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HomeMy WebLinkAboutWQ0016376_Monitoring - 06-2020_20201027FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page of _k- Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa County: Duplin Month: June Year: 2020 PPI: 001 Flow Measuring Point: __. Influent L�j Effluent No now generated Parameter Monitoring Point: Influent Effluent ❑ Groundwater Lowering ❑ Surface Water Parameter Code 0 50050 00310 00940 50060 31616 00610 0L0625 00620 00600 00400 00665 70300 3!0 0N'NN5 0 > y U C N ~ O L N d 'D �d > C W U E ._ U C E Q C 0a) CD Y a) d OCL ZO O 0U a > nrn t'0 24-hr hrs GPD mg/L mg/L mg/L #/100 mL mg/L mg/L mg/L mg/L su mg/L mg/L mg/L 1 07:00 10 68.970 2 07:00 10 72,010 3 07:00 10 77,890 4 07:00 10 78,970 5 07:00 10 80,010 6 07:00 10 78,900 7 00:00 0 20,000 8 07:00 10 71,280 9 07:00 10 80,100 10 07:00 10 79,280 11 07:00 10 79,220 12 07:00 10 79,890 131 07:00 10 72,890 141 00:00 0 20,000rN 151 07:00 10 70,820 1Vj 16 07:00 10 81,980 17 07:00 10 78,170 S S 18 07:00 10 78,700 Q 19 07:00 10 69,110 (� 20 00:00 0 20,000 21 00:00 0 20,000 22 07:00 10 69,280 23 07:00 10 73,700 24 07:00 10 75,080 25 07:00 10 83,110 26 07:00 10 80,780 27 07:00 10 71,780 28 00:00 0 20,000 29 07:00 10 78,920 80 45 29500 64.3 65.1 <0.02 65.1 7.03 7.79 284 86 30 07:00 10 79,180 31 Average: 67,001 80.00 45.00 29.500.00 64.30 65.10 0.00 65.10 7.79 284.00 86.00 Daily Maximum: 83,110 80.00 45.00 29,500.00 64.30 65.10 0.02 65.10 7.03 7.79 284.00 86.00 Daily Minimum: 20,000 80.00 45.00 29,500.00 64.30 65.10 0.02 65.10 7.03 7.79 284.00 86.00 Sampling Type: Recorder Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Monthly Avg. Limit: 100,260 Daily Limit: Sample Frequency: Recorder Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page __�, - of A - Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa County: Duplin Month: June Year: 2020 PPI: 002 Flow Measuring Point: Influent 2 Effluent ] No Flow generated Parameter Monitoring Point: Influent ❑ Effluent ❑ Groundwater Lowering ❑ Surface water Parameter Code 11. 50050 00625 00610 00620 00665 31616 00600 > cc > Q E U~ 0 o C O y E d F U O 3 o LL t R C y mat Y o �- Z 0 I c o E Q y M Z U) z o o o ~ 0 t a d LL 0 U C y 0 0 Z 24-hr hrs GPD mg/L mg/L mg/L mg/L #/100 mL mg/L 1 1 07:00 10 68,970 2 07:00 10 72,010 3 07:00 10 77,890 4 07:00 10 78,970 5 07:00 10 80,010 6 07:00 10 78,900 7 00:00 0 20,000 8 07:00 10 71,280 9 07:00 10 80,100 10 07:00 10 79,280 11 07:00 10 79,220 12 07:00 10 79,890 13 07:00 10 72,890 14 00:00 0 20,000 15 07:00 10 70,820 16 07:00 10 81,980 17 07:00 10 78,170 18 07:00 10 78,700 19 07:00 10 69,110 20 00:00 0 20,000 21 00:00 0 20,000 22 07:00 10 69,280 231 07:00 10 73,700 24 07:00 10 75,080 25 07:00 10 83,110 26 07:00 10 80,780 27 07:00 10 71,780 28 00:00 0 20,000 29 07:00 10 78,920 1.4 0.5 0.87 0.18 105 30 07:00 10 79,180 31 Average: 67,001 1.40 0.50 0.87 0.18 105.00 Daily Maximum: 83,110 1.40 0.50 0.87 0.18 105.00 Daily Minimum: 20,000 1.40 0.50 0.87 0.18 105.00 Sampling Type: Recorder Grab Grab Grab Grab Grab Monthly Avg. Limit: Daily Limit: Sample Frequency: Recorder Monthly Monthly Monthly Monthly Monthly FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page J of Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa County: Duplin Month: June Year: 2020 PPI: 003 Flow Measuring Point: _ Influent Effluent ❑ No Flow generated Parameter Monitoring Point: ❑ Influent ❑Effluent ❑Groundwater Lowering ❑ Surface water Parameter Code 0 50050 00625 00610 00620 00665 31616 00600 j ` Q E O C O y E a; P- O 3 2Y LL E M C d M o _ :� Z F M C o E E Q y .. Z V) n m t o a H a E �c o - LL p U C A rn o 2 H ... Z 24-hr hrs GPD mg/L mg/L mg/L mg/L #/100 mL mg/L 1 07:00 10 68,970 2 07:00 10 72,010 3 07:00 10 77,890 4 07:00 10 78,970 5 07:00 10 80,010 6 07:00 10 78,900 7 00:00 0 20,000 8 07:00 10 71,280 9 07:00 10 80,100 10 07:00 10 79,280 11 07:00 10 79,220 121 07:00 10 79,890 13 07:00 10 72,890 14 00:00 0 20,000 15 07:00 10 70,820 16 07:00 10 81,980 17 07:00 10 78,170 181 07:00 10 78,700 19 07:00 10 69,110 20 00:00 0 20,000 21 00:00 0 20,000 22 07:00 10 69,280 23 07:00 10 73,700 24 07:00 10 75,080 25 07:00 10 83,110 26 07:00 10 80,780 27 07:00 10 71,780 28 00:00 0 20,000 29 07:00 10 78,920 1.7 1.1 0.03 0.15 160 30 07:00 10 79,180 31 Average: 67,001 1.70 1.10 0.03 0.15 160.00 Daily Maximum: 83,110 1.70 1.10 0.03 0.15 160.00 Daily Minimum: 20,000 1.70 1.10 0.03 0.15 160.00 Sampling Type: Recorder Grab Grab Grab Grab Grab Monthly Avg. Limit: Daily Limit: Sample Frequency: Recorder Monthly Monthly Monthly Monthly Monthly FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page ( of Sampling Person(s) Name: GERALD LAMAR MATTHEWS Name Certified Laboratories Name: Environmentat Chemists INC. Name: Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? M Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: GERALD LAMAR MATTHEWS Permittee: SAM VILLARI Certification No.: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Official's Title: OWNER Has the ORC changed since the previous NDMR? yes ❑ No Phone Number: 910-293-2157 Permit Expiration: 11/30/2025 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _I- of Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: June Year: 2020 Field Name: 1 Field Name: 2 Field Name: 3 Field Name: 4 Did irrigation occur Area (acres): 0.65 Area (acres): 1.16 Area (acres): 1.12 Area (acres): 1.07 at this facility? Cover Crop:OATS Cover Crop: P� OATS Cover Crop: P� OATS Cover Cro P� OATS ❑ YES ❑ NO Hourfy Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated? /I YES NO Field Irrigated? YES ❑ NO Field Irrigated? YES `, No Field Irrigated? 0 YES ❑ NO T O V d m E o % CL ' a c C d W o A 0) O O d v Ed ° i v _ rn J E rn O m a E 0 7G O CL > Q o (P 0)E T` 0)d %O ° v E 00- a ' rn E rn O O m� E 3 m O °'~ icc 'a m •w 0)E G� vC M O J rn C_ 7`0 X oX 0 J 3: °F in in in gal min in in gal min in in gal min in in gal min in in 1 C 8,220 23 0.47 0.47 14,669 42 0.47 0.47 14,163 40 0.47 0.47 13,531 39 0.47 0.47 2 C 54 0 7,794 23 0.44 0.44 13,910 42 0.44 0.44 13,430 40 0.44 0.44 12,830 39 0.44 0.44 3 C 3,864 12 0.22 0.22 6,896 21 0.22 0.22 6,658 20 0.22 0.22 6,361 19 0.22 0.22 4 C 7,297 21 0.41 0.41 13,022 38 0.41 0.41 12,573 36 0.41 0.41 12,011 35 0.41 0.41 5 C 7,725 23 0.44 0.44 13,786 42 0.44 0.44 13,310 40 0.44 0.44 12,716 39 0.44 0.44 6 R 0.01 7 C 8 C 3,931 12 0.22 0.22 7,015 21 0.22 0.22 6,773 20 0.22 0.22 6,471 19 0.22 0.22 9 C 3,084 12 0.17 0.17 5,504 21 0.17 0.17 5,315 20 0.17 0.17 5,077 19 0.17 0.17 10 CL 5,591 21 0.32 0.32 9,978 38 0.32 1 0.32 9,634 36 0.32 0.32 9,204 35 0.32 0.32 11 R 1 12 C 13 C 14 C 151 C 16 R 0.02 17 C 18 C 19 CL 20 C 211 C 221 C 23 C 24 C 7,843 23 0.44 0.44 13,997 42 0.44 0.44 13,514 40 0.44 0.44 12,911 39 0.44 0.44 25 R 0.02 26 R 0.03 27 C 281 C 29 C 66 0 7,085 23 0.40 0A0 13,644 42 0.43 0.43 12,208 40 0.40 0.40 11,663 39 0.40 0.40 30 C 4,995 16 0.28 0.28 8,914 29 0.28 0.28 8,607 28 0.28 0.28 8,222 27 0.28 0.28 31 Monthly Loading: 67,429 3.82 121,335 3.85 116,185 3.82 110,997 3.82 12 Month Floating Total (in): 17.42 17.42 17.42 17.42 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: June Year: 2020 Did irrigation occur Field Name: 5 Field Name: 6 Field Name: 7 Field Name: 8 Area (acres): 1.19 Area (acres): 1.17 Area (acres): 1.05 Area (acres): 1.25 at this facility? Cover Crop:OATS Cover Crop: P: OATS Cover Crop: P� OATS Cover Cro P� OATS ❑ YES P1 NO Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated? ',J YES ❑ NO Field Irrigated? YES ❑ NO Field Irrigated? ❑ YES ` NO Field Irrigated? ❑✓ YES ❑ NO m 'o O VO. t d m � 16 1= I— _00 i6 O. N o`. c m O OI p J (A rn O W C N O- 0 0.i Q N .d„ 01 ~ C f6 J= E Tay 7` C K 0 IC J d-o N O.o. i Q � 01 r £ 01 ~_ rn T c 16 J= E T rn 7` C X O 10 J dv N O' i Q N d 0) ~ >+ M J= >, ` X O /6 J £ N 3 Q 9 Q a N w ~ rn T lC J= E X O <6 J 3 OF in in in gal min in in gal min in in gal min in in gal min in in 1 C 15,048 43 0.47 0.47 14,795 42 0.47 0.47 13,278 38 0.47 0.47 15,807 45 0.47 0.47 2 C 54 0 14,269 43 0.44 0.44 14,030 42 0.44 0.44 12,591 36 0.44 0.44 14,989 45 0.44 0.44 3 C 7,074 21 0.22 0.22 6,955 21 0.22 0.22 6,242 19 0.22 0.22 7,431 22 0.22 0.22 4 C 13,358 39 0.41 0.41 13,134 38 0.41 0.41 11,787 34 0.41 0.41 14,032 40 0.41 0.41 5 C 14,142 43 0.44 0.44 13,905 42 0.44 0.44 12,478 1 38 0.44 0.44 14,855 45 0.44 0.44 61 R 1 0.01 7 C 8 C 7,196 21 0.22 0.22 7,075 21 0.22 0.22 6,350 19 0.22 0.22 7,559 22 0.22 0.22 9 C 5,647 21 0.17 0.17 5,552 21 0.17 0.17 4,982 19 0.17 0.17 1 5,931 22 0.17 0.17 10 CL 10,236 39 0.32 0.32 10,064 38 0.32 1 0.32 9,032 34 1 0.32 0.32 10,752 40 0.32 0.32 11 R 1 121 C 13 C 14 C 15 C 16 R 0.02 17 C 18 C 191 CL 201 C 21 C 22 C 23 C 24 C 14,359 43 0.44 0.44 14,118 42 0.44 0.44 12,670 38 0.44 0.44 15,083 45 0.44 0.44 25 R 0.02 261 R 1 0.03 27 C 28 C 29 C 66 0 12,971 43 0.40 0.40 12,753 42 0.40 0.40 11,445 38 0.40 0.40 13,626 45 0.40 0.40 30 C 9,145 30 0.28 0.28 8,991 29 0.28 0.28 8,069 26 0.28 0.28 9,606 31 0.28 0.28 31 Monthly Loading: 123,445 3.82 121,372 3.82 108,924 3.82 129,671 3.82 12 Month Floating Total (in): 17.42 17.42 17.42 17.42 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page j__ of Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: June Year: 2020 Did irrigation Field Name: 9 Field Name: 10 Field Name: 11 Field Name: 12 occur Area (acres): 1 Area (acres): 1.46 Area (acres): 1.43 Area (acres): 1.23 at this facility? Cover Crop:OATS Cover Crop: P� OATS Cover Crop: P� OATS Cover Crop: P� OATS 0 YES No Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated? YES J NO Field Irrigated? YES ] No Field Irrigated? YES J No Field Irrigated? YES No o m d Q c 0 U ` a c m m° J fn O x m y E p O� Q H C rn �6 D a O J E rn �6 X o M R= O J d v E p Q Q v N .� C _ rn >+c A C3 M O J E rn 3_ c x o 16 �p = O 2 J d a E G1 p Q % Q v N L _ rn >.c 'a 16 C3 M O J E T U) 7` C_ XM o v t6 = O 2 J m y E d p Q i Q a N ` _ rn T c 16 C a O J E T rn 3- c x o rp = O J °F in in in gal min in in gal min in in gal min in in gal min in in 1 C 12,645 36 0.47 0.47 18,462 53 0.47 0.47 18,083 51 0.47 0.47 15,554 44 0.47 0.47 2 C 54 0 11,991 36 0.44 0.44 17,507 53 OA4 0.44 17,147 51 0.44 0.44 14,749 44 0.44 0.44 3 C 5,945 18 0.22 0.22 8,660 26 0.22 0.22 8,501 26 0.22 0.22 7,312 22 0.22 0.22 4 C 11,226 32 OA1 0.41 1 16,389 47 0.41 0.41 16,053 46 0.41 0.41 13,808 40 0.41 0.41 5 C 1 11,884 36 0.44 0.44 17,351 53 1 0.44 0.44 16,995 1 51 0.44 1 0.44 14,618 1 44 0.44 0.44 6 R 0.01 7 C 8 C 6,047 18 0.22 0.22 8,829 26 0.22 0.22 8,648 26 0.22 0.22 7,438 22 0.22 0.22 9 C 4,745 18 0.17 0.17 6,928 26 0.17 0.17 6,786 26 0.17 0.17 5,836 22 0.17 0.17 10 CL 8,601 32 0.32 0.32 12,558 47 0.32 0.32 12,300 46 0.32 0.32 10,580 40 0.32 0.32 11 R 1 12 C 13 C 14 C 15 C 16 R 0.02 171 C 18 C 19 CL 20 C 21 C 22 C 23 C 24 C 12,066 36 0.44 0.44 17,617 53 0.44 0.44 17,255 51 0.44 0.44 14,842 44 0.44 0.44 25 R 0.02 26 R 0.03 27 C 281 C 29 C 66 0 10,900 36 0.40 0.40 15,915 53 0.40 0.40 15,588 51 0.40 0.40 13,408 44 0.40 0.40 30 C 7,684 25 0.28 0.28 11,219 37 0.28 0.28 10,989 36 0.28 0.28 9,452 31 0.28 0.28 31 Monthly Loading: 103,734 3.82 151,435 3.82 148,345 3.82 127,597 3.82 12 Month Floating Total (in): 17.42 17.42 17.42,1A 17.42 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 4 of Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: June Year: 2020 Field Name: 13 Field Name: 14E Field Name: 14W Field Name: 15 Did irrigation occur Area (acres): 2.16 Area (acres): 13.73 Area (acres): 7.7 Area (acres): 0.73 at this facility Cover Crop: OATS Cover Crop: OATS Cover Crop: OATS Cover Crop: OATS ❑ YES ❑ No Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 31.6 Annual Rate (in): 24.21 Annual Rate (in): 30.44 Weather Freeboard Field Irrigated? ❑ YES NO Field Irrigated? YES ❑ No Field Irrigated? YES NO Field Irrigated? ❑ YES ❑ NO >. p m v t m ie m G o is - a v ` CL o 0 rn O J fA o rn Y f- E d a 0 Q � Q m «' E rn i- _ `o M A 0 0 J 3 T _ 'v ,� J E m c. O C. % a an d E A H r >, c o to ,� 0 J �` c E 'i"s ,� = 0 J E m a 0 0 i Q d E i- = c ea v ❑ 0 J E v o _ 0 J £ m a O a i Q d d E o rn H •= >, c iii -0 to G 0 J c £ 'v K o A M= 0 J °F in in in gal min in in gal min in in gal min in in gal min in in 1 C 1 27,314 78 0.47 0.36 9,231 26 0.47 0.47 2 C 54 0 25,901 78 0.44 0.34 8,753 26 0.44 0.44 3 C 12,841 39 0.22 0.22 4,340 13 0.22 0.22 4 C 24,247 70 0.41 0,35 8,195 24 0.41 0.41 5 C 25,670 78 0.44 0.34 8,676 1 26 0.44 1 0.44 6 R 0.01 7 C 8 C 13,062 39 0.22 0.22 129,362 384 0.35 0.05 72,549 216 0.35 0.10 4,415 13 0.22 0.22 91 C 1 10,246 39 0.17 0.17 128,671 384 0.35 0.05 72,161 216 0.35 0.10 1 3,464 13 0.17 0.17 10 CL 18,579 70 0.32 0.27 121,563 346 0.33 0.06 68,175 194 0.33 0.10 6,279 24 0.32 0.32 11 R 1 12 C 13 C 14 C 151 C 161 R 1 0.02 17 C 18 C 19 CL 20 C 21 C 221 C 1 114,177 346 0.31 0.05 64,033 194 0.31 0.09 231 C 24 C 1 26,063 78 0.44 0.34 76,954 263 0.21 0.05 43,157 147 0.21 0.08 8,808 26 0.44 0.44 25 R 0.02 26 R 0.03 27 C 28 C 29 C 66 0 23,545 78 0.40 0.31 45,987 L 154 0.12 0.05 25,790 86 0.12 0.09 7,957 26 0.40 0.40 30 C 1 16,598 54 0.28 0.28 384,985 554 1.03 0.40 215,906 86 1.03 0.72 5,610 18 0.28 0.28 31 Monthly Loading: 224,066 3.82 1,001,699 2.69 561,771 2.69 75,728 3.82 12 Month Floating Total (in): 17.42 21.36 21.36 17.42 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin1 1 • irrigation occur Area (acres): Area (acres): Area (acres): at this facility? YES 7j NOHourly '.te (in): Hourly -. I • -. Hourly Rate (in): Annua[Rate(iny Annual Rate (iny ••Ar Irrigated? Field Irrigated? Field Irrigated? logo Monthly Loading:Field 1 • : iiiaii�aaa�iiii�iiiiiii,oiiaii. 111 iiaiioiiiii 11• ,wo FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page to of I_ Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? ❑� Compliant ❑ Non -Compliant L] Compliant ❑ Non -Compliant D Compliant ❑ Non -Compliant ❑J Compliant ❑ Non -Compliant 0 Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Gerald Lamar Matthews Permittee: Sam Villari Certification No.: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Official's Title: Owner Has the ORC changed since the previous NDAR-1? ❑ yes 0 No Phone Number: 910-293-2157 Permit Exp.: 11/30/25 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page -J- of S Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: June Year: 2020 Field Name: Zone 1 Field Name: Zone 2 Field Name: Zone 3 Field Name: Zone 4 Field Name: Zone 5 Area (acres): 0.65 Area (acres): 1.16 Area (acres): 1.12 Area (acres): 1.07 Area (acres): 1.19 Cover Crop: Coastal Bermude Cover Crop: Coastal Bermude Cover Crop: Coastal Bermudz Cover Crop: Coastal Bermude Cover Crop: Coastal Bermuda Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? 2 YES ❑ NO Field Loaded? _°' YES - NO Field Loaded? 0 YES ❑ No Field Loaded? YES NO Field Loaded? ❑ YES ❑ No a N Z c a Q2 U Z a o > J E Z ) 0.Q a E Z c a N M 2 a) r£ Q2 Z Q a , «0Z o > 2 J E a 0Q2 Z c a C> U Z Q 2, M o o a) E ; c Q a > a 1 O 5@ J Q£:Z 'ac L CL Q d -6 a> a , 07Z o 2-6 >n J Qo E d7 Month gal 0 mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac July 27.3 0.0 0.0 0 27.3 0.0 0.0 0 27.3 0.0 0.0 0 27.3 0.0 0.0 0 27.3 0.0 0.0 August 0 27.7 0.0 0.0 0 27.7 0.0 0.0 0 27.7 0.0 0.0 0 27.7 0.0 0.0 0 27.7 0.0 0.0 September 149,379 21.4 41.0 41.0 146,177 21.4 22.5 22.5 146,177 21.4 23.3 23.3 144,045 21.4 24.0 24.0 143,007 21.4 21.4 21.4 October 0 38 0.0 41.0 0 38 0.0 22.5 0 38 0.0 23.3 0 38 0.0 24.0 0 38 0.0 21.4 November 0 33.2 0.0 41.0 0 33.2 0.0 22.5 0 33.2 0.0 23.3 0 33.2 0.0 24.0 0 33.2 0.0 21.4 December 0 46.2 0.0 41.0 0 46.2 0.0 22.5 0 46.2 0.0 23.3 0 46.2 0.0 24.0 0 46.2 0.0 21.4 January 25,030 43.5 14.0 55.0 44,672 43.5 14.0 36.5 43,131 43.5 14.0 37.3 41,204 43.5 14.0 38.0 45,825 43.5 14.0 35.4 February 29,973 43 16.5 71.5 53,491 43 16.5 53.0 51,647 43 16.5 53.8 49,341 43 16.5 54.5 54,875 43 16.5 52.0 March 42,537 48 26.2 97.7 75,912 48 26.2 79.2 73,294 48 26.2 80.0 70,023 48 26.2 80.7 77,876 48 26.2 78.2 April 30,195 48 18.6 116.3 53,886 48 18.6 97.8 52,029 48 18.6 98.6 49,706 48 18.6 99.3 55,280 48 18.6 96.7 May 42,852 38.4 21.1 137.4 76,474 38.4 21.1 118.9 73,837 38.4 21.1 119.7 70,542 38.4 21.1 120.4 78,451 38.4 21.1 117.9 June 67,429 32.4 28.0 165.5 121,335 32.4 28.3 147.2 116,185 32.4 28.0 147.7 1 11,997 32.4 3.0 123.5 123,445 32.4 28.0 145.9 12 Month Floating PAN Load (Ibs/ac/yr): 165.5 147.2 147.7 VlAfffflll" 123.5 rlAff4" 145.9 350.00 Annual PAN Load Limit (Ibs/ac/yr): 350V111 V, V1111111AVIIA 350.00FEUR 350.00E/Eff/M/Em 350.00 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page _;__ of �_ Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: June Year: 2020 Field Name: Zone 6 Field Name: Zone 7 Field Name: Zone 8 Field Name: Zone 9 Field Name: Zone 10 Area (acres): 1.17 Area (acres): 1.05 Area (acres): 1.25 Area (acres): 1 Area (acres): 1.46 Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? [�] YES NO Field Loaded? 2 YES ❑ NO Field Loaded? ❑ YES NO Field Loaded? YES ❑ NO Field Loaded? ❑ YES NO Qd C�do a aaC ° ac m z r z a 0 W z ° z d z ° z � a a v o a a oa A M o 0. a ia a o aaa>a a 16 o Q r J R d o J z Q N A d :EZ m W M o J z CD m:Eo0 J Z E J EZ E L E Q E J E E d Q E rc Q U o U a < o a 0 '0o U a ' a� o U a 0a Uo U a -6 > Month gal 0 mg/L lbs/ac lbslac gal mg/L Ibs/ac Ibs/ac gal mg/L lbs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L lbs/ac lbs/ac July 27.3 0.0 0.0 0 27.3 0.0 0.0 0 27.3 0.0 0.0 0 27.3 0.0 0.0 0 27.3 0.0 0.0 August 0 27.7 0.0 0.0 0 27.7 0.0 0.0 0 27.7 0.0 0.0 0 27.7 0.0 0.0 0 27.7 0.0 0.0 September 141,911 21.4 21.6 21.6 140,844 21.4 23.9 23.9 148,313 21.4 21.2 21.2 148,313 21.4 26.5 26.5 180,323 21.4 22.0 22.0 October 0 38 0.0 21.6 0 38 0.0 23.9 0 38 0.0 21.2 0 38 0.0 26.5 0 38 0.0 22.0 November 0 33.2 0.0 21.6 0 33.2 0.0 23.9 0 33.2 0.0 21.2 0 33.2 0.0 26.5 0 33.2 0.0 22.0 December 0 46.2 0.0 21.6 0 46.2 0.0 23.9 0 46.2 0.0 21.2 0 46.2 0.0 26.5 0 46.2 0.0 1 22.0 January 45,055 43.58 14.0 35.6 40,334 43.5 13.9 37.9 48,136 43.5 14.0 35.1 38,510 43.5 14.0 40.4 56,224 43.5 14.0 36.0 February 53,953 43 16.5 52.2 48,420 43 16.5 54.4 57,641 43 16.5 51.7 46,113 43 16.5 57.0 67,324 43 16.5 52.6 March 76,567 48 26.2 78.4 68,714 48 26.2 80.6 81,803 48 26.2 77.9 65,442 48 26.2 83.2 95,545 48 26.2 78.7 April 54,352 48 18.6 97.0 48,777 48 18.6 99.2 58,068 48 18.6 96.5 46,453 48 18.6 101.8 67,823 48 18.6 97.3 May 77,133 38.4 21.1 118.1 69,224 38.4 21.1 120.3 82,408 38.4 21.1 117.6 65,925 38.4 21.1 122.9 96,252 38.4 21.1 118.5 June 121,372 1 32.4 28.0 146.1 108,924 32.4 28.0 148.4 129,671 32.4 28.0 145.6 103,734 32.4 1 28.0 150.9 11 151,435 32.4 28.0 I 146.5 12 Month Floating PAN Load 146.1 148.4 145.6 150.9 146.5 (Ibs/ac/yr): Annual PAN Load Limit 350 350.00 350.00 350.00 350.00 (Ibs/ac/yr): FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page 3 of S Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: June Year: 2020 Field Name: Zone 11 Field Name: Zone 12 Field Name: Zone 13 Field Name: Zone 14E Field Name: Zone 14W Area (acres): 1.43 Area (acres): 1.23 Area (acres): 2.16 Area (acres): 13.73 Area (acres): 7.7 Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermudz Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? ❑' YES NO Field Loaded? L11 YES ❑ NO Field Loaded? [A YES NO Field Loaded? IJl YES _ NO Field Loaded? ❑ YES ❑ NO ZamOio Z >' mQ aa ZN Z d Zd aa Z 0 d Z a Z a> � o Za Z a a aQ a a. o a o aa N o ;o 16 7Eo Z m :o J Z Q N o� >, M 0 J N p J ZM Q y M p7J J J 7a NC C £ NC - a dr - a 7z a o a � o o o > 0 a 0 ° > > > L) > > Month gal 0 mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac July 27.3 0.0 0.0 0 27.3 0.0 0.0 0 27.3 0.0 0.0 1,508,137 1 27.3 25.0 25.0 750,224 27.3 22.2 22.2 August 0 27.7 0.0 0.0 0 27.7 0.0 0.0 0 27.7 0.0 0.0 969,573 27.7 16.3 41.3 482,314 27.7 14.5 36.7 September 203,796 21.4 25.4 25.4 165,386 21.4 24.0 24.0 99,231 21.4 8.2 8.2 856,196 21.4 11.1 52.5 426,914 21.4 9.9 46.5 October 0 38 0.0 25.4 0 38 0.0 24.0 0 38 0.0 8.2 0 38 0.0 52.5 0 38 0.0 46.5 November 0 33.2 0.0 25.4 0 33.2 0.0 24.0 0 33.2 0.0 8.2 431,699 33.2 8.7 61.2 214,749 33.2 7.7 1 54.3 December 0 46.2 0.0 25.4 0 46.2 0.0 24.0 0 46.2 0.0 8.2 645,371 46.2 18.1 79.3 214,749 33.2 7.7 62.0 January 55,068 43.5 14.0 39.4 47,365 43.5 14.0 38.0 83,180 43.5 14.0 22.2 416,791 43.5 11.0 90.3 233,744 43.5 11.0 73.0 February 65,942 43 16.5 55.9 56,719 43 16.5 54.5 99,604 43 16.5 38.7 489,300 43 12.8 103.1 274,406 43 12.8 85.8 March 93,582 48 26.2 82.1 80,494 48 26.2 80.7 141,354 48 26.2 64.9 322,736 48 9.4 112.5 180,996 48 9.4 95.2 April 66,428 48 18.6 100.7 80,494 48 26.2 106.9 100,341 48 18.6 83.5 736,314 48 21.5 133.9 412,895 48 21.5 116.7 May 94,274 38.4 21.1 121.9 81,143 38.4 21.1 128.0 142,400 38.4 21.1 104.6 579,702 38.4 13.5 147.5 325,106 1 38.4 13.5 130.2 June 148,345 32.4 28.0 149.9 127,597 32.4 28.0 156.1 224,066 32.4 28.0 132.E 1,001,699 32.4 19.7 167.2 561,771 32.4 19.7 149.9 12 Month Floating PAN Load 149.9 156.1 132.6 167.2 149.9 (Ibs/aclyr): Annual PAN Load Limit 350 350.00 350.00 350.00 350.00 (Ibs/ac/yr): _ FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page 6 of Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: June Year: 2020 Field Name: Zone 15 Field Name: Zone 16 Field Name: Zone 17 Field Name: Field Name: Area (acres): 0.73 Area (acres): 1.25 Area (acres): 0.82 Area (acres): Area (acres): Cover Crop: Norfolk Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Cover Crop: Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? 0 YES ❑ NO Field Loaded? '_- YES -1 NO Field Loaded? ❑� YES ❑ NO Field Loaded? -' YES `_i NO Field Loaded? ❑ YES ❑ NO Qa > Q Q Q Q Q > a aa'`° w o 0. ; v o o o o NQ a Q N �Oc r Q Gl A l0 Z O JQm Z q CA o L O Z Q 1 CT an L Oj J m C mJ T 10 O JJ j E Z0 E E Q J E JE E Oo Q o > o o a Month gal 0 mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac July 27.3 0.0 0.0 11,310 27.3 2.1 2.1 9,500 27.3 2.6 2.6 August 0 27.7 0.0 0.0 0 27.7 0.0 2.1 0 27.7 0.0 2.6 September 87,493 21.4 21.4 21.4 52,381 21.4 7.5 9.5 44,000 21.4 9.6 12.2 October 0 38 0.0 21.4 0 38 0.0 9.5 0 38 0.0 12.2 November 0 33.2 0.0 21.4 0 33.2 0.0 9.5 0 33.2 0.0 12.2 December 0 46.2 0.0 21.4 0 46.2 0.0 9.5 0 46.2 0.0 12.2 January 28,112 43.5 14.0 35.4 23,420 43.5 6.8 16.3 15,363 43.5 6.8 19.0 February 33,663 43 16.5 51.9 0 43 0.0 16.3 0 43 0.0 19.0 March 47,771 48 26.2 78.1 24,998 48 8.0 24.3 16,399 48 8.0 27.0 April 33,911 48 18.6 96.7 31.371 48 10.0 34.4 20,580 48 10.0 37.1 May 48,126 38.4 21.1 117.8 19,846 38.4 5.1 39.5 13,019 38.4 5.1 42.1 June 75,728 1 32.4 28.0 145.8 50,918 1 38.4 13.0 52.5 33,403 38.4 13.0 55.2 12 Month Floating PAN Load 145.8 52.5 55.2 0.0 0.0 (Ibs/ac/yr): 0.00 Annual PAN Load Limit 350 350.00 350.00 0.00 (Ibs/ac/yr): FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page _�7 of ,- Did the mass loading rates exceed the limits in Attachment B of your permit? 2✓ Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Gerald Lamar Matthews Permittee: SAM VILLARI Certification Number: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Official's Title: OWNER Has the ORC changed since the previous NDMLR? ❑ Yes D No Phone No.: 910-293-2157 Permit Exp.: 11/30/25 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 • sM ANALYTICAL & CONSULTING CHEMISTS The Pork Company 892 Penny Branch Road Warsaw NC 28398 Attention: Gerald Matthews Lab ID Sample ID: 20-26591 Site: Upstream #1 Test Ammonia Nitrogen Total Kjeldahl Nitrogen (TKN) Total Phosphorus Fecal Coliform Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Lab ID Sample ID: 20-26592 Site: Downstream #1 Test Ammonia Nitrogen Total Kieldahl Nitrogen (TKN) Total Phosphorus Fecal Coliform Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Comment. Reviewed by: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax inl'oi zlenvironmentalchemists.com Date of Report: Jul 10, 2020 Customer PO #: Customer ID: 08100099 Report #: 2020-10594 Project ID: Effluent / Streams Collect Date/Time Matrix Sampled by 6/29/2020 8:45 AM Water Gerald Matthews Method Results Date Analyzed EPA 350 1 EPA 3512 SM 4500 P F SM 9222D MF EPA 353 2 EPA 3532 Subtraction Method Method Collect Date/Time Matrix 6/29/2020 9:00 AM Water 0.5mg/L 07/01/2020 1.4 mg/L 07/08/2020 0.18 mg/L 07/03/2020 105Colonies/100mL 06/29/2020 0.09 mg/L 06/30/2020 0.96 mg/L 07/08/2020 0.87 mg/L 07/10/2020 Sampled by Gerald Matthews Results Date Ana EPA 3501 1.1 mg/L 07/01/2020 EPA 351.2 1.7 mg/L 07/08/2020 SM 4500 P F 0.15 mg/L 07/03/2020 SM 9222D MF 160 Colonies/100mL 06/29/2020 EPA 353 2 0.03 mg/L 06/30/2020 EPA 353 2 1.32 mg/L 07/08/2020 Subtraction Method 1.29 mg/L 07/10/2020 Report # 2020-10594 Page 2 of 2 Environmental Chemists, Inc. envirochem j6602 Windmill Way, Wilmington, NtC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, ;ANC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS into(a�emirontnenrllehemists.com The Pork Company Date of Report: Jul 10, 2020 892 Penny Branch Road Customer PO #: Warsaw NC 28398 Customer ID: 08100099 Attention: Gerald Matthews Report #: 2020-10594 Project ID: Effluent / Streams Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-26590 Site: Effluent 6/29/2020 8:30 AM Water Gerald Matthews Test Method Results Date Analyzed PAN Used 30% Mineralization Rate. Calculation 32.4 mg/L 07/10/2020 Ammonia Nitrogen EPA 350 1 64.3 mg/L 07/02/2020 Total Kieldahl Nitrogen (TKN) EPA 351.2 65.1 mg/L 07/08/2020 Total Dissolved Solids (TDS) SM2540C 284mg/L 07/01/2020 Residue Suspended (TSS) SM 2540 D 86.0 mg/L 06/29/2020 Chloride SM 4500 CI E 45 mg/L 07/01 /2020 Total Phosphorus SM 4500 P F 7.79 mg/L 07/03/2020 BOD SM 5210 B 80 mg/L 06/29/2020 Fecal Coliform SM 9222D MF 29500 Colonies/100ml- 06/29/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2 0.08 mg/L 06/30/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 0.04 mg/L 07/08/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/10/2020 Total Nitrogen (Calc) Total Nitrogen Total Nitrogen 65.1 mg/L 07/10/2020 RepoC # 2020-10594 Page 1 of 2 Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemista.com Client: The Pork Company -Warsaw PROJECT NAME: WWTF Effluent REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Gerald Matthews, ORC PHONE/FAX: Permit Number: W00016376 email: 614(( ' 14 P Y�46A, Samwea Bv: C aGrG17t II 1r 44L mi QARA01 a �n­ Sample Identification p Collection d E S- 4 o° 0 _ 6 a o. 8' t E " m J= z PRESERVATION av = Oull, al. = aluuge, umer: ANALYSIS REQUESTED Date Time Temp _ °_ $ o = 0 Z 0 = o PPI 001 (Effluent-1 /month) c pH (field): C c1 G-(q 11(� b�� X X BOD,TSS,NO2 NO3,NH3,TKN,Total P, PAN, Total N IV C G G C X I IFecal Coliform G March, July, November PPI 002 (Upstream) C ,i 2�1 X X k y� If I X I JTDS, Chloride (triannuals) TKpie -AN, NH3,NO3,NO2,Total P, Fecal, Tot -t'`►?J� : �;:/1` C G G C 91 G PPI 003 (Downstream)® •Lys '� C X X ,,�� -A jk T�N, t H3,NO3,NO2,Total P, Fecal,Tot I C P G G C P G G Samples due 1/month Transfer 42 Relinquished By: Date/Time R eived By: Date/Time 2. Temnnraturo when Rorni..n.l• r• A ..__,_A. f Delivered Comments: -1 nCsanlpie ri esiea: _ Received By: �, -- - -- Date:--- zJ�-Lc' Time: I ' 10 _ - - ----------- —TURNAROUND: N A Environmental Chemist, Inc., 'Nilmington, NC Lab $094 Client: Sample Receipt Checklist i�-i-t✓ �O �K. a.�.�ot of samele• �.t�.,...,, �602 Windmill Way Nilm+ngton, NC 28405 910 392.0223 Date: Report NumberIQ_�0 5 y ❑ YES D NO ---I-----P, u �edEx LJ Other ❑ v/A 1. Wert custody seals present on the cooler? ❑ YES C] 140 N/A 2. if custody seals weft present, were the ntact/unbroken? Or final temperature upon receipt 5• 'C Corrected temperature upon receipt C How temperature taken: D Temperature Blank Against Bottles R Gun 10' Thomas Traceable S/N 192S11657 R Gun Correwtwn Factor T: 0.0 ❑ YES ❑ v0 3. if temperature of cooler exceeded 6'C, was Pro ect M r./C1/► notified? YES ❑ 140 4. Were proper Gust txedures (relinquished/received) followed? YES ❑ v0 5. Here sample ID's listed on the COC? YES ❑ 40 6. were sam les IO's listed on sample containers? 311 YES D NO 7. were co+lection date and time listed on the COC? YES D NO 8. 'were tests to be performed listed on the COC? YES D NO 9. Did samples arrive In proper containers for each test? YES D 40 10. Did samples arrive In good condition for each test? YES D 40 11. Nas adequate sampitvoil avadabler YES D 40 112. 'were samples received within OfOpef holdin time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of c2? • O YES ❑ NO 14. were cyanide samples received at a pH >12? YES D 40 i 15 were sulfide samples received at a pH >9? YES ❑ 40 116. were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? " vE5 O 40 117 'Nero Suifide/Cyanide received at O YES '❑ 1140 I a chlorine residual of <0 5 m/L? 1,18 'Nero orthophosphate samples filtered in the field within 15 minutes? i ' HOC/Volatile+ are pH checked at !Ime of analysts and recorded on the bMchsheet. '• 3actena samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: Must be completed for any sampiels► Incorrectly preserved or vlth headsoace) Sample(s) by adding (cycle one): vere received Incorrectly preserved and were adjusted accordirgly -I.SOJ NO, yCl 4a0H Time of preservation: se' f more than ore preservative !s needed, notate n comments below NOtt VOt�t'p er ;lrY �C! mmld,itllV rOr nC Of�ectt y Or-eserved samples. Cttam a ^ew sarrole or ndt,fv the State ab ,f 1Ireoed!o ar`alvzed 0V !Me C�StOmer Nho was ^Otf•ed .'.at! Jr^d time. volatile+ Sample(s) vere received with headsoace COMMENTS: nr no .gym