Trichlorophenol
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
2,4-Dinitrotoluene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Hexachlorobenzene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Hexachlorobutadiene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Hexachloroethane
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Nitrobenzene
ND
0.0500
mg/L
02/26/1912:10
02/27/1911:33
1
Pentachlorophenol
ND
0.250
mg/L
02/26/1912:10
02/27/1911:33
1
Pyridine
ND
0.100
mg/L
02/26/1912:10
02/27/1911:33
1
Cresols
ND
0.100
mg/L
02/26/1912:10
02/27/1911:33
1
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
88
25- 112
02/26/19 12:10
02/27/19 11.33
1
2-Fluorophenol (Surr)
85
61-105
02/26/19 12:10
02127119 11:33
1
2-Fluorobiphenyl
85
62- 105
02/26/19 12:10
02/27/19 11:33
1
Nitrobenzene-d5 (Surr)
87
64-105
02126119 12:10
02/27/19 11:33
1
Phenol-d5 (Surr)
87
47-105
02/26/19 12:10
02/27/19 11:33
1
Terphenyl-04 (Surr)
74
45-130
02/26/19 12:10
02127119 11:33
1
TestAmerica Nashville
l7.
d
Page 12 of 31
3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: EPA 8081 B - ®rganochlorine Pesticides (GC)
Lab Sample ID: MB 180-271365/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271475
Prep Batch: 271365
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Chlordane (technical) ND
0.00500
mglL
02/26/19 11:00
02l27/19 13:14 1
Endrin ND
0.000500
mg/L
02/26/19 11:00
02/27/19 13:14 1
gamma-BHC (Lindane) ND
0,000500
mg/L
02/26/19 11:00
02/27/19 13:14 1
Heptachlor ND
0.000500
mg/L
02/26/19 11:00
02/27/19 13:14 1
Heptachlor epoxide ND
0.000500
mg/L
02/26/19 11:00
02/27/19 13:14 1
Methoxychlor ND
0.000500
mg/L
02/26/19 11:00
02/27/19 13:14 1
Toxaphene ND
0.0400
mg/L
02/26/19 11:00
02/27/19 13:14 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCB Decachlorobiphenyl (Surr) 94
62 -150
02/26/19 11:00
Zi2 27/19 13.14 1
Tetrachloro-m-xylene 91
54 -138
02/26/19 11:00
02127119 13:14 1
ILab
Sample ID: LCS 180-271365/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271475
Prep Batch: 271365
Spike LCS
LCS
%Rec.
Analyte
Added Result
Qualifier
Unit D %Rec
Limits
Endrin
0.0100 0.009924
—
mg/L 99
71-134
gamma-BHC (Lindane)
0.0100 0.008481
mg/L 85
66 -127
Heptachlor
0.0100 0.009290
mg/L 93
66 -134
Heptachlor epoxide
0.0100 0.008870
mg/L 89
65 -141
Methoxychlor
0.0100 0.01001
mg/L 100
59 -131
LCS LCS
Surrogate %Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surr) 95
62 -150
Tetrachloro-m-xylene 96
54 -138
Lab Sample ID: LCSD 180-271365/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271475
Prep Batch: 271365
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier Unit
D %Rec
Limits RPD Limit
Endrin
0.0100
0.009900
mg/L
99
71 -134 0 18
gamma-BHC(Lindane)
0.0100
0.008743
mg/L
87
66-127 3 15
Heptachlor
0.0100
0.009428
mg/L
94
66 -134 1 15
Heptachlor epoxide
0.0100
0.008791
mg/L
88
65 -141 1 15
Methoxychlor
0.0100
0.009889
mg/L
99
59 -131 1 28
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surr)
95
62-150
Tetrachloro-m-xylene
93
54 -138
TestAmerica Nashville
Page 13 of 31 3/6/2019

P,
QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Method: EPA 8081 B - ®rganochlorine Pesticides (GC) (Continued)
Lab Sample ID: LB 180-271274/16-E
Matrix: Solid
Analysis Batch: 271475
Analyte
LB LB
Result Qualifier
RL
Chlordane (technical)
ND
0.00500
Endrin
ND
0.000500
gamma-BHC (Lindane)
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500
Toxaphene
ND
0.0400
LB LB
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surr)
98
62-150
Tetrachloro-m-xylene
92
54 -138
TestAmerica Job ID: 490-168890-1
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 271365
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/1911:00
02/27/1914:15
1
mg/L
02/26/1911:00
02/27/1914:15
1
mg/L
02/26/1911:00
02/27/1914:15
1
mg/L
02/26/1911:00
02/2711914:15
1
mg/L
02/26/1911:00
02/27/1914:15
1
mg/L
02/26/1911:00
02/27/1914:15
1
mg/L
02/26/1911:00
02/27/1914:15
1
Prepared
Analyzed
Dil Fac
02/26/1911:00
02/27/1914.15
1
0212611911:00
0212711914:15
1
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: MB 180-271476/1-A
Matrix: Solid
Analysis Batch: 271567
Analyte
MB MB
Result Qualifier
RL
PCB-1016
ND
16.7
PCB-1221
ND
16.7
PCB-1232
ND
16.7
PCB-1242
ND
16.7
PCB-1248
ND
16.7
PCB-1254
ND
16.7
PCB-1260
ND
16.7
MB MB
Surrogate
%Recovery Qualifier
Limits
Tetrachloro-m-xylene (Surr)
91
51-116
DCB Decachlorobiphenyl (Surr)
94
44 -116
Lab Sample ID: LCS 180-271476/2-A
Matrix: Solid
Analysis Batch: 271567
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch:271476
MDL Unit
D Prepared
Analyzed
Dil Fac
ug/Kg
02/27/19 09:52
02/28/19 13:54
1
ug/Kg
02/27/19 09:52
02/28/19 13:54
1
ug/Kg
02/27/19 09:52
02/28/19 13:54
1
ug/Kg
02/27/19 09:52
02/28/19 13:54
1
ug/Kg
02/27/19 09:52
02/28/19 13:54
1
ug/Kg
02/27/19 09:52
02/28/19 13:54
1
ug/Kg
02/27/19 09:52
02/28/19 13:54
1
Prepared
Analyzed
Dil Fac
02/27/19 09:52
02/28/19 13:54
1
02127119 09:52
02/28/19 13:54
1
Analyte
Spike
Added
LCS LCS
Result Qualifier
PCB-1016
1330
1090
PCB-1260
1330
1059
LCS LCS
Surrogate
%Recovery Qualifier
Limits
Tetrachloro-m-xylene (Surr)
85
51-116
DCB Decachlorobiphenyl (Surr)
87
44 -116
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271476
%Rec.
Unit D %Rec Limits
ug/Kg 82 57-114
ug/Kg 79 55-112
TestAmerica Nashville
Page 14 of 31
3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Lab Sample ID: 490-168890-1 MS
Matrix: Sludge
Analysis Batch: 271567
Sample Sample Spike MS MS
Analyte Result Qualifier Added Result Qualifier
PCB-1016 ND 2610 1775
PCB-1260 ND 2610 1824
MS MS
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene (Surr) 66 51-116
DCB Decachlorobiphenyl (Surr) 72 44 -116
Lab Sample ID: 490-168890-1 MSD
Matrix: Sludge
Analysis Batch: 271567
Sample Sample Spike MSD MSD
Analyte Result Qualifier Added Result Qualifier
PCB-1016 ND 2520 1626
PCB-1260 ND 2520 1636
MSD MSD
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene (Surr) 64 51-116
DCB Decachlorobiphenyl (Surr) 71 44 -116
Method: EPA 8151A - Herbicides (GC)
Lab Sample ID: MB 180-271391/1-A
Matrix: Solid
Analysis Batch: 271555
Client Sample ID: McCall Farms
Prep Type: Total/NA
Prep Batch: 271476
%Rec.
Unit D %Rec Limits
ug/Kg+ 68 57 -114
ug/Kg 70 55-112
Client Sample ID: McCall Farms
Prep Type: Total/NA
Prep Batch: 271476
%Rec. RPD
Unit
D %Rec Limits RPD Limit
ug/Kg
64 57 - 114 9 34
ug/Kg
65 55-112 11 16
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271391
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
2,4-D
ND
0.0400
mg/L
02/26/19 14:30
02/27/19 20:57
20
Silvex (2,4,5-TP)
ND
0.0100
mg/L
02/26/19 14:30
02/27/19 20:57
20
2,4,5-T
ND
0.0100
mg/L
02/26/19 14:30
02/27/19 20:57
20
MB MB
Surrogate %Recovery Qualifier Limits
2, 4-Dichlorophenylacetic acid 71 20 - 105
Lab Sample ID: LCS 180-271391/2-A
Matrix: Solid
Analysis Batch: 271555
Analyte
Silvex (2,4,5-TP)
2,4,5-T
Surrogate
2,4-Dichlorophenylacetic acid
Spike
Added
0.200
0.0500
0.0500
LCS LCS
%Recovery Qualifier
Limits
67
20-105
Prepared Analyzed Dil Fac
02/26/19 14:30 02/27119 20:57 20
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271391
LCS LCS
%Rec.
Result Qualifier
Unit
D %Rec
Limits
0.1340
mg/L
67
10 - 000
0.03454
mg/L
69
23 -109
0.02981
mg/L
60
11 -101
TestAmerica Nashville
Page 15 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Method: EPA 8161A - Herbicides (GC) (Continued)
Lab Sample ID: LCSD 180-271391/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271555
Prep Batch: 271391
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier Unit
D %Rec Limits RPD Limit
2,4-D
0.200
0.1578 mg/L
79 10 -100 16 35
Silvex (2,4,5-TP)
0.0500
0.04003 mg/L
80 23 -109 15 35
2,4,5-T
0.0500
0.03558 mg/L
71 11 -101 18 35
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
2,4-Dichlorophenylaceticacid 78
20-105
Lab Sample ID: LB 180-271274/16-G
Matrix: Solid
Analysis Batch: 271555
Analyte
Silvex (2,4,5-TP)
2,4,5-T
Surrogate
2,4-Dichlorophenylacetic acid
LB LB
Result Qualifier
RL
ND
0.0400
ND
0.0100
ND
0.0100
LB LB
%Recovery Qualifier
Limits
60
20 -105
Method: EPA 6010D - Metals (ICP)
Lab Sample ID: MB 180-271365/1-A
Matrix: Solid
Analysis Batch: 271499
Analyte
MB MB
Result Qualifier
RL
Arsenic
ND
0.0500
Barium
ND
0.200
Cadmium
ND
0.0500
Chromium
ND
0.0500
Lead
ND
0.0500
Selenium
ND
0.0500
Silver
ND
0.0500
Lab Sample ID: LCS 180-271355/2-A
Matrix: Solid
Analysis Batch: 271499
Analyte
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch:271391
MDL Unit
D Prepared
Analyzed Dil Fac
mg/L
02/26/19 14:30
02/27/19 22:24 20
mg/L
02/26/19 14:30
02/27/19 22:24 20
mg/L
02/26/19 14:30
02/27/19 22:24 20
Prepared
Analyzed Dil Fac
02/26/19 14:30
02/27/19 22:24 20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271355
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
mg/L
02/26/19 12:20
02/27/19 07:50
1
Spike
Added
LCS LCS
Result Qualifier
0.500
0.5281
2.00
2.051
0.0500
0.05449
0.200
0.2054
0.500
0.5102
0.500
0.5558
0.0500
0.05381
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch:271355
Unit
D %Rec
%Rec.
Limits
mg/L
106
80 - 220
mg/L
103
80 -120
mg/L
109
80 -120
mg/L
103
80 -120
mg/L
102
80 -120
mg/L
111
80 -120
mg/L
108
80 -120
TestAmerica Nashville
Page 16 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: EPA 6010D - Metals (ICP) (Continued)
Lab Sample ID: LB 180-271274/1-C
Matrix: Solid
Analysis Batch: 271499
Analyte
LB LB
Result Qualifier
RL
Arsenic
ND
0.500
Barium
ND
2.00
Cadmium
ND
0.500
Chromium
ND
0.500
Lead
ND
0.500
Selenium
ND
0.500
Silver
ND
0.500
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 271355
MDL Unit
D Prepared
Analyzed
Dil Fac
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
mg/L
02/26/19 12:20
02/27/19 08:00
1
Method: EPA 7470A - Mercury (CVAA)
Lab Sample ID: MB 180-271342/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271395
Prep Batch: 271342
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Mercury ND
0.000200 mg/L
02/26/1911:05 02/26/1916:00 1
Lab Sample ID: LCS 180-27134212-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271395
Prep Batch: 271342
Spike LCS LCS
%Rec.
Analyte
Added Result Qualifier
Unit D %Rec Limits
Mercury
0.00250 0.002605
mg/L 104 80 -120
Lab Sample ID: LB 180-27127411-B
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271396
Prep Batch: 271342
LB LB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Mercury ND
0.000200 mg/L
02/26/1911:05 02/26/1916:02 1
Lab Sample ID: 180-86915-A-1-1 MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample Sample
Spike MS MS
%Rec.
Analyte Result Qualifier
Added Result Qualifier
Unit D %Rec Limits
Mercury ND
0.00500 0.005020
mg/L 100 75-125
Lab Sample ID: 180-86915-A-1-J MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample Sample
Spike MSD MSD
%Rec. RPD
Analyte Result Qualifier
Added Result Qualifier
Unit D %Rec Limits RPD Limit
Mercury ND
0.00500 0.005026
mglL 101 75 -125 0 20
TestAmerica Nashville
Page 17 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Method: 1010A - Ignitability, Pensky-Martens
Closed -Cup Method
Lab Sample ID: MB 490-57837211
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
MB MB
Analyte Result Qualifier
RL RL Unit
D Prepared Analyzed Dil Fac
Flashpoint >200
1.00 Degrees F 03/01/19 17:29 1
Lab Sample ID: LCS 490-57837212
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Flashpoint
81.0
81.20
Degrees F 100 94. 106
Lab Sample ID: LCSD 490-578372/14
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Flashpoint
81.0
83.40
Degrees F 103 94 -106 3 20
Lab Sample ID: 280-120182-A-1 DU
Client Sample ID: Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
Sample Sample
DU DU
RPD
Analyte Result Qualifier
Result Qualifier
Unit D RPD Limit
Flashpoint 128
134.3
Degrees F 5 10
Method: 254OG - SM 254OG
Lab Sample ID: 180-86358-B-20 DU
Client Sample ID: Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271450
Sample Sample
DU DU
RPD
Analyte Result Qualifier
Result Qualifier
Unit D RPD Limit
Percent Moisture 26.5
28.2
% 6 10
Percent Solids 73.5
71.8
% 2 10
Method: EPA 9012E - Cyanide, Total andor Amenable
Lab Sample ID: MB 180-271760/4-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Cyanide, Total ND
0.500 mg/Kg
03/01/19 12:40 03/01/19 19:23 1
Lab Sample ID: HLCS 180-271760/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Spike HLCS HLCS
%Rec.
Analyte
Added Result Qualifier
Unit D %Rec Limits
Cyanide, Total
0.250 0.2479
mg/Kg 99 90.110
TestAmerica Nashville
Page 18 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method: EPA 9012E - Cyanide, Total andor Amenable (Continued)
Lab Sample ID: LCS 180-27176013-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Spike
LCS LCS
%Rec..
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Cyanide, Total
190
114.2
mg/Kg 60 26 -139
Lab Sample ID: LLCS 180-27176011-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Spike
LLCS LLCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Cyanide, Total
0.0500
0.04970
mg/Kg 99 90 -110
Lab Sample ID: 180-87076-D-1-B MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits
Cyanide, Total 2.35
18.1
18.61
mg/Kg 90 75.125
Lab Sample ID: 180-87076-D-1-C MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Cyanide, Total 2.35
18.1
18.92
mg/Kg 91 75 -125 2 20
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 180-27131911-A
Matrix: Solid
Analysis Batch: 271334
MB MB
Analyte Result Qualifier RL
Sulfide ND 30.0
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271319
MDL Unit D Prepared Analyzed Dil Fac
mg/Kg 02/26/19 09:35 02/26/19 11:15 1
Lab Sample ID: LCS 180-271319/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271334 Prep Batch: 271319
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Sulfide 150 144.3 mg/Kg 97 85 -115
Lab Sample ID: 490-168890-1 MS
Matrix: Sludge
Analysis Batch: 271334
Sample Sample Spike MS MS
Analyte Result Qualifier Added Result Qualifier Unit
Sulfide 111 293 436.2 mg/Kg
Client Sample ID: McCall Farms
Prep Type: Total/NA
Prep Batch: 271319
%Rec.
D %Rec Limits
111 75-125
TestAmerica Nashville
Page 19 of 31 3/6/2019

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
TestAmerica Job ID: 490-168890-1
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: 490-168890-1 MSD Client Sample ID: McCall Farms
Matrix: Sludge Prep Type: Total/NA
Analysis Batch: 271334 Prep Batch: 271319
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Sulfide 111 292 408.7 mg/Kg 1� 102 75 -125 7 20
Method: EPA 9045D - pH
Lab Sample ID: LCS 180-271606/1
Matrix: Solid
Analysis Batch: 271506
Analyte
pH
Lab Sample ID: 180-86977-J-1 DU
Matrix: Solid
Analysis Batch: 271506
Sample Sample
Analyte Result Qualifier
pH 3.6
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
7.00 7.0 SU 101 99-101
Client Sample ID: Duplicate
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
3.6 SU 0 2
TestAmerica Nashville
Page 20 of 31 3/6/2019

QC Association Summary
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
GC/MS VOA
Analysis Batch: 271299
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 8260D
271312
LB 180-271312/1-A
Method Blank
TCLP
Solid
EPA 8260D
271312
LCS 180-271299/3
Lab Control Sample
Total/NA
Solid
EPA 8260D
490-168891-A-1-B MS
Matrix Spike
TCLP
Solid
EPA 8260D
271312
490-168891-A-1-C MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 8260D
271312
Leach Batch: 271312
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 1311
LB 180-271312/1-A
Method Blank
TCLP
Solid
EPA 1311
490-168891-A-1-B MS
Matrix Spike
TCLP
Solid
EPA 1311
490-168891-A-1-C MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 1311
GC/MS Semi VOA
Leach Batch: 271274
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 1311
LB 180-271274/1-D
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 271367
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
3510C
271274
LB 180-27127411-D
Method Blank
TCLP
Solid
3510C
271274
MB 180-271367/1-A
Method Blank
Total/NA
Solid
3510C
LCS 180-271367/2-A
Lab Control Sample
Total/NA
Solid
3510C
LCSD 180-271367/3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Analysis Batch: 271438
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
8270E
271367
LB 180-271274/1-D
Method Blank
TCLP
Solid
8270E
271367
MB 180-271367/1-A
Method Blank
Total/NA
Solid
8270E
271367
LCS 180-271367/2-A
Lab Control Sample
Total/NA
Solid
8270E
271367
LCSD 180-271367/3-A
Lab Control Sample Dup
Total/NA
Solid
8270E
271367
GC Semi VOA
Leach Batch: 271274
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
EPA 1311
LB 180-271274/16-E
Method Blank
TCLP
Solid
EPA 1311
LB 180-271274/16-G
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 271365
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
3510C
271274
LB 180-271274/16-E
Method Blank
TCLP
Solid
3510C
271274
MB 180-271365/1-A
Method Blank
Total/NA
Solid
3510C
LCS 180-271365/2-A
Lab Control Sample
Total/NA
Solid
3510C
TestAmerica Nashville
Page 21 of 31 3/6/2019

QC Association Summary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
GC Semi VOA (Contin
Prep Batch: 271365 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LCSD 180-271365/3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Prep Batch: 271391
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
8151A
271274
LB 180-271274/16-G
Method Blank
TCLP
Solid
8151A
271274
MB 180-271391/1-A
Method Blank
Total/NA
Solid
8151A
LCS 180-27139112-A
Lab Control Sample
Total/NA
Solid
8151A
'
LCSD 180-271391/3-A
Lab Control Sample Dup
Total/NA
Solid
8151A
Analysis Batch: 271475
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
all Farms
TCLP
Sludge
EPA 8081 B
271365
LB 180-271274/16-E
Method Blank
TCLP
Solid
EPA 8081 B
271365
MB 180-271365/1-A
Method Blank
Total/NA
Solid
EPA 8081B
271365
LCS 180-271365/2-A
Lab Control Sample
Total/NA
Solid
EPA 8081 B
271365
LCSD 180-271365/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8681 B
271365
Prep Batch: 271476
Lab Sample ID
Client Sample ID
490-168890-1
all Farms
MB 180-271476/1-A
Method Blank
LCS 180-271476/2-A
Lab Control Sample
490-168890-1 MS
McCall Farms
490-168890-1 MSD
McCall Farms
Analysis Batch: 271555
Prep Type
Matrix
Method Prep Batch
Total/NA
Sludge
3541
Total/NA
Solid
3541
Total/NA
Solid
3541
Total/NA
Sludge
3541
Total/NA
Sludge
3541
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
all Farms
TCLP
Sludge
EPA 8151A
271391
LB 180-271274/16-G
Method Blank
TCLP
Solid
EPA 8151A
271391
MB 180-271391/1-A
Method Blank
Total/NA
Solid
EPA 8151A
271391
LCS 180-271391/2-A
Lab Control Sample
Total/NA
Solid
EPA 8151A
271391
LCSD 180-271391/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8151A
271391
Analysis Batch: 271567
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
all Farms
Total/NA
Sludge
EPA 8082A
271476
MB 180-271476/1-A
Method Blank
Total/NA
Solid
EPA 8082A
271476
LCS 180-271476/2-A
Lab Control Sample
Total/NA
Solid
EPA 8082A
271476
490-168890-1 MS
McCall Farms
Total/NA
Sludge
EPA 8082A
271476
490-168890-1 MSD
McCall Farms
Total/NA
Sludge
EPA 8082A
271476
Metals
Leach Batch: 271274
Lab Sample ID
Client Sample ID
Prep Type
490-168890-1
McCall Farms
TCLP
LB 180-271274/1-B
Method Blank
TCLP
LB 180-271274/1-C
Method Blank
TCLP
180-86915-A-1-1 MS
Matrix Spike
TCLP
Matrix
Method Prep Batch
Sludge
EPA 1311
Solid
EPA 1311
Solid
EPA 1311
Solid
EPA 1311
TestAmerica Nashville
Page 22 of 31
3/6/2019

CSC Association Summary
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Metals (Continued)
Leach Batch: 271274 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-86915-A-1-J MSD Matrix Spike Duplicate
TCLP
Solid
EPA 1311
Prep Batch: 271342
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1 McCall Farms
TCLP
Sludge
7470A
271274
LB 180-271274/1-B Method Blank
TCLP
Solid
7470A
271274
MB 180-271342/1-A Method Blank
Total/NA
Solid
7470A
LCS 180-271342/2-A Lab Control Sample
Total/NA
Solid
7470A
180-86915-A-1-1 MS Matrix Spike
TCLP
Solid
7470A
271274
180-86915-A-1-J MSD Matrix Spike Duplicate
TCLP
Solid
7470A
271274
Prep Batch: 271355
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168890-1
McCall Farms
TCLP
Sludge
3010A 271274
LB 180-271274/1-C
Method Blank
TCLP
Solid
3010A 271274
MB 180-271355/1-A
Method Blank
Total/NA
Solid
3010A
LCS 180-271355/2-A
Lab Control Sample
Total/NA
Solid
3010A
Analysis Batch: 271395
Lab Sample ID
Client Sample ID
Prep Type
490-168890-1
McCall Farms
TCLP
LB 180-271274/1-B
Method Blank
TCLP
MB 180-271342/1-A
Method Blank
Total/NA
LCS 180-271342/2-A
Lab Control Sample
Total/NA
180-86915-A-1-1 MS
Matrix Spike
TCLP
180-86915-A-1-J MSD
Matrix Spike Duplicate
TCLP
Analysis Batch: 271499
Matrix
Method
Prep Batch
Sludge
EPA 4470A
271342
Solid
EPA 7470A
271342
Solid
EPA 7470A
271342
Solid
EPA 7470A
271342
Solid
EPA 7470A
271342
Solid
EPA 7470A
271342
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
all Farms
TCLP
Sludge
EPA 601 OD
271355
LB 180-271274/1-C
Method Blank
TCLP
Solid
EPA 601 OD
271355
MB 180-271355/1-A
Method Blank
Total/NA
Solid
EPA 601 OD
271355
LCS 180-271355/2-A
Lab Control Sample
Total/NA
Solid
EPA 601 OD
271355
'
General Chemistry
Prep Batch: 271319
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
9030E
MB 180-271319/1-A
Method Blank
Total/NA
Solid
9030B
LCS 180-271319/2-A
Lab Control Sample
Total/NA
Solid
9030B
490-168890-1 MS
McCall Farms
Total/NA
Sludge
9030E
490-168890-1 MSD
McCall Farms
Total/NA
Sludge
9030B
Analysis Batch: 271334
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
all Farms
Total/NA
Sludge
EPA 9034
271319
MB 180-271319/1-A
Method Blank
Total/NA
Solid
EPA 9034
271319
LCS 180-271319/2-A
Lab Control Sample
Total/NA
Solid
EPA 9034
271319
490-168890-1 MS
McCall Farms
Total/NA
Sludge
EPA 9034
271319
TestAmerica Nashville
Page 23 of 31 3/6/2019

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
wwwramor-o • 7evw9xw@ai ,*i* :I z
General Chemistry (Continued)
Analysis Batch: 271334 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1 MSD McCall Farms
Total/NA
Sludge
EPA 9034
271319
Analysis Batch: 271450
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1 all Farms
Total/NA
Sludge
254OG
_
180-86358-B-20 DU Duplicate
Total/NA
Solid
2540G
Analysis Batch: 271506
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1 all Farms
Total/NA
Sludge
EPA 9045D
LCS 180-271506/1 Lab Control Sample
Total/NA
Solid
EPA 9045D
180-86977-J-1 DU Duplicate
Total/NA
Solid
EPA 9045D
Prep Batch: 271760
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
9012B
MB 180-271760/4-A
Method Blank
Total/NA
Solid
9012B
HLCS 180-271760/2-A
Lab Control Sample
Total/NA
Solid
9012E
LCS 180-271760/3-A
Lab Control Sample
Total/NA
Solid
9012B
LLCS 180-271760/1-A
Lab Control Sample
Total/NA
Solid
9012B
180-87076-D-1-B MS
Matrix Spike
Total/NA
Solid
9012E
180-87076-D-1-C MSD
Matrix Spike Duplicate
Total/NA
Solid
9012E
Analysis Batch: 271809
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
EPA 9012B
271760
MB 180-271760/4-A
Method Blank
Total/NA
Solid
EPA 9012B
271760
HLCS 180-271760/2-A
Lab Control Sample
Total/NA
Solid
EPA 9012E
271760
LCS 180-271760/3-A
Lab Control Sample
Total/NA
Solid
EPA 9012B
271760
LLCS 180-271760/1-A
Lab Control Sample
Total/NA
Solid
EPA 9012E
271760
180-87076-D-1-B MS
Matrix Spike
Total/NA
Solid
EPA 9012B
271760
180-87076-D-1-C MSD
Matrix Spike Duplicate
Total/NA
Solid
EPA 9012B
271760
Analysis Batch: 578372
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168890-1
McCall Farms
Total/NA
Sludge
1010A
MB 490-578372/1
Method Blank
Total/NA
Solid
1010A
LCS 490-578372/2
Lab Control Sample
Total/NA
Solid
1010A
LCSD 490-578372/14
Lab Control Sample Dup
Total/NA
Solid
1010A
280-120182-A-1 DU
Duplicate
Total/NA
Solid
1010A
TestAmerica Nashville
0
Page 24 of 31 3/6/2019

Lab Chronicle
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Client Sample ID: McCall Farms
Lab Sample ID: 490-168890-1
Date Collected: 02/19/19 10:00
Matrix: Sludge
Date Received: 02/21/19 08:55
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
TCLP
Leach
EPA 1311
25 g
500 mL
271312
02/26/19 08:16
TAH
TAL PIT
TCLP
Analysis
EPA 8260D
1
0.125 mL
5 mL
271299
02/26/19 10:29
KLG
TAL PIT
TCLP
Leach
EPA 1311
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
TCLP
Prep
3510C
200 mL
10.0 mL
271367
02/26/19 12:10
CBY
TAL PIT
TCLP
Analysis
8270E
1
1 mL
1 mL
271438
02/27/19 16:57
VVP
TAL PIT
TCLP
Leach
EPA 1311
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
TCLP
Prep
3510C
100 mL
40.0 mL
271365
02/26/19 11:00
CBY
TAL PIT
�.
TCLP
Analysis
EPA 8081B
1
271475
02/27/19 15:48
DFE
TAL PIT
TCLP
Leach
EPA 1311
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
TCLP
Prep
8151A
100 mL
10.0 mL
271391
02/26/19 14:30
CBY
TAL PIT
TCLP
Analysis
EPA 8151A
20
271555
02/28/19 00:53
JBF
TAL PIT
TCLP
Leach
EPA 1311
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
TCLP
Prep
3010A
5 mL
50 mL
271355
02/26/19 12:20
NAM
TAL PIT
TCLP
Analysis
EPA 601 OD
1
271499
02/27/19 09:08
RJG
TAL PIT
TCLP
Leach
EPA 1311
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
TCLP
Prep
7470A
50 mL
50 mL
271342
02/26/19 11:05
RJR
TAL PIT
TCLP
Analysis
EPA 7470A
1
271395
02/26/19 16:16
KA
TAL PIT
Total/NA
Analysis
1010A
1
578372
03/01/19 17:29
VRP
TAL NSH
Total/NA
Analysis
2540G
1
271450
02/27/19 08:43
JMS
TAL PIT
Total/NA
Analysis
EPA 9045D
1
20.05 g
20 mL
271506
02/27/19 12:00
JMS
TAL PIT
Client Sample ID: McCall Farms
Lab
Sample ID: 490-168890-1
Date Collected: 02/19/19 10:00
Matrix: Sludge
Date Received: 02/21/19 08:55
Percent Solids: 51.2
I
Batch
Batch
Dil
Initial
Final
Batch
Prepared
`p
Prep Type
Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Prep
3541
15.1 g
20.0 mL
271476
02/27/19 09:52
BAP
TAL PIT
Total/NA
Analysis
EPA 8082A
1
271567
02/28/19 14:50
JMO
TAL PIT
Total/NA
Prep
9012B
1.04 g
50 mL
271760
03/01/19 12:40
BSH
TAL PIT
Total/NA
Analysis
EPA 9012E
1
271809
03/01/19 19:30
JAS
TAL PIT
Total/NA
Prep
9030B
5.03 g
50 mL
271319
02/26/19 09:35
SES
TAL PIT
Total/NA
Analysis
EPA 9034
1
271334
02/26/19 11:22
SES
TAL PIT
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
Page 25 of 31 3/6/2019

Method Summary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168890-1
Project/Site: McCall Farms
Method
Method Description
Protocol
Laboratory
EPA 8260D
Volatile Organic Compounds by GC/MS
SW846
TAL PIT
8270E
Semivolatile Organic Compounds (GC/MS)
SW846
TAL PIT
EPA 8081 B
Organochlorine Pesticides (GC)
SW846
TAL PIT
EPA 8082A
Polychlorinated Biphenyls (PCBs) by Gas Chromatography
SW846
TAL PIT
EPA 8151A
Herbicides (GC)
SW846
TAL PIT
EPA 601OD
Metals (ICP)
SW846
TAL PIT
EPA 7470A
Mercury (CVAA)
SW846
TAL PIT
1010A
Ignitability, Pensky-Martens Closed -Cup Method
SW846
TAL NSH
2540G
SM 2540G
SM22
TAL PIT
EPA 9012E
Cyanide, Total andor Amenable
SW846
TAL PIT
EPA 9034
Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL PIT
EPA 9045D
pH
SW846
TAL PIT
3010A
Preparation, Total Metals
SW846
TAL PIT
3510C
Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL PIT
3541
Automated Soxhlet Extraction
SW846
TAL PIT
5030C
Purge and Trap
SW846
TAL PIT
7470A
Preparation, Mercury
SW846
TAL PIT
8151A
Extraction (Herbicides)
SW846
TAL PIT
9012B
Cyanide, Total and/or Amenable, Distillation
SW846
TAL PIT
9030E
Sulfide, Distillation (Acid Soluble and Insoluble)
SW846
TAL PIT
EPA 1311
TCLP Extraction
SW846
TAL PIT
Protocol References:
SM22 = Standard Methods For The Examination Of Water And Wastewater, 22nd Edition
SW846 ='Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
1,'0
Page 26 of 31 3/6/2019

Accreditation/Certification Summary
Client: Bio-Nomics Services., Inc.
Project/Site: McCall Farms
Laboratory: TestAmerica Nashville
The accreditabons/certifications listed below are applicable to this report.
TestAmerica Job ID: 490-168890-1
CAuthority Program EPA Region Identification Number Expiration Date
South Carolina State Program 4 84009 [phone] *
Laboratory: TestAmerica Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
South Carolina State Program 4 89014 04-30-19
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method
Prep Method
Matrix
Analyte
2540G
Sludge
Percent Moisture
2540G
Sludge
Percent Solids
8270E
3510C
Sludge
1,4-Dichlorobenzene
8270E
3510C
Sludge
2,4,5-Tdchlorophenol
8270E
3510C
Sludge
2,4,6-Trichlorophenol
8270E
3510C
Sludge
2,4-Dinitrotoluene
8270E
3510C
Sludge
Cresols
8270E
3510C
Sludge
Hexachlorobenzene
8270E
3510C
Sludge
Hexachlorobutadiene
8270E
3510C
Sludge
Hexachloroethane
8270E
3510C
Sludge
Nitrobenzene
8270E
3510C
Sludge
Pentachlorophenol
8270E
3510C
Sludge
Pyridine
EPA 8151A
8151A
Sludge
2,4,5-T
EPA 8151A
8151A
Sludge
2,4-D
EPA 8151A
8151A
Sludge
Silvex (2,4,5-TP)
EPA 8260D
Sludge
1,1-Dichloroethene
EPA 8260D
Sludge
1,2-Dichloroethane
EPA 8260D
Sludge
2-Butanone (MEK)
EPA 8260D
Sludge
Benzene
EPA 8260D
Sludge
Carbon tetrachloride
EPA 8260D
Sludge
Chlorobenzene
EPA 8260D
Sludge
Chloroform
EPA 8260D
Sludge
Tetrachloroethene
EPA 8260D
Sludge
Trichloroethene
EPA 8260D
Sludge
Vinyl chloride
EPA 9012E
9012B
Sludge
Cyanide, Total
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
TestAmerica Nashville
Page 27 of 31 3/6/2019

a
r'
TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN COOLER RECEIPT FORM 490-168890 Chain of Custody
Cooler Received/Opened On 2/2112019 @ 8:55
j
v Time Samples Removed From Gooier ��J r Time Samples Placed In Storage (5 A
(2 Hour Window)
1. Tracking # (last 4 digits, FedEx) Courier: FedEx
IR Gun ID 17960358 pH Strip Lot Chlorine Strip Lot
2. Temperature of rep, sample or temp blank when opened: J Degrees Celsius
3. If Item #2 temperature is 0°C or less, was the representative sample or temp blank frozen?
YES NO..CA)
4. Were custody seals on outside of cooler?
/�EI,S... NO ... NA i
If yes, how many and where:
y
5. Were the seals intact, signed, and dated correctly? '
�...NO...NA
6. Were custody papers inside cooler?
l�
...NO ... NA
v
7. Were custody seals on containers. YES NN and Intact
YES...NO... A
Were these signed and dated correctly?
YES ... NO.
�N�
8. Packing mall used? Bubblewrap Plastic bag Peanuts Vermiculite Foam Insert Paper Other None
9. Cooling process: IC Ice -pack Ice (direct contact) Dry Ice
Other None
10._.Did all contalners arrive In good -condition (unbroken)? — -- - — —
YE ...NO...NA
11. Were all container labels complete (#, date, signed, pres., etc)?
cE ... NO ... NA
12. Did all container labels and tags agree with custody papers?
... NO ... NA
13a. Were VOA vials received? o
YES.�5...NA
s
b. Was there any observable headspace present in any VOA vial?
YES...NO... JA
Aft
Larger than this.
14. Was there a Trip Blank In this cooler? YES..NJ1�..NA If multiple coolers, sequence #
I certify that I unloaded the cooler and answered questionn--s7-14 (intial) '
15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level? YES ...NO..[NAl
b. Did the bottle labels Indicate that the correct preservatives were used .NO...NAA
16. Was residual chlorine present? YES ... NO.. [�)�
certify that I checked for chlorine and pH as per SOP and answered questions 15-16 (intial) d
17. Were custody tapers properly filled out (ink, signed, etc)? E ...NO ... NA
18. Did you sign the custody'papers in the appropriate place? Y� ...NO ... NA
i
19. WerQ cpfrect containers used.Yor the analysis requested? YE ... NO ... NA
20. Was sufficient am�ouo of sample sent in each container? YE ..NO ... NA i
! I certify that I entered this protect into LIMS and answered questions 17-20 {intial)
i
i
•• I certify that I attached a label With the unique LIMS number to each container (intiafl
21. Were ere.Non-Conformance issues at login? YES...NO Was a NCM generated? YES.. NO...#
B1S = Broken 6 shiprrir<n(
Cooler Receipt For n.doc LF-I Revised 8/23(17
EPage A of 31 - 3/6/2019 �

t
C
Nashville
2960 Foster Creighton Drive
Chain of Custody record
Nashville, TN 37204
nhnne. 615726 0177 fax [phone]
Test medca
LOG: 490
168890 THE LEADER IN ENVIRONMENTAL TESTING
Client Contact
Project Manager: Vaughn Stevenson
Site Contact:
Date:
2/2
I
COC No
Bio-Nomic Services
Tel/Fax:
Lab Contact:
Ken
Hayes
Carrier:
I of 1 COCs
516 Rountree Road
Fs`d
(;
-"
I°
W
u
CC
cG
a
H
U
p
a
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U
a
F
a
H
a
F
w
A
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c4
Y
0
F.
a
a
Job No.
Charlotte, NC 28217
Calendar C) or Work Days (W)
704-529-0000
TAT if different from Below
2 weeks
0 1 week
� 2days
L] 1 day
Sample Sample Sample # or',
Date Time Type Matrix Cant
SDG No.
Project Name: McCall Farms
State: NC
P O# 48765
Sample Identification
Sample Specific Notes:
McCall Farms
2/19/2019
1000
*solid
*solid
X
X
X
X
X
X
X
X
X
*Use Alternate Matrix: Sludge
Preservation Used, 1= Ice, 2= HCI; 3= MSO4; 4=HNO3; 5--NaOH; 6= Other
ESaimplesposal
Possible Hazard Identification
Non -Hazard Maminable =Skin Irritant Poison B Unknownrn
(A fee may be assessed if samples are retained longer than t month)
To Client Disposal By Lab Archive For Months
Special Instructions/QC Requirements & Comments: *Alternate Matrix: Sludee
i
Relinquished by:
ionrvtcc�
Company:
Date/Time:
Re c ' ed /
( �
Company:
�Ar
Date ime: /
d��.0 t9 � Lr)gQo
r
Relinquished by
Company:
Da e/I'ime:
Received by:
Company:
Dateftime: 1 I
Relinquished by:
Company:
Dafe/Tirhe:
Received by.
Company:
-4 4s
Date/rime:
0zlzIAK
MY

O_
W
W
N
O
TestAmerica Nashville
2960 Foster Creighton Drive stAmeriea
Chain of Custody Record
Nashville. TN 37204
Phone [phone] Fax [phone] ADER IN ENVIRUUME41AL TESIINU
Client Information (Sub Contract Lab) samp.er. Hayes, Ken 490 168890 Chain of Custody i330.1
Mont Cc lacti Phone: E-Mail:
Shipping/Receiving [e-mail] JNorth Carolina Page 1 of 1
Company:
Accreditation Required (See note):
Job a:
TestAmerica Laboratories, Inc.
State Program - North Carolina (WW/SW); State Program - ...
490.168890-1
Address:
Duo Dale Requested:
Preservation Codes:
301 Alpha Drive, RIDC Park,
2122/2019
Analysis
Requested
A-HCL M-flexano
B - NoOH N - None
City:
TAT Requested (days):
_
Pittsburgh
C - Zn Acetate 0 - AsNaO2
D - Nitric Acid P - Na204S
Slate. Zip:
PA,15238
o
E-NoHSO4 0-Na2SO3
F-MeOH R-Na2S203
Phurle;
PO 0:
412-963-7058(Tel) 412-963-2468(Fax)
0
Z
o
?
"
i
O-AmcMor S-H2SD4
H- Ascorb c Acid T- TSP Dodecahydrale
1- Ice U - Acetone
EmaiC
WO 0:
m o-
vi
a
-aa
.'"o`
3
m
e
J - Of Water V-MCAA
K-EDTA W-PI4.5
ProiectName:
Projects:
McCall Farms
49001945
0 3
nC.
y
J
r
o
a
J
o
a
d
m
a
c
L- EDA Z •other (specify)
Other:
Silo:
SSOWA:
to
`o
Sample
Matrix
S
Type
(w .I�,s.aow,
tlr
m
3
o
rd
m
Ul
c
?
z
Sample
(C=comp,
o. sore,
t
A
m
n
o
o
m
"
Sample Identification - Client ID Lab ID
Sam le Date
Time
G= rab
eT.TaaW,A xY
fI "a'.
m
m
o
.m
m
m
'tie
t°-
S ecial Instructions/Note:
Preservation Code;
McCall Farms (490.168890-1)
2119/19
0:OD
Eastern
Solid
X
X
X
X
I X
X
X
X
X
X
X
1
4
Note: Since laboratory acciedilalions are subject to change. TostAmenca Laboratories, Inc. places the ownership of method, analyze & accreddaton compliance upon out subcontract laboratories. This sample shipment 1s forwarded under chainof-custody. If the laboratory does not
currently maintain accreditation in the Stale of Orgin listed above for analysislieslshnatrix being analyzed, the samples must be slipped back to the TestAmerica laboratory or other instructions vill be provided. Any changes to accreditation status should be brought to TestArnerica
labomichos. Inc, attention immediately. tau requested accrod:latrons are current Iodate. return the signed Chain of Custody attesting to said compheance to TestAmerica Laboratories, Inc.
Possible Hazard Identification
Sample Disposal (A fed may be assessed If samples are rdtalned longer than 1 month)
Unconfirmed
I Return To Client Disposal By Lab Archive For Months
Deliverable Requested: I, 11, Ili, IV, Other (specify) Primary Deliverable Rank: 2
Special Instructions/QC Requirements:
Empty Kit Relinquished by: Date: Time: Method of shipmenb
Re!inquished_hy:
Zelfime:
Company
Recu edby.
Dale ime:
Company.
tom//
66
►►AAtt
��
ellnquhshed by.
Dalurrimu:
Company
Received by.
Date/Timu:
Company
Relinquished by:
Dale/Timo:
Company
Received by.
Daterrime:
Company
Custody Seals Intact:
Custody Seal No.;
Cooler Temperagoo(s)'C and Other Remarks:
1 Yes A No
Ver. (11/1 hh019

Client: Bio-Nomics Services., Inc.
Login Number: 168890
List Number: 2
Creator: Say, Thomas C
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Job Number: 490-168890-1
SDG Number:
List Source: TestAmerica Pittsburgh
List Creation: 02/23/19 11:33 AM
TestAmerica Nashville
Page 31 of 31 3/6/2019
E13

RECEIVED/NCDENR/DWR
2019 ANNUAL REPORT
LAN® APPLICATION PROGRAM
BIO-NOMIC SERVICES, INC.
PERMIT #WQ0039053
Prepared For:
Bio-Nomic Services
530 Woodlawn St
Belmont, NC 28012
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231 B Summerfield Road
Sur merfield, North Carolina 27358
January 2019
JAN 14 2019
WQROS
MOORESVILLE'REGIONAL OFFICE
RECEIVED/NCDEOIDWR
JAN - 9 2019
Non -Discharge
Permitting Unit
,RC.FA F
JAN — 9 2019
INFORMATION PROCESSING UNIT

January 8, 2019
NCDEQ-DWR Non -Discharge Branch
512 North Salisbury Street
9" Floor, Office #942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
Reference: 2018 LAND APPLICATION ANNUAL REPORT
Bio-Nomic Services, Inc.
Permit No. WQ0039053
WMSS Project No. 15-18 Ph: 09
Non -Discharge Permitting Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Bio-Nomic Services, Inc. (Bio-
Nomics) for the above referenced permit. WMSS compiled this report using data gathered during the
compliance year by Bio-Nomics. This data includes: 1) Class A Annual Distribution and Marketing /
Surface Disposal Certification and Summary Form (DMSDF).
Bio-Nomics did not land apply any residuals under this permit during the calendar year of 2018.
If there is any further information required or questions regarding this annual report please do not
hesitate to contact the Bio-Nomic Services, Inc. or WMSS for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
NC Land Application/Residuals Operator
422753
Enclosures
Shared\WMSS Projects\2015\15-18 Bio-Nomics\Phase 09 - Class A Permit\2018 Annual Report\2018 ANNUAL REPORT.doc

TABLE OF CONTENTS
SECTION NO. TITLE
DMSDF

DMSDF

CLASS A ANNUAL, DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL. CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039053 FACILITY NAME: BIO-NOMIC SERVICES, INC.
PHONE: [phone] COUNTY: MECKLENBURG OPERATOR: Peter P. Fleetwood - President
FACILITY TYPE (please check.one): ❑ Surfoce Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation durine the nest calendar Year? Yes 11 No i+1 — b If No akin nnrts A- R_ C "nd rardifv fnrm hainw
PartA*: Part B*:
Month
Sources(s) (include.NPDES # if
applicable)
V lume (dry tons Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
August
September
October
November
December
Total. from FORM DMSDF (sup)
Totals: Annual (da tons):tons):1
0
.0
0
0
Amendments used: I
I Bullan A ent s used:
* if more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)r
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit Q Yes*
(including but not limited to items 1-3 below). issued by the Division of Water Resources: © No 0 If No, explain In Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware .that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
f
Signature of Permittee ' lYate
Signature of Preparer"
(if different from Permi(tee)
**Preparer is defined ind0 CFR Pan 503.9(r) and 15A NCAC 2T -1102 (26)
*NO LAND APPLICATION OCCURRED DURING THE 2018 CALENDAR YEAR
Date
DENR FORM DMSDF (1212006)

\VV
2017 ANNUAL REPORT
LAND APPLICATION PROGRAM
BIO-NOMIC SERVICES, INC.
PERMIT #WQ0039053
Prepared For:
Bio-Nomic Services
530 Woodlawn St
Belmont, NC 28012
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231 B Surmnerfield Road
Summerfield, North Carolina 27358
January 2018
RECEIVEDINCDeNRIDWR
JAN 16 2018
WQROS
MOORESVILLE REGIONAL OFFICE
)�C'
®�vRprO�s
s�ctign V 1i J

Willcox&mabe
SOIL SOLUTIONS
January 4, 2018
NCDEQ-DWR
512 North Salisbury Street
6`1 Floor, Room 640A
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
Reference: 2017 LAND APPLICATION ANNUAL REPORT
Bio-Nomic Services, Inc.
Permit No. WQ0039053
WMSS Project No. 15-18 Ph: 09
Non -Discharge Permitting Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all -monitoring -and reporting
requirements as specified in the above referenced permit on behalf of Bio-Nomic Services, Inc. (Bio-
Nomics) for the above referenced permit. WMSS compiled this report using data gathered during the
compliance year by Bio-Nomics. This data includes: 1) Class A Annual Distribution and Marketing /
Surface Disposal Certification and Summary Form (DMSDF).
Bio-Nomics did not land apply any residuals cinder this permit during the calendar year of 2017.
If there is any fitrther information required or questions- regarding this annual report please do not
hesitate to contact the Bio-Nomic Services, Inc. or WMSS for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
/ k�: i-� A I � - �-
Marlin Mabe
NC Land Application/Residuals Operator
#22753
Enclosures
Shared\WMSS Projects\2015\15-18 Bio-Nomics\Phase 09 - Class A Permit\2017 Annual Report\2017 ANNUAL REPORT.doc
Willcox & Mabe Soil Solutions, PLLC / 1205 W. Bessemer Avenue, Suite 202 / Greensboro, NC 27408 / Rob 336.339.9128 or
Martin 336.312.1396 / www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
DMSDF

IAll ti61 sly

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: W90039053 FACILITY NAME: -' BIO•NOMIC SERVICES, INC.
PHONE: [phone] COUNTY: MECKLENBURG OPERATOR: Peter P. Fleetwood - President
FACILITY TYPE (please check one): 1] Surface Disposal (com$iete Part A (Source(s) and "Residual In" Volume only) and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation durine the vast calendar year? Yes Q No El —► If No skid starts A. B. C and certify form below
Part A-:
Part B-:
Month
Sources(s) (include NPDES # lf
Valumc
(dry tons
Recipient Information
Amendmapplicable) Bulldog Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended usc(s)
January
February
March
APO
i4la
June
July
--
Au st
September
October
November
December
Total from FORM DMSDF (sup)
- --
Totals: Annual loss ..
0-
--0
- ®
- 0
.
- Amcadmear s) used:
-DuWd A rn s used:
" Ifnioro space is required, anacb additional information sheets (FORM DMSDP(supp)): Total Numbcr of Form DMSDF (Supp)i
Part C:
Facility was eomplinat during the past calendar year with all conditions of the land application permit El Yes -
(including but not limited to Items 1-3 below) issued by the Division of Water Resources: © No ---► If No, Explain In Narrative
1. All monitoring was done is accordance with the permit and reported for the year as required and three (3) topics of certified laboratory mulls are attached
2. All operation and maintenonce requirements were compiled with or, in the case ofa deviation, prior authorization was received fitim the Division of Water Resources.
3. No contravention of Ground Water Quality SWula ds occurred at a monitoring well.
"I certify, under penalty of law, that the above Information Is, to the hest of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false Information, Including the possibility or lines and Imprisonment for knowing vlolatiota. "
Signature of Parninee ^ Da Signature orPncparcr-" patc
(if different from Pcnnitta)
"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
-NO LAND APPLICATION OCCURRED DURING THE 2017 CALENDAR YEAR
08NR FORM DMSDF (I2=06)