NC0056839_Regional Office Historical File Pre 2018

Pharr-Palomar Pharr Yarns,Inc. / 4A)2 &4 ZDZ5 4)U/)�l
Pharr International,Inc. P.O.Box 1939
EsancE
Sylvania Yarn Systems,Inc. 100 Main Street
McAdenville,NC 28101-1939 NC DEPT,OF E1�11�IRON jgJ
AND NATURAL R
Telephone:[phone]
YOORES'VlLLE PS Orl
Facsimile: 704/824-0072 -477
V/44 .
JAN 0 9 2004
January 6,2004
Mr. John Leslie ,ATE QUiAL BY SECTION
Division of Water Quality SECTION
NC DENR
P H R R 919 North Main Street
YARNS Mooresville,NC 28115
Re: Pharr Yarns, Inc
No.2 Fuel Oil Spill Incident
Occurring on January 5,2004
Gaston County
Dear Mr.Leslie:
A spill of no. 2 fuel was discovered at approximately 9:00 am on Monday, January 5, 2004 by
Scottie Theel; the boiler operator. The location was Stowe Downtown Complex; Continental
Boiler fuel oil feed return line where the piping enters the ground to the 7,500 gallon
underground storage tank Facility ID #: 0-029136, Certificate #: 2003083460. A leak of an
estimated 50 gallons was discharged on the ground with the remaining oil traveling west 10 feet
to the parking lot pavement and then 50 feet to a storm water drain discharging into an unnamed
tributary where it was contained approximately 100 feet downstream. The petroleum
contaminated soil was removed and transported to Environmental Soils, Inc. Non-Hazardous
Waste Mainfest# 16145 & 16146. The approximately 10 to 20 gallons of contained fuel oil on
the water was removed by skimming and oil absorbent materials. HAZ-MAT Transportation
and Disposal. Inc was the contractor performing the clean up and disposal operation. Final
disposal of the water and oil was their facility for fuel oils blending, Non-Hazardous Special
Waste Manifest # 19391 and 19499. Please find attached copies of the above manifest. There
was no fish kill or any evidence of contamination of the stream.
When the spill was discovered our Pharr Yarns Emergency Pollution Incident Procedures were
enacted as follows:
0900: Spill was discovered by Scottie Theel.
0900:The fuel oil pump was turned of and locked out which stopped the leak.
0905: Mike Church,Environmental Engineer,and Jimmy Simpson,plant engineer was
contacted.
0910: Our Emergency Response Contractor,HAZ-MAT was contacted.Jack Holder took our
information and advised that they would leave with the required equipment and personnel
within 15 minutes.Pharr Yarns personnel responded,placed oil absorbent booms in the
stream to contain the fuel oil,and also at the out fall of the storm drain into the stream.
1000: HAZ-MAT arrived and began the clean up.
1700: HAZ-MAT had removed most of the oil and had contained the remaining oil sheen with
absorbent booms and pads.The decision was made to continue the operation the next
morning at daylight.

Page 2
0830:Tuesday 1/6/04.HAZ-MAT returned and continued the clean up.
0900:The contaminated soil was removed and transported to Environmental Soils.
The leak was corrected by replacing the piping at the point of the leak.The
remaining piping was inspected and found to be in excellent condition.
1600: HAZ-MAT concluded the clean up
1630: Mike Church contacted the NC DENR, Water Quality Section,Mr.John
Leslie to report the spill and advise of the completion with no harm to the
Environment.
Please contact me at(704)823-2310 if any other information is needed.
Sincerely,
u G"
Mike Church,
Pharr Yarns Environmental Engineer
I ■

- T HAZ-MAT 3 1
TRANSPORTATION AND DISPOSAL Manifest No.
• P. O. BOX 37392 • CHARLOTTE, N.C. 28237
i ° [phone] P.O. No.
o.M o�,� FAX (7b 4) 375-7183
NON-HAZARDOUS SPECIAL WASTE Job No.
Section I. GENERATOR a.a. n,
GENERATOR LOCATION WORK CONTRACTED BY
Bill To(If different from information at left)
NAME 111,11rr '�gra`5
ORIGINATING ADDRESS _ NAME
MAILING ADDRESS ADDRESS
CITY • 1 e P iNkefr1 vi ST ATE tti C ZIP CITY ST ATE ZIP
PHONE NO. PHONE NO.
CONTACT NAME /`1‘k C.14 1,11e'c h CONTACT NAME
DES.OF WASTE: Uj Type ruts Quantity
Section II. INVOICE'INFORMATION GALLONS DRUMS
DESCRIPTION QUANTITY LINE TOTAL
1. WATER,OIL&COOLANT PUMPED FROM TANKS OR DRUMS •"�
2. OFF SPEC LIGHT OIL,WATER&GAS PUMPED FROM TANKS OR DRUMS
3. 55 GALLON DRUMS REMOVED-SOLID
4. 55 GALLON DRUMS REMOVED-LIQUID
5.
6.
7.
8.
9. ARRIVAL TIME: g '3 n -
10. DEPARTURE TIME: L�^, 3 a
GENERATOR'S CERTIFICATION::: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law,has been properly
described,classified and packaged,and is in proper condition for transportation according to applicable regulations;AND,if the waste is a treatment residue of a previously restrictec
hazardous waste subject to the Land Disposal Restrictions, I certify and warrant that the waste has been treated in accordance with the requirements of 40 CFR Part 268 and is no longe.
a hazardous waste as defined by 40 CFR Part 261.
• 44; re C4 c4 VC _214/u L b 610
Generator Authorized Agent Name Signature Shipment Date
Section III: TRANSPORTER a®.pmt t •r n rmrz•. r�`p-t.t r l ..in
fwara.a ram}
HAZ-MAT TRANSPORTER II
TRANSPORTATION AND DISPOSAL e. Name_
P. O. BOX 37392 • CHARLOTTE, N.C. 28237 f. Address
a.Driver Name/TiUe< f- V 1`Cn g.Driver Name/Title
b.Phone No.'Z64. 31 rk 13 OO c.Truck No. —V g h.Phone No. i.Truck No.
Hazardous Waste Transporter Permits j.Transporter II Permit Nos.
EPA NCR 000003186
EP CD048461370 N
d. PIN 01L � y�
Driver Signature Shipient Date Driver Signature Shiprent Date
I Section IV.i' FACILITY INFORMATION AND CERTIFICATE OF DISPOSAL
Site Name: Haz-Mat Transportation & Disposal. Inc. a. Phone No. 704-332-5600
Physical Address: 210 Dalton Avenue b. Maiing Address: p.O. Box 37392
Charlotte. N.C. 28237 Charlotte. N.C. 28237
e.Discrepancy Indication Space
This is to certify that all non-hazardous material removed from above location has been received and will be disposed of in accordance with applicable local,state and federal regulations in the following manner:(1)Petroleum products
are blended into a beneficial reusable fuel for use in large industrial burners.(2)Waste waters are to be treated with polymers,pH adjusters,and a flocculant,then flows through a dissolved air flotation system for pretreatment separation.
then into the CMUD sanitation sewer system under permit IUP15012. (3) Sludges from treatment systems are hauled to E.P.A. approved facilities for proper disposal. Manifest and certificate of disposal are on file
(4)Our treatment system operates on a first in,first out basis and product should be processed within seven days.
SIGNATURE OF FACILITY AGENT DATE
MONTH DAY . YEAR

• uhz-MAC,• HAZ-MAT Manifest No. 19499
,EAi. TRANSPORTATION AND DISPOSAL
o i.
.Ie . 'A P. O. BOX 37392 • CHARLOTTE, N.C. 28237 r (704)) 332-5600 p0.No. (4 (s'o
?�� ONLY FAX[phone]
r' Job No.
�,,,**°""'� NON-HAZARDOUS SPECIAL WASTE
ISection I. GENERATOR{Generator completes allot Section A,
GENERATOR L 1C,ATION t� C WORK CONTRACTED BY
NAME
Ir\Ct r V VGl,Y 1 ' C Bill To(If different from information at left)
ORIGINATING ADDRESS NAME
MAILING ADDRESS ADDRESS
n /
CITY l l c ` ' cA el^V III e ST ATE l A'.'i£ ZIP CITY ST ATE ZIP
PHONE NO. PHONE NO.
CONTACT NAME (n ►K e C n LA rC h•• CONTACT NAME �� •
DES.OF WASTE: 1 V I 'I k l i t((I 3 IM
No. Type Units Quantity
Section II. INVOICE INFORMATION GALLONS DRUMS
DESCRIPTION QUANTITY UNE TOTAL
1. WATER,OIL&COOLANT PUMPED FROM TANKS OR DRUMS . /(o0
2. OFF SPEC UGHT OIL,WATER&GAS PUMPED FROM TANKS OR DRUMS
3. 55 GALLON DRUMS REMOVED-SOLID -
4. 55 GALLON DRUMS REMOVED-LIQUID
5.
6.
7.
8. I
9. ARRIVAL TIME: 5.' *J ',"
10. DEPARTURE TIME CA.hi tNi
GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law,has been properly
described,classified and packaged,and is in proper condition for transportation according to applicable regulations;AND,if the waste is a treatment residue of a previously restrictec
hazardous waste subject to the Land Disposal Restrictions, I certify and warrant that the waste has been treated in accordance with the requirements of 40 CFR Part 268 and is no longe
a hazardous wa t as defined by 40 CFR Part 261. -.—, , /
! Y
* Generator Authorized Agent Name Signature Shipment Date
ISection III. TRANSPORTER ,sP2,53 mini. ; 'ta 4,7'un`portrCC` pl"'•iv
HAZ-MAT TRANSPORTER II
TRANSPORTATION AND DISPOSAL e. Name —
P. O. BOX 37392 • CHARLOTTE, N.C. 28237 f. Address
a.Driver Name/Title A il al•-/�to l 0eDriver Name/Tale
^ N3 g.
b.Phone No. ?o • 32 • lam' , , c.Truck No. �TZ h.Phone No. i.Truck No.
HazardouAasta Transporter Permits j.Transporter II Permit Nos.
EPA NCR.000003186
EPA NC0048461370 _- ,fI
t �f� ; U *) 7
d Derive Signature gnature v `•`"� Shiment Date Driver Signature hipiem Date
I :Section IV. FACILITY INFORMATION AND CERTIFICATE OF DISPOSAL
Site Name: Haz-Mat Transportation & Disposal. Inc. a. Phone No. 704-332-5600
Physical Address: 210 Dalton Avenue b. Maiing Address: P.O. Box 37392
Charlotte, N.C. 28237 Charlotte. N.C. 28237
e.Discrepancy Indication Space
This is to certify that all non-hazardous material removed from above location has been received and will be disposed of in accordance with applicable local,state and federal regulations in the following manner:(1)Petroleum product
are blended into a beneficial reusable fuel for use in large industrial burners.(2)Waste waters are to be treated with polymers,pH adjusters,and a flocculant,then flows through a dissolved air flotation system for pretreatment separation
then into the CMUD sanitation sewer system under permit IUP/5012. (3) Sludges from treatment systems are hauled to E.P.A. approved facilities for proper disposal. Manifest and certificate of disposal are on file
(4)Our treatment system operates on a first in,first out basis and product should be processed within seven days.
SIGNATURE OF FACILITY AGENT DATE
MONTH DAY YEAR

Environmental Soils Inc.
PO Box 295 • Lattimore,NC 28089
Phone [phone] • Fax [phone]
Non-Hazardous Waste Manifest # 161 a.6
Date / - / - ' Load Number
(numbered sequentially as trucks are dispatched)
ENVIRONMENTAL CONSULTANT.
Contact: Phone: Fax:
GENERATOR: - �i i f _ t,r t�`f'l l •
Address: t), r� « , �� 1`i,, 114 t�;! ( County:
Contact: tV (.1 ��c c r � _ Phone: 7c 4.- )'-'
WASTE ORIGINATION POINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION:(ex.UST or other source) /Yr. 4 t '.° C : 1 / .< ��
f �
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS:In lieu ofsubmitting analytical data(methods
8240 and 8270)verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue,I am submitting this Certfcate of Waste
Constituents.I cert f that I am familiar with the source of contamination of the soil and further certj the source,to
the best of my knowledge,contains no contaminants other than that listed above.
TRANSPORTER — f l !_ t1?)
Contact: ` .-- / _ I< •!"/ / Phone:
As the carrier,I certify that the materials described above being shipped under this non-hazardous materials
manifest are properly classified,packaged,labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
4I /cW
i
go O _
TRUCK#: ' TAG#: VOLUME: 'O -I/' 3
TRUCK DRIVER SIGNATURE: .% c-,^ "_ DATE: /` 7 - o y
DESTINATION: Environmental Soils Inc. 910 Crowdy Rd, Shelby,NC 28150 Dedicated Land Application
Site Permit#SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature:%�' �- Date: / `" /
y ,
Signature: ) '� LU .�' �-z . Date: 4-1
/ -
Company Name Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore,NC 28089
Phone 704,434-0075 • Fax [phone]
/— Non-Hazardous Waste Manifest # 1614 5
Date — Load Number
(numbered sequentially as trucks are dispatched)
ENVIRONMENTAL CONSULTANT
Contact: Phone: Fax:
GENERATOR 1-1 r'r- r 4 r-rUS
i'} l c� ; ,► rc(
Address: , �C �1, C. r�:�, >U'(.1 rti C County:
Contact: k t_ F i` Phone: --1 C;q 3
WASTE ORIGINATION POINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION: (ex.UST or other source) /Y 1/1 G / / r // 1
( I
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS:In lieu ofsubmitting analytical data(methods
8240 and 8270)•ver(ing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue,I am submitting this Certificate of Waste
Constituents.I cent)that I am familiar with the source of contamination of the soil and further certtft the source,to
the best of my knowledge,contains no contaminants other than that listed above.
/72
TRANSPORTER •
Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non-hazardous materials
manifest are properly classified,packaged,labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK#: TAG#: VOLUME: "3r.. 'r - i r_+ 3
TRUCK DRIVER SIGNATURE: ( �•.�^, f :u o
DATE: / � � - y
DESTINATION: Environmental Soils Inc. 910 Crowdy Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit#SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facilitynature:
Signature: 1=-t Date: / — .r. —
-Si nature: - -7- Date: l
-- ,
Company Name Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Pharr-Palomar Pharr Yarns,Inc.
Pic DEPT.OF Eliw;;ANIBIT
Pharr International,Inc. P.O.Box 1939 AND NATURAL RESOURCES
Sylvania Yarn Systems,Inc. 100 Main Streetrr SV}�E F G4o ,j
(.� ,.. .
McAdenville,Nt 28101 1939 ;
„
Telephone:[phone]
Facsimile: 704/824-0072 MAY 2 0 2003
May 14, 2003 WATER oo urfsErrripi
Mr. Samar Bou-ghasale
Division of Water Quality
P H AR R NCDENR
YARNS 919 North Main Street
Mooresville, North Carolina 28115
Re: Pharr Yarns, Space Dye Division
Fuel Oil Spill
Gaston County
Dear Mr. Bou-ghasale:
Please find attached our report of the fuel oil spill that was reported by telephone on
April 21 s`. The spill was contained and the contaminated soil removed for disposal
by our spill response contractor. We estimated that approximately 85 gallons was
captured near the facility and approximately 15 gallons was removed in the
containment area described in the report.
If any other information is needed please contact me at [phone].
Sincerely,
,..-27/dcy
Mike Church
Pharr Yarns Environmental Engineer

Pharr-Palomar Pharr Yarns,Inc.
Pharr International,Inc. P.O.Box 1939
Sylvania Yarn Systems,Inr. 100 Main Street
McAdenville,NC 28101-1939
Telephone:[phone] .
Facsimile: 704/824-0012
April 28, 2003
Re: Space Dye Oil Spill, SPCC Report
Friday, August 18, 2003
PHARR
YARNS 4:45 PM I was advised by James Davis of a spill of No. 6 fuel oil
from the Space Dye boiler room traveling east and downhill
toward the South Fork River where it was contained by natural
ground topography. However heavy rain caused some of the fuel
oil to enter a natural drainage ditch. The river had risen to three
feet above flood level, causing concern about the fuel oil entering
the river.
4:50 PM I called our Emergency Response Contractor, Haz-Mat, Jack
Holder, who advised that all his equipment was in use and that
he would contact Hepaco for immediate response.
5:00 PM Bob Baxter of Hepaco called and I advised him of our needs.
James Davis called Vernan Sherrill Backhoe Service who arrived
within minutes and removed most of the oil contaminated soil
• and placed it on plastic for disposal. George Altice placed
two floating booms from our emergency inventory below the
spill in the old abandoned raceway prior to reaching the river.
7:00 PM Hepaco arrived, placed an 18 inch floating boom on the
flooded area below the two existing booms and the river to
make sure that no fuel could reach the river, and began their
cleanup procedures.
Saturday April 19, 2003
12:00 AM The cleanup continued at the contained area by Hepaco and their
vac truck was used at the boiler room to clean up the fuel oil spill.
02:00 AM Any remaining fuel oil was contained and the river level was
receding, the clean up was discontinued until the next morning.

Page 2
7:00 AM Hepaco arrived and began removing the remaining oil with a
floating skimmer and absorbent material.
3 :00 PM Hepaco completed their cleanup service.
Monday, April 21, 2003
9:00 AM After the river receded to normal level, some of the remaining
fuel oil on the banks of the contained area had attached
to vines, other vegetation, and debris. Absorbent material was
placed in the old raceway area upstream of the floating booms.
Straw was applied to the banks and a controlled burn with
post cleanup accomplished the final removal of fuel oil.
April 28, 2003
9:00 AM Final removal of the contaminated soil was transported by
Haz-Mat for approved disposal.
Cause of the spill: A leak of approximately 100 gallons in the boiler
recirculation piping system located near the pump was not detected. The
drainage ditch from the boiler room to the oil separation / pumping station
overflowed outside of the boiler room at an open 90 degree connection box to
underground piping ending at the oil separation / pumping station. The spill
occurred when the water softener automatically backwashed causing the ditch
to overflow. Failure of the oil alarm and wastewater transfer pumping station
allowed the drain to overflow.
Corrective action taken to prevent future spills New and improved pump
controls have been installed which alternate the dual pumps and provide a back
up in case of pump failure. A purchase order has been issued for a state of the
art fuel leak detection alarm. The controller output will be connected to our
plant security 24 hour call service for the oil detection alarm and high water
alarm for the pumping system. Inspection of all of the piping from the fuel oil
underground storage tanks to the boiler room was conducted and all piping
with evidence of corrosion has been replaced.
Closer attention to the existing Pharr Yarns Environmental Procedures which
include the Fuel Oil SPCC Check List and Storm Water Pollution Prevention
Plan Check List along with the physical improvements will help to prevent and
insure that no future oil spills occur.
Events recorded by: Mike Church, Pharr Yarns Environmental Engineer

Pharr-Palomar Pharr Yarns,Inc.
Pharr International,Inc. P.O.Box 1939
Sylvania Yarn Systems,Inc. 100 Main Street
McAdenville,NC 28101.1939
Telephone:[phone] •
Facsimile: 704/824-0072
April 28, 2003
Re: Space Dye Oil Spill, SPCC Report
Friday, August 18, 2003
PHARR
YARNS 4:45 PM I was advised by James Davis of a spill of No. 6 fuel oil
from the Space Dye boiler room traveling east and downhill
toward the South Fork River where it was contained by natural
ground topography. However heavy rain caused some of the fuel
oil to enter a natural drainage ditch. The river had risen to three
feet above flood level, causing concern about the fuel oil entering
the river.
4:50 PM I called our Emergency Response Contractor, Haz-Mat, Jack
Holder, who advised that all his equipment was in use and that
he would contact Hepaco for immediate response.
5:00 PM Bob Baxter of Hepaco called and I advised him of our needs.
James Davis called Vernan Sherrill Backhoe Service who arrived
within minutes and removed most of the oil contaminated soil
and placed it on plastic for disposal. George Altice placed
two floating booms from our emergency inventory below the
spill in the old abandoned raceway prior to reaching the river.
7:00 PM Hepaco arrived, placed an 18 inch floating boom on the
flooded area below the two existing booms and the river to
make sure that no fuel could reach the river, and began their
cleanup procedures.
Saturday April 19, 2003
12:00 AM The cleanup continued at the contained area by Hepaco and their
vac truck was used at the boiler room to clean up the fuel oil spill.
02:00 AM Any remaining fuel oil was contained and the river level was
receding, the clean up was discontinued until the next morning.

Page 2
7:00 AM Hepaco arrived and began removing the remaining oil with a
floating skimmer and absorbent material.
3 :00 PM Hepaco completed their cleanup service.
Monday, April 21, 2003
9:00 AM After the river receded to normal level, some of the remaining
fuel oil on the banks of the contained area had attached
to vines, other vegetation, and debris. Absorbent material was
placed in the old raceway area upstream of the floating booms.
Straw was applied to the banks and a controlled burn with
post cleanup accomplished the final removal of fuel oil.
April 28, 2003
9:00 AM Final removal of the contaminated soil was transported by
Haz-Mat for approved disposal.
Cause of the spill: A leak of approximately 100 gallons in the boiler
recirculation piping system located near the pump was not detected. The
drainage ditch from the boiler room to the oil separation / pumping station
overflowed outside of the boiler room at an open 90 degree connection box to
underground piping ending at the oil separation / pumping station. The spill
occurred when the water softener automatically backwashed causing the ditch
to overflow. Failure of the oil alarm and wastewater transfer pumping station
allowed the drain to overflow.
Corrective action taken to prevent future spills: New and improved pump
controls have been installed which alternate the dual pumps and provide a back
up in case of pump failure. A purchase order has been issued for a state of the
art fuel leak detection alarm. The controller output will be connected to our
plant security 24 hour call service for the oil detection alarm and high water
alarm for the pumping system. Inspection of all of the piping from the fuel oil
underground storage tanks to the boiler room was conducted and all piping
with evidence of corrosion has been replaced.
Closer attention to the existing Pharr Yarns Environmental Procedures which
include the Fuel Oil SPCC Check List and Storm Water Pollution Prevention
Plan Check List along with the physical improvements will help to prevent and
insure that no future oil spills occur.
Events recorded by: Mike Church, Pharr Yarns Environmental Engineer

PiF7j. AMichael F. Easley,Governor
9P6 William G. Ross Jr.,Secretary
North Carolina Department of Environment and Natural Resources
cf) Alan W. Klimek, P.E. Director
> Division of Water Quality
January 31, 2003 ACDEPT•OF ENVIRONMENT
`l. rtirILIRAL RESOURCES
5278IMOWESV tLLE RF~ICMA! NFL
Mr. Mike Church
'� T-
Pharr Yarns, Inc.PO Box 1939 FEB 0 3 2003
McAdensville, NC 28101-
QUALSUBJECT: Wastewater/Groundwater Laboratory Certification Renewal
FIELD PARAMETERS ONLY ` � arTIO.N
Dear Mr. Church:
The Department of Environment and Natural Resources, in accordance with the provisions of NC GS
143-215-.3 (a) (10), 15 NCAC 2H .0800, is pleased to renew certification for your laboratory to perform
specified environmental analyses required by EMC monitoring and reporting regulations 15 NCAC 2B
.0500, 2H .0900 and 2L .0100, .0200, .0300, and 2N .0100 through .0800.
Enclosed for your use is a certificate describing the requirements and limits of your certification.
Please review this certificate to insure that your laboratory is certified for all parameters required to
properly meet your certification needs.
Please contact us at 919-733-3908 if you have questions or need additional information.
Sincerely,
Steve W. Tedder
Laboratory Section Chief
Enclosure
cc: James W. Meyer
Chester E. Whiting
Mooresville Regional Office
NCDENtit
Laboratory Section N. C. Division of Water Quality 1623 Mail Service Center Raleigh, NC 27699-1623
[phone] Fax: [phone] Internet: dwglab.org Customer Service 1-800-623-7748

STATE OF NORTH CAROLINA DEPARTMENT OF THE
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
LABORATORY CERTIFICATION PROGRAM
In accordance with the provisions of N.C.G.S. 143-215.3(a)(1), 143-215.3(a)(10)and NCAC 2H.0800:
Field Parameter Only
%ç2oTAT r ›,, 11/ .
ry
)° J. t L , -i •
PHARR YARNS, INC.
Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data to DWQ for
compliance with NPDES effluent, surface water, groundwater, and pretreatment regulations.
By reference 15A NCAC 2H.0800 is made a part of this certificate.
This certificate does not guarantee validity of data generated, but indicates the methodology, equipment, quality control procedures,
records, and proficiency of the laboratory have been examined and found to be acceptable.
This certificate shall be valid until December 31, 2003
Certificate No. 5278
WL----- -eoc- /---______
Steve W. Tedder

Attachment I
North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Pharr Yarns, Inc. Certificate Number: 5278
Address: PO Box 1939 Effective Date: 01/31/2003
McAdensville, NC 28101- Expiration Date: 12/31/2003
Date of Last Amendment:
The above named laboratory,having duly met the requirements of 15A NCAC 2H.0800,is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
INORGANICS
RESIDUAL CHLORINE
Std Method 4500 CI G
CONDUCTIVITY
Std Method 2510E
DISSOLVED OXYGEN
Std Method 4500 0 G
pH
Std Method 4500 H B
RESIDUE SETTLEABLE
Std Method 2540F
TEMPERATURE
Std Method 2550E
This certification requires maintance of an acceptable quality assurance program,use of approved methodology,and satisfactory performance on evaluation samples. Laboratories are
subject to civil penalties and/or decertification for infractions as set forth in 15A NCAC 2H.0807.