NC0020052_Regional Office Historical File Pre 2018

ATA
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory Donald van der Vaart
Governor Secretary
May 26, 2015
Subject: Lagoon Closure for Town of McAdenville WWTP
Church Street
McAdenville, NC
Permit No.: NC0020052/WQ0024588
Gaston County
The Town of McAdenville WWTP applied for and received a Lagoon Closure Plan in May of 2004.
The Lagoon was sampled and soils sample results indicate no contaminant were present in the
lagoon sediments. Activity for this site did not indicate the closure had actually occurred.
The site has now come under the management of Two Rivers Utilities. In a phone conversation
with Stephanie Sheringer it was confirmed the pond had been back-filled and the closure was
completed.
This file is now considered to be inactive.
Sincerely,
j,_44.4
z
elit Watson
Hydrogeologist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
CC: File
Mooresville Regional Office
610 East Center Avenue,Suite 301,Mooresville,North Carolina 28115
Phone:[phone]/Fax:[phone]/Customer Service:1-877-623-6748
Internet:www.ncdenr.gov
An Equal Opportunity\Affirmative Action Employer—Made in part by recycled paper

ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS
Checklist and Instruction Items
The purpose of the following checklist and instruction items is to aid in the development of a closure plan for
a permitted Non-Discharge wastewater pond or lagoon to be submitted to the appropriate APS Regional
office for approval.
The following checklist allows the applicant to identify the type of lagoon to be closed, and the preferred closure
and disposal options. The selected options include references to instruction items(e.g. Item A)found on
subsequent pages of this attachment. The instruction items describe what steps are expected to be complete prior to
approval of the closure plan, including expected sampling and monitoring,and final certifications of complete
closure. Note that the following steps are not all inclusive,as each site is unique and may have varying site
conditions. In addition,flowcharts(Attachment B)have been provided as an alternate to the instructional Items A-
H. These charts contain the same information, but give a visual representation of the closure process. For
questions,contact the approving APS Regional Supervisor. Please check all items below that apply and submit a
completed copy with the lagoon closure plan.
1. Type of Pond or Lagoon System
a.Primary and Secondary Biological Wastewater Lagoon Systems(examples: food processing treatment
lagoons,municipal treatment systems without pretreatment programs,neighborhood treatment systems).
b.Primary and Secondary Industrial Wastewater Lagoon Systems(examples: non-food type industrial
treatment systems,municipal treatment systems with pretreatment program).
c.Tertiary Wastewater Pond Systems( examples: wastewater biological treatment systems with tertiary
treatment to include infiltration disposal pond systems,effluent polishing pond systems).
II. Closure Options—Structure
a. Conversion to Non-Wastewater Pond—Change of Use(Item B)
)( b.Complete or partial removal of structure(Items G)
c. Site Reclamation(Item F and H)
HI. Final Liquid and Solid Content Disposal Options
a. Wastewater Disposal to Onsite Permitted Field(Item A)
> b. Wastewater Disposal through Pump and Haul(Item A)
c. Sludge Disposal to Permitted Site(Items C and D)
A d. Sludge Left in Place(Items C and E)
IV. Sampling and Monitoring Requirements
a. Wastewater Sampling Required(Items A and B)
,( b. Soil and Sludge Sampling Required(Items C and F)
c.Groundwater Monitoring Required(Item G)
V. Final Certification Required for Closure Activities,as required in Item I.
a. Structural Deconstruction(Professional Engineer or Hydrogeologist)
X b. Wastewater Disposal(Facility ORC)
c. Sludge Disposal(ORC/Licensed Sludge Land Application Contractor)
d. Other(Explain: )
A-1
Attachment A June 22,2012

ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS
Item A. Wastewater Sampling,Analysis, and Disposal
1. Pond samples require a composite sampling technique. Samples should be composited from several
locations. An adequate number of representative and composite samples should be taken and developed
respectively.
2. For permitted disposal sites,sample and analyze wastewater in accordance with permit conditions. In the
absence of permit specified monitoring,sample for the following parameters:
a. Fecal coliform bacteria,chlorine residuals(if used as disinfectant),total nitrogen,BOD5,TSS,pH.
b. Other parameters may be required based on waste streams,as directed by the APS Regional
Supervisor.
3. All wastewater samples must be analyzed by a DWQ-certified laboratory.
4. Once the wastewater is sampled,the pond/lagoon can be dewatered to a permitted disposal site(uniform
application of wastewater)or through a pump and haul permit.
5. Remove or plug all inflow and outflow piping,etc to the pond/lagoon
Item B. Conversion to Non-Wastewater Pond(Tertiary Treatment Ponds Only2
6. Determine pond liquid volume(if water accumulates after complete disposal per Item A, Wastewater
Sampling,Analysis, and Disposal).
7. If some sludge remains,sludge can be left in place, in accordance with Item E#23 below. Otherwise,
remove all residuals and dispose of properly per Item D, Sludge and Soil Disposal.
8. Disinfect and/or treat pond to meet Item B#11 requirements below.
9. Sample pond (see Item A, Wastewater Sampling, Analysis, and Disposal)
10. No pond discharge is allowed to surface water without prior approval from an appropriate Surface Water
Section Regional Office.Note that pond discharge to class SA waters is not allowable.
11. All discharges must meet water quality standards applicable to receiving stream classification or per limits
provided by DWQ when water quality stream standards for monitored parameters are not defined.
Item C. Soil and Sludge Analysis
12. All soil and sludge samples require a composite sampling technique. An adequate number of
representative and composite samples should be taken and developed respectively. Thickness of sludge or
soil and surface acreage should be considered. Example: one composite sample per acre foot.
13. All soil and sludge samples must be analyzed by a DWQ-certified laboratory.
14. For biological wastewater lagoons systems and tertiary wastewater pond systems,soil or sludge shall be
sampled for: •
a. Pathogen and Vector Attraction Reductions.Testing should be done per 15A NCAC 02T .1100. If
project concerns only a tertiary pond,and pond sediments/sludge meets Class A pathogen
reduction requirements(maximum of 1000 fecal coliform bacteria colonies per gram of total
solids), additional characterization for pH,metals,nutrients,and solids as stated in 14.b and 14.c
(below) may not be required,as determined on a case by case basis.
b. Arsenic,cadmium,chromium,copper, lead,mercury,molybdenum,nickel,selenium,zinc,TKN,
ammonia nitrogen,nitrate/nitrite,nitrogen,phosphorus, sodium,calcium,magnesium(mg/kg dry
wt basis), percent total solids and pH.
c. Other parameters may be required based on waste streams,as directed by the APS Regional
Supervisor.
A-2
Attachment A June 22,2012

ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS
15. For industrial wastewater lagoon systems,this should be the same as biological wastewater lagoon system
sampling plus site-specific parameters and hazardous characterization to include,but not limited to,TCLP,
ignitability,corrosivity and reactivity.
16. If the sludge or soil samples are:
a. Required to be analyzed for hazardous characteristics and results exceed hazardous characteristics
regulatory limits,the material needs to be removed and reported to and managed in accordance
with the Hazardous Waste Section in the Division of Waste Management.
b. Not required to be analyzed for hazardous characteristics or results do not exceed the hazardous
characteristics regulatory limits,the soil can be left in place if the following conditions are met :
i. Total concentrations of contaminants in soil do not exceed protection of groundwater soil
concentrations for North Carolina based on 2L standards,as calculated using the Transport
Model for Calculation of Soil-to-Groundwater Concentrations from the USEPA 1996 Soil
Screening Guidance document. (The EPA Transport model can be found in the"Soil
Remediation Goals Table"at http://portal.ncdenr.org/web/wm/sf/ihs/ihsguide or the"2L,
MCL,and Soil Screening Levels Table"at
http://portal.ncdenr.org/web/wm/hw/technical/guidance.)
ii. Total concentrations of contaminants in the soil exceed protection of groundwater soil
concentrations for North Carolina,but results do not exceed naturally-occurring
background concentrations,
iii. A more stringent soil clean-up level is not necessary due to site specific conditions as
determined by the Division.
For sludge left in place,see Item E, Sludge Left in Place. For sludge disposal, see Item D,Sludge
and Soil Disposal.
c. Not required to be analyzed for hazardous characteristics or results do not exceed hazardous
characteristics regulatory limits, but total concentration results exceed corresponding protection of
groundwater soil concentrations for North Carolina as calculated using the Transport Model from
the USEPA 1996 Soil Screening Guidance document described in 16(b)(i),soil and sludge must be
disposed of according to Item D, Sludge and Soil Disposal. For soils that exceed protection of
groundwater levels,Item G,Groundwater Post Closure Monitoring,must also be considered.
17. For ponds or lagoon bottoms that intercept groundwater,Regional Offices will determine what type of
sampling is required for the remaining contents on a case by case basis.
Item D. Sludge and Soil Disposal
18. Measure surface area and depth of sludge and soil(if required)to determine disposal volume
19. Sample sludge and soil(if required)for permitted disposal option including pathogen and vector attraction
reduction verification(see Item C, Soil and Sludge Analysis)
20. If a tertiary pond and sludge/sediments meet Class A pathogen and vector attraction reduction
requirements,sludge/sediments can be land applied uniformly on site without sludge permitting action
(additional sludge or soil characterization may not be required, as determined on a case by case basis).
21. If sludge or soil does not meet Class A pathogen and vector attraction reduction requirements,
sludge/sediments may require a permit modification to land apply.
22. Pathogen and vector attraction reduction testing will not be required if sludge or soil is taken to a permitted
compost or another treatment facility for further stabilization.
A-3
Attachment A June 22,2012

ATTACHMENT A CLOSURE OF PERMITTED WASTEWATER PONDS AND LAGOONS
Item E. Sludge Left in Place
23. For closure purposes,the Division of Water Quality considers it practical to remove sludge content from
structures. The Division will evaluate the applicability of leaving any remaining volume of sludge content
in the structure on a case-by case basis. Sufficient technical justification shall be provided to support such
recommendation.
Item F. Liner Demolition/Disaosal
24. If a synthetic liner is present, remove synthetic liner,scarify/rip/disk underlying material in cases where
there is no potential benefit for reuse of the structure based on projected future site use.
a. If there are no historical problems with the lagoon(documented seepage,etc.)and the liner is intact
after dewatering with no visible indications of seepage, soil sampling may still,be required on a
case-by-case basis.
b. If liner and/or lagoon issues are documented,the soil material under the synthetic liner should be
sampled according to Item C, Soil and Sludge Analysis.
25. If clay liner is present, scarify/rip/disk and/or remove and reuse as cap if filling. If the liner is natural clay,
sampling may be required on a case by case basis if the following conditions are not met:
a. Based on existing groundwater monitoring data,no groundwater violations are present,
b. Domestic wastewater systems only,
c. Surficial layer of earthen material(top 6"— 12")removed,and
d. All sludge removed and the remaining material is only soil and not co-mingled soil/sludge.
26. If the clay liner does not meet the conditions in#25 above, the clay liner should be sampled according to
Item C, Soil and Sludge Analysis.
27. If a pond or lagoon does not have a liner,the underlying soil should be sampled according to Item C, Soil
and Sludge Analysis.
Item G. Groundwater Post Closure Monitoring
28. For facilities with no historic groundwater monitoring,monitoring may be required based on post closure
soil sample results. Contact Regional Office for directions. If groundwater monitoring is not required,
permittee can petition the Division for rescission once the site is reclaimed.
29. For ponds or lagoons with historic groundwater monitoring and no groundwater violations were detected,
no further groundwater monitoring will be required,as recommended by the Regional Office based on
existing data.
30. For ponds or lagoons with historic groundwater monitoring and/or 15A NCAC 2L standards were
exceeded,the following actions would be required:
a. Maintain permit with limited actions as recommended by the Regional Office(e.g.annual
groundwater monitoring and reporting).
b. Continue groundwater monitoring as permitted for a minimum of three sampling events.
i. If there are no further groundwater exceedances detected or exceedances show a trend of
lowering toward groundwater standards,the permittee could petition the Division for
permit rescission.
ii. If groundwater exceedances continue at the same level,continued monitoring and or site
evaluation would be required at the Regional Office Supervisor's discretion.
c. In lieu of groundwater monitoring,the Permittee may provide predictive calculations,acceptable to
the Director, to demonstrate groundwater standards can be met at the property boundary.
A-4
•
Attachment A June 22,2012

ATTACHMENT A CLOSURE OF PERMIITbD WASTEWATER PONDS AND LAGOONS
Item H. Berms/Lagoon Walls and Site Reclamation*
31. In cases where retention of municipal structures provides no value based on projected future site use, it is
recommended that minimal demolition be performed to breach or remove sidewalls(dependent on the size)
when the liner is demolished. Minimal demolition may be considered feasible in cases where retention of
the structure or a portion thereof poses minimal risks based on conditions such as low population densities
of surrounding areas, low hazard environment, low probability of encroaching development,etc.
32. For privately owned and higher risk municipal structures,more extensive structure demolition is
recommended to include,but not be limited to,removal of berms/dike walls and general grading of project
site.
33. If structure is completely constructed at or below grade,fill with clean material(partial or complete,
depending on size)and/or grade site to minimize any hazards posed by existing conditions.
34. If structure is finished in the groundwater table,see Item C#17.
35. Stabilize the site with vegetation.Establishment of trees,grasses,and other viable cover crops should be
considered to assist site stabilization and with removing any remaining nutrients.
*Recognize the added value of planned reclamation efforts. Reclamation activities incorporating created artificial
wetland systems,planted trees, and other pro-active actions viewed as either mitigation efforts or secondary
environmental protection measures may assist with enabling the closure project to qualify for recognition and
benefit from other environmental programs, such as those offered through conservation easements.
Item I. Final Certifications
36. For deconstruction including berm removal,berm breaching, or liner destruction, submit a letter certified
by the overseeing professional engineer that action was taken according to the approved plan,as well as all
local and state regulations.
37. For wastewater disposal, submit a copy of the monitoring report that documents lagoon wastewater disposal
activities,certified by the facility ORC.
38. For sludge disposal,submit a copy of the records documenting lagoon sludge disposal,certified by the
licensed sludge land application contractor if land applied. If sludge was disposed of in a landfill,records
from the receiving facility shall be provided.
39. Sampling results from any post-closure sampling conducted at the facility to document proper removal of
sludge in accordance with the approved closure plan shall be submitted.
40.Photos of closure activities documenting conditions prior to initiating closure,closure activities,and post-
closure conditions are recommended, but not required.
41. Other.
A-5
Attachment A June 22,2012

ATTACHMENT B
The following flowcharts are a visual alternate to the information provided in Instructional
Items A-H in Attachment A. The checklist provided in Attachment A must still be
completed, whether the Instruction Items or flowcharts are used. Final certification
requirements are only found in Item I in Attachment A.

Attachment B—Closure of Permitted Wastewater Ponds and Lagoons
Flow Chart 1 —Wastewater Sampling and Disposals
START HERE
Does the site
have permit YES Sample lagoon wastewater in
accordance with the permit
specific
monitoring? conditions.
NO
V
Using an adequate number o-f-'\.
representative composite
samples,test for fecal coliform
bacteria,chlorine residuals (if
used as disinfectant),total
nitrogen,BOD5,TSS,and pH.
Other parameters may be
required by Regional Office
based on waste streams.
•
Samples should be
composited from several
locations. All samples must
be analyzed by a DWQ-
certified laboratory.
Dewater pond/lagoon to
permitted disposal site or
through a pump and haul permit
issued by DWQ.
•
Remove or plug all inflow and
outflow piping.
If water accumulates after disposal,
determine pond liquid volume and
disinfect/treat pond(If necessary)to meet
If you have a water quality standards applicable to
tertiary pond, YES receiving stream classification or per limits
do you want to provided by DWQ when water quality
convert to non- stream standards for monitored
wastewater? parameters are not defined. Sample as in
previous step. END If sludge remains,
proceed to Flow Chart 2—Sludge
NO Analysis and Disposal.
Does sludge YES .J Proceed to Flow Chart 2—Sludge Analysis
remain? and Disposal.
NO
•
Proceed to Flow Chart 3—Liner
Demolition and Disposal.
'No pond discharge Is allowed to surface water without prior approval from an appropriate Surface Water Section Regional Office. All discharges
must meet water quality standards applicable to receiving stream classification or per limits provided by the Division of Water Quality when water
quality standards for monitored parameters are not defined.Pond discharges to dass SA waters Is NOT allowable.
Attachment B1 June 22,2012

Attachment B—Closure of Permitted Wastewater Ponds and Lagoons
Flow Chart 2—Sludge Analysis and Disposal
CONTINUED FROM FLOW CHART 1—WASTEWATER SAMPLING,ANALYSIS,AND DISPOSAL Determine volume of sludge then
Do the results excavate. Manage and report
What type of wastewater lagoon system is present? en us YESd hazardous material in accordance with
r
waste Hazardous Waste Section guidelines.
characteristics? Proceed to Flow Chart 3—Liner
Nil ,II Demolition and Disposal.
1 . , NO .
Biological' ( Industrie Tertiay •
V V
i using an adequate number of \ / Using an adequate number off groundwater results ( May require permit modificationrepresentative \
Ualrg an adequate number of representative composite samples, soil levels to land
representative and compositesampand composite test for Pathogen and Vector for calculated YES Contact DWQ Regional Office
samples,test for: test Attraction Reduction per 16A
1. Pathogen end Vector 1. Pathogen and Vector NCAC 02T per \ .1100?a .1 Model the Iusing the �JS Proceed to Flow3—
Attraction Reduction per 1sA NCACsport for more infoimation.
Attraction 0 Reduction0023 1996 Soil Screening Liner Demolition and Disposal.
15A NCAC 02T.1100�' 2. Arsenic,cadmium, Guidance document? ` /
2. Arsenic,cadmium, chromium.copper,lead,
chromium,copper,lead, mercury,mercury,molybdenum, moybdenm, Do samples
deice',selenium.zinc, nickel,selenium.zinc. YES
meet Class A
TKN,ammonia nitrogen, —i_-
TKN.ammonia nitrogen, pathogen
i
nitrate/nitrite,nitrogen.
rifretehdtrite.nitrogen, re I
phosphorous.sodium, requirements?phosphorous.sodium, calcium.and magnesium NO I
calcium,and magnesium In
in mgAcg dry weight basis, W
mg/kg dry weight Dams. percent total solids,and NO
percent total solids,and PH.
3. Site-specific / Sludge can be left in place or land
( Test for arsenic,cadmium, applied uniformly on site without
dhromitm,popper,bad,meraxy, Do samples DWQ pe g action:,
molybdenum. nickel,selenium, meet Class A YES If sludge is left in place,proceed to
Pathogen Flow Chart 6—Groundwater Post
zinc,TKN'ammonia nitrogen. reduction Closure Monitoring.
phosphMita,orous,
nitrogen, requirements? If sludge Is land applied,proceed to
phosphorous,sodium.calcium, Flow Chart 3—liner Demolition
and magnesium In mg/kg dry and Disposal
weight basis,percent total solids.
Samples v , and pH.,
required to be YES ' Teat for TCLP.ignitabitiy, NO /tested for May require permit modification to
hazardous and reactivity., , land apply.
characteristics? Contact DWQ Regional Office for
more hfonnation.
NO ` ` ProceedDemolition and Disposal f
r For ponds or lagoon bottoms that intercept groundwater,DWQ will determine what type of sampling is required for the remaining contents on a case by case basis. •
r Pathogen and vector attraction reduction testing will not be required if sludge/s taken to a pemtited compost or another treatment fedlity for further stabilization.
Samples to be analyzed by DWQ-certified laboratory.
For closure purposes,DWQ considers it practical to remove sludge content horn structures. DWQ will evaluate the applicability of leaving any remaining volume of sludge on a case by case basis. Sufficient technical justification shall be provided to support such
recommendation.
Attachment B2 June 22,2012

Attachment B—Closure of Permitted Wastewater Ponds and Lagoons
Flow Chart 3—Liner Demolition and Disposals
CONTINUED FROM FLOW CHART 1—WASTEWATER SAMPLING,ANALYSIS,AND DISPOSAL OR
FLOW CHART 2—SLUDGE ANALYSIS AND DISPOSAL
What
type of
liner is
present?
V • V
Clay Uner No Liner Synthetic Uner
l I l , , /
V
V
1 ( V 1 �• i. Remove liner,
[ *'
Scarify/rip/disk and/or Sod sampling isscarify/rip/disk
remove and reuse as required. underlying material in
cap if filling. Proceed to Flow cases where there is no
J ` Chart 4. J potential benefit for
reuse of the structure
based on projected
future site use. )
Are all of the
following true?
a. Groundwater
sampling has been
documented and no
groundwater
violations are Soil sampling is required. , Historical
present. NO Proceed to Flow Chart 4— < YES problems or
b. The system is Soil Analysis and damaged
domestic waste- l Disposal. / liner?
water only.
c. The surficial layer of
earthen material
was removed. NO
d. No residuals
remain. V
Soil sampling may be required
on a case-by-case basis.
Proceed to Flow Chart 6—
Groundwater Post Closure
YES ` Monitoring.
V
Proceed to Flow Chart 6— ,
Site Reclamation.
'For closure purposes.the DWQ considers it practical to remove sludge content from structures. DWQ will evaluate the applicability of leaving any
remaining volume of sludge content in the structure on a case-by-case basis. Sufficient technical justifkation shall be provided to support
recommendation.
Attachment 133 June 22,2012

Attachment B—Closure of Permitted Wastewater Ponds and Lagoons
Flow Chart 4—Soil Analysis and Disposal
Determine volume of sot then
CONTINUED FROM FLOW CHART 3—UNER DEMOLITION AND DISPOSAL results excavate. Manage and report
Do the1 YES material in accordance Wth
What type of wastewater lagoon system is present? exceed hazardous Hazardous Waste Section guidelines.
wrote
• . for ? Proceed to Flow Chart 5—
Groundwater Post Closure
Monitoring. J
y y NO .
r •
Biological Industrial' Tertiary'
` •'lI ` Do the results
fee-Using an adequate number or / Using en adequate number of \ exceed
groundwater
Groundwater post closure
Using an adequate number of representative and composite repreaerdative composite samples. protection sot levels monitoring required.
representative and composite samples,test for: test for Pathogen and Vector for NC as cdck/eted YE Proceed to Flow Chart 5—
samples.test for: Attraction Reduction per 15A using the Transport Groundwater Post Closure
1. Pathogen and Vector 1. Pathogen and Vector NCAC 02T.110g 2.s !Nadel in the USEPA
Attraction per Attraction Reduction per ` / 1996 SoN Screening , Monitoring.
NCAC Reduction02T.1100z' 15A NCAC 02T.1100z, Guidance doh'
152. Arsenic,cadmium,
2. Arsenic,cadmium,
chromium,copper,lead. fin'COS,lead.
molmercury,molybdenum. mercury, +, Do samples
nickel,selenium,zinc,
nickel,selenium,zinc, 7KN,ammonia nitrogen,
meet Class A YES 1
TKN,ammonia rs'trogen, pathogen —r—
nitrate/nitrite,ratrogen. nitrat°� B'
phosphorous,Sodium phosphorous,sonfkxrn, I
r re
duction
?
calcium,and magnesium in calcium,and rtmapnasium NO 1
nmgAcg dry weight balls, in rig dry weight basis, 1
lids,and PM total solids.and
percent tote!so NO 1
s PH. " 1
�' \ 3. Site specMc pararrteters.'� r Teat for arsenic,cadmium. I
chromium,copper,lead,mercury, W
molybdenum,nickel,selenium, Do samples SoN can be left in place.
zinc,TKN,ammonia nitrogen, meet Class A YES 4 Proceed to Flow Chart 5—
nitrete/Nl ire.nitrogen, ^^'Tpathogen Groundwater Post Closure
phosphorous.sodium,calcium, reduction Mongering. y
and magnesium In mglkg dry requirements?
weight basis.percent total scads.
Samples V `and phis J."
•
required to be YES Test for TCLP,Ignitabity, NO l
tested for Y,and reactivity., May require permit modification to 1
corrosivit
hazardous , land apply.
•
characteristics? Contact DWO Regional Office for
c > more information.
Proceed to Flow Chart 5—
NO Groundwater Post Closure
. \ Monitoring. J
For ponds or lagoon bottoms that intercept groundwater,DWG)will determine what type of sampling is required for the remaining contents on a case by case basis.
r Pathogen and vector attraction reduction testing will not be required N sludge is taken toe permitted compost or another treatment facility for further stabilization.
r Samples to be analyzed by DWD-certilled laboratory.
•II soil concentration results exceed groundwater protection levels but do not exceed naturally occurring soil background concenbataoons,then they are not considered art exceedance.
Attachment 84 June 22,2012

Attachment B—Closure of Permitted Wastewater Ponds and Lagoons
Flow Chart 5—Groundwater Post Closure Monitoring
CONTINUED FROM
FLOW CHART 2—SLUDGE ANALYSIS AND DISPOSAL,
FLOW CHART 3—LINER DEMOLITION AND DISPOSAL,OR
FLOW CHART 4—SOIL ANALYSIS AND DISPOSAL
Has there e—
been historic NO Is groundwater NO Proceed to Flow Chart 6—
groubeen hi
• ) monitoring Site Reclamation.
monitoring? required? •
YES
V `
YES Contact DWG Regional Office to
approve well locations before
` installation.
Sampling of
welts indicate NO No further groundwater monitoring
ter is required. Proceed to Flow
groundwater violationsto Chart 6—Site Reclamation.
l
YES
Maintain permit with limited actions. In lieu of groundwater monitoring,predictive calculations,
Continue groundwater monitoring as acceptable to the Director,can be submitted to demonstrate
permitted for minimum of three groundwater standards can be met at the property
` sampling events. J boundary. Proceed to Flow Chart 6—Site Reclamation. J
After minimum of
three sampling
events,are r `
groundwater NO `I Proceed to Flow Chart 6—Site
violations detected l Reclamation.
or exceedances
not showing a
lowering trend?
YES
V
Continue monitoring on a schedule
set by DWQ Regional Office
Supervisor.
5 l
Attachment 136 June 22,2012

Attachment B—Closure of Permitted Wastewater Ponds and Lagoons
Flow Chart 6—Site Reclamation)
CONTINUED FROM FLOW CHART 3—LINER DEMOLITION AND DISPOSAL OR
FLOW CHART 5—GROUNDWATER POST CLOSURE MONITORING
Berms/Lagoon Walls'
•
•
YES Is the structure
privately owned
or high risk
municipal?
NO
Is the structure Fill with clean material and/or
completely YES
constructed at or > grade site. Stabilize the site
below grade? with vegetation. END
A
NO
Is the structure
finished in the NO
groundwater
table?
YES
/ 1
Contact DWQ Regional Office to
determine what type of sampling
will be required. Then,proceed
to appropriate Flow Chart.
Recommended more extensive structure demolition
(e.g.removal of berms/dike walls,general grading,
etc.). Stabilize the site with vegetation. END
'Recognize the added value of planned reclamation efforts. Reclamation activities incorporating created orttjicial wetland systems,planted trees,and other pro-
active actions viewed as either mitigation efforts or secondary environmental protection measures may assist with enabling the closure project to qualify for
recognition and benefit from other environmental programs,such as those offered through conservation easements.
In cases where retention of municipal structures provides no value based on projected future site use,it is recommended that minimal demolition be performed to
breach or remove sidewalk(dependent on the size)when the liner is demolished. Minimal demolition maybe considered feasible In cases where retention of the
structure or a portion thereof poses minimal risks based on conditions such as low population densities of surrounding areas,low hazard environment,low
probability of encroaching development,etc.
Attachment B6 June 22,2012

w A rF Michael F.Easley,Governor
9William G.Ross Jr.,Secretary
O� QG E-Dv
North Carolina Department of Environment and Natural Resources
Vj r Alan W.Klimek,P.E.Director
Division of Water Quality
Aquifer Protection Section
May 27, 2005
Town of McAdenville
ATTN: Jerry Helton, Mayor
100 Main Street
McAdenville,NC 28101
Subject: WWTP Waste Lagoon Closure
Church Street
McAdenville,NC
Gaston Co.
Dear Mr. Helton:
Our office has received the document entitled"Closure Plan for the Abandoned Polishing Pond".
According to the Closure Plan,the former polishing pond was utilized as part of one of the Town's domestic
wastewater treatment plants, located at the end of Church Road on land owned by Pharr Yams, Inc. The pond
was abandoned in 1992 due to poor performance and was subsequently removed from the NPDES permit. All
liquids have previously been removed from the pond and closure samples did not reveal any remaining
constituents of concern.
The submitted closure plan appears to meet the necessary elements of the Aquifer Protection Section's
"Guidelines for the Closure of Treatment Ponds and Lagoons,August 18,2003". Our office has no objection to
the plan as it was submitted. If you have further questions,please me at(704) 235-2185, or by email at
[e-mail].
Sincerest Regards,
Bruce Parris
Hydrogeologist II
BRP/brp
G:\Dem\GW\incidents\McAdenville Lagoon Closure 5/27/05
ri
Division of Water Quality/Aquifer Protection Section/Mooresville Regional Office Phone: [phone] Fax: [phone] NCD-
610 E.Center St.,Suite 301,Mooresville,NC 28115 Internet:http://aw.ehnr.state.nc.us

. • '"� .r .f iS \ C
.. , g....bk.'.; N ADE NVI LL k N.C.
•_---* • ►- 4. ���� _-- 1 NCO R PO RAT ED 1 883
7.7
6Y THE RIVER 100 MAIN STREET
[phone] McA I ,. I 'RI `•��,, -sr
A • fai t-.�fw •I',
GVD
April 5, 2005
APR 1 3 2005
Mr. Bruce Parris
Groundwater Section - MOORESVILLE REGIONAL OFFICE
NCDENR DWQ-GROUNDWATER SECTION
610 East Center Avenue, Suite 301
Mooresville,North Carolina 28005
Subject: Closure of Pond
Town of McAdenville
Gaston County
Dear Mr. Parris:
The Town of McAdenville would like to remove the existing abandoned pond by grading
the walls and filling with soil as needed to landscape the area. Please find attached the
Closure Plan submitted for your consideration.
The contractor would like to begin deconstruction activities as soon as possible after the
required thirty-day notification process. As stated in the closure plan, the surrounding
area is under construction for residential houses including water and sewer lines.
Please contact James Davis, ORC at [phone] or myself if any other information is
needed.
Sincerely,
G CI 71, 2 ic '
Jerry Helton, Mayor
Cc: S. Shepherd
W. Cozart
J. Davis

April 4, 2005
Town of McAdenville
Wastewater Treatment Plant
NPDES No. NC0020052
Closure Plan for the Abandoned Polishing Pond
Table of Contents
SECTION PAGE
1.0 INTRODUCTION 1
1.1 Purpose
1.2 Background 1
1.3 Site Description ..1
2.0 FIELD INFORMATION 1
2.1 Sampling Plan 2
2.2 DWQ Certified Laboratory 2
3.0 CLOSURE PLAN 2
3.1 Quantity and Characteristics of Materials for Disposal 2
3.2 Assessment of Alternatives 2
3.3 Reclamation Plan .2
3.4 Vicinity Map ...3
3.5 Location Map 4
4.0 EROSION AND SEDIMENT CONTROL PLAN ,2
APPENDICES
Appendix A...Five Polishing Pond Sediment Samples, Pharr Yarns#1 through #5
Appendix B Five Pond Soil Samples from Walls & Floor, Pond #1 through #5
Prepared for: The Town of McAdenville
Prepared by: Mike Church
Assistant WWTP ORC

Page 1
1.0 INTRODUCTION
The Town of McAdenville wishes to permanently close and remove the subject
wastewater post treatment process. The wastewater treatment plant, constructed in 1965,
added the polishing pond in 1972 to improve removal of any suspended solids in the
effluent prior to disinfection and discharge to the South Fork of the Catawba River. The
polishing pond failed to improve the plant performance and was abandoned in 1992 and
then removed from the NPDES Permit in 2004.
While the wastewater treatment plant is located on property owned by the Town of
McAdenville, the polishing pond was constructed on property owned by Pharr Yarns
with their permission to use the property as needed. Upon consideration of these facts, the
Town of McAdenville wishes to absolve any future use of the property.
1.1 Purpose
The purpose of the closure of the subject polishing pond is to protect the quality of the
groundwater while accomplishing an improvement of the property and surrounding area.
1.2 Background
As stated in the introduction, the polishing pond was added to the treatment process for
additional removal any fine suspended solids that were carried over from the clarifier
process. However, no improvement was accomplished with the post treatment and it was
determined that the pond was actually a detriment and produced more suspended solids
due to algae growth. The wastewater influent is from domestic customers only with no
industrial users. As shown in the analysis of soil and sludge from the polishing pond area,
no pollution was found.
1.3 Site Description
The subject property is at the end of Church Street in McAdenville. The surrounding area
of the Town of McAdenville is being developed by Wesleyan Development, LLC for
residential use. The wastewater collection s stem extension is under construction at this
time; Construction Permit No.i; The fenced in area of the pond covers .82
acres. The water level area covers .52 acres. ` /1 iG a c)L r�SL
444.
2.0 FIELD INFORMATION
The major elements of the pond structure are the compacted natural soil walls and floor.
The contents of the abandoned basin is from rainwater only and is evaporated during dry
conditions. The structure is sound with no erosion of surface water into the basin. All
wastewater was removed from the basin prior to abandonment.
`7c) 866--- 6 726

Page 2
2.1 Sampling Plan
Sampling of the sediment in the pond was collected from 5 locations; 4 from the
perimeter and 1 near the center of the pond and analyzed for nutrients using EPA
Methods 351.2 and 365.2 and TCLP Metals. Sampling of the natural liner of the pond
was collected from 5 locations; 4 from the perimeter and 1 of the native soil near the
center of the pond and analyzed for TCLP Characteristics. See appendices A and B.
2.2 DWG Certified Laboratory
Par Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483
Charlotte,NC 28241 — 1483
Phone: [phone]
NC Cert. No. 20
3.0 CLOSURE PLAN
3.1 Quantity and Characteristics of Materials for Disposal
No material will be disposed of Analysis of the sediment and native soil and contents of
the pond show no contamination as verified in appendices A and B.
3.2 Assessment of Alternatives
The walls of the pond will be completely eliminated and the material incorporated in the
existing site. These materials will not cause a contravention of the groundwater quality
beneath the structure. The surface will be capped with landscaping and seeding of the
soil.
3.3 Reclamation Plan
Reclamation of the site is shown in the attached location map. There will be no treatment,
storage, or disposal of the materials.
3.4 Vicinity Map .See attached map.
3.5 Location Map See attached map.
4.0 EROSION AND SEDIMENT CONTROL PLAN...Not required due to the land
disturbing activity of less than one acre of land.

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ROAD CLASSIFICATION -- • SCALE 1 :24 000
LIGHT-DUTY ROAD,HARD OR 0 1 MILE
PRIMARY HIGHWAY IMPROVED SURFACE ;,— `'
HARD SURFACE � ': ` •
0 7000 FEET
SECONDARY HIGHWAY HARD SURFACE UNIMPROVED =ROAD = ='
—— —
1 0 1 KILOMETER
Latitude 35°15'22" Longitude 81°04'21" ; ;' I I
Map # F14SE Sub-basin 030836 CONTOUR INTERVAL 20 FEET
Stream Class WS-III • QUAD LOCATION Town of McAdenville
Discharge Class 100% Domestic NC0020052
Receiving Stream South Fork Catawba River • Gaston County
WWTP
Design Q 0.13 MGD

TPARPAR Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483 1LABORAToRESINC1.
lv () eo s1 r
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
A ire0 CI irx A ..
,. ,, / e
REPORT OF ANALYSES c &C /0-,e i+ D aiv
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
PO BOX 1939 DATE: 11/23/04
McADENVILLE, NC 28101-
SAMPLE NUMBER- 60567 SAMPLE ID- PHARR YARNS #1 SAMPLE MATRIX- SO
DATE SAMPLED- 11/10/04 TIME SAMPLED- 1500
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 1 of 5
ANALYSIS
ANALYSIS , METHOD DATE TIME BY RESULT UNITS
KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.14 mg/L
TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 0.44 mg/L
TCLP METALS TCLP 11/17/04 1207 CT
ARSENIC TCLP 11/17/04 1207 CT < 0.5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm
LEAD TCLP 11/17/04 1207 CT < 0.5 ppm
MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm
SILVER TCLP 11/17/04 1207 CT < 0.5 ppm
LABORATORY DIRECTORd(...217,14,„_

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES.INC. PO B 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
PO BOX 1939 DATE: 11/23/04
McADENVILLE, NC 28101-
SAMPLE NUMBER- 60568 SAMPLE ID- PHARR YARNS #2 SAMPLE MATRIX- SO
DATE .SAMPLED- 11/10/04 TIME SAMPLED- 1510
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 2 of 5
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.15 mg/L
TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 1.46 mg/L
TCLP METALS TCLP 11/17/04 1207 CT
ARSENIC TCLP 11/17/04 1207 CT < 0.5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm
LEAD TCLP 11/17/04 1207 CT < 0.5 ppm
MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm
SILVER TCLP 11/17/04 1207 CT < 0.5 ppm
eiL44.e._ela!
LABORATORY DIRECTOR

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES. INC. PO BOX 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
PO BOX 1939 DATE: 11/23/04
McADENVILLE, NC 28101-
SAMPLE NUMBER- 60569 SAMPLE ID- PHARR YARNS #3 SAMPLE MATRIX- SO
DATE SAMPLED- 11/10/04 TIME SAMPLED- 1520
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 3 of 5
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.14 mg/L
TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 0.39 mg/L
TCLP METALS TCLP 11/17/04 1207 CT
ARSENIC TCLP 11/17/04 1207 CT < 0 .5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm
LEAD TCLP 11/17/04 1207 CT < 0 .5 ppm
MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm
SILVER TCLP 11/17/04 1207 CT < 0.5 ppm
LABORATORY DIRECTOR

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO BOX 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
PO BOX 1939 DATE: 11/23/04
McADENVILLE, NC 28101-
SAMPLE NUMBER- 60570 SAMPLE ID- PHARR YARNS #4 SAMPLE MATRIX- SO
DATE SAMPLED- 11/10/04 TIME SAMPLED- 1530
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 4 of 5
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.13 mg/L
TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 0.39 mg/L
TCLP METALS TCLP 11/17/04 1207 CT
ARSENIC TCLP 11/17/04 1207 CT < 0 .5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm
LEAD TCLP 11/17/04 1207 CT 0.74 ppm
MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm
SILVER TCLP 11/17/04 1207 CT < 0.5 ppm
LABORATORY DIRECTOR

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES, INC. PO BOX 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
PO BOX 1939 DATE: 11/23/04
McADENVILLE, NC 28101-
SAMPLE NUMBER- 60571 SAMPLE ID- PHARR YARNS #5 SAMPLE MATRIX- SO
DATE SAMPLED- 11/10/04 TIME SAMPLED- 1540
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 5 of 5
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.10 mg/L
TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 0 .47 mg/L
TCLP METALS TCLP 11/17/04 1207 CT
ARSENIC TCLP 11/17/04 1207 CT < 0.5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm
LEAD TCLP 11/17/04 1207 CT < 0.5 ppm
MERCURY TCLP 11/17/04 1207 CT < 0 .02 ppm
SELENIUM TCLP 11/17/04 1207 CT < 0 .1 ppm
SILVER TCLP 11/17/04 1207 CT < 0 .5 ppm
LABORATORY DIRECTOR

11 BAR CHAIN OF CUSTODY
LABORATORIES,INC. PAR Laboratories, Inc
111111111111111 Phone [phone]
Fax [phone].
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories,Inc.and the North
Carolina Department of Environmental and Natural Resources.
Company Name (billing) Comments/Special Instructions
PHARR YARNS g� /1 5y / iY
Address eerCh �(>G, �'-t .
PO BOX 1939 TEMP. OF SAMPLE WHEN TAKEN
City, State & Zip Code N/�
McADENVILLE, NC 28101
_ Point of Contact & Telephone Number
MIKE CHURCH 824-3551 EXT. 310
Sample taken by: mike °4
IS THIS FOR STATE or EPA REPORTING? YES _X_ NO
*Sample type: DW WW GWMW HW Soil _. Other
Sample Temp upon receipt: °C
** Preserved: Yes No >e' Teflon Liner/ Zero Headspace: Yes _ No _N/A )'
Client Sample I.D. Set Up Collection Analyses
(Sample Location / Number) Comp Grab Preserv. Date/Time Date/Time Requested
131-14 kr * l II-l als-a 0 Tc�-O. /1i,71nP��s �l s
y,rHs , f
/1 I # Y , //—/. 5—ia (4 c ( 1
I1 1 ( , 3 )( /-/o/% It ( I
if
f tt- 1 �( i I l oA-3o ' ` `
1
Relinquished by: Date/Time Received by: Date/Time
W '(le /1.‘--4"z--(--X.//%/—d 4/ 47....,,,,-- ,/--- (//,,b, /,SS
Relinquished by:
Date/Time Received by: Date/Time
• C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste
•• See Other Side

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES.INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.p arlabs.com A/9f4c1/x (.J ICJ
/ 5,-,int,a Im;
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
SAMPLE NUMBER- 62681 SAMPLE ID- PY DWTP POND SOIL #1 SAMPLE MATRIX- SO
DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 0930
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH RECEIVED BY- RE
TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab
Page 1 of 10
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
TCLP CHARACTERISTICS TCLP 02/16/05 SK
pH VALUE TCLP 02/16/05 SK 6.09 S.U.
CORROSIVITY TCLP 02/16/05 SK NON
REACTIVITY TCLP 02/16/05 SK NON
FLASH POINT TCLP 02/16/05 SK < 200 degrees F
IGNITABILITY TCLP 02/16/05 SK NON
PAINT FILTER TEST TCLP 02/16/05 SK NFL
TCLP METALS TCLP 02/16/05 SK
ARSENIC TCLP 02/16/05 SK < 0.5 ppm
BARIUM TCLP 02/16/05 SK < 10 ppm
CADMIUM TCLP 02/16/05 SK < 0.1 ppm
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm
LEAD TCLP 02/16/05 SK < 0.5 ppm
MERCURY TCLP 02/16/05 SK < 0.02 ppm
SELENIUM TCLP 02/16/05 SK < 0. 1 ppm
SILVER TCLP 02/16/05 SK < 0.5 ppm
TCLP PESTICIDES TCLP 02/16/05 SK
ENDRIN TCLP 02/16/05 SK < 0.002 ppm
LINDANE TCLP 02/16/05 SK < 0.04 ppm
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm
TOXAPHENE TCLP 02/16/05 SK < 0.05 ppm

[PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cart#20;SC Cart#99003
www.parlabs.corn
Page 2 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62681
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2, 4-D TCLP 02/16/05 SK < 1 ppm
2,4,5-TP(SILVEX) TCLP 02/16/05 SK < 0.1 ppm
TCLP ORGANICS TCLP 02/16/05 SK
BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
CHLOROFORM TCLP 02/16/05 SK < 0. 6 ppm
o-CRESOL TCLP 02/16/05 SK < 20 ppm
p-CRESOL TCLP 02/16/05 SK < 20 ppm
m-CRESOL TCLP 02/16/05 SK < 20 ppm
1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm
1,2-DICHLOROETHANE TCLP 02/16/05 SK < 0.05 ppm
1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm
2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm
2, 4,5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
2,4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm
VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
LABORATORY DIRECTOR 1.......4"............_ Arr

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
SAMPLE NUMBER- 62682 SAMPLE ID- PY DWTP POND SOIL #2 SAMPLE MATRIX- SO
DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 0940
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH RECEIVED BY- RE
TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab
Page 3 of 10
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
TCLP CHARACTERISTICS TCLP 02/16/05 SK
pH VALUE TCLP 02/16/05 SK 7.30 S.U.
CORROSIVITY TCLP 02/16/05 SK NON
REACTIVITY TCLP 02/16/05 SK NON
FLASH POINT TCLP 02/16/05 SK < 200 degrees F
IGNITABILITY TCLP 02/16/05 SK NON
PAINT FILTER TEST TCLP 02/16/05 SK NFL
TCLP METALS TCLP 02/16/05 SK
ARSENIC TCLP 02/16/05 SK < 0.5 ppm
BARIUM TCLP 02/16/05 SK < 10 ppm
CADMIUM TCLP 02/16/05 SK < 0.1 ppm
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm
LEAD TCLP 02/16/05 SK < 0.5 ppm
MERCURY TCLP 02/16/05 SK < 0.02 ppm
SELENIUM TCLP 02/16/05 SK < 0.1 ppm
SILVER TCLP 02/16/05 SK < 0.5 ppm
TCLP PESTICIDES TCLP 02/16/05 SK
ENDRIN TCLP 02/16/05 SK < 0.002 ppm
LINDANE TCLP 02/16/05 SK < 0.04 ppm
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm
TOXAPHENE TCLP 02/16/05 SK < 0.05 ppm

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
MEW Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
Page 4 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62682
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2, 4-D TCLP 02/16/05 SK < 1 ppm
2, 4,5-TP(SILVEX) TCLP 02/16/05 SK < 0.1 ppm
TCLP ORGANICS TCLP 02/16/05 SK
BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
CHLOROFORM TCLP 02/16/05 SK < 0.6 ppm
o-CRESOL TCLP 02/16/05 SK < 20 ppm
p-CRESOL TCLP 02/16/05 SK < 20 ppm
m-CRESOL TCLP 02/16/05 SK < 20 ppm
1,4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm
1,2-DICHLOROETHANE TCLP 02/16/05 SK < 0.05 ppm
1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm
2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm
2,4, 5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
2, 4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm
VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
LABORATORY DIRECTOR Cam(/

PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES.IN) PAR
PG Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20,SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
SAMPLE NUMBER- 62683 SAMPLE ID- PY DWTP POND SOIL #3 SAMPLE MATRIX- SO
DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 0945
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH RECEIVED BY- RE
TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab
Page 5 of 10
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
TCLP CHARACTERISTICS TCLP 02/16/05 SK
pH VALUE TCLP 02/16/05 SK 6.80 S.U.
CORROSIVITY TCLP 02/16/05 SK NON
REACTIVITY TCLP 02/16/05 SK NON
FLASH POINT TCLP 02/16/05 SK < 200 degrees F
IGNITABILITY TCLP 02/16/05 SK NON
PAINT FILTER TEST TCLP 02/16/05 SK NFL
TCLP METALS TCLP 02/16/05 SK
ARSENIC TCLP 02/16/05 SK < 0.5 ppm
BARIUM TCLP 02/16/05 SK < 10 ppm
CADMIUM TCLP 02/16/05 SK < 0. 1 ppm
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm
LEAD TCLP 02/16/05 SK < 0.5 ppm
MERCURY TCLP 02/16/05 SK < 0.02 ppm
SELENIUM TCLP 02/16/05 SK < 0. 1 ppm
SILVER TCLP 02/16/05 SK < 0.5 ppm
TCLP PESTICIDES TCLP 02/16/05 SK
ENDRIN TCLP 02/16/05 SK < 0.002 ppm
LINDANE TCLP 02/16/05 SK < 0.04 ppm
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm
TOXAPHENE TCLP 02/16/05 SK < 0.05 ppm

[PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
Page 6 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62683
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2,4-D TCLP 02/16/05 SK < 1 ppm
2, 4,5-TP(SILVEX) TCLP 02/16/05 SK < 0.1 ppm
TCLP ORGANICS TCLP 02/16/05 SK
BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
CHLOROFORM TCLP 02/16/05 SK < 0. 6 ppm
o-CRESOL TCLP 02/16/05 SK < 20 ppm
p-CRESOL TCLP 02/16/05 SK < 20 ppm
m-CRESOL TCLP 02/16/05 SK < 20 ppm
1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm
1,2-DICHLOROETHANE TCLP 02/16/05 SK < 0.05 ppm
1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm
2,4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm
2, 4,5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
2,4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm
VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
a\.........444 ....22E
LABORATORY DIRECTOR

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
1111111111111, Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
SAMPLE NUMBER- 62684 SAMPLE ID- PY DWTP POND SOIL #4 SAMPLE MATRIX- SO
DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 0950
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH RECEIVED BY- RE
TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab
Page 7 of 10
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
TCLP CHARACTERISTICS TCLP 02/16/05 SK
pH VALUE TCLP 02/16/05 SK 6.10 S.U.
CORROSIVITY TCLP 02/16/05 SK NON
REACTIVITY TCLP 02/16/05 SK NON
FLASH POINT TCLP 02/16/05 SK < 200 degrees F
IGNITABILITY TCLP 02/16/05 SK NON
PAINT FILTER TEST TCLP 02/16/05 SK NFL
TCLP METALS TCLP 02/16/05 SK
ARSENIC TCLP 02/16/05 SK < 0.5 ppm
BARIUM TCLP 02/16/05 SK < 10 ppm
CADMIUM TCLP 02/16/05 SK < 0. 1 ppm
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm
LEAD TCLP 02/16/05 SK < 0.5 ppm
MERCURY TCLP 02/16/05 SK < 0.02 ppm
SELENIUM TCLP 02/16/05 SK < 0.1 ppm
SILVER TCLP 02/16/05 SK < 0.5 ppm
TCLP PESTICIDES TCLP 02/16/05 SK
ENDRIN TCLP 02/16/05 SK < 0.002 ppm
LINDANE TCLP 02/16/05 SK < 0.04 ppm
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm
TOXAPHENE TCLP 02/16/05 SK < 0.05 ppm

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
Page 8 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62684
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2,4-D TCLP 02/16/05 SK < 1 ppm
2,4,5-TP(SILVEX) TCLP 02/16/05 SK < 0. 1 ppm
TCLP ORGANICS TCLP 02/16/05 SK
BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
CHLOROFORM TCLP 02/16/05 SK < 0.6 ppm
o-CRESOL TCLP 02/16/05 SK < 20 ppm
p-CRESOL TCLP 02/16/05 SK < 20 ppm
m-CRESOL TCLP 02/16/05 SK < 20 ppm
1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm
1,2-DICHLOROETHANE TCLP 02/16/05 SK < 0.05 ppm
1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm
2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm
2,4,5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
2, 4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm
VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
LABORATORY DIRECTOR O

[PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 4114.83
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
SAMPLE NUMBER- 62685 SAMPLE ID- PY DWTP POND SOIL #5 SAMPLE MATRIX- SO
DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 1005
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH RECEIVED BY- RE
TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab
Page 9 of 10
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
TCLP CHARACTERISTICS TCLP 02/16/05 SK
pH VALUE TCLP 02/16/05 SK 7.37 S.U.
CORROSIVITY TCLP 02/16/05 SK NON
REACTIVITY TCLP 02/16/05 SK NON
FLASH POINT TCLP 02/16/05 SK < 200 degrees F
IGNITABILITY TCLP 02/16/05 SK NON
PAINT FILTER TEST TCLP 02/16/05 SK NFL
TCLP METALS TCLP 02/16/05 SK
ARSENIC TCLP 02/16/05 SK < 0.5 ppm
BARIUM TCLP 02/16/05 SK < 10 ppm
CADMIUM TCLP 02/16/05 SK < 0.1 ppm
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm
LEAD TCLP 02/16/05 SK < 0.5 ppm
MERCURY TCLP 02/16/05 SK < 0.02 ppm
SELENIUM TCLP 02/16/05 SK < 0.1 ppm
SILVER TCLP 02/16/05 SK < 0.5 ppm
TCLP PESTICIDES TCLP 02/16/05 SK
ENDRIN TCLP 02/16/05 SK < 0.002 ppm
LINDANE TCLP 02/16/05 SK < 0.04 ppm
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm
TOXAPHENE TCLP 02/16/05 SK < 0.05 ppm

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO BOX 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
Page 10 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62685
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2,4-D TCLP 02/16/05 SK < 1 ppm
2, 4,5-TP(SILVEX) TCLP 02/16/05 SK < 0.1 ppm
TCLP ORGANICS TCLP 02/16/05 SK
BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
CHLOROFORM TCLP 02/16/05 SK < 0.6 ppm
o-CRESOL TCLP 02/16/05 SK < 20 ppm
p-CRESOL TCLP 02/16/05 SK < 20 ppm
m-CRESOL TCLP 02/16/05 SK < 20 ppm
1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm
1,2-DICHLOROETHANE TCLP 02/16/05 SK < 0.05 ppm
1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm
2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm
2,4,5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
2, 4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm
VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
LABORATORY DIRECTOR Fr

PAR , CHAIN OF CUSTODY
usoRaroRres,INC. r' -, PAR Laboratories, Inc
Phone [phone]
IIIMMIN Fax [phone].
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories,Inc. and the North
Carolina Department of Environmental and Natural Resources.
Company Name (billing) Comments/Special Instructions
PHARR YARNS
Address
PO BOX 1939 TEMP. OF SAMPLE WHEN TAKEN
City, State & Zip Code
McADENVILLE, NC 28101
_ Point of Contact & Telephone Number
MIKE CHURCH 824-3551 EXT. 310
Sample taken by: Ai if/C' C 9cc J-c
IS THIS FOR STATE or EPA REPORTING? YES _X_ NO
*Sample type: DW WW GWMW HW Soil V Other
Sample Temp upon receipt: °C
** Preserved: Yes No )/ Teflon Liner/ Zero Headspace: Yes _ No _N/A
Client Sample I.D. Set Up Collection Analyses
(Sample Location/Number) Comp Grab Preserv. Date/Time Date/Time Requested
Ply rr &a kie S
tT P p©k1d , 1 'l 1-y frfv IC z p
it It 1I tt2_ !/ "//o yyo TcLP
ZI 11 It t$3 7-- /D9 s T4f
L` `I If Ct9 7- z--��c s T'cip 1
ilt , , �� 2—7CO 7z L P
•
Relinquished by: Date/Time Received by: Date/Time
7elin1A/;: ue,t ' f -5._-<:3s II3 z-
d -Q-0 5 1130
qu;sh d by:
Date/Time Rec ved by: Date/Time
• C =Composite = ab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste
•• See Other Si e /

April 4, 2005
Town of McAdenville
Wastewater Treatment Plant
NPDES No. NC0020052
Closure Plan for the Abandoned Polishing Pond
Table of Contents
SECTION PAGE
1.0 INTRODUCTION 1
1.1 Purpose
1.2 Background 1
1.3 Site Description 1
2.0 FIELD INFORMATION 1
2.1 Sampling Plan 2
2.2 DWQ Certified Laboratory ..2
3.0 CLOSURE PLAN .2
3.1 Quantity and Characteristics of Materials for Disposal 2
3.2 Assessment of Alternatives ..2
3.3 Reclamation Plan ..2
3.4 Vicinity Map ...3
3.5 Location Map 4
4.0 EROSION AND SEDIMENT CONTROL PLAN 2
APPENDICES
Appendix A...Five Polishing Pond Sediment Samples, Pharr Yarns#1 through #5
Appendix B Five Pond Soil Samples from Walls & Floor,Pond #1 through #5
Prepared for: The Town of McAdenville
Prepared by: Mike Church
Assistant WWTP ORC

Page 1
1.0 INTRODUCTION
The Town of McAdenville wishes to permanently close and remove the subject
wastewater post treatment process. The wastewater treatment plant, constructed in 1965,
added the polishing pond in 1972 to improve removal of any suspended solids in the
effluent prior to disinfection and discharge to the South Fork of the Catawba River. The
polishing pond failed to improve the plant performance and was abandoned in 1992 and
then removed from the NPDES Permit in 2004.
While the wastewater treatment plant is located on property owned by the Town of
McAdenville, the polishing pond was constructed on property owned by Pharr Yarns
with their permission to use the property as needed. Upon consideration of these facts, the
Town of McAdenville wishes to absolve any future use of the property.
1.1 Purpose
The purpose of the closure of the subject polishing pond is to protect the quality of the
groundwater while accomplishing an improvement of the property and surrounding area.
1.2 Background
As stated in the introduction, the polishing pond was added to the treatment process for
additional removal any fine suspended solids that were carried over from the clarifier
process. However, no improvement was accomplished with the post treatment and it was
determined that the pond was actually a detriment and produced more suspended solids
due to algae growth. The wastewater influent is from domestic customers only with no
industrial users. As shown in the analysis of soil and sludge from the polishing pond area,
no pollution was found.
1.3 Site Description
The subject property is at the end of Church Street in McAdenville. The surrounding area
of the Town of McAdenville is being developed by Wesleyan Development, LLC for
residential use. The wastewater collection system extension is under construction at this
time; Construction Permit No. WQ0024588. The fenced in area of the pond covers .82
acres. The water level area covers .52 acres.
2.0 FIELD INFORMATION
The major elements of the pond structure are the compacted natural soil walls and floor.
The contents of the abandoned basin is from rainwater only and is evaporated during dry
conditions. The structure is sound with no erosion of surface water into the basin. All
wastewater was removed from the basin prior to abandonment.

Page 2
2.1 Sampling Plan
Sampling of the sediment in the pond was collected from 5 locations; 4 from the
perimeter and 1 near the center of the pond and analyzed for nutrients using EPA
Methods 351.2 and 365.2 and TCLP Metals. Sampling of the natural liner of the pond
was collected from 5 locations; 4 from the perimeter and 1 of the native soil near the
center of the pond and analyzed for TCLP Characteristics. See appendices A and B.
2.2 DWG Certified Laboratory
Par Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483
Charlotte,NC 28241 — 1483
Phone: [phone]
NC Cert. No. 20
3.0 CLOSURE PLAN
3.1 Quantity and Characteristics of Materials for Disposal
No material will be disposed of. Analysis of the sediment and native soil and contents of
the pond show no contamination as verified in appendices A and B.
3.2 Assessment of Alternatives
The walls of the pond will be completely eliminated and the material incorporated in the
existing site. These materials will not cause a contravention of the groundwater quality
beneath the structure. The surface will be capped with landscaping and seeding of the
soil.
3.3 Reclamation Plan
Reclamation of the site is shown in the attached location map. There will be no treatment,
storage, or disposal of the materials.
3.4 Vicinity Map .See attached map.
3.5 Location Map See attached map.
4.0 EROSION AND SEDIMENT CONTROL PLAN...Not required due to the land
disturbing activity of less than one acre of land.

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I I
ROAD CLASSIFICATION ' SCALE 1 :24 000
•
LIGHT-DUTY ROAD,HARD OR 0 1 MILE
PRIMARY HIGHWAY IMPROVED SURFACE —
HARD SURFACE -
0. 7000 FEET
•
SECONDARY HIGHWAY UNIMPROVED ROAD — ;— —
HARD SURFACE 00 = — = 1 KILOMETER
1 ., . 0
04121 I
r
Latitude 35°15'22" Longitude 81°04'21"
INTERVAL 20 FEET
Map # F14SE Sub-basin Q30836
Stream Class WS-III QUAD LOCATION Town of McAdenville
Discharge Class 100% Domestic NC0020052
Receiving Stream South Fork Catawba River Gaston County
WWTP
Design Q 0.13 MGD
7 t1 //:,„_. :. /1A, , P1 3 ' -

(PAR PAR Laboratories, Inc.
2217 Graham Park Drive _
L480RATORIES.INC PO Box 411483 D t'j ( ( ' (-3i,i1 44
r
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
Afreq
CI,x A ?
1„ I f
REPORT OF ANALYSES ed i Erb+ ,C//J'/0/
7
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
PO BOX 1939 DATE: 11/23/04
McADENVILLE, NC 28101-
Al
r.•.:, SAMPLE NUMBER- 60567 SAMPLE ID- PHARR YARNS #1 SAMPLE MATRIX- SO
DATE SAMPLED- 11/10/04 TIME SAMPLED- 1500
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 1 of 5
ANALYSIS
ANALYSIS , METHOD DATE TIME BY RESULT UNITS
EL KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.14 mg/L
iffiri TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 0.44 mg/L
TCLP METALS TCLP 11/17/04 1207 CT
ARSENIC TCLP 11/17/04 1207 CT < 0.5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm
LEAD TCLP 11/17/04 1207 CT < 0.5 ppm
MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm
SILVER TCLP 11/17/04 1207 CT < 0.5 ppm
es.......44,_ or
LABORATORY DIRECTOR

J
PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
PO BOX 1939 DATE: 11/23/04
McADENVILLE, NC 28101-
SAMPLE NUMBER- 60568 SAMPLE ID- PHARR YARNS #2 SAMPLE MATRIX- SO
DATE SAMPLED- 11/10/04 TIME SAMPLED- 1510
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 2 of 5
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.15 mg/L
TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 1.46 mg/L '
TCLP METALS TCLP 11/17/04 1207 CT "- —
ARSENIC TCLP 11/17/04 1207 CT < 0.5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm ;^:
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm i
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm
LEAD TCLP 11/17/04 1207 CT < 0.5 ppm
MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm =-IM
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm
SILVER TCLP 11/17/04 1207 CT < 0.5 ppm "
erN....4"............. Off •-r ".
' LABORATORY DIRECTOR
4
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PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
wi
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
'- : PO BOX 1939
DATE: 11/23/04
;x; •: McADENVILLE, NC 28101-
y�3.
a�!�:� SAMPLE NUMBER- 60569 SAMPLE ID- PHARR YARNS #3 SAMPLE MATRIX- SO
a DATE SAMPLED- 1Z/1C/04
` TIME SAMPLED- 1520
'-Y DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 3 of 5
ANALYSIS .-
ANALYSIS METHOD DATE TIME BY RESULT UNITS ,�,fi''
AKJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.14 mg/L 'TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 0.39 mg/L -4
TCLP METALS TCLP 11/17/04 1207 CTf
ARSENIC TCLP 11/17/04 1207 CT < 0.5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm 0.
;
g' CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm Vif"
n'W -
+ LEAD TCLP 11/17/04 1207 CT < 0.5 ppm Y
"i MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm I
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm s ,
P ,.Xr SILVER TCLP 11/17/04 1207 CT < 0.5 ppm V
1........4, 0(....".........
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LABORATORY DIRECTOR
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PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
REPORT OF ANALYSES
4;t
.: ,; Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
e PO BOX 1939 DATE: 11/23/04
MCADENVILLE, NC 28101-
SAMPLE NUMBER- 60570 SAMPLE ID- PHARR YARNS #4 SAMPLE MATRIX- SO
DATE SAMPLED- 11 /10 �04
%� � � � TIME SAMPLED- 1530
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 4 of 5
"il ANALYS I S
u,g ANALYSIS METHOD DATE TIME BY RESULT UNITS
.A
kV
+V
"� ' KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.13 mg/L
TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 0.39 mg/L41
TCLP METALS TCLP 11/17/04 1207 CT Aho
ARSENIC TCLP 11/17/04 1207 CT < 0.5 ppm ,,t--4,
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm s;c,
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm =..�
LEAD TCLP 11/17/04 1207 CT 0.74 ppm
MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm
SILVER TCLP 11/17/04 1207 CT < 0.5 ppm .,,,
4
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/PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES.INC. PO Box 41 1483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: NOV 04
PO BOX 1939 DATE: 11/23/04
McADENVILLE, NC 28101-
SAMPLE NUMBER- 60571 SAMPLE ID- PHARR YARNS #5 SAMPLE MATRIX- SO
DATE SAMPLED- 11/10/04 TIME SAMPLED- 1540
DATE RECEIVED- 11/11/04 SAMPLER- MIKE CHURCH RECEIVED BY- MJ
TIME RECEIVED- 1158 DELIVERED BY- MIKE CHURCH TYPE SAMPLE- Grab
Page 5 of 5
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
KJELDAHL NITROGEN EPA 351.2 11/20/04 1245 CT 0.10 mg/L
TOTAL PHOSPHOROUS EPA 365.2 11/20/04 1140 CT 0.47 mg/L
TCLP METALS TCLP 11/17/04 1207 CT
ARSENIC TCLP 11/17/04 1207 CT < 0.5 ppm
BARIUM TCLP 11/17/04 1207 CT < 10 ppm
CADMIUM TCLP 11/17/04 1207 CT < 0.1 ppm
CHROMIUM TCLP 11/17/04 1207 CT < 0.5 ppm
LEAD TCLP 11/17/04 1207 CT < 0.5 ppm
MERCURY TCLP 11/17/04 1207 CT < 0.02 ppm
SELENIUM TCLP 11/17/04 1207 CT < 0.1 ppm
SILVER TCLP 11/17/04 1207 CT < 0.5 ppm
S‘.......11•4. or
LABORATORY DIRECTOR
e.4
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PAR CHAIN OF CUSTODY
LABORATORIES.INC. PAR Laboratories, Inc
Phone [phone]
Fax [phone].
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories,Inc.and the North
Carolina Department of Environmental and Natural Resources.
Company Name (billing) Comments/Special Instructions
PHARR YARNS n /1 5m ,/�h .—
Address e4C f -ZL9G-->q *3(-t .4,4
PO BOX 1939 TEMP. OF SAMPLE WHEN TAKEN
City, State & Zip Code �/
McADENVILLE, NC 28101
Point of Contact & Telephone Number
MIKE CHURCH 824-3551 EXT. 310
Sample taken by: 44 1k€ °,61�,
IS THIS FOR STATE or EPA REPORTING? YES _X_ NO
*Sample type: DW WW GWMW HW Soil )C Other
Sample Temp upon receipt: °C
** Preserved: Yes No x Teflon Liner/ Zero Headspace: Yes _No _N/A A
Client Sample I.D. Set Up Collection Analyses
(Sample Location/Number) Comp Grab Preserv. Date/Time Date/Time Requested
/� *I %O-0 rc4� /j/fnPii 11,
/—L1�i VT ya ryt s II— / /
II 11 't Ji-/op If ` 1
it if 14 i/"Pik_To 11 ' t ` `
), 1, - )( 1No�sz/o t 1 , , 1 t
1
Relinquished by:
Date/Time Received by: Date/Time
/// �:WO � _ ////—o _ !" ii�i/Jay r/S�i Date/Time
Relinquished by: Date/Time Received by:
•
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste
See Other Side

PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES.INC. PO BOX 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003 6--
wwwparlabs.com AppeC4j
t, r
�S. / > l'�'J /a7
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
.0- SAMPLE NUMBER- 62681 SAMPLE ID- PY DWTP POND SOIL #1 SAMPLE MATRIX- SO
. ' DATE SAMPLED- 02/09/05 LOCATION- DWTP
TIME SAMPLED- 0930
' DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH
RECEIVED BY- RE
` � TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON
"`'' TYPE SAMPLE- Grab
t;,. >r Page 1 of 10
,,t;
Yam,
;, ANALYSIS
- "- ANALYSIS METHOD DATE TIME BY RESULT UNITS
TCLP CHARACTERISTICS TCLP 02/16/05 SK '�",
pH VALUE TCLP 02/16/05 SK 6.09 S.U. 9
CORROSIVITY TCLP 02/16/05 SK NON IP: .
REACTIVITY TCLP 02/16/05 SK NON
FLASH POINT TCLP 02/16/05 SK < 200 degrees F
IGNITABILITY TCLP 02/16/05 SK NON
PAINT FILTER TEST TCLP 02/16/05 SK NFL
TCLP METALS TCLP 02/16/05 SK
ARSENIC TCLP 02/16/05 SK < 0.5 ppm
BARIUM TCLP 02/16/05 SK < 10 ppm
CADMIUM TCLP 02/16/05 SK < 0.1 ppm
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm
LEAD TCLP 02/16/05 SK < 0.5 ppm
MERCURY TCLP 02/16/05 SK < 0.02 ppm
SELENIUM TCLP 02/16/05 SK < 0.1 ppm
SILVER TCLP 02/16/05 SK < 0.5 ppm
TCLP PESTICIDES TCLP 02/16/05 SK
ENDRIN TCLP 02/16/05 SK < 0.002 ppm
LINDANE TCLP 02/16/05 SK < 0.04 ppm
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm
TOXAPHENE TCLP 02/16/05 SK < 0.05 ppm
.AT.
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[PAR
PAR Laboratories, Inc.
2217 Graham Park Drive
L AQORATORIES.INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
Page 2 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62681
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2, 4-D TCLP 02/16/05 SK < 1 ppm
2, 4, 5-TP(SILVEX) TCLP 02/16/05 SK < 0.1 ppm
TCLP ORGANICS TCLP 02/16/05 SK
BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
CHLOROFORM TCLP 02/16/05 SK < 0. 6 ppm
o-CRESOL TCLP 02/16/05 SK < 20 ppm
p-CRESOL TCLP 02/16/05 SK < 20 ppm .,iw
m-CRESOL TCLP 02/16/05 SK < 20 ppm
1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm
1,2-DICHLOROETHANE TCLP 02/16/05 SK < 0.05 ppm
l, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm
ik 2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
it41 HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
_' METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm
2, 4,5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
I.1,
, 2, 4, 6-TRICHLORPHENOLTCLP02/16/05SK < 0.2 ppm
,, VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
ill
S‘..... ., ....4"........._ op
LABORATORY DIRECTOR

��� PAR Laboratories, Inc_
2217 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
SAMPLE NUMBER- 62682 SAMPLE ID- PY DWTP POND SOIL #2 SAMPLE MATRIX- SO
DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 0940
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH RECEIVED BY- RE
TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab
Page 3 of 10
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
TCLP CHARACTERISTICS TCLP 02/16/05 SK 1,,,,,
pH VALUE 1,
TCLP 02/16/05 SK 7.30 S.U.
CORROSIVITY TCLP 02/16/05 SK NON
REACTIVITY TCLP 02/16/05 SK NON
FLASH POINT TCLP 02/16/05 SK < 200 degrees F i
IGNITABILITY TCLP 02/16/05 SK NON
PAINT FILTER TEST TCLP 02/16/05 SK NFL
TCLP METALS TCLP 02/16/05 SK 1;
0 LT ARSENIC ,
TCLP 02/16/05 SK < 0.5 ppm k•.
BARIUM TCLP 02/16/05 SK < 10 ppm r-
CADMIUM TCLP 02/16/05 SK < 0. 1 ppm
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm
LEAD TCLP 02/16/05 SK < 0.5 ppm
MERCURY TCLP 02/16/05 SK < 0.02 ppm
SELENIUM TCLP 02/16/05 SK < 0.1 ppm
SILVER TCLP 02/16/05 SK < 0.5 ppm `*"
TCLP PESTICIDES TCLP 02/16/05 SK
ENDRIN TCLP 02/16/05 SK < 0.002 ppm ,•,,0
LINDANE TCLP 02/16/05 SK < 0.04 ppm I
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm .:'`,
TOXAPHENE TCLP 02/16/05 SK < 0.05 ppm ", =I
, ,•
r,+;xs,
..9 { 4LYLL,

[PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES.INC. PO Box 411483
Charlotte, NC 28241-1483
IIII Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
Page 4 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62682
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
x CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2, 4-D TCLP 02/16/05 SK < 1 ppm
2, 4,5-TP(SILVEX) TCLP 02/16/05 SK < 0.1 ppm
TCLP ORGANICS TCLP 02/16/05 SK ;;qfti I
BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
.' CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
`iCHLOROFORM TCLP 02/16/05 SK < 0.6 ppm
o-CRESOL TCLP 02/16/05 SK < 20 ppm ` 1
i.`i '' p-CRESOL TCLP 02/16/05 SK < 20 ppm
m-CRESOL TCLP 02/16/05 SK < 20 ppm
1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm
1, 2-DICHLOROETHANE V
TCLP 02/16/05 SK < O.OS ppm 1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm
2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm
2, 4, 5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
2, 4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm
VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
, s
LABORATORY DIRECTORj'‘-',..]4;M4..^,- 1AP
u
M

PAR Laboratories, Inc.
PAR 2217 Graham Park Drive
• LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
SAMPLE NUMBER- 62683 SAMPLE ID- PY DWTP POND SOIL #3 SAMPLE MATRIX- SO
DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 0945
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH RECEIVED BY- RE
TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab KV
Page 5 of 10 r
ti
'X`V
ANALYSIS ,,
ANALYSIS METHOD DATE TIME BY RESULT UNITS ' �
;,i
TCLP CHARACTERISTICS TCLP 02/16/05 SK '
070 pH VALUE TCLP 02/16/05 SK 6.80 S.U.
10 CORROSIVITY TCLP 02/16/05 SK NON
REACTIVITY TCLP 02/16/05 SK NON Qy
FLASH POINT TCLP 02/16/05 SK < 200 degrees F
IGNITABILITY TCLP 02/16/05 SK NON
PAINT FILTER TEST TCLP 02/16/05 SK NFL
5
TCLP METALS TCLP 02/16/05 SK
ARSENIC TCLP 02/16/05 SK < 0.5 ppm
BARIUM TCLP 02/16/05 SK < 10 ppm
CADMIUM TCLP 02/16/05 SK < 0. 1 ppm
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm ill
LEAD TCLP 02/16/05 SK < 0.5 ppm 'gi�
MERCURY' ,'n,"
TCLP 02/16/05 SK < 0.02 ppm 'w,k
SELENIUM TCLP 02/16/05 SK < 0.1 ppm
SILVER TCLP 02/16/05 SK < 0.5 ppm :^ III
• TCLP PESTICIDES TCLP 02/16/05 SK `'4
"`' ENDRIN TCLP 02/16/05 SK < 0.002 ppm
LINDANE TCLP 02/16/05 SK < 0.04 ppm
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm
TOXAPHENE mt.
TCLP 02/16/05 SK < 0.05 ppm h"'
g tl

[PAR PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATOF?IES INC
PO Box 41 1483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
Page 6 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62683
ANALYSIS
IC ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2, 4-D TCLP 02/16/05 SK < 1 ppm
2, 4, 5-TP(SILVEX) TCLP 02/16/05 SK < 0.1 ppm
'`l -
TCLP ORGANICS TCLP 02/16/05 SK
-a BENZENE TCLP 02/16/05 SK < 0.05 ppm
t%,
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
r CHLOROFORM TCLP 02/16/05 SK < 0. 6 ppm
4',
o-CRESOL TCLP 02/16/05 SK < 20 ppm
p-CRESOL TCLP 02/16/05 SK < 20 ppm
m-CRESOL TCLP 02/16/05 SK < 20 ppm
1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm ;;:_
1,2-DICHLOROETHANE TCLP 02/16/05 SK < 0.05 ppm ,; "i
1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm ",;a.
2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm 1Fr ;
HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm }*
2, 4,5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
2,4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm
VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
etk' Ssi..... ..444......, Ap,,i,
LABORATORY DIRECTOR
I
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��� PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES, INC PO Box 411483
Charlotte, NC 28241-1483
11111111 Phone: [phone]; Fax: [phone]
NC Cert#20:SC Cert#99003
www.parlabs.corn
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
p
'k' SAMPLE NUMBER- 62684 SAMPLE ID- PY DWTP POND SOIL #4 SAMPLE MATRIX- SO
^',., DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 0950
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH
RECEIVED BY- RE
fir- TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON
TYPE SAMPLE- Grab
+'' Page 7 of 10
c ANALYSIS
": ANALYSIS METHOD DATE TIME BY RESULT UNITS ;.
w4 '
TCLP CHARACTERISTICS TCLP 02/16/05 SK
ate pH VALUE TCLP 02/16/05 SK 6.10 S.U. ..i
CORROSIVITY TCLP 02/16/05 SK NON ''
REACTIVITY TCLP 02/16/05 SK NON
JO FLASH POINT TCLP 02/16/05 SK < 200 degrees F .A '
IGNITABILITY TCLP 02/16/05 SK NON g ', ,k,
�� I
PAINT FILTER TEST TCLP 02/16/05 SK NFL
TCLP METALS TCLP 02/16/05 SK
ARSENIC TCLP 02/16/05 SK < 0.5
ppm ra,,
BARIUM TCLP 02/16/05 SK < 10 ppm PY
';,
CADMIUM TCLP 02/16/05 SK < 0. 1 ppm *,
CHROMIUM TCLP 02/16/05 SK < 0.5 ppma
LEAD TCLP 02/16/05 SK < 0.5 ppm
MERCURY TCLP 02/16/05 SK < 0.02 ppm -:.
SELENIUM TCLP 02/16/05 SK < 0. 1 ppm i? ;:;
SILVER TCLP 02/16/05 SK < 0.5 ppm
TCLP PESTICIDES TCLP 02/16/05 SK `"'`.;
xj
ENDRIN TCLP 02/16/05 SK < 0.002 ppm
LINDANE TCLP 02/16/05 SK < 0.04 ppm i '•J'
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppm
TOXAPHENE TCLP 02/16/05 SK < 0.05 ppm
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PAR Laboratories, Inc.
[PAR 2217 Graham Park Drive
aeor�aroRiEs.INC
PO Box 41 1483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.corn
Page 8 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62684
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2, 4-D TCLP 02/16/05 SK < 1 ppm
2, 4,5-TP(SILVEX) TCLP 02/16/05 SK < 0.1 ppm
TCLP ORGANICS TCLP 02/16/05 SK
BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm
CHLOROFORM TCLP 02/16/05 SK < 0.6 ppm
o-CRESOL TCLP 02/16/05 SK < 20 ppm
p-CRESOL TCLP 02/16/05 SK < 20 ppm
m-CRESOL TCLP 02/16/05 SK < 20 ppm T.
1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm
1,2-DICHLOROETHANE TCLP 02/16/05 SK < 0.05 ppm
1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm
2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
'` HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm 3
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm t
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm K+`
2, 4,5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm Ae;
2, 4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm
VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm ``'',rrLABORATORY DIRECTOR 1 OF
•
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't e .`Ss#Naf4.'#14, .s : ' r�!A!�' :' 4 4k�7, �`'

��� PAR Laboratories, Inc-
221 7 Graham Park Drive
LABORATORIES,INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
REPORT OF ANALYSES
Attn: MIKE CHURCH
PHARR YARNS PROJECT NAME: FEB 05
PO BOX 1939 DATE: 02/22/05
McADENVILLE, NC 28101-
n dip
SAMPLE NUMBER- 62685 SAMPLE ID- PY DWTP POND SOIL #5 SAMPLE MATRIX- SO
DATE SAMPLED- 02/09/05 LOCATION- DWTP TIME SAMPLED- 1005
DATE RECEIVED- 02/09/05 SAMPLER- MIKE CHURCH RECEIVED BY- RE
•
TIME RECEIVED- 1245 DELIVERED BY- GREG JOHNSON TYPE SAMPLE- Grab 40':.`
Page 9 of 10 c ;
ANALYSIS A.HT
ANALYSIS METHOD DATE TIME BY RESULT UNITS NP
TCLP CHARACTERISTICS TCLP 02/16/05 SK
pH VALUE TCLP 02/16/05 SK 7.37 S.U.
CORROSIVITY TCLP 02/16/05 SK NON
REACTIVITY TCLP 02/16/05 SK NON ""';^[
FLASH POINT TCLP 02/16/05 SK < 200 degrees F
IGNITABILITY TCLP 02/16/05 SK NON ',,:-
PAINT FILTER TEST TCLP 02/16/05 SK NFL '
TCLP METALS TCLP 02/16/05 SK44
I
F :( ARSENIC TCLP .1"
02/16/05 SK < 0.5 ppm *,'
y* BARIUM TCLP 02/16/05 SK < 10 ppm "F '
CADMIUM TCLP 02/16/05 SK < 0.1 ppm -'1.'
CHROMIUM TCLP 02/16/05 SK < 0.5 ppm `"
LEAD TCLP 02/16/05 SK < 0.5 ppm -1`1
i6.
MERCURY ,,,
TCLP 02/16/05 SK < 0.02 ppm
SELENIUM TCLP 02/16/05 SK < 0.1 ppm
r SILVER +1
M TCLP 02/16/05 SK < 0.5 ppm V1
TCLP PESTICIDES TCLP 02/16/05 SK
aIy„)I
ENDRIN TCLP 02/16/05 SK < 0.002 ppm ,,t
LINDANE TCLP 02/16/05 SK < 0.04 ppm
METHOXYCHLOR TCLP 02/16/05 SK < 1 ppmTOXAPHENE TCLP 02/16/05 SK < 0.05 ppm
f
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��� PAR Laboratories, Inc.
2217 Graham Park Drive
LABORATORIES.INC. PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert#20;SC Cert#99003
www.parlabs.com
Page 10 of 10
CONTINUATION OF DATA FOR SAMPLE NUMBER 62685
t* ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
"1 CHLORDANE TCLP 02/16/05 SK < 0.003 ppm
HEPTACHLOR (AND ITS EPDXIDE) TCLP 02/16/05 SK < 0.0008 ppm
TCLP HERBICIDES TCLP 02/16/05 SK
2,4-D TCLP 02/16/05 SK < 1 ppm
°` "` 2,4, 5-TP(SILVEX) TCLP 02/16/05 SK < 0. 1 ppm
``��wl TCLP ORGANICS TCLP 02/16/05 SK
- BENZENE TCLP 02/16/05 SK < 0.05 ppm
CARBON TETRACHLORIDE TCLP 02/16/05 SK < 0.05 ppm
CHLOROBENZENE TCLP 02/16/05 SK < 10 ppm i A
„ CHLOROFORM TCLP 02/16/05 SK < 0. 6 ppm � <,
o-CRESOL TCLP 02/16/05 SK < 20 ppm
: p-CRESOL TCLP 02/16/05 SK < 20 ppm
;, m-CRESOL TCLP 02/16/05 SK < 20 ppm
'4. •. 1, 4-DICHLOROBENZENE TCLP 02/16/05 SK < 0.75 ppm :4
1,2-DICHLOROETHANE 4w
- r TCLP 02/16/05 SK < 0.05 ppm # -� ,
1, 1-DICHLOROETHYLENE TCLP 02/16/05 SK < 0.07 ppm i..a '
2, 4-DINITROTLUENE TCLP 02/16/05 SK < 0.013 ppm
•
'� +( HEXACHLOROBENZENE TCLP 02/16/05 SK < 0.013 ppm
•
HEXACHLOROBUTDIENE TCLP 02/16/05 SK < 0.05 ppm
`' HEXACHLOROETHANE TCLP 02/16/05 SK < 0.3 ppm
METHYL ETHYL KETONE TCLP 02/16/05 SK < 20 ppm
NITROBENZENE TCLP 02/16/05 SK < 0.2 ppm
PENTACHLOROPHENOL TCLP 02/16/05 SK < 10 ppm
PYRIDINE TCLP 02/16/05 SK < 0.5 ppm
TETRACHLORETHYLENE TCLP 02/16/05 SK < 0.07 ppm
TRICHLOROETHYLENE TCLP 02/16/05 SK < 0.05 ppm
2,4, 5-TRICHLOROPHENOL TCLP 02/16/05 SK < 40 ppm
2, 4, 6-TRICHLORPHENOL TCLP 02/16/05 SK < 0.2 ppm ' I
rI 4 VINYL CHLORIDE TCLP 02/16/05 SK < 0.02 ppm
LABORATORY DIRECTOR
1
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PAR CHAIN OF CUSTODY
LABORATORIES.INC. PAR Laboratories, Inc
Phone [phone]
Fax [phone].
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories,Inc. and the North
Carolina Department of Environmental and Natural Resources.
Company Name (billing) Comments/Special Instructions
PHARR YARNS
Address
PO BOX 1939 TEMP. OF SAMPLE WHEN TAKEN
City, State & Zip Code
McADENVILLE, NC 28101
Point of Contact & Telephone Number
MIKE CHURCH 824-3551 EXT. 310
Sample taken by: %,j//C< G,41
c,t t-
IS THIS FOR STATE or EPA REPORTING? YES _X_ NO
*Sample type: DW WW GWMW HW Soil Other
Sample Temp upon receipt: °C
** Preserved: Yes No v Teflon Liner/ Zero Headspace: Yes _ No — N/A /�
Client Sample I.D. Set Up Collection Analyses
(Sample Location / Number) Comp Grab Preserv. Date/Time Date/Time Requested
PliirXI tes
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Relinquished by: Date/Time Received by: Date/Time
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Relinquish d by: Date/Time Rec ved by: Date/Time
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• C Composite ab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste
" ee Other Si e