WQ0006984_Regional Office Historical File Pre 2018 (4)

28GRO2£i=t Boger 11iTeniie '
4 Boger, Avenue
27428
SYNA
wwwsynagro.com
Sent via email
Mr. Laurie Russell
South Fork Industries
100 West Pine Street/P.O. Box 740
Maiden, NC28650
Dear Nis. Russell:
Enclosed is Synagro's monthly report for October 2019. This report covers land application
operations. in Catawba and Lincoln Counties.
If you Have any questions, please contact me: at 336-703-8681.
Sincerelyy,
Alex Fos
Technical Services Specialist
Enclosure

October 2019
LAND APPLICATION OF RESIDUALS
DUALS
MONTHLY REPORT
South Fork Industries, NC
Catawba and Lincoln Counties.

SYNAGRO CENTRAL, LLC
435 WILLIAMS- COURT, SUITE 100
BALTIMORE, MD 21220
PROJECT: 2105
- SOUTH FORK INDUSTRIES, INC., NC
10/1/2019 thru 10131/2019
PLANT: 01 - SOUTH FORK INDUSTRIES- MAIDEN
PLANT
Field: NC-CA-00006-0-0001-
Farmer/Site Operator DENNIS LUTZ
Date Applied
Total Applied
Unit
Tvve
10/4/2019
198,400.00
G
TXLIQ
TXLIQ Gallons:
198,400.00
Field Total (Gallons):
198,400.00
Field: NC-CA-00006-0-0002-
Farmer/Site Operator DENNIS LUTZ
Date Applied
Total Applied
Unit
Type
10/7/2019
161,200.00
G
TXLIQ .
TXLIQ Gallons:
161,200.00
Field Total (Gallons):
161,200.00
Field: NC-LT-00035-0-0001-
FarmerlSite Operator JAMES JARRETT
Date Applied
Total Applied
Unit
Type
10/1/2019
124, 000.00
G
TXLIQ
10/2/2019
186;000.00
G
TXLIQ
10/3/2019
192,200.00
G
TXLIQ
TXLIQ Gallons:
502,200.00
Field Total (Gallons):
502,200.00
Plant Total Gallons:
861,800.00
Printed: 11 /27/2019
Page 1 of 1
__ - ___
12:32

Dosage Rate. Evaluation Report
Product Type: SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID (SFIMPTXL)
Sample Date 9/17/2619
Report # 19-262-0016
Parameter
PA-N (Injected)
PA-N (Surface w/ Incorp.)
PA-N (Surface w/o Incorp.)
TKN (TKN)
Ammonia Nitrogen (Am)
Nitrate Nitrogen (Nin)
Organic Nitrogen (Orn)
Total Phosphorus (P)
Total Phosphate (P205)
Estimated Avail. P205
Total Potassium (K)
Total Potash (K20)
Arsenic (As)
Cadmium (Cd)
Chromium (Cr)
Copper (Cu) -
Lead (Pb)
Mercury (Hg)
Molybdenum (Mo)
Nickel (Ni)
Selenium (Se)
Zinc (Zn) .
Aluminum (AI)
Calcium (Ca)
Iron (Fe)
Sodium (Na)
Sulfur (S)
Magnesium (Mg)
Manganese (Mn)
Usage From 9/1/2019 To 12/31/2019
PPltll(mg/kg)
Lbs/DryTon
22301
44.601
22301
44.601
19361
38.721
60600
121.2
6880
11.76
<4.72
<0.009
64720
109.44
5960
11.92
13648.4
27.297
6864
13.708
727
1.464
872.4
1.745
<5
<0.01
<1
<0.002
118
0.236
413
0.826
4.56
0.009
0.0529
<0.001
2.78
0.006
32.2
0.064
<5
<0.01
854
1.708
3080
6.16
6140
10.28
7200
14.4
6400
12.8
24500
49
943
1.886
113
0.226
Percent Solids: 5.08 % . pH Level: 7.1
Calculations
PA-N (ppm) = [ (fl) (ppm Org. N) ] + [ (V1) (ppm Ammonia N) j + (ppm Nitrate N)
P x 2.3 = Total P205 Total P205 x .5 = Estimated available P205
K x-1.2 = K20
ppm or mg/kg x .002 = Ibs/dry ton
Biosolids/Residuals Application State: NORTH CAROLINA
Organic Nitrogen Mineralization Rate (fl): For AEROBICALLY DIGESTED 30.00%
Ammonia Nitrogen Non Volatilized Fraction (V1): For Injected:1.00
For Surface w/ Incorp.A.00 --
For Surface w/o Incorp.:0.50
NR = Data not Reported to Synagro or Data not Required
Notes: --
2105 01 TXLIQ — Control # 75959 12:51:34 11/27/2019

7621 Whitepine Road, Richmond, VA 23237
Main 904-743-9401 ° Fax [phone]
www.waypointanalytical.com
9/27/2019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical. Testing
Report Number: 19-262-001.6
Project Description: South Fork Industries
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/19/201.9 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performedasrequired by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the. USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be. analyzed within 16 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis: unless otherwise indicated. This report shall not be reproduced except in full, and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you.have any questions or need additional information.
Sincerely,
per• �. cjy�
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis.in question at laboratory's expense, or the refund of the charges paid for performance of said analysis..
Page 1 of .b

Wa­ypoint.
ANALYTICAL
AU Whitepine Road, Richmond, VA 23237
Main 804 743-9401 ° Fax [phone]
www.waypointanalytical:c(i m
Sample. Summary Table
Report dumber: 19-262-0016
Client Project Description: South Fork Industries
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
66268
south fork
Solids
09/17/2019 10:50
09/19/2019
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
SM-4500-NH3C
WTN
68268
south fork
Solids
09/1.712019 10:50
09/19/2019
9045D
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019,
4500NO3F-A11
IVTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
6010D
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
SW-7471B
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
SM-4500-NH3C-TKN
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
SM-254OG
WTN
­WTN, Waypoint Analytical - TN, Memphis, TN, Certification: #460181- Virginia- -
Page 2"6f 6

Report. Number;: 19-262-QQ16
Account Number: 46622
-Submitted By: Alex Fox
Send To: Synagro Central LM Technical
MaryBrewer
284 Boger Road
Mocksville , NC 27028
Lab Number 68268
:Sample Id'a south fork
Way I pointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804443-9401 ° Fax [phone]
www.waypointe nalytical.com
Project :.South Fork Industries
REPORT OF ANALYSIS
Date Sampled: 9/1:7/2019 10:50:00
Date Received: 09/19/2019 00:00
Date Reported:, 09/27/2019
`Total Solids"
5.08
ADM_
09/20/20 9 1638
Moisture *
94.90
ADM
09/20/2019 16:38
Total Kje.ldahi•Nitrogen
6.06
60600
250
JPJ
09/26/2019 13:00
'Phosphorus
0.00
5960
50,0
BKN
09/24/2099 21.42
,Potassium
0.07
727
50.0
BKN
09/24/2019 21:42
:Sulfur
2.45
-245.00
50.0
BKN
09/24/2019 21:42
Calcium
0.51
5.140
260
BKN
09124/2019 21:42
;Magnesium
0,09
943
50.0
BKN
09/24/2019. 21:42
Sodium
064
6400
.250
BKN
09/24/2019 21:42
Iron
7200.
%0
BKN
09/24/2019 21:42
Aluminum
3080
50.0
BKN
09/24/2019 21:49
,Manganese
113.
5.00
BKN
09/24/2019 21:42
Capper
413
2.50
BKN.
09/24/2019 21:42
Zinc
854
125
BKN
09/24/2019 21;42
Ammonia Nitrogen
0.59
5680
100
JPJ
09/26/2019 .13:00
Organic..N
6A7
54720
250
09126/201913:00
Nitrate+Nitrite=N
s4.72
4.72
ZBD
09124/2019 15 33
Ali values are on a dry weight basis except as noted by asterisk. Detection limit on all N'series is on a wet basis.
B.-; 'nalyte detected in blank
H -Beyond holding
time
Apj G
Oarreports and [Wters are_lor the.exclusive'and confidential use of our clients, and may not be reproduced in amole or°part; normay any reference be made
to the.work, thg resin s, or the company: in any advertising, news release: or other public announcements without obtaining our prior written authorization.
Page 3 of .6
SM-2540G
5M-254OG
SM-460.MH3C7TKN
60:10D
60101)
60101)
6010D
6.019D.
6010D
6010D
6010D
6010D
6010D
6010D
SM-:4500-NH3C
CALCULATION
450.0NO3F=2.011
Paudc McGroary
Agronomist
I
i

Report Number: 19-2,62-0016
, Accou nt-Number: 46622
.:Submitted*, By, Alex Fox
' Ser d. To Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville ; NC;27028
Waypoint,
ANALYTICAL
76211N41liepine 11oadr Richmond, VA 2323.7
Main 804-743;9401 U Fax [phone]
www.waypointa nalytical.com
Project,: South Fork Industries
REPOh'T OF'ANALYSIS Date sampled: 9/17/2019 1050:00
Lab Number: 68268 Date Received: 09/19/2019 00:00
Sample Id south.fork. Date Reported: 09/2712019.
Cadmium
Chromium
Nickel
Lead
Arsenic.
`Mercury.
Selenium
pH n.
:Molyb.denum
.Comments:
7.1
<1.OU
118
32,2
4.56'
< ,00
0.0529
<6, 00
2.78
1.00
BKN
09/24/2019 21:42
60.101)
2.50
BKN
09/24/2019 21:42
6610D
2:50
BKN
09/24/2019 2142
6010D
3100
BKN
09/24/2019 21:42
6010D
5.00
BKN
.09/24/2019 21:42
6010D
0,0151
TJS
09/241201913:41
SW-7471B
&00
BKN
0.9/24/2019 21 42
6010D
JSL
09/24/2019 06r50
90450
2.50
BKN
09/24/201:9 21:42
6010D
All Values are on. a dry weight basis.except as noted by asterisk. Detection limit on all N series is :on a wet basis.'
6::-:Analyte'detected Imblank H - Beyond holding time I G oo
cOurreports and letters are for the, exctu$[Ve. and confidential use of our cilent5, and:nlay not be reproduced in whole or part, nor -may any reference be made Pauric McGroary
to the:work, the results, or the company in any advertising, news release: or other public announcements nithout obtaining our priorwritten.authonzatimn' Agronomist
Page 4 of 6
0

a
s
7621 Whitepine Road, Richmond, VA 23237
Waypoi n Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number: 19-262-0016
Shipping Method
0. Fed. Ex 0 US Postal 0 Lab
® UPS 0.. Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
® Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
O' Yes
0 No Not Required
Custody seals intact on sample bottles?
0 Yes
0 No Not Required
Chain of Custody (COC) present?
I* Yes
0 No
COC agrees with sample label(s)?
0 Yes
a No
COC properly completed
® Yes
a No
Samples in proper containers?
is Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
9 Yes
0 No
All samples received within holding time?
® Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling.
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
O No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
NIA
Trip Blanks received with VOAs
0 Yes
0 No
® N/A
Soil VOA method 5036 — compliance criteria met
O Yes
G No
I N/A
r.._ High concentration container (48 hr)
Low concentration Encore samplers (48 hr)
F High concentration pre -weighed (methanol -14
d) F Low cone pre-weldhed
vials (Sod Bis -14-d)
Special precautions or instructions included?
0 Yes
No
Comments:
Signature Brandi Watson Date & Time I09/19/2019 13:40:02
Page 5 of 6

SAMPLING LOG #
CUSTOMER: SYNAGR®
� L®; II1� 1111�1Ullllillllllllk111�N�6Vllullllli� HAIN OF CUSir®DY
-'9RCR®� �e�
;�,EOULV echnical �
PROJECT MANAGER: K NIX
Synaaro Gen ra
Smith Focklndustnes
Wd sampling procedures
703
.7vu uurrrry me collection of these samples.
Phone:
4"
SAMPLEPI
A & L
CUSTOMER SAMPLING
SAMPLE
# OF
SAMPLING METHOD METHOD
LAB #
SAMPLE I.D. LOCATION
TYPE
CONTAINERS
DATE TIME PRESERVED SHIPPED
Sak7� j"t►rh{1/�
(
�
� n���� t�
_
� �D�.CO
7 rl _ U P<
Relinquished by Sampler: gate, e Recieved by: REMARKS:
J� Time
Relinquished by: Date Time Recieved by:
Relinquished by: Date Time Recieve by:
u alL�l�
SPECIAL INSTRUCTIONS:
1� For monitoring purposes. PO#:
i
SAMPLE
ANALYSIS REQUEST
i
1.D.
SLI
SL2
NH4 N
M03 N
Orgartie
N
Cd
Cr
Ni
Pb
As
H 9
Se
N H
CaCO3
equiV.
Volatile
Solids
Mo.
CI
NOZ N
kAA900W100or
'7Ll: Total Solids (Moisture), Total }Celdahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
Page 6 of 6

FIELD REPORT
SOUTH FORK INDUSTRIES, INC., NC Synagro Field: NC-CA-00006-0-0001
October 2019
Permit No.: WQ0006984 Latitude: 35.46'42"
County: CATAWBA Longitude: 81.16'42"
Crop: FESCUE PASTURE Acres: 16.8 (6.804 ha)
Rate: 216.00 LBS PAN/ACRE
Applic. Method: SURFACE APPL.
GALLONS APPLIED: Month to Date: 198,400.00 Year to Date:-198,400.00
DRY TONS/ACRE APPLIED: Month to Date: 2.50 Year to Date: 2.50
Cumulative: 15.39
********POUNDS PER ACRE APPLIED *******
( Kilograms per Hectare Applied )
PARAMETER
MONTH TO DATE
YEAR
TO DATE
CUMULATIVE
PAN
96.87
96.87
P
29.82
29.82
K
3.64
3.64
As
0.03
(0.03)
0.03
(0.03)
0.09
(0.10)
Cd
<.01
(<.01)
<.01
(<.01)
0.05
(0.06)
Cr
0.59
(0.66)
0.59
(0.66)
0.98
(1.10)
Cu
2.07
(2.32)
2.07
(2.32)
27.44
(30.73)
Pb
0.02
(0.02)
0.02
(0.02)
0.17
(0.19)
Hg-
<.01
(<.01)
<.01
(<.01)
0.01
(0.01)
Mo
0.01
(0.01)
0.01
(0.01)
0.14
(0.16)
Ni
0.16
(0.18)
0.16
(0.18)
0.82
(0.92)
Se
0.03
(0.03)
0.03
(0.03)
0.12
(0.13)
Zn
4.27
(4.18)
4.27
(4.78)
12.21
(13.68)
DAILY FIELD LOADING SHEET
DATE PCT. WEATHER
APPLIED TYPE SOLIDS AMOUNT UNIT DRY TONS CONDITIONS
10/04/2019 SFIMPTX! 5.08 198,400.00 GALLONS 42.03 FAIR
TOTALS: 198,400.00 GALLONS 42.03 DT
38.12 MT
"NR" = Data not reported to Synagro Technologies, Inc or Data not required.
SOIL RAINFALL
CONDITIONS PAST 24 Hr
DRY 0-<1/2"

FIELD REPORT
SOUTH FORK INDUSTRIES, INC., NC
October 2019
Permit No.: WQ0006984
County: CATAWBA
Crop: FESCUE PASTURE
Rate: 216.00 LBS PAN/ACRE
Applic. Method: SURFACE APPL.
Synagro Field: NC-CA-00006-0-0002
Latitude: 35.36'39"
Longitude: 81.17'07"
Acres: 13.3 (5.387 ha)
GALLONS APPLIED: Month to Date: 161,200.00 Year to Date:
DRY TONS/ACRE APPLIED: Month to Date: 2.57 Year to Date:
Cumulative:
********POUNDS PER ACRE APPLIED *******
( Kilograms per Hectare Applied }
161,200.00
2.57
18.21
PARAMETER
MONTH TO DATE
YEAR
TO DATE
CUMULATIVE
PAN
99.42
99.42
P.
30.60
30.60
K
3.73
3.73
As
0.03
(0.03)
0.03
(0.03)
0.11
(0.12)
Cd
<.01
(<.01)
<.01
(<.01)
0.06
(0.07)
Cr
0.61
(0.68)
0.61
(0.68)
1.11
(1.24)
Cu
2.12
(2.37)
2.12
(2.37)
31.11
(34,84)
Pb
0.02
(0.02)
0.02
(0.02)
0.20
(0.22)
Hg
<.01
(<.01)
<.01
(<.01)
0.01
(0.01)
Mo
0.01
(0.01)
0.01
(0.01)
0.17
(0.19)
Ni
0.17
(0.19)
0.17
(0.19)
0.98
(1.10)
Se
0.03
(0.03)
0.03
(0.03)
0.13
(0.15)
Zn
4.39
(4.92)
4.39
(4.92)
12.87
(14.41)
DAILY FIELD LOADING SHEET
DATE PCT. WEATHER
APPLIED TYPE SOLIDS AMOUNT UNIT DRYTONS CONDITIONS
10/07/2019 SFIMPTXL 5.08 161,200.00. GALLONS 34.15 FAIR
TOTALS: 161,200.00 GALLONS 34.15 DT
30.97 MT
"NR" = Data not reported to Synagro Technologies, Inc or Data not required.
SOIL RAINFALL
CONDITIONS PAST 24 Hr
DRY 0-<1/2"

FIELD REPORT
SOUTH FORK INDUSTRIES, INC., NC
October 2019
Permit No.: WQ0006984
County: LINCOLN
Crop: FESCUE PASTURE
Rate: 216.00 LBS PAN/ACRE
Applic. Method: SURFACE APPL.
Synagro Field: NC-LT-00035-0-0001
Latitude: 35.32'54"
Longitude: 81.18' 1.3"
Acres: 35.4 (14.337 ha)
GALLONS APPLIED: Month to Date: 502,200.00 Year to Date: 502,200.00
DRY TONS/ACRE APPLIED: Month to Date: 3.01 Year to Date: 3.01
Cumulative: 7.98
********POUNDS PER ACRE APPLIED *******
( Kilograms per Hectare Applied }
PARAMETER
MONTH TO DATE
YEAR
TO DATE
CUMULATIVE
PAN
116.37
116.37
P
35.82
.35.82
K
4.37
4.37
AS
0.03
(0.03)
0.03
(0.03)
0.06
(0.07)
Cd
<.01
(<.01)
<.01
(<.01)
0.02
(0.02)
Cr
0.71
(0.80)
0.71
(0:80)
0.89
(1.00)
Cu
2.48
(2.78)
2.48
(2.78)
16.19
(18.13)
Pb
0.03
(0.03)
0.03
(0.03)
0.10
(0.11)
Hg
<.01
(<.01)
<.01
(<.01)-
<.01
(<.01)
Mo
0.02
(0.02)
0.02
(0.02)
0.07
(0.08)
Ni
0.19
(0.21)
0.19
(0.21)
0.56
(0.63)
Se
0.03
(0.03)
0.03
(0.03)
0.05
(0.06)
Zn
5.13
(5.75)
5.13
(5.75)
8.19
(9.17)
DATE
PCT.
APPLIED
TYPE
SOLIDS
10/01/2019
SFIMPTXL
5.08
10/02/2019
SFIMPTXL
5.08
10/03/2019
SFIMPTXL
5.08
TOTALS:
DAILY FIELD LOADING SHEET
WEATHER
AMOUNT
UNIT
DRY TONS
CONDITIONS
124,000.00
GALLONS
26.27
FAIR
186,000.00
GALLONS
39.40
FAIR
192,200.00
GALLONS
40.71
FAIR.
502,200.00
GALLONS
106.38 DT
96.49 MT
"NR" = Data not reported to Synagro Technologies, Inc or Data not required.
SOIL
RAINFALL
CONDITIONS
PAST 24 H[
DRY
0-<1/2"
DRY
0-<1/2"
DRY
0-<1/2"

ComnlianceJnsnection Report
Permit: WO0006984 Effective: 02/16/15 Expiration: 04/30/18 Owner : Delta Apparel Inc
SOC: Effective: Expiration: Facility: Maiden, NC Plant Residuals Land Application Progrs
County: Catawba PO Box 37
Region: Mooresville
Maiden NC 286500037
Contact Person: Marshall Puryear Title: Phone: [phone] Ext.17
Directions to Facility:
System Classifications: LA,
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 03/07/2017 Entry Time: 11:30AM
Primary Inspector: Edward Watson
Secondary Inspector(s):
Certification:
Reason for Inspection: Routine
Permit Inspection Type: Land Application of Residual Solids (503)
Facility Status: Compliant Not Compliant
Question Areas:
Miscellaneous Questions Record Keeping
(See attachment summary)
Phone:
Exit Time: 01:OOPM
Phone:
Inspection Type: Annual Report Review
0 Sampling
Page: 1

pertnit: WQ0006984 Owner - Facility: Delta Apparel Inc
Inspection Date: 03107/2017 Inspection Type: Annual Report Review Reason for Visit: Routine
Inspection Summary:
This is for the purpose of Annaul Review only. The report is complete and appears to be in compliance with the permit.
Page: 2

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Permit: WO0006984 Owner -Facility: Delta Apparel Inc
Inspection Date: 03/07/2017 Inspection Type : Annual Report Review
Type
Distribution and Marketing
Land Application
Reason for Visit: Routine
Yes No NA NE
Page: 4

Compliance Inspection Report
Permit: WQ0006984 Effective: 02/16/15 Expiration: 04/30/18 Owner: Delta Apparel Inc
SOC: Effective: Expiration: Facility: South Fork Industries, Inc.
535 Elm Grove Rd
County: Lincoln
Region: Mooresville
Maiden NC 286500037
Contact Person: Marshall Puryear Title: Phone: [phone] Ext.17
Directions to Facility:
System Classifications: LA,
Primary ORC: Robert Michael Cox
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 01/23/2017
Primary Inspector: Edward Watson
Secondary Inspector(s):
Certification: 13191 Phone: [phone]
Entry Time: 10:30AM Exit Time: 11:45AM
Phone:
Reason for Inspection: Routine . Inspection Type: Compliance Evaluation
Permit Inspection Type: Land Application of Residual.Solids (503)
Facility Status: Compliant Not Compliant
Question Areas:
Miscellaneous Questions Record Keeping Treatment
Sampling Pathogen and Vector Attraction Storage
Transport
(See attachment summary)
0
Page: 1

Permit: W00006984 Owner - Facility: Delta Apparel Inc
Inspection Date: 01/23/2017 Inspection Type: Compliance Evaluation Reason for visit: Routine
Temperature corrected ❑
d. Salmonella (Class A, all test must be < 3MPN/4 gram day) ❑ ❑ M ❑
e. Time/Temp on: ❑ ❑ M ❑
Digester (MCRT) ❑
Compost ❑
Class A lime stabilization ❑
f. Volatile Solids Calculations ❑ ❑ M ❑
g. Bench -top Aerobic/Anaerobic digestion results ❑ ❑ M ❑
Comment: This is an industrial facility and has a 503 Exempt Permit.
Treatment
Yes No NA NE
Check all that apply
Aerobic Digestion
Anaerobic Digestion
❑
Alkaline Pasteurization (Class A)
❑
Alkaline Stabilization (Class B)
❑
Compost
❑
Drying Beds
❑
Other
❑
Comment: Treatment is by aeration.
Sampling Yes No NA NE
Describe sampling:
Samples are collected prior to land application. Anaylsis is performed by an offsite certified laboratory.
Is sampling adequate? ■ ❑ ❑ ❑
Is sampling representative? M ❑ ❑ ❑
Comment: Samples are collected at the effluent pipe These are grab samples
Transport Yes No NA NE
Is a copy of the permit in the transport vehicle? ❑ ❑ ❑ 0
Is a copy of the spill control plan in the vehicle? ❑ ❑ ❑
Is the spill control plan satisfactory? ❑ ❑ ❑
Does transport vehicle appear to be maintained? ❑ ❑ ❑
Comment: The facility is not expected to land apply this year. All previous transportation records were
removed when Delta sold the facility.
Page: 4

610 E Center Ave, Mooresville, NC to 610 E Center Ave, Mooresville, NC - Google Maps
610 E Center Ave, Mooresville, NC to 610 Drive 85.3 miles,1 h 58 min
E Center Ave, Mooresville, NC
Map data ©2016 Google 2 mi s
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Mooresville, NC 28115
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PAT MCCRORY
Goveivor
o
WaterResources
ENVIRONMENTAL DUALITY
May 12, 2016
Mr. Steve Slaughter, Plant Manager
Delta Apparel, Inc.
Post Office Box 37
Maiden, North Carolina 28650
DONALD R. VAN DER VAART
Secretmy
S. JAY ZIMMERMAN
Director
Subject: Non -Discharge Permit Inspection and
Acknowledgement of Receipt of the 2015.Annual Report
Delta Apparel, Inc. - Permit No.: WQ0006984
Land Application of Residuals (503 Exempt)
Catawba County
Dear Mr. Slaughter:
Enclosed you will find the report for the compliance inspection conducted on April 7th
2016 for the. referenced permit. The 2015 Annual Report was received and. reviewed
on -site March 8th, 2016. The report indicated there was no land application under this
permit in 2015.
I would like to thank Wayne Kelly for his time during the inspection. There were a
couple if issues noted to maintain overall compliance:
• Synagro had recently been land applying, so the lagoon level had been lowered
and appeared to meet the 2ft of freeboard requirement; however, there was
visual evidence that residual levels were within 2ft of freeboard and close to the
lagoon berm at creek -side. Please note that at least 2ft of freeboard is required
from the lowest point of the lagoon and a gauge level with inch or tenths of a
foot increments is likely to be required with permit renewal.
• The permit expiration date is April 30, 2018. A renewal application is due 180
days prior to expiration.
The report should be self-explanatory; however, I may be reached by phone (704-235-
2184) or email (maria.schuftba-ncdenr.gov) with questions.
Sincerely,
Maria Schulte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
State of North Carolina I Environmental Quality 1 Water Resources I Water Quality Regional Operations
Mooresville Regional Office) 610 East Center Avenue, Suite 3011 Mooresville, North Carolina 28115
704 663 1699

A
Attachment: W00006984 Inspection Report & ORE form
CC: Wayne Kelly, WWTP ORC (email)
Marshall Puryear, Synagro (email)
Kipp Glazier, CO-LAU (email)

State of North Carolina Department of Environmental Quality
Division of Water Resources
Pat McCrory, Governor
Donald R. van der Vaart, Secretary
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
Owner: Delta Apparel
Permit #: W00006994
Permittee Contact: Steve Slaughter
WWTP Contact: Wayne Kelly WWTP ORQ
LA ORC Name: Robert M. (Mike) Cox #13191
LA BU ORC: Marshall Puryear #904465
County: Catawba
Issued:02/15/2016 Expiration:04/30/2018
Telephone No.: 828-428-9921
Telephone No.: 828-428-9921 ext. 290
Telephone No.: 704-718-2804
Telephone No.: 434-738-8002
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of Inspection
Collection System Spray Irrigation X Sludge Other
Inspection Date(s): April 7, 2016
Inspection Summary: (additional comments may be included on attached pages)
This inspection included site visits to the facility and a recent land application at fields: NC-CA-06-02 & 03.
Please note:
• The sludge storage lagoon needs better monitoring for freeboard water levels, as noted in the
cover letter.
• The MRO should be informed of any changes to the contact information noted above.
Is a follow-up inspection necessary _yes X no?
Inspector Name/Title: Maria Schutte, Environmental Specialist; Edward Watson - Hydro eolo ist
Telephone No.: 704-663-1699 Fax No. 704-663-6040
Date of Inspection: 04/06/2016

Residuals Inspection
WQ0006984 Delta Apparel — Catawba County
pg. 2
Type of Residual
X Land Application (class B) Distribution and Marketing (class A)
Record Keeping
Y-yes N-no N/A -not applicable N/E-not evaluated
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
Y TCLP analysis, NE SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y Hauling records (# gal and/or ton hauled during calendar year to date)
NE Field loading records, Y Field site maps and information
NA Records of lime purchased
NA Pathogen & Vector Attraction Reduction
Comments: There was no land application in 2015, so soils and fleld information was not examined. A recent
geld application site was visited as part of this inspection — see the comments under fields below. The most
recent records available were reviewed on -site.
Pathogen & Vector Attraction Reduction WVAR) records
Comments: Not applicable — This facility is 503 exempt, as they only process industrial wastewater.
Treatment
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime Other -describe
Comments: Per previous inspections, the storage lagoon has never had a -freeboard marker. as thev utilize a
weir and plumbing which returns any overtlow to the head of the plant; however, it has been assumed that the
lagoon berms were o fequal elevation, but during this visit it was observed that the berm at creek -side appears to
be a low point from evidence of water level/residuals staining within the 2 eet of required free board. As noted
in the cover letter, this will most likely require the installation of an appropriate water level gauge during the
next permit renewal.
Storage
Number of days/weeks/months of storage: Per prior inspections, approximately 1yr. Delta Apparel did not
land apply in 2015, but evidence of reduced free -board in the lagoon(s), shows they may have held residuals for
too long; and, a yearly event may be necessary to maintain the 2 foot freeboard requirement.,
Describe storage: StoryZe is a IMG clay -lined lagoon at the WWTP.
Odors present Y Vectors present N
Transport Recent LA activity had been halted due to rain. The application/transport vehicle was on -site at
the time of inspection, mixing the lagoon. Odors were stronger than noted during past inspections.
Spill control plan in transport vehicle? Y
Does transport vehicle appear to be maintained? Y
Condition of land application equipment on site: NA- same equipment for hauling see above.

Residuals Inspection -
` WQ0006984 Delta Apparel — Catawba County
pg. 3
Sampling
Describe Sampling: Residuals sampling is handled by SYNAGRO in accordance with the permit requirements.
Is sampling adequate? NE Is. sampling representative? NE * Sampling should be' ade irate if the instructions
noted in the "Sampling Plan" are followed
Field Sites (end use for class B biosolids) Land application activity was halted due to recent rain. Fields —
NC-CA-06-02 & 03 was visited as part of this inspection.
Field identification: NC-CA-06-02&03
Y Permit on site during application
Y Buffers adequate
N Documented exceedances of PAN limits
N Signs of runoff / ponding
Y Spill plan on site
Y Cover crop specified in permit
Y Site condition adequate
Y Rain Gauge on site during application
Are there any limiting slopes on fields?
Y 10 % for surface application NA 18% for subsurface application
* Comment: Ed Waston (DWR) noted to Mike Cox there was increasing erosion (>2ft vertical ledge) around
the on -site pond that may require extension of the buffer during future applications.
Odors/vectors
Describe any nuisance conditions and any corrective actions needed. NA
Odors present Y, minor — not as bad as at the plant.
Vectors present N
Monitoring well(s) Y/N: NA
If yes, location of well(s):
Comment: This permit currently does not require groundwater monitoring. Per previous inspection
resorts: Monitoring wells are located on fields owned by Delta. Ground water monitoring wells are no longer
required to be sampled; however, the permit (issued 10-23-97) states that the wells are not to be abandoned.
Other noted conditions

Schutte, Maria
From: Marshall Puryear <[e-mail]>
Sent: Monday, March 28, 2016 3:00 PM
To: Schutte, Maria
Subject: Delta apparel
Maria, Synagro plans on starting Delta Apparel on Wednesday March 30th at NC LT 120 Wayne Gilbert farm and then
moving to NC CA 06 Dennis Lutz.
Thanks
Marshall
IJ
Your Partner for a cleaner, greener world
Marshall Puryear
Technical Services Manager
284 Boger Road Mocksville, NC 27028
0: 1-336-998-7150 x 17 1 M: 1-434-738-8002
[e-mail] I www.synagro.com
Facebook I Twitter I Linkedin

A
IF
F�LE
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory John E. Skvarla,
Governor Secretary
une 4, 2014
Mr. Steve Slaughter, Plant Manager
Delta Apparel, Inc.
P.O. Box 37
Maiden, North Carolina 28650
Subject: Non -Discharge Permit Inspection
Delta Apparel, Inc. - Permit No.: W00006984
Land Application of Residuals (503 Exempt)
Catawba County
Dear Mr. Slaughter:
The Mooresville Regional Office (MRO) received a complaint on May 6th, 2014, from
Candy Houser, concerning odors from a land application event near her residence. Per
conversation(s) with Ms. Houser, she wishes to revoke the set -back waiver for field
NC-LT-120-01 signed by her husband, Danny Houser. The MRO conducted a field
inspection on May 7t. , 2014. There was no active land application at the time of
inspection.
Field conditions noted at time of inspection:
Y-yes N-no NE -not evaluated NA -not applicable
Y Buffers adequate NE Permit/spill plan on site during application
Y Site condition adequate Y Cover crop specified in permit
N Signs of runoff / ponding NE Rain gauge on site during application
Are there any limiting slopes on fields?
N 10 % for surface application NA 18% for subsurface application
Odors present: Minimal odors were detected.
Vectors present: No vectors were detected.
Comments: The field application was typical. Buffer flags were visible and agree with the
application map. This inspection finds that field compliance has been met for the subject
permit. The MRO noted that there is open space between the land application field and
the Houser residence, with no vegetative buffer for odors should prevailing winds blow
toward their residence.
Mooresville Regional Office, 610 East Center Avenue, Mooresville, North Carolina 28155
Phone: [phone] Internet: www.ncdenr.gov
An Equal Opportunity %Affirmative Action Employer— Made in part by recycled paper

The MRO has already discussed this complaint/inspection with your land application
contractor, SYNAGRO; and, their staff is aware of the required buffer change for future
events on this field. The MRO requests that an updated map depicting the 400 foot
buffer around the Houser residence be sent to my email address below.
I may be reached by phone at [phone] or email (maria.schutte(a-ncdenr.gov)
should you-have-an---y-questions.—
Sincerely,
Maria Schulte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
CC: Wayne Kelly, WWTP ORC (email)
Marshall Puryear, Synagro (email)
Eric Thompson, Synagro (email)
Ed Hardee, LAU Compliance, CO -Raleigh (email)

AGZA. - FILE
HCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Resources
Pat McCrory Thomas A. Reeder John Skvarla
Governor Director Secretary
January 31, 2014
Mr. Steve Slaughter, Plant Manager
Delta Apparel, Inc.
Post Office Box 37
Maiden, North Carolina 28650
Subject: Non -Discharge Permit Inspection
Delta Apparel, Inc. - Permit No.: WQ0006984
Land Application of Residuals (503 Exempt)
Catawba County
Dear Mr. Slaughter:
Enclosed you will find the report for the compliance inspection that was conducted on
January 9th, 2014. The inspection included the WWTP residuals processing and storage, and a
records review. The Mooresville Regional Office (MRO) would like to thank Wayne Kelly (WWTP
ORC) for his time and the tour of the WWTP facility.
The residuals processing and storage areas were free of odors and vectors at the time of
inspection, and the entire WWTP facility appeared well maintained. Most records and data were
available for review; however, there are a couple of data issues to address to maintain overall
compliance with the conditions of your permit.
The Sodium Absorption Rate (SAR) calculation is routinely high for this facility, which
requires further assessment per permit condition 11.10. Our records show this issue was
addressed in 2004, via a letter from Eric Thompson, a licensed soil scientist and employee at
SYNAGRO, your land application subcontractor. The MRO believes this issue should be re-
examined and recommends you again seek the advice and expertise of Mr. Thompson
regarding any potential impact to your permitted fields.
A copy of the most recent TCLP results was unavailable for review at the time of
inspection. This issue is just mentioned as a reminder for future inspections, as Mr. Kelly
did offer to obtain a copy from your subcontractor, SYNAGRO. The MRO is aware that
sampling and land application of residuals is handled by SYNAGRO, but recommends you
ensure you are receiving and reviewing results for potential issues to remain compliant with
permit requirements.
• Please note your permit expiration date is April 30, 2018.
Division of Water Resources / Water Quality Regional Operations Section / Mooresville Regional Office - 1�71�
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115 One
1� olrtll�arolina
Phone: [phone] Fax: [phone] i Customer Service: 1-877-623-6748
Internet: www.ncwater.org
An Equal Opportunity 1 Affirmative Action Employer

The attached report should be self-explanatory; however, if you have any questions
concerning this report, I may be reached at [phone].
Sincerely,
Maria Schutte
Environmental Specialist
cc: Wayne Kelly, WWTP ORC (email)
Eric Thompson, Synagro (email)
Chonticha McDaniel, Residuals Management, CO-LAU (email)

le
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Resources
Pat McCrory, Governor
John Skvarla, Secretary
Thomas A. Reeder, Director
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
. GENERAL INFORMATION
City/Town/Owner: Delta Apparel County: Catawba
Permit No.: W00006984 Issued: 05/01/2009 Expiration: 04/30/2018
Permittee Contact: Steve Slaughter Telephone No.: 828-428-9921
ORC Name: Wayne Kelly WWTPO Telephone No.: 828-428-9921 ext. 290
LA Contractor: Eric Thompson(SYNAGRO) Telephone No.: 336-971-9085
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Date(s): December 5, 2013
Inspection Summary: (additional comments may be included on attached pages)
This inspection covers permit #WQ0003902 (Class B - 503 Exempt), and included a records review, and
residuals handling and storage at the Delta Apparel WWTP.
The residuals processing and storage areas were free of odors and vectors at the time of inspection, and the
WWTP facility appeared well maintained. The cover letter noted some data issues to be addressed. The
Sodium Absorption Ratio (SAR) is of primary concern.
The current permit will expire on 04/30/18. A renewal application is due 180 days prior to expiration.
Is a follow-up inspection necessary _yes X no
Inspector(s): _Maria Schulte - Environmental Specialist
Telephone No.: 704-663-1699 Fax No.: 704-663-6040
Date of Inspection: January 9t`, 2014

Residuals Inspection
WQ0006984 Delta apparel
Pg 2
Type of Residual
X Land Application (class B)
Record Keepin�
Y-yes N-no NE -not evaluated
NA -not applicable
Distribution and Marketing (class A)
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
N TCLP analysis, * Y SSFA (Standard Soil Fertility Analysis).
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD
N Hauling records (# gal and/or ton hauled during calendar year to date)
* Y Field loading records, * Y Field site maps and information
NA Records of lime purchased
NA Pathogen & Vector Attraction Reduction
* Comments: Soil analyses and field loading sheets were reviewed in the 2012 Annual Report and were not
requested for review during- this inspection The most recent TCLP results from 2013 were not available on
site, but Mr. Kelly offered to obtain them form SYNAGRO The MRO did not see that as necessary at this time
as the 2013 AR will be arriving shortly, but recommends that Delta ensure data is received and reviewed in the
future to maintain compliance with permit conditions
Pathoun & Vector Attraction Reduction records
Comments: Not applicable — This facility is 503 exempt, as they only process industrial wastewater.
Treatment
X Aerobic digestion Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime Other -describe
Comments: Storage lagoon has never had a freeboard marker, as they utilize a weir and plumbing which
returns any overflow to the head of the plant.
Transport No land application was taking place at the time of inspection
Spill control plan in transport vehicle? NE
Does transport vehicle appear to be maintained? NE
Storage
Number of days/weeks/months of storage: Lagoon can hold residuals for approximatelyyear
Describe storage: The Delta WWTP has a 1 MG storage lagoon.
Odors present N
Comments:
Vectors present N

.'
Residuals Inspection
WQ0006984 Delta apparel
pg 3
Sampling
Describe Sampling: Residuals sampling is handled by SYNAGRO in accordance with the permit
requirements.
Is sampling adequate? NE Is sampling representative? NE
Field Sites (end use for class B biosolids) No land application was takingplace during this inspection.
Field identification:
Permit on site during application Spill plan on site
Buffers adequate Cover crop specified in permit
Documented exceedances of PAN limits Site condition adequate
Signs of runoff / ponding Rain Gauge on site during application
Are there any limiting slopes on fields?
10 % for surface application 18% for subsurface application
* Comment:
Monitoring well(s) Y/N: Y
If yes, location of well(s):
Comment: Monitoring wells are located on fields owned by Delta. Per the last inspection report, ground water
monitoring wells are no longer required to be sampled; however, the permit (issued 10-23-97) states that the
wells are not to be abandoned.
Odors/vectors
Describe any nuisance conditions and any corrective actions needed. NA
Odors present N
Vectors present N
Other noted conditions

4
Zvi IN A ; ER
0FILE
Beverly caves Purdue, Governor
Dee Freeman, Secretary
Department Environment and Natural Resources
J [
North Carolina of
-I
Coleen H. Sullins, Director
Division of Water Quality
AQUIFER PROTECTION SECTION
September 21, 2011
Mr. Gene Hudgens, Plant Manager
Delta Apparel, Inc.
Post Office Box 37
Maiden, NC 28650
Subject: Permit No. WQ0006984
Land Application Inspection
Catawba County
Dear Mr. Hudgens:
Enclosed is the land application inspection report conducted on September 9, 2011. This
inspection evaluated the sludge lagoon, the current analytical data, and the 2010 annual report for the
Land Application Program for Delta Apparel and was found compliant.
Please note that in 2009, North Carolina enacted SL 2009-406 and in 2010, North Carolina
enacted 2010-177. Both laws extended coverage of certain government permits and approvals that are
current and valid at any point between Jan. 1, 2008 and Dec. 31, 2010 under Chapter 23, Article 21 of
the North Carolina General Statutes. With the passing of the above State Laws, Vour permit has been
extended to April 30, 2017.
The report should be self-explanatory; however, if you have any questions, please contact me at
704-235-2186.
Sincerely,
Ellen Huffman,
Environmental Specialist
Mooresville Region
Attachment
cc: Central Files
Jackie Harvell, Maintenance Supervisor, Delta Apparel, Inc.
Scott Berg, SYNAGRO
MRO
One
Division of Water Quality / Aquifer Protection Section / Mooresville Regional Office Phone: [phone] Fax: [phone] NorthCaroHna
610 East Center Avenue, Suite 301, Mooresville, NC 28115 Customer Service 1-877-623-6748 Internet: wNw.ncwaterquality.orq Natimallf

40
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Beverly Eaves Purdue, Governor
Dee. Freeman, Secretary
Coleen Sullins, Director
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Delta Apparel
Permit No.: WQ0006984
Expiration Date: April 14, 2014
Permittee Contact: Jackie Harvell
ORC Name: Wayne Kelly, WWTPO
Reason for Inspection
County: Catawba
Issuance Date: May 1, 2009
Extended exp. Date April 30, 2017*
Telephone No.: 828/428-9921 ext.290
Telephone No.: same
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summar9r:
*In 2009, North Carolina enacted SL 2009-406and in 2010, North Carolina enacted 2010-177.
Both laws extended coverage of certain government permits and approvals that are current
and valid at any point between Jan. 1, 2008 and Dec. 31, 2010 under Chapter 23, Article 21 of
the North Carolina General Statutes. Please note that with the passing of the above State
Laws, your permit was extended to April 30, 2017.
A field visit to the latest land application event was performed in April 2011. Field conditions
were found compliant. SYNAGRO is the current land application contractor. The wastewater
ORC was on vacation at the time of inspection. Review of the 2010 annual report & current
laboratory data submitted by email from the contractor, reflects compliance with the land
application permit. The MRO has not received any odor complaints this year.
Is a follow-up inspection necessary yes X no
Inspector Ellen. Huffman / Env. Specialist
Telephone No. 704/235-2186 Fax No. 704/663-6040 email: ellen.huffman(a)_ncdenr.gov
Date of Inspection September 9, 2011

Residuals Inspection
Sept. 9, 2011
Delta Apparel WQ0006984
pg2of3
Type of Residual
X Land Application (class B) Distribution and Marketing (class A)
Y-yes N-no N/A -not applicable N/E-not evaluated
Record Keeping
N/E Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
N/E TCLP analysis Y SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals
Y Hauling records
Y Field loading records Y Field site maps and information
N/A Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Treatment (check treatment type(s) used)
X Aerobic digestion
Transport No land application activity at time of inspection.
Permit in transport vehicle? Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Storage
Number of days/weeks/months storage 12 months
Describe storage: aerated sludge lagoon.
Spill control plan on storage site? Yes No N/A X
X Lagoon- Is lagoon lined X(clay)
Sampling
Is sampling adequate? Y Is sampling representative? Y
Monitoring well(s) Y/N: Y
If yes, location of well(s) see comment below.
Comment: Ground water monitoring wells are no longer required to be sampled; however,
the permit (issued 10-23-97) states that the wells are not to be abandoned.

a
Residuals Inspection pg 3 of 3
Delta Apparel WQ0006984
Field Sites (end use for class B biosolids)
No land application activity at time of inspection. A field inspection was
performed in April 2011. Site conditions reflect compliances
Y Permit on site during application Y Spill plan on site
Y Buffers adequate Y Cover crop specified in permit
N/E Documented exceedances of PAN limits Y Site condition adequate
N Signs of runoff / ponding _ (if no, improvements
recommended) N/E Rain Gauge on site during application
Odors/vectors
Odors present
Vectors present
Describe any nuisance conditions and any corrective actions needed

JUN-09-2010 11:30 From:
To:17046636040 P.1/1
June 9, 2010
MEMORANDUM
TO: Ellen Huffman, NCDENR-MRO
FROM: Scott Berg, Technical Services Manager
RE: Land Application of 13iosolids in Catawba Conty
Please consider this a fonnal notification of Synagro's plans to land apply residuals from the
Delta Apparel WWTP (Maiden, NC) to sites owned by Clay Neil, Harold Sherrill, Tim
Hefner and Mika Sigmmon. This will be the first land application event to these fams, since
the land was added to the program as of 06/03/2010.
This notification is in accordance with the Delta Apparel Inc. Residual Solids Permit No.
WQ0006984, issued by NC DENR/DWQ. Section I.10. states "...the appropriate local
governmental official (i.e., county manager) shall be notified at least 24 hours prior to the
initial residuals land application event on any new site so that they will be aware that
residuals land application activities have commenced on the site".
Please call me at [phone] ext. 13 if you have any questions or need any additional
information.
Thanks.

r
F W ATF
Beverly Eaves Purdue, Governor
Dee Freeman, Secretary
r North Carolina Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
AQUIFER PROTECTION SECTION
December 15, 2009
Mr. Gene Hudgens, Plant Manager
Delta Apparel, Inc.
Post Office Box 37
Maiden, NC 28650
Subject: Permit No. W00006984
Land Application Inspection
Catawba County
Dear Mr. Hudgens:
Enclosed is the land application inspection report conducted on December 11, 2009. This
inspection evaluated the sludge lagoon, the current analytical data, and the 2008 annual report for the
Land Application Program for Delta Apparel.
A file review of the 2008 annual report reflects compliance. All necessary records were available
at the time of this inspection and reflect compliance. Inspection of the lagoon found one small area of
erosion on the creek side of the lagoon berm that needs to be filled in.
The report should be self-explanatory; however, if you have any questions, please contact me at
704-235-2186.
Sincerely,
p
Ellen Huffman, /l/
Environmental Specialist
Mooresville Region
Attachment
cc: Central Files
Jackie Harvell, Maintenance Supervisor, Delta Apparel, Inc.
One
Division of Water Quality / Aquifer Protection Section / Mooresville Regional Office Phone: [phone] Fax: [phone] NoTthcarolina
610 East Center Avenue, Suite 301, Mooresville, NC 28115 Customer Service 1-877-623-6748 Internet: www.ncwateroualit--. - d►'uwnally

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Beverly Eaves Purdue, Governor
Dee Freeman, Secretary
Coleen Sullins, Director
/ •
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Delta Apparel
Permit No.: WQ0006984
Last Amended Date: N/A
If applicable SOC Issuance Date: N/A
Permittee Contact: Jackie Harvell
ORC Name: Wayne Kelly, WWTPO
Reason for Inspection
County: Catawba
Issuance Date: May 1, 2009
Expiration Date: April 14, 2014
Expiration Date: N/A
Telephone No.: 828/428-9921 ext.290
Telephone No.: same
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
Delta Apparel, Inc. (formally Delta Mills) land applies sludge generated from the industrial
wastewater treatment plant. A field visit to the latest land application event was performed in
July 2009. No more land application is expected until next year. SYNAGRO is the current land
application contractor. Review of the 2008 annual report & current laboratory data reflected
compliance with the land application permit. There have been no odor complaints for 2009.
Inspection of the lagoon found one small area of erosion on the creek side of the lagoon berm
that needs to be filled in.
Is a follow-up inspection necessary _yes X no
Inspector(s) Name(s)/Title(s) Ellen Huffman / Env. Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection December 11, 2009

Residuals Inspection
Delta Apparel WQ0006984
Type of Residual
X Land Application (class B)
Record Keeping
Y/N
Distribution and Marketing (class A)
Pg 2
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
N/E TCLP analysis Y SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y Hauling records (# gal. and/or tons hauled during calendar year to date)
Y Field loading records Y Field site maps and information
N/E Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Treatment (check treatment type(s) used)
X Aerobic digestion
Transport No land application activity at time of inspection.
Permit in transport vehicle? Spill control plan in transport vehicle?
Does transport vehicle appear to be maintained?
Operation & Maintenance records No land application activity at time of inspection.
Condition of land application equipment on site
Stogy
Number of days/weeks/months storage 12 months
Describe storage: aerated sludge lagoon.
Spill control plan on storage site? Yes No N/A-. X
X Lagoon - Is lagoon lined X cla
Sampling
Is sampling adequate? Y Is sampling representative? Y
Monitoring wells) Y/N: Y
If yes, location of well(s) see comment below.
Comment: Ground water monitoring_ wells are no longer required to be sampled; however, the permit
(issued 10-23-97) states that the wells are not to be abandoned.

It -
Residuals Inspection Check List pg 3
Delta Apparel WQ0006984
Field Sites (end use for class B biosolids)
No land application activity at time of inspection.
Permit on site during application Spill plan on site
Buffers adequate Cover crop specified in permit
Documented exceedances of PAN limits Site condition adequate
Signs of runoff / ponding (if no, improvements recommended)
Rain Gauge on site during application
Odors/vectors No land application activity at time of inspection.
Odors present
Vectors present
.Describe any nuisance conditions and any corrective actions needed

0Ef_Ci10H uL
06 J H 2 0 PM 4: (2
CERTIFIED MAIL RETURN RECEIPT REQUESTED
Public Utilities
January 12, 2006
Ms. Shannon Mohr Thornburg, Environmental Engineer II
NCDENR-DWQ
Land Application Unit/Aquifer Protection Section
1636 Mail Service Center
Raleigh, NC 27699-1636
Cily of Hickory
Post Office Box 398
Hickory, NC 28W3-0398
Phone: [phone]
Fax: [phone]
email: kgnee►(a dhickory.mus
U lJ ll FE
JA N 2 6 2006
NC DENR MRO
DWQ - Aquifer Protection
SUBJECT: Response to Notice of Violation No. Nov-2006-SP-0001
Permit No. WQ0004563
City of Hickory, Catawba County
Hickory Regional Compost Facility & Catawba "ORGRO" Distribution Program
Dear Ms. Thornburg:
The purpose of this correspondence is to respond to your letter received January 10, 2006
reference a Notice of Violation at the Hickory Regional Compost Facility. The responses below
are formatted to match the order of reasons for non-compliance as documented in your letter for
simplicity of referencing. Responses are as follows:
1) The Hickory Water Treatment Facility is an approved residuals source generating facility
to deliver and discharge at the Hickory Regional Compost Facility; however, this is the
emergency backup plan in the event we cannot dispose of in the normal fashion.
Throughout the year 2004 the Hickory Water Treatment Facility did not discharge any
residuals at the Hickory Regional Compost Facility; therefore, there was no activity to
monitor or record. All residuals discharged at the facility are logged, recorded and
reported. To avoid future confusion, we are modifying record keeping documents to
reflect the Hickory WTP as a potential source as we do the facilities regular users.

Ms. Shannon Mohr Thornburg, Environmental Engineer II
Page Two
January 12, 2006
2) The requirement for performing a corrosivity, ignitability and reactivity analysis was
overlooked by the operators of the facility. Upon discovery of this requirement in the
permit, we notified the department and preparations were made to have the tests
performed. We have since completed two (2) tests for these parameters. Please find the
analytical results attached.
3) The requirement of reporting the plant available nitrogen in the annual report was
overlooked during submittal of the 2004 Annual Report. The calculation was performed
based on the formula supplied in earlier correspondence and documented on the process
spreadsheet records maintained on site. Submittals have been modified to include this on
future reports. Attached please find the results.
We have reviewed the permit and all pertinent forms to ensure that corrections are made for future
submittals on the above items and other items you documented. Should you have any questions or
desire additional information, please do not hesitate contacting me at [phone] or via e-mail
at [e-mail]. Thank you for your assistance and cooperation in resolving these
issues.
Sincerely,
Kevin B. Greer, PE
Assistant Public Services Director
Attachments
pc: Mick Berry, City Manager/City of Hickory
Chuck Hansen, PE/Public Services Director/City of Hickory
Jimmy Clark, Public Works Director/City of Conover
Barry Edwards, PE/Director of Engineering & Utilities/Catawba County
Wayne Carroll, Veolia Water North America

acEAnalytical °
www.pacelabs.com
September 2, 2005
Mr. Richard Swartz (Project Manager)
Pace Analytical Services, Inc
Charlotte Laboratory
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Dear Mr. Swartz:
F'ROfEGT10N SEA
06 JAH, 20 PM 4= 12
Pace Analytical Services, Inc.
5203 Triangle Lane
Export, PA 15632
Phone., 724.733.1161
Fax. • 724.327.7793
Enclosed are analytical results for samples submitted to Pace Analytical by Pace Analytical Services, Inc. The
samples were received on August 26, 2005. The results reported in this project meet the requirements as
specified in Chapter 5 of the NELAC Standards. Any deviations or discrepancies from the NELAC standards are
documented in the case narrative(s) of this report. Please reference Pace project number 05-5004 when inquiring
about this report.
Client Site: Charlotte Laboratory
Client Ref.: 92101874/Veolia Water
Pace Sample Client Sample
Identification Identification
0508-2822 . 923027855/C0MP0ST3
General Comments: Cooler temperature 2 ° C upon receipt: Ice was present.
Please call me if you have any questions regarding the information contained within this report.
Sincerely,
Rachel D. Christner
Project Manager
RDC: jld
Enclosures
Page 1 of
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, .
without the written consent of Pace Analytical Services, Inc.
.M AC�pq
s n \.
Paea 1 of')

accAnalytical
www.pacelabs.com
Mr. Richard Swartz (Project Manager)
Pace Analytical Services, Inc
Charlotte Laboratory
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Client Site: Charlotte Laboratory
Client Ref.: 92101874/Veolia Water
General Chemistry
Pace Analytical Services, Inc.
5203 Triangle Lane
Export, PA 15632
- Phone:[phone]
Fax. 724:327.7793
Lab Project ID: 05-5004
Lab Sample ID: 0508-2822
Client Sample ID: 923027855/COMPOST3
Sample Matrix: Solid
Date Sampled: 08/25/2005
Date Received: 08/26/2005
Test
Method
Result
Reporting
Units
Anal
Analysis
Blank
Limityst
Date
BlankMethod
Result
Cyanide (Reactive)
7.3.3.2/90141l> -
<1.0:
1.0;
mg/kg
BLC
08/29/2005
0042396-1
<1.0
pH
90451 )
; 7.53
1.00 ;
pH
CAD
08/29/2005
0042358-1 i5.19
Sulfide ( Reactive)
90300)
<10 :
10 -
mg/kg
BLC
08/29/2005
0042397-1 i
<10
U.S. Environmental Protection Agency, 1996, Test Methods for Evaluating Solid Waste, SW-846, 3rd ed., Office of Solid Waste and .
Emergency Response, Washington, DC.
Sample Comments: Results reported on an as received basis.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 2 of 2 6 '`

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Ignitablllty
by EPA 1030
Client Sample ID: 962027855/compostl-3 Analyzed By. NIO
Client Project ID: 92101874 Date Collected: 8/25/200512:45
Lab Sample ID: G150-329-1A Date Received: 8/27/2005
Lab Project, ID: G150-329 Matrix: Solid
Parameter Result Units Date
Analyzed
Ignitablility < 0.8 mm/sec 8/29/2005
Reviewed By:
2 of 4
N.C. Certification #481 S.C. Certification #99029

mlceAnalyfical@
www.pacelabs.com
October 24, 2005
Mr. Richard Swartz (Project Manager)
Pace Analytical Services, Inc
Charlotte Laboratory
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Dear Mr. Swartz:
Pace Analytical Services, Inc.
.: , ,�_.::- rr .. 5203 Tniangle Lane
.•., :"��]1:ElljR 10) - r Export, PA 15632
�II I �I✓�1�� �%1.4
Phone: [phone]
Fax: [phone]
OG JA 20 PM 4: (?
Enclosed are analytical results for samples submitted to -Pace -Analytical- by Pace Analytical Services,- Inc: The
samples were received on October 12, 2005. The results reported in this project meet the requirements as
specified in Chapter 5 of the NELAC Standards. Any deviations or discrepancies from the NELAC standards
are documented in the case narrative(s) of this report. Please reference Pace project number 05-5890 when
inquiring about this report.
Client Site: Charlotte Laboratory
Client Ref.: 92104419 - Veolia
Pace Sample Client Sample
Identification Identification
0510-1466 9216169822 (Compost)
General Comments: Cooler temperature 5 ° C upon receipt. Ice was present.
Please call me if you have any questions regarding the information contained within this report.
Sincerely,
Penelope J. estrick
Project Manager
PJG: jld
Enclosures
Pagel of
REPORT OF LABORATORY ANALYSIS,
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pauc: 1 of 9

Client Sample ID: 926169822/Compost
Client Project ID: 92104419
Lab Sample ID: G150-333-1A
Lab Project ID: G150-333
Parameter Result:
Ignitabillity < 0.8
Comments:
Results for Ignitabllity
by EPA 1030
Analyzed By: EAW
Date Collected: 10/3/2005 08:50
Date Received: 10112/2005
Matrbc: Soil
Units
;� mmisec
N r: r:Fr2TIFir'.ATION 9dRJ
Date
Analyzed
10/19/2005
Reviewed By:
2 nf 4

laceAnalytical °
www.pacelabs.com
Mr. Richard Swartz (Project Manager)
Pace Analytical Services, Inc
Charlotte Laboratory
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Client Site: Charlotte Laboratory
Client Ref.: 92104419 - Veolia
General Chemistry
Pace Analytical Services, Inc.
5203 Triangle Lane
Export PA 15632
Phone: [phone]
Fax: [phone]
Lab ProjectID:
05-5890
Lab Sample ID:
0510-1466
Client Sample ID:
9216169822
(Compost)
Sample Matrix:
Solid -
Date Sampled:
10/03/2005
Date Received:
10/12/2005
Test
Method
Result
Reporting
Limit
Units
Analyst
Analysis
Date
Method
Blank ID
Blank
Result
Cyanide (Reactive)
7.3.3.2/90140)
<1.0,
1.0
mg/kg
BLC
10/17/2005 0043733-1
<1.0
90450
7.98
1.00 pH
AKL 10/14/2005 _ 0043656 1 5.81
Sulfide (Reactive)
90306>
; <10
10
- mg/kg
BLC
10/17/2005 0043704-1
<10
(1) U.S. Environmental Protection Agency, 1996, Test Methods for Evaluating Solid Waste, SW-846, 3rd ed., Office of Solid Waste and
Emergency Response, Washington, DC.
Sample Comments: Results reported on an as received basis.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ALC09
:�O •�\Oqy
Paae 2 of 2

It
VEOLIA WATER NORTH AMERICA OPERATING SERVICES
REGIONAL COMPOST FACILITY, HICKORY
Metals, Nutrients, and Pathogen,.,, _0
P�
2004
Date
1/13/2004
2/10/2004
3/9/2004
4/12/2004
5/11/2004
6/8/2004
7/13/2004
8/16/2004
9/15/2004
10/4/2004
11/15/2004
12/13/2004
Percent Moisture
33.7
41.6
47.1
43.8
35.9
18.8
21.6
53.3
53.9
28.6
59.7
61.6
Percent Solids
66.3
53.3
52.9
56.2
64.1
81.2
78.4
46.7
46.1
74.4
40.3
38.4
Limits
AVG
mg/kg
MIN
mglkg
MAX
mg/kg
Aluminum
6,500.01
8,700.0
6,100.0
7,300.0
5.400.0
12,000.0
Arsenic
41 rngfkg
2.10
2.30
3.00
2.50
3.90
3.00
4.10
4.20
220
1.90
3.30
7.90
3.371
1.90
4.10
Cadmium
39 mg/kgmg1kg
0.70
0.63
0.82
0.82
1.20
0.75
1.10
0.94
0.50
0.24
0.45
3.20
0.95
0.24
1.20
Chromium
1,200 mg1kq-
Copper
1,500 mg/kgmglkg
170.0
200.0
190.0
220.0
240.0
240.0
240.0
260.0
290.0
200.0
300.0
410.0
246.67
170.00
240.00
Lead
300 mcUkg
24.01
22.0
24.01
27.0
25.0
22.0
21.0
23.0
28.0
21.0
32.0
37.0
25.50
21.00
27.00
Mercury
17 rngfkg
0.30
0.45
0.19
0.40
0.20
nld
1.60
0.74
0.92
0.28
0.13
0.56
0.52
0.13
1.60
Mol bdnum
75 mg1kg
11.0
9.4
8.9
12.0
7.4
10.0
6.7
10.0
NID
5.6
7.5
15.0
9.43
5.60
12.00
Nickel
420 mg[kg
6.9
6.6
8.6
8.4
7.2
5.0
6.6
7.9
20.0
5.3
7.3
13.0
8.57
5.00
8.60
Selenium
36 mqlkg
1.50
1.90
2.10
2.50
2.50
1.80
2.201
3.30
3.40
2.30
4.00
4.60
- 2.68
1.50
2.50
Zinc
2,800 mglkg
450.0
430.0
460.0
520.0
520.0
430.0
530.0
620.0
710.01
480.0
750.01
750.0
554.17
430.00
530.00
TKN
12,000
1,800
8,700
3,900
9,700
24,000
7500.00
12000.00
Ammonia Nitrogen
3900
1,900
1100
7500
1,700
3,100
2300.00
3900.00
Nitrate -Nitrogen
32.00
30.00
120.00
35.00
27.00
68.00
60.67
120.00
Total Phosphorous
2,830.00
230.00
202.00
4,880.00
8,890.00
234.00
1087.33
2830.00
Salmonella
3 MPN/4
<3
<3
<3
<4
BRL
<1.1
Fecal Col'rform
1000 MPN!
H
8.00
7.13
7.83
7.50
8.13
8.04
7.65
7.13
8.00
PAN
2,792
970
1,430
3,425
1,677
3.708
1730.67
970.00
2792.00
Total Nitrogen
1.20%
1.80%
0.9%
0.4%
1.0%
24%
1.29%
0.39%
1.80%
VEOLIA WATER NORTH AMERICA OPERATING SERVICES

F W ATF Michael F. Easley, Gove or
�\O�0 9Q(r William G. Ross Jr., Secretary
1
North Carolina Department of Environment and Natural Resources
r Alan W. Klimek, P. E. Director
CO
Division of Water Quality
Coleen H. Sullins, Deputy Director
Division of Water Quality
November 5, 2003
Mr. Gene Hudgens, Plant Manager
Delta Apparel, Inc.
Post Office Box 37
Maiden, NC 28650
Subject: Permit No. WQ0006984
Land Application Inspection
Catawba County
Dear Mr. Hudgens:
Enclosed is the Land Application Inspection report for the inspection conducted on October
29, 2003 by Ms. Ellen Huffman with this Office.
The inspection revealed compliance with the subject permit, including laboratory analyses,
record keeping, and lagoon maintenance.
The inspection report should be self-explanatory; however, if you have any questions, please
contact Mrs. Huffinan or me at [phone].
Sincerely,
1
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Attachment
cc: Non -discharge compliance
Allen McCree, Delta Apparel
N. C. Division of Water Quality, Mooresville Regional Office, 919 North Main Street, Mooresville NC 28115 [phone]
A*A
NCaENR
Customer Service
1-877-623-6748

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F..Easley, Governor
William G. Ross, Jr. Secretary
Alan W. Klimek, P.E. Director
woo
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Delta Apparel County: Catawba
Permit No.: WQ0006984 * Issuance Date: October 23, 1997
Last Amended Dale: N/A Expiration Date: Sept. 30, 2002
If applicable SOC Issuance Date: N/A Expiration Date: N/A
Permittee Contact: Allen McCree Telephone No.: 828/428-9921
ORC Name: Allen McCree Telephone No.: same
* This permit is currently being renewed
Reason for Inspection.
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pales)
Delta Apparel, inc. (formally Delta Mills) land applies sludge generated from it's industrial
wastewater treatment plant. A site visit and records review was performed on October 29, 2003.
No land application activity was occurring at the time of inspection. Residuals from the plant were
land applied this past July. No more land application is expected until next year. Bio-Nomic
Services, Inc. is the current land application contractor. Review of the 2002 annual report &
laboratory data reflected compliance with the land application permit. There have been no odor
complaints for 2003, to date. Clariant Corporation's Mt. Holly East wastewater treatment facility
( & monofil) is currently the alternate means for sludge disposal, if weather deters use of land
application. Delta Apparel is investigating future sewer hookup to the Town of. Maidens wwtp.
Is a foilow-up inspection necessary des X no
inspectors) Name(s)/Title(s) Ellen HuLfman / Env. Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040

Residuals Inspection Check List
Delta Apparel WQ0006984
P9 -5
Sampiin6
Describe Sampling: Due to poor mixing capabilities, the Permittee used to sample each truck and
composite the sample. Aerators (added in June of 1999) have corrected the mixing problems
producing a more representative sludge sample thereby eliminating the need for compositing_
Is sampling adequate? Y Is sampling representative? Y
Field Sites (end use for class B biosolids)
No land application activity at time of inspection.
permit on site during application
Buffers adequate
Documented exceedances of PAN limits
Signs of runoff/ ponding
Rain Gauge on site during application
Are there any limiting slopes on fields? ' i'N N
No land application activity at time of inspection.
ivionitoring weals) T/N: T
If yes, location of well(s) see comment below.
Spiii plan on site
Cover crop specified in permit
Site condition adequate
(if no, improvements recommended) _
Comment: Ground water monitoring wells are no longer required to be sampled. however
the permit issued 10-23-97) states that the wells are not to be abandoned.
Odors/vectors No land application activity at time of inspection.
Odors present No
Vectors present No
Describe any nuisance conditions and any corrective actions needed
None

- _,
'State of North Carolina
Department of Environment
and Natural .Resources
Division of Water Quality
Michael F. Easley, Governor
Sherri Evans -Stanton, Acting Secretary
Kerr T. Stevens, Director
IT X
94
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Delta Apparel
Permit No.: WQ0006984
Last Amended Date: N/A
If applicable SOC Issuance Date: N/A
Permittee Contact: Allen McCree
ORC Name: Allen McCree
Reason for Inspection
County: Catawba
Issuance Date: xxxxxxxxxxxxxxxxxxx
Expiration Date: Sept. 30, 2002
Expiration Date: N/A
Telephone No.: 828/428-9921
Telephone No.: same
X ROUTINE COMPLAINT FOLLOW-UP OTHER
LEge of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached paw
Delta Apparel, Inc. (formally Delta Mills) land applies sludge from an industrial wastewater
treatment plant. A site visit and records review was performed on October 29, 2003. No land
application activity was occurring at the time of inspection. Residuals from the plant are usually
land applied once a year, in the spring. Bio-Nomic Services, Inc. is the current land application
contractor. Review of the 2002 annual report & laboratory data reflects compliance with the land
application permit. There have been no odor complaints for 2003 to date.
is a follow-up inspection necessary X __yes no
Inspector(s) Name(s)/Title(s) Ellen Huf'unan / Env. Technician V
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection March 8, 2001

� s

Residuals Inspection Check List
Delta Apparel WQ0006984
Type of Residual
X Land Application (class B)
Distribution and Marketing (class A)
pg 1
Record Keening
Y/N
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
Y TCLP analysis N SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y Hauling records (# gal. and/or tons hauled during calendar year to date)
Y Field loading records Y Field site maps and information
VZAjL_P?Records of lime purchased
N/A Pathogen & Vector Attraction Reduction
Comments: SSFA sample was being collected the
application activity to occur this spring.
in preparation for land
Pathogen & Vector Attraction Reduction Records N/A
(check which methods apply)
Fecal coliform
SM 9221 E (Class A or B)
(Class A, all test must be <1000 iv1PN / dry gram)
{� (Class B, Geometric mean of 7 samples/monitoring period - <2.0* 106 CFU /dry gram)
SM 9222 D (Class B only)
(Geometric mean of 7 samples/monitoring period for Class B <2.0* 106 CFU / dry gram)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry
I ime7fiemp records
Digester (MCRT) Compost Class A lime stabilization
Volatile solids calculations
Bench -top aerobic/anaerobic digestion results
pH records for lime stabilization ( Class A or B )
Treatment (check treatment type(s) used)
X Aerobic digestion n/a Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion - Drying beds (may not meet 503's)
Alkaline Stabilization Lime other -describe
Compost (check treatment type used) N/A
Windrow Aerated Static Pile In vessel Other

OF W A �_'ZR Michael F. Easley, Govemor
O� QG William G. Ross, Jr.,Secretary
y North Carolina Department of Environment and Natural Resources
CO
j r
� Gregory J. Thorpe, Ph.D.
0 Acting director
Division of Water Quality
April 9, 2002
Mr. Joe Hubbard, Plant Manager
Delta Apparel, Inc.
Post Office Box 37
Maiden, NC 28650
Subject: Permit No. WQ0006984
Land Application Inspection
Catawba County
Dear Mr. Hubbard:
Enclosed is the Land Application Inspection Report for the inspection of the subject facility
conducted on March 20, 2002 by Ms. Ellen Huffinan with this Office.
The Report indicates compliance with laboratory data and record keeping, including the 2001
annual report. A file review revealed that this office received no odor complaints for 2001.
The inspection report should be self-explanatory; however, if you have any questions, please
contact Mrs. Huffman or me at [phone].
Attachment
cc: Non -discharge compliance
h: W 00006984de1ta0402.doc
A
NQENR
Customer Service
1 800 623-7748
Sincerely,
io.-�✓u
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Mooresville Regional Office PHONE [phone]
919 North Main Street, Mooresville, NC 28115 FAX [phone]

w
State of North Carolina
Department of Environment
and Natural Resources
Division of Water -Quality
- A
Michael F. Easley, Governor
William G. Ross, Jr., Secretary NCDENR
Gregory J. Thrope, Ph.D., Acting Director NORTH C A io_NA DE:mrtTKENT OF
ENvj:zoN1+CRT ANC NAT.1RAL RG^.^.l1ZZCL^.
Non -Discharge Compliance Inspection
WQ Permit Number
W00006984
County
Catawba
Permittee
Delta Apparel Incorporated
Npdes Number(s)
I�LC0006190
Issuance Date
9/8/2000
Expiration Date
9/30/2002
Soc Issuance Date
Soc ExpirationDate
Permittee Contact
Gene Hudgens
Phone Permittee Contact
828/428-9921
ORC Certification *
13244
ORC Name
Allen McCrea
Phone ORC
704/428-9921
24hr Contact Name
Allen McCrea
Phone 24hr
704/428-9921
Reason For Inspection (Select One) 10 Routine p Complaint p Follow -Up O Other...
Type Of Inspection (Select One) 10 Collection System O Spray Irrigation p Residual
Inspection Summary
Inspector's Name
Phone Inspector
Inspection Date
Ellen Huffman
7041663-1699
3/20/2002
Inspector's Title
Fax Inspector
Env. Specialist II
7041663-6040
page 1

... Non Discharge Compliance Residual Inspection
Permittee IDelta Apparel incorporated
Permit Number #QO006984
Inspection Date 1312012002
Type
* Land Application O Distribution and Marketing
Record Keepin
Was a copy of current permit available? OQ Yes O No O NIA
Were current metals and nutrient analysis available? (see permit for frequency) O Yes OQ No O NIA
a. TCLP analysis? O Yes No O NIA
b. SSFA ( Standard Soil Fertility Analysis)? 10 Yes No O NIA
Were nutrient and metal loading calculated to determine most limiting parameters? YTD O Yes O No-* N/A
Were hauling records available? 10 Yes O No O§ N/A
How many gallons / tons hauled during the calendar year to date?
Were field loading records available? 10 Yes O No 0 NIA
Were records of lime purchased available? 10 Yes O No O� NIA
❑ Fields
❑ Pathogen and Vector Attraction Reduction (if applicable)
Were Operation and Manintance records present? 10 Yes O No * N/A
Were Operation and Manintance records Complete? O Yes O No NIA
Has the land application equipment been calibrated? 10 Yes O No NIA
Pathogen and Vector Attraction (if applicable):
a. Fecal coliform SM 9221 E ( Class A or B) O Yes O No Oi NIA
O ( Class A, all test must be <1000 MPN / dry gram)
O (Geometric mean of 7 samples per monitoring period for Class B <2.0'106 CFU / dry gram )
Fecal:coliform SM 9222 D ( Class B only) 10 Yes O No NIA
O ( Geometric mean of 7 samples per monitoring period for Class B <2.0*106 CFU / dry gram)
b. Salmonella ( Class A, all tests must be < 3MPN / 4 grams dry 10 Yes O No OQ N/A
c. Time / Temp on: 1Yes O No * NIA
❑ Digester ( MCRT) ❑ Compost ❑ Class A lime stabilization
d. Volatile Solids Calculations.
e. Bench -Top Aerobic/ Anaerobic digestion results.
f. pH records fo Lime Stabilization (Class A or B).
Treatment
Equipment
O Yes O No N/A
O Yes O No OQ N/A
O Yes O No NIA
® Aerobic Digestion ❑ Alkaline Stabilization .(Other)
❑ Auto Thermophilic Aerobic Digestion ❑ Compost (Windrow)
❑ Anaerobic.Digestion ❑ Compost (Aerated Static Pile)
❑ Drying Beds ❑ Other
❑ Alkaline Stabilization (Lime)
Additional
Equipment
page 2

T i
Non Discharge Compliance Residual Inspection
Permittee IDelta Apparel Incorporated
Permit Number IWQ0006984
Inspection Date 1312012002
Transport
Was a copy of the permit in transport vehicle? O Yes O No NIA
Was a copy of the spill control plan in vehicle? 10 Yes O No * NIA
Did transport vehicle appear to be maintained? 10 Yes O No NIA
Storage
® Lagoon ❑ AST ❑ UST ❑ Septic Tank ❑ Drying Beds ❑ Concrete Storage Pads
How many months storage?
9 months
Was a copy of the spill control plan on site? 10 Yes O No NIA
If Applicable:
Is lagoon lined? O Yes No O NIA
Above Ground Tank ❑ Aerated ❑ Mixed Aerated Hp: Mixed Hp:
Under Ground Tank ❑ Aerated ❑ Mixed I Aerated Hp: Mixed Hp:
Sampling
DescribeSampling:
Mee ffe
Was sampling adequate?
Was sampling representative?
Disposal
0 Yes O No O N/A
Yes O No O N/A
Were buffers adequate? O Yes O No O N/A
Is the cover crop type specified in permit? 10 Yes O NoO N/A
Were exceedence of PAN limits documented? 10 Yes O NoO NIA
Was the application site in good condition? 10 Yes O No OQ NIA
Was the site free of runoff / ponding?
Was the acreage specified in the permit being utilized?
Was the application equipment present and operational?
Were there any limiting slopes on disposal field?
(10% for surface application)
(18% for subsurface application)
Are monitoring wells called for in permit?
Was there access restrictions and / or signage?
Was a copy of the permit on site during application events?
Was the application site free of odors or vectors?
Were nutrient / crop removal practices in place?
O Yes O NoO N/A
O Yes O NoO N/A
O Yes O NoO N/A
O Yes O No O� NIA
O Yes O No O NIA
O Yes O No *N/A
O Yes O No * N/A
O Yes O No *NC
O Yes O No NIA
O Yes O No * NIA

OF WATER Michael F. Easley, Governor
O� pG William G. Ross, Jr.,Secretary
� y North Carolina Department of Environment and Natural Resources
r
j Gregory J. Thorpe, Ph.D.
Acting director
Division of Water Quality
March 5, 2002
Mr. Charles Hansen, Public Services Director
City of Hickory
Post Office Box 398
Hickory, NC 28603-0398
Subject: Hickory Compost Inspection
Permit No. WQ0004563
Catawba County
Dear Mr. Hansen:
Enclosed is the Hickory Class A Compost Facility inspection report for the inspection conducted on
February 13, 2002 by Ms. Ellen Huffman with this Office.
The report indicates compliance with your State issued permit and notes a substantial reduction in the
number of odor complaints received by this office in the last three years. The plant's contract operators should
be commended for their efforts in keeping this facility in compliance with all permit requirements.
The attached report should be self-explanatory, however, if you have any questions, please contact
Mrs. Huffman or me at [phone].
Attachment
cc: Non -discharge compliance
Hickory Compost Facility
EBH
NCDEW
Customer Service
1 800 623-7748
Sincerely,
D. Rek Gleason, P.E.
Water Quality Regional Supervisor
Mooresville Regional Office PHONE [phone]
919 North Main Street, Mooresville, NC 28115 FAX [phone]

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross, Jr., Secretary
Gregory J. Thrope, Ph.D., Acting Director
NCDENR
NORTH CAiO_ NA DEf&RTKENT OF
ENVRONrVCNT AND NAT.1RAL RC.^..^.URCC-.
Non -Discharge Compliance Inspection
WQ Permit Number
W00004563
County
Catawba
Permittee
Ham.: city of -
comoostLaludge Npdes Number(s)
NCO020401 NCO024252
NCO040797 NC002427
Issuance Date
6/1/2001
NCO036196 NCO039594
NCO024261 NCO032662
Expiration Date
5/31/2006
NCO081370
.Soc Issuance Date
�ll'ff
Soc ExpirationDate
AIA
Permittee Contact
Mr. Charles Hansen Phone Permittee Contact
8281323-7670
ORC Certification #
N/A
ORC Name
Wayne Carroll
Phone ORC
8281465-1401
24hr Contact Name
Wayne Carroll
Phone 24hr
828/466-1401
Reason For Inspection
(Select One)
10 Routine p Complaint Q Follow -Up
o Other...
Type Of Inspection (Select One)
10 Collection System p Spray Irrigation
O Residual
Inspection Summary
Inspector's Name Ellen Huffman Inspector's Title Env. Specialist 11 -7 21-11
Phone Inspector 704/663-1699 Fax Inspector 704/663-6040
Inspection Date 2/13/2002
page 1

10
Non Discharge Compliance Residual Inspection
Permittee IHickory, City of - compost/sludge
Permit Number IWQ0004563
Inspection Date 2/13/2002
O Land Application * Distribution and Marketing
Record KeeDin
Was a copy of current permit available? * Yes O No O NIA
Were current metals and nutrient analysis available? (see permit for frequency) Yes O No O N/A
a. TCLP analysis? * Yes O No O N/A
b. SSFA ( Standard Soil Fertility Analysis)? O Yes O No * N/A
Were nutrient and metal loading calculated to determine most limiting parameters? YTD 10 Yes O No NIA
Were hauling records available? * Yes O No O NIA
How many gallons / tons hauled during the calendar year to date? INIA
Were field loading records available? O Yes O No N/A
Were records of lime purchased available? 10 Yes O NoO N/A
❑ Fields
❑ Pathogen and Vector Attraction Reduction (if applicable)
Were Operation and Manintance records present? 10 Yes O NoO NIA
Were Operation and Manintance records Complete? O Yes O NoO NIA
Has the land application equipment been calibrated? 10 Yes O No * N/A
Pathogen and Vector Attraction (if applicable):
a. Fecal coliform SM 9221 E ( Class A or B) 10 Yes O No 0 N/A
O ( Class A, all test must be <1000 MPN / dry gram )
O (Geometric mean of 7 samples per monitoring period for Class B <2.0*106 CFU / dry gram )
Fecal coliform SM 9222 D ( Class B only) 10 Yes O No N/A
O ( Geometric mean of 7 samples per monitoring period for Class B <2.0*106 CFU / dry gram )
b. Salmonella ( Class A, all tests must be < 3MPN / 4 grams dry) O Yes O No O N/A
c. Time / Temp on: * Yes O No O N/A
❑ Digester ( MCRT) ® Compost ❑ Class A lime stabilization
d. Volatile Solids Calculations.
e. Bench -Top Aerobic/ Anaerobic digestion results.
f. pH records fo Lime Stabilization (Class A or B).
Treatment
Equipment
C Yes O No O N/A
O Yes O No O� N/A
O Yes O No N/A
❑ Aerobic Digestion ❑ Alkaline Stabilization (Other)
❑ Auto Thermophilic Aerobic Digestion ❑ Compost (Windrow)
❑ Anaerobic Digestion ® Compost (Aerated Static Pile)
❑ Drying Beds ® Other
❑ Alkaline Stabilization (Lime)
Additional
Equipment
page 2

Non Discharge Compliance Residual Inspection
Permittee lHickory, City of - compostisludge
Permit Number #QO004563
Inspection Date 2/13/2002
Transport
Was a copy of the permit in transport vehicle? 0 Yes 0 No NIA
Was a copy of the spill control plan in vehicle? 10 Yes 0 No DQ N/A
Did transport vehicle appear to be maintained? 10 Yes 0 No @) N/A
Storage
❑ Lagoon ❑ AST ❑ UST ❑ Septic Tank ❑ Drying Beds ® Concrete Storage Pads
How many months storage?
30 days
Was a copy of the spill control plan on site? 10 Yes 0 No DQ NIA
If Applicable:
Is lagoon lined? 10 Yes 0 No DQ NIA
Above Ground Tank JE1 Aerated ❑ Mixed Aerated Hp: Mixed Hp: l
Under Ground Tank ❑ Aerated ❑ Mixed Aerated Hp: Mixed Hp:
Sampling
Describe Sampling:
sampling performed for pathogen, vector attraction nutient and metals are taken -during each monitoring pe mod by the
compost operatmons contractor in accordance with the permit and EPA standards.
Was sampling adequate? 0 Yes 0 No 0 N/A
Was sampling representative? * Yes 0 No 0 N/A
Disposal
Were buffers adequate? 0 Yes 0 No * NIA
Is the cover crop type specified in permit? 10 Yes 0 No * NIA
Were exceedence of PAN limits documented? 10 Yes 0 No * N/A
Was the application site in good condition? 10 Yes 0 No * NIA
Was the site free of runoff / ponding? 10 Yes 0 ko NIA
Was the acreage specified in the permit being utilized? 10 Yes 0 No NIA
Was the application equipment present and operational? 0 Yes 0 No NIA
Were there any limiting slopes on disposal field?
(10% for surface application)
10 Yes 0 No0 NIA
(18% for. subsurface application)
10 Yes 0 NoO N/A
Are monitoring wells called for in permit?
10 Yes 0 No DQ N/A
Was there access restrictions and / or signage?
10 Yes 0 No0 N/A
Was a copy of the permit on site during application events?
10 Yes 0 No DQ NIA
Was the application site free of odors or vectors?
10 Yes 0 No * N/A
Were nutrient / crop removal practices in place?
10 Yes 0 No * N/A

10
AOW
wATFMichael F. Easley
Governor
William G: Ross, Jr.,Secretary
North Carolina Department of Environment and Natural Resources
-� Kerr T. Stevens, Director
Division of Water Quality
March 8, 2001
Mr. Joe Hubbard, Plant Manager
Delta Apparel, Inc.
Post Office Box 37
Maiden, NC 28650
Subject: Permit No. WQ0006984
Land Application Inspection
Catawba County
Dear Mr. Hubbard:.
Enclosed is the Land Application Inspection report for the inspection conducted on
March 8, 2001 by Ms. Ellen Huffman with this Office. The inspection is part of our initiative to
inspect all land application permits during each calendar year.
The attached report indicates compliance with your land application permit, including
maintenance of laboratory data and record keeping. You and your staff should be commended
for their efforts.
The inspection report should be self-explanatory; however, if you have any questions,
please contact Mrs. Huffman or me at [phone].
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Attachment
cc: Non -discharge compliance
h:De1ta030801.doc
VAW
NCDtNR
Customer Service Mooresville Regional Office, 919 North Main Street, Mooresville, NC 28115
PHONE [phone]
1 800 623-7748
FAX [phone]

T
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
Sherri Evans -Stanton, Acting Secretary
Kerr T. Stevens, Director
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Delta Apparel
Permit No:: W00006984
Last Amended Date: N/A
If applicable SOC Issuance Date: N/A
Permittee Contact: Allen McCree
ORC Name: Allen McCree
Reason for Inspection
County: Catawba
Issuance Date: October 23, 1997
Expiration Date: Sept. 30, 2002
Expiration Date: N/A
Telephone No.: 828/428-9921
Telephone No.: same
X ROUTINE COMPLAINT FOLLOW-UP - OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Summary: (additional comments may be included on attached pages)
Delta Apparel, Inc. (formally Delta Mills) land applies sludge from an industrial wastewater
treatment plant. A site visit and records review was performed on March 8, 2001; however, no
land application activity was occurring at the time of inspection. Residuals from the plant are
usually land applied once a year, in the spring. Bio-Nomic Services, Inc. is the current land
application contractor. Review of the 2000 annual report & laboratory data reflects compliance
with the land application permit. Aerators were added to the sludge storage lagoon in June of
1999 to reduce odor problems. This has apparently proven to be very effective.
Is a follow-up inspection necessary _yes X no
Inspector(s) Name(s)/Title(s) Ellen Huffman / Env. Technician V
Telephone No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection March 8, 2001

Residuals Inspection Check List
Delta Apparel WQ0006984
Type of Residual
X Land Application (class B) .Distribution and Marketing (class A)
pg 1
Record Keeping
Y/N
Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
Y TCLP analysis N SSFA (Standard Soil Fertility Analysis)
Y Nutrient and metals loading calculations (to determine most limiting parameter) YTD
Y -Hauling records (# gal. and/or tons hauled during calendar year to date)
Y Field loading records Y Field site maps and information
N/A Records of lime purchased -
N/A Pathogen & Vector Attraction Reduction
Comments: SSFA sample was being collected the day of this inspection in preparation for land
application activity to occur this spring.
Pathogen & Vector Attraction Reduction Records N/A
(check which methods apply)
Fecal coliform
SM 9221 E (Class A or B)
(C1ass.A, all test must be <1000 MPN / dry gram)
(Class B, Geometric mean of 7 samples/monitoring period - <2.0* 10' CFU / dry gram)
SM 9222 D (Class B only)
(Geometric mean of 7 samples/monitoring period for Class B <2.0* 106 CFU / dry gram)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry
Time / Temp records
Digester (MCRT) Compost Class A lime stabilization _
Volatile solids calculations
Bench -top aerobic/anaerobic digestion results
pH records for lime stabilization (Class A or B )
Treatment; (check treatment type(s) used)
X Aerobic digestion n/a Autothermal Thermophilic Aerobic Digestion
Anaerobic digestion Drying beds (may not meet 503's)
Alkaline Stabilization Lime other -describe
Compost (check treatment type used) N/A
Windrow Aerated Static Pile In vessel Other

A
Residuals Inspection Check List pg 2
Delta Apparel WQ0006984
Transport No land application activity at time of inspection.
Permit in transport vehicle? Spill control plan in transport vehicle? _
Does transport vehicle appear to be maintained?
.Operation & Maintenance records Noland application activity at time of inspection.
Calibration records of land application equipment
Condition of land application equipment on site
Storage
Number of days/weeks/months storage 9 months
Describe storage: aerated sludge lagoon.
(if more than 2 yrs, does facility have Surface Disposal Permit?)
Spill control plan on storage site? Yes No N/A X
X Lagoon - Is lagoon lined X cla
Aboveground tank N/A In ground tank N/A
Aerated Mixed Aerated Mixed
N/A Drying beds N/A Concrete storage pads
Sampling
Describe Sampling: Permittee used to sample each truck and composite the sample due to poor
storage mixing capabilities. Aaerators (added in June of 1999) have corrected the mixing problems
producing a more representative sludge sample eliminating the need for a composite sample.
Is sampling adequate? Y Is sampling representative? Y
Field Sites (end use for class B biosolids) Field identification
No land. application.activity at time of inspection.
Permit on site during application
Buffers adequate
Documented exceedances of PAN limits
Signs of runoff / ponding
Rain Gauge on site during application
Comments -
Spill plan on site
Cover crop specified in permit
Site condition adequate
(if no, improvements recommended) _
Are there any limiting slopes on fields? Y/N N

No land application activity at time of inspection.
10 % for surface application
Residuals Inspection Checklist
Delta Apparel WQ0006984
18% for subsurface application
Monitoring wells) Y/N: Y
If yes, location of well(s) see comment below.
pg 3
Comment: Ground water monitoring wells are no longer required to be sampled; however,
the permit (issued 10-23-97) states that the wells are not to be abandoned.
Odors/vectors No land application activity at time of inspection.
Odors present
Vectors present
Describe any nuisance conditions and any corrective actions needed

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State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T. Stevens, Director
&1?9'W'A
ARA
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner City of Hickory RCF
Non -Discharge Permit No. WQ0004563
Issuance Date May 23, 1996
Permittee Contact Graham Gilley
ORC Name Wayne Carroll
24hr Contact Name Wayne Carroll
Reason for Inspection
X ROUTINE COMPLAINT
County Catawba
NPDES-includes 10 sources, see file
Expiration Date Anri130, 2001
Telephone No. 828/465-1401
Telephone No. 828/465-1401
Telephone No. 828/465-1401
FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Infection Summary: (additional comments may be included on attached pages)
Based on the inspection, the subject facility is in compliance with its non -discharge permit. The last
inspection was on Februaryl3, 2002. Review of the 2002 annual report also reflects compliance.
There have been no odor complaints for 2003 to date.
Is aJollow-up inspection necessary _yes X no
Inspector(s) Name(s)/Title(s) Ellen B. Huffman /Environmental Specialist
Telephone No. 704/663-1699 Fax No. 704/663-6040 Date of Inspection 10/29/2003

Residuals Inspection pg 2
Type of Residual
Land Application (class B) X Distribution and Marketing (class A)
Record Keeping
Y/N
r,/ Y Copy of current permit available at residual generating site
Y Current metals and nutrient analysis (see permit for frequency)
/ Y TCLP analysis n/a SSFA (Standard Soil Fertility Analysis)
N/A Nutrient and metals loading calculations (to determine most limiting parameter) YTD!
� Y Hauling records- 4 gal/tons hauled during calendar year to date
N/A Field loading records n/a Field site maps and information
N/A Records of lime purchased
Y Pathogen & Vector Attraction Reduction
Comments: All records reflect compliance and were readily available for review.
Pathogen & Vector Attraction Reduction records (check which methods apply)
Fecal coliform
X Salmonella (Class A, all tests must be < 3MPN / 4 grams dry)
Time / Temp records
Compost X
Volatile Solids Calculations—X
Treatment
c
Compost (check treatment type used)
Windrow Aerated Static Pile X* In vessel X Other
Comments: It was suggested during the last inspection that the facility calibrate the process
temperature probes on a regular basis. This calibration log is currently kept -in the lab.
Aerated static pile treatment is also checked because the facility is also usingthismethod for
end curing the compost to meet 503s.
Transport N/A�
Permit in transport vehicle? Spill control plan in transport vehicle�
Does transport vehicle appear to be maintained?
Comments:
�� V

Residuals Inspection
Res. pg 3
Storage
Number of months storage
Describe storage: Cement curing pad for final curing and storage. The pad has space for 15 days
storage/curing at the current volume of sludge received for treatment. -;:;'
(If more than two years, does facility have Surface Disposal Permit?)
Comment - ne_ U
Sp ill control plan on Sto dr ge site? N/�S
La oqn - Is lagoon lined i
Above ground tank, In groun&ta
Aerated Mixed Aerated IVI, ' 7ed X
Drying beds n rete storage padsComments: Influent s' ludge receiving a has a spill control plan in pla storage area for
co Rost has do water control in place.
Sampling
Describe Sampling.
Sampling is performed according to EPA 40 CFI, part 503 guidelines.
Is sampling adequate X Is sampling representative X C U C s
Monitoring well(s) in permit: No
If yes, Location of well(s)
Odors/vectors
Odors present N
Vectors present N
Describe any nuisance conditions and any corrective actions needed.
Minimal odors at the facility were only noticeable in the immediate vicinity of processing areas and
were not, in the opinion of the state inspectors present, considered strong enough to be a nuisance
at the time of inspection (around 11:00 AM). No flies or other vectors were noticeable in anv areas
of the facility.

435 Williams Court, Suite 100
Baltimore, MD 21220
wwwv synagro. com
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVEDlNCDENF IDWR
WQROS
MOORESVILLE REGIONAL OFF ib�
s V
Re: 2019 .Annual Report for Permit No. WQ0006984
Dear NCDEQ:
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of South Fork Industries, NC.
If you have any questions or comments, please contact Everette Owens at 828-428-9921 or Alex
Fox at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Everette Owens, South Fork Industries
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

SOUTH FORK INDUSTRIES, INC., NC
RESIDUALS LAND APPLICATION -PROGRAM
Permit No. WQ0006984
2019 ANNUAL REPORT

South Fork Industries, Inc., NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WO0006984 County Catawba Year 2019
Facility Name (as shown on permit) South Fork Industries NPDES No. NC0006190
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summarv:
Total number of application fields in the permit: 6
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 182.56
Total number of acres utilized for land application during the year: 65.5
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T A 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Everette Owens. Plant Manaaer
Permittee Vame and Title (type or print) Signature of Perr ittDa
94
Signatu of Preparer* Date Signatu nd Appli Date
(if different from Permittee) (if different from ermittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY - LAN® APPLICATION IN NC
SOUTH FORK INDUSTRIES, INC., NC
SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
October 2019 861,800.00 G 182.56 D 165.58
YEARLY TOTAL 861,800.00 G 182.56 D 165.58
1/30/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional. parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006984
Facility Name: SOUTH FORK INDUSTRIES, INC., NC
NPDES# : NC0006190
or WQ# (residual only)
WWTP Name: SOUTH FORK INDUSTRIES- MAIDEN PLANT
Residuals Analysis Data
Product Type
TXLIQ.`
Date Sampled (grab) or 09/17/19;
.
Date Composited
Percent Solids
5. 08
PARAMETERS (mg/kg dry weight)
Arsenic
<5
Cadmium
<1
Mercury
0.0529
Chromium
118
Copper
413
Lead
4.56
Molybdenum
2.78
Nickel
32.2
Selenium
<5
Zinc
854
Total Phosphorus
5960
TKN
60600
Ammonia -Nitrogen
5880
Nitrate and Nitrite
<4.72
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X L�_/'
(SIGNATURE JgFr PREPARER)
Date Z '2 if - L.j z ,o
DENR FORM RSSF (5/2003) Printed: Friday - February 7, 2020 at 18:05:50 for: 2105 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
WQ0006984
Facility Name
SOUTH FORK INDUSTRIES, INC.,
NPDES#
N60006190
or WQ# (residual only)
WWTP Name
SOUTH FORK INDUSTRIES -
Residual Analysis Data
Product Type
TXLIQ
Date Sampled
09/17/19
Date Composited
Percent Soilds
5.08
PARAMETERS (mg/kg dry weight)'
Aluminium
3080
Calcium
5140
Magnesium
943
pH
7.10
Potasium
727
Sodium
6400
PAN
19361
SAR
4.8417
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information ' cluding the possibility of fines and imprisonment for knowing violations."
X — Date 2 - Z
(SIGNATUR PREPARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/7/2020 6:07:25 PM

0 C)
Waypiint
ANALYTICAL
9/27/2019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-262-0016
Project Description: South Fork Industries
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/19/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pw« X. G&-r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

0
•
Waypoint, 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-262-0016
Client Project Description: South Fork Industries
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
SM-4500-NH3C
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
9045D
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
4500NO3F-2011
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
6010D
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
SW-7471B
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
SM-4500-NH3C-TKN
WTN
68268
south fork
Solids
09/17/2019 10:50
09/19/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia

Report Number: 19-262-0016
Account Number: 46622
Submitted By: Alex Fox
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68268
Sample Id : south fork
Waypoi
0 (D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 * Fax [phone]
www.waypointanalytical.com
Project : South Fork Industries
REPORT OF ANALYSIS Date Sampled: 9/17/2019 10:50:00
Date Received: 09/19/2019 00:00
Date Reported: 09/27/2019
Total Solids *
5.08
ADM
09/20/2019 16:38
SM-2540G
Moisture *
94.90
ADM
09/20/2019 16:38
SM-2540G
Total Kjeldahl Nitrogen
6.06
60600
250
JPJ
09/26/2019 13:00
SM-4500-NH3C-TKN
Phosphorus
0.60
5960
50.0
BKN
09/24/2019 21:42
6010D
Potassium
0.07
727
50.0
BKN
09/24/2019 21:42
601 OD
Sulfur
2.45
24500
50.0
BKN
09/24/2019 21:42
601 OD
Calcium
0.51
5140
250
BKN
09/24/2019 21:42
601 OD
Magnesium
0.09
943
50.0
BKN
09/24/2019 21:42
6010D
Sodium
0.64
6400
250
BKN
09/24/2019 21:42
6010D
Iron
7200
50.0
BKN
09/24/2019 21:42
6010D
Aluminum
3080
50.0
BKN
09/24/2019 21:42
601 OD
Manganese
113
5.00
BKN
09/24/2019 21:42
6010D
Copper
413
2.50
BKN
09/24/2019 21:42
6010D
Zinc
854
12.5
BKN
09/24/2019 21:42
6010D
Ammonia Nitrogen
0.59
5880
100
JPJ
09/26/2019 13:00
SM-4500-NH3C
Organic N
5.47
54720
250
09/26/2019 13:00
CALCULATION
Nitrate+Nitrite-N
<4.72
4.72
ZBD
09/24/201915:33
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist

Report Number: 19-262-0016
Account Number: 46622
Submitted By: Alex Fox
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68268
Sample Id : south fork
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Molybdenum
Comments:
B
wavno' 1 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 11 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Project : South Fork Industries
REPORT OF ANALYSIS
Date Sampled: 9/17/2019 10:50:00
Date Received: 09/19/2019 00:00
Date Reported: 09/27/2019
<1.00
1.00
BKN
09/24/2019 21:42
601 OD
118
2.50
BKN
09/24/2019 21:42
601 OD
32.2
2.50
BKN
09/24/2019 21:42
6010D
4.56
3.00
BKN
09/24/2019 21:42
6010D
<5.00
5.00
BKN
09/24/2019 21:42
601 OD
0.0529
0.0151
TJS
09/24/2019 13:41
SW-7471 B
<5.00
5.00
BKN
09/24/2019 21:42
601 OD
7.1
JSL
09/24/2019 06:50
9045D
2.78
2.50
BKN
09/24/2019 21:42
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
{? MC ON�i
1i6 1" ir�J
Pauric McGroary
Agronomist

Way7621
��'��.M Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form,
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number: 19-262-0016
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1'
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: IBrandi Watson Date 8 Time: 9/19/2019 13:40:02

SAMP i LOG
minat
CUSTOMER: SYNAG O
�I
PROJECT MANAGER: Alt --Vic
Phone: (375�) Jo.3 a t
A & L CUSTOMER
LAB # SAMPLE I.D.
ta.
SAMPLING
LOCATION
;__6 —tw-
SAMPLE
TYPE
6/
Relinquished by Sampler: ate
yj7v
Relinquished by: Date
Relinquished by: Date
UO'> R
SPECIAL INSTRUCTIONS:
2, For TATE} g purposes.
oses.
(Sp
Time
r
Time
Time
16 aAON OfF C�N.I8700v
IIIII{Illliliillllllll{llll�1111111{ll1{III{lIN{Illllllllllllll{I (3-19-1309 RECORD
Synaaro CentralTechnical
South Fork Industries
OF
CONTAINERS
l
Recieved by:
1
Recieved by:
91d sampling procedures
u�Gu UU[Illy me collection of these samples.
ISAMPLE
C
SAMPLING METHOD METHOD
BATE
TIME PRESERVED SHIPPED
POD:
SAMPLE ANALYSIS REQUEST
➢'D' SLI + SL2 I NF➢ -N NO,, -NJ Organic
$N Cd Cr Ni Pb As H� Se nH
�&A -%4 ;��; Fy�:O' A"o
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
n
REMARKS:
Sands I Mo. CI I NO2 N
I
Pacre 6 nf 6

Sodium Absorption Ratio, Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2105-01-TXLIQ-NC SOUTH FORK INDUSTRIES, INC., NC 9/17/2019 911/2019-12/31/2019 4.8417
MAIDEN PLANT TEXTILE RESID. LIQUID
Na mg/1 = (Na mg/kg x % Solids) _ 100 = (6400 x 5.0800) + 100 = 325.12
Ca mg/1 = (Ca mg/kg x % Solids) _ 100 = (5140 x 5.0800) _ 100 = 261.112
Mg mg/I = (mg mg/kg x % Solids) = 100 = (943 x 5.0800) = 100 = 47.9044
Na meq = Na mg/I = Molec.Wgt.Na = 325.12 23 = 14.1357
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 261.112 = 20 = 13.0556
Mg meq = Mg mg/I = Molec.Wgt.Mg = 47.9044 = 12 = 3.99203
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 14.1357 = SgrRoot[0.5(13.0556+3.99203)] = 4.84171
Printed: 2/7/2020
Page 1 17:55

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SOUTH FORK INDUSTRIES, INC., NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS LUTZ PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 42.03
SITE #: NC CA 00006 FIELD# : CA 00006 0001 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 16.80 ACRES PERMITTED: 16.80
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
10/4/19
198,400.00 (G)
11809.5241
5.08
2.502
SFIWTX
DRY
0-<1/2"
SUR
0.5
0.30
60,600. p
5,880.00 p
4.72 p
19361
FESCUE PASTURE
Oct-19
198,400.00 (G)
11,809.524
I
1
1
1
Total Gallons/Ac:
Total Wet Tons/Ac:
11,809.52
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
97
0.025
0.005
0.590
2.066
0.023
<.001
0.014
0.161
0.025
4.273 29.82
Cumulative lbs/acre
0.094
0.049
0.985
27.437
0.173
0.014
0.143
0.819
0.116
12.209
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
j
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SFIMPTXL = SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME : SOUTH FORK INDUSTRIES, INC., NC PREDOMINANT SOIL SERIES: LLOYD
OWNER: DENNIS LUTZ PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 34.15
SITE #: NC CA 00006 FIELD# : CA 00006 0002 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 13.30 ACRES PERMITTED: 13.30
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
m
(pp )
crop
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
10/7/19
161,200.00 (G)
12120.3011
5.08
2.568
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
60,600. p
5,880.00 p
4.72 p
19361
FESCUE PASTURE
Oct-19
161,200.00 (G)
12,120.301
I
1
1
Total Gallons/Ac:
Total Wet Tons/Ac:
12,12u.3u
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
99
0.026
0.005
0.606
2.121
0.023
<.001
0.014
0.165
0.026
4.385
30.60
Cumulative Ibs/acre
0.107
0.060
1.108
31.109
0.197
0.015
0.171
0.975
0.135
12.114
_.
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SFIMPTXL = SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
--
X�L ✓� Z/Z 7
4.
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SOUTH FORK INDUSTRIES, INC., NC PREDOMINANT SOIL SERIES: CECIL
OWNER: JAMES JARRETT PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 106.38
SITE #: NC LT 00035 FIELD# : LT 00035 0001 OPERATOR: JAMES JARRETT CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 35.40 ACRES PERMITTED: 35.40
Page
Lime Applied ***
Date
Lbs Ac
DATE or
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
-
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1011119
124,000.00 (G)
3502.825
5.08
0.742
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
60,600. p
5,880.00 p
4.72 p
19361
FESCUE PASTURE
10/2/19
186,000.00 (G)
5254.237
5.08
1.113
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
60,600. p
5,880.00 p
4.72 p
19361
FESCUE PASTURE
10/3/19
192,200.00 (G)
5429.379
5.08
1.150
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
60,600. p
5,880.00 p
4.72 p
19361
FESCUE PASTURE
Oct-19
1 502,200.00 (G)
14,186.441
Total Gallons/Ac:
Total Wet Tons/Ac:
14,186.44
..,u. �.u�... ��.-.�. v.vv
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
116
0.030
0.006
0.709
2.482
0.027
<.001
0.017
0.194
0.030
5.133 35.82
Cumulative lbs/acre
0.056
0.024
0.889
16.190
0.100
0.005
0.066
0.562
0.055
8.190
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
jj
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SFIMPTXL = SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

SECTION 4

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis -
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: South Fork Industries
Lot Number:UJ30008
Date Completed: 11/13/2019
11 /14/2019 10:52 AM
Approved and released by:
Lab Director - Greenville: Lucas Odom
Q ACCRg��
4{�eOR{CtOPy
A C C R E D I T'E D
Do�—
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] . Fax [phone] www.shealylab.com.
Pagel of 9

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UJ30008
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
TCLP VOCs
The method blank for analytical batch 35131 contained Tetrachloroethene greater than the acceptance
criteria. The associated sample, UJ30008-001, did not contain detections for the target analyte;
therefore, re -extraction and/or re -analysis of sample was not performed.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 9

t,uem: aynagro
Description: South Fork
Date Sampled:10/29/2019 1100
Date Received:10/30/2019
LaDoraiory IU: ujjuuuts-uui
Matrix: Solid
% Solids: 4.69 10/31/2019 0031
Inorganic
non-metals
,i Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date
Batch
(% Solids) SM 2540G
1
10/31/2019 0031 KFE
34027
1
(Ignitability) 1010A
1
11/08/2019 1039 SLC
35076
1
(Reactive Cya) 7.3.3
1
11/12/2019 1740 KFE 11/11/2019 1008
1
(Reactive Sul) 7.3.4
1
11/11/2019 1612 HET 11/11/2019 1008
1
(Soil pH meas) 9045D
1
11/07/2019 2227 HET
34692
CAS Analytical
Parameter
Number Method
Result Q
LOCI DL
Units
Run
% Solids
SM 254OG
4.69
%
1
Ignitability (Pensky-Martens Closed -Cup)
1010A
>140
140 0
° F
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 18.9 ° C
9045D
6.8
su
1
TCLP Volatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/5030B 8260D 10 11/09/2019 2116 STM 35131 11/07/2019 2013
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Benzene
71-43-2
8260D
ND
0.050
0.0040
mg/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
0.10
0.020
mg/L
1
Carbon tetrachloride
56-23-5
8260D
ND
6.050
0.0040
mg/L
1
Chlorobenzene
108-90-7
8260D
ND
0.050
0.0040
mg/L
1
Chloroform
67-66-3
8260D
ND
0.050
0.0040
mg/L
1
,,,.Dichloroethane
107-06-2
8260D
ND
0.050
0.0040
mg/L
1
,.Dichloroethene
75-35-4
8260D
ND
0.050
0.0040
mg/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.050
0.0040
mg/L
1
Trichloroethene
79-01-6
8260D
ND
0.050
0.0040
mg/L
1
Vinyl chloride
75-01-4
8260D
ND
0.010
0.0040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
95 70-130
1,2-Dichloroethane-d4
93 70-130
Toluene-d8
102 70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 11/13/2019 1323 SCD 11/10/2019 1607 35161 11/07/2019 0137
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 0.0050 mg/L 1
2,4-Dihitrotoluene 121-14-2 8270E ND 0.080 0.0050 mg/L 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
-- —fit of holding time W = Reported on wet weight basis
y Environmental Services, Inc.
pub vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 9

t,uenu aynagro
Description: South Fork
Date Sampled:10/29/2019 1100
Date Received:10130/2019
Laooratory iU: UJsuuuu-uu1
Matrix: Solid
% Solids: 4.69 10/31/2019 0031
TCLP Semivolatiles
i Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1311/3520C 8270E 1 11/13/2019 1323 SCD 11/10/2019 1607 35161 11/07/2019 0137
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Hexachlorobenzene
118-74-1
8270E
ND
0.040
0.0050
mg/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.040
0.0050
mg/L
1
Hexachloroethane
67-72-1
8270E
ND
0.040
0.010
mg/L
1
2-Methylphenol
95-48-7
8270E
ND
0.040
0.010
mg/L
1
3+4-Methylphenol
106-44-5
8270E
0.026 J
0.040
0.015
mg/L
1
Nitrobenzene
98-95-3
8270E
ND
0.040
0.015
mg/L
1
Pentachlorophenol
87-86-5
8270E
ND
0.20
0.020
mg/L
1
Pyridine
110-86-1
8270E
ND
0.040
0.0050
mg/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.040
0.0050
mg/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.040
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
88 37-129
2-Fluorophenol
49 24-127
Nitrobenzene-d5
84 38-127
Phenol-d5
65 28-128
Terphenyl-d14
120 10-148
2,4,6-Tribromophenol
93 41-144
TCLP Herbicides
R--n Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1311 /8151 A 8151A 1 11 /12/2019 1926 DAL1 11 /11 /2019 1959 35264 11 /07/2019 0137
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2,4-D 94-75-7 8151A ND 0.020 0.0050 mg/L 1
2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 0.0013 mg/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
DCAA 74 50-112
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 3660B13665A 8082A 1 11/06120191637 CHG 11/05/20191521 34628
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units Run
Aroclor 1016
12674-11-2
8082A
ND
630
ug/kg 1
Aroclor 1221
11104-28-2
8082A
ND
630
ug/kg 1
Aroclor 1232
11141-16-5
8082A
ND
630
ug/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
u --it of holding time W = Reported on wet weight basis
Iy Environmental Services, Inc.
iuo vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 9

L,uenu bynagro
Description: South Fork
Date Sampled:10/29/2019 1100
Date Received:10/30/2019
LaDora>ory tu: uJsuuuu-uu1
Matrix: Solid
% Solids: 4.69 10/31/2019 0031
PCBs by GC
a Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
3550C 366013/3665A 8082A 1 11/06/20191637 CHG 11/05/20191521 34628
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Aroclor 1242
53469-21-9
8082A
ND
630
ug/kg
1
Aroclor 1248
12672-29-6
8082A
ND
630
ug/kg
1
Aroclor 1254
11097-69-1
8082A
ND
630
ug/kg
1
Aroclor 1260
11096-82-5
8082A
ND
630
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl 76 41-132
Tetrachloro-m-xylene 56 35-106
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 11/11/2019 1504 DAL1 11/08/2019 1238 35022 11/07/2019 0137
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
gamma-BHC (Lindane)
58-89-9
8081B
ND
0.00040
0.00017
mg/L
1
Chlordane
57-74-9
8081B
ND
0.0040
0.0015
mg/L
1
Endrin
72-20-8
8081B
ND
0.00040
0.00015
mg/L
1
Heptachlor
76-44-8
8081B
ND
0.00040
0.00015
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
0.00016
mg/L
1
Methoxychlor
72-43-5
8081 B
ND
0.0016
0.00021
mg/L
1
aphene
8001-35-2
8081B
ND
0.0080
0.0030
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
77 20-131
Tetrachloro-m-xylene
84 26-132
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
Leachate Date
1 1311/3010A
6010D
1 11/09/2019 1527 KSH2
11/08/2019 0908 34990
11/07/2019 0137
1 1311/7470A
7470A
1 11/09/2019 1102 KSH2
11/08/2019 1447 35005
11/07/2019 0137
2 1311/3010A
601OD
1 11/11/2019 0847 LLL
11/08/2019 0908 34990
11/07/2019 0137
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Arsenic
7440-38-2 6010D
0.045 J 0.15
0.025
mg/L
1
Barium
7440-39-3 6010D
0.32 0.25
0.031
mg/L
2
Cadmium
7440-43-9 6010D
ND 0.050
0.0060
mg/L
1
Chromium
7440-47-3 6010D
0.078 J 0.10
0.013
mg/L
1
Lead
7439-92-1 6010D
ND 0.10
0.047
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
- ^` it of holding time W = Reported on wet weight basis
,( Environmental Services, Inc.
iuo vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 9

Liienuaynagro
Description: South Fork
Date Sampled:10/29/2019 1100
Date Received:10/30/2019
t-aDoratory lu: ujsuuuu-uui
Matrix: Solid
% Solids: 4.69 10/31/2019 0031
TCLP Metals
i Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
Leachate Date
1311/3010A
6010D
1
11/09/2019 1527 KSH2
11/08/2019 0908 34990
11/07/2019 0137
1 1311 /7470A
7470A
1
11 /09/2019 1102 KSH2
11/08/2019 1447 35005
11 /07/2019 0137
2 131113010A
6010D
1
11/11/2019 0847 LLL
11/08/2019 0908 34990
11/07/2019 0137
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6
7470A
ND
0.0020
0.00091
mg/L
1
Selenium
7782-49-2
601OD
ND
0.20
0.085
mg/L
1
Silver
7440-22-4
6010D
ND
0.10
0.021
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
^,at of holding time W = Reported on wet weight basis
Environmental Services, Inc.
Tuts vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 9

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SHEALY ENVIRONMENTAL SERVICES, INC.
�;Irta1y klviNIInlomit Scrvicc3, Inc. I Vi 1 a. I
reucnmmul. Nwnbu: MEMISC-1.1 Mudw; Lxtc: W201IS
Sample Receipt Cheeldist (SRQ
client; synagro Cookillisnected bvfdaie: ` K l 10i'l o."19 T of #: U130048
'leans of receipt; ❑ 5ESI El Clit rit X1 IJP$ ❑ Fc iF..x t thel:
❑ Yes
k h°o
I. Wore custody seals pl�-,setit on the cooler?
EjyL!,4LJ
No
UTNA
_ If atL,iitcl' `tCAIS'•vCT4 rL'3CLll, :VCIC tae ' intact and I1017ral{e i?
T4 Strip TD: NA Chlorine S trip LD: Nil 'rowed bv: NA
Or�'nal Iumpv Urr. vegan roccipt / Derived (Corrected) temperawzy, upon T cipt %Solid Snap -Cup Ig•
5.0 f J.0 ars NA jNA nC 'NA ,'NA ]C NA ;NA oC
b'IelBtud ❑ 71 Bla7].;C% r'tiaittSt 141t1CS lit C;wl ID: 5 TT'i llt#ilf)rYCGt1Jll Factor: °C
h4edlod (il'molAnt: ltrn Ice ❑ lce Pacluq ❑ Dr • lee ❑ Ntmu
❑ Y cs
El No
®Nth
3. Ir lerrapuratt:ru oIFwry uvolar ox=c,4ed 6.10 "U, Nvas P rlojesr 3elnnager Notified?
r1-4 •vas T*:odtiwdby: phone . ani ai 11 face-m-f•ae,e (circle one).
® Y v-s
❑ No
El NA
4. Is tho votrlmacial couricr's packing Slip aimnlied to tlli$ font?
Yes
❑ No
5. Were proper ous lady procedure t followed?
® `;'es
❑ No
t<. Wue ample 1Ds listed on the COC?
® )('es
❑ No
?. VdGc sample Ii)s listed are all tatniple contai.r;crs?
El 'Yes
WIN
9. Was collection date & brae listed tyn (hc Coe?
❑ Yes
WINO
19, Was collection drltu "& tine ➢i.0--d cri all sample concaifier52
0 WE
❑ N'ol
10. Did all container label :nR)rmation (EI), date, [tube) agree with the COC'?
® Yes
❑ No
11. were. testa 10 be F-erlonuetl ltslW zin the COC?
' ®
Yes
❑ 1�'0
12, Did all samples arrive vl lEee prrtpur mynbiin,:m far � arh test andlor in good condition
(unbrokL;n, lids on, ctc.)7 .—_-..- —
Yes
❑ NU
II Was adNuaLr: sumplu volume Is ailstblo''
® 3t'es
Lj he
14. Wereall iampics rcccivcd Within Vz dic ho Iding drrM or 48 liours, whichever cones first.,
SC,m
No
15. Wcrc any samples Containers missingkx"ss (circle one) ;;tt,nples NJ UJ liSjCd tm COC�'
El �'
LINO
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1 fi": Far VOA and RSK-175 saraipl�, Won: bubblcw prcsent �"pea•;ize" (!fs"or 6rmm in diamo..mr
in any of the V0A t'ials2
[j Yes
No
VJ NA
17- Weru al T)R01nic1alr.-'wxtrir.N samples received at n pH of•- 2?
0 Yus
❑ N❑
91 NA
18- Wcm rill ryanidc simples received at v Ii ;' 12 mi&l sulfldc samples roccived at 2 f,I I --- 91?
C9 Yes
❑ NtY
O NA
19- Wem nll applicLllifc 'H.Irl NicyanlderPbefI0V625 (<0.SmgJ.) satrap os - e Ol residual
c}tlr�rinc?
20 V e,Y rlicnt romarkslrequests (i.e. requested dilutions, MS -180 designations, etc...)
Correctly transcribed non the COC ititu Lho comment tmmion hi LIMS7
❑Y es
El No
VJNA
❑ 5fcs
No
21. Was the quote number listed on the container label`? 1I 'es: Quote tJ NA
Sartiple Preservation Wuvt be cortipMCd fur any saulple(s) inL*rrectly rT,-.SctVCd or with headspaor.)
Saruplc(s) NA wcm m-ceil ad lneonrecdy prrSCn cd and vicrc ad•im ed areardi;5-ly
in aemplc rcceitzng -.tdtia NA earl. of cimle one: MS04, HNO3, HCI, NuQH using SR t NA _
ime nPPmtcnation NA li'mon- th3aonopresarvative is needed, rentei.n the rormnents below.
Sample(s) NA vtIere received with bubbiL-i :ors mm in diarn..to.1%
Samples(s) 1NA very rttiuivud with'1'RC> 0.5 M&II. (IF419 is no) and wefe
,:djusied a=nrdingly in samplo receiving With sodiuttt tltic wF[I(c (Nst;S-.Ut `:'Ltlr Shealy JD: NA
R bar-code labels applied by; NIEC:- Date: 1 t1130i 19
collunents:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 9

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: South Fork Industries
WWTP Name: South Fork Industries
Monitoring Period: From 01/01/ 2019 To 12/31/19
WQ Permit Number: WQ 00006984
NPDES Number: NC0006190
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlienhle to alternative nerfnrmed (Class A nr Clnae Rl rmmnlete the fnllnwina mnnitnrina dntn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10tothe 6th
MPN
<583
<611
<637
MPN/g
0
Annual
Grab
Sm9221C
Coliform
power per gram
E
of total solids
CFU
CFU/g
1000 MPN per grain of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Allc Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Everette Owens, Plant Manager
Preparer Name and Title (type or print)
Z.7 f-LoL�
Signature reparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results STATESVILLE
ANALYTICAL
5ynagro
s
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 09/23/2019
Reported: 09/25/2019
For:
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190923-16-01
Fecal Coliforms
1
<583
MPN/g
SM92210E-2006
09/24/2019
WC
190923-16-01
Percent Solids
1
3.43
%
SM254OB-2011
09/24/2019
WC
190923-16-02
Fecal Coliforms
2
<599
MPN/g
SM92210E-2006
09/24/2019
WC
190923-16-02
Percent Solids
2
3.34
%
SM2540B-2011
09/24/2019
WC
190923-16-03
Fecal Coliforms
3
<637
MPN/g
SM92210E-2006
09/24/2019
WC
190923-16-03
Percent Solids
3
3.14
%
SM2540B-2011
09/24/2019
WC
190923-16-04
Fecal Coliforms
4
<613
MPN/g
SM92210E-2006
09/24/2019
WC
190923-16-04
Percent Solids
4
3.26
%
SM2540B-2011
09/24/2019
WC
30923-16-05
Fecal Coliforms
5
<621
MPN/g
SM92210E-2006
09/24/2019
WC
190923-16-05
Percent Solids
5
3.22
%
SM2540B-2011
09/24/2019
WC
190923-16-06
Fecal Coliforms
6
<612
MPN/g
SM92210E-2006
09/24/2019
WC
190923-16-06
Percent Solids
6
3.27
%
SM25408-2011
09/24/2019
WC
190923-16-07
Fecal Coliforms
7
<615
MPN/g
SM92210E-2006
09/24/2019
WC
190923-16-07
Percent Solids
7
3.25
%
SM2540B-2011
09/24/2019
WC
Respectfully submitted,
rOP vp' j-y-2t-)
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190923-16-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190923-16-02
Temp on Arrival: 3.2
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190923-16-03
Temp on Arrival: 3.2
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190923-16-04
Temp on Arrival: 3.2
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190923-16-05
Temp on Arrival: 3.2
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 190923-16-06 Temp on Arrival: 3.2
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190923-16-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 c Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Client:
Fr TESVILLEANAINTICAL
122 Court Street • P.O. Sox 228
Slatesvillc, NC 28687
Address: �. 70 / , / y
Srr ! /U• � -Z (U C �'
Contact Person:
/{ Phone q 3 ?G - 703- UA 1 FAX# v 0 z
0Custody
ChAin of
Record
PC H X 5 KJ• ��� Requisitioned by: (Time o
Customer
Sample IN
Lab ID o
Time Sampled
(Grab Only)
Dale Sampled
(Grab Only)
d
Matrix
s �y y
Parameters for,malysis
Q
Relinquished by:
Received by:
Relinquished by:
Received by:
Composite Sampling
Time begin
Time end
Composite Sampling
Time begin
Time end
X Time % . DS am, 0 Date I / Z%L� Sampled by:
L ^� ��1,� Time am, 6 Date 91Z31._'r Transported by:
Y
Time am, pm Date _/ /_ Holding times met:
Time am, pm Date _/_/_ /
Compliance work:
#1:
am, pm Date _/ /_ Non-compliance work:
am, pm Date _/_/_
Loh Comments: Samples Transported On Ice:
#2:
am, pm Date
am, pm Date
Initials:
rn
N O
I'- '.'t
tb a)
O EL
1\
00
LD
W
N
V
Z
v
_j
IU
V)
W
[V
N
X
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Co
0
a

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project:
South Fork Industries
Field
S )IH71
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pH 11
(from soil analysis)
Applied(CCE Eq.)
CA-06-01
6.5
O.OT/Ac.
CA-06-02
6.0
O.OT/Ac.
CA-06-03
5.8
0.4 T/AC
.5 Tons
11/15/19
LT-35-1
5.6
0.6 T/Ac.
.75 Tons
11/15/19

SECTION 7

NCDA&CS A
omic Division Phone: [phone]
Website: wvn
;gr.gov/agronomi/
Report No.
:0-SL012709
Client: Alex Fox
Advisor:
Predictive
Synagro
284 Boger Rd
;= k�
Soil Report
Mehlich-3 Extraction
Mocksville, Nc27o2s
Links to Helpful Information
Sampled County: Catawba
P tY
Client ID: 501947
Advisor ID:
Sampled: 10/29/2019 Received: 10/30/2019 Completed: 11/08/2019
Farm: CA-06 Dennis Luke
Sample ID: 1
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M
0.0
120-200 80
10 0 0
pH$
0
0 0
Note: 12 Note:
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.36 1.00
9.2 91 0.8 6.7
25 76
56 31
41
350 216
99
99
241 0.1 1
Sample ID: 2A
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M
0.0
120-200 60
0 0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.41 0.92
9.8 82 1.7 6.0
32 193
48 25
65
1083 667
154
154
291 0.1 1
Sample ID: 2B
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M
0.0
120-200 80
20 0 0
pH$
0
0 0
Note: 12 Note:
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.46 1.01
8.9 88 1.0 6.5
25 66
55 30
47
1159 704
129
129
271 0.1 1
North Carolina
�c±tt:ICllp 7(ll5t iUl6il LLD71i1SI�tiiIC11i
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Trox/er. Commissioner ofAgriculture

NCDA&CS P omic Division Phone: [phone] Website: wwu gr.gov/agronomi/
Report No. !0-SL012709
Alex Fox
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full i
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/oboart4.htmY fsFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilize]
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.govlaaronomilbyrst.htm
Page 2 of 2
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

NCDA&CS p omic Division Phone: [phone] Website: wwv gr.gov/agronomi/ Report No. '.0-SL004626
Client: Dennis Lutz Advisor: Alex Fox
Predictive 2531 Cattle Creek Farm Rd Synagro
Newton, NC 28658 284 Boger Rd
Soil Report Mehlich-3 Extraction Mocksville, NC 27028
Sampled County :Catawba
Links to Helpful Information
Client ID: 244145 Advisor ID: 501947
Sampled: 09/10/2019
Received: 09/12/2019 completed: 09/21/2019
Farm: NC-CA-6
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.4
120-200 90
0
0 0
0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC
BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.56 0.96 8.7
80 1.7 5.8 20 116
49 24 76
1461
894
135 135
258 0.1 1
Norlh Carolina
i�, .
]"okictu lrtrc I'w4d Ckmiwi knU
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS A omic Division Phone: [phone] Website: ww% gr.gov/agronomi/ Report No. 10-SL004626
Dennis Lutz Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat(
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncaqr.gov/agronomi/pubs.htm.
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
N
Na
N 03-N
ORG
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmVfsFind information that P-1
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205
S-1
Test Results SS-1
W/V
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov/agronomi/uyrst.htm
mineral -organic soil class
nitrogen
sodium
nitrate nitrogen
organic soil class
current soil pH
phosphorus index
phosphate
sulfur index
soluble salt index
weight per volume
zinc availability index
zinc index

NCDA&CS A omic Division
Phone: [phone]
Website: wwv gr.gov/agronomi/
ReportNo. :0-SL012712
�•��"'- . ; �,,F
Client: Alex Fox
Advisor:
Predictive
Synagro
284 Boger Rd
Mehlich-3 Extraction
Soil Report
Mocksville, NC 27028
41
Links to Helpful Information
Sampled CountyLincoln
Client ID: 501947
Advisor ID:
Sampled: 10/20/2019 Received: 10/30/2019 completed: 11/08/2019 Farm: NC-Lt-35 Jarret Ottman
Sample ID: 01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.6 120-200 100
80 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al
Cu-I Na
ESP SS-1 NO3-N
0.27 1.05 6.0 76 1.4 5.6 16 30 51 22
59 1402 858 70 70
112 0.2
3
k. Nort.h Carolina
3obaCiu 3nr�C Furul t.'�:miu�b++l�m
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner ofAcrriculture

NCDA&CS A omic Division Phone: [phone] Website: wwv gr.gov/agronomi/ Report No. 0-SL012712
Alex Fox Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full i
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/aaronomi/obpart4.htmi fsFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizei
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.gov/agronomi/uvrst.htm
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS -I
soluble salt index
WN
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

SOUTH FORK INDUSTLM.ES, NC L_ -
RESIDUALS LAND APPLICATI&PPOR,66 RAM
Permit No. VVQ0006984
2017 ANNUAL REPORT
PECEIVEDINCDENROWR
WQR0S
MOORESVILLE RE&ONAL O=Fl(,E
R EG-OVEDIN C D E N R/D lJV R
wap \
os \
MOORESVILLE REGIO W OFFiCE

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00006984 County Catawba Year 2017
Facility Name (as shown on permit) South Fork Industries NPDES No. NC0006190
Land Application Operator Svnagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
YES X NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilized for land application during the year:
Part B — Annual Compliance Statement:
Facility was compliant during Lalgaar y 0 tl o "Sne fldnorr2si
rmit (inclu'ut not limited to items
1-13 l40 plo iss P WleL ii i i ti w i
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T . 1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fries and imprisonment for
knowing violations."
Everette Owens, Plant Manager
Permittee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
Si tur ofPermittee Date
-7—2i og
Signatur f Land Applier [Date%
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

435 Williams Court, Suite 100
Baltimore, NO 21220
www.synagro.com
FEBRUARY 27, 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
MAR 01 2019
Re: 2018 Annual Report for Permit No. WQ0006984
Dear NCDEQ:
RECE1VED1NCDENRIDWR
VIAR 25 2019
W� 1ROS
MOORESVILLE REGIONAL OFFICE
RECEIVEDUDENWR
MAR e 1 2019
Non -Discharge
Permitting Unit
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of South Fork Industries, NC.
If you have any questions or comments, please contact Everette Owens at 828-428-9921 or Erik
Bruce at [phone].
Sincerely,
6 L
Derrick Shivar
Environinental Compliance Manager
Enclosures
cc: Everette Owens, South Fork Industries
Erik Bruce,-Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

SOUTH FORK INDUSTRIES, INC., NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0006984
2018 ANNUAL REPORT

South Fork Industries, Inc., NC
Residuals Land Application Program
2018 Annual Report
TABLE OF CONTENTS
Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WO0006984 County Catawba Year 2018
Facility Name (as shown on permit) South Fork Industries NPDES No. NC0006190
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 16
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 123.12
Total number of acres utilized for land application during the year: 49.70
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T. I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." 7
Everette Owens, Plant Manager
Permittee Name and Title (type or print) Signature of PcrAittA
Signature of Preparer* Date Signatib of Land AppliV
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
SOUTH FORK INDUSTRIES, INC., NC
'SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
MONTHNEAR
September 2018
YEARLY TOTAL
. AMOUNT UNIT
1,004,400.00 G
1,004,400.00 G
DRY TONS UNIT
123.12 D
123.12 D
DRY METRIC
TONS
111.68
111.68
1 /28/2019

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006984
Facility Name: SOUTH FORK INDUSTRIES, INC., NC
NPDES# : NC0006190
or WQ# (residual only)
WWTP Name: SOUTH FORK INDUSTRIES- MAIDEN PLANT
Residuals Analysis Data
Product Type
TXLIQ
Date Sampled (grab) or 01
/ 12 / 18
Date Composited
Percent Solids
2.94
PARAMETERS (mg/kg dry weight)
Arsenic
<3
Cadmium
<2
Mercury
<0.4
Chromium
21
Copper
458
Lead
<5
Molybdenum
<5
Nickel
11.8
Selenium
<5
Zinc
803
Total Phosphorus
4330
TKN
73200
Ammonia -Nitrogen
4750
Nitrate and Nitrite
<15.6
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X 4-1� Date �Z 7-
(SIGNATURE QF-PREPARER)
DENR FORM RSSF (5/2003) Printed: Monday - January 28 2019 at 19:01:56 for: 2105 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006984
Facility Name: SOUTH FORK INDUSTRIES, INC., NC
NPDES# : NC0006190
or WQ# (residual only)
WWTP Name: SOUTH FORK INDUSTRIES- MAIDEN PLANT
Residuals Analysis Data
Product Type TXLIQ
Date Sampled (grab) or 01/12/18
Date Composited
Percent Solids 2.94
PARAMETERS (mg/kg dry weight)
Aluminum
836
Calcium
4240
Magnesium
829
pH
7.70
Potassium
747
Sodium
7410
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X Date
Z -Z� -/�,
(SIGNATURE OF
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Monday - January 28 2019 at 19:08:30 for: 2105 01

Page: 1 of 2
Report Number: 18-017-0207
Account Number: 46488
Send To: SYNAGRO CENTRAL LLC/SALISBURY
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58113
Sample Id : South Fork Industries
•
Waypoin(2t,�
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : South Fork Industries
REPORT OF ANALYSIS Date Sampled: 1/12/2018 11:15:00
Date Received: 01/17/2018 00:00
Date Reported: 01/24/2018
Total Solids
2.94
29400
100.0
JM
01/17/2018 13:20
SM-2540G
Moisture "
97.05
100.0
JM
01/17/2018 13:20
SM-2540G
Total Kjeldahl Nitrogen
7.32
73200
50.0
JM
01/18/2018 09:30
SM-4500-NH3C-TKN
Total Phosphorus
0.43
4330
100
MOS
01/23/2018 16:53
6010C
Total Potassium
0.07
747
100
MOS
01/23/2018 16:53
6010C
Total Sulfur
2.48
24800
100
MOS
01/19/2018 16:21
6010C
Total Calcium
0.42
4240
100
MOS
01/19/2018 16:21
6010C
Total Magnesium
0.08
829
100
MOS
01/19/2018 16:21
6010C
Total Sodium
0.74
7410
100
MOS
01/23/2018 16:53
6010C
Total Iron
2700
100
MOS
01/19/2018 16:21
6010C
Total Aluminum
836
100
MOS
01/19/2018 16:21
6010C
Total Manganese
114
5.00
MOS
01/19/2018 16:21
6010C
Total Copper
458
5.00
MOS
01/19/2018 16:21
6010C
Total Zinc
803
5.00
MOS
01/19/2018 16:21
6010C
Ammonia Nitrogen
0.48
4750
50.0
JM
01/18/2018 09:30
SM-4500-NH3C
Organic N
6.84
68450
50.0
01/18/2018 09:30
CALCULATION
Nitrate+Nitrite-N
<15.6
15.6
MMT
01/19/2018 08:32
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk.
Detection limit on all N series
is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 18-017-0207
Account Number: 46488
Wavpoint,,(2)
CW ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Send To: SYNAGRO CENTRAL LLC/SALISBURY
Project : South Fork Industries
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
REPORT OF ANALYSIS
Date Sampled: 1/12/2018 11.-15:00
Lab Number: 58113
Date Received: 01/17/2018 00:00
Sample Id : South Fork Industries
Date Reported: 01/24/2018
RESULT
RESULT'
QUANTITATIONANALYSIS
PARAMETER
.
,. •.
Total Cadmium
<2.00
2.00
MOS
01/19/2018 16:21 6010C
Total Chromium
21.0
5.00
MOS
01/19/2018 16:21 6010C
Total Nickel
11.8
5.00
MOS
01/19/2018 16:21 6010C
Total Lead
<5.00
5.00
MOS
01/19/2018 16:21 6010C
Total Arsenic
<3.00
3.00
MOS
01/23/2018 16:53 6010C
Total Mercury
<0.400
0.400
MOS
01/22/2018 15:59 SW-7471 B
Total Selenium
<5.00
5.00
MOS
01/24/2018 12:27 6010C
pH. 7.7
1.0
JM
01/19/2018 08:35 9045D
Total Molybdenum
<5.00
5.00
MOS
01/19/2018 16:21 6010C
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made pofic- PIC 60Wr
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist

SAMPLING LOG # A 1s L EA,
7621 Whii
/ Richmonc
CUSTOMER: SYNA RO ®804/743-6.
PROJECT MANAGER:
Phone:{3�% _703 ��� r_Uce�Sy��C(I�•cakv
A & L CUSTOMER
LAB # SAMPLE I.D.
S i �..�� ..ems
Relinquished by Sampler:
Relinquished by:
Relinquished by:
SAMPLING,
LOCATION
06V�
SAMPLE
TYPE
co �"e
Date Time
l(o I 2.'.G0
ate Time
11 1
T
ate Time
SPECIAL INSTRUCTIONS:
1=or—__._ ._ monitoring
_purposes.
Illllllllllillllillllllllllllillllllll Ngill llllllllllllllllll
02 0�018'
South Fork Industries
# OF
CONTAINERS
i
Recieved by:
n I(Pdl�s1.`r'`�IS
; Is) lei
. ­..... C„u< t, )apt uper neia sampnng proceaures
were used during the collection of these samples.
SAMPLER
SAMPLING METHOD METHOD
DATE TIME PRESERVED SHIPPED
1711C� I1,LS
Rec' d by:
Recieved by:
PO#:
REMARKS:
u
le-r-
ANALYSIS REQUEST
SAMPLE
LD.
SLE
SL2
NH -N
a
NO -N
a
Organic
N
Cd
Cr
NI
Pb
As
Hg
Se
PH
CaCO3
equiv.
Volatile
Solids
Mo
CI
NO2 N
o r
P10
vo
X40
yvo
!Ui'"
Boo
1050
P1050
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, -Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2105-01-TXLIQ-NC SOUTH FORK INDUSTRIES, INC., NC 1/12/2018 1/l/2018-12/31/2018 4.6597
MAIDEN PLANT TEXTILE RESID. LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (7410 x 2.9400) + 100 = 217.854
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (4240 x 2.9400) + 100 = 124.656
Mg mg/I = (mg mg/kg x % Solids) + 100 = (829 x 2.9400) + 100 = 24.3726
Na meq = Na mg/I i- Molec.Wgt.Na = 217.854 _ 23 = 9.47191
Ca meq = Ca mg/I + Molec.Wgt.Ca = 124.656 + 20 = 6.2328
Mg meq = Mg mg/I + Molec.Wgt.Mg = 24.3726 _ 12 = 2.03105
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 9.47191 + SgrRoot[0.5(6.2328+2.03105)] = 4.65974
Printed: 2/11/2019
Page 1 09:06

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SOUTH FORK INDUSTRIES, INC., NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS LUTZ PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 36.49
SITE #: NC CA 00006 FIELD# : CA 00006 0001 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 16.80 ACRES PERMITTED: 16.80
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/20/18
161,200.00 (G)
9595.238
2.94
1.176
SFRVIPTX
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
4,750.00 p
15.60 p
22926
FESCUE PASTURE
9/21/18
136,400.00 (G)
8119.048
2.94
0.995
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
4,750.00 p
15.60 p
22926
FESCUE PASTURE
Sep-18
1 297,600.00 (G)
17,714.286
i otal (jauons/Ac: 17,714.29
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
100
0.013
0.009
0.091
1.989
0.022
0.002
0.022
0.051
0.022
3.488
18.81
Cumulative lbs/acre
0.069
0.044
0.394
25.371
0.150
0.013
0.129
0.658
0.091
7.937
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
¢¢
162
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SFIMPTXL = SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SOUTH FORK INDUSTRIES, INC., NC PREDOMINANT SOIL SERIES: HIWASSEE
OWNER: DENNIS LUTZ PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 34.21
SITE #: NC CA 00006 FIELD# : CA 00006 0002 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 13.30 ACRES PERMITTED: 13.30
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/11/18
167,400.00 (G)
12586.466
2.94
1.543
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
4,750.00 p
15.60 p
22926
FESCUE PASTURE
9/12/18
111,600.00 (G)
8390.977
2.94
1.029
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
4,750.00 p
15.60 p
22926
FESCUE PASTURE
Sep-18
1 279,000.00 (G)
20,977.443
1 Mill 1T411Ul1b/HU: LU,7//.44
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
118
0.015
0.010
0.108
2.356
0.026
0.002
0.026
0.061
0.026
4.130
22.27
Cumulative lbs/acre
0.081
0.055
0.502
28.988
0.174
0.015
0.156
0.810
0.109
8.488
FF
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
153
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8L'
1339.0
267.9
15.0
375.0
89.0
2500.0
SFIMPTXL = SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
19
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SOUTH FORK INDUSTRIES, INC., NC PREDOMINANT SOIL SERIES: PACOLET
OWNER: DENNIS LUTZ PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 52.45
SITE #: NC CA 00006 FIELD# : CA 00006 0003 OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 19.60 ACRES PERMITTED: 19.60
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/12/18
49,600.00 (G)
2530.612
2.94
0.310
SFIWTX
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
4,750.00 p
15.60 p
22926
FESCUE PASTURE
9/13/18
173,600.00 (G)
8857.143
2.94
1.086
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
73,200, p
4,750.00 p
15.60 p
22926
FESCUE PASTURE
9/14/18
179,800.00 (G)
9173.469
2.94
1.125
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
73,200. p
4,750.00 p
15.60 p
22926
FESCUE PASTURE
9/21/18
24,800.00 (G)
1265.306
2.94
0.155
SFIMPTX
DRY
0-<1/2"
SUR
0.5
0.30
73,200, p
4,750.00 p
15.60 p
22926
FESCUE PASTURE
Sep-18
1 427,800.00 (G)
21,826.530
ioiat Uaiions/Ac: zi,rszb.�s
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
123
0.016
0.011
0.112
2.451
0.027
0.002
0.027
0.063
0.027
4.297
23.17
Cumulative lbs/acre
0.068
0.045
0.394
21.433
0.148
0.014
0.132
0.549
0.122
7.179
m
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
151
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 j
375.0
89.0
2500.0 q,
SFIMPTXL = SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
ZbL
l
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019

SECTION 4

msumfoll
A.rTdl,,vffxal Li3bPrasorie.
February 01, 2018
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: South Fork Industries
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://wivw.settek.com
Dear Erik Bruce: Order No.: 18010751
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/17/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
1-1
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 26

Summit Environmental Technologies, Inc.
� 3310 Win St'MMIT. Case lr N
arratlVe
BVIFtO#dktel'iAL7C�d@Ltd"1� 9Ptef_ Cuyahoga Falls, Ohio44223 WO#: 18010751
/aielf{f .sboal�arte� _` TEL: [phone] FAX: [phone]
Website: http:/hvww.settekcom Date: 2/1/2018
CLIENT: Synagro
Project: South Fork Industries
WorkOrder Narrative:
18010751: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the.customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Notes:
18010751-001AMS SVOC-BNA_TCLP(8270): MS exhibited low recovery for Pyridine. Pyridine is a
known poor performer.
18010751-001AMSD SVOC-BNA_TCLP(8270): MSD exhibited low recovery for Pyridine. Pyridine is
a known poor performer.
Original
Page 2 of 26

Summit Environmental Technologies, In Qualifiers and Acronyms
SUM801pir 3310 Win 5
i VI�tC�tJAAEddiI.L fL 1iCdL?L G��?, INC. Cuyahoga Falls, Ohio 4422 WO#: 18010751
Anafy6r--f Lalaetr4ia6P4 TEL: [phone] FAX.- (330) 253-446
Website: httD://ivww.settek.co Date: 2/1/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
In Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/M B+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 26

Summit Environmental Technologies, Inc.
fn as'" SAM I 1[ 3310 Win St.
Cuyahoga Falls, Ohio 44223
Avr-34ttirai T_pbpratories TEL: [phone] FAX.- [phone]
Website: http:/hvivw.settek.com
Workorder
Sample Summary
WO#: 18010751
01-Feb-18
CLIENT: Synagro
Project: South Fork Industries
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
18010751-001 South Fork Industries
1/12/2018 11:00:00 AM 1/17/2018 2:00:00 PM Sludge
Page 4 of 26

'MSUIAMITSummit Environmental Technologies, Inc. DATES REPORT
3310 Win St.
FNVI€JOWAIEWT L atrC9MOLOGIliS, UIC. Cuyahoga Falls, Ohio 44223 WO#: 18010751
4 ? J,trJrCaJ J Urfa"q i trsrdt v TEL: [phone] FAX.- [phone]
Website: htto:llwiviv.settek.com 01-Feb-18
Client: Synagro
Project: South Fork Industries
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
18010751-OOIA South Fork Industries 1/12/2018 11:00:00 AM Sludge Ignitability of Solids (SW-846: 1030)
1/25/2018 1:00:00 PM
pH (SW9045D)
1/23/2018 1:53:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
1/24/2018 11:28:00 AM
Reactive Sulfide (9034)/7.3.4.2
1/24/2018 11:28:00 AM
TCLP Herbicides Analysis (SW1311/81/22/2018 6:00:00 PM
1/23/2018 11:30:00 A
1/26/2018 11:43:00 PM
TCLP Mercury Analysis (SW 1311/74-i1/22/2018 6:00:00 PM
1/23/2018 11:10:00 A
1/23/2018 2:17:00 PM
TCLP Metals Analysis (SW1311/6010 1/22/2018 6:00:00 PM
1/23/2018 12:00:27 PM
1/23/2018 8:36:26 PM
TCLP Pesticides Analysis (SW1311/8(1/22/2018 6:00:00 PM
1/26/2018 3:44:00 PM
TCLP Semi-Volatiles Analysis 1/22/2018 6:00:00 PM
1/24/2018 7:00:00 AM
1/24/2018 6:58:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
1/23/2018 6:00:00 PM
1/24/2018 6:57:00 PM
Original
Page 5 of 26

Summit Environmental Technologies, Inc. Analytical Report
M9 StIfAlmir3310 Win St. i�
rrAfIRONMENTAL T2CHUOLOGIE5,RQQ. Cuyahoga Falls, Ohio44223 (base report)
An3;ptio-al Liabarzato"-cr;q TEL: [phone] FAX: [phone] WO#: 18010751
Website: http://wwN.settek.com Date Reported: 2/1/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/12/2018 11:00:00 AM
Lab ID: 18010751-001A
Project: South Fork Industries
Client Sample ID South Fork Industries
Analyses Result
RL
Qual Units
DF
Date Analyzed ,
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: EAM
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
0.00200
mg/L
1
1/23/2018 2:17:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW3010A
Analyst: KMS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND
0.500
mg/L
1
1/23/2018 8:36:26 PM
TCLP Barium(Ba) ND
5.00
mg/L
1
1/23/2018 8:36:26 PM
TCLP Cadmium(Cd) ND
0.100
mg/L
1
1/23/2018 8:36:26 PM
TCLP Chromium(Cr) ND
0.200
mg/L
1
1/23/2018 8:36:26 PM
TCLP Lead(Pb) ND
0.500
mg/L
1
1/23/2018 8:36:26 PM
TCLP Selenium(Se) ND
0.0500
mg/L
1
1/23/2018 8:36:26 PM
TCLP Silver(Ag) ND
0.500
mg/L
1
1/23/2018 8:36:26 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND
0.0800
mg/L
2
1/24/2018 6:58:00 PM
2,4,5-Trichlorophenol ND
0.200
mg/L
2
1/24/2018 6:58:00 PM
2,4,6-Trichlorophenol ND
0.200
mg/L
2
1/24/2018 6:58:00 PM
2,4-Dinitrotoluene ND
0.0400
mg/L
2
1/24/2018 6:58:00 PM
o-Cresol ND
0.200
mg/L
2
1/24/2018 6:58:00 PM
m/p-Cresol(s) ND
0.200
mg/L
2
1/24/2018 6:58:00 PM
Cresols, Total ND
4.00
mg/L
2
1/24/2018 6:58:00 PM
Hexachloro-1,3-butadiene ND
0.0160
mg/L
2
1/24/2018 6:58:00 PM
Hexachlorobenzene ND
0.0400
mg/L
2
1/24/2018 6:58:00 PM
Hexachloroethane ND
0.0800
mg/L
2
1/24/2018 6:58:00 PM
Nitrobenzene ND
0.0800
mg/L
2
1/24/2018 6:58:00 PM
Pentachlorophenol ND
0.200
mg/L
2
1/24/2018 6:58:00 PM
Pyridine ND
0.200
mg/L
2
1/24/2018 6:58:00 PM
Surr: 2-Fluorophenol 41.5
10 - 109
%Rec
2
1/24/2018 6:58:00 PM
Surr: Phenol-d6 20.4
10 - 109
%Rec
2
1/24/2018 6:58:00 PM
Surr: Nitrobenzene-d5 78.6
19 - 120
%Rec
2
1/24/2018 6:58:00 PM
Surr: 2,4,6-Tribromophenol 52.3
10 - 120
%Rec
2
1/24/2018 6:58:00 PM
Surr: 2-Fluorobiphenyl 71.5
22 - 117
%Rec
2
1/24/2018 6:58:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 6 of 26

Summit Environmental Technologies, Inc. Analytical Report
1B Ir 3310 Win St.
EP4l11iiONNIE_NTALTEC!%i'dOWGI25,IdC. Cuyahoga Falls, Ohio44223 (base report)
?sra%Irtir�sl L'r�ia€ar8ti7r/e TEL: [phone] FAX.- [phone] WO#: 18010751
Website: htta://ivww.settek.com Date Reported: 2/1/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/12/2018 11:00:00 AM
Lab ID: 18010751-OOIA
Project: South Fork Industries
Client Sample ID South Fork Industries
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14
80.3
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
72.9
Surr: DCB
73.3
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)
2,4-D
ND
2,4,5-TP
ND
Surr: DCAA
77.1
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
SW8270D SW3510C Analyst: BJH
34 - 116 %Rec
SW8081
0.0100
mg/L
0.0200
mg/L
0.00100
mg/L
0.00100
mg/L
0.00100
d mg/L
0.00100
mg/L
0.00100
mg/L
10 - 119
%Rec
10 - 119
%Rec
SW8151A
1.00 mg/L
0.500 d mg/L
20 - 140 %Rec
SW8260B
2 1/24/2018 6:58:00 PM
Analyst: JBN
1 1/26/2018 3:44:00 PM
1 1/26/2018 3:44:00 PM
1 1/26/2018 3:44:00 PM
1 1/26/2018 3:44:00 PM
1 1/26/2018 3:44:00 PM
1 1/26/2018 3:44:00 PM
1 1/26/2018 3:44:00 PM
1 1/26/2018 3:44:00 PM
1 1/26/2018 3:44:00 PM
SW8161A Analyst: JBN
1 1/26/2018 11:43:00 PM
1 1/26/2018 11:43:00 PM
1 1/26/2018 11:43:00 PM
SW1311 M Analyst: CTB
0.0500
mg/L
10
1/24/2018 6:57:00 PM
0.0500
mg/L
10
1/24/2018 6:57:00 PM
0.250
mg/L
10
1/24/2018 6:57:00 PM
0.0500
mg/L
10
1/24/2018 6:57:00 PM
0.0500
mg/L
10
1/24/2018 6:57:00 PM
0.0500
mg/L
10
1/24/2018 6:57:00 PM
0.0500
mg/L
10
1/24/2018 6:57:00 PM
0.0500
mg/L
10
1/24/2018 6:57:00 PM
0.0500
mg/L
10
1/24/2018 6:57:00 PM
0.0200
mg/L
10
1/24/2018 6:57:00 PM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
0 RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 26

asulomixt
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
In
i hr1IR4Nt,9ENTd L 3 ECii�dLdG1E5, 7Pd
Cuyahoga Falls, Ohio 44223
(base report)
Amgly ir.,a1 Lattaraform5
TEL: [phone] FAX: [phone]
WO#: 18010751
Website: huy.-Ilivwiv.settek.com
Date Reported: 2/1/2018
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
1/12/2018 11:00:00 AM
Lab ID:
18010751-OOIA
Project:
South Fork Industries
Client Sample ID South Fork Industries
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB
-SOLID
SW8260B
SW1311M
Analyst: CTB
TCLP VOLATILES ANALYSIS
Surr: 4-Bromofluorobenzene
92.7
70 - 130
%Rec
10
1/24/2018 6:57:00 PM
Surr: Dibromofluoromethane
107
70 - 130
%Rec
10
1/24/2018 6:57:00 PM
Surr: Toluene-d8
94.5
70 - 130
%Rec
10
1/24/2018 6:57:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.500 mg/Kg 1
1/24/2018 11:28:00 AM
RCI-SOLID-W/ IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1
1/25/2018 1:00:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH 7.4
s.u.@20.4C 1
1/23/2018 1:53:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive 30.0
25.0 mg/Kg 1
1/24/2018 11:28:00 AM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
0 RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 26

Summit Environmental Technologies, Inc.
Accreditation
Program
Ir 3310 Win St.
Anal teS Report
y P
Fir-WROtAbIE14 AL':`fCHMOLOGit5,WC,
Cuyahoga Falls, Ohio44223
Areflr6e1 t flhaa aYnrJt s
TEL: [phone] FAX [phone]
WO#:
18010751
Website: htty://wivw.settek.com
01-Feb-18
Client: Synagro
State: NW
Project: South Fork Industries
Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
18010751-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4,5-TP
A
Sludge
TCLP Herbicides Analysis (SWI311/8151)
2,4-D
A
Sludge
TCLP Herbicides Analysis (SWI311/8151)
DCAA
A
Sludge
TCLP Mercury Analysis (SW131 in470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SWI311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Tetrachloro-m-xylene
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Tribromophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorophenol
A
Key Key
NC WW SCM A Accredited NC WW SCM U Unavailable
Original #1
Page 9 of 26

Summit Environmental Technologies, Inc.
Accreditation
Program
3310 Win St.
msumfoly
Analytes Report
WIPalENTAL': ECH610LOG1=S,
INC;. Cuyahoga Falls, Ohio 44223
Y
/st -Ilyt6ral LRhoratoCFP5
TEL: [phone] FAX.- [phone]
WO#:
18010751
Website: htto://ivww.settekcom
01-Feb-18
Client: Synagro
State: NW
Project: South Fork Industries
Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
18010751-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
3,4-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene-d5
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Phenol-d6
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
p-Terphenyl-dl4
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
4-Bromofluorobenzene
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chlorofonn
A
Sludge
TCLP Volatiles Analysis
Dibromofluoromethane
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Toluene-d8
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original #1
Page 10 of 26

Sunrmit Environmental Technologies, Inc.fnsum' 3310 Win St.
QC SUMMARY REPORT
EN'<MQUTAHNTALL[CIMOLOGISS, iNC
Cuyahoga Falls, Ohio 44223
Arrafyflrai Ctrbgratorles TEL: [phone] FAX.- [phone]
WO#: 18010751
Website: http://www.settek.corn
01-Feb-18
Client:
Synagro
Project:
South Fork Industries
BatchID: 30522
TCLP Mercury ND 0,00200
TCLP Mercury 0.00411 0.00200 0.00400 0 103 80 120
TCLP Mercury 0.00539 0.00200 0.00400 0 135 75 125 S
TCLP Mercury 0.00511 0.00200
0.00400 0 128 75
125
0.00539 5.33 20 S
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit Original
P Second column confinnation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 11 of 26

m9summist
Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
FNVlROr4f,9ENTALTEC!ItlOLCGIES, 1KC Cuyahoga Falls, Ohio44223 WO#: 18010751
r' n.wiyurrs/ L hVratarier TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: 30522
Sample ID 18010789-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/23/2018
RunNo: 79771
client ID: BatchQC
Batch ID: 30522
TestNo: SW7470A SW7470A
Analysis Date: 1/23/2018
SegNo: 1387928
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 12 of 26

' Summit Environmental Technologies, Inc.summi-ot 3310 Win St. QC SUMMARYREPORT
Erv'JIRCMPAENTAL 6ECIRIO. GIES, 7h"C Cuyahoga Falls, Ohio 44223 WO#: 18010751
Analyfl-,31 Lei or=xvrier- TEL: [phone] FAX.- [phone]
Website: hitp:/hviviv.settek.com 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: 30532
Sample ID 18010705-001AMS
SampType: MS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79852
Client ID: BatchQC
Batch ID: 30532
TestNo: SW8260B SW1311M
Analysis Date: 1/24/2018
SegNo: 1390632
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.191
0.0500
0.200
0
95.6
39.9
160
1,2-Dichloroethane
0.205
0.0500
0.200
0
102
42.5
157
MEK
0.922
0.250
1.00
0
92.2
16.6
227
Benzene
0.196
0.0500
0.200
0
97.8
38.1
155
Carbon tetrachloride
0.162
0.0500
0.200
0
80.8
40.8
162
Chlorobenzene
0.187
0.0500
0.200
0
93.6
35.7
168
Chloroform
0.200
0.0500
0.200
0
100
18.3
199
Tetra chi oroethene
0.169
0.0500
0.200
0
84.7
10
261
Trichloroethene
0.172
0.0500
0.200
0
85.8
23.8
175
Vinyl chloride
0.187
0.0200
0.200
0
93.3
10
165
Surr:4-Bromofluorobenzene
526
500.0
105
84.6
130
Surr: Dibromofluoromethane
495
500.0
99.0
71.4
127
Surr: Toluene-d8
508
500.0
102
74.6
127
Sample ID 18010705-001AMSD
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79852
Client ID: BatchQC
Batch ID: 30532
TestNo: SW8260B SW1311M
Analysis Date: 1/24/2018
SegNo: 1390533
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.188
0.0500
0.200 0 94.0
39.9
160
0.191 1.69
25
1,2-Dichloroethane
0.207
0.0500
0.200 0 104
42.5
157
0.205 1.16
25
MEK
0.879
0.250
1.00 0 87.9
16.6
227
0.922 4.78
25
Benzene
0.190
0.0500
0.200 0 95.1
38.1
155
0.196 2.75
25
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 13 of 26

Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRON&IEyTALTECIM0LOG IES, WC,
Cuyahoga Falls, Ohio44223
rkrr�tr•cic , 4trbtarare�rbes TEL: [phone] FAX: [phone]
WO#: 18010751
Website: hftp://lvvviv.settek.coni
01-Feb-18
Client:
Synagro
---------------
---------------
Project:
South Fork Industries
BatchID: 30532
Sample ID 18010705-001AMSD
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79852
client ID: BatchQC
Batch ID: 30532
TestNo: SW8260B SW1311M
Analysis Date: 1/24/2018
SegNo: 1390533
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.158
0.0500
0.200
0
79.2
40.8
162
0.162
1.88
25
Chlorobenzene
0.189
0.0500
0.200
0
94.4
35.7
168
0.187
0.798
25
Chloroform
0.197
0.0500
0.200
0
98.6
18.3
199
0.200
1.36
25
Tetrachloroethene
0.171
0.0500
0.200
0
85.6
10
261
0.169
0.999
25
Trichloroethene
0.172
0.0500
0.200
0
86.2
23.8
175
0.172
0.523
25
Vinyl chloride
0.186
0.0200
0.200
0
93.1
10
165
0.187
0.215
25
Surr:4-Bromofluorobenzene
523
500.0
105
84.6
130
0
25
Surr: Dibromofluoromethane
501
500.0
100
71.4
127
0
25
Surr: Toluene-d8
517
500.0
103
74.6
127
0
25
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 14 of 26

Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
misumm1wr
ENIVROW01ENTAI.3ECHUGLOGIES, NC Cuyahoga Falls, Ohio44223 WO#: 18010751
tttratg-ticai Lx�larsior/ TEL: [phone] FAX.- [phone]
Website: httn:/hvwiv.settek.com 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: 30532
Sample ID MB-30532
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 1/23/2018
RunNo: 79841
client ID: PBS
Batch ID: 30532
TestNo: SW8260B SW1311M
Analysis Date: 1/24/2018
SegNo: 1390072
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichooroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
461
Surr: Dibromofluoromethane
532
Surr: Toluene-d8
468
500.0 92.2 70 130
500.0 106 70 130
500.0 93.7 70 130
Sample ID 18010822-00laMS
SampType: MS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79841
client ID: BatchQC
Batch ID: 30532
TestNo: SW8260B SW1311M
Analysis Date: 1/24/2018
SegNo: 1390079
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.189
0.0500
0.200 0 94.5
39.9
160
1,2-Dichloroethane
0.211
0.0500
0.200 0 106
42.5
157
MEK
0.985
0.250
1.00 0.0932 89.2
16.6
227
Benzene
0.212
0.0500
0.200 0.0111 101
38.1
155
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 15 of 26

SumparrSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ctVVlRptdll4uTr,LTGC3i1a0L0Gl�S, WC Cuyahoga Falls, Ohio44223
P4ttaPy: tic+=1 t,�borasrarips WO#: 18010751
TEL: [phone] FAX.- [phone]
Website: http://Wwiv.settek.com 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: 30532
Sample ID 18010822-00laMS
SampType: MS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79841
client ID: BatchQC
Batch ID: 30632
TestNo: SW8260B SW1311M
Analysis Date: 1/24/2018
SegNo: 1390079
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Carbon tetrachloride
0.208
0.0500
0.200
0
104
40.8
162
Chlorobenzene
0.201
0.0500
0.200
0
100
35.7
168
Chloroform
0.218
0.0500
0.200
0
109
18.3
199
Tetrachloroethene
0.205
0.0500
0.200
0
102
10
261
Trichloroethene
0.214
0.0500
0.200
0
107
23.8
175
Vinyl chloride
0.183
0.0200
0.200
0
91.4
10
165
Surr:4-Bromofluorobenzene
471
500.0
94.2
84.6
130
Surr: Dibromofluoromethane
522
500.0
104
71.4
127
Surr: Toluene-d8
463
500.0
92.6
74.6
127
Sample ID 18010822-00laMSD
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79841
;lient ID: Batch=
Batch ID: 30532
TestNo: SW8260B SW1311M
Analysis Date: 1/24/2018
SegNo: 1390080
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.197
0.0500
0.200
0
98.6
39.9
160
0.189 4.20
25
1,2-Dichloroethane
0.219
0.0500
0.200
0
110
42.5
157
0.211 3.77
25
MEK
1.07
0.250
1.00
0.0932
97.2
16.6
227
0.985 7.83
25
Benzene
0.209
0.0500
0.200
0.0111
99.2
38.1
155
0.212 1.33
25
Carbon tetrachloride
0.207
0.0500
0.200
0
104
40.8
162
0.208 0.481
25
Chlorobenzene
0.197
0.0500
0.200
0
98.4
35.7
168
0.201 1.96
25
Chloroform
0.215
0.0500
0.200
0
107
18.3
199
0.218 1.53
25
Tetra chi oroethene
0.202
0.0500
0.200
0
101
10
261
0.205 1.18
25
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected
below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 16 of 26

Summit Environmental Technologies, Inc.M-Surdmrr 3310 Win St. QC SUMMARY REPORT
E%.vlgQN1AEW. Al iEC1RJ0 AG1ES, ;NC Cuyahoga Falls, Ohio 44223 WO#: 18010751
ft.nfr iicai L rSai;eiprie TEL: [phone] FAX.- [phone]
Website: http://lvwlv.settek.coni 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: 30532
Sample ID 18010822-00laMSD
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 79841
client ID: BatchQC
Batch ID: 30532
TestNo: SW8260B SW1311M
Analysis Date: 1/24/2018
SegNo: 1390080
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Trichloroethene
0.203 0.0500
0.200
0 102
23.8
175 0.214
5.09
25
Vinyl chloride
0.200 0.0200
0.200
0 99.8
10
165 0.183
8.89
25
Surr:4-Bromofluorobenzene
476
500.0
95.3
84.6
130
0
25
Surr: Dibromofluoromethane
525
500.0
105
71.4
127
0
25
Surr: Toluene-d8
476
500.0
95.2
74.6
127
0
25
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to detennine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 17 of 26

t
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
.a 3310 Win St.
8WIR0UNIENTAL TEC®i ML.GGIES, *41C Cuyahoga Falls, Ohio 44223
WO#: 18010751
Arrailvtdral f;;7b ararnrpgr TEL: [phone] FAX. [phone]
Website: httD://wivw.settek.corn 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: 30543
Sample ID mb-30543
SampType: mblk
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/23/2018
RunNo: 79954
Client ID: PBS
Batch ID: 30543
TestNo: SW8151A SW8151A
Analysis Date: 1/26/2018
SegNo: 1393402
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0 d
Surr: DCAA 363 500.0 72.6 20 140
Sample ID Ics-30543
SampType: Ics
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/2312018
RunNo: 79954
Client ID: LCSS
Batch ID: 30543
TestNo: SW8151A SW8151A
Analysis Date: 112612018
SegNo: 1393403
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D
ND
1.00 0.500
0 81.1
62.6
125
2,4,5-TP
ND
0.500 0.500
0 83.6
52.5
128
Surr: DCAA
432
500.0
86.3
20
140
Sample ID 18010671-001ams
SampType: ms
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/23/2018
RunNo: 79954
Client ID: Batch=
Batch ID: 30543
TestNo: SW8151A SW8151A
Analysis Date: 1/26/2018
SegNo: 1393404
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 81.5 37 105
2,4,5-TP ND 0.500 0.500 0 81.5 38 106
Surr: DCAA 399 500.0 79.8 20 140
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 18 of 26

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENIOROW015.14TAL. 7EC.moLC43mfS, 8P C Cuyahoga Falls, Ohio 44223 WO#: 18010751
AnslyUl.-at twtoraaQfie= TEL: [phone] FAX.- [phone]
Website: httD://wivw.settek.com 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: 30543
Sample ID 18010671-001amsd
SampType: msd
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/23/2018
RunNo: 79954
Client ID: BatchQC
Batch ID: 30543
TestNo: SW8151A SW8151A
Analysis Date: 1/26/2018
SegNo: 1393405
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D ND 1.00 0.500 0 83.3 37 105 0 0 30
2,4,5-TP ND 0.500 0.500 0 85.0 38 106 0 0 30
Surr: DCAA 423 500.0 84.5 20 140 0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Penn it Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 19 of 26

:MSUMMI-11L Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENVI�©MAENTAL YECIRJOLOG1ES, WC Cuyahoga Falls, Ohio 44223 WO#: 18010751
r-t!raty 2fcaP .t "trb"drazAra�a TEL: [phone] FAX.- [phone]
Website: http://ivivw.settek.coni 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: R79750
Sample ID LCS-R79750
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@20.2C
Prep Date:
RunNo: 79750
Client ID: LCSS
Batch ID: R79750
TestNo: SW9045D
Analysis Date: 1/23/2018
SegNo: 1387446
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.0 7.0 0 101 90 110
Sample ID 18010675-004ADUP
SampType: DUP
TestCode: pH S(9045D) Units: s.u.@20.4C
Prep Date:
RunNo: 79750
Client ID: BatchQC
Batch ID: R79750
TestNo: SW9045D
Analysis Date: 1/23/2018
SegNo: 1387448
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 6.2
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
6.2 0.6 10
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 20 of 26

SUMMIMIL
Summit Environmental Technologies, Inc.In 3310 Win St.
QC SUMMARY REPORT
=PtVlgQbJf1ENTA1. LECUNOLOGIES, 1N.rC
Arts'ir;,iica3f f.%abars7vt•i€tf
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
WO#: 18010751
Website: htto://www.settek.com
01-Feb-18
Client:
Synagro
Project:
South Fork Industries
BatchID• R79874
Cyanide, Reactive ND 0.500
Cyanide, Reactive 0.968 0.500 1.000 0 96.8 85 110
Cyanide, Reactive 1.05 0.500 1.000 0 105 81.6 122
Sample ID 18010675-005AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 79874
Client ID: Batch=
Batch ID: R79874
TestNo: SW9014
Analysis Date: 1/2412018
SegNo: 1390916
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
1.13 0.500
1.000 0 113 81.6
122
1.054 7.22 10
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit
P
Second column conffnnation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Original
Page 21 of 26

SUMMINIL
Summit Environmental Technologies, Inc.Mn 3310 Win St.
QC SUMMARY REPORT
ENVIROMAENTAL CCHUOLBGIES, INIC
Cuyahoga Falls, Ohio 44223
WO#: 18010751
tt v�PG tical t abor4iarl��
TEL: [phone] FAX.- [phone]
Website: hgp.-Mvww.settek.com
01-Feb-18
Client:
Synagro
Project:
South Fork Industries
BatchID: R79874
Sample ID 18010675-006AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 79874
Client ID: BatchQC
Batch ID: R79874
TestNo: SW9014
Analysis Date: 112412018
SegNo: 1390916
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 22 of 26

Summit Environmental Technologies, Inc.Pr SUMMI-11L 3310 Win St. QC SUMMARY REPORT
ENVK0141,1ENTAL.TECIRMLOGIES,PIC Cuyahoga Falls, Ohio44223
Iltr:�t�•tdr.,�i Ltsmpr::inriev TEL: [phone] FAX.- [phone]
WO#: 18010751
Website: h-tto:/hviviv.settek.com 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: R79884
Sample ID LCS-R79884
SampType: LCS
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 79884
,lient ID: LCSS
Batch ID: R79884
TestNo: SW1030
Analysis Date: 1/25/2018
SegNo: 1391034
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
6.22
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
7.240 0 85.9 70 130
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 23 of 26

SUMMINt
Surttmit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
crti'dIROi•JP,INTIi4 TEC:;rdOL4GIES, 7f C
Cuyahoga Falls, Ohio 44223
Anaf,vtf=l twborxorieu TEL:
[phone] FAX: [phone]
WO#: 18010751
Website: http://iviviv.settek.cont
01-Feb-18
Client:
Synagro
Project:
South Fork Industries
BatchID: R79887
Sulfide, Reactive ND 25.0
Sulfide, Reactive 4620 25.0 4800 0 96.2 85 115
Sulfide, Reactive 4410 25.0 4800 0 91.9 80 120
Sulfide, Reactive
4500 25.0
4800 0 93.8 80
120
4410 2.02 30
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 24 of 26

Summit Environmental Technologies, Inc.ffl sulvirarr 3310 Win St. QC SUMMARY REPORT
ENVIR©UPENTAL YEMMOLOGIES, 7NC Czzyahoga Falls, Ohio 44223 WO#: 18010751
rin3trrticai tWborarorrt? TEL: [phone] FAX.- [phone]
Website: hap://tnwiv.settek.com 01-Feb-18
Client: Synagro
Project: South Fork Industries BatchID: R79887
Sample ID 18010675-005AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 79887
Client ID: BatchQC
Batch ID: R79887
TestNo: SW9034
Analysis Date: 1/24/2018
SegNo: 1391071
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 25 of 26

Summit Environmental Technologies, InG Analysis Request/Chain of Custody
3310 Win Street For Summit Environmental Technologies; Inc. use only
Cuyahoga Falls, Ohio 44223 Tel: [phone] Fax: [phone]
Page of SET Na
ComC� ,, Name (Please Print)
Project Name
<,^
r rz
'
u
,a
�I
'
,`
Comypanyy-` ddre
Project Address
�P
Client Phone.No. 33L - a3 yI
Report to
Client Fax No. Please Fax Results,(
PO#
Client Email Please Email Results ✓
Quote Na
Contact Person
Sampled by �+ JN ��
Ohio VAP samples ✓ ❑
Check ifJI
Sample Identificafloti
C
Cd�ectted'
EIY M b Date J M" be approved
Rash Requested By: lab mans Datc by ger
White and yellow'pagec should axompany samples to the laboratory.
NoWComments:
Eby o t�
he client retains the pink pagm
State of Sample Origin.—O
Check 'If FOR COMPUANCE
126459 oft
Page 26 of 26

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
South Fork Industries
South Fork Industries
WQ Permit Number: WQ 00006984
NPDES Number: NC0006190
Monitoring Period: From 01/01/ 2018 To 12/31/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlieahle to alternative nerfnrmed (Class A nr Class R) emmnlete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61'
MPN
<557
<716
<885
MPN/g
0
Annual
Grab
Sm9221C
Coliform
power per gram
E
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Everette Owens, Plant Manager
Pre rer Name and T' e (type or print)
Z•LZ--19
Signature reparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
02/06/2018
Reported:
02/08/2018
For:
South Fork Ind
Comments:
Geometric Mean <716 MPN/g
Sample Number Parameter . Sample ID Result Unit Method Analyzed Analyst
180206-28-01
Fecal Coliforms
SF1
<735
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-01
Percent Solids
SF1
2.72
%
SM25408-1997
02/06/2018
WC
180206-28-02
Fecal Coliforms
SF2
<885
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-02
Percent Solids
SF2
2.26
%
SM2540B-1997
02/06/2018
WC
180206-28-03
Fecal Coliforms
SF3
<557
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-03
Percent Solids
SF3
3.59
%
SM2540B-1997
02/06/2018
WC
180206-28-04
Fecal Coliforms
SF4
<660
MPN/g
SM92210E-2006
02/07/2018
WC
- - 180206-28-04
Percent Solids
SF4
3.03
ova
SM254❑B-1997
02/06/2018
WC
180206-28-05
Fecal Coliforms
SF5
<851
MPN/g
SM92210E-2005
02/07/2018
WC
180206-28-05
Percent Solids
SF5
2.35
%
SM254❑B-1997
02/06/2018
WC
180206-28-06
Fecal Coliforms
SF6
<676
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-06
Percent Solids
SF6
2.96
%
SM2540&1997
02/06/2018
WC
180206-28-07
Fecal Coliforms
SF7
<704
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-07
Percent Solids
SF7
2.84
%
SM254OB-1997
02/06/2018
WC
Respectfully submitted,
'AID I
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 180206-28-01 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-02 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-03 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-04 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28=05 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-06 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-07 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

e S
5NV'-O-qrO�STATESVILLE
-
ANALYTICAL
Address:
122CartStreet • PO, Box228
Slatesville,NC 28687
Contact Person:
It rub
1 I
Phone It
FAX#
Chain of
Custody Record
PO # Requisitioned by: (Time Date)
c 0. �V✓1
cuslomer
Sampie IDO
Leh -ID M
Time Sampled
(Dmb Only)
bate Sampled
(Grab Only)
g
5
Matrix
y W
t'ara,neie,a requested for snalyvis
O_2y-
i
02,53 ,
e.c. s `7
sl�
`-7
Relinquished by:
Time zU
�a ( !
Q, pm Date �l / �
Sampled by:
Received by:
Time ZC�
am, pm Date/� l�
Transported by:
Relinquished by:
Time
am, pm Date/ !
Holding times met: J
Received by:
Time
am, pm Date
Composite Sampling #1 •
_/
Compliance work:
Time begin
am, pm Date �_/
Non-compliance work:
Time end
am, pm Date
Composite Sampling
#2•
Lab Comments:
Samples Transported On Ice;
Time begin
am, pm Date _/
Time end
am, pm Date
initials:
00
ID
Ip
N
Ln
41
N
0
a

SECTION 6

Agricultural Lime Application Log
Year: 2018
Project
South Fork Industries
Field
Soil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pH
(from soil analysis)
Applied(CCE Eq.)
CA-06-01 7.3 O.OT/Ac.
CA-06-02 5.6 1.OT/Ac.
CA-06-03 5.7 1.OT/Ac.
O.OT/Ac.
O.OT/Ac.
*Lime will be applied when conditions improve.

SECTION 7

Page 1 of 2
Report Number: 19-014-0615
Account Number:46488 Waypoeinto
Send To: SYNAGRO CENTRAL LLC/SALISBURY ANALYTICAL
Mary Brewer "Every acre... Everyyear.'4M
284 BOGER RD
MOCKSVILLE INC 27028
Farm: CA-06
SOIL ANALYSIS REPORT
Date Received: 01/14/2019 Date Of Analysis: 01/15/2019 Date Of Report: 01/18/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Dennis Lutz
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
NC = North Carolina Fertilitv Index Value
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
ova
Soil
Ibs/A
M3
K
M g
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meg1100g
01
20513
4.9
134
26 L
43 VL
107 L
1708 VH
15 VL
7.3
0.0
9.6
MIN
010203
M
NC = 22
NC: 22
2 J20514
10.6
150
24 L
176 VH
227 H
780 L
27 VL
5.6
6.74
1.9
8.3
M-0
010203
VH
NC = 20
NC = 90
3
20515
8.8
150
61 H
198 VH
228 H
761 L
32 VL
5.7
6.76
1.7
8.1
M-O
010203
VH
NC = 51
NC = 101
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
m Rate pp
ppm Rate
ppm Rate
ms/cm Rate
01
1.1
9.3
89.0
0.7
0.0
10 L
4.5 H
133 VH
79 VH
2.9 H
0.6 M
010203
NC = 21
NC = 112.5
NC = 831
NC = 145.0
2
5.4
22.8
47.0
1.4
22.9
28 H
4.9 H
108 VH
145 VH
7.4 VH
0.7 M
_T
010203
NC = 58
NC = 122.5
NC = 675
NC = 370.0
3
6.3
23.5
47.0
1.7
21.0
24 M
4.8 H
206 VH
95 VH
4.4 VH
0.6 M
010203
NC = 50
NC = 120.0
NC = ,
NC = 220.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: cc
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc.
Pauric McGroary

Page 2 of 2
Report Number: 19-014-0615
Account Number: 46488 Waypoint-(D
Send To: SYNAGRO CENTRAL LLC/SALISBURY ANALYTICAL
Mary Brewer Every acre... Every year. "rn,
284 BOGER RD
MOCKSVILLE NC 27028
Farm: CA-06
Date Received: 01/14/2019
Date Of Report: 01/18/2019 SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Dennis Lutz
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
01
Adjust pH to 6.0
0
0.0
0
0
0
010203
2
Adjust pH to 6.0
0
1.0
0
0
0
010203
3
Adjust pH to 6.0
0
1.0
0
0
0
010203
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the �OIW�6 i"C
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

RECEIVED/NCDENR/DWR
-6 ?017
WQROS RECEIVED
�LJ
MOORESVILLE REGIONAL OE510E
FEB 2,7 2017
Information Processing Unit
DWR Section
DELTA APPAREL, INC. — MAIDEN, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0006984
2016 ANNUAL REPORT

Delta Apparel, Inc. - Maiden, NC
Residuals Land Application Program
2016 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Pages
3. Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/ Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00006984 County Catawba Year 2016
Facility Name (as shown on permit) Delta Apparel, Inc./Maiden Plant NPDES No. NC0006190
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 16
Total number of fields utilized for land application during the year: 5
Total amount of dry tons applied during the year for all application sites: 163.11
Total number of acres utilized for land application during the year: 90.8
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2016 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Permittee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
6 `h .17
e Date
Signature of Land Applier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2016 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
DELTA APPAREL, INC., NC
DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
MONTHNEAR
January 2016
March 2016
April 2016
YEARLY TOTAL
DRY METRIC
AMOUNT UNIT
DRY TONS
UNIT
TONS
316,200.00
G
25.32
D
22.97
291,400.00
G
39.97
D
36.25
713,000.00
G
97.82
D
88.73
1,320,600.00
G
163.11
D
147.95
2/2/2017

ANNUAL RESIDUALS SAMPLING SUMMARY FARM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006984
Facility Name: DELTA APPAREL, INC., NC
NPDES# : NCO006190
or WQ# (residual only)
WWTP Name: DELTA APPAREL - MAIDEN PLANT
Residuals Analysis Data
Product Type
TxzzQ
Date Sampled (grab) or 03/30/16
Date Composited
Percent Solids
3.29
PARAMETERS (mg/kg dry weight)
Arsenic
<3
Cadmium
<2
Mercury
<0.4
Chromium
15
Copper
785
Lead
<5
Molybdenum
<5
Nickel
24
Selenium
<5
Zinc
101
Total Phosphorus
5630
TKN
64700
Ammonia -Nitrogen
4260
Nitrate and Nitrite
<2
Laboratory
Waypoint Analytical Virginia Inc.
WAYPOINT ANALYTICAL
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF PREP
Date 2_/f �
DENR FORM RSSF (5/2003) Printed: Thursday - February 2 2017 at 08:33.06 for: 2105 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0006984
Facility Name: DELTA APPAREL, INC., NC
NPDES# : NC0006190
or WQ# (residual only)
WWTP Name: DELTA APPAREL - MAIDEN PLANT
Residuals Analysis Data
Product Type TXLIQ
Date Sampled (grab) or 03/30/16
Date Composited
Percent Solids 3.29
PARAMETERS (mg/kg dry weight)
Aluminum
2500
Calcium
4060
Magnesium
1160
pH
7.71
Potassium
3890
Sodium
55100
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
M
FURE OF PREPARER)
NR - Data Not Reported or Data Not Required
Date?-- /J"- Z i
DENR FORM RSSF-B (7/2002) Printed: Thursday - February 2 2017 at 08:33:30 for 2105 01

Page: 1 of 2
Report Number: 16-091-0205
Account Number: 46718
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL/DELTA APPAREL
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56474
Sample Id: DELTA
•
Waypoint
ANALYTICAL
Project: DELTA
NC CERT#257
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 3/30/2016 10:10:00
Date Received: 03/31/2016 00:00
Date Reported: 04/05/2016
Total Solids *
3.29
32900
100.0
JM
03/31/2016 14:50
SM-2540G
Moisture *
96.71
100.0
JM
03/31/2016 14:50
SM-254OG
Total Kjeldahl Nitrogen
6.47
64700
10.0
JM
04/01/2016 08:50
SM-4500-NH3C-TKN
Total Phosphorus
0.56
5630
100
KM
04/01/2016 10:55
SW 6010C
Total Potassium
0.39
3890
100
KM
04/01/2016 10:55
SW 6010C
Total Sulfur
2.89
28900
100
KM
04/01/2016 10:55
SW 601QC
Total Calcium
0.41
4060
100
KM
04/01/2016 10:55
SW 6010C
Total Magnesium
0.12
1160
100
KM
04/01/2016 10:55
SW 6010C
Total Sodium
5.51
55100
100
KM
04/01/2016 10:55
SW 6010C
Total Iron
2980
100
KM
04/01/2016 10:55
SW 6010C
Total Aluminum
2500
100
KM
04/01/2016 10:55
SW 6010C
Total Manganese
140
5
KM
04/01/2016 10:55
SW 6010C
Total Copper
785
5
KM
04/01/2016 10:55
SW 6010C
Total Zinc
101
5
KM
04/01/2016 10:55
SW 6010C
Ammonia Nitrogen
0.43
4260
10.0
JM
04/01/2016 08:50
SM-4500-NH3C
Organic N
6.04
60440
10.0
04/01/2016 08:50
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
04/01/2016 08:50
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
04/01/2016 10:55
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made 6NA
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 16-091-0205
Account Number: 46718
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL/DELTA APPAREL
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56474
Sample Id: DELTA
•
Waypoint
ANALYTICAL
Project : DELTA
NC CERT#257
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 3/30/2016 10:10:00
Date Received: 03/31/2016 00:00
Date Reported: 04/05/2016
Total Chromium
15
5
KM
04/01/2016 10:55
SW 6010C
Total Nickel
24
5
KM
04/01/2016 10:55
SW 6010C
Total Lead
<5
5
KM
04/01/2016 10:55
SW 6010C
Total Arsenic
<3.0
3.0
KM
04/01/2016 10:55
SW 6010C
Total Mercury
<0.4
0.4
KM
04/04/2016 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
04/01/2016 10:55
SW 6010C
pH (Standard Units) *
7.71
2.00
JM
04/01/2016 08:50
SW-9045D
Total Molybdenum
<5
5
KM
04/01/2016 10:55
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2105-01-TXLIQ-NC DELTA APPAREL, INC., NC MAIDEN 3/30/2016 31112016-1213112016 35.4991
PLANT TEXTILE RESID. LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (55100 x 3.2900) _ 100 = 1812.79
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (4060 x 3.2900) _ 100 = 133.574
Mg mg/I = (mg mg/kg x % Solids) = 100 = (1160 x 3.2900) = 100 = 38.164
Na meq = Na mg/I _ Molec.Wgt.Na = 1812.79 _ 23 = 78.817
Ca meq = Ca mg/I : Molec.Wgt.Ca = 133.574 _ 20 = 6.6787
Mg meq = Mg mg/I + Molec.Wgt.Mg = 38.164 = 12 = 3.18033
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 78.817 _ SgrRoot[0.5(6.6787+3.18033)] = 35.4991
Printed: 2/2/2017
Page 1 08:34

FACILITY NAME: DELTA APPAREL, INC., NC
DWNER: DENNIS LUTZ
SITE #: NC CA 00006 FIELD# : CA 00006 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HIWASSEE
PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 31.47
OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20.10 ACRES PERMITTED: 20.10
Page
Lune Applied ***
Date
Lbs/Ae
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
'tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
(PP-)
Crop
MONTH
Total
Per Acre
Solids
3/31/16
99,200.00 (G)
4935.323
3.29
0.677
DAMPTXL
DRY
0-<1/2"
SUR
0.5
0.30
64,700.p
4,260.00 p
2.00 p
20264
FESCUE
Mar-16
99,200.00 (G)
4,935.323
4/4/I6
130,200.00 (G)
6477,6121
3.29
0.889
DRY
0-<I/2"
SUR
0.5
0.30
64,700. p
4,260.00 p
2.00 p
20264
FESCUE
Apr-16
130,200.00 (G)
6,477.612
JDAMPTXL
I
1
Total Gallons/Ac: 11,412.94
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
63
0.009
0.006
0.047
2.458
0.016
0.001
0.016
0.075
0.016
0.316
17.63
Cumulative lbs/acre
0.066
1 0.045
0.394
26.633
1 0.148
0.012
0.131
1 0.749
0.083
4.358
_
1
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
(
}
216
_
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
i
1339.0
267.9
15.0 ` ' lg 375.0
89.0
4 M
2500.0
DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
X l7
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

FACILITY NAME: DELTA APPAREL, INC., NC
)WNER: DENNIS LUTZ
IITE #: NC CA 00006 FIELD# : CA 00006 0003
tESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: PACOLET
PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 37.43
OPERATOR: DENNIS LUTZ CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 19.30 ACRES PERMITTED: 19.30
Page: 1
Lime Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (VM (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/4/16
68,200.00 (G)
3533.679
3.29
0.485
DAMPTXL
DRY
0-<1/2"
SUR
0.5
0.30
64,700. p
4,260.00 p
2.00 p
20264
I FESCUE
4/5/16
204,600.00 (G)
10601.036
3.29
1.454
DAMPTXL
DRY
0-<1/2"
SUR
0.5
0.30
64,700. p
4,260.00 p
2.00 p
20264
FESCUE
Apr-16
272,800.00 (G)
14,134.715
Total Gallons/Ac: 14,134.72
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.012
0.008
0.058
3.045
0.019
0.002
0.019
0.093
0.019
0.392
21.84
79
Cumulative lbs/acre
0.052
1 0.035
1 0.282
18.982
1 0.121
0.012
0.106
1 0.486
0.096
2.881
€
` #
PAN Limit (lbs/acre) 1st Cro /2nd Crop
31
16'ermit
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
t
1339.0
267.9
15.0 375.0
89.0
2500.0 a
y t
DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
x &V6 I � 1, -17/i -�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

ACILITY NAME: DELTA APPAREL, INC., NC
WNER: HAROLD SHERRILL
1TE #: NC CA 00020 FIELD# : CA 00020 0001
ESIDUAL SOURCE(S):* See.list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HIWASSEE
PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 25.32
OPERATOR: WALLY SAINE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 16.80 ACRES PERMITTED: 16.80
Page: 1
Lune Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pprn)
Crop
MONTH
Total
Per Acre
Solids
1/6/16
173,600.00 (G)
10333.333
1.92
0.827
DAMPTXL
MOIST
0-<I/2"
SUR
0.5
0.30
55,700. p
4,170.00 p
185.00 p
17729
I FESCUE
1/7/16
142,600.00 (G)
8488.0951
1.92
0.680
DAMPTXL
DRY
0-<1/2"
SUR
0.5
0.30
55,700. p
4,170.00 p
185.00 p
17721
FESCUE
Jan-16
1 316,200.00 (G)
18,821.428
Total Gallons/Ac: 18,821.43
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
annual lbs/acre
53
0.009
0.006
0.057
2.637
0.015
0.001
0.015
0.081
0.015
0.253
15.94
umulative Ibs/acre
0.034
0.022
0.238
15.929
0.091
0.011
0.075
0.391
0.065
2.630
I
ermit PAN Limit (lbs/acre) 1st Cro /2nd Crop
202
t
t�
,D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0 r
6
)AMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
(SIGNATURE OF LAND APPLIER) DATE /I
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

'ACILITY NAME: DELTA APPAREL, INC., NC
)WNER: HAROLD SHERRILL
ITE #: NC CA 00020 FIELD# : CA 00020 0002
LESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HIWASSEE
PERMIT #: WQ0006984 ANNUAL DRY TONS APPLIED: 42.53
OPERATOR: WALLY SAINE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20.70 ACRES PERMITTED: 20.70
Page
Lane Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TI{N
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/6/16
204,600.00 (G)
9884.058
3.29
1.356
DAMPTXL
DRY
0-<I/2"
SUR
0.5
0.30
64,700.p
4,260.00 p
2.00 p
20264
FESCUE
4/8/16
105,400.00 (G)
5091.787
3.29
0.699
DAMPTXL
DRY
0-<1/2"
SUR
0.5
0.30
64,700. p
4,260.00 p
2.00 p
20264
FESCUE
Apr-16
1 310,000.00 (G)
14,975.845
"Total Ciallons/Ac: 14,975.85
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
83
0.012
0.008
0.062
3.226
0.021
0.002
0.021
0.099
0.021
0.415
23.13
umulative Ibs/acre
0.025
0.016
0.196
12.611
0.075
0.007
0.060
0.329
0.050
2.249
t t
ennit PAN Limit (lbs/acre) 1st Crop/2nd Crop
i '
F
1
s i
;
s
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
t i 375.0
89.0
2500.0 k
6
DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
X d7Z) -7
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infornation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
�ACILITY NAME: DELTA APPAREL, INC., NC PREDOMINANT SOIL SERIES: GASTON
)WNER: WAYNE GILBERT PERMIT #: W00006984 ANNUAL DRY TONS APPLIED: 26.37
ITE #: NC LT 00120 FIELD# : LT 00120 0001 OPERATOR: WAYNE GILBERT CATION EXCHANGE CAPACITY (NON-503):
:ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.90 ACRES PERMITTED: 13.90
Page
Lune Applied
***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
MONTH
3/30/16
142,600.00 (0)
10258.993
3.29
1.407
DAMPTXL
DRY
0-<1/2"
SUR
0.5
0.30
64,700.p
4,260.00 p
2.00 p
20264
I FESCUE
3/31/16
49,600.00 (G)
3568.345
3.29
0.490
DAMP=
DRY
0-<1/2"
SUR
0.5
0.30
64,700. p
4,260.00 p
2.00 p
20264
FESCUE
Mar-16
1 192,200.00 (G)
13,827.338
1
Dotal Gallons/Ac: 13,827.34
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
P
PAN
TOTALS:
Annuallbs/acre
F0.383
77
0.011
0.008
0.057
2.978
0.019
0.002
0.019
0.091
0.019
21.36
Cumulative Ibs/acre
0.076
1 0.065
0.474
33.526
1 0.274
0.016
0.175
1 0.996
0.103
`'
7.907 t. ': ;_
;
1
1
_
^.
.ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
-
r . i
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
ti
DAMPTXL = DELTA APPAREL, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
X fv-�rl 7- c it
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Itijectioti/Incorporation 1.0
* Application Method:. SUR -Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

EF{;+IRt_4tdfeSEN`!'AL a_r���6Lf�G1=5. sFd��
�3rfat� ircal Lahcrat�r:�F.s
April 18, 2016
Marshall Puryear
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Delta Apperall
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http:/hvww.settek.com
Dear Marshall Puryear: Order No.: 16032064
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/31/2016 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
�R ..PITZ
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North
Dakota R-201, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001,
Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 9957C
Page 1 of 32
Page 1 of 34

r, Summit Environmental Technologies, Inc. Case Narrative
ffi t� m 3310 Win St. 1
r-,IN rIPC1NMENUAL :ECPHOL IGIES, NC. Cuyahoga Falls, Ohio 44223 w0#: 16032064
ArrA1yb`:-31 Lnharai3rl 5 TEL: [phone] FAX: [phone]
Website: ho.-Ilviviv.settekcom Date: 4/18/2016
CLIENT: Synagro _
Project: Delta Apperall
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway
Haddock, GA 31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
The information contained in this analytical report is the sole property of Summit Enviromnental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency.
Any comments or problems with the analytical events associated with this report are noted below.
Analytical Comments for tclp-svoc-cpest tclp(8081), Sample 16032064-00lams, Batch ID 19729 : The
TCLP Pesticides MS (Batch 19729) exhibited high recovery for Heptachlor; All samples were ND.
Revision v1
Page 2 of 32
Page 2 of 34

Summit Environmental Technologies, Inc. Case Narrative
SUMMIT 3310 Win St.
M:rinoNMEhTAL'lMMOLLILG:ES,3PtC_ Cuyahoga Falls, Ohio44223 Wo#: 16032064
AP-zliytical LRbeorsio e5 TEL: [phone] FAX.- [phone]
Website: htfP.-1Avww.settek.com Date: 4/18/2016
CLIENT: Synagro
Project: Delta Apperall
Analytical Comments for telp-svoc-herb_telp(8151), Sample les-19797, Batch ID 19797 : The TCLP
Herbicides LCS (Batch 19797) exhibited high recovery for 2,4,5-TP; All reported samples were ND.
Analytical Comments for svoc-BNA_TCLP(8270), Sample LCS-19802, Batch ID 19802 : The TCLP
SVOC LCS (Batch 19802) exhibited outlying recoveries for Acid Compounds; The MS and MSD
exhibited control.
Revision vl
Page 3 of 32
Page 3 of 34

Summit Environmental Technologies, In
Qualifiers and Acronyms
Ir 3310 Win
rWVIROWAEWTu`.L I-MINOLQG1=5, NQ. Cuyahoga Falls, Ohio 4421 WO#: 16032064
A;7iilytrcal L'ahox9roFfe,: TEL: [phone] FAX.- (330) 253-446
Website: httD://www.settek.co. Date: 4/18/2016
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
BIMB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLA
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 4 of 32
Page 4 of 34

wr
Summit Environmental Technologies, Inc.
Workorder
3310 Win St.
Sample Summary
FUVIRONMEWAL G_C3 .0Lawi-s, wr_
Cuyahoga Falls, Ohio 44223
Arralytical LzboraiorlQS
TEL: [phone] FAX: [phone]
WO#: 16032064
Website: hQ.-lAvww.settek.com
31-Tan-17
CLIENT:
Synagro
Project:
Delta Apperall
Lab SampleID Client Sample ID Tag No Date Collected
Date Received Matrix
16032064-001
Delta
3/30/2016 10:00:00 AM
3/31/2016 12:15:00 PM Sludge
Page 5 of 32
Page 5 of 34

M9@_ Summit Environmental Technologies, Inc. 7
Ir 3310Win St. AnalyticalRepoPt
�_. t;rin�hllelENT L2_ i Fdr]Lt�€ cS; wc- Cuyahoga Falls, Ohio44223 (base report)
Art-3i,rti,_a! TEL: [phone] FAX. [phone] WO#: 16032064
Website: http://www.settek.com Date Reported: 4/18/2016
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/30/2016 10:00:00 AM
Lab ED: 16032064-001A
Project: Delta Apperall
Client Sample ID Delta
Analyses Result PQL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA-PEST/HERB-LIQUID
TCLP MERCURY ANALYSIS (1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA-PEST/HERB-LIQUID
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
RC I
FLASHPOINT (EPA 1010)
Flashpoint (200oF) >200
TCLP METALS, VOC, BNA-PEST/HERB-LIQUID
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1, 3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
101
Surr: Phenol-d6
95.0
Surr: Nitrobenzene-d5
106
Surr: 2,4,6-Tribromophenol
95.4
SW7470A SW7470A Analyst: ALJ
0.00200 mg/L 1 4/6/2016 5:05:32 PM
SW6010C SW3010A Analyst: VVK
0.500
mg/L
1
4/7/2016 1:46:27 PM
5.00
mg/L
1
4/7/2016 1:46:27 PM
0.100
mg/L
1
4/7/2016 1:46:27 PM
0.200
mg/L
1
4/7/2016 1:46:27 PM
0.500
mg/L
1
4/7/2016 1:46:27 PM
0.500
mg/L
1
4/7/2016 1:46:27 PM
0.500
mg/L
1
4/7/2016 1:46:27 PM
SW1010 Analyst: TAH
°F 1 4/4/2016 12:27:08 PM
SW8270C SW3510C Analyst: CxA
0.200
mg/L
2
4/14/2016 12:23:00 PM
0.500
mg/L
2
4/14/2016 12:23:00 PM
0.500
mg/L
2
4/14/2016 12:23:00 PM
0.200
mg/L
2
4/14/2016 12:23:00 PM
10.0
mg/L
2
4/14/2016 12:23:00 PM
0.200
mg/L
2
4/14/2016 12:23:00 PM
0.200
mg/L
2
4/14/2016 12:23:00 PM
0.200
mg/L
2
4/14/2016 12:23:00 PM
0.200
mg/L
2
4/14/2016 12:23:00 PM
0.500
mg/L
2
4/14/2016 12:23:00 PM
0.500
mg/L
2
4/14/2016 12:23:00 PM
10 - 109
%Rec
2
4/14/2016 12:23:00 PM
10 - 109
%Rec
2
4/14/2016 12:23:00 PM
19 - 120
%Rec
2
4/14/2016 12:23:00 PM
10 - 120
%Rec
2
4/14/2016 12:23:00 PM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
RL Reporting Detection Limit W Sample container temperature is out of limit as specified at testcode
Revision v1
Page 6 of 32
Page 6 of 34

5401W101T
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
FTWIrROMMENTALTEC3-NOLL.IG189,s^dC_
fn
Cuyahoga Falls, Ohio44223
(base report)
k.rraP;+ticaP Loboratories
TEL: (330)
253-8211 FAX: [phone]
WO#: 16032064
Website: http:AAwww.settekcom
Date Reported: 4/18/2016
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/30/2016 10:00:00 AM
Lab ID: 16032064-001A
Project: Delta Apperall
Client Sample ED Delta
Analyses Result
PQL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA-PEST/HERB-LIQUID
SW8270C
SW3510C Analyst: CxA
SVOC 8270 TCLP BNA LIST
Surr: 2-Fluorobiphenyl
109
22 - 117
%Rec
2 4/14/2016 12:23:00 PM
Surr: p-Terphenyl-d14
107
34 - 116
%Rec
2 4/14/2016 12:23:00 PM'
TCLP METALS, VOC, BNA-PEST/HERB-LIQUID
SW8081A
SW3510C Analyst: JBN
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total
ND
0.0250
mg/L
1 4/6/2016 8:27:00 PM
Toxaphene
ND
0.0500
mg/L
1 4/6/2016 8:27:00 PM
Endrin
ND
0.00250
mg/L
1 4/6/2016 8:27:00 PM
gamma-BHC
ND
0.00250
mg/L
1 4/6/2016 8:27:00 PM
Heptachlor
ND
0.00250
QM+ mg/L
1 4/6/2016 8:27:00 PM
Heptachlor epoxide
ND
0.00250
mg/L
1 4/6/2016 8:27:00 PM
Methoxychlor
ND
0.00250
mg/L
1 4/6/2016 8:27:00 PM
Surr: TCMX
99.7
5 - 119
%Rec
1 4/6/2016 8:27:00 PM
TCLP SVOC HERBICIDES FOR NPW(8151)
SW8151A
SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
ND
1.00
mg/L
1 4/12/2016 4:24:00 AM
2,4,5-TP
ND
0.100
QL+ mg/L
1 4/12/2016 4:24:00 AM
TCLP METALS, VOC, BNA-PEST/HERB-LIQUID
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
1,1-Dichloroethene
ND
0.100
mg/L
1 4/6/2016 12:01:00 PM
1,2-Dichloroethane
ND
0.100
mg/L
1 4/6/2016 12:01:00 PM
MEK
ND
2.00
mg/L
1 4/6/2016 12:01:00 PM
Benzene
ND
0.100
mg/L
1 4/6/2016 12:01:00 PM
Carbon tetrachloride
ND
0.100
mg/L
1 4/6/2016 12:01:00 PM
Chlorobenzene
ND
0.100
mg/L
1 4/6/2016 12:01:00 PM
Chloroform
ND
0.100
mg/L
1 4/6/2016 12:01:00 PM
Tetrachloroethene
ND
0.100
mg/L
1 4/6/2016 12:01:00 PM
Trichloroethene
ND
0.100
mg/L
1 4/6/2016 12:01:00 PM
Vinyl chloride
ND
0.200
mg/L
1 4/6/2016 12:01:00 PM
Surr: 4-Bromofluorobenzene
99.0
70 - 130
%Rec
1 4/6/2016 12:01:00 PM
Surr: Dibromofluoromethane
99.2
70 - 130
%Rec
1 4/6/2016 12:01:00 PM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
RL Reporting Detection Limit W Sample container temperature is out oflimit as specified at testcode
Revision vl
Page 7 of 32
Page 7 of 34

SUMMKOF
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
F-71V1;MAIEW"rALT-ECPXZOLGG1=s;Inc.
ED
Cuyahoga Falls, Ohio44223
(base report)
Elnattrcaf L;_f�eraiga'ie5
TEL: [phone] FAX.- [phone]
WO#: 16032064
Website: htty.-1Avww.settek.com
Date Reported: 4/18/2016
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/30/2016 10:00:00 AM
Lab ID: 16032064-001A
Project: Delta Apperall
Client Sample ID Delta
Analyses Result
PQL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA-PEST/HERB-LIQUID
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
Surr: Toluene-d8
98.5
70 - 130 %Rec
1 4/6/2016 12:01:00 PM
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)
Cyanide, Reactive
ND
0.500 mg/L
1 4/4/2016 2:21:00 PM
RCI
A4500-H+B
Analyst: DHC
PH (SM4 500-H+ B)
pH
7.69
s.u.@19.1C
1 415/2016 11:40:00 AM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (EPA 9034)
Sulfide, Reactive
ND
25.0 mg/L
1 4/4/2016 2:21:00 PM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
RL Reporting Detection Limit W Sample container temperature is out of limit as specified at testcode
Revision v1
Page 8 of 32
Page 8 of 34

=a Summit Environmental Technologies, Inc.fT, QC SUMMARY REPORT
% y o � � _ 3310 Win St.
tr;wlkra,rarni;r�I Ak 1 raatac LUGi�:s; INC. Cuyahoga Falls, Ohio 44223
?4,r, 3.tilPi':caf �?n191n�ips TEL: [phone] FAX.- [phone] WO#: 16032064
Wehsite: http:/hviviv.settelc.coni 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19729
Sample ID mb-19729
SampType: mblk
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 4/6/2016
RunNo: 52011
Client ID: PBW
Batch ID: 19729
TestNo: SW8081A SW3510C
Analysis Date: 4/6/2016
SegNo: 822537
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Chlordane, total
ND
0.0250
Toxaphene
ND
0.0500
Endrin
ND
0.00250
gamma-BHC
ND
0.00250
Heptachlor
ND
0.00250
Heptachlor epoxide
ND
0.00250
Methoxychlor
ND
0.00250
Surr: TCMX
57.6
50.00 115 5 119
Sample ID Ics-19729
SampType: Ics
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 4/6/2016
RunNo: 52011
Client ID: LCSW
Batch ID: 19729
TestNo: SW8081A SW3510C
Analysis Date: 4/6/2016
SegNo: 822538
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.0183
0.00250
0.0250
0
73.1
20
157
gamma-BHC
0.0178
0.00250
0.0250
0
71.4
22
137
Heptachlor
0.0176
0.00250
0.0250
0
70.2
24
121
Heptachlor epoxide
0.0177
0.00250
0.0250
0
70.9
27
152
Methoxychlor
0.0162
0.00250
0.0250
0
64.8
1
199
Surr: TCMX
32.2
50.00
64.4
5
119
Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Revision v1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 9 of 32
Page 9 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUA01"INT 3310 Win St.
�r;,v��cr�:r�buah IAI. r 9:h:9- RULCY,01`s, INC. Cuyahoga Falls, Ohio 44223
�tln,g(l M-csf LzboraforioF TEL: [phone] FAX.- [phone] WO#: 16032064
Website: htty://iv3vw.settelc.coni 31-Jan-17
Client: Synaglo
Project: Delta Apperall BatchID: 19729
Sample ID 16032064-001ams
SampType: ms
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 4/6/2016
RunNo: 52011
Client ID: Delta
Batch ID: 19729
TestNo: SW8081A SW3510C
Analysis Date: 4/6/2016
SegNo: 822539
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.0316
0.00250
0.0250
0
126
20
157
gamma-BHC
0.0280
0.00250
0.0250
0
112
22
137
Heptachlor
0.0309
0.00250
0.0250
0
123
24
121 S
Heptachlor epoxide
0.0302
0.00250
0.0250
0
121
27
152
Methoxychlor
0.0316
0.00250
0.0250
0
127
1
199
Surr: TCMX
59.4
50.00
119
5
119
Sample ID 16032064-001amsd
SampType: msd
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 4/6/2016
RunNo: 52011
Client ID: Delta
Batch ID: 19729
TestNo: SW8081A SW3510C
Analysis Date: 4/6/2016
SegNo: 822540
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Endrin
0.0285
0.00250
0.0250
0
114
20
157
0.0316
10.5
30
gamma-BHC
0.0259
0.00250
0.0250
0
104
22
137
0.0280
8.00
30
Heptachlor
0.0275
0.00250
0.0250
0
110
24
121
0.0309
11.3
30
Heptachlor epoxide
0.0277
0.00250
0.0250
0
ill
27
152
0.0302
8.96
30
Methoxychlor
0.0278
0.00250
0.0250
0
111
1
199
0.0316
12.9
30
Surr: TCMX
40.8
50.00
81.6
5
119
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision V1
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 10 of 32
Page 10 of 34

11 , Summit Environmental Technologies, Inc.
3310 Win St. QC SUMMARY REPORT
NZ0e:vlrrV1.4Wi;Nla,I,.tuuUi-- s,irte. Cuyahoga Falls, Ohio44223
A nztt;rtl�1 LTborgtofief TEL: [phone] FAX.- [phone] WO#: 16032064
Website: hgp.-Ilwivw.settelc.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID• 19731
Sample ID MB-19731
SampType: MBLK
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 4/6/2016
RunNo: 52306
-lient ID: PBW
Batch ID: 19731
TestNo: SW8270C SW3510C
Analysis Date: 4/13/2016
SegNo: 828359
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0200
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
1.82
Surr: Phenol-d6
1.79
Surr: Nitrobenzene-d5
2.01
Surr: 2,4,6-Tribromophenol
1.86
Surr: 2-Fluorobiphenyl
1.95
Surr: p-Terphenyl-d14
1.99
2.500
73.0
10
109
2.500
71.7
10
109
2.500
80.6
19
120
2.500
74.3
10
120
2.500
78.2
22
117
2.500
79.5
34
116
Sample ID LCS-19731
SampType: LCS
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 4/6/2016
RunNo: 52306
Client ID: LCSW
Batch ID: 19731
TestNo: SW8270C SW3510C
Analysis Date: 4/13/2016
SegNo: 828361
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank E Value above quantitation range
J Analyte detected below quantitation limits M Manual Integration used to determine
ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit ReV1510n Vl
PL Permit Limit R RPD outside accepted recovery limits Page 11 of 32
Page 11 of 34

Summit Environmental Technologies, Inc
St.. QC SUMMARY REPORT'
�} ,,�,.� 3310 Win St
trNITWINrnuN JAI. a 7:ti7frlrauts3ttS; INC. Cuyahoga Falls, Ohio 44223
Anafirtl.cRf >!>TboratDrie� TEL: [phone] FAX.- [phone] WO#: 16032064
Website: htto.-Mvww.settelr.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19731
Sample ID LCS-19731
SampType: LCS
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 4/6/2016
RunNo: 52306
-lient ID: LCSW
Batch ID: 19731
TestNo: SW8270C SW3510C
Analysis Date: 4/1312016
SegNo: 828361
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.896
0.100
1.000
0
89.6
10
134
2,4,5-Trichlorophenol
0.904
0.250
1.000
0
90.4
27
154
2,4,6-Trichlorophenol
0.953
0.250
1.000
0
95.3
27
154
2,4-Dinitrotoluene
0.974
0.0200
1.000
0
97.4
29
149
Cresols, Total
ND
5.00
3.000
0
60.3
20
125
Hexachloro-1,3-butadiene
0.819
0.0200
1.000
0
81.9
14
126
Hexachlorobenzene
0.900
0.0200
1.000
0
90.0
10
162
Hexachloroethane
0.814
0.100
1.000
0
81.4
30
123
Nitrobenzene
0.870
0.100
1.000
0
87.1
25
190
Pentachlorophenol
0.722
0.250
1.000
0
72.2
10
186
Pyridine
0.353
0.250
1.000
0
35.2
10
130
Surr: 2-Fluorophenol
1.94
2.500
77.5
14
110
Surr: Phenol-d6
1.90
2.500
76.1
10
110
Surr: Nitrobenzene-d5
2.01
2.500
80.3
11
110
Surr: 2,4,6-Tribromophenol
2.01
2.500
80.6
13
125
Surr: 2-Fluorobiphenyl
1.97
2.500
79.0
10
110
Surr: p-Terphenyl-d14
2.07
2.500
82.7
14
135
Sample ID 16040041-001AMSD
SampType: MSD
TestCode: svoc-BNA T Units: mg/L
Prep Date: 4/6/2016
RunNo: 52306
Client ID: BatchQC
Batch ID: 19731
TestNo: SW8270C SW3510C
Analysis Date: 4/13/2016
SegNo: 828364
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Revision V1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 12 of 32
Page 12 of 34

Sunimit Environmental Technologies, Inc. QC SUMMARY REPORT
: 3310 Wire St. 1. SUMMARY 1V1jVjliC\ Y REPORT
i\ 1
x� rarti:w i.A,r i rt,rta,.uLvt�s; rr.r Cuyahoga Falls, Ohio 44223
Ariat41t4caf L"Sb,1,rgTOrie,5 TEL: [phone] FAX.- [phone] WO#: 16032064
Website: httv:/hviviv.settek.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchlD: 19731
Sample ID 16040041-001AMSD
SampType: MSD
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 4/6/2016
RunNo: 52306
client ID: BatchQC
Batch ID: 19731
TestNo: SW8270C SW3510C
Analysis Date: 4/13/2016
SegNo: 828364
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene
0.838
0.200
1.000
0
83.8
10
134
0
0
30
2,4,5-Trichlorophenol
0.868
0.500
1.000
0
86.8
27
154
0
0
30
2,4,6-Trichlorophenol
0.915
0.500
1.000
0
91.5
27
154
0
0
30
2,4-Dinitrotoluene
0.925
0.0400
1.000
0
92.5
29
149
0
0
30
Cresols, Total
ND
10.0
3.000
0
61.9
20
125
0
0
30
Hexachloro-1,3-butadiene
0.764
0.0400
1.000
0
76.4
14
126
0
0
30
Hexachlorobenzene
0.879
0.0400
1.000
0
87.9
10
162
0
0
30
Hexachloroethane
0.783
0.200
1.000
0
78.3
30
123
0
0
30
Nitrobenzene
0.800
0.200
1.000
0
80.0
25
190
0
0
30
Pentachlorophenol
0.669
0.500
1.000
0
66.9
10
186
0
0
30
Pyridine
ND
0.500
1.000
0
43.3
10
130
0
0
30
Surr: 2-Fluorophenol
2.03
2.500
81.1
10
109
0
Surr: Phenol-d6
2.01
2.500
80.6
10
109
0
Surr: Nitrobenzene-d5
2.16
2.500
86.3
19
120
0
-
Surr: 2,4,6-Tribromophenol
2.28
2.500
91.1
10
120
0
Surr:2-Fluorobiphenyl
2.12
2.500
84.8
22
117
0
Surr: p-Terphenyl-d14
2.33
2.500
93.1
34
116
0
Sample ID 16040041-001AMS
SampType: MS
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 4/6/2016
RunNo: 52306
Client ID: BatchQC
Batch ID: 19731
TestNo: SW8270C SW3510C
Analysis Date: 4/13/2016
SegNo: 828368
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision V l
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 13 of 32
Page 13 of 34

SununitEnvironrnentalTechnologies, Inc. QC SUMMARY REPORT
t i 3310 Win St.
r +Ixp.r�rn N I=v: r t tne,�aLtrt]r.ts, rra:.. Cuyahoga Falls, Ohio 44223
Alrtaft�.t,'-uaf Labo,rgturir rs TEL: [phone] FAX.- [phone] WO#: 16032064
Website: htto:/hvrvw.settek.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19731
Sample ID 16040041-001AMS
SampType: MS
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 4/6/2016
RunNo: 52306
Client ID: BatchQC
Batch ID: 19731
TestNo: SW8270C SW3510C
Analysis Date: 4/1312016
SegNo: 828368
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene
0.571
0.200
1.000
0
57.1
10
134
2,4,5-Trichlorophenol
0.603
0.500
1.000
0
60.3
27
154
2,4,6-Trichlorophenol
0.635
0.500
1.000
0
63.5
27
154
2,4-Dinitrotoluene
0.637
0.0400
1.000
0
63.7
29
149
Cresols, Total
ND
10.0
3.000
0
37.2
20
125
Hexachloro-1,3-butadiene
0.553
0.0400
1.000
0
55.3
14
126
Hexachlorobenzene
0.597
0.0400
1.000
0
59.7
10
162
Hexachloroethane
0.561
0.200
1.000
0
56.1
30
123
Nitrobenzene
0.606
0.200
1.000
0
60.6
25
190
Pentachlorophenol
ND
0.500
1.000
0
47.4
10
186
Pyridine
ND
0.500
1.000
0
26.4
10
130
Surr: 2-Fluorophenol
1.44
2.500
57.7
10
109
Surr: Phenol-d6
1.46
2.500
58.2
10
109
Surr: Nitrobenzene-d5
1.61
2.500
64.2
19
120
Surr: 2,4,6-Tribromophenol
1.58
2.500
63.4
10
120
Surr:2-Fluorobiphenyl
1.56
2.500
62.6
22
117
Surr: p-Terphenyl-d14
1.57
2.500
62.7
34
116
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v1
Page 14 of 32
Page 14 of 34

SuAftamlot
Summit Environmental Technologies, Inc.
3310Win St.
QC SUMMARY REPORT
LNNIKVVNTAI.N111,1!:-C#lf9ULFJG1:S:Jtw Cuyahoga Falls, Ohio44223
I6n.�fVUcsf Laborgro,�ie:7 TEL: [phone] FAX.- [phone]
WO#: 16032064
Website: http✓linviv.settek.com
31-Jan-17
Client:
Synagro
Project:
Delta Apperall
BatchED: 19734
>ample ID MB-19734
SampType: MBLK
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 4/6/2016
RunNo: 52037
'lient ID: PBW
Batch ID: 19734
TestNo: SW6010C SW3010A
Analysis Date: 4/7/2016
SegNo: 823714
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-19734
SampType: LCS
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 4/6/2016
RunNo: 52037
;lient ID: LCSW
Batch ID: 19734
TestNo: SW6010C SW3010A
Analysis Date: 4/7/2016
SegNo: 823715
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Arsenic(As)
1.96
0.500
2.000
0
98.2
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
98.5
80
120
TCLP Cadmium(Cd)
1.97
0.100
2.000
0
98.6
80
120
TCLP Chromium(Cr)
1.96
0.200
2.000
0
98.1
80
120
TCLP Lead(Pb)
2.00
0.500
2.000
0
99.9
80
120
TCLP Selenium(Se)
1.99
0.500
2.000
0
99.4
80
120
TCLP Silver(Ag)
1.03
0.500
1.000
0
103
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit ReV1510ri Vl
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 15 of 32
Page 15 of 34

ITSummit Environmental Technologies, Inc. QC SUMMARY 0R1
3310 Win St. t
r ravlxwwbv;r;1 1. 9ta&97dC]LUi1t a; INC. Cuyahoga Falls, Ohio 44223
��nat.04r.Frr Lzboratrlr es TEL: [phone] FAX.- [phone] WO#: 16032064
Website: http://www.settelc.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19740
Sample ID MB-19740
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/6/2016
RunNo: 51997
Client ID: PBW
Batch ID: 19740
TestNo: SW7470A SW7470A
Analysis Date: 4/6/2016
SegNo: 822259
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury ND 0.00200
Sample ID LCS-19740
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/6/2016
RunNo: 51997
Client ID: LCSW
Batch ID: 19740
TestNo: SW7470A SW7470A
Analysis Date: 4/6/2016
SegNo: 822260
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury 0.00400 0.00200 0.00400 0 100 80 120
Sample ID 16032064-001AMS
SampType: MS
TestCode:
HG TCLP(74 Units: PPM
Prep Date: 4/6/2016
RunNo: 51997
Client ID: Delta
Batch ID: 19740
TestNo:
SW7470A SW7470A
Analysis Date: 4/6/2016
SegNo: 822264
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00410 0.00200 0.00400 0 103 75 125
Sample ID 16032064-001AMSD
SampType: MSD
TestCode: HG TCLP(74 Units: PPM
Prep Date: 4/6/2016
RunNo: 51997
Client ID: Delta
Batch ID: 19740
TestNo: SW7470A SW7470A
Analysis Date: 4/6/2016
SegNo: 822265
Analyte
Result
PQL SPK value SPK Ref Val
%REC LovvLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00407 0.00200
0.00400 0 102 75
125
0.00410 0.734 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to detennine
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit Revision V 1
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 16 of 32
Page 16 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
surnia,111- 3310 Win St.
-+ IHVIN511.NIAl. II. -CH ULQUlws,aINC, Cuyahoga Falls, Ohio44223
!1rta(v East LxbaxaloriEr� TEL: [phone] FAX.- [phone] WO#: 16032064
Website: hgp.-Ilivivtv.settelc.coni 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19740
Sample ID 16032064-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/6/2016
RunNo: 51997
Client ID: Delta
Batch ID: 19740
TestNo: SW7470A SW7470A
Analysis Date: 4/6/2016
SegNo: 822265
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
Page 17 of 34
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v1
Page 17 of 32

� Summit Environmental Technologies, ri,c.S, QC SUMMARY REPORT
Ed+, -r`, 3310 Win St.
Lra91iur.NrAroN Iut,.o r.�:;era�at.rt�tzs.; m;Z, Cuyahoga Falls, Ohio 44223 WO#: 16032064
akna,'lridcr I La barafo,ripu TEL: [phone] FAX.- [phone]
Website: hQ.-Ilivivw.setiefc.coni . 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19797
Sample ID mb-19797
SampType: mblk
TestCode: telp-svoc-her Units: mg/L
Prep Date: 4/5/2016
RunNo: 52341
Client ID: PBW
Batch ID: 19797
TestNo: SW8151A SW8151A
Analysis Date: 411112016
SegNo: 828624
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D ND 1.00
2,4,5-TP ND 0.100 -
Surr: DCAA 1050 2250 46.6 20 140
Sample ID Ics-19797
SampType: Ics
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 4/5/2016
RunNo: 52341
Client ID: LCSW
Batch ID: 19797
TestNo: SW8151A SW8151A
Analysis Date: 411112016
SegNo: 828625
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D
ND
1.00 0.450
0 96.9
37
105
2,4,5-TP
0.495
0.100 0.450
0 110
38
106 S
Surr: DCAA
2580
2250
115
20
140
Sample ID 16031562-001ams
SampType: ms
TestCode: telp-svoc-her Units: mg/L
Prep Date: 4/5/2016
RunNo: 52341
Client ID: BatchQC
Batch ID: 19797
TestNo: SW8151A SW8151A
Analysis Date: 4/1112016
SegNo: 828626
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D ND 1.00 0.450 0 90.9 37 105
2,4,5-TP 0.410 0.100 0.450 0 91.1 38 106
Surr: DCAA 2210 2250 98.4 20 140
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit ReV151ori V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 18 of 32
Page 18 of 34

Summit Environmental Technolo ies, Inc.
', sunim-ur 3310 Win St.
QC SUMMARY REPORT
ti 1HUI-•0,11.N IAL ;'1 ;KNULtl0itS1 JK . Cuyahoga Falls, Ohio 44223 WO#: 16032064
6.r?94.,PLv7P Laboratnfiea TEL: [phone] FAX. [phone]
Website: htto.Ilwivii,.settelc.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19797
Sample ID 16031562-001amsd
SampType: msd
TestCode: telp-svoc-her Units: mg/L
Prep Date: 4/5/2016
RunNo: 52341
Client ID: BatchQC
Batch ID: 19797
TestNo: SW8151A SW8151A
Analysis Date: 4/11/2016
SegNo: 828627
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D ND 1.00 0.450 0 89.2 37 105 0 0 30
2,4,5-TP 0.408 0.100 0.450 0 90.7 38 106 0.410 0.439 30
Surr: DCAA 2200 2250 97.7 20 140 0 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision Vl
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 19 of 32
Page 19 of 34

Summit Environmental Technologies, Inc. QC SUMMARY 1\lam' PORT
1 l� " ' 3310 Win St.
:viMcar+rah:AIAl, IIACH ULUGILS,IN . Cuyahoga Falls, Ohio44223
v d6nat4`fi:afff Labo;ratp,�k F TEL: [phone] FAX: [phone] WO#: 1G0320G4
Website: htto://wivw.settek.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19797
Sample ID 16031562-001ams
SampType: ms
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 4/5/2016
RunNo: 52230
Client ID: BatchQC
Batch ID: 19797
TestNo: SW8151A SW8151A
Analysis Date: 4/11/2016
SegNo: 826608
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDL]mit Qua]
2,4-D
ND
1.00 0.450
0 90.9
37
105
2,4,5-TP
0.410
0.100 0.450
D 91.1
38
106
Surr: DCAA
2210
2250
98.4
20
140
Sample ID 16031562-001amsd
SampType: msd
TestCode: telp-svoc-her Units: mg/L
Prep Date: 4/5/2016
RunNo: 52230
Client ID: BatchQC
Batch ID: 19797
TestNo: SW8151A SW8151A
Analysis Date: 4/11/2016
SegNo: 826609
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D
ND
1.00 0,450
0 89.2
37
105
0 0
30
2,4,5-TP
0.408
0.100 0.450
0 90.7
38
106
0.410 0.439
30
Surr: DCAA
2200
2250
97.7
20
140
0
30
Sample ID mb-19797
SampType: mblk
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 4/5/2016
RunNo: 52230
Client ID: PBW
Batch ID: 19797
TestNo: SW8151A SW8151A
Analysis Date: 4/11/2016
SegNo: 826632
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D
2,4,5-TP
Surr: DCAA
ND 1.00
ND 0.100
1050 2250
46.6 20 140
Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
ReV1S10ri Vl
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 20 of 32
Page 20 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
M1^ I17- 3310 Win St.
�rrvlrc� rrGn:ry IAI1 r 1:d 1%iQULSti31�S; AC. Cuyahoga Falls, Ohio 44223
WO#: 16032064
.t;7a.tk(ti,caf C.xhtr,r,=.atnFia6z TEL: [phone] FAX- [phone]
Website: http://wivw.settek.com 3I-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: 19797
Sample ID Ics-19797
SampType: Ics
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 4/5/2016
RunNo: 52230
Client ID: LCSW
Batch ID: 19797
TestNo: SW8151A SW8151A
Analysis Date: 4/11/2016
SegNo: 826633
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D ND 1.00 0.450 0 96.9 37 105
2,4,5-TP 0.495 0.100 0.450 0 110 38 106
Surr: DCAA 2580 2250 115 20 140
S
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit ReV1S10ri Vl
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 32
Page 21 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
M9 sumpan 3310 Win St.
ercwlxUIN61l.N I Al. 11 L'a�ati4aLotlt s'; irtw. Cuyahoga Falls, Ohio 44223
A„r ar (eflzsf Laborwturieo: TEL: [phone] FAX.- [phone] WO#: 16032064
Website: htip://www.settefc.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchlD: R51845
Sample ID LCS-R51845
SampType: LCS
TestCode: FlashPt_NP Units: T
Prep Date:
RunNo: 51845
'lient ID: LCSW
Batch ID: R51845
TestNo: SW1010
Analysis Date: 4/4/2016
SegNo: 819416
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Flashpoint (200°F)
115
120.0 0 95.8
90 110
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank B Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Revision v1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 22 of 32
Page 22 of 34

Summit Environmental Technologies,lrzc.QC SUMMARY REPORT
SRuralaNT 3310 Win St.
E;NA'1KV'NrnraNI+�.64r.�ata�raLtrt�t AU. Cuyahoga Falls, Ohio44223
FT
l•�SIk`G:u3P Laborwar-ie6 TEL: [phone] FAX- [phone] W0#: 16032064
Website: http://lviviv.settelf.coni 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: R51910
Sample ID 16040033-001ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: sm.@21.2C,
Prep Date:
RunNo: 51910
lient ID: BatchQC
Batch ID: R51910
TestNo: A4500-H+B
Analysis Date: 4/5/2016
SegNo: 821060
knalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
pH
7.65
7.650 0 10
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Revision v1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 23 of 32
Page 23 of 34

Summit Environmental Technologies, Inc. Q
U Iva i � - 3310 Win St. C SUMMARY REPORT
Ir;:vlK Q7NNIUN I RI, a takdrJOLU1Jk:S, JNUw Cuyahoga Falls, Ohio 44223
-dl.caf La boraroriou TEL: [phone] FAX.- [phone] WO#: 16032064
Website: hgp.•11www.se1tek.con2 31-Jmt-17
Client: Synagro
Project: Delta Apperall BatchID: R51910
Sample ID LCS-R51910
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@20.5C
Prep Date:
RunNo: 51910
Client ID: LCSW
Batch ID: R51910
TestNo: A4500-H+B
Analysis Date: 4/5/2016
SegNo: 820651
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.03 7.000 0 100 85 115
Sample ID 16032064-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@19.1C
Prep Date:
RunNo: 51910
Client ID: Delta
Batch ID: R51910
TestNo: A4500-H+B
Analysis Date: 4/5/2016
SegNo: 820653
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH 7.69 7.690 0 5
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Revision V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 24 of 32
Page 24 of 34

_ Suntnait Environmental Technologies, Inc. 3310 Win St. �J QC SUMMARY
Y T 1� n rL PORT
IH�a a I. 4 i'
;r err utuUt�s; ante. Cuyahoga Falls, Ohio44223
A �aIl.C2 csf Ln-bor ir]Fa@5 TEL: [phone] FAX.- [phone] WO#: 16032064
r+• �
Website: hav:Ilivww.settek.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchlD: R51929
Sample ID 16032066-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 51929
Client ID: BatchQC
Batch ID: R51929
TestNo: SW9014
Analysis Date: 4/4/2016
SegNo: 820998
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive 1.03 0.500 1.000 0.09400 93.4 85 115 H
Sample ID 16032066-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 51929
Client ID: BatchQC
Batch ID: R51929
TestNo: SW9014
Analysis Date: 4/4/2016
SegNo: 820999
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.06 0.500 1.000 0.09400 96.2 85 115 1.028 2.69 30 H
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to detennine
Revision V 1
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 25 of 32
Page 25 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
M-9 al 3310 [flin St.
t 1HQ Nrn N 1AI. N 1;A;HNULrJGU:S, TIC. Cuyahoga Falls, Ohio 44223 WO#: 16032064
A.r,.igyUwJ LaZl PrwtoF.re5 TEL: [phone] FAX.- [phone]
Website: hQ.-1 vivw.settekconz 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: R51929
Sample ID MB-R51929
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 51929
;Iient ID: PBW
Batch ID: R51929
TestNo: SW9014
Analysis Date: 4/4/2016
SegNo: 820995
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID LCS-R51929
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 51929
client ID: LCSW
Batch ID: R51929
TestNo: SW9014
Analysis Date: 4/4/2016
SegNo: 820996
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive 1.07 0.500 1.000 0 107 85 110
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision vl
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 26 of 32
Page 26 of 34

i Summit Environmental Technologies, Inc. 4 ° g I3310 win St.
QC SUMMARY REPORT'
�.�
tr,'A-1HUrarrn:N lAh a'Iaaa:rcaLdti3tes, INC. Cuyahoga Falls, Ohio 44223 WO#: 16032064
_ m_ ; 4 at4rdcal Lartaof�torF�S TEL: [phone] FAX.- [phone]
Website: htm://iviviv.settelc.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: R51936
Sample ID 16032066-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 51936
Client ID: BatchQC
Batch ID: R51936
TestNo: SW9034
Analysis Date: 4/4/2016
SegNo: 821234
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive 3940 25.0 3950 0 99.7 80 120 H
Sample ID 16032066-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 51936
Client ID: BatchQC
Batch ID: R51936
TestNo: SW9034
Analysis Date: 4/4/2016
SegNo: 821235
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 3930 25.0 3950 0 99.5 80 120 3940 0.254 30 H
Qualifiers: 'k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision v1
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 27 of 32
Page 27 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
""Itlinklar 3310 Win St.
vlrurarmr.IAL rI;G:HNIJUJUI�:ti,1KC. Cuyahoga Falls, Ohio44223 WO#: 16032064
A 4 naaVtj� �T LaZ;or9toFdev TEL: [phone] FAX.- [phone]
Website: htto://lvivw.settelc.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchED: R51936
Sample ID MB-R51936
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 51936
Client ID: PBW
Batch ID: R51936
TestNo: SW9034
Analysis Date: 4/4/2016
SegNo: 821232
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID LCS-R51936
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 51936
Client ID: LCSW
Batch ID: R51936
TestNo: SW9034
Analysis Date: 4/4/2016
SegNo: 821233
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive
3980 25.0 3950 0 101 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision V 1
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 28 of 32
Page 28 of 34

sm"Irl-
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
';*� 3310 Win St.
eW0Ixc1.rarn1u.IA[- fhL xCf,4L4C3rwa; INC Cuyahoga Falls, Ohio 44223
WO#: 16032064
,<k.nel1�4l,ca.f Cdxihcarqtraries TEL: [phone] FAX.- [phone]
Website: htto✓/wivw.settek.coni 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchID: R52021
Sample ID LCS 20PP13 VOC-S-
SampType: LCS
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 52021
:lient ID: LCSW
Batch ID: R52021
TestNo: SW8260B
Analysis Date: 4/6/2016
SegNo: 822715
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0198
0.00600
0.0200
0
99.0
71
138
Benzene
0.0189
0.00500
0.0200
0
94.4
75
137
Chlorobenzene
0.0190
0.00500
0.0200
0
94.9
77
132
Trichloroethene
0.0200
0.00500
0.0200
0
99.8
64
119
Surr: 4-Bromofluorobenzene
50.4
50.00
101
70
130
Surr: Dibromofluorom ethane
49.6
50.00
99.2
70
130
Surr: Toluene-d8
48.9
50.00
97.7
70
130
Sample ID
LCSD 20PPB VOC-S SampType: LCSD
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 52021
lient ID:
LCSS02 Batch ID: R52021
TestNo: SW8260B
Analysis Date: 4/6/2016
SegNo: 822716
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0190
0.00500
0.0200
0
94.8
71
138
0.0198
4.38 30
Benzene
0.0188
0.00500
0.0200
0
93.8
75
137
0.0189
0.691 30
Chlorobenzene
0.0185
0.00500
0.0200
0
92.6
50
150
0.0190
2.45 30
Trichloroethene
0.0189
0.00500
0.0200
0
94.5
64
119
0.0200
5.41 30
Surr: 4-Bromofluorobenzene
50.6
50.00
101
70
130
0 0
Surr:'Dibromofluoromethane
49.5
50.00
98.9
70
130
0 0
Surr: Toluene-d8
50.0
50.00
100
70
130
0 0
Qualifiers: 'k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit ReVIS10ri Vl
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 29 of 32
Page 29 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
4 it, 3310 Win St.
r +IrcQ!Nri N 1:u- o t:r:rallouvUIt :S, INC. Cuyahoga Falls, Ohio 44223 WO#: 16032064
- ?4.�tattrl;;ral C;Ttaar aro,�ir?� TEL: [phone] FAX [phone]
Website: http:/Avww.settelccom 31-Tan-17
Client: Synagro
Project: Delta Apperall BatchID: R52021
Sample ID MBLK
SampType: MBLK
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 52021
client ID: PBW
Batch ID: R52021
TestNo: SW8260B
Analysis Date: 4/6/2016
SegNo: 822717
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
48.5
Surr: Dibromof! uoromethane
51.2
Surr: Toluene-d8
49.2
50.00 96.9 70 130
50.00 102 70 130
50.00 98.4 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision Vl
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits' Page 30 of 32
Page 30 of 34

I s� Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
cc t IHQ N611 A IP6 i k.UH -0U LU I. :1� , INC. Cuyahoga Falls, Ohio 44223 WO#: 16032064
!6.�:3tyUi ai L;Toalatr��Ft r TEL: [phone] FAX [phone]
Website: hap.-Ilivrviv.settek..com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchED: R52021
Sample ID 16032064-001Ams
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 52021
,lient ID: Delta
Batch ID: R52021
TestNo: SW8260B
Analysis Date: 4/6/2016
SegNo: 822732
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.197
0.100
0.200
0
98.4
39.9
160
1,2-Dichloroethane
0.198
0.100
0.200
0
98.9
42.5
157
MEK
ND
2.00
1.00
0
111
16.6
227
Benzene
0.202
0.100
0.200
0
101
38.1
155
Carbon tetrachloride
0.186
0.100
0.200
0
92.9
40.8
162
Chlorobenzene
0.201
0.100
0.200
0
101
35.7
168
Chloroform
0.201
0.100
0.200
0
100
18.3
199
Tetrachloroethene
0.205
0.100
0.200
0
103
10
261
Trichloroethene
0.201
0.100
0.200
0
101
23.8
175
Vinyl chloride
0.223
0.200
0.200
0
111
10
165
Surr:4-Bromofluorobenzene
489
500.0
97.9
84.6
130
Surr: Dibromofluoromethane
496
500.0
99.3
71.4
127
Surr: Toluene-d8
491
500.0
98.2
74.6
127
Sample ID 16032064-001Amsd
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 52021
client ID: Delta
Batch ID: R52021
TestNo: SW8260B
Analysis Date: 4/6/2016
SegNo: 822733
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.192
0.100
0.200
0
96.2
39.9
160
0.197
2.26
25
1,2-Dichloroethane
0.207
0.100
0.200
0
104
42.5
157
0.198
4.59
25
MEK
ND
2.00
1.00
0
118
16.6
227
0
0
25
Benzene
0.206
0.100
0.200
0
103
38.1
155
0.202
2.06
25
Qualifiers: ;k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision V 1
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 31 of 32
Page 31 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Zwrr
, 3310 Win St.
LN'A-1KFJ;r-+r11:M l} k 0 f.i;H ULrj0R:s, JK . Cuyahoga Falls, Ohio 44223 WO#: 16032064
11 wly l.rsf Laboralur,, 8 TEL: [phone] FAX.- [phone]
Website: http:/hvww.settelc.com 31-Jan-17
Client: Synagro
Project: Delta Apperall BatchED: R52021
Sample ID 16032064-001Amsd
SampType: MSD
TestCode: TCLP-VOC-M Units: mg1L
Prep Date:
RunNo: 52021
'lient ID: Delta
Batch ID: R52021
TestNo: SW8260B
Analysis Date: 4/6/2016
SegNo: 822733
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDL]mit Qua]
Carbon tetrachloride
0.190
0.100
0.200
0
94.8
40.8
162
0.186
2.08 25
Chlorobenzene
0.201
0.100
0.200
0
101
35.7
168
0.201
0 25
Chloroform
0.205
0.100
0.200
0
102
18.3
199
0.201
1.97 25
Tetrachloroethene
0.199
0.100
0.200
0
99.4
10
261
0.205
3.07 25
Trichloroethene
0.197
0.100
0.200
0
98.6
23.8
175
0.201
2.16 25
Vinyl chloride
0.234
0.200
0.200
0
117
10
165
0.223
5.03 25
Surr:4-Bromofluorobenzene
484
500.0
96.8
84.6
130
0 25
Surr: Dibromofluoromethane
514
500.0
103
71.4
127
0 25
Surr: Toluene-d8
488
500.0
97.5
74.6
127
0 25
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank B Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Revision V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 32 of 32
Page 32 of 34

mSummit Environmental Tediliologie.s, Inc.
3310 \Nqil Stre�i Analysis Request/Chain of Custody
Cud tlur a Palls, Ohin 223 Tel: 330,253.82 11 Fax: [phone] Four SUIDI'llit Environmental Teditiologies- Inc. u.,;e ()Illy
=11111.11)y Name flllcwsc prinl)
Pr7lecl Name
Page
IllIS Fri - No.
Analytical Para.meteri and Methods
L
Con pany Ad
X
Vrojmi Address
:0
JL
Clicot Phone No. S
Report to
o
14
00.
-Client Fax No. please F,
C7,
si 11 11, clicill Email
Quote No.
CAI
coriutcl soon p
All
Sampled by
Check if Ohio ' AP SninplLs V
M L2
#
z-
CD
0
h

DC-T 02/16116
Rim 15
Summit Environmental Technologies, Inc.
Cooler Receipt Form
Initials of person inspecting(( cooler and samples:
1(00`7 ' 0 L }
Client
I I
Order Number.
Date Received: Time Received;
Date cooler(s) opened and samples Inspected:
Number of Coolers/Boxes:
N/A
Shipper. F UPS DHL Airborne US Postal Walk-in Pickup Other.
Packaging: Peanuts B I�Y et, Paper Foam None Other
Tape on cooler/box:
N NIA
Custody Seals intact
Y N
C-O-C in plastic
CY- N NIA
Ice Blue Ice
present 1,a6se . / melted NIA
Sample Temperature IR Gun #16020459 CF
� U `C t � " � 'C WA
Radiological Testing Instrument serial n35127
Y 6U NIA
(see page 2 for scan results)
-Use 1 sheet per sample for Radiological Testing. If sample Is NOT, the Radiological Safety Officer must be notified
Immediately.
C-O•C filled out properly
C N NIA
Samples in separate bags
(Y_� N NIA
Sample containers intact'
Y N NIA
'If no, list broken sample(s):
Sample label(s) complete (ID, date, etc.)
Y
N
N/A
G
Label(s) agree with O-C
Y
N
N/A
Correct containers used
N
NIA
Sufficient sample received
(Y
N
NIA
Samples received within holding time
N
Bubbles absent from 40 mL vials"
Y
N
NIA
" Samples with bubbles <Smm are acceptable.
Indicate bubble size if >6mm.
Was client contacted about samples
Y N
Will client send new samples
Y N
Client contact,
DateMme:
Logged in by:
Page 1 of 2
Page 34 of 34

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name Delta Apparel, Inc. Permit Number WQ0006984
WWTP Name Delta Apparel, Inc. WVdTP NPDES # NC0006190
1
Monitoring Period: From 01/01/16 To 12/31/16
Pathogen Reduction (40CFR 503.32) - Please indicate level achieved and alternative performed
Class A
Alternative 1 Alternative 2 Alternative 3
Class B
Alternative 4
Alternative 1
Alternative 5
Alternative 2
Alternative 6
Alternative 3
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens";
Aerobic Dig. Air Dry Anaerobic Dig. Compost Lime Stab.
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable
Pathogen Dens i
No. of
Freq. Of
Sample
Analytical
Level in
Exceed
Analysis
Type
Tech.
Sludge
Min. Geo. Max. Units
Mean
Fecal
2x106
MPN/g
Coliform
MPN/g or
2x106
CFU/g
CFU/g
1000
MPN
MPN/g
Salmonella
3 MINI
bacteria
4 g
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed
Option 1 Option 2 Option 3 Option 4 Option 5
Option 6 Option 7 Option 8 Option 9 Option 10
No vector attraction options were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law that the athogen requirements In 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CVR 503.33phave not been met." (Please note if you check this statement
attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the athogen and
vector attraction reduction requirements have been met. I am aware that there are significant penalties For false
certification including fine and imprisonment."
Preparer Name and Title Land Applier Naine and Title (if applicable)
Signature of Preparer Date Signature of Land Applier (if applicable) Date
Pathogen and Vector Attraction Reduction is not required by permit, no
signatures required.

Agricultural Lime Application Log
Year: 2016
Project: Delta Apparel
Field Soil Lime Requirement Tons/Acre Date Applied
(state-county-site-Feldl qH (from soil analvsislF Tons/Acre
Eq.) il
CA-6-2
6.0
O.OT/Ac.
CA-6-3
5.9
0.8T/Ac.
CA-20-1
5.9
0.8T/Ac.
CA-20-2
5.7
0.8T/Ac.
LT-120-1
6.5
O.OT/Ac.
*Lime will be applied when conditions improve.

Page 1 of 2
Report Number: 17-027-0554
Account Number:46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoint
ANALYTICAL
"Every acre... Every year. "rM
SOIL ANALYSIS REPORT
Date Received: 01/27/2017 Date Of Analysis: 01/30/2017 Date Of Report: 01/31/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Grower: Dennis Lutz
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
e �°
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
CA-6-2
16787
8.5
150
61 H
66 L
202 VH
688 M
43 L
6.0
1.0
6.5
I MIN
VH
NC = 51
NC = 34
CA-6-3
16788
8.3
150
53 H
70 L
231 VH
612 L
36 L
5.9
6.82
1.1
6.4
MIN
VH
NC = 44
NC = 36
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
CA-6-2
2.6
25.9
52.9
2.9
15.4
14 L
3.7 H
95 VH
118 VH
6.2 VH
0.4 L
0.11 VL
NC=29
NC=92.5
NC=594
NC=310.0
CA-6-3
2.8
30.1
47.8
2.4
17.2
10 L
2.5 M
142 VH
84 VH
3.1 VH
0.3 VL
0.11 VL
1
1
NC=21
NC=62.5
NC=888
NC=155.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: ?,wi;, mF GaN-r
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble
Analysts prepared by: WaypolntAnalytical Virginia, Inc.
C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm.
Pauric McGroary

Page 2 of 2
Report Number: 17-027-0554
Account Number:46493
Waypoint 7621 0 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax [phone]
Send To: Synagro Central LLC/ Statesville ANALYTICAL www.waypointanalytical.com
Mary Brewer "Every acre... Every year."TM Grower: Dennis Lutz
284 Boger Road
Mocksville NC 27028
Date Received: 01/27/2017
Date Of Report: 01/31/2017 SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
CA-6-2
Adjust pH to 6.0
0
0.0
0
0
0
CA-6-3
Adjust pH to 6.0
0
0.8
0
0
0
Comments
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 1 of 2
Report Number: 17-027-0555
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville INC 27028
Date Received: 01/27/2017
Waypoint.0
ANALYTICAL
"Every acre... Every year.'4M
SOIL ANALYSIS REPORT
Date Of Analysis: 01/30/2017 Date Of Report: 01/31/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Grower: Wally Saine
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
o �°
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
CA-20-1
16789
7.9
150
144 VH
218 VH
204 H
806 M
30 VL
5.9
6.80
1.3
7.7
I MIN
VH
NC = 120
NC = 112
CA-20-2
16790
4.9
142
26 L
117 VH
113 H
383 L
46 M
5.7
6.84
0.9
4.3
MH
NC = 22
NC = 60
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO,N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm
Rate
CA-20-1
7.3
22.1
52.3
1.7
16.9
12 L
11.2 VH
34 H
254 VH
3.3 VH
0.3 VL
0.12
VL
NC=25
NC=280.0
NC=213
NC=165.0
CA 20-2
7.0
21.9
44.5
4.7
20.9
14 L
3.8 H
74 VH
94 VH
2.9 H
0.1 VL
0.08
VL
1
NC=29
NC=95.0
NC=463
NC=145.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by. haw« o
C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm.
Analysis prepared by: Waypoint Analytical Virginia, Inc.
Pauric McGroary

Page 2 of 2
Report Number: 17-027-0555 '
Account Number:46493
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 ° Fax [phone]
Send To: Synagro Central LLC/ Statesville ANALYTICAL www.waypointanalytical.com
Mary Brewer "Every acre... Every year. Grower: Wally Saine
284 Boger Road
Mocksville NC 27028
Date Received: 01/27/2017
Date Of Report: 01/31/2017 SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
CA-20-1
Adjust pH to 6.0
0
0.8
0
0
0
CA-20-2
Adjust pH to 6.0
0
0.8
0
0
0
Comments
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 1 of 1
Report Number: 17-027-0553
Account Number:46493
Waypointo
Send To: Synagro Central LLC/ Statesville ANALYTICAL
Mary Brewer "Every acre... Every year. "m,
284 Boger Road
Mocksville NC 27028
SOIL ANALYSIS REPORT
Date Received: 01/27/2017 Date Of Analysis: 01/30/2017 Date Of Report: 01/31/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Wayne Gilbert
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
°
�°
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meg1100g
meq/100g
LT-120-1
16786
7.9
150
10 VL
68 L
287 VH
803 M
31 VL
6.5
0.5
7.2
IMIN
VH
NC = 8
NC = 35
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO,N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
LT-120-1
2.4
33.2
55.8
1.9
6.9
7 VL
1.8 L
93 VH
63 VH
4.0 VH
0.4 L
0.11 VL
NC=15
NC=45.0
NC=581
NC=200.0
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Date Received: 01/27/2017
Date Of Report: 01/31/2017
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: waypointAnalytical Virginia, Inc.
Salts ms/cm x 640 = ppm.
SOIL FERTILITY RECOMMENDATIONS
by: IV 6CONr
Pauric McGroary
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
KO
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
lb/A
LT-120-1
Adjust pH to 6.0
0
0.0
0
0
0
Comments
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.

RECEIVEDINCDENRIDWR
�i\,,AR 8 Z016
WQROS
MOORESVILLE REGIONAL OFFICE
,i 7 � 9;i�' -,
DELTA APPAREL, INC. — IUTAIGE�9', NC-D
RESIDUALS LAND APPLICAT19ttRM. WM
Permit No. WQ0006994`,`-G"iC)`l
2015 ANNUAL REPORT

ANNUAL. LAND APPLICATION CERTIFICATION FORT.
WQ Permit t WOOON984 County Catawba Year 2015
Facility Name (as shown on permit) Delta Angel. IncJMaiden Plant NPDES No. NC0006190
Land Application Operator &j@gm Phone# LEM 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
YES X NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A— ResidualsA.pplication Summary:
Total number of application fields in the permit:
Toted number of fields utilized for land application during the year.
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilized for land application during the year
Part B — Annual Compliance Statement
not limited to items
`0 own
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No nmoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification•
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief; true, accurate, and complete. ]
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations"
SteveSdaugbter Plant Manager a-18,a01
Permittee Name and Title (type or print) S of 'flee Date
Signature of preparce Date Signature of Land Applier Date
(if different Born Pemuttee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 02T .1102 (26) DENR FORM ACF (12 2006)