NC0005274_Regional Office Historical File Pre 2018 (2)

�1\RO DIVISION OF WATER QUALITY-GROUNDWATER SECTION
rWATER
QUALITY MONITORING: P.O. BOX 29578
Foradditional forms RALEIGH,NC 27626-0578 *' . r;'i orNCE REPORT FORM please write or call: [phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER:(REQUIRED)
Facility Name Crompton & Knowles Colors Incorporated Non-Discharge MAY is 1998
Address 1602 North Main Street NPDES NC 000527/i
Lowell, N. C. 2R County Gactcn TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Ul(1::.-2 '. _;.i.11T
Well Location Upgradient From Wastewater Treatment Plant Lagoon Sept Tank/grain,Fieigj 4, ,,oN
Well Identification Number MW-1 Well Depth 100 Ft.
Well Diameter 2" Sample (Screened) Interval 90 Ft. To 1 nn Ft. Spray Field Subsurface Low Pressure
p Piping(LPP)
Depth to Water Level 76.75 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 0 ft. above land surface X Other
Gallons of water pumped/bailed before sampling 12.6 Rotary Distributor
Field Analysis: pH 6.70 Specific Conductance 295 uMhos Temp. 18.2 °C Odor None Appearance Clear
Date Sample Collected 04-06-98 Date Lab Sample Analyzed 04-06-98 to - 04-16-98
Laboratory Name Pace Analytical Certification No. 12
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD < 25 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA mg/I
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb- Lead < 0- 1 o mg/I
Coliform: MF Total NA /100m Phosphorus: Total as P NA mg/ Zn - Zinc 0 099 mg/I
(Note:Use MPN method for highly turbid samples) Al -Aluminum NA mg/ Pesticides/Herbicides
Dissolved Solids: Total 190 mg/ Ba - Barium NA mg/ (Specify Compounds)
pH (when analyzed) NA units Ca - Calcium NA mg/ NA n =' ug/I
TOC < 0.50 mg/ Cd - Cadmium NA mg/ NA — .-ug/1
Chloride 14 mg/ Chromium: Total < 0.010 mg/ NA = g/1
Arsenic NA mg/ Cu - Copper < 0.010 mg/ Other (Specify Compounds and —
Grease and Oils < 5 mg/ Fe - Iron NA mg/ Concentration units)
Hardness: Total NA mg/ Hg - Mercury NA mg/ TSS 20 /1
Phenol <0.005 mg/ K - Potassium NA mg/
Sulfate 33 mg/ Mg - Magnesium NA mg/
Specific Conductance NA uMhos Mn - Manganese NA mg/ ;,,
Total Ammonia NA mg/ Na - Sodium NA mg/ '
TKN as N NA mg/
I C TIF THAT REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
►'yJ colloidal concentrations. (see#3 on back)
f'` -2y/f !c 9� * See back for instructions.
Si nature of Permittee ( Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE#4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!!
Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
lab within 24 hours.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
ESA-600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
• 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See#4. above)
10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company,corporation, or governmental body to sign official documents.

DIVISION OF WATER QUALITY-GROUNDWATER SECTION
OUNDWATER QUALITY MONITORING: P.O.BOX 29578I P
For additional forms RALEIGH,NC 27626-0578
COMPLIANCE REPORT FORM please write or call: [phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name Crompton & Knnw1 PS Call nrs Tnrnrpnratarl Non-Discharge
Address 1602 North Main Street NPDES NC 0005276
Lowell, N. C. 23098 County (Tastnn TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Well Location Downgradients frnm Wastewater Treatmant Plant Lagoon Septic Tank/Drain Field
Well Identification Number MW-2 Well Depth 29.0 Ft.
Well Diameter 2" Sample (Screened) Interval 19.0 Ft. To 99.0 Ft. Spray Field PSiping
gr(LPPLow-Pressure
)
Depth to Water Level 17.16 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 1 .5 ft. above land surface x Other
Gallons of water pumped/bailed before sampling 5.8 Rotary Distributor
Field Analysis: pH 6.19 Specific Conductance 342 uMhos Temp. 15.7 °C Odor None Appearance RPd/Brown
Date Sample Collected 04-06-98 Date Lab Sample Analyzed 04-06-98 to 04-16-98
Laboratory Name Pace Analytical Certification No. 1 9
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD 29 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA mg/I
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb- Lead < 0 10 mg/I
Coliform: MF Total NA /100m Phosphorus: Total as P NA mg/ Zn -Zinc o_lo mg/I
(Note:Use MPN method for highly turbid samples) Al -Aluminum NA mg/ Pesticides/Herbicides
Dissolved Solids: Total 280 mg/ Ba- Barium NA mg/ (Specify Compounds)
pH (when analyzed) NA units Ca - Calcium NA mg/ NA 7 ugh! -
TOC 1,2 mg/ Cd - Cadmium NA mg/ NA `- ug/I
Chloride 64 mg/ Chromium: Total 0-0f6. mg/ NA - :" ug/I
Arsenic NA mg/ Cu - Copper 0.11 mg/ Other (Specify Compounds and ---
Grease and Oils < 5 mg/ Fe - Iron NA mg/ Concentration units) -
Hardness: Total NA mg/ Hg - Mercury NA mg/ TSS -420 mg/1
Phenol <0.005 mg/ K - Potassium NA mg/ �`
Sulfate 18 mg/ Mg - Magnesium NA mg/ _,
Specific Conductance NA uMhos Mn - Manganese NA mg/ ra
Total Ammonia NA mg/ Na - Sodium NA mg/ N
TKN as N NA mg/
I CERT THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
n colloidal concentrations. (see#3 on back)
1 , / 7 /r * See back for instructions.
Signature of Permittee (or Authorized Agent*) /Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE#4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD U!
Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
lab within 24 hours.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT ARE A PART QE SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR,SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per Title 15, North Carolina Administrative Code,Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA-600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods,3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See#4. above)
10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company,corporation, or governmental body to sign official documents.

DIVISION OF WATER QUALITY-GROUNDWATER SECTION
PLFrimFOI°AlliNID:IPC(TEEFil
QUALITY MONITORING; P.o.sox 29578
For additional formsRALEIGH,NC 27626-0578
PORT FORM please write or call: [phone]
I
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name Crompton & KTowl PR (:n1 me TnporporatPd Non-Discharge AA��QQ��??
Address 1602 North Ma-in StrPPt NPDES 74
TYPE OF DISPOSAL 'BEING MONITORED
Lowe]1, N. C. 7Rn98 County Gaston (REQUIRED)
Well Location Downgr client from Wastewater Treatment Plant Lagoon Septic Tank/Drain Field
Well Identification Number Nw-3 Well Depth 27.1 Ft. Spray Field Subsurface Low Pressure
Well Diameter 7" Sample (Screened) Interval 17.1 Ft. To 27.1 Ft. Piping(LPP)
Depth to Water Level 15.94 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 1.5 ft. above land surface x Other
Gallons of water pumped/bailed before sampling 5.5 Rotary Distributor
Field Analysis: pH 8.54 Specific Conductance 27400 uMhos Temp. 14.4°C OdoChcm- -A 1 Appearance Jett Black
Date Sample Collected 04-06-98 Date Lab Sample Analyzed 04-0f—oR to n4-16-98
Laboratory Name Pace Analyf-;ra1 Certification No. l2
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD 2500 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA mg/I .
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb- Lead L O.io p g/I
Coliform: MF Total NA /100m Phosphorus: Total as P NA mg/ Zn -Zinc 0.13 '-'3 m g/I
•(Note:Use MPN method for highly turbid samples) Al - Aluminum NA mg/ Pesticides/Herbicides _ ' -
Dissolved Solids: Total 9200 mg/ Ba- Barium NA mg/ (Specify Compounds)
pH (when analyzed) NA units Ca - Calcium NA mg/ NA — _ug/I
TOC 120 mg/ Cd - Cadmium NA mg/ NA . U /I
Chloride 4000 mg/ Chromium: Total 0.13 mg/ NA ug/I
Arsenic NA mg/ Cu - Copper 2.2 mg/ Other (Specify Compounds and . ' i
Grease and Oils 5 mg/ Fe - Iron NA mg/ Concentration units)
J
fHardness: Total NA mg/ Hg - Mercury NA mg/ TSS r,) 1941 mg/1
Phenol 4.6 mg/ K - Potassium NA mg/ Benzene =4b ug/1
Sulfate 1200 mg/ Mg - Magnesium NA mg/ Chlorobenaenc 79 ug/1
Specific Conductance NA uMhos Mn - Manganese NA mg/ 1 ,2-D;rhlorohenzene 51i ug/1
Total Ammonia NA mg/ Na - Sodium NA mg/ PhPnoi 2200 ug/1
TKN as N NA mg/ 1,9,4 Trirhlorohew7oae 1800 ugh1
Nnnthn1l.RT 7.8 u6/1
I CE IFY THAT THIS REPORT IS TRUE AND ACCURATE. Values snouid rt 5.8 u /1
e N-Ni ro odinbecmin
Note: t aissoived and g
colloidal concentrations. (see#3 on back)
''` 27//. / C y P . See back for instructions.
Signature of Pe mittee (or Authorized Agent*) ` Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE#4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!!
Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
lab within 24 hours.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT ARE A PART QE SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per Title 15, North Carolina Administrative Code,Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA-600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods,3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See#4. above)
10.The sample container should be labeled at the time of collection with the facility name,well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company,corporation, or governmental body to sign official documents.

k\A II DIVISION OF WATER QUALITY-GROUNDWATER SECTION
GROUNDWATER QUALITY MONITORING: `' P.O. BOX 29578
For additional forms RALEIGH,NC 27626-0578
COMPLIANCE REPORT FORM please write or call: {919)733-3221
Type or Use a ball-point pen and press firmly. PERMIT NUMBER:(REQUIRED)
Facility Name Crompton R, Knnw1 s Colo.rs Incorporated Non-Discharge rr_-, r
Address 1609 North Main Street NPDES NC 000527ii
Lowell, N. C. 28098 County Gaston TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) •
Well Location Downgradient from Wastewater Treatment P1 ant Lagoon Septic Tank/Drain Field
Well Identification Number MW-2 Well Depth 79.0 Ft.
Well Diameter 2" Sample (Screened) Interval 19.0 Ft. To 79.0 Ft. Spray Field Subsurface
ping(LPP;ow-Pressure
Depth to Water Level 16.67ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 1.5 ft. above land surface X Other
Gallons of water pumped/bailed before sampling 6. Rotary Distributor
Field Analysis: pH 6.03 Specific Conductance 319 uMhos Temp._14 0 °C Odor None Appearance Turbid
Date Sample Collected 01-21-98 Date Lab Sample Analyzed 01-21-9R to n 1-99-98
Laboratory Name Pace Analytical Certification No. 17
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD < 25 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA mg/I
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb - Lead 4 0.005 mg/I
Coliform: MF Total NA /100m Phosphorus: Total as P _NA mg/ Zn - Zinc 0.011 =, mg/I
(Note:Use MPN method for highly turbid samples) Al - Aluminum NA mg/ Pesticides/Herbicides
Dissolved Solids: Total 250 mg/ Ba- Barium NA mg/ (Specify Compounds) m r:r.
pH (when analyzed) NA units Ca - Calcium NA mg/ NA cc) =: /I
TOC 5.2 mg/ Cd - Cadmium NA mg/ NA i;.-; ,tiW
Chloride 71 mg/ Chromium: Total < 0.01 0 mg/ NA . ug/1
Arsenic NA mg/ Cu - Copper 0.012 mg/ Other (Specify Compounds and
Grease and Oils 4 1.0 mg/ Fe - Iron NA mg/ Concentration units) = x -
Hardness: Total NA mg/ Hg - Mercury NA mg/ TcS 37 tJ% <_ G/L
Phenol < 0.005 mg/ K - Potassium NA mg/ �;
Sulfate 40 mg/ Mg - Magnesium NA mg/
Specific Conductance NA uMhos Mn - Manganese NA mg/
Total Ammonia NA mg/ Na - Sodium NA mg/
TKN as N NA mg/
I CERT THAT THIS ORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
/f `Z 9 ,,/} colloidal concentrations. (see#3 on back)
4a/41W(-„
� * See back for instructions.
Sin re of Permittee (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96 31�/�1 , �-,

•
COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE#4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!!
Unfiltered samples must be collected for metals,then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
lab within 24 hours.
Sample preparation in the laboratory(extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT ARE A PART QE SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA-600/4-79-020, as revised March 1983;
q • (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
f ; publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol.49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3•volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volume&are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above)
10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company,corporation, or governmental body to sign official documents.

DIVISION OF WATER QUALITY-GROUNDWATER SECTION
GROUNDWATER QUALITY MONITORING: P.O. BOX 29578
For additional forms RALEIGH,NC 27626-0578
COMPLIANCE REPORT FORM please write or call: [phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name Crompton & Knowles Colors Incorporated Non-Discharge
Address 1602 North Main Street NPDES
Lowell. N. C. 28098 County Gaston TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Well Location Upgradient from Wastewater Treatment Plant Lagoon Septic Tank/Drain Field
Well Identification Number MW-1 Well Depth 100 Ft.
n Spray Field Subsurface Low-Pressure
Well Diameter 2 Sample (Screened) Interval 90 Ft. To 100 Ft. Piping(LPP)
Depth to Water Level 76.08 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 0 ft. above land surface N Other
Gallons of water pumped/bailed before sampling 13.0 Rotary Distributor
Field Analysis: pH 6.65 Specific Conductance 136 uMhos Temp. 15.6 °C Odor None Appearance Turbid
Date Sample Collected 01-21-98 Date Lab Sample Analyzed 01-21-98 to 01-29-98
Laboratory Name Pace Analytical Certification No. 12
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD < 25 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA mg/I
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb - Lead < 0.005 -r, g/I
Coliform: MF Total NA. /100m Phosphorus: Total as P NA mg/ Zn -Zinc 0.012 T g/I
(Note:Use MPN method for highly turbid samples) Al - Aluminum NA mg/ Pesticides/Herbicides L---
Dissolved Solids: Total 120 mg/ Ba - Barium NA mg/ (Specify Compounds) r z
v
pH (when analyzed) NA units Ca - Calcium NA mg/ NA --"
TOC 0.73 mg/ Cd - Cadmium NA mg/ NA - t_t9/1
Chloride 4 mg/ Chromium: Total <0.010 mg/ NA ..2/1
Arsenic NA mg/ Cu - Copper < 0.010 mg/ Other (Specify Compounds andcmF' r s
Grease and Oils 41.0 mg/ Fe - Iron NA mg/ Concentration units)
Hardness: Total NA mg/ Hg - Mercury NA mg/ TSS 32 MG/L
Phenol <0.005 mg/ K - Potassium NA mg/
Sulfate 18 mg/ Mg - Magnesium NA mg/
Specific Conductance NA uMhos Mn - Manganese NA mg/
Total Ammonia NA mg/ Na - Sodium NA mg/
TKN as N NA mg/
I CE'PHAT TH REPOR IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
' _ .41 9-/i 61 9 S,- colloidal concentrations. (see#3 on back)
4 I4',4, / * See back for instructions.
Signature of Permittee (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

_ ,
F
COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!!
Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
lab within 24 hours.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT ARE A PART Qf SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
• (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency pUblication number
EPA-600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods,3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
•
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
F
5. IMeasurciand record the depth of water in the well prior to pumping or bailing any water from the well.
•••
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is availablg.to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See#4. above)
• 10.The sample container should be labeled at the time of collection with the facility name,well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents.
L. - - ---- • .

DIVISION OF WATER QUALITY GROUNDWATER SECTION
GROUNDWATER QUALITY MONITORING; P.O. BOX 29578
For additional forms RALEIGH,NC 27626-0578
COMPLIANCE REPORT FORM please write or call: [phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER:(REQUIRED)
Facility Name Crompton & Knowles Colors Incorporated Non-Discharge
Address 1602 North Main Street NPDES NC TYPE OF DISPOSAL OPERATION 74
BEING MONITORED
Lowell, N. C. 28098 County Gaston (REQUIRED)
Well Location Downgradient from Wastewater Treatment. P1 ant Lagoon Septic Tank/Drain Field
Well Identification Number MW-3 Well Depth 27.1 Ft.
Well Diameter 2" Sample (Screened) Interval 17.1 Ft. To 27.1 Ft. Spray Field Subsurface Low Pressure
P Piping(LPP)
Depth to Water Level 14.47 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 1.5 ft. above land surface — Other
Gallons of water pumped/bailed before sampling 9. Rotary Distributor
Field Analysis: pH 6.52 Specific Conductance 918 uMhos Temp. 11.6 oC Odor Chemica]Appearance Dark Brown
Date Sample Collected 01-21-98 Date Lab Sample Analyzed 01-21-98 to 01-29-98
Laboratory Name Pace Analytical Certification No. 12
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO `''
m —
.
-n r.ti
COD 140 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA c {'sing/I
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb - Lead 0.007 —N, 11g/1
Coliform: MF Total NA /100m Phosphorus: Total as P NA mg/ Zn -Zinc 0.10 1 mg/I
(Note:Use MPN method for highly turbid samples) Al - Aluminum NA mg/ Pesticides/Herbicides ' ;
Dissolved Solids: Total 840 mg/ Ba - Barium NA mg/ (Specify Compounds) r-'=`=.
pH (when analyzed) NA units Ca - Calcium NA mg/ NA en ;;,1g/I
TOC 45 mg/ Cd - Cadmium NA mg/ NA . ; ug/I
Chloride 200 mg/ Chromium: Total 0.011 mg/ NA . ug/I
Arsenic NA mg/ Cu - Copper 0.25 mg/ Other (Specify Compounds and
Grease and Oils 41.0 mg/ Fe - Iron NA mg/ Concentration units)
Hardness: Total NA mg/ Hg - Mercury NA mg/ TSS 350 MG/L
Phenol 0.056 mg/ K- Potassium NA mg/
Sulfate 150 mg/ Mg - Magnesium NA mg/
Specific Conductance NA uMhos Mn - Manganese NA mg/
Total Ammonia NA mg/ Na - Sodium NA mg/
TKN as N NA mg/
I CE I THAT THI PORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see#3 on back)
,p-/l"`oi� * See back for instructions.
Signature of Permittee (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

.• —^-- ,—..—...."."—...4"r",—.-1.,-....e.•••—•••.•.--.R..........—...&---,..m.—..+, _ . _
)
i
c
COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
c
! 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE#4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
t
! 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!!
I Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
! lab within 24 hours.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT ARE A PART.Q.E SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
1 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
t the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA-600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
, - publication number SW-846;
-.. (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
E. . October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well i8 pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. ,
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. _
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See#4. above)
10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company,corporation, or governmental body to sign official documents.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
•
February 04, 1998
Mr. Bobby Lamb
Crompton & Knowles Colors, Inc.
P.O. Box 848
1602 North Main Street
Lowell , NC 28098
RE: PACE Project No. 680120.580
Client Reference: Monitoring Wells
Dear Mr. Lamb:
Enclosed is the report of laboratory analyses for samples received
January 21 , 1998.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
Kelly H. allace
Project Manager
Enclosures
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking TN UST Water 90090
NC Drinking Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Crompton & Knowles Colors, Inc. February 04, 1998
P.O. Box 848 PACE Project Number: 680120580
1602 North Main Street
Lowell , NC 28098
Attn: Mr. Bobby Lamb
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001303
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: MWl
Parameter JJnitc PRI MFTHOD DATE ANALYZED
FIELD ANAIYSIS
GROUND WATER FIELD PARAMETERS
pH (Field) Units 6.65 01/21 /98
Specific Conductivity(Field) umhos/cm2 10 136 01 /21 /98
Static Water Level (Depth) feet 0.01 76.08 01 /21 /98
Temperature (Field) Degrees C 15.6 01/21/98
Volume Prepumped Gallons 0. 1 13.0 01/21 /98
INORGANIC ANAIYSTS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand mg/L 25 ND 5220 D 01/22/98
Chloride mg/L 1 4 325.3 01/23/98
Chromium mg/L • 0.010 ND 200.7 01/29/98
Copper mg/L 0.010 0.010 200.7 01/29/98
Lead mg/L 0.005 ND 239.2 01/28/98
Oil & Grease mg/L 1 ND 5520 B 01 /28/98
Phenol , Low Level mg/L 0.005 ND 420.1 01/27/98
Solids, Total Dissolved mg/L 1 120 2540 C 01/26/98
Solids, Total Suspended mg/L 1 32 2540 D 01/22/98
Sulfate mg/L 10 18 375.4 01/28/98
Total Organic Carbon mg/L 0.5 0.73 5310C 01 /30/98
Zinc mg/L 0.010 0.012 200.7 01/29/98
GROUND WATER FIELD PARAMETERS
Odor NONE 01/21 /98
Appearance SL TURBID 01 /21 /98
ORGANIC ANAIYSIS
VOLATILE ORGANICS 624
Chloromethane ug/L 5.0 ND 01/22/98
Chloroethene (Vinyl chloride) ug/L 5.0 ND 01/22/98
Laboratory Certification IDs Laboratory Certification lDa
NC NC Drinking Water ter 37706 REPORT OF LABORATORY ANALYSIS KY DrinkingTs Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 2 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001303
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: MW1
Parameter Writs PRI METHOD DATE ANAIYZED
ORGANIC ANAIYSIS
VOLATILE ORGANICS 624
Bromomethane ug/L 5.0 ND 01/22/98
Chloroethane ug/L 5.0 ND 01/22/98
Trichlorofluoromethane ug/L 5.0 ND 01/22/98
1 ,1-Dichloroethene ug/L 5.0 ND 01 /22/98
Dichloromethane ug/L 5.0 ND 01/22/98
trans-1 ,2-Dichloroethene ug/L 5.0 ND 01/22/98
1 ,1-Dichloroethane ug/L 5.0 ND 01/22/98
cis-1 ,2-Dichloroethene ug/L 5.0 ND 01 /22/98
Chloroform ug/L 5.0 ND 01/22/98
1 ,1 ,1-Trichloroethane ug/L 5.0 ND 01/22/98
1 ,2-Dichloroethane ug/L 5.0 ND 01 /22/98
Carbon tetrachloride ug/L 5.0 ND 01 /22/98
Benzene ug/L 5.0 ND 01/22/98
Trichloroethene ug/L 5.0 ND 01/22/98
1 ,2-Dichloropropane ug/L 5.0 ND 01/22/98
Bromodichloromethane ug/L 5.0 ND 01/22/98
2-Chloroethoxyethene ug/L 10 ND 01/22/98
cis-1 ,3-Dichloropropene ug/L 5.0 ND 01/22/98
Toluene ug/L 5.0 ND 01/22/98
trans-1 ,3-Dichloropropene ug/L 5.0 ND 01/22/98
1 ,1 ,2-Trichloroethane ug/L 5.0 ND 01/22/98
Dibromochloromethane ug/L 5.0 ND 01/22/98
Tetrachloroethene ug/L 5.0 ND 01/22/98
Chlorobenzene ug/L 5.0 ND 01/22/98
Ethylbenzene ug/L 5.0 ND 01/22/98
Bromoform ug/L 5.0 ND 01/22/98
1 ,1 ,2,2-Tetrachloroethane ug/L 5.0 ND 01 /22/98
1 ,3-Dichlorobenzene ug/L • 5.0 ND 01/22/98
1 ,4-Dichlorobenzene ug/L 5.0 ND 01/22/98
1 ,2-Dichlorobenzene ug/L 5.0 ND 01/22/98
Surrogate - Dibromofluoromethane I 99 01/22/98
Laboratory Certification IDs •
Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TM Drinking
T List Water 90090
NC Drinking Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 3 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001303
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: WW1
Paramptpr Units . PRL METHOD DATE ANAIYZED
ORGANIC ANAIYSIS
VOLATILE ORGANICS 624
Surrogate - Toluene-d8 % 105 01/22/98
Surrogate - Bromofluorobenzene % 106 01 /22/98
BASE/NEUTRALS AND ACIDS 625
N-Nitrosodimethylamine ug/L 5.0 ND 01/27/98
bis(2-Chloroethyl )ether ug/L 5.0 ND 01/27/98
Phenol ug/L 5.0 ND 01 /27/98
2-Chlorophenol ug/L 5.0 ND 01 /27/98
1 ,3-Dichlorobenzene ug/L 5.0 ND 01 /27/98
1 ,4-Dichlorobenzene ug/L 5.0 ND 01 /27/98
1 ,2-Dichlorobenzene ug/L 5.0 ND 01/27/98
bis(2-Chloroisopropyl )ether ug/L 5.0 ND 01/27/98
Hexachloroethane ug/L 5.0 ND 01/27/98
N-Nitrosodi-n-propylamine ug/L 5.0 ND 01/27/98
Nitrobenzene ug/L 5.0 ND 01 /27/98
3,5,5-Trimethyl-2-cyclohexen-l-one ug/L 5.0 ND 01 /27/98
2-Nitrophenol ug/L 5.0 ND 01/27/98
2,4-Dimethylphenol ug/L 5.0 ND 01/27/98
bis(2-Chloroethoxy)methane ug/L 5.0 ND 01/27/98
2,4-Dichlorophenol. ug/L 5.0 ND 01/27/98
1 ,2,4-Trichlorobenzene ug/L 5.0 ND 01/27/98
Naphthalene ug/L 5.0 ND 01/27/98
Hexachlorobutadiene ug/L 5.0 ND 01/27/98
4-Chloro-3-methylphenol ug/L 5.0 ND 01/27/98
Hexachlorocyclopentadiene ug/L 10 ND 01/27/98
2,4,6-Trichlorophenol ug/L 5.0 ND 01/27/98 .
2-Chloronaphthalene ug/L 5.0 ND 01/27/98
Acenaphthylene ug/L 5.0 ND 01 /27/98
Dimethyl phthalate ug/L 5.0 ND 01/27/98
2,6-Dinitrotoluene ug/L 5.0 ND 01/27/98
Acenaphthene ug/L 5.0 ND 01/27/98
2,4-Dinitrophenol ug/L 25 ND 01/27/98
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 . REPORT OF LABORATORY ANALYSIS KY g Water 90090
UST List
Drinking Water 37706 TN UST
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
• Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 4 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001303
Date Collected: 01 /21/98
Date Received: 01/21/98
Client Sample ID: WW1
Parameter units PRI METHOD DATE ANAIY7FR
ORGANIC ANAI YSIS
BASE/NEUTRALS AND ACIDS 625
2,4-Dinitrotoluene ug/L 5.0 ND 01/27/98
4-Nitrophenol ug/L 25 ND 01 /27/98
Fluorene ug/L 5.0 ND 01/27/98
4-Chlorophenyl phenyl ether ug/L 5.0 ND 01/27/98
Diethyl phthalate ug/L 5.0 ND 01/27/98
2-Methyl-4,6-dinitrophenol ug/L 25 ND 01 /27/98
N-Nitrosodiphenylamine ug/L 5.0 ND 01/27/98
4-Bromophenyl phenyl ether ug/L 5.0 ND 01/27/98
Hexachlorobenzene ug/L 5.0 ND 01/27/98
Pentachlorophenol ug/L 25 ND 01/27/98
Phenanthrene ug/L 5.0 ND 01/27/98
Anthracene ug/L 5.0 ND 01 /27/98
Di-n-butyl phthalate ug/L 5.0 ND 01/27/98
Fluoranthene ug/L 5.0 ND 01 /27/98
Benzidine ug/L 50 ND 01/27/98
Pyrene ug/L 5.0 ND 01/27/98
Benzyl butyl phthalate ug/L 5.0 ND 01/27/98
3,3-Dichlorobenzidine ug/L 10 ND 01/27/98
Benz[a]anthracene , ug/L 5.0 ND 01/27/98
Chrysene ug/L 5.0 ND 01/27/98
bis(2-Ethylhexyl )phthalate ug/L 5.0 ND 01/27/98
Di-n-octylphthalate ug/L 5.0 ND 01/27/98
Benzo[b]fluoranthene ug/L 5.0 ND 01/27/98
Benzo[k]fluoranthene ug/L 5.0 ND 01/27/98
Benzo[a]pyrene ug/L 5.0 ND 01 /27/98
Indeno[1 ,2,3-cd]pyrene ug/L 5.0 ND 01/27/98
Dibenz[a,h]anthracene ug/L 5.0 ND 01/27/98
Benzo[g,h,i]perylene ug/L 5.0 ND 01/27/98
Surrogate - 2-Fluorophenol % 18 01/27/98
Surrogate - Phenol-d5 % 13 01/27/98
Surrogate - Nitrobenzene-d5 % 55 01/27/98
Laboratory Certification IDs Laboratory Certification IDs
NC Winking r 12 REPORT 'JrLABORATORY ANALYSIS TN Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 5 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001303
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: MW1
Parameter Units PRL METHOD DATE ANAIY7ED
ORGANIC ANAI YSTS
BASE/NEUTRALS AND ACIDS 625
Surrogate - 2-Fluorobiphenyl % 50 01 /27/98
Surrogate - 2,4,6-Tribromophenol % 80 01 /27/98
Surrogate - Terphenyl-d14 % 94 01/27/98
Date Extracted, Base/Neutrals and Acids Date 012298 01/22/98
•
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinking ater Water 37706 REPORT OF LABORATORY ANALYSIS TN Drinking
ST° s Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 6 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001311
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: MW2
Parameter units PRL METHOD DATF ANAI Y7FI)
FIELD ANAIYSTS
GROUND WATER FIELD PARAMETERS
pH (Field) Units 6.03 01/21/98
Specific Conductivity(Field) umhos/cm2 10 319 01/21/98
Static Water Level (Depth) feet 0.01 16.67 01/21/98
Temperature (Field) Degrees C 14.0 01/21/98
Volume Prepumped Gallons 0. 1 6.0 01 /21/98
INORGANIC ANAIYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand mg/L 25 ND 5220 D 01 /22/98
Chloride mg/L 1 71 325.3 01/23/98
Chromium mg/L 0.010 ND 200.7 01/29/98
Copper mg/L 0.010 0.012 200.7 01/29/98
Lead mg/L 0.005 ND 239.2 01 /28/98
Oil & Grease mg/L 1 ND 5520 B 01 /28/98
Phenol , Low Level mg/L 0.005 ND 420. 1 02/02/98
Solids, Total Dissolved mg/L 1 260 2540 C 01/26/98
Solids, Total Suspended mg/L 1 37 2540 D 01/22/98
Sulfate mg/L 25 40 375.4 01/28/98
Total Organic Carbon mg/L 0.5 5.2 5310C 01/30/98
Zinc mg/L 0.010 0.011 200.7 01/29/98
GROUND WATER FIELD PARAMETERS
Odor NONE • 01/21/98
Appearance TURBID 01/21/98
f)RGANIC ANAI YSTS
VOLATILE ORGANICS 624
Chloromethane ug/L 5.0 ND 01/22/98
Chloroethene (Vinyl chloride) ug/L 5.0 ND 01/22/98
Bromomethane ug/L 5.0 ND 01/22/98
Chloroethane ug/L 5.0 ND 01/22/98
Trichlorofluoromethane ug/L 5.0 ND 01/22/98
1 ,1-Dichloroethene ug/L 5.0 ND 01/22/98
Laboratory Certification IDs Laboratory Certification IDs
NC Winking Water
12 REPORT OF LABORATORY ANALYSIS TN
Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace/Analytical Huntersville,NC 28078
Tel:[phone]
•
Fax:[phone]
Mr. Bobby Lamb i February 04, 1998
Page 7 PACE Project Number: 680120580
Client 'eference: Monitjring Wells
PACE Sa ple Number: 92 0001311
Date Collected: 01/21/98
Date Re eived: '. 01/21/98
Client 'ample ID: I MW2
. n a i Units PRL I4FTHOD PATF ANAIY7ED
s
VOLATILE ORGANICS ! 624
Dichlor. ethane ug/L 5.0 ND 01/22/98
trans-1 ,2-Dichloroethen'e ug/L 5.0 ND 01/22/98
1 ,1-Dichloroethane ug/L 5.0 ND 01 /22/98
cis-1 ,2-1Dichloroethene ; • ug/L 5.0 ND 01 /22/98
ChlorofCrm . ug/L 5.0 ND 01/22/98
1 ,1 ,1-Trichloroethane ug/L 5.0 ND 01/22/98
1 ,2-Dic loroethane ug/L 5.0 ND 01/22/98
Carbon tetrachloride ug/L 5.0 ND 01/22/98
Benzene ' ug/L 5.0 ND 01/22/98
Trichlorfoethene ug/L 5.0 ND 01/22/98
1 ,2-Dic loropropane i , ug/L 5.0 ND 01/22/98
Bromodidhloromethane ug/L 5.0 ND 01/22/98
2-Chlordethoxyethene ug/L 10 ND 01/22/98
cis-1 ,34Dichloropropene ug/L 5.0 ND 01/22/98
Toluene ug/L 5.0 ND 01/22/98
trans-1 3-Dichloropropene • ug/L 5.0 ND 01/22/98
1 ,1 ,2-Tdichloroethane i ug/L 5.0 ND 01/22/98
Dibromo hloromethane ug/L 5.0 ND 01/22/98
Tetrach oroethene , ug/L 5.0 ND 01/22/98
Chlorob nzene 1 i ug/L 5.0 ND 01/22/98
EthylbOzene ug/L 5.0 ND 01/22/98
Bromoform j ug/L 5.0 ND 01/22/98
1 ,1 ,2,2-Tetrachloroethane ug/L 5.0 ND 01/22/98
1 ,3-Dichlorobenzene ug/L 5.0 ND 01/22/98
i
1 ,4-Dichlorobenzene ? ug/L 5.0 ND 01/22/98
1 ,2-Dichlorobenzene I ug/L 5.0 ND 01/22/98
Surroga e - Dibromoflubromethane % 104 01/22/98
Surroga e - Toluene-d8 % 102 01/22/98
Surroga e - Bromofluorbbenzene % 99 01/22/98
BASE/NE TRALS AND ACIDS 1 625
N-Nitro odimethylaminei , ug/L 5.0 ND 01/27/98
i
:.. .,•.. :.ill .c.I ■
NC Wastewat r 12 s � Laboratory Certification Ds
NC Drinking ater 37706 REPORT OF LABORATORY ANALYSIS TN Drinking water 90090
Sc 99006 : TN UST List
This report shall not be reproduced,except in full, VA Drinking Water 213
f without the written consent of Pace Analytical Services,Inc.

I
i Pace Analytical Services,Inc.
i. 9800 Kincey Avenue,Suite 100
Pace A naly4cal Huntersville,NC 28078
Tel:[phone]
I i
Fax:[phone]
1
Mr. Bobby La ib February 04, 1998
P.ge 8 1 PACE Project Number: 680120580
Client Reference: Morjitoring Wells
i
P' E Sample Number: 92 0001311
Date Collected: 01/21/98
Daite Received: 01/21/98
Client Sample ID: MW2
Units PRI METHOD J)ATF ANAI YZED
1
1
BA, E/NEUTRALS AND ACIDS 625
bijs(2-Chloroethyl )ether ug/L 5.0 ND 01/27/98
Phenol I ug/L 5.0 ND 01/27/98
2-Chlorophenol i ug/L 5.0 ND 01/27/98
1 ,3-Dichlorobenzene ug/L 5.0 ND 01/27/98
1 ,'4-Dichlorobenzene : ug/L 5.0 ND 01 /27/98
1 ,2-Dichlorobenzene ug/L 5.0 ND . 01 /27/98
bis(2-Chloroisopropyl)ether ug/L 5.0 ND 01 /27/98
Hexachloroethane ug/L 5.0 ND 01/27/98
N,Nitrosodi-n-propylamine ug/L 5.0 ND 01/27/98
Niitrobenzene; ug/L 5.0 ND 01/27/98
3J5,5-Trimethyl-2-cy4lohexen-l-one ug/L 5.0 ND 01/27/98
2HNitrophenol ug/L 5.0 ND 01/27/98
i
2j4-Dimethylphenol ug/L 5.0 ND 01/27/98
bijs(2-Chloroethoxy)methane ug/L 5.0 ND 01/27/98
24-Dichlorophenol ug/L 5.0 ND 01/27/98
l ,:,2,4-Trichlprobenze6e ug/L 5.0 ND 01/27/98
Naphthalene i ug/L 5.0 ND 01/27/98
Hexachlorobutadiene ug/L 5.0 ND 01/27/98
4-Chloro-3-methylphertol ug/L 5.0 ND 01/27/98
H 'xachlorocyclopentadiene ug/L 10 ND 01/27/98
2,4,6-Trichlorophenol ug/L 5.0 ND 01/27/98
21Chloronaphthalene ! ug/L 5.0 ND 01/27/98
Aenaphthylene I ug/L 5.0 ND 01/27/98
Dimethyl phthalate ug/L 5.0 ND 01/27/98
2,6-Dinitrotoluene ug/L 5.0 ND 01/27/98
A enaphthene' ug/L 5.0 ND 01/27/98
2 ;4-Dinitrophenol ug/L 25 ND • 01/27/98
2j4-Dinitrotoluene ! ug/L 5.0 ND 01/27/98
4 Nitropheno1 ug/L 25 ND 01/27/98
Fluorene ug/L 5.0 ND 01/27/98
4-Chlorophen0 phenyl ether ug/L 5.0 ND 01/27/98
LabOratory Certification IDs ` Laboratory Certification IDs
NC Winking Water
37 ! REPORT OF LABORATORY ANALYSIS TN UST water 90090
NC Drinking Water �7706 Ust
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

1 Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Aialytical Huntersville,NC 28078
Tel:[phone]
•
Fax:[phone]
I
Mr. Bobby Lamb February 04, 1998
Page 9 I i PACE Project Number: 680120580
Client Reference: Monitoring Wells
I l
PACE Sample Number: 92 0001311
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample! ID: MW2
Parameter tlnitc PRI METHOD DATE ANALY7FD
I
ORGANIC ANAIYSIS
BASE/NEUTRAL AND ACIDS 625
Diethyl phth late ug/L 5.0 ND 01/27/98
2-Methyl-4,6-dinitrophenol ug/L 25 ND 01 /27/98
N-Nitrosodiph;enylamine ug/L 5.0 ND 01/27/98
4-Bromophenyll phenyl ether ug/L 5.0 ND 01 /27/98
Hexachlorobenzene ug/L 5.0 ND 01/27/98
Pentachlorophenol ug/L 25 ND 01/27/98
Phenanthrene ug/L 5.0 ND 01/27/98
Anthracene ug/L 5.0 ND 01/27/98
Di-n-butyl phthalate ug/L 5.0 ND 01/27/98
Fluoranthene ug/L 5.0 ND 01/27/98
Benzidine ug/L 50 ND 01 /27/98
Pyrene ug/L 5.0 ND 01 /27/98
Benzyl butyl phthalate ug/L 5.0 ND 01/27/98
3,3-Dichlorobenzidine ug/L 10 ND 01/27/98
Benz[a]anthracene ug/L 5.0 ND 01/27/98
Chrysene ug/L 5.0 ND 01/27/98
bis(2-Ethylhexyl)phthalate ug/L 5.0 ND 01/27/98
Di-n-octylphthalate ug/L 5.0 ND 01/27/98
Benzo[b]fluoranthene ug/L 5.0 ND 01/27/98
Benzo[k]fluoranthene ug/L 5.0 ND 01/27/98
Benzo[a]pyrene ug/L 5.0 ND 01/27/98
Indeno[1,2,3-cd]pyrene ug/L 5.0 ND 01/27/98
Dibenz[a,h]anthracene ug/L 5.0 ND 01/27/98
Benzo[g,h,i ]perylene ug/L 5.0 ND 01/27/98
Surrogate - 2-Fluorophenol % 26 01/27/98
Surrogate - Phenol-d5 % 20 01/27/98
Surrogate - Nitrobenzene-d5 % 61 01/27/98
Surrogate - 2-Fluorobiphenyl % 55 01 /27/98
Surrogate - 2,4,6-Tribromophenol % 79 01/27/98
Surrogate - Terphenyl-d14 % 96 01/27/98
Date Extracted, Base/Neutrals and Acids Date 012298 01/22/98
Laboratory Certification IDs Laboratory Certification IDs
NC KY Drinkin
NC Drinking Water ewater 37706 REPORT OF LABORATORY ANALYSIS TN UST List Water 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 10 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001320
Date Collected: 01/21/98
Date Received: 01 /21 /98
Client Sample ID: MW3
ParamPtPr Units PRL METHOD DATE ANALYZED
FTFI D ANAI YSIS
GROUND WATER FIELD PARAMETERS
pH (Field) Units 6.52 01/21 /98
Specific Conductivity(Field) umhos/cm2 10 918 01/21 /98
Static Water Level (Depth) feet 0.01 14.47 01/21 /98
Temperature (Field) Degrees C 11 .6 01/21 /98
Volume Prepumped Gallons 0. 1 9.0 01/21 /98
INORGANIC ANAIYSTS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand mg/L 125 140 5220 D 01/22/98
Chloride mg/L 1 200 325.3 01/23/98
Chromium mg/L 0.010 0.011 200.7 01/29/98
Copper mg/L 0.010 0.25 200.7 01 /29/98
Lead mg/L 0.005 0.007 239.2 01/28/98
Oil & Grease mg/L 1 ND 5520 B 01/28/98
Phenol , Low Level mg/L 0.010 0.056 420.1 02/02/98
Solids, Total Dissolved mg/L 1 840 2540 C 01/26/98
Solids, Total Suspended mg/L 1 350 2540 D 01/22/98
Sulfate mg/L 100 150 375.4 01/28/98
Total Organic Carbon mg/L 1 .0 45 5310C 01/30/98
Zinc mg/L 0.010 0.10 200.7 01/29/98
GROUND WATER FIELD PARAMETERS
Odor CHEMICAL 01 /21/98
Appearance DARK BROWN 01/21/98
ORGANIC ANAIYSTS
VOLATILE ORGANICS SF 624
Chloromethane ug/L 50 ND 01/23/98
Chloroethene (Vinyl chloride) ug/L 50 ND 01/23/98
Bromomethane ug/L 50 ND 01/23/98
Chloroethane ug/L 50 ND 01/23/98
Trichlorofluoromethane ug/L 50 ND 01/23/98
1 ,1-Dichloroethene ug/L 50 ND 01/23/98
Laboratory Certification IDg Laboratory Certification Ds
NC NC Drink ng Water ewater 37706 REPORT OF LABORATORY ANALYSIS TN Drinking t 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
• Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 11 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001320
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: MW3
Parameter Units PRI MFTHOD DATF ANAIY7F1
ORGANIC ANAI YSIS
VOLATILE ORGANICS SF 624
Dichloromethane ug/L 50 ND 01 /23/98
trans-1 ,2-Dichloroethene ug/L 50 ND 01/23/98
1 ,1-Dichloroethane ug/L 50 ND 01 /23/98
cis-1 ,2-Dichloroethene ug/L 50 ND 01 /23/98
Chloroform ug/L 50 ND 01 /23/98
1 ,1 ,1-Trichloroethane ug/L 50 ND 01/23/98
1 ,2-Dichloroethane ug/L 50 ND 01 /23/98
Carbon tetrachloride ug/L 50 ND 01 /23/98
Benzene ug/L 50 ND 01 /23/98
Trichloroethene ug/L 50 ND 01/23/98
1 ,2-Dichloropropane ug/L 50 ND 01 /23/98
Bromodichloromethane ug/L 50 ND 01/23/98
2-Chloroethoxyethene ug/L 100 ND 01/23/98
cis-1 ,3-Dichloropropene ug/L 50 ND 01/23/98
Toluene ug/L 50 ND 01/23/98
trans-1 ,3-Dichloropropene ug/L 50 ND 01 /23/98
1 ,1 ,2-Trichloroethane ug/L 50 ND 01/23/98
Dibromochloromethane ug/L 50 ND 01/23/98
Tetrachloroethene , ug/L 50 ND 01/23/98
Chlorobenzene ug/L 50 ND 01/23/98
Ethylbenzene ug/L 50 ND 01/23/98
Bromoform ug/L 50 ND 01 /23/98
1 ,1 ,2,2-Tetrachloroethane ug/L 50 ND 01/23/98
1 ,3-Dichlorobenzene ug/L 50 ND 01/23/98
1 ,4-Dichlorobenzene ug/L 50 ND -. 01/23/98
1 ,2-Dichlorobenzene ug/L 50 ND 01/23/98
Surrogate - Dibromofluoromethane % 101 01 /23/98
Surrogate - Toluene-d8 % 106 01/23/98
Surrogate - Bromofluorobenzene % 97 01/23/98
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinkiewater ng ng Water 37706 REPORT OF LABORATORY ANALYSIS KY DrinkingSTU Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
, Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 12 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001320
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: MW3
Parampter Units. PRL METHOD PATF ANALYZED
ORGANIC ANAIYSIS
BASE/NEUTRALS AND ACIDS (1 ) 625
N-Nitrosodimethylamine ug/L 5.0 ND 01/27/98
bis(2-Chloroethyl )ether ug/L 5.0 ND 01/27/98
Phenol ug/L 5.0 ND 01 /27/98
2-Chlorophenol ug/L 5.0 ND 01 /27/98
1 ,3-Dichlorobenzene ug/L 5.0 ND 01 /27/98
1 ,4-Dichlorobenzene ug/L 5.0 ND 01 /27/98
1 ,2-Dichlorobenzene ug/L 5.0 ND 01/27/98
bis(2-Chloroisopropyl )ether ug/L 5.0 ND 01/27/98
Hexachloroethane ug/L 5.0 ND 01 /27/98
N-Nitrosodi-n-propylamine ug/L 5.0 ND 01 /27/98
Nitrobenzene ug/L 5.0 ND 01/27/98
3,5,5-Trimethyl-2-cyclohexen-l-one ug/L 5.0 ND 01/27/98
2-Nitrophenol ug/L 5.0 ND 01 /27/98
2,4-Dimethylphenol ug/L 5.0 ND 01 /27/98
bis(2-Chloroethoxy)methane ug/L 5.0 ND 01/27/98
2,4-Dichlorophenol ug/L 5.0 ND 01/27/98
1 ,2,4-Trichlorobenzene ug/L 5.0 ND 01/27/98
Naphthalene ug/L 5.0 ND 01/27/98
Hexachlorobutadien,e ug/L 5.0 ND 01/27/98
4-Chloro-3-methylphenol ug/L 5.0 ND 01/27/98
Hexachlorocyclopentadiene ug/L 10 ND 01 /27/98
2,4,6-Trichlorophenol ug/L 5.0 ND 01/27/98
2-Chloronaphthalene ug/L 5.0 ND 01/27/98
Acenaphthylene ug/L 5.0 ND 01/27/98
Dimethyl phthalate ug/L 5.0 ND 01/27/98
•
2,6-Dinitrotoluene ug/L 5.0 ND 01/27/98
Acenaphthene ug/L 5.0 ND 01 /27/98
2,4-Dinitrophenol ug/L 25 ND 01/27/98
2,4-Dinitrotoluene ug/L 5.0 ND 01/27/98
4-Nitrophenol ug/L 25 ND 01/27/98
Fluorene ug/L 5.0 ND 01/27/98
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinking ter 37706 REPORT OF LABORATORY ANALYSIS TN UUSnTk Ust
i ICY Water 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 13 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001320
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: MW3
ParamPtPr linitc PRI METHOD DATE ANALY7Ff)
ORGANIC ANAI YSTT
BASE/NEUTRALS AND ACIDS (1 ) 625
4-Chlorophenyl phenyl ether ug/L 5.0 ND 01/27/98
Diethyl phthalate ug/L 5.0 ND 01/27/98
2-Methyl-4,6-dinitrophenol ug/L 25 ND 01 /27/98
N-Nitrosodiphenylamine ug/L 5.0 ND 01 /27/98
4-Bromophenyl phenyl ether ug/L 5.0 ND 01 /27/98
Hexachlorobenzene ug/L 5.0 ND 01 /27/98
Pentachlorophenol ug/L 25 ND 01/27/98
Phenanthrene ug/L 5.0 ND 01/27/98
Anthracene ug/L 5.0 ND 01/27/98
Di-n-butyl phthalate ug/L 5.0 ND 01 /27/98
Fluoranthene ug/L 5.0 ND 01 /27/98
Benzidine ug/L 50 ND 01/27/98
Pyrene ug/L 5.0 ND 01/27/98
Benzyl butyl phthalate ug/L 5.0 ND 01 /27/98
3,3-Dichlorobenzidine ug/L 10 ND 01/27/98
Benz[a]anthracene ug/L 5.0 ND 01/27/98
Chrysene ug/L 5.0 ND 01 /27/98
bis(2-Ethylhexyl )phthalate ug/L 5.0 ND 01/27/98
Di-n-octylphthalabe ug/L 5.0 ND 01/27/98
Benzo[b]fluoranthene ug/L 5.0 ND 01/27/98
Benzo[k]fluoranthene ug/L 5.0 ND 01/27/98
Benzo[a]pyrene ug/L 5.0 ND 01/27/98
Indeno[1 ,2,3-cdlpyrene ug/L 5.0 ND 01/27/98
Dibenz[a,h]anthracene ug/L 5.0 ND 01/27/98
Benzo[g,h,i]perylene ug/L 5.0 ND 01/27/98
Surrogate - 2-Fluorophenol % 20 01/27/98
Surrogate - Phenol-d5 % 15 01/27/98
Surrogate - Nitrobenzene-d5 % 40 01/27/98
Surrogate - 2-Fluorobiphenyl % 25 01/27/98
Surrogate - 2,4,6-Tribromophenol % 51 01/27/98
Surrogate - Terphenyl-d14 % 42 01/27/98
Laboratory Certification IDs Laboratory Certification IDs
NC VVastewater 12 KYNC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN UST Ust
Drinking Water 90090
TNst
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 14 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001320
Date Collected: 01/21 /98
Date Received: 01/21/98
Client Sample ID: MW3
Parameter jlnitc PRI METHOD DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS AND ACIDS (1 ) 625
Date Extracted, Base/Neutrals and Acids Date 012298 01/22/98
Laboratory Certification IDs Laboratory Certification IDs
NC KY Drinkin
NC Dank g Water tewater 37706 REPORT OF LABORATORY ANALYSIS TN UST List Water 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services,Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 15 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001338
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: Eq Blank
Parameter Units PRL METHOD fATF ANAIYZFD
fR(;ANTC ANAI YSIS
VOLATILE ORGANICS 624
Chloromethane ug/L 5.0 ND 01/23/98
Chloroethene (Vinyl chloride) ug/L 5.0 ND 01/23/98
Bromomethane ug/L 5.0 ND 01 /23/98
Chloroethane ug/L 5.0 ND 01 /23/98
Trichlorofluoromethane ug/L 5.0 ND 01 /23/98
1 ,1-Dichloroethene ug/L 5.0 ND 01/23/98
Dichloromethane ug/L 5.0 ND 01 /23/98
trans-1 ,2-Dichloroethene ug/L 5.0 ND 01 /23/98
1 ,1-Dichloroethane ug/L 5.0 ND 01/23/98
cis-1 ,2-Dichloroethene ug/L 5.0 ND 01 /23/98
Chloroform ug/L 5.0 ND 01 /23/98
l ,l ,l-Trichloroethane ug/L 5.0 ND 01/23/98
1 ,2-Dichloroethane ug/L 5.0 ND 01 /23/98
Carbon tetrachloride ug/L 5.0 ND 01/23/98
Benzene ug/L 5.0 ND 01/23/98
Trichloroethene ug/L 5.0 ND 01/23/98
1 ,2-Dichloropropane ug/L 5.0 ND 01/23/98
Bromodichloromethane ug/L 5.0 ND 01/23/98
2-Chloroethoxyethene ug/L 10 ND 01/23/98
cis-1 ,3-Dichloropropene ug/L 5.0 ND 01/23/98
Toluene ug/L 5.0 ND 01/23/98
trans-1 ,3-Dichloropropene ug/L 5.0 ND 01/23/98
1 ,1 ,2-Trichloroethane ug/L 5.0 ND 01/23/98
Dibromochloromethane ug/L 5.0 ND 01/23/98
Tetrachloroethene ug/L 5.0 ND 01/23/98
Chlorobenzene ug/L 5.0 ND 01/23/98
Ethylbenzene ug/L 5.0 ND 01/23/98
Bromoform ug/L 5.0 ND 01/23/98
1 ,1 ,2,2-Tetrachloroethane ug/L 5.0 ND 01/23/98
1 ,3-Dichlorobenzene ug/L 5.0 ND 01/23/98
1 ,4-Dichlorobenzene ug/L 5.0 ND 01/23/98
Laboratory Certification IDa Laboratory Certification IDs
NC Winking Water
12 REPORT OF LABORATORY ANALYSIS TN U water 90090
NC Drinking Water 37706 List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 16 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001338
Date Collected: 01/21/98
Date Received: 01 /21 /98
Client Sample ID: Eq Blank
Parameter Units PRI METHOD DATE ANAIY7ED
ORGANIC ANAI YSTS
VOLATILE ORGANICS 624
1 ,2-Dichlorobenzene ug/L 5.0 ND 01/23/98
Surrogate - Dibromofluoromethane % 93 01/23/98
Surrogate - Toluene-d8 % 103 01 /23/98
Surrogate - Bromofluorobenzene % 97 01/23/98
•
)oratory Certification IDs Laboratory Certification IDs
NC Wastewater
Water 3706 REPORT OF LABORATORY ANALYSIS TN UST Lis KY Drinkin Water 90090
t
NC Drinking7
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 17 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001346
Date Collected: 01/21/98
Date Received: 01/21/98
Client Sample ID: Trip Blank
Parameter Units. PRL METHOD DATE ANALYZED
ORGANIC ANAI YSTS
VOLATILE ORGANICS 624
Chloromethane ug/L 5.0 ND 01/23/98
Chloroethene (Vinyl chloride) ug/L 5.0 ND 01/23/98
Bromomethane ug/L 5.0 ND 01 /23/98
Chloroethane ug/L 5.0 ND 01 /23/98
Trichlorofluoromethane ug/L 5.0 ND 01 /23/98
1 ,1-Dichloroethene ug/L 5.0 ND 01/23/98
Dichloromethane ug/L 5.0 5.0 PC 01/23/98
trans-1 ,2-Dichloroethene ug/L 5.0 ND 01/23/98
l ,l-Dichloroethane ug/L 5.0 ND 01/23/98
cis-1 ,2-Dichloroethene ug/L 5.0 ND 01/23/98
Chloroform ug/L 5.0 ND 01/23/98
1 ,1 ,1-Trichloroethane ug/L 5.0 ND 01/23/98
1 ,2-Dichloroethane ug/L 5.0 ND 01/23/98
Carbon tetrachloride ug/L 5.0 ND 01/23/98
Benzene ug/L 5.0 ND 01/23/98
Trichloroethene ug/L 5.0 ND 01/23/98
1 ,2-Dichloropropane ug/L 5.0 ND 01/23/98
Bromodichloromethane ug/L 5.0 ND 01 /23/98
2-Chloroethoxyethene ug/L 10 ND 01 /23/98
cis-1 ,3-Dichloropropene ug/L 5.0 ND 01/23/98
Toluene ug/L 5.0 ND 01/23/98
trans-1 ,3-Dichloropropene ug/L 5.0 ND 01/23/98
1 ,1 ,2-Trichloroethane ug/L 5.0 ND 01/23/98
Dibromochloromethane ug/L 5.0 ND 01/23/98
Tetrachloroethene ug/L 5.0 ND • 01/23/98
Chlorobenzene ug/L 5.0 ND 01/23/98
Ethylbenzene ug/L 5.0 ND 01/23/98
Bromoform ug/L 5.0 ND 01/23/98
1 ,1 ,2,2-Tetrachloroethane ug/L 5.0 ND 01/23/98
1 ,3-Dichlorobenzene ug/L 5.0 ND 01/23/98
1 ,4-Dichlorobenzene ug/L 5.0 ND 01/23/98
Laboratory Certification IDs Laboratory Certification IDs
NC Drinking Water r 37706 REPORT OF LABORATORY ANALYSIS TN UST List
` 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
• Fax:[phone]
Mr. Bobby Lamb February 04, 1998
Page 18 PACE Project Number: 680120580
Client Reference: Monitoring Wells
PACE Sample Number: 92 0001346
Date Collected: 01/21 /98
Date Received: 01/21/98
Client Sample ID: Trip Blank
Parameter Units PRI METHOD DATE ANALYZED
ORGANIC ANAI YSIS
VOLATILE ORGANICS 624
1 ,2-Dichlorobenzene ug/L 5.0 ND 01/23/98
Surrogate - Dibromofluoromethane % 103 01/23/98
Surrogate - Toluene-d8 7° 101 01 /23/98
Surrogate - Bromofluorobenzene % 107 01 /23/98
These data have been reviewed and are approved for release.
CAi
y Margaret S. Harding
Manager, Laboratory Operations
Laboratory Certification IDs Laboratory Certification IDs
NC Winking r 12 REPORT OF LABORATORY ANALYSIS TN UST Us Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
•
Fax:[phone]
Mr. Bobby Lamb FOOTNOTES February 04, 1998
Page 19 for pages 1 through 18 PACE Project Number: 680120580
Client Reference: Monitoring Wells
ND Not detected at or above the PRL.
PC Possible laboratory contaminant.
PRL PACE Reporting Limit
SF Elevated detection limit due to excessive sample foaming.
(1 ) Two surrogate recoveries low and slightly out of limits. Re-extraction
unusable do to a laboratory accident.
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 3770612 KY Drinking REPORT OF LABORATORY ANALYSIS TN UST List Water 90090
NC Drinking Water
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 20 PACE Project Number: 680120580
Client Reference: Monitoring Wells
Chemical Oxygen Demand
Batch: 92 68592
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units Ea Blank 920000242 92 0000242 Ref)
Chemical Oxygen Demand mg/L 25 ND
Chemical Oxygen Demand mg/L 50 810 820 1%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units ERL Valup Recv
Chemical Oxygen Demand mg/L 25 500 101%
Lgboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TN Us Water 90090
NC Drinking Water 37706 TN USTST U List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
•
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 21 PACE Project Number: 680120580
Client Reference: Monitoring Wells
Chloride
Batch: 92 68626
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units pa Blank 920000R97 92 0000R97 Ref)
Chloride mg/L 1 ND 380 380 0%
SPIKE:
Spike
Parameter jlnite 920000R97 Spike Rery
Chloride mg/L 1 380 100 90%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Rery
Chloride mg/L 1 20.0 99%
•
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drink ng Water tewater 37706 REPORT OF LABORATORY ANALYSIS TN UST Lis Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 22 PACE Project Number: 680120580
Client Reference: Monitoring Wells
Lead
Batch: 92 68773
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter linits E L Blank 920000897 92 0000897 RPf)
Lead mg/L 0.005 ND ND ND NC
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl
parameter Units RBL 920000R97 Spike Rery Rery Ref)
Lead mg/L 0.005 ND 0.025 109% 112% 3%
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter knits E L Value Rery Rery RPD
Lead mg/L 0.005 0.025 96% 105% 9%
Laboratory Certification IDs Laboratory Certification IDs
NC KY Drinkin
NC Drinking Water Watewater 37706 REPORT OF LABORATORY ANALYSIS TN UST List Water 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 23 PACE Project Number: 680120580
Client Reference: Monitoring Wells
Oil & Grease
Batch: 92 68792
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK:
Method
Parameter Unite PBL Blank
Oil & Grease mg/L 1 ND
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units ERL Value Rery
Oil & Grease mg/L 1 50.0 89%
•
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinking ater 12 Water 37706 REPORT OF LABORATORY ANALYSIS KYTNN Drinking Water 90090
UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
• Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 24 PACE Project Number: 680120580
Client Reference: Monitoring Wells
Solids, Total Dissolved
Batch: 92 68679
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920001311 of
Parameter Unite ERL Blank MW2 92 0001311 RED
Solids, Total Dissolved mg/L 1 ND 260 260 0%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Unitc EBL Value Recv
Solids , Total Dissolved mg/L 1 100 103%
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinkinter g NN USSTT List
37706 REPORT 'JrOF LABORATORY ANALYSIS 2 T U Water 90090
ist
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
•
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 25 PACE Project Number: 680120580
Client Reference: Monitoring Wells
Solids, Total Suspended
Batch: 92 68591
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units PRI Blank 920000900 92 0000900 RPD
Solids, Total Suspended mg/L 1 ND 14 17 19%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units EBL Value Rery
Solids, Total Suspended mg/L 1 100 93%
(,,oratory Certification IDs Laboratory Certification IDs
NC Winking r 2 REPORT OF LABORATORY ANALYSIS KY DrinkingST Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 26 PACE Project Number: 680120580
Client Reference: Monitoring Wells
Sulfate
Batch: 92 68809
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
parameter llnits ERL Blank 920001710 92 0001710 Ref)
Sulfate mg/L 10 ND
Sulfate mg/L 100 120 120 0%
SPIKE:
Spike
Parameter llnits ERL 920002377 Spike Rery
Sulfate mg/L 10 ND 20 104%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units 2BL Value Rery
Sulfate mg/L 10 20 97%
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drink ng Water ewater 37706 REPORT OF LABORATORY ANALYSIS TN UST Us Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 27 PACE Project Number: 680120580
Client Reference: Monitoring Wells
ICP QUALITY CONTROL
Batch: 92 68855
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units ERL Blank 920004744 92 0004744 RPI)
INDIVIDUAL PARAMETERS
Chromium mg/L 0.010 ND ND NC
Copper mg/L 0.010 0.015 0.016 6%
Lead mg/L 0. 10 ND ND NC
Nickel mg/L 0.05 ND ND NC
Zinc mg/L 0.010 0. 15 0. 15 0%
ICP QUALITY CONTROL
Cadmium mg/L 0.010 ND ND NC
Aluminum mg/L 0.10 ND
Antimony mg/L 0.20 ND
Arsenic mg/L 0.50 ND
Barium mg/L 0.010 ND
Beryllium mg/L 0.010 ND
Boron mg/L 0.10 ND
Cadmium mg/L 0.010 ND
Calcium mg/L 0.10 ND
Chromium mg/L 0.010 ND
Cobalt mg/L 0.010 ND
Copper mg/L 0.010 ND
Iron mg/L 0.050 ND
Lead mg/L 0. 10 ND
Magnesium mg/L 0.20 ND
Manganese mg/L 0.010 ND
Molybdenum mg/L 0.05 ND
Nickel mg/L 0.05 ND
Potassium mg/L 1 .0 ND
Selenium mg/L 0.50 ND
Silver mg/L 0.050 ND
Sodium mg/L 0.20 ND
Thallium mg/L 0.50 ND
Tin mg/L 0.20 ND
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinkingin ater Water 37706 REPORT OF LABORATORY ANALYSIS TN UST Us Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 28 PACE Project Number: 680120580
Client Reference: Monitoring Wells
ICP QUALITY CONTROL
Batch: 92 68855
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units PRI Blank 920004744 92 0004744 RPI)
Titanium mg/L 0.010 ND
Vanadium mg/L 0.010 ND
Zinc mg/L 0.010 ND
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl
Parameter Units 2.RL 920004744 Spike Rery Rery RPD
Aluminum mg/L 0. 10 0.63 50 92% 92% 0%
Antimony mg/L 0.20 ND 2.0 99% 99% 0%
Arsenic mg/L 0.50 ND 2.0 88% 90% 2%
Barium mg/L 0.010 0.25 1 .0 89% 89% 0%
Beryllium mg/L 0.010 ND 1 .0 93% 93% 0%
Boron mg/L 0. 10 0.39 1 .0 92% 91% 1%
Cadmium mg/L 0.010 ND 1 .0 90% 90% 0%
Calcium mg/L 0. 10 84 50 84% 84% 0%
Chromium mg/L 0.010 ND 1 .0 90% 91% 1%
Cobalt mg/L 0.010 0.017 1 .0 88% 88% 0%
Copper mg/L 0.010 0.015 1 .0 92% 93% 1%
Iron mg/L 0.050 1 .0 25 90% 90% 0%
Lead mg/L 0. 10 ND 2.0 88% 90% 2%
Magnesium mg/L 0.20 14 25 89% 89% 0%
Manganese mg/L 0.010 1 .3 1 .0 86% 87% 1%
Molybdenum mg/L 0.05 ND 1 .0 96% 94% 2%
Nickel mg/L 0.05 ND 1 .0 90% 91% 1%
Potassium mg/L 1 .0 7.7 50 87% 87% 0%
Selenium mg/L 0.50 ND 2.0 94% 94% 0%
Silver mg/L 0.050 ND 1 .0 68% 69% 1%
Sodium mg/L 0.20 17 50 90% 90% 0%
Thallium mg/L 0.50 ND . 2.0 85% 86% 1%
Tin mg/L 0.20 ND 1 .0 88% 88% 0%
Titanium mg/L 0.010 0.015 1 .0 95% 95% 0%
Laboratory Certification IDs Laboratory Certification IDs
NC NC Dunking Water 37706 REPORT OF LABORATORY ANALYSIS TN'UST Lewater 12 KY ist r 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 29 PACE Project Number: 680120580
Client Reference: Monitoring Wells
ICP QUALITY CONTROL
Batch: 92 68855
Samples: 92 0001303, 92 0001311 , 92 0001320
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl
Parameter Units Ea 920004744 Spike Rery Rery RFD
Vanadium mg/L 0.010 ND 1 .0 937° 937° 0%
Zinc mg/L 0.010 0.15 2.0 90% 907° 0%
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter Units. EU Value Rery Rery Ref)
Aluminum mg/L 0.10 50 97% 98% 1%
Antimony mg/L 0.20 2.0 102% 102% 0%
Arsenic mg/L 0.50 2.0 95% 96% 1%
Barium mg/L 0.010 1 .0 97% 97% 0%
Beryllium mg/L 0.010 1 .0 100% 100% 0%
Boron mg/L 0. 10 1 .0 98% 987° 0%
Cadmium mg/L 0.010 1 .0 98% 98% 07°
Calcium mg/L 0.10 50 98% 98% 0%
Chromium mg/L 0.010 1 .0 98% 98% 0%
Cobalt mg/L 0.010 1 .0 96% 967° 0%
Copper mg/L 0.010 1 .0 98% 99% 1%
Iron mg/L 0.050 25 97% 98% 1%
Lead mg/L 0. 10 2.0 97% 98% 1%
Magnesium mg/L 0.20 25 99% 100% 1%
Manganese mg/L 0.010 1 .0 97% 97% 0%
Molybdenum mg/L 0.05 1 .0 98% 987° 0%
Nickel mg/L 0.05 1 .0 96% 97% 1%
Potassium mg/L 1 .0 50 92% 98% 6%
Selenium mg/L 0.50 2.0 102% 100% 2%
Silver mg/L 0.050 1 .0 96% 95% 1%
Sodium mg/L 0.20 50 96% 100% 4%
Thallium mg/L 0.50 2.0 93% 94% 1%
Tin mg/L 0.20 1 .0 91% 95% 4%
Titanium mg/L 0.010 1 .0 99% 99% 0%
Vanadium mg/L 0.010 1 .0 100% 100% 0%
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinkinginater Water 37706 REPORT OF LABORATORY ANALYSIS TN UST Using Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 30 PACE Project Number: 680120580
Client Reference: Monitoring Wells
ICP QUALITY CONTROL
Batch: 92 68855
Samples: 92 0001303, 92 0001311 , 92 0001320
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter llnits per, Value Rery Rery RPn
Zinc mg/L 0.010 2.0 98% 98% 0%
•
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 2 REPORT OF LABORATORY ANALYSIS Drinking Water 90090
3 TN
NC Drinking Water 7706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 31 PACE Project Number: 680120580
Client Reference: Monitoring Wells
BASE/NEUTRALS AND ACIDS
Batch: 92 68768
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK:
Method
Parameter llnitc ERL Blank
N-Nitrosodimethylamine ug/L 5.0 ND
bis(2-Chloroethyl )ether ug/L 5.0 ND
Phenol ug/L 5.0 ND
2-Chlorophenol ug/L 5.0 ND
1 ,3-Dichlorobenzene ug/L 5.0 ND
1 ,4-Dichlorobenzene ug/L 5.0 ND
1 ,2-Dichlorobenzene ug/L 5.0 ND
bis(2-Chloroisopropyl )ether ug/L 5.0 ND
Hexachloroethane ug/L 5.0 ND
N-Nitrosodi-n-propylamine ug/L 5.0 ND
Nitrobenzene ug/L 5.0 ND
3,5,5-Trimethyl-2-cyclohexen-l-one ug/L 5.0 ND
2-Nitrophenol ug/L 5.0 ND
2,4-Dimethylphenol ug/L 5.0 ND
bis(2-Chloroethoxy)methane ug/L 5.0 ND
2,4-Dichlorophenol ug/L 5.0 ND
1 ,2,4-Trichlorobenzene ug/L 5.0 ND
Naphthalene ug/L 5.0 ND
Hexachlorobutadiene ug/L 5.0 ND
4-Chloro-3-methylphenol ug/L 5.0 ND
Hexachlorocyclopentadiene ug/L 10 ND
2,4,6-Trichlorophenol ug/L 5.0 ND
2-Chloronaphthalene ug/L 5.0 ND
Acenaphthylene ug/L 5.0 ND
Dimethyl phthalate ug/L 5.0 ND
2,6-Dinitrotoluene ug/L 5.0 ND
Acenaphthene ug/L 5.0 ND
2,4-Dinitrophenol ug/L •25 ND
2,4-Dinitrotoluene ug/L 5.0 ND
4-Nitrophenol ug/L 25 ND
Fluorene ug/L 5.0 ND
4-Chlorophenyl phenyl ether ug/L 5.0 ND
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinking Water ewater 37706 REPORT OF LABORATORY ANALYSIS TN UST Li Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 32 PACE Project Number: 680120580
Client Reference: Monitoring Wells
BASE/NEUTRALS AND ACIDS
Batch: 92 68768
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK:
Method
Parameter Units EEL Blank
Diethyl phthalate ug/L 5.0 ND
2-Methyl-4,6-dinitrophenol ug/L 25 ND
N-Nitrosodiphenylamine ug/L 5.0 ND
4-Bromophenyl phenyl ether ug/L 5.0 ND
Hexachlorobenzene ug/L 5.0 ND
Pentachlorophenol ug/L 25 ND
Phenanthrene ug/L 5.0 ND
Anthracene ug/L 5.0 ND
Di-n-butyl phthalate ug/L 5.0 ND
Fluoranthene ug/L 5.0 ND
Benzidine ug/L 50 ND
Pyrene ug/L 5.0 ND
Benzyl butyl phthalate ug/L 5.0 ND
3,3-Dichlorobenzidine ug/L 10 ND
Benz[a]anthracene ug/L 5.0 ND
Chrysene ug/L 5.0 ND
bis(2-Ethylhexyl )phthalate ug/L 5.0 ND
Di-n-octylphthalate ug/L 5.0 ND
Benzo[b]fluoranthene ug/L 5.0 ND
Benzo[klfluoranthene ug/L 5.0 ND
Benzo[a]pyrene ug/L 5.0 ND
Indeno[1 ,2,3-cdlpyrene ug/L 5.0 ND
Dibenz[a,h]anthracene ug/L 5.0 ND
Benzo[g,h,i ]perylene ug/L 5.0 ND
Surrogate - 2-Fluorophenol % 32
Surrogate - Phenol-d5 % 23 .
Surrogate - Nitrobenzene-d5 % 67
Surrogate - 2-Fluorobiphenyl % 58
Surrogate - 2,4,6-Tribromophenol % 86
Surrogate - Terphenyl-d14 % 90
•
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS TN Drinking Wate` 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 33 PACE Project Number: 680120580
Client Reference: Monitoring Wells
BASE/NEUTRALS AND ACIDS
Batch: 92 68768
Samples: 92 0001303, 92 0001311 , 92 0001320
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter Units .BL Value Rery RPry RPD
N-Nitrosodimethylamine ug/L 5.0 50 42% 36% 15%
bis(2-Chloroethyl )ether ug/L 5.0 50 62% 56% 10%
Phenol ug/L 5.0 50 28% 24% 15%
2-Chlorophenol ug/L 5.0 50 60% 54% 11%
1 ,3-Dichlorobenzene ug/L 5.0 50 60% 567° 7%
1 ,4-Dichlorobenzene ug/L 5.0 50 58% 52% 11%
1 ,2-Dichlorobenzene ug/L 5.0 50 56% 56% 0%
bis(2-Chloroisopropyl )ether ug/L 5.0 50 70% 64% 9%
Hexachloroethane ug/L 5.0 50 52% 50% 4%
N-Nitrosodi-n-propylamine ug/L 5.0 50 70% 62% 12%
Nitrobenzene ug/L 5.0 50 66% 60% 10%
3,5,5-Trimethyl-2-cyclohexen-l-one ug/L 5.0 50 64% 60% 6%
2-Nitrophenol ug/L 5.0 50 68% 62% 9%
2,4-Dimethylphenol ug/L 5.0 50 54% 64% 17%
bis(2-Chloroethoxy)methane ug/L 5.0 50 68% 60% 13%
2,4-Dichlorophenol ug/L 5.0 50 72% 64% 12%
1 ,2,4-Trichlorobenzene ug/L 5.0 50 68% 60% 13%
Naphthalene ug/L 5.0 50 72% 64% 12%
Hexachlorobutadiene ug/L 5.0 50 62% 54% 147°
4-Chloro-3-methylphenol ug/L 5.0 50 70% 66% 6%
Hexachlorocyclopentadiene ug/L 10 50 28% 26% 7%
2,4,6-Trichlorophenol ug/L 5.0 50 72% 66% 9%
2-Chloronaphthalene ug/L 5.0 50 74% 68% 8%
Acenaphthylene ug/L 5.0 50 70% 64% 9%
Dimethyl phthalate ug/L 5.0 50 78% 74% 5%
2,6-Dinitrotoluene ug/L 5.0 50 80% 74% 8%
Acenaphthene ug/L 5.0 50 76% 72% 5%
2,4-Dinitrophenol ug/L 25 50 42% 36% 15%
2,4-Dinitrotoluene ug/L 5.0 50 86% 72% 18%
4-Nitrophenol ug/L 25 50 34% 30% 13%
Fluorene ug/L 5.0 50 80% 72% 11%
4-Chlorophenyl phenyl ether ug/L 5.0 50 78% 74% 5%
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY N UST water 90090
NC Drinking Water 37706Ust
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 34 PACE Project Number: 680120580
Client Reference: Monitoring Wells
BASE/NEUTRALS AND ACIDS
Batch: 92 68768
Samples: 92 0001303, 92 0001311 , 92 0001320
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter units Pa Value Bery Rery RPf)
Diethyl phthalate ug/L 5.0 50 82% 72% 13%
2-Methyl-4,6-dinitrophenol ug/L 25 50 80% 72% 11%
N-Nitrosodiphenylamine ug/L 5.0 50 82% 78% 5%
4-Bromophenyl phenyl ether ug/L 5.0 50 94% 90% 4%
Hexachlorobenzene ug/L 5.0 50 84% 76% 10%
Pentachlorophenol ug/L 25 50 82% 78% 5%
Phenanthrene ug/L 5.0 50 80% 78% 3%
Anthracene ug/L 5.0 50 82% 78% 5%
Di-n-butyl phthalate ug/L 5.0 50 80% 76% 5%
Fluoranthene ug/L 5.0 50 80% 72% 11%
Benzidine ug/L 50 100 38% 25% 41%
Pyrene ug/L 5.0 50 94% 84% 11%
Benzyl butyl phthalate ug/L 5.0 50 88% 82% 7%
3,3-Dichlorobenzidine ug/L 10 100 94% 88% 7%
Benz[a]anthracene ug/L 5.0 50 86% 80% 7%
Chrysene ug/L 5.0 50 90% 84% 7%
bis(2-Ethylhexyl )phthalate ug/L 5.0 50 84% 78% 7%
Di-n-octylphthalate ug/L 5.0 50 80% 74% 8%
Benzo[b]fluoranthene ug/L 5.0 50 86% 72% 18%
Benzo[k]fluoranthene ug/L 5.0 50 76% 76% 0%
Benzo[a]pyrene ug/L 5.0 50 80% 76% 5%
Indeno[1 ,2,3-cd]pyrene ug/L 5.0 50 82% 76% 8%
Dibenz[a,h]anthracene ug/L 5.0 50 84% 76% 10%
Benzo[g,h,i ]perylene ug/L 5.0 50 80% 76% 5%
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drink ng Water tewater 37706 REPORT OF LABORATORY ANALYSIS m Drinking Lst r 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services,Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 35 PACE Project Number: 680120580
Client Reference: Monitoring Wells
VOLATILE ORGANICS
Batch: 92 68662
Samples: 92 0001303, 92 0001311 , 92 0001320, 92 0001338, 92 0001346
METHOD BLANK:
Method
Parameter llnitc p$L Blank
Chloromethane ug/L 5.0 ND
Chloroethene (Vinyl chloride) ug/L 5.0 ND
Bromomethane ug/L 5.0 ND
Chloroethane ug/L 5.0 ND
Trichlorofluoromethane ug/L 5.0 ND
1 ,1-Dichioroethene ug/L 5.0 ND
Dichloromethane ug/L 5.0 ND
trans-1 ,2-Dichloroethene ug/L 5.0 ND
1 ,1-Dichloroethane ug/L 5.0 ND
cis-1 ,2-Dichloroethene ug/L 5.0 ND
Chloroform ug/L 5.0 ND
1 ,1 ,1-Trichloroethane ug/L 5.0 ND
1 ,2-Dichloroethane ug/L 5.0 ND
Carbon tetrachloride ug/L 5.0 ND
Benzene ug/L 5.0 ND
Trichloroethene ug/L 5.0 ND
1 ,2-Dichloropropane ug/L 5.0 ND
Bromodichloromethane ug/L 5.0 ND
2-Chloroethoxyethene ug/L 10 ND
cis-1 ,3-Dichloropropene ug/L 5.0 ND
Toluene ug/L 5.0 ND
trans-1 ,3-Dichloropropene ug/L 5.0 ND
1 ,1 ,2-Trichloroethane ug/L 5.0 ND
Dibromochloromethane ug/L 5.0 ND
Tetrachloroethene ug/L 5.0 ND
Chlorobenzene ug/L 5.0 ND •
Ethylbenzene ug/L 5.0 ND
Bromoform ug/L 5.0 ND
1 ,1 ,2,2-Tetrachioroethane ug/L 5.0 ND
1 ,3-Dichlorobenzene ug/L 5.0 ND
1 ,4-Dichlorobenzene ug/L 5.0 ND
1 ,2-Dichlorobenzene ug/L 5.0 ND
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinking Water ewater 37706 REPORT 'Jr LABORATORY ANALYSIS TN UST LisstWater 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 36 PACE Project Number: 680120580
Client Reference: Monitoring Wells
VOLATILE ORGANICS
Batch: 92 68662
Samples: 92 0001303, 92 0001311 , 92 0001320, 92 0001338, 92 0001346
METHOD BLANK:
Method
Parameter llni tc EB,L Rlank
Surrogate - Dibromofluoromethane % 90
Surrogate - Toluene-d8 % 105
Surrogate - Bromofluorobenzene % 100
SPIKE AND SPIKE DUPLICATE:
Spike
920001303 Spike Dupl
Parameter Units .R.. MW1 Spike Rery Rery RED
Chloromethane ug/L 5.0 ND 20 140% 145% 4%
Chloroethene (Vinyl chloride) ug/L 5.0 ND 20 110% 110% 0%
Bromomethane ug/L 5.0 ND 20 95% 80% 17%
Chloroethane ug/L 5.0 ND 20 120% 105% 13%
Trichlorofluoromethane ug/L 5.0 ND 20 120% 110% 9%
1 ,1-Dichloroethene ug/L 5.0 ND 20 110% 105% 5%
Dichloromethane ug/L 5.0 ND 20 80% 80% 0%
trans-1 ,2-Dichloroethene ug/L 5.0 ND 20 105% 100% 5%
1 ,1-Dichloroethane ug/L 5.0 ND 20 105% 100% 5%
cis-1 ,2-Dichloroethene ug/L 5.0 ND 20 105% 95%° 10%
Chloroform ug/L 5.0 ND 20 110% 100% 10%
1 , 1 , 1-Trichloroethane ug/L 5.0 ND 20 105% 100% 5%
1 ,2-Dichloroethane ug/L 5.0 ND 20 110% 105% 5%
Carbon tetrachloride ug/L 5.0 ND 20 90%° 100% 11%
Benzene ug/L 5.0 ND 20 95% 100% 5%
Trichloroethene ug/L 5.0 ND 20 105% 110% 5%
1 ,2-Dichloropropane ug/L 5.0 ND 20 100% 105% 5%
Bromodichloromethane ug/L 5.0 ND 20 90% 95% 5%
cis-1 ,3-Dichloropropene ug/L 5.0 ND 20 100% 105% 5%
Toluene ug/L 5.0 ND 20 90% 100% 11%
trans-1 ,3-Dichloropropene ug/L 5.0 ND 20 95% 100% 5%
1 ,1 ,2-Trichloroethane ug/L 5.0 ND 20 85% 90% 6%
Dibromochloromethane ug/L 5.0 ND 20 85% 90% 6%
Tetrachloroethene ug/L 5.0 ND 20 100% 115% 14%
Chlorobenzene ug/L 5.0 ND 20 95% 100% 5%
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater
37706 REPORT OF LABORATORY ANALYSIS TN UST List Water 90090
KY Drinking
NC Drinking Water
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
. Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 37 PACE Project Number: 680120580
Client Reference: Monitoring Wells
VOLATILE ORGANICS
Batch: 92 68662
Samples: 92 0001303, 92 0001311 , 92 0001320, 92 0001338, 92 0001346
SPIKE AND SPIKE DUPLICATE:
Spike
920001303 Spike Dupl
Parameter Units al MW1 Spike Nary RPry Ref)
Ethylbenzene ug/L 5.0 ND 20 90% 100% 11%
Bromoform ug/L 5.0 ND 20 80% 95% 17%
1 ,1 ,2,2-Tetrachloroethane ug/L 5.0 ND 20 85% 100% 16%
1 ,3-Dichlorobenzene ug/L 5.0 ND 20 105% 115% 9%
1 ,4-Dichlorobenzene ug/L 5.0 ND 20 105% 115% 9%
1 ,2-Dichlorobenzene ug/L 5.0 ND 20 105% 110% 5%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units EL WW1 Rery
Chloromethane ug/L 5.0 20 90%
Chloroethene (Vinyl chloride) ug/L 5.0 20 95%
Bromomethane ug/L 5.0 20 100%
Chloroethane ug/L 5.0 20 110%
Trichlorofluoromethane ug/L 5.0 20 105%
1 ,1-Dichloroethene ug/L 5.0 20 105%
Dichloromethane ug/L 5.0 20 95%
trans-1 ,2-Dichloroethene ug/L 5.0 20 100%
1 ,1-Dichloroethane ug/L 5.0 20 100%
cis-1 ,2-Dichloroethene ug/L 5.0 20 100%
Chloroform ug/L 5.0 20 100%
1 ,1 ,1-Trichloroethane ug/L 5.0 20 95%
1 ,2-Dichloroethane ug/L 5.0 20 105%
Carbon tetrachloride ug/L 5.0 20 95%
Benzene ug/L 5.0 20 105%
Trichloroethene ug/L 5.0 20 110%
1 ,2-Dichloropropane ug/L 5.0 20 115%
Bromodichloromethane ug/L 5.0 • 20 100%
2-Chloroethoxyethene ug/L 10 40 48%
cis-1 ,3-Dichloropropene ug/L 5.0 20 115%
Toluene ug/L 5.0 20 100%
trans-1 ,3-Dichloropropene ug/L 5.0 . 20 110%
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinking Wastewater
37706 REPORT OF LABORATORY ANALYSIS TN UST Listwater 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA February 04, 1998
Page 38 PACE Project Number: 680120580
Client Reference: Monitoring Wells
VOLATILE ORGANICS
Batch: 92 68662
Samples: 92 0001303, 92 0001311 , 92 0001320, 92 0001338, 92 0001346
LABORATORY CONTROL SAMPLE:
Reference
ParamPtPr Jlnits .ERL ValnP RPry
1 ,1 ,2-Trichloroethane ug/L 5.0 20 100%
Dibromochloromethane ug/L 5.0 20 100%
Tetrachloroethene ug/L 5.0 20 110%
Chlorobenzene ug/L 5.0 20 105%
Ethylbenzene ug/L 5.0 20 100%
Bromoform ug/L 5.0 20 110%
1 ,1 ,2,2-Tetrachloroethane ug/L 5.0 20 100%
1 ,3-Dichlorobenzene ug/L 5.0 20 115%
1 ,4-Dichlorobenzene ug/L 5.0 20 110%
1 ,2-Dichlorobenzene ug/L 5.0 20 110%
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater
37706 REPORT OF LABO KY RATORY ANALYSIS TN UST Drinking 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb FOOTNOTES February 04, 1998
Page 39 for pages 20 through 38 PACE Project Number: 680120580
Client Reference: Monitoring Wells
NC No calculation due to value below detection limit.
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
RPD Relative Percent Difference
•
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater r 2 REPORT OF LABORATORY ANALYSIS TKYN Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

•
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PASI, Inc Charlotte February 03, 1998
9800 Kincey Avenue, Suite 100 PACE Project Number: 680120580
•Huntersville, NC 28078 NC Wastewater Lab Cert. #40
NC Drinkingwater Lab Cert. #37712
SC Lab Cert. #99030
Attn: Project Management
Client Reference: Crompton & Knowles
PACE Sample Number: 92 0001303
Date Collected: 01/21/98
Date Received: 01/23/98
Client Sample ID: MW1
Parameter Units PRl_ METHOD DATE ANAI Y7FI)
INORGANIC ANAIYSTS
INDIVIDUAL PARAMETERS
Phenol mg/L 0.005 ND 420. 1 01/27/98
Total Organic Carbon mg/L 0.5 0.73 5310C 01 /30/98
PACE Sample Number: 92 0001311
Date Collected: 01 /21/98
Date Received: 01 /23/98
Client Sample ID: MW2
Parameter Ifni is PRI METHOD DATE ANAI Y7FI
INORGANIC ANAIYSIS
INDIVIDUAL PARAMETERS
Phenol mg/L 0.005 ND 420.1 02/02/98
Total Organic Carbon mg/L 0.5 5.2 5310C 01/30/98

Project Management February 03, 1998
Page 2 PACE Project Number: 680120580
Client Reference: Crompton & Knowles
PACE Sample Number: 92 0001320
Date Collected: 01/21/98
Date Received: 01/23/98
Client Sample ID: MW3
Parameter Units PRL _ „ METHOD DATE ANAIY7ED
INORGANTC ANAIYSTS
INDIVIDUAL PARAMETERS
Phenol mg/L 0.010 0.056 420. 1 02/02/98
Total Organic Carbon mg/L 1 .0 45 5310C 01/30/98
These data have been reviewed and are approved for release.
Walter L. Miller
Operations Manager

Project Management FOOTNOTES February 03, 1998
Page 3 for pages 1 through 2 PACE Project Number: 680120580
Client Reference: Crompton & Knowles -
ND Not detected at or above the PRL.
PRL PACE Reporting Limit

Project Management QUALITY CONTROL DATA February 03, 1998
Page 4 PACE Project Number: 680120580
Client Reference: Crompton & Knowles
Phenol
Batch: 93 50387
Samples: 92 0001303
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
parameter Units PRI Blank 920000900 92 0000900 RPM
Phenol mg/L 0.005 ND 0.023 0.030 26%
SPIKE:
920001303 Spike
Parameter units EEL MW1 Spike Jery
Phenol mg/L 0.005 ND 0.025 92%
LABORATORY CONTROL SAMPLE:
Reference
Parameter llnits EBL Value Rery
Phenol mg/L 0.005 0.025 92%

Project Management QUALITY CONTROL DATA February 03, 1998
Page 5 PACE Project Number: 680120580
Client Reference: Crompton & Knowles
Phenol
Batch: 93 50562
Samples: 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920001311 of
Parameter llnitc BaL Blank MW? 92 0001311 RED
Phenol mg/L 0.005 ND ND ND NC
SPIKE:
920001320 Spike
Parameter !!nits EEL MW3 Spike Rery
Phenol mg/L 0.010 0.056
Phenol mg/L 0.025 0.025 120%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units Ea Value Rery
Phenol mg/L 0.005 0.025 92%

Project Management QUALITY CONTROL DATA February 03, 1998
Page 6 PACE Project Number: 680120580
Client Reference: Crompton & Knowles
Total Organic Carbon
Batch: 93 50540
Samples: 92 0001303, 92 0001311 , 92 0001320
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920001303 of
Parameter Units .ERL Rank MW1 92 0001301 RPD
Total Organic Carbon mg/L 0.5 ND 0.73 0.76 4%
SPIKE:
920001303 Spike
Parameter Units. p$L MW1 Spike Rery
Total Organic Carbon mg/L 0.5 0.73 2.00 110%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units. Pa Value Rery
Total Organic Carbon mg/L 0.5 5.000 102%

Project Management FOOTNOTES February 03, 1998
Page 7 for pages 4 through 6 PACE Project Number: 680120580
Client Reference: Crompton & Knowles
NC No calculation due to value below detection limit.
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
RPD Relative Percent Difference

Pace Analytical 385183
CHAIN-OF-CUSTODY RECORD
Analytical Request
r ,,, Turn around Time
Client C(0 re)04-0 rl :IS /1 ''( 1". 1 Report To: ;111,- /2.;0 f i/ L A- ,...2, Pace Client No. 6,/S/ 74'
0 24 Hours
Address /(7 0 ,L, ,a /2/4..•A,' .c fr"--"-}..1 Bill To: 0 48 Hours Pace Project Manager r I ! to
_ 0 3-5 Days
4,-...• ,' 74/i i i'V (..-- ..,, ,e'(;* P.O.#/Billing Reference 0 1 Week 2 Weeks Pace Project No. eoie 0 5.7v 0
/
,/ Ergormal 14 Days
Phone ( --fla q/ ,7 . 1 7 .t) -- (;' i A (i 6c Project Name/No. 47,1 ,-,, I/0,/,--fr A.-' 1'--C *Requested Due Date:
Sampled By(PRINT); ,---, u) ANALYSES ,
CC PRESERVATIVES
/ w REQUEST
/1' ,// 1 I ' '• ft)/ --' • i,...vi.,,.. i il",--, z
zt. a \ (,4- ,7 ki
Sampler Si9natyre f Date Sampled 1— > \ \ \ .
A5 K°4-t
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NO. ' . SAMPLE DESCRIPTION. z D 1 1 > Z z ), /Pi ‘.) REMARKS
1 ik) i f ',..; i)
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COOLER NOS. . BAILERS OUT/ ilTmEBMER I RELINQUISHED BY/AFFILIATION I DATE TIME I ACCEPTED BY/AFFILIATION I DATE TIME
DATE I SHIPMENT METHODRETURNED/DATE m
et4D 7F - ... j_ii K_ i '' i
--- -
e'
Additional Comments
--SAMPLE CONDITION
Temp: °C Received on Ice: Y IN Sealed Cooler: Y/(N ,) Samples Intact()/N pl-fL /z./
SEE REVERSE SIDE FOR INSTRUCTIONS

DIVISION OF WATER QUALITY-GROUNDWATER SECTION
GROUNDWATER QUALITY MONITORING: \\''` ' , P.O.BOX 29578
For additional forms RALEIGH,NC 27626-0578
COMPLIANCE REPORT FORM please write or call: [phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name Crompton & Knowles Colors Ineorporated Non-Discharge
,
Address 1602 North Main Strppt TYPE OF DISPOSAL OPERATION BEING MONITORELY 1 - ";`.
Lowell. N. C. 28098 County Gaston (REQUIRED)
Well Location Downgradient from Wastewater Treatment Plant ____X_ Lagoon Septic Tank/Drain Field
Well Identification Number MW-3 Well Depth 27.1 Ft. .
Well Diameter 2�—Sam le (Screened) Interval 1 (LPP)
Ft. To 22 1 Ft. Spray Field 'Subsurface�Low-f?[e��rg
p Piping
Depth to Water Level 18.80 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 1.5 ft. above land surface Other
Gallons of water pumped/bailed before sampling 4.0 Rotary Distributor
Field Analysis: pH 8.65 Specific Conductance 26800 uMhos Temp. 16.0 °C Odor ChemicaAppearance Black
Date Sample Collected 09-11-97 Date Lab Sample Analyzed 09-11-97 to 09-23-97
Laboratory Name Pace Analytical Certification No. 12
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD 5900 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA mg/I
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb- Lead o 007 , mg/I
Coliform: MF Total NA /100m Phosphorus: Total as P NA mg/ Zn - Zinc 0 20 mg/I
(Note:Use MPN method for highly turbid samples) Al -Aluminum NA mg/ Pesticides/Herbicides o ;_
Dissolved Solids: Total 22,000 mg/ Ba - Barium NA mg/ (Specify Compounds) r)
pH (when analyzed) NA units Ca - Calcium NA mg/ NA ug/I
TOC 2,900 mg/ Cd - Cadmium NA mg/ NA a' ._;; ug/I
Chloride 10.000 mg/ Chromium: Total 0.25 mg/ NA --) : ug/I
Arsenic NA mg/ Cu - Copper 3.1 mg/ Other (Specify Compounds and -
Grease and Oils 2.0 mg/ Fe - Iron NA mg/ Concentration units) r''
71
Hardness: Total NA mg/ Hg - Mercury NA mg/ T55 64'Q MG/L
Phenol 16.0 mg/ K - Potassium NA mg/ Benzene 48CP UG/L
Sulfate 990.0 mg/ Mg - Magnesium NA mg/ Phenol 3300 UG/L
Specific Conductance NA uMhos Mn - Manganese NA mg/ 1.7,4—Trirhlnrnhpnzpnp 77nn TTG/L
Total Ammonia NA mg/ Na - Sodium NA mg/ Bpnzid-i_np 2Rnn TTG/L
TKN as N NA mg/
I CE'MO HAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see#3 on back)
` iii /_ titiqt
* See back for instructions.
Signa ure of Permittee (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96 / .,y 9 ,

COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE#4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Metals Analyses: Use Standard Method 3030C for sample preparation(mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!!
Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
lab within 24 hours.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT ARE A PART.QE SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA-600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods,3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volumes ar&removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See#4. above)
10.The sample container should be labeled at the time of collection.with the facility.nam and,e,well identification number date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company,corporation, or governmental body to sign official documents.
L_ _ _
{ 9

DIVISION OF WATER QUALITY-GROUNDWATER SECTION
GROUNDWATER QUALITY MONITORING: P.O. BOX 29578
For additional forms RALEIGH,NC 27626-0578
COMPLIANCE REPORT FORM please write or call: [phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name Crompton & Knowl ea Col ors Tnrorpora tart Non-Discharge
Address 1602 North Main Street NPDES NC 0005274
Lowell. N.C. 28098 County Gaston TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Well Location Downgradient From Wastewater Treatment Plant N Lagoon Septic Tank/Drain Field
Well Identification Number MW-2 Well Depth 29.0 Ft. Spray Field Subsurface Low Pressure
Well Diameter 2" Sample (Screened) Interval 19.0 Ft. To 29.0 Ft. Piping(LPP)
Depth to Water Level 19.50 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 1.5 ft. above land surface Other
Gallons of water pumped/bailed before sampling 5.0 Rotary Distributor
Field Analysis: pH 6.16 Specific Conductance 616 uMhos Temp. 17.5 °C Odor None Appearance Turbid
Date Sample Collected 09-11-97 Date Lab Sample Analyzed 09-11-97 to 09-23-97
Laboratory Name Pace Analytical Certification No. 12
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD 40 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA mg/I
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb - Lead 0.014 -, mg/I
Coliform: MF Total NA /100m Phosphorus: Total as P NA mg/ Zn - Zinc 0.094 VD mg/I
(Note:Use MPN method for highly turbid samples) Al - Aluminum NA mg/ Pesticides/Herbicides
Dissolved Solids: Total 400 mg/ Ba - Barium NA mg/ (Specify Compounds) ` •
_4
pH (when analyzed) NA units Ca - Calcium NA mg/ NA — ` Ig/I
TOC 3.6 mg/ Cd - Cadmium NA mg/ NA cf/ g/1
Chloride 12 mg/ Chromium: Total 0.017 mg/ NA -o - Ugh
Arsenic NA mg/ Cu - Copper 0.12 mg/ Other (Specify Compounds and `
Grease and Oils 1 .o mg/ Fe - Iron NA mg/ Concentration units) .• -
Hardness: Total NA mg/ Hg - Mercury NA mg/ T55 4-s9l MG/L
Phenol <0.005 mg/ K - Potassium NA, mg/
Sulfate 28 mg/ Mg - Magnesium NA mg/
Specific Conductance NA uMhos Mn - Manganese NA mg/
Total Ammonia NA mg/ Na - Sodium NA mg/
TKN as N NA mg/
I CERAP HAT THIS R RT IS UE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see#3 on back)
►91 „ p� �j 7
lawn v cf/ 1-`61 / * See back for instructions.
Signa e o Permittee (or Authorized Agent) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE#4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!!
Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
lab within 24 hours.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) 1N THE •
GROUNDWATER, NOT THOSE THAT ARE A PART Q SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association,American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA-600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is .
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See#4. above)
10.The sample container should be labeled at the time of collection with the facility name,well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents.

• DIVISION OF WATER QUALITY-GROUNDWATER SECTION
GROUNDWATER QUALITY MONITORING: P.O. BOX 29578
For additional forms RALEIGH,NC 27626-0578
COMPLIANCE REPORT FORM please write or call: [phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name Crompton K Knowles Colors Tnr.o pn-i-.g ed Non-Discharge
Address 1602 North Main Street NPDES NC 0005274
TYPE OF DISPOSAL OPERATION BEING MONITORED
Lowell, N.C. MAR County Gaston (REQUIRED)
Well Location Upgradient from Wastewater Treatment- P1 ant X Lagoon Septic Tank/Drain Field
Well Identification Number MW-1 Well Depth 100 Ft.
Well Diameter 2" Sample (Screened) Interval 90 Ft. To 100 Ft. Spray Field Piping
ubngrfLPPLow Pressure
P 9( )
Depth to Water Level 83-19 ft. below measuring point (before sampling) Land Application of Sludge
Measuring point is 0 ft. above land surface Other
Gallons of water pumped/bailed before sampling 9.0 Rotary Distributor
Field Analysis: pH 6.67 Specific Conductance 197 uMhos Temp. 7n_8 °C Odor None Appearance Clear
Date Sample Collected 09-11-97 Date Lab Sample Analyzed 09-11-97 to 09-93-97
Laboratory Name Pace Analyt:ral Certification No. 12
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD 4 25 mg/ Nitrite (NO2) as N NA mg/ Ni - Nickel NA mg/I
Coliform: MF Fecal NA /100m Nitrate (NO3) as N NA mg/ Pb - Lead < 0.005 mg/I
Coliform: MF Total NA /100m Phosphorus: Total as P NA mg/ Zn - Zinc 0.033 mg/I
(Note:Use MPN method for highly turbid samples) Al - Aluminum NA mg/ Pesticides/Herbicides
Dissolved Solids: Total 150 mg/ Ba - Barium NA mg/ (Specify Compounds)
pH (when analyzed) NA units Ca - Calcium NA mg/ NA +—I .. ug/I
TOC 1.8 mg/ Cd - Cadmium NA mg/ NA C --:'' ug/I
Chloride 4.0 mg/ Chromium: Total 40.010 mg/ NA `-4 ) ug/I
Arsenic NA mg/ Cu - Copper 0.013 mg/ Other (Specify Compounds and LT
Grease and Oils -41.o mg/ Fe - Iron NA mg/ Concentration units) ,'
Hardness: Total NA mg/ Hg - Mercury NA mg/ -rr5 -L' 49. VGA
Phenol < 0.005 mg/ K- Potassium NA mg/ '
Sulfate 16.0 mg/ Mg - Magnesium NA mg/ 4- . =�
Specific Conductance NA uMhos Mn - Manganese NA mg/ --f
Total Ammonia NA mg/ Na - Sodium NA mg/
TKN as N NA mg/
I C Alp THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
WI
=� colloidal concentrations. (see#3 on back)
1110K�r %i,Lio lip 1 ( CQ K 7 * See back for instructions.
• r
Si•n. ure of Permittee (or Au orized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

T .
. _ .
COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI-
FIED FOR THE METHOD USED (SEE#4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!!
Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the
lab within 24 hours.
Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.
3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GROUNDWATER, NOT THOSE THAT ARE A PART Of SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
the following publications, or by other methods approved beforehand by the Director, Division of Environmental
Management:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number .
EPA-600/4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. ,
7. Determinatign for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See#4. above) .
10.The sample container should be labeled at the time of collection with the facility name,well identification number and date and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company,corporation, or governmental body to sign official documents.

crie CROMPTON & KNOWLES
COLORS INCORPORATED
P.O.Box 848(Spencer Mtn.Rd.),Lowell,NC 28098
[phone]•Fax[phone]
October 15, 1997
Ms. Betty Wilcox
Environmental Chemist
Groundwater Section -
North Carolina Division of Water Quality �;
P.O. Box 29535
Raleigh, North Carolina 27626-0535 "-
Subject: Groundwater Monitoring Report
Dear Ms. Wilcox:
Enclosed you will find the Groundwater Monitoring Report for our facility located in Lowell,
North Carolina. This groundwater monitoring fulfills the current NPDES permit (NC0005274)
groundwater monitoring requirements and the remedial monitoring requirements of the site
Corrective Action Plan as approved by the NCDEM-Mooresville Regional office.
If you have any questions, please do not hesitate to contact me at 704-824-9526, ext. 60.
Sincerely,
Bobmb
Environmental Engineer
p
cc:
Luther Buchanan
Rod Lang
Barry Dobinsky

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical' Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
September 25, 1997
Mr. Bobby Lamb
Crompton & Knowles Colors, Inc.
P.O. Box 848
1602 North Main Street
Lowell , NC 28098
RE: PACE Project No. 670911.580
Client Reference: Monitoring Wells September 1997
Dear Mr. Lamb: '
Enclosed is the report of laboratory analyses for samples received
September 11, 1997.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
69,64.W0.(2aCCQ
Kelly H. Wallace
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Crompton & Knowles Colors, Inc. September 25, 1997
P.O. Box 848 PACE Project Number: 670911580
1602 North Main Street
Lowell , NC 28098 NC Wastewater Lab Cert. #12
NC Drinkingwater Lab Cert. #37706
SC Lab Cert. #99006
Attn: Mr. Bobby Lamb
. Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183215
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-1
Parameter Units PRL METHOD DATE ANALYZED
FIELD ANALYSIS
GROUND WATER FIELD PARAMETERS
pH (Field) Units 0.01 6.67 09/11/97
Specific Conductivity(Field) umhos/cm2 10 197 09/11/97
Static Water Level (Depth) feet 0.01 83.19 09/11/97
Temperature (Field) Degrees C 20.8 09/11/97
Volume Prepumped Gallons 0.1 9.0 09/11/97
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand mg/L 25 ND 5220 D 09/17/97
Chloride mg/L 1 4.0 325.3 09/18/97
Chromium mg/L 0.010 ND 200.7 09/15/97
Copper mg/L 0.010 0.013 200.7 09/15/97
Lead mg/L 0.005 ND 239.2 09/22/97
Oil & Grease mg/L 1 ND 5520 B 09/23/97
Phenol , Low Level mg/L 0.005 ND 420.1 09/17/97
Solids, Total Dissolved mg/L 1 150 2540 C 09/17/97
Solids, Total Suspended mg/L 1 49 2540 D 09/17/97
Sulfate mg/L 10 16 375.4 09/19/97
Total Organic Carbon mg/L 1.0 1.8 5310C 09/16/97
Zinc mg/L 0.010 0.033 200.7 09/15/97
GROUND WATER FIELD PARAMETERS
Odor NONE 09/11/97
Appearance CLEAR 09/11/97
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
Anal +.,� 9800 Kincey Avenue,Suite 100
ytical Ialy ical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 2 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183215
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-1
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS 624
Chloromethane ug/L 5.0 ND 09/20/97
Chloroethene (Vinyl chloride) ug/L 5.0 ND 09/20/97
Bromomethane ug/L 5.0 ND 09/20/97
Chloroethane ug/L 5.0 ND 09/20/97
Trichlorofluoromethane ug/L 5.0 ND 09/20/97
1,1-Dichloroethene ug/L 5.0 ND 09/20/97
Dichloromethane ug/L 5.0 ND 09/20/97
trans-1,2-Dichloroethene ug/L 5.0 ND 09/20/97
1,1-Dichloroethane ug/L 5.0 ND 09/20/97
cis-1,2-Dichloroethene ug/L 5.0 ND 09/20/97
Chloroform ug/L 5.0 ND 09/20/97
1,1,1-Trichloroethane ug/L 5.0 ND 09/20/97
1,2-Dichloroethane ug/L 5.0 ND 09/20/97
Carbon tetrachloride ug/L 5.0 ND 09/20/97
Benzene ug/L 5.0 ND 09/20/97
Trichloroethene ug/L 5.0 ND 09/20/97
1,2-Dichloropropane ug/L 5.0 ND 09/20/97
Bromodichloromethane ug/L 5.0 ND 09/20/97
2-Chloroethoxyethene ug/L 10 ND 09/20/97
cis-1,3-Dichloropropene ug/L 5.0 ND 09/20/97
Toluene ug/L 5.0 ND 09/20/97
trans-1,3-Dichloropropene ug/L 5.0 ND 09/20/97
1,1,2-Trichloroethane ug/L 5.0 ND 09/20/97
Dibromochloromethane ug/L 5.0 ND 09/20/97
Tetrachloroethene ug/L 5.0 ND 09/20/97
Chlorobenzene ug/L 5.0 ND 09/20/97
Ethylbenzene ug/L 5.0 ND 09/20/97
Bromoform ug/L 5.0 ND 09/20/97
1,1,2,2-Tetrachloroethane ug/L 5.0 ND 09/20/97
1,3-Dichlorobenzene ug/L 5.0 ND 09/20/97
1,4-Dichlorobenzene ug/L 5.0 ND 09/20/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
Pace Analytical 9800 Kin Avenue,Suite 100
Hununtersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 3 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183215
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-1
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS 624
1,2-Dichlorobenzene ug/L 5.0 ND 09/20/97
Surrogate - Dibromofluoromethane % 110 09/20/97
Surrogate - Toluene-d8 % 103 09/20/97
Surrogate - Bromofluorobenzene % 107 09/20/97
BASE/NEUTRALS AND ACIDS 625
N-Nitrosodimethylamine ug/L 5.0 ND 09/15/97
bis(2-Chloroethyl)ether ug/L 5.0 ND 09/15/97
Phenol ug/L 5.0 ND 09/15/97
2-Chlorophenol ug/L 5.0 ND 09/15/97
1,3-Dichlorobenzene ug/L 5.0 ND 09/15/97
1,4-Dichlorobenzene ug/L 5.0 ND 09/15/97
1,2-Dichlorobenzene ug/L 5.0 ND 09/15/97
bis(2-Chloroisopropyl)ether ug/L 5.0 ND 09/15/97
Hexachloroethane ug/L 5.0 ND 09/15/97
N-Nitrosodi-n-propylamine ug/L 5.0 ND 09/15/97
Nitrobenzene ug/L 5.0 ND 09/15/97
3,5,5-Trimethyl-2-cyclohexanone ug/L 5.0 ND 09/15/97
2-Nitrophenol ug/L 5.0 ND 09/15/97
2,4-Dimethylphenol ug/L 5.0 ND 09/15/97
bis(2-Chloroethoxy)methane ug/L 5.0 ND 09/15/97
2,4-Dichlorophenol ug/L 5.0 ND 09/15/97
1,2,4-Trichlorobenzene ug/L 5.0 ND 09/15/97
Naphthalene ug/L 5.0 ND 09/15/97
Hexachlorobutadiene ug/L 5.0 ND 09/15/97
4-Chloro-3-methylphenol ug/L 5.0 ND 09/15/97
Hexachlorocyclopentadiene ug/L 10 ND 09/15/97
2,4,6-Trichlorophenol ug/L 5.0 ND 09/15/97
2-Chloronaphthalene ug/L 5.0 ND 09/15/97
Acenaphthylene ug/L 5.0 ND 09/15/97
Dimethyl phthalate ug/L 5.0 ND 09/15/97
2,6-Dinitrotoluene ug/L 5.0 ND 09/15/97
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
e.�,� +:lC^� 9800 Kincey Avenue,Suite 100
MrPEU�P L y Se$ombor 24, ville,NC 28078
PACE Project NumB >�94- 121580
Page 4 Fax:[phone]
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183215
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-1
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS AND ACIDS 625
Acenaphthene ug/L 5.0 ND 09/15/97
2,4-Dinitrophenol ug/L 25 ND 09/15/97
2,4-Dinitrotoluene ug/L 5.0 ND 09/15/97
4-Nitrophenol ug/L 25 ND 09/15/97
Fluorene ug/L 5.0 ND 09/15/97
4-Chlorophenyl phenyl ether ug/L 5.0 ND 09/15/97
Diethyl phthalate ug/L 5.0 ND 09/15/97
2-Methyl-4,6-dinitrophenol ug/L 25 ND 09/15/97
N-Nitrosodiphenylamine ug/L 5.0 ND 09/15/97
4-Bromophenyl phenyl ether ug/L 5.0 ND 09/15/97
Hexachlorobenzene ug/L 5.0 ND 09/15/97
Pentachlorophenol ug/L 25 ND 09/15/97
Phenanthrene ug/L 5.0 ND 09/15/97
Anthracene ug/L 5.0 ND 09/15/97
Di-n-butyl phthalate ug/L 5.0 ND 09/15/97
Fluoranthene ug/L 5.0 ND 09/15/97
Benzidine ug/L 50 ND 09/15/97
Pyrene ug/L 5.0 ND 09/15/97
Benzyl butyl phthalate ug/L 5.0 ND 09/15/97
3,3-Dichlorobenzidine ug/L 10 ND 09/15/97
Benz[a]anthracene ug/L 5.0 ND 09/15/97
Chrysene ug/L 5.0 ND 09/15/97
bis(2-Ethylhexyl)phthalate ug/L 5.0 ND 09/15/97
Di-n-octylphthalate ug/L 5.0 ND 09/15/97
Benzo[b]fluoranthene ug/L 5.0 ND 09/15/97
Benzo[k]fluoranthene ug/L 5.0 ND 09/15/97
Benzo[a]pyrene ug/L 5.0 ND 09/15/97
Indeno[1,2,3-cd]pyrene ug/L 5.0 ND 09/15/97
Dibenz[a,h]anthracene ug/L 5.0 ND 09/15/97
Benzo[g,h,i]perylene ug/L 5.0 ND 09/15/97
Surrogate - 2-Fluorophenol % 43 09/15/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 5 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183215
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-1
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS AND ACIDS 625
Surrogate - Phenol-d5 % 35 09/15/97
Surrogate - Nitrobenzene-d5 % 69 09/15/97
Surrogate - 2-Fluorobiphenyl % 76 09/15/97
Surrogate - 2,4,6-Tribromophenol % 96 09/15/97
Surrogate - Terphenyl-d14 % 131 09/15/97
Date Extracted, Base/Neutrals and Acids Date 091597 09/15/97
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 6 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183223
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-2
Parameter Units PRL METHOD DATE ANALYZED
FIELD ANALYSIS
GROUND WATER FIELD PARAMETERS
pH (Field) Units 0.01 6.16 09/11/97
Specific Conductivity(Field) umhos/cm2 10 616 09/11/97
Static Water Level (Depth) feet 0.01 19.50 09/11/97
Temperature (Field) Degrees C 17.5 09/11/97
Volume Prepumped Gallons 0.1 5.0 09/11/97
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand mg/L 25 40 5220 D 09/17/97
Chloride mg/L 1 12 325.3 09/18/97
Chromium mg/L 0.010 0.017 200.7 09/15/97
Copper mg/L 0.010 0.12 200.7 09/15/97
Lead mg/L 0.005 0.014 239.2 09/22/97
Oil & Grease mg/L 1 1 5520 B 09/23/97
Phenol , Low Level mg/L 0.005 ND 420.1 09/16/97
Solids, Total Dissolved mg/L 1 400 2540 C 09/17/97
Solids, Total Suspended mg/L 1 590 2540 D 09/17/97
Sulfate mg/L 10 28 375.4 09/19/97
Total Organic Carbon mg/L 1.0 3.6 5310C 09/16/97
Zinc mg/L 0.010 0.094 200.7 09/15/97
GROUND WATER FIELD PARAMETERS
Odor NONE 09/11/97
Appearance TURBID 09/11/97
ORGANIC ANALYSIS
VOLATILE ORGANICS 624
Chloromethane ug/L 5.0 ND 09/16/97
Chloroethene (Vinyl chloride) ug/L 5.0 ND 09/16/97
Bromomethane ug/L 5.0 ND 09/16/97
Chloroethene ug/L 5.0 ND 09/16/97
Trichlorofluoromethane ug/L 5.0 ND 09/16/97
1,1-Dichloroethene ug/L 5.0 ND 09/16/97
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 7 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183223
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-2
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS 624
Dichloromethane ug/L 5.0 ND 09/16/97
trans-1,2-Dichloroethene ug/L 5.0 ND 09/16/97
1,1-Dichloroethane ug/L 5.0 ND 09/16/97
cis-1,2-Dichloroethene ug/L 5.0 ND 09/16/97
Chloroform ug/L 5.0 ND 09/16/97
1,1,1-Trichloroethane ug/L 5.0 ND 09/16/97
1,2-Dichloroethane ug/L 5.0 ND 09/16/97
Carbon tetrachloride ug/L 5.0 ND 09/16/97
Benzene ug/L 5.0 ND 09/16/97
Trichloroethene ug/L 5.0 ND 09/16/97
1,2-Dichloropropane ug/L 5.0 ND 09/16/97
Bromodichloromethane ug/L 5.0 ND 09/16/97
2-Chloroethoxyethene ug/L 10 ND 09/16/97
cis-1,3-Dichloropropene ug/L 5.0 ND 09/16/97
Toluene ug/L 5.0 ND 09/16/97
trans-1,3-Dichloropropene ug/L 5.0 ND 09/16/97
1,1,2-Trichloroethane ug/L 5.0 ND 09/16/97
Dibromochloromethane ug/L 5.0 ND 09/16/97
Tetrachloroethene ug/L 5.0 ND 09/16/97
Chlorobenzene ug/L 5.0 ND 09/16/97
Ethylbenzene ug/L 5.0 ND 09/16/97
Bromoform ug/L 5.0 ND 09/16/97
1,1,2,2-Tetrachloroethane ug/L 5.0 ND 09/16/97
1,3-Dichlorobenzene ug/L 5.0 ND 09/16/97
1,4-Dichlorobenzene ug/L 5.0 ND 09/16/97
1,2-Dichlorobenzene ug/L 5.0 ND 09/16/97
Surrogate - Dibromofluoromethane % 99 09/16/97
Surrogate - Toluene-d8 % 97 09/16/97
Surrogate - Bromofluorobenzene % 97 09/16/97
BASE/NEUTRALS AND ACIDS 625
N-Nitrosodimethylamine ug/L 5.0 ND 09/15/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb • September 25, 1997
Page 8 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183223
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-2
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS AND ACIDS 625
bis(2-Chloroethyl)ether ug/L 5.0 ND 09/15/97
Phenol ug/L 5.0 ND 09/15/97
2-Chlorophenol ug/L 5.0 ND 09/15/97
1,3-Dichlorobenzene ug/L 5.0 ND 09/15/97
1,4-Dichlorobenzene ug/L 5.0 ND 09/15/97
1,2-Dichlorobenzene ug/L 5.0 ND 09/15/97
bis(2-Chloroisopropyl)ether ug/L 5.0 ND 09/15/97
Hexachloroethane ug/L 5.0 ND 09/15/97
N-Nitrosodi-n-propylamine ug/L 5.0 ND 09/15/97
Nitrobenzene ug/L 5.0 ND 09/15/97
3,5,5-Trimethyl-2-cyclohexanone ug/L 5.0 ND 09/15/97
2-Nitrophenol ug/L 5.0 ND 09/15/97
2,4-Dimethylphenol ug/L 5.0 ND 09/15/97
bis(2-Chloroethoxy)methane ug/L 5.0 ND 09/15/97
2,4-Dichlorophenol ug/L 5.0 ND 09/15/97
1,2,4-Trichlorobenzene ug/L 5.0 ND 09/15/97
Naphthalene ug/L 5.0 ND 09/15/97
Hexachlorobutadiene ug/L 5.0 ND 09/15/97
4-Chloro-3-methylphenol ug/L 5.0 ND 09/15/97
Hexachlorocyclopentadiene ug/L 10 ND 09/15/97
2,4,6-Trichlorophenol ug/L 5.0 ND 09/15/97
2-Chloronaphthalene ug/L 5.0 ND 09/15/97
Acenaphthylene ug/L 5.0 ND . 09/15/97
Dimethyl phthalate ug/L 5.0 ND 09/15/97
2,6-Dinitrotoluene ug/L 5.0 ND 09/15/97
Acenaphthene ug/L 5.0 ND 09/15/97
2,4-Dinitrophenol ug/L 25 ND 09/15/97
2,4-Dinitrotoluene ug/L 5.0 ND 09/15/97
4-Nitrophenol ug/L 25 ND 09/15/97
Fluorene ug/L 5.0 ND 09/15/97
4-Chlorophenyl phenyl ether ug/L 5.0 ND 09/15/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 9 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183223
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-2
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS AND ACIDS 625
Diethyl phthalate ug/L 5.0 ND 09/15/97
2-Methyl-4,6-dinitrophenol ug/L 25 ND 09/15/97
N-Nitrosodiphenylamine ug/L 5.0 ND 09/15/97
4-Bromophenyl phenyl ether ug/L 5.0 ND 09/15/97
Hexachlorobenzene ug/L 5.0 ND 09/15/97
Pentachlorophenol ug/L 25 ND 09/15/97
Phenanthrene ug/L 5.0 ND 09/15/97
Anthracene ug/L 5.0 ND 09/15/97
Di-n-butyl phthalate ug/L 5.0 ND 09/15/97
Fluoranthene ug/L 5.0 ND 09/15/97
Benzidine ug/L 50 ND 09/15/97
Pyrene ug/L 5.0 ND 09/15/97
Benzyl butyl phthalate ug/L 5.0 ND 09/15/97
3,3-Dichlorobenzidine ug/L 10 ND 09/15/97
Benz[a]anthracene ug/L 5.0 ND 09/15/97
Chrysene ug/L 5.0 ND 09/15/97
bis(2-Ethylhexyl)phthalate ug/L 5.0 ND 09/15/97
Di-n-octylphthalate ug/L 5.0 ND 09/15/97
Benzo[b]fluoranthene ug/L 5.0 ND 09/15/97
Benzo[k]fluoranthene ug/L 5.0 ND 09/15/97
Benzo[a]pyrene ug/L 5.0 ND 09/15/97
Indeno[1,2,3-cd]pyrene ug/L 5.0 ND 09/15/97
Dibenz[a,h]anthracene ug/L 5.0 ND 09/15/97
Benzo[g,h,i]perylene ug/L 5.0 ND 09/15/97
Surrogate - 2-Fluorophenol % 44 09/15/97
Surrogate - Phenol-d5 % 37 09/15/97
Surrogate - Nitrobenzene-d5 % 74 09/15/97
Surrogate - 2-Fluorobiphenyl % 85 09/15/97
Surrogate - 2,4,6-Tribromophenol % 106 09/15/97
Surrogate - Terphenyl-d14 % 120 09/15/97
Date Extracted, Base/Neutrals and Acids Date 091597 09/15/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 10 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183231
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-3
Parameter Units PRL METHOD DATE ANALYZED
FIELD ANALYSIS
GROUND WATER FIELD PARAMETERS
pH (Field) Units 0.01 8.65 09/11/97
Specific Conductivity(Field) umhos/cm2 10 26800 09/11/97
Static Water Level (Depth) feet 0.01 18.80 09/11/97
Temperature (Field) Degrees C 16.0 09/11/97
Volume Prepumped Gallons 0.1 4.0 & DRY 09/11/97
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand mg/L 250 5900 5220 D 09/17/97
Chloride mg/L 1 10000 325.3 09/18/97
Chromium mg/L 0.010 0.25 200.7 09/15/97
Copper mg/L 0.010 3.1 200.7 09/15/97
Lead mg/L 0.005 0.007 239.2 09/22/97
Oil & Grease mg/L 1 2 5520 B 09/23/97
Phenol , Low Level mg/L 1.6 16 420.1 09/17/97
Solids, Total Dissolved mg/L 1 22000 2540 C 09/17/97
Solids, Total Suspended mg/L 1 640 2540 D 09/17/97
Sulfate mg/L 500 990 375.4 09/19/97
Total Organic Carbon mg/L 20 2900 5310C 09/16/97
Zinc mg/L 0.010 0.20 200.7 09/15/97
GROUND WATER FIELD PARAMETERS
Odor CHEMICAL 09/11/97
Appearance BLANK 09/11/97
ORGANIC ANALYSIS
VOLATILE ORGANICS I1 624
Chloromethane ug/L 250 ND 09/16/97
Chloroethene (Vinyl chloride) ug/L 250 ND 09/16/97
Bromomethane ug/L 250 ND 09/16/97
Chloroethane . ug/L 250 ND 09/16/97
Trichlorofluoromethane ug/L 250 ND 09/16/97
1,1-Dichloroethene ug/L 250 ND 09/16/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 11 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183231
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-3
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS I1 624
Dichloromethane ug/L 250 ND 09/16/97
trans-1,2-Dichloroethene ug/L 250 ND 09/16/97
1,1-Dichioroethene ug/L 250 ND 09/16/97
cis-1,2-Dichloroethene ug/L 250 ND 09/16/97
Chloroform ug/L 250 ND 09/16/97
1,1,1-Trichloroethane ug/L 250 ND 09/16/97
1,2-Dichloroethane ug/L 250 ND 09/16/97
Carbon tetrachloride ug/L 250 ND 09/16/97
Benzene ug/L 250 480 09/16/0
Trichloroethene ug/L 250 ND 09/16/97
1,2-Dichloropropene ug/L 250 ND 09/16/97
Bromodichloromethane ug/L 250 ND 09/16/97
2-Chloroethoxyethene ug/L 500 ND 09/16/97
cis-1,3-Dichloropropene ug/L 250 ND 09/16/97
Toluene ug/L 250 ND 09/16/97
trans-1,3-Dichloropropene ug/L 250 ND 09/16/97
1,1,2-Trichloroethane ug/L 250 ND 09/16/97
Dibromochloromethane ug/L 250 ND 09/16/97
Tetrachloroethene ug/L 250 ND 09/16/97
Chlorobenzene ug/L 250 ND 09/16/97
Ethylbenzene ug/L 250 ND 09/16/97
Bromoform ug/L 250 ND 09/16/97
1,1,2,2-Tetrachloroethane ug/L 250 ND 09/16/97
1,3-Dichlorobenzene ug/L 250 ND 09/16/97
1,4-Dichlorobenzene ug/L 250 ND 09/16/97
1,2-Dichlorobenzene ug/L 250 ND 09/16/97
Surrogate - Dibromofluoromethane % 102 09/16/97
Surrogate - Toluene-d8 % 100 09/16/97
Surrogate - Bromofluorobenzene % 95 09/16/97
BASE/NEUTRALS AND ACIDS 625
N-Nitrosodimethylamine ug/L 25 ND 09/15/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 12 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183231
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-3
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS AND ACIDS 625
bis(2-Chloroethyl)ether ug/L 25 ND 09/15/97
Phenol ug/L 250 3300 09/15/97
2-Chlorophenol ug/L 25 ND 09/15/97
1,3-Dichlorobenzene ug/L 25 ND 09/15/97
1,4-Dichlorobenzene ug/L 25 ND 09/15/97
1,2-Dichlorobenzene ug/L 25 ND 09/15/97
bis(2-Chloroisopropyl)ether ug/L 25 ND 09/15/97
Hexachloroethane ug/L 25 ND 09/15/97
N-Nitrosodi-n-propylamine ug/L 25 ND 09/15/97
Nitrobenzene ug/L 25 ND 09/15/97
3,5,5-Trimethyl-2-cyclohexanone ug/L 25 ND 09/15/97
2-Nitrophenol ug/L 25 ND 09/15/97
2,4-Dimethylphenol ug/L 25 ND 09/15/97
bis(2-Chloroethoxy)methane ug/L 25 ND 09/15/97
2,4-Dichlorophenol ug/L 25 ND 09/15/97
1,2,4-Trichlorobenzene ug/L 250 2700 09/15/97
Naphthalene ug/L 25 ND 09/15/97
Hexachlorobutadiene ug/L 25 ND 09/15/97
4-Chloro-3-methylphenol ug/L 25 ND 09/15/97
Hexachlorocyclopentadiene ug/L 50 ND 09/15/97
2,4,6-Trichlorophenol ug/L 25 ND 09/15/97
2-Chloronaphthalene ug/L 25 ND 09/15/97
Acenaphthylene ug/L 25 ND 09/15/97
Dimethyl phthalate ug/L 25 ND 09/15/97
2,6-Dinitrotoluene ug/L 25 ND 09/15/97
Acenaphthene ug/L 25 ND 09/15/97
2,4-Dinitrophenol ug/L 125 ND 09/15/97
2,4-Dinitrotoluene ug/L 25 ND 09/15/97
4-Nitrophenol ug/L 125 ND 09/15/97
Fluorene ug/L 25 ND 09/15/97
4-Chlorophenyl phenyl ether ug/L 25 ND 09/15/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 13 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183231
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: MW-3
Parameter Units PRL METHOD DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS AND ACIDS 625
Diethyl phthalate ug/L 25 ND 09/15/97
2-Methyl-4,6-dinitrophenol ug/L . 125 ND 09/15/97
N-Nitrosodiphenylamine ug/L 25 ND 09/15/97
4-Bromophenyl phenyl ether ug/L 25 ND 09/15/97
Hexachlorobenzene ug/L 25 ND 09/15/97
Pentachlorophenol ug/L 125 ND 09/15/97
Phenanthrene ug/L 25 ND 09/15/97
Anthracene ug/L 25 ND 09/15/97
Di-n-butyl phthalate ug/L 25 ND 09/15/97
Fluoranthene ug/L 25 ND 09/15/97
Benzidine ug/L 2500 2800 09/15/97
Pyrene ug/L 25 ND 09/15/97
Benzyl butyl phthalate ug/L 25 ND 09/15/97
3,3-Dichlorobenzidine ug/L 50 ND 09/15/97
Benz[a]anthracene ug/L 25 ND 09/15/97
Chrysene ug/L 25 ND 09/15/97
bis(2-Ethylhexyl)phthalate ug/L 25 ND 09/15/97
Di-n-octylphthalate ug/L 25 ND 09/15/97
Benzo[b]fluoranthene ug/L 25 ND 09/15/97
Benzo[k]fluoranthene ug/L 25 ND 09/15/97
Benzo[a]pyrene ug/L 25 ND 09/15/97
Indeno[1,2,3-cd]pyrene ug/L 25 ND 09/15/97
Dibenz[a,h]anthracene ug/L 25 ND 09/15/97
Benzo[g,h,i]perylene ug/L 25 ND 09/15/97
Surrogate - 2-Fluorophenol % 44 09/15/97
Surrogate - Phenol-d5 % 34 09/15/97
Surrogate - Nitrobenzene-d5 % 71 09/15/97
Surrogate - 2-Fluorobiphenyl % 61 09/15/97
Surrogate - 2,4,6-Tribromophenol % 103 09/15/97
Surrogate - Terphenyl-d14 % 30 09/15/97
Date Extracted, Base/Neutrals and Acids Date 091597 09/15/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 14 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183240
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: Trip
Parameter Units PRL Blank METHOD DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS 624
Chloromethane ug/L 5.0 ND 09/20/97
Chloroethene (Vinyl chloride) ug/L 5.0 ND 09/20/97
Bromomethane ug/L 5.0 ND 09/20/97
Chloroethene ug/L 5.0 ND 09/20/97
Trichlorofluoromethane ug/L 5.0 ND 09/20/97
1,1-Dichloroethene ug/L 5.0 ND 09/20/97
Dichloromethane ug/L 5.0 10 C3 09/20/97
trans-1,2-Dichloroethene ug/L 5.0 ND 09/20/97
1,1-Dichloroethane ug/L 5.0 ND 09/20/97
cis-1,2-Dichloroethene ug/L 5.0 ND 09/20/97
Chloroform ug/L 5.0 ND 09/20/97
1,1,1-Trichloroethane ug/L 5.0 ND 09/20/97
1,2-Dichloroethane ug/L 5.0 ND 09/20/97
Carbon tetrachloride ug/L 5.0 ND 09/20/97
Benzene ug/L 5.0 ND 09/20/97
Trichloroethene ug/L 5.0 ND 09/20/97
1,2-Dichloropropane ug/L 5.0 ND 09/20/97
Bromodichloromethane ug/L 5.0 ND 09/20/97
2-Chloroethoxyethene ug/L 10 ND 09/20/97
cis-1,3-Dichloropropene ug/L 5.0 ND 09/20/97
Toluene ug/L 5.0 ND 09/20/97
trans-1,3-Dichloropropene ug/L 5.0 ND 09/20/97
1,1,2-Trichloroethane ug/L 5.0 ND 09/20/97
Dibromochloromethane ug/L 5.0 ND 09/20/97
Tetrachloroethene ug/L 5.0 ND 09/20/97
Chlorobenzene ug/L 5.0 ND 09/20/97
Ethylbenzene ug/L 5.0 ND 09/20/97
Bromoform ug/L 5.0 ND 09/20/97
1,1,2,2-Tetrachloroethane ug/L 5.0 ND 09/20/97
1,3-Dichlorobenzene ug/L 5.0 ND 09/20/97
1,4-Dichlorobenzene ug/L 5.0 ND 09/20/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 15 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183240
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: Trip
Parameter Units PRL Blank METHOD DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS 624
1,2-Dichlorobenzene ug/L 5.0 ND 09/20/97
Surrogate - Dibromofluoromethane % 110 09/20/97
Surrogate - Toluene-d8 104 09/20/97
Surrogate - Bromofluorobenzene % 112 09/20/97
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
Pace Analytical 9800 Kincey Avenue,Suite 100
Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 16 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183258
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: Equipment
Parameter Units PRL Blank METHOD DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS 624
Chloromethane ug/L 5.0 ND 09/20/97
Chloroethene (Vinyl chloride) ug/L 5.0 ND 09/20/97
Bromomethane ug/L 5.0 ND 09/20/97
Chloroethane ug/L 5.0 ND 09/20/97
Trichlorofluoromethane ug/L 5.0 ND 09/20/97
1,1-Dichloroethene ug/L 5.0 ND 09/20/97
Dichloromethane ug/L 5.0 5.2 C3 09/20/97
trans-1,2-Dichloroethene ug/L 5.0 ND 09/20/97
1,1-Dichloroethane ug/L 5.0 ND 09/20/97
cis-1,2-Dichloroethene ug/L 5.0 ND 09/20/97
Chloroform ug/L 5.0 ND 09/20/97
1,1,1-Trichioroethane ug/L 5.0 ND 09/20/97
1,2-Dichloroethane ug/L 5.0 ND 09/20/97
Carbon tetrachloride ug/L 5.0 ND 09/20/97
Benzene ug/L 5.0 ND 09/20/97
Trichloroethene ug/L 5.0 ND 09/20/97
1,2-Dichioropropane ug/L 5.0 ND 09/20/97
Bromodichloromethane ug/L 5.0 ND 09/20/97
2-Chloroethoxyethene ug/L 10 ND 09/20/97
cis-1,3-Dichloropropene ug/L 5.0 ND 09/20/97
Toluene ug/L 5.0 ND 09/20/97
trans-1,3-Dichloropropene ug/L 5.0 ND 09/20/97
1,1,2-Trichioroethane ug/L 5.0 ND 09/20/97
Dibromochloromethane ug/L 5.0 ND 09/20/97
Tetrachioroethene ug/L 5.0 ND 09/20/97
Chlorobenzene ug/L 5.0 ND 09/20/97
Ethylbenzene ug/L 5.0 ND 09/20/97
Bromoform ug/L 5.0 ND • 09/20/97
1,1,2,2-Tetrachloroethane ug/L 5.0 ND 09/20/97
1,3-Dichlorobenzene ug/L 5.0 ND 09/20/97
1,4-Dichlorobenzene ug/L 5.0 ND 09/20/97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb September 25, 1997
Page 17 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
PACE Sample Number: 92 0183258
Date Collected: 09/11/97
Date Received: 09/11/97
Client Sample ID: Equipment
Parameter Units PRL Blank METHOD DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS 624
1,2-Dichlorobenzene ug/L 5.0 ND 09/20/97
Surrogate - Dibromofluoromethane % 110 09/20/97
Surrogate - Toluene-d8 % 101 09/20/97
Surrogate - Bromofluorobenzene % 106 09/20/97
These data have been reviewed and are approved for release.
Margaret S. Harding
Manager, Laboratory Operations
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
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Mr. Bobby Lamb FOOTNOTES September 25, 1997
Page 18 for pages 1 through 17 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
C3 Common laboratory contaminant.
I1 Sample was diluted due to the presence of elevated concentrations of
target/non-target compounds.
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
•
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
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Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 19 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
Chemical Oxygen Demand
Batch: 92 63898
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units PRL Blank 920185269 92 0185269 RPD
Chemical Oxygen Demand mg/L 25 ND 150 150 5%
SPIKE:
Spike
Parameter Units PRL 920185269 Spike Recv
Chemical Oxygen Demand mg/L 25 150 200 90%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Chemical Oxygen Demand mg 500 99%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
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Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 20 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
Chloride
Batch: 92 63984
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920183231 of
Parameter Units PRL Blank MW-3 92 0183231 RPD
Chloride mg 1 ND 10000 9800 2%
SPIKE:
Spike
Parameter Units PRL 920184165 Spike Recv
Chloride mg/L 1 2.5 5.0 106%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Chloride mg/L 1 20.0 101%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 21 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
Lead
Batch: 92 64091
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920183215 of
Parameter Units PRL Blank MW-1 92 0183215 RPD
Lead mgmg/L T.005 N ND ND NC
SPIKE AND SPIKE DUPLICATE:
Spike
920183215 Spike Dupl
Parameter Units PRL MW-1 Spike Recv Recv RPD
Lead mg/L 0.005 ND 0.020 0% 93% 15%
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter Units PRL Value Recv Recv RPD
Lead mg/L 0.005 0.020 108% 98% 10%
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
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Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 22 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
Oil & Grease
Batch: 92 64118
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK:
Method
Parameter Units PRL Blank
Oil & Grease mg/L 1 ND
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Oil & Grease mg/L 1 50.0 91%
•
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
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Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 23 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
Solids, Total Dissolved
Batch: 92 63913
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920183215 of
Parameter Units PRL Blank MW-1 92 0183215 RPD
Solids, Total Dissolved mg/L 1 ND 150 140 7%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Solids, Total Dissolved mg/L 1 100 101%
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 24 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
Solids, Total Suspended
Batch: 92 63919
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units PRL Blank 920182820 92 0182820 RPD
Solids, Total Suspended mg/L 1 ND 10 68 149%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Solids, Total Suspended mg/L 1 100 91%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
AnalyticalPacAnalyticalHuntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 25 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
Sulfate
Batch: 92 64015
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method 920183223 of
Parameter Units PRL Blank MW-2 92 0183223 RPD
Sulfate mg/L 10 ND 28 29 4%
SPIKE:
920183215 Spike
Parameter Units PRL MW-1 Spike Recv
Sulfate mg/L 10 16 20.0 107%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Sulfate mg/L 10 20.0 102%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 26 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
ICP QUALITY CONTROL
Batch: 92 63807
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units PRL Blank 920182030 92 0182030 RPD
INDIVIDUAL PARAMETERS
Calcium mg/L 0.10 62 63 2%
Copper mg/L 0.010 ND ND NC
Iron mg/L 0.050 0.28 0.28 0%
Manganese mg/L 0.010 0.023 0.023 0%
Nickel mg/L 0.05 ND ND NC
Sodium mg/L 0.20 15 15 0%
Zinc mg/L 0.010 0.29 0.29 0%
ICP QUALITY CONTROL
Barium mg/L 0.010 0.094 0.095 1%
Aluminum mg/L 0.10 ND
Antimony mg/L 0.20 ND
Arsenic mg/L 0.50 ND
Barium mg/L 0.010 ND
Beryllium mg/L 0.010 ND
Boron mg/L 0.10 ND
Cadmium mg/L 0.010 ND
Calcium mg/L 0.10 ND
Chromium mg/L 0.010 ND
Cobalt mg/L 0.010 ND
Copper mg/L 0.010 ND
Iron mg/L 0.050 ND
Lead mg/L 0.10 ND
Magnesium mg/L 0.20 ND
Manganese mg/L 0.010 ND
Molybdenum mg/L 0.05 ND
Nickel mg/L 0.05 ND
Potassium mg/L 1.0 ND
Selenium mg/L 0.50 ND
Silver mg/L 0.050 ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 27 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
ICP QUALITY CONTROL
Batch: 92 63807
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units PRL Blank 920182030 92 0182030 RPD
Sodium mg/L 0.20 ND
Thallium mg/L 0.50 ND
Tin mg/L 0.20 ND
Titanium mg/L 0.010 ND
Vanadium mg/L 0.010 ND
Zinc mg/L 0.010 ND
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl -
Parameter Units PRL 920182030 Spike Recv Recv RPD
Aluminum mg/L 0.10 0.29 50 97% 0%
Antimony mg/L 0.20 ND 2.0 98% 97% 1%
Arsenic mg/L 0.50 ND 2.0 104% 100% 4%
Barium mg/L 0.010 0.094 1.0 98% 98% 0%
Beryllium mg/L 0.010 ND 1.0 101% 101% 0%
Boron mg/L 0.10 0.22 1.0 98% 97% 1%
Cadmium mg/L 0.010 ND 1.0 100% 100% 0%
Calcium mg/L 0.10 62 50 94% 94% 0%
Chromium mg/L 0.010 ND 1.0 98% 98% 0%
Cobalt mg/L 0.010 ND 1.0 96% 96% 0%
Copper mg/L 0.010 ND 1.0 100% 100% 0%
Iron mg/L 0.050 0.28 25 96% 96% 0%
Lead mg/L 0.10 ND 2.0 101% 98% 3%
Magnesium mg/L 0.20 30 25 100% 102% 2%
Manganese mg/L 0.010 0.023 1.0 97% 97% 0%
Molybdenum mg/L 0.05 0.18 1.0 97% 94% 3%
Nickel mg/L 0.05 ND 1.0 100% 99% 1%
Potassium mg/L 1.0 19 50 100% 100% 0%
Selenium mg/L 0.50 ND 2.0 100% 107% 7%
Silver mg/L 0.050 ND 1.0 86% 86% 0%
Sodium mg/L 0.20 15 50 98% 97% 1%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 28 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
ICP QUALITY CONTROL
Batch: 92 63807
Samples: 92 0183215, 92 0183223, 92 0183231
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl
Parameter Units PRL 920182030 Spike Recv Recv RPD
Thallium mg/L 0.50 ND 2.0 95% 99% 4%
Tin mg/L 0.20 ND 1.0 96% 103% 7%
Titanium mg/L 0.010 ND 1.0 99% 99% 0%
Vanadium mg/L 0.010 ND 1.0 101% 100% 1%
Zinc mg/L 0.010 0.29 2.0 100% 99% 1%
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter Units PRL Value Recv Recv RPD
Aluminum mg/L 0.10 50 94% 95% - 1%
Antimony mg/L 0.20 2.0 94% 95% 1%
Arsenic mg/L 0.50 2.0 99% 98% 1%
Barium mg/L 0.010 1.0 95% 97% 2%
Beryllium mg/L 0.010 1.0 98% 99% 1%
Boron mg/L 0.10 1.0 97% 97% 0%
Cadmium mg/L 0.010 1.0 98% 98% 0%
Calcium mg/L 0.10 50 94% 95% 1%
Chromium mg/L 0.010 1.0 97% 97% 0%
Cobalt mg/L 0.010 1.0 95% 97% 2%
Copper mg/L 0.010 1.0 97% 99% 2%
Iron mg/L 0.050 25 95% 96% 1%
Lead mg/L 0.10 2.0 98% 98% 0%
Magnesium mg/L 0.20 25 99% 100% 1%
Manganese mg/L 0.010 1.0 95% 97% 2%
Molybdenum mg/L 0.05 1.0 96% 97% 1%
Nickel mg/L 0.05 1.0 93% 96% 3%
Potassium mg/L 1.0 50 96% 102% 6%
Selenium mg/L 0.50 2.0 101% 106% 5%
Silver mg/L 0.050 1.0 96% 97% 1%
Sodium mg/L 0.20 50 96% 99% 3%
Thallium mg/L 0.50 2.0 100% 99% 1%
Tin mg/L 0.20 1.0 96% 103% 7%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 29 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
ICP QUALITY CONTROL
Batch: 92 63807
Samples: 92 0183215, 92 0183223, 92 0183231
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter Units PRL Value Recv Recv RPD
Titanium mg/L 0.010 1.0 97% 98% 1%
Vanadium mg/L 0.010 1.0 98% 100% 2%
Zinc mg/L 0.010 2.0 98% 99% 1%
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace AnaJytinaI Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 30 PACE Project Number: 670911580
•
Client Reference: Monitoring Wells September 1997
BASE/NEUTRALS AND ACIDS
Batch: 92 63839
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK:
Method
Parameter Units PRL Blank
N-Nitrosodimethylamine ug/L �.0 ND
bis(2-Chloroethyl)ether ug/L 5.0 ND
Phenol ug/L 5.0 ND
2-Chlorophenol ug/L 5.0 ND
1,3-Dichlorobenzene ug/L 5.0 ND
1,4-Dichlorobenzene ug/L 5.0 ND
1,2-Dichlorobenzene ug/L 5.0 ND
bis(2-Chloroisopropyl)ether ug/L 5.0 ND
Hexachloroethane ug/L 5.0 ND
N-Nitrosodi-n-propylamine ug/L 5.0 ND
Nitrobenzene ug/L 5.0 ND
3,5,5-Trimethyl-2-cyclohexanone ug/L 5.0 ND
2-Nitrophenol ug/L 5.0 ND
2,4-Dimethylphenol ug/L 5.0 ND
bis(2-Chloroethoxy)methane ug/L 5.0 ND
2,4-Dichlorophenol ug/L 5.0 ND
1,2,4-Trichlorobenzene ug/L 5.0 ND
Naphthalene ug/L 5.0 ND
Hexachlorobutadiene ug/L 5.0 ND
4-Chloro-3-methylphenol ug/L 5.0 ND
Hexachlorocyclopentadiene ug/L 10 ND
2,4,6-Trichlorophenol ug/L 5.0 ND
2-Chloronaphthalene ug/L 5.0 ND
Acenaphthylene ug/L 5.0 ND
Dimethyl phthalate ug/L 5.0 ND
2,6-Dinitrotoluene ug/L 5.0 ND
Acenaphthene ug/L 5.0 ND
2,4-Dinitrophenol ug/L 25 ND
2,4-Dinitrotoluene ug/L 5.0 ND
4-Nitrophenol ug/L 25 ND
Fluorene ug/L 5.0 ND
4-Chlorophenyl phenyl ether ug/L 5.0 ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 31 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
BASE/NEUTRALS AND ACIDS
Batch: 92 63839
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK:
Method
Parameter Units PRL Blank
Diethyl phthalate ug/L 5.0 ND
2-Methyl-4,6-dinitrophenol ug/L 25 ND
N-Nitrosodiphenylamine ug/L 5.0 ND
4-Bromophenyl phenyl ether ug/L 5.0 ND
Hexachlorobenzene ug/L 5.0 ND
Pentachlorophenol ug/L 25 ND
Phenanthrene ug/L 5.0 ND
Anthracene ug/L 5.0 ND
Di-n-butyl phthalate ug/L 5.0 ND
Fluoranthene ug/L 5.0 ND
Benzidine ug/L 50 ND
Pyrene ug/L 5.0 ND
Benzyl butyl phthalate ug/L 5.0 ND
3,3-Dichlorobenzidine ug/L 10 ND
Benz[a]anthracene ug/L 5.0 ND
Chrysene ug/L 5.0 ND
bis(2-Ethylhexyl )phthalate ug/L 5.0 ND
Di-n-octylphthalate ug/L 5.0 ND
Benzo[b]fluoranthene ug/L 5.0 ND
Benzo[k]fluoranthene ug/L 5.0 ND
Benzo[a]pyrene ug/L 5.0 ND
Indeno[1,2,3-cd]pyrene ug/L 5.0 ND
Dibenz[a,h]anthracene ug/L 5.0 ND
Benzo[g,h,i]perylene ug/L 5.0 ND
Surrogate - 2-Fluorophenol % 36
Surrogate - Phenol-d5 % 26
Surrogate - Nitrobenzene-d5 % 65
Surrogate - 2-Fluorobiphenyl % 72
Surrogate - 2,4,6-Tribromophenol % 89
Surrogate - Terphenyl-d14 % 98
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 32 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
BASE/NEUTRALS AND ACIDS
Batch: 92 63839
Samples: 92 0183215, 92 0183223, 92 0183231
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter Units PRL Value Recv Recv RPD
N-Nitrosodimethylamine ug �.0 50 44% 13%
bis(2-Chloroethyl)ether ug/L 5.0 50 74% 78% 5%
Phenol ug/L 5.0 50 32% 34% 6%
2-Chlorophenol ug/L 5.0 50 68% 74% 8%
1,3-Dichlorobenzene ug/L 5.0 50 60% 66% 10%
1,4-Dichlorobenzene ug/L 5.0 50 62% 70% 12%
1,2-Dichlorobenzene ug/L 5.0 50 64% 70% 9%
bis(2-Chloroisopropyl)ether ug/L 5.0 50 74% 84% 13%
Hexachioroethane ug/L 5.0 50 58% 64% 10%
N-Nitrosodi-n-propylamine ug/L 5.0 50 80% 86% 7%
Nitrobenzene ug/L 5.0 50 68% 72% • 6%
3,5,5-Trimethyl-2-cyclohexanone ug/L 5.0 50 70% 76% 8%
2-Nitrophenol ug/L 5.0 50 64% 76% 17%
2,4-Dimethylphenol ug/L 5.0 50 70% 72% 3%
bis(2-Chloroethoxy)methane ug/L 5.0 -50 68% 74% 8%
2,4-Dichlorophenol ug/L 5.0 50 68% 78% 14%
1,2,4-Trichlorobenzene ug/L 5.0 50 64% 68% 6%
Naphthalene ug/L 5.0 50 70% 78% 11%
Hexachlorobutadiene ug/L 5.0 50 56% 60% 7%
4-Chloro-3-methylphenol ug/L 5.0 50 80% 90% 12%
Hexachlorocyclopentadiene ug/L 10 50 28% 40% 35%
2,4,6-Trichlorophenol ug/L 5.0 50 68% 80% 16%
2-Chloronaphthalene ug/L 5.0 50 70% 82% 16%
Acenaphthylene ug/L 5.0 50 72% 80% 11%
Dimethyl phthalate ug/L 5.0 50 84% 96% 13%
2,6-Dinitrotoluene ug/L 5.0 50 78% 92% 16%
Acenaphthene ug/L 5.0 50 78% 84% 7%
2,4-Dinitrophenol ug/L 25 50 46% 68% 39%
2,4-Dinitrotoluene ug/L 5.0 50 86% 106% 21%
4-Nitrophenol ug/L 25 50 36% 44% 20%
Fluorene ug/L 5.0 50 84% 92% 9%
4-Chiorophenyl phenyl ether ug/L 5.0 50 78% 92% 16%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 33 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
BASE/NEUTRALS AND ACIDS
Batch: 92 63839
Samples: 92 0183215, 92 0183223, 92 0183231
LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:
Reference Dupl
Parameter Units PRL Value Recv Recv RPD
Diethyl phthalate ug/L 5.0 50 88% 98% 11%
2-Methyl-4,6-dinitrophenol ug/L 25 50 72% 92% 24%
N-Nitrosodiphenylamine ug/L 5.0 50 78% 90% 14%
4-Bromophenyl phenyl ether ug/L 5.0 50 84% 98% 15%
Hexachlorobenzene ug/L 5.0 50 84% 88% 5%
Pentachlorophenol ug/L 25 50 74% 92% 22%
Phenanthrene ug/L 5.0 50 86% 94% 9%
Anthracene ug/L 5.0 50 84% 96% 13%
Di-n-butyl phthalate ug/L 5.0 50 90% 98% 9%
Fluoranthene ug/L 5.0 50 92% 100% 8%
Benzidine ug/L 50 100 196% 208% . 6%
Pyrene ug/L 5.0 50 84%. 106% 23%
Benzyl butyl phthalate ug/L 5.0 50 86% 100% 15%
3,3-Dichlorobenzidine ug/L 10 100 82% 99% 19%
Benz[a]anthracene ug/L 5.0 50 82% 100% 20%
Chrysene ug/L 5.0 50 82% 100% 20%
bis(2-Ethylhexyl )phthalate ug/L 5.0 50 80% 94% 16%
Di-n-octylphthalate ug/L 5.0 50 88% 94% 7%
Benzo[b]fluoranthene ug/L 5.0 50 92% 96% 4%
Benzo[k]fluoranthene ug/L 5.0 50 88% 88% 0%
Benzo[a]pyrene ug/L 5.0 50 86% 96% 11%
Indeno[1,2,3-cd]pyrene ug/L 5.0 50 78% 96% 21%
Dibenz[a,h]anthracene ug/L 5.0 50 76% 96% 23%
Benzo[g,h,i]perylene ug/L 5.0 50 76% 90% 17%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 34 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
VOLATILE ORGANICS
Batch: 92 64014
Samples: 92 0183223, 92 0183231
METHOD BLANK:
Method
Parameter Units PRL Blank
Chloromethane ug/L ST6 ND
Chloroethene (Vinyl chloride) ug/L 5.0 ND
Bromomethane ug/L 5.0 ND
Chloroethene ug/L 5.0 ND
Trichlorofluoromethane ug/L 5.0 ND
1,1-Dichloroethene ug/L 5.0 ND
Dichloromethane ug/L 5.0 ND
trans-1,2-Dichloroethene ug/L 5.0 ND
1,1-Dichloroethane ug/L 5.0 ND
cis-1,2-Dichloroethene ug/L 5.0 ND
Chloroform ug/L 5.0 ND -
1,1,1-Trichloroethane ug/L 5.0 ND
1,2-Dichloroethane ug/L 5.0 ND
Carbon tetrachloride ug/L 5.0 ND
Benzene ug/L 5.0 ND
Trichloroethene ug/L 5.0 ND
1,2-Dichloropropene ug/L 5.0 ND
Bromodichloromethane ug/L 5.0 ND
2-Chloroethoxyethene ug/L 10 ND
cis-1,3-Dichloropropene ug/L 5.0 ND
Toluene ug/L 5.0 ND
trans-1,3-Dichloropropene ug/L 5.0 ND
1,1,2-Trichloroethane ug/L 5.0 ND
Dibromochloromethane ug/L 5.0 ND
Tetrachloroethene ug/L 5.0 ND
Chlorobenzene ug/L 5.0 ND
Ethylbenzene ug/L 5.0 ND
Bromoform ug/L 5.0 ND
1,1,2,2-Tetrachloroethane ug/L 5.0 ND
1,3-Dichlorobenzene ug/L 5.0 ND
1,4-Dichlorobenzene ug/L 5.0 ND
1,2-Dichlorobenzene ug/L 5.0 ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 35 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
VOLATILE ORGANICS
Batch: 92 64014
Samples: 92 0183223, 92 0183231
METHOD BLANK:
Method
Parameter Units PRL Blank
Surrogate - Dibromofluoromethane % 100
Surrogate - Toluene-d8 % 99
Surrogate - Bromofluorobenzene % 99
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Chloromethane ug/L 5.0 20 100%
Chloroethene (Vinyl chloride) ug/L 5.0 20 100%
Bromomethane ug/L 5.0 20 110%
Chloroethane ug/L 5.0 20 95% .
Trichlorofluoromethane ug/L 5.0 20 85%
1,1-Dichloroethene ug/L 5.0 20 90%
Dichloromethane ug/L 5.0 20 90%
trans-1,2-Dichloroethene ug/L 5.0 20 90%
1,1-Dichloroethane ug/L 5.0 20 95%
cis-1,2-Dichloroethene ug/L 5.0 20 115%
Chloroform ug/L 5.0 20 100%
1,1,1-Trichloroethane ug/L 5.0 20 100%
1,2-Dichloroethane ug/L 5.0 20 100%
Carbon tetrachloride ug/L 5.0 20 105%
Benzene ug/L 5.0 20 100%
Trichloroethane ug/L 5.0 20 120%
1,2-Dichloropropane ug/L 5.0 20 100%
Bromodichloromethane ug/L 5.0 20 95%
2-Chloroethoxyethene ug/L 10 40 393%
R1
cis-1,3-Dichloropropene ug/L 5.0 20 95%
Toluene ug/L 5.0 20 100%
trans-1,3-Dichloropropene ug/L 5.0 20 90%
1,1,2-Trichloroethane ug/L 5.0 20 95%
Dibromochloromethane ug/L 5.0 20 90%
Tetrachloroethene ug/L 5.0 20 90%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 36 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
VOLATILE ORGANICS
Batch: 92 64014
Samples: 92 0183223, 92 0183231
•
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Chlorobenzene ug/L 5.0 20 85%
Ethylbenzene ug/L 5.0 20 85%
Bromoform ug/L 5.0 20 90%
1,1,2,2-Tetrachloroethane ug/L 5.0 20 90%
1,3-Dichlorobenzene - ug/L 5.0 20 100%
1,4-Dichlorobenzene ug/L 5.0 20 100%
1,2-Dichlorobenzene ug/L 5.0 20 100%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 37 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
VOLATILE ORGANICS
Batch: 92 64229
Samples: 92 0183215, 92 0183240, 92 0183258
METHOD BLANK:
Method
Parameter Units PRL Blank
Chloromethane ug/L 5.0 ND
Chloroethene (Vinyl chloride) ug/L 5.0 ND
Bromomethane ug/L 5.0 ND
Chloroethane ug/L 5.0 ND
Trichlorofluoromethane ug/L 5.0 ND
1,1-Dichloroethene ug/L 5.0 ND
Dichloromethane ug/L 5.0 ND
trans-1,2-Dichloroethene ug/L 5.0 ND
1,1-Dichloroethane ug/L 5.0 ND
cis-1,2-Dichloroethene ug/L 5.0 ND
Chloroform ug/L 5.0 ND
1,1,1-Trichloroethane ug/L 5.0 ND
1,2-Dichloroethane ug/L 5.0 ND
Carbon tetrachloride ug/L 5.0 ND
Benzene ug/L 5.0 ND
Trichloroethene ug/L 5.0 ND
1,2-Dichloropropane ug/L 5.0 ND
Bromodichloromethane ug/L 5.0 ND
2-Chloroethoxyethene ug/L 10 ND
cis-1,3-Dichloropropene ug/L 5.0 ND
Toluene ug/L 5.0 ND
trans-1,3-Dichloropropene ug/L 5.0 ND
1,1,2-Trichloroethane ug/L 5.0 ND
Dibromochloromethane ug/L 5.0 ND
Tetrachloroethene ug/L 5.0 ND
Chlorobenzene ug/L 5.0 ND
Ethylbenzene ug/L 5.0 ND
Bromoform ug/L 5.0 ND
1,1,2,2-Tetrachloroethane ug/L 5.0 ND
1,3-Dichlorobenzene ug/L 5.0 ND
1,4-Dichlorobenzene ug/L 5.0 ND
1,2-Dichlorobenzene ug/L 5.0 ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 38 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
VOLATILE ORGANICS
Batch: 92 64229
Samples: 92 0183215, 92 0183240, 92 01832/58
METHOD BLANK:
Method
Parameter Units PRL Blank
Surrogate - Dibromofluoromethane % 111
Surrogate - Toluene-d8 % 108
Surrogate - Bromofluorobenzene % 102
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl
Parameter Units PRL 930459048 Spike Recv Recv RPD
Chloromethane ug/L S.0 ND 20 115% 120% 4%
Chloroethene (Vinyl chloride) ug/L 5.0 ND 20 105% 120% 13%
Bromomethane ug/L 5.0 ND 20 100% 115% .14%
Chloroethane ug/L 5.0 ND 20 95% 110% 15%
Trichiorofluoromethane ug/L 5.0 ND 20 85% 95% 11%
1,1-Dichloroethene ug/L 5.0 ND 20 90% 100% 11%
Dichloromethane ug/L 5.0 ND 20 80% 90% 12%
trans-1,2-Dichloroethene ug/L 5.0 ND 20 90% 100% 11%
1,1-Dichloroethane ug/L 5.0 ND 20 90% 100% 11%
cis-1,2-Dichloroethene ug/L 5.0 ND 20 100% 110% 10%
Chloroform ug/L 5.0 ND 20 95% 100% 5%
1,1,1-Trichloroethane ug/L 5.0 ND 20 80% 90% 12%
1,2-Dichloroethane ug/L 5.0 ND 20 90% 105% 15%
Carbon tetrachloride ug/L 5.0 ND 20 85% 105% 21%
Benzene ug/L 5.0 ND 20 90% 100% 11%
Trichloroethene ug/L 5.0 ND 20 90% 100% 11%
1,2-Dichloropropane ug/L 5.0 ND 20 90% 105% 15%
Bromodichloromethane ug/L 5.0 ND 20 85% 95% 11%
cis-1,3-Dichloropropene ug/L 5.0 ND 20 75% 90% 18%
Toluene • ug/L 5.0 ND 20 85% 100% 16%
trans-1,3-Dichloropropene ug/L 5.0 ND 20 75% 90% 18%
1,1,2-Trichloroethane ug/L 5.0 ND 20 85% 95% 11%
Dibromochloromethane ug/L 5.0 ND 20 80% 90% 12%
Tetrachloroethene ug/L 5.0 ND 20 75% 90% 18%
Chlorobenzene ug/L 5.0 ND 20 80% 85% 6%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 39 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
VOLATILE ORGANICS
Batch: 92 64229
Samples: 92 0183215, 92 0183240, 92 0183258
SPIKE AND SPIKE DUPLICATE:
Spike
Spike Dupl
Parameter Units PRL 930459048 Spike Recv Recv RPD
Ethylbenzene ug/L �.0 ND 20 80% 90% 12%
Bromoform ug/L 5.0 ND 20 75% 85% 13%
1,1,2,2-Tetrachloroethane ug/L 5.0 ND 20 90% 100% 11%
1,3-Dichlorobenzene ug/L 5.0 ND 20 90% 100% 11%
1,4-Dichlorobenzene ug/L 5.0 ND 20 90% 105% 15%
1,2-Dichlorobenzene ug/L 5.0 ND 20 85% 110% 26%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv -
Chloromethane TOE- 5.0 20 140%
Chloroethene (Vinyl chloride) ug/L 5.0 20 140%
Bromomethane ug/L 5.0 20 130%
Chloroethane ug/L 5.0 20 120%
Trichiorofluoromethane ug/L 5.0 20 100%
1,1-Dichloroethene ug/L 5.0 20 110%
Dichloromethane ug/L 5.0 20 105%
trans-1,2-Dichloroethene ug/L 5.0 20 105%
1,1-Dichloroethane ug/L 5.0 20 110%
cis-1,2-Dichloroethene ug/L 5.0 20 105%
Chloroform ug/L 5.0 20 110%
1,1,1-Trichloroethane ug/L 5.0 20 100%
1,2-Dichloroethane ug/L 5.0 20 115%
Carbon tetrachloride ug/L 5.0 20 110%
Benzene ug/L 5.0 20 110%
Trichloroethene ug/L 5.0 20 105%
1,2-Dichloropropane ug/L 5.0 20 115%
Bromodichloromethane ug/L 5.0 20 110%
2-Chloroethoxyethene ug/L 10 40 78%
cis-1,3-Dichloropropene ug/L 5.0 20 115%
Toluene ug/L 5.0 20 110%
trans-1,3-Dichloropropene ug/L 5.0 20 115%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
Pace Analytical 9800 Kincey Avenue,Suite 100
Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb QUALITY CONTROL DATA September 25, 1997
Page 40 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
VOLATILE ORGANICS
Batch: 92 64229
Samples: 92 0183215, 92 0183240, 92 0183258
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
1,1,2-Trichloroethane ug/L 5T 20 115%
Dibromochloromethane ug/L 5.0 20 105%
Tetrachloroethene ug/L 5.0 20 90%
Chlorobenzene ug/L 5.0 20 95%
Ethylbenzene ug/L 5.0 20 95%
Bromoform ug/L 5.0 20 105%
1,1,2,2-Tetrachloroethane ug/L 5.0 20 110%
1,3-Dichlorobenzene ug/L 5.0 20 115%
1,4-Dichlorobenzene ug/L 5.0 20 115%
1,2-Dichlorobenzene ug/L 5.0 20 115%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville, NC 28078
Tel:[phone]
Fax:[phone]
Mr. Bobby Lamb FOOTNOTES September 25, 1997
Page 41 for pages 19 through 40 PACE Project Number: 670911580
Client Reference: Monitoring Wells September 1997
NC No calculation due to value below detection limit.
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
R1 Recovery falls outside the quality control limit, however, this compound is not
detected in the associated sample(s) .
RPD Relative Percent Difference
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

PASI, Inc Charlotte September 23, 1997
9800 Kincey Avenue, Suite 100 PACE Project Number: 670911580
Huntersville, NC 28078 NC Wastewater Lab Cert. #40
NC Drinkingwater Lab Cert. #37712
SC Lab Cert. #99030
Attn: Project Management
Client Reference: Crompton & Knowles
PACE Sample Number: 92 0183215
Date Collected: 09/11/97
Date Received: 09/15/97
Client Sample ID: MW-1
Parameter Units PRL C&K METHOD DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Phenol mg/L 0.005 ND 420.1 09/17/97
Total Organic Carbon mg/L 1.0 1..8 5310C 09/16/97
PACE Sample Number: 92 0183223
Date Collected: 09/11/97
Date Received: 09/15/97
Client Sample ID: MW-2
Parameter Units PRL C&K METHOD DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Phenol mg/L 0.005 ND 420.1 09/16/97
Total Organic Carbon mg/L 1.0 3.6 5310C 09/16/97

Project Management September 23, 1997
Page 2 PACE Project Number: 670911580
Client Reference: Crompton & Knowles
PACE Sample Number: 92 0183231
Date Collected: 09/11/97
Date Received: 09/15/97
Client Sample ID: MW-3
Parameter Units PRL C&K METHOD DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Phenol mg/L 1.6 16 420.1 09/17/97
Total Organic Carbon mg/L 20 2900 5310C 09/16/97
These data have been reviewed and are approved for release.
Walter L. Miller
Operations Manager

Project Management FOOTNOTES September 23, 1997
Page 3 for pages 1 through 2 PACE Project Number: 670911580
Client Reference: Crompton & Knowles
ND Not detected at or above the PRL.
PRL PACE Reporting Limit

Project Management QUALITY CONTROL DATA September 23, 1997
Page 4 PACE Project Number: 670911580
Client Reference: Crompton & Knowles
Phenol
Batch: 93 47021
Samples: 92 0183223
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units PRL Blank 920183916 92 0183916 RPD
Phenol mg/L 0.005 ND 0.020 0.020 0%
SPIKE:
920183223
MW-2 Spike
Parameter Units PRL C&K Spike Recv
Phenol mg/L 0.005 ND 0.025 112%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Phenol mgmg L 0.005 0.025 1 9

Project Management QUALITY CONTROL DATA September 23, 1997
Page 5 • PACE Project Number: 670911580
Client Reference: Crompton & Knowles
Phenol
Batch: 93 47063
Samples: 92 0183215, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
920183231 Duplicate
Method MW-3 of
Parameter Units PRL Blank C&K 92 0183231 RPD
Phenol mg/L 0.005 ND
Phenol mg/L 1.6 16
Phenol mg/L 1.7 17 6%
SPIKE:
920183215
MW-1 Spike
Parameter Units PRL C&K Spike Recv
Phenol mg/L 0.005 ND 0.025 92%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Phenol mg/L 0.005 0.025 96%

Project Management QUALITY CONTROL DATA September 23, 1997
Page 6 PACE Project Number: 670911580
Client Reference: Crompton & Knowles
Total Organic Carbon
Batch: 93 47020
Samples: 92 0183215, 92 0183223, 92 0183231
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units PRL Blank 920181905 92 0181905 RPD
Total Organic Carbon mg/L 0.5 ND 0.82 0.84 2%
SPIKE:
Spike
Parameter Units PRL 920181905 Spike Recv
Total Organic Carbon mgmg/L 01.6 0.82 2.00 104%
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units PRL Value Recv
Total Organic Carbon mg/L 0.5 5.000 101%

Project Management FOOTNOTES September 23, 1997
Page 7 • for pages 4 through 6 PACE Project Number: 670911580
Client Reference: Crompton & Knowles
ND Not detected at or above the PRL.
PRL PACE Reporting Limit
RPD Relative Percent Difference

•
376659
Pace Analytical
CHAIN-OF-CUSTODY RECO
RD
Analytical Request
Report To: '�
Client C f U`M plc— -f'� A.c L,J e I '' f l' UvV L�'� v Pace Client No. �O/�i�' �/
Address P 0 . v F�,1 Bill To: Pace Project Manager �/'/W
p W P!/// A/✓ p P.O.#/Billing Reference Pace Project No. �O 9�� S� U
Phone (Fog) e2 l7 q5"a. b Project Name/No. ,G�r i rr�7 �✓{/�„) 'Requested Due Date:
co Sampled By(PRINT): PRESERVATIVES ANALYSES ��
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Sam ler Si atur Date Sampled 7 4/,//� ze`ec
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REMARKS
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COOLER NOS. BAILERS SHIPMENT METHOD ITEM RELINQUISHED BY/AFFILIATION ACCEPTED BY/AFFILIATION DATE TIME
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Additional Comments '° JIPIIP ;,� � ,;: ,,,,
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PL CE.REPO T. F0RM s = . a� . *.--, . `' . fAL!l iGH;'No; 2r3-tt$7 ... Ph n ..( )
FACILITY INFORMATION . Please Print Clearly or Type� PERM(T#: EXPIRATION DATE: �5-31-1998
Facility Name:. • • Crompton& Knowles colors inco prated Non-Discharge UIC
(0 Permit Name(ii different): M b NPIJES Dif'D0Q5�79
FacilityAddress: 1602 North Main Street �
- Lo ell "' NC 280 County Gaston TYPE OF Pf�BMiTTED OPERATION BEING MONITOREDDEC •r'-•Cl`
t Bobby Lamb '• t �•► Telephone [phone] Ext 60 �9 Remediaton:Infiltration Gallery
Contact Person: p Spray Field X name:naaa►:.Pump/Ad Treat Method ran
Well LI:cation/Site Name: Up Gradient No.of Wells to be Sampled:Hromp3emik_ Rotary Distributor Land App!icatton of Sludge c f t-i
Well Identificatloh'Number(from Permit): MW-I For Groundwater Treatment Systems Other: (-) {''
Well Depth: 100 ft. Well Diameter._____Iy..2 in- Check One:
• Screened Interval: - 90 ft.to 100 ft. 0 Influent (98) NOTE; Values should reflect dissolved and rv. `•_'
Depth to Water Levee 92 68 ft.beloty.measuring point. ElEffluent (99) colloidal concentrations. `O' N
Measuring Point is '' -0 ft.above land surface.
Gallons of water pumped/bailed before sampling: 5.5 Date sample collected: r19 0A-9R Date sample.anaiyied:0 9-9g
Field analysis. pH',6 77 ,Specific Conductance 276 uMhos Laboratory Name:Pace Analytical Laboratory
Temp. 18 5 °C,Odor Nnnp Appearance Slightly Turbid Certification No. 12 cr..)
pARAM Iffl (Samples for metals were collected unfiltered X YES NO and field acidified .._.I__( YES NO)
COD • .. <25 mgll Nitrite (NO2) as N . . NA mg/I Ni-Nickel . NA mg/1
Cotiform: Mt Fecal • NA /10Om1 Nitrate (NO3) as N NA mg/I Pb-Lead <0.005 mg/I
Cotiform: MF Total NA ./100m1 Phosphorus:Total as P N A mg/1 Zn-Zinc - 0.029 mgn
(Note:Use MPN method for hlgtdy turbid samples) Orthophosphate NA mg/1 Ammonia Nitrogen - N A mg/I •
Dissolved-Solids:Total ‘ '220 mgn Al-Aluminum NI mg/1 Other (Specify Compounds and Concentration Units) '.
pH (when analyzed) . . NA units Ba- Barium NA_ mg/1 Total Su s.pended Solids 110 411g/1 ' -
TOC ' ' 3.2 mg/I Ca - Calcium -DJA mg/l .
Chloride ' ' 3.6 mgn Cd-Cadmium NA mg/1 ••
Arsenic - • NA- mull Chromium: Total <0.01 mg/I -_ " . .
Grease and Oils '37 mg/I Cu-Copper 0.036 mg/1
-
Phenol <0.005 tng/I Fe- Iron NA mg/I ORGANICS: (GC,GC/MS,HPLC) •
Sulfate <5 _mg/1 Hg -Mercury NA mg/1 (Specify test and method#.Attach lab report.)
Specific Conductance
-
N A uMhos K- Potassium NA _mg/I Report Attached? Yes. :(1) No (0). .-
Total Ammonia N A mg/I Mg-Magnesium- NA_ mg/I VOC : method# Q
TKN as N •- NA mg/I Mn -Manganese N A mg/1 S P.rn \t?3C_ _: method#' • 2.
• : method#
I certify that,to the best of my knowledge and belief,the information submitted In this report is true,accurate,and complete,and that the laboratory analytical data was producsd
ktising approved methods of analysis by a North Carolina D1Nq(formerly DEM)certified laboratory,i am aware that there are significant penalties for submitting false lnfprmatlon, •
:including the possibility of fines and imprisonment for knowing violations. - • -
• 1 ►its 'ttchan Plan Mapaper
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. . * fermi =: l• .ho nl ame die-React print or typo . . - -
GW 59 Rev.4196 1 etmo/" .4 u :o r Authorized Agent) pato)

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FAC1LITY IUFORMATIOI4 Please Print Clearly or Type --
Facility Name:_ ' ' Crompton&•Knowles Colors lnco►Uorated PEIRMir II: EXPIRATION UAIE: (S-31-1998
Permit Name(if different): Non-Discharge UIC___�
1602 North Mai►i Street NPUESJL0005?7 _----._-..__
Facility Address: .
Lc� 11 (su«+' 1(; ?809S County (iastou BIT.OF PE.BMl it ,u OPERA!ION BEING MO N1I t ORED . .
Contact Person: Bobby Lamb t op) Telephone#: 70<I-824-9526 Ext * --- Lagoon _Rernedialon:�Infiltration Gallery
Well Location/Site Name: Duwit Gradic;tlt No.of Welts to be Sampled: Spray Field X nemediation:lslt�tpirLid i'teatf�lt alls�cl
• 1O;,e'rr'!t Rotary Distributor Land Application of Sludge •
Well identilicatioh'Number(from Permit): MW-3 rcFo„ecGkr°Qumn
dwater Treatment Systems _ _ Other:
Well Depth: ` - • • 27. 1 ft. Well Diameter: 2-In. :
Screened Interval: • 17 1 ft to 27 11E Influent (98) go 1 i values should reflect dissolved and ' ' -.
Depth to Water Levek 18.78 it.belovtr.measuring paint. Effluent (99) colloidal concentrations.
Measuring Point Is ' ' 1-5 ft,above land surface. •
)`) (,S-<)g Date Sarlrple ataalyzed:t►`)-tiu-fit
Gallons of water pumpedlbailed before sampling: 4.0 Date sample collected:
Field analysis:. pH';8 48 ,Specific t onductance. 10500 uMhos Laboratory Name: Pace AnalvtjcaL(.akw itoty , r s
Temp. 16 7 °C,Odor Chemical Appearance Black Certification No. 1,2 •
Y
PARAMETt,$M(Samples for metals were collected unfiltered X YES NO and field acidified X `YES _NO)
COD - . 5700 mg/I Nitrite (NO2) as N NA mg/ NI Nickel . _.-_. = NA trig/I
Conform: MI±Fecal • NA /10Om1 Nitrate (NO3) as N NA mg/ Pb-Lead , 0 Q. 7 tog/1
Colitorm: MF Total NA_/100rn1 Phosphorus:Total as P N a rrtg! Zn-Zinc ._� 0117 mg/I
tNote:Use MPH method for highly turbid samples) Orthophosphate N A rug/ Ammonia Nitrogen__.. _ t. .L (\L\ rng/l -
Dissolve dSolids:Total 20000 mg/I AI-Aluminum N A Mg/ Other(Specify Comp'>unds and Concentration Units)-.
pH (when analyzed) . - • NA units Ba-Barium .NA. mg/ :halal.Suspeuili'.cr._Solids._ .2200 jay"!
TOC - 3280 mg/i Ca - Calcium NA� rig/ --_._____ -__.
Chloride •. . 83300 mg/I Cd-Cadmium_ _N, mg/ SeeAtlacl)tnval __�__. ___.._._.__
Arsenic • - NA _ mg/I Chromium: Total 0.29 mg/ —
Grease and.Oils . g 4 mg/I Cu- Copper 2.9 mg/ y _____ •
.....__ ___:___ .
Phenol mg/I Fe- Iron.___ NA ti lug! ORGANICS: (CGC,GC/Ms,l u'I_c.�l '
Sulfate _ 130Q.,.,mg/I - Hg -Mercury .- NA lug! (Specify test and method ff. Attach lab let)ort.) '
Specific Conductance . - . N A uMhos K- Potassium NA mg/ Report Attached? Yes_ _-..(i) No______(0).
Total Ammonia N A mg/I Mg-Magnesium NA mg/ VOC : nr'uurri If . , -.r LI '
TKN as N •. N A mg/I Mn-Manganese _ N A, ntg/l 2) _t rk, \I (,)C, : method#r /�,1-i ___^
method#-
I r _ , p true,at curdle;and bbtlpiete,and that the laboratory enelyticsl'deta tr/as prt5duced
Sind y that,tdthi etha t of my alyti fb ya and b C Old
M atottiielty bt M)Eertttled labotatatl,I ftltti aware that 1H9 a ere bIdtllticatl( etiallies'tit subirllltlli lai'sti lhfdr 1 rt
using approved Itipthbus at analy�l�by r1 N lift, � ., .
p ., �. . mkt Ij ,
includitig the passlbIlity of fines and tifit rlstmrttatit Eot lotWit t Ibtatif its, ,
a and title T't7r a,,t tan ) �-,� -
•
ennriie Arrll ized ngerrq Plea print or type •
., 2 cf' � ) l
GW-59 Rev.4/96 I n ru o er r to, orAultwrize ry gent if,7 ` /L� t l` /�-'�
9 ( 9 ) I / (Darn) •

Attachment To MW-3 GMR
Benzene 650 ug/L
Chlorobenzene 120 ug/L
1,2-Dichlorobenzene 67 ug/L
• Phenol 5000 ug/L
1,2,4-Trichlorobenzene 4600 ug/L
Benzidine 55000 ug/L

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FACILITY INFORMATION Please Print Clearly or Type PERMIT#: EXPIRATION DATE: 05-31-1998
Facility Name:. • Crompton&-Knowles Colors incorporated Non discharge U1C
Permit Name(if dilleretit): NP[7�S 1�C 0005�79
Facility Address: 1602 North Main Street
Lowell Preece
Nci NC 280�t X County Gaston TYPE OF PERMITTED OPERATION BEING MONITORED
Bobby Lamb ••• t Tele one#: 704-824-9526 Ext 60 Lagoon Rer'nediation:infiltration Gallery
•
Contact Person: pit Spray Field X Remedlatlar. Pump sand Treat MOM •
Well Location/Site Name: Down Gradient No.of Wells to be Sampled:RramPe
•
. �°} Rotary Distributor Land Application of Sludge c o
Well ldentiflcatroh•Number(from Permit): MW-2 _ For Groundwater Treatment Systems Other:
. Well Depth: . .• • •-29, ft. Well Diameter: 2 in. - - O . •
Check One: N- ,
Screened Interval: - 19 ft.to 29 ft. 0 Influent (98) iIOTE; Values should reflect dissolved and
Depth to Water Levee 19.48 tt belouy.measuring point. ❑ Effluent (99) colloidal concentrations.
Measuring Point is ' ' 1-5 ft.above land surface. -
Gallons of water pumped/bailetif before samplIng: 5.4 Date sample collected: 99-08 98 Date sample analyzed:04 -9R
Field analysis:. pH',6 22 ,Specific Conductance 473 uMhos Laboratory Name: Pace Analytical Laboratory . ` '
- Temp. 16 5 °C,Odor Nnnp Appearance Turbid Certification No. 12 en
rAflAMcrg.n (Samples for metals were collected unfiltered X YES NO and field acidified X YES NO) -. r _i-
COD 32 mgll Nitrite (NO2)as N NA mg/I NI-Nickel • NA' 'mg/1
Colitorm: M1 Fecal - NA /100m1 Nitrate (NO3) as N NA mg/I Pb- Lead • �.�x0.005-mgll
Coliform: MF Total NA_l100m) Phosphorus: Total as P NA mg/I Zn-Zinc �—; 0.966'mg/l
(Nets:Use MPN method for highly turbid samples) Orthophosphate NA mg/I Ammonia Nitrogen - •• lNf A--mg/l •
Dissolved-Solids:Total , •320 mg/l Al-Aluminum N A. ing11 Other(Specify Compounds and Cooenirrtlon Units)'. '.
pH (when analyzed) . . - ' NA units Ba-Barium NA - mg/1 Tnta1 s11.spe. deL Snlidg 1100 i•n Jl • '•
TOC 5.9 mg/I Ca- Calcium NA mg/I Methylene Chloride 5.1 ug7i
Chloride • ' • 80 mg/1 Cd-Cadmium NA mg/1 .
Arsenic - ' NA -mg/I Chromium: Total 0.012 mg/I , ' • •
Grease and Oils . `-5 mg/I Cu- Copper 0.074 mg/I - . •
Phenol - '0.005 mg/I Fe- iron NA mg/I ORGANICS: (OC,GC/MS,HPLC) -
Sulfate 20 mg/I Hg -Mercury NA mg/l (Specify test and method#.Attach lab report.)
Specific Conductance - - • . l A uMhos K- Potassium NA mg/I Report Attached? Yes x-(1) No (0}. -
Total Ammonia N A mg/I Mg-Magnesium NA, mg/I VOC : method#.• -• Co 2..4•'
TKN as N •- NA mg/I Mn-Manganese NA mg/I �c-'„n, V OC_ : method#R /0-2,5 -
: method#_
_ -
I certify that,to the best of my knowledge and belief,the information submitted In this report Is true,accurate,and complete, and that the laboratory analytical dpta was produced
using.approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory,I am aware that there are significant penalties`or submitting false information,
including the possibility of fines and imprisonment for knowing violations. . .
i.r they Buchana P . .t Mapaper
J . Pe a Aufhor(xe�i A .nl ame: ir Title-Plloa a print or typo , •, . • '
GW-59 Rev.4/99 - }v�`s ( /1 a„--._
Q„T� /oho /q . . '
• Sign a o� emviee( ts razed •gent) L' S C (Oatej •

i
E.xdfill.4/ CROMPTON & KNOWLES COLORS INCORPORATED
P.O. Box 848 N. Main St.)
Lowell, NC 28098098, USA
704-824-9526 • Fax: [phone]
COLORS www.ckcolors.com
October 28, 1998
Ms. Betty Wilcox
Environmental Chemist .�, ' ,
Groundwater Section ` -
0
Permits and Compliance Unit
P.O. Box 29578 a -
Raleigh, North Carolina 27626-0578 ham, -=_
•• C .
N _{
Subject: Groundwater Monitoring Report r,,
Dear Ms. Wilcox:
Enclosed you will find the Groundwater Monitoring Report for our facility located in Lowell,
North Carolina. This groundwater monitoring fulfills the current NPDES permit (NC0005274)
groundwater monitoring requirements and the remedial monitoring requirements of the site
Corrective Action Plan as approved by the NCDEM-Mooresville Regional office.
The report of laboratory analysis for MW-3 indicated in footnote (3) that the response to
benzidine by EPA Method 625 was over the calibration range for this compound. The
reported results for this compound should be considered an estimate. We have arranged to
have this monitoring well re-sampled on October 29th and analyzed again for this compound.
We will submit results of this analysis as soon as they are available.
If you have any questions, please do not hesitate to contact me at 704-824-9526, ext. 40.
Sincerely,
"td i'l (04-(6,
Rodney Lang
Manager of Environmental Operations
cc: Luther Buchanan
Barry Dobinsky
Matt Joyner
Bobby Lamb

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
September 24, 1998
Mr. Bobby Lamb
Crompton & Knowles
P.O. Box 848
1602 N. Main St.
Lowell, NC 28098
RE: Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
Dear Mr. Lamb:
Enclosed are the results of analyses for sample(s) received by the laboratory on September 8. 1998. If you have any
questions concerning this report, please feel free to contact me.
Sincerely.
Ofj,CQ/2--
(61
Kelly Wallace
• Project Manager
Enclosures
Laboratory Certification IDs j oratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TKY Drinking N UST ListWater 90090
NC Drinking Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

I
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 1
^ompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
SO2 N. Main St.
well, NC 28098
ttn: Mr. Bobby Lamb
lone:
Aid results are reported on a wet weight basis
ace Sample No: 92101443 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-1 Date Received: 09/08/98
3rameters Results Units PRL Analyzed Analyst CAS# Footnotes
field Services
Monitoring Well Data Method: Prep Method:
Field pH 6.77 Std. Units 09/08/98 JJQ
Field Specific Conductance 276 umhos/cm 09/08/98 JJQ
Field Temperature 18.5 deg C 09/08/98 JJQ
Static Water Level 92.68 feet 09/08/98 JJQ
•
etals
ICP Metals Method: EPA 200.7 Prep Method: EPA 3010
Chromium ND mg/L 0.01 09/16/98 AB1 7440-47-3
Copper 0.036 mg/L 0.01 09/16/98 AB1 7440-50-8
Zinc 0.029 mg/L 0.01 09/16/98 AB1 7440-66-6
Date Digested 09/15/98
Lead by Furnace. Method 239.2 Method: EPA 239.2 Prep Method: EPA 200F
Lead ND mg/L 0.005 09/24/98 TYM 7439-92-1
Date Digested 09/21/98
et Chemistry
Total Dissolved Solids Method: EPA 160.1 Prep Method: EPA 160.1
Total Dissolved Solids 220 mg/L 1 09/09/98 JAS 1
Total Suspended Solids Method: EPA 160.2 Prep Method: EPA 160.2
Total Suspended Solids 110 mg/L 1 09/11/98 DRP
Hexane Extractable Material Method: EPA 1664 Prep Method: EPA 3510
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TKY Drinking N UST Lis Water 90090
NC Drinking Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

t
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 2
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ace Sample No: 92101443 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-1 Date Received: 09/08/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
Oil and Grease 37 mg/L 5 09/17/98 JML
Chloride(Mercuric Nitrate) Method: EPA 325.3 Prep Method: EPA 325.3
Chloride 3.6 mg/L 1 09/17/98 DRP
Sulfate.Automated Colorimetric Method: EPA 375.2 Prep Method: EPA 375.2
Sulfate ND mg/L 5 09/16/98 TYM
Chemical Oxygen Demand Method: EPA 410.4 Prep Method: EPA 410.4
Chemical Oxygen Demand ND mg/L 25 09/09/98 TTB
/MS -- VOA
Volatile GC/MS by 624 Method: EPA 624 Prep Method: EPA 624
Chloromethane ND ug/L 5 09/18/98 VFT 74-87-3
Vinyl Chloride ND ug/L 5 09/18/98 VFT 75-01-4
Bromomethane ND ug/L 5 09/18/98 VFT 74-83-9
Chloroethane ND ug/L 5 09/18/98 VFT 75-00-3
Trichlorofluoromethane ND ug/L 5 09/18/98 VFT 75-69-4 _— .
1.1-Dichloroethene ND ug/L 5 09/18/98 VFT 75-35-4
Methylene Chloride ND ug/L 5 09/18/98 VFT 75-09-2
trans-1.2-Dichloroethene ND ug/L 5 09/18/98 VFT 156-60-5
1.1-Dichloroethane ND ug/L 5 09/18/98 VFT 75-34-3
cis-1.2-Dichloroethene ND ug/L 5 09/18/98 VFT 156-59-2
Chloroform ND ug/L 5 09/18/98 VFT 67-66-3
1.1.1-Trichloroethane ND ug/L 5 09/18/98 VFT 71-55-6
1.2-Dichloroethane ND ug/L 5 09/18/98 VFT 107-06-2
Carbon Tetrachloride ND ug/L 5 09/18/98 VFT 56-23-5
Benzene ND ug/L 5 09/18/98 VFT 71-43-2
Trichloroethene ND ug/L 5 09/18/98 VFT 79-01-6
1.2-Dichloropropane ND ug/L 5 09/18/98 VFT 78-87-5
Bromodichloromethane ND ug/L 5 09/18/98 VFT 75-27-4
2-Chloroethyl Vinyl Ether ND ug/L 10 09/18/98 VFT 110-75-8
cis-1.3-Dichloropropene ND ug/L 5 09/18/98 VFT 10061-01-5
Toluene ND ug/L 5 09/18/98 VFT 108-88-3
trans-1.3-Dichloropropene ND ug/L 5 09/18/98 VFT 10061-02-6
1.1.2-Trichloroethane ND ug/L 5 09/18/98 VFT 79-00-5
Dibromochloromethane ND ug/L 5 09/18/98 VFT 124-48-1
Tetrachloroethene ND ug/L 5 09/18/98 VFT 127-18-4
Chlorobenzene ND ug/L 5 09/18/98 VFT 108-90-7
Laboratory Certification IDs Laboratory Certification IDs
NNC
C Waste gater 123'7 REPORT OF LABORATORY ANALYSIS KY Dr'T ugwater 90090
WaSC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

t
Pace Analytical Services,Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 3
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ace Sample No: 92101443 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-1 Date Received: 09/08/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
Ethyl benzene ND ug/L 5 09/18/98 VFT 100-41-4
Bromoform ND ug/L 5 09/18/98 VFT 75-25-2
1,1,2,2-Tetrachloroethane ND ug/L 5 09/18/98 VFT 79-34-5
1.3-Dichlorobenzene ND ug/L 5 09/18/98 VFT 541-73-1
1,4-Dichlorobenzene ND ug/L 5 09/18/98 VFT 106-46-7
1,2-Dichlorobenzene ND ug/L 5 09/18/98 VFT 95-50-1
Dibromofluoromethane (S) 98 X 09/18/98 VFT 1868-53-7
Toluene-d8 (S) 104 X 09/18/98 VFT 2037-26-5
4-Bromofluorobenzene (S) 103 X 09/18/98 VFT 460-00-4
C/MS -- Semi-VOA
Extractables in Water by 625 Method: EPA 625 Prep Method: EPA 625 SF
N-Nitrosodimethylamine ND ug/L 5 09/18/98 DHJ 62-75-9
bis(2-Chloroethyl)ether ND ug/L 5 09/18/98 DHJ 111-44-4
Phenol ND ug/L 5 09/18/98 DHJ 108-95-2
2-Chlorophenol ND ug/L 5 09/18/98 DHJ 95-57-8
1,3-Dichlorobenzene ND ug/L 5 09/18/98 DHJ 541-73-1
1,4-Dichlorobenzene ND ug/L 5 09/18/98 DHJ 106-46-7
1,2-Dichlorobenzene ND ug/L 5 09/18/98 DHJ 95-50-1
bis(2-Chloroisopropyl)ether ND ug/L 5 09/18/98 DHJ 39638-32-9
Hexachloroethane ND ug/L 5 09/18/98 DHJ 67-72-1
N-Nitroso-di-n-propylamine ND ug/L 5 09/18/98 DHJ 621-64-7
Nitrobenzene ND ug/L 5 09/18/98 DHJ 98-95-3
Isophorone ND ug/L 5 09/18/98 DHJ 78-59-1
2-Nitrophenol ND ug/L 5 09/18/98 DHJ 88-75-5
2.4-Dimethylphenol ND ug/L 5 09/18/98 DHJ 105-67-9
bis(2-Chloroethoxy)methane ND ug/L 5 09/18/98 DHJ 111-91-1
2,4-Dichlorophenol ND ug/L 5 09/18/98 DHJ 120-83-2
1.2.4-Trichlorobenzene ND ug/L 5 09/18/98 DHJ 120-82-1
Naphthalene ND ug/L 5 09/18/98 DHJ 91-20-3
Hexachlorobutadiene ND ug/L 5 09/18/98 DHJ 87-68-3
4-Chloro-3-methylphenol ND ug/L 5 09/18/98 DHJ 59-50-7
Hexachlorocyclopentadiene ND ug/L 10 09/18/98 DHJ 77-47-4
2,4,6-Trichlorophenol ND ug/L 5 09/18/98 DHJ 88-06-2
2-Chloronaphthalene ND ug/L 5 09/18/98 DHJ 91-58-7
Acenaphthylene ND ug/L 5 09/18/98 DHJ 208-96-8
Dimethylphthalate ND ug/L 5 09/18/98 DHJ 131-11-3
2.6-Dinitrotoluene ND ug/L 5 09/18/98 DHJ 606-20-2
Acenaphthene ND ug/L 5 09/18/98 DHJ 83-32-9
Laboratory Certification IDs Laboratory Certfication IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services.Inc.

1
s
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 4
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
'ace Sample No: 92101443 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-1 Date Received: 09/08/98
'arameters Results Units PRL Analyzed Analyst CAS# Footnotes
2.4-Dinitrophenol ND ug/L 25 09/18/98 DHJ 51-28-5
2.4-Dinitrotoluene ND ug/L 5 09/18/98 DHJ 121-14-2
4-Nitrophenol ND ug/L 25 09/18/98 DHJ 100-02-7
Fluorene ND ug/L 5 09/18/98 DHJ 86-73-7
4-Chlorophenyl-phenylether ND ug/L 5 - 09/18/98 DHJ 7005-72-3
Diethylphthalate ND ug/L 5 09/18/98 DHJ 84-66-2
4.6-Dinitro-2-methylphenol ND ug/L 25 09/18/98 DHJ 534-52-1
N-Nitrosodiphenylamine ND ug/L 5 09/18/98 DHJ 86-30-6
4-Bromophenyl-phenylether ND ug/L 5 09/18/98 DHJ 101-55-3
Hexachlorobenzene ND ug/L 5 09/18/98 DHJ 118-74-1
Pentachlorophenol ND ug/L 25 09/18/98 DHJ 87-86-5
Phenanthrene ND ug/L 5 09/18/98 DHJ 85-01-8
Anthracene ND ug/L 5 09/18/98 DHJ 120-12-7
Di-n-butylphthalate ND ug/L 5 09/18/98 DHJ 84-74-2
Fluoranthene ND ug/L 5 09/18/98 DHJ 206-44-0
Benzidine ND ug/L 50 09/18/98 DHJ 92-87-5
Pyrene ND ug/L 5 09/18/98 DHJ 129-00-0
Butylbenzylphthalate ND ug/L 5 09/18/98 DHJ 85-68-7
3,3'-Dichlorobenzidine ND ug/L 10 09/18/98 DHJ 91-94-1
Benzo(a)anthracene ND ug/L 5 09/18/98 DHJ 56-55-3
Chrysene ND ug/L 5 09/18/98 DHJ 218-01-9
bis(2-Ethylhexyl)phthalate ND ug/L 5 09/18/98 DHJ 117-81-7
Di-n-octylphthalate ND ug/L 5 09/18/98 DHJ 117-84-0
Benzo(b)fluoranthene ND ug/L 5 09/18/98 DHJ 205-99-2
Benzo(k)fluoranthene ND ug/L 5 09/18/98 DHJ 207-08-9
Benzo(a)pyrene ND ug/L 5 09/18/98 DHJ 50-32-8
Indeno(1,2,3-cd)pyrene ND ug/L 5 09/18/98 DHJ 193-39-5
Dibenz(a,h)anthracene ND ug/L 5 09/18/98 DHJ 53-70-3
Benzo(g.h.i)perylene ND ug/L 5 09/18/98 DHJ 191-24-2
Nitrobenzene-d5 (S) 44 X 09/18/98 DHJ 4165-60-0
2-Fluorobiphenyl (S) 50 X 09/18/98 DHJ 321-60-8
Terphenyl-d14 (S) 77 X 09/18/98 DHJ 1718-51-0
Phenol-d6 (S) 24 X 09/18/98 DHJ 13127-88-3
2-Fluorophenol (S) 29 X 09/18/98 DHJ 367-12-4
2,4,6-Tribromophenol (S) 81 X 09/18/98 DHJ 118-79-6
Date Extracted 09/09/98
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

i
Y
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 5
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ace Sample No: 92101468 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-2 Date Received: 09/08/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
ield Services
Monitoring Well Data Method: Prep Method:
Field pH 6.22 Std. Units 09/08/98 JJQ
Field Specific Conductance 473 umhos/cm 09/08/98 JJQ
Field Temperature 16.5 deg C 09/08/98 JJQ
Static Water Level 19.48 feet 09/08/98 JJQ
etals
ICP Metals Method: EPA 200.7 Prep Method: EPA 3010
Chromium 0.012 mg/L 0.01 09/16/98 AB1 7440-47-3
Copper 0.074 mg/L 0.01 09/16/98 AB1 7440-50-8
Zinc 0.066 mg/L 0.01 09/16/98 AB1 7440-66-6
Date Digested 09/15/98
Lead by Furnace. Method 239.2 Method: EPA 239.2 Prep Method: EPA 200F
Lead ND mg/L 0.005 09/24/98 TYM 7439-92-1
Date Digested 09/21/98
et Chemistry
Total Dissolved Solids Method: EPA 160.1 Prep Method: EPA 160.1
Total Dissolved Solids 320 mg/L 1 09/09/98 JAS 1
Total Suspended Solids Method: EPA 160.2 Prep Method: EPA 160.2
Total Suspended Solids 1100 mg/L 1 09/11/98 DRP
Hexane Extractable Material Method: EPA 1664 Prep Method: EPA 3510
Oil and Grease ND mg/L 5 09/17/98 JML
Chloride(Mercuric Nitrate) Method: EPA 325.3 Prep Method: EPA 325.3
Chloride 80 mg/L 1 09/17/98 DRP
Sulfate.Automated Colorimetric Method: EPA 375.2 Prep Method: EPA 375.2
Sulfate 20 mg/L 5 09/16/98 TYM
Chemical Oxygen Demand Method: EPA 410.4 Prep Method: EPA 410.4
Chemical Oxygen Demand 32 mg/L 25 09/09/98 TTB
C/MS -- VOA
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TN Drink 90090
NC Drinking Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services.Inc.

I
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 6
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ace Sample No: 92101468 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-2 Date Received: 09/08/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
Volatile GC/MS by 624 Method: EPA 624 Prep Method: EPA 624
Chloromethane ND ug/L 5 09/18/98 VFT 74-87-3
Vinyl Chloride ND ug/L 5 09/18/98 VFT 75-01-4
Bromomethane ND ug/L 5 09/18/98 VFT 74-83-9
Chloroethane ND ug/L 5 09/18/98 VFT 75-00-3
Trichlorofluoromethane ND ug/L 5 09/18/98 VFT 75-69-4
1.1-Dichloroethene ND ug/L 5 09/18/98 VFT 75-35-4
Methylene Chloride 5.1 ug/L 5 09/18/98 VFT 75-09-2 2
trans-1.2-Dichloroethene ND ug/L 5 09/18/98 VFT 156-60-5
1.1-Dichloroethane ND ug/L 5 09/18/98 VFT 75-34-3
cis-1.2-Dichloroethene ND ug/L 5 09/18/98 VFT 156-59-2
Chloroform ND ug/L 5 09/18/98 VFT 67-66-3
1.1,1-Trichloroethane ND ug/L 5 09/18/98 VFT 71-55-6
1.2-Dichloroethane ND ug/L 5 09/18/98 VFT 107-06-2
Carbon Tetrachloride ND ug/L 5 09/18/98 VFT 56-23-5
Benzene ND ug/L 5 09/18/98 VFT 71-43-2
Trichloroethene ND ug/L 5 09/18/98 VFT 79-01-6
1.2-Dichloropropane ND ug/L 5 09/18/98 VFT 78-87-5
Bromodichloromethane ND ug/L 5 09/18/98 VFT 75-27-4
2-Chloroethyl Vinyl Ether ND ug/L 10 09/18/98 VFT 110-75-8
cis-1.3-Dichloropropene ND ug/L 5 09/18/98 VFT 10061-01-5
Toluene ND ug/L 5 09/18/98 VFT 108-88-3
trans-1.3-Dichloropropene ND ug/L 5 09/18/98 VFT 10061-02-6
1.1.2-Trichloroethane ND ug/L 5 09/18/98 VFT 79-00-5
Dibromochloromethane ND ug/L 5 09/18/98 VFT 124-48-1
Tetrachloroethene ND ug/L 5 09/18/98 VET 127-18-4
Chlorobenzene ND ug/L 5 09/18/98 VFT 108-90-7
Ethylbenzene ND ug/L 5 09/18/98 VFT 100-41-4
Bromoform ND ug/L 5 09/18/98 VFT 75-25-2
1.1.2.2-Tetrachloroethane ND ug/L 5 09/18/98 VFT 79-34-5
1.3-Dichlorobenzene ND ug/L 5 09/18/98 VFT 541-73-1
1.4-Dichlorobenzene ND ug/L 5 09/18/98 VFT 106-46-7
1.2-Dichlorobenzene ND ug/L 5 09/18/98 VFT 95-50-1
Dibromofluoromethane (S) 101 X 09/18/98 VFT 1868-53-7
Toluene-d8 (S) 102 X 09/18/98 VET 2037-26-5
4-Bromofluorobenzene (S) 102 X 09/18/98 VFT 460-00-4
C/MS -- Semi-VOA
Extractables in Water by 625 Method: EPA 625 Prep Method: EPA 625 SF
Laboratory Certification IDs J.aboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS ►Y Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

i
I.
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 7
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
'ace Sample No: 92101468 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-2 Date Received: 09/08/98
'arameters Results Units PRL Analyzed Analyst CAS# Footnotes
N-Nitrosodimethylamine ND ug/L 5 09/18/98 DHJ 62-75-9
bis(2-Chloroethyl)ether ND ug/L 5 09/18/98 DHJ 111-44-4
Phenol ND ug/L 5 09/18/98 DHJ 108-95-2
2-Chlorophenol ND ug/L 5 09/18/98 DHJ 95-57-8
1.3-Dichlorobenzene ND ug/L 5 09/18/98 DHJ 541-73-1
1.4-Dichlorobenzene ND ug/L 5 09/18/98 DHJ 106-46-7
1.2-Dichlorobenzene ND ug/L 5 09/18/98 DHJ 95-50-1
bis(2-Chloroisopropyl)ether ND ug/L 5 09/18/98 DHJ 39638-32-9
Hexachloroethane ND ug/L 5 09/18/98 DHJ 67-72-1
N-Nitroso-di-n-propylamine ND ug/L 5 09/18/98 DHJ 621-64-7
Nitrobenzene ND ug/L 5 09/18/98 DHJ 98-95-3
Isophorone ND ug/L 5 09/18/98 DHJ 78-59-1
2-Nitrophenol ND ug/L 5 09/18/98 DHJ 88-75-5
2.4-Dimethylphenol ND ug/L 5 09/18/98 DHJ 105-67-9
bis(2-Chloroethoxy)methane ND ug/L 5 09/18/98 DHJ 111-91-1
2.4-Dichlorophenol ND ug/L 5 09/18/98 DHJ 120-83-2
1.2.4-Trichlorobenzene ND ug/L 5 09/18/98 DHJ 120-82-1
Naphthalene ND ug/L 5 09/18/98 DHJ 91-20-3
Hexachlorobutadiene ND ug/L 5 09/18/98 DHJ 87-68-3
4-Chloro-3-methylphenol ND ug/L 5 09/18/98 DHJ 59-50-7
Hexachlorocyclopentadiene ND ug/L 10 09/18/98 DHJ 77-47-4
2.4.6-Trichlorophenol ND ug/L 5 09/18/98 DHJ 88-06-2
2-Chloronaphthalene ND ug/L 5 09/18/98 DHJ 91-58-7
Acenaphthylene ND ug/L 5 09/18/98 DHJ 208-96-8
Dimethylphthalate ND ug/L 5 09/18/98 DHJ 131-11-3
2.6-Dinitrotoluene ND ug/L 5 09/18/98 DHJ 606-20-2
Acenaphthene ND ug/L 5 09/18/98 DHJ 83-32-9
2.4-Dinitrophenol ND ug/L 25 09/18/98 DHJ 51-28-5
2,4-Dinitrotoluene ND ug/L 5 09/18/98 DHJ 121-14-2
4-Nitrophenol ND ug/L 25 09/18/98 DHJ 100-02-7
Fluorene ND ug/L 5 09/18/98 DHJ 86-73-7
4-Chlorophenyl-phenylether ND ug/L 5 09/18/98 DHJ 7005-72-3
Diethylphthalate ND ug/L 5 09/18/98 DHJ 84-66-2
4.6-Dinitro-2-methylphenol ND ug/L 25 09/18/98 DHJ 534-52-1
N-Nitrosodiphenylamine ND ug/L 5 09/18/98 DHJ 86-30-6
4-Bromophenyl-phenylether ND ug/L 5 09/18/98 DHJ 101-55-3
Hexachlorobenzene ND ug/L 5 09/18/98 DHJ 118-74-1
Pentachlorophenol ND ug/L 25 09/18/98 DHJ 87-86-5
Phenanthrene ND ug/L 5 09/18/98 DHJ 85-01-8
Anthracene ND ug/L 5 09/18/98 DHJ 120-12-7
Laboratory Certification IDs Laboratory Certification IDs
NC NC Ding Water 37706 ewater 12 REPORT OF LABORATORY ANALYSIS TKYN Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

r
'
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 8
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ice Sample No: 92101468 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-2 Date Received: 09/08/98
trameters Results Units PRL Analyzed Analyst CAS# Footnotes
Di-n-butylphthalate ND ug/L 5 09/18/98 DHJ 84-74-2
Fluoranthene ND ug/L 5 09/18/98 DHJ 206-44-0
Benzidine ND ug/L 50 09/18/98 DHJ 92-87-5
Pyrene ND ug/L 5 09/18/98 DHJ -129-00-0
Butylbenzylphthalate ND ug/L 5 09/18/98 DHJ 85-68-7
3,3'-Dichlorobenzidine ND ug/L 10 09/18/98 DHJ 91-94-1
Benzo(a)anthracene ND ug/L 5 09/18/98 DHJ 56-55-3
Chrysene ND ug/L 5 09/18/98 DHJ 218-01-9
bis(2-Ethylhexyl)phthalate ND ug/L 5 09/18/98 DHJ 117-81-7
Di-n-octylphthalate ND ug/L 5 09/18/98 DHJ 117-84-0
Benzo(b)fluoranthene ND ug/L 5 09/18/98 DHJ 205-99-2
Benzo(k)fluoranthene ND ug/L 5 09/18/98 DHJ 207-08-9
Benzo(a)pyrene ND ug/L 5 09/18/98 DHJ 50-32-8
Indeno(1,2,3-cd)pyrene ND ug/L 5 09/18/98 DHJ 193-39-5
Dibenz(a,h)anthracene ND ug/L 5 09/18/98 DHJ 53-70-3
Benzo(g,h,i)perylene ND ug/L 5 09/18/98 DHJ 191-24-2
Nitrobenzene-d5 (S) 78 X 09/18/98 DHJ 4165-60-0
2-Fluorobiphenyl (S) 75 X 09/18/98 DHJ 321-60-8
Terphenyl-d14 (S) 86 X 09/18/98 DHJ 1718-51-0
Phenol-d6 (S) 36 X 09/18/98 DHJ 13127-88-3
2-Fluorophenol (S) 50 X 09/18/98 DHJ 367-12-4
2,4,6-Tribromophenol (S) 96 X 09/18/98 DHJ 118-79-6
Date Extracted 09/09/98
L boratory Certification 1Ds
Jaboratopr Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS ►Y Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services. Inc.

i
Pace Analytical Services,Inc.
9800 Kincey Avenue,Suite 100
pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 9
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ace Sample No: 92101484 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-3 Date Received: 09/08/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
field Services
Monitoring Well Data Method: Prep Method:
Field pH 8.49 Std. Units 09/08/98 JJQ
Field Specific Conductance 30500 umhos/cm 09/08/98 JJQ
Field Temperature 16.7 deg C 09/08/98 JJQ
Static Water Level 18.78 feet 09/08/98 JJQ
etals
ICP Metals Method: EPA 200.7 Prep Method: EPA 3010
Chromium 0.29 mg/L 0.1 09/17/98 AB1 7440-47-3
Copper 2.9 mg/L 0.1 09/17/98 AB1 7440-50-8
Zinc 0.17 mg/L 0.1 09/17/98 AB1 7440-66-6
Date Digested 09/16/98
Lead by Furnace. Method 239.2 Method: EPA 239.2 Prep Method: EPA 200F
Lead 0.027 mg/L 0.005 09/24/98 TYM 7439-92-1
Date Digested 09/21/98
et Chemistry
Total Dissolved Solids Method: EPA 160.1 Prep Method: EPA 160.1
Total Dissolved Solids 20000 mg/L 1 09/09/98 JAS 1
Total Suspended Solids Method: EPA 160.2 Prep Method: EPA 160.2
Total Suspended Solids 2200 mg/L 1 09/11/98 DRP
Hexane Extractable Material Method: EPA 1664 Prep Method: EPA 3510
Oil and Grease ND mg/L 5 09/17/98 JML
Chloride(Mercuric Nitrate) Method: EPA 325.3 Prep Method: EPA 325.3
Chloride 8300 mg/L 1 09/17/98 DRP
Sulfate.Automated Colorimetric Method: EPA 375.2 Prep Method: EPA 375.2
Sulfate 1300 mg/L 500 09/16/98 TYM
Chemical Oxygen Demand Method: EPA 410.4 Prep Method: EPA 410.4
Chemical Oxygen Demand 5700 mg/L 1000 09/09/98 TTB
0/MS -- VOA
Laboratory Certification IDs Laboratory Certification IDs
NC
NC Waste Drter 12 inking 37706 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

t
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 10
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ace Sample No: 92101484 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-3 Date Received: 09/08/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
Volatile GC/MS by 624 Method: EPA 624 Prep Method: EPA 624
Chloromethane ND ug/L 50 09/19/98 VFT 74-87-3
Vinyl Chloride ND ug/L 50 09/19/98 VFT 75-01-4
Bromomethane ND ug/L 50 09/19/98 VFT 74-83-9
Chloroethane ND ug/L 50 09/19/98 VFT 75-00-3
Trichlorofluoromethane ND ug/L 50 09/19/98 VFT 75-69-4
1.1-Dichloroethene ND ug/L 50 09/19/98 VFT 75-35-4
Methylene Chloride ND ug/L 50 09/19/98 VFT 75-09-2
trans-1.2-Dichloroethene ND ug/L 50 09/19/98 VFT 156-60-5
1.1-Dichloroethane ND ug/L 50 09/19/98 VFT 75-34-3
cis-1.2-Dichloroethene ND ug/L 50 09/19/98 VFT 156-59-2
Chloroform ND ug/L 50 09/19/98 VFT 67-66-3
1.1.1-Trichloroethane ND ug/L 50 09/19/98 VFT 71-55-6
1.2-Dichloroethane ND ug/L 50 09/19/98 VFT 107-06-2
Carbon Tetrachloride ND ug/L 50 09/19/98 VFT 56-23-5
Benzene 650 ug/L 50 09/19/98 VFT 71-43-2
Trichloroethene ND ug/L 50 09/19/98 VFT 79-01-6
1.2-Dichloropropane ND ug/L 50 09/19/98 VFT 78-87-5
Bromodichloromethane ND ug/L 50 09/19/98 VFT 75-27-4
2-Chloroethyl Vinyl Ether ND ug/L 100 09/19/98 VFT 110-75-8
cis-1.3-Dichloropropene ND ug/L 50 09/19/98 VFT 10061-01-5
Toluene ND ug/L 50 09/19/98 VFT 108-88-3
trans-1.3-Dichloropropene ND ug/L 50 09/19/98 VFT 10061-02-6
1.1.2-Trichloroethane ND ug/L 50 09/19/98 VFT 79-00-5
Dibromochloromethane ND ug/L 50 09/19/98 VFT 124-48-1
Tetrachloroethene ND ug/L 50 09/19/98 VFT 127-18-4
Chlorobenzene 120 ug/L 50 09/19/98 VFT 108-90-7
Ethylbenzene ND ug/L 50 09/19/98 VFT 100-41-4
Bromoform ND ug/L 50 09/19/98 VFT 75-25-2
1.1.2.2-Tetrachloroethane ND ug/L 50 09/19/98 VFT 79-34-5
1.3-Dichlorobenzene ND ug/L 50 09/19/98 VFT 541-73-1
1.4-Dichlorobenzene ND ug/L 50 09/19/98 VFT 106-46-7
1.2-Dichlorobenzene 67 ug/L 50 09/19/98 VFT 95-50-1
Dibromofluoromethane (S) 98 X 09/19/98 VFT 1868-53-7
Toluene-d8 (S) 103 X 09/19/98 VFT 2037-26-5
4-Bromofluorobenzene (S) 101 X 09/19/98 VFT 460-00-4
:MS -- Semi-VOA
Extractables in Water by 625 Method: EPA 625 Prep Method: EPA 625 SF
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TM Drinking
k Water 90090
NC Drinking Water 37706List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services.Inc.

i
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 11
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
'ace Sample No: 92101484 Date Collected: 09/08/98 Matrix: Water
.lient Sample ID: MW-3 Date Received: 09/08/98
'arameters Results Units PRL Analyzed Analyst CAS# Footnotes
N-Nitrosodimethylamine ND ug/L 500 09/22/98 DHJ 62-75-9
bis(2-Chloroethyl)ether ND ug/L 500 09/22/98 DHJ 111-44-4
Phenol 5000 ug/L 500 09/22/98 DHJ 108-95-2
2-Chlorophenol ND ug/L 500 09/22/98 DHJ 95-57-8
1.3-Dichlorobenzene ND ug/L 500 09/22/98 DHJ 541-73-1
1.4-Dichlorobenzene ND ug/L 500 09/22/98 DHJ 106-46-7
1.2-Dichlorobenzene ND ug/L 500 09/22/98 DHJ 95-50-1
bis(2-Chloroisopropyl)ether ND ug/L 500 09/22/98 DHJ 39638-32-9
Hexachloroethane ND ug/L 500 09/22/98 DHJ 67-72-1
N-Nitroso-di-n-propylamine ND ug/L 500 09/22/98 DHJ 621-64-7
Nitrobenzene ND ug/L 500 09/22/98 DHJ 98-95-3
Isophorone ND ug/L 500 09/22/98 DHJ 78-59-1
2-Nitrophenol ND ug/L 500 09/22/98 DHJ 88-75-5
2.4-Dimethylphenol ND ug/L 500 09/22/98 DHJ 105-67-9
bis(2-Chloroethoxy)methane ND ug/L 500 09/22/98 DHJ 111-91-1
2.4-Dichlorophenol ND ug/L 500 09/22/98 DHJ 120-83-2
1.2.4-Trichlorobenzene 4600 ug/L 500 09/22/98 DHJ 120-82-1
Naphthalene ND ug/L 500 09/22/98 DHJ 91-20-3
Hexachlorobutadiene ND ug/L 500 09/22/98 DHJ 87-68-3
4-Chloro-3-methylphenol ND ug/L 500 09/22/98 DHJ 59-50-7
Hexachlorocyclopentadiene ND ug/L 1000 09/22/98 DHJ 77-47-4
2,4.6-Trichlorophenol ND ug/L 500 09/22/98 DHJ 88-06-2
2-Chloronaphthalene ND ug/L 500 09/22/98 DHJ 91-58-7
Acenaphthylene ND ug/L 500 09/22/98 DHJ 208-96-8
Dimethylphthalate ND ug/L 500 09/22/98 DHJ 131-11-3
2.6-Dinitrotoluene ND ug/L 500 09/22/98 DHJ 606-20-2
Acenaphthene ND ug/L 500 09/22/98 DHJ 83-32-9
2.4-Dinitrophenol ND ug/L 2500 09/22/98 DHJ 51-28-5
2.4-Dinitrotoluene ND ug/L 500 09/22/98 DHJ 121-14-2
4-Nitrophenol ND ug/L 2500 09/22/98 DHJ 100-02-7
Fluorene ND ug/L 500 09/22/98 DHJ 86-73-7
4-Chlorophenyl-phenylether ND ug/L 500 09/22/98 DHJ 7005-72-3
Diethylphthalate ND ug/L 500 09/22/98 DHJ 84-66-2
4.6-Dinitro-2-methylphenol ND ug/L 2500 09/22/98 DHJ 534-52-1
N-Nitrosodiphenylamine ND ug/L 500 09/22/98 DHJ 86-30-6
4-Bromophenyl-phenyl ether ND ug/L 500 09/22/98 DHJ 101-55-3
Hexachlorobenzene ND ug/L 500 09/22/98 DHJ 118-74-1
Pentachlorophenol ND ug/L 2500 09/22/98 DHJ 87-86-5
Phenanthrene ND ug/L 500 09/22/98 DHJ 85-01-8
Anthracene ND ug/L 500 09/22/98 DHJ 120-12-7
LaPonitoniCertificationICIs Laboratory Certification IDs
NC Dnnk ng Water emmder 3»06 REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

i
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 12
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ace Sample No: 92101484 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: MW-3 Date Received: 09/08/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
Di-n-butylphthalate ND ug/L 500 09/22/98 DHJ 84-74-2
Fluoranthene ND ug/L 500 09/22/98 DHJ 206-44-0
Benzidine 55000 ug/L 5000 09/22/98 DHJ 92-87-5 3
Pyrene ND • ug/L 500 • 09/22/98 DHJ 129-00-0
Butylbenzylphthalate ND ug/L 500 09/22/98 DHJ 85-68-7
3.3'-Dichlorobenzidine ND ug/L 1000 09/22/98 DHJ 91-94-1
Benzo(a)anthracene ND ug/L 500 09/22/98 DHJ 56-55-3
Chrysene ND ug/L 500 09/22/98 DHJ 218-01-9
bis(2-Ethylhexyl)phthalate ND ug/L 500 09/22/98 DHJ 117-81-7
Di-n-octylphthalate ND ug/L 500 09/22/98 DHJ 117-84-0
Benzo(b)fluoranthene ND ug/L 500 09/22/98 DHJ 205-99-2
Benzo(k)fluoranthene ND ug/L 500 09/22/98 DHJ 207-08-9
Benzo(a)pyrene ND ug/L 500 09/22/98 DHJ 50-32-8
Indeno(1.2,3-cd)pyrene ND ug/L 500 09/22/98 DHJ 193-39-5
Dibenz(a.h)anthracene ND ug/L 500 09/22/98 DHJ 53-70-3
Benzo(g,h,i)perylene ND ug/L 500 09/22/98 DHJ 191-24-2
Nitrobenzene-d5 (S) 0 X 09/22/98 DHJ 4165-60-0 4
2-Fluorobiphenyl (S) 0 X 09/22/98 DHJ 321-60-8 •
Terphenyl-d14 (S) 0 X 09/22/98 DHJ 1718-51-0
Phenol-d6 (S) 0 X 09/22/98 DHJ 13127-88-3
2-Fluorophenol (S) 0 X 09/22/98 DHJ 367-12-4
2.4.6-Tribromophenol (S) 0 X 09/22/98 DHJ 118-79-6
Date Extracted 09/09/98
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drink ng Water ewater 37706 REPORT OF LABORATORY ANALYSIS KY TN UST Ustwater 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 13
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
'ace Sample No: 92101492 Date Collected: 09/08/98 Matrix: Water
:lient Sample ID: EQUIPMENT BLANK Date Received: 09/08/98
'arameters Results Units PRL Analyzed Analyst CAS# Footnotes
;CMS -- VOA
Volatile GC/MS by 624 Method: EPA 624 Prep Method: EPA 624
Chloromethane ND ug/L 5 09/18/98 VFT 74-87-3
Vinyl Chloride ND ug/L 5 09/18/98 VFT 75-01-4
Bromomethane ND ug/L 5 09/18/98 VFT 74-83-9
Chloroethane ND ug/L 5 09/18/98 VFT 75-00-3
Trichiorofluoromethane ND ug/L 5 09/18/98 VFT 75-69-4
1,1-Dichloroethene ND ug/L 5 09/18/98 VET 75-35-4
Methylene Chloride 9.0 ug/L 5 09/18/98 VFT 75-09-2 2
trans-1.2-Dichloroethene ND ug/L 5 09/18/98 VFT 156-60-5
1.1-Dichloroethane ND ug/L 5 09/18/98 VFT 75-34-3
cis-1.2-Dichloroethene ND ug/L 5 09/18/98 VFT 156-59-2
Chloroform ND ug/L 5 09/18/98 VFT 67-66-3
1,1,1-Trichloroethane ND ug/L 5 09/18/98 VFT 71-55-6
1.2-Dichloroethane ND ug/L 5 09/18/98 VET 107-06-2
Carbon Tetrachloride ND ug/L 5 09/18/98 VFT 56-23-5
Benzene ND ug/L 5 09/18/98 VFT 71-43-2
Trichloroethene ND ug/L 5 09/18/98 VET 79-01-6
1.2-Dichloropropane ND ug/L 5 09/18/98 VET 78-87-5
Bromodichloromethane ND ug/L 5 09/18/98 VET 75-27-4
2-Chloroethyl Vinyl Ether ND ug/L 10 09/18/98 VFT 110-75-8
cis-1.3-Dichloropropene ND ug/L 5 09/18/98 VFT 10061-01-5
Toluene ND ug/L 5 09/18/98 VET 108-88-3
trans-1,3-Dichloropropene ND ug/L 5 09/18/98 VFT 10061-02-6
1.1.2-Trichloroethane ND ug/L 5 09/18/98 VFT 79-00-5
Dibromochloromethane ND ug/L 5 09/18/98 VFT 124-48-1
Tetrachloroethene ND ug/L 5 09/18/98 VFT 127-18-4
Chlorobenzene ND ug/L 5 09/18/98 VFT 108-90-7
Ethyl benzene ND ug/L 5 09/18/98 VFT 100-41-4
Bromoform ND ug/L 5 09/18/98 VFT 75-25-2
1,1.2,2-Tetrachloroethane ND ug/L 5 09/18/98 VFT 79-34-5
1.3-Dichlorobenzene ND ug/L 5 09/18/98 VFT 541-73-1
1.4-Dichlorobenzene ND ug/L 5 09/18/98 VFT 106-46-7
1,2-Dichlorobenzene ND ug/L 5 09/18/98 VFT 95-50-1
Dibromofluoromethane (S) 102 X 09/18/98 VFT 1868-53-7
Toluene-d8 (S) 102 X 09/18/98 VFT 2037-26-5
4-Bromofluorobenzene (S) 102 X 09/18/98 VFT 460-00-4
l aboratopt Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical SPrvievaa Inf.

r
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 14
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
'ace Sample No: 92101500 Date Collected: 09/08/98 Matrix: Water
lient Sample ID: TRIP BLANK Date Received: 09/08/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
C/MS -- VOA
Volatile GC/MS by 624 Method: EPA 624 Prep Method: EPA 624
Chloromethane ND ug/L 5 09/18/98 VFT 74-87-3
Vinyl Chloride ND ug/L 5 09/18/98 VFT 75-01-4
Bromomethane ND ug/L 5 09/18/98 VFT 74-83-9
Chloroethane ND ug/L 5 09/18/98 VFT 75-00-3
Trichlorofluoromethane ND ug/L 5 09/18/98 VFT 75.69-4
1.1-Dichloroethene ND ug/L 5 09/18/98 VFT 75-35-4
Methylene Chloride 9.2 ug/L 5 09/18/98 VFT 75.09-2 2
trans-1.2-Dichloroethene ND ug/L 5 09/18/98 VFT 156-60-5
1.1-Dichloroethane ND ug/L 5 09/18/98 VFT 75-34-3
cis-1.2-Dichloroethene ND ug/L 5 09/18/98 VFT 156-59-2
Chloroform ND ug/L 5 09/18/98 VFT 67-66-3
1.1.1-Trichloroethane ND ug/L 5 09/18/98 VFT 71.55-6
1.2-Dichloroethane ND ug/L 5 09/18/98 VFT 107-06-2
Carbon Tetrachloride ND ug/L 5 09/18/98 VFT 56-23-5
Benzene ND ug/L 5 09/18/98 VFT 71-43-2
Trichloroethene ND ug/L 5 09/18/98 VFT 79-01-6
1.2-Dichloropropane ND ug/L 5 09/18/98 VFT 78.87-5
Bromodichloromethane ND ug/L 5 09/18/98 VFT 75-27-4
2-Chloroethyl Vinyl Ether ND ug/L 10 09/18/98 VFT 110-75-8
cis-1,3-Dichloropropene ND ug/L 5 09/18/98 VFT 10061-01-5
Toluene ND ug/L 5 09/18/98 VFT 108-88-3
trans-1.3-Dichloropropene ND ug/L 5 09/18/98 VFT 10061-02-6
1.1.2-Trichloroethane ND ug/L 5 09/18/98 VFT 79-00-5
Dibromochloromethane ND ug/L 5 09/18/98 VFT 124-48-1
Tetrachloroethene ND ug/L 5 09/18/98 VFT 127-18-4
Chlorobenzene ND ug/L 5 09/18/98 VFT 108-90-7
Ethylbenzene ND ug/L 5 09/18/98 VFT 100-41-4
Bromoform ND ug/L 5 09/18/98 VFT 75-25-2
1,1.2.2-Tetrachloroethane ND ug/L 5 09/18/98 VFT 79-34-5
1.3-Dichlorobenzene ND ug/L 5 09/18/98 VFT 541-73-1
1.4-Dichlorobenzene ND ug/L 5 09/18/98 VFT 106-46-7
1.2-Dichlorobenzene ND ug/L 5 09/18/98 VFT 95-50-1
Dibromofluoromethane (S) 103 X 09/18/98 VFT 1868-53-7
Toluene-d8 (S) 102 X 09/18/98 VFT 2037-26-5
4-Bromofluorobenzene (S) 100 X 09/18/98 VFT 460-00-4
Laboratory Certification IDs Laboratory Certification IDs
NC
NC Dn k ewater ng Water 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services.Inc

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 15
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ce Sample No: 92101518 Date Collected: 09/08/98 Matrix: Water
ient Sample ID: RW-1 Date Received: 09/08/98
rameters Results Units PRL Analyzed Analyst CAS# Footnotes
t Chemistry
Chloride(Mercuric Nitrate) Method: EPA 325.3 Prep Method: EPA 325.3
Chloride 1700 mg/L 1 09/17/98 DRP
Sul fate.Automated Colorimetric Method: EPA 375.2 Prep Method: EPA 375.2
Sulfate ND mg/L 500 09/16/98 TYM 5
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TKY Drinking N DST Water 90090
NC Drinking
Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 16
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
4RAMETER FOOTNOTES
Not Detected
Not Calculable
2L Pace Reporting Limit
S) Surrogate
1] Analyte is found in the associated blank as well as in the sample (CLP B-Flag).
2] The analyte was found in an associated blank. as well as in the sample.
3] The response was over the calibration range for this compound. Reported results should be considered an estimate.
4] Spike and/or surrogate recoveries could not be calculated due to sample dilution.
5] The detection limits for all compounds for this analysis are elevated due to matrix interference.
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 17
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
602 N. Main St.
owell. NC 28098
ttn: Mr. Bobby Lamb
hone:
C Batch ID: 2574 QC Batch Method: EPA 625 SF
nalysis Method: EPA 625 Analysis Description: Extractables in Water by 625
ssociated Pace Samples: 92101443 92101468 92101484
=TROD BLANK: 92102722
ssociated Pace Samples:
92101443 92101468 92101484
Method
Blank
arameter Units Result PRL Footnotes
-Nitrosodimethylamine ug/L ND 5
is(2-Chloroethyl)ether ug/L ND 5
nenol ug/L ND 5
-Chlorophenol ug/L ND 5
,3-Dichlorobenzene ug/L ND 5
.4-Dichlorobenzene ug/L ND 5
.2-Dichlorobenzene ug/L ND 5
is(2-Chloroisopropyl)ether ug/L ND 5
exachloroethane ug/L ND 5
-Nitroso-di-n-propylamine ug/L ND 5
itrobenzene ug/L ND 5
sophorone ug/L ND 5
-Nitrophenol ug/L ND 5
.4-Dimethylphenol ug/L ND 5
is(2-Chloroethoxy)methane ug/L ND 5
.4-Dichlorophenol ug/L ND 5
.2.4-Trichlorobenzene ug/L ND 5
3phthalene ug/L ND 5
?xachlorobutadiene ug/L ND 5
•Chloro-3-methylphenol ug/L ND 5
?xachlorocyclopentadiene ug/L ND 10
.4.6-Trichlorophenol ug/L ND 5
•Chloronaphthalene ug/L ND 5
:enaphthylene ug/L ND 5
imethylphthalate ug/L ND 5
Laboratory Certification IDs Laboratory Certification IDs
NC
NC Wastewa Drinking Water ter 12 REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services. Inc.

•
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 18
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ETHOD BLANK: 92102722
ssociated Pace Samples:
92101443 92101468 92101484
Method
- - - - _ Blank - -
arameter Units Result PRL Footnotes
.6-Dinitrotoluene ug/L ND 5
cenaphthene ug/L ND 5
.4-Dinitrophenol ug/L ND 25
.4-Dinitrotoluene ug/L ND 5
-Nitrophenol ug/L ND 25
luorene ug/L ND 5
-Chlorophenyl-phenylether ug/L ND 5
iethylphthalate ug/L ND 5
.6-Dinitro-2-methylphenol ug/L ND 25
-Nitrosodiphenylamine ug/L ND 5
-Bromophenyl-phenyl ether ug/L ND 5
a xachlorobenzene ug/L ND 5
a ntachlorophenol ug/L ND 25
'enanthrene ug/L ND 5
ithracene ug/L ND 5
i-n-butylphthalate ug/L ND 5
luoranthene ug/L ND 5
anzidine ug/L ND 50
yrene ug/L ND 5
itylbenzylphthalate ug/L ND 5
.3'-Dichlorobenzidine ug/L ND 10
a nzo(a)anthracene ug/L ND 5
hrysene ug/L ND 5
is(2-Ethylhexyl)phthalate ug/L ND 5
i-n-octylphthalate ug/L ND 5
a nzo(b)fluoranthene ug/L ND 5
a nzo(k)fluoranthene ug/L ND 5
anzo(a)pyrene ug/L ND 5
ideno(1.2,3-cd)pyrene ug/L ND 5
ibenz(a.h)anthracene ug/L ND 5
a nzo(g,h,i)perylene ug/L ND 5
itrobenzene-d5 (S) X 76
-Fluorobiphenyl (S) X 81
arphenyl-d14 (S) X 85
ienol-d6 (S) X 34
-Fluorophenol (S) X 49
,4,6-Tribromophenol (S) X 94
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NC
NC Dunking Water water 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

k
0
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 19
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ABORATORY CONTROL SAMPLE: 92115930
Spike LCS Spike
'arameter Units Conc. Result X Rec Footnotes
1-Nitrosodimethylamine _ - - . - -ug/L 50 - 2.400 4.80
)is(2-Chloroethyl)ether ug/L 50 6.600 13.2
'henol ug/L 50 3.800 7.60
'-Chlorophenol ug/L 50 6.400 12.8 1
.3-Dichlorobenzene ug/L 50 3.800 7.60
,4-Dichlorobenzene • ug/L 50 4.000 8.00 1
.2-Dichlorobenzene ug/L 50 4.800 9.60 1
ls(2-Chloroisopropyl)ether ug/L 50 2.900 5.80 2
'exachloroethane ug/L 50 3.600 7.20 1
-Nitroso-di-n-propylamine ug/L 50 16.10 32.2
itrobenzene ug/L 50 10.70 21.4 1
sophorone ug/L 50 21.00 42.0
-Nitrophenol ug/L 50 14.20 28.4 1
.4-Dimethylphenol ug/L 50 17.00 34.0
is(2-Chloroethoxy)methane ug/L 50 16.40 32.8 1
.4-Dichlorophenol ug/L 50 17.30 34.6
.2.4-Trichlorobenzene ug/L 50 10.50 21.0 1
aphthalene ug/L 50 12.00 24.0
exachlorobutadiene ug/L 50 7.700 15.4 1
-Chloro-3-methylphenol ug/L 50 28.20 56.4
exachlorocyclopentadiene ug/L 50 7.000 14.0
.4.6-Trichlorophenol ug/L 50 29.10 58.2
-Chloronaphthalene ug/L 50 24.20 48.4 1
cenaphthylene ug/L 50 30.00 60.0
imethylphthalate ug/L 50 40.80 81.6
.6-Dinitrotoluene ug/L 50 48.00 96.0
cenaphthene ug/L 50 42.40 84.8
.4-Dinitrophenol ug/L 50 43.00 86.0
.4-Dinitrotoluene ug/L 50 48.00 96.0
-Nitrophenol ug/L 50 17.00 34.0
luorene ug/L 50 38.00 76.0
-Chlorophenyl-phenyl ether ug/L 50 37.00 74.0
i ethyl phthalate ug/L 50 45.00 90.0
.6-Dinitro-2-methylphenol ug/L 50 38.00 76.0
-Nitrosodiphenylamine ug/L 50 37.00 74.0
-Bromophenyl-phenyl ether ug/L 50 38.00 76.0
?.xachlorobenzene ug/L 50 37.00 74.0
3ntachlorophenol ug/L 50 45.00 90.0
ienanthrene ug/L 50 40.00 80.0
ithracene ug/L 50 42.00 84.0
i-n-butylphthalate ug/L 50 45.00 90.0
Laboratory Certification IDs laboratory Certification IDs
NC
NC Dunking Water 37706 12 REPORT OF LABORATORY ANALYSIS finking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services inr

i
1
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 20
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ABORATORY CONTROL SAMPLE: 92115930
Spike LCS Spike
'arameter Units Conc. Result X Rec Footnotes
luoranthene ug/L _ _50_ _ - _46.00 92.0 - - -
enzidine ug/L 50 141.0 282
yrene ug/L 50 42.00 84.0
utylbenzylphthalate ug/L 50 43.00 86.0
.3'-Dichlorobenzidine ug/L 50 39.00 78.0
enzo(a)anthracene ug/L 50 42.00 84.0
hrysene ug/L 50 42.00 84.0
is(2-Ethylhexyl)phthalate ug/L 50 42.00 84.0
i-n-octylphthalate ug/L 50 46.00 92.0
enzo(b)fluoranthene ug/L 50 46.00 92.0
enzo(k)fluoranthene ug/L 50 42.00 84.0
enzo(a)pyrene ug/L 50 44.00 88.0
ndeno(1.2.3-cd)pyrene ug/L 50 42.00 84.0
ibenz(a.h)anthracene ug/L 50 41.00 82.0
enzo(g,h.i)perylene ug/L 50 42.00 84.0
itrobenzene-d5 (S) 22 3
-Fluorobiphenyl (S) _ 47
erphenyl-d14 (S) 83
nenol-d6 (S) 8 3
•Fluorophenol (S) 5 3
.4.6-Tribromophenol (S) 87
AMPLE DUPLICATE: 92103761
Dup.
arameter Units 92101443 Result RPD Footnotes
-Nitrosodimethylamine ug/L ND ND NC
is(2-Chloroethyl)ether ug/L ND ND NC
nenol ug/L ND ND NC
-Chlorophenol ug/L ND ND NC
.3-Dichlorobenzene ug/L ND ND NC
.4-Dichlorobenzene ug/L ND ND NC
.2-Dichlorobenzene ug/L ND ND NC
is(2-Chloroisopropyl)ether ug/L ND ND NC
machloroethane ug/L ND ND NC
-Nitroso-di-n-propylamine ug/L ND ND NC
itrobenzene ug/L ND ND NC
sophorone ug/L ND ND NC
-Nitrophenol ug/L ND ND NC
.4-Dimethylphenol ug/L ND ND NC
Laboratory Certification IDs Laboratory Certification IDs
NCNC Wastewa Drinking Water 37706 ter 1 REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

I
1
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 21
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
AMPLE DUPLICATE: 92103761
Dup.
'arameter Units 92101443 Result RPD Footnotes
,i s(2-Chl oroethoxy)methane . - ug/L . . _ ND . . ND _ _ _ _ .NC
'.4-Di chl orophenol ug/L ND ND NC
.2.4•Trichlorobenzene ug/L ND ND NC
aphthalene ug/L ND ND NC
exachlorobutadiene ug/L ND ND NC
-Chloro-3-methyl phenol ug/L ND ND NC
exachl orocycl opentadi ene ug/L ND ND NC
,4,6-Trichlorophenol ug/L ND ND NC
-Chl oronaphthal ene ug/L ND ND NC
cenaphthylene ug/L ND ND NC
imethylphthalate ug/L ND ND NC
.6-Dinitrotoluene ug/L ND ND NC
cenaphthene ug/L ND ND NC
.4-Dinitrophenol ug/L ND ND NC
.4-Dinitrotoluene ug/L ND ND NC
•Nitrophenol ug/L ND ND NC
luorene ug/L ND ND NC
-Chlorophenyl-phenyl ether ug/L ND ND NC
ethyl phthalate ug/L ND ND NC
.6-Di nitro-2-methyl phenol ug/L ND ND NC
•Nitrosodi phenyl amine ug/L ND ND NC
-Bromophenyl-phenyl ether ug/L ND ND NC
exachlorobenzene ug/L ND ND NC
entachiorophenol ug/L ND ND NC
nenanthrene ug/L ND ND NC
nthracene ug/L ND ND NC
i-n-butylphthalate ug/L ND ND NC
luoranthene ug/L ND ND NC
enzidine ug/L ND ND NC
yrene ug/L ND ND NC
itylbenzylphthalate ug/L ND ND NC
,3'-Dichlorobenzidine ug/L ND ND NC
enzo(a)anthracene ug/L ND ND NC
nrysene ug/L ND ND NC
is(2-Ethylhexyl)phthalate ug/L ND ND NC
i-n-octylphthalate ug/L ND ND NC
enzo(b)fluoranthene ug/L ND ND NC
enzo(k)fl uoranthene ug/L ND ND NC
enzo(a)pyrene ug/L ND ND NC
ndeno(1.2.3-cd)pyrene ug/L ND ND NC
ibenz(a,h)anthracene ug/L ND ND NC
Laboratory Certification IDa Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TKY Drinking N UST List Water 90090
NC Drinking Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

f
I
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 22
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
AMPLE DUPLICATE: 92103761
Dup.
'arameter Units 92101443 Result RPD Footnotes
•enzo(g.h.i)peryl ene ug/L - ND - ND - - - NC - - - - - - - _
;itrobenzene-d5 (S) X 44 79 0
-Fluorobiphenyl (S) X 50 70 0
erphenyl-d14 (S) X 77 90 0
henol-d6 (S) X 24 36 0
'-Fluorophenol (S) X 29 50 0
.4.6-Tribromophenol (S) X 81 92 0
AMPLE DUPLICATE: 92107796
Dup.
arameter Units 92107432 Result RPD Footnotes
-Nitrosodimethylamine ug/L ND ND NC
is(2-Chloroethyl)ether ug/L ND ND NC
henol ug/L ND ND NC
-Chlorophenol ug/L ND ND NC
.3-Dichlorobenzene ug/L ND ND NC
.4-Dichlorobenzene ug/L ND ND NC
.2-Dichlorobenzene ug/L ND ND NC
's(2-Chloroisopropyl)ether ug/L ND ND NC
exachloroethane ug/L ND ND NC
-Nitroso-di-n-propylamine ug/L ND ND NC
itrobenzene ug/L ND ND NC
sophorone ug/L ND ND NC
-Nitrophenol ug/L ND ND NC
,4-Dimethylphenol ug/L ND ND NC
is(2-Chloroethoxy)methane ug/L ND ND NC
,4-Dichlorophenol ug/L ND ND NC
.2.4-Trichlorobenzene ug/L ND ND NC
aphthalene ug/L ND ND NC
exachlorobutadiene ug/L ND ND NC
-Chloro-3-methylphenol ug/L ND ND NC
exachlorocyclopentadiene ug/L ND ND NC
.4.6-Trichlorophenol ug/L ND ND NC
-Chloronaphthalene ug/L ND ND NC
cenaphthylene ug/L ND ND NC
imethylphthalate ug/L ND ND NC
.6-Dinitrotoluene ug/L ND ND NC
cenaphthene ug/L ND ND NC
.4-Dinitrophenol ug/L ND ND NC
Laboratory Certification IDs Laboratory Certification IDs
NC NC WasteDrinking Water 12 REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services.Inc.

i
'
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 23
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
1MPLE DUPLICATE: 92107796
Dup.
irameter Units 92107432 Result RPD Footnotes
4-Dinitrotoluene - ug/L - - - - -ND- - - - - - ND NC
•Nitrophenol ug/L ND ND NC
Iuorene ug/L ND ND NC
,Chlorophenyl-phenyl ether ug/L ND ND NC
iethylphthalate ug/L ND ND NC
,6-Di nitro-2-methyl phenol ug/L ND ND NC
•Nitrosodiphenylamine ug/L ND ND NC
.Bromophenyl-phenyl ether ug/L ND ND NC
?xachlorobenzene ug/L ND ND NC
?ntachlorophenol ug/L ND ND NC
ienanthrene ug/L ND ND NC
ithracene ug/L ND ND NC
i-n-butylphthalate ug/L ND ND NC
Iuoranthene ug/L ND ND NC
?nzidine ug/L ND ND NC
rrene ug/L ND ND NC
rtyl benzyl phthal ate . ug/L ND ND NC
3'-Di chl orobenzi di ne ug/L ND ND NC -
?nzo(a)anthracene ug/L ND ND NC
irysene ug/L ND ND NC
I s(2-Ethyl hexyl)phthal ate ug/L ND ND NC
i-n-octylphthalate ug/L ND ND NC
anzo(b)fluoranthene ug/L ND ND NC
?nzo(k)fluoranthene ug/L ND ND NC
mzo(a)pyrene ug/L ND ND NC
;deno(1.2,3-cd)pyrene ug/L ND ND NC
ibenz(a,h)anthracene ug/L ND ND NC
?nzo(g,h,i)perylene ug/L ND ND NC
itrobenzene-d5 (S) X 78 79 0
•Fluorobiphenyl (S) X 80 82 0
?rphenyl-d14 (S) X 76 72 0
Ienol-d6 (S) X 33 34 0
•Fl uorophenol (S) X 47 47 0
4.6-Tribromophenol (S) X 95 98 0
Laboratory Certification IDs Laboratory Certification IDs
NC
NC Dnnk ng Water 37706 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
TN UST Ust
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services.Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 24
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
602 N. Main St.
owell. NC 28098
ttn: Mr. Bobby Lamb
hone:
C Batch ID: 2661 QC Batch Method: EPA 160.1
nalysis Method: EPA 160.1 Analysis Description: Total Dissolved Solids
ssociated Pace Samples: 92101443 92101468 92101484
ETHOD BLANK: 92102771
ssociated Pace Samples:
92101443 92101468 92101484
Method
Blank
3rameter Units Result PRL Footnotes
)tal Dissolved Solids mg/L 15 1
BBORATORY CONTROL SAMPLE: 92102797
Spike LCS Spike
3rameter Units Conc. Result X Rec Footnotes
)tal Dissolved Solids mg/L 100 122.0 122 4
SIMPLE DUPLICATE: 92102789
Dup.
3rameter Units 9299249 Result RPD Footnotes
:tal Dissolved Solids mg/L 5600 5600 0 4
Laboratory Certification IDs Laboratory Certification IDs
NC
NC Wastewat Drinking Water er 12 REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

a
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 25
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
602 N. Main St.
owell, NC 28098
ttn: Mr. Bobby Lamb
hone:
C Batch ID: 2667 QC Batch Method: EPA 410.4
nalysis Method: EPA 410.4 Analysis Description: Chemical Oxygen Demand
ssociated Pace Samples: 92101443 92101468 92101484
ETHOD BLANK: 92103068
ssociated Pace Samples:
92101443 92101468 92101484
Method
Blank
arameter Units Result PRL Footnotes
hemical Oxygen Demand mg/L ND 25
ATRIX SPIKE: 92103076 Matrix
Spike Spike Spike
arameter Units 9299249 Conc. Result X Rec Footnotes
hemical Oxygen Demand mg/L 1170 400 1592 105
ABORATORY CONTROL SAMPLE: 92103092
Spike LCS Spike
arameter Units Conc. Result X Rec Footnotes
hemical Oxygen Demand mg/L 500 501.0 100
AMPLE DUPLICATE: 92103084
Dup.
arameter Units 9299249 Result RPD Footnotes
hemical Oxygen Demand mg/L 1200 1200 1
)oratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

1ti
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 26
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
602 N. Main St.
owell, NC 28098
ttn: Mr. Bobby Lamb
hone:
C Batch ID: 2756 QC Batch Method: EPA 160.2
nalysis Method: EPA 160.2 Analysis Description: Total Suspended Solids
ssociated Pace Samples: 92101443 92101468 92101484
ETHOD BLANK: 92106061
ssociated Pace Samples:
92101443 92101468 92101484
Method
Blank
rameter Units Result PRL Footnotes
.tal Suspended Solids mg/L ND 1
4B0RATORY CONTROL SAMPLE: 92106087
Spike LCS Spike
3rameter Units Conc. Result % Rec Footnotes
'tal Suspended Solids mg/L 100 94.00 94.0
}MPLE DUPLICATE: 92106079
Dup.
rameter Units 9299397 Result RPD Footnotes
tal Suspended Solids mg/L 8.000 9.000 12
IDoratory Certification IDs J�boratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services.Inc.

1111
Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 27
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
602 N. Main St.
owell, NC 28098
ttn: Mr. Bobby Lamb
hone:
C Batch ID: 2814 QC Batch Method: EPA 3010
nalysis Method: EPA 200.7 Analysis Description: ICP Metals
ssociated Pace Samples: 92101443 92101468
ETHOD BLANK: 92107622
ssociated Pace Samples:
92101443 92101468
Method
Blank
arameter Units Result PRL Footnotes
nromium mg/L ND 0.01
apper mg/L ND 0.01
Inc mg/L ND 0.01
4TRIX SPIKE & MATRIX SPIKE DUPLICATE: 92107630 92107648 Matrix Matrix Spike
Spike Spike Spike Sp. Dup. Dup
arameter Units 92101096 Conc. Result X Rec Result X Rec RPD Footnotes
nromium mg/L 0.01000 1.000 1.040 103 1.070 106 3
upper mg/L 0.01500 1.000 1.035 102 1.040 102 0
inc mg/L 0.1000 2.000 2.190 104 2.240 107 2
4BORATORY CONTROL SAMPLE & LCSD: 92107663 92107671 Spike
Spike LCS Spike LCSD Dup
arameter Units Conc. Result X Rec Result X Rec RPD Footnotes
iromium mg/L 1.000 0.9570 95.7 0.9270 92.7 3
apper mg/L 1.000 0.9540 95.4 0.9230 92.3 3
inc mg/L 2.000 1.920 96.0 1.880 94.0 2
Laboratory Certification IDs j,aboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TKY Drinking N UST Ugwater 90090
NC Drinking Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 28
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
AMPLE DUPLICATE: 92107655
Dup.
arameter Units 92101104 Result RPD Footnotes
nromi um - -mg/L- - - - - ND -ND - - - - NC
upper mg/L ND ND NC
inc mg/L 0.1000 0.07500 33
Laboratory Certification IDs Laboratory Certification IDs
NC
NC Dank w ter 127o6 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 29
rompton & Knowles Pace Project Number: 921533
%0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
602 N. Main St.
.Dwell, NC 28098
,ttn: Mr. Bobby Lamb
hone:
C Batch ID: 2890 QC Batch Method: EPA 3010
nalysis Method: EPA 200.7 Analysis Description: ICP Metals
ssociated Pace Samples: 92101484
ETHOD BLANK: 92110832
.ssociated Pace Samples:
92101484
Method
Blank
arameter Units Result PRL Footnotes
hromium mg/L ND 0.01
opper mg/L ND 0.01
inc mg/L ND 0.01
ATRIX SPIKE & MATRIX SPIKE DUPLICATE: 92112077 92112085 Matrix Matrix Spike
Spike Spike Spike Sp. Dup. Dup
arameter Units 92102177 Conc. Result X Rec Result X Rec RPD Footnotes
hromium mg/L 0 1.000 0.9740 97.4 0.9740 97.4 0
opper mg/L 0 1.000 0.9610 96.1 0.9610 96.1 0
inc mg/L 0.004000 2.000 1.930 96.3 1.930 96.3 0
ABORATORY CONTROL SAMPLE & LCSD: 92110873 92110881 Spike
Spike LCS Spike LCSD Dup
arameter Units Conc. Result X Rec Result X Rec RPD Footnotes
hromium mg/L 1.000 0.9550 95.5 0.9810 98.1 3
opper mg/L 1.000 0.9370 93.7 0.9650 96.5 3
inc mg/L 2.000 1.900 95.0 1.940 97.0 2
Laboratory Certification IDg Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 30
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
AMPLE DUPLICATE: 92110865
Dup.
arameter Units 92101484 Result RPD Footnotes
hromium . .. - - - - - - mg/L 0.2900 - 0.2300 23
opper mg/L 2.900 2.600 11
inc mg/L 0.1700 0.1500 12
•
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater
stewat r 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NCTN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services.Inc.

Pace Analytical Services,Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersvilie,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 31
:rompton & Knowles Pace Project Number: 921533
'.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
.602 N. Main St.
.owel1, NC 28098
,ttn: Mr. Bobby Lamb
'hone:
C Batch ID: 2940 QC Batch Method: EPA 375.2
nalysis Method: EPA 375.2 Analysis Description: Sul fate,Automated Colorimetric
ssociated Pace Samples: 92101443 92101468 92101484 92101518
ETHOD BLANK: 92112374
ssociated Pace Samples:
92101443 92101468 92101484 92101518
Method
Blank
arameter Units Result PRL Footnotes
ulfate mg/L ND 5
ATRIX SPIKE: 92112382 Matrix
Spike Spike Spike
3rameter Units 9297193 Conc. Result X Rec Footnotes
11fate mg/L 0 20 17.82 89.1
\BORATORY CONTROL SAMPLE: 92112408
Spike LCS Spike
3rameter Units Conc. Result X Rec Footnotes
ilfate mg/L 20 24.06 120
AMPLE DUPLICATE: 92112390
Dup.
3rameter Units 9297219 Result RPD Footnotes
ilfate mg/L ND ND NC
I..boratory Certification IDs
I,aboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 32
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
602 N. Main St.
owel1, NC 28098
ttn: Mr. Bobby Lamb
hone:
C Batch ID: 2977 QC Batch Method: EPA 3510
nalysis Method: EPA 1664 Analysis Description: Hexane Extractable Material
ssociated Pace Samples: 92101443 92101468 92101484
ETHOD BLANK: 92113935
ssociated Pace Samples:
92101443 92101468 92101484
Method
Blank
arameter Units Result PRL Footnotes
it and Grease mg/L ND 5
ABORATORY CONTROL SAMPLE: 92113943 __
Spike LCS Spike
arameter Units Conc. Result X Rec Footnotes
it and Grease mg/L 40 19.00 47.5 5
Laboratory Certification IDs
NC Wastewater 12 Laboratory Certification IDs
NC Drinking Water 37706 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 33
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
502 N. Main St.
Dwell, NC 28098
ttn: Mr. Bobby Lamb
lone:
Batch ID: 3015 QC Batch Method: EPA 325.3
ialysis Method: EPA 325.3 Analysis Description: Chloride(Mercuric Nitrate)
ssociated Pace Samples: 92101443 92101468 92101484 92101518
=THOD BLANK: 92115815
ssociated Pace Samples:
92101443 92101468 92101484 92101518
Method
Blank
3rameter Units Result PRL Footnotes
iloride mg/L ND 1
\BORATORY CONTROL SAMPLE: 92115849
Spike LCS Spike
3rameter Units Conc. Result X Rec Footnotes
iloride mg/L 20 20.40 102
kMPLE DUPLICATE: 92115831
Dup.
irameter Units 92112747 Result RPD Footnotes
iloride mg/L 6.100 6.100 0
Laboratory Certification IDs J.boratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services,Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 34
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
502 N. Main St.
owell, NC 28098
tn: Mr. Bobby Lamb
none:
Batch ID: 3121 QC Batch Method: EPA 200F
nalysis Method: EPA 239.2 Analysis Description: Lead by Furnace. Method 239.2
3sociated Pace Samples: 92101443 92101468 92101484
_THOD BLANK: 92119544
:sociated Pace Samples:
92101443 92101468 92101484
Method
Blank
3rameter Units Result PRL Footnotes
ad mg/L ND 0.005
\TRIX SPIKE & MATRIX SPIKE DUPLICATE: 92119551 92119569 Matrix Matrix Spike
Spike Spike Spike Sp. Dup. Dup
3rameter Units 92107473 Conc. Result X Rec Result X Rec RPD Footnotes
aad mg/L 0.005300 0.0250 0.02790 90.4 0.02580 82.0 10
ABORATORY CONTROL SAMPLE & LCSD: 92119585 92119593 Spike
Spike LCS Spike LCSD Dup
3rameter Units Conc. Result X Rec Result X Rec RPD Footnotes
aad mg/L 0.0250 0.02470 98.8 0.02460 98.4 0
AMPLE DUPLICATE: 92119577
Dup.
3rameter Units 92104611 Result RPD Footnotes
?ad mg/L ND ND NC
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinking Water ter 3»os REPORT OF LABORATORY ANALYSIS KY UST UsstWater 90090
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 35
rompton & Knowles Pace Project Number: 921533
.0. Box 848 Client Project ID: Monitoring Wells Sept. 1998
602 N. Main St.
owell. NC 28098
ttn: Mr. Bobby Lamb
none:
Batch ID: 3144 QC Batch Method: EPA 624
nalysis Method: EPA 624 Analysis Description: Volatile GC/MS by 624
ssociated Pace Samples: 92101443 92101468 92101484 92101492 92101500
ETHOD BLANK: 92120146
ssociated Pace Samples:
92101443 92101468 92101484 92101492 92101500
Method
Blank
arameter Units Result PRL Footnotes
nloromethane ug/L ND 5
inyl Chloride ug/L ND 5
-omomethane ug/L ND 5
11oroethane ug/L ND 5
-ichlorofluoromethane ug/L ND 5
.1-Dichloroethene ug/L ND 5
?thylene Chloride ug/L 6.4 5 6
•ans-1.2-Di chl oroethene ug/L ND 5
,1-Dichloroethane ug/L ND 5
is-1.2-Dichloroethene ug/L ND 5
iloroform ug/L ND 5
.1.1-Trichloroethane ug/L ND 5
,2-Dichloroethane ug/L ND 5
irbon Tetrachloride ug/L ND 5
mzene ug/L ND 5
-ichloroethene ug/L ND 5
.2-Dichloropropane ug/L ND 5
-omodichloromethane ug/L ND 5
-Chloroethyl Vinyl Ether ug/L ND 10
s-1.3-Dichloropropene ug/L ND 5
Auene ug/L ND 5
-ans-1.3-Dichloropropene ug/L ND 5
1.2-Trichloroethane ug/L ND 5
bromochloromethane ug/L ND 5
atrachloroethene ug/L ND 5
Laboratory Certification IDs Laboratory Certification IDs
NC
NC Dnnk ng Water 37ewater 12 706 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 36
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
-THOD BLANK: 92120146
ssociated Pace Samples:
92101443 92101468 92101484 92101492 92101500
Method
- - - - - - - Blank
3rameter Units Result PRL Footnotes
ilorobenzene ug/L ND 5
:hylbenzene ug/L ND 5
^omoform ug/L ND 5
.1.2.2-Tetrachloroethane ug/L ND 5
.3-Dichlorobenzene ug/L ND 5
.4-Dichlorobenzene ug/L ND 5
2-Dichlorobenzene ug/L ND 5
,bromofluoromethane (S) X 103
)luene-d8 (S) X 104
•Bromofluorobenzene (S) X 104
\BORATORY CONTROL SAMPLE: 92120153
Spike LCS Spike
:rameter Units Conc. Result % Rec Footnotes
iloromethane ug/L 50 51.00 102
nyl Chloride ug/L 50 44.00 88.0
'omomethane ug/L 50 77.00 154
iloroethane ug/L 50 49.00 98.0
•ichlorofluoromethane ug/L 50 43.00 86.0
1-Dichloroethene ug/L 50 49.00 98.0
?thylene Chloride ug/L 50 43.00 86.0
-ans-1.2-Dichloroethene ug/L 50 49.00 98.0
1-Dichloroethane ug/L 50 50.00 100
s-1.2-Dichloroethene ug/L 50 51.00 102
lloroform ug/L 50 52.00 104
1.1-Trichloroethane ug/L 50 52.00 104
2-Dichloroethane ug/L 50 50.00 100
:rbon Tetrachloride ug/L 50 49.00 98.0
?nzene ug/L 50 47.00 94.0
•ichloroethene ug/L 50 48.00 96.0
2-Dichloropropane ug/L 50 49.00 98.0
•omodichloromethane ug/L 50 48.00 96.0
Chloroethyl Vinyl Ether ug/L 100 49.00 49.0
s-1.3-Dichloropropene ug/L 50 46.00 92.0
Iluene ug/L 50 46.00 92.0
ans-1.3-Dichloropropene ug/L 50 46.00 92.0 •
LaDoratory Certification IDs Laboratory Certification IDs
NC D inki iastewnking ter 3nos REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 37
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
ABORATORY CONTROL SAMPLE: 92120153
Spike LCS Spike
arameter Units Conc. Result X Rec Footnotes
.1.2-Tri chl oroethane - - ug/L 50 - - - -44.00 88.0 - - - - - - - - -
ibromochloromethane ug/L 50 48.00 96.0
etrachloroethene ug/L 50 44.00 88.0
hlorobenzene ug/L 50 46.00 92.0
thylbenzene ug/L 50 44.00 88.0
^omoform ug/L 50 51.00 102
.1.2.2-Tetrachloroethane ug/L 50 48.00 96.0
.3-Dichlorobenzene ug/L 50 46.00 92.0
.4-Dichlorobenzene ug/L 50 46.00 92.0
.2-Dichlorobenzene ug/L 50 48.00 96.0
ibromofluoromethane (S) 115
oluene-d8 (S) 105
•Bromofluorobenzene (S) 100
4MPLE DUPLICATE: 92120161
Dup.
3rameter Units 92110428 Result RPD Footnotes
lloromethane ug/L ND ND NC
nyl Chloride ug/L ND ND NC
-omomethane ug/L 69.00 30.00 77 7
lloroethane ug/L ND ND NC
-ichlorofluoromethane ug/L ND ND NC
.1-Dichloroethene ug/L ND ND NC
ethylene Chloride ug/L ND ND NC
^ans-1.2-Dichloroethene ug/L ND ND NC
.1-Dichloroethane ug/L ND ND NC
s-1.2-Dichloroethene ug/L ND ND NC
iloroform ug/L 15.00 14.00 6
.1.1-Trichloroethane ug/L ND ND NC
2-Dichloroethane ug/L ND ND NC
3rbon Tetrachloride ug/L ND ND NC
enzene ug/L ND ND NC
-ichloroethene ug/L ND ND NC
.2-Dichloropropane ug/L ND ND NC
-omodichloromethane ug/L ND ND NC
-Chloroethyl Vinyl Ether ug/L ND ND NC
is-1.3-Dichloropropene ug/L ND ND NC
Auene ug/L ND ND NC
^ans-1.3-Dichloropropene ug/L ND ND NC
Laboratory Certification IDs Laboratory Certification IDs
NC
NC Drinking Water 37706 water 12 REPORT OF LABORATORY ANALYSIS TN Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services,Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/24/98
PAGE: 38
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
AMPLE DUPLICATE: 92120161
Dup.
arameter Units 92110428 Result RPD Footnotes
.1.2-Trichloroethane - ug/L ND ND - - - -NC - --
ibromochloromethane ug/L ND ND NC
etrachloroethene ug/L ND ND NC
hlorobenzene ug/L ND ND NC
thylbenzene ug/L ND ND NC
romoform ug/L ND ND NC
.1.2.2-Tetrachloroethane ug/L ND ND NC
.3-Dichlorobenzene ug/L ND ND NC
,4-Dichlorobenzene ug/L 94.00 95.00 1
.2-Dichlorobenzene ug/L ND ND NC
ibromofluoromethane (S) X 96 90 0
oluene-d8 (S) X 104 102 0
-Bromofluorobenzene (S) X 99 99 0
Laboratory Certification IDs Laboratory Certification IDs
NC NC Drinking Water ter 3nos REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
TN UST List
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue,Suite 100
Pace Analytical Huntersville,NC 28078
Tel:[phone]
Fax:[phone]
DATE: 09/24/98
PAGE: 39
Pace Project Number: 921533
Client Project ID: Monitoring Wells Sept. 1998
UALITY CONTROL DATA PARAMETER FOOTNOTES
onsistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate X Rec and RPD values.
D Not Detected
C Not Calculable
RL Pace Reporting Limit
PD Relative Percent Difference
S) Surrogate
1] Recovery outside QC limits, however, this compound is not detected in the associated samples.
2] Recovery outside QC limits, however this compound is not detected in the associated samples.
3] The Surrogate recovery value exceeded the established laboratory control limit value.
4] Analyte is found in the associated blank as well as in the sample (CLP B-Flag).
5] LCS is below QC limits.
6] Possible laboratory contaminant.
7] The duplicate analysis was outside QC limits due to matrix interference.
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS TM Drink
g Water 90090
NC Drinking Water 37706
SC 99006 This report shall not be reproduced,except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical Asheville,NC 28801
Tel:[phone]
Fax:[phone]
DATE: 09/21/98
PAGE: 1
1SI Inc. Charlotte Pace Project Number: 93970
300 Kincey Ave. Client Project ID: Crompton & Knowles=921533
Jite 100
Antersville, NC 28078
:tn: Project Management
lone: [phone]
)lid results are reported on a wet weight basis
ice Sample No: 9343567 Date Collected: 09/08/98 Matrix: Water
ient Sample ID: MW 1 101443 Date Received: 09/10/98
irameters Results Units PRL Analyzed Analyst CAS# Footnotes
Chemistry
Phenolics, Total Recoverable Method: EPA 420.1 Prep Method: EPA 420.1
Phenolics, Total Recoverable ND mg/L 0.005 09/15/98 TRW 108-95-2
Total Organic Carbon Method: EPA 9060 Prep Method: EPA 9060
Total Organic Carbon 3.2 mg/L 0.5 09/18/98 BSP 7440-44-0
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced,except in full, FL Environmental 96317
SC Environmental 99030
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
5Pace Analytical A eviUe, NC Drive81
Asheville,NC 28801
Tel:[phone]
Fax:[phone]
DATE: 09/21/98
PAGE: 2
Pace Project Number: 93970
Client Project ID: Crompton & Knowles 921533
'ace Sample No: 9343575 Date Collected: 09/08/98 Matrix: Water
:lient Sample ID: MW 2 101468 Date Received: 09/10/98
'arameters Results Units PRL Analyzed Analyst CAS# Footnotes
Jet Chemistry
Phenolics, Total Recoverable Method: EPA 420.1 Prep Method: EPA 420.1
Phenolics, Total Recoverable ND mg/L 0.005 09/15/98 TRW 108-95-2
Total Organic Carbon Method: EPA 9060 Prep Method: EPA 9060
Total Organic Carbon 5.9 mg/L 0.5 09/18/98 BSP 7440-44-0
NC a Certification IDs REPORT OF LABORATORY ANALYSIS TN ratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 FL Environmental 96317
SC Environmental 99030 This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
q .,��, 54 Ravenscroft Drive
f1 Pace J IalytlCal Asheville,NC 28801
Tel:[phone]
Fax:[phone]
DATE: 09/21/98
PAGE: 3
Pace Project Number: 93970
Client Project ID: Crompton & Knowles 921533
ace Sample No: 9343583 Date Collected: 09/08/98 Matrix: Water .r
lient Sample ID: MW 3 101484 Date Received: 09/10/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
et Chemistry
Phenolics, Total Recoverable Method: EPA 420.1 Prep Method: EPA 420.1
Phenolics, Total Recoverable 8.4 mg/L 1 09/15/98 TRW 108-95-2
Total Organic Carbon Method: EPA 9060 Prep Method: EPA 9060
Total Organic Carbon 3280 mg/L 20 09/18/98 BSP 7440-44-0
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712
Sc Environmental 99030 This report shall not be reproduced,except in full, FL Environmental 96317
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical Asheville,NC 28801
Tel:[phone]
Fax:[phone]
DATE: 09/21/98
PAGE: 4
Pace Project Number: 93970
Client Project ID: Crompton & Knowles 921533
ace Sample No: 9343591 Date Collected: 09/08/98 Matrix: Water —
tient Sample ID: RW 1 101518 Date Received: 09/10/98
arameters Results Units PRL Analyzed Analyst CAS# Footnotes
et Chemistry
Total Organic Carbon Method: EPA 9060 Prep Method: EPA 9060
Total Organic Carbon 78 mg/L 5 09/18/98 BSP 7440-44-0
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 FL Environmental 96317
SC Environmental 99030 This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical Asheville,NC 28801
Tel:[phone]
Fax:[phone]
DATE: 09/21/98
PAGE: 5
Pace Project Number: 93970
Client Project ID: Crompton & Knowles 921533
WAMETER FOOTNOTES
Not Detected
Not Calculable
2L Pace Reporting Limit
•
Laboratory Certification IDg Laboratory Certification IDs
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced,except in full, FL Environmental 96317
SC Environmental 99030
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical Asheville,NC 28801
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/21/98
PAGE: 6
ASI Inc. Charlotte Pace Project Number: 93970
800 Kincey Ave. Client Project ID: Crompton & Knowles 921533
uite 100
untersville, NC 28078
ttn: Project Management
hone: [phone]
_
C Batch ID: 1092 QC Batch Method: EPA 420.1
nalysis Method: EPA 420.1 Analysis Description: Phenolics, Total Recoverable
ssociated Pace Samples: 9343567 9343575 9343583
ETHOO BLANK: 9347899
ssociated Pace Samples:
9343567 9343575 9343583
Method
Blank
arameter Units Result PRL Footnotes
ienolics, Total Recoverable mg/L ND 0.005
ATRIX SPIKE: 9347923 Matrix
Spike Spike Spike
arameter Units 9344359 Conc. Result % Rec Footnotes
henolics, Total Recoverable mg/L 0 0.0287 0.03333 116
ABORATORY CONTROL SAMPLE: 9347907
Spike LCS Spike
arameter Units Conc. Result % Rec Footnotes
henolics, Total Recoverable mg/L 0.0250 0.02700 108
AMPLE DUPLICATE: 9347915
Dup.
arameter Units 9345174 Result RPD Footnotes
henolics, Total Recoverable mg/L 0.01600 0.01800 12
I.boratocy Certification IDS Laboratory Certification IDs
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced,except in full, FL Environmental 96317
SC Environmental 99030 without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical Asheville,NC 28801
Tel:[phone]
Fax:[phone]
QUALITY CONTROL DATA DATE: 09/21/98
PAGE: 7
`SI Inc. Charlotte Pace Project Number: 93970
300 Kincey Ave. Client Project ID: Crompton & Knowles 921533
Jite 100
mtersville, NC 28078
:tn: Project Management
lone: [phone]
Batch ID: 1171 QC Batch Method: EPA 9060
lalysis Method: EPA 9060 Analysis Description: Total Organic Carbon
;sociated Pace Samples: 9343567 9343575 9343583 9343591
=TROD BLANK: 9351503
:sociated Pace Samples:
9343567 9343575 9343583 9343591
Method
Blank
arameter Units Result PRL Footnotes
;tat Organic Carbon mg/L ND 0.5
;TRIX SPIKE: 9351511 Matrix
Spike Spike Spike
]rameter Units 9343567 Conc. Result % Rec Footnotes
)tal Organic Carbon mg/L 3.200 2.000 5.600 120
1BORATORY CONTROL SAMPLE: 9351537
Spike LCS Spike
arameter Units Conc. Result % Rec Footnotes
)tal Organic Carbon mg/L 5.000 5.162 103
AMPLE DUPLICATE: 9351529
Dup.
arameter Units 9343567 Result RPD Footnotes
otal Organic Carbon mg/L 3.200 3.200 0
Laboratory Certification IDs Laboratory Certification Ds
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced,except in full, FL Environmental 96317
SC Environmental 99030
without the written consent of Pace Analytical Services,Inc.

Pace Analytical Services, Inc.
54 Ravenscroft Drive
Pace Analytical Asheville,NC 28801
Tel:[phone]
Fax:[phone]
DATE: 09/21/98
PAGE: 8
Pace Project Number: 93970
Client Project ID: Crompton & Knowles 921533
IUALITY CONTROL DATA PARAMETER FOOTNOTES
:onsistent with EPA guidelines unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
ID Not Detected
IC Not Calculable
'RL Pace Reporting Limit
:PD Relative Percent Difference
L aboratope Certification IDs Laboratory Certification IDs
NC Wastewater 40 REPORT OF LABORATORY ANALYSIS TN Drinking Water 02980
NC Drinking Water 37712 FL Environmental 96317
SC Environmental 99030 This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.