WQ0011038_Regional Office Historical File Pre 2018 (4)

Water Resources
Environmental Quality
ROY COOPER
� v Governor
MICHAEL S. REGAN
-- Secretary LINDA CULPEPPER
Interim Director:
February 9, 2018
Ms. Pem Carter, Senior Environmental Engineer via Email
CNA Holdings, LLC - Shelby Facility
2525 Blacksburg Road
Grover, North Carolina 28073
Subject: Non -Discharge Permit Inspection
And Acknowledgement of Receipt of the 2017
Annual Report
CNA Holdings, Inc. Celanese Shelby Plant
Permit # WQ0011038
Land Application of Residuals
Cleveland County
Dear Ms. Carter:
Enclosed you will find the report for the compliance inspection. conducted on February. 7tn,
2018 for the referenced permit. You will receive a separate report for the NPDES inspection
(permit #NC0004952) conducted by Ori Tuvia, also from the Mooresville Regional Office
(MRO).
In addition, A copy of the 2017 Annual Report was received at the MRO, on February 5tr,
2018. The report indicates there was no land application activity conducted under- this permit
in 2017. Per our conversation, should you choose to rescind, the request maybe directed to -
Nathaniel.ThornburaCaD-ncdenr.gov.
I would like to thank you and Mr. Sparks (WWTP ORC) for your time during the inspection. The
attached report should be self-explanatory; however, I may be reached by phone [phone])
or email (maria. schuttea-ncdenr.aov) with questions:
Sincerely, !
Maria Schutte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
- Division of Water Resources, NCDENR
Attachment(s): Inspection Report February 2018
CC: Nicole B. Coffee, Site Leader, CNA Holdings (email)
State of North Carolina f Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115
704 663 1699

of North Carolina Department of Environmental Quality
on of Water Resources
Roy Cooper, Governor
Michael S. Regan, Secretary
Linda Culpepper, Interim Director
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Owner: CNA Holdings, Inc. — Shelby County: Cleveland
Permit #: W00011038 (non-503) Issued: 12/19/2014 Expiration: 04/30/2020
Permittee Contact: Pem Carter (Sr. Env. Engineer) Phone: [phone] Email: pem.carterkcelanese.com
Additional Contact: Nicole B. Coffee (Site Leader) Phone: [phone] Email: nicole.coffeegcelanese:com
ORC Name: Roy Whittaker #13283 Phone: [phone] x115 Email: roy.whittaker(c�r�,emaresourcesinc.com
B/U ORC: Brent Collins #27651 Phone: [phone] (cell) Email: brent.collinsnemaresourcesinc.com
B/U ORC: Jonathan Hill (Sprint Waste) #27659 Phone: [phone] (cell) Email: jhill cgsprintwaste.com
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP Facility Start-up
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Date(s): February 7, 2018
Inspection Summary: (additional comments may be included on attached pages)
This inspection included a review of records and residuals processing and storage at the WWTP. The facility
continues to manage their residuals in the on -site storage lagoons. Data records were found to be in excellent
order.
Please note the issues below to maintain overall compliance:
• Per conversation, Rip -Rap placed for berm stabilization was verified as free from contaminants. The
documentation was requested to be emailed to: Maria.Schutte(a),ncdenr.jEov.
• Lagoon storage requires two feet of freeboard be maintained. The appropriate water level gauges, with
inch or tenths of afoot increments, need to be placed at the lowest point of each lagoon berm. And
weekly levels documented.
• The MRO should be informed of any changes to the contact information noted above. Please email
corrections/updates to Maria Schulte at the email address above.
Is a follow-up inspection necessary _yes X no?
Inspector Name/Title: Maria Schulte, Environmental Specialist; Ori Tuvia, Engineer
Telephone No.: 704-663-1699 Fax No. 704-663-6040
Date of Inspection: 2%7/2018

ials Inspection
11038 CNA Holdings, Inc. — Shelby Plant — Cleveland County
,f Residual
X Land Application (class B)
Record Keeping
Y-yes N-no N/A -not applicable
Distribution and Marketing (class A)
N/E-not evaluated
Page 2
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
Y TCLP analysis, NE SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y Hauling records (# gal and/or ton hauled during calendar year to date)
Y Field loading records, NE Field site maps and information
Y Records of lime purchased
Y Pathogen & Vector Attraction Reduction (Fecal analyses were done for the renewal application)
Comments: All residuals records are maintained at the WWTP. Data reviewed appeared to meet permit
requirements. There has been no land application since 2009 and no event is planned. Plant production and
residuals generation is very low and the facili4y has ample lagoon storage. Upper management will determine
whether to retain this permit or apply for rescission.
Pathogen & Vector Attraction Reduction (PVAR) records
This permit is 503 exempt — Pathogen and Vector Attraction Reduction analyses are not required
Sampling
Describe Sampling: There was no land application for 2017 — sampling was not observed
Is sampling adequate? NE Is sampling representative? NE
Treatment
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime Other -describe
Transport No land application was taking place during this inspection.
Spill control plan in transport vehicle? NA
Does transport vehicle appear to be maintained? NA
Storage
Number of days/weeks/months of storage: Per prior inspections, estimated at 1095 days.
Describe storage: Sludge Residuals are stored in 2 unlined lagoons estimated at 1.66 MG and 2.23 MG.
Appropriate water level gauges are to be installed at the lagoons, as noted on the first page of this report.
Odors present N Vectors present N
Field Sites (end use for class B biosolids) No land application was taking place during this inspection.
Field identification: NA — See note above.

F01
scharge Permit Inspection Page 3
1038 CNA Holdings, Inc. — Shelby Plant — Cleveland County
Monitoring well(s) Y/N: NA
If yes, location of well(s):
Comment: This permit does not require groundwater monitoring_
Odors/vectors No active land application was taking place during this inspection. Odors and vectors were
not detected at the WWTP storage lagoons at the time of inspection.
Describe any nuisance conditions and any corrective actions needed. NA
Odors present N
Vectors present N
Other noted conditions
Note for future inspections: This facility requires safety instruction for entry and PPE (steel toed shoes,
eyeglasses and hard-hat if in the industrial plant). The safety instruction is valid for 1 year.
Pem Carter is planned to retire from her position in June 2018. Her replacement has not been determined.

Water. Resources
ENVIRONMENTAL QUALITY
November 4, 2016
�="-"Z7overnor.
DONALD R. VAN DER VAART
Secretary
S..JAY ZIMMERMAN
Director
Ms. Pem Carter, Senior Environmental Engineer
CNA Holdings, LLC = Shelby Facility
2525 Blacksburg Road
Grover, North Carolina 28073
Subject: Non-DischargePermit Inspection
CNA Holdings, Inc. Celanese Shelby -Plant
Permit.No.: WQ0011038
Land Application of Residuals
Cleveland County
Dear Mt. Carter:
Staff of the Mooresville..Regional Office.(MRO) conducted a compliance inspection on October 20th,
2016, for the CNA Holdings, Inc: Celanese Shelby Plant land application program. The inspection
included the WWTP residuals processing, storage. and on=site records, maintenance.
I would like to thank you for your time during the inspection. The attached report, should be self-
explanatory;. however, I may be reached at maria.schutte0-ncdenr.gov or [phone], With any
questions.
Sincerely,
Maria Schulte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operationi Section -
Division of Water: Resources, NCDEQ
Enclosures) Inspection Report October 2016
CC: Rafael Gonzalez, Site Leader, CNA Holdings (email)
State of North Carolina J Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional, Office) 616 East Center Avenue, Suite 3011 Mooresville, North Carolina 28115
— ----. 704,663 1699_ =__ —

State of North Carolina Department of Environmental Quality
Division of Water Resources
Pat McCrory, Governor
Donald R. van der Vaart, Secretary
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Owner: CNA Holdings,.Inc. — ShelbyPlant County: Cleveland
Permit #:_W00011038 (non 503) Issued: 12/19/2014 Expiration: 04/30/2020
Permittee Contact: Pem Carter (Sr. Env. Engineer) Phone: [phone] Email: pem.ciAerncelanese.com
Additional Contact: Rafael Gonzales (Site Leader) Phone: [phone] Email: [e-mail]
ORC Name:. Roy L. Whittaker #13283 Telephone No.: 33.6-766-0328 ext 115
B/U ORC: Brent Collins (EMA) #27651 Telephone No.: 336-399-3646 (cell)
71
Reason for Inspection
X . ROUTINE COMPLAINT FOLLOW-UP Facility Start-up
Type of inspection
Collection System Spray Irrigation ' X Sludge Other.
Inspection Date(s): October 20, 2016
Inspection Summary. • (additional comments may be included on attached pages)
This inspection included'a review of records and residuals processing and storage at the WWTP. The
facility continues to. manage their residuals in: .the on -site storage lagoons. Data records: were found to be in
excellent order. Lagoon berms were being addressed for some routine maintenance for vegetation and
replacement of rip -rap.
Please note the issues below to maintain overall compliance:
• Evaluate source of rip -rap to ensure there are no cross contamination concerns. Email information to .
Maria.Sehutte(a ncdenr.aov.
• The MRO should be informed of any changes to the contact information noted above. Please email
corrections/updates to Maria Schulte at the email address above.
Is a follow-up inspection necessary _yes ' X no?
Inspector Name/Title: Maria Schulte, Environmental: Specialist; Edward Watson, Hydrogeologist; Ori Tuvia, Engineer
Telephone No.: 704-235-2184 Fax,N6. 704-663-6040
Date of Inspection: 10/20/2016

FV�Discharge Permit Inspection Page 2011038 CNN foldimgs,Inc. — Shelby Plant —.Cleveland County
Type of Residual
X Land Application (class B) Distribution and Marketing (class A)
Record Keeping
Y-yes N-no N/A -not applicable N/E-not evaluated
Y Copy of current permit: available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
Y TCLP analysis, NE . SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine. most limiting parameter) YTD
Y Hauling records. (# gal and/or ton Hauled during calendar year to date)
Y Fieldloading-records; NE Field site maps and information
Y Records of lime purchased
Y Pathogen & Vector Attraction Reduction (Fecal analyses were done,for the renewal application)
Comments: All residudls records are:maintained at the WWTP. Data:reviewed appeared to meet permit
requirements There has been no land application since 2009 and no event is planned. Plant production
and residuals generation is very low and the facili has ample 1 oon.storae.
:Pathogen & Vector Attraction Reduction (PVAR) records
This permit is 503 exempt - Pathogen and Vector Attraction Reduction analyses.are not required..
Sampling
Describe Sampling: There was no land application for 2015 — sampling was. not observed
Is sampling adequate?. NE Is sampling representative? NE
Treatment
X Aerobic. digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime Other -describe
Transport No land application was takiM place during this inspection.
Spill controt plan in transport vehicle? NA
Does transport vehicle appear to be maintained? NA
Storage
Number of days/weeks/months of storage,: Per prior inspections; estimatedys: at. da
Describe storage: Sludge Residuals are stored in 2 unlined lagoons estimated at 1.66 MG and 2.23 MG.
Odors present N Vectors present N
Field Sites .(end use for class B biosolids) No land application was takmk &ce duiin this inspection.
Field identification: NA — See note above.

Non -Discharge Permit Inspection
WQ0011038.CNA Holdings, Inc. Shelby Plant — Cleveland County
Monitorink wells) Y/N: NA .
.If yes, location of well(s):
Comment: This permit does not requireoundwater n2onitorin
Odors/vectors. No active land application was takinplace during this inspection Odors and vectors
were not detected at the WWTP storazlagoons at the time of inspection
Describe any nuisance conditions and any corrective actions needed. NA
Odors present N
Vectors present N
Other noted. conditions
Note. for future inspections — this .facility requiressafety instruction for entry.

Pat McCrory
Governor
vw
A r'
_
NCDENR
North Carolina Department of Environment and Natural Resources
January 9, 2015
Ms. Pem Carter, Senior Environmental Engineer
CNA Holdings, LLC - Shelby Facility
2525 Blacksburg Road
Grover, North Carolina 28073
Dear Ms. Carter:
Donald van der Vaart
Secretary
Subject: Non -Discharge Permit Inspection
CNA Holdings, Inc. Celanese Shelby Plant
Permit No.: WQ0011038
Land Application of Residuals
Cleveland County
Enclosed you will find the report for the compliance inspection that was conducted on
December 5th, 2014 for the CNA Holdings, Inc. Celanese Shelby Plant, land application
program. The inspection included a review of: records, the residuals processing and
storage areas; and, a review of field sites noted in the permit renewal currently_ in
process with permitting staff at our Central Office in Raleigh.
The attached report should be self-explanatory; however, should you have questions
about the report or your renewal, please contact me by phone [phone]) or email
(maria.schutte(D-ncdenr.gov).
Sincerely,
Maria Schutte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
Attachment(s): WQ00110381nspection Report
cc: Luis Mendoza, Site Leader, CNA Holdings, Inc. Celanese. Shelby Plant (email)
Ed Hardee, Residuals Management, CO-LAU (email)
Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115
Phone: [phone] / Fax: [phone]/Customer Service 1-877-623-6748
Internet: www.ncdenr.gov

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Resources
Pat McCrory, Governor
Donald van der Vaart, Secretary
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: CNA Holdings, Inc. —Shelby Plant
Permit No.: W00011038 (non 503)
Permittee Contact: Pem Carter (Sr. Env. Engineer)
Additional Contact: Luis Mendoza (Site Leader)
ORC Name: Roy L. Whittaker #13283
B/U ORC: Brent Collins (EMA) #27651
County: Cleveland
Issued: 05/03/2006 Expiration: 04/30/2015
Telephone No.: 704-480-4700 or 5726
Telephone No.: 704-480-5728
Telephone No.: 336-766-0328 ext 115
Telephone No.: 336-399-3646 (cell
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Date(s): December 5, 2014
Inspection Summary: (additional comments may be included on attached pages)
This inspection was conducted in conjunction with the permit renewal, and included a records review and
residuals processing and storage at the WWTP. Land Application (LA) field sites were visited on the same
day, including EMA Resources staff, as part of the renewal process.
Data records were found to be in excellent order. The residuals storage lagoons were free of odors and
vectors at the time of inspection. Lagoon berms need some routine maintenance for vegetation removal.
Please note:
• CNA Holdings, Inc. LA renewal is nearing completion with permitting staff at our Central Office in
Raleigh. Questions may be directed to Trov.Dobv(a),ncdenr.gov in the Central Office or
Maria.Schutte(a-,ncdenr.gov in the Mooresville office.
• The MRO should be informed of any changes to the contact information noted above.
Is a follow-up inspection necessary _yes X no
Inspector(s): Maria Schulte - Environmental Specialist
Telephone No.: 704-663-1699 Fax No.: 704-663-6040
Date of Inspection: December 5t', 2014

tals Inspection
1103 8 CNA Holdings, Inc. — Shelby Plant — Cleveland County
if Residual
x Land Application (class B)
Record Keeping
Y-yes N-no N/A -not applicable
Distribution and Marketing (class A)
N/E-not evaluated
pg. 2
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
Y TCLP analysis, * Y SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y Hauling records (# gal and/or ton hauled during calendar year to date)
Y Field loading records, Y Field site maps and information (w/Renewal Package)
Y Records of lime purchased
Y Pathogen & Vector. Attraction Reduction (Fecal analyses were done for the renewal application)
Comments: All residuals records are maintained at the WWTP. Data reviewed appeared to meet permit
requirements. There has been no land application since 2009, but an event is expected to take place in the
spring of 2015.
Pathogen & Vector Attraction Reduction (PVAR) records
This permit is 503 exempt — Pathogen and Vector Attraction Reduction analyses are not required
Sampling
Describe Sampling: There was no land application for 2014 — sampling was not observed
Is sampling adequate? NE Is sampling representative? NE
Treatment
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime Other -describe
Transport No land application was taking place during this inspection.
Spill control plan in transport vehicle? NA
Does transport vehicle appear to be maintained? NA
Storage
Number of days/weeks/months of storage: Per prior inspections, estimated at 1095 days.
Describe storage: Sludge Residuals are stored in 2 unlined lagoons estimated at 1.66 MG and 2.23 MG.
Odors present N Vectors present N

Residuals Inspection
WQ0011038 CNA Holdings, Inc. - Shelby Plant — Cleveland County
Field Sites (end use for class B biosolids) No land application was taking place during this inspe
but an event is expected in the spring of 201 S.
Field identification: Field sites were visited on same day and reviewed for buffers, with EMA Resources staff,
as part of the permit renewal process. Noted in the staffport that afield has been lost to chicken houses
and family is likely to utilize chicken litter on ad'acent f elds. LA contractor has already discussed
tracking those loading rates with the farmer/owner.
Permit on site during application Spill plan on site
Y Buffers adequate Cover crop specified in permit
Documented exceedances of PAN limits Site condition adequate
Signs of runoff / ponding Rain Gauge on site during application
Are there any limiting slopes on fields?
10 % for surface application 18% for subsurface application
Monitoring well(s) Y/N: NA
If yes, location of well(s):
Comment: This permit does not require groundwater monitoring_
Odors/vectors No active land application was taking place during this inspection. Odors and vectors
were not detected at the WWTP storage lagoons at the time of inspection.
Describe any nuisance conditions and any corrective actions needed. NA
Odors present N
Vectors present N
Other noted conditions
Note for future inspections — this facility requires a safety instruction video once per year.

Pat McCrory
Governor
Ar-MA FILE
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Thomas A. Reeder
Director
Ms. Pem Carter, Senior Environmental Engineer
CNA Holdings, Inc. - Ticona
2525 Blacksburg Road
Grover, North Carolina 28073
Dear Ms. Carter:
John Skvarla
Secretary
October 29, 2013
Subject: Non -Discharge Permit Inspection
CNA Holdings, Inc. - Ticona - Permit No.: WQ0011038
Land Application of Residuals
Cleveland County
Enclosed you will find the report for the compliance inspection that was conducted on
October 2nd, 2013 for the CNA Holdings, Inc. — Ticona, land application program. The inspection
included the WWTP residuals storage, and records review.
Please note the current permit is set to expire on 04/30/2015, which means the renewal
application package is due for submittal by 10/30/2014 (180 days prior to expiration).
Should you have any questions concerning this report or your permit renewal, I may be reached at
[phone].
Sincerely,
Maria Schutte
Environmental Specialist
Attachment(s): WQ0011038 Inspection Report
cc: Luis Mendoza, Site Leader, Ticona (email)
Chonticha McDaniel, Residuals Management, CO-LAU (email)
Division of Water Resources / Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115
Phone: [phone] Fax: [phone] l Customer Service: 1-877-623-6748
Internet: www.ncwater.org
An Equal Opportunity i Affirmative Action Employer
Nne
orthCaroEna
;Vaturalty

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Resources
Pat McCrory, Governor
John Skvarla, Secretary
Thomas A. Reeder, Director
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: CNA Holdings, Inc. - Ticona
Permit No.: WQ0011038 (non 503)
Permittee Contact: Pem Carter (Sr. Env. Engineer)
Additional Contact: Luis Mendoza (Site Leader)
ORC Name: Brent Collins (EMA) #27651
B/U ORC: Roy L. Whittaker #13283
County: Cleveland
Issued: 05/03/2006 Expiration: 04/30/2015
Telephone No.: 704-480-4700 or 5726
Telephone No.: 704-480-5728
Telephone No.: 336-399-3646 (cell_
Telephone No.: 336-766-0328 ext 115
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Date(s): October 2"" 2013
Inspection Summary: (additional comments may be included on attached pages)
This inspection included a records review and WWTP inspection of the CNA Holdings, Inc, facility
(permit # NC 0004952). Per previous inspection reports, sludge storage is estimated to be 1095 days,
perhaps longer when flow is reduced. Ticona has not land applied in a few years, but currently plans to in
Spring of 2014. EMA Resources is the current land application contractor.
Land Application records are filed on -site and were well organized. Both the WWTP and records
appeared to be maintained in accordance with permit conditions. The current permit is due to expire on
April 30tr', 2015.
Celanese is the parent company of Ticona, and per discussion with Pem Carter, they plan a name
change to Celanese.
Is a follow-up inspection necessary _yes X no
Inspector(s): Maria Schutte - Environmental Specialist
Telephone No.: 704-663-1699 Fax No.: 704-663-6040
Date of Inspection: October 2nd, 2013

s Inspection
)38 CNA Holdings, Inc. - Ticona — Cleveland County
Type of Residual
X Land Application (non-503 industrial/commercial)
Comments:
Record Keeping
Y-yes N-no NE -not evaluated NA -not applicable
Pg 2
Land Application (Class B 503 municipal)
Y Copy of current permit available at residual generating site
NA Current metals and nutrient analysis (see permit for frequency)
NA TCLP analysis, NA SSFA (Standard Soil Fertility Analysis)
NA Nutrient and metals loading calculations (to determine most limiting parameter) YTD
NA Hauling records (# gal and/or ton hauled during calendar year to date)
NA Field loading records, Y Field site maps and information
NA Records of lime purchased
NA Pathogen & Vector Attraction Reduction
Comments: There was no land application in 2012 - no testing required.
Pathogen & Vector Attraction Reduction records Not Applicable
This permit is 503 exempt — Pathogen and Vector attraction reduction is not required.
Sampling
Describe Sampling: No land application for 2012 — no sampling
Is sampling adequate? NE Is sampling representative? NE
Treatment
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime Other -describe
Transport
Spill control plan in transport vehicle? NE
Does transport vehicle appear to be maintained? NE
Comments:
Storage
Number of days/months storage: Per previous inspection reports, estimated at 1095 dates.
Storage: CNA - Ticona has 2 unlined storage lagoons estimated at 1.66 MG and 2.23 MG.
Odors present N Vectors present N
Comments:

Residuals Inspection
WQ0011038 CNA Holdings, Inc. - Ticona — Cleveland County
Field Sites (end use for class B biosolids)
Not examined — no land application activity in recent years.
Per Pem Carter Ticona expects to land avl2ly in spring of 2014
Field identification:
Permit on site during application Spill plan on site
Buffers adequate _ Cover crop specified in permit
Documented exceedances -of PAN limits _ Site condition adequate
Signs of runoff / ponding — Rain Gauge on site during application
Are there any limiting slopes on fields?
10 % for surface application 18% for subsurface application
Odors/vectors
Describe any nuisance conditions and any corrective actions needed. No odors or vectors were detected at
the WWTP at the time of this inspection.
Odors present N
Vectors present N
Monitoring well(s) Y/N: NA
If yes, location of well(s): There are monitoring wells on -site, but they are unrelated to this permit.
Other noted conditions
Note for future inspections — this facility requires a safety instruction video once per year.

PEMC12:02D
NC Department of Environmental and Natural Resources
Aquifer Protection Division- Mooresville
610 East Center, Suite 30-i
Mooresville, NC. 28115
Dear Ms. Huffman,
Ticona
Ticona
2525 Blacksburg Road
Grover, NC 28073-9641
Carolina Star Worksite
ISO 9001, ISOlrS 16949,
ISO 17025, and ISO 14001
Subject: Land Application Permit No. W00011038
CNA Holdings, Inc,; Ticona Polymers, Shelby Plant
2525 Blacksburg Road, Grover, NC 28073
This is to inform you that the following communications pertaining to the above Water Quality
Permit should be directed as follows:
Facility/Technical Contact Authorized / Invoice Contact
PEM Carter, Env. Eng. Luis Mendoza, Site Leader
704-480-5726 704-480-5728
[e-mail] [e-mail]
Please correct your records, and communicate to others in need of this information. We request
the removal of all previous contacts you may have listed for our facility, for they are no longer
employed at this facility. Thank you for prompt attention to this request and if you should have
any further questions, please feel free to contact me at [phone], or via email at
[e-mail]
PEM Cart
Sr. Environmental Engineer
Ticona
Celanese
Ticona
A business of Celanese

QF W AT �RQ Beverly Eaves Purdue, Governor
FILEDee Freeman, Secretary
r North Carolina Department of Environment and Natural Resources
—i
Coleen H. Sullins, Director
Division of Water Qualify
AQUIFER PROTECTION SECTION
August 25, 2010
Mr. John Groves, Plant Manager
CNA Holdings, Inc.
2525 Blacksburg Rd.
Grover, North Carolina 28073
Subject: Land Application Inspection
Permit No. WQ0011038 (non-503)
Cleveland County
Dear Mr. Groves:
Enclosed is the inspection report for the inspection of the non -discharge Land
Application that was conducted on August 17, 2010. The report indicates compliance with the
subject permit, including lab data, and record keeping.
The attached report should be self-explanatory, however, if you have any questions,
please contact me at [phone].
Sincerely,
U
Ellen Huffman
Environmental Specialist
Cc: EMA Resources
Ed Hardee, LAU Residuals Program Coordinator
MRO files
Division of Water Quality / Aquifer Protection Section / Mooresville Regional Office Phone: [phone] Fax: [phone] NonrthCarolina;�\
610 East Center Avenue, Suite 301, Mooresville, NC 28115 Customer Service 1-877-623-6748 Internet: mvw.ncwaterquaIitV.orq Naturally UY

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Beverly H. Purdue, Governor
Dee freeman, Secretary
Colleen H. Sullins, Director
.0F
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings, Inc. County: Cleveland
Permit No.: WQ0011038 (non 503) Issuance Date: May 3, 2006
Last Amended Date: N/A Expiration Date: April 28, 2011
SOC Issuance Date (if applicable): N/A Ext. Expiration Date: April 28. 2014
Permittee Contact: Pem Carter Telephone No.: 704/480-4700
ORC Name: Roy L. Whittaker Telephone No.: 336/766=032-8 -ext-115
ORC Cert.#: 13283 B/UC:' Brent Collins #27651
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
CNA Holdings, Inc, is permitted to apply 570 dry tons of sludge per year from the CNA
Holdings, Inc. wwtp (permit # NC 0004952). Sludge storage is estimated to be 1095 days. This
may be longer as wwtp flows (permitted for 0.8 MGD) are currently averaging 108,000 gallons
per day. EMA Resources is the current land application contractor. There are no plans for any
land application activity for 2010. A review of last year's land application annual report reflects
compliance.
Is a follow-up inspection necessary _yes X no
Inspector(s) Name(s)/Title(s) Ellen Huffman./ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 08-17-2010

WQ0011038 CNA Holdings, Inc. pg 2
August 17, 2010
Y- Yes N- No N/A -not applicable N/E-Not evaluated
Type of Residual
Land Application (class B, non-503)
Record Keepin Y/N
Y Copy of current permit available at residual generating site
N/A Current metals and nutrient analysis (quarterly)
N/A TCLP analysis (annually), SSFA (Standard Soil Fertility Analysis)
N/A Nutrient and metals loading calculations (to determine most limiting parameter) YTD
N/A Hauling records (# gal and/or ton hauled during calendar year to date)
N/A Field loading records, Y Field site maps and information
N/A Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Comment: There is no land application planned for 2010 therefore, no testing required.
Pathogen & Vector Attraction Reduction Records N/A
Pathogen and vector attraction reduction is not required by this permit.
Treatment
X Aerobic digestion Anaerobic digestion
Transport
Spill control plan in transport vehicle? N/E
Does transport vehicle appear to be maintained? N/E
Operation & Maintenance records
Condition of land application equipment on site N/E
Storage
Number of days/weeks/months of storage 1095 days (estimated)
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
Sampling
Describe Sampling: Metals and nutrient sampling are taken as grab samples by the land application
contractor from the storage lagoons prior to land application. Sampling is in accordance with the
permit and EPA standards.
Is sampling adequate? Yes Is sampling representative? Yes

WQ0011038 CNA Holdings, Inc.
August 17, 2010
Application Field N/E
Permit on site during application
Buffers adequate
Documented exceedances of PAN limits
Signs of runoff / ponding
pg 3
Spill plan on site
Cover crop specified in permit
Site condition adequate
Rain Gauge on site during application
Are there any limiting slopes on fields?
(10 % for surface application. 18% for subsurface application)
Monitoring well(s) Y/N: N
If yes, location of well(s)
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Odors present no
Vectors present no
Describe any nuisance conditions and any corrective actions needed.
None noted

Beverly Eaves Purdue, Governor
Dee Freeman, Secretary
North Carolina Department of Environment and Natural Resources`
t
Coleen H. Sullins, Director �\
Division of Water Quality
AQUIFER PROTECTION SECTION
February 16, 2009
Mr. John Groves, Plant Manager
CNA Holdings, Inc.
2525 Blacksburg Rd.
Grover, North Carolina 28073
Subject: Land Application Inspection
Permit No. WQ0011038 (non-503)
Cleveland County
Dear Mr. Groves:
Enclosed is the inspection report for the inspection of the non -discharge Land
Application that was conducted on February 11, 2009. The report indicates compliance with the
subject permit, including lab data, and record keeping.
The attached report should be self-explanatory, however, if you have any questions,
please contact me at [phone].
Si cerely,
&"--zrv"�
4
Ellen Huffman
Environmental Specialist
Cc: EMA Resources
Ed Hardee, LAU Residuals Program Coordinator
MRO files
Division of Water Quality / Aquifer Protection Section / Mooresville Regional Office Phone: [phone] Fax: [phone] NoonAhCarolina
610 East Center Avenue, Suite 301, Mooresville, NC 28115 Customer Service 1-877-623-6748 Internet: www.ncwate[guality.org d►a mIr"Ib,

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Beverly H. Purdue, Governor
Dee freeman, Secretary
Colleen H. Sullins, Director
e��
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings, Inc.
PermitNo.: W00011038 (non 503)
Last Amended Date: N/A
SOC Issuance Date (if applicable): N/A
Permittee Contact: Pem Carter
ORC Name: Roy L. Whittaker
ORC Cert.#: 13283
Reason for Inspection
County: Cleveland
Issuance Date: May 3, 2006
Expiration Date: April 28. 2011
Expiration Date: N/A
Telephone No.: 704/480-4700
Telephone No.: 336/766-0328 ext 115
B/U ORC: Brent Collins #27651
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the CNA
Holdings, Inc. wwtp (permit # NC 0004952). Sludge storage is estimated to be 1095 days.
CNA has three treatment ponds in series and one storage pond where sludge is stored for land
application. EMA Resources is the current land application contractor. The sludge truck
loading area at the storage facility appeared neat and clean. There was no land application
activity at the time of this inspection. A review of last years land application records including
analysis, hauling, and loading, reflect compliance. Future sludge cleaning from pond A was
discussed.
Is a follow-up inspection necessary _yes X no
Inspector(s) Names)/Title(s) Ellen Huffman/ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 02 112009

WQ0011038 CNA Holdings, Inc. pg 2
February 11, 2009
Y- Yes N- No N/A -not applicable N/E-Not evaluated
Type of Residual
Land Application (class B)
Record Keeping Y/il
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (quarterly)
Y TCLP analysis (annually), SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y Hauling records (# gal and/or ton hauled during calendar year to date)
Y Field loading records, Y Field site maps and information
N/A Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Comment: Pathogen and vector attraction reduction is not required by this permit.
Pathogen & Vector Attraction Reduction Records N/A
Treatment
X Aerobic digestion Anaerobic digestion
Alkaline Stabilization Lime other -describe
Transport
Spill control plan in transport vehicle? N/E
Does transport vehicle appear to be maintained? N/E
Operation & Maintenance records
Condition of land application equipment on site N/E
Storage
Number of days/weeks/months of storage 1095 days(estimated)
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
Sampling
Describe Sampling: Metals and nutrient sampling are taken as grab samples by the land application
contractor from the storage laszoons prior to land apmlication. Samnlina is in accordance with the
permit and EPA standards.
Is sampling adequate? Yes Is sampling representative? Yes

WQ0011038 CNA Holdings, Inc.
february 11, 2009
Application Field N/E
Field identification
Permit on site during application
Buffers adequate
_ Documented exceedances of PAN limits
Signs of runoff / ponding
pg 3
_ Spill plan on site
Cover crop specified in permit
Site condition adequate
Rain Gauge on site during application
Are there any limiting slopes on fields? No
10 % for surface application. 18% for subsurface application
Monitoring wells) Y/N: N
If yes, location of well(s)
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Odors present no
Vectors present no
Describe any nuisance conditions and any corrective actions needed.
None noted

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
Aquifer Protection Section
March 23, 2007
Mr. Darrell Fisher, Interim Plant Manager
CNA Holdings, Inc. TYCONA Plant
P.O. Box 87, Hwy 198
Shelby, North Carolina 28152
Subject: Land Application Inspection
Permit No. WQ0011038
Cleveland County
Dear Mr. Fisher:
Enclosed is the land application inspection report for the inspection conducted on February 28, 2007.
Records indicate that CNA has not land applied since 2004. It was noted at the time of inspection that
the storage lagoons are all full and CNA will have to land apply soon, in order to comply with the required
freeboard minimum of 2 feet (24 inches) in each sludge lagoon.
The report should be self-explanatory; however, if you have any questions, please contact me at 704-
235-2186.
Attachment
cc: Central Files
WQ APS, Mooresville Regional Office
Pem Carter, Environmental Engineer, CNA TYCONA
6ENR
Customer Service
1 877-623-6748
Sincerely,
Ellen Huffman,
Environmental Specialist
Mooresville Region
Mooresville Regional Office, 919 North Main Street, Mooresville, NC 28115 PHONE [phone]
FAX [phone]

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
Sherri Evans -Stanton, Acting Secretary
Kerr T. Stevens, Director
Aliv
W •
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings, Inc.
Permit No.: WQ0011038
Last Amended Date: N/A
SOC Issuance Date(if applicable): N/A
Permittee Contact:
Pem Carter
ORC Name: Jean Creech
ORC Cert.#: 987974
Reason for Inspection
County:
Cleveland
Issuance Date: May 3, 2006
Expiration Date: April 28, 2011
Expiration Date: N/A
Telephone No.: 704/480-4700
Telephone No.: 704/752-8673
B/U ORC: not assigned
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the facility's
wwtp (permit # NC 0004952). Sludge storage is estimated to be 1095 days. Records indicate that
CNA has not land applied since 2004. It was noted at the time of inspection that the storage
lagoons are all full and CNA will have to land apply soon, in order to comply with the required
freeboard minimum of 2 feet (24 inches) in each sludge lagoon.
SYNAGRO is the current land application contractor.
CNA should call the regional office when they are ready to land apply this year.
Is a follow-up inspection necessary X yes no
Inspector(s) Name(s)/Title(s) Ellen Huffinan/ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 02/28/07

Q0011038 CNA Holdings, Inc. 02/28/07
Tyne of Residual
X Land Application (class B) Distribution and Marketing (class A)
Pg 2
Record Keeping Y/N Not evaluated.
Y Copy of current permit available at residual generating site
N/E Current metals and nutrient analysis (see permit for frequency)
N/E TCLP analysis, SSFA (Standard Soil Fertility Analysis)
N/E Nutrient and metals loading calculations (to determine most limiting parameter) YTD
N/E Hauling records (# gal and/or ton hauled during calendar year to date)
N/E Field loading records, Field site maps and information
N/E Records of lime purchased
N/E Pathogen & Vector Attraction Reduction
Comments: The permittee has of land applied since 2004. Vector attraction reduction is not
required by this permit. There has been no land application for 2002 or 2003.
Treatment
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime other -describe
Transport Not evaluated
Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Comment: A spill control plan was placed in each truck before the inspection was over.
Operation & Maintenance records
Condition of land application equipment on site N/E
Storage
Number of days/weeks/months of storage 1095 days
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
NCAC 2T .1109(c)(1)(G)states: If liquid residuals are to be placed in the unit, a
decanting system and freeboard marker shall be required.
Sampling
Describe Sampling: Metals and nutrient sampling are taken as grab by SYNAGRO from the
storage lagoons prior to land application. Sampling is in accordance with the permit and EPA
standards.
Is sampling adequate? Yes Is sampling representative? Yes

WQ0011038 CNA Holdings, Inc.
Application Field(s)
Field identification
Permit on site during application
Buffers adequate
Doc. PAN limits
Signs of runoff / ponding
02/28/07
Not evaluated.
Are there any limiting slopes on fields?
10 % for surface, 18% for subsurface application
Monitoring wells) Y/N: N/A
If yes, location of well(s)
Spill plan on site
Cover crop specified in permit
Site condition adequate
Rain Gauge on site during application
pg 3
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Odors present
Vectors present
Describe any nuisance conditions and any corrective actions needed.
None noted

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date of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross, Secretary
Coleen H. Sullins, Director
A lf'?WIA
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings, Inc.
Permit No.: W00011038 (non 503)
Last Amended Date: N/A
SOC Issuance Date (if applicable): .N/A
Permittee Contact: Pem Carter
ORC Name: Roy L. Whittaker
ORC Cert.#: 13283
Reason for Inspection
County: Cleveland
Issuance Date:
May 3, 2006
Expiration Date:
April 28, 2011
Expiration Date:
N/A
Telephone No.:
704/480-4700
Telephone No.:
336/766-0328 ext 115
B/U ORC: Brent Collins #27651
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other '1
Inspection Summary: (additional comments may be included on attached pages)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the CNA
Holdings, Inc. wwtp (permit # NC 0004952). Sludge storage is estimated to be 1095 days.
The sludge truck loading area at the storage facility appeared neat and clean. EMA Resources is
the current land application contractor. Application was in progress during this inspection. A
field inspection at the application site reflected compliance. It was noted that metals sampling in
May reported elevated lead, exceeding compliance limits. Extensive re -testing in June from four
areas of the storage lagoon could not duplicate the high lead number previously reported and
reflects compliance. A review of previous metal analyses (from annual reports) shows that there
is no history of elevated lead.
Is a follow-up inspection necessary __yes X no
Inspector(s) Name(s)/Title(s) Ellen Huffman/ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 07 012008

wQ0011038 CNA Holdings, Inc.
Y- Yes N- No N/A -not applicable N/E-Not evaluated
Type of Residual
Land Application (class B)
pg 2
Record Keeping Y/N
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (quarterly)
N/E TCLP analysis (annually), SSFA (Standard Soil Fertility Analysis)
N/E Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y Hauling records (# gal and/or ton hauled during calendar year to date)
N/E Field loading records, Y Field site maps and information
N/A Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Comment: Pathogen and vector attraction reduction is not required by this permit.
Pathogen & Vector Attraction Reduction Records N/A
Treatment
X Aerobic digestion Anaerobic digestion
Alkaline Stabilization Lime other -describe
Transport
Spill control plan in transport vehicle? Y
Does transport vehicle appear to be maintained? Y
Comment: None
Operation & Maintenance records
Condition of land application equipment on site Very good
Storage
Number of days/weeks/months of storage 1095 days (estimated)
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
Sampling
Describe Sampling: Metals and nutrient sampling are taken as grab samples by the land application
contractor from the storage lagoons Drior to land application. Sampling is in accordance with the
permit and EPA standards.
Is sampling adequate? Yes Is sampling representative? Yes

w0011038 CNA Holdings, Inc.
Application Field
Field identification
Y Permit on site during application
Y Buffers adequate
N Documented exceedances of PAN limits
N Signs of runoff / ponding
pg 3
Y Spill plan on site
Y Cover crop specified in permit
Y Site condition adequate
N Rain Gauge on site during application
Are there any limiting slopes on fields? No
10 % for surface application. 18% for subsurface application
Monitoring wells) Y/N: N
If yes, location of well(s)
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Odors present no
Vectors present no
Describe any nuisance conditions and any corrective actions needed.
None noted

APR 2 7 Ti cona
Certified Mail 7005 1160 0004 9234 7654
Return Receipt to PEM Carter NC DENR MRO
DWQ - Aquifer Protection icona
April 22 2009 2525 Blacksburg Road
P Grover, NC 28073-9641
Carolina Star Worksite
ISO 9001, lSO/TS 16949,
PEMC09:16e ISO 17025,and ISO 14001
NC Department of Environmental and Natural Resources
Aquifer Protection Division- Mooresville
610 East Center, Suite 301
Mooresville, NC. 28115
Dear Ms. Huffman,
Subject: Land Application Permit No. WQ0011038
CNA Holdings, Inc,; Ticona Polymers, Shelby Plant
2525 Blacksburg Road, Grover, NC 28073.
This is to inform you that the following communications pertaining to the above Water Quality
Permit should be directed as follows:
Facility/Technical Contact Authorized / Invoice Contact
PEM Carter, Env. Eng. Lanny Duvall, Site Director
704-480-4900 704-480-4980
pem.carter(cb-ticona.com Ian ny.duvall(a-)celanese.com
Please correct your records, and communicate to others in need of this information. We request
the,removal. of.all previous contacts: you may have listed for our facility,. for they are. no, longer
employed at this facility. Thank you for prompt attention to this request and if you should have
any further questions, please feel free to contact me at [phone], or via email at
pem.carterO-ticona.com .
In rely,
PEM Carter
Sr. Environmental Engineer
Ticona
Celanese
Ticona
A business of Celanese

Michael F. Easley, Governor
William G. Ross Jr., Secretary
I L E rth Carolina Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
AQUIFER PROTECTION SECTION
July 18, 2008
Mr. John Groves, Plant Manager
CNA Holdings, Inc.
P.O. Box 87, Hwy 198
Shelby, North Carolina 28152
Subject: Land Application Inspection
Permit No. WQ0011038 (non-503)
Cleveland County
Dear Mr. Sando:
Enclosed is the inspection report for the inspection of the non -discharge Land
Application that was conducted on July 1, 2008. The report indicates compliance with the
subject permit, including lab data, record keeping, and field conditions.
The attached report should be self-explanatory, however, if you have any questions,
please contact me at [phone].
Sincerely,
Ellen Huffman
Environmental Specialist
Cc: EMA Resources
Ed Hardee, LAU Residuals Program Coordinator
MRO files
Division of Water Quality / Aquifer Protection Section / Mooresville Regional Office Phone: [phone] Fax: [phone] NorthCarolina
610 East Center Avenue, Suite 301, Mooresville, NC 28115 Internet: www.ncwateroualitv.ora NatuCallty

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross, Secretary
Coleen H. Sullins, Director
NON -DISCHARGE COMPLIANCE INSPECTION
Permittee: CNA Holdings, Inc.
Permit No.: WQ0011038 (non 503)
Last Amended Date: N/A
SOC Issuance Date (if applicable): N/A
Permittee Contact: Pem Carter
ORC Name: Roy L. Whittaker
ORC Cert.#: 13283
Reason for Inspection
County: Cleveland
Issuance Date: May 3, 2006
Expiration Date: April 28, 2011
Expiration Date: N/A
Telephone No.: 704/480-4700
Telephone No.: 336/766-0328 ext l l5
B/U ORC: Brent Collins #27651
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the CNA
Holdings, Inc. wwtp (permit # NC 0004952). Sludge storage is estimated to be 1095 days.
The sludge truck loading area at the storage facility appeared neat and clean. EMA Resources is
the current land application contractor. Application was in progress during this inspection. A
field inspection at the application site reflected compliance. It was noted that metals sampling in
May reported elevated lead, exceeding compliance limits. Extensive re -testing in June from four
areas of the storage lagoon could not duplicate the high lead number previously reported and
reflects compliance. A review of previous metal analyses (from annual reports) shows that there
is no history of elevated lead.
Is a follow-up inspection necessary des X no
Inspector(s) Name(s)/Title(s) Ellen Huffman/ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 07 012008

rQ0011038 CNA Holdings, Inc.
Y- Yes N- No N/A -not applicable N/E-Not evaluated
Type of Residual
Land Application (class B)
Pg 2
Record Keeping Y/N
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (quarterly)
N/E TCLP analysis (annually), SSFA (Standard Soil Fertility Analysis)
N/E Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y Hauling records (# gal and/or ton hauled during calendar year to date)
N/E Field loading records, Y Field site maps and information
N/A Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Comment: Pathogen and vector attraction reduction is not required by this permit.
Pathogen & Vector Attraction Reduction Records N/A
Treatment
X Aerobic digestion Anaerobic digestion
Alkaline Stabilization Lime other -describe
Transport
Spill control plan in transport vehicle? Y
Does transport vehicle appear to be maintained? Y
Comment: None
Operation & Maintenance records
Condition of land application equipment on site Very good
Storage
Number of days/weeks/months of storage 1095 days(estimated)
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
Sampling
Describe Sampling: Metals and nutrient sampling are taken as grab samples by the land application
contractor from the storage lagoons prior to land application. Sampling is in accordance with the
permit and EPA standards.
Is sampling adequate? Yes Is sampling representative? Yes

WQ0011038 CNA Holdings, Inc.
Application Field
Field identification
PK -'
Y Permit on site during application Y Spill plan on site
Y Buffers adequate Y Cover crop specified in permit
N Documented exceedances of PAN limits Y Site condition adequate
N Signs of runoff / ponding N Rain Gauge on site during application
Are there any limiting slopes on fields? No
10 % for surface application. 18% for subsurface application
Monitoring wells) Y/N: N
If yes, location of well(s)
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Odors present no
Vectors present no
Describe any nuisance conditions and any corrective actions needed.
None noted

Report Number:
R08162-8005
Account Number:
46245
To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43182
SAMPLE ID: ZSOUT�i--L AGO -ON MIXED=CO 1
A&L EASTERN LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237
[phone] • Fax No. [phone]
FOR: TICONA-SHELBY
NC CERT #257
REPORT OF ANALYSIS
copy: ROY WHITAKER
DATE SAMPLED:E6/5/2Q08°°�2'030="
DATE RECEIVED:6/_1= D8 �_QQ0
DATE REPORTED: 6/13/2008 PAGE: 1
Solids, Total (As is)
3.45
34500
100
KM
06/10/08
16:00
SM 2540G
Nitrogen, Total Kjeldahl
4.29
42900
10
JM
06/11/08
16:00
EPA 351.3
Phosphorus
1.14
11400
100
KM
06/11/08
16:00
SW 846-3051/6010B
Potassium
0.28
2800
100
KM
06/11/08
16:00
SW 846-3051/601013
Sulfur
1.10
11000
100
KM
06/11/08
16:00
SW 846-3051/6010B
Calcium
1.24
12400
100
KM
06/11/08
16:00
SW 846-3051/601013
Magnesium
0.36
3600
100
KM
06/11/08
16:00
SW 846-3051/601013
Sodium
0.49
4900
100
KM
06/11/08
16:00
SW 846-3051/601013
Iron
23500
1
KM
06/11/08
16:00
SW 846-3051/601013
Aluminum
27300
10
KM
06/11/08
16:00
SW 846-3051/6010B
Manganese
1010
1
KM
06/11/08
16:00
SW 846-3051/601013
Copper
330
1
KM
06/11/08
15:00
SW 846-3051/601013
Zinc
451
1
KM
06/11/08
16:00
SW 846-3051/601013
Nitrogen, Ammonia (as N)
0.67
6700
10
JM
06/11/08
14:00
EPA 350.2
Nitrogen, Organic (N)
3.62
36200
100
DCH
CALCULATION
Nitrogen, NO3+NO2
58
1
KS
06/11/08
15:00
SM 4500-NO3F
Cadmium
1.2
1
KM
06/11/08
16:00
SW 846-3051/601013
Chromium
316
5
KM
06/11/08
16:00
SW 846-3051/601013
All values are on a dry weight basis except as noted. *Detection Limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
PA111 r' u ('W11

Report Number:
R08162-8005 A&L EASTERN LABORATORIES, INC.
Account Number: 7621 Whitepine Road • Richmond, Virginia 23237 U
46245 [phone] - Fax No. [phone]
TO: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43182
SAMPLE ID: SO, ` TH�LAGt70N�MiXEa: CO.M
FOR: TICONA-SHELBY
NC CERT #257
REPORT OF ANALYSIS
copy: ROY WHITAKER
DATE SAMPLED: 6/5/2008 2030
DATE RECEIVED: 6/10/2008 1000
DATE REPORTED: 6/13/2008 PAGE: 2
Nickel
51
5
KM
06/11/08
16:00
SW 846-3051/601013
add
'9x
5
KM
06/11/08
16:00
SW 846-3051/601OB
Arsenic
15.4
1.0
KM
06/11/08
15:00
SW 846-601 OB
Mercury
1.1
0.4
KM
06/13/08
15:00
SW 846-7471A
Selenium
1.0
1.0
KM
06/11/08
15:00
SW 846-601OB
pH (Std. Unit, As is)
6.98
0.01
RD
06/11/08
12:30
SW 846-9045C
Solids, Volatile(Organic Matter)
58.29 582900
100
KS
06/11/08
16:00
SM 2540G
Molybdenum
22
5
KM
06/11/08
16:00
SW 846-3051/601013
All values are on a dry weight basis except as noted. *Detection Limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
. PAI 11

Report Number:
R08162-8007
Account Number:
46245
To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43184
SAMPLE ID: SOUTH LAGOON 9-E-ARE-A-
Solids, Total (As is)
'Lead-J
3.67
A&L EASTERN LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237
[phone] • Fax No. [phone]
FOR: TICONA-SHELBY
NC CERT #257
REPORT
ESULT DETECTION LIMIT ANALYSIS
mg/kg) (mg/kg*) ANALYST DATE
36700 100 KM 1. 1:
0. O:
copy: ROY WHITAKER
DATE SAMPLEp.-`/5/2O08wOJO
DATE RECEIVED: 6/10/2008 1000
DATE REPORTED: 6/13/2008 PAGE: 1
16:00
16:00
SM 2540G
SW 846-3051/601OB
All values are on a dry weight basis except as noted. *Detection Limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
vni 11 rr. H rrui i

Report Number:
R08162-8006 A&L EASTERN LABORATORIES INC.
Account Number: 7621 Whitepine Road • Richmond, Virginia 23237 At,
46245 [phone] • Fax No. [phone]
TO: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43183
SAMPLE ID: SOUTH LAGOONIANFLUENT A"R-EA-1
Solids, Total (As is)
Lead
18.11
FOR: TICONA-SHELBY
NC CERT #257
REPORT OF ANALYSIS
RESULT DETECTION LIMIT ANALYSIS
(mg/kg) (mg/kg`) ANALYST DATE
00 100 KM 0. 0:
qqH3 5 KM 0. 0:
copy: ROY WHITAKER
DATE SAMPLED: 6/5/2008 2040
DATE RECEIVED: 6/ ��.8�r1 OIYO
DATE REPORTED: 6/13/2008 PAGE: 1
16:00 SM 2540G
16:00 SW 846-3051/601013
All values are on a dry weight basis except as noted. *Detection Limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part nor may any reference be made
rA
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.-
Pal 11 r• N r.Hi

Report Number:
R08162-8008
Account Number:
46245
TO: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43185
SAMPLE ID: SOUTI�=LA-QOON�EFFEVENT
Solids, Total (As is)
CLea`"'�d-
3.79
A&L EASTERN LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237
[phone] • Fax No. [phone]
FOR: TICONA-SHELBY
NC CERT#257
REPORT OF ANALYSIS
ESULT DETECTIONLIMIT ANALYSIS
mg/kg) (mg/kg*) ANALYST DATE
5 KM 0. 1
atL
copy: ROY WHITAKER
DATE SAMPLED: 6/5/2008 2100
DATE RECEIVED: 6/10/2008 1000
DATE REPORTED: 6/13/2008 PAGE: 1
16:00 SM 2540G
16:00 SW 846-3051/601OB
All values are on a dry weight basis except as noted. *Detection Limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
PAIII r` W ra-11I

"!M08i49-W8003
Account Number:
46245
To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43004
SAMPLE ID LtJ!DGEzI_AGOO-N
A&L EASTERN LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237
[phone] • Fax No. [phone]
FOR: TICONA-SHELBY
NC CERT #257
REPORT OF ANALYSIS
REPORT PRINTED 6/3/2008
copy: ROY WHITAKER
DATE SAMPLED T/-2�00 5-,J 230
DATE RECEIVED:2$008 TOO.O�
DATE REPORTED: 6/2/2008 PAGE: 1
Solids, Total (As is)
6.23
62300
100
KM
05/28/08
16:00
SM 2540G
Nitrogen, Total Kjeldahl
2.18
21800
10
JM
05/29/08
16:00
EPA 351.3
Phosphorus
0.64
6400
100
KM
05/29/08
16:00
SW 846-3051/601013
Potassium
0.27
2700
100
KM
05/29/08
16:00
SW 846-3051/601013
Sulfur
0.64
6400
100
KM
05/29/08
16:00
SW 846-3051/601OB
Calcium
2.13
21300
100
KM
05/29/08
16:00
SW 846-3051/601013
Magnesium
1.21
12100
100
KM
05/29/08
16:00
SW 846-3051/601OB
Sodium
0.35
3500
100
KM
05/29/08
16:00
SW 846-3051/601013
Iron
16500
1
KM
05/29/08
16:00
SW 846-3051/601013
Aluminum
16100
10
KM
05/29/08
16:00
SW 846-3051/601013
Manganese
482
1
KM
05/29/08
16:00
SW 846-3051/601013
Copper
199
1
KM
05/29/08
15:00
SW 846-3051/601013
Zinc
280
1
KM
05/29/08
16:00
SW 846-3051/601013
Nitrogen, Ammonia (as N)
0.30
3000
10
JM
05/29/08
14:00
EPA 350.2
Nitrogen, Organic (N)
1.88
18800
100
DCH
CALCULATION
Nitrogen, NO3+NO2
< 1
1
KS
05/30/08
15:00
SM 4500-NO3F
Cadmium
< 1
1
KM
05/29/08
16:00
SW 846-3051/601013
Chromium
316
5
KM
05/29/08
16:00
SW 846-3051/601OB
All values are on a dry weight basis except as noted. *Detection
Limit on all
N series is on
a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
—
�-
PAIII r. W r-H1I

"1490W-8UU3
Account Number:
46245
To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43004
SAMPLE ID: SLUDGE LAGOON
A&L EASTERN LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237
[phone] • Fax No. [phone]
FOR: TICONA-SHELBY
NC CERT #257
REPORT OF ANALYSIS
REPORT PRINTED 6/3/2008
copy: ROY WHITAKER
DATE SAMPLED: 5/27/2008 1230
DATE RECEIVED: 5/28/2008 1000
DATE REPORTED: 6/2/2008 PAGE: 2
Nickel
81
5
KM
05/29/08
16:00
SW 846-3051/601OB
L
1410
5
KM
06/02/08
16:00
SW 846-3051/601OB
Arsenic
10.3
1.0
KM
05/29/08
15:00
SW 846-601013
Mercury
0.6
0.4
KM
05/30/08
15:00
SW 846-7471A
Selenium
1.3
1.0
KM
05/29/08
15:00
SW 846-601013
pH (Std. Unit, As is)
6.79
0.01
RD
0.5/29/08
12:30
SW 846-9045C
Solids, Volatile(Organic Matter)
63.31 633100
100
JM
05/29/08
16:00
SM 2540G
Molybdenum
15
5
KM
05/29/08
16:00
SW 846-3051/601013
All values are on a dry weight basis except as noted. *Detection Limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. N,
pni n r•. N r.Ni i

Repj,4L ,ber:
R08149-8004
Account Number:
46245
TO: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43005
SAMPLE ID: OL18f NG"PONE),A�
A&L EASTERN LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237
[phone] • Fax No. [phone]
FOR: TICONA-SHELBY
NC CERT #257
REPORT OF ANALYSIS
copy: ROY WHITAKER
DATE SAMPLED: 5/27/2008 1330 -
DATE RECEIVED: 5/28/2008 1000
DATE REPORTED: 6/2/2008 PAGE: 1
Solids, Total (As is)
2.09
20900
100
KM
05/28/08
16:00
SM 2540G
Nitrogen, Total Kjeldahl
3.06
30600
10
JM
05/29/08
16:00
EPA 351.3
Phosphorus
0.45
4500
100
KM
05/29/08
16:00
SW 846-3051/601 OB
Potassium
0.18
1800
100
KM
05/29/08
16:00
SW 846-3051/601013
Sulfur
0.68
6800
100
KM
05/29/08
16:00
SW 846-3051/601 OB
Calcium
0.53
5300
100
KM
05/29/08
16:00
SW 846-3051/601OB
Magnesium
0.35
3500
100
KM
05/29/08
16:00
SW 846-3051/601OB
Sodium
0.56
5600
100
KM
05/29/08
16:00
SW 846-3051/601013
Iron
18400
1
KM
05/29/08
16:00
SW 846-3051/601013
Aluminum
17400
10
KM
05/29/08
16:00
SW 846-3051/601013
Manganese
255
1
KM
05/29/08
16:00
SW 846-3051 /6010B
Copper
182
1
KM
05/29/08
15:00
SW 846-3051 /601 OB
Zinc
222
1
KM
05/29/08
16:00
SW 846-3051 /601 OB
Nitrogen, Ammonia (as N)
0.43
4300
10
JM
05/29/08
14:00
EPA 350.2
Nitrogen, Organic (N)
2.63
26300
100
DCH
CALCULATION
Nitrogen, NO3+NO2
< 1
1
KS
05/30/08
15:00
SM 4500-NO3F
Cadmium
< 1
1
KM
05/29/08
16:00
SW 846-3051/601OB
Chromium
246
5
KM
05/29/08
16:00
SW 846-3051/601OB
All values are on a dry weight basis except as noted. *Detection Limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization."'
PAI11 r. W rH1I

Rest ember:
R08149-8004
Account Number:
46245
To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE, NC 27028
LAB NUMBER: 43005
SAMPLE ID: POLISHING POND A
A&L EASTERN LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237
[phone] • Fax No. [phone]
FOR: TICONA-SHELBY
NC CERT #257
REPORT OF ANALYSIS
copy: ROY WHITAKER
DATE SAMPLED: 5/27/2008 1330
DATE RECEIVED: 5/28/2008 1000
DATE REPORTED: 6/2/2008 PAGE: 2
Nickel
85
5
KM
05/29/08
16:00
SW 846-3051/601013
J%Lre—aqdlff
AKRAW5
KM
05/29/08
16:00
SW 846-3051/601013
Arsenic
9.7
1.0
KM
05/29/08
15:00
SW 846-601013
Mercury
< 0.4
0.4
KM
05/30/08
15:00
SW 846-7471A
Selenium
< 1.0
1.0
KM
05/29/08
15:00
SW 846-601013
pH (Std. Unit, As is)
6.53
0.01
RD
05/29/08
12:30
SW 846-9045C
.Solids, Volatile(Organic Matter)
44.91 449100
100
JM
05/29/08
16:00
SM 2540G
Molybdenum
20
5
KM
05/29/08
16:00
SW 846-3051/601013
All values are on a dry weight basis except as noted. *Detection Limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
PAI 11

�F wATF9
�v
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Mr. Ed McKinley, Plant Manager
CNA Holdings, Inc. TYCONA Plant
2525 Blacksburg Rd.
Grover, North Carolina 28073-9641
Dear Mr. Fisher:
Alan W. Klimek, P.E. Director
Division of Water Quality
Aquifer Protection Section
April 04, 2007
Subject: Notice of Deficiency
Land Application Inspection
Permit No. WQ0011038
Cleveland County
Enclosed is the land application inspection report for the inspection conducted on February 28, 2007.
Records indicate that CNA has not land applied since 2004. It was noted at the time of inspection that
the storage lagoons are all full and freeboard is less than 24 inches. CNA will have to land apply soon, in order
to comply with the required freeboard minimum of 2 feet (24 inches) in each sludge lagoon. A follow-up
inspection of this facility is tentatively scheduled for July 19, 2007
The report should be self-explanatory; however, if you have any questions, please contact me at 704-
235-2186.
Sincerely,
r
Ellen Huffman,
Environmental Speclist
Mooresville Region
Attachment
cc: Central Files
WQ APS, Mooresville Regional Office
Pem Carter, Environmental Engineer, CNA TYCONA
N MR
Customer Service Mooresville, Regional Office, 919 'North Main Street, Mooresville, NC 28115 PHONE [phone]
1 877-623-6748 FAX [phone]

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
Sherri Evans -Stanton, Acting Secretary
Kerr T. Stevens, Director
NCDIENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings, Inc.
PermitNo.: W00011038
Last Amended Date: N/A
SOC Issuance Date(if applicable): N/A
Permittee Contact: Pem Carter
ORC Name: Jean Creech
ORC Cert.#: 987974
Reason for Inspection
County: Cleveland
Issuance Date:
May 3, 2006
Expiration Date:
April 28, 2011
Expiration Date:
N/A
Telephone No.:
704/480-4700
Telephone No.:
704/752-8673
B/U ORC: not assigned
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summarv: (additional comments may be included on attached pages)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the facility's
wwtp (permit # NC 0004952). Sludge storage is estimated to be 1095 days. Records indicate that
CNA has not land applied since 2004. It was noted at the time of inspection that the storage
lagoons are all full. Lagoon freeboard is < 24 inches. CNA will have to land apply soon, in order
to comply with the required freeboard minimum of 2 feet (24 inches) in each sludge lagoon.
SYNAGRO is the current land application contractor.
CNA should call the regional office when they are ready to land apply this year.
A, followup inspection is scheduled for July 19, 2007.
Is a follow-up inspection necessary X yes no
Inspector(s)Names)/Title(s) Ellen Huffinan/ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 02/28/07

o
i'
WQ0011038 CNA Holdings, Inc.
02/28/07
Pg 2
Tvpe of Residual
X Land Application (class B)
Distribution and Marketing (class A)
Record Keeping Y/N Not evaluated.
Y Copy of current permit available at residual generating site
N/E Current metals and nutrient analysis (see permit for frequency)
N/E TCLP analysis, SSFA (Standard Soil Fertility Analysis)
N/E Nutrient and metals loading calculations (to determine most limiting parameter) YTD
N/E Hauling records (# gal and/or ton hauled during calendar year to date)
N/E Field loading records, Field site maps and information
N/E Records of lime purchased
N/E Pathogen & Vector Attraction Reduction
Comments: The permittee has of land applied since 2004. Vector attraction reduction is not
required by this permit. There has been no land application for 2002 or 2003.
Treatment
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion'
Anaerobic digestion Drying beds (may not meet 503's)
.Alkaline Stabilization Lime other -describe
Transport Not evaluated
Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Comment: A spill control plan was placed in each truck before the inspection was over.
Operation & Maintenance records
Condition of land application equipment on site N/E
Storage
Number of days/weeks/months of storage 1095 days
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
NCAC 2T .1109(c)(1)(G)states: If liquid residuals are to be placed in the unit, a
decanting system and freeboard marker shall be required.
Sampling
Describe Sampling: Metals and nutrient sampling are taken as grab samples by SYNAGRO from the
storage lagoons prior to land application. Sampling is in accordance with the permit and EPA
standards.
Is sampling adequate? Yes Is sampling representative? Yes

WQ0011038 CNA Holdings, Inc. 02/28/07
Application Field(s)
Field identification
Permit on site during application
Buffers adequate
Doc. PAN limits
Signs of runoff / ponding
Not evaluated.
Are there any limiting slopes on fields?
10 % for surface, 18% for subsurface application
Monitoring well(s) Y/N: N/A
If yes, location of well(s)
Spill plan on site
Cover crop specified in permit
Site condition adequate
Rain Gauge on site during application
pg 3
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Odors present
Vectors present
Describe any nuisance conditions and any corrective actions needed.

�OF WAtF
Michael F. Easley, Governor
0G William G. Ross Jr., Secretary
r North Carolina Department of Environment and Natural Resources
O Y Alan W. Klimek, P.E. Director
Division of Water Quality
Mr. Darrell Fish erjpbefim Ploht Manager
CNA Holdings K. TYCONA Plant
P.O. Box,, , Hwy 198
Shelbv orth Carolina 28152
,2— &a4-'
.�„�• ov � �P� 9 3_g a ��
Dear Mr. Fisher:
Aquifer Protection Section
March 23, 2007
Subject: Land Application Inspection
Permit No. WQ0011038
Cleveland County
Enclosed is the land application inspection report for the inspection conducted on February 28, 2007.
Records indicate that CNA has not land applied since 2004. It was noted at the time of inspection that
the storage lagoons are all full and CNA will have to land apply soon, in order to comply with the required
freeboard minimum of 2 feet (24 inches) in each sludge lagoon.
The report should be self-explanatory; however, if you have any questions, please contact me at 704-
235-2186.
Attachment
cc: Central Files
WQ APS, Mooresville Regional Office
Pem Carter, Environmental Engineer, CNA TYCONA
VAM
NCID NR
Customer Service
1 877-623-6748
Sincerely,
Ellen Huffman,
Environmental Specialist
Mooresville Region
Mooresville Regional Office, 919 North Main Street, Mooresville, NC 28115 PHONE [phone]
FAX [phone]

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
Sherri Evans -Stanton, Acting Secretary
Kerr T. Stevens, Director
0)
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings, Inc.
Permit No.: WQ0011038
Last Amended Date: N/A
SOC Issuance Date(if applicable): N/A
Permittee Contact: Perri Carter
ORC Name: Jean Creech
ORC Cert.#: 987974
Reason for Inspection
County: Cleveland
Issuance Date:
May 3, 2006
Expiration Date:
April 28, 2011
Expiration Date:
N/A
Telephone No.:
704/480-4700
Telephone No.:
704/752-8673
B/U ORC: not assigned
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the facility's
wwtp (permit # NC 0004952). Sludge storage is estimated to be 1095 days. Records indicate that
CNA has not land applied since 2004. It was noted at the time of inspection that the storage
lagoons are all full and CNA will have to land apply soon, in order to comply with the required
freeboard minimum of 2 feet (24 inches) in each sludge lagoon.
SYNAGRO is the current land application contractor.
CNA should call the regional office when they are ready to land apply this year.
Is a follow-up inspection necessary X yes
no
Inspector(s) Name(s)/Title(s) Ellen Huffman/ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 02/28/07

WQ0011038 CNA Holdings, Inc. 02/28/07 pg 2
Tyne of Residual
X Land Application (class B)
Distribution and Marketing (class A)
Record Keeping Y/N Not evaluated.
Y Copy of current permit available at residual generating site
N/E Current metals and nutrient analysis (see permit for frequency)
N/E TCLP analysis, SSFA (Standard Soil Fertility Analysis)
N/E Nutrient and metals loading calculations (to determine most limiting parameter) YTD
N/E Hauling records (# gal and/or ton hauled during calendar year to date)
N/E Field loading records, Field site maps and information
N/E Records of lime purchased
N/E Pathogen & Vector Attraction Reduction
Comments: The permittee has of land applied since 2004. Vector attraction reduction is not
required by this permit. There has been no land application for 2002 or 2b03.
Treatment
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime other -describe
Transport Not evaluated
Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Comment: A spill control plan was placed in each truck before the inspection was over.
Operation & Maintenance records
Condition of land application equipment on site N/E
Storage
Number of days/weeks/months of storage 1095 days
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
NCAC 2T .1109(c)(1)(G)states: If liquid residuals are to be placed in the unit, a
decanting system and freeboard marker shall be required.
Sampling
Describe Sampling: Metals and nutrient sampling are taken as grab samples by SYNAGRO from the
storage lagoons prior to land application. Sampling is in accordance with the permit and EPA
standards.
Is sampling adequate? Yes Is sampling representative? Yes

WQ0011038 CNA Holdings, Inc. 02/28/07 pg 3
Application Field(s)
Field identification
Permit on site during application
Buffers adequate
Doc. PAN limits
Signs of runoff / ponding
Not evaluated.
Are there any limiting slopes on fields?
10 % for surface, 18% for subsurface application
Monitoring wells) Y/N: N/A
If yes, location of well(s)
Spill plan on site
Cover crop specified in permit
Site condition adequate
Rain Gauge on site during application
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Odors present _
Vectors present
Describe any nuisance conditions and any corrective actions needed.
None noted

t<
• o�CF W ATF9QG
r
O �
Mr. John Groves, Plant Manager
CNA Holdings, Inc.
P.O. Box 87, Hwy 198
Shelby, North Carolina 28152
Dear Mr. Groves:
Michael F. Easley, Governor
William G. Ross, Jr.,Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
Coleen Sullins, Deputy Director
Division of Water Quality
June 15, 2004
Subject: Land Application Inspection
Permit No. WQ0011038
Cleveland County
Enclosed is the land application inspection report for the inspection conducted on June 3, 2004 by Ms. Ellen
Huffman with this Office.
The report indicates compliance with the subject permit, however; the transport trucks did not have spill plans
on board which is a requirement of permit condition I part 7. There -was no rain gauge at the application field. It is
recommended that a rain gauge be placed at the field the day before land application to insure that there has been no
rainfall greater than'/z inches prior to application per permit condition H part 13.
The inspection report should be self-explanatory, however, if you have any questions, please contact Ms.
Huffman or me at [phone].
Sincerely,
D. Rex G eeason,.E.
Water Quality Regional Supervisor
Attachment
cc: Non -Discharge Compliance
Ms. Pent Carter, Senior Environmental Engineer, CNA Holdings, Inc
SYNAGRO
A*A
NCDENR
Customer Service Mooresville Regional Office, 919 North Main Street, Mooresville, NC 28115 PHONE
[phone]
1 877-623-6748 FAX
[phone]

.1
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
Sherri Evans -Stanton, Acting Secretary
Kerr T. Stevens, Director
son
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings, Inc.
Permit No.: WQ0011038
Last Amended Date: N/A
SOC Issuance Date(if applicable): N/A
Permittee Contact: Pem Carter
ORC Name: Robert Wilcox
ORC Cert.#: 13285
Reason for Inspection
County: Cleveland
Issuance Date: Aug. 4, 2000
Expiration Date: July 31, 2005
Expiration Date: N/A
Telephone No.: 704/480-4700
Telephone No.: 336/766-0328 ext 115
B/U ORC: John Coats cert. not valid
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the facility's
wwtp (permit # NC 0004952). Sludge storage is estimated to be 1095 days. Because CNA has a
large volume of storage they only expect to land apply every other year, and until the recent
application in June, 2004, have not land applied.since 2001. SYNAGRO is the current land
application contractor. The land application event took place the first two weeks of June 2004. An
inspection on June 3, 2004 reflected compliance; however, the transport trucks did not have spill
plans on board which is a requirement of permit condition I part 7. There was no rain gauge at the
application field. It is recommended that a rain gauge be placed at the field the day before land
application to insure that there has been no rainfall greater than '/z inches prior to application per
permit condition II part 13.
Is a follow-up inspection necessary _yes X no
Inspector(s) Name(s)/Title(s) Ellen Huffman/ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 06/03/04

WQ0011038 CNA Holdings, Inc.
Tyne of Residual
X Land Application (class B)
Distribution and Marketing (class A)
pg 2
Record Keeping Y/N
Y Copy of current permit available at residual generating site
N/A Current metals and nutrient analysis (see permit for frequency)
N/A TCLP analysis, SSFA (Standard Soil Fertility Analysis)
N/A Nutrient and metals loading calculations (to determine most limiting parameter) YTD
N/A Hauling records (# gal and/or ton hauled during calendar year to date)
N/A Field loading records, Field site maps and information
N/A Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Comments: Pathogen and vector attraction reduction is not required by this permit. There has
been no land application for 2002 or 2003.
Pathogen & Vector Attraction Reduction Records N/A
Treatment
X Aerobic digestion _
Anaerobic digestion _
Alkaline Stabilization Lime
Autothermal Thermophilic Aerobic Digestion
Drying beds (may not meet 503's)
other -describe
Compost N/A
Windrow Aerated Static Pile In vessel Other
Transvort
Spill control plan in transport vehicle? No
Does transport vehicle appear to be maintained? Yes
Comment: A spill control plan was placed in each truck before the inspection was over.
Operation & Maintenance records
Condition of land application equipment on site good
Storage
Number of days/weeks/months of storage 1095 days
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
Sampling
Describe Sampling: Metals and nutrient sampling are taken as grab_samples by SYNAGRO from the
storage lagoons prior to land application. Sampling is in accordance with the permit and EPA
standards.

Is sampling adequate? Yes Is sampling representative? Yes
WQ0011038 CNA Holdings, Inc.
Application Field
Field identification
Yes Permit on site during application
Yes Buffers adequate
No Documented exceedances of PAN limits
No Signs of runoff/ ponding
Are there any limiting slopes on fields? No
10 % for surface application
18% for subsurface application
Monitoring wells) Y/N: N
If yes, location of well(s)
pg 3
Yes Spill plan on site
Yes Cover crop specified in permit
Yes Site condition adequate
No Rain Gauge on site during application
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Odors present no
Vectors present no
Describe any nuisance conditions and any corrective actions needed.
None noted

s �
OF W A7FR Michael F. Easley, Govemo
p William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
r Alan W. Klimek, P.E. Director
Division of Water Quality
O
September 27, 2002
Mr. John Groves, Plant Manager
CNA Holdings, Inc.
P.O. Box 87, Hwy 198
Shelby, North Carolina 28152
Subject: Land Application Inspection
Permit No. WQ0011038
Cleveland County
Dear Mr. Groves:
Enclosed is the land application inspection report for the inspection conducted on September
26, 2002 by Ms. Ellen Huffman with this Office. The report indicates compliance with the subject
permit.
The report should be self-explanatory, however, if you have any questions, please contact
Mrs. Huffinan or me at [phone].
Sincerely,
D. Rex Gleason, F.E.
Water Quality Regional Supervisor
Attachment
cc: Non -Discharge Compliance
Ms. Pem Carter, Senior Environmental Engineer, CNA Holdings, Inc
H: CNA0902.doc
NCDEPR
Customer Service Mooresville Regional Office PHONE [phone]
1 800 623-7748 919 North Main Street, Mooresville, NC 28115 FAX [phone]

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
Sherri Evans -Stanton, Acting Secretary
Kerr T. Stevens, Director
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings_ Inc.
Permit No.: W00011038
Last Amended.Date: N/A
SOC Issuance Date(if applicable): N/A
Permittee Contact: Pem Carter
ORC Name: Robert Wilcox
ORC CertA 13285
Reason for Inspection
County: Cleveland
Issuance Date: Aug. 4, 2000
Expiration Date: July 31, 2005
Expiration Date: N/A
Telephone No.:. 704/480-4700
Telephone No.: 336/766-0328 ext 115
B/U ORC: John Coats cert. not valid
X ROUTINE . COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached paaes)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the facility's
Wwtp (permit # NC 0004952). CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG. CNA
also has a MG polishing pond. Sludge storage is estimated to be 1095 days, includung the
polishing -pond. CNA expects land application activity to occur every other year-ana does not
expect to -land apply any.sludge during 2002. Inspection of the storage lagoons and areview of the
annual report for 2001-indicates compliance. SYNAGRO is the current contractor.
Is a follow-up inspection necessary _yes X no
Inspector(s) Name(s)/Title(s) Ellen Huffman/ Environmental Specie
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 9/26/02

WQ0011038 CNA Holdings, Inc. pg 2
Type of Residual
X Land Application (class B) Distribution and Marketing (class A)
Record 1Keepin YIN
Y Copy of current permit available at residual generating site
N/A Current metals and nutrient analysis (see permit for frequency)
N/A TCLP analysis, SSFA (Standard Soil Fertility Analysis)
N/A Nutrient and metals loading calculations (to determine most limiting parameter) YTD
N/A Hauling records (# gal and/or ton hauled during calendar year to date)
N/A Field loading records, Field site maps and information
N/A Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Comments: Pathogen and vector attraction reduction is not required by this permit. There has
been no land application for 2002.
Pathogen & Vector Attraction Reduction Records N/A
(check which methods apply)
Fecal coliform
SM 9221 E (Class A or B)
(Class A, all test must be <1000 MPN / dry gram)
(Class B, Geometric mean of 7 samples/monitoring period - <2.0*106 CFU / dry gram)
SM 9222 D (Class B only)
(Geometric mean of 7 samples/monitoring period for Class B <2.0* 106 CFU / dry gram)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry
Time / Temp records
Digester (MCRT) Compost Class A lime stabilization _
Volatile solids calculations
Bench -top aerobic/anaerobic digestion results
pH records for lime stabilization ( Class A or B )
SOUR calculations
Treatment (check treatment type(s) used)
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime other -describe
Compost (check treatment type used) N/A
Windrow Aerated Static Pile In vessel Other

_.---�.._._..a.......�...._........,...._�..w,a�..::..x _. __.�.-„..:..rc..:o:.�...-ye...�.e:- �,.._._�a..-.:s:r;.y--se'.e.:.s:.::"'���.i.:f:...;,-e:¢...�=-,�r'_.'-::1..�s�.•"c,,..f.":�n.....sip'a,r.�.�?_w`�-c�.�.�m�.iti..'.i�.._ / .....,_
K
WQ0011038 CNA Holdings, Inc.
Transport Where was no land application activity at the time of inspection.
Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Operation & Maintenance records
There was no land application activity at the time of inspection.
Condition of land application equipment on site
Storage
Number of days/weeks/months of storage 1095 days
Describe storage: CNA has 2 unlined storage lagoons: 1.66 MG and 2.23 MG.
pg 3
Sampling
Describe Sampling: Metals, and nutrient sampling are taken as grab samples by SYNAGRO from
the storaae lagoons prior to land application Sampling is in accordance with the permit and EPA
standards.
Is sampling adequate? Yes Is sampling representative? Yes
Field Sites (end use for class B biosolids)
There was no land application activity at the time of inspection.
Field identification
Permit on site during application
Buffers adequate
Documented exceedances of PAN limits
Signs of runoff / ponding
Rain Gauge on site during application
Are there any limiting slopes on fields? Y/N
10 % for surface application
Comment:
Spill plan on site
Cover crop specified in permit
Site condition adequate
(if no, improvements recommended) _
18% for subsurface application

s
�r
WQ0011038 CNA Holdings, Inc. pg 4
Monitoring well(s) Y N: N
If yes, location of well(s)
Comment: There are no groundwater monitoring wells related to this permit; however, there are
groundwater remediation wells on the facility's plant site.
Odors/vectors
Comment: There was no land application activity at the time of inspection.
Odors present _
Vectors present
Describe any nuisance conditions and any corrective actions needed.

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
Sherri Evans -Stanton, Acting Secretary
Kerr T. Stevens, Director
02
WON
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Permittee: CNA Holdings, Inc.
Permit No.: W0001.1038
Last Amended Date: N/A
SOC Issuance Date(if applicable): N/A
Permittee Contact: Pem Carter
ORC Name: Robert Wilcox
ORC Cert.#: 13285
Reason for Inspection
County: Cleveland
Issuance Date:
Aug. 4, 2000
Expiration Date:
July 31, 2005
Expiration Date:
N/A
Telephone No.:
704/480-4700
Telephone No.:
336/766-0328 ext 115
B/U ORC: John Coats cert. not valid
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pares)
CNA Holdings, Inc., is permitted to apply 570 dry tons of sludge per year from the plant's wwtp
( permit # NC 0004952). There has been no land application activity for 2002. CNA has 2
unlined storage lagoons: 1.66 MG and 2.23 MG. CNA also has a polishing pond with a 3 MG
volume. Sludge storage is estimated to be 1095 days, includung the polishing pond. CNA
expects land application activity to occur every other year and does not expect to land apply any
sludge during 2002. Inspection of the storage lagoons Review of the annual report for 2001
indicates compliance. SYNAGRO is the current contractor.
Is a follow-up inspection necessary _des X no
Inspector(s) Name(s)/Title(s) Ellen Huffman/ Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection 9/26/02

Residuals Inspection pg 2
WQ0011038 CNA Holdings, Inc. 9/26/02
Type of Residual
X Land Application (class B)
Distribution and Marketing (class A)
Record KeepinS Y/N
Y Copy of current permit available at residual generating site
N/A Current metals and nutrient analysis (see permit for frequency)
N/A TCLP analysis, SSFA (Standard Soil Fertility Analysis)
N/A Nutrient and metals loading calculations (to determine most limiting parameter) YTD
N/A Hauling records (# gal and/or ton hauled during calendar year to date)
N/A Field loading records, Field site maps and information
N/A Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Comments: Pathogen and Vector Attraction Reduction is not required by this permit. There has
been no land application for 2002.
Pathogen & Vector Attraction Reduction Records N/A
(check which methods apply)
Fecal coliform
SM 9221 E (Class A or B)
(Class A, all test must be <1000 MPN / dry gram)
(Class B, Geometric mean of 7 samples/monitoring period - <2.0* 106 CFU / dry gram)
SM 9222 D (Class B only)
(Geometric mean of 7 samples/monitoring period for Class B <2.0*106 CFU / dry gram)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry
Time / Temp records
Digester (MCRT) Compost Class A lime stabilization _
Volatile solids calculations
Bench -top aerobic/anaerobic digestion results
pH records for lime stabilization ( Class A or B )
SOUR calculations
Treatment (check treatment type(s) used)
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime other -describe
Compost (check treatment type used) N/A
Windrow Aerated Static Pile In vessel Other

-11
,r
6 -
iicona
1999
July 30, 1999 .;��.� ��
JLM:99:036`,,fiH Y' of Shelby Plant
Highway 198
Shelby, NC 28152
Certified Mall Telephone [phone]
NC Department of Environment, Health, and Natural Resources
Division of Water Quality
P. O. Box 29535
Raleigh, North Carolina 27626-0535
Attn: Mr. Kevin Barnett
Re: NPDES Land Residuals Application Permit Number WQ0011038 for
HNA Holdings, Inc., Shelby, NC — Change in Owner/Operator Name
The purpose of this memorandum. is.to inform you that the name of the
owner/operator of the Shelby; NG, facility of HNA Holdings, Inc. (formerly known
as_Hoechst Celanese Corporation) is changing. Effective 8/16/99, the HNA
Holdings' Shelby, NC, facility will be a part of CNA Holdings, Inc. (Celanese
North America Holdings,-Inc.),This change is a part of the global reorganization
of the Hoechst companies. No changes will occur in the site's operations or
management with the change in the operator's name.
The NPDES residuals land application permit for this facility, WQ0011038, needs
to be changed to indicate the owner/operator's name change to CNA Holdings,
Inc. Any fees required to make this change should be billed to CNA Holdings,
Inc., and sent to my attention.
All correspondence concerning the permit name change should be sent to my
attention. If you have any questions concerning this change, or if any additional
information is required, please feel free to contact me at [phone], or via
email at imtnctnurray @ticona.com.
Hoechst N
Ticona - A member of the
Hoechst Group

July 29, 1999
JLM:99:035
Certified Mail
NC Department of Environment, Health, and Natural Resources
Division of Water Quality
P. O. Box 29535
Raleigh, North Carolina 27626-0535
Attn: Mr. Mark McIntire
iicona
Ticona, ...
Shelby Plant
Highway 198
Shelby, NC 28152 -
Telephone [phone]
Re: NPDES Permit Number NC0004952 for HNA Holdings, Inc., Shelby,
NC — Change in Owner/Operator Name
The purpose of this memorandum is to inform you that the owner/operator of the
Shelby, NC, facility of HNA Holdings, Inc. (formerly known as Hoechst Celanese
Corporation)is, changing, Effective.:8/16/99,j; a HNA Holdings' Shelby, NC,
facility will be a part of CNA Holdings, Inc. (Celanese North America Holdings,
Inc.:) This change is a part of the global reorganization of the Hoechst companies.
No changes will occur in the site's operations or management with the change in
the- operator's -name....,.
The NPDES permit for this facility, NC0004952, was issued earlier this year. Any
fees required to make this change should be billed to CNA Holdings, Inc., and
sent to my attention.
All correspondence concerning the permit name change should be sent to my
attention. If you have any questions concerning this change, or if any additional
information is required, please feel free to contact me at [phone], or via
email at immcmurray aDticona.com.
With Best Regards,
YV-AG _
Jerry L. McMurray
Staff Environmental/Safety Engineer
Ticona - A member of the
Hoechst Group

■
State of North Carolina
T�IWA
Department of Environment,
Health and Natural Resources •
Mooresville Regional Office
James B. Hunt, Governor p E H N
Jonathan B. Howes, Secretary
Linda Diane Long, Regional Manager
DIVISION OF.ENVIRONMENTAL MANAGEMENT
September 19, 1995
Hoechst Celanese
Post Office Box 860
Mount Holly, North Carolina 2812.0
Attention: Mr. Carrol Whaley
Subject: Hoecsht Celanese
Permit JWQ0002544
Gaston, Lincoln and Catawba County, N.C.
Dear Mr. Whaley:
The Groundwater Section of the Mooresville Regional Office
received the groundwater monitoring report for the subject
facility on September 1, 1995. A review of the report and two
previous reports received on May 16, 1995 and December 16, 1994
reveals that method detection limits (MDLs) are above standard
levels as established in Commission Rule 15A NCAC 2L .0202 and in
the subject permit. In particular, VOC analysis and fecal
coliform MDLs are above the standards. Note that standards in 2L
are constituent dependent and that fecal coliform shall not
exceed 1 organism per 100 ml.
Should you have any questions, please call me at (704) 663-
1699, ext. 241.
Sincerely,
Steven Bogra
Hydrogeological Technician
SEB
919 North Main Street, Mooresville, North Carolina 28115 Telephone [phone], FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

p, C. DEFT. OF NATURAL
RLSOURCrS AND
coa.rsu,,iT,1'IBBi'6F ENVIRONMENTAL MANAGEMENT
September 4, 1991
SEP 1 01991
oi�4 c [';;;,�l;i�Ei;IAL K�.flAGEh1ENY
OFFICE
M E M O
TO: Barbara Christian
Mooresville Regional Office .
FROM: Perry F. Nelson, l Chief/f
Groundwater Section v�
SUBJECT: Hoechst Celanese Landfill
I have discussed subject site with Jesse and advised him to
monitor Hoechst Celanese progress in the implementation of their
corrective action plan.
As we have issued an NOV for groundwater standards
violations, the company is proceeding toward remediation in a
responsible manner, and the site is relatively low on your
priority list, I see no need for heavy involvement by your staff.
I am unable, at this time, to provide you with clear
guidance on our responsibility with regard to sites in which the
Solid Waste Management Division is involved.
The following paragraphs generally describe my views on how
we ought to handle situations involving SWMD. I would appreciate
your views and Brenda's as well.
Where Solid Waste Management Division is clearly the lead
agency for enforcement of environmental rules, and finds
themselves unable to discharge their regulatory responsibility,
and groundwater violations have occurred, then the Division of
Environmental Management should provide the environmental "safety
net" and implement its regulatory authority as appropriate.
To be more specific, where a facility has caused groundwater
contamination and that facility is, or would normally be, under
the regulatory authority of the Solid Waste Managaement Division
(hazardous waste, solid waste or Superfund) and the SWMD is
unable to accept or continue its lead agency role, we the
Groundwater Section, must step into the breach and use our own
authority to. protect or cleanup the groundwaters. We should
issue an NOV, if we have not already issued one, and require
cleanup under the terms of an SOC (until such time as SOC' s are
no longer required).

Barbara Christian
Page Two
September 4, 1991
Conversely, where we discover, or are the first responder to
an incident involving a facility clearly identified as the source
of groundwater contamination, and the contamination is as a
result of the release or disposal of hazardous wastes, we should
inform the SWMD immediately, in -writing, of our intention to
advise the responsible party of the violation and the pertinent
regulatory requirements under the DEM rules, and our intention to
defer to the SWMD as the lead regulatory agency but retain the
right of enforcement should the facility fail to act in
accordance with SWMD's requirements, or should other
circumstances develop which made enforcement action by DEM
necessary.
For facilities which are on the State Superfund Section's
inactive site list, I believe we should exercise any authority we
have to implement cleanup of any such site we find to be a
significant problem. It is my understanding that the Superfund
Section would not discourage our involvement.
cc: Ted Bush
Burrie Boshoff
PFN/asn:Hoechst.

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