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WQ0006984_Regional Office Historical File Pre 2018
LE AL, NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory Donald van der Vaart Governor Secretary April 2, 2015 Mr. Steve Slaughter, Plant Manager Delta Apparel, Inc. P.O. Box 37 Maiden, North Carolina 28650 Subject: Acknowledgement of Receipt of the 2014 Annual Report Delta Apparel, Inc. - Permit No.: WQ0006984 Land Application of Residuals (503 Exempt) Catawba County Dear Mr. Slaughter: The Mooresville Regional Office (MRO) received and reviewed the 2014 Annual Report for the above permit. The data submitted appears to be in accordance with permit requirements. The residuals produced from this facility routinely show a high Sodium Absorption Ratio (SAR). The SAR issue was addressed in a February 7th, 2014 letter from Eric Thompson (SYNAGRO), which satisfies the requirement of permit condition 11.10. I may be reached by phone at (704) 663-1699 or email (maria.schutte(&-ncdenr.gov) should you have any questions. Sincerely, Maria Schutte, Environ ental Specialist Mooresville Regional Office Water Quality Regional Operations Section Division of Water Resources, NCDENR . CC: Wayne Kelly, WWTP ORC (email) Marshall Puryear, SYNAGRO (email) Eric Thompson, SYNAGRO (email) Ed Hardee, LAU Compliance,. CO -Raleigh (email) Mooresville Regional Office 610 East Center Avenue, Suite 301, Mooresville, North Carolina 28155 Phone: 704-663-16991 Fax: Jor-663-6040 / Customer Service 1-877-623-6748 Internet: www.nedenr.gov , vl "FCE'VLt-DAVCDENFMWFj MAR 9 2015 FA00REsvILL WOROS E REGIONAL OFFICE DELTA APPAREL, INC. — MAIDEN, NC RESIDUALS LAND APPLICATION PROGRAM CL5J\ Permit No. WQ0006984 2014 ANNUAL REPORT Al 791 ZJ Delta Apparel, Inc. - Maiden, NC Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, & Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Pages 3. Field Summary Forms 4. TCLP Analysis 6. Pathogen Reduction/ Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00006984 County Catawba Year 2014 Facility Name (as shown on permit) Delta Apparel. Inc./Maiden Plant NPDES No. NC0006190 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and Part Band proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 16 Total number of fields utilized for land application during the year: 6 Total amount of dry tons applied during the year for all application sites: 353.55 Total number of acres utilized for land application during the year: 119.1 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water QualityX YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Steve Slaughter, Plant Manager Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Pennittee) i i n e Da 1213 �015 Signature of Land Applier Date (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 20J4 ANNUAL OPERATIONS SUMMARY - LARD APPLICATION DELTA APPAREL, INC., NC DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE REBID. LIQUID MONTH/YEAR May 2014 YEARLY TOTAL AMOUNT UNIT 1,469,400.00 G 1,469,400.00 G DRY TORTS UNIT 353.55 D 353.55 D DRY METRIC TONS 320.66 320.66 1 /31 /2015 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006984 - Laboratory Facility Name: DELTA APPAREL, INC., NC A&L Eastern Laboratories Inc. NPDES# : NCO006190 or WQ# (residual only) WWTP Name: DELTA APPAREL - MAIDEN PLANT Residuals Analysis Data Product Type TXLIQ TXLIQ TXLIQ TXLIQ Date Sampled (grab) or 03/14/14 05/13/14 12/22/14 12/22/14 Date Composited Percent Solids 5.77 4.87 2.89 2.98 PARAMETERS (mg/kg dry weight) Arsenic <3 <3 <3 <3 Cadmium <2 <2 <2 <2 Mercury <0.4 <0.4 <0.4 <0.4 Chromium 9 71 11 11 Copper 639 691 699 700 Lead <5 <5 <5 <5 Molybdenum <5 <5 <5 <5 Nickel 17 43 22 22 Selenium <5 <5 <5 <5 Zinc 60 99 58 55 Total Phosphorus 6120 5100 5640 5490 TKN 79200 62200 66400 69100 Ammonia -Nitrogen 4510 12300 4150 3690 Nitrate and Nitrite <2 18.5 <2 <2 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and' evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date , —2 Irza 0rC;�_0 C ,s— DENR FORM RSSF (5/2003) Printed: Saturday - January 31, 2015 at 13:53:23 for: 2105 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006984 Facility Name: DELTAAPPAREL, INC., NC NPDES# : NC0006190 or WQ# (residual only) WWTP Name: DELTA APPAREL - MAIDEN PLANT Residuals Analysis Data Laboratory A&L Eastern Laboratories Inc. Product Type TXLIQ TXLIQ TXLIQ TXLIQ Date Sampled (grab) or 03/14/14 05/13/14 12/22/14 12/22/14 Date Composited Percent Solids 5.77 4.87 2.89 2.98 PARAMETERS (mg/kg dry weight) Aluminum 1100 10400 1900 2100 Calcium 2590 3280 4290 4270 Magnesium 1010 1520 1240 1190 pH 7.51 8.14 7.72 7.65 Potassium 3180 4440 4140 4320 Sodium 37200 45600 52200 53600 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date -0 OF NR - Data Not Reported or Data Not Required DENR FORM RSSF-13 (7/2002) Printed: Saturday - January 31 2015 at 13:53.46 for: 2105 01 Product Code Product Name Sample Date Report Range Ratio 2105-01-TXLIQ-NC DELTA APPAREL, INC., NC MAIDEN 3/14/2014 411/2014-6/30/2014 37.5880 PLANT TEXTILE RESID. LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (37200 x 5.7700) + 100 = 2146.44 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (2590 x 5.7700) + 100 = 149.443 Mg mg/I = (mg mg/kg x % Solids) = 100 = (1010 x 5.7700) _ 100 = 58.277 Na meq = Na mg/I = Molec.Wgt.Na = 2146.44 = 23 = 93.3235 Ca meq = Ca mg/I = Molec.Wgt.Ca = 149.443 + 20 = 7.47215 Mg meq = Mg mg/I = Molec.Wgt.Mg = 58.277 + 12 = 4.85642 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 93.3235 = SgrRoot[0.5(7.47215+4.85642 (]=�J37.588 Printed: 1/31/2015 Page 1 13:45 1�y 1�f ` n � � r rl y. r �� .J L•J \•! l f F• �� •' , \•` 'I.1 ��l i.r a u� 4 �• \ J j'• Product Code Product Name Sample Date ReportRange Ratio 2105-01-TXLIQ-NC DELTA APPAREL, INC., NC MAIDEN 5/13/2014 / / - / / 36.2927 PLANT TEXTILE RESID. LIQUID Na mg/I = (Na mg/kg x % Solids) = 100 = (45600 x 4.8700) _ 100 = 2220.72 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (3280 x 4.8700) + 100 = 159.736 Mg mg/I = (mg mg/kg x % Solids) + 100 = (1520 x 4.8700) _ 100 = 74.024 Na meq = Na mg/I + Molec.Wgt.Na = 2220.72 _ 23 = 96.553 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 159.736 _ 20 = 7.9868 Mg meq = Mg mg/I + Molec.Wgt.Mg = 74.024 + 12 = 6.16867 SAR = Na meq - SgrRoot[0.5 x (Ca meq + Mg meq)] = 96.553 _ SgrRoot[0.5(7.9868+6.16867�]'=- 36.2927 Printed: 1 /31 /2015 Page 1 13:54 �' a �l i1'� .� � ,re " .•�'' • * .� .}': . if P, � . � q t e�', /j1 '�� 'c LJ L L e t � � 1 1 � � '�� l � �f V Lam•. � i 4 � :�k � � v/ i �0 i Product Code Product Name Sample Date. Report Range Ratio 2105-01-TXLIQ-NC DELTA APPAREL, INC., NC MAIDEN 12/22/2014 / / - / / 30.6060 PLANT TEXTILE RESID. LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (52200 x 2.8900) _ 100 = 1508.58 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (4290 x 2.8900) - 100 = 123.981 Mg mg/I = (mg mg/kg x % Solids) = 100 = (1240 x 2.8900) + 100 = 35.836 Na meq = Na mg/I = Molec.Wgt.Na = 1508.58 _ 23 = 65.5904 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 123.981 + 20 = 6.19905 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 35.836 = 12 = 2.98633 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 65.5904 _ SgrRoot[0.5(6.19905+2.98633)] 30.606 Printed: 1/31/2015 Page 1 13:45 .� Y �pi i r♦�� ° �.. V 1 A ' f . �l •` _ i ; �R f a_ j> ,,�. s '.1 Ct i I; .� Product Code Product Name Sample Date ReportRange Ratio 2105-01-TXLIQ-NC DELTA APPAREL, INC., NC MAIDEN 12/22/2014 / / - / / 32.1751 PLANT TEXTILE RESID. LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (53600 x 2.9800) - 100 = 1597.28 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (4270 x 2.9800) - 100 = 127.246 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1190 x 2.9800) _ 100 = 35.462 Na meq = Na mg/I + Molec.Wgt.Na = 1597.28 _ 23 = 69.447 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 127.246 + 20 = 6.3623 Mg meq = Mg mg/I = Molec.Wgt.Mg = 35.462 + 12 = 2.95517 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 69.447 _ SgrRoot[0.5(6.3623+2.95517)] = �.�J51 Printed: 1 /31 /2015 Page 1 13:46 ANNUAL LAND APPLICATION + + LD SUMMARY FORM FACILITY NAME: DELTA APPAREL, INC., NC PREDOMINANT SOIL SERIES: CECIL OWNER: WILLIAM SAINE PERMIT ti: WQ0006984 SITE #: NC CA 00005 FIELD# : CA 00005 0001 A OPERATOR: TODD EDWARDS RESIDUAL SOURCE(S):"' See list at bottom ofreport ANNUAL DRY TONS APPLIED: 47.74 CATION EXCHANGE CAPACITY (NON 503): ACRES UTILIZED: 26.70 ACRES PERMITTED: 26.70 Page: 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic'Yards (CY) or Wet Tons (WT) (specify) % . Dry Tons Per Residual Site Cond. Dry, Wet, Incites Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TICN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/13/14 24,800.00 (G) 928.839 5.77 0.223 DAMP= DRY 0-<1/2" SUR 0.5 0.30 79,200.p 4,510.00 p 2.00 p 24664 FESCUE 5/14/14 173,600.00 (G) 6501.8731 5.77 1.564 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664 FESCUE Ality-14 198,400.00 (G) 7,430.712 Total Gallons/Ac: 7,430.71 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 88 0.011 0.007 0.032 2.285 0.018 0.001 0.018 0.061 0.018 0.215 21.88 Cumulativelbs/acre 0.050 0.032 0.344 24.971 0.132 0.010 0.105 0.674 0.057 4.953 l''tvta��`rmji rtt.0 q+' 1 1 Permit Limit 1 acre r � PANL i (bsl ) 1st Crop/2ndCop �ta°.�d,' it rAa 4a-~<7r ?.. .t• 34f_` P,; .,(,17Y,+. R's9i`�;'�'l.it'; s'L Li:..�',4 vjl r_�G'�1�w 5'-�i rw,7 \f eP' �.3 "; ';lh x ^"J'^l�lSr .,. P,p.l�u'n .�,i �v�k..;.,. 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 h<+w��' ` Y'' 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X ©2—L3 (SIGNATURE OF LAN APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for lorowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg "" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation a ""' See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: DELTA APPAREL, INC., NC PREDOMINANT SOIL SERIES: CECIL OWNER: DENNIS LUTZ PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 59.67 SITE #: NC CA 00006 FIELD# : CA 00006 0001 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 20.40 ACRES PERMITTED: 20.40 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip, Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation THIN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/8/14 167,400.00 (G) 8205.882 5.77 1.974 DAMPTXL DRY 0- 1/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664 I FESCUE 5/9/14 80,600.00 (G) 3950.980 5.77 0.951 DAMPT.NL DRY 0- 1/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664 FESCUE May-14 248,000.00 (G) 12,156.862 Total Gallons/Ac: 12,156.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Amoral lbs/acre 144 0.018 0.012 0.053 3.738 0.029 0.002 0.029 0.099 0.029 0.351 35.80 Cumulative lbs/acre 0.056 0.036 0.303 23.382 0.129 0.012 0.107 0.606 0.070 4.449 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X If 2—li-) ' ) (SIGNATURE OF L APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonnnent for luiowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/lcg *'r Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: DENNIS LUTZ SITE #: NC CA 00006 FIELD# : CA 00006 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: IIIWASSEE PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 65.64 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 20.10 ACRES PERMITTED: 20.10 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN m in ) Cro p Total Per Acre MONTH 5/9/14 148,800.00 (G) 7402.985 5.77 1.781 DAMPTXL DRY 0-<I/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664 I FESCUE 5/12/14 124,000.00 (G) 6169.154 5.77 1.484 DAMPTXL DRY 0-<I/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664 FESCUE May-14 272,800.00 (G) 13,572.139 Total Gallons/Ac: 13,572.14 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 161 0.020 0.013 0.059 4;173 0.033 0.003 0.033 0.111 0.033 0.392 39.97 Cumulative Ibs/acre 0.056 0.039 0.347 24.174 0.132 0.011 0.115 0.674 0.067 4.042 Permit PAN Limit (lbs/acre) 1st Crop/2nd CropT 216 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X (SIGNATURE OP D APPL R) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hrjection/hicorporation 1.0 "• Application Method: SUR - Surface, INJ - hijection, SUR1N - hicorporation :r•:r•:r. See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: DENNIS LUTZ SITE #: NC CA 00006 FIELD# : CA 00006 0003 RESIDUAL SOURCE(S):* See list at bottom of report [AHA:L:LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: HIWASSEE PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 71.61 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 19.30 ACRES PERMITTED: 19.30 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pp"') Crop MONTH Total Per Acre Solids 5/12/14 111,600.00 (G) 5782.383 5.77 1.391 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 79,200.p 4,510.00 p 2.00 p 24664 I FESCUE 5/13/14 186,000.00 (G) 9637.306 5.77 2.319 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664 FESCUE May-14 1 297,600.00 (G) 15,419.689 Total Gallons/Ac: 15,419.69 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 183 0.022 0.015 0.067 4.742 0.037 0.003 0.037 0.126 0.037 0.445 45.41 Cumulative Ibs/acre 0.041 1 0.027 1 0.223 1 15.937 1 0.102 0.010 0.086 1 0.393 0.076 2.490 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop i 216 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 i 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X 2-0 / (SIGNATURE X0AND 'LIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ - hijection, SURIN- Incorporation *'`* See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: WADE SAINE SITE #: NC LT 00038 FIELD# : LT 00038 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: MASADA PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 49.23 OPERATOR: WADE ICENHOUR CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 14.60 ACRES PERMITTED: 14.60 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 5/7/14 148,800.00 (G) 10191.781 5.77 2.452 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664 I FESCUE 5/8/14 55,800.00 (G) 3821.918 5.77 0.920 DAMPTXL DRY 0- 1/2" SUR 0.5 0.30 79,200.p 4,510.00 p 2.00 p 24664 FESCUE May-14 1 204,600.00 (G) 14,013.699 1 Total Gallons/Ac: 14,013.70 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 166 0.020 0.013 0.061 4.309 0.034 0.003 0.034 0.115 0.034 0.405 41.27 Cumulative lbs/acre 0.047 0.035 0.330 21.387 0.117 0.008 0.094 0.625 0.053 3.632 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 y 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X L,12_4 1,41 (SIGNATURE OF LAND IER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or nig/Icg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN- hicorporation r** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: DELTA APPAREL, INC., NC PREDOMINANT SOIL SERIES: GASTON OWNER: WAYNE GILBERT PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 59.67 SITE #: NC LT 00120 FIELD# : LT 00120 0001 OPERATOR: WAYNE GILBERT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.00 ACRES PERMITTED: 18.00 Page: 1 Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/6/14 186,000.00 (G) 10333.333 5.77 2.486 DAMPTXL DRY 0-<I/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664. I FESCUE 5/7/14 62,000.00 (G) 3444.444 5.77 0.829 DAMPTXL DRY 0-<I/2" SUR 0.5 0.30 79,200. p 4,510.00 p 2.00 p 24664 FESCUE May-14 1 248,000.00 (G) 13,777.777 1 Total Gallons/Ac: 13,777.78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 164 0.020 0.013 0.060 4.237 0.033 0.003 0.033 0.113 0.033 0.398 40.58 Cumulative lbs/acre 0.064 0.058 0.417 30.548 0.255 0.014 0.156 0.905 0.084 7.523 T ------- Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID x f L Lo (SIGNATURE OF LAND PLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or tng/lcg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 r Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 Y11 F14TVIROHIr1PTIiL1Er;;[.lr]LG March 26, 2014 Eric Thompson Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Delta Dear Eric Thompson: Sununit Enviromnental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX. (330) 253-4489 Website: hM2:1Ammv.settek.conr Order No.: 14031663 Summit Enviromnental Technologies, Inc. received 1 sample(s) on 3/14/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, A-W-� Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arkansas 88-0735, Califomia 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-01-1-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon 0I-1200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 6 ou Fr , ONMENTALI 0 L 0 S I E 5: ;Pic Anm'yff!-�zl L-bof-afor�e,�k SununitEnviroynnental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX. (330) 253-4489 Mebsite: hUp.-11Jvmv.settekcom Workorder Sample Summary WO#: 14031663 26-Mar-14 CLIENT: Synagro Project: Delta Lab SampleID Client Sample ED Tag No Date Collected Date Received Matrix 14031663-001 Delta 3/14/2014 10:00:00 AM 3/19/2014 9:45:00 AM Sludge Page 2 of 6 z iLr j,' Stnnn:itErxvironmental Technologies, Inc. y��� Narrative htiit�i,�_1�ju}!� Li 3310YVinSt. �.r 1 Ft;'dl^nr}CIF1cJTALTEC;'=!Obac-1_c,;,tt; Cuyahoga Falls, Ohio WO#: 14031663 Ans? •cc�i i ibo;.,?hwies TEL: (330) 253-8211 FAX: (330) 253-4489 Website: httP:/Amvmsettekcon: Date: 3/26/2014 CLIENT: Synagro Project: Delta This report uz its entirety consists of the documents listed below. All documents contain the Sumnnit Enviromnental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with these results and data should be considered as esti hated. Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any comments or problems with the analytical events associated with this report are noted below. Original Page 3 of 6 RNVInOHMENTAL :cL`t Cc'��GG:cS, INC Ar.at,dicai L;=4 t71-i3h);,Fe Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hgg.-lAtnviv.settekcon? WO#: 14031663 Date Reported 3/26/2014 Company: Synagro Address: 284 Boger Rd. Mocksville NC 27028 Received: 3/14/2014 Project#: Delta TCLP Metals Analysis (6010) Client E# Lab EN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 001 3/14/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 3/24/2014 VVK Delta 001 3/14/2014 TCLP Barium(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 3/24/2014 VVK Delta 001 3/14/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 3/24/2014 VVK Delta 001 3/14/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 6010 C 1 5.0 . 3/24/2014 VVK Delta 001 3/14/2014 TCLP Lead(Pb) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 3/24/2014 VVK Delta 001 3/14/2014 TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 3/24/2014 VVK Delta 001 3/14/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 3/24/2014 VVK TCLP Mercury Analysis (1311/7470) Client ID# Lab IID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 001 3/14/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 3/24/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client ION Lab )m# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 001 3/14/2014 Chlordane, total 0.010 ND mg/L Sludge EPA 8081 B 1 0.030 3/25/2014 JBN Delta 001 3/14/2014 Toxaphene 0.10 ND mg/L Sludge EPA 8081 B 1 0.50 3/25/2014 JBN Delta 001 3/14/2014 Endrin 0.0020 ND mg/L Sludge EPA 8081 B 1 0.020 3/25/2014 JBN Delta 001 3/14/2014 gamma-BHC 0.0020 ND mg/L Sludge EPA 8081 B 1 0.40 3/25/2014 JBN Delta 001 3/14/2014 Heptachlor 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 3/25/2014 JBN Delta 001 3/14/2014 Heptachlor epoxide 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 3/25/2014 JBN Delta 001 3/14/2014 Methoxychlor 0.0020 ND mg/L Sludge EPA 8081 B 1 10 3/25/2014 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 001 3/14/2014 1,1-Dichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 3/24/2014 MES Delta 001 3/14/2014 1,2-Dichloroetharie 0.10 ND mg/L Sludge EPA 8260B 1 0.50 3/24/2014 MES Delta 001 3/14/2014 Benzene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 3/24/2014 MES Delta 001 3/14/2014 Carbon tetrachloride 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 3/24/2014 MES Delta 001 3/14/2014 Chlorobenzene 0.10 ND mg/L Sludge EPA 8260 B 1 100 3/24/2014 MES Delta 001 3/14/2014 Chloroform 0.10 ND mg/L Sludge EPA 8260 B 1 6.0 3/24/2014 MES Delta 001 3/14/2014 Tetrachloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 3/24/2014 MES Delta 001 3/14/2014 Trichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 3/24/2014 MES Delta 001 3/14/2014 Vinyl chloride 0.20 ND mg/L Sludge EPA 8260 B 1 0.20 3/24/2014 MES Delta 001 3/14/2014 MEK 2.0 ND mg/L Sludge EPA 8260 B 1 200 3/24/2014 MES Page 4 of 6 Ir 6wR tiwEwrAL7ct^a'C.;r1L[1GIE5,PIC; ll�!� Aj afv, --. i L;�baraiar/r5 SununitEnvironmental Technologies, bsc• WO#: 14031663 3310 Win St. Cuyahoga Falls, Ohio 44223 Date Reported 3/26/2014 TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: htb:11wivw.settek.con: Address: 284 Boger Rd. Mocksville NC 27028 Received: 3/14/2014 Project#: Delta SVOC 8270 TCLP BNA List Client EN Lab IN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 001 3/14/2014 1,4-Dichlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 7.5 3/26/2014 JBN Delta 001 3/14/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 400 3/26/2014 JBN Delta 001 3/14/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 2.0 3/26/2014 JBN Delta 001 3/14/2014 2,4-Dinitrotoluene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 3/26/2014 JBN Delta . 001 3/14/2014 Cresols, Total 5.0 ND mg/L Sludge EPA 8270 C 1 200 3/26/2014 JBN Delta 001 3/14/2014 Hexachloro-1,3- 0.10 ND mg/L Sludge EPA 8270 C 1 0.50 3/26/2014 JBN butadiene Delta 001 3/14/2014 Hexachlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 3/26/2014 JBN Delta 001 3/14/2014 Hexachloroethane 0.10 ND mg/L Sludge EPA 8270 C 1 3.0 3/26/2014 JBN Delta 001 3/14/2014 Nitrobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 2.0 3/26/2014 JBN Delta 001 3/14/2014 Pentachlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 100 3/26/2014 JBN Delta 001 3/14/2014 Pyridine 0.25 ND mg/L Sludge EPA 8270 C 1 5.0 3/26/2014 JBN SVOC SW-846: 8321 Herbicides-TCLP Client F D# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 001 3/14/2014 2,4-D 5.0 ND mg/L Sludge EPA 8321 A 1 10 3/25/2014 AMZ Delta 001 3/14/2014 2,4,5-TP 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 3/25/2014 AMZ Page 5 of 6 r (i. aiJ it rP{VI nS� hl lel Et,ITAL I Er HNO L0,»GI E s,. ptc,, Ucoi Usi7Qre3ft7�rt ., Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL. (330) 253-8211 FAX.- (330) 253-4489 Website: htto:1Aiunv.settekcou: WO#: 14031663 Date Reported 3/26/2014 Company: Synagro Address: 284 Boger Rd. Mocksville NC 27028 Received: 3/14/2014 Project#: Delta Client EN Lab ID# Collected Analyse Result Units Matrix Method Dk+ RL Run Analyst Delta 001 3/14/2014 Flashpoint (140T) >200 T Sludge EPA 1010 1 3/20/2014 TJR Delta 001 3/14/2014 Cyanide, Reactive ND ppm Sludge EPA 9014 1 0.50 3/21/2014 TIR Delta 001 3/14/2014 pH 6.5 s.u. Sludge EPA 9045 D 1 3/19/2014 AYS Delta 001 3/14/2014 Sulfide, Reactive ND ppm Sludge EPA 9034 1 25 3/21/2014 TIR Page 6 of 6 RcY. 12 Data: 07127113 Summit Environmental Technologies, inc. Cooley Receipt form Cfunl: t)r�� In teals c{ person inspzpting COolerand sa:iPl Order Number. E)ate Raceivad(I L f rme Recel pate coofer(s) op=ned and sampt=s i spertetl: J q /L� Number cf Ceo!ers/Boaes:�_ WA Shfpper. FEE) 6Z(DJ DHL Airborne US Postal Walk-in Pi:3mp a:ber. pa"1"iging: Paanwa Bubblawii8 P a >P r Foam None OIhEr UPC on coolerfbox• -^ Custody Seats intact N WA � t�1 C•o•C in plastF N NIA Ita-Blu _ Oy N IVAelce present 1 absent 1 melted N,rq Sample Tcmperalura IR Gun SS6.� 0359 CF D -C _ .� tC RadiologiwfTestinq Instrument serial il35727 n'A y {see pag: 2 forscan resLdts) Use1sheet per sample for RadlofogleaiTesting, N Immediately. ifsamptoIsHOP,thaRadlologfcalSaietyOificormusttrenoGifed Gp-C filled orat propsrly N Sa;rypl„-g in separate bags N/A Saropla Wntainers intact- y N N 'If no, list broken svr•nnters NIA Sampfo labels) Complete (It,, date. etc.) LabelG s) agree with O.0 N N N+A Coved canlalners used � • NIA Sugrjeni sample received M N , tfA Bubbleg absent from AO rriL vials•• NIA Y N Sampes with bubbles aEmm are axepfahfa. Mdicate bubble size it'rtxrun_ Was client contacted about sarnp;es y wig Client send new sampfes N Client Contact. Y rf t.oi ml in G:WO WR OIDo armant Corltrcl Temp ales - TraMrg}S"y,f-re e(pf Rev.12 47--2T 13.t3pc . •FAgo i o'f2 •. Summit ct n enter[ Technologies, inc. 3310 �V a Stratrr:et Analysis Request/Chain/Chain of Custody Cuyahoga Fails, .Ohio 44, 223 Tel: 330.253.$211 Fax: 33U 253.440 lictr Summit Environmental Technologies; lnc. use only Company Nuw��z//. (I !case Print) proje/c�t Numc Analyt[cal.P;t".slriaera' apd Methaib - Company 2,94 �Aeddrs/} 70s Projcct Addres s ..-- SA�✓1 S � a49CV —L6 , 1-1C 4h616 .� a Client. Phone No. Rt:porr In ClicnlFIX ho. PIVI" rax Resultc Sb -d Cl£i [Email /� pIE:lNaMaitResttlt$2 Qeolc�Vo. , �T�OM aAd d id, 0r . e Contact Pelson Sanplud by check if Oltio 4i1P samples ✓ c -4 y err sinnple Idzntifieation Dote Time Collected Collected J LPL He In utahed bp W Time Received b : Dale 'Glnc NoteslConmrenle: e3 -1regoo'. Rece 'e - Dale abue S ish Rcyt.utilcQ R. Must 6e ;PPru.1'd pale Ur lab nn unu¢r " A'hilc and }nllox pa4ec slmulil aceuml ny samples :o dw InFurawiti'q'ir client realwi die phik page. 92402 2R0n ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name Delta Apparel Inc. WWTP Name Delta Apparel, Inc. WWTP Monitoring Period: From 01/01/14 Permit Number WQ0006984 NPDES # NC0006190 To 12/31/14 Pathogen Reduction (40CFR 503.32) - Please indicate level achieved and alternative performed Class A Alternative 1 Alternative 4 Class B Alternative 1 Alternative 2 Alternative 5 Alternative 2 Alternative 3 Alternative 6 Alternative 3 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"; Aerobic Dig. Air Dry Anaerobic Dig. Compost Lime Stab. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Pathogen Densi 'No. of Freq. Of Sample Analytical Level in Exceed Analysis Type Tech. Sludge Min. Geo. Max. Units Mean Fecal 2x106 MPN/g Coliform MPN/g or 2x 106 CFU/g CFU/g 1000 MPN MPN/g Salmonella 3 MPN/ bacteria 4 g Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed Option 1 Option 2 Option 3 Option 4 Option 5 Option 6 Option 7 Option 8 Option 9 Option 10 No vector attraction options were performed % CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the athoen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CPR 59.33 have been met." "I certify, under penalty of law that the pathogen requirements In 40 CFR 503.32 and the vector attraction reduction requirement in CVR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Preparer Name and Title Land Applier Name and Title (if applicable) Signature of Preparer Date Signature of Land Applier (if applicable) Date Pathogen and Vector Attraction Deduction is not required by permit, no signatures required. Agricultural Lime Application Log Year: 2014 Project: Delta Apparel, Inc. Field Soil pH Lime Requirement Tons/Acre Date Applied (state -county -site -field code) 1 11 T/ac (calculated) I Applied ii NC-CA-5-1A 6.8 N/A N/A N/A _ NC-CA-6-1 6.8 N/A N/A N/A _ NC-CA-6-2 5.5 1.3 NC-CA-6-3 5.9 0.2 NC-LT-38-1 6.8 N/A N/A N%A. NC-LT-120-1 6.5 N/A N/A N/A Page 1 of 1 Report Number: 15-027-0676 Account Number:46718TL www,Send To: SYNAGRO CENTRAL/DELTA APPAREL aleastern,com Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/27/2015 Date Of Analysis: 01/28/2015 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-8401 Fax (804) 271.6446 Grower: SAINE/EDWARDS DELTAANNUAL SOIL ANALYSIS .REPORT Date Of Report: 01/28/2015 Submitted By: ERIC THOMPSON Farm ID: CA-5 Analytical Method(s): Mehlich 3 Organic.Matter Phosphorus Potassium Magnesium Calcium -Sodium pH Acidity C,E.0 Sample ID Field ID Lab Number % Rate ENR Mehlich3. Reserve K Mg Ca Na =Soil, <Buffer' . .H Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm -Rate: pH index meq/100g meq/100g 1A 12271 10.0 VH 150 95 H 290 VH 537 VH 1639 M 37 VL 6.8 0.4 14.0 NC=79 NC=148 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl Al % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm - Rate ppm 1A 22 M 9.2 VH 45 H 157 VH 9.3 VH 1.2 M 0.19 VL 5.3 32.0 58.5 1.1 2.9 " NC=46 NC=230.0 NC=281 NC=465.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/1009 maximum of thirty days after testing. by; pAµrio m° GSA H (High); VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble ,analysis prepared by: A&L Eastern Laboratories, Inc. v C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 1 of 1 Report Number: 15-027-0677 Y Account Number: 46718 !"!� Send To: SYNAGRO CENTRAL/DELTA APPAREaleastertl,com Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/27/2015 Date Of Analysis: 01/28/2015 A&L Easters Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (004) 271-6446 Grower: LUTZ DELTAANNUAL SOIL ANALYSIS REPORT Date Of Report: 01/28/2015 Submitted By: ERIC THOMPSON Farm ID: CA-6 Analytical Method(s): Mehlich 3 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab . % Rate ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number Ibs/A ppm, Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 1 120 VH 328 VH 523 VH 1449 M 34 VL 12272 11.4 VH 150 6.8 0.4 13.0 NC=100 NC=168 _ 2 H 284 VH H 992 L 64 L -` 12273 14.2 VH 150 176 1296 5.5 6.64 2.9 11.4 = NC 63 C= N145 � 3 37 M 388 VH 303 VH 930 L 50 L I 12274 10.7 VH 150 5.9 6.76 1.7 10.1 = NC 31 NC=198 �� Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1 17 M 9.4 VH 60 VH 120 VH 8.3 VH 1A M 0.17 VL 6.5 33.5 55.7 1.1 2.9 INC =35 NC=235.0 NC=375 NC=415.0 2 H H VH VH 11.1 VH 0.9 M 0.2 VL 6.4 21.6 43.5 2.4 25.7 134 16.6 �92 �155 NC = 71 NC = 165.0 NC = 575 NC = 555.0 3 M 5.9 H 116 VH VH 6.3 VH 0.7 M 0.27 VL 9.9 25.0 46.0 2.2 17.2 124 1110 NC=50 NC=147.5 NC=725 NC=315.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a / soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. v C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 1 of 1 Report Number: 15-020-0566 Account Number:46718 tLj www.Send To: SYNAGRO CENTRAUDELTAAPPARELaleastent.com Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/20/2015 Date Of Analysis: 01/21/2015 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (604) 271-6446 Grower: SAINE/ISENHOUR DELTAANNUAL SOIL ANALYSIS REPORT Date Of Report: 01/23/2015 Submitted By: ERIC THOMPSON Farm ID: LT-38 Analytical Method(s): Mehlich 3 Organic Matter, Phosphorus Potassium -. Magnesium Calcium Sodium. J pH " Acidity QE.0 Sample ID' Lab Field ID Number % Rate ENR Mehlich 3 Reserve K - Mg Ca Na - Soil- Buffer H- Ibs7A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meg1100g megl100g 1 31 M 44 VL 360 VH 1072 M 47 L 07468 6.3 H 150 6.8 0.3 8.9 NC=26 NC=23 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS CI Al % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate 'ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1 9 VL 4.7 H 44 H 80 VH 4.6 VH 0.8 M 0.08 VL 1.3 33.7 60.2 2.3 2.9 NC = 19 NC = 117.5 NC = 275 NC = 230.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), megl100g maximum of thirty days after testing. me H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: t1 PAu�'6 e0"' C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary Page 1 of 1 Report Number: 15-020-0568� p Account number: 46718 1,;,� �U `" 0 www,aleasterii.com Send To: SYNAGRO CENTRAL/DELTAAPPAREL Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 n�ro Qo, or„per• n•t1,)n19n1F natp of Anaivsisr 01/21/2015 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743 9401 Fax (804) 271 6446 Grower: W GILBORT DELTAANNUAL SOIL ANALYSIS REPORT Date Of Report: 01/23/2015 Submitted By: ERIC THOMPSON Farm ID: LT-120 Analytical Method(s): Mehlich 3 Z Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 1 Reserve K Mg Ca Na Soil Buffer - H Field ID Number % Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 1 07471 12.3 VH 150 23 L 177 H 400 VH 1323 M 60 L 6.5 0.9 11.5 NC=19 NC=91 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS Cl AI Field ID % % % % % PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate ms/cm Rate PP m Rate ppm 1 18 M 6.2 H 80 VH 57 VH 9.9 VH 1.2 M 0.1 VL 3.9 29.0 57.5 2.3 7.4 NC = 37 NC = 155.0 NC = 500 NC = 495.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: ��rric umc G� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc, v C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary „Vr�� ��*A ILE NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory Governor Mr. Steve Slaughter, Delta Apparel, Inc. P.O. Box 37 Plant Manager Maiden, North Carolina 28650 Dear Mr. Slaughter: John E. Skvarla, III Secretary Subject: Acknowledgement of Receipt of the 2013 Annual Report Delta Apparel,'lnc. - Permit No.: WQ0006984 Land Application of Residuals (503 Exempt) Catawba County The Mooresville Regional Office (MRO) received and reviewed the 2013 Annual Report for the above permit. The data submitted appears to be in accordance with requirements of your permit. The high Sodium Absorption Ratio (SAR) was addressed in the February 7, 2014 letter from Eric Thompson (Synagro), which satisfies the requirement of permit condition 11.10. may be reached by phone at (704) 663-1699 or email (maria.schutte(@ncdenr.gov) should you have any questions. Sincerely, Maria Schutte, Environmental Specialist Mooresville Regional Office Water Quality Regional Operations Section Division of Water Resources, NCDENR CC: Wayne Kelly, WWTP ORC (email) Marshall Puryear, Synagro (email) Eric Thompson, Synagro (email) Ed Hardee, LAU Compliance, CO -Raleigh (email) Mooresville Regional Office, 610 East Center Avenue, Mooresville, North Carolina 28155 Phone: 704-663-16991 Internet: www.ncdenr.gov An Equal Opportunity 1 Affirmative Action Employer — Made in part by recycled paper k" 'e l 1 J L014 DELTA APPAREL, INC. — MAIDEN, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0006984 2013 ANNUAL REPORT Delta Apparel, Inc. -Maiden, NC Residuals Land Application Program 2013 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, & Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Pages 3. Field Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/ Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00006984 County Catawba Year 2013 Facility Name (as shown on permit) Delta Apparel. Inc./Maiden Plant NPDES No. NC0006190 Land Application Operator Svnagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and Part Band proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summ Total number of application fields in the permit: 16 Total number of fields utilized for land application during the year: 5 Total amount of dry tons applied during the year for all application sites: 133.04 Total number of acres utilized for land application during the year: 96.7 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2013 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Steve Slauehter, Plant Manager Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2013 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION DELTA APPAREL, INC., NC DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID MONTHNEAR April 2013 May 2013 YEARLY TOTAL AMOUNT UNIT 812,200.00 G 775,000.00 G 1,587,200.00 G DRY TONS UNIT 68.08 D 64.96 D 133.04 D DRY METRIC TONS 61.76 58.91 120.67 2/7/2014 2013 ANNUAL REPORT PROJECT: FACILITY: NPDES PERMIT NUMBER: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPAR€R OF LAND APPLICATION ANNUAL REPORT: Delta Apparel, Inc. Delta Apparel, Inc., WWTP P.O. Box 37 (100 West Pine Street Maiden, NC 28650 NC0006190 Steve Slaughter, Plant Manager Delta Apparel, Inc., WWTP P.O. Box 37 (100 West Pine Street) Maiden, NC 28650 828-428-9921 Wayne Kelly, ORC Delta Apparel, Inc., WWTP P.O. Box 37 Maiden, NC 28650 828-428-9921, ext. 290 Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006984 Facility Name: DELTA APPAREL, INC., NC_ NPDES# : NC0006190 or WQ# (residual only) WWTP Name: DELTA APPAREL - MAIDEN PLANT Residuals Analysis Data Product Type TXLIQ Date Sampled (grab) or 03/13/13 Date Composited Percent Solids 2.01 PARAMETERS (mg/kg dry weight) Arsenic <3 Cadmium <2 Mercury 1.2 Chromium 11 Copper 939 Lead <5 Molybdenum <5 Nickel 19 Selenium 5 Zinc 132 Total Phosphorus 4970 TKN 57700 Ammonia -Nitrogen 5470 Nitrate and Nitrite 114 Laboratory A&L EASTERN LABORATORIES, INC. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X TURE OF PREP Date �r " C� o DENR FORM RSSF (5/2003) Printed: Friday - February 7 2014 at 10:42.25 for: 2105 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006984 Facility Name: DELTA APPAREL, INC., NC NPDES# : NC0006190 or WQ# (residual only) WWTP Name: DELTA APPAREL - MAIDEN PLANT Residuals Analysis Data Product Type TXLIQ Date Sampled (grab) or 03/13/13 Date Composited Percent Solids 2.01 PARAMETERS (mg/kg dry weight) Aluminum 1800 Calcium 6650 Magnesium 978 pH 7.86 Potassium 5420 Sodium 79800 Laboratory A&L EASTERN LABORATORIES, INC. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date C;,? r/ 9'"�lg y / NR - Data Not Reported or Data Not Required DENR FORM RSSF-B (7/2002) Printed: Friday - February 7 2014 at 10:42:47 for: 2105 01 Page: 1 of 2 Report Number: 13-078-0203 Account Number: 46718 Submitted By: ERIC THOMPSON Send To: SYNAGRO CENTRAUDELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 92500 Sample Id : DELTA �L A&L. Eastern Laboratories, Inc: 7621 Whitepine Road Richmond, Virginia 23237 (004) 743-9401 Fax (604) 271-6446 www aleastern.com Project: DELTA NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/13/2013 12:45:00 Date Received: 03/19/2013 00:00 Date Reported: 03/22/2013 Total Solids * 2.01 20100 100.0 JM 03/19/2013 14:44 SM-254OG Moisture * 97.99 106.0 JM 03/19/2013 14:44 SM-2540G Total Kjeldahl Nitrogen 5.77 57700 10.0 JM 03/20/2013 08:10 SM-4500-NH3C-TKN Total Phosphorus 0.50 4970 100 KM 03/20/2013 08:25 SW 6010C Total Potassium 0.54 5420 100 KM 03/20/2013 08:25 SW 6010C Total Sulfur 3.06 30600 100 KM 03/20/2013 08:25 SW 6010C Total Calcium 0.67 6650 100 KM 03/20/2013 08:25 SW 6010C Total Magnesium 0.10 978 100 KM 03/20/2013 08:25 SW 6010C Total Sodium 7.98 79800 100 KM 03/20/2013 08:25 SW 6010C Total Iron 3340 100 KM 03/20/2013 08:25 SW 6010C Total Aluminum 1800 100 KM 03/20/2013 08:25 SW 6010C Total Manganese 62 5 KM 03/20/2013 08:25 SW 6010C Total Copper 939 5 KM 03/20/2013 08:25 SW 6010C Total Zinc 132 5 KM 03/20/2013 08:25 SW 6010C Ammonia Nitrogen 0.55 5470 10.0 JM 03/20/2013 08:10 SM-4500-NH3C . Organic N 5.22 52230 10.0 03/20/2013 08:10 CALCULATION Nitrate+Nitrite-N 114 2.00 JM 03/20/2013 08:10 SM-450ONO3F Total Cadmium <2.0 2.0 KM 03/20/2013 08:25 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made ,(i? to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 13-078-0203 Account Number: 46718 Submitted By: ERIC THOMPSON Send To: SYNAGRO CENTRAUDELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 92500 Sample Id : DELTA LA&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-94QI Fax (604) 271-696 www aleastern.coni Project : DELTA NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/13/2013 12:45:00 Date Received: 03/19/2013 00:00 Date Reported: 03/22/2013 Total Chromium 11 5 KM 03/20/2013 08:25 SW 6010C Total Nickel 19 5 KM 03/20/2013 08:25 SW 6010C Total Lead <5 5 KM 03/20/2013 08:25 SW 6010C Total Arsenic <3.0 3.0 KM 03/20/2013 08:25 SW 6010C Total Mercury 1.2 DA KM 03/20/2013 12:00 SW-7471 B Total Selenium 5.0 5.0 KM 03/20/2013 08:25 SW 6010C pH (Standard Units) * 7.86 2.00 JM 03/20/2013 08:10 SW-9045D Total Molybdenum <5 5 KM 03/20/2013 08:25 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2105-01-TXLIQ-NC DELTA APPAREL, INC., NC MAIDEN 3/13/2013 4/l/2013-5/31/2013 34.1891 PLANT TEXTILE RESID. LIQUID Na mg/I = (Na mg/kg x % Solids) = 100 = (79800 x 2.0100) _ 100 = 1603.98 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (6650 x 2.0100) _ 100 = 133.665 Mg mg/I = (mg mg/kg x % Solids) = 100 = (978 x 2.0100) = 100 = 19.6578 Na meq = Na mg/I = Molec.Wgt.Na = 1603.98 = 23 = 69.7383 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 133.665 _ 20 = 6.68325 Mg meq = Mg mg/1— Molec.Wgt.Mg = 19.6578 = 12 = 1.63815 + 1 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 69.7383 _ SgrRoot[0.5(6.68325+1.63815)] = 34.1891 Printed: 2/7/2014 Page 1 10:45 Agricultural Lime Application Log Year: 2013 Project: Delta Apparel, Inc. Field (state -county -site -field code) Soil pHqJ Lime RequirementTons/Acre (from soil F- Applied -11 Date Applied NC-CA-6-1 5.4 0.9 NC-CA-6-2 6.6 0.0 NC-CA-6-3 6.1 0.0 IA NC-CA-20-1 5.9 0.0 7 -NYA,- NC-CA-22-1 5.6 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: DELTA APPAREL, INC., NC PREDOMINANT SOIL SERIES: CECIL OWNER: DENNIS LUTZ PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 21.31 SITE #: NC CA 00006 FIELD# : CA 00006 0001 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 20.40 ACRES PERMITTED: 20.40 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 4/22/13 130,200.00 (G) 6382.353 2.01 0.535 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 57,700.p 5,470.00 p 114.00 p 18518 FESCUE 4/23/13 124,000.00 (G) 6078.431 2.01 0.509 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 57,700. p 5,470.00 p 114.00 p 18518 FESCUE Apr-13 254,200.00 (G) 1 12,460.784 Total Gallons/Ac: 12,460.78 As Cd Cr. Cu Ph Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.006 0.004 0.023 1.961 0.010 0.003 0.010 0.040 0.010 0.276 10.38 39 Cumulative Ibs/acre 0.039 1 0.024 1 0.250 19.643 1 0.099 0.009 0.078 1 0.507 0.040 4.098 ' Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop k I 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 2679 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X 0 (SlGNAJTJRE 0 AND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for lwowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Ityection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: DENNIS LUTZ SITE #: NC CA 00006 FIELD# : CA 00006 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: HIWASSEE PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 25.46 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 20.10 ACRES PERMITTED: 20.10 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppin) Crop MONTH Total Per Acre Solids 4/23/13 62,000.00 (G) 3084.577 2.01 0.259 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 57,700. p 5,470.00 p 114.00 p 18518 FESCUE 4/24/13 167,400.00 (G) 8328.358 2.01 0.698 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 57,700. p 5,470.00 p 114.00 p 18518 FESCUE 4/25/13 74,400.00 (G) 3701.493 2.01 0.310 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 57,700. p 5,470.00 p 114.00 p 11118 FESCUE Apr-13 303,800.00 (G) 15,114.428 Total Gallons/Ac: 15,114.43 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 47 0.008 0.005 0.028 2.379 0.013 0.003 0.013 0.048 0.013 0.334 12.59 Cumulative lbs/acre 0.037 0.025 0.288 20.001 0.100 0.009 0.082 0.563 0.035 3.650 � Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop �, ? -° 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 l 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID IV X !4 (SIGN RE OF AND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: DENNIS LUTZ SITE #: NC CA 00006 FIELD# : CA 00006 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: I-HWASSEE PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 21.31 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 19.30 ACRES PERMITTED: 19.30 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppnl) Crop MONTH Total Per Acre Solids 4/25/13 80,600.00 (G) 4176.166 2.01 0.350 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 57,700. p 5,470.00 p 114.00 p 18518 I FESCUE 4/26/13 173,600.00 (G) 8994.819 2.01 0:754 DAMPTXL DRY 0-<I/2" SUR 0.5 0.30 57,700. p 5,470.00 p 114.00 p 18118 FESCUE Apr-13 1 254,200.00 (G) 139170.985 1 Total Gallons/Ac: 13,170.98 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.007 0.004 0.024 2.073 0.011 0.003 0.011 0.042 0.011 0.291 10.97 41 Cumulative lbs/acre 0.019 1 0.012 1 0.157 1 11.195 1 0.064 0.007 0.049 0.267 0.039 2.045 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop f a r 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X %� J r (SIGNA RE OF L D APPLIER) DATE "I ce tfy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/lcg *`r Volatilization Rate: Surface 0.5, hrjection/Incorporation 1.0 k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: HAROLD SHERRILL SITE #: NC CA 00020 FIELD# : CA 00020 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LLOYD PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 34.30 OPERATOR: WALLY SAINE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 16.80 ACRES PERMITTED: 16.80 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/9/13 204,600.00 (G) 12178.571 2.01 1.021 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 57,700. p 5,470.00 p 114.00 p 18518 I FESCUE 5/10/13 204,600.00 (G) 12178.571 2.01 1.021 DAMPTXL DRY 0-<1/2" SUR. 0.5 0.30 57,700.p 5,470.00 p 114.00 p 18118 FESCUE May-13 1 409,200.00 (G) 24,357.142 1 Total Gallons/Ac: . 24,357.14 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.012 0.008 0.045 3.834 0.020 0.005 0.020 0.078 0.020 0.539 20.29 76 Cumulative lbs/acre 0.025 1 0.016 1 0.181 1 13.292 1 0.076 0.010 0.060 1 0.310 0.050 2.377 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 i' DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID x G` ® X9% �f (SIGNA OF LPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/lcg k* Volatilization Rate: Surface 0.5, hrjection/Incorporation 1.0 V Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: MICHAEL SIGMON SITE #: NC CA 00022 FIELD# : CA 00022 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LLOYD PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 30.66 OPERATOR: TIME HEFNER CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 20.10 ACRES PERMITTED: 20.10 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) . % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/1/13 198,400.00 (G) 9870.647 2.01 0.827 DAMPTXL MOIST 0-<I/2" SUR 0.5 0.30 57,700. p 5,470.00 p 114.00 p 8518FESCUE F11511 5/4/13 167,400.00 (G) 8328.358 2.01 0.698 DAMPTXL MOIST 0-<1/2" SUR 0.5 0.30 57,700.p 5,470.00 p 114.00 p FESCUE May-13 1 365,800.00 (G) 18,199.005 Total Gallons/Ac: 18,199.00 As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.009 0.006 0.034 2.865 0.015 0.004 0.015 0.058 0.015 0.403 15.16 56 Cumulative Ibs/acre 0.009 0.006 0.034 1 2.865 1 0.015 1 0.004 0.015 1 0.058 0.015 0.403 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop ' : 7' .w 1 216 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID Iq X (SIGNAT OF LAr APPLIER) DATE "I certify, under pen ty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for luiowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014 LABORATORY REPORT Client Synagro Southeast 284 Boger Fad. Mocksville, NC 27028 Order Number 1304674 Project Number Delta Issued Wednesday, March 27, 2013 Total Number of Pages 5 (excluding C.O.C. and cooler receipt form) Approved C QA Manage Certifications: A2LA/DOD 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943. Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH- 13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146. Louisiana 04061 and LA12004, Maine 2012015, Maryland 339. Massachusetts M-OPH923, Michigan (Reg.5), Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 5 WG-15J, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 "analytical Integrity" - EPA Certified . NEL.AP Certified 3310 Win Street • Cuyahoga Palls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489 Web Site: www.settek.com ENVIRONMENTALiUMMIT TECHNOLOGIES, •-4 `'f ' lytical Laboratories Sample Summary Client: Synagro Southeast Order Number: 1304674 Laboratory ID Client ID Matrix Sampling Date 1304674-01 Delta Solid 3/13/2013 "Analytical Integrity" - EPA Certified - NELAP Certified 3310 Win Street - Cuyahoga Palls, Ohio 44223 - Phone: 330-253-3211 - Fax: 330.253-4439 Web Site: wwmsettek.com �•�'� l�`• . �''� � � �,.�� ma`s � ' � ";;. 4 ENVIRONMENTAL TECHNOLOGIES, Analytical, ., Report Narrative Client: Synagro Southeast Order Number: 1304674 Solid sample results are reported on a wet weight basis except as noted. No problems were encountered during analysis of this order number, except as noted. Method of analysis for TCLP Volatiles is EPA 1311/8260. Method of analysis for TCLP Metals is EPA 1311/6010 and 1311/7471. Method of analysis for TCLP BNA is EPA 1311/8270. Method of analysis for TCLP Pesticides is EPA 131118081. Method of analysis for TCLP Herbicides is EPA 1311/8151. Data Qualifiers: B = Analyte found in the method blank J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ) C = Analyte has been confirmed by another instrument or method E = Analyte exceeds the upper limit of the calibration curve. D = Sample or extract was analyzed at a higher dilution X = User defined data qualifier. S = Surrogate out of control limits U = Undetected a = Not Accredited by NELAC ND = Non Detected at LOQ DF = Dilution Factor Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor) Limit Of Detection (LOD) = Method Detection Limit Practical Quantitation Limit (PQL) = (same as LOQ) Method Detection Limit (MDL) = (same as LOD) Reporting Detection Limit (RDL) = (same as LOD) Estimated uncertainty values are available upon request. Matrices: A = Air C = Cream DW = Drinking Water L = Liquid 0 = Oil SL = Sludge SO = Soil S = Solid T = Tablet TC = TCLP Extract WW = Waste Water W = Wipe The test results meet the requirements of the NELAC standard, except where noted. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. "Analytical Integrity" • EPA Certified • NELAP Certified 3310 Win Street Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211 - Matt: 330-253-4489 Web Site: www.settek.com ENVIRONMENTAL TECHNOLOGIES, INC. March 27,2013 Analytical Laboratories Client: Synagro Southeast Address: 284 Boger Rd. Mocksville, NC 27028 Received: 3/,19/2013 Project #: Delta TCLP Voletites Client ID# lab ID# Collected Anal3g Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 1304674-01 13-Mar-13 1,1-Dichloroethene 0.1 ND mg/L S 1311 1 0.7 22-Mar-13 MS Delta 130467+01 13-Mar-13 1,2-Dichloroethane 0.1 ND mg/L S 1311 1 0.5 22-Mar-13 MS Delta 130467401 13-Mar-13 2-Butanone (MEK) 2 ND mg/L S 1311 1 200 22-Mar-13 MS Delta 1304674-01 13-Mar-13 Benzene 0.1 ND mg/L S 1311 1 0.5 22-Mar-13 MS Delta 1304674-01 13-Mar-13 Carbon Tetrachloride 0.1 ND mg/L S 1311 1 0.5 22-Mar-13 MS Delta 1304674-01 13-Mar-13 Chlorobenzene 0.1 ND mg/L S 1311 1 100 22-Mar-13 MS Delta 1304674-01 13-Mar-13 Chloroform 0.1 ND mg/L S 1311 1 6 22-Mar-13 MS Delta 1304674-01 13-Mar-13 Tetrachloroethene 0.1 ND mg/L S 1311 1 0.7 22-Mar-13 MS Delta 1304674-01 13-Mar-13 Trichloroethene 0.1 ND mg/L S 1311 1 0.5 22-Mar-13 MS Delta 130467+01 13-Mar-13 Vinyl Chloride 0.2 ND mg/L S 1311 1 0.2 22-Mar-13 MS TCLP BNA Client M# Lab ID# Collected AnalAe Reo Lmt Result Units Matrix Method DF RegLyl Run Analyst Delta 130467+01 13-Mar-13 1,4-Dichlorobenzene 0.1 ND mg/L S 1311 1 7.5 22-Mar-13 AE Delta 130467+01 13-Mar-13 2,4,5-Tdchlorophenol 0.25 ND mg/L S 1311 1 400 22-Mar-13 AE Delta 1304674-01 13-Mar-13 2,4,6-Tdchlorophenol 0.25 ND mg/L S 1311 1 2 22-Mar-13 AE Delta 1304674-01 13-Mar-13 2,4-Dinitrotoluene 0.1 ND mg/L S 1311 1 0.13 22-Mar-13 AE Delta 1304674-01 13-Mar-13 Cresols 5 ND mg/L S 1311 1 200 22-Mar-13 AE Delta 1304674-01 13-Mar-13 Hexachloro-1,3-butadiene 0.1 ND mg/L S 1311 1 0.5 22-Mar-13 AE Delta 1304674-01 13-Mar-13 Hexachlorobenzene 0.1 ND mg/L S 1311 1 0.13 22-Mar-13 AE Delta 1304674-01 13-Mar-13 Hexachloroethane 0.1 ND mg/L S 1311 1 3 22-Mar-13 AE Delta 1304674-01 13-Mar-13 Nitrobenzene 0.1 ND mg/L S 1311 1 2 22-Mar-13 AE Delta 1304674-01 13-Mar-13 Pentachlorophenol 0.25 ND mg/L S 1311 1 100 22-Mar-13 AE Delta 1304674-01 13-Mar-13 Pyridine 0.25 ND mg/L S 1311 1 5 22-Mar-13 AE TCLP Pesticides Client ID# Lab ID# Collected Analvte Rep Lmt Result Units Matrix Method DF ReoLyi Run Analyst Delta 130467+01 13-Mar-13 Chlordane 0.01 ND mg/L S 1311 1 0.03 25-Mar-13 KMG Delta 1304674-01 13-Mar-13 Endrin 0.002 ND mg/L S 1311 1 0.02 25-Mar-13 KMG Delta 1304674-01 13-Mar-13 Gamma-BHC 0.002 ND mg/L S 1311 1 0.4 25-Mar-13 KMG Delta 1304674-01 13-Mar-13 Heptachlor 0.002 ND mg/L S 1311 1 0.008 25-Mar-13 KMG Delta 1304674-01 13-Mar-13 Heptachlor Epoxide 0.002 ND mg/L S 1311 1 0.008 25-Mar-13 KMG Delta 1304674-01 13-Mar-13 Methoxychlor 0.002 ND mg/L S 1311 1 10 25-Mar-13 KMG Delta 1304674-01 13-Mar-13 Toxaphene 0.1 ND mg/L S 1311 1 0.5 25-Mar-13 KMG TCLP Herbicides Client Lab ID# Collected Analyse Rep Lmt Result Units Matrix Method DF RegLyl Run Analyst Delta 1304674-01 13-Mar-13 2,4,5-TP(Silvex) 0.5 ND rtig/L S 1311 1 1 22-Mar-13 KMG Delta 1304674-01 13-Mar-13 2,4,D 5 ND mg/L S 1311 1 10 22-Mar-13 KMG TCLP Arsenic Client 1D4 Lab ID# Collected Anal% Rep Lmt Result Units Matrix Method DF RegUl Run Analyst Delta 1304674-01 13-Mar-13 TCLP Arsenic 0.5 ND mg/L S 1311 1 5 21-Mar-13 WK Page 4 "Analytical lntearity" • EPA Certified! - NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211 • Pax: 330-253-4489 Web Site: www.settek.com UMMIT ENVIRONMENTAL TECHNOLOGIES, INC. March 27 2013 Analytical Laboratories Client: Synagro Southeast Address: 284 Boger Rd. Mocksville, NC 27028 Received: V19/2013 Project#: Delta TCLP Barium Client LD# Lab ID# Collected AnaJA Rep Lmt Result Units Matrix Method DF ReaLvl Run Analyst Delta 1304674-01 13-Mar-13 TCLP Barium 5 ND mg/L S 1311 1 100 21-Mar-13 VVK TCLP Cadmium Client ID# Lab ID# Collected Analvte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 1304674-01 13-Mar-13 TCLP Cadmium 0.1 ND mg/L S 1311 1 1 21-Mar-13 WK TCLP Chromium ClientlD# Tab ID# Collected AnalAe RepLmt Result Units Matrix Method DF RggLyl Run Analyst Delta 1304674-01 13-Mar-13 TCLP Chromium 0.2 ND mg/L S 1311 1 5 21-Mar-13 VVK TCLP Lead Client IN Lab ID# Collected An Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Delta 1304674-01 13-Mar-13 TCLP Lead 0.5 ND mg/L S 1311 1 5 21-Mar-13 VVK TCLP Mercury Client ID# Lab ID# Collected AngW Rep Lmt Result Units Matrix Method DF RegLvl Rua Analyst Delta 1304674-01 13-Mar-13 Mercury 0.002 ND mg/L S 1311 1 0.2 21-Mar-13 ALI TCLP Se Client ID# Lab ID# Collected AnalA Rep Lmt Result Units Matrix Method DF ReoLyl Run Analyst Delta 1304674-01 13-Mar-13 TCLP Selenium 0.5 ND mg/L S 1311 1 1 21-Mar-13 VVK TCLP Silver Client ID# Lab ID# Collected Anal vte Rep Lmt Result Units Matrix Method DF ReaLvl Run Anal st Delta 1304674-01 13-Mar-13 TCLP Silver 0.5 ND mg/L - S 1311 1 5 21-Mar-13 VVK Client IN Lab ID# -Collected Analvte Result Units Matrix Method DF LQQ Run Analyst Delta 1304674-01 13-Mar-13 Flash Point >140F S 1010 1 20-Mar-13 TAH Client ID# Lab LD# Collected Anaiyte Result Units Matrix Method DF LONG Run Analyst Delta 130%74-01 13-Mar-13 pH 7.44 @ 18.2C s.u. S 9040 1 0.01 19-Mar-13 SML Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF LOB. Run Analyst Delta 1304674-01 13-Mar-13 Reactive Cyanide ND ppm S 7.3.3.2 1 0.5 20-Mar-13 TIP, Client ID# Lab LD# Collected Anal Lte esiilt Units Matrix Method DF LO�](. Run Analyst Delta 130467401 13-Mar-13 Reactive Sulfide 30.0ppm S 7.3.4.2 1 25 20-Mar-13 TIR i Page 5 "Analytical Integrity" • EPA Certified • NELAP Certified 3310 Jilin Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253,8211 • Fax: 330-253-4489 Web Site: www.settek.com mmit Environmental Technologies, Inc. i.,italysis Request/Chain of Custody 3310 Wm Street Cuyahoga _ __ Ohio . - . _ _ _ lei: _ _ _ _ __ _ _ _ _ _ For Summit Environmental Technologies, Inc. use only l� C:uyahoga Falls, Ohio 44L13 'lei: 330.L53.82i l Fax: 330.253.4489 Page ! of..�_. SET No. Company Na�me (Please Print) Project Name �;.:_,` ;- - � IINNIIIILIIINIIIIIIIH . - IIIp11 W���lu���I�I�U�N11 Company Address Project Address � •4~ . � -'. �; IIII11111111111111nINIIIII�IIINI�I�nIInIININIIINtIIIIIIIINI�ININNIIIINIII�IIII tvtOCKSvct.� N c 27o zg . 3 4 Order ID: 1304674 COC Client Phone No.73� _ I , �O $ Report to 77 Age r 'Client Fax No, Please -R ax es � PO# o-of SaCut Email Please Email Results ✓ Quote No. Contact one a 4�1 G t� Sam led by �, Check it Ohio YAP samples :a e+e �i� Psi �. �- Date lime # Sample Identification ` �" ' ` _ - Collected - Collected,'' C9- ,Li: W Z ����i�■iiiiiii�■iii (1MAl:RJAMMM1NRR1I Date by -lab manager ����i�■iiiiiii�■iii (1MAl:RJAMMM1NRR1I Date by -lab manager Summit Environmental Technologies Inc. I�IlII�IIIIIIII�IIIIIl1�IItI1�N+�1 IIII�UIIItl�IIEIIIuI�Ill�ll�l� Cooler Receipt Form ^ 1 UI tl Order ID: 1304674 COOLER ClientQt ro Order ID: Log In Initials: Date Received:_ °i -13 Time Received: 10M Date opened: 3- Number of Coolers o e : N/A Unpacked by: Shipper: FED UPS DHL Airborne US Postal Walk-in Pickup Other: Packaging: Peanuts ubble W Paper Foam None Other. Tape on cooler0Q� M1l N/A Custody Seals intact, N N/A C-O-C in plastic N NIA Coolant: Ice_ Blue ice_Water _Nonek C-O-C filled out properly Samples in separate bags Sample containers intact *If no, list broken sample(s): Sample Temperature Yr d °C 'n N N/A 6D N N/A L.J N NIA Sample label(s) complete (ID, date, etc.) V N NIA Label(s) agree with C-O-C Q-) N N/A Corrept containers used N N/A Sufficient sample received Q� N N/A Samples at correct pH? (list below) Y N Bubbles absent from 40'mL vials" Y N `• Samples with bubbles less than the size of a pea are acceptable. Client contact: DateMme: Comments: ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name Delta Apparel, Inc. WWTP Name Delta Apparel, Inc. WWTP Monitoring Period: From 01/01/13 Permit Number WQ0006984 NPDES # NC0006190 To 12/31/13 Pathogen Reduction (40CFR 503.32) - Please indicate level achieved and alternative performed Class A Alternative 1 Alternative 4 Class B Alternative 1 Alternative 2 Alternative 5 Alternative 2 Alternative 3 Alternative 6 Alternative 3 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"; Aerobic Dig. Air Dry Anaerobic Dig. Compost Lune Stab. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Pathogen Density No. of Freq. Of Sample Analytical Level in Exceed Analysis Type Tech. Sludge Min. Geo. Max. Units Mean Fecal 2xl 06 MPN/g Coliform MPN/g or CFU/g 2xl06 CFU/g 1000 MPN MPN/g Salmonella 3 MPN/ bacteria 4 g Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed Option 1 Option 2 Option 3 Option 4 Option 5 Option 6 Option 7 Option 8 Option 9 Option 10 No vector attraction options were performed X CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the CPR en requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 50N.33 have been met." "I certify, under penalty of law that the athogen requirements In 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33phave not been met." (Please note if you check this statement . attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather. and evaluate the information used to determine that the athogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties or false certification including fine and imprisonment." Preparer Name and Title Land Applier Name and Title (if applicable) Signature of Preparer Date Signature of Land Applier (if applicable) Date Pathogen and Vector Attraction Reduction is not required by permit, no signatures required. NCDA&CS A _ _ __Dmic Division Phone: (919) 733-2655 Website: www.n-_.__jovlagronomi/ Report No. FY1, - 11193 Client: Wally Saine Advisor: Synagro Central ry Predictive 4697 Startown Rd. Attn:Eric Thompson 707 Westside Dr. 284 Boger Rd Soil Report Mehlich-3 Extraction Newton, NC 28658 Mocksville, NC 27028 �t ;' V -ti�i.YtR4F1 Sampled County: Catawba Sampled: 10/14/2013 Received: 10/17/2013 Completed: 10/28/2013 Farm: CA-20 Links to Helpful Information Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.0 120-200 -0 0 0 0 0 0 0 0 Note: 12 2-Fescue/OGrass/Tim, 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in g/cd; CEC and Na in meq/100 cm3; NO3-N in mgldrrP]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.41 0.93 8.9 84 1.4 5 9� 72 129 53 24 38 186 129 129 252 252 182 0.2 2 North Carolina 'robncck? lrrust F'uud Conviiissloii Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS .-.y.-..omic Division Phone: (919) 733-2656 Website: www.r...q..!jov1agronornI/ Report No. FY14-sLu11193 Wally Saine Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is M mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mnn Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to gNote: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obi)art4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P205 phosphate 8-1 sulfur index Test Results SS-1 soluble salt index wtv weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.aov/aaronomi/uvrst.htm for more information. NCDA&CS Division Phone: (919) 733-2655 Predictive ,� .a Soil Report Website: www.n__,:. jov/agronomi/ Client: Tim Hefner 2942 Elbow Rd Newton, NC 28658 Mehlich-3 Extraction Sampled County: Catawba Report No. FYI,: -_ 11194 Advisor: Synagro Central Attn:Eric Thompson 284 Boger Rd Mocksville, NC 27028 Sampled: 10/14/2013 Received: 10/17/2013 Completed: 10/28/2013 Farm: CA-22 Links to Helpful Information Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.6 120-200 40 0 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, 0.0 120-200 40 0 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cnr ; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.36 0.96 9.3 84 1.5 5.6 41 104 56 22 43 451 288 288 316 316 96 0.1 1 —,-North 'Carolina TdbaccoTrusz FLutdCan miussicon Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS omic Division Phone: (919) 733-2655 Website: www.n__,..gov/agronomi/ Report No. FY1, __ 11194 Tim Hefner Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-1 copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or otherlarge areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient.levels. If $, pH$, $pH, C or Z Mn-I Mn- manganese index mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncaargov/agronomi/obpart4.htm#fs to find P-I phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index: W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.pov/aaronomi/uvrst.htm for more information. NCDA&CS Ate_ __�_mic Division Phone: (919) 733-2655 Website: www.nc_„____iv/agronomi/ Report No. FY14• -_ - _ 1195 Client: Dennis Lutz Advisor: Synagro Central Predictive 2531 Cattle Creek Farm Rd Attn: Eric Thompson 7 F o-ia� Newton, NC 28658 284 Boger Rd :i Soil Re o Mehlich-3 Extraction Mocksville, NC 27028 Repoft County : Catawba •err �ti� Sampled: 10/14/2013 Received: 10/17/2013 Completed: 10/28/2013 Farm: CA-06 Links to Helpful Information Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) I More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.9 120-200 20 0 0 0 0 0 0 0 Note: 12 2-Fescue/OGrass/Tim, 0.0 120-200 20 0 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in g/crrf; CEC and Na in meq/100 cO; NO3-N in mgldrrf]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.96 9.6 81 1.8 5 4 54 117 52 23 61 343 223 223 195 195 386 0.3 3 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 120-200 10 0 0 0 pH$ 0 0 0 Note: 12 Note: 2-Fescue/OGrass/Tim, 0.0 120-200 10 0 0 0 pH$ 0 0 0 Note: 12 Note: Test Results [units - WN in g/cd; CEC and Na in meq/100 Cm3; NO3-N in mgldnt3]: Soil Class: Mineral HM% W/V CEC BS% , Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 0.91 14.3 97 0.5 6.6 58 192 55 35 64 208 133 133 189 189 305 0.3 2 Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 100 0 0 0 0 0 0 0 Note: 12. 2- Fescue/OGrass/Tim, 0.0 120-200 100 0 0 0 0 0 0 0 Note: 12 Test Results [units - WN in 9/crrr3; CEC and Na in meq/100 cd; NO3-N in mg/dff?]: Soil Class: Mineral - HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.86 9.7 88 1.2 6.1 18 98 55 27 38 541 340 340 113 113 216 0.3 3 1`+torth Carolina. x:. J Tobacco Tnist Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture WCDA&CS j 3mic Division Phone: (919) 733-2655 Website: www.n__,,..govlagronomi/ Report No. FYI, 11195 Dennis Lutz Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K2O potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mq% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese Mn-All Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-O mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncagr..pov/agronomi/obpart4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The. first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm for more information. DELTA APPAREL, INC. - MAIDEN, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0006984 2012 ANNUAL REPORT /4 2013 Delta Apparel, Inc. o Maiden, NC Residuals Land Application Program 2012 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, & Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Pages 3. Field Summary Forms 4. TCLP Analysis 6. Pathogen Reduction/ Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00006984 County Catawba Year 2012 Facility Name (as shown on permit) Delta Apparel, Inc./Maiden Plant NPDES No. NC0006190 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 16 Total number of fields utilized for land application during the year: 7 Total amount of dry tons applied during the year for all application sites: 299.93 Total number of acres utilized for land application during the year: 141.5 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2012 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the. possibility of fines and imprisonment for knowing violations." Steve Slaujzhter, Plant Manager Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) 13 a e i Dat Signature of Land Applier Date (if different from Permittee and`Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) IDENR FORM ACF (12/2006) 2012 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION DELTA APPAREL, INC., NC JELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS May 2012 1,853,800.00 G 299.93 D 272.08 YEARLY TOTAL 1,853,800.00 G 299.93 D 272.08 2/19/2013 2012 ANNUAL REPORT PROJECT: FACILITY: NPDES PERMIT NUMBER: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: Delta Apparel, Inc. Delta Apparel, Inc., WWTP P.O. Box 37 (100 West Pine Street Maiden, NC 28650 NC0006190 Steve Slaughter, Plant Manager Delta Apparel, Inc., WWTP P.O. Box 37 (100 West Pine Street) Maiden, NC 28650 828-428-9921 Wayne Kelly, ORC Delta Apparel, Inc., WWTP P.O. Box 37 Maiden, NC 28650 828-428-9921, ext. 290 Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: W00006984 Facility Name: DELTA APPAREL, INC., NC NPDES# : NC0006190 or WQ# (residual only). WWTP Name: DELTA APPAREL = MAIDEN PLANT Residuals Analysis Data Product Type TXL10 TXLIQ Date Sampled (grab) or 04/23/12 10/16/12 Date Composited Percent Solids 3 c 88 3.24 PARAMETERS (mg/kg dry weight) Arsenic 2 <3 Cadmium 1 <2 Mercury 0.8 <0.4 Chromium 16 14 Copper 1230 1000 Lead 7 6 Molybdenum <5 <5 Nickel 29 22 Selenium 5 <5 Zinc 272 117 Total Phosphorus 4940 5570 TKN 66000 65700 Ammonia -Nitrogen 5930 3090 Nitrate and Nitrite <2 225 Laboratory A&L EASTERN LABORATORIES, INC. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X - Date r-,-;? ( NATURE OF PRE ER) DENR FORM RSSF (5/2003) Printed: Tuesday - February 19, 2013 at 08:43:41 for: 2105 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006984 Facility Name: DELTA APPAREL, INC., NC NPDES# : NC0006190 or WQ# (residual only) !!VWTP Name: DELTA APPAREL - MAIDEN PLANT Residuals Analysis Data Product Type TXLIQ TXLIQ Date Sampled (grab) or 04/23/12 10/16/12 Date Composited Percent Solids 3.88 3.24 PARAMETERS (mg/kg dry weight) Aluminum 2600 2700 Calcium 2870 3790 Magnesium 1280 1180 pH 7.82 7.70 Potassium 4650 4390 Sodium 72100 63600 Laboratory A&L EASTERN LABORATORIES, INC. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that gdalified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X NR - Data Not Reported or Data Not Required Date��r�3 DENR FORM RSSF-B (7/2002) Printed: Tuesday - February 19, 2013 at 08:44:08 for: 2105 01 Page: 1 of 2 Report Number: 12-115-0206 Account Number: 46718 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL/DELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 87555 Sample Id: DELTA A&L Eastern Laboratories ` 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 The One Source. Project: DELTA NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/23/2012 09:30:00 Date Received: 04/24/2012 00:00 Date Reported: 04/30/2012 Total Solids ' 3.88 38800 100.0 JM 04/24/2012 15:29 SM-2540G Moisture' 96.12 100.0 JM 04/24/201215:29 SM-2540G Total Kjeldahl Nitrogen 6.60 66000 .10.0 JM 04/25/2012 08:44 SM-4500-NH3C-TKN Total Phosphorus 0.49 4940 100 KM 04/25/2012 12:26 SW 6010C Total Potassium 0.46 4640 100 KM 04/25/2012 12:26 SW 6010C Total Sulfur 3.31 33100 100 KM 04/25/2012 12:26 SW 6010C Total Calcium 0.29 2870 100 KM 04/25/2012 12:26 SW 6010C Total Magnesium 0.13 1280 100 KM 04/25/2012 12:26 SW 6010C Total Sodium 7.21 72100 100 KM 04/25/2012 12:26 SW 6010C Total Iron 3780 1 KM 04/25/2012 12:26 SW 6010C Total Aluminum 2600 10 KM 04/25/2012 12:26 SW 6010C Total Manganese 206 1 KM 04/25/2012 12:26 SW 6010C Total Copper 1230 1 KM 04/25/2012 12:26 SW 6010C Total Zinc 272 1 KM 04/25/2012 12:26 SW 6010C Ammonia Nitrogen 0.59 5930 10.0 JM 04/25/2012 08:44 SM-4500-NH3C Organic N 6.01 60070 10.0 04/25/2012 08:44 CALCULATION Nitrate+Nitrite-N <2.00 1.00 JM 04/25/2012 08:45 SM-450ONO3F Total Cadmium 1.0 1.0 KM 04/25/2012 12:26 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 12-115-0206 Account Number: 46718 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAUDELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 87555 Sample Id : DELTA Lt�j A&L EasternLaboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 The One Source. Project: DELTA NC CERT#257 REPORT OFANALYSIS Date Sampled: 4/23/2012 09:30:00 Date Received: 04/24/2012 00:00 Date Reported: 04/30/2012 Total Chromium 16 5 KM 04/25/2012 12:26 SW 6010C Total Nickel 29 5 KM 04/25/2012 12:26 SW 6010C Total Lead 7 5 KM 04/25/2012 12:26 SW 6010C Total Arsenic 2.0 1.0 KM 04/25/2012 12:26 SW 6010C Total Mercury 0.8 0.4 KM 04/25/2012 09:00 SW-7471 B Total Selenium 5.0 1.0 KM 04/25/2012 12:26 SW 6010C pH (Standard Units) * 7.82 0.01 JM 04/25/2012 08:44 SW-9045D Total Volatile Solids 74.20 742000 100.0 JM 04/24/2012 15:29 SM-2540G Total Molybdenum <5 5 KM 04/25/2012 12:26 SW 6010C Comments: QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Fe", "P", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Rate® Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2105-01-TXLIQ-NC DELTA APPAREL, INC., NC MAIDEN 4/23/2012 4130/2012-5/3112012 55.2107 PLANT TEXTILE RESID. LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (72100 x 3.8800) = 100 = 2797.48 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (2870 x 3.8800) _ 100 = 111.356 Mg mg/I = (mg mg/kg x % Solids) - 100 = (1280 x 3.8800) + 100 = 49.664 Na meq = Na mg/I + Molec.Wgt.Na = 2797.48 _ 23 = 121.63 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 111.356 + 20 = 5.5678 Mg meq = Mg mg/I = Molec.Wgt.Mg = 49.664 + 12 = 4.13867 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 121.63 + SgrRoot[0.5(5.5678+4.13867)] = 55.2107 Printed: 2/19/2013 Page 1 08:44 Page: 1 of 2 - -- Report Number: 12-291-0205 A&L Eastern Laboratories, Inc. Account Number: 46718 7621 White ineRoad Richmond Virginia 23237 804 743-9401 Fax 804 271-6446 Submitted By: ERIC THOMPSON www.aleastem.com Send To: SYNAGRO CENTRAL/DELTA APPAREL Project: DELTA Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 10/16/2012 10:30:00 Lab Number: 89911 Date Received: 10/17/2012 00:00 Sample Id : DELTA Date Reported: 10/23/2012 Total Solids ' 3.24 32400 100.0 JM 10/17/2012 15:15 SM-2540G Moisture' 96.76 100.0 JM 10/17/201215:15 SM-2540G Total Kjeldahl Nitrogen 6.57 65700 10.0 JM 10/18/2012 08:44 SM-4500-NH3C-TKN Total Phosphorus 0.56 5570 100 BW 10/18/2012 08:30 SW 6010C Total Potassium 0.44 4390 100 BW 10/18/2012 08:30 SW 6010C Total Sulfur 3.19 31900 100 BW 10/18/2012 08:30 SW 6010C Total Calcium 0.38 3790 100 BW 10/18/2012 08:30 SW 6010C Total Magnesium 0.12 1180 100 BW 10/18/2012 08:30 SW 6010C Total Sodium 6.36 63600 100 BW 10/18/2012 08:30 SW 6010C Total Iron 3740 100 BW 10/18/2012 08:30 SW 6010C Total Aluminum 2700 100 BW 10/18/2012 08:30 SW 6010C Total Manganese 111 5 BW 10/18/2012 08:30 SW 6010C Total Copper 1000 5 BW 10/18/2012 08:30 SW 6010C Total Zinc 117 5 BW 10/18/2012 08:30 SW 6010C Ammonia Nitrogen 0.31 3090 10.0 JM 10/18/2012 08:44 SM-4500-NH3C Organic N 6.26 62610 10.0 10/18/2012 08:44 CALCULATION Nitrate+Nitrite-N 225 2.00 JM 10/18/2012 08:45 SM-450ONO3F Total Cadmium <2.0 2.0 BW 10/18/2012 08:30 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ((�� to the won(, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior. written authorization. Debbie Holt Page: 2 of 2 Report Number: 12-291-0205 Account Number: 46718 Submitted By: ERIC THOMPSON Send To: SYNAGRO CENTRAL/DELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 89911 Sample Id: DELTA 0A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.W6 wwwaleastern.com Project: DELTA NC CERT#257 REPORT OF ANALYSIS Date Sampled: 10/16/2012 10:30:00 Date Received: 10/17/2012 00:00 Date Reported: 10/23/2012 Total Chromium 14 5 BW 10/18/2012 08:30 SW 6010C Total Nickel 22 5 BW 10/18/2012 08:30 SW 6010C Total Lead 6 5 BW 10/18/2012 08:30 SW 6010C Total Arsenic <3.0 3.0 BW 10/18/2012 08:30 SW 6010C Total Mercury <0.4 0.4 JM 10/18/2012 13:15 SW-7471 B Total Selenium <5.0 5.0 BW 10/18/2012 08:30 SW 6010C pH (Standard Units) * 7.70 2.00 JM 10/18/2012 08:50 SW-9045D Total Molybdenum <5 5 BW 10/18/2012 08:30 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "TKN". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive; and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company In any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt � s � t v f f e -v 1� �-i � � • : ^. � pp ice` � i!� a � 8� ^si r +.. �1° Ma's e •.�F r,r � t i r 1� � �,) � t�a f �/ ( F.� I � � t �: i, S.. 0 i/� � t F ia�5 �. f �.Ff � l .._i d Product Code Product Name Sample Date Report Range Ratio 2105-01-TXLIQ-NC DELTA APPAREL, INC., NC MAIDEN 10/16/2012 / / - / / 41.4903 PLANT TEXTILE RESID. LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (63600 x 3.2400) _ 100 = 2060.64 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (3790 x 3.2400) _ 100 = 122.796 Mg mg/I = (mg mg/kg x % Solids) = 100 = (1180 x 3.2400) _ 100 = 38.232 Na meq = Na mg/I = Molec.Wgt.Na = 2060.64 = 23 = 89.593 Ca meq = Ca mg/I - Molec.Wgt.Ca = 122.796 _ 20 = 6.1398 Mg meq = Mg mg/I = Molec.Wgt.Mg = 38.232 = 12 = 3.186 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 89.593 = SgrRoot[0.5(6.1398+3.186)] = 41.4903 Printed: 2/19/2013 Page 1 08:45 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: WILLIAM SAINE SITE #: NC CA 00005 FIELD# : CA 00005 0001 A RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 53.17 OPERATOR: TODD EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 26.70 ACRES PERMITTED: 26.70 Page: 1 Lime Applied k** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip, Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppnm) Crop MONTH Total Per Acre Solids 5/8/12 124,000.00 (G) 4644.195 3.88 0.751 DAMPTXL DRY 0-<I/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 I FESCUE 5/9/12 86,800.00 (G) 3250.936 3.88 0.526 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 I FESCUE 5/10/12 117,800.00 (G) 4411.985 3.88 0.714 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 21911 FESCUE May-12 328,600.00 (G) 12,307.116 Total Gallons/Ac: 12,307.12 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 84 Annuallbs/acre 0.008 0.004 0.064 4.898 0.028 0.003 0.020 0.115 0.020 1.083 19.67 Cumulative lbs/acre 0.040 0.025 0.312 22.686 0.114 0.009 0.087 0.613 0.039 4.738 { } 216 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 f 1339.0 267.9 15.0 , i- 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID r x (SIGNATU - OF LAND PLIER) DATE "I certify, nder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hmcorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2013 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: DENNIS LUTZ SITE #: NC CA 00006 FIELD# : CA 00006 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 16.05 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 10.00 ACRES PERMITTED: 20.40 Page: 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- all- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/1/12 99,200.00 (G) 9920.000 1 3.88 1.605 DAMPTXL DRY 0-<I/2" SUR 0.5 0.30 66,000. p 5,930.00 T 2.00 p 20988 FESCUE May-12 1 99,200.00 (G) 9,920.000 Total Gallons/Ac: 9,920.00 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 67 Annuallbs/acre 0.006 0.003 0.051 3.948 0.022 0.003 0.016 0.093 0.016 0.873 15.86 Cumulative lbs/acre 0.033 0.020 0.227 17.682 0.089 0.007 0.068 0.467 0.030 3.822 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop a a FD Cumulative Pollutant Rate Limit (lbs/acre) 36.6 34 8 = .; 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X I _� Gd� 4 o S, (SIGNA RE OF AND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2013 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: DENNIS LUTZ SITE #: NC CA 00006 FIELD# : CA 00006 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: HIWASSEE PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 41.13 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 19.30 ACRES PERMITTED: 19.30 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/1/12 74,400.00 (G) 3854.922 3.88 0.624 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 FESCUE 5/2/12 179,800.00 (G) 9316.062 3.88 1.507 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 21988 1 FESCUE May-12 254,200.00 (G) 13,170.984 Total Gallons/Ac: 13,170.98 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 89 Annuallbs/acre 0.009 0.004 0.068 5.242 0.030 0.003 0.021 0.124 0.021 1.159 21.05 Cumulative Ibs/acre 0.012 0.008 0.132 9.122 0.053 0.005 0.038 0.225 0.028 1.753 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop x 216 ' Y FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 si DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID ;9 X _11, �"` s e , i 9 (SIGNAT OF APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0 k Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2013 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: HAROLD SHERRILL SITE #: NC CA 00020 FIELD# : CA 00020 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICA'>TION FIELD SUMMARY FORM PREDOMINANT SOUL SERIES: LLOYD PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 39.12 OPERATOR: WALLY SAINE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 16.80 ACRES PERMITTED: 16.80 Page: I Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/3/12 217,000.00 (G) 12916.667 3.88 2.090 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 I FESCUE 5/8/12 24,800.00 (G) 1476.190 3.88 0.239 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 1 FESCUE May-12 241,800.00 (G) 14,392.857 Total Gallons/Ac: 14,392.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 98 Annuallbs/acre 0.009 0.005 0.075 5.729 0.033 0.004 0.023 0.135 0.023 1.267 23.01 Cumulative lbs/acre 0.013 0.008 0.136 9.458 0.055 0.005 0.040 0.232 0.030 1.838 t s ' s 216 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop > ;_ FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 4 = 1339.0 267.9 15.0 375.0 89.0 2500.0 , DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X (SIGN URE O AND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 k Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2013 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: HAROLD SHERRILL SITE #: NC CA 00020 FIELD# : CA 00020 0002 RESIDUAL SOURCE(S): * See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LLOYD PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 49.15 OPERATOR: WALLY SAINE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 20.70 ACRES PERMITTED: 20.70 Page: 1 Lime Applied *** Date Lbs/Ac ±7 allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) U �� Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/4/12 117,800.00 (G) 5690.821 3.88 0.921 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 I FESCUE 5/7/12 186,000.00 (G) 8985.507 1 3.88 1.454 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 21188 1 FESCUE May-12 1 303,800.00 (G) 14,676.328 Total Gallons/Ac: 14,676.33 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 100 Annual lbs/acre 0.010 0.005 0.076 5.841 0.033 0.004 0.024 0.138 0.024 1.292 23.46 Cumulative lbs/acre 0.013 0.008, 1 0.135 9.385 1 0.055 0.005 0.039 0.230 0.030 1.834 ` 202 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop x F G > €4 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 * 375.0 89.0 2500.0 t.. DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X �e-01 13/-1-1SZ>� (SIGN RE OF• AND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2013 FACILITY NAME: DELTA APPAREL, INC., NC OWNER: JAMES JARRETT SITE #: NC LT 00035 FIELD# : LT 00035 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 43.14 OPERATOR: JAMES JARRETT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 30.00 ACRES PERMITTED: 39.30 Page: 1 Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/10/12 37,200.00 (G) 1240.000 3.88 0.201 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 I FESCUE 5/11/12 130,200.00 (G) 4340.000 3.88 0.702 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 FESCUE 5/18/12 99,200.00 (G) 3306.667 3.88 0.535 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 FESCUE May-12 266,600.00 (G) 8,886.667 Total Gallons/Ac: 8,886.67 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 60 Annuallbs/acre 0.006 0.003 0.046 3.537 0.020 0.002 0.014 0.083 0.014 0.782 14.21 Cumulative lbs/acre 0.026 0.018 0.180 13.708 0.073 0.005 0.050 0.368 0.025 3.058 3 # 216 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X bzzzl/lp (SIGNATI OFAD D APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 k Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2013 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: DELTA APPAREL, INC., NC PREDOMINANT SOIL SERIES: GASTON OWNER: WAYNE GILBERT PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 58.18 SITE #: NC LT 00120 FIELD# : LT 00120 0001 OPERATOR: WAYNE GILBERT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): * See list at bottom of report ACRES UTILIZED: 18.00 ACRES PERMITTED: 18.00 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 5/18/12 18,600.00 (G) 1033.333 3.88 0.167 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 I FESCUE 5/19/12 99,200.00 (G) 5511.111 3.88 0.892 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20911 I FESCUE 5/21/12 142,600.00 (G) 7922.222 3.88 1.282 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 20988 Ij FESCUE 5/22/12 99,200.00 (G) 5511.111 3.88 0.892 DAMPTXL DRY 0-<1/2" SUR 0.5 0.30 66,000. p 5,930.00 p 2.00 p 21988 FESCUE May-12 359,600.00 (G) 19,977.777 Total Gallons/Ac: 19,977.78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 136 Annual lbs/acre 0.013 0.006 0.103 7.952 0.045 0.005 0.032 0.187 0.032 1.758 31.94 Cumulative lbs/acre 0.045 0.045 0.357 26.311 0.222 0.012 0.123 0.793 0.051 7.126 ' 209 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop t 8' s FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 r DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID X 0d (S1GNA O AND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2013 S UMMUT ENVIRONMENTAL TECHNOLOGIES, INC. Analytical L.abora ogles Client Synagro Southeast 284 Boger Rd. Mocksville, NC 27028 Order Number 1209169 Project Number Delta Apparel Issued Thursday, April 26, 2012 Total Number of Pages 5 (excluding C.O.C. and cooler receipt form) Approved By: QA Manager NELAC Accreditation #E87688 ";analytical Integrity" - EPA Certified • iVELAP Certified 33,10 Win street • CGAyni ofp Falh-3, Ohio 44223 o Phon(--: 330-263-8211 , Rix: 330••153-4489 Web ito: www.S'L-'t1Y:kxom ENVIRONMENTAL TECHNOLOGIES, INC. A n�lytirall.:,ei�Qi'��t��rins Client: Synagro Southeast Order Number: 1209169 Laboratory ID Client ID 1209169-01 DELTA Sample Summary Matrix 2 Sampling Date Sludge 4/23/2012 "Analytical Integrity" • EPA Certified • NE"LAn Certified 3310 Win Street - Cuyahoga oga Falls, Ohio 44223 o F'itow-,: 3,90-2 i3.82'11 •Fax: 330-253-413139 Web ;pile: www. sellokxom EU, I S MMIT ENVIRONMENTAL TECHNOLOGIES, INC. Report Narrative Client: Synagro Southeast Order Number: 1209169 3 No problems were encountered during analysis of this order number, except as noted. Data Qualifiers: B = Analyte found in the method blank J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ) C = Analyte has been confirmed by another instrument or method E = Analyte exceeds the upper limit of the calibration curve. D = Sample or extract was analyzed at a higher dilution X = User defined data qualifier. S = Surrogate out of control limits U = Undetected a = Not Accredited by NELAC ND = Non Detected at LOQ DF = Dilution Factor Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor) Limit Of Detection (LOD) = Laboratory Detection Limit Estimated uncertainty values are available upon request. Matrices: A = Air C = Cream DW = Drinking Water L = Liquid O = Oil SL = Sludge SO = Soil S = Solid T = Tablet TC = TCLP Extract WW = Waste Water W = Wipe The test results meet the requirements of the NELAC standard, except where noted. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. "Analytical Integrity" • EPA Certified • NELAP Certified 33,10 Win Street • i uy:allag a {gall:,, Ohlo 114223 a Phianc,,: 330-253-8211 - Fax: 330-263.4489 Web Site): www. eftelccorn ENVIRONMENTAL TECHNOLOGIES, INC. April 26, 2012 �,,; Analytical If-c311E)ri'dorh -9 Client: Synagro Southeast Address: 284 Boger Rd. Mocksville, NC 27028 Received: 4/24/2012 Project t!: Delta Apparel TCLP Volatiles Client IDN Lab IDN Collected Anahne Rep Lmt Result Units Matrix Method DF RegLvi Run Analyst DELTA 1209169-01 23-Apr-12 Chloroform 0A ND mg/L SL 1311 1 6 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 1,2-Dichloroethane 0.1 ND mg/L SL 1311 1 0.5 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 Benzene 0.1 ND mg/L SL 1311 1 0.5 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 Carbon tetrachloride 0.1 ND mg/L SL 1311 1 0.5 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 Trichloroethene 0.1 ND mg/L SL 1311 1 0.5 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 1,10chloroethene 0.1 ND mg/L SL 1311 1 0.7 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 Tetrachloroethene 0.1 ND mg/L SL 1311 1 0.7 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 Chlorobenzene 0.1 ND mg/L SL 1311 1 100 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 2-Butanone (MEK) 2 ND m9/L SL 1311 1 200 25-Apr-12 MS DELTA 1209169-01 23-Apr-12 Vinyl Chloride 0.2 ND mg/L SL 1311 1 0.2 25-Apr-12 MS -_.-,.__......_......_._.. TCLP BNA Client IN Lab IN Collected Analyle Rea Lmt Result Units N-litrix Method DF RegLvl Rim Analyst DELTA 1209169-01 23-Apr-12 2,4,5-Trichlorophenol 0.25 ND mg/L SL 1311 1 400 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 Hexachloroethane 0.1 ND mg/L SL 1311 1 3 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 Cresols 5 ND mg/L SL 1311 1 200 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 Nitrobenzene 0.1 ND mg/L SL 1311 1 2 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 2,4,6--Trichlorophenol 0.25 ND mg/L SL 1311 1 2 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 Pentachlorophenol 0.25 ND mg/L SL 1311 1 100 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 Hexachloro-1,3-butadiene 0.1 ND mg/L SL 1311 1 0.5 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 Pyridine 0.25 ND mg/L SL 1311 1 5 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 2,4-Dinitrotoluene 0.1 ND mg/L SL 1311 1 0.13 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 1,4-Dichlorobenzene 0.1 ND mg/L SL 1311 1 7.5 26-Apr-12 AE DELTA 1209169-01 23-Apr-12 Hexachlorobenzene 0.1 ND mg/L SL 1311 1 0.13 26-Apr-12 AE TCLP Pesticides Client IDN Lib IDN Collected Anahhe Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst DELTA 1209169-01 23-Apr-12 Heptachlor Epoxide 0.002 ND mg/L SL 1311 1 0.008 25-Apr-12 KMG DELTA 1209169-01 23-Apr-12 Endrin 0,002 ND mg/L SL 1311 1 0.02 25-Apr-12 KMG DELTA 1209169-01 23-Apr-12 Chlordane 0.01 ND mg/L SL 1311 1 0.03 25-Apr-12 KMG DELTA 1209169-01 23-Apr-12 Gamma-BHC 0.002 ND mg/L SL 1311 1 0.4 25-Apr-12 KMG DELTA 1209169-01 23-Apr-12 Toxaphene 0.1 ND mg/L SL 1311 1 0.5 25-Apr-12 KMG DELTA 1209169-01 23-Apr-12 Methoxychlor 0.002 ND mg/L SL 1311 1 10 25-Apr-12 KMG DELTA 1209169-01 23-Apr-12 Heptachlor 0.002 ND mg/L SL 1311 1 0,008 25-Apr-12 KMG TCLP Herbicides Client IDN Lab ID# Collected Anal le Rep Lmt Result Units N-latrix Method DF RegLvl Rim Analyst DELTA 1209169-01 23-Apr-12 2,4,S-TP(Silvex) 0.5 ND mg/L SL 1311 1 1 25-Apr-12 KMG DELTA 1209169-01 23-Apr-12 2,4,D 5 ND mg/L SL 1311 1 10 25-Apr-12 KMG TCLP Arsenic Client iDN Lab IDN Collected Anahl Reo Lmt Result Units Matrix Method DF RegLvl Run Analyst DELTA 1209169-01 23-Apr-12 TCLP Arsenic 0.5 ND nag/L SL 1311 1 5 25-Apr-12 VVK Page 4 "Analytical Integrity" • EPA Certified • NELAP Certified 3310 Win htr 3% - Cuy�flfloclta 1= all:s, Ohio 44223 0 :'hone;: 330-263-8?'I'i • Fax: 330-253-11,189 We/) Site; wwws 'ttekxom Client ID DELTA Clicnt ID# DELTA Clicnt ID# DELTA 3� y� M IT U005 _ ENVIRONMENTAL TECHNOLOGIES, INC. A 1�[ Iyl�wi/ L aboratoiie y Lab In# Collected AnalLqe 1209169-01 23-Apr-12TCLP Barium Lab ID# Collected Analtle 1209169-01 23-Apr-12 TCLP Cadmium Lab IN Collected Anah-te 1209169-01 23-Apr-12 TCLP Chromium TCLP Barium Rep Lmt Result 5 ND TCLPCadmium Rep Lml Result 0.1 ND April 26, 2012 Client: Synagro Southeast Address: 28413oger Rd. Mocksville, NC 27028 Received: 4/24/2012 Project #: Delta Apparel Units Matrix Method DF RegLvi Run Analyst mg/L SL 1311 1 100 25-Apr-12 WK ( n' s Matrix Method DF RegLvl JLtm Aiialyst mg/L SL 1311 1 1 25-Apr-12 WK TCLP Chromium Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 0.2 ND mg/L SL 1311 1 5 25-Apr-12 WK TCLP Lead Client ID# Lab IN Colt Attal)le Rep Lmt Result Units Matrix Method DF RegLvi Run Analyst DELTA 1209169-01 23-Apr-12 TCLP Lead 0.5 ND mg/L SL 1311 — .._.... 1 5 25-Apr-12 VI/K —..... -................--•---- ._....- — - TCLP Mercury Client ID# Lab ID# Collected Au__. ?I}Ke Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst DELTA 1209169-01 23-Apr-12 Mercury 0.002 ND mg/L SL 1311 1 0.2 25-Apr-12 AU TCLP Selenium Client ID# Lab Ill# Collected Ana134c Rep Lmt Result Units Matrix Method DF RegLvi Run Aualvst DELTA 1209169-01 23-Apr-12 TCLP Selenium 0.5 ND mg/L SL 1311 1 1 25-Apr-12 WK TCLP Silver Client ID# Lab ID# Collected Attalyle Re Lm Resul Units Matrix Method DF RegLvl Run Anafs-st DELTA 1209169-01 23-Apr-12 TCLP Silver 0.5 ND mg/L SL 1311 1 5 25-Apr-12 WK Client ID# Lab ID# Collected Aualytc Result Units Matrix Method DF LOQ Run Analyst DELTA 1209169-01 23-Apr-12 Flash Point > 140 OF SL 1010 1 25-Apr-12 TAH Client ID# Lab 1D9 Collected Analyie Result Utiits Matrix Method DF LOLL Run Analyst DELTA 1209169-01 23-Apr-12 pH 7.94@19.7 C S.U. SL 9040 1 0.01 24-Apr-12 JRK Client ID# Lab 1D9 Collected Anal 1e Result Units Matrix Method DF LOQ Rijil Aiialyst DELTA 1209169-01 23-Apr-12 Reactive Cyanide ND mg/kg SL 7.3.3.2 1 0.5 25-Apr-12 TIR Client 1D# Lab 1D# Collected Anal�Ke Result Urtiis Matrix Method DF LOQ Run Aualvst DELTA 1209169-01 23-Apr-12 Reactive Sulfide ND mg/kg SL 7.3.4.2 1 25 25-Apr-12 TIR Page 5 "Analytical Integrity" • EPA Certified • NELAP Certified 3310 Will Str(?Ot • CLIY,;1110fj'R F',111.3, 01110 44223 o roh(. ne: 330-263-82,11 , Fax: 330,.2 ;3-n43J Web Site: www.s„ tlek.coni „ummit Environmental Technologies, Inc. lna�ys s Req,uest/Chain of Custody Win Street �-- For Summit EnvironmentalCuy II�[�IIIIIIIII��II���II�� 11![1[IIUI[Illlllllllillillillllill[IIIIIIII Cuyahoga Falls, Ohio 44223 Tel: 330 253.8211 Fax: 330 ZS3.4489 Company Name (Please Print) Company Address o Zg � � �' ni1V(Z AIL,-(—C Client Phone No. 3 O z q3 q . O Boa Client Fax No. Please Fax Results ✓El Client Email Please F,mai! Results ✓ C ntact erson Sampled by �� E,Qc i r Psi # Sample Identification Project Name W4aL, Project Address J � � Report P0# Quote No. Check if Ohio VAP samples ✓ Date Collected L q c [] P: Cn me I Tune c . a Collected ;. U U.. 4 Q0 II{!I!{I11111i[I[llll{I1111111[{I[llll�lllll�li[Il�il�lll[lllllllllllllll4 Order V e c � a z lase 1D: 1209169 COC Chccl: Awivtiml Box IF Olt The Notes/Comments: cwVot &C client -mine the. pink nape. - C n 7 A •t Rehm :wished :1i ::., ... Date . ' . Tune .: ' Received: b - Date ... '. ,Time ': . RececyCd:XA Date' . ;lime' , Z, Must be approved hush Requested By: ate by lab mana;er 1 _..... U t.,ti,,,..,t.,... Wnite and yellow pages snouts-uvn7wa.ry am..y,...� ... ..... ........ _....,. ...- - ------------ --- f O ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name Delta Apparel, Inc. ' • � • .iL�Z1II17S�Y! WWTP Name Delta Apparel, Inc. WWTP Monitoring Period: From 01/01/12 NPDES # NC0006190 To 12/31/12 Pathogen Reduction (40CFR 503.32) - Please indicate level achieved and alternative performed Class A Alternative 1 Alternative 4 Class B Alternative 1 Alternative 2 Alternative 5 Alternative 2 Alternative 3 Alternative 6 Alternative 3 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"; Aerobic Dig. Air Dry Anaerobic Dig. Compost Lime Stab. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Pathogen Densi No. of Freq. Of Sample Analytical Level in Exceed Analysis Type Tech. Sludge Min. Geo. Max. Units Mean Fecal 2x 10 MPN/g Coliform MPN/g or 2x106 CFU/g CFU/g 1000 MPN MPN/g Salmonella 3 MPN/ bacteria 4 g Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed Option 1 Option 2 Option 3 Option 4 Option 5 Option 6 Option 7 Option 8 Option 9 Option 10 rr� � ;�- a , t No vector attraction options were performed X n ®3'1 J r Q -% ti .t;� YGS�G .lit-r Y c, CERTIFICATION STATEMENT (please check the appropriate statement) �F "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attracti n reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law that the pathogen requirements In 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties For false certification including fine and imprisonment." Preparer Name and Title Land Applier Name and Title (if applicable) Signature of Preparer Date Signature of Land Applier (if applicable) Date Pathogen and Vector Attraction Reduction is not required by permit, no signatures required. Agricultural Lime Application Log Year: 2012 Project: Delta Apparel, Inc. Field Soil pH Lime Requirement Tons/Acre Date Applied (state-county-site-field code) 1 1, (from soil analysis) Applied il NC-CA-5-1A 6.7 0.0 - N/A NC-CA-6-1 6.4 0.0 NC-CA-6-3 6.4 0.0 NC-CA-20-1 6.0 0.0 WA, NC-CA-20-2 6.0 0.0 M' NC-LT-35-1 6.0 0.0 NC-LT-1 20-1 6.9 0.0 A V -, -, I Page 1 of 1 yy _ - ,-_- _ _. Report Number: 12-289-0677 V Y Account Number: 46718 '�'�( Waleastern.com Send To: SYNAGRO CENTRALlDELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 10/15/2012 Date Of Analvsis: 10/16/2012 A&L Casters Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: WM R SAINE DELTA ANNUAL SOIL ANALYSIS REPORT Date Of Report: 10/17/2012 Submitted By: ERIC THOMPSON Farm ID: CA-5 Analytical Method(s): Mehlich 3 Organic Matter. Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number o /o Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100g meq/100g 1A 54 H 281 VH 530 H 1329 M 77 L 10174 6.7 H 150 6.7 6.87 0.6 12.7 NC = 45 NC = 144 1 B 54 H 367 VH H 980 M 22 VL 10175 5.5 H 146 [357 1 6.5 6.86 0.7 9.6 NC = 45 NC = 188 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca a H NO3N S Zn Mn Fe Cu B SS CI Al Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1A 19 M 10.5 VH 29 H 114 VH 9.1 VH 1.1 M 0.34 VL 5.7 34.8 52.3 2.6 4.5 NC = 48 NC = 262.5 NC = 181 I NC = 455.0 1 B L 9.8 VH 20 M VH 2.8 H 0.8 M 0.29 VL 9.8 31.0 51.0 1.0 7.4 112 199 NC=30 NC=245.0 NC=125 NC=140.0 Values on this report represent the plant available nutrients in t e soil. Rating after each value: VL (Very Low), L (Low), M (Mediu ), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: % (percent), ppm (parts per million), Ibs/A (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Salts ms/cm x 640 = ppm. 0 This report applies to sample(s) tested. Samples are retained a maximum of thirty days after testing. t� by: p�ylca m G Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary NCDA&CS Ag 1c Division Phone: (919)733-2655 Web site: www.neagr.gov/agronoi . Report No: 42709 ,:cru, Grower: Lutz, Dennis Copies To: Synagro Central r.— 2531 Cattle Creek Farm Rd .a x 170 k-p�� So Newton, NC 28658 r ��� dJ ort '`�'•tirno}"�' Fann: CA-6 SERVING N.C. RESIDENTS FOR OVER 60 YEARS Received: 0510212012 Completed: 05/09/2012 Links to Helpful Information Catawba County Agronomist Comments 12 Field Information Applied Lime Recommendations Sample No. Last Crop Mo Yr T/A Crop or Year Lime N P205 K20 Mg S Cu Zn B Mn See Note 1 1st Crop: Fes/OG/Pim,M 0 120-200 0 0 0 0 0 0 .0 0 12 2nd Crop: Fes/OG/Pim,M 0 120-200 0 0 0 0 0 0 .0 0 12 Test Results °� P d Soil Class HM% W/V CEC BS% Ac p H P-I K-1 Ca% Mglo Mn-1 Mn-AI(1) Mn-AI(2) Zn-I Zn-AI Cu-1 S-1 SS-1 NO3-N NH4-N Na MIN 0.81 0.86 14.9 93.0 1.1 6.4 74 101 59.0 30.0 206 135 135 241 241 265 58 0.1 Field Information - Applied Lime Recommendations Sample No. Last Crop Mo Yr TIA Crop or Year Linte N P205 K20 Mg S Cu & B Mn See Note 3 1st Crop: Fes/OG/fim,M 0 120-200 50-70 0 0 0 0 0 .0 0 12 2nd Crop: Fes/OG/fim,M 0 120-200 50-70 0 0 0 0 0 .0 0 12 Test Results : - 2 , $ C/," Soil Class HM% W/V CEC BS% Ac pH P-I K-1 Ca% Mg% Mn-1 Mn-AI(1) Mn-AI(2) Zn-I Zn-AI Cu-I S-I SS-1 NO3-N NH4-N Na MIN 0.41 0.91 11.8 91.0 1.1 6.4 34 114 56.0 30.0 1286 783 783 190 190 172 41 0.3 Aorth Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. -1 Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tobacco Trust Fund Conlmisston NCDA&CS ) _ )mic Division Phone: (919) 733-2655 Website: www.i _ govlagronomi/ Report No. FY )00811 �_. Predictive Client: Wally Saine 4697 Startown Rd. Advisor: Synagro Central Attn:Wayne 707 Westside Dr. 284 Boger Rd Mehlich-3 Extraction SoR Report Newton, NC 28658 Mocksville, NC 27028 County: Catawba `,- Links to Helpful Information Samled: Received: 07/10/2012 P Completed: 07/12/2012 Farm: CA 20 Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fes/OG/Tim,M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - Fes/OG/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in glcrrP; CEC and Na in meq/100 crrr3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.32 0.89 10.1 80 2.0 6.0 67 99 50 25 49 655 410 410 274 274 236 0.9 9 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fes/OG/Tim,M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - Fes/O G/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cd; NO3-N in mg/cld]: Soil Class: Mineral HM% W/V CEC BS%, Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.95 9.3 81' 1.8 6.0 73 98 51 25 51 258 171 171 217 217 168 0.7 8 North Carolina l jp.t�c. A Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS A omic Division Phone: (919) 733-2655 Website: www. goviagronomi/ Client: /James/Ottman Jarrett Predictive 3688 Killian Rd Lincolnton, NC 28092 Soil Report Mehlich-3 Extraction County: Lincoln Sampled: Received: 07/10/2012 Completed: 07/12/2012 Farm: LT 35 Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) Report No. FY D00812 Advisor: Synagro 284 Boger Rd Mocksville, NC 27028 Links to Helpful Information More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fes/OG/Tim,M 0.0 120-200 50 0 0 0 0 0 0 0 Note: 12 2 - Fes/OG/Tim, M 0.0 120-200 50 0 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in g/cnn ; CEC and Na in meq/100 cd; NO3-N in mg/dm3]: Soil Class: Mineral HM% WIV CEC . BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.32 0.99 8.1 80 1.6 6.0 39 84 54 21 47 934 577 577 139 139 198 0.8 10 North Caroline J�,h C4.r Iii; 11i?r.il Li:�iY�ci s•I«In Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS : omic Division Phone: (919) 733-2665 Website: www, _.gov/agronomi/ Report No. FY 000814 Client. Wayne Gilbert Advisor: Synagro /Y£ :lf.l' Predictive 884 Cat Square Rd 284 Boger Rd i f 0 Vale, NC 28168 MOCKSVILLE, NC 27028 Ill('c,�y.%iil K3k Ilk, 3=I e ®� Report - Mehlich 3 Extraction County: Lincoln Links to Helpful Information sampled: Received: 07/10/2012 Completed: 07/12/2012 Farm: LT 120 Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fes/OG/Tim,M 0.0 120-200 90 0 0 0 pH$ 0 0 0 Note: 12 Note: 2 - Fes/OG/Tim, M 0.0 120-200 90 0 0 0 pH$ 0 0 0 Note: 12 Note: Test Results [units - W/V in g/crrr ; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.18 0.87 11.7 95 0.6 6.9 21 98 59 32 44 408 248 248 133 133 354 0.8 7 ,North Carolina bXCu., Iiy' Kuril t:.,iY�:d'rs>i4su Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture )0-0II/, SYNAGFZQ A Rejiduals Management Company June 2, 2010 Mr. Jackie Harvell Delta Apparel, Inc. P.O. Box37 Maiden, NC 28650 Dear Mr. Harvell: Enclosed is Synagro's monthly report for April 2010. This report covers land application operations in Catawba and Lincoln Counties. If you have any questions, please contact me at 336-998-7150, extension 13. Th nkkyou, Scott Berg Tecluiical Services Manager Enclosure 284 Boger Road • Mocksville, NC 27028-7619 m Ph: (336) 998-7150 • Fax: (336) 998-8450 a Toll Free: (877) 267-2687 SYNAGPvO A .Residuals Management Company April 2010 LAND APPLICATION OF RESIDUALS MONTHLY REPORT Delta Apparel, Inc. Catawba and Lincoln Counties A better tomorrow for our Client Triangle: The GENERATOR, The LANDOWNER, and The ENVIRONMENT 6� ♦ A ® A A A A A A SYNAGRO CENTRAL, LLC 7014 EAST BALTIMORE STREET BALTIMORE, MD 21224 PROJECT: 2105 - DELTA APPAREL, INC., NC 4/1/2010 thru 4/30/2010 PLANT: 01 - DELTA APPAREL - MAIDEN PLANT Field: NC-CA-00005-0-0001-A FarmerlSite Operator TODD EDWARDS Date Applied 4/26/2010 4/27/2010 TXLIQ Gallons: Field Total (Gallons): Field., NC-CA-00006-0-0001- Farmer/Site Operator DENNIS LUTZ Date Applied 4/30/2010 TXLIQ Gallons: Field Total (Gallons): Field: NC-CA-00006-0-0002- Farmer/Site Operator DENNIS LUTZ Date Applied 4/28/2010 4/29/2010 4/30/2010 TXLIQ Gallons. Field Total (Gallons): Field: NC-LT-00122-0-0001- Farmer/Site Operator NICKY WOODRUFF Date Applied 4/23/2010 4/24/2010 TXLIQ Gallons: Page 1 of 2 Total Applied Unit Type 173,600.00 G TXLIQ 148,800,00 G TXLIQ 322,400.00 322,400,00 Total Applied Unit Type 99, 200.00 G TXL I Q 99,200.00 99,200.00 Total Applied Unit Type 136,400.00 G TXLIQ 117,800.00 G TXLIQ 49,600,00 G TXLIQ 303,800.00 303,800,00 Total Applied Unit Type 99,200.00 G TXLIQ 80,600.00 G TXLIQ 179,800.00 Printed: 5/20/2010 11:27 Field Total (Gallons): 179,800.00 Plant Total Gallons. 905,200.00 Printed: 5/20/2010 Page 2 of 2 11:27 Product Type. DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID (DAMPTXL) Sample Date 4/6/2010 Usage From 4/1/2010 To 4/30/2010 Report # 10-085-0204 & 10-099-0213 Parameter PPM(nng/kg) Lbs/® on PA-N (Injected) 26811 53.622 PA-N (Surface w/ Incorp,) 26811 53.622 PA-N (Surface w/o Incorp.) 23861 47.722 TKN (TKN) 75600 151.2 Ammonia Nitrogen (Am) 5900 11.8 Nitrate Nitrogen (Nin) <1 <0.002 Organic Nitrogen (Orn) 69700 139.4 Total Phosphorus (P) 5370 10.74 Total Phosphate (P205) 12351 24.702 Estimated Avail. P205 6175.5 12.351 Total Potassium (K) 2500 5 Total Potash (K20) 3000 6 Arsenic (As) 1 0.002 Cadmium (Cd) <1 <0,002 Chromium (Cr) 30 0.06 Copper (Cu) 1310 2.62 Lead (Pb) 6 0.012 Mercury (Hg) <0.4 <0.001 Molybdenum (Mo) <5 <0.01 Nickel (Ni) 45 0.09 Selenium (Se) 2 0.004 Zinc (Zn) 160 0.32 Aluminum (AI) 3600 7.2 Calcium (Ca) 4010 8.02 Iron (Fe) 4280 8.56 Sodium (Na) 46200 92.4 Sulfur (S) 31500 63 Magnesium (Mg) 1430 2.86 Manganese (Mn) 180 0.36 Percent Solids: 2.71 % PH Level: 7.3 Calculations PA-N (ppm) = [ (fl) (ppm Org. N) ] + [ (V1) (ppm Ammonia N) ] + (ppm Nitrate N) P x 2.3 = Total P205 Total P205 x .5 = Estimated available P205 Kx1.2=K20 ppm or mglkg x .002 = lbs/dry ton Biosolids/Residuals Application State: NORTH CAROLINA Organic Nitrogen Mineralization Rate (fl): For AEROBICALLY DIGESTED 30.00% Ammonia Nitrogen Non -Volatilized Fraction (V1): For injected:1.00 For Surface w/ Incorp.:1.00 For Surface w/o Incorp.:0.50 NR = Data not Reported to Synagro or Data not Required Notes: %Solids and Nutrients results are from A&L EAstern Lab Report # 10-099-0213 sampled on 4/6/10. All other parameters were taken form A&L Eastern Lab Report # 10-085-0204 sampled on 3123/10. 2105 01 TXLIQ Control 9 45013 10:29:37 6/2/2010 Page: 1 of 1 Report Number. 10-099-0213 Account Number: 46718 Submitted By: SCOTT BERG Send To: SYNAGRO CENTRAUDELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 75840 Sample Id: DELTA APPAREL LAGOON 2 A &L Eastern Laboratories, Inc. 7621whitepineRoad Rtchnlond,Virg1nia-23237 (884)743-84Qt 'Pax(8Q4)27t-6446 m )WM.a1-1abs-e.astem.ebm Project: DELTA APPAREL LAGOON #2 NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 4/6/2010 11:35:00 Date Received: 04/09/2010 00:00 Date Reported: 04/15/2010 Total Solids * 2.71 27100 100.0 KM 04/09/2010 14:44 SM-2540G Moisture * 97.29 100.0 KM 04/09/2010 14:44 SM-2540G Total Kjeldahl Nitrogen 7.56 75600 10.0 JM 04/12/2010 07:59 SM-4500-NH3C-TKN Ammonia Nitrogen 0.59 5900 10.0 JM 04/12/2010 07:59 SM-4500-NH3C Organic N 6.97 69700 10.0 04/12/2010 07:59 CALCULATION Nitrate+Nitrite-N <1.00 1.00 JM 04/12/2010 08:00 SM-450ONO3F Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Oflr rfpUlt.S and letters HfL'• f0r'il)e EXr,.j(rSIVB and COnr(fo.?i7Hl use of our clients, dn(I may not be r9j)rO:lUf,P-d :n 4Y%iU1Q Orp3'7. normay any reference be made to the wak rho rmh1s, or the company in any advertising, news release, or other public ehnour?cee)erts wtt)out cbtainrag our pier written authorization. Pauric McGroary Page: 1 of 2 Report Number: 10-085-0204 Account Number: 46718 Submitted By: SCOTT BERG Send To: SYNAGRO CENTRAL/DELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 75608 Sample Id : DELTA MARCH 2O10 Y A &L Eastern Laboratories, Inc. 7521WhbpineRoad Rlchmond,YrgiMa23237 (804)743-Ml fax(804)271.W6 ivvliv:21-tabs-easteth.co m Project: DELTA MARCH 2O10 NC CERT # 257 REPORT OFANALYS/S Date Sampled: 3/23/2010 11:35:00 Date Received: 03/26/2010 00:00 Date Reported: 04/01/2010 Total Solids * 1.79 17900 100.0 JM 0312612010 15:00 SM-2540G Moisture * 98,21 100.0 JM 03/26/2010 15:00 SM-2540G Total Keldahl Nitrogen 7.65 76500 10.0 JM 03/29/2010 07:59 SM-4500-NH3C-TKN Total Phosphorus 0.54 5370 100 KM 03/29/2010 09:15 SW-6010B Total Potassium 0.25 2600 100 KM 03/29/2010 09:15 SW-60108 Total Sulfur 3.15 31500 100 KM 03/29/2010 09:15 SW-6010B Total Calcium 0A0 4010 100 KM 03/29/2010 09:15 SW-6010B Total Magnesium 0.14 1430 100 KM 03/29/2010 09:15 SW-6010B Total Sodium 4.62 46200 100 : KM 03/29/2010 09:15 SW-6010B Total Iron 4280 1 KM 03/29/2010 09:15 SW-6010B Total Aluminum 3600 10 KM 03/29/2010 09:15 SW-6010B Total Manganese 180 1 KM 03/29/2010 09:15 SW-6010B Total Copper 1310 1 KM 03/29/2010 09:15 SW-6010B Total Zinc 160 1 KM 03/29/2010 09:15 SW-6010B Ammonia Nitrogen 0.62 6150 10.0 JM 03/29/2010 07:59 SM-4500-NH3C Organic N 7.03 70350 10.0 03/29/2010 07:59 CALCULATION Nitrate+Nitrite-N 95.0 1.00 JM 03/29/2010 08:00 SM-450ONO3F Total Cadmium <1.0 1.0 KM 03/29/2010 09:15 SW-6010B All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. C Y Our reao,ts and letters are forlhe exciusrde and wrF�ienva! use of our clients, and m y not be reprodaced in whole or parf, nor may any reference be mad ' e to the work. the results, of the company rr, any adverticing, news refoase, or other aub;rb announcements v lthout oblaining our pnrr ivn'0 eo autnoraat/on. CG Pauric McGroary Page: 2 of 2 Report Number: 10-085-0204 Account Number: 46718. Submitted By: SCOTT BERG Send To: SYNAGRO CENTRAL/DELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 75608 Sample Id : DELTA MARCH 2O10 A&L Eastern Laboratories, Inc. 70 Whitepine Road Richmond, Virginia 23231 (804)74M401 Pax (804) 271. Wa WwWal4abs-easteM.com Project: DELTA MARCH 2O10 NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 3/23/2010 11:35:00 Date Received: 03/26/2010 00:00 Date Reported: 04101/2010 Total Chromium 30 5 KM 03/29/2010 09:15 SW-6010B Total Nickel 45 5 KM 03/29/2010 09:15 SW-6010B Total Lead 6 5 KM 03/29/2010 09:15 SW-6010B Total Arsenic 1.0 1.0 KM 03/29/2010 09:15 SW-601013 Total Mercury <0.4 0.4 KM 03/29/2010 13:30 SW-7471A Total Selenium 2.0 1.0 KM 03/29/2010 09:15 SW-6010B pH (as received)_* 7.30 JM 03/29/2010 08:00 SW-9045D Total Volatile Solids 77,84 778400 100.0 JM 03/26/2010 15:00 SM-254OG Total Molybdenum <5 5 KM 03/29/2010 09:15 SW-6010B Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. r V Our reports and testers ere for the exclusive and confdential use of our chants, and may not be taproduced in whole or part, nor mayary reference be made to the wage. the results, or the company in any advertising, news release, or other public enno;rncements without obtaining our p lorwritten authorization. F Nw Pauric McGroary FIELD REPORT DELTA APPAREL, INC., NC April 2010 Permit No.: WQ0006984 County: CATAWBA Crop: FESCUE Rate: 216.00 LBS PAN/ACRE Applic. Method: SURFACE APPI . Synagro Field: NC-CA-00005-0-0001-A Latitude: . 35.34'48" Longitude: 81.15'42" Acres: 26.7 (10.814 ha) GALLONS APPLIED: Month to Date: 322,400.00 Year to Date: 322,400.00 DRY TONS/ACRE APPLIED: Month to Date: 1.36 Year to Date: 1.36 Cumulative: 6.69 POUNDS PER ACRE APPLIED'*"'** ( Kilograms per Hectare Applied ) PARAMETER MONTH TO DATE YEAR TO DATE CUMULATIVE PAN 65.12 65.12 P 14.66 14.66 K 6.82 6.82 AS <.01 (<.01) <.01 (<.01) 0.03 (0.03) Cd <.01 (<.01) <.01 (<.01) 0.02 (0.02) Cr 0.08 (0.09) 0.08 (0.09) 0.25 (0.28) Cu 3.58 (4.01). 3.58 (4.01) 17.79 (19.92) Pb 0.02 (0.02) 0.02 (0.02) 0.09 (O.lo) Hg <.01 (<.01) <.01 (<.01) <.01 (<.01) MO 0.01 (0.01) 0.01 (0.01) 0.07 (0.08) Ni 0.12 (0.13) 0.12 (0.13) 0.50 (0.56) Se <.01 (<.01) <.01 (<.01) 0.02 (0.02) Zn 0.44 (0.49) 0.44 (0.49) 3.66 (4.10) DAILY FIELD LOADING SHEET DATE PCT_ WEATHER SOIL RAINFALL APPLIED TYPE SOLIDS AMOUNT UNIT DRYTONS CONDITIONS CONDITIONS PAST24 Hr 04/26/2010 DAMPTXL 2.71 173,600.00 GALLONS 19.62 PARTLY CLOUDY DRY 0-<1/2" 04/27/2010 DAMPTXL 2.71 148,800.00 GALLONS 16.82 PARTLY CLOUDY DRY 0-<1/2" TOTALS: 322,400.00 GALLONS 36.43 DT 33.05 MT "NR" = Data not reported to Synagro Technologies, Inc or Data not required. FIELD REPORT DELTA APPAREL, INC., NC April 2010 Permit No.: WQ0006984 County: CATAWBA Crop:' FESCUE Rate: 216.00 LBS PAN/ACRE Applic. Method: SURFACE APPL. Synagro Field: NC-CA-00006-0-0001 Latitude: 35.46'42" Longitude: 81.16'42" Acres: 20.4 (8.262 ha) GALLONS APPLIED: Month to Date: 99,200.00 Year to Date: 99,200.00 DRY TONS/ACRE APPLIED: Month to Date: 0.55 Year to Date: 0.55 Cumulative: 5.14 POUNDS PER ACRE APPL.IED"��**� ( Kilograms per Hectare Applied } PARAMETER MONTH TO DATE YEAR TO DATE CUMULATIVE PAN 26.22 26.22 P 5.90 5.90 K 2.75 2.75 As <.01 (<.01) <.01 (<.01) 0.03 (0.03) Cd <.01 (<.01) <.01 (<.01) 0.02 (0.02) Cr 0.03 (0.03) 0.03• (0,03) 0.18 (0.20) CU 1.44 (1.61) 1.44 (1.61) 13.73 (15.38) Pb <.01 (<.01) <.01 (<.01) 0.07 (0.08) Hg <.01 (<.01) <.01 (<.01) <.01 (<.01) MO <.01 (<.01) <.01 (<.01) 0.05 (0.06) Ni 0.05 (0.06) 0.05.(0.06) 0.37 (0.41) Se <.01 (<.01) <.01 (<.01) 0.01 (0.01) Zn 0.18 (0.20) 0.18 (0.20) 2.95 (3..30) DAILY FIELD LOADING SHEET DATE PCT. WEATHER SOIL RAINFALL APPLIED TYPE SOLIDS AMOUNT UNIT DRY TONS CONDITIONS CONDITIONS PAST 24 Hr 04/30/2010 DAMPTXL 2.71 99,200.00 GALLONS 11.21 FAIR DRY 0-<1/2" TOTALS: 99,200.00 GALLONS 11.21 DT 10.17 MT "NR" = Data not reported to Synagro Technologies, Inc or Data not required. FIELD REPORT DELTA APPAREL, INC., NC April 2010 Permit No.: WQ0006984 County: CATAWBA Crop: FESCUE Rate: 216.00 LBS PAN/ACRE Applic. Method: SURFACE APPL. GALLONS APPLIED: Month to Date: DRY TONS/ACRE APPLIED: Month to Date: Synagro Field: NC-CA-00006-0-0002 Latitude: 35.36'39" Longitude: 81.17'07" Acres: 20.1 (8.141 ha) 303,800.00 Year to Date: 303,800.00 1.71 Year to Date: 1.71 Cumulative: 5.65 ********POUNDS PER ACRE APPLIED ( Kilograms per Hectare Applied } PARAMETER MONTH TO DATE YEAR TO DATE CUMULATIVE PAN 81.51 81.51 P 18.34 18.34 K 8.54 8.54 As <.01 (<.01) <.01 (<.01) 0.03 (0.03) Cd <.01 (<.01) <.01 (<.01) 0.02 (0.02) Cr 0.10 (0.11) 0.10 (0.•11) 0.21 (0.24) Cu 4.48 (5.02) 4.48 (5.02) 14.58 (16:33) Pb 0.02 (0.02) 0.02 (0.02) 0.07 (0.08) Hg <.01 (<.01) <.01 (<.01) <.01 (<.01) Mo 0.02 (0.02) 0.02 (0.02) 0.06 (0.07) Ni 0.15 (0.17) 0.15 (0.17) 0.44 (0.49) Se <.01 (<.01) <.01 (<.01) 0.02 (0.02)' Zn 0.55 (0.62) 0.55 (0.62) 2.85 (3.19) DAILY FIELD LOADING SHEET DATE PCT. WEATHER SOIL RAINFALL APPLIED TYPE SOLIDS AMOUNT UNIT DRY TONS CONDITIONS CONDITIONS PAST 24 Hr 04/28/2010 DAMPTXL 2.71 136,400.00 GALLONS 15.41 FAIR MOIST .0-<1/2" 04/29/2010 DAMPTXL 2.71 117,800.00 GALLONS 13.31 FAIR DRY 0-<1/2" 04130/2010 DAMPTXL 2.71 49,600.00 GALLONS 5.61 FAIR DRY 0-<1/2" TOTALS: 303,800.00 GALLONS 34.33 DT 31.14 MT "NR" = Data not reported to Synagro Technologies, Inc or Data not required. FIELD REPORT DELTA APPAREL, INC., NC April 2010 Permit No.: WQ0006984 County: LINCOLN Crop: FESCUE Rate: 167.00 LBS PAN/ACRE Applic. Method: SURFACE APPL. Synagro Field: NC-LT-00122-0-0001 Latitude: 35.29'52" Longitude: 81.23'30" Acres: 15.6 (6.318 ha) GALLONS APPLIED: Month to Date: 179,800.00 Year to Date: 179,800.00 DRY TONS/ACRE APPLIED: Month to Date: 1.30 Year to Date: 1.30 Cumulative: 4.20 POUNDS PER ACRE APPLIED****** { Kilograms per Hectare Applied } PARAMETER MONTH TO DATE YEAR TO DATE CUMULATIVE PAN 62.16 62.16 P 13.99 13.99 K 6.51 6.51 As <.01 (<.01) <.01 (<.01) 0.01 (0.01) Cd <.01 (<.01) <.01 (<.01) 0.03 (0.03) Cr 0.08 (0.09) 0.08 (0.09) 0.14 (0.16) Cu 3.41 (3.82) 3.41 (3.82) 8.12 (9.09) Pb 0.02 (0.02) 0.02 (0.02) 0.13 (0.15) Hg <.01 (<.01) <.01 (<.01) <.01 (<.01) Mo 0.01 (0.01) 0.01 (0.01) 0.05 (0.06) Ni 0.12 (0.13) 0.12 (0.13) 0.34 (0.38) Se <.01 (<.01) <.01 (<.01) 0.01 (0.01) Zn 0.42 (0.47) 0.42 (0.47) 3.33 (3..73) DAILY FIELD LOADING SHEET DATE PCT. WEATHER SOIL RAINFALL APPLIED TYPE SOLIDS AMOUNT UNIT DRY TONS CONDITIONS CONDITIONS PAST 24 Hr . 04/23/2010 DAMPTXL 2.71 99,200.00 GALLONS 11.21 CLOUDY DRY 0 <1/2" 04/24/2010 DAMPTXL 2.71 80,600.00 GALLONS 9.11 CLOUDY DRY 0-<1/2" TOTALS: ------------ 179,800 00 GALLONS 20.32 DT 18.43 MT "NR" = Data not reported to Synagro Technologies, Inc or Data not required. Page: 1 of 2 Report Number: 11-082-0211 J( A&L Eastern Laboratories, Inc. Account Number: 46718 M ` 7621 Whitepine Road Richmond, Virginia23237 (804)743-W1 ,Fax (804)271.SW Submitted By: SCOTT BERG wwwaleastem.com Send To: SYNAGRO CENTRAUDELTA APPAREL Project :L+T�A�NI�4RCH201� Mary Brewer NC CERT#257�'Y 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS. Lab Number: 81530 Sample Id: DELTA MARCH 2O11 Date Sampled: 3/17/2011 11:15:00 Date Received:Q373%20 Date Reported: 03/28/2011 Total Solids * 2.57 25700 100.0 JM 03/23/2011 15:00 SM-2540G Moisture " 97.43 100.0 JM 03/23/2011 15:00 SM-2540G Total Kjeldahl Nitrogen 7.20 72000 10.0 JM 03/24/2011 07:54 SM-4500-NH3C-TKN Total Phosphorus 0.41 4100 100 KM 03/25/2011 14:46 SW 6010C Total Potassium 0.44 4350 100 , KM 03/25/2011 14:46 SW 6010C Total Sulfur 3.09 30900 100 KM 03/25/2011 14:46 SW 6010C Total Calcium -- - - _ 0.31___ _ __ __ 3110 _ _ 100 _ T — KM 03/25/2011 14:46 SW 6010C Total Magnesium 0.12 1210 100 _ KM 03%25%2011 1446 -- ----—SW-6010C — — -- -- Total Sodium 4.91 49100 100 KM 03/25/2011 14:46 SW 6010C Total Iron 4040 1 KM 03/25/2011 14:46 SW 6010C Total Aluminum 4400 10 KM 03/25/2011 14:46 SW 6010C Total Manganese 180 1 KM 03/25/2011 14:46 SW 6010C Total Copper 1150 1 KM 03/25/2011 14:46 SW 6010C Total Zinc 176 1 KM 03/25/20.11 14:46 SW 6010C Ammonia Nitrogen 0.43 4280 10.0 JM 03/24/2011 07:54 SM-4500-NI3C Organic N 6.77 67720 10.0 03/24/2011 0.7:54 CALCULATION Nitrate+Nitrite-N 136 1.00 JM 03/24/201107:55 SM-450ONO3F Total Cadmium <1.0 1.0 KM 03/25/2011 14:46 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ` 1 V 4 to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. / 4 Debbie Holt Page: 2 of 2 Report Number: 11-082-0211 Account Number: 46718 Submitted By: SCOTT BERG Send To: SYNAGRO CENTRAL/DELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 81530 Sample Id: DELTA MARCH 2O11 A&L Eastem Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 wwwaleastemcom Project: DELTA MARCH 2O11 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/17/2011 11:15:00 Date Received: 03/23/2011 00:00 Date Reported: 03/28/2011 Total Chromium 19 5 KM 03/25/2011 14:46 SW 6010C Total Nickel 30 5 KM 03/25/2011 14:46 SW 6010C Total Lead 7 5 KM 03/25/2011 14:46 SW 6010C Total Arsenic 1.0 1.0 KM 03/25/2011 14:46 SW 6010C Total Mercury <0.4 0.4 KM 03/24/2011 12:00 SW-7471 B Total Selenium 2.0 1.0 KM 03/25/2011 14:46 SW 6010C pH (Standard Units) 7.88 JM 03/24/2011 07:54 SW-9045D Total Volatile Solids 78.14 781400 100.0 JM 03/23/2011 15:00 SM-2540G Total Molybdenum <5 5 KM 03/25/2011 14:46 SW 6010C Comments: QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Fe", "Mn", AND "P", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made ft�4 to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. 4,&W Debbie Holt A Rear Operating Period Covered: From Tlbrm t� RESIDUALS APPLICATION SUMMARY Southeast Region Project: rT f Application County / State: Date submitted J -- y-- C �. Completed BY:_-- j I1 11 Mm- M./ MW { f MM * If acres to be reported doesn't matcbtq net acres permitted, show calculations for deleted acres on the Net Acreage Reduction Caic. Sheet. ** See application method codes on ac Where Required: ❑ Certified Operator " Inspected Signature License No. Operator's Signature Comments: White — Region RMS Canary — Prniex:r Mana our SU MIT ENVIRONMENTAL TECHNOLOGIES, INN. Analytical Laboratories 3 Report Narrative Client: Synagro Southeast Order Number: 1004314 No problems were encountered during analysis of this order number, except as noted. Data Qualifiers: B = Analyte found in the method blank J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ) C = Analyte has been confirmed by another instrument or method E = Analyte exceeds the upper limit of the calibration curve_ D = Sample or extract was analyzed at a higher dilution X = User defined data qualifier. S = Surrogate out of control limits U = Undetected, a = Not Accredited by NELAC ND = Non Detected at LOQ DF = Dilution Factor Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor) Limit Of Detection (LOD) = Laboratory Detection Limit Estimated uncertainty values are available upon request, matrices: A=Air C = Cream DW = Drinking Water L = Liquid O = Oil SL = Sludge SO = Soil S = Solid T = Tablet TC = TCLP Extract WW = Waste Water W = Wipe The test results meet the requirements of the NELAC standard, except where noted, The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc, and that of the client. It cannot be reproduced in any form vAthout the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. Is not responsible for use or Interpretation of the data included herein. "Analytical Integrity" • EPA. Certified • NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 • Fax: 330--253-4489 Web Site: www.settek.com S1 UMMIT ENVIRONMENTAL TECHNOLOGIES, INC. April02,2010 _ Analytical Laboratories Client: Synagro Southeast Address: 284 Boger Rd. Mocksville, NC 27028 Received: 3/2612010 Project #: Delta Apparel TCLP Metals Client ID # Lab ID# Coliected Analyte Rep Lmt Result Units Matrix Method DF Re4Lvl Run Analyst Delta lagoon 1004314-01 23-Mar-10 Cadmium 0.1 <0.1 mg/1 SL 1311 1 1 30-Mar-10 WK Delta Lagoon 100431+01 23-Mat-10 Chromium 0.2 <0.2 mg/f SL 1311 1 5 30-Mar-10 WK Delta lagoon 1004314-01 23-Mar-10 Selenium 0.5 <0.5 mg/l SL 1311 1 1 30-Mar-10 WK Delta Lagoon 1004314-01 23-Mar-10 Arsenic 0.5 <0.5 mg/l SL 1311 1 5 30-Mar-10 WK Delta Lagoon 1004314-01 23-Mar-10 Lead 0.5 <0.5 mg/f SL 1311 1 5 30-Mar-10 WK Delta Lagoon 1004314-01 23-Mar-10 Silver 0.5 <0.5 mg/l SL 1311 1 5 30-Mar-10 WK Delta Lagoon 1004314-01 23-Mar-1013arium 5 <5.0 mg/1 SL 1311 1 100 30-Mar-10 WK Delta Lagoon 1004314-01 23-Mar-10 Mercury 0,002 <0.002 mg/f SL 1311 1 0.2 30-Mar-10 WK TCLP Volai iles Client [D# Lab ID # .ol eeted Analyte Rep Lmt Resuh Units Matrix Mehod al- It= An0.IVst Delta Lagoon 1004311-01 23-Mar-10 Benzene 0.1 <0.1 mg/L SL 1311 1 0.5 31-Mar-10 MS Delta Lagoon 1004314-01 23-Mar-10 2-Butanone (MEK) 2 <2.0 mg/L SL 1311 1 200 31-Mar-10 MS Delta Lagoon 1004314-01 23-Mar-10 Vinyl Chloride 0.2 <0.2 mg/L SL 1311 1 0.2 31-Mar 10 MS Delta Lagoon 1004314-01 23-Mar-10 Chlorobenzene 0A <0.1 mg/L SL 1311 1 100 31-Mar-10 MS Delta Lagoon 1004314-01 23-Mar-10 Chloroform 0.1 <0.1 mg/L SL 1311 1 6 31-Mar-10 MS Delta Lagoon 1004314-01 23-Mar-10Tetrachloroethene 0.1 <0.1 mg/L SL 1311 1 0.7 31-Mar-10 MS Delta Lagoon ' 1004314-01 23-Mar-10 1,1-Dichloroethene 0,1 <0_1 mg/L SL 1311 1 0.7 31-Mar-10 MS Delta Lagoon 1004314-01 23-Mar-10 Carbon tetrachloride 0.1 <0.1 mg/L SL 1311 1 0.5 31-Mar-10 MS Delta Lagoon 1004314-01 23-Mar-101,2-Dichloroethane 0.1 <0.1 mg/L SL 1311 1 0.5 31-Mar-10 MS Delta Lagoon 1004314-01 23-Mar-10 Trfchloroethene 0.1 <0.1 mg/L SL 1311 1 0.5 31-Mar-10 MS TCLP HNA Client ID # Lab ID # Collect,xi Analyt Rep Lmt Result Uniu Matrix Mctitud DF RegLyl Run Analyst Delta Lagoon 1004314-01 23-Mar-10 Hexachlorcethane 0.1 <0.1 mg/I SL 1311 1 3 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-10 2,4-Dinitrotoluene 0.1 <0.1 mg/I SL 1311 1 0.13 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-10 Hexachlorobenzene 0.1 <0.1 mg/I SL 1311 1 0.13 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-101,4-Dichlorobenzene 0.1 <0.1 mg/I SLR 1311 1 7.5 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-102,4,6-Trichlorophenol, 0.25 <0,25 mg/I SL 131l 1 2 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-10 Pyddfne 0.25 <0.25 mg/I SL 1311 1 5 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-10 Pentachlorophenol 0.25 <0.25 mg/l SL 1311 1 100 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-10 2,4,5-Ttichlorophenol 0.25 <0.25 mg/1 SL 1311 1 400 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-10 Cresols 5 <S.0 mg/I SL 1311 1 200 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar-10 Hexachloro-1,3-butadiene 0.1 <0.1 mg/I SL 1311 1 0.5 31-Mar-10 AE Delta Lagoon 1004314-01 23-Mar40 Nitrobenzene 0.1 <0.1 mg/I SL 1311 1 2 31-Mar-10 AE Page 4 ",analytical Integrity" • EPA Certified - NELAP Certified 3310 Win Street • Cuyahoga Fails, Ohio 44223 e Phone: 330-253-8211 • Fax: 330-253-4489 Web Site: www settek. com r ' ENviRoNNi{rNTALTECHNOLOGIES, INC. Analytical Laboratories 4 Client Synagro, Southeast 284 Boger Rd. Mocksville, NC 27028 Order Number 1004314 Project Number Delta Apparel Issued Friday, April 02, 2010 Total Number of Pages 5 (excluding C.O.G. and cooler receipt form) Approved By: 4�41-a-w QA Manager NELAC Accreditation #E87688 "Analytical integrity" • EPA Certified . NEL P Certified 3310 Win Streef Cuyahoga Fails, Ohio 44223 n Phone: 330-253-8211 • Fax: 330-253-4489 Web Site: www.settek.com SUMMIT ENVIRONMENTAL TECHNOLOCiES, INC. Analytical Laboratories 2 Sample Summary Client: Synagro Southeast Order Number: 1004314 Laboratory ID Client ID Matrix Sampling Date 1004314-01 Delta Lagoon Sludge 3/23/2010 Analytical lntearify" • EPIC Certified • NELAP Certified 33,10 Win Street • Cuyahoga Falls, Ohio 44223 o Phone: 330-253-3211 • Fax: 330-2.63-4489 Web Site: wwwsettek.com Client ID# Delta Lagoon Delta Lagoon Delta Lagoon Delta Lagoon Delta Lagoon Delta Lagoon Delta Lagoon Client ID# Delta Lagoon Delta Lagoon Client lD# Delta Lagoon Client lD# Delta Lagoon Client IN Delta Lagoon Client ID# Delta Lagoon Client ID# Delta Lagoon SUMMIT ENVIRONMENTAL TECHNOLOGIES, INC. Analytical Laboratories TCLP Pesticides fah ID €T Collected Analyte Reo Lint Result 1004314-01 23-Mar-10 Enddn 0.002 <0.002 1004314-01 23-Mar-10 Toxaphene 0.1 <0.1 1004314-01 23-Mar-10 Chlordane 0.01 <0.01 IOG1314-01 23-Mar-10 Gamma-8HC 0.002 <0.002 lOG4314-01 23-Mar-10 Heptachlor Epoxide 0.002 <0.002 1004314-01 23-Mar-10 Heptachlor 0.002 <0.002 1004314-01 23-Mar-10 Methoxychlor 0.002 <0.002 lab ID# Collected nal:de 1004314-01 23-Mar-10 2,4,5-TP(Silvex) 1004314-01 23-Mar-10 2,4,0 . Lab 1D9 Collected Analc 1004314-01 23-Mar-10 Flash Point Iab ID # Collected Analc 1004314-01 23-Mar-10 PCBs Lab III# Collecl,(i Anal e 1004314-01 23-Mar-10 pH Lab ID# Collected Anal 1004314-01 23-Mar-10 Reactive Cyanide Iah ID# Collee d Anale IOU4314-01 23-Mar-10 Reactive Sulfide TCLP Herbicides Rep Lml Result 0.5 <0.5 5 <5.0 Result >14OF Result <0.2 April 02, 2010 Client: Synagro Southeast Address: 284 Boger Rd. Macksville, NC 27028 Received: 3/26/2010 Project #: Delta Apparel Units Matrix Method DF RegLvl Run Analyst mg/i 5L 1311 1 0.02 31-Mar-10 KMG mg/l SL 1311 1 0.5 31-Mar--10 KMG mg/l SL 1311 1 0.03 31-Mar-10 KMG mg/I SL 1311 . 1 0A 31-Mar-10 KMG mg/I SL 1311 1 0,008 31-Mar-10 KMG mg/l SL 1311 1 0.008 31-Mar-10 KMG mg/! SL 1311 1 10 31-Mar-10 KMG Uni c Matrix Method DF RegLvl Run Analyst mg/l SL 1311 1 1 30-Mar-10 KMG mg/I SL 1311 1 10 30-Mar-10 KMG Units Matrix Method DF LQS Run Anal st SL 1010 I 29-Mar-10 DVW Units Matrix Method DF LOQ Run Analyst mg/kg SL 8082 1 0.2 31-Mar-10 AE Result Units Matrix Method DF LOD Run An ] st 7.15 su@20.1C SL 9040 1 0.01 29-Mar-10 DCT Ttesult <0.5 Result <25.0 Units Matrix Method Dr L 0 Q Run Analyst mg/kg SL 7.3.3.2 1 OS 29-Mar-10 TRB Units Matrix Method TOF LOQ Run An 1st mg/kg SL 7.3.4.2 1 25 29-Mar-10 TRS Page 5 "Analytical Integrity" , EPA Certified • 1NELAP Certified 3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 • Fax: 330-253-4489 Web Site: www.settek.com. Summit Environmental Technologies, Inc, Cooler Receipt Form � Client: SttOrder Number:��Q 3 j Date Received: Time Received: /(SDO Number of C Boxes: N/A Shipper: (:FEDg UPS DHL Airborne US Postal Walk-in Pickup Other. Packaging: Peanuts Bubble Wrap Paper Foam None Other: r - Tape on cooler/box: Y N N/A Custody Seals intact N N/A C-O-C in plastic Y N N/A Ice Blue ice present / absent / meiied N/A Sample Temperature "C N/A C-0-0 filled out properly Y N N/A Samples in separate bags N NJA Sample containers Intact* (Y 1 N N/A "I€ no, list broken sample(s): Sample label(s) complete (ID, date, etc.) 0 N N/A Label(s) agree with C-O-C N N/A Correct containers used Y N N/A Sufficient sample received N N/A Bubbles absent from 40 mL vials" Y N N/A Samples with bubbles less than the size of a pea are acceptable. Was client contacted about samples Y N Will client send new samples y N Client contact: Date/Time: Logged in by:_ Rev. 6 M9Summit EI><vironl<nentaZ lechnologies, Inc. A�.�l��� ������� ®� ��S$�� 3310 Win Street y Cuyahoga Falls, Oleo 44223 Tel: 330.253.8211 Fax: 330.253.4489 For Summit Environmental Thchnologies, Inc. use only Client Flame S D .9 2D Project Name L 140, A�p� r�� G7 � Qe o CJ rage 1 0 � argg"i B z 01__1 SEI Na Analy-fleal Parameters and Methods Client Addressp Z8,A( �Eie )LO f D MV1111L- f,uc a"7D� Project Address 5 7 @ c � � n � � v l Client Phone No. 336 9f 3 — 74�7v - Report to ,ell LqE.�'� Client liar No, Please Fax Results ✓ ❑ 3156 9NB evi o PO# Client Email Quote No.� Contact Person P77" `3L—'726 Sampled by �DOjl' CSC ��7 Check 1P Ohlo YAP samples ✓ � # Sample Identification !fie! La Date Collected Time Collected 3 a� to i 3of� X 6 L_ NA I2 wished Date 75tneRkgrgeived b : ]pate Time Notes/Comments-, `y � 6e Ila.�,, V ,04�- ltecelved in lab by: Date Time hush Requested: Days Must be approved by lab manager White and yellow pages should --company samples to the laboratory. The -3ient retains the pink page, 2 8539 Page. 2 of 2 Report Number: 10-085-0204 Account Number: 46718 Submitted By: SCOTT BERG Send To: SYNAGRO CENTRAL/DELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number : 75608 Sample Id : DELTA MARCH 2O10 ' v 9 vrww. at- tabs -eastern. com A&L Eastern Laboratories, Inc. 7621WhltspinoRoad Richmond,Arginla=37 (004)M-e4o1 Fax (e041 271-6446 Project: DELTA MARCH 2O10 NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 3/23/2010 11:35:00 Date Received: 03/26/2010 00:00 Date Reported; 04/01/2010 Total Chromium 30 5 KM 03/29/2010 09:15 SW-6010B Total Nickel 45 5 KM 03/29/2010 09:15 SW-60106 Total Lead 6 5 KM 03/29/2010 09:15 SW-6010B Total Arsenic 1.0 1.0 KM 03/29/2010 09:15 SW-6010B Total Mercury <0.4 0.4 KM 03/29/2010 13:30 SW-7471A Total Selenium 2.0 1.0 KM 03/29/2010 09:15 SW-6010B pH (as received) * 7,30 JM 03/29/2010 08:00 SW-9045D Total Volatile Solids 77.84 778400 100.0 JM 03/26/2010 15:00 SM-2540G Total Molybdenum <5 5 KM 03/29/2010 09:15 SW-6010B Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.. C Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results; or the company in any advertising, news release, or other public announcernents without obtaining our pdar.vrilten authorization. Pauric McGroary Page: 1 of 2 Report Number: 10-085-0204 Account Number: 46718 Submitted By: SCOTT BERG Send To: SYNAGRO CENTRAL/DELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number, 75608 Sample 1d : DELTA MARCH 2O10 99 A &L Eastem Laboratories, Inc. 7621 Whitepine Road Rlchmond, Virginia 23237 (804) 743-9401 Fax (%4] 271.6445 vrtwr.al •labs•eastern.com Project; DELTA MARCH 2O10 NC CERT 4 257 REPORT OFANALYSIS Date Sampled: 3/23/2010 11:35:00 Date Received: 03/26/2010 00:00 Date Reported: 04/01/2010 Total Solids " 1.79 17900 100.0 JM 03/26/2010 15:00 SM-2540G Moisture' 98.21 100.0 JM 03126/201015:00 SM-254OG Total Kjeldahl Nitrogen 7.65 76500 10.0 JM 03/29/2010 07:59 SM-4500-NH3C TKN Total Phosphorus 0.54 5370 100 KM 03/29/2010 09:15 SW-6010B Total Potassium 0.25 2500 100 KM 03/29/2010 09:15 SW-601013 Total Sulfur 3.15 31500 100 KM 03/29/2010 09:15 SW-6010B Total Calcium 0.40 4010 100 KM 03/29/2010 09:15 SW-6010B Total Magnesium 0.14 1430 100 KM 03/29/2010 09:16 SW-6010B Total Sodium 4.62 46200 100 KM 03/29/2010 09:15 SW-6010B Total Iron 4280 1 KM 03/29/2010 09:15 SW-601013 Total Aluminum 3600 10 KM 03/29/2010 09:15 SW-6010B Total Manganese 180 1 KM 03/29/2010 09:15 SW-6010B Total Copper 1310 1 KM 03/29/2010 09:15 SW-60108 Total zinc 160 1 KM 03/29/2010 09:15 SW-6010B Ammonia Nitrogen 0.62 6150 10.0 JM 03/29/2010 07:59 SM-4500-NH3C Organic N 7.03 70350 10.0 03/29/2010 07:59 CALCULATION Nitrate+Nitrlte-N 95.0 1.00 JM 03/29/2010 08:00 SM-450ONO3F Total Cadmium <1,0 110 KM 03/29/2010 09:15 SW-6010B All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis, Our reports and tellers are for the exclusive and confidential use orour clients, and may not be reproduced in t4vhole or part, nor may any reference be made p PSG, j� Pr to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. i i� Pauric McGroary Page: 1 of 1 Report Number: 10-099-0213 Account Number: 46718 Submitted By: SCOTT BERG Send To: SYNAGRO CENTRALIDELTA APPAREL Mary Brewer 284 BOGER RD MOCKSVILLE, NC 27028 Lab Number: 75840 Sample Id : DELTA APPAREL LAGOON 2 99 . A &L Eastern Lab®ratodes, Inc. 7521 Whitepilia Road Rkhmond, Virginia 23237 (8D4) 743-W1 Fax ($9.) 271-6446 wm al •l abs•eas tern.c o m Project: DELTA APPAREL LAGOON #2 NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 416/2010 11:35:00 Date Received: 04/09/2010 00:00 Date Reported: 04/15/2010 Total Solids * 2.71 27100 100.0 KM 04/09/2010 14:44 SM-254OG Moisture * 97.29 100.0 KM 04/09/2010 14:44 SM-254OG Total Kjeldahl Nitrogen 7.66 75600 10.0 JM 04/12/2010 07:59 SM-4500-NH3C-TKN Ammonia Nitrogen 0.59 5900 10.0 JM 04/12/2010 07:59 SM-4500-NH3C Organic N' 6.97 69700 10.0 04/12/2010 07:59 CALCULATION Nitrate+Nitrite-N <1.00 1.00 JM 04/12/2010 06:00 SM-450ONO3F Comments: All values are on a dry weight basis except as noted by asterisk, Detection limit on all N series is on a wet basis. j C Our reports and letters are for the exclusive and confidential use or our clients, and may not be reproduced in whole or part. nor may any reference be made to the work, the results. or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary OF W A r�RpG Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources December 30, 2005 CERTIFIED MAIL 7002 2410 0003 0273 3754 RETURN RECEIPT REQUESTED MR. MICK W. BERRY, CITY MANAGER CITY OF HICKORY POST OFFICE Box 398 HICKORY, NORTH CAROLINA 28603 Dear Mr. Berry: Alan W. Klimek, P.E., Director Division of Water Quality p ���uv��n JAN - 4 2006 L Protection Subject: 2004 Annual Report Review and Notice of Violation No. NOV-2006-SP-0001 Permit No. WQ0004563 City of Hickory Hickory Regional Compost Facility and Catawba ORGRO Distribution Program Distribution of Residual Solids (503) Catawba County The Division of Water Quality's (Division) Land Application Unit acknowledges receipt of the annual report for the 2004 calendar year submitted in support of the above:referenced permit on February 17, 2005. The Division has performed a thorough technical review of the information presented in this annual report. Based on this review, the Division has determined that the residuals distribution program is not compliant with the conditions of Permit No. WQ0004563, issued on April 17, 2003, for the following reasons: Condition III. 3. a. of this permit requires that records regarding the source and amount of residuals accepted for treatment at the Hickory RCF be kept. While such records were included in the annual report, they were limited to the wastewater treatment plant and septage sources only. Similar records for the Hickory Water Treatment Plant, also approved in Condition II. 3. a. to deliver residuals to the Hickory RCF for treatment, were not included in the annual report. Condition III. 8. of this permit . requires that all monitoring, including these accepted sources/amounts, be reported in the annual report and submitted to the Division no later than March Is' of the year following the product distribution event. 2. Condition IIl. 4. of this permit requires that the Class A EQ residuals product be analyzed for corrosivity, ignitability, and reactivity as well as toxicity characteristics leaching procedure (TCLP) at least annually in order to demonstrate that the product is non -hazardous under the Resource Conservation and Recovery Act (RCRA). While a report showing the passing TCLP analytical results was included in the annual report, no evidence could be found that the corrosivity, ignitability, and reactivity analyses were perfonned on the product during the 2004 calendar year. Condition IIl. 8. of this permit requires that all monitoring, including the results of the corrosivity, ignitability, and reactivity analyses, be reported in the annual report and submitted to the Division no later than March 1" of the year following the product distribution event. No ethCarolina Naturally Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 Phone (919) 733-3221 Customer Service Internet: www.newaterquality.org 2728 Capital Boulevard Raleigh, NC 27604 Fax (919) 715-0588 1-877-623-6748 Fax (919)715-6048 An Equal Opportunity/Affirmative Action Employer - 50% Recycled/10% Post Consumer Paper Mr. Mick W. Berry December 30, 2005 Page 2 Condition I11. 5. of this permit requires that the Class A EQ residuals product be analyzed for certain parameters, at a frequency commiserate with the volume of product distributed during the calendar year. Based:on information presented in the annual report, monitoring was required on a once per every 60-day period. A summary sheet as well as reports of the analytical work shows that most of the monitoring was complete and in compliance with the required pollutant ceiling and monthly average concentrations. However, results for plant available nitrogen (i.e., by calculation), as required by this condition, were not included for any of the six required monitoring periods. Condition I11. 8. of this permit requires that all monitoring, including the results of the calculated plant available nitrogen concentrations of the product, be reported in the annual report and submitted to the Division no later than March I" of the year following the product distribution event. To prevent further action, carefully review these violations and respond in writing within 30 calendar days of receiving this correspondence. Your response, which should address the cause of your non -compliant status as well as what actions you plan to take to rectify this status and to prevent its recurrence, should be sent to the following address: Ms. Shannon Mohr Thornburg, Environmental Engineer II Land Application Unit Aquifer Protection Section NCDENR-DWQ 1636 Mail Service Center Raleigh, North Carolina 27699-1636 The following other review comments are being provided for informational purposes only so that future operations and annual reports preparation procedures may be adjusted to avoid potential compliance problems: 1. The most current certification and summary form that details the annual Class A EQ residuals product marketing and distribution activities (i.e., Form DMSDF) was not used in preparing the annual report. A copy of this form is enclosed herein for review and reference. An electronic version of this form is also available for download from www.newaterquality.org/lau/main.html. 2. The most current forms that summarize the analytical results for the Class A EQ residuals product (i.e., Form RSSF and Form RSSF-B) were not used in preparing the annual report. A copy of each of these forms is enclosed herein for review and reference. Electronic versions of these forms are also available for download from www.newaterquality.org/lau/main.html. There appears to be a typographical error in the information that was presented in the annual residuals sampling summary form included in the annual report. Specifically, the result box for the nickel analysis for the December 2004 sampling event was left blank. From a review of the laboratory report for this sampling event, it appears as if the nickel concentration was 13.0 milligrams per kilogram. The Division cannot determine whether or not the 13.0-milligram per kilogram nickel concentration recorded for the additional November 2004 sampling event was also a typographical error, as the laboratory report for that sampling event was not included. 4. The pH analysis for the Class A EQ residuals product may have been conducted outside of EPA recommended immediate hold time. The Division recommends that this issue be discussed with the Division -certified laboratory to ensure that a valid analytical result is received in the future. Mr. Mick W. Berry December 30, 2005 Page 3 It is strongly recommended, per page 67 of EPA's guidance document entitled "Control of Pathogens and Vector Attraction in Sewage Sludge," that "multiple [microbiological] samples per sampling event be analyzed" for the Class A EQ residuals product. Chapter 9 of this document provides a lot of guidance regarding sampling procedures, and a thorough comparison of these recommendations with the existing sampling/monitoring plan for the Hickory RCF may help to prevent additional problems with relying on a single sample of product to analyze for sabnonella sp. (and the potential for laboratory error) to prove pathogen reduction compliance. This correspondence does not preclude further action by the Division for additional violations of any applicable statutes, regulations, or permits, and please be aware that nothing in this correspondence should be construed as removing the City of Hickory from the responsibility for complying with its permit in full. If you need anyadditional information concerning this correspondence, please d not hesitate to contact Ms. Thornburg by telephone at (919) 715-6167 or via e-mail at shannon.thoM ur �ncmail.net. % Sincerely / i 1 im . Colson, P. .,Supervisor Land Application Unit Enclosures cc: Mr. Wayne Carroll, Veolia Water North America Operating Services, L.L.C. Mr. Kevin B. Greer, P.E., City of Hickory _ f s Ei16Huffman;_MooresviRe Regional Officee_Aquifer,Protectiori Section il APS Central Files - Permit File WQ0004563 ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM PERMIT #: FACILITY NAME: PHONE: COUNTY: OPERATOR: FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? ❑ Yes ❑ No No If No skip parts A, B; C and certify form below Part A*: Part B*: Month (. Sources s include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January February March April May June - July August September October November December Totals: Annual (dry tons): Amendments) used: Bulking Agent(s) used: it more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year with all conditions of the permit (including but not limited to items 1-3 below) -issued by the Division of Water Quality. ❑ Yes ❑ No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received -from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Date Signature of.Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF (11/2005) 4 \1 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: Laboratory: 1) Facility Name: 2) NPDES # or 3) ' WQ#: 4) WWTP Name: 5) Residual Analvsis Data Sample or Composite Date Ism "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer Date DENR FORM RSSF (5/2003) rmi4: County: C Year: a b0 Facility Name (as shown on permit): � ik. qq 406 'r &-14..1 iu e . Land Application Operator: A l l e Al /n c2 a Phone: Land application of residual solids as allowed by the permit occurred during the past calender-year? )( Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: ' Total number of fields land application occurred during the year: Iq Total amount of dry tons applied during the year for all application sites: , 5- Total number of acres land application occurred during the year: Part B: Facility was compliant during calendar year A0 6,4 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. ErYes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0. or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies'of certified laboratory results are attached. 6. The `facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). T All general requirements in 40 CFR, Part -503.12 and'management practices in 40 CFR Part 503.14 were . complied with (applicable to. 40 CFR Part 503 .regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a' deviation, prior authorization was received from the Division of.Wdter-Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well'or explanations of. violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. . 11.=No runoff of residuals from the application sites onto adjacent property or nearby surface. waters has occurred. 12. All buffer requirements as specified on the permit were. maintained during each application''of residuals': "I certify, under penalty of law, that the above information is, to the best of my knowlpdgeland, elief, true, ub accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines an i8prisonment §rzknowing violations." G-) m v ehi'e- all 1-1Q�, � c e zm Permittee Name and title (type or prt�n � , n�o Signature of Pe tee Date a m;U Z Signature of Prepazer* m Date Signiture of Lan Applier Date (if different from Permittee) _0, o m? (if different from Permittee and Preparer) * Preparer is defined in .40 CFR Part 5032 . m Author Daryl D. Merritt DENR FORM ACF (7/2002). ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your per may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number:) ('J 0 00 �p q y(4 Laboratory: Facility Name: NPDES # or WQ#: N c o 0o c0 i a a WWTP Name: Residual Analvsis Data 1) /� » .j9,i �Lrl>>°c e s� Jwt 2) 3) 4) 5) Sample or CompositeDate a. "I certify, under penalty of law,'that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer Date Author Daryl D. Merritt DENR FORM RSSF (7/2002) ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM PERMIT #: (A)Q p ()p FACILITY NAME: f)e. PHONE: g2,g_ 4,IT - et gal COUNTY: ifea_4a ja, 6 o— OPERATOR: c �f !l&nr /i) !fie e_ FACILITY TYPE (please check one): ® Surface Disposal (complete .Part A (Source(s)' and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete'Parts A, B, and C) Was the facility in operation during the past calendar year? § Yes ❑No - No If No skip parts A. B. C and certify form below Part A*: - - Part B*: MontMonthAdmendment/ Sources s (include NPDES # if applicable) Volume (dry tons) Residual In Product Out Bulking Agent Recipient Information Name(s) Volume (dry tons) Intended use(; January February March April May June e r 1 c /� 3 > d July G x} 1 9- August September October ij November December Totals: Annual (dry tons): -----[—Bulking Admendment(s) used: 1 Agents) used: * If more space than given is required, please attach. additional information sheet(s). ❑ Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year Ab0 :. with. all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Quality. ® Yes ❑ No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies. of certified laboratory results are attache 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Wate Quality. 3. No contravention of Ground Water Quality. Standards occurred at a monitoring. well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are sigm ii ant penalties for submitting false informaiton, including -the possibility of fines and imprisonment for knowing violations." Signatu of Permitte Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) Author Daryl D. Merritt DENR FORM DMSDF (7/2002) Solid results are reported on a Lab Sample No: 924283781 Client Sample ID: SLUDGE PO Metals Metals, Trace ICP Aluminum Cadmium Calcium--''> Copper Lead` Magnesium Nickel Potassium Sodium Zinc Date Digested Wet Chemistry Percent Moisture Percent Moisture Total Percent Solids Percent Solids Pace Analytical Services, Inc. 9800 Kincey /lvenue, Suite 100 Huntersville, NC 28078' Phone. 704.875.9092 Fax:704.875.9091 Lab Project Number: 9268019 Client Project ID: Sludge Pond basis Project Sample Number: 9268019-001. Date Collected: 05/24/04 10:30 Matrix: Soil Date Received: 05/26/04 13:05 Results Units Report Limit DF Analyzed By CAS No. Qual Re" Prep/Method: EPA 3050 / EPA.6010 880 mg/kg 380 38.3 06/01/04 17:31 LBG 7429-90-5 ND mg/kg 3.8 38.3 06/01/04 17:31 LBG 7440-43-9 9500 mg/kg 380 .' 38.3 06/01/04 17:31 LBG 7440-70-2 190 mg/kg 7.7 38.3 06/01/04 17:31 LBG 7440-50-8 ND mg/kg 19. 38.3 06/01/04 17:31 LBG 7439-92-1 2900 mg/kg 380 38.3 06/01/04 17:31,LBG 7439-95-4 21. mg/kg 19. 38.3 06/01/04.17:31 LBG 7440-02-0 4500 mg/kg 3800 38.3 06/01/04 17:31 LBG 7440-09-7 31000 mg/kg 3800 38.3 06/01/04 17.:31 LBG 7440-23-5 340 mg/kg 38. 38.3 06/01/04 17:31 LBG 7440-66-6 06/01/04 06/01/04 Method: % Moisture 97.5 % 1.0 05/27/04 11:31 EDF Method: EPA 160.3 2.5 I; 1.0 05/28/04 DHW Nitrogen, Ammonia Method: EPA 350.1 Modified Nitrogen, Ammonia 3000 mg/kg Total Kjeldahl Nitrogen, Soil Method: EPA 351.2 Nitrogen, Kjeldahl, Total 62000 mg/kg Nitrogen. Nitrate plus Nitrite Method: EPA 353.2 Modified Nitrate as N ND mg/kg Nitrite as N ND mg/kg Phosphorus, Total, Soil Method: EPA 365.2 Phosphorus 3080 mg/kg _PH Method: EPA 9045 PH 7.80 units Plant Available Nitrogen Method: Date: 06/16/04 21. 2.1 06/02/04 09:12 MMG 7727-37-9 4500 447 06/01/04 15:07 ARH 41. 41. 407 4.1 06/02/04 15:27 ARH 4.1 06/02/04 15:27 ARH 40.7 06/02/04 11:13 MMG 7723-14-0 1.0 06/04/04 17:20 MDK REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. 1 Page: 1 of 13 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 NC Drinking Water 37712 N ACCpgO SC Environmental 99030 FL NELAP E87648 <i11e�7C ace Analytical ° www.pacelabs.com Solid results are reported on a dry we Lab Sample No: 924144066 Client Sample ID: SLUDGE POND Metals Trace ICP Metals efCLPLeach Date Digested/` f�,` Trace ICP etals. TCLP Leach Chromium Lead Selenium Silver Date Digested Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax. 704.875.9091 Lab Project Number: 9265452 Client Project ID: Sludge Pond 4/21/04 idht basis Project Sample Number: 9265452-001 Date Collected: 04/21/04 11:00 4/21 Matrix: Other Date Received: 04/22/04 14:30 Results Units Report Limit OF Analyzed By CAS No. Qual RegLmt Method: EPA 6010 04/26/04 Prep/Method: EPA 3010 / EPA 6010 ND mg/l 0.025 0.082 mg/l 0.025 ND mg/l 0.0050 ND mg/1 0.010 ND mg/l 0.025 0.029 mg/l 0.025 ND mg/l 0.010 04/29/04 04/26/04 1.0 05/04/04 19:39 LBG 7440-38-2 1.0 05/04/04 19:39 LBG 7440-39-3 1.0 05/04/04 19:39 LBG 7440-43-9 1.0 05/04/04 19:39 LBG 7440-47-3 1.0 05/04/04 19:39 LBG 7439-92-1 1.0 05/04/04 19:39 LBG 7782-49-2 1.0 05/04/04 19:39 LBG 7440-22-4 04/29/04 Mercury, CVAAS, TCLP Leachate Method: EPA 7470 Mercury ND mg/l 0.00020 1.0 04/29/04 GUMS Semivolatiles Semivolatile Organics, TCLP 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachloro-1.3-butadiene Hexachlorobenzene Hexachloroethane 2-Methylphenol (o-Cresol) 3&4-Methylphenol Nitrobenzene Pentachlorophenol Pyridine 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) - -Phenol-d5 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Date Extracted Date: 05/05/04 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FL NELAP E87648 Prep/Method: EPA 3510 / EPA 8270 ND mg/l 0.75 ND mg/1 0.013 ND mg/l 0.056 NO mg/l 0.013 NO mg/1. 0.30 ND mg/l 0.010 0.073 mg/l 0.010 NO mg/l 0.20 ND mg/l 10. NO mg/l 0.50 ND mg/l 40. NO mg/l 0.20 49 % 50 X 64 X 25 X 33 % 63 X 04/30/04 ALV 7439-97-6 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04 19:37 BET 1.0 05/01/04.19:37 BET 1.0 05/.01/04 19:37 BET 04/30/04 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 1�o IN AC ~opO�c <<ne ac= 106-46-7 121-14-2 87-68-3 118-74-1 67-72-1 95-48-7 98-95-3 87-86-5 110-86-1 95-95-4 88.06-2 4165-60-0 321-60-8 1718-51-0 4165-62-2 367-12-4 Page: 1 of 15 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 `% . ace Analytical ° www.pacelabs.com ,�' Lab Sample No: 924144066 Client Sample ID: SLUDGE POND, GC Semivolatiles Pesticides, TCLP Lei gamma-BHC (Lindane Chlordane Endrin or Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) Date Extracted Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9265452 Client Project ID: Sludge Pond 4/21/04 Project Sample Number: 9265452-001, Date Collected: 04/21/04 11:00 Matrix: Other Date Received: 04/22/04 14:30 Results Units Report Limit OF Analyzed By CAS No. Qual RegLmt Prep/Method: EPA 3510 / EPA 8081 NO mg/l 0.040 ND mg/l 0.0030 ND mg/l 0.0020 NO mg/l 0.00080 ND mg/l 1.0 NO mg/l 0.050 96 % 59 X 04/29/04 Acid Herbicides, TCLP Leachate Prep/Method: EPA 3510 / EPA 8151 1.0 05/03/04 17:26 RPJ 58-89-9 1.0 05/03/04 17:26 RPJ 57-74-9 1.6 05/03/04 17:26 RPJ 72-20-8 1.0 05/03/04 17:26 RPJ 76-44-8 1.0 05/03/04 17:26 RPJ 72-43-5 1.0 05/03/04 17:26 RPJ 8001-35-2 1.0 05/03/04 17:26 RPJ 877-09-8 1.0 05/03/04 17:26 RPJ 2051-24-3 04/29/04 2.4-D ND mg/l 1.0 1.0 04/30/04 15:58 JEM 94-75-7 2.4,5-TP (Silvex) NO mg/l 0.10 1.0 04/30/04 15:58 JEM 93-72-1 2,4-DCPA (S) 72 % 1.0 04/30/04 15:58 JEM 19719-28-9 Date Extracted 04/25/04 04/25/04 GUMS Vol ati l es Volatile Organics, TCLP Leach. Method: EPA 8260 Benzene NO mg/l 0.010 1.0 05/01/04 15:50 RWS 71-43-2 2-Butanone (MEK) 0..074 mg/l 0.010 1.0 05/01/04 15:50 RWS 78-93-3 Carbon tetrachloride NO mg/l 0.010 1.0 05/01/04 15:50 RWS 56-23.5 Chlorobenzene NO mg/l 0.010 1.0 05/01/04 15:50 RWS 108-90-7 Chloroform ND mg/l 0.010 1.0 05/01/04 15:50 RWS 67-66-3 1,2-Dichloroethane ND mg/l 0.010 1.0 05/01/04 15:50 RWS 107.06-2 1.1-Dichloroethene NO mg/1 0.010 1.0 05/01/04 15:50 RWS 75-35-4 Tetrachloroethene NO mg/l 0.010 1.0 05/01/04 15:50 RWS 127-18.4 Trichloroethene ND mg/l 0.010 1.0 05/01/04 15:50 RWS 79-01-6 Vinyl chloride NO mg/l 0.010 1.0 05/01/04 15:50 RWS 75-01.4 Toluene-d8 (S) 97 % 1.0 05/01/04 15:50 RWS 2037-26-5 4-Bromofluorobenzene (S) 78 % 1.0 05/01/04 15:50 RWS 460-00.4 Dibromofluoromethane (S) 89 % 1.0 05/01/04 15:50 RWS 1868-53-7 1.2-Dichloroethane-d4 (S) .76 X 1.0 05/01/04 15:50 RWS 17060-07-0 Date: 05/05/04 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FL NELAP E87648 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. P AC�pgo «ne ace= Page: 2 of 15 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED.FOR EACH APPLICATION FIELD. PLACE A "N/V IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: e �.�-� �op� r� I C , Permit #: � p0a(o4 5rq Annual Dry Tons Applied: E Q , q Owner: Ab praia.h1� Operator: 1QN Al eQee_ D&1 % t"re(,, TCation Exchange Capacity (non 503): e Site #: _ 1 Field #: NA Acres Utilized: > Acres Permitted: j Cd A S Totals Per Acre ° Solids As Deci- al Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, iS Inches Precip. Past 24 Hrs. Appli- cation Meth- od** Voli- tila- zation Rate* Miner- ala- zation Rate TKN Ammo nia- Ni- . trogen Ni- trate- Ni- trogen PAN 1 PAN 2 Must Select Crop 1 or Croi 2 G 1. Cu.Yd. Report Totals T Gal. I inSwN Crop 1 Crop e f67,6Q6 3,30000 S 3 iJe 3000 <X2 ,3 NA Encig N/l -42000 TOTALS: 33 g00 , �' As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A plied Annual lbs/acre N A 3, 117CQ, 31 NA Date lbs/ac Current Cumulative lbs/acre D 101�(d 1 146 co I W03 1 4, wK— , b(a27 10, X11 D OAS q s0 1000 a so FS-0 0 1.2,50 1 NA Prior Years Cumulative lbs/acre Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty'.of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." oam,l% *Application Method: $ -Surface, IN - Injection, INC - Incorporatioi Signature of Land Applier Date . **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Author Daryl D. Merritt DENR FORM FSF (7/2002) A1111 VAL.lV1v 1 ALJ XAJ.UJJ" JJ%Jr3L"ll\lT 0V1111V1C11\1 V"XXIV1 Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: 'D ej+e, A ja pa re- I 1 t4c , Total Dry Tons Applied (Annual): S z 9 Permit #: .i-JQ 000 t. Q %,4 Cation Exchange Capacity (non 503 only): Operator: Afi-eN /7)Ckee- lfc,.Aeag«l Owner: 14Le . Ue—A,� Acres Used: / S Acres Permitted: / Site #: Field #: AIA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): I . MOMENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): TO "Il Total Phos- phorusEEMENEENEEMEN "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting'false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt - DENR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Del&. . 4 a zka rp j .. L n .. Permit #: jC)L� WI) &q Annual Dry Tons Applied: Owner: A k e r ��.,��� Operator: M.CIQ e e— De. li c n ation Exchange Capacity (non 503): Site #: — Field #: Acres Utilized: j Gj Acres Permitted: 19 Specify Totals per Acre ° Solids As Deci- al Dry Tons . Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet MoiS Inches Preci past 24 Hrs. Appli- cation Meth- od** Voli- tila- zation Rate* Miner- Ala- zation Rate T KN Ammo nia- Ni- trogen Ni- trate- Ni- trogen pAN 1 PAN 2Crop Must Select 1 or CroQ 2 Crop 1 Crop Tumei 3:Z.S061 1710 6,15 2 91 636,560 S 5,45 h.. s - 1,20.00 TOTALS: N4, gq .9 As Cd Cr Cu Pb Hg Mo Ni Se zn P PAN 1 PAN 2 Lime Applied Annual lbs/acre 5' S3 A4A IS2,91 NA Date lbs/ac Current Cumulative lbs/acre 3411 _L2SS 1 1, 2617 1 2 Ole Qlb:z 14,341 125s, !20 17 60 G U a SO nO - -0 0 Prior Years Cumulative lbs/acre Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty.of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. "&z 221*Application. Method: S - Surface, IN - Injection, INC - Incorporatior Signature of Land Applier Date . **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Author Daryl D. Merritt DENR FORM FSF (7/2002) ���... v.aa. ..au aaau� aas✓a+y a�vC>Y a1�v vvlvilvaAt\i i'vi�lvi Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: J)p �, /� n art r e I . 1 hl c . Total Dry Tons Applied (Annual): Permit #: p /te!2 Sn{ ,t� Cation Exchange Capacity (non 503 only): r] , Operator: iQil�nr e /✓P.I 4al,-, y T.,C Owner: %�, tug,{t,,4 Acres Used: cj Acres Permitted: 1 R Site #: 4 _ Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Total Phos- Eiiii■E:iiE: Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submittingfalse information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD, PLACE A "N/A" IN A BLANK OP. BOX WHEN NOT APPLICABLE. Facility Name: Q eAL A,ate b)Q 0 r)d&q � 4, Annual Dry Tons Applied: 17 _ ,� r e �; i ,� c Permit #: Owner: t a G . Operator: c Cation Exchange Capacity non 503 Site #: jar ,! _ 3 Field #: Acres Utilized: f p Acres Permitted: 16 Q Specify Totals Per Acre o Solids As Dec' a Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, wet is Inches Preci p' Past 24 Hrs. Appli- cation Meth- od** Voli- tila- zation Rate* Miner- ala- zation Rate TKN Ammo nia- Ni- trogen Ni- trate- Ni- trogen PAN 1 PAN 2 Must Selec Crop 1 or Cr( P 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 1)16001 06 5 S1,22006 3 0co <rd2. 3 D Nr4 TOTALS: hob As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annual lbs/acre A N q p /4 1$ 1(Q ,'7 p )W,4 Date lbs/a. Current Cumulative lbs/acre s 3 10 �Zo to I 11,Qj4 1 1 ,'7qo 1voc J0313p l i 7 O 9 1.2E0 p 1 4 1 Aso I so Prior Years Cumulative lbs/acre Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �222 g *Application Method: S - Surface, IN - Injection, INC - Incorporatio: Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Author Daryl D. Merritt DENR FORM FSF (7/2002) 1'11\ 11 V C,L LVAA2 1 L'>LJ X AAI LIJ 11"t9L11\ %T 0 V LV11Vlti1x i S' lJl\1Vl • Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: ,[7� �-�_ n ' Total Dry Tons Applied (Annual): o2 17 Permit#: (�)©� q T Cation Exchange Capacity (non 503 only): Operator: A fl,eni IyKkee- . Delfa_i4eenrd, X... Owner: p6ern;aJ4-ti.4 Acres Used: Acres Permitted: p Site #: 4 — 3 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg%kg, % Solids use Raw Percent #): Total Phos- LphorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting'false.information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) i ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED.FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: 40QA0re-1 1 �� , Permit #: dUn/o95f Annual Dry Tons Applied: #)f, .t1 Owner: A bg_rm0_+kq Operator: ,qll enF /I')�2e� . pe/F44an, «/ . Cation Exchange Capacity (non 503): Site #: ,q _ ,r� Field #: Acres Utilized: J , S Acres Permitted: 1 a, , S � A Specify Totals Per. Acre Solids As Deci- a Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, i Inches Precip. Past 24 Hrs. Appli- cation � Meth- od** Voli- tila- zation Rate* Miner- ala- zation Rate TKN Ammo nia- Ni- trogen Ni- trate- Ni- trogen PAN 1 PAN 2 Must Select Crop 1 or Cro P 2 ' Cu.Yd. Report Totals in Gal. Crop 1 Crop TAV - 31-400 — 3�' D�l�w rn D S 5 000 3 060 < a- Iq 1. 4h( e N TOTALS: 1,36400. 2 As Cd Cr Cu Pb Hg Mo Ni Se Zn P jPAN1 PAN 2 Lime Applied Annual lbs/acre 1} ] a 3 , i q I , A Date lbs/ac Current Cumulative lbs/acre D,�q 3 ,73 T , 2417 1 T 03q7 3 77(% , 2 (, g 266116001 Hr0 - p Prior Years Cumulative lbs/acre Permitted C. P. L. R. * * * Permit PAN Limit 1 st/2nd Crop "I certify, -under penalty' 'of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that'qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: $ - Surface, IN -'Injection, INC - Incorporatioi Signature of Land Applier Date . **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Author Daryl D. Merritt DENR FORM FSF (7/2002) - a\vaau a. _a-i.---1 LWJMXVA . Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: e (��� r� !fin r . 1 n! G . Total Dry Tons Applied (Annual): .41 4 Permit #: �) /� p p p q �cF Cation Exchange Capacity (non 503 only): Operator: en1_Owner: Acres Used: i , j Acres Permitted: . S Site #: Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg%kg, % Solids use Raw Percent #): MW Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- Phorus-ENNEENNEENEEN "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting'false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt - DENR FORM MFLSF (7/2002) "NCDA, e 'A-'"" 6ihit"DiVi I V 9 on 40W -te�ekl, fg-, 9r,011 -�J-1-14, ,"Ro4i Grower.- Delta Mills Apparel, Inc. Copies to: a PO Box 37 . . . . . . . . . . . . . . . . . . . . . . . . . . . soil 100 West Pine St. Maiden, NC 28650 Test Report Farm: Abernathy 4/26/04 SERVING N.C. CITIZENS FOR OVER 50 YEARS Catawba County Agronomist Comments: C 12 Field Information3 d1- -6en-6fit" o", Sample No. Last Crop Ko Yr TIA Crop or Year Lime N R05 KO Mg Cu Zu B Mn See Note A01 1st Crop: Fes/0G/Tirn,M 0 120-200 70-90 0 0 0 0 0 12 2nd Crop,: Test Results Soil Class HM%6 W/V CEC BS% Ac PH P-I K-I Ca% Mg% Mn-IMn-AI (1)Mn-AI (2) Zn-1 Zn-Al Cu-I S-I SS -I NO3-N AB-N Na MIN 0.27 1.06 .5 88.0 1.1 6.3 26 168 51.0 29.0 414 261 84 84 98 76 0.2 ring 10 ilJj"1in*',k6 AV o fintn- A-ati-ons nen Sample No. Last Crop Mo Yr TIA Crop or Year Lime N R05 KO Mg Cu Zu B Mn See Note A02 1st Crop: Fes/OG/Tim,M -3T 120-200 120-140 10-30 0 0 0 0 12 2nd Crop: Test Results Soil Class HM?lo W/V CEC Bklo Ac PH P-I K-I Ca% Mg% Mn-I Mn-Al (1) Mn-Al (2) &-1 Zn-Al Cu-I S-I SS -I NO3-N AB-N Na MIN 0.56 0.92 7.8 83.0 1.3 5.8 6 64 56.0 23.0 277 183 167 107 149 71 0.2 -FieldInformations Tie1" ame 41` eko mmen u6 s Sample No. Last Crop Mo Yr TIA Crop or'Year Lime N D05 ko Mg Cu Zn B Mn See Note A03 1st Crop: Fes/OG/Tim,M 0 120-200 120-140 0 0 0 0 0 12 2nd Crop.: Test Results Soil Class HW16 W/V CEC BS% Ac pH P-I K-I Ca% Mg% Mn-I Mn-Al (1) Mn-Al (2) Zn-I Zn-Al Cu-I S-I SS-1 NO3-NA71i-N Na MIN 0.36 1.06 .1 87.0 1.2 *6.0 6 187 51.0 26.0 252 168 88 88 95 80 0.2 rma �fiddlfifo A`- &-Liine ;Recommendations ` A Sample No. Last Crop Mo Yr TIA Crop or Year Lime N D05 ko Mg Cu Zn B Mn See Note A04 1st Crop: Fes/OG/Tim,M -3T 12 0-200 100-120 40-60 0 0 0 0 12 2nd Crop: Test Results Soil Class HM016 W/V CEC BS% Ac pH P-I K-I Ca% Mg% Mn-I Mn-Al (1) Mn-Al (2) Zn-I Zn-Al Cu-1 S-I SS -I NO3-N NH-N Na MIN 0.51 0.95 8.0 84.0 1.3 5.8 14 47 56.0 25.0 199 136 124 124 131 57 0.2 >M111) SYNAGIZO A Residuals Management Company October 28, 2004 Mr. Gene Hudgens, Plant Manager Delta Apparel, Incorporated Post Office Box 37 Maiden, NC 28650 Dear Mr. Hudgens: As part of the technical staff here at Synagro, Jonathan Hill and I have been reviewing your recently renewed permit, number "WQ0006984", for the land application of residuals from your Maiden plant According to part 11.10. of the permit, a sludge analysis dated "06/16/04" indicates that the residuals have a sodium absorption ratio of (approximately)11. Thus, it is my responsibility to review these results and make recommendations for maintaining the integrity of the land application sites. According to soil test reports for 5 samples taken this year, all of the samples show 0.2 milli -equivalents of sodium per 100 cubic centimeters of soil. The publication "Understanding the Soil Test Report", from the -Agronomic Division of NCDA & CS states that values less than 0.4 milli -equivalents per 100 cubic centimeters are inconsequential to plant nutrition. Additionally, it appears that 0.4 value is important only in sandier soils with low cation exchange capacity. For the recent samples, the cation exchange capacity ranges from 7.0 to 9.5. According to the publication cited above, your land application sites do not have low cation exchange capacity. Thus, the sites recently soil tested appear to have good characteristics for the land application of your plants residuals. It does not appear that any actions are necessary to maintain the integrity of your sites, other than the required monitoring. Thank you for this opportunity to assist your project. Sincerely, 5.0 SOIL SC fian Th°� LU gEric Thompson ----Licensed Soil Scientist -in the State of North Carolina..'€ License Number 1238 q� 1233 �" no�cna c Cc: J. Hill, Technical Services Director 6220-A Hackers Bend Court, Winston-Salem, NC 27103 0 Ph: (336) 766-0328 • Fax: (336) 766-8652 • Toll Free: (877) 267-2687 pi. S"AGBIvO A Residuals Management Company October 28, 2004 Mr. Gene Hudgens, Plant Manager Delta Apparel, Incorporated Post Office Box 37 Maiden, NC 28650 Dear Mr. Hudgens: As part of the technical staff here at Synagro, Jonathan Hill and 1 have been reviewing your recently renewed permit; number V40006984", for the land application of residuals from your Maiden plant. According to part 11.10. of the permit, a sludge analysis dated "06116104" indicates that the residuals have a sodium absorption ratio of (approximately)11. Thus, it is my responsibility to review these results and make recommendations for maintaining the integrity of the land application sites. According to soil test reports for 5 samples taken phis year, all of the samples show 0.2 milli -equivalents of sodium per 100 cubic centimeters of soil. The publication "Understanding the Soil Test Report", from the Agronomic Division of NCDA & CS'states that values less than 0.4 milli -equivalents per 100 cubic centimeters are inconsequential to plant nutrition. Additionally, it appears that 0.4 value is important only in sandier soils with low cation exchange capacity. For the recent samples, the cation exchange capacity ranges from 7.0 to 9.5. According to the publication cited above, your land application sites do not have low cation exchange capacity. Thus, the sites recently soil tested appear to have good characteristics for the land application of your plant's residuals. It does not :appear that any actions are necessary to maintain the integrity of your sites, other than the required monitoring. Thank you for this opportunity to assist your project Sincerely, �Q SOIL SCE, on Tho W _ Enc Thompson Licensed Soil Scientist in the State of North Carolina License Number 1238 ``®""�• 1238 .• � IVOf� Cc: J. Hill, Technical Services Director 6220-A Hackers Bend Court, Winston-Salem, NC 27103 • Ph: (336) 766-0328 0 Fax: (336) 766-8652 • 'loll Free: (877) 267-2687