NC0005177_Regional Office Historical File Pre 2018 (6)

Water Pollution Control System Operator Designation Form itAl; 1 4 2016
1Wi
WPCSOCC RECEIVEDINCDENRIDWR
�/� NCAC 15A 8G .020I WORDS
1• Ctit-Ito / nay 0.QERESVILLE REGIONAL OFFICE
Permittee Owner/Officer Name: (� i V 151�N �/�U�. I y "�m�q t,1
Mailing Address: p.o, oX 1 /5
City: EE1✓1 v. Cl-T) State: N C Zip:Zeato - Phone#: 10j4- Q (. 3-7(01 C-)
Email address: 1 1 Y+^e -:0.1r, @ -- c . Co rn
At(1.Signature: Date: - JY{ilRLI} ?mil C
Facility Name: RAC C 1 L I.T N\v lw 111'►✓\tom r•-1 Permit#: t4C()005 l 1
County: t1•6101\..N
SUBMIT A SEPARATE FORM FOR EACH TYPE SYSTEM!
Facility Type/Grade (CHECK ONLY ONE):
Biological Collection Physical/Chemical Surface Irrigation Land Application
Operator in Responsible Charge(ORC)
Print Full Name: l NL' S , A-t 1t_-1_► Email: t bayle_y �,i. lj 1 it'5�c e r-v-
ic. c
- fit Z 4 Z. - //
Certificate Type/Grade/Number: P C.�14\4/G/WW 2130 Work Phone#: 104-(e C5=1(o3O
Signature: A. 11 Date: 3— -5' i 6
"I certify that I agree to my designation as the Operator in Responsible Charge for the facility noted. I understand and will abide by the rules
and regulations pertaining to the responsibilities of the ORC as set forth in I5A NCAC 08G.0204 and failing to do so can result in Disciplinary
Actions by the Water Pollution Control System Operators Certification Commission."
Back-Up Operator in Responsible Charge(BU ORC)
Print Full Name: Inici)Pr L G. D f JB 7 Email: /)1 ICI!h , .1)EAL/ART t F jn C. C0fi
Certificate Type/Grade/Number: PC /219 9 700 3 Work Phone#: 7o4/- 84 8' 7/97
Signature: ,C. vr/ Date: 3/3Aao
"1 certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in 15A NCAC 08G.0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Mail,fax or email the WPCSOCC, 1618 Mail Service Center, Raleigh, NC 27699-1618 Fax: [phone]
orieina/to: Email: certadmin(a,ncdenr.Qov
Mail or fax a con'to the Asheville Fayetteville Mooresville Raleigh
appropriate Regional Office: 2090 US Hwy 70 225 Green St 610 E Center Ave 3800 Barrett Dr
Swannanoa 28778 Suite 714 Suite 301 Raleigh 27609
Fax:[phone] Fayetteville 28301-5043 Mooresville 28115 Fax:[phone]
Phone:[phone] Fax:[phone] Fax:[phone] Phone:[phone]
Phone:[phone] Phone: [phone]
Washington Wilmington Winston-Salem
943 Washington Sq Mall 127 Cardinal Dr 450 W. Hanes Mall Rd
Washington 27889 Wilmington 28405-2845 Winston-Salem 27105
Fax:[phone] Fax:[phone] Fax:[phone]
Phone:[phone] Phone:[phone] Phone:[phone]
Revised 05-2015

WPCSOCC Operator Designation Form, cont.
Facility Name: F '• I4C- L.eTt}Lk)m. btV6StEDr.l Permit#: NC, 000 5l11
Back-Up Operator in Responsible Charge(BU ORC)
Print Full Name: &IbCK J b '4 Dis&I N Email: Pkt-Ctiesaitypti.1 Fim 04
Certificate Type/ ill de/Nu ber:f) II 9101 5-7s Work Phone#: Z 0"1"1b _59 i(j
Signature: "'� ) f
, Date: 3-3" .011o
"I certify that I agree to my desi• io, as a Back-up perator in Responsible Charge for the facility noted.I understand and will abide by the
rules and regulations pertaining I, he esponsibilitie f the BU ORC as set forth in 15A NCAC 08G.0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Back-Up Operator in Responsible Charge(BU ORC)
Print Full Name:l.iE5Jy)tie4J Mfiniki,0/..) Email: Le�Gs. rndr web 4)44,.dew.
Certificate Type/ rade/N mber:� Work Phone#: 70 8— . s -55-b 7
71
Signature: < Date: .3/3/2-0 i
"I certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in ISA NCAC 08G.0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Back-Up Operator in Responsible Charge(BU ORC)
Print Full Name: h tckA t 1 l,,JA yid f a l'eui1JS Email:M(Chh ^�el. D it,/IJVS .7 Fitt < <Dill
Certificate Type/Grade/Number: pc. i- / F 9 S f Work Phone#: ?0q- 1'6 2-PO
Signature: W Mow Z54,-_y Date: 3. 3• 2016'
"I certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in ISA NCAC 08G.0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Back-Up Operator in Responsible Charge(BU ORC)
Print Full Name: Email:
Certificate Type/Grade/Number: Work Phone#:
Signature: Date:
"I certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted.I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in ISA NCAC 08G.0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Revised 05-2015

•
A •A //A70
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director
Secretary
•
January 7, 2011
Mr. Rodney Willis.
Environmental Engineer, Site ORC
FMC Lithium Division
P. O. Box 795
Bessemer City,NC 28016
Subject Issuance of Renewal NPDES Permit
. NPDES Permit NC0005177
Gaston County
Class I
Dear Mr. Willis:
Division personnel have reviewed and approved your application for renewal of the subject permit.
Accordingly, we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North
Carolina and the U.S.Environmental Protection Agency dated October 15, 2007 (or as subsequently amended).
Summary of Changes in Renewal Permit from Existing Permit
1) Outfall 001: Total Suspended Solids Limits were converted to concentration-based limits and reduced.
2) Outfall 001. Total Chloride monitoring was reduced to quarterly.
3) Outfall 001:-Magnesium and Ammonia as nitrogen monitoring were removed.
4) Outfall 001:Special condition narrative for toxicity test was updated
5) Outfall 004: Total Chloride monitoring was reduced to quarterly.
6) Outfall 004: Methyl chloride and ethylbenzene monitoring were removed
7) Outfall 004 Recitepriarmt narrative was removed.
8) Section B: Stormwater Discharge Narrative was updated.
9) Section B: Toluene monitoring with benchmark was added as pollutant of interest.
10)Stormwater Annual Report form was added.
11)Technical correction for Receiving Stream was made. Correct Receiving Stream is "Unnamed tributary
to First Creek".
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days
Page 1 of 2
1617 Mail Service Center,Raleigh,North Carolina 27699-1617
Location:512 N.Salisbury St.Raleigh,North Carolina 27604 One
Phone:[phone] FAX:[phone] Customer Service:1-877-623-6748 .NorthCarolina
Internet:www.nnity\Affirmative
rg
Action
1��ur����
An Equal Opportunity 1 Affirmative Action Employer j

a. 4
following receipt of this letter. This request must be in the form of a written petition, conforming to Chapter
150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings (6714 Mail
Service Center, Raleigh, North Carolina 27699-6714). Unless such demand is made, this decision shall be final
and binding.
Please note that this permit is not transferable except after notice to the Division. The Division may
require modification or revocation and reissuance of the permit. This permit does not affect the legal
requirements to obtain other permits which may be required by the Division of Water Quality or permits
required by the Division of Land Resources, the Coastal Area Management Act or any other federal or local
governmental permits that may be required.
If you have any questions concerning this permit,please contact Ron Berry at telephone number(919)
807-6396 or at email [e-mail].
Sincerely,
y\.
tyr-i' Coleen H. Sullins
Attachments
Cc: Mooresville Regional Office/Surface Water Protection Section/
EPA Region IV/Pamala Meyer(email)
Stormwater/Robert Patterson(email)
Environmental Sciences Section/Aquatic Toxicology Unit/Susan Meadows (email)
Central Files
NPDES Unit
Page 2 of 2
•

► Permit NC0005177
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission,and the Federal Water Pollution Control Act,as amended,
FMC Corporation
is hereby authorized to discharge wastewater and stormwater from a facility located at the
FMC Lithium Division
NC Highway 161 west of Bessemer City
Gaston County
to receiving waters designated as an unnamed tributary to First Creek in the Catawba River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I,
II III, and IV hereof.
The permit shall become effective February 1, 2011.
This permit and the authorization to discharge shall expire at midnight on August 31, 2015.
Signed this day January 7, 2011.
Coleen H. Sullins,Director
Division of Water Quality
By Authority of the Environmental Management Commission

Permit NC0005177
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby
revoked, and as of this issuance, any previously issued permit bearing this number is no longer effective.
Therefore, the exclusive authority to operate and discharge from this facility arises under the permit
conditions, requirements, terms, and provisions included herein.
FMC Corporation
is hereby authorized to:
1. Continue operation of an existing 0.615 MGD wastewater treatment facility consisting of:
• reverse osmosis filtration systems,
• hydrogen peroxide addition,
• pH adjustment systems,
• R&D pond,
• lower retention pond, and
• effluent flow weir.
Facility is located at FMC's Lithium Division off NC Highway 161 west of Bessemer
City in Gaston County.
2. Continue operation of a stormwater conveyance system and two ponds, the first for one
sedimentation and the second for polishing; and
3. Discharge treated wastewater and stormwater (Outfall 001), and stormwater, boiler
blowdown, and cooling water (Outfall 004) at the locations specified on the attached
map. The receiving stream for Outfall 001 & Outfall 004 is an unnamed tributary to First
Creek, a class C water in the Catawba River Basin.

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USGS Quad: F13SE Bessemer City, NC
Latitude Longitude
Facility: 35 16' 45.8„N 81 18 31.3 W
Outfall 001: 35° 15' 43.6"N 81° 17' 54.9" W
Outfall 004: 35° 15' 42.8"N 81° 17' 57.3" W North Facility Location
Stream Class: C ,
Subbasin: 03-08-37 HUC: 03050101 FMC-Lithium Division NC0005177
Receiving Stream: UT to First Creek Gaston County

Part I, Section A Permit NC0005177. ,
SECTION A: WASTEWATER DISCHARGES
A. (1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - OUTFALL 001
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to
discharge treated industrial wastewater and stormwater from Outfall. 001. Such discharges shall be
limited and monitored by the Permittee as specified below:
EFFLUENT LIMITS MONITORING REQUIREMENTS
CHARACTERISTICS Monthly Daily Measurement Sample Sample
Average Maximum Frequency Type -Location
Flow 0.615 MGD Continuous Recording Influent or
(50050) Effluent
BOD, 5-day,20°C 30.0 mg/I 45.0 mg/1 Monthly Grab Effluent
(C0310)
Total Suspended Solids (TSS) 30.0 mg/1 45.0 mg/1 2/Month Grab Effluent
(00530)
Dissolved Oxygen(DO) Not less than 5.0 mg/1, Weekly Grab Effluent
(00300) daily average
pH Not less than 6.0 S.U. nor Weekly Grab Effluent
(00400) greater than 9.0 S.U.
Conductivity, µmobs/cm Monthly Grab Effluent
(00094)
Total Chloride, mg/1 Quarterly Grab Effluent
(00940)
Total Nitrogen(TN), mg/1
TN=(NO2-N +NO3-N) +TKN Quarterly Grab Effluent
(C0600)
Total Phosphorus(TP),mg/1
(C0665) Quarterly Grab Effluent
Chronic Toxicity 2
(TGP3B, THP3B) Quarterly Grab Effluent
Footnote:
1. Values shall be measured and reported to minimum detection limit of 5 µg/l.
2. Chronic Toxicity (Ceriodaphnia) @ 78%, January, April, July, October; see section A.
(3)of this permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.
Part 1, Section A
Page 1 of 4

'Part I, Section A Permit NC0005177
A. (2.)EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - OUTFALL 004
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to
discharge stormwater, boiler blowdown, steam condensate and non-contact cooling water from Outfall
004. Such discharges shall be limited and monitored by the Permittee as specified below:
EFFLUENT LIMITS MONITORING REQUIREMENTS
CHARACTERISTICS Monthly Daily Measurement Sample Sample
Average Maximum Frequency Type Location
Flow(MGD) ' - - Monthly Instantaneous Effluent
(50050)
Total Suspended Solids,
mg/1 (TSS) Monthly Grab Effluent
(00530)
pH Not less than 6.0 S.U. Monthly Grab Effluent
(00400) nor greater than 9.0 S.U.
Conductivity, µmohs/cm Monthly Grab Effluent •
(00094)
Total Chloride,mg/1 Quarterly Grab Effluent
(00940)
Footnote:
1. Where no measurable discharge occurs, "no discharge" shall be clearly noted on the submitted
monthly discharge monitoring report(DMR).
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.
There shall be no chromium, zinc or copper added to the treatment system except as pre-approved
additives to biocidal compounds.
The permittee shall obtain approval from the Division's Aquatic Toxicology Unit prior to the use of any
biocide (not previously approved by the Division) in the effluent discharged under this permit.
Approval for use of any biocide not previously approved should be requested at least 90 days in advance
of any planned usage.
Contact the Aquatic Toxicology Unit for detailed instructions on requesting approval of biocides:
NC DENR/DWQ/Aquatic Toxicology Unit
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
SEE PART I,SECTION B FOR ADDITIONAL STORMWATER REQUIREMENTS.
•
Part 1, Section A
Page 2 of 4

Part I, Section A Permit NC0005177
A. (3.) CHRONIC TOXICITY PERMIT LIMIT (Quarterly)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant
mortality to Ceriodaphnia dubia at an effluent concentration of 78%.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in
the "North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or
subsequent versions or "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure"
(Revised-February 1998) or subsequent versions. The tests will be performed during the months of
January, April, July, and October. Effluent sampling for this testing shall be performed at the NPDES
permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the
permit limit, then multiple-concentration testing shall be performed at a minimum, in each of the two
following months as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test
Procedure" (Revised-February 1998) or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the
highest concentration having no detectable impairment of reproduction or survival and the lowest
concentration that does have a detectable impairment of reproduction or survival. The definition of
"detectable impairment," collection methods, exposure regimes, and further statistical methods are
specified in the "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised-
February 1998)or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent
Discharge Monitoring Form (MR-1) for the months in which tests were performed, using the parameter
code TGP3B for the pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3
(original) is to be sent to the'following address:
Attention: NC DENR/DWQ/Environmental Sciences Section
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Section no later
than 30 days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate
signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if
chlorine is employed for disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is
required, the permittee will complete the information located at the top of the aquatic toxicity (AT) test
form indicating the facility name, permit number, pipe number, county, and the month/year of the report
with the notation of"No Flow" in the comment area of the form. The report shall be submitted to the
Environmental Sciences Section at the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required,monitoring
will be required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division
of Water Quality indicate potential impacts to the receiving stream, this permit may be re-opened and
modified to include alternate monitoring requirements or limits.
Part 1, Section A
Page 3 of 4

Part I, Section A Permit NC0005 177
If the Permittee monitors any pollutant more frequently then required by this permit, the results of such
monitoring shall be included in the calculation and reported data submitted on the DMR and all AT
Forms.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control
organism survival, minimum control organism reproduction, and appropriate environmental controls,
shall constitute an invalid test and will require immediate follow-up testing to be completed no later than
the last day of the month following the month of the initial monitoring.
Part 1, Section A
Page 4 of 4

Part I, Section B Permit NC0005 177
•
SECTION B: STORMWATER DISCHARGES
B. (1.)FINAL LIMITATIONS AND CONTROLS
During the period beginning on the effective date of the permit and lasting until expiration,the permittee
is authorized to discharge stormwater from Outfall 004. Such discharges shall be controlled, limited and
monitored as specified below:
STORMWATER POLLUTION PREVENTION PLAN
The permittee shall develop and continue to update a Stormwater Pollution Prevention Plan (SPPP),
herein after referred to as the Plan. The Plan shall be considered public information and shall include, at
a minimum,the following items:
1. Site Plan. The site plan shall provide a description of the physical facility and the potential
pollutant sources which may be expected to contribute to contamination of stormwater
discharges. The site plan shall contain the following:
(a) A general location map (USGS quadrangle map or appropriately drafted equivalent map),
showing the facility's location in relation to transportation routes and surface waters, the
name of the receiving water(s) to which the stormwater outfall(s) discharges, or if the
discharge is to a municipal separate storm sewer system, the name of the municipality
and the ultimate receiving waters, and accurate latitude and longitude of the point(s) of
discharge. The general location map (or alternatively the site map) shall identify whether
each receiving water is impaired (on the state's 303(d) list of impaired waters) or is
located in a watershed for which a TMDL has been established, and what the
parameter(s) of concern are.
(b) A narrative description of storage practices, loading and unloading activities, outdoor
process areas, dust or particulate generating or control processes, and waste disposal
practices. A narrative description of the potential pollutants which could be expected to
be present in the stormwater discharge from each outfall.
(c) A site map drawn to scale (including a distance legend) showing: the site property
boundary, the stormwater discharge outfalls, all on-site and adjacent surface waters and
wetlands, industrial activity areas (including storage of materials, disposal areas, process
areas, loading and unloading areas, and haul roads), site topography, all drainage features
and structures, drainage areas for each outfall, direction of flow in each drainage area,
industrial activities occurring in each drainage area, buildings, existing BMPs, and
impervious surfaces. The site map must indicate the percentage of each drainage area
that is impervious.
(d) A list of significant spills or leaks of pollutants that have occurred at the facility during
the three (3)previous years and any corrective actions taken to mitigate spill impacts.
(e) Certification that the stormwater outfalls have been evaluated for the presence of non-
stormwater discharges. The certification statement will be signed in accordance with the
requirements found in Part II, Standard Conditions, Section B, Paragraph 11. The
•
Part 1, Section B
Page 1 of 12 '

Part I, Section B Permit NC0005177
permittee shall re-certify annually that the stormwater outfalls have been evaluated for
the presence of non-stormwater discharges.
2. Stormwater Management Plan. The stormwater management plan shall contain a narrative
description of the materials management practices employed which control or minimize the
exposure of significant materials to stormwater, including structural and nonstructural measures.
The stormwater management plan, at a minimum, shall incorporate the following:
(a) Feasibility Study. A review of the technical and economic feasibility of changing the
methods of operations and/or storage practices to eliminate or reduce exposure of
materials and processes to stormwater. Wherever practical, the permittee shall prevent
exposure of all storage areas, material handling operations, and manufacturing or fueling
operations. In areas where elimination of exposure is not practical, the stormwater
management plan shall document the feasibility of diverting the stormwater runoff away
from areas of potential contamination.
(b) Secondary Containment Requirements and Records. Secondary containment is required
for: bulk storage of liquid materials; storage in any amount of Section 313 of Title III of
the Superfund Amendments and Reauthorization Act (SARA) water priority chemicals;
and storage in any amount of hazardous substance in order to prevent leaks and spills
from contaminating stormwater runoff. A table or summary of all such tanks and stored
materials and their associated secondary containment areas shall be maintained. If the
secondary containment devices are connected to stormwater conveyance systems, the
connection shall be controlled by manually activated valves or other similar devices
(which shall be secured closed with a locking mechanism), and any stormwater that
accumulates in the containment area shall be at a minimum visually observed for color,
foam, outfall staining, visible sheens and dry weather flow, prior to release of the
accumulated stormwater. Accumulated stormwater shall be released if found to be
uncontaminated by any material. Records documenting the individual making the
observation, the description of the accumulated stormwater, and the date and time of the
release shall be kept for a period of five years.
(c) BMP Summary. A listing of site structural and non-structural Best Management
Practices (BMP) shall be provided. The installation and implementation of BMPs shall
be based on the assessment of the potential for sources to contribute significant quantities
of pollutants to stormwater discharges and data collected through monitoring of
stormwater discharges. The BMP Summary shall include a written record of the specific
rationale for installation and implementation of the selected site BMPs. The BMP
Summary shall be reviewed and updated annually.
3. Spill Prevention and Response Plan. The Spill Prevention and Response Plan (SPRP) shall
incorporate an assessment of potential pollutant sources based on a materials inventory of the
facility. Facility personnel (or the team) responsible for implementing the SPRP shall be
identified in a written list incorporated into the SPRP and signed and dated by each individual
acknowledging their responsibilities for the plan. A responsible person shall be on-site at all
times during facility operations that have the potential to contaminate stormwater runoff through
spills or exposure of materials associated with the facility operations. The SPRP must be site
stormwater specific. Therefore, an oil Spill Prevention Control and Countermeasure plan
• (SPCC) may be a component of the SPRP, but may not be sufficient to completely address the
Part 1, Section B
Page 2of12

Part I, Section B Permit NC0005 177 ,
stormwater aspects of the SPRP. The common elements of the SPCC with the SPRP may be
incorporated by reference into the SPRP.
4. Preventative Maintenance and Good Housekeeping Program. A preventative maintenance and
good housekeeping program shall be developed. The program shall list all stormwater control
systems, stormwater discharge outfalls, all on-site and adjacent surface waters and wetlands,
industrial activity areas (including material storage areas, material handling areas, disposal areas,
process areas, loading and unloading areas, and haul roads), all drainage features and structures,
and existing structural BMPs. The program shall establish schedules of inspections,
maintenance, and housekeeping activities of stormwater control systems, as well as facility
equipment, facility areas, and facility systems that present a potential for stormwater exposure or
stormwater pollution. Inspection of material handling areas and regular cleaning schedules of
these areas shall be incorporated into the program. Timely compliance with the established
schedules for inspections, maintenance, and housekeeping shall be recorded in writing and
maintained in the SPPP.
5. Employee Training. Training programs shall be developed and training provided at a minimum
on an annual basis for facility personnel with responsibilities for: spill response and cleanup,
preventative maintenance activities, and for any of the facility's operations that have the potential
'to contaminate stormwater runoff. Facility personnel (or team) responsible for implementing the
training shall be identified, and their annual training shall be documented by the signature of
each employee trained.
6. Responsible Party. The Stormwater Pollution Prevention Plan shall identify a specific
position(s) responsible for the overall coordination, development, implementation, and revision
to the Plan. Responsibilities for all components of the Plan shall be documented and position
assignments provided.
7. Plan Amendment. The permittee shall amend the Plan whenever there is a change in design,
construction, operation, or maintenance which has a significant effect on the potential for the
discharge of pollutants to surface waters. All aspects of the Stormwater Pollution Prevention
Plan shall be reviewed and updated on an annual basis. The annual update shall include an
updated list of significant spills or leaks of pollutants for the previous three years, or the notation
that no spills have occurred. The annual update shall include written re-certification that the
stormwater outfalls have been evaluated for the presence of non-stormwater discharges. Each
annual update shall include a documented re-evaluation of the effectiveness of the BMPs listed
in the BMP Summary of the Stormwater Management Plan.
The Director may notify the permittee when the Plan does not meet one or more of the minimum
requirements of the permit. Within 30 days of such notice, the permittee shall submit a time
schedule to the Director for modifying the Plan to meet minimum requirements. The permittee
shall provide certification in writing(in accordance with Part II, Standard Conditions, Section B,
Paragraph 11)to the Director that the changes have been made.
8. Facility Inspections. Inspections of the facility and all stormwater systems shall occur as part of
the Preventative Maintenance and Good Housekeeping Program at a minimum on a semi-annual
schedule,once during the first half of the year(January to June), and once during the second half
(July to December), with at least 60 days separating inspection dates (unless performed more
Part 1, Section B
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Part I, Section B Permit NC0005177
frequently than semi-annually). These facility inspections are different from, and in addition to,
the stormwater discharge characteristic monitoring required in Part 1, Section B. (2.).
9. Implementation. The permittee shall implement the Plan. Implementation of the Plan shall
include documentation of all monitoring, measurements, inspections, maintenance activities, and
training provided to employees, including the log of the sampling data and of actions taken to
implement BMPs associated with the industrial activities, including vehicle maintenance
activities. Such documentation shall be kept on-site for a period of five years and made available
to the Director or the Director's authorized representative immediately upon request.
B. (2.)MINIMUM MONITORING AND REPORTING REQUIREMENTS
1. Analytical monitoring of stormwater discharges shall be performed as specified in Table 1. All
samples shall be collected from a discharge resulting from a representative storm event. The
required monitoring will result in a minimum of ten analytical samplings being conducted over
the term of the permit at each stormwater discharge outfall (SDO).
A representative storm event is a storm event that measures greater than 0.1 inches of rainfall.
The time between this storm event and the previous storm event measuring greater than 0.1
inches must be at least 72 hours. A single storm event may have a period of no precipitation of
up to 10 hours. For example, if it rains but stops before producing any collectable discharge, a
sample may be collected if the next rain producing a discharge begins within 10 hours.
2. If the stormwater is controlled by a detention pond, and that pond discharges only in response to
a storm event exceeding a 25-year, 24-hour storm, the pond shall be considered a non-
discharging stormwater control system and not subject to NPDES requirements, unless the
discharge causes a violation of water quality standards.
3. Stormwater samples analyzed in accordance with the terms of this permit shall be submitted on
forms provided by the Director no later than March 1 following the year in which sampling was
required to the DWQ Central Office. Stormwater samples analyzed in accordance with the terms
of this permit shall be submitted to the Division on Discharge Monitoring Report forms provided
by the Director. The permittee shall also submit an Annual Summary Data Monitoring Report to
the appropriate DWQ Regional Office (RO) by March 1 of each year. The submittal shall be on
forms supplied by the Division. Addresses for each RO can be found here:
http://portal.ncdenr.org/web/wq/home/ro/
4. Specific monitoring requirements:
(a) Stormwater from FMC Lithium—Bessemer City. Monitoring in Table 1 applies to all of the
stormwater discharges associated with industrial activity that discharge to the surface waters
of the state.
Table 1: Analytical Stormwater Monitoring Requirements
Discharge Measurement Sample Sample
Characteristics Units Frequency 1 Type 2 Location 3
Total Suspended Solids (TSS) mg/1 semi-annual Grab SDO
Biochemical Oxygen Demand
(BOD), 5-day,20°C mg/1 semi-annual Grab SDO
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Part I, Section B Permit NC0005177
Total Petroleum Hydrocarbons
(TPH), EPA Method 1664A mg/I semi-annual Grab SDO
(SGT-HEM)
Total Nitrogen(TN)4 mg/1 semi-annual Grab SDO
Total Phosphorus (TP)4 mg/1 semi-annual Grab SDO
Toluene 4 mg/1 semi-annual Grab SDO
pH S.U. semi-annual Grab SDO
Total Rainfall 5 inches semi-annual Rain Gauge -
Footnotes:
1. Measurement Frequency: Twice per year during a representative storm event.
2. Grab samples shall be collected within the first 30 minutes of discharge.
3. Sample Location: Samples shall be collected at each stormwater discharge
outfall(SDO)unless representative outfall status has been granted.
4. The permittee may discontinue monitoring for TN, TP, and Toluene after four
(4) consecutive samples if all values are below the benchmarks in Table 4.
5. For each sampled representative storm event the total precipitation must be
recorded. An on-site rain gauge or local rain gauge reading must be recorded.
The permittee shall complete the minimum 11 analytical samplings in accordance with the
schedule specified below in Table 2. A minimum of 60 days must separate Period 1 and
Period 2 sample dates unless monthly monitoring has been instituted under a Tier Two
response.
Table 2: Monitoring Schedule
Monitoring period Sample
Number Start End
Year 1 —Period 1 1 January 1, 2011 June 30, 2011
Year 1 —Period 2 2 July 1,2011 December 31, 2011
Year 2—Period 1 3 January 1, 2012 June 30, 2012
Year 2—Period 2 4 July 1,2012 December 31, 2012
Year 3 —Period 1 5 January 1, 2013 June 30, 2013
Year 3 —Period 2 6 July 1,2013 December 31, 2013
Year 4—Period 1 7 January 1, 2014 June 30, 2014
Year 4—Period 2 8 July 1, 2014 December 31, 2014
Year 5 —Period 1 9 January 1, 2015 June 30, 2015
During Renewal 10 July 1, 2015 December 31, 2015
Process 2 11+ January 1, 2016 June 30. 2016
Footnotes:
1. If no discharge occurs during the sampling period, the permittee must record
"No Flow" on a monitoring report within 30 days of the end of the sampling
period and maintain this record in the SPPP.
2. Maintain semi-annual monitoring during permit renewal process. If at the
expiration of this permit, the permittee has submitted an application for
renewal of coverage before the submittal deadline, the permittee will be
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Page 5 of 12 •

Part I, Section B Permit NC0005177
considered for renewed coverage. The applicant must continue semi-annual
monitoring until the renewed permit is issued.
(b) Facilities which have any vehicle maintenance activity occurring on-site which uses more
than 55 gallons of new motor oil per month when averaged over the calendar year shall
perform analytical monitoring as specified below in Table 3. This monitoring shall be
performed at all stormwater discharge outfalls which discharge stormwater runoff from
vehicle maintenance areas, in accordance with the schedule presented in Table 2. All
analytical monitoring shall be performed during a representative storm event.
Table 3: Analytical Monitoring Requirements for On-Site Vehicle Maintenance
Dischar a Characteristics Units Measurement Sample Sample
g Frequency Type 2 Location 3
pH S.U. semi-annual Grab SDO
Total Petroleum Hydrocarbons
(TPH), EPA Method 1664A mg/1 semi-annual Grab SDO
(SGT-HEM)
Total Suspended Solids (TSS) mg/I semi-annual Grab SDO
Total Rainfall 4 inches semi-annual Rain Gauge New Motor Oil Usage gallons/month semi-annual Estimate -
Footnotes:
1. Measurement Frequency: Twice per year during a representative storm event,
for each year until either another permit is issued for this facility or until this
permit is revoked or rescinded. If at the end of this permitting cycle the
permittee has submitted the appropriate paperwork for a renewal permit before
the submittal deadline, the permittee will be considered for a renewal
application. The applicant must continue semi-annual monitoring until the
renewed permit is issued. See Table 2 for schedule of monitoring periods
through the end of this permitting cycle.
2. If the stormwater runoff is controlled by a stormwater detention pond a grab
sample of the discharge from the pond shall be collected within the first 30
minutes of discharge from the pond.
3. Sample Location: Samples shall be collected at each stormwater discharge
outfall (SDO) that discharges stormwater runoff from area(s) where vehicle
maintenance activities occur.
4. For each sampled representative storm event the total precipitation must be
recorded. An on-site or local rain gauge reading must be recorded.
Monitoring results shall be compared to the benchmark values in Table 4. The benchmark
values in Table 4 are not permit limits but should be used as guidelines for the permittee's
SPPP. Exceedances of benchmark values require the permittee to increase monitoring,
increase management actions, increase record keeping, and/or install stormwater Best
Management Practices(BMPs), as provided in 3. below.
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Part I, Section B Permit NC0005177 ' •
5. The permittee shall report the analytical results from each sample within the monitoring period.
The permittee shall compare monitoring results to the benchmark values in Table 4. The
benchmark values in Table 4 are not permit limits but should be used as guidelines for the
permittee's Stormwater Pollution Prevention Plan (SPPP). Exceedances of benchmark values
require the permittee to increase monitoring, increase management actions, increase record
keeping, and/or install stormwater Best Management Practices (BMPs) in a tiered program. See
the descriptions of Tier One and Tier Two.
Table 4: Benchmark Values for Analytical Monitoring
Discharge Characteristics Units Benchmark
Total Suspended Solids (TSS) mg/1 100.0
Biochemical Oxygen Demand g/
(BOD), 5-day, 20°C m 1 30.0
Total Petroleum Hydrocarbons
(TPH),EPA Method 1664A(SGT- mg/1 15.0
uFX/fl
Total Nitrogen(TN) mg/1 30.0
Total Phosphorus(TP) mg/1 2.0
Toluene mg/1 0.055
pH S.U. 6.0—9.0
Tier One
If: The first valid sampling results are above a benchmark value,or outside of the benchmark
range, for any parameter at any outfall;
Then: The permittee shall:
1. Conduct a stormwater management inspection of the facility within two weeks of receiving
sampling results.
2. Identify and evaluate possible causes of the benchmark value exceedance.
3. Identify potential and select the specific: source controls,operational controls,or physical
improvements to reduce concentrations of the parameters of concern, or to bring
concentrations within the benchmark range.
4. Implement the selected actions within two months of the inspection.
5. Record each instance of a Tier One response in the Stormwater Pollution Prevention Plan.
Include the date and value of the benchmark exceedance,the inspection date,the personnel
conducting the inspection,the selected actions, and the date the selected actions were
implemented.
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Part I, Section B Permit NC0005177
Tier Two
If: During the term of this permit,the first valid sampling results from two consecutive monitoring
periods are above the benchmark values, or outside of the benchmark range, for any specific
parameter at a specific discharge outfall;
Then: The permittee shall:
1. Repeat all the required actions outlined above in Tier One.
2. Immediately institute monthly monitoring for all parameters at every outfall where a
sampling result exceeded the benchmark value for two consecutive samples. Monthly
(analytical and qualitative)monitoring shall continue until three consecutive sample results
are below the benchmark values or within the benchmark range.
3. If no discharge occurs during the sampling period,the permittee is required to record "No
Flow on a monthly monitoring report to comply with reporting requirements.
4. Maintain a record of the Tier Two response in the Stormwater Pollution Prevention Plan.
During the term of this permit, if the valid sampling results required for the permit monitoring
periods exceed the benchmark value, or are outside the benchmark range, for any specific parameter
at any specific outfall on four occasions, the permittee shall notify the DWQ Regional Office
Supervisor in writing within 30 days of receipt of the fourth analytical results. DWQ may but is
not limited to:
• require that the permittee revise, increase, or decrease the monitoring frequency for the
remainder of the permit;
• require the permittee to install structural stormwater controls;
• require the permittee to implement other stormwater control measures; or
• require that the permittee implement site modifications to qualify for the No Exposure
Exclusion.
6. If a facility is required to sample multiple stormwater discharge locations, the permittee may
petition the Director to sample at a reduced number of outfalls. These outfalls would be granted
"Representative Outfall Status" (ROS). DWQ may grant Representative Outfall Status if
discharges from a single outfall are representative of discharges from multiple outfalls.
Approved ROS will reduce the number of outfalls where analytical sampling requirements apply.
Qualitative observations shall be recorded for all outfall locations.
7. This site discharges to impaired waters experiencing problems with biological integrity (North
Second Creek) and excessive nutrient loading (High Rock Lake watershed). If a Total
Maximum Daily Load (TMDL) is approved for this segment of North Second Creek or High
Rock Lake,the permittee may be required to monitor for the pollutant(s)of concern in the future
and submit results to the Division of Water Quality. The Division will consider the monitoring
results in determining whether additional BMPs are needed to control the pollutant(s) of concern
to the maximum extent practicable.
If additional BMPs are needed to achieve the required level of control, the permittee will be
required to (1) develop a strategy for implementing appropriate BMPs, and (2) submit a
timetable for incorporation of those BMPs into the permitted Stormwater Pollution Prevention
Plan.
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Part I, Section B Permit NC0005 177
8. Qualitative monitoring requires a visual inspection of each stormwater outfall regardless of
representative outfall status and shall be performed as specified in Table 5, during the analytical
monitoring event. [If analytical monitoring is not required, the permittee still must conduct semi-
annual qualitative monitoring.] Qualitative monitoring is for the purpose of evaluating the
effectiveness of the Stormwater Pollution Prevention Plan (SPPP) and assessing new sources of
stormwater pollution.
9.
Table 5: Qualitative Stormwater Monitoring Requirements
Discharge Characteristics Frequency ' Monitoring Location 2
Color semi-annual SDO
Odor semi-annual SDO
Clarity semi-annual SDO
Floating Solids semi-annual SDO
Suspended Solids semi-annual SDO
Foam semi-annual SDO
Oil Sheen semi-annual SDO
Erosion or deposition at the outfall semi-annual SDO
Other obvious indicators of semi-annual SDO
stormwater pollution
Footnotes:
1. Measurement Frequency: Twice per year during a representative storm event, for
each year until either another permit is issued for this facility or until this permit is
revoked or rescinded. If at the end of this permitting cycle the permittee has
submitted the appropriate paperwork for a renewal permit before the submittal
deadline, the permittee will be considered for a renewal application. The applicant
must continue semi-annual monitoring until the renewed permit is issued. See
Table 2 for schedule of monitoring periods through the end of this permitting cycle.
2. Monitoring Location: Qualitative monitoring shall be performed at each
stormwater discharge outfall (SDO)regardless of representative outfall status.
In the event an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the
discovery. This documentation will be maintained with the SPPP.
10. The permittee shall record the required qualitative monitoring observations on the SDO
Qualitative Monitoring Report form provided by the Division, and shall retain the completed
forms on site. Visual monitoring results should not be submitted to the Division, except upon
DWQ's specific requirement to do so.
•
Part 1, Section B
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Part I, Section B Permit NC0005177
11. RECORDS RETENTION
Along with the Stormwater Pollution Prevention Plan, qualitative monitoring shall be
documented and records maintained at the facility. Copies of analytical monitoring results shall
also be maintained on-site. The permittee shall retain records of all monitoring information,
including all calibration and maintenance records and all original strip chart recordings for
continuous monitoring instrumentation, and copies of all reports required by this individual
permit for a period of at least 5 years from the date of the sample, measurement, report or
application. This period may be extended by request of the Director at any time.
12. BYPASSING OF STORMWATER CONTROL FACILITIES
Bypass is prohibited, and the Director may take enforcement action against a permittee for
bypass unless:
a. The bypass was unavoidable to prevent loss of life, personal injury or severe property
damage; and
b. There were no feasible alternatives to the bypass, such as the use of auxiliary control
facilities, retention of stormwater or maintenance during normal periods of equipment
downtime or dry weather. This condition'is not satisfied if adequate backup controls should '
have been installed in the exercise of reasonable engineering judgment to prevent a bypass
which occurred during normal periods of equipment downtime or preventive maintenance;
and
c. The permittee submitted notices as required under,Part III, Section C of this permit.
If the Director determines that it will meet the three conditions listed above, the Director may
approve an anticipated bypass after considering its adverse effects.
13. STORMWATER DEFINITIONS
1. Best Management Practices (BMPs)
Measures or practices used to reduce the amount of pollution entering surface waters. BMPs
may take the form of a process, activity, or physical structure. More information on BMPs can be
found at: http://cfpub.epa.gov/npdes/stormwater/menuofbmps/index.cfm.
2. Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above
ground storage container having a capacity of greater than 660 gallons or with multiple above
ground storage containers having a total storage capacity of greater than 1,320 gallons.
3. Municipal Separate Storm Sewer System (MS4)
A stormwater collection system within an incorporated area of local self-government such as a
city or town.
4. No Exposure
A condition of no exposure means that all industrial materials and activities are protected by a
storm resistant shelter or acceptable storage containers to prevent exposure to rain, snow,
snowmelt, or runoff. Industrial materials or activities include, but are not limited to, material
handling equipment or activities, industrial machinery, raw materials, intermediate products, by-
Part 1, Section B
• Page 10 of 12

Part I, Section B Permit NC0005177 .
products, final products, or waste products. DWQ may grant a No Exposure Exclusion from
NPDES Stormwater Permitting requirements only if a facility complies with the terms and
conditions described in 40 CFR §122.26(g)
5. Point Source Discharge
Any discernible, confined and discrete conveyance, including but specifically not limited to, any
pipe, ditch, channel, tunnel, conduit, well, discrete fissure, container, rolling stock, or
concentrated animal feeding operation from which pollutants are or may be discharged to waters
of the state.
6. Representative Outfall Status
When it is established that.-the discharge of stormwater runoff from a single .outfall is
representative of the discharges at multiple outfalls, the DWQ may grant representative outfall
status. Representative outfall status allows the permittee to perform analytical monitoring at a
reduced number of outfalls.
7. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus
sufficient freeboard to allow for the 25-year,24-hour storm event.
8. Section 313 Water Priority Chemical
A chemical or chemical category which:
(a) Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund
Amendments and Reauthorization Act (SARA) of 1986, also titled the Emergency
Planning and Community Right-to-Know Act of 1986;
(b) Is present at or above threshold levels at a facility subject to SARA title III, Section 313
reporting requirements; and
(c) That meets at least one of the following criteria:
(1) Is listed in appendix D of 40 CFR part 122 on either Table II (organic priority
pollutants), Table III (certain metals, cyanides, and phenols) or Table IV (certain
toxic pollutants and hazardous substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A) of the CWA at
40 CFR 116.4; or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
9. Significant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and
plastic pellets; finished materials such as metallic products; raw materials used in food
processing or production; hazardous substances designated under section 101(14) of CERCLA;
any chemical the facility is required to report pursuant to section 313 of Title III of SARA;
fertilizers; pesticides; and waste products such as ashes, slag and sludge that have the potential to
be released with stormwater discharges.
10. Significant Spills
Includes, but is not limited to: releases of oil or hazardous substances in excess of reportable
quantities under section 311 of the Clean Water Act (Ref: 40 CFR 110.10 and CFR 117.21) or
section 102 of CERCLA(Ref: 40 CFR 302.4).
Part 1, Section B
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Part I, Section B Permit NC0005177
11. Stormwater Associated with Industrial Activity
The discharge from any point source which is used for collecting and conveying stormwater and
which is directly related to manufacturing, processing or raw material storage areas at an
industrial site. Facilities considered to be engaged in "industrial activities" include those
activities defined in 40 CFR 122.26(b)(14). The term does not include discharges from facilities
or activities excluded from the NPDES program.
12. Stormwater Discharge Outfall (SDO)
The point of departure of stormwater from a discernible, confined, or discrete conveyance,
including but not limited to, storm sewer pipes, drainage ditches, channels, spillways, or
- .ehannelized collection areas, from which stormwater flows directly or indirectly into waters of
the State of North Carolina.
13. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following
rainfall or as a result of snowmelt.
12. Total Flow
The flow corresponding to the time period over which the sample collection occurs. The total
flow calculated based on the size of the area draining to the outfall, the amount of the built-upon
(impervious) surfaces within the drainage area, and the total amount of rainfall occurring during
the sampling period.
13. Total Maximum Daily Load (TMDL)
TMDLs are written plans for attaining and maintaining water quality standards, in all seasons,
for a specific water body and pollutant. (A list of approved TMDLs for the state of North
Carolina can be found at http://h2o.enr.state.nc.us/tmd1/).
14. Vehicle Maintenance Activity
Vehicle rehabilitation, mechanical repairs, painting, fueling, lubrication, vehicle cleaning
operations, or airport deicing operations.
15. Visible Sedimentation
Solid particulate matter, both mineral and organic,that has been or is being transported by water,
air, gravity,or ice from its site of origin which can be seen with the unaided eye.
16. 25-year,24 hour storm event
The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average,
once in 25 years.
Part 1, Section B
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NPDES Permit Standard Conditions
Page 1 of 18
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
Section A. Definitions
2/Month
Samples are collected twice per month with at least ten calendar days between sampling events. These samples
shall be representative of the wastewater discharged during the sample period.
3/Week
Samples are collected three times per week on three separate calendar days.These samples shall be representative
of the wastewater discharged during the sample period.
Act or"the Act"
The Federal Water Pollution Control Act,also known as the Clean Water Act(CWA),as amended,33 USC 1251,et.
seq.
Annual Average
The arithmetic mean of all "daily discharges"of a pollutant measured during the calendar year. In the case of fecal
coliform,the geometric mean of such discharges.
Arithmetic Mean
The summation of the individual values divided by the number of individual values.
Bypass
The known diversion of waste streams from any portion of a treatment facility including the collection system,
which is not a designed or established or operating mode for the facility.
Calendar Day
The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any
consecutive 24-hour period that reasonably represents the calendar day may be used for sampling.
Calendar Week
The period from Sunday through the following Saturday.
Calendar Quarter
One of the following distinct periods: January through March, April through June,July through September, and
October through December.
Composite Sample
A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 ml in
such a manner as to result in a total sample representative of the wastewater discharge during the sample period.
The Director may designate the most appropriate method (specific number and size of aliquots necessary,the time
interval between grab samples,etc.) on a case-by-case basis. Samples may be collected manually or automatically.
Composite samples may be obtained by the following methods:
(1) Continuous:a single,continuous sample collected over a 24-hour period proportional to the rate of flow.
(2) Constant time/variable volume: a series of grab samples collected at equal time intervals over a 24 hour
period of discharge and combined proportional to the rate of flow measured at the time of individual
sample collection,or
(3) Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period
with the time intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow recorder and
totalizer, and the preset gallon interval between sample collection fixed at no greater than 1/24 of the
expected total daily flow at the treatment system,or
(4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period
at a constant time interval. Use of this method requires prior approval by the Director. This method may
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NPDES Permit Standard Conditions
Page 2 of 18
only be used in situations where effluent flow rates vary less than 15 percent. The following restrictions
also apply:
> Influent and effluent grab samples shall be of equal size and of no less than 100 milliliters
> Influent samples shall not be collected more than once per hour.
> Permittees with wastewater treatment systems whose detention time<24 hours shall collect effluent
grab samples at intervals of no greater than 20 minutes apart during any 24-hour period.
➢ Permittees with wastewater treatment systems whose detention time exceeds 24 hours shall collect
effluent grab samples at least every six hours;there must be a minimum of four samples during a 24-
hour sampling period.
Continuous flow measurement
Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance
activities on the flow device.
Daily Discharge
The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the
calendar day for purposes of sampling. For pollutants measured in units of mass, the "daily discharge" is
calculated as the total mass of the pollutant discharged over the day. The "daily discharge" concentration
comprises the mean concentration for a 24-hour sampling period as either a composite sample concentration or the
arithmetic mean of all grab samples collected during that period. (40 CFR 122.2)
Daily Maximum
The highest"daily discharge"during the calendar month.
Daily Sampling
Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in
the permit. Sampling shall be conducted on weekdays except where holidays or other disruptions of normal
operations prevent weekday sampling. If sampling is required for all seven days of the week for any permit
parameter(s),that requirement will be so noted on the Effluent Limitations and Monitoring Page(s).
DWQ or"the Division"
The Division of Water Quality,Department of Environment and Natural Resources.
EMC
The North Carolina Environmental Management Commission
EPA
The United States Environmental Protection Agency
Facility Closure
Cessation of all activities that require coverage under this NPDES permit.Completion of facility closure will allow
this permit to be rescinded.
Geometric Mean
The Nth root of the product of the individual values where N= the number of individual values. For purposes of
calculating the geometric mean,values of"0" (or"< [detection level]")shall be considered=1.
Grab Sample
Individual samples of at least 100 ml collected over a period of time not exceeding 15 minutes.Grab samples can be
collected manually. Grab samples must be representative of the discharge (or the receiving stream, for instream
samples).
Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the CWA.
Instantaneous flow measurement
A measure of flow taken at the time of sampling,when both the sample and flow will be representative of the total
discharge.
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' NPDES Permit Standard Conditions
Page 3 of 18
Monthly Average(concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar month. In the case of
fecal coliform,the geometric mean of such discharges.
Permit Issuing Authority
The Director of the Division of Water Quality.
Quarterly Average(concentration limit)
The average of all samples taken over a calendar quarter.
Severe property damage
Substantial physical damage to property, damage to the treatment facilities which causes them to become
inoperable, or substantial and permanent loss of natural resources which can reasonably be expected to occur in
the absence of a bypass.Severe property damage excludes economic loss caused by delays in production.
Toxic Pollutant:
Any pollutant listed as toxic under Section 307(a)(1)of the CWA.
Upset
An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance
with permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance
caused by operational error, improperly designed treatment facilities, inadequate treatment facilities, lack of
preventive maintenance,or careless or improper operation.
Weekly Average(concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar week. In the case of
fecal coliform,the geometric mean of such discharges.
Section B. General Conditions
1. Duty to Comply
The Permittee must comply with all conditions of this permit. Any permit noncompliance constitutes a
violation of the CWA and is grounds for enforcement action; for permit termination, revocation and
reissuance,or modification;or denial of a permit renewal application[40 CFR 122.41].
a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the
CWA for toxic pollutants and with standards for sewage sludge use or disposal established under section
405(d) of the CWA within the time provided in the regulations that establish these standards or
prohibitions or standards for sewage sludge use or disposal,even if the permit has not yet been modified
to incorporate the requirement.
b. The CWA provides that any person who violates section[s] 301,302,306,307,308,318 or 405 of the Act,or
any permit condition or limitation implementing any such sections in a permit issued under section 402,
or any requirement imposed in a pretreatment program approved under sections 402 (a) (3) or 402 (b) (8)
of the Act, is subject to a civil penalty not to exceed $37,500 per day for each violation. [33 USC 1319 (d)
and 40 CFR 122.41 (a) (2)]
c. The CWA provides that any person who negligently violates sections 301,302,306,307,308,318,or 405 of
the Act,or any condition or limitation implementing any of such sections in a permit issued under section
402 of the Act, or any requirement imposed in a pretreatment program approved under section 402(a)(3)
or 402(b)(8) of the Act, is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment of not more than 1 year, or both. In the case of a second or subsequent conviction for a
negligent violation, a person shall be subject to criminal penalties of not more than $50,000 per day of
violation,or by imprisonment of not more than 2 years,or both. [33 USC 1319(c) (1)and 40 CFR 122.41 (a)
(2)]
d. Any person who knowingly violates such sections, or such conditions or limitations is subject to criminal
penalties of$5,000 to$50,000 per day of violation,or imprisonment for not more than 3 years, or both. In
the case of a second or subsequent conviction for a knowing violation,a person shall be subject to criminal
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penalties of not more than $100,000 per day of violation, or imprisonment of not more than 6 years, or
both. [33 USC 1319(c)(2)and 40 CFR 122.41 (a)(2)]
e. Any person who knowingly violates section 301,302,303,306,307,308,318 or 405 of the Act,or any permit
condition or limitation implementing any of such sections in a permit issued under section 402 of the Act,
and who knows at that time that he thereby places another person in imminent danger of death or serious
bodily injury,shall,upon conviction,be subject to a fine of not more than$250,000 or imprisonment of not
more than 15 years,or both. In the case of a second or subsequent conviction for a knowing endangerment
violation, a person shall be subject to a fine of not more than $500,000 or by imprisonment of not more
than 30 years, or both. An organization, as defined in section 309(c)(3)(B)(iii) of the CWA, shall, upon
conviction of violating the imminent danger provision,be subject to a fine of not more than$1,000,000 and
can be fined up to$2,000,000 for second or subsequent convictions. [40 CFR 122.41 (a)(2)]
f. Under state law,a civil penalty of not more than$25,000 per violation may be assessed against any person
who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North
Carolina General Statutes§143-215.6A]
g. Any person may be assessed an administrative penalty by the Administrator for violating section 301,302,
306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such
sections in a permit issued under section 402 of this Act. Administrative penalties for Class I violations are
not to exceed $16,000 per violation, with the maximum amount of any Class I penalty assessed not to
exceed $37,500. Penalties for Class II violations are not to exceed $16,000 per day for each day during
which the violation continues, with the maximum amount of any Class II penalty not to exceed $177,500.
[33 USC 1319(g)(2)and 40 CFR 122.41 (a)(3)]
2. Duty to Mitigate
The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in
violation of this permit with a reasonable likelihood of adversely affecting human health or the environment
[40 CFR 122.41 (d)].
3. Civil and Criminal Liability
Except as provided in permit conditions on "Bypassing" (Part II. C. 4), "Upsets" (Part II. C. 5) and "Power
Failures" (Part II. C. 7), nothing in this permit shall be construed to relieve the Permittee from any
responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309
of the Federal Act,33 USC 1319. Furthermore, the Permittee is responsible for consequential damages, such as
fish kills,even though the responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee
from any responsibilities, liabilities, or penalties to which the Permittee is or may be subject to under NCGS
143-215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Property Rights
The issuance of this permit does not convey any property rights in either real or personal property, or any
exclusive privileges,nor does it authorize any injury to private property or any invasion of personal rights,nor
any infringement of Federal,State or local laws or regulations [40 CFR 122.41 (g)].
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical structures or
facilities or the undertaking of any work in any navigable waters.
7. Severability
The provisions of this permit are severable. If any provision of this permit,or the application of any provision
of this permit to any circumstances, is held invalid, the application of such provision to other circumstances,
and the remainder of this permit,shall not be affected thereby[NCGS 150B-23].
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8. Duty to Provide Information
The Permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any information which
the Permit Issuing Authority may request to determine whether cause exists for modifying, revoking and
reissuing, or terminating this permit or to determine compliance with this permit. The Permittee shall also
furnish to the Permit Issuing Authority upon request,copies of records required by this permit [40 CFR 122.41
(h)].
9. Duty to Reapply
If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit,
the Permittee must apply for and obtain a new permit[40 CFR 122.41 (b)].
10. Expiration of Permit
The Permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date,the Permittee shall submit such information,forms,and
fees as are required by the agency authorized to issue permits no later than 180 days prior to the expiration
date. Any Permittee that has not requested renewal at least 180 days prior to expiration, or any Permittee that
does not have a permit after the expiration and has not requested renewal at least 180 days prior to expiration,
will subject the Permittee to enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et.seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and
certified [40 CFR 122.41 (k)].
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible
corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in
charge of a principal business function, or any other person who performs similar policy or decision
making functions for the corporation, or (b) the manager of one or more manufacturing, production,
or operating facilities, provided, the manager is authorized to make management decisions which
govern the operation of the regulated facility including having the explicit or implicit duty of making
major capital investment recommendations, and initiating and directing other comprehensive
measures to assure long term environmental compliance with environmental laws and regulations;
the manager can ensure that the necessary systems are established or actions taken to gather complete
and accurate information for permit application requirements;and where authority to sign documents
has been assigned or delegated to the manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,respectively;or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or
ranking elected official[40 CFR 122.22].
b. All reports required by the permit and other information requested by the Permit Issuing Authority shall
be signed by a person described in paragraph a. above or by a duly authorized representative of that
person.A person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility for the overall
operation of the regulated facility or activity,such as the position of plant manager,operator of a well
or well field, superintendent, a position of equivalent responsibility, or an individual or position
having overall responsibility for environmental matters for the company. (A duly authorized
representative may thus be either a named individual or any individual occupying a named position.);
and
(3) The written authorization is submitted to the Permit Issuing Authority[40 CFR 122.22]
c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate
because a different individual or position has responsibility for the overall operation of the facility,a new
authorization satisfying the requirements of paragraph (b) of this section must be submitted to the
Director prior to or together with any reports, information, or applications to be signed by an authorized
representative [40 CFR 122.22]
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d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the
following certification [40 CFR 122.22]. NO OTHER STATEMENTS OF CERTIFICATION WILL BE
ACCEPTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the
Permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned
changes or anticipated noncompliance does not stay any permit condition[40 CFR 122.41 (f)].
13. Permit Modification,Revocation and Reissuance,or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the
permit, revoking and reissuing the permit, or terminating the permit as allowed by the laws, rules, and
regulations contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North
Carolina Administrative Code,Subchapter 2H.0100;and North Carolina General Statute 143-215.1 et.al.
14. Annual Administering and Compliance Monitoring Fee Requirements
The Permittee must pay the annual administering and compliance monitoring fee within thirty days after
being billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 2H.0105
(b) (2)may cause this Division to initiate action to revoke the permit.
Section C. Operation and Maintenance of Pollution Controls
1. Certified Operator
Upon classification of the permitted facility by the Certification Commission, the Permittee shall employ a
certified water pollution control treatment system operator in responsible charge (ORC)of the water pollution
control treatment system. Such operator must hold a certification of the grade equivalent to or greater than the
classification assigned to the water pollution control treatment system by the Certification Commission. The
Permittee must also employ one or more certified Back-up ORCs who possess a currently valid certificate of
the type of the system. Back-up ORCs must possess a grade equal to(or no more than one grade less than)the
grade of the system[15A NCAC 8G.02011.
The ORC of each Class I facility must:
➢ Visit the facility as often as is necessary to insure proper operation of the treatment system;the
treatment facility must be visited at least weekly
➢ Comply with all other conditions of 15A NCAC 8G.0204.
The ORC of each Class II,III and IV facility must:
➢ Visit the facility as often as is necessary to insure proper operation of the treatment system;the
treatment facility must be visited at least five days per week,excluding holidays
➢ Properly manage and document daily operation and maintenance of the facility
➢ Comply with all other conditions of 15A NCAC 8G.0204.
Once the facility is classified, the Permittee shall submit a letter to the Certification Commission designating
the operator in responsible charge:
a. Within 60 calendar days prior to wastewater being introduced into a new system
b. Within 120 calendar days of:
➢ Receiving notification of a change in the classification of the system requiring the designation of a new
ORC and back-up ORC
➢ A vacancy in the position of ORC or back-up ORC.
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2. Proper Operation and Maintenance
The Permittee shall at all times provide the operation and maintenance resources necessary to operate the
existing facilities at optimum efficiency. The Permittee shall at all times properly operate and maintain all
facilities and systems of treatment and control (and related appurtenances) which are installed or used by the
Permittee to achieve compliance with the conditions of this permit. Proper operation and maintenance also
includes adequate laboratory controls and appropriate quality assurance procedures. This provision requires
the Permittee to install and operate backup or auxiliary facilities only when necessary to achieve compliance
with the conditions of the permit[40 CFR 122.41 (e)].
NOTE: Properly and officially designated operators are fully responsible for all proper operation and
maintenance of the facility, and all documentation required thereof, whether acting as a contract operator
[subcontractor]or a member of the Permittee's staff.
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a Permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this permit[40 CFR 122.41
(c)].
4. Bypassing of Treatment Facilities
a. Bypass not exceeding limitations[40 CFR 122.41 (m) (2)]
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded,
but only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject
to the provisions of Paragraphs b.and c.of this section.
b. Notice [40 CFR 122.41 (m)(3)]
(1) Anticipated bypass. If the Permittee knows in advance of the need for a bypass, it shall submit prior
notice, if possible at least ten days before the date of the bypass; including an evaluation of the
anticipated quality and effect of the bypass.
(2) Unanticipated bypass. The Permittee shall submit notice of an unanticipated bypass as required in
Part II. E. 6.(24-hour notice).
c. Prohibition of Bypass
(1) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take
enforcement action against a Permittee for bypass,unless:
(A) Bypass was unavoidable to prevent loss of life,personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment facilities,
retention of untreated wastes or maintenance during normal periods of equipment downtime.
This condition is not satisfied if adequate backup equipment should have been installed in the
exercise of reasonable engineering judgment to prevent a bypass which occurred during normal
periods of equipment downtime or preventive maintenance;and
(C) The Permittee submitted notices as required under Paragraph b.of this section.
(2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take
enforcement action against a Permittee for a bypass as provided in any current or future system-wide
collection system permit associated with the treatment facility.
(3) The Permit Issuing Authority may approve an anticipated bypass,after considering its adverse effects,
if the Permit Issuing Authority determines that it will meet the three conditions listed above in
Paragraph c. (1)of this section.
5. Upsets
a. Effect of an upset[40 CFR 122.41 (n) (2)]:An upset constitutes an affirmative defense to an action brought
for noncompliance with such technology based permit effluent limitations if the requirements of
paragraph b. of this condition are met. No determination made during administrative review of claims
that noncompliance was caused by upset, and before an action for noncompliance, is final administrative
action subject to judicial review.
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b. Conditions necessary for a demonstration of upset: Any Permittee who wishes to establish the
affirmative defense of upset shall demonstrate,through properly signed,contemporaneous operating logs,
or other relevant evidence that:
(1)An upset occurred and that the Permittee can identify the cause(s)of the upset;
(2)The Permittee facility was at the time being properly operated;and
(3)The Permittee submitted notice of the upset as required in Part II.E.6. (b)of this permit.
(4)The Permittee complied with any remedial measures required under Part II.B.2.of this permit.
c. Burden of proof[40 CFR 122.41 (n) (4)]: The Permittee seeking to establish the occurrence of an upset has
the burden of proof in any enforcement proceeding.
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of
wastewaters shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to
prevent any pollutant from such materials from entering waters of the State or navigable waters of the United
States. The Permittee shall comply with all existing Federal regulations governing the disposal of sewage
sludge. Upon promulgation of 40 CFR Part 503, any permit issued by the Permit Issuing Authority for the
utilization/disposal of sludge may be reopened and modified, or revoked and reissued, to incorporate
applicable requirements at 40 CFR 503. The Permittee shall comply with applicable 40 CFR 503 Standards for
the Use and Disposal of Sewage Sludge (when promulgated) within the time provided in the regulation,even
if the permit is not modified to incorporate the requirement. The Permittee shall notify the Permit Issuing
Authority of any significant change in its sludge use or disposal practices.
7. Power Failures
The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 2H.0124) to
prevent the discharge of untreated or inadequately treated wastes during electrical power failures either by
means of alternate power sources,standby generators or retention of inadequately treated effluent.
Section D. Monitoring and Records
1. Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and
nature of the permitted discharge. Samples collected at a frequency less than daily shall be taken on a day and
time that is characteristic of the discharge over the entire period the sample represents. All samples shall be
taken at the monitoring points specified in this permit and,unless otherwise specified,before the effluent joins
or is diluted by any other wastestream, body of water, or substance. Monitoring points shall not be changed
without notification to and the approval of the Permit Issuing Authority[40 CFR 122.41 (j)].
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each month and reported
on a monthly Discharge Monitoring Report (DMR) Form (MR 1,1.1, 2,3) or alternative forms approved by the
Director, postmarked no later than the last calendar day of the month following the completed reporting
period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of
these,and all other reports required herein,shall be submitted to the following address:
NC DENR/ Division of Water Quality /Surface Water Protection Section
ATTENTION:Central Files
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
3. Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be
selected and used to ensure the accuracy and reliability of measurements of the volume of monitored
discharges. The devices shall be installed, calibrated and maintained to ensure that the accuracy of the
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measurements is consistent with the accepted capability of that type of device. Devices selected shall be
capable of measuring flows with a maximum deviation of less than 10% from the true discharge rates
throughout the range of expected discharge volumes. Flow measurement devices shall be accurately calibrated
at a minimum of once per year and maintained to ensure that the accuracy of the measurements is consistent
with the accepted capability of that type of device. The Director shall approve the flow measurement device
and monitoring location prior to installation.
Once-through condenser cooling water flow monitored by pump logs, or pump hour meters as specified in
Part I of this permit and based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Laboratories used for sample analysis must be certified by the Division. Permittees should contact the
Division's Laboratory Certification Section (919 733-3908 or http://portal.ncdenr.org/web/wq/lab/cert) for
information regarding laboratory certifications.
Facilities whose personnel are conducting testing of field-certified parameters only must hold the appropriate
field parameter laboratory certifications.
Test procedures for the analysis of pollutants shall conform to the EMC regulations (published pursuant to
NCGS 143-215.63 et.seq.),the Water and Air Quality Reporting Acts,and to regulations published pursuant to
Section 304(g), 33 USC 1314, of the CWA (as amended), and 40 CFR 136; or in the case of sludge use or
disposal, approved under 40 CFR 136, unless otherwise specified in 40 CFR 503, unless other test procedures
have been specified in this permit[40 CFR 122.41].
To meet the intent of the monitoring required by this permit, all test procedures must produce minimum
detection and reporting levels that are below the permit discharge requirements and all data generated must
be reported down to the minimum detection or lower reporting level of the procedure. If no approved
methods are determined capable of achieving minimum detection and reporting levels below permit discharge
requirements, then the most sensitive (method with the lowest possible detection and reporting level)
approved method must be used.
5. Penalties for Tampering
The CWA provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any
monitoring device or method required to be maintained under this permit shall,upon conviction,be punished
by a fine of not more than$10,000 per violation,or by imprisonment for not more than two years per violation,
or by both. If a conviction of a person is for a violation committed after a first conviction of such person under
this paragraph,punishment is a fine of not more than$20,000 per day of violation,or by imprisonment of not
more than 4 years,or both[40 CFR 122.41].
6. Records Retention
Except for records of monitoring information required by this permit related to the Permittee's sewage sludge
use and disposal activities, which shall be retained for a period of at least five years (or longer as required by
40 CFR 503),the Permittee shall retain records of all monitoring information,including:
➢ all calibration and maintenance records
➢ all original strip chart recordings for continuous monitoring instrumentation
➢ copies of all reports required by this permit
➢ copies of all data used to complete the application for this permit
These records or copies shall be maintained for a period of at least 3 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time [40
CFR 122.41].
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit,the Permittee shall record
the following information[40 CFR 122.41]:
a. The date,exact place,and time of sampling or measurements;
b. The individual(s)who performed the sampling or measurements;
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c. The date(s)analyses were performed;
d. The individual(s)who performed the analyses;
e. The analytical techniques or methods used;and
f. The results of such analyses.
8. Inspection and Entry
The Permittee shall allow the Director, or an authorized representative (including an authorized contractor
acting as a representative of the Director),upon the presentation of credentials and other documents as may be
required by law,to;
a. Enter upon the Permittee's premises where a regulated facility or activity is located or conducted, or
where records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this
permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment),
practices,or operations regulated or required under this permit;and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise
authorized by the CWA,any substances or parameters at any location[40 CFR 122.41 (i)].
Section E Reporting Requirements
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit. The
discharge of any pollutant identified in this permit more frequently than or at a level in excess of that
authorized shall constitute a violation of the permit.
2. Planned Changes
The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or
additions to the permitted facility[40 CFR 122.41 (1)].Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR
122.29(b);or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged. This notification applies to pollutants subject neither to effluent limitations in the permit,nor
to notification requirements under 40 CFR 122.42(a) (1).
• c. The alteration or addition results in a significant change in the Permittee's sludge use or disposal
practices,and such alteration, addition or change may justify the application of permit conditions that are
different from or absent in the existing permit,including notification of additional use or disposal sites not
reported during the permit application process or not reported pursuant to an approved land application
plan.
3. Anticipated Noncompliance
The Permittee shall give advance notice to the Director of any planned changes to the permitted facility or
other activities that might result in noncompliance with the permit[40 CFR 122.41 (1) (2)].
4. Transfers
This permit is not transferable to any person without approval from the Director. The Director may require
modification or revocation and reissuance of the permit to document the change of ownership. Any such
action may incorporate other requirements as may be necessary under the CWA[40 CFR 122.41 (1)(3)].
5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit[40 CFR 122.41 (1) (4)].
a. Monitoring results must be reported on a Discharge Monitoring Report(DMR) (See Part II. D. 2) or forms
provided by the Director for reporting results of monitoring of sludge use or disposal practices.
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b. If the Permittee monitors any pollutant more frequently than required by this permit, the results of such
monitoring shall be included in the calculation and reporting of the data submitted on the DMR.
6. Twenty-four Hour Reporting
a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that
potentially threatens public health or the environment. Any information shall be provided orally within 24
hours from the time the Permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the Permittee becomes aware of the circumstances. The written
submission shall contain a description of the noncompliance, and its cause; the period of noncompliance,
including exact dates and times,and if the noncompliance has not been corrected,the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the
noncompliance[40 CFR 122.41 (1) (6)].
b. The Director may waive the written report on a case-by-case basis for reports under this section if the oral
report has been received within 24 hours.
c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response
personnel at(800)662-7956,[phone] or(919)733-3300.
7. Other Noncompliance
The Permittee shall report all instances of noncompliance not reported under Part II. E. 5 and 6. of this permit
at the time monitoring reports are submitted.The reports shall contain the information listed in Part II. E. 6. of
this permit[40 CFR 122.41 (1) (7)].
8. Other Information
Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or
submitted incorrect information in a permit application or in any report to the Director, it shall promptly
submit such facts or information[40 CFR 122.41 (1)(8)].
9. Noncompliance Notification
The Permittee shall report by telephone to either the central office or the appropriate regional office of the
Division as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following:
a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts
of wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a
sludge digester; the known passage of a slug of hazardous substance through the facility; or any other
unusual circumstances.
b. Any process unit failure,due to known or unknown reasons,that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps,aerators,compressors,etc.
c. Any failure of a pumping station,sewer line,or treatment facility resulting in a by-pass without treatment
of all or any portion of the influent to such station or facility.
Persons reporting such occurrences by telephone shall also file a written report within 5 days following first
knowledge of the occurrence.
10. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3 (a)(2)or Section 308 of the Federal Act,33
USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the
offices of the Division. As required by the Act, effluent data shall not be considered confidential. Knowingly
making any false statement on any such report may result in the imposition of criminal penalties as provided
for in NCGS 143-215.1(b)(2)or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The CWA provides that any person who knowingly makes any false statement,representation,or certification
in any record or other document submitted or required to be maintained under this permit, including
monitoring reports or reports of compliance or noncompliance shall,upon conviction,be punished by a fine of
not more than$25,000 per violation,or by imprisonment for not more than two years per violation,or by both
[40 CFR 122.41].
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12. Annual Performance Reports
Permittees who own or operate facilities that collect or treat municipal or domestic waste shall provide an
annual report to the Permit Issuing Authority and to the users/customers served by the Permittee(NCGS 143-
215.1C). The report shall summarize the performance of the collection or treatment system, as well as the
extent to which the facility was compliant with applicable Federal or State laws, regulations and rules
pertaining to water quality. The report shall be provided no later than sixty days after the end of the calendar
or fiscal year,depending upon which annual period is used for evaluation.
The report shall be sent to:
NC DENR/ Division of Water Quality / Surface Water Protection Section
ATTENTION:Central Files
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
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PART III
OTHER REQUIREMENTS
Section A. Construction
The Permittee shall not commence construction of wastewater treatment facilities,nor add to the plant's treatment
capacity, nor change the treatment process(es) utilized at the treatment plant unless the Division has issued an
Authorization to Construct(AtC)permit. Issuance of an AtC will not occur until Final Plans and Specifications for
the proposed construction have been submitted by the Permittee and approved by the Division.
Section B. Groundwater Monitoring
The Permittee shall, upon written notice from the Director, conduct groundwater monitoring as may be required
to determine the compliance of this NPDES permitted facility with the current groundwater standards.
Section C. Changes in Discharges of Toxic Substances
The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe (40 CFR
122.42):
a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent
basis, of any toxic pollutant which is not limited in the permit,if that discharge will exceed the highest of the
following "notification levels";
(1) One hundred micrograms per liter(100 pg/L);
(2) Two hundred micrograms per liter(200 pg/L)for acrolein and acrylonitrile;five hundred micrograms per
liter (500 pg/L) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol; and one milligram per liter (1
mg/L)for antimony;
(3) Five times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge, on a non-routine or
infrequent basis,of a toxic pollutant which is not limited in the permit,if that discharge will exceed the highest
of the following"notification levels";
(1) Five hundred micrograms per liter(500 pg/L);
(2) One milligram per liter(1 mg/L)for antimony;
(3) Ten times the maximum concentration value reported for that pollutant in the permit application.
Section D. Evaluation of Wastewater Discharge Alternatives
The Permittee shall evaluate all wastewater disposal alternatives and pursue the most environmentally sound
alternative of the reasonably cost effective alternatives. If the facility is in substantial non-compliance with the
terms and conditions of the NPDES permit or governing rules, regulations or laws, the Permittee shall submit a
report in such form and detail as required by the Division evaluating these alternatives and a plan of action within
60 days of notification by the Division.
Section E. Facility Closure Requirements
The Permittee must notify the Division at least 90 days prior to the closure of any wastewater treatment system
covered by this permit. The Division may require specific measures during deactivation of the system to prevent
adverse impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit
continue at the permitted facility.
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PART IV
SPECIAL CONDITIONS FOR MUNICIPAL FACILITIES
Section A. Definitions
In addition to the definitions in Part II of this permit,the following definitions apply to municipal facilities:
Indirect Discharge or Industrial User
Any non-domestic source that discharges wastewater containing pollutants into a POTW regulated under section
307(b), (c)or(d)of the CWA. [40 CFR 403.3(i)and(j)]
Interference
Inhibition or disruption of the POTW treatment processes;operations;or its sludge process,use,or disposal which
causes or contributes to a violation of any requirement of the POTW's NPDES Permit or prevents sewage sludge
use or disposal in compliance with specified applicable State and Federal statutes, regulations, or permits. [15A
NCAC 2H.0903(b) (13)]
Pass Through
A discharge which exits the POTW into waters of the State in quantities or concentrations which, alone or with
discharges from other sources, causes a violation, including an increase in the magnitude or duration of a
violation,of the POTW's NPDES permit,or of an instream water quality standard. [15A NCAC 2H.0903(b) (23)]
Publicly Owned Treatment Works(POTW)
A treatment works as defined by Section 212 of the CWA, owned by a State or local government entity. This
definition includes any devices and systems used in the storage,treatment,recycling and reclamation of municipal
sewage or industrial wastes of a liquid nature. It also includes sewers, pipes, and other conveyances only if they
convey wastewater to a POTW. The term also means the local government entity, or municipality, as defined in
section 502(4) of the CWA, which has jurisdiction over indirect discharges to and the discharges from such a
treatment works. [15A NCAC 2H.0903(b)(27)]
"Significant Industrial User"or"SIU"
An industrial user that discharges wastewater into a publicly owned treatment works and that [15A NCAC
2H.0903(b)(34)]:
(a) discharges an average of 25,000 gallons or more per day of process wastewater to the POTW (excluding
sanitary,noncontact cooling and boiler blowdown wastewaters)or;
(b) contributes more than 5 percent of the design flow of the POTW treatment plant or more than 5 percent of the
maximum allowable headworks loading of the POTW treatment plant for any pollutant of concern,or;
(c) is required to meet a national categorical pretreatment standard,or;
(d) is, regardless of Parts (a), (b), and (c) of this definition, otherwise determined by the POTW, the Division, or
the EPA to have a reasonable potential for adversely affecting the POTW's operation or for violating any
pretreatment standard or requirement or POTW's receiving stream standard, or to limit the POTW's sludge
disposal options.
Section B. Publicly Owned Treatment Works(POTWs)
All POTWs are required to prevent the introduction of pollutants into the POTW which will interfere with the
operation of the POTW, including interference with its use or disposal of municipal sludge, or pass through the
treatment works or otherwise be incompatible with such treatment works. [40 CFR 403.2]
All POTWs must provide adequate notice to the Director of the following[40 CFR 122.42(b)]:
1. Any new introduction of pollutants into the POTW from an indirect discharger, regardless of the means of
transport, which would be subject to section 301 or 306 of CWA if it were directly discharging those
pollutants;and
2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger as
influent to that POTW at the time of issuance of the permit.
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3. For purposes of this paragraph, adequate notice shall include information on (1) the quality and quantity of
effluent introduced into the POTW, and (2) any anticipated impact that may result from the change of the
quantity or quality of effluent to be discharged from the POTW.
Section C. Municipal Control of Pollutants from Industrial Users.
1. Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs from industries
using the municipal system may be present in the Permittee's discharge.At such time as sufficient information
becomes available to establish limitations for such pollutants, this permit may be revised to specify effluent
limitations for any or all of such other pollutants in accordance with best practicable technology or water
quality standards.
2. Prohibited Discharges
a. Under no circumstances shall the Permittee allow introduction of pollutants or discharges into the waste
treatment system or waste collection system which cause or contribute to Pass Through or Interference as
defined in 15A NCAC 2H.0900 and 40 CFR 403. [40 CFR 403.5(a) (1)]
b. Under no circumstances shall the Permittee allow introduction of the following wastes in the waste
treatment or waste collection system[40 CFR 403.5(b)]:
(1) Pollutants which create a fire or explosion hazard in the POTW, including, but not limited to,
wastestreams with a closed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees
Centigrade using the test methods specified in 40 CFR 261.21;
(2) Pollutants which cause corrosive structural damage to the POTW,but in no case discharges with pH
lower than 5.0,unless the works is specifically designed to accommodate such discharges;
(3) Solid or viscous pollutants in amounts which cause obstruction to the flow in the POTW resulting in
Interference;
(4) Any pollutant, including oxygen demanding pollutants (BOD, etc.) released in a Discharge at a flow
rate and/or pollutant concentration which will cause Interference with the POTW;
(5) Heat in amounts which will inhibit biological activity in the POTW resulting in Interference,but in no
case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C (104°F)
unless the Division,upon request of the POTW,approves alternate temperature limits;
(6) Petroleum oil, non-biodegradable cutting oil, or products of mineral oil origin in amounts that will
cause Interference or Pass Through;
(7) Pollutants which result in the presence of toxic gases,vapors,or fumes within the POTW in a quantity
that may cause acute worker health and safety problems;
(8) Any trucked or hauled pollutants,except at discharge points designated by the POTW.
c. The Permittee shall investigate the source of all discharges into the POTW,including slug loads and other
unusual discharges, which have the potential to adversely impact the permittee's Pretreatment Program
and/or the operation of the POTW.
The Permittee shall report such discharges into the POTW to the Director or the appropriate Regional
Office. Any information shall be provided orally within 24 hours from the time the Permittee became
aware of the circumstances. A written submission shall also be provided within 5 days of the time the
Permittee becomes aware of the circumstances. The written submission shall contain a description of the
discharge, the investigation into possible sources; the period of the discharge, including exact dates and
times; and if the discharge has not ceased, the anticipated time it is expected to continue;and steps taken
or planned to reduce,eliminate,and prevent reoccurrence of the noncompliance,
3. With regard to the effluent requirements listed in Part I of this permit,it may be necessary for the Permittee to
supplement the requirements of the Federal Pretreatment Standards (40 CFR, Part 403) to ensure compliance
by the Permittee with all applicable effluent limitations. Such actions by the Permittee may be necessary
regarding some or all of the industries discharging to the municipal system.
4. The Permittee shall require any Industrial User discharging to the POTW to meet Federal Pretreatment
Standards developed under Section 307(b) of the Act as amended (which includes categorical standards and
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specific local limits, best management practices and narrative requirements). Prior to accepting wastewater
from any Significant Industrial User, the Permittee shall either develop and submit to the Division a new
Pretreatment Program or a modification of an existing Pretreatment Program, for approval as required under
section D below as well as 15A NCAC 2H.0907(a)and(b). [40 CFR 122.44(j)(2)]
5. This permit shall be modified, or alternatively, revoked and reissued, to incorporate or modify an approved
POTW Pretreatment Program or to include a compliance schedule for the development of a POTW
Pretreatment Program as required under Section 402 (b) (8) of the CWA and implementing regulations or by
the requirements of the approved State pretreatment program,as appropriate.
Section D. Pretreatment Programs
Under authority of sections 307(b) and (c) and 402 (b) (8) of the CWA and implementing regulations 40 CFR 403,
North Carolina General Statute 143-215.3 (14) and implementing regulations 15A NCAC 2H.0900, and in
accordance with the approved pretreatment program, all provisions and regulations contained and referenced in
the Pretreatment Program Submittal are an enforceable part of this permit. [40 CFR 122.44(j) (2)]
The Permittee shall operate its approved pretreatment program in accordance with Section 402(b) (8)of the CWA,
40 CFR 403,15A NCAC 2H.0900,and the legal authorities,policies,procedures,and financial provisions contained
in its pretreatment program submission and Division approved modifications thereof. Such operation shall
include but is not limited to the implementation of the following conditions and requirements. Terms not defined
in Part II or Part IV of this permit are as defined in 15A NCAC 2H.0903 and 40 CFR 403.3.
1. Sewer Use Ordinance(SUO)
The Permittee shall maintain adequate legal authority to implement its approved pretreatment program. [15A
NCAC 2H.0905 and .0906;40 CFR 403.8(f)(1)and 403.9(b) (1),(2)]
2. Industrial Waste Survey(IWS)
The permittee shall implement an IWS consisting of the survey of users of the POTW, as required by 40 CFR
403.8 (f) (2) (i-iii) and 15A NCAC 2H.0905 [also 40 CFR 122.44 (j) (1)], including identification of all industrial
users that may have an impact on the POTW and the character and amount of pollutants contributed to the
POTW by these industrial users and identification of those industrial users meeting the definition of SIU. The
Permittee shall submit a summary of its IWS activities to the Division at least once every five years, and as
required by the Division.The IWS submission shall include a summary of any investigations conducted under
paragraph C.2.c.of this Part.
3. Monitoring Plan
The Permittee shall implement a Division-approved Monitoring Plan for the collection of facility specific data
to be used in a wastewater treatment plant Headworks Analysis (HWA) for the development of specific
pretreatment local limits. Effluent data from the Plan shall be reported on the DMRs (as required by Part II,
Section D,and Section E.5.). [15A NCAC 2H.0906(b) (2)and .0905]
4. Headworks Analysis(HWA)and Local Limits
The Permittee shall obtain Division approval of a HWA at least once every five years, and as required by the
Division. Within 180 days of the effective date of this permit (or any subsequent permit modification) the
Permittee shall submit to the Division a written technical evaluation of the need to revise local limits (i.e., an
updated HWA or documentation of why one is not needed) [40 CFR 122.44]. The Permittee shall develop, in
accordance with 40 CFR 403.5 (c)and 15A NCAC 2H.0909,specific Local Limits to implement the prohibitions
listed in 40 CFR 403.5 (a) and (b) and 15A NCAC 2H.0909. Pursuant to 40 CFR 403.5, local limits are
enforceable Pretreatment Standards as defined by 40 CFR 403.3(1).
5. Industrial User Pretreatment Permits(IUP)&Allocation Tables
In accordance with NCGS 143-215.1, the Permittee shall issue to all significant industrial users, permits for
operation of pretreatment equipment and discharge to the Permittee's treatment works. These permits shall
contain limitations, sampling protocols, reporting requirements, appropriate standard and special conditions,
and compliance schedules as necessary for the installation of treatment and control technologies to assure that
their wastewater discharge will meet all applicable pretreatment standards and requirements. The Permittee
shall maintain a current Allocation Table (AT) which summarizes the results of the HWA and the limits from
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•
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all IUPs. Permitted IUP loadings for each parameter cannot exceed the treatment capacity of the POTW as
determined by the HWA. [15A NCAC 2H.0909, .0916, and .0917; 40 CFR 403.5, 403.8 (f) (1) (iii); NCGS 143-
215.67(a)]
6. Authorization to Construct(AtC)
The Permittee shall ensure that an Authorization to Construct permit (AtC) is issued to all applicable
industrial users for the construction or modification of any pretreatment facility. Prior to the issuance of an
AtC, the proposed pretreatment facility and treatment process must be evaluated for its capacity to comply
with all Industrial User Pretreatment Permit (IUP) limitations. [15A NCAC 2H.0906 (b) (6) and .0905; NCGS
143-215.1 (a)(8)]
7. POTW Inspection&Monitoring of their IUs
The Permittee shall conduct inspection, surveillance, and monitoring activities as described in its Division
approved pretreatment program in order to determine, independent of information supplied by industrial
users, compliance with applicable pretreatment standards. [15A NCAC 2H .0908(d); 40 CFR 403.8(f)(2)(v)]
The Permittee must:
a. Inspect all Significant Industrial Users(SIUs)at least once per calendar year;and
b. Sample all Significant Industrial Users (SIUs) at least twice per calendar year for all permit-limited
pollutants,once during the period from January 1 through June 30 and once during the period from July 1
through December 31, except for organic compounds which shall be sampled at least once per calendar
year; For the purposes of this paragraph, "organic compounds" means the types of compounds listed in
40 CFR 136.3(a),Tables IC,ID,and IF,as amended.
8. IU Self Monitoring and Reporting
The Permittee shall require all industrial users to comply with the applicable monitoring and reporting
requirements outlined in the Division-approved pretreatment program,the industry's pretreatment permit, or
in 15A NCAC 2H .0908. [15A NCAC 2H .0906(b)(4) and .0905; 40 CFR 403.8(f)(1)(v) and (2)(iii); 40 CFR
122.44(j)(2)and 40 CFR 403.12]
9. Enforcement Response Plan(ERP)
The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards
promulgated pursuant to section 307(b) and (c) of the Clean Water Act (40 CFR 405 et. seq.), prohibitive
discharge standards as set forth in 40 CFR 403.5 and 15A NCAC 2H .0909, and specific local limitations. All
remedies, enforcement actions and other, shall be consistent with the Enforcement Response Plan (ERP)
approved by the Division. [15A NCAC 2H.0906(b)(7)and.0905; 40 CFR 403.8(0(5)]
10. Pretreatment Annual Reports(PAR)
The Permittee shall report to the Division in accordance with 15A NCAC 2H .0908. In lieu of submitting
annual reports,Modified Pretreatment Programs developed under 15A NCAC 2H.0904(b)may be required to
submit a partial annual report or to meet with Division personnel periodically to discuss enforcement of
pretreatment requirements and other pretreatment implementation issues.
For all other active pretreatment programs, the Permittee shall submit two copies of a Pretreatment Annual
Report (PAR) describing its pretreatment activities over the previous twelve months to the Division at the
following address:
NC DENR/Division of Water Quality /Surface Water Protection Section
Pretreatment,Emergency Response,and Collection Systems(PERCS)Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
These reports shall be submitted according to a schedule established by the Director and shall contain the
following:
a.) Narrative
A brief discussion of reasons for, status of, and actions taken for all Significant Industrial Users (SIUs) in
Significant Non-Compliance(SNC);
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b.) Pretreatment Program Summary(PPS)
A pretreatment program summary(PPS)on specific forms approved by the Division;
c.) Significant Non-Compliance Report(SNCR)
The nature of the violations and the actions taken or proposed to correct the violations on specific forms
approved by the Division;
d.) Industrial Data Summary Forms(IDSF)
Monitoring data from samples collected by both the POTW and the Significant Industrial User (SIU) in
SNC.These analytical results must be reported on Industrial Data Summary Forms(IDSF)or other specific
format approved by the Division;
e.) Other Information
Copies of the POTW's allocation table, new or modified enforcement compliance schedules, public notice
of SIUs in SNC,and any other information,upon request,which in the opinion of the Director is needed to
determine compliance with the pretreatment implementation requirements of this permit;
11. Public Notice
The Permittee shall publish annually a list of Significant Industrial Users (SIUs) that were in Significant Non-
Compliance (SNC) as defined in the Permittee's Division-approved Sewer Use Ordinance with applicable
pretreatment requirements and standards during the previous twelve month period. This list shall be
published within four months of the applicable twelve-month period. [15A NCAC 2H .0903(b)(35), .0908(b)(5)
and.0905 and 40 CFR 403.8(f)(2)(viii)]
12. Record Keeping
The Permittee shall retain for a minimum of three years records of monitoring activities and results, along
with support information including general records,water quality records,and records of industrial impact on
the POTW. [15A NCAC 2H.0908(f); 40 CFR 403.12(o)]
13. Funding and Financial Report
The Permittee shall maintain adequate funding and staffing levels to accomplish the objectives of its approved
pretreatment program. [15A NCAC 2H .0906(a)and.0905;40 CFR 403.8(f)(3),403.9(b)(3)]
14. Modification to Pretreatment Programs
Modifications to the approved pretreatment program including but not limited to local limits modifications,
POTW monitoring of their Significant Industrial Users (SIUs), and Monitoring Plan modifications, shall be
considered a permit modification and shall be governed by 40 CFR 403.18, 15 NCAC 2H .0114 and 15A NCAC
2H.0907.
Version 10/29/2010

SOC PRIORITY PROJECT:
To:Western NPDES Unit
Surface Water Protection Section
Attention: Charles Weaver
Date: March 31, 2010
NPDES STAFF REPORT AND RECOMMENDATIONS
County: Gaston
NPDES Permit No.: NC000005177
PART I - GENERAL INFORMATION
1. Facility and address: FMC Lithium
1115 Bessemer City Kings Mountain Hwy
Hwy 161
Bessemer City,NC 28016
2. Date of investigation: March 29, 2010
3. Report prepared by: B. Dee Browder,Environmental Engineer
4. Person contacted and telephone number: Rodney Willis, ORC, [phone]
5. Directions to site: From I-77 S merge onto I-485 S via exit 19B toward Spartanburg
(11.6 miles). Merge onto I-485 S via exit 19B toward Spartanburg(11.6 miles). Take
the I-85/US-29/US-74 , exit 9-10,toward Greensboro/Spartanburg/Wilkinson Blvd. (0.4
mi). Merge onto I-85 S via exit 10B toward Gastonia/Spartanburg (17.4 miles). Take the
Edgewood Road exit, exit 13,toward Bessemer City(0.2 mile). Turn right onto
Edgewood Road (0.9 mile). Edgewood Road becomes Athenia Pl. (0.4 mile).
Athenia Pl. becomes E. Alabama Ave. (0.9 mile). Turn right onto S 14TH St. (0.0 mile).
Turn left onto NC-161. (1.3 miles). 1115 Bessemer City Kings Mountain Hwy is on the
left.
Total Travel Estimate: 1 hour 2 minutes/ 54.63 miles mile).

6. Discharge point(s): Latitude: 35° 15' 44"
Longitude: 81° 17' 57"
USGS Quad No.: F 13 SE
7. Receiving stream or affected surface waters: UT to Abernathy Creek
a. Classification: C
b. River Basin.: Catawba
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
1. a. Volume of wastewater: 0.615 MGD
b. What is the current permitted capacity: N/A MGD
c. Date(s) and construction activities allowed by previous ATCs issued in the
previous two years: N/A
d. Description of existing or substantially constructed WWT facilities: The existing
facility consists of two reverse osmosis treatment units, hydrogen peroxide feed
for chlorine neutralization,hydroxide scrubber area roof drain, compressor
condensate,pH adjustment, condensate, cooling tower overflow(various locations
throughout facility)„ lithium hypochlorite scrubber waters, miscellaneous salts,
phosphate wastes,boiler blow down, stormwater from chlorine recovery floor,
and other roof drains, yard drains, and drainage from facilities on west site of
Hwy.
e. Description of proposed WWT facilities: N/A
f. Possible toxic impacts to surface waters: There are no toxic impacts expected.
g. Pretreatment Program(POTWs only): Not Needed.
2. Residual handling and utilization/disposal scheme:N/A
a. If residuals are being land applied specify DWQ Permit No.
PART III - OTHER PERTINENT INFORMATION
1. Special monitoring or limitations (including toxicity) requests: None at this time.
2. Important SOC/JOC or Compliance Schedule dates: N/A
3. Alternative analysis evaluation
a. Spray Irrigation: N/A
b. Connect to regional sewer system: N/A
c. Subsurface: N/A
d. Other disposal options: N/A

PART IV -EVALUATION AND RECOMMENDATIONS
The FMC Corporation,Lithium Division NPDES permit is under review for renewal of their
discharge permit. The systems were observed to be in good working order at the time of the field
review. At the time of the site visit there was significant flow at the outfall due to heavy rainfall.
There are groundwater remediation well throughout the plant site. These wells are covered under
NC Hazardous Water Section NCD000771964.
This permit combines a wastewater permit with an industrial stormwater permit. MRO
recommends that the permit be reviewed for consistency with the most recent stormwater testing,
observation, and permit requirements.
The facility has collected and submitted analytical data and requests that ethyl benzene and
methyl chloride be removed from the permit.
MRO recommends that the permit b ren wed.
3131110
Signature of Report Preparer Date
Water Quality Regional Supervisor Date
h:\dsr\dsr08\.dsr

•.A
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
March 8, 2010
RODNEY S WILLIS
wiHFi - 9 2010
ENVIRONMENTAL ENGINEER, SITE ORC
FMC LITHIUM DIVISION
PO BOX 795
BESSEMER CITY NC 28016
► IIs �Th
Subject: Receipt of permit renewal application
NPDES Permit NC0005177
Lithium Division Plant
Gaston County
►6(1II'S
Dear Mr. Willis:
The NPDES Unit received your permit renewal application on March 1, 2010. A member of the NPDES
Unit will review your application. They will contact you if additional information is required to complete your
permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit
expires.
If you have any additional questions concerning renewal of the subject permit, please contact Ron Berry at
[phone].
Sincerely,
Dina Sprinkle
Point Source Branch
cc: CENTRAL FILES
"IIIIIIMMIIIIMPRIMPM /Surface Water Protection
NPDES Unit
1617 Mail Service Center,Raleigh,North Carolina 27699-1617 •
Location:512 N.Salisbury St Raleigh,North Carolina 27604 One
Phone:[phone] FAX:[phone] Customer Service:1-877-623-6748 North Carolina
Internet:www.ncwaterquality.org Naturally Equal Opportunity 1 Affirmative Action Employer

tRtt ,j..,rt ,._ ,,,,,,._
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-FMC - - O
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CERTIFIED MAIL
RETURN RECEIPT REQUESTED
February 26, 2010
Mrs. Dina Sprinkle
NC DENR/DWQ/Point Source Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Re: NPDES Renewal Application—Permit No.NC0005177
Dear Mrs. Sprinkle:
FMC Corporation—Lithium Division, located in Bessemer City, Gaston County
("FMC")hereby requests renewal of NPDES Permit No.NC0005177. This renewal
application is being submitted at least 180 days prior to the expiration date of the current
permit on August 31, 2010. FMC requests that if a new permit is not issued by the
expiration date, that the current permit remain in force until superceded by a new permit.
Enclosed are one signed original and two copies of US EPA Form 2C and attachments.
Please note the following:
• One change has occurred since issuance of the last permit involving the addition
of a stormwater control pump in our R&D pond identified as contributing flow
number 11 on page one of Form 2C of the application and also shown on the
facility Process Flow Diagram (PFD).
• The enclosed process flow diagram has been numbered for use with the treatment
systems referenced on US EPA Form 2C.II.B, for your convenience.
• Included is the Pace Analytical Services report including the quality control data.
Air Treatment Construction Energy Fine Chemicals Glass&Ceramics Greases&Lubricants Polymers Pool Water Treatment
PO Box 795 Phone:[phone] [e-mail]
Bessemer City,NC 28016 Fax:[phone] www.fmclithium.com
MARKETS SERVED

FMC looks forward to discussing the permit renewal with the Division of Water Quality.
If you have questions feel free to contact me at 704-868-7630 or by e-mail to
[e-mail].
Sincerely b�
Rodney S. Willis —
Environmental Engineer, Site ORC
FMC Lithium Division
Bessemer City,NC ( c44 67
Enclosures

s
FMC Corporation—Lithium Division
NPDES Permit Renewal,February 2010
Permit No.NC0005177
Sludge Management Plan
In February 1999, FMC discontinued operation of its two sanitary sewer package plants
by directing all sanitary sewer wastewater and laboratory drains to the Bessemer City
POTW. Therefore,no Sludge Management Plan is required.
to.4. k)AL
Rodney Willis Da e
Environmental Engineer
FMC Corporation—Lithium Division

EPA I.D.NUMBER(copy from Item I of Form I) Form Approved.
OMB No.2040-0086.
Please print or type in the unshaded areas only. NCD000771964 Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
ZC f•EPA EXISTING MANUFAAPPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
CTURING,COMMERCIAL,MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I.OUTFACE LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(list) 1.DEG. 2.MIN. 3.SEC. 1.DEG. 2.MIN. 3.SEC. D.RECEIVING WATER(name)
001 35.00 15.00 43.00 81.00 17.00 54.00 U.T. of Abernethy Creek
004 35.00 15.00 43.00 81.00 17.00 54.00 U.T. of Abernethy Creek
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall,provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2)The average flow contributed by each operation; and (3)The treatment received by the wastewater. Continue on additional sheets if
necessary.
1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1
1) Misc. Salts and Cat. Phosphate _5,000 gals/mth None
001 X X
2) LiOCL Air Scrubber Waste Water H202 Addition and Equalization
-100 gpm 2 L
3) Boiler Slowdown None
-15 gpm X X
4)LiCl RO permeate and condesate _9,550 GPD Reverse Osmosis 1 S
5) QA Lab, HVAC cooling water -32 gpm None
X X
6) Compressor Condensate None X X
<1 gpm
7) Li Hydroxide RO -5,000 gals/mth Reverse Osmosis 1 B
8) Battery Metal Cooling Tower <10 gpm None X X
9) Combined Plant Waste Water 130 gpm pH adjustment 2 K
10) Li Hydroxide Cooling Twr. None X X
35 gpm
11) R&D Pond stormwater management 10 gpm Setteling X X
Site Stormwater *including Settling 1 V
004 0.50 MGD
* Boiler Blowndown
* Process Condensate
* Cooling Water
OFFICIAL USE ONLY(effluent guidelines sub-categories)
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
©YES(complete the following table) ❑NO(go to Section III)
3.FREQUENCY 4.FLOW
a.DAYS PER B.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in mgd) (specify with units)
1.OUTFALL CONTRIBUTING FLOW (speck PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(list) (list) average) (spec average) AVERAGE DAILY AVERAGE DAILY (in days)
001 1) Misc. Salts and Cat. Phosphate --- 6 --- 0.005 --- 5,000 gal ---
11) R&D Pond stormwater management 7 6 --- 0.015 ---- 0.010 MG 180
5) QA Lab, HVAC cooling water 7 --- 6.5 0.072 50 gpm 0.072 MG 90
III.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
❑YES(complete Item III-B) ®NO(go to Section IV)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
❑YES(complete Item III-C) 0 NO(go to Section IV)
C.If you answered"yes"to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION 2.AFFECTED OUTFALLS
a.QUANTITY PER DAY b.UNITS OF MEASURE C.OPERATION,PRODUCT,MATERIAL,ETC. (list outfall numbers)
(specify)
IV.IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any impie ,entation schedule for the construction, upgreuing or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
O YES(complete the following table) 2 NO(go to Item IV-B)
1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 4.FINAL COMPLIANCE DATE
3.BRIEF DESCRIPTION OF PROJECT
AGREEMENT,ETC.
a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
B. OPTIONAL:You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
❑MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D.NUMBER(copy from Item 1 of Form 1)
CONTINUED FROM PAGE 2 NC000771964
V INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding—Complete one set of tables for each outfall—Annotate the outfall number in the space provided.
NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
VI POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
YES(list all such pollutants below) ❑NO(go to Item VI-B)
Toluene
Potential discharge only through outfall 004.
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII.BIOLOGICAL TOXICITIIIIIIIMIIINMIMMMIMIIIMINMIMIMIII TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
©YES(ident fy the test(s)and describe their purposes below) ❑NO(go to Section VIII)
Chronic Toxicity, Presently required by our NPDES discharge Permit of outfall 001.
VIII.CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
®YES(list the name,address,and telephone number of,and pollutants analyzed by, ❑NO(go to Section IX)
each such laboratory or firm below)
A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (list)
Pace Analytical Services 9800 Kincey Ave. Suite 100 704-875-9092 See page 3 of Pace
Huntersville, NC 28078 Analytical report
Pace Analytical Services 2225 Riverside Dr. See page 3 of Pace
Asheville, NC 828-254-7176 Analytical report
IX.CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.lam aware that there
are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A.NAME&OFFICIAL TITLE(type or print) B.PHONE NO.(area code&no.)
Robert Haire rt.. AP r�,�,,.-(M - (704) 868-7650
C.SIGNATURE I Fi4 i D.DATE SIG D
Z 16 ZO10
EPA Form 0-2C(8-90) PAGE 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copy from Item 1 of Form 1)
on separate sheets(use the same format)instead of completing these pages. NC000771964
SEE INSTRUCTIONS.
OUTFALL NO.
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C) 001
PART A-You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (specifyifblank) (optional)
b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
(1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
1.POLLUTANT CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Biochemical Oxygen 15.0 mg/1 22.9 lb --- --- 2.17 mg/1 1987 lbs 12 mg/1 lbs
Demand(BOD)
b.Chemical Oxygen <25.0 mg/1 --- --- --- --- 1 mg/1 lbs
Demand(COD)
Do not Wish to
c.Total Organic Carbon
(TOC) 5.9 mg/1 --- --- --- --- --- 1 mg/1 lbs apply for "net"
d.Total 11.0 m 1 28.2 lb --- --- 3.19 m /1 7.94 lbs 24 m /1 lbs eligibility
Solidss(Suspended
g/ g g
e.Ammonia(asN) 0.15 mg/1 0.33 lb --- --- 0.01 mg/1 --- 12 mg/1 lbs
VALUE VALUE VALUE VALUE
f.Flow 0.490 MG 14.6 MG 109.80 MG 1 yr --- MG
g.Temperature VALUE VALUE VALUE oC VALUE
(winter) 10.2 --- 7.9 7
h.Temperature VALUE 29 VALUE VALUE 28 11 oC VALUE
(summer)
MINIMUM MAXIMUM MINIMUM MAXIMUM �, ' 1f / s >? a 07e0 �`1'
l F ' 1�f STANDARD UNITS r ' w ,i? �� e
I.pH 7 4 8.7 --- - s it i „ �< .� //.b 5 2 y io , i,C r �S �
r,.,e' �.,>..,,a�M,.._.,z_ u�".�,:-:,,�.a°.,_/as'k ems. �,� ���"�S
PART B- Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either
directly,or indirectly but expressly, in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a,you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AVERAGE
AND a b. a.MAXIMUM DAILY VALUE (if available) (if available) VALUE
CAS NO. BELIEVED BELIEVED d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide 0.80 1 mg/1
(24959-67-9) ` ,
b.Chlorine,Total X <0.10 1 mg/1
Residual
c.Color `X <20 1 ADMI
d.Fecal Coliform X <1.0 1 CFU/10 Om
e. 84-4e(1 X , `
(16984-48-8) ` , 0.51 1 mg/1
f.Nitrote-Nitrite
(as N) X <0.10 <0.10 4 mg/1 l
EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT -
2.MARK'le 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
AND a. b. a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen, ` ,
Total organic(as X 1.1 1 mg/1
N)
h.oil and X <5.0 1 mg/1
Grease
I.Phosphorus ` /
(as P),Total X <0.10 1 mg/1
(7723-14-0) , ` .
j.Radioactivity
(1)Alpha,Total X 6.99+-2.34 1 pCi/L
(2)Beta,Total X 4.38+-1.36 1 pCi/L
(3)Radium, X -.115+-.33 1 pCi/L
Total
(4)Radium226, X .175+-.201 1 pCi/L
Total
Sulfate( X
(also,) 297 1 mg/1
(14808-79-8)
I.Sulfide X <0.10 1 mg/1
m.Sulfite
(also,) X <2.00 1 mg/1
(14265-45-3)
n.Surfactants X <0.1 1 mg/1
o.Aluminum, X
Total <100 1 ug/1
(7429-90-5)
p.Barium,Total
(7440-39-3) X 31.8 1 ug/1
Boron,q. Total
(7440-42-8)
X 79.8 1 ug/1
/�
r.Cobalt,Total(7440-48-4) X <5.0 1 ug/1
Iron,
Tota
(439- 9-6) X <50.0 1 ug/1
(7439�9-8)
t.Magnesium, X
Total 36600 1 ug/1
(7439-95-4)
u.Molybdenum, X
Total <5.0 1 ug/1
(7439-98-7)
v.Manganese, X
Total 59.1 1 ug/1
(7439-96-5)
w.Tin,(7440- 1-5) X <5.0 1 ug/1
(7440 31-5)
x.Titanium,
Total X <5.0 1 ug/1
(7440-32-6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D.NUMBER(copy fromI'tem 1 of Form I) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC000771964 001
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark"X"in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2a(secondary industries,nonprocess wastewater outfalls,and nonrequired GC/MS
fractions),mark"X'in column 2-b for each pollutant you know or have reason to believe is present.Mark"X"in column 2-c for each pollutant you believe is absent If you mark column 2a for any pollutant,you must
provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein,acrylonitrile,2,4 dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged.Note that there are 7 pages to this part,please review each carefully.Complete one table(all 7 pages)for each outfall.See instructions for
additional details and requirements.
2.MARK"X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BEUEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of-available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
METALS,CYANIDE,AND TOTAL PHENOLS
1M.Antimony,Total X <5 0 1 ug/1
(7440-36-0) ,`/`
2M
(74 Arsenic,- ) Total X 7� <5 0 1 ug/1
(744038 2)
3M.Beryllium,Total(7440-41-7) X�/ X <5 0.0 1 ug/1
4M.Cadmium,Total(7440-3-9) /� X�/ X <1 0 1 ugh 1
5M.Chromium,TX X <1 0 1 ug/1
Total(7440-47-3) /� `,
(7440-50-8) 7�
Copper, X <5 0 1 ug/1
7M(74 Lead,Total-1) X X <5.0 1 ug/1
8M.Mercury,Total �/ 0.2 0 1 ugh 1
(7439-97-6) X `/X,`
9M.Nickel,Total X X <5.0 1 ugh 1
(7440-02-0) , ` .
Tot l Sel(778249- X X <10.0 1 ug/1
Total(7782-49-2)
11M.Silver,Total(7440-22-4) X�/ X <5.0 1 ug/1
12M.Thal
(744 -28 X X <10.0 1 ug/1
um,
Total(7440-28 0) ^ ,` ,
13M.Zinc,Total
(7440-66-6)
X X <10.0 1 ug/1
/�
Total Cyanide,Total(57-12-5) /�X X <0.0050 1 mg/1
15M.Phenols,Total /��/ X <5 3 ug/1
DIOXIN
2,3,7,8-Tetra- DESCRIBE RESULTS
chlorodibenzo-P-
Dioxin(1764-01-6)
EPA Form 3510-2C(8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT -
2.MARK"X" 3.EFFLUENT •
4.UNITS 5.INTAKE(optional)
-
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONC1) ENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION-VOLATILE COMPOUNDS
1V. 8 X X <100 1 ug/1
(107-02-8)
2V.Acrylonitrile X X <100 1 ug/1
(107-13-1)
3V.(71-43-2) X X <5.0 1 ug/1
71
4V.Bis(Chloro-
` / `/
methyl)Ether x J( <5.0 1 ug/1
(542-88-1) , ` , `
5V.B5omofonn(75-25-2) X X <5 0 1 ug/1
6V.Carbon
Tetrachloride X X <5.0 1 ug/1
(56-23-5)
7V.Chiorobenzene X X <5.0 1 ug/1
(108-90-7)
8V.Chlorodi- \/
bromomethane x <5.0 1 ug/1
(124-48-1)
9V.
Chloroethane
(75-00-3) X X <10.0 1 ug/1
10V.2 X X
ethylvinylnyl Ether <10.0 1 ug/1
(110-75-8)
11V.7- Chloroform(6 66-3) X X
12V.Dichloro-
bromomethane X X <5.0 1 ug/1
(75-27-4)
13V.Dichloro-
dilluoromethane X X <5.0 1 ug/1
(75-71-8)
14V.1, 5-3oro X X <5.0 1 ug/1
(7
ethane(75343)
15V.1,2-Dichloro X X <5.0 1 ug/1
ethane(107-06-2)
16V.1,1 Dichloro-
X X <5.0 1 ug/1
ethylene(75-35-4)
17V.1, oro X X <5.0 1 ug/1
propanee(78-87-5)
18V.1,3-Dichloro-
X X <5.0 1 ug/1
propylene
(542-75-6)
19V.Ethylbenzene X X <5 0 1 ug/1
(100-41-4) ` <10.0
,
20V.Methyl 1 ug/1
Bromide(74-83-9) `X `/X`,
21V.Methyl y X <5.0 1 ug/1
Chloride(74-87-3) ,`
EPA Form 3510-2C(8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
2.MARK"X" 3.EFFLUENT •
4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (ifavailable) VALUE(f available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(rfavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS(continued)
(ccontinued)
22V.Methylene
Chloride(75-09-2) X 7r; <5 0 1 ug/1
23V.1,1,2,2-
Tetrachloroethane X X <5.0 1 ug/1
(79-34-5)
24V.Tetrachloro-
ethylene(127-18-4) X X <5 0 1 ug/1
25V.Toluene X X <5.0 1 ug/1
(108-88-3)
26V.1,2 Trans-
Dichloroethylene X X <5.0 1 ug/1
(156-60-5)
e7V.tha 1,e1,1-55-6)oro X X <5.0 1 ug/1
ethane(7155-0)
28V.1,1,2-Trichloro X X <5.0 1 ug/1
ethane(79-00-5)
29V eehr
eththylenne(79-01-6)
X X <5 0 1 ug/1
-0
30V.Trichloro-
fluoromethane X X <10.0 1 ug/1
(75-69-4)
31V.Vinyl Chloride X X <5 0 1 ug/1
(75-01-4)
GC/MS FRACTION—ACID COMPOUNDS `,
1a 2 Chlorophenol X X <5.3 1 ug/1
(95-57-8)
2a 2,4-Dichloro-
phenol
X X <2.1 1 ug/1
phenol(120-83-2) .
3a2,4-Dimethyl- X X <5 3 1 ug/1
phenol(105-67-9) X
4a4,6-Dinitro-O- X X <4 2 1 ug/1
Cresol(534-52-1) .
Dinitro- X X <14.7 1 ug/1
phenol
phenol(51-28-5)
6a 2 Nitrophenol X X <5.3 1 ug/1
(88-75-5)
7a4-Nitrophenol X X <21.1 1 ug/1
(100-02-7) /�
8a P-C - �/ X <4 2 1 ug/1
Cresol(59-50-5950-7) X
9a Pentachloro X X <21.1 1 ug/1
phenol(87-865)
10A.08 PhenolX X <5 3 1 ug/1
(108-95-2)-2)
11A.2,4,6Tnchloro-
X X <2.1 1 ug/1
phenol(88-05-2) /�
EPA Form 3510-2C(8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT -
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BEUEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS
113.Acenaphthene 1 u 1
(83-32-9) `, g/
2B.Acenaphtylene X <5 3 1 ug/1
(208-96-8)
3B.Anthracene
(120-12-7) /�X/ X <5 3 1 ug/1
4B.Benzidine
(92-87-5)
X X <26 3 1 ug/1
5B(92
a (a) X X
Anthracene <2.1 1 ug/1
(56-55-3)
68.Benzo(a) X X <1.1 1 ug/1
Pyrene(50-32-8)
7B.3,4-Benzo-
fluoranthene X X <5,3 1 ug/1
(205-99-2)
88.Benzo(ghi) X X <5.3 1 ugh 1
Perylene(191-24-2)
9B.Benzo(k)
Fluoranthene X X <2.1 1 ug/1
(207-08-9)
10B.Bis(2-Chloro-
ethoxy)Methane X X <5.3 1 ug/1
(111-91-1)
11B.Bis(2-Chloro-
ethyl)Eflrer X X <4.2 1 ug/1
(111-44-4)
12B.Bis(2-
Chloroisopropyl) X X <5.3 1 ug/1
Ether(102-80-1)
13B.Bis(2-Ethyl-
` '
hezyl)Phthalate X X <5.3 1 ug/1
(117-81-7)
14B.4-Bromophenyl
Phenyl Ether X X <5.3 1 ug/1
(101-55-3)
15B.Butyl Benzyl X X <5.3 1 ug/1
Phthalate(85-68-7)
16B.2-Chloro-
naphthalene X X <2.1 1 ugh 1
(91-58-7)
17B.4-Chloro-
phenyl Phenyl Ether X X <5 3 1 ug/1
(7005-72-3)
18B.Chrysene X X <5 3 1 ug/1
(218-01-9)
19B.Dibenzo(a,h)
Anthracene X X <5.3 1 ug/1
(53-70-3)
20B.1,2 Dichloro- X X <5.3 1 ug/1
benzene(95-50-1)
21B.1,3-DI-chloro- X X�/ <5 3 1 ug/1
benzene(541-73-1)
EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2.MARK"X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (ifavailable) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
(1) (1) (1) ANALYSES TRATION b.MASS (1) ANALYSES
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS(continued)
beB.nzene(106-46- X
X <5.3 1 ug/1
23Bben dine3,3-(91-94- X X <10.5 1 ug/1
benzidine(91-94-1)
24B.Diethyl X X <5.3 1 ug/1
Phthalate(84-66-2)
25B.Phthalate
lte Dimethyl -
Phthalate X <5.3 1 ug/1
(131-11-3) `,
26B.Di-N-Butyl X <5.3 1 ug/1
Phthalate(84-74-2) ,,`
27B.2,4-Dinitro- X <z 1 1 ug/1
toluene(121-14-2) `//`
28B.2,6-Dinitro- 7� <4.2 1 ug/1
toluene(606-20-2)
29B.Di-e P (117-
Phthalate 117-84-0) X X <5.3 1 ug/1
P
30B. (as Azo
as Azo <5.3 1 ugh 1
benzene)(122-66-7)
31B.FIuoranthene v X <5 3 1 ug/1
(206-44-0) ^ `/`,
32B.Fluorene X <5.3 1 ug/1
(86-73-7) `, `,
33B.Hexachloro- X <1.1 1 ug/1
benzene(118-74-1)
34B.Hexachloro-
v
butadiene(87-68-3) ^ <2.1 1 ugh 1
35Bcyd He tadiene _ I
cyGopentadiene X <5.3 1 ug/1
(77-47-4) ` ,
36B Hexachloro- X <5.3 1 ug/1
ethane(67-72-1)
(1,2,3 cd)Pyrene X <5.3 1 ugh 1
(193-39-5) ` ,
38B.Isophorone X <5.3 1 ug/1
(78-59-1) ,,`
39B.Naphthalene X <5 3 1 ug/1
(91-20-3) ,` `/
408.Nitrobenzene v 7� <4 2 1 ugh
1
(98-95-3)
41B.N-Nitro-
sodimethylamine , ` ,
sadimethylamine x X <2.1 1 ug/1
(62-75-9)
42B.N-Nitrosodi-
N-Propylamine `,
X X <4 2 1 ug/1
(621-64-7)
EPA Form 3510-2C(8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND e. b. C. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- — (1) b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
43B.N soli
sodiphenenylalamine <5.3 1 ug/1
(86-30-6)44B ` ,
Phenanthrene X 7� <5.3 1 ug/1
(85-01-8)
45B.Pyrene
(129-00-0) X X <5.3 1 ug/1
46B.1,2,4111-
chlorobenzene X X <5.3 1 ug/1
(120-82-1)
GC/MS FRACTION—PESTICIDES
1 P.Aldrin X
(309-00-2)
2P.a-BHC X
(319-84-6)
3P.6-BHC X
(319-85-7)
4P.y-BHC �/
(58-89-9) X
5P.8-BHC �/
(319-86-8) X
6P.Chlordane X(57-74-9)
7P.4,4'-DDT X(50-29-3)
8P.4,4'-DDE X
(72-55-9)
9P.4,4'-DDD X
(72-54-8)
10P.Dieldrin X
(60-57-1)
11P.a-Enosulfan �/
(115-29-7) X .
12P.6-Endosulfan X
(115-29-7)
13P.Endosulfan X
Sulfate
(1031-07-8)
14P.Endrin �/
(72-20-8) X
15P. drin X
Aldehyde
(7421-93-4)
16P.Heptachlor �/
(76-44-8) X
EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
NC000771964 001
CONTINUED FROM PAGE V-8
2.MARK"X° 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—PESTICIDES(continued)
17P.Heptachlor ` ,
Epoxide X
(1024-57-3)
18P.PCB-1242 �/
(53469-21-9) /�
19P.PCB-1254
(11097-69-1) X
20P.PCB-1221
(11104-28-2) X
21P.PCB-1232 v
(11141-16-5)
22P.PCB-1248 �/
(12672-29-6) �\
23P.PCB-1260 v
(11096-82-5)
24P.PCB-1016 v
(12674-11-2)
25P.Toxaphene
(8001-35-2) X
EPA Form 3510-2C(8-90) PAGE V-9

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copy from Item 1 of Form 1) -
on separate sheets(use the same format)instead of completing these pages. NC000771964
SEE INSTRUCTIONS.
OUTFACE NO.
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C) 004
PART A-You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (specifyifblank) (optional)
b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
(1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
1.POLLUTANT CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Biochemical Oxygen <2 0 --- --- --- --- --- 1 mg/1
Demand(BOD) .
b.Chemical Oxygen <2 5 0 --- --- --- --- 1 mg/1
Demand(COD)
Do not Wish to
(c.TOC)alOrganicCarbon 5 7 __- --- 1 mg/1 apply for "net"
d.Total Suspended 6.3 >224 12 mg/1 lbs eligibility
Solids(TSS)
e.Ammonia(asN) <0.10 --- --- 1 mg/1
VALUE VALUE VALUE VALUE
f.Flow >4.254 --- 12 MGD
g.Temperature VALUE VALUE VALUE VALUE
12.3 "C
(winter)
h.Temperature VALUE VALUE VALUE VALUE
(summer) 25.4
°C
MINIMUM MAXIMUM MINIMUM MAXIMUM r y,y ,V
i.pH --- --- STANDARD UNITS /� / ji ;� y 1,0 ; ta'
,I,,.et x,au:« da xh:
PART B- Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either
directly,or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a,you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT f b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE I I a.LONG TERM AVERAGE
AND a b. a.MAXIMUM DAILY VALUE (if available) (if available) VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
([available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide
(24959-67-9)
b.Chlorine,Total
Residual NA
c.Color
d.Fecal Coliform
e.Fluoride
(16984-48-8)
f.Nitrate-Nitrite
(as N)
EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT •
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
AND a. b. a.MAXIMUM DAILY VALUE (If available) (if available) AVERAGE VALUE
CAS NO. BEUEVED BEUEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ifavaiiable) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen,
Total Organic(as
M
h.Oil and
Grease
i.Phosphorus
(as P),Total
(7723-14-0)
j.Radioactivity
(1)Alpha,Total
(2)Beta,Total NA
(3)Radium,
Total
(4)Radium 226,
Total
k.Sulfate •
(as SO,)
(14808-79-8)
I.Sulfide
(aS)
m.Sulfite
(as SOS)
(14265-45-3)
n.Surfactants
o.Aluminum,
Total
(7429-90-5)
p.Barium,Total
(7440-39-3)
q.Boron,Total
(7440-42-8)
r.Cobalt,Total
(7440r48-4)
s.Iron,Total
(7439-89-6)
t Magnesium,
Total
(7439-95-4)
u.Molybdenum,
Total
(7439-98-7)
v.Manganese,
Total
(7439-96-5)
w.Tin,Total
(7440-31-5)
x.Titanium,
Total
(7440-32-6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D.NUMBER(copyfrom Item 1 of Fonn 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC000771964 004
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark°X"in column 2a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2a(secondary industries,nonprocess wastewater outfalls,and nonrequired GC/MS
fractions),mark"X"in column 2-b for each pollutant you know or have reason to believe is present.Mark"X"in column 2-c for each pollutant you believe is absent.If you mark column 2a for any pollutant,you must
provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein,acrylonitrile,2,4 dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages)for each outfall.See instructions for
additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
([available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
METALS,CYANIDE,AND TOTAL PHENOLS
1 M.Antimony,Total
(7440-36-0)
2M.Arsenic,Total
(7440-38-2)
3M.Beryllium,Total
(7440-41-7)
4M.Cadmium,Total NA
(7440-43-9)
5M.Chromium,
Total(7440-47-3)
6M.Copper,Total
(7440-50-8)
7M.Lead,Total
(7439-92-1)
8M.Mercury,Total
(7439-97-6)
9M.Nickel,Total
(7440-02-0) •
10M.Selenium,
Total(7782-49-2)
11M.Silver,Total
(7440-22-4)
12M.Thallium,
Total(7440-28-0)
13M.Zinc,Total
(7440-66-6)
14M.Cyanide,
Total(57-12-5)
15M.Phenols,
Total
DIOXIN
2,3,7,8-Tetra- DESCRIBE RESULTS
chlorodibenzo-P-
Dioxin(1764-01-6) CONTINUE ON REVERSE
EPA Form 3510-2C(8-90) PAGE V-3

CONTINUED FROM THE FRONT •
2.MARK"X" 3.EFFLUENT • 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. o. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BEUEVED BEUEVED (1) (1) (1)
(1)
d.NO.OF a.CONCEN- b.NO.OF
0/available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS ,CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS
1 V.Accrolein
(107-02-8)
2V.Acrylonitrile
(107-13-1)
3V.Benzene
(71-43-2) NA
4V.Bis(Chloro-
methyl)Ether •
(542-88-1)
5V.Bromoform
(75-25-2)
6V.Carbon
Tetrachloride
(56-23-5)
7V.Chlorobenzene
(108-90-7)
8V.Chlorodi-
bromomethane
(124-48-1)
9V.Chloroethane
(75-00-3)
10V.2-Chloro-
ethylvinyl Ether
(110-75-8)
11V.Chloroform
(67-66-3)
12V.Dichloro-
bromornethane
(75-27-4)
13V.Dichloro-
difluoromethane
(75-71-8)
14V.1,1-Dichloro-
ethane(75-34-3)
15V.1,2-Dichloro-
ethane(107-06-2)
16V.1,1-Dichloro-
ethylene(75-35-4)
17V.1,2-Dichloro-
propane(78-87-5)
18V.1,3-Dichloro-
propylene
(542-75-6)
19V.Ethylbenzene
(100-41-4)
20V.Methyl
Bromide(74-83-9)
21V.Methyl
Chloride(74-87-3)
EPA Form 3510-2C(8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4 •
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. a a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
0/available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS(continued)
22V.Methylene
Chloride(75-09-2)
23V.1,1,2,2-
Tetrachloroethane
(79-34-5)
24V.Tetrachloro-
ethylene(127-18-4) NA
25V.Toluene
(108-88-3)
26V.1,2-Trans-
Dichloroethylene
(156-60-5)
27V.1,1,1-Trichloro-
ethane(71-55-6)
28V.1,1,2-Trichloro-
ethane(79-00-5)
29V Trichloro-
ethylene(79-01-6)
30V.Trichloro-
fluoromethane
(75-69-4)
31V.Vinyl Chloride
(75-01-4)
GC/MS FRACTION—ACID COMPOUNDS
1A.2-Chlorophenol
(95-57-8)
2A.2,4-Dichloro-
phenol(120-83-2)
3k 2,4-Dimethyl-
phenol(105-67-9)
4k 4,6-Dinitro-0-
Cresol(534-52-1)
5A.2,4-Dinitro-
phenol(51-28-5)
6k 2-Nitrophenol
(88-75-5)
7A.4-Nitrophenol
(100-02-7)
8A.P-Chloro-M-
Cresol(59-50-7)
9A.Pentachloro-
phenol(87-86-5)
10A.Phenol
(108-95-2)
11A.2,4,6-Trichloro-
phenol(88-05-2)
EPA Form 3510-2C(8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (ijavailable) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(favailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS
18.Acenaphthene
(83-32-9)
2B.Acenaphtylene
(208-96-8)
3B.Anthracene
(120-12-7)
4B.Benzidine NA
(92-87-5)
5B.Benzo(a)
Anthracene
(56-55-3)
6B.Benzo(a)
Pyrene(50-32-8)
7B.3,4-Benzo-
fluoranthene
(205-99-2)
8B.Benzo(ghi)
Perylene(191-24-2)
9B.Benzo(k)
Fluoranthene
(207-08-9)
10B.Bis(2-Chloro-
ethoxy)Methane
(111-91-1)
11B.Bis(2-Chloro-
ethyl)Ether
(111-44-4)
12B.Bis(2-
Chlorolcopropyl)
Ether(102-80-1)
13B.Bis(2-Ethyl-
beryl)Phthalate
(117-81-7)
14B.4-Bromophenyl
Phenyl Ether
(101-55-3)
15B.Butyl Benzyl
Phthalate(85-68-7)
16B.2-Chloro-
naphthalene
(91-58-7)
17B.4-Chloro-
phenyl Phenyl Ether
(7005-72-3)
18B.Chrysene
(218-01-9)
19B.Dibenzo(qh)
Anthracene
(53-70-3)
20B.1,2-Dichloro-
benzene(95-50-1)
21B.1,3-Di-chloro-
benzene(541-73-1)
EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2.MARK"X° 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
22B.1,4-Didiloro-
benzene(106-46-7)
23B.3,3-Dichloro-
benzidine(91-94-1)
24B.Diethyl
Phthalate(84-66-2)
25B.Dimethyl
Phthalate
(131-11-3)
26B.Di-N-Butyl NA
Phthalate(84-74-2)
27B.2,4-Dinitro-
toluene(121-14-2)
28B.2,6-Dinitro-
toluene(606-20-2)
29B.Di-N-Octyi
Phthalate(117-84-0)
30B.1,2-Diphenyl-
hydrazine(as Azo-
benzene)(122-66-7)
31B.Fluoranthene
(206-44-0)
32B.Fluorene
(86-73-7)
33B.Hexachloro-
benzene(118-74-1)
34B.Hexachloro-
butadiene(87-68-3)
35B.Hexachloro-
cyclopentadiene
(77-47-4)
36B Hexachloro-
ethane(67-72-1)
37B.Indeno
(1,2,3-cd)Pyrene
(193-39-5)
38B.Isophorone
(78-59-1)
39B.Naphthalene
(91-20-3)
40B.Nitrobenzene
(98-95-3)
41B.N-Nitro-
sodimethylamine
(62-75-9)
42B.N-Nitrosodi-
N-Propylamine
(621-64-7)
EPA Form 3510-2C(8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT •
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BEUEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(favailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
43B.N-Nitro-
sodiphenylamine
(86-30-6)
44B.Phenanthrene
(85-01-8)
45B.Pyrene
(129-00-0)
46B.1,2,4-Tri-
chlorobenzene
(120-82-1)
GC/MS FRACTION—PESTICIDES
1P.Aldrin
(309-00-2)
2P.a-BHC
(319-84-6) NA
3P.11-BHC
(319-85-7)
4P.y-BHC
(58-89-9)
5P.6-BHC
(319-86-8)
6P.Chlordane
(57-74-9)
7P.4,4'-DDT
(50-29-3)
8P.4,4'-DDE
(72-55-9)
9P.4,4'-DDD
(72-54-8)
10P.Dieldrin
(60-57-1)
11 P.a-Enosulfan
(115-29-7)
12P.fI-Endosulfan
(115-29-7)
13P.Endosulfan
Sulfate
(1031-07-8)
14P.Endrin
(72-20-8)
15P.Endrin
Aldehyde
(7421-93-4)
16P.Heptachlor
(76-44-8)
EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9

•
EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
NC000771964 004
CONTINUED FROM PAGE V-8
2.MARK"X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE favailable) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ijavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—PESTICIDES(continued)
17P.Heptachlor
Epoxide
(1024-57-3) NA
18P.PCB-1242
(53469-21-9)
19P.PCB-1254
(11097-69-1)
20P.PCB-1221
(11104-28-2)
21P.PCB-1232
(11141-16-5)
22P.PCB-1248
(12672-29-6)
23P.PCB-1260
(11096-82-5)
24P.PCB-1016
(12674-11-2)
25P.Toxaphene
(8001-35-2)
EPA Form 3510-2C(8-90) PAGE V-9

® Pace Analytical Services,Inc. Pace Analytical Services,Inc.
ace/InalyticaI 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wawpacelabscom Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
February 19, 2010
Mr. Rodney Willis
FMC Corporation-Lithium Division
Hwy 161
PO Box 795
Bessemer City, NC 28016
RE: Project: NPDES- RENEW
Pace Project No.: 9261607
Dear Mr. Willis:
Enclosed are the analytical results for sample(s) received by the laboratory on January 20, 2010.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted.All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
M wac�
Erin Waters
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS Page 1 of 41
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[phone] [phone]
CERTIFICATIONS
Project: NPDES-RENEW
Pace Project No.: 9261607
Pennsylvania Certification IDs
1638 Roseytown Road Suites 2,3&4 Greensburg,PA Massachusetts Certification#:M-PA1457
15601 Maryland Certification#:308
Alabama Certification#:41590 Maine Certification#:PA0091
Wisconsin/PADEP Certification Louisiana/NELAC Certification#:LA080002
West Virginia Certification#:143 Louisiana/NELAC Certification#:4086
Washington Certification#:C1941 Kentucky Certification#:90133
Virginia Certification#:00112 Kansas/NELAC Certification#:E-10358
Virgin Island/PADEP Certification Iowa Certification#:391
Utah/NELAC Certification#:ANTE Indiana/PADEP Certification
Texas/NELAC Certification#:T104704188-09 TX Illinois/PADEP Certification
Tennessee Certification#:TN2867 Idaho Certification
South Dakota Certification Hawaii/PADEP Certification
Puerto Rico Certification#:PA01457 Guam/PADEP Certification
Pennsylvania/NELAC Certification#:65-282 Georgia Certification#:968
Oregon/NELAC Certification#:PA200002 Florida/NELAC Certification#:E87683
North Carolina Certification#:42706 Delaware Certification
New York/NELAC Certification#:10888 Connecticut Certification#:PH 0694
New Mexico Certification Colorado Certification
New Jersey/NELAC Certification#:PA 051 Califomia/NELAC Certification#:04222CA
New Hampshire/NELAC Certification#:2976 Arkansas Certification
Nevada Certification Arizona Certification#:AZ0734
Montana Certification#:Cert 0082 Wyoming Certification#:8TMS-Q
Missouri Certification#:235
Michigan/PADEP Certification
Ormond Beach Certification IDs
8 East Tower Circle Ormond Beach,FL 32174 Michigan Certification#:9911
Wyoming Certification:FL NELAC Reciprocity Massachusetts Certification#:M-FL1264
Virginia Certification#:00432 Maine Certification#:FL1264
Texas Certification:FL NELAC Reciprocity Louisiana Certification#:LA090012
Tennessee Certification#:TN02974 Kentucky Certification#:90050
Puerto Rico Certification#:FL01264 Kansas Certification#:E-10383
Pennsylvania Certification#:68-547 Hawaii Certification:FL NELAC Reciprocity
North Carolina Certification#:12710 Guam Certification:FL NELAC Reciprocity
New York Certification#:11608 Georgia Certification#:955
New Jersey Certification#:FL765 Florida Certification#:E83079
New Hampshire Certification#:2958 Connecticut Certification#:PH 0216
Nevada Certification:FL NELAC Reciprocity Colorado Certification:FL NELAC Reciprocity
Montana Certification#:Cert 0074 Arizona Certification#:AZ0735
Mississippi Certification:FL NELAC Reciprocity Alabama Certification#:41320
Charlotte Certification IDs
9800 Kincey Ave.-Ste 100 Huntersville,NC 28078 North Carolina Field Services Certification#:5342
West Virginia Certification#:357 North Carolina Wastewater Certification#:12
Connecticut Certification#:PH-0104 Pennsylvania Certification#:68-00784
Florida/NELAP Certification#:E87627 South Carolina Certification#:990060001
Kentucky UST Certification#:84 South Carolina Drinking Water Cert.#:990060003
Louisiana/LELAP Certification#:04034 Tennessee Certification#:04010
New Jersey Certification#:NC012 Virginia Certification#:00213
North Carolina Drinking Water Certification#:37706
Asheville Certification IDs
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
Louisiana/LELAP Certification#:03095 Tennessee Certification#:2980
New Jersey Certification#:NC011 Virginia Certification#:00072
North Carolina Bioassay Certification#:9 West Virginia Certification#:356
North Carolina Drinking Water Certification#:37712 2225 Riverside Dr.Asheville,NC 28804
North Carolina Wastewater Certification#:40 Connecticut Certification#:PH-0106
Pennsylvania Certification#:68-03578 Massachusetts Certification#:M-NC030
South Carolina Bioassay Certification#:99030002
REPORT OF LABORATORY ANALYSIS Page 2 of 41
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ce alytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Pactl Asheville,NC 28804 Huntersville,NC 28078
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SAMPLE ANALYTE COUNT
Project: NPDES-RENEW
Pace Project No.: 9261607
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
9261607001 001-NPDES Orion Electrode SDH 1 PASI-A
EPA 1664A CLW 1 PASI-C
EPA 200.7 EWS 22 PASI-A
SM 9222D KDF 1 PASI-C
EPA 245.1 JMW 1 PASI-A
EPA 625 EAO 64 PASI-O
EPA 624 DLK 35 PASI-C
EPA 900.0m JC2 2 PASI-PA
EPA 903.1 RMD 1 PASI-PA
EPA 904.0 MBT 1 PASI-PA
SM 2540D LEP 1 PASI-A
SM 4500F/C TEE 1 PASI-A
SM 4500-S2D TEE 1 PASI-A
SM 5210B SAJ 1 PASI-A
TKN-NH3 Calculation WWB 1 PASI-A
EPA 300.0 HEM 1 PASI-O
EPA 350.1 SHB 1 PASI-A
EPA351.2 SHB 1 PASI-A
EPA 353.2 DMN 3 PASI-A
EPA 365.1 JDA 1 PASI-A
EPA420.4 JDA 1 PASI-A
SM 4500-CN-E JDA 1 PASI-A
SM 5220D LEP 1 PASI-A
SM 5310B RAB 1 PASI-A
ASTM D516-90 SHB 1 PASI-A
9261607002 004-NPDES SM 2540D LEP 1 PASI-A
SM 5210B SAJ 1 PASI-A
EPA 350.1 SHB 1 PASI-A
SM 5220D LEP 1 PASI-A
SM 5310B RAB 1 PASI-A
REPORT OF LABORATORY ANALYSIS Page 3 of 41
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[phone] [phone]
ANALYTICAL RESULTS
DO
Project: NPDES-RENEW .-------
Pace Pro'--. , -• • 9261607
Sample, 001-NPDES Lab ID: 9261607001 Collected: 01/20/10 09:55 Received: 01/20/10 12:38 Matrix:Water
-arameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Total Res CI,Orion Electrode Analytical Method:Orion Electrode
Chlorine,Total Residual ND mg/L 0.10 1 01/29/10 14:08 7782-50-5 H1,H6
HEM,Oil and Grease Analytical Method:EPA 1664A
Oil and Grease ND mg/L 5.0 1 01/21/10 09:28
200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA 200.7
Aluminum ND ug/L 100 1 01/22/10 15:22 01/27/10 04:09 7429-90-5
Antimony ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-36-0
Arsenic ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-38-2
Barium 31.8 ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-39-3
Beryllium ND ug/L 1.0 1 01/22/10 15:22 01/27/10 04:09 7440-41-7
Boron 79.8 ug/L 50.0 1 01/22/10 15:22 01/27/10 04:09 7440-42-8
Cadmium ND ug/L 1.0 1 01/22/10 15:22 01/27/10 04:09 7440-43-9
Chromium ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-47-3
Cobalt ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-48-4
Copper ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-50-8
Iron ND ug/L 50.0 1 01/22/10 15:22 01/27/10 04:09 7439-89-6
Lead ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7439-92-1
Magnesium 36600 ug/L 100 1 01/22/10 15:22 01/27/10 04:09 7439-95-4
Manganese 59.1 ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7439-96-5
Molybdenum ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7439-98-7
Nickel ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-02-0
Selenium ND ug/L 10.0 1 01/22/10 15:22 01/27/10 04:09 7782-49-2
Silver ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-22-4
Thallium ND ug/L 10.0 1 01/22/10 15:22 01/27/10 04:09 7440-28-0
Tin ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-31-5
Titanium ND ug/L 5.0 1 01/22/10 15:22 01/27/10 04:09 7440-32-6
Zinc ND ug/L 10.0 1 01/22/10 15:22 01/27/10 04:09 7440-66-6
MBIO 9222D Fecal Coliform CHT Analytical Method:SM 9222D
Fecal Coliforms ND CFU/100 mL 1.0 1 01/20/10 13:30
245.1 Mercury Analytical Method:EPA 245.1 Preparation Method:EPA 245.1
Mercury ND ug/L 0.20 1 01/21/10 12:30 01/22/10 14:11 7439-97-6
625 MSSV Analytical Method:EPA 625
1,2,4-Trichlorobenzene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 120-82-1
1,2-Diphenylhydrazine ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 122-66-7
2,4,6-Trichlorophenol ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 88-06-2
2,4-Dichlorophenol ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 120-83-2
2,4-Dimethylphenol ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 105-67-9
2,4-Dinitrophenol ND ug/L 14.7 1 01/22/10 18:40 01/28/10 14:28 51-28-5
2,4-Dinitrotoluene ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 121-14-2
2,6-Dinitrotoluene ND ug/L 4.2 1 01/22/10 18:40 01/28/10 14:28 606-20-2
2-Chloronaphthalene ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 91-58-7
2-Chlorophenol ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 95-57-8
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 4 of 41
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without the written consent of Pace Analytical Services,Inc..

/ /9 Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalyfical. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
` Asheville,NC 28804 Huntersville,NC 28078
t [phone] [phone]
ANALYTICAL RESULTS CO I
Project: NPDES-RENEW
Pace Proje .: 9261607
Sample: 001-NPDES Lab ID: 9261607001 Collected: 01/20/10 09:55 Received: 01/20/10 12:38 Matrix:Water
-arameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625
2-Methylphenol(o-Cresol) ND ug/L 4.2 1 01/22/10 18:40 01/28/10 14:28 95-48-7
2-Nitrophenol ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 88-75-5
3,3'-Dichlorobenzidine ND ug/L 10.5 1 01/22/10 18:40 01/28/10 14:28 91-94-1
3&4-Methylphenol(m&p Cresol) ND ug/L 4.2 1 01/22/10 18:40 01/28/10 14:28
4,6-Dinitro-2-methylphenol ND ug/L 21.1 1 01/22/10 18:40 01/28/10 14:28 534-52-1
4-Bromophenylphenyl ether ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 101-55-3
4-Chloro-3-methylphenol ND ug/L 21.1 1 01/22/10 18:40 01/28/10 14:28 59-50-7
4-Chlorophenylphenyl ether ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 7005-72-3
4-Nitrophenol ND ug/L 21.1 1 01/22/10 18:40 01/28/10 14:28 100-02-7
Acenaphthylene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 208-96-8
Anthracene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 120-12-7
Butylbenzylphthalate ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 85-68-7
Benzo(k)fluoranthene ND ug/L 4.2 1 01/22/10 18:40 01/28/10 14:28 207-08-9
Benzo(g,h,i)perylene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 191-24-2
Benzo(a)anthracene ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 56-55-3
Benzidine ND ug/L 26.3 1 01/22/10 18:40 01/28/10 14:28 92-87-5
Benzo(b)fluoranthene ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 205-99-2
Benzo(a)pyrene ND ug/L 1.1 1 01/22/10 18:40 01/28/10 14:28 50-32-8
bis(2-Chloroethoxy)methane ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 111-91-1
bis(2-Chloroethyl)ether ND ug/L 4.2 1 01/22/10 18:40 01/28/10 14:28 111-44-4
bis(2-Chloroisopropyl)ether ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 108-60-1
bis(2-Ethylhexyl)phthalate ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 117-81-7
Chrysene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 218-01-9
Dibenz(a,h)anthracene ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 53-70-3
Dimethylphthalate ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 131-11-3
Di-n-butylphthalate ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 84-74-2
Di-n-octylphthalate ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 117-84-0
Diethylphthalate ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 84-66-2
Fluorene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 86-73-7
Fluoranthene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 206-44-0
Hexachloro-1,3-butadiene ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 87-68-3
Hexachlorobenzene ND ug/L 1.1 1 01/22/10 18:40 01/28/10 14:28 118-74-1
Hexachlorocyclopentadiene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 77-47-4
Hexachloroethane ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 193-39-5
Isophorone ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 78-59-1
Naphthalene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 91-20-3
N-Nitroso-di-n-propylamine ND ug/L 4.2 1 01/22/10 18:40 01/28/10 14:28 621-64-7
Nitrobenzene ND ug/L 4.2 1 01/22/10 18:40 01/28/10 14:28 98-95-3
N-Nitrosodimethylamine ND ug/L 2.1 1 01/22/10 18:40 01/28/10 14:28 62-75-9
N-Nitrosodiphenylamine ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 86-30-6
Phenol ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 108-95-2
Phenanthrene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 85-01-8
Pentachlorophenol ND ug/L 21.1 1 01/22/10 18:40 01/28/10 14:28 87-86-5
Pyrene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 129-00-0
1,2-Dichlorobenzene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 95-50-1
1,3-Dichlorobenzene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 541-73-1
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 5 of 41
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without the written consent of Pace Analytical Services,Inc..
t N ACCOBOB
iii0

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aceAnalytical 2225 Riverside Dr. 9800 Kinsey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
ANALYTICAL RESULTS ©n I
Project: NPDES-RENEW
Pace Pro61607
Sample: 001-NPDES Lab ID: 9261607001 Collected: 01/20/10 09:55 Received: 01/20/10 12:38 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625
1,4-Dichlorobenzene ND ug/L 5.3 1 01/22/10 18:40 01/28/10 14:28 106-46-7
Nitrobenzene-d5(S) 83 % 37.3-107.7 1 01/22/10 18:40 01/28/10 14:28 4165-60-0
2-Fluorobiphenyl(S) 74 % 35.3-102.4 1 01/22/10 18:40 01/28/10 14:28 321-60-8
Terphenyl-d14(S) 86 % 50.1-115.1 1 01/22/10 18:40 01/28/10 14:28 1718-51-0
Phenol-d6(S) 27 % 10-47.1 1 01/22/10 18:40 01/28/10 14:28 13127-88-3
2-Fluorophenol(S) 41 % 16.3-59.8 1 01/22/10 18:40 01/28/10 14:28 367-12-4
2,4,6-Tribromophenol(S) 78 % 54.2-114.4 1 01/22/10 18:40 01/28/10 14:28 118-79-6
624 Volatile Organics Analytical Method:EPA 624
Acrolein ND ug/L 100 1 01/24/10 10:43 107-02-8
Acrylonitrile ND ug/L 100 1 01/24/10 10:43 107-13-1
Benzene ND ug/L 5.0 1 01/24/10 10:43 71-43-2
Bromodichloromethane ND ug/L 5.0 1 01/24/10 10:43 75-27-4
Bromoform ND ug/L 5.0 1 01/24/10 10:43 75-25-2
Bromomethane ND ug/L 10.0 1 01/24/10 10:43 74-83-9
Carbon tetrachloride ND ug/L 5.0 1 01/24/10 10:43 56-23-5
Chiorobenzene ND ug/L 5.0 1 01/24/10 10:43 108-90-7
Chloroethane ND ug/L 10.0 1 01/24/10 10:43 75-00-3
2-Chloroethylvinyl ether ND ug/L 10.0 1 01/24/10 10:43 110-75-8
Chloroform ND ug/L 5.0 1 01/24/10 10:43 67-66-3
Chloromethane ND ug/L 5.0 1 01/24/10 10:43 74-87-3
Dibromochloromethane ND ug/L 5.0 1 01/24/10 10:43 124-48-1
Dichlorodifluoromethane ND ug/L 5.0 1 01/24/10 10:43 75-71-8
1,1-Dichloroethane ND ug/L 5.0 1 01/24/10 10:43 75-34-3
1,2-Dichloroethane ND ug/L 5.0 1 01/24/10 10:43 107-06-2
1,1-Dichloroethene ND ug/L 5.0 1 01/24/10 10:43 75-35-4
trans-1,2-Dichloroethene ND ug/L 5.0 1 01/24/10 10:43 156-60-5
1,2-Dichloropropane ND ug/L 5.0 1 01/24/10 10:43 78-87-5
cis-1,3-Dichloropropene ND ug/L 5.0 1 01/24/10 10:43 10061-01-5
trans-1,3-Dichloropropene ND ug/L 5.0 1 01/24/10 10:43 10061-02-6
Ethylbenzene ND ug/L 5.0 1 01/24/10 10:43 100-41-4
Methylene Chloride ND ug/L 5.0 1 01/24/10 10:43 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 5.0 1 01/24/10 10:43 79-34-5
Tetrachloroethene ND ug/L 5.0 1 01/24/10 10:43 127-18-4
Toluene ND ug/L 5.0 1 01/24/10 10:43 108-88-3
1,1,1-Trichloroethane ND ug/L 5.0 1 01/24/10 10:43 71-55-6
1,1,2-Trichloroethane ND ug/L 5.0 1 01/24/10 10:43 79-00-5
Trichloroethene ND ug/L 5.0 1 01/24/10 10:43 79-01-6
Trichlorofluoromethane ND ug/L 10.0 1 01/24/10 10:43 75-69-4
Vinyl chloride ND ug/L 5.0 1 01/24/10 10:43 75-01-4
Dibromofluoromethane(S) 98 % 88-113 1 01/24/10 10:43 1868-53-7
4-Bromofluorobenzene(S) 107 % 86-111 1 01/24/10 10:43 460-00-4
Toluene-d8(S) 98 % 92-105 1 01/24/10 10:43 2037-26-5
1,2-Dichloroethane-d4(S) 94 % 70-130 1 01/24/10 10:43 17060-07-0
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 6 of 41
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without the written consent of Pace Analytical Services,Inc..
�i�r Glt71L..11

. (
Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAna/ iCat 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: NPDES-RENEW 00
Pace Proj t • 9261607 -�
Sample: 001-NPDES Lab ID: 9261607001 Collected: 01/20/10 09:55 Received: 01/20/10 12:38 Matrix:Water
meters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method:SM 2540D
Total Suspended Solids ND mg/L 8.3 1 01/22/10 16:06
4500FC Fluoride Analytical Method:SM 4500F/C
Fluoride 0.51 mg/L 0.10 1 01/26/10 18:51 16984-48-8
4500S2D Sulfide Water Analytical Method:SM 4500-S2D
Sulfide ND mg/L 0.10 1 01/22/10 17:00
5210B BOD,5 day Analytical Method:SM 5210B
BOD,5 day ND mg/L 2.0 1 01/21/10 15:28 01/26/10 09:09
Total Organic Nitrogen Calc. Analytical Method:TKN-NH3 Calculation
Total Organic Nitrogen 1.1 mg/L 0.50 1 02/09/10 15:57
300.0 IC Anions 28 Days Analytical Method:EPA 300.0
Bromide 0.80 mg/L 0.20 2 01/25/10 19:58 24959-67-9
350.1 Ammonia Analytical Method:EPA 350.1
Nitrogen,Ammonia ND mg/L 0.10 1 01/28/10 13:43 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2
Nitrogen,Kjeldahl,Total 1.1 mg/L 0.50 1 02/08/10 10:38 7727-37-9
353.2 Nitrogen,NO2/NO3 unpres Analytical Method:EPA 353.2
Nitrogen,Nitrate ND mg/L 0.10 1 01/21/10 21:50
Nitrogen,Nitrite ND mg/L 0.10 1 01/21/10 21:50
Nitrogen,NO2 plus NO3 ND mg/L 0.10 1 01/21/10 21:50
365.1 Phosphorus,Total Analytical Method:EPA 365.1
Phosphorus ND mg/L 0.10 1 01/26/10 15:58 7723-14-0
420.4 Phenolics,Total Analytical Method:EPA 420.4
Phenol ND mg/L 0.010 1 01/25/10 14:26 108-95-2
4500CNE Cyanide,Total Analytical Method:SM 4500-CN-E
Cyanide ND mg/L 0.0050 1 01/26/10 17:52 57-12-5
5220D COD Analytical Method:SM 5220D
Chemical Oxygen Demand ND mg/L 25.0 1 01/29/10 11:20
5310E TOC Analytical Method:SM 5310B
Total Organic Carbon 5.9 mg/L 1.0 1 01/21/10 22:30 7440-44-0
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 7 of 41
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aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: NPDES-RENEW
Pace Project No.: 9261607
Sample: 01- PDES Lab ID: 9261607001 Collected: 01/20/10 09:55 Received: 01/20/10 12:38 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
ASTM D516-90 Sulfate Water Analytical Method:ASTM D516-90 00 (—
Sulfate 297 mg/L 100 20 01/26/10 13:24 14808-79-8
Sample 004- DES Lab ID: 9261607002 Collected: 01/20/10 10:12 Received: 01/20/10 12:38 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method:SM 2540D 00 4—
Total Suspended Solids ND mg/L 8.3 1 01/22/10 16:07
5210B BOD,5 day Analytical Method:SM 5210B
BOD,5 day ND mg/L 2.0 1 01/21/10 15:28 01/26/10 09:09
350.1 Ammonia Analytical Method:EPA 350.1
Nitrogen,Ammonia ND mg/L 0.10 1 01/28/10 13:45 7664-41-7
5220D COD Analytical Method:SM 5220D
Chemical Oxygen Demand ND mg/L 25.0 1 01/29/10 11:20
5310E TOC Analytical Method:SM 5310B
Total Organic Carbon 5.7 mg/L 1.0 1 01/21/10 22:30 7440-44-0
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 8 of 41
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' (' 1 wwwpacelabs.com
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607 •
QC Batch: BIO/1678 Analysis Method: Orion Electrode
QC Batch Method: Orion Electrode Analysis Description: Total Res CI,Orion Electrode
Associated Lab Samples: 9261607001
METHOD BLANK: 395889 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine,Total Residual mg/L ND 0.10 01/29/10 14:06 H6
LABORATORY CONTROL SAMPLE: 395890
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chlorine,Total Residual mg/L 0.45 H6
SAMPLE DUPLICATE: 395891
9261607001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine,Total Residual mg/L ND ND H6
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 9 of 41
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aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwparxfaGscarrt Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: GCSV/7042 Analysis Method: EPA 1664A
QC Batch Method: EPA 1664A Analysis Description: 1664 HEM,Oil and Grease
Associated Lab Samples: 9261607001
METHOD BLANK: 392949 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 01/21/10 09:24
LABORATORY CONTROL SAMPLE: 392950
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 38.7 97 78-114
MATRIX SPIKE SAMPLE: 392951
9261586005 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 13.0 40 45.1 80 78-114
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 10 of 41
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aceAnaly�ieal 2225 Riverside 04 9800 Kincey Ave. Suite nc.
wwwpaceittecom
Asheville,NC 288 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: MPRP/5722 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9261607001
METHOD BLANK: 393571 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Aluminum ug/L ND 100 01/27/10 02:08
Antimony ug/L ND 5.0 01/27/10 02:08
Arsenic ug/L ND 5.0 01/27/10 02:08
Barium ug/L ND 5.0 01/27/10 02:08
Beryllium ug/L ND 1.0 01/27/10 02:08
Boron ug/L ND 50.0 01/27/10 02:08
Cadmium ug/L ND 1.0 01/27/10 02:08
Chromium ug/L ND 5.0 01/27/10 02:08
Cobalt ug/L ND 5.0 01/27/10 02:08
Copper ug/L ND 5.0 01/27/10 02:08
Iron ug/L ND 50.0 01/27/10 02:08
Lead ug/L ND 5.0 01/27/10 02:08
Magnesium ug/L ND 100 01/27/10 02:08
Manganese ug/L ND 5.0 01/27/10 02:08
Molybdenum ug/L ND 5.0 01/27/10 02:08
Nickel ug/L ND 5.0 01/27/10 02:08
Selenium ug/L ND 10.0 01/27/10 02:08
Silver ug/L ND 5.0 01/27/10 02:08
Thallium ug/L ND 10.0 01/27/10 02:08
Tin ug/L ND 5.0 01/27/10 02:08
Titanium ug/L ND 5.0 01/27/10 02:08
Zinc ug/L ND 10.0 01/27/10 02:08
LABORATORY CONTROL SAMPLE: 393572
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Aluminum ug/L 5000 4660 93 85-115
Antimony ug/L 500 479 96 85-115
Arsenic ug/L 500 456 91 85-115
Barium ug/L 500 449 90 85-115
Beryllium ug/L 500 474 95 85-115
Boron ug/L 500 501 100 85-115
Cadmium ug/L 500 449 90 85-115
Chromium ug/L 500 461 92 85-115
Cobalt ug/L 500 458 92 85-115
Copper ug/L 500 458 92 85-115
Iron ug/L 5000 4710 94 85-115
Lead ug/L 500 456 91 85-115
Magnesium ug/L 5000 4610 92 85-115
Manganese ug/L 500 453 91 85-115
Molybdenum ug/L 500 477 95 85-115
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 11 of 41
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aeeAnalytiGalwiwowiabs.com 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
1 [phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
LABORATORY CONTROL SAMPLE: 393572
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nickel ug/L 500 457 91 85-115
Selenium ug/L 500 449 90 85-115
Silver ug/L 250 232 93 85-115
Thallium ug/L 500 437 87 85-115
Tin ug/L 500 469 94 85-115
Titanium ug/L 500 471 94 85-115
Zinc ug/L 500 451 90 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 393573 393574
MS MSD
9261771001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Aluminum ug/L 0.28 5000 5000 5370 5600 102 106 70-130 4
mg/L
Antimony ug/L ND 500 500 508 531 102 106 70-130 4
Arsenic ug/L ND 500 500 491 516 98 103 70-130 5
Barium ug/L 0.038 500 500 486 506 90 94 70-130 4
mg/L
Beryllium ug/L ND 500 500 497 520 99 104 70-130 5
Boron ug/L 0.059 500 500 556 580 99 104 70-130 4
mg/L
Cadmium ug/L 0.0020 500 500 460 480 92 96 70-130 4
mg/L
Chromium ug/L ND 500 500 474 494 95 99 70-130 4
Cobalt ug/L ND 500 500 464 484 93 97 70-130 4
Copper ug/L 0.039 500 500 525 546 97 101 70-130 4
mg/L
Iron ug/L 0.48 5000 5000 5190 5400 94 98 70-130 4
mg/L
Lead ug/L 0.0052 500 500 459 480 91 95 70-130 4
mg/L
Magnesium ug/L 9.0 5000 5000 13800 14300 96 105 70-130 3
mg/L
Manganese ug/L 0.039 500 500 497 514 92 95 70-130 3
mg/L
Molybdenum ug/L ND 500 500 497 520 99 104 70-130 5
Nickel ug/L 0.0098 500 500 469 488 92 96 70-130 4
mg/L
Selenium ug/L ND 500 500 479 500 96 100 70-130 4
Silver ug/L ND 250 250 242 252 96 100 70-130 4
Thallium ug/L ND 500 500 428 446 85 88 70-130 4
Tin ug/L ND 500 500 486 501 96 99 70-130 3
Titanium ug/L 0.0056 500 500 480 501 95 99 70-130 4
mg/L
Zinc ug/L 0.23 500 500 710 730 96 100 70-130 3
mg/L
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 12 of 41
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® Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalyfical 2225 Riverside Dr. 9800 KinceyAve. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
www.pacelabs.caa
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
SAMPLE DUPLICATE: 393575
9261536005 Dup
Parameter Units Result Result RPD Qualifiers
Aluminum ug/L 4620 4700 2
Antimony ug/L 9.3 9.0 3
Arsenic ug/L ND 4.1J
Barium ug/L 71.0 72.9 3
Beryllium ug/L ND ND
Boron ug/L 6600 6790 3
Cadmium ug/L ND ND
Chromium ug/L 271 279 . 3
Cobalt ug/L 24.6 24.9 1
Copper ug/L 146 171 16
Iron ug/L 22200 22600 2
Lead ug/L 61.5 68.5 11
Magnesium ug/L 4330 4410 2
Manganese ug/L 226 232 3
Molybdenum ug/L ND 2.1J
Nickel ug/L 256 264 3
Selenium ug/L ND ND
Silver ug/L 233 230 1
Thallium ug/L ND ND
Tin ug/L 7.2 6.3 14
Titanium ug/L 14.0 14.5 4
Zinc ug/L 856 880 3
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 13 of 41
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aceAnalytical 2225 Riverside Dr. 9800 KlnceyAve. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
iniwinatiab&con [phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: MBCH/2707 Analysis Method: SM 9222D
QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform-CHT
Associated Lab Samples: 9261607001
METHOD BLANK: 393071 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 01/20/10 13:30
SAMPLE DUPLICATE: 393072
9261607001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU/100 mL ND ND
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 14 of 41
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(/# aceA nalyticaiI 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
tali pia` Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: MERP/2618 Analysis Method: EPA 245.1
QC Batch Method: EPA 245.1 Analysis Description: 245.1 Mercury
Associated Lab Samples: 9261607001
METHOD BLANK: 392940 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 01/22/10 13:08
LABORATORY CONTROL SAMPLE: 392941
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 103 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 392942 392943
MS MSD
9261661008 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.6 2.6 102 102 70-130 0
SAMPLE DUPLICATE: 392944
9261661009 Dup
Parameter Units Result Result RPD Qualifiers
Mercury ug/L ND ND
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 15 of 41
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a/+p Q►}ali/+�) 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
VV4I u� eVG�1: Asheville,NC 28804 Huntersville,NC 28078
vwdwpacel [phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: MSSV/1678 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 9261607001
METHOD BLANK: 35783 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene ug/L ND 5.0 01/22/10 09:43
1,2-Dichlorobenzene ug/L ND 5.0 01/22/10 09:43
1,2-Diphenylhydrazine ug/L ND 5.0 01/22/10 09:43
1,3-Dichlorobenzene ug/L ND 5.0 01/22/10 09:43
1,4-Dichlorobenzene ug/L ND 5.0 01/22/10 09:43
2,4,6-Trichlorophenol ug/L ND 2.0 01/22/10 09:43
2,4-Dichlorophenol ug/L ND 2.0 01/22/10 09:43
2,4-Dimethyiphenol ug/L ND 5.0 01/22/10 09:43
2,4-Dinitrophenol ug/L ND 14.0 01/22/10 09:43
2,4-Dinitrotoluene ug/L ND 2.0 01/22/10 09:43
2,6-Dinitrotoluene ug/L ND 4.0 01/22/10 09:43
2-Chloronaphthalene ug/L ND 2.0 01/22/10 09:43
2-Chlorophenol ug/L ND 5.0 01/22/10 09:43
2-Methylphenol(o-Cresol) ug/L ND 4.0 01/22/10 09:43
2-Nitrophenol ug/L ND 5.0 01/22/10 09:43
3&4-Methylphenol(m&p Cresol) ug/L ND 4.0 01/22/10 09:43
3,3'-Dichlorobenzidine ug/L ND 10.0 01/22/10 09:43
4,6-Dinitro-2-methylphenol ug/L ND 20.0 01/22/10 09:43
4-Bromophenylphenyl ether ug/L ND 5.0 01/22/10 09:43
4-Chloro-3-methylphenol ug/L ND 20.0 01/22/10 09:43
4-Chlorophenylphenyl ether ug/L ND 5.0 01/22/10 09:43
4-Nitrophenol ug/L ND 20.0 01/22/10 09:43
Acenaphthylene ug/L ND 5.0 01/22/10 09:43
Anthracene ug/L ND 5.0 01/22/10 09:43
Benzidine ug/L ND 25.0 01/22/10 09:43
Benzo(a)anthracene ug/L ND 2.0 01/22/10 09:43
Benzo(a)pyrene ug/L ND 1.0 01/22/10 09:43
Benzo(b)fluoranthene ug/L ND 2.0 01/22/10 09:43
Benzo(g,h,i)perylene ug/L ND 5.0 01/22/10 09:43
Benzo(k)fluoranthene ug/L ND 4.0 01/22/10 09:43
bis(2-Chloroethoxy)methane ug/L ND 5.0 01/22/10 09:43
bis(2-Chloroethyl)ether ug/L ND 4.0 01/22/10 09:43
bis(2-Chloroisopropyl)ether ug/L ND 5.0 01/22/10 09:43
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 01/22/10 09:43
Butylbenzylphthalate ug/L ND 5.0 01/22/10 09:43
Chrysene ug/L ND 5.0 01/22/10 09:43
Di-n-butylphthalate ug/L ND 5.0 01/22/10 09:43
Di-n-octylphthalate ug/L ND 5.0 01/22/10 09:43
Dibenz(a,h)anthracene ug/L ND 2.0 01/22/10 09:43
Diethylphthalate ug/L ND 5.0 01/22/10 09:43
Dimethylphthalate ug/L ND 5.0 01/22/10 09:43
Fluoranthene ug/L ND 5.0 01/22/10 09:43
Fluorene ug/L ND 5.0 01/22/10 09:43
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 16 of 41
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• Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnal ical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
•' Asheville,NC 28804 Huntersville,NC 28078
www.pacelaba,ccm
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
METHOD BLANK: 35783 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hexachloro-1,3-butadiene ug/L ND 2.0 01/22/10 09:43
Hexachlorobenzene ug/L ND 1.0 01/22/10 09:43
Hexachlorocyclopentadiene ug/L ND 5.0 01/22/10 09:43
Hexachloroethane ug/L ND 5.0 01/22/10 09:43
Indeno(1,2,3-cd)pyrene ug/L ND 2.0 01/22/10 09:43
Isophorone ug/L ND 5.0 01/22/10 09:43
N-Nitroso-di-n-propylamine ug/L ND 4.0 01/22/10 09:43
N-Nitrosodimethylamine ug/L ND 2.0 01/22/10 09:43
N-Nitrosodiphenylamine ug/L ND 5.0 01/22/10 09:43
Naphthalene ug/L ND 5.0 01/22/10 09:43
Nitrobenzene ug/L ND 4.0 01/22/10 09:43
Pentachlorophenol ug/L ND 20.0 01/22/10 09:43
Phenanthrene ug/L ND 5.0 01/22/10 09:43
Phenol ug/L ND 5.0 01/22/10 09:43
Pyrene ug/L ND 5.0 01/22/10 09:43
2,4,6-Tribromophenol(S) % 94 54.2-114.4 01/22/10 09:43
2-Fluorobiphenyl(S) % 72 35.3-102.4 01/22/10 09:43
2-Fluorophenol(S) % 46 16.3-59.8 01/22/10 09:43
Nitrobenzene-d5(S) % 68 37.3-107.7 01/22/10 09:43
Phenol-d6(S) % 36 10-47.1 01/22/10 09:43
Terphenyl-d14(S) % 96 50.1-115.1 01/22/10 09:43
LABORATORY CONTROL SAMPLE: 35784
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,2,4-Trichlorobenzene ug/L 50 38.5 77 38.2-88.5
1,2-Dichlorobenzene ug/L 50 33.4 67 37-82.8
1,2-Diphenylhydrazine ug/L 50 37.9 76 51.1-110.6
1,3-Dichlorobenzene ug/L 50 32.9 66 35-80.8
1,4-Dichlorobenzene ug/L 50 32.7 65 34.2-83.2
2,4,6-Trichlorophenol ug/L 50 42.4 85 44.2-106.3
2,4-Dichlorophenol ug/L 50 39.6 79 42.2-100.1
2,4-Dimethylphenol ug/L 50 38.3 77 36.6-99.1
2,4-Dinitrophenol ug/L 50 57.0 114 10-191
2,4-Dinitrotoluene ug/L 50 53.9 108 59.1-113.2
2,6-Dinitrotoluene ug/L 50 50.0 100 55.8-107.9
2-Chloronaphthalene ug/L 50 37.8 76 37.8-102.1
2-Chlorophenol ug/L 50 33.2 66 33.6-86.4
2-Methylphenol(o-Cresol) ug/L 50 34.9 70 30.2-88
2-Nitrophenol ug/L 50 38.1 76 37.2-99.5
3&4-Methylphenol(m&p Cresol) ug/L 50 33.0 66 30.6-82.2
3,3'-Dichlorobenzidine ug/L 50 36.6 73 48.7-109
4,6-Dinitro-2-methylphenol ug/L 50 48.0 96 15.9-136.5
4-Bromophenyiphenyl ether ug/L 50 43.9 88 53.5-106.3
4-Chloro-3-methylphenol ug/L 50 49.8 100 47.7-103.1
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 17 of 41
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u�c i

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Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceArralylical a 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
nrpocsla6a.�m Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
LABORATORY CONTROL SAMPLE: 35784
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
4-Chlorophenylphenyl ether ug/L 50 48.1 96 47.8-103.1
4-Nitrophenol ug/L 50 23.9 48 12.6-59.9
Acenaphthylene ug/L 50 41.9 84 42.9-101.7
Anthracene ug/L 50 45.4 91 51.5-113.7
Benzidine ug/L 50 6J 12 10-99.3
Benzo(a)anthracene ug/L 50 45.7 91 58.5-111.1
Benzo(a)pyrene ug/L 50 48.7 97 59.3-111.7
Benzo(b)fluoranthene ug/L 50 51.1 102 58.7-111.9
Benzo(g,h,i)perylene ug/L 50 41.3 83 61-116.3
Benzo(k)fluoranthene ug/L 50 53.8 108 58.6-114.3
bis(2-Chloroethoxy)methane ug/L 50 40.2 80 35.7-100.1
bis(2-Chloroethyl)ether ug/L 50 32.2 64 30.5-98.4
bis(2-Chlorolsopropyl)ether ug/L 50 35.9 72 33.6-89.2
bis(2-Ethylhexyl)phthalate ug/L 50 48.3 97 59.1-119.3
Butylbenzylphthalate ug/L 50 48.5 97 57.3-118.7
Chrysene ug/L 50 46.9 94 56.4-113.1
Di-n-butylphthalate ug/L 50 51.1 102 53.7-121.4
Di-n-octylphthalate ug/L 50 44.8 90 49.3-125.6
Dibenz(a,h)anthracene ug/L 50 ' 42.8 86 60.2-117.1
Diethylphthalate ug/L 50 53.4 107 49.9-119.6
Dimethylphthalate ug/L 50 47.6 95 52.4-109.8
Fluoranthene ug/L 50 51.3 103 56.2-115.1
Fluorene ug/L 50 45.9 92 47.6-107.9
Hexachloro-1,3-butadiene ug/L 50 39.0 78 33.1-94.7
Hexachlorobenzene ug/L 50 43.8 88 53.2-115.6
Hexachlorocyclopentadiene ug/L 50 29.3 59 13.3-90.2
Hexachloroethane ug/L 50 34.4 69 36.8-83.5
Indeno(1,2,3-cd)pyrene ug/L 50 42.2 84 59-116.5
Isophorone ug/L 50 40.3 81 38.8-105.6
N-Nitroso-di-n-propylamine ug/L 50 33.4 67 31.3-104.4
N-Nitrosodimethylamine ug/L 50 18.3 37 19.6-57.2
N-Nitrosodiphenylamine ug/L 50 42.4 85 55-104
Naphthalene ug/L 50 38.8 78 36.6-94.1
Nitrobenzene ug/L 50 33.9 68 36.6-93.1
Pentachlorophenol ug/L 50 56.0 112 31-127
Phenanthrene ug/L 50 46.0 92 53.7-111.2
Phenol ug/L 50 16.3 33 10-47.2
Pyrene ug/L 50 48.0 96 57.7-113.5
2,4,6-Tribromophenol(S) % 114 54.2-114.4
2-Fluorobiphenyl(S) % 70 35.3-102.4
2-Fluorophenol(S) % 43 16.3-59.8
Nitrobenzene-d5(S) % 74 37.3-107.7
Phenol-d6(S) % 34 10-47.1
Terphenyl-d14(S) % 94 50.1-115.1
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 18 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
C N♦CCCgO'
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Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnaIytica! 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwpaaelabscan Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 35786 35785
MS MSD
9261462003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,2,4-Trichlorobenzene ug/L ND 50 50 17.1 15.9 34 32 38.2-88. 7 MO
1,2-Dichlorobenzene ug/L ND 50 50 16.1 16.6 32 33 37-82.8 3 MO
1,2-Diphenylhydrazine ug/L ND 50 50 36.8 31.2 74 62 51.1-110 16
1,3-Dichlorobenzene ug/L ND 50 50 20.1 17.1 40 34 35-80.8 16 MO
1,4-Dichlorobenzene ug/L ND 50 50 21.1 17.0 42 34 34.2-83. 22 MO
2,4,6-Trichlorophenol ug/L ND 50 50 45.2 39.3 90 78 44.2-106 14
2,4-Dichlorophenol ug/L ND 50 50 19.9 21.3 40 43 42.2-100 7 MO
2,4-Dimethylphenol ug/L ND 50 50 43.8 27.5 88 55 36.6-99. 46 R1
2,4-Dinitrophenol ug/L ND 50 50 44.2 47.0 88 94 10-191 6
2,4-Dinitrotoluene ug/L ND 50 50 36.7 38.1 73 76 59.1-113 4
2,6-Dinitrotoluene ug/L ND 50 50 37.1 37.4 74 75 55.8-107 .8
2-Chloronaphthalene ug/L ND 50 50 32.8 28.6 66 57 37.8-102 14
2-Chlorophenol ug/L ND 50 50 28.4 27.7 57 55 33.6-86. 3
2-Methylphenol(o-Cresol) ug/L ND 50 50 44.4 40.9 89 82 30.2-88 8 MO
2-Nitrophenol ug/L ND 50 50 21.7 21.3 43 43 37.2-99. 2
3&4-Methylphenol(m&p ug/L 22.8 50 50 51.4 56.1 57 67 30.6-82. 9
Cresol)
3,3'-Dichlorobenzidine ug/L ND 50 50 11.7 11.0 23 22 48.7-109 6 MO
4,6-Dinitro-2-methylphenol ug/L ND 50 50 38.6 34.2 77 68 15.9-136 12
4-Bromophenylphenyl ether ug/L ND 50 50 37.3 35.4 75 71 53.5-106 5
4-Chloro-3-methylphenol ug/L ND 50 50 23.2 31.7 46 63 47.7-103 31 MO
4-Chlorophenylphenyl ether ug/L ND 50 50 35.5 38.5 71 77 47.8-103 8
4-Nitrophenol ug/L ND 50 50 19.2J 31.2 38 62 12.6-59. MO
Acenaphthylene ug/L ND 50 50 32.4 33.2 65 66 42.9-101 2
Anthracene ug/L ND 50 50 31.6 36.4 63 73 51.5-113 14
Benzidine ug/L ND 50 50 ND ND 0 0 10-99.3 MO
Benzo(a)anthracene ug/L ND 50 50 37.7 36.8 75 74 58.5-111 2
Benzo(a)pyrene ug/L ND 50 50 37.9 36.7 76 73 59.3-111 3
Benzo(b)fluoranthene ug/L ND 50 50 38.0 37.5 76 75 58.7-111 1
Benzo(g,h,i)perylene ug/L ND 50 50 39.1 36.6 78 73 61-116.3 7
Benzo(k)fluoranthene ug/L ND 50 50 35.7 37.0 71 74 58.6-114 4
bis(2-Chloroethoxy)methane ug/L ND 50 50 18.9 22.9 38 46 35.7-100 19
bis(2-Chloroethyl)ether ug/L ND 50 50 26.1 23.0 52 46 30.5-98. 12
bis(2-Chloroisopropyl)ether ug/L ND 50 50 26.6 25.2 53 50 33.6-89. 6
bis(2-Ethylhexyl)phthalate ug/L 6.1 50 50 42.7 42.2 73 72 59.1-119 1
Butylbenzylphthalate ug/L ND 50 50 37.4 38.8 71 74 57.3-118 4
Chrysene ug/L ND 50 50 38.1 37.0 76 74 56.4-113 3
Di-n-butylphthalate ug/L ND 50 50 30.0 34.9 57 67 53.7-121 15
Di-n-octylphthalate ug/L ND 50 50 38.9 33.4 78 67 49.3-125 15
Dibenz(a,h)anthracene ug/L ND 50 50 39.3 36.8 79 74 60.2-117 7
Diethylphthalate ug/L ND 50 50 39.0 42.5 69 76 49.9-119 9
Dimethylphthalate ug/L ND 50 50 34.7 37.0 69 74 52.4-109 6
Fluoranthene ug/L ND 50 50 24.5 32.2 49 64 56.2-115 27 MO
Fluorene ug/L ND 50 50 35.7 36.9 71 73 47.6-107 3
Hexaohloro-1,3-butadiene ug/L ND 50 50 16.7 14.3 33 29 33.1-94. 16 MO
Hexachlorobenzene ug/L ND 50 50 36.5 34.7 73 69 53.2-115 5
Hexachlorocyclopentadiene ug/L ND 50 50 18.4 10.0 37 20 13.3-90. 59 R1
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 19 of 41
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without the written consent of Pace Analytical Services,Inc..
C N Accc9p'
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o Pace Analytical Services,Inc. Pace Analytical Services,Inc.
=Analytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwparxfabaccm Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 35786 35785
MS MSD
9261462003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Hexachloroethane ug/L ND 50 50 19.6 13.7 39 27 36.8-83. 35 MO
Indeno(1,2,3-cd)pyrene ug/L ND 50 50 39.2 37.0 78 74 59-116.5 6
Isophorone ug/L ND 50 50 21.4 21.2 43 42 38.8-105 1
N-Nitroso-di-n-propylamine ug/L ND 50 50 28.3 24.9 57 50 31.3-104 13
N-Nitrosodimethylamine ug/L ND 50 50 24.0 17.8 48 36 19.6-57. 30
N-Nitrosodiphenylamine ug/L ND 50 50 37.6 35.5 75 71 55-104 6
Naphthalene ug/L ND 50 50 19.2 18.5 35 33 36.6-94. 4 MO
Nitrobenzene ug/L ND 50 50 19.4 19.0 39 38 36.6-93. 2
Pentachlorophenol ug/L ND 50 50 49.6 48.6 99 97 31-127 2
Phenanthrene ug/L ND 50 50 44.0 34.9 88 69 53.7-111 23
Phenol ug/L ND 50 50 30.1 32.0 54 58 10-47.2 6 MO
Pyrene ug/L ND 50 50 37.2 45.2 74 90 57.7-113 19
2,4,6-Tribromophenol(S) % 80 92 54.2-114
2-Fluorobiphenyl(S) % 58 56 35.3-102
2-Fluorophenol(S) % 50 44 16.3-59.
Nitrobenzene-d5(S) % 40 38 37.3-107
Phenol-d6(S) % 48 51 10-47.1 S7
Terphenyl-d14(S) % 66 88 50.1-115
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 20 of 41
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without the written consent of Pace Analytical Services,Inc..
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® Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: MSV/9742 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 9261607001
METHOD BLANK: 394291 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1-Trichloroethane ug/L ND 5.0 01/24/10 09:50
1,1,2,2-Tetrachloroethane ug/L ND 5.0 01/24/10 09:50
1,1,2-Trichloroethane ug/L ND 5.0 01/24/10 09:50
1,1-Dichloroethane ug/L ND 5.0 01/24/10 09:50
1,1-Dichloroethene ug/L ND 5.0 01/24/10 09:50
1,2-Dichloroethane ug/L ND 5.0 01/24/10 09:50
1,2-Dichloropropane ug/L ND 5.0 01/24/10 09:50
2-Chloroethylvinyl ether ug/L ND 10.0 01/24/10 09:50
Acrolein ug/L ND 100 01/24/10 09:50
Acrylonitrile ug/L ND 100 01/24/10 09:50
Benzene ug/L ND 5.0 01/24/10 09:50
Bromodichloromethane ug/L ND 5.0 01/24/10 09:50
Bromoform ug/L ND 5.0 01/24/10 09:50
Bromomethane ug/L ND 10.0 01/24/10 09:50
Carbon tetrachloride ug/L ND 5.0 01/24/10 09:50
Chlorobenzene ug/L ND 5.0 01/24/10 09:50
Chloroethane ug/L ND 10.0 01/24/10 09:50
Chloroform ug/L ND 5.0 01/24/10 09:50
Chloromethane ug/L ND 5.0 01/24/10 09:50
cis-1,3-Dichioropropene ug/L ND 5.0 01/24/10 09:50
Dibromochloromethane ug/L ND 5.0 01/24/10 09:50
Ethylbenzene ug/L ND 5.0 01/24/10 09:50
Methylene Chloride ug/L ND 5.0 01/24/10 09:50
Tetrachloroethene ug/L ND 5.0 01/24/10 09:50
Toluene ug/L ND 5.0 01/24/10 09:50
trans-1,2-Dichloroethene ug/L ND 5.0 01/24/10 09:50
trans-1,3-Dichloropropene ug/L ND 5.0 01/24/10 09:50
Trichloroethene ug/L ND 5.0 01/24/10 09:50
Trichlorofluoromethane ug/L ND 10.0 01/24/10 09:50
Vinyl chloride ug/L ND 5.0 01/24/10 09:50
1,2-Dichloroethane-d4(S) % 90 70-130 01/24/10 09:50
4-Bromofluorobenzene(S) % 105 86-111 01/24/10 09:50
Dibromofluoromethane(S) % 97 88-113 01/24/10 09:50
Toluene-d8(S) % 97 92-105 01/24/10 09:50
LABORATORY CONTROL SAMPLE: 394292
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 18.8 94 52-162
1,1,2,2-Tetrachloroethane ug/L 20 20.5 102 46-157
1,1,2-Trichloroethane ug/L 20 20.3 102 52-150
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 21 of 41
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without the written consent of Pace Analytical Services,Inc..
Acccq
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Pace• (0
to Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
mvwpacefebxca+t Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
LABORATORY CONTROL SAMPLE: 394292
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1-Dichloroethane ug/L 20 19.9 99 59-155
1,1-Dichloroethene ug/L 20 19.0 95 1-234
1,2-Dichloroethane ug/L 20 17.8 89 49-155
1,2-Dichloropropane ug/L 20 18.5 92 1-210
2-Chloroethylvinyl ether ug/L 40 35.2 88 1-305
Acrolein ug/L 100 79.6J 80 15-152
Acrylonitrile ug/L 100 86.1J 86 75-132
Benzene ug/L 20 19.2 96 37-151
Bromodichloromethane ug/L 20 17.9 89 35-155
Bromoform ug/L 20 20.6 103 45-169
Bromomethane ug/L 20 15.9 80 1-242
Carbon tetrachloride ug/L 20 22.7 114 70-140
Chlorobenzene ug/L 20 22.9 114 37-160
Chloroethane ug/L 20 18.4 92 14-230
Chloroform ug/L 20 19.0 95 51-138
Chloromethane ug/L 20 19.2 96 1-273
cis-1,3-Dichloropropene ug/L 20 17.6 88 1-227
Dibromochloromethane ug/L 20 20.2 101 53-149
Ethylbenzene ug/L 20 21.7 108 37-162
Methylene Chloride ug/L 20 17.8 89 1-221
Tetrachloroethene ug/L 20 23.5 117 64-148
Toluene ug/L 20 20.1 101 47-150
trans-1,2-Dichloroethene ug/L 20 18.1 91 54-156
trans-1,3-Dichloropropene ug/L 20 17.1 86 17-183
Trichloroethene ug/L 20 20.9 105 71-157
Trichlorofluoromethane ug/L 20 19.0 95 17-181
Vinyl chloride ug/L 20 17.8 89 1-251
1,2-Dichloroethane-d4(S) % 89 70-130
4-Bromofluorobenzene(S) % 108 86-111
Dibromofluoromethane(S) % 94 88-113
Toluene-d8(S) % 98 92-105
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 22 of 41
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without the written consent of Pace Analytical Services,Inc..
p,N AC e,ONO
4 0

Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
swtrpBCelab&ccvn Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WET/11193 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 9261607001,9261607002
METHOD BLANK: 393713 Matrix: Water
Associated Lab Samples: 9261607001,9261607002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 01/22/10 16:03
LABORATORY CONTROL SAMPLE: 393714
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 238 95 80-120
SAMPLE DUPLICATE: 393715
9261700001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND ND
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 23 of 41
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without the written consent of Pace Analytical Services,Inc..
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1

o Pace Analytical Services,Inc. Pace Analytical Services,Inc.
(// 2CeAnwww,pookibuoritaI icai 2225 Riverside Dr. 9800 Klncey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WET/11224 Analysis Method: SM 4500F/C
QC Batch Method: SM 4500F/C Analysis Description: SM4500FC Fluoride Water
Associated Lab Samples: 9261607001
METHOD BLANK: 394969 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fluoride mg/L ND 0.10 01/26/10 18:51
LABORATORY CONTROL SAMPLE: 394970
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Fluoride mg/L 2.5 2.5 100 90-110
MATRIX SPIKE SAMPLE: 394971
9261167001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Fluoride mg/L 3.0 2.5 5.2 88 75-125
MATRIX SPIKE SAMPLE: 394972
9261200001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Fluoride mg/L 0.80 2.5 3.1 92 75-125
SAMPLE DUPLICATE: 394973
9261550001 Dup
Parameter Units Result Result RPD Qualifiers
Fluoride mg/L 3.1 2.9 7
SAMPLE DUPLICATE: 394974
9261554001 Dup
Parameter Units Result Result RPD Qualifiers
Fluoride mg/L 0.65 0.57 13
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 24 of 41
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without the written consent of Pace Analytical Services,Inc..
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® Pace Analytical Services,Inc. Pace Analytical Services,Inc.
+�I+p Qt7Q�i/��I+9� 2225 Riverside Dr. 9800 KinceyAve. Suite 100
MM
GtVV n�2 ecelab t Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WET/11201 Analysis Method: SM 4500-S2D
QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water
Associated Lab Samples: 9261607001
METHOD BLANK: 393809 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide mg/L ND 0.10 01/22/10 17:00
LABORATORY CONTROL SAMPLE: 393810
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Sulfide mg/L .5 0.52 104 90-110
MATRIX SPIKE SAMPLE: 393811
9261571001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Sulfide mg/L ND .5 ND 0 75-125 MO
SAMPLE DUPLICATE: 393812
9261571002 Dup
Parameter Units Result Result RPD Qualifiers
Sulfide mg/L ND ND
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 25 of 41
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without the written consent of Pace Analytical Services,Inc..
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Jz

® Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnatyticalbwmpacetabs.com 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WET/11176 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD,5 day
Associated Lab Samples: 9261607001,9261607002
METHOD BLANK: 393095 Matrix: Water
Associated Lab Samples: 9261607001,9261607002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
BOD,5 day mg/L ND 2.0 01/26/10 09:09
LABORATORY CONTROL SAMPLE: 393096
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
BOD,5 day mg/L 198 186 94 84-115
SAMPLE DUPLICATE: 393097
9261607001 Dup
Parameter Units Result Result RPD Qualifiers
BOD,5 day mg/L ND ND
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 26 of 41
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without the written consent of Pace Analytical Services,Inc..
ACC04��
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e Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
c a al.` .ccm Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/2774 Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 9261607001
METHOD BLANK: 37443 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Bromide mg/L ND 0.10 01/25/10 12:18
LABORATORY CONTROL SAMPLE: 37444
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Bromide mg/L 10 9.7 97 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 37445 37446
MS MSD
356346001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Bromide mg/L 0.20 10 10 9.6 9.6 94 94 90-110 .04
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 37447 37448
MS MSD
9261607001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Bromide mg/L 0.80 20 20 19.5 19.5 93 94 90-110 .2
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 27 of 41
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o

e Pace Analytical Services,Inc. Pace Analytical Services,Inc.
ace Analytical
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
VCinw►)6t� abs•com Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6667 Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1 Analysis Description: 350.1 Ammonia
Associated Lab Samples: 9261607001,9261607002
METHOD BLANK: 395771 Matrix: Water
Associated Lab Samples: 9261607001,9261607002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,Ammonia mg/L ND 0.10 01/28/10 13:27
LABORATORY CONTROL SAMPLE: 395772
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen,Ammonia mg/L 5 5.5 110 90-110
MATRIX SPIKE SAMPLE: 395773
9261560001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Nitrogen,Ammonia mg/L 559 5 559 1 90-110 MO
MATRIX SPIKE SAMPLE: 395775
9261600001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Nitrogen,Ammonia mg/L ND 5 5.5 111 90-110 MO
SAMPLE DUPLICATE: 395774
9261565001 Dup
Parameter Units Result Result RPD Qualifiers
Nitrogen,Ammonia mg/L 0.24 0.19 25 R1
SAMPLE DUPLICATE: 395776
9261607001 Dup
Parameter Units Result Result RPD Qualifiers
Nitrogen,Ammonia mg/L ND ND
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 28 of 41
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without the written consent of Pace Analytical Services,Inc..
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® Pace Analytical Services,Inc. Pace Analytical Services,Inc.
acemalytical 2225 Riverside Dr. 9800 Kinney Ave. Suite 100
uwwjlabscan Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6718 Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 9261607001
METHOD BLANK: 399503 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,Kjeldahl,Total mg/L ND 0.50 02/08/10 10:36
LABORATORY CONTROL SAMPLE: 399504
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen,Kjeldahl,Total mg/L 5 5.4 107 90-110
MATRIX SPIKE SAMPLE: 399505
9261607001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Nitrogen,Kjeldahl,Total mg/L 1.1 5 6.3 105 90-110
MATRIX SPIKE SAMPLE: 399507
9262322001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Nitrogen,Kjeldahl,Total mg/L ND 5 5.4 99 90-110
SAMPLE DUPLICATE: 399506
9262416002 Dup
Parameter Units Result Result RPD Qualifiers
Nitrogen,Kjeldahl,Total mg/L 3.3 3.5 6
SAMPLE DUPLICATE: 399508
9262322002 Dup
Parameter Units Result Result RPD Qualifiers
Nitrogen,Kjeldahl,Total mg/L ND ND
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 29 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
M ACCO
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Pace Analytical Services,Inc. Pace Analytical Services,Inc.
CD�al ticaf 2225 Riverside Dr. 9800 Klncey Ave. Suite 100
tr xH vur Asheville,NC 28804 Huntersville,NC 28078
wwwpacel [phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6630 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate+Nitrite,Unpres.
Associated Lab Samples: 9261607001
METHOD BLANK: 393510 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen,Nitrate mg/L ND 0.10 01/21/10 21:46
Nitrogen,Nitrite mg/L ND 0.10 01/21/10 21:46
Nitrogen,NO2 plus NO3 mg/L ND 0.10 01/21/10 21:46
LABORATORY CONTROL SAMPLE: 393511
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen,Nitrate mg/L 5 5.0 100 90-110
Nitrogen,Nitrite mg/L 1 1.1 107 90-110
Nitrogen,NO2 plus NO3 mg/L 5 5.0 100 90-110
MATRIX SPIKE SAMPLE: 393519
9261779002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Nitrogen,Nitrate mg/L ND 5 5.8 115 90-110 MO
Nitrogen,Nitrite mg/L 1.4 1 2.8 140 90-110 MO
Nitrogen,NO2 plus NO3 mg/L 0.23 5 5.8 110 90-110
SAMPLE DUPLICATE: 393522
9261779003 Dup
Parameter Units Result Result RPD Qualifiers
Nitrogen,Nitrate mg/L ND ND
Nitrogen,Nitrite mg/L 0.85 0.84 1
Nitrogen,NO2 plus NO3 mg/L 0.16 0.16 0
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 30 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
,N CCOyQ,
it.
1ti

® Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6650 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus,Total
Associated Lab Samples: 9261607001
METHOD BLANK: 394744 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/L ND 0.10 01/26/10 15:01
LABORATORY CONTROL SAMPLE: 394745
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phosphorus mg/L 1 1.1 106 90-110
MATRIX SPIKE SAMPLE: 394746
9261361002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Phosphorus mg/L 1.5 1 2.7 120 90-110 MO
MATRIX SPIKE SAMPLE: 394748
9261537003 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Phosphorus mg/L 229 1 230 107 90-110
SAMPLE DUPLICATE: 394747
9261362001 Dup
Parameter Units Result Result RPD Qualifiers
Phosphorus mg/L 1.7 1.6 3
SAMPLE DUPLICATE: 394749
9261537005 Dup
Parameter Units Result Result RPD Qualifiers
Phosphorus mg/L 248 248 0
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 31 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
V N�cecyc'
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• Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceArralytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
xavw.paCslabstaont Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6639 Analysis Method: EPA 420.4
QC Batch Method: EPA 420.4 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 9261607001
METHOD BLANK: 394298 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenol mg/L ND 0.010 01/25/10 14:20
LABORATORY CONTROL SAMPLE: 394299
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phenol mg/L .25 0.25 98 90-110
MATRIX SPIKE SAMPLE: 394300
9261462003 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Phenol mg/L 0.027 .25 0.22 78 90-110 MO
SAMPLE DUPLICATE: 394301
9261462004 Dup
Parameter Units Result Result RPD Qualifiers
Phenol mg/L 0.027 0.040 38 R1
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 32 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
M ACC.
11t1� n
4Iz

• Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalyticaI 2225 Riverside Dr. 9800 KlnceyAve. Suite 100
wnvwpecefabs.carrr Asheville,NC 28804 Huntersvilie,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6647 Analysis Method: SM 4500-CN-E
QC Batch Method: SM 4500-CN-E Analysis Description: 4500CNE Cyanide,Total
Associated Lab Samples: 9261607001
METHOD BLANK: 394547 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide mg/L ND 0.0050 01/26/10 19:40
LABORATORY CONTROL SAMPLE: 394548
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Cyanide mg/L .1 0.091 91 80-120
MATRIX SPIKE SAMPLE: 394549
9261334005 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Cyanide mg/L 0.0059 .1 0.090 84 75-125
SAMPLE DUPLICATE: 394550
9261536006 Dup
Parameter Units Result Result RPD Qualifiers
Cyanide mg/L ND ND
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 33 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
ti

®(0e
Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aeeAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwpacelabscom Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6669 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 9261607001,9261607002
METHOD BLANK: 395913 Matrix: Water
Associated Lab Samples: 9261607001,9261607002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 01/29/10 11:20
LABORATORY CONTROL SAMPLE: 395914
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 762 102 90-110
MATRIX SPIKE SAMPLE: 395915
9261877002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L ND 750 1550 207 75-125 MO
MATRIX SPIKE SAMPLE: 395923
9261658001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 4910 750 6110 160 75-125 MO
SAMPLE DUPLICATE: 395922
9261877003 Dup
Parameter Units Result Result RPD Qualifiers
Chemical Oxygen Demand mg/L ND ND
SAMPLE DUPLICATE: 395924
9261659001 Dup
Parameter Units Result Result RPD Qualifiers
Chemical Oxygen Demand mg/L 2530 2490 2
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 34 of 41
This report shall not be reproduced,except In full,
without the written consent of Pace Analytical Services,Inc..
era .,
ti
1

e Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalytica! 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6625 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: 5310E TOC
Associated Lab Samples: 9261607001,9261607002
METHOD BLANK: 393042 Matrix: Water
Associated Lab Samples: 9261607001,9261607002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L ND 1.0 01/21/10 22:30
LABORATORY CONTROL SAMPLE: 393043
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Organic Carbon mg/L 25 24.5 98 90-110
MATRIX SPIKE SAMPLE: 393044
9261620001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Total Organic Carbon mg/L 963 25 964 3 75-125 MO
MATRIX SPIKE SAMPLE: 393045
9261620002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Total Organic Carbon mg/L 236 25 260 96 75-125
SAMPLE DUPLICATE: 393046
9261620004 Dup
Parameter Units Result Result RPD Qualifiers
Total Organic Carbon mg/L 117 118 1
SAMPLE DUPLICATE: 393047
9261620005 Dup
Parameter Units Result Result RPD Qualifiers
Total Organic Carbon mg/L 238 240 1
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 35 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..

s Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnat tical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
ceIa s(dl Asheville,NC 28804 Huntersville,NC 28078
wwwpa [phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: WETA/6649 Analysis Method: ASTM D516-90
QC Batch Method: ASTM D516-90 Analysis Description: ASTM D516-90 Sulfate Water
Associated Lab Samples: 9261607001
METHOD BLANK: 394738 Matrix: Water
Associated Lab Samples: 9261607001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 5.0 01/26/10 12:27
LABORATORY CONTROL SAMPLE: 394739
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Sulfate mg/L 20 19.8 99 90-110
MATRIX SPIKE SAMPLE: 394740
9261420001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Sulfate mg/L 33.3 20 48.9 78 75-125
MATRIX SPIKE SAMPLE: 394742
9261309001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Sulfate mg/L 221 20 238 86 75-125
SAMPLE DUPLICATE: 394741
9261420002 Dup
Parameter Units Result Result RPD Qualifiers
Sulfate mg/L 35.1 35.2 0
SAMPLE DUPLICATE: 394743
9261309002 Dup
Parameter Units Result Result RPD Qualifiers
Sulfate mg/L 1370 1360 1
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 36 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
iG rM AG co„,4
uLz

e Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
pacelabs.can Asheville,NC 28804 Huntersville,NC 28078
www [phone] [phone]
ANALYTICAL RESULTS
Project: NPDES-RENEW
Pace Project No.: 9261607
Sample: 001-NPDES Lab ID: 9261607001 Collected: 01/20/10 09:55 Received: 01/20/10 12:38 Matrix:Water
PWS: Site ID: Sample Type:
Parameters Method Act±Unc(MDC) Units Analyzed CAS No. Qual
Gross Alpha EPA 900.0m 6.99±2.34 (2.71) pCi/L 02/10/10 13:14 12587-46-1
Gross Beta EPA 900.0m 4.38±1.36 (1.60) pCi/L 02/10/10 13:14 12587-47-2
Radium-226 EPA 903.1 0.175±0.201 (0.158) pCi/L 02/11/10 11:30 13982-63-3
Radium-228 EPA 904.0 -0.115±0.330 (0.813) pCi/L 02/11/10 11:44 15262-20-1
•
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 37 of 41
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without the written consent of Pace Analytical Services,Inc..
M1 M ACCpy.,

Pace Analytical Services,Inc. Pace Analytical Services,Inc.
aceAnalyticaI 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
sovwpecefabscmr Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: RADC/4134 Analysis Method: EPA 903.1
QC Batch Method: EPA 903.1 Analysis Description: 903.1 Radium-226
Associated Lab Samples: 9261607001
METHOD BLANK: 135064 Matrix: Water
Associated Lab Samples: 9261607001
Parameter Act±Unc(MDC) Units Analyzed Qualifiers
Radium-226 -0.054±0.279 (0.645) pCi/L 02/11/10 11:07
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 38 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
p gCCOq'
4�

® Pace Analytical Services,Inc. Pace Analytical Services,Inc.
f�it�V/�MalYti al 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
com
V/111 crI9J*Gtt Asheville,NC 28804 Huntersville,NC 28078
wwwin [phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: RADC/4170 Analysis Method: EPA 900.0m
QC Batch Method: EPA 900.0m Analysis Description: 900.0 Gross Alpha/Beta
Associated Lab Samples: 9261607001
METHOD BLANK: 136641 Matrix: Water
Associated Lab Samples: 9261607001
Parameter Act±Unc(MDC) Units Analyzed Qualifiers
Gross Alpha -0.422±0.407 (1.49) pCi/L 02/05/10 09:35
Gross Beta 0.119±0.573 (1.39) pCi/L 02/05/10 09:35
Date:02/19/2010 09:48AM REPORT OF LABORATORY ANALYSIS Page 39 of 41
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without the written consent of Pace Analytical Services,Inc..

Pace Analytical Services,Inc. Pace Analytical Services,Inc.
a�+p dna/UticaI 2225 Riverside Dr. 9800 KinceyAve. Suite 100
xwr patelabscarrt Asheville,NC 28804 Huntersville,NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: NPDES-RENEW
Pace Project No.: 9261607
QC Batch: RADC/4139 Analysis Method: EPA 904.0
QC Batch Method: EPA 904.0 Analysis Description: 904.0 Radium 228
Associated Lab Samples: 9261607001
METHOD BLANK: 135071 Matrix: Water
Associated Lab Samples: 9261607001
Parameter Act±Unc(MDC) Units Analyzed Qualifiers
Radium-228 -0.0663±0.287 (0.711) pCi/L 02/11/10 11:45
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 40 of 41
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without the written consent of Pace Analytical Services,Inc..
M rCCCgC
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1

aeeAnalytical Pace Analytical Services,Inc. l Services,Inc.
2225 Riverside Dr. 9800 lyticaAve. Suite 100
Asheville,NC 28804 Pace AnalyticaHuntersville,NC 28078
[phone] [phone]
QUALIFIERS
Project: NPDES-RENEW
Pace Project No.: 9261607
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to changes in sample preparation,dilution of
the sample aliquot,or moisture content.
ND-Not Detected at or above adjusted reporting limit.
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
S-Surrogate
1,2-Diphenylhydrazine(8270 listed analyte)decomposes to Azobenzene.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
Pace Analytical is NELAP accredited.Contact your Pace PM for the current list of accredited analytes.
U-Indicates the compound was analyzed for,but not detected.
LABORATORIES
PAST-A Pace Analytical Services-Asheville
PAST-C Pace Analytical Services-Charlotte
PAST-O Pace Analytical Services-Ormond Beach
PASI-PA Pace Analytical Services-Greensburg
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H6 Analysis initiated more than 15 minutes after sample collection.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
S7 Surrogate recovery outside control limits(not confirmed by re-analysis).
Date:02/19/2010 09:48 AM REPORT OF LABORATORY ANALYSIS Page 41 of 41
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc..
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Oc. 1f J A)�- Michael F.Easley,Governor
Q William G.Ross Jr.,Secretary
0 (. North Carolina Department of Environment and Natural Resources`
` , Alan W.Klimelc,P.E.Director
Y" Division of Water Quality
0 <
DIVISION OF WATER QUALITY
•
May 9, 2006
Mr. Enrique Bertran, Plant Manager
FMC Corporation, Lithium Division
Box 795
Besssemer City,North Carolina 28016
Subject: NPDES Permit NC0005177
• FMC Lithium Corporation
Gaston County
•
Dear Mr. Bertran:
•
Our records indicate that NPDES Permit No.NC0005177 was issued on April 26, 2006
for the discharge of wastewater to the surface waters of the State from your facility. The purpose
of this letter is to advise you of the importance of the Permit and the liabilities in the event of
failure to comply with the terms and conditions of the Permit. If you have not already done so, it
is suggested that you thoroughly read the Permit. Of particular importance are Pages 4 and 5.
Pages 4 and 5 set forth the effluent limitations and monitoring requirements for your
discharge. Your discharge must not exceed any of the limitations set forth. The section headed
"Monitoring Requirements" describes the measurement frequencies, sample types and sampling
locations. Upon commencement of your discharge (or operation), you must initiate the required
monitoring. The monitoring results must be entered on reporting forms furnished or approved by
this Agency. For new permits/facilities,the Division may supply an initial small stock of these
forms; however, if you fail to receive the forms, please contact this Office as quickly as possible.
The forms, including directions for their completion, and other important information are also
available at http://h2o.enr.state.nc.us/NPDES/documents.html. It is imperative that all applicable
parts be completed, and the original and one copy be submitted as required.
Please be advised that an annual fee may be required for your facility; if so,you will
receive a statement from our Raleigh Office., It is imperative that the fee be paid in a timely
manner so as to prevent enforcement action or possible revocation of your permit.
The remaining parts of the Permit set forth definitions, general conditions and special
conditions applicable to the operation of wastewater treatment facilities and/or discharge(s). The
NgN"orthCaaturrafyo na
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N.C.Division of Water Quality,Mooresville Regional Office,610 E.Center Ave.Suite 301,Mooresville NC 28115 [phone] Customer Service
1-877-623-6748

conditions include special reporting requirements in the event of noncompliance, bypasses,
treatment unit/process failures, etc. Also addressed are requirements for a certified wastewater
treatment plant operator if you are operating wastewater treatment facilities. Any changes in
operation of wastewater treatment facilities, quantity and type of wastewater being treated or
discharged, expansions and/or upgrading of wastewater treatment facilities must be permitted or
approved by this Agency.
To maintain compliance with discharge limitations,proper operation and maintenance of
a wastewater treatment facility and the development of a process control program are essential.
For those facilities having chlorine tablet disinfection, please be advised that chlorine tablets
approved for wastewater treatment use must be used; swimming pool tablets are not approved.
Also, be advised that DWQ staff need to have access to the facility's discharge point into the
receiving stream; please maintain a path along the outfall line to facilitate that access.
Failure to comply with the terms and conditions of an NPDES Permit subjects the
Permittee to enforcement action pursuant to Section 143-215.6 of the North Carolina General
Statutes. A civil penalty of up to $25,000 per violation (and/or criminal penalties) may be
assessed for such violations. If you find at any time that you are unable to comply with the terms
and conditions of the Permit, you should contact this Office immediately. A Special Order by
Consent (SOC) may be necessary while pursuing action to obtain compliance.
As a final note, an NPDES Permit is normally issued for a five-year period. Permits are
not automatically renewed. Renewal requests must be submitted to this Agency no later than 180
days prior to expiration. Please make note of the expiration date of your Permit. This date is set
forth on Page 1 of the Permit. Also note that NPDES Permits are not automatically transferable.
If you, as the Permittee, cease to need this Permit, then you should request that the Division of
Water Quality rescind the Permit or request that DWQ reissue the Permit to another party, if
necessary.
As mentioned previously, the purpose of this letter is to advise you of the importance of
your NPDES Permit. Please read the Permit and contact this Office at 704/663-1699 in
Mooresville if you have any questions or need clarification. We look forward to providing any
assistance.
Sincerely,
bfrf?
D. Rex Gleason, P.E.
Surface Water Protection Regional Supervisor
A:\NPDESLTR.WQ

F WA7 Michael F.Easley,Governor
O �p State of North Carolina
G William G. Ross,Jr., Secretary
t-/IIIT61
C/) . Department of Environment and Natural Resources
O �}� '\n/ . vlti UEPT.O Ian W.Klimek, Director
(� "fl_i ATit^r- Division of-Water Quality
April 26, 2006
Mr. Enrique Bertran, Plant Manager APR 2 8 20^
FMC Corporation, Lithium Division
Box 795
Bessemer City, North Carolina 28016
ITER 011 A I!TY Cr
Subject: NPDES Permit Issuance
Permit NC0005 177
FMC Lithium Corporation
Gaston County
Dear Mr. Bertran:
Division personnel have reviewed and approved your application for renewal of
the subject permit. Accordingly, we are forwarding the attached NPDES discharge
permit. This permit is issued pursuant to the requirements of North Carolina General
Statute 143-215.1 and the Memorandum of Agreement between North Carolina and
the U.S. Environmental Protection Agency dated May 9, 1994 (or as subsequently
amended).
The permit authorizes FMC Lithium Corporation to discharge up to 0.615 MGD
of treated wastewater, stormwater, boiler blowdown and cooling water from the FMC
Corporation WWTP to an unnamed tributary to Abernethy Creek, a class C water in
the Catawba River Basin. The permit includes discharge limitations /or monitoring
for flow,biochemical oxygen demand (BOD), total suspended solids (TSS), dissolved
oxygen, NH3, chloride, magnesium, chronic toxicity and other parameters.
The following modifications from the February 15, 2006 draft permit will remain
in the final permit:
Outfall 001
• The results of the priority pollutant analysis submitted by your facility
detected the presence of magnesium. The concentration reported was
evaluated in the reasonable potential analysis and was determined to exceed
the allowable concentration for protection of water quality (using EPA's
national water quality criteria). Based on this data, quarterly monitoring for
magnesium is recommended to be included in the permit.
• Deletion of quarterly monitoring for copper and zinc. A review of data
indicated that there was no reasonable potential for the parameters to
exceed the water quality action level standard. No"ehcaroli
atura/!
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh,NC 27699-1617 Phone[phone]
Customer Service Internet: www.ncwaterqualitv.org Location: 512 N.Salisbury St. Raleigh,NC 27604
Fax [phone] 1-877-623-6748
An Equal Opportunity/Affirmative Action Employer—50%Recycled/10%Post Consumer Paper

Permit No. NC0005177
FMC Lithium
Page 2
Outfall 004
■ The addition of quarterly monitoring for ethylbenzene and methyl chloride.
Information provided in the application indicated the potential discharge of
these constituents through this outfall. Quarterly monitoring is
recommended so that an evaluation of water quality can be done upon next
permit renewal.
If any parts, measurement frequencies or sampling requirements contained
in this permit are unacceptable to you, you have the right to an adjudicatory
hearing upon written request within thirty (30) days following receipt of this letter.
This request must be in the form of a written petition, conforming to Chapter 150B
of the North Carolina General Statutes, and filed with the office of Administrative
Hearings, 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless
such a demand is made, this permit shall be final and binding.
Please take notice that this permit is not transferable. The Division may
require modification or revocation and reissuance of the permit. This permit does
not affect the legal requirements to obtain other permits, which may be required by
the Division of Water Quality, or permits required by the Division of Land
Resources, Coastal Area Management Act, or any other Federal or Local
governmental permits may be required.
If you have any questions or need additional information, please contact Ms.
Jacquelyn Nowell at telephone number [phone], extension 512.
Sincerely,
7 decv-r--)
tci_ Alan W. Klimek, P.E.
cc: NPDES File
Aquatic Toxicology Unit
EPA Region IV/Attn. Marshall Hyatt
Central Files

Permit NC0005177
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1,other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission,and
the Federal Water Pollution Control Act,as amended,
FMC Corporation
is hereby authorized to discharge wastewater and stormwater from a facility located at the
FMC Lithium Division
NC Highway 161 west of Bessemer City
. Gaston County
to receiving waters designated as an unnamed tributary to Abernethy Creek in the Catawba River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II
III,and IV hereof.
The permit shall become effective June 1,2006.
This permit and the authorization to discharge shall expire at midnight on August 31,2010.
Signed this day April 26,2006.
•
Ae.„__ 79) ede42,9,
eta—Alan W.Klimek,P.E.,Director
Division of Water Quality
By Authority of the Environmental Management Commission

Part I Permit NC0005177
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility,whether for operation or discharge are hereby revoked,
and as of this issuance,any previously issued permit bearing this number is no longer effective.Therefore,
the exclusive authority to operate and discharge from this facility arises under the permit conditions,
requirements,terms,and provisions included herein.
FMC Corporation is hereby authorized to:
1. Continue operation of an existing 0.615 MGD wastewater treatment facility consisting of:
• reverse osmosis filtration,
• hydrogen peroxide addition,
d pH adjustment systems,and
• the Lower pond
Facility is located at FMC Corporation's Lithium Division off NC Highway 161 west of
Bessemer City in Gaston County; j.
2. Continue operation of a stormwater conveyance system and two sedimentation and
polishing ponds;and
3. Discharge treated wastewater (outfall 001) and stormwater, boiler blowdown, and cooling
water (004) at the locations specified on the attached map. The receiving stream is an
unnamed tributary to Abernethy Creek, a class C water in the Catawba River Basin.
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FMC Lithium Division - NC0005177 Facility
Location •
USGS Quad Name: Bessemer City Lat.: 34249158v
Receiving Stream: UT Abernethy Creek Long.: 78°49 23"
Stream Class: C 3�°/5�YY Not to SCALE
Subbasin: Catawba -030837 Sl a /►11 P" North

Part I Permit NC0005177
SECTION A: LIMITATIONS AND CONTROLS
(1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS [001]
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to discharge
treated industrial wastewater from Outfall 001. Such discharges shall be limited and monitored by the Permittee as
specified below:
EFFLUENT LIMITATIONS MONITORING REQUIREMENTS
PARAMETER Measurement
Monthly Average Daily Maximum Sample Type Sample Location
Frequency .
Flow 0.615 MGD Continuous Recording Influent or Effluent
BOD5 30.0 mg/L 45.0 mg/L Monthly Grab Effluent
Total Suspended Solids 333.9 pounds/day 1001.7 pounds/day 2/Month Grab Effluent
Dissolved Oxygen Daily Average > 5.0 mg/L Weekly Grab Effluent
pH Between 6.0 and 9.0 Standard Units Weekly Grab Effluent
NH3-N Monthly Grab Effluent
Chloride Monthly Grab Effluent
Magnesium Quarterly Grab Effluent
Total Nitrogen Quarterly Grab Effluent
Total Phosphorus Quarterly Grab Effluent
Conductivity Monthly Grab Effluent
Chronic Toxicity' Quarterly Grab Effluent
Footnotes:
1 Chronic Toxicity(Ceriodaphnia) @ 78%,January,April,July,October;see section A. (3) of this permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.

Part I Permit NC0005177
(2) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS [004]
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to discharge
stormwater, boiler blowdown, steam condensate and non-contact cooling water from Outfall 004. Such discharges
shall be limited and monitored by the Permittee as specified below:
EFFLUENT LIMITATIONS MONITORING REQUIREMENTS
PARAMETER Measurement
Monthly Average! Daily Maximum Sample Type Sample Location
Frequency
Flow(MGD)' Monthly Instantaneous Effluent
Total Suspended Solids Monthly Grab Effluent
pH Between 6.0 and 9.0 Standard Units Monthly Grab Effluent
Conductivity Monthly Grab Effluent
Chloride Monthly Grab Effluent
Ethylbenzene Quarterly Grab Effluent
Methyl Chloride Quarterly Grab Effluent
Footnotes:
i Where no measurable discharge occurs, "no discharge" shall be clearly noted on the submitted monthly discharge
monitoring report(DMR).
> One set of samples per year shall be collected during a discharge resulting from a representative storm event.
A representative storm shall be any storm event that causes a discharge through outfall 004. Failure to
monitor storm events in accordance with.the specified frequency shall constitute a violation of this permit.
For each representative storm event,the total precipitation,storm duration,and total flow shall be recorded.
> Total flow shall be: (a) measured continuously; (b) calculated based on the amount of area draining to the
outfall, the amount of built-upon (impervious) area, and the total amount of rainfall; or (c) estimated by the
measurement of flow at 20 minute intervals during the rain event. "Sample Collected During a Representative
Storm Event" shall be clearly marked on the DMR to indicate the samples were taken during a representative
storm event.
There shall be no chromium,zinc or copper added to the treatment system except as pre-approved
additives to biocidal compounds.
The permittee shall obtain approval from the Division's Aquatic Toxicology Unit prior to the use of any biocide (not
previously approved by the Division)in the effluent discharged under this permit. Approval for use of any biocide
not previously approved should be requested at least 90 days in advance of any planned usage.
Contact the Aquatic Toxicology Unit for detailed instructions on requesting approval of biocides:
NC DENR/DWQ/Aquatic Toxicology Unit
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.
SEE PART I,SECTION C FOR ADDITIONAL STORMWATER REQUIREMENTS.

Part I Permit NC0005177
(3) CHRONIC TOXICITY PERMIT LIMIT (Quarterly)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 78%.
The permit holder shall perform at a minimum,quarterly monitoring using test procedures outlined in the"North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure,"Revised February 1998,or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure"(Revised-February 1998) or subsequent
versions.The tests will be performed during the months of January,April,July, and October.Effluent sampling
for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the
permit limit,then multiple-concentration testing shall be performed at a minimum,in each of the two
following months as described in"North Carolina Phase II Chronic Whole Effluent Toxicity Test
Procedure"(Revised-February 1998)or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of"detectable impairment,"collection
methods,exposure regimes,and further statistical methods are specified in the"North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised-February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the
pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the
following address:
Attention: North Carolina Division of Water Quality
Environmental Sciences Section
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Section no later than 30 days
after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required,the
permittee will complete the information located at the top of the aquatic toxicity(AT) test form indicating the facility
name,permit number,pipe number,county,and the month/year of the report with the notation of"No Flow"in the
comment area of the form. The report shall be submitted to the Environmental Sciences Section at the address cited
above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required,monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re-opened and modified to include
alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document,such as minimum control organism
survival,minimum control organism reproduction,and appropriate environmental controls, shall constitute an invalid
test and will require immediate follow-up testing to be completed no later than the last day of the month following
the month of the initial monitoring.

Part I Permit NC0005177
SECTION B: Schedule of Compliance
1. The Permittee shall comply with final effluent limitations by the effective date of the permit
2. The Permittee shall at all times provide the operation and maintenance necessary to operate the existing
facilities in accordance with Part II.C.2 of this permit.
SECTION C: FINAL Monitoring Requirements FOR STORMWATER DISCHARGES
During the period beginning on the effective date of the permit and lasting until expiration, the permittee is
authorized to discharge stormwater associated with industrial activity from outfall 004. Such discharges shall be
controlled,limited,and monitored as specified below.
1. Stormwater Pollution Prevention Plans
The permittee shall develop and continue to update a Stormwater Pollution Prevention Plan,herein after referred to
as the Plan. The Plan shall be considered public information in accordance with Part II,Section E. 10 of this permit.
The Plan shall include,at a minimum,the following items:
a. Site Plan: The site plan shall provide a description of the physical facility and the potential pollutant
sources which may be expected to contribute to contamination of regulated stormwater discharges.
The site plan shall contain the following:
(1) A general location map (USGS quadrangle map, or appropriately drafted equivalent map),
showing the facility's location in relation to transportation routes and surface waters,and the
name of the receiving water(s) to which the stormwater outfall(s) discharges. If the
discharge is to a municipal separate storm sewer system, the name of the municipality and
the ultimate receiving waters, and accurate latitude and longitude of the point(s) of discharge
must be shown.
(2) A narrative description of storage practices, loading and unloading activities, outdoor
process areas, dust or particulate generating or control processes, and waste disposal
practices.
(3) A site map (or series of maps) drawn to scale with the distance legend indicating location of
industrial activities (including storage of materials, disposal areas,process areas, and loading
and unloading areas), drainage structures, drainage areas for each outfall and activities
occurring in the drainage area,building locations and impervious surfaces, the percentage of
each drainage area that is impervious. For each outfall, a narrative description of the
potential pollutants which could be expected to be present in the regulated stormwater
discharge.
(4) A list of significant spills or leaks of pollutants that have occurred at the facility during the 3
previous years and any corrective actions taken to mitigate spill impacts.
Certification that the stormwater outfalls have been evaluated for the presence of non-
5)
stormwater discharges. The certification statement will be signed in accordance with the
requirements found in Part II,Section B. 11.
b. Stormwater Management Plan: The stormwater management plan shall contain a narrative
description of the materials management practices employed which control or minimize the
exposure of significant materials to stormwater, including structural and non-structural measures.
The stormwater management plan,at a minimum,shall incorporate the following:
(1) A study addressing the technical and economic feasibility of changing the methods of
operations and/or storage practices to eliminate or reduce exposure of materials and

Part I Permit NC0005177
processes to stormwater. Wherever practicable the permittee should consider covering
storage areas, material handling operations, manufacturing or fueling operations to prevent
materials exposure to stormwater. In areas where elimination of exposure is not practicable,
the stormwater management plan shall document the feasibility of diverting the stormwater
runoff away from areas of potential contamination.
✓ (2) A schedule to provide secondary containment for bulk storage of liquid materials,storage of
Section 313 of Title III of the Superfund Amendments and Reauthorization Act (SARA)
water priority chemicals, or storage of hazardous materials to prevent leaks and spills from
contaminating stormwater runoff. If the secondary containment devices are connected
directly to stormwater conveyance systems, the connection shall be controlled by manually
activated valves or other similar devices [which shall be secured with a locking mechanism]
and any stormwater that accumulates in the containment area shall be at a minimum visually
observed prior to release of the accumulated stormwater. Accumulated stormwater shall be
released if found to be uncontaminated. Records documenting the individual making the
observation, the description of the accumulated stormwater and the date and time of the
release shall be kept for a period of five years.
43) A narrative description of Best Management Practices (BMPs) to be considered such as, but
not limited to, oil and grease separation, debris control, vegetative filter strips, infiltration
and stormwater detention or retention,where necessary. The need for structural BMPs shall
be based on the assessment of potential of sources contributing significant quantities of
pollutants to stormwater discharges and data collected through monitoring of stormwater
discharges.
„(4) Inspection schedules of stormwater conveyances and controls and measures to be taken to
limit or prevent erosion associated with the stormwater systems.
Spill Prevention and Response Plan: The Spill Prevention and Response Plan shall incorporate a risk
assessment of potential pollutant sources based on a materials inventory of the facility. Facility
personnel (or team) responsible for implementing the plan shall be identified in the plan. A
responsible person shall be on-site at all times during facility operations that have the potential to
contaminate stormwater runoff through spills or exposure of materials associated with the facility
operations.
.fit. Preventative Maintenance and Good Housekeeping Program: A preventative maintenance program
shall be developed. The program shall document schedules of inspections and maintenance activities
of stormwater control systems, plant equipment and systems. Inspection of material handling areas
and regular cleaning schedules of these areas shall be incorporated into the program.
e. Training schedules shall be developed and training provided at a minimum on an annual basis on
proper spill response and cleanup procedures and preventative maintenance activities for all
personnel involved in any of the facility's operations that have the potential to contaminate
stormwater runoff. Facility personnel (or team) responsible for implementing the training shall be
identified in the plan.
The Stormwater Pollution Prevention Plan shall identify a specific position(s) responsible for the
overall coordination, development,implementation,and revision to the Plan. Responsibilities for all
components of the Plan shall be documented and position(s) assignments provided.
g. Plan Amendment: The permittee shall amend the Plan whenever there is a change in design,
construction, operation, or maintenance which has a significant effect on the potential for the
discharge of pollutants via a point source to surface waters. The Stormwater Pollution Prevention
Plan shall be reviewed and updated on an annual basis.
The Director may notify the permittee when the Plan does not meet one or more of the minimum
requirements of the permit. Within 30 days of such notice, the permittee shall submit a time

•
Part I Permit NC0005177
schedule to the Director for modifying the Plan to meet minimum requirements. The permittee
shall provide certification in writing (in accordance with Part II,Standard Conditions,Section B.11.)
to the Director that the changes have been made.
h. Facility Inspections: Inspections of the facility and all stormwater systems shall occur at a minimum
on a semiannual schedule, once in the fall (September - November) and once during the spring
(April - June). The inspection and any subsequent maintenance activities performed shall be
documented, recording date and time of inspection, individual(s) making the inspection and a
narrative description of the facility's stormwater control systems, plant equipment and systems.
Records of these inspections shall be incorporated into the Stormwater Pollution Prevention Plan.
Visual monitoring as required in Part II, Section A.2. shall be performed in addition to facility
inspections.
i. Implementation: Implementation of the Plan shall include documentation of all monitoring,
measurements,inspections,maintenance activities and training provided to employees, including the
log of the sampling data.Activities taken to implement BMPs associated with the industrial activities,
including vehicle maintenance activities,must also be recorded. All required documentation shall be
kept on-site for a period of five years and made available to the Director or his authorized
representative immediately upon request.
2. Visual Monitoring
Visual monitoring requires a qualitative visual inspection of each stormwater outfall, regardless of representative
outfall status, for the purpose of evaluating the effectiveness of the Stormwater Pollution Prevention Plan and
assessing new sources of stormwater pollution. No analytical tests are required. Visual monitoring of stormwater
outfalls does not need to be performed during a representative storm event.
Stormwater Discharge Characteristics Frequency' Monitoring Type2 Monitoring Location3
Color Semi-Annual Visual SDO
Odor Semi-Annual Observation SDO
Clarity Semi-Annual Visual SDO
Floating Solids Semi-Annual Visual SDO
Suspended Solids Semi-Annual Visual SDO
Foam Semi-Annual Visual SDO
Oil Sheen Semi-Annual Visual SDO
Other obvious indicators of stormwater Semi-Annual Visual SDO
NOTES:
1 The first visual monitoring event during the term of the permit must be performed during the initial analytical monitoring
event. All subsequent visual monitoring will be performed twice per year,once in the spring and once in the fall.
2 Monitoring requires a qualitative observation of each stormwater outfall. No analytical testing or sampling is required.
3 Stormwater Discharge Outfall(SDO).
SECTION D: STORMWATER DEFINITIONS
1. Best Management Practices (BMPs)
Schedules of activities,prohibitions of practices,maintenance procedures,and other management practices to
prevent or reduce the pollution of waters of the United States. BMPs also include treatment requirements,
operation procedures, and practices to control plant site runoff,spillage or leaks,sludge or waste disposal, or
drainage from raw material storage.

Part I Permit NC0005177
2. Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers having a total storage capacity of greater than 1,320 gallons.
3. Point Source Discharge
Any discernible, confined and discrete conveyance, including but specifically not limited to, any pipe, ditch,
channel, tunnel, conduit, well, discrete fissure, container, rolling stock, or concentrated animal feeding
operation from which pollutants are or may be discharged to waters of the state.
4. Runoff Coefficient
The fraction of total rainfall that is not infiltrated into or otherwise retained by the soil, concrete,asphalt or
other surface upon which it falls that will appear at the conveyance as runoff.
5. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25-year,24-hour storm event.
6. Section 313 Water Priority Chemical
A chemical or chemical category which:
a. Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right-to-
Know Act of 1986;
b. Is present at or above threshold levels at a facility subject to SARA title III, Section 313 reporting
requirements;and
c. That meet at least one of the following criteria:
(1) Is listed in appendix D of 40 CFR part 122 on either Table II (organic priority pollutants),Table III
(certain metals, cyanides, and phenols) or Table IV (certain toxic pollutants and hazardous
substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A)of the CWA at 40 CFR 116.4;or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
7. Significant Materials
Includes, but is not limited to: raw materials; fuels;materials such as solvents, detergents, and plastic pellets;
finished materials such as metallic products;raw materials used in food processing or production;hazardous
substances designated under section 101(14) of CERCLA; any chemical the facility is required to report
pursuant to section 313 of Title III of SARA; fertilizers;pesticides; and waste products such as ashes, slag
and sludge that have the potential to be released with stormwater discharges.
8. Significant Spills
Includes,but is not limited to:releases of oil or hazardous substances in excess of reportable quantities under
section 311 of the Clean Water Act(Ref: 40 CFR 110.10 and CFR 117.21) or section 102 of CERCLA (Ref:
40 CFR 302.4).
9. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall or as a
result of snowmelt.
10. Total Flow
The flow corresponding to the time period over which the sample collection occurs. The total flow
calculated based on the size of the area draining to the outfall, the amount of the built-upon (impervious)
surfaces within the drainage area,and the total amount of rainfall occurring during the sampling period.
11. Visible Sedimentation
Solid particulate matter,both mineral and organic, that has been or is being transported by water,air,gravity,
or ice from its site of origin which can be seen with the unaided eye.

•
NPDES Permit Requirements
Page 1 of 16
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
Section A. Definitions
2/Month
Samples are collected twice per month with at least ten calendar days between sampling events.
3/Week
Samples are collected three times per week on three separate calendar days.
Act or"the Act"
The Federal Water Pollution Control Act,also known as the Clean Water Act,as amended,33 USC 1251,et seq.
Annual Average
The arithmetic mean of all "daily'discharges" of a pollutant measured during the calendar year. In the case of fecal
coliform, the geometric mean of such discharges.
Arithmetic Mean
The summation of the individual values divided by the number of individual values.
Bypass
The known diversion of waste streams from any portion of a treatment facility including the collection system,which
is not a designed or established or operating mode for the facility.
Calendar Day
The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any
consecutive 24-hour period that reasonably represents the calendar day may be used for sampling.
Calendar Quarter
One of the following distinct periods: January through March, April through June, July through September, and
October through December.
Composite Sample
A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 ml in
such a manner as to result in a total sample representative of the wastewater discharge during the sample period. The
Director may designate the most appropriate method (specific number and size of aliquots necessary, the time
interval between grab samples, etc.) on a case-by-case basis. Samples may be collected manually or automatically.
Composite samples may be obtained by the following methods:
(1) Continuous:a single,continuous sample collected over a 24-hour period proportional to the rate of flow.
(2) Constant time/variable volume: a series of grab samples collected at equal time intervals over a 24.hour
period of discharge and combined proportional to the rate of flow measured at the time of individual sample
collection,or
(3) Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period
with the time intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow recorder and
totalizer, and the preset gallon interval between sample collection fixed at no greater than 1/24 of the
expected total daily flow at the treatment system,or
(4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period at
a constant time intervaL This method may only be used in situations where effluent flow rates vary
less than 15 percent. The grab samples shall be taken at intervals of no greater than 20 minutes apart
during any 24-hour period and must be of equal size and of no less than 100 milliliters. Use of this method
requires prior approval by the Director.
Version 6J20/2003

NPDES Permit Requirements
Page 2 of 1.6
In accordance with (4) above,influent grab samples shall not be collected more than once per hour.
Effluent grab samples shall not be collected more than once per hour except at wastewater treatment systems
having a detention tune of greater than 24 hours. In such cases, effluent grab samples may be collected at
intervals evenly spaced over the 24-hour period that are equal in number of hours to the detention time of the
system in number of days. However, the interval between effluent grab samples may not exceed six hours nor
the number of samples less than four during a 24-hour sampling period.
Continuous flow measurement
Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance
activities on the flow device.
Daily Discharge
The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the
calendar day for purposes of sampling. For pollutants measured in units of mass,the "daily discharge"is calculated as
the total mass of the pollutant discharged over the day. The "daily discharge" concentration comprises the mean
concentration for a 24-hour sampling period as either a composite sample concentration or the arithmetic mean of all
grab samples collected during that period. (40 CFR 122.3)
Daily Maximum
The highest"daily discharge"during the calendar month.
Daily Sampling
Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the
permit The Division expects that sampling shall be conducted on weekdays except where holidays or other
disruptions of normal operations prevent weekday sampling. If sampling is required for all seven days of the week
for any permit parameter(s),that requirement will be so noted on the Effluent Limitations and Monitoring Page(s).
DWQ or"the Division"
The Division of Water Quality,Department of Environment and Natural Resources.
EMC
The North Carolina Environmental Management Commission.
Facility Closure
The cessation of wastewater treatment at a permitted facility,or the cessation of all activities that require coverage
under the NPDES. Completion of facility closure will allow this permit to be rescinded.
Geometric Mean
The Nth root of the product of the individual values where N = the number of individual values. For purposes of
calculating the geometric mean,values of"0"(or"< [detection level]") shall be considered=1.
Grab Sample
Individual samples of at least 100 ml collected over a period of time not exceeding 15 minutes. Grab samples can be
collected manually. Grab samples must be representative of the discharge (or the receiving stream, for ins tream
samples).
Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
Instantaneous flow measurement
A measure of flow taken at the time of sampling,when both the sample and flow will be representative of the total
discharge.
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Monthly Average (concentration limit)
The arithmetic mean of all"daily discharges" of a pollutant measured during the calendar month. In the case of fecal
coliform, the geometric mean of such discharges.
Permit Issuing Authority
The Director of the Division of Water Quality.
Quarterly Average (concentration limit)
The average of all samples taken over a calendar quarter.
Severe property damage
Substantial physical damage to property, damage to the treatment facilities which causes them to become inoperable,
or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage excludes economic loss caused by delays in production.
Toxic Pollutant
Any pollutant listed as toxic under Section 307(a)(1)of the Clean Water Act
Upset
An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance with
permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance caused by
operational error, improperly designed treatment facilities, inadequate treatment facilities, lack of preventive
maintenance,or careless or improper operation.
Weekly Average(concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar week. In the case of fecal
coliform, the geometric mean of such-discharges.
Section B. General Conditions
1. Duty to Comply
The Permittee must comply with all conditions of this permit. Any permit noncompliance constitutes a violation
of the Clean Water Act and is grounds for enforcement action;for permit termination,revocation and reissuance,
or modification;or denial of a permit renewal application [40 CFR 122.41].
a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants and with standards for sewage sludge use or disposal established under
section 405(d) of the Clean Water Act within the time provided in the regulations that establish these
standards or prohibitions or standards for sewage sludge use or disposal, even if the permit has not yet been
modified to incorporate the requirement.
b. The Clean Water Act provides that any person who violates section 301,302,306,307,308,318 or 405 of the
Act, or any permit condition or limitation implementing any such sections in a permit issued under section
402, or any requirement imposed in a pretreatment program approved under sections 402(a)(3) or 402(b)(8)
of the Act,is subject to a civil penalty not to exceed $25,000 per day for each violation. [40 CFR 122.41 (a)
(2)]
c. The Clean Water Act provides that any person who negligently violates sections 301,302,306,307,308,318, or
405 of the Act, or any condition or limitation implementing any of such sections in a permit issued under
section 402 of the Act, or any requirement imposed in a pretreatment program approved under section
402(a)(3) or 402(b)(8) of the Act,is subject to criminal penalties of$2,500 to $25,000 per day of violation, or
imprisonment of not more than 1 year, or both. In the case of a second or subsequent conviction for a
negligent violation, a person shall be subject to criminal penalties of not more than $50,000 per day of
violation,or by imprisonment of not more than 2 years,or both. [40 CFR 122.41 (a) (2)]
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d. Any person who knowingly violates such sections, or such conditions or limitations is subject to criminal
penalties of$5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. In
the case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal
penalties of not more than $100,000 per day of violation,or imprisonment of not more than 6 years,or both.
[40 CFR 122.41 (a) (2)]
e. Any person who knowingly violates section 301,302,303,306,307,308,318 or 405 of the Act,or any permit
condition or limitation implementing any of such sections in a permit issued under section 402 of the Act,
and who knows at that time that he thereby places another person in imminent danger of death or serious
bodily injury, shall,upon conviction, be subject to a fine of not more than $250,000 or imprisonment of not
more than 15 years, or both. In the case of a second or subsequent conviction for a knowing endangerment
violation,a person shall be subject to a fine of not more than$500,000 or by imprisonment of not more than
30 years, or both. An organization, as defined in section 309(c)(3)(B)(ui) of the CWA, shall, upon conviction
of violating the imminent danger provision,be subject to a fine of not more than$1,000,000 and can be fined
up to$2,000,000 for second or subsequent convictions. [40 CFR 122.41 (a) (2)]
f. Under state law, a civil penalty of not more than $25,000 per violation may be assessed against any person
who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North
Carolina General Statutes § 143-215.6A]
g. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302,
306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such
sections in a permit issued under section 402 of this Act. Administrative penalties for Class I violations are
not to exceed$10,000 per violation,with the maximum amount of any Class I penalty assessed not to exceed
$25,000. Penalties for Class II violations are not to exceed $10,000 per day for each.day during which the
violation continues, with the maximum amount of any Class II penalty not to exceed $125,000. [40 CFR
122.41 (a) (3)]
2. Duty to Mitigate
The Permittee shall take all reasonable steps to rninirni7e or prevent any discharge or sludge use or disposal in
violation of this permit which has a reasonable likelihood of adversely affecting human health or the environment
[40 CFR 122.41 (d)].
3. Civil and Criminal Liability
Except as provided in permit conditions on "Bypassing" (Part II. C. 4), "Upsets" (Part II. C. 5) and "Power
Failures" (Part II. C. 7), nothing in this permit shall be construed to relieve the Permittee from any
responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309
of the Federal Act, 33 USC 1319. Furthermore, the Permittee is responsible for consequential damages, such as
fish kills,even though the responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee
from any responsibilities,liabilities, or penalties to which the Permittee is or may be subject to under NCGS 143-
215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for
consequential damages; such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Property Rights
The issuance of this permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor
any infringement of Federal,State or local laws or regulations [40 CFR 122.41 (g)].
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical structures or
facilities or the undertaking of any work in any navigable waters.
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7. Severability
The provisions of this permit are severable. If any provision of this permit, or the application of any provision of thi
permit to any circumstances,is held invalid, the application of such provision to other circumstances, and the remainde
of this permit, shall not be affected thereby[NCGS 150B-231
8. Duty to Provide Information
The Permittee shall furnish to the Permit Issuing Authority,within a reasonable time, any information which the
Permit Issuing Authority may request to determine whether cause exists for modifying,revoking and reissuing,or
terminating this permit or to determine compliance with this permit. The Permittee shall also furnish to the
Permit Issuing Authority upon request,copies of records required by this permit [40 CFR 122.41 (h)].
9. Duty to Reapply
If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit,the
Permittee must apply for and obtain a new permit [40 CFR 122.41 (b)].
10. Expiration of Permit
The Permittee is not authorized to discharge after the expiration date. In order. to receive automatic
authorization to discharge beyond the expiration date, the Permittee shall submit such information, forms, and
fees as are required by the agency authorized to issue permits no later than 180 days prior to the expiration date.
Any Permittee that has not requested renewal at least 180 days prior to expiration, or any Permittee that does not
have a permit after the expiration and has not requested renewal at least 180 days prior to expiration,will subject
the Permittee to enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and certified
[40 CFR 122.41 (k)].
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible
corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in
charge of a principal business function, or any other person who performs similar policy or decision
making functions for the corporation,or (b) the manager of one or more manufacturing,production, or
operating facilities,provided,the manager is authorized to make management decisions which govern the
operation of the regulated facility including having the explicit or implicit duty of making major capital
investment recommendations, and initiating and directing other comprehensive measures to assure long
term environmental compliance with environmental laws and regulations; the manager can ensure that
the necessary systems are established or actions taken to gather complete and accurate information for
permit application requirements; and where authority to sign documents has been assigned or delegated
to the manager in accordance with corporate procedures
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,respectively-,or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or
ranking elected official [40 CFR 122.22].
b.. All reports required by the permit and other information requested by the Permit Issuing Authority shall be
signed by a person described in paragraph a. above or by a duly authorized representative of that person. A
person is a duly authorized representative only if
1. The authorization is made in writing by a person described above;
2. The authorization specified either an individual or a position having responsibility for the overall
operation of the regulated facility or activity,such as the position of plant manager, operator of a well or
well field, superintendent, a position of equivalent responsibility, or an individual or position having
overall responsibility for environmental matters for the company. (A duly authorized representative may
thus be either a named individual or any individual occupying a named position.);and
3. The written authorization is submitted to the Permit Issuing Authority[40 CFR 12222]
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c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate
because a different individual or position has responsibility for the overall operation of the facility, a new
authorization satisfying the requirements of paragraph (b) of this section must be submitted to the Director
prior to or together with any reports, information, or applications to be signed by an authorized
representative [40 CFR 122.22]
d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the
following certification [40 CFR 122.22]:
'I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the
Permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned
changes or anticipated noncompliance does not stay any permit condition [40 CFR 122.41 (f)].
13: Permit Modification.Revocation and Reissuance_or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the
permit,revoking and reissuing the permit,or terminating the permit as allowed by the laws,rules, and regulations
contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina
Administrative Code,Subchapter 2H.0100;and North Carolina General Statute 143-215.1 et.at
14. Annual Administering and Compliance Monitoring Fee Requirements
The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being
billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 2H.0105 (b) (4)
may cause this Division to initiate action to revoke the permit
Section C. •Operation and Maintenance of Pollution Controls
1. Certified Operator
Upon classification of the permitted facility by the Certification Commission, the Permittee shall.employ a
certified water pollution control treatment system operator in responsible charge (ORC) of the water pollution
control treatment system. Such operator must hold a certification of the grade equivalent to or greater than the
classification assigned to the water pollution control treatment system by the Certification Commission. The
Permittee must also employ one or more certified Back-up.ORCs who possess a currently valid certificate of the
type of the system. Back-up ORCs must possess a grade equal to(or no more than one grade less than) the grade
of the system [15A NCAC 8G.0201].
The ORC of each Class I facility must
> Visit the facility at least weekly
> Comply with all other conditions of 15A NCAC 8G.0204.
The ORC of each Class II,III and IV facility must
> Visit the facility at least daily,excluding weekends and holidays
> Properly manage and document daily operation and maintenance of the facility
> Comply with all other conditions of 15A NCAC 8G.0204.
Once the facility is classified, the Permittee shall submit a letter to the Certification Commission designating the
operator in responsible charge:
a. Within 60 calendar days prior to wastewater being introduced into a new system
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b. Within 120 calendar days of:
➢ Receiving notification of a change in the classification of the system requiring the designation of a
new ORC and back-up ORC
➢ A vacancy in the position of ORC or back-up ORC.
2. Proper Operation and Maintenance
The Permittee shall at all times provide the operation and maintenance resources necessary to operate the existing
facilities at optimum efficiency. The Permittee shall at all times properly operate and maintain all facilities and
systems of treatment and control (and related appurtenances) which are installed or used by the Permittee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the Permittee to install
and operate backup or auxiliary facilities only when necessary to achieve compliance with the conditions of the
permit[40 CFR 122.41 (e)].
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a Permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this permit [40 CFR 122.41
(c)].
4. Bypassing of Treatment Facilities
a. Bypass not exceeding limitations [40 CFR 122.41 (m) (2)]
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but
only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject to the
provisions of Paragraphs b.and c. of this section.
b. Notice [40 CFR 122.41 (m)'(3)]
(I) Anticipated bypass. If the Permittee knows in advance of the need for a bypass, it shall submit prior
notice, if possible at least ten days before the date of the bypass; including an evaluation of the
anticipated quality and effect of the bypass.
(2) Unanticipated bypass. The Permittee shall submit notice of an unanticipated bypass as required in Part
II.E. 6. (24-hour notice).
c. Prohibition of Bypass
(I) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for bypass,unless:
(A) Bypass was unavoidable to prevent loss of life,personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the.use of auxiliary treatment facilities,
retention of untreated wastes or maintenance during normal periods of equipment downtime. This
condition is not satisfied if adequate backup equipment should have been installed in the exercise of
reasonable engineering judgment to prevent a bypass which occurred during normal periods of
equipment downtime or preventive maintenance;and
(C) The Permittee submitted notices as required under Paragraph b.of this section.
(2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for a bypass as provided in any current or future system-wide collection system
permit associated with the treatment facility.
(3) The Permit Issuing Authority may approve an anticipated bypass,after considering its adverse effects,if
the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph c.
(1) of this section.
5. Upsets
a. Effect of an upset [40 CFR 122.41 (n) (2)]: An upset constitutes an affirmative defense to an action
brought for noncompliance with such technology based permit effluent limitations if the requirements of
paragraph b. of this condition are met. No determination made during administrative review of claims that
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noncompliance was caused by upset, and before an action for noncompliance, is final administrative action
subject to judicial review.
b. Conditions necessary for a demonstration of upset A Permittee who wishes to establish the
affirmative defense of upset shall demonstrate, through properly signed,contemporaneous operating logs,or
other relevant evidence that
(1)An upset occurred and that the Permittee can identify the cause(s) of the upset;
(2)The Permittee facility was at the time being properly operated;and
(3)The Permittee submitted notice of the upset as required in Part II.E. 6. (b) (B) of this permit.
(4)The Permittee complied with any remedial measures required under Part II.B.2. of this permit
d. Burden of proof[40 CFR 122.41 (n) (4)]: The Permittee seeking to establish the occurrence of an
upset has the burden of proof in any enforcement proceeding.
6. Removed Substances
Solids,sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters
shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant
from such materials from entering waters of the State or navigable waters of the United States. The Permittee
shall comply with all existing Federal regulations governing the disposal of sewage sludge. Upon promulgation of
40 CFR Part 503, any permit issued by the Permit Issuing Authority for the utilization/disposal of sludge may be
reopened and modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR 503. The
Permittee shall comply with applicable 40 CFR 503 Standards for the Use and Disposal of Sewage Sludge (when
promulgated) within the time provided in the regulation, even if the permit is not modified to incorporate the
requirement The Permittee shall notify the Permit Issuing Authority of any significant change in its sludge use
or disposal practices.
7. Power Failures
The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 2H.0124 —
Reliability) to prevent the discharge of untreated or inadequately treated wastes during electrical power failures
either by means of alternate power sources, standby generators or retention of inadequately treated effluent
Section D. Monitoring and Records
1. Representative Sampling
Samples collected and measurements taken,as required herein,shall be characteristic of the volume and nature of
the permitted discharge. Samples collected at a frequency less than daily shall be taken on a day and time that is
characteristic of the discharge over the entire period the sample represents. All samples shall be taken at the
monitoring points specified in this permit and, unless otherwise specified, before the effluent joins or is diluted
by any other wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to and the approval of the Permit Issuing Authority[40 CFR 12241 (j)].
2. Reporting
Monitoring results obtained during the previous month(s) shall be summari,ed for each month and reported on a
monthly Discharge Monitoring Report (DMR) Form (MR 1, Ll, 2, 3) or alternative forms approved by the
Director,postmarked no later than the 28th day following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of
these,and all other reports required herein,shall be submitted to the following address:
NC DENR/Division of Water Quality/Water Quality Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
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3. Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected
and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. The
devices shall be installed,calibrated and maintained to ensure that the accuracy of the measurements is consistent
with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a
maximum deviation of less than 10% from the true discharge rates throughout the range of expected discharge
volumes. Flow measurement devices shall be accurately calibrated at a minimum of once per year and maintained
to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device.
The Director shall approve the flow measurement device and monitoring location prior to installation.
Once-through condenser cooling water flow monitored by pump logs,or pump hour meters as specified in Part I
of this permit and based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations (published pursuant to.
NCGS 143-215.63 et. seq.), the Water and Air Quality Reporting Acts, and to regulations published pursuant to
Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act (as Amended), and 40 CFR 136; or in
the case of sludge use or disposal,approved under 40 CFR 136,unless otherwise specified in 40 CFR 503,unless
other test procedures have been specified in this permit [40 CFR 122.41].
To meet the intent of the monitoring required by this permit, all test procedures must produce minimum
detection and reporting levels that are below the permit discharge requirements and all data generated must be
reported down to the minimum detection or lower reporting level of the procedure. If no approved methods are
determined capable of achieving minimum detection and reporting levels below permit discharge requirements,
then the most sensitive (method with the lowest possible detection and reporting level) approved method must
be used.
5. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate,any
monitoring device or method required to be maintained under this permit shall,upon conviction,be punished by
a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or
by both. If a conviction of a person is for a violation committed after a first conviction of such person under this
paragraph,punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not more
than 4 years,or both [40 CFR 122.41].
6. Records Retention
Except for records of monitoring information required by this permit related to the Permittee's sewage sludge
use and disposal activities,which shall be retained for a period of at least five years (or longer as required by 40
CFR 503),the Permittee shall retain records of all monitoring information,including.
➢ all calibration and maintenance records
➢ all original strip chart recordings for continuous monitoring instrumentation
➢ copies of all reports required by this permit
➢ copies of all data used to complete the application for this permit
These records or copies shall be maintained for a period of at least 3 years from the date of the sample,
measurement,report or application. This period may be extended by request of the Director at any time [40 CFR
122.41].
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the Permittee shall record
the following information [40 CFR 122.41]:
a. The date,exact place,and time of sampling or measurements;
b. The individual(s)who performed the sampling or measurements;
c. The date(s)analyses were performed;
d. The individual(s)who performed the analyses;
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e. The analytical techniques or methods used;and
f. The results of such analyses.
8. Inspection and Entry
The Perrnittee shall allow the Director,or an authorized representative (including an authorized contractor acting
as a representative of the Director),upon the presentation of credentials and other documents as may be required
by law, to;
a. Enter upon the Permittee's premises where a regulated facility or activity is located or conducted, or where
records must be kept under the conditions of this permit•,
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this
permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment),practices,
or operations regulated or required under this permit;and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise
authorized by the Clean Water Act,any substances or parameters at any location [40 CFR 122.41 (i)].
Section E Reporting Requirements
L Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit The discharge
of any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall
constitute a violation of the permit.
2. Planned Changes
The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or
additions to the permitted facility[40 CFR 122.41 (1)]. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR
12229(b);or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged. This notification applies to pollutants subject neither to effluent limitations in the permit,nor to
notification requirements under 40 CFR 122.42(a) (1).
c. The alteration or addition results in a significant change in the Permittee's sludge use or disposal practices,
and such alternation, addition or change may justify the application of permit conditions that are different
from or absent in the existing permit,including notification of additional use or disposal sites not reported
during the permit application process or not reported pursuant to an approved land application plan.
3. Anticipated Noncompliance
The Permittee shall give advance notice to the Director of any planned changes to the permitted facility or other
activities that might result in noncompliance with the permit [40 CFR 12241 (1) (2)].
4. Transfers
This permit is not transferable to any person except after notice to the Director. The Director may require
modification or revocation and reissuance of the permit to document the change of ownership. Any such action
may incorporate other requirements as may be necessary under the Clean Water Act [40 CFR 122.41 (1) (3)].
5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit [40 CFR 122.41 (1) (4)].
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part II. D. 2) or forms
provided by the Director for reporting results of monitoring of sludge use or disposal practices.
b. If the Permittee monitors any pollutant more frequently than required by this permit, the results of such
monitoring shall be included in the calculation and reporting of the data submitted on the DMR.
•
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6. Twenty-four Hour Reporting
a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that
potentially threatens public health or the environment. Any information shall be provided orally within 24
hours from the time the Permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the Permittee becomes aware of the circumstances. The written
submission shall contain a description of the noncompliance, and its cause; the period of noncompliance,
including exact dates and times, and if the noncompliance has not been corrected, the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the
noncompliance [40 CFR 122.41 (1) (6)].
b. The Director may waive the written report on a case-by-case basis for reports under this section if the oral
report has been received within 24 hours.
c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response
personnel at(800) 662-7956, [phone] or(919)733-3300.
7. Other Noncompliance
The Permittee shall report all instances of noncompliance not reported-under Part II. E. 5 and 6. of this permit at
the time monitoring reports are submitted. The reports shall contain the information listed in Part II. E. 6. of
this permit [40 CFR 122.41 (1) (7)].
8. Other Information
Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or
submitted incorrect information in a permit application or in any report to the Director, it shall promptly submit
such facts or information [40 CFR 122.41 (1) (8)].
9. Noncompliance Notification
The Permittee shall report by telephone to either the central office or the appropriate regional office of the
Division as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following
a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of
wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge
digester; the known passage of a slug of hazardous substance through the facility; or any other unusual
circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps,aerators,compressors,etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass directly to receiving
waters without treatment of all or any portion of the influent to such station or facility.
Persons reporting such occurrences by telephone shall also file a written report within 5 days following first
knowledge of the occurrence.
l0. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act,33
USC 1318,all reports prepared in accordance with the terms shall be available for public inspection at the offices
of the Division of Water Quality. As required by the Act, effluent data shall not be considered confidential.
Knowingly making any false statement on any such report may result in the imposition of criminal penalties as
provided for in NCGS 143-215.1(b)(2) or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this permit,including
monitoring reports or reports of compliance or noncompliance shall,upon conviction, be punished by a fine of
Version 6r20/2003

NPDES Permit Requirements
Page 12 of 16.
not more than $25,000 per violation, or by imprisonment for not more than two years per violation, or by both
[40 CFR 122.411
12. Annual Performance Reports
Permittees who own or operate facilities that collect or treat municipal or domestic waste shall provide an annual
report to the Permit Issuing Authority and to the users/customers served by the Permittee (NCGS 143-215.1 C).
The report shall summarize the performance of the collection or treatment system,as well as the extent to which
the facility was compliant with applicable Federal or State laws, regulations and rules pertaining to water quality.
The report shall be provided no later than sixty days after the end of the calendar or fiscal year, depending upon
which annual period is used for evaluation.
PART III
OTHER REQUIREMENTS
Section A. Construction
The Permittee shall not commence construction of wastewater treatment facilities,nor add to the plant's treatment
capacity,nor change the treatment process(es)utilized at the treatment plant unless the Division has issued an
Authorization to Construct(AtC)permit. Issuance of an AtC will not occur until Final Plans and Specifications for
the proposed construction have been submitted by the Permittee and approved by the Division.
Section B. Groundwater Monitoring
The Permittee shall,upon written notice from the Director of the Division of Water Qrality,conduct groundwater
monitoring as may be required to determine the compliance of this NPDES permitted facility with the current
groundwater standards.
Section C. Changes in Discharges of Toxic Substances
The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe(40 CFR 122.42):
a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent
basis,of any toxic pollutant which is not limited in the permit,if that discharge will exceed the highest of the
following "notification levels";
(I) One hundred micrograms per liter(100 pg/L);
(2) Two hundred micrograms per liter (200 pg/L) for acrolein and acrylonitrile; five hundred micrograms
per liter(500!AWL) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol;and one milligram per liter
(1 mg/L) for antimony;
(3) Five times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge, on a non-routine or
infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the
highest of the following"notification levels";
(1) Five hundred micrograms per liter(500 pg/L);
(2) One milligram per liter(1 mg/L) for antimony;
(3) Ten times the maximum concentration value reported for that pollutant in the permit application.
Section D. Evaluation of Wastewater Discharge Alternatives
The Permittee shall evaluate all wastewater disposal alternatives and pursue the most environmentally sound
alternative of the reasonably cost effective alternatives. If the facility is in substantial non-compliance with the terms
and conditions of the NPDES permit or governing rules,regulations or laws,the Permittee shall submit a report in
such form and detail as required by the Division evaluating these alternatives and a plan of action within 60 days of
notification by the Division.
Section E. Facility Closure Requirements
The Permittee must notify the Division at least 90 days prior to the closure of any wastewater treatment system
covered by this permit. The Division may require specific measures during deactivation of the system to prevent
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NPDES Permit Requirements
Page 13 of 16
adverse impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit
continue at the permitted facility.
PART IV
SPECIAL CONDITIONS FOR MUNCIPAL FACILITIES
Section A. Publicly Owned Treatment Works (POTWs)
All POTWs must provide adequate notice to the Director of the following:
1. Any new introduction of pollutants into the POTW from an indirect discharger which would be subject to
section 301 or 306 of CWA if it were directly discharging those pollutants;and
2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger
as influent to that POTW at the time of issuance of the permit.
3. For purposes of this paragraph,adequate notice shall include information on (1) the quality and quantity of
effluent introduced into the POTW,and (2) any anticipated impact of the change on the quantity or quality
of effluent to be discharged from the POTW.
Section B. Municipal Control of Pollutants from Industrial Users.
1. Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs from
industries acing the municipal system may be present in the Permittee's discharge. At such time as
sufficient information becomes available to establish limitations for such pollutants, this permit may be
revised to specify effluent limitations for any or all of such other pollutants in accordance with best
practicable technology or water quality standards.
2. Under no circumstances shall the Permittee allow introduction of the following wastes in the waste
treatment systems:
a. Pollutants which create a fire or explosion hazard in the POTW, including, but not limited to,
wastestreaass with a dosed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees
Centigrade using the test methods specified in 40 CFR 261.21;
b. Pollutants which will cause corrosive structural damage to the POTW, but in no case Discharges
with pH lower than 5.0,unless the works is specifically designed to accommodate such Discharges;
c. Solid or viscous pollutants in amounts which will cause obstruction to the flow in the POTW
resulting in Interference;
d. Any pollutant,including oxygen demanding pollutants (BOD, etc) released in a Discharge at a flow
rate and/or pollutant concentration which will cause Interference with the POTW;
e. Heat in amounts which will inhibit biological activity in the POTW resulting in Interference,but in
no case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C
(104°F)unless the Division,upon request of the POTW,approves alternate temperature limits;
f. Petroleum oil, nonbiodegradable cutting oil, or products of mineral oil origin in amounts that will
cause interference or pass through;
g. Pollutants which result in the presence of toxic gases, vapors, or fumes within the POTW in a
quantity that may cause acute worker health and safety problems;
h. Any trucked or hauled pollutants,except at discharge points designated by the POTW.
3. With regard to the effluent requirements listed in Part I of this permit, it may be necessary for the
Permittee to supplement the requirements of the Federal Pretreatment Standards (40 CFR, Part 403) to
ensure compliance by the Permittee with all applicable effluent limitations. Such actions by the Permittee
may be necessary regarding some or all of the industries discharging to the municipal system.
4. The Permittee shall require any industrial discharges sending influent to the permitted system to meet
Federal Pretreatment Standards promulgated in response to Section 307(b) of the Act. Prior to accepting
wastewater from any significant industrial user, the Permittee shall either develop and submit to the
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NPDES Permit Requirements
Page 14 of i6
Division a Pretreatment Program for approval per 15A NCAC 2H .0907(a) or modify an existing
Pretreatment Program per 15A NCAC 2H .0907(b).
5. - This permit shall be modified,or alternatively,revoked and reissued,to incorporate or modify an approved
POTW Pretreatment Program or to include a compliance schedule for the development of a POTW
Pretreatment Program as required under Section 402(b)(8) of the Clean Water Act and implementing
regulations or by the requirements of the approved State pretreatment program,as appropriate.
Section C. Pretreatment Programs
Under authority of sections 307(b) and(c)and 402(b)(8) of the Clean Water Act and implementing regulations 40
CFR Part 403, North Carolina General Statute 143-215.3 (14) and implementing regulations 15A NCAC 2H
.0900, and in accordance with the approved pretreatment program, all provisions and regulations contained and
referenced in the Pretreatment Program Submittal are an enforceable part of this permit.
The Permittee shall operate its approved pretreatment program in accordance with Section 402(b)(8) of the Clean
Water Act, the Federal Pretreatment Regulations 40 CFR Part 403, the State Pretreatment Regulations 15A
NCAC 2H .0900, and the legal authorities, policies, procedures, and financial provisions contained in its
pretreatment program submission and Division approved modifications there of. Such operation shall include
but is not limited to the implementation of the following conditions and requirements:
1. Sewer Use Ordinance(SUO)
The Permittee shall maintain adequate legal authority to implement its approved pretreatment program.
2 Industrial Waste Survey(IWS)
The Permittee shall update its Industrial Waste Survey (IWS) to include all users of the sewer collection
system at least once every five years.
3. Monitoring Plan
The Permittee shall implement a Division approved Monitoring Plan for the collection of facility specific
data to be used in a wastewater treatment plant Headworks Analysis (HWA) for the development of
specific pretreatment local limits. Effluent data from the Plan shall be reported on the DMRs (as required
by Part II,Section D,and Section E.5.).
4. Headworks Analysis (HWA) and Local Limits
The Permittee shall obtain Division approval of a Headworks Analysis (HWA) at least once every five
years, and as required by the Division. Within 180 days of the effective date of this permit (or any
subsequent permit modification) the Permittee shall submit to the Division a written technical evaluation
of the need to revise local limits (i.e., an updated HWA or documentation of why one is not needed) [40
CFR 12242]. The Permittee shall develop,in accordance with 40 CFR 403.5(c) and 15A NCAC 2H..0909,
specific Local Limits to implement the prohibitions listed in 40 CFR 403.5(a) and (b) and 15A NCAC 2H
.0909.
5. Industrial User Pretreatment Permits (IUP)&Allocation Tables
In accordance with NCGS 143-215.1,the Permittee shall issue to all significant industrial users,permits for
operation of pretreatment equipment and discharge to the Permittee's treatment works. These permits
shall contain limitations, sampling protocols, reporting requirements, appropriate standard and special
conditions, and compliance schedules as necessary for the installation of treatment and control
technologies to assure that their wastewater discharge will meet all applicable pretreatment standards and
requirements. The Permittee shall maintain a current Allocation Table (AT)which su*n*nari7es the results
of the Headworks Analysis (HWA) and the limits from all Industrial User Pretreatment Permits (IUP).
Permitted IUP loadings for each parameter cannot exceed the treatment capacity of the POTW as
determined by the HWA.
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NPDES Permit Requirements
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6. Authorization to Construct(A to C)
The Permittee shall ensure that an Authorization to Construct permit (AtC) is issued to all applicable
industrial users for the construction or modification of any pretreatment facility. Prior to the issuance of
an AtC, the proposed pretreatment facility and treatment process must be evaluated for its capacity to
comply with all Industrial User Pretreatment Permit(IUP)limitations.
7. POTW Inspection&Monitoring of their SIUs
The Permittee shall conduct inspection, surveillance,and monitoring activities as described in its Division
approved pretreatment program in order to determine,independent of information supplied by industrial
users,compliance with applicable pretreatment standards. The Permittee must
a. Inspect all Significant Industrial Users (SIUs)at least once per calendar year,and
b. Sample all Significant Industrial Users (SIUs) at least twice per calendar year for all permit-
limited pollutants, once during the period from January 1 through June 30 and once during the
period from July 1 through December 31,except for organic compounds which shall be sampled
once per calendar year,
8. SIU Self Monitoring and Reporting
The Permittee shall require all industrial users to comply with the applicable monitoring and reporting
requirements outlined in the Division approved pretreatment program,the industry's pretreatment permit,
or in 15A NCAC 2H.0908.
9. Enforcement Response Plan(ERP)
The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards
promulgated pursuant to section 307(b) and (c) of the Clean Water Act (40 CFR 405 et. seq.),prohibitive
discharge standards as set forth in 40 CFR 403.5 and 15A NCAC 2H .0909, and specific local limitations.
All enforcement actions shall be consistent with the Enforcement Response Plan (ERP) approved by the
Division.
10. Pretreatment Annual Reports (PAR)
The Permittee shall report to the Division in accordance with 15A NCAC 2H .0908. In lieu of submitting
annual reports, Modified Pretreatment Programs developed under 15A NCAC 2H .0904 (b) may be
required to meet with Division personnel periodically to discuss enforcement of pretreatment requirements
and other pretreatment implementation issues.
For all other active pretreatment programs,the Permittee shall submit two copies of a Pretreatment Annual
Report(PAR) describing its pretreatment activities over the previous twelve months to the Division at the
following address:
NC DENR/DWQ /Pretreatment Unit
1617 Mail Service Center
Raleigh,NC 27699-1617
These reports shall be submitted according to a schedule established by the Director and shall contain the
following
a.) Narrative
A brief discussion of reasons for, status of, and actions taken for all Significant Industrial
Users (SIUs)in Significant Non-Compliance(SNC);
b.) Pretreatment Program Summary(PPS)
• A pretreatment program,summary(PPS)on specific forms approved by the Division;
c.) Significant Non-Compliance Report(SNCR)
The nature of the violations and the actions taken or proposed to correct the violations on
specific forms approved by.the Division;
d.) Industrial Data Summary Forms (IDSF)
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NPDES Permit Requirements
Page 16ofle
Monitoring data from samples collected by both the POTW and the Significant Industrial
User (SIU). These analytical results must be reported on Industrial Data Summary Forms
(IDSF) or other specific format approved by the Division;
e.) Other Information
Copies of the POTW's allocation table,new or modified enforcement compliance schedules,
public notice of SIUs in SNC, and any other information, upon request, which in the
opinion of the Director is needed to determine compliance with the pretreatment
implementation requirements of this permit;
11. Public Notice
The Permittee shall publish annually a list of Significant Industrial Users (SIUs) that were in Significant
Non-Compliance (SNC) as defined in the Permittee's Division approved Sewer Use Ordinance with
applicable pretreatment requirements and standards during the previous twelve month period. This list
shall be published within four months of the applicable twelve-month period.
12. Record Keeping
The Permittee shall retain for a minimum of three years records of monitoring activities and results,along
with support information including general records,water quality records,and records of industrial impact
on the POTW.
13. Funding and Financial Report
• The Permittee shall maintain adequate funding and staffing levels to accomplish the objectives of its
approved pretreatment program.
14. Modification to Pretreatment Programs
Modifications to the approved pretreatment program including but not limited to local limits
modifications, POTW monitoring of their Significant Industrial Users (SIUs), and Monitoring Plan
modifications,shall be considered a permit modification and shall be governed by 15 NCAC 2H.0114 and
15A NCAC 2H.0907..
Version 6.'20l2003

SOC PRIORITY PROJECT: No
To: Permits and Engineering Unit
Water Quality Section
Attention: Jackie Nowell
Date: January 19, 2006
NPDES STAFF REPORT AND RECOMMENDATIONS
County: Gaston
NPDES Permit No.: NC0005177
MRO No.: 05-45
PART I - GENERAL INFORMATION
1. Facility and address: FMC Corporation, Lithium Division
1115 Bessemer City-Kings Mountain Highway
Post Office Box 795
Bessemer City,N.C. 28016
2. Date of investigation: December 5 , 2005
3. Report prepared by: Michael L. Parker, Environmental Engineer II
4. Person contacted and telephone number: Kimberly Weathers, [phone]
5. Directions to site: The Lithium plant is located on the south(left) side of Hwy. 161 0.1
mile west of the jct. of Hwy. 161 and SR 1402,just west of Bessemer City.
6. Discharge point(s), list for all discharge points: -
Latitude: 35° 15' 44"
Longitude: 81° 17' 57"
Attach a USGS Map Extract and indicate treatment plant site and discharge point on map.
USGS Quad No.: F 13 SE
7. Site size and expansion area consistent with application: Yes. Ample area exists for the
construction of additional WWT facilities, if necessary.
8. Topography(relationship to flood plain included): The site encompasses several hundred
acres with varying topography(3-10% slopes). The main WWT pond is located in a
surface drainage feature, however, it appears to be protected from flooding.
9. Location of nearest dwelling: Approx. 1000± feet from the WWTP site.

Page Two
10. Receiving stream or affected surface waters: U. T. to Abernathy Creek
a. Classification: C
b. River basin and subbasin no.: Catawba 030837
c. Describe receiving stream features and pertinent downstream uses: Flow
observed in the receiving stream at the point of discharge. Downstream uses are
primarily agriculture. No other dischargers are known for a reasonable distance
downstream.
PART II- DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
Outfall 001 Outfall 004
1. a. Volume of wastewater: 0.615 MGD Intermittent
b. What is the current permitted capacity: 0.615 MGD (outfall 001)
c. Actual treatment capacity of current facility(current design capacity): 0.615 MGD
d. Date(s) and construction activities allowed by previous ATCs issued in the
previous two years: There have been no ATCs issued in the past two (2)years.
e. Description of existing or substantially constructed WWT facilities: The existing
WWT facilities at outfall 001 consist of two (2) Reverse Osmosis treatment units
followed by a hydrogen peroxide feed for chlorine neutralization,pH adjustment
(H2SO4 acid), and an 18 acre industrial WWT lagoon with a flow meter with
totalizer. Wastewater treated by these treatment processes include discharges of
lithium hydroxide, lithium chloride, and a discharge from a lithium hypochlorite
particulate air scrubber. There is also wastewater entering this outfall from floor
area sumps, boiler blowdown, wet particulate air scrubbers, and stormwater.
There is also a small, earthen pond(referred to as the R&D pond in the renewal
application)that receives condensate, cooling tower overflow, and stormwater.
The water is typically recycled back into the plant, however, if an overflow does
occur, the discharge from this pond will eventually travel through a series of
small, earthen settling ponds prior to reaching the receiving stream and
discharging at outfall 004.
f. Description of proposed WWT facilities: There are no WWT facilities proposed at
this time.
g. Possible toxic impacts to surface waters: This facility has had a consistent
compliance record with respect to toxicity testing.
2. ' Residual handling and utilization/disposal scheme: As the result of changes in the
manufacturing process, there are essentially no residuals generated at this time.
Previously, residuals were removed from the main treatment pond and stockpiled on-site.
These solids were used throughout the site to fill uneven terrain and stabilize roads.

Page Three
3. Treatment plant classification: Class II (no change from previous rating).
4. SIC Code(s): 2819, 2869 Wastewater Code(s): 32, 31, 02
5. MTU Code(s): 50000
PART III - OTHER PERTINENT INFORMATION
1. Is this facility being constructed with Construction Grant Funds or are any public monies
involved(municipals only)?No. Public monies were not used in the construction of this
facility.
2. Special monitoring or limitations (including toxicity) requests: None at this time.
3. Important SOC/JOC or Compliance Schedule dates: This facility is neither under an SOC
nor is one being considered at this time.
4. Alternative analysis evaluation: There are no known on-site or off-site alternatives that
are currently available which would eliminate the need to discharge.
PART IV- EVALUATION AND RECOMMENDATIONS
The permittee, FMC Corporation, Lithium Division (FMC), requests renewal of the
subject Permit. There have been no changes at this facility since the permit was last renewed nor
are any proposed in this renewal.
Pending receipt and approval of the yet-to-be-issued draft permit, it is recommended that
the Permit be renewed as requested.
- 7(:da.,/c ,2 7 /',:z-2,- / , 74,
Signature of Report Prep er ate
,,,, -,,F.,,r2c,'6
Water Quality Regional Supervisor Date
h:\dsr\dsr05\lithium.sr ,

\J
OF W A T�9 /t � Michael F.Easley,Governor
0 QC- O William G.Ross Jr.,Secretary
`� Noah Carol-a n 4EnyaCotttnentc,and Natural Resources
A dd{Vr``iNKVr,�rt
n�� AND NATI toN.REs uRegio nek P.E.Director
MOORESW. ' 1 romegf Water Quality
�1.
d 41
MAR 0 8 2005
March 7,2005
Enrique Bertran
S
FMC Corp.
P.O. Box 795 WATE` y°�`�' Y'����'{��, (CCT O(
Bessemer City,North Carolina 28016
Subject: Receipt of permit renewal application
NPDES Permit NC0005177
Lithium Division Plant
Gaston County
Dear Mr. Bertran:
The NPDES Unit received your permit renewal application on March 7,2005. A member of the NPDES Unit will
review your application. They will contact you if additional information is required to complete your permit renewal. You
should expect to receive a draft permit approximately 30-45 days before your existing permit expires. The requirements in
your existing permit will remain in effect until the permit is renewed(or the Division takes other action).
If you have any additional questions concerning renewal of the subject permit,please contact me at [phone],
extension 363.
Sincerely,
btAr5-
Carolyn Bryan
Point Source Branch
cc: CENTRAL FILES
%Mooresville Pegionat ee tilt
NPDES Unit
NNaoe Carolina
turally
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh,NC 27699-1617 Phone[phone] Customer Service
Internet: h2o.enr.state.nc.us 512 N.Salisbury St. Raleigh,NC 27604 FAX [phone] 1-877-623-6748

M C
ILr61 2 Wn -Th
� r l
CERTIFIED MAIL MAR 7 2005 ?.1
RETURN RECEIPT REQUESTED
- 'ii-t ()Lump(
STY
March 3, 2005 G;3ANCH
Mr. Charles H. Weaver, Jr.
NCDENR/Water Quality/NPDES Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: NPDES Renewal Application—Permit No. NC0005177
Dear Mr. Weaver:
FMC Corporation—Lithium Division, located in Bessemer City, Gaston County
("FMC")hereby requests renewal of NPDES Permit No. NC0005177. This renewal
application is being submitted at least 180 days prior to the expiration date of the current
permit on August 31, 2005. FMC requests that if a new permit is not issued by the
expiration date, that the current permit remain in force until superceded by a new permit.
No changes have taken place since issuance of the last permit. Enclosed are one signed
original and two copies of US EPA Form 1, Form 2C and attachments.
Please note the following:
• Actual laboratory reports are attached in lieu of filling in the blanks on the
application, and
• The enclosed process flow diagram has been numbered for use with the treatment
systems referenced on US EPA Form 2C.II.B, for your convenience.
FMC looks forward to discussing the permit renewal with the Division of Water Quality.
Please contact me at 704-868-5897 with any questions.
Sincerely yours,
Kiln erly Weathers
vironmental Manager
Enclosures
Air Treatment Construction Energy Fine Chemicals Glass&Ceramics Greases&Lubricants Polymers Pool Water Treatment
PO Box 795 Phone:[phone] lithium_info©fmc.com
Bessemer City,NC 28016 Fax:[phone] www.fmclithium.com
MARKETS SERVED

Please print or type in the unshaded areas only
(fill-in areas are spaced for elite type, i.e., 12 characters/inch). For Approved. OMB No. 2040-0086. Approval expires 5-3'1-92
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER
r GENERAL INFORMATION S T/A CF NCD000771964 D
Consolidated Permits Program
GENERAL (Read the "General Instructions"before starting.) 1 2 12 14 15.
LABEL ITEMS GENERAL INSTRUCTIONS.
If a preprinted label has been provided,
I. EPA 1.D. NUMBER affix it in the designated space. Review the
information carefully; if any of it is
incorrect, cross through it and enter the
III. FACILITY NAME correct data in.theappropriate fill-in area
below.Also, if.any of the preprinted data is
absent (the area to the left of the label
V. FACILITY PLEASE PLACE LABEL IN THIS SPACE appear),'pea ee`provia ttinthehproperfilld-
MAILING LIST in area(s) below. If the label is complete
and correct you need not complete Items
I, III, V, and V I(except VI-B which must be
VI. FACILITY completed regardless). Complete all items-
if no label has been proved. Refer to the
instructions for detailed item descriptions
LOCATION and for the legal authorization under which
this data is collected.
II. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer"yes"to any
questions, you must submit this form and the supplemental from listed in the parenthesis following the question.Mark"X"in the box in the,third column if
the supplemental form is attached, If you answer"no'to each question,you need not submit any of these forms. You may answer"no"if your activity is
excluded from permit requirements;see Section C of the instructions.See also, Section D of the instructions for definitions of bold-faced terms.
MARK"X" MARKX"
SPECIFIC QUESTIONS YES NO FORM SPECIFIC QUESTIONS YES NO FORM
ATTACHED,: ATTACHED
A. Is this facility a publicly owned treatment works. - B Does or will this facility (either existing or
which results in a discharge to waters of then ❑ ® ❑ proposed) include a concentrated animal ❑ ® ❑
U.S.?(FORM 2A) feeding operation or aquatic animal
production facility which results in a discharge
16 17 18 to waters:of the U.S.?(FORM 2B) 19 20 21
C. Is this facility which currently results in ® ❑ ® D. Is this proposal facility(other than those described El ® Eldischarges to waters of the U.S. other than in A or B above)which will result in a discharge
those described in A or B above?(FORM 2C) 22 23 - 24 to waters of the U.S.?(FORM 2D) 25 26 27
E. Does or will this facility treat, store, or dispose of F Do you or will you inject at this facility industrial or
hazardous wastes?(FORM 3) ® ❑ ❑ municipal effluent below the lowermost stratum ❑ ® ❑
containing, within one quarter mile of the well
bore, underground sources of drinking water?
28 29 30 (FORM 4) 31 32 33
G. Do you or will you inject at this facility any H. Do you or will you inject:at this facility fluids for
produced water other fluids which are brought to special processes such as mining of sulfer by the
the surface in connection with conventional oil or ❑ ❑ Frasch process,solution mining of minerals,in ❑ ® ❑
natural, gas production, inject fluids used for situ combustion of fossil fuel,or recovery of
enhanced recovery of oil or natural gas, or inject geothermal energy?(FORM 4)
fluids for storage of liquid hydrocarbons?
(FORM 4) 34 35 36 37 38 39
I. Is this facility a proposed stationary source J. Is this facility a proposed stationary source
which is one of the 28 industrial categories listed which is NOT one of the 28 industrial categories
in the instructions and which will potentially emit ❑ ® ❑ listed in the instructions-and&which will potentially ❑ ® ❑
100 tons per year of any air pollutant regulated emit 250 tons per year of any air pollutant
under the Clean Air Act and may affect or be regulated under the Clean Air Act and may affect
located in an attainment area? FORM 5 40 41 42 or be located in an attainment.are? FORM 5 43 44 45
III. NAME OF FACILITY
c SKIP FMC Corporation Lithium Division
1
15 16-29 30 69 . .
IV. FACILITY CONTACT '1-'
A. NAME&TITLE(last, first, &title) B. PHONE(area code&no.)
c Weathers, Kimberly Environmental Manager 704 868 5897
15 16 -. . 45 46 48 49 51 52 55 _ ...
V. FACILITY MAILING ADDRESS •
A.STREET OR P.O. BOX
c Box 795
15 16 45
B. CITY OR TOWN C.STATE D.ZIP CODE
c Bessemer City NC 28016
4
15 l 16 40 41 42 47 51
VI. FACILITY LOCATION ""
A.STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
c 1115 Bessemer City Kings Mountain Highway
5
15 16 45
B. COUNTY NAME
Gaston
46 70
C. CITY OR TOWN D. STATE E.ZIP CODE F. COUNTY CODE
c Bessemer City NC 28016
6
15 16 40 I 41 42 47 51 52 54
h;1':1 RORM 351(1-1 (3 00) CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
VII. SIC CODES (4-digit, in order of priority
A. FIRST B.SECOND
c (specify) 7 (specify)
5 16 17 2819 157
16 19' 2869
C.THIRD 0:..FOURTH
(specify) 7 (specify)
15 16 17 15 11G 19 I
VIII. OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
c FMC Corporation VIII-A also the owner.?
8 E YES ❑ NO
18 19 55
C.STATUS OF OPERATOR(Enter the appropriate letter into the answer box;if"Other,"specify.) _ D. PHONE(area code&no)
F=FEDERAL M=PUBLIC(other than federal or state) p (specify) c 215 299 6000
S=STATE 0=OTHER(specify) A
P=PRIVATE 56 15 16 18 19 21 22 25
E.STREET°OR PO BOX
1735 Market Street
26 55
F. CITY OR TOWN G. STATE H.ZIP CODE IX. INDIAN LAND
c Philadelphia PA 19103 Is the facility located on Indian lands?
B ❑ YES © NO
15 16 40 42 42 47 51 _
X. EXISTING ENVIRONMENTAL PERMITS
A. NPDES (Discharges to Surface Water) D. PSD(Air Emissions from Proposed Sources)
9 N I NC0005177 9 P 8
15 16 17 18 30 15 16 17 18 30
B. UIC(Underground Injection of Fluids E.OTHER(specify) (Specify)
9 T I N/A 9 T e [3560T41 Title V Air Permit
15 16 17 18 30 15 16 17 18 30
C. RCRA(Hazardous Wastes) E.OTHER(specify) (Specify)
C T I C T 8
9 R 9
15 16 17 18 30 15 16 17 18 30:..
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the ma. area. See instructions for precise requirements.
XII. NATURE OF BUSINESS (provide a brief description)
Chemical Manufacturing of various Lithium based compounds. Research Development and Laboratory analysis
XIII. CERTIFICATION (see instructions)
I certify under penalty of law that I have;personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry,of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurat- l,5 complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fine :nd ioriso ,fient.
A. NAME&OFFICIAL TITLE(type or print) B.S ': / C. DATE SIGNED
-111
COMMENTS FOR OFFICIAL USE ONLY ' =°"'
c
C
15 16 55
I{1'A FORM 3510-1 (8-90)

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!TA)N) 472 GROVER 13 MI. 17r 30r r 474
¢ca ATANAURG.S. C.47 Ml.
ROAD CLASSIFICATION SCALE 1 :24 000
PRIMARY HIGHWAY LIGHT-DUTY ROAD,HARD OR 0 1 MILE
HARD SURFACE Mg/Ii1=7..=0 IMPROVED SURFACE -
0 7000 FEET I SECONDARY HIGHWAY
HARD SURFACE UNIMPROVED ROAD = = = c .-01 9
1 0 1 KILOMETER
Latitude 35°15'43" Longitude 81°17'54" sawiq wzt= I I
Map # F13SE Sub-basin 030837 CONTOUR INTERVAL 20 FEET
Stream Class C QUAD LOCATION
FMC Corporation
Discharge Class 31 32 02 NC0005177
Receiving Stream UT to Abernethy Creek Gaston County
Design Q 0.615 MGD Permit expires 9/30/01 Lithium Division WWTP

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REFERENCE: Base Map Source: USGS 7.5 Min.Topo. Quad.,•Bessemer City, NC(1993).
2000' 0 2000'• i FMC
BESSEMER CITY, NORTH CAROLINA
Approximate Scale: 1"=2000'
•
t;
SITE LOCATION MAP
_
QUAD LOCATION FIGURE
06/16/03 SYR-D85-LAS, LBR, DJH
37650001/37650n01.cdr

EPA I.D.NUMBER(copy from Item 1 Of Form 1) FormAppro
OMMBB No.20ve-
0-0086.
t 9 �„ Approval expires8-31-98.
9PlaaseI print or type in the unshaded areas only. 1 I�)Y*.rs) o7� A
FORM I U.S. ENVIRONMENTAL PROTECTION AGENCY
1 in fa 1 rik • APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
i L r. I EXISTING MANUFACTURING,COMMERCIAL,MINING AND SILVICULTURAL OPERATIONS
1 WOES Consolidated Permits Program
I I.OUTFALL LOCATION -
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
i A.OUTFALL B. LATITUDE C. LONGITUDE
NUMS:ER D. RECEIVING WATER(name)
(iLni ).O<O. 2.MIN. .1.1tC. I.DSO. 2.M.. 3. •EC.
ICYO 3 15 �-� `8� �� b4- (j.T. of ACSR6�6E.TH' CREEK.
_
too 4 3 5 I 43 RDi t 71 S - O.T 6,r- em-S C hi&
9
II.FLO ,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIESMIIIIIIIMIIIIIIIIIIIIIIIIIIIIMIMIIIIIIIII
A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent,
and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average
flows between intakes, operations, treatment-units, and outfalls. If a water balance cannot be determined (e.g, for certain mining activities),provide a
pictorial description of the nature and amount of any sources of water and any collection or treatment measures.
S. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater,sanitary wastewater,
cooling water,and storm water runoff;(2)The average flow contributed by each operation;and (3) The treatment received by the wastewater.Continue
on additional sheets if necessary.
Lour-I 2.OPERATION(S)CONTRI.UTING FLOW 3.TREATMENT
'FALLNOI b. AVERAGE FLOW a.DESCRIPTION Ib• LIST CODE6 FROM-
(list) I a.OPERATION(Rat) (Include units) I TABLE 2C-t
°�'1 i iv ai , SALE , �� Nb, q/w ) Nac) E.
.�'8 G? fie . X. V� LC,E R� a
14 . - Ro PemEA3v ;
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1.OFFICIAL USE ONLY(affluent guidelines assb-ceg/gor(fa)
:
=PA Form 3510-2C (8-90) PAGE 1 OF 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
XYZ3(complete the following table) ❑NO(go to Section III)
3. FREQUENCY 4, FLOW
S. OUTS ALL 2. OPERATiONrS) a. DAYS b.MONTHS a. FLOW RATE b.TOTAL VOLUME
NUMBER CONTRIBUTING FLOW PER WEEK PER YEAR (in mgd) (specify with units) 4 OUR-
1.LONrs TERN Z.MA%IMUM I.LONO TERM ] %IMUM ATION
gist) �l7Sf) (specify (specify AVER TE• DAILY AVERAGE TI DAILY days)
average) average) (in
�fit.teuS
LUCK. 5 PEgivtEaS. 7 - -
'® L O pR®. ale — cled.0 0,015 --
•
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Waterat Act apply to your facility?IYI
YES(complete Item III-B). NO(to to Section IV)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
YES.(complete Item Ill-C) E No(go to Section IV)
C. If you answered"yes"to Item Ill-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units
used in the applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION 2. AFFECTED
U N C. ION,PRODUCT,MATERIAL. ETC. OUTFALLS
g, QATITY r<R DAY b,umvs or MewsuRE (specify) (list outfall numbers)
of �
•
IV. IMPROVEMENTS
A. Are you now required by any Federal,State or local authority to meet any implementation schedule for the construction,upgrading or operation of waste-
water treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,
but is not limited to, permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant
or loan conditions. vas(complete the following table) ,NO(go to Item IV-B)
IDENTIFICATION OF CONDITION. 2.AFFECTED OUTFALLS A.FINA 1 T DAcc2
ETC.
3.BRIEF DESCRIPTION OF PROJECT PLIANGE
AGREEMENT,. e.Rs- •Ro-
•.No. b.•ousts or niscNAAAA
la 1
•
-B. OPTIONAL:You may attach additional sheets describing any additional water pollution control programs(or other environmental projects which may affect
your discharges) you now have underway or which you:plan. Indicate whether each program is now underway or planned,and indicate your actual or
• Planned schedules for construction, MARK `x (!'DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
a►:
EPA Form 3510-2C(Rev.2-86) PAGE 2 OF 4 CONTINUE ON PAGE 3

•
1
EPA 1.0. NUMBER(copy from Item I of Form I)
CONTINUED FROM PAGE 2 '1 -31C-• °' 9
+V.INTAKE'AND'EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding—Complete one set of tables for each outfall—Annotate the outfall number in the space provided.
NOTE: Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be
discharged from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your
possession.
1. POLLUTANT 2.SOURCE 1. POLLUTANT 2. SOURCE
1\31 A
•
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or
byproduct?
V.y (list all such pollutants below) NO(go to Item VI-B)
LC,ALDR.IbE
Mess. C'1J A -- U'E-b L 1 /T EC P L.TY
TH1S PL ; qs,„s sT M AMR C L.' Ttkft0q
PAGE 3 OF 4 CONTINUE ON REVERS
EPA Form 3510-2C (8-90)

i
CONTINUED FROM THE FRONT
VII. BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made ()many of your discharges or on a
receiving water in relationio to your discharge within the last 3 years?
IJ�Yes(identify the test(s)and describe their purposes below) ENO (go to Section VIII)
E . C C)1 p CAC. TOY+.1 GIfi' C. IVJFI PM A4I AI)
P Pc I-� ME-ET CA.)?-1" MPbSS
VIIi.CONTRACT ANALYSIS INFORMATION
' Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
xe
vEs (list the name,address,and telephone number of,and pollutants El NO(go to Section IX)
',, analyzed by, each such laboratory or firm below)
C.TELEPI-IDNE D.POLLUTANTS ANALYZED
A. NAME S.ADDRESS (area code&no.) (list)
1-'F..l Lc- 4 �'321 q1 e) a` s
C (4_i.42)` )NC. Zate. 7c -5E:9-lam ALL-
Tsmp. 4 c )
11X,CERTIFICATION ;- -, . . _ ;
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who manage the system or
!- those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.
I am aware that there are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A. NAME &OFFICIAL TITLE(type or print) e, PHONE NO.(area code& no.)
C.SIGNAT E D. DATE SIGNED
.. 0&-7 .-7-X-54.4-) — Zzi-A-22— pd-A24. ...6n_ (7D4-,)r&c:t'----x -co
I ' ' \ 0-A1-74/
PAGE 4 OF 4
EPA , 3510-2C (8-90)

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•
- STORMWATERS
ROOF DRAINS: 164,862 a.I.
-50%OF MANF.BLDG.90,500 SF DRAINAGE y
FLOWS TO PLANT PROr=o9 SEWER AREA
VIA.NORTH AND SOUTH DRAINS INCLUDES
ROOF DRAINS
1 MISC.SALTS.CAT PHOSPHATE WASTE _�1 MH11 EXPO
^ WATER TANK PUMP(-100 GPM)Q) BELOW
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EXPOSED `---
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uJ
Q HYPO EFF. HYPO EFF. -10 GPM(I)SHIPPING AREA COOLING TOWERS
SAMPLE E0009 p SAMPLE[0004
0 aMH N
a - EXPOSED
•
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Ce O BOILER BLOW DOWN(-15 GPM) O EXPOSED
45
NORTH DRAIN SAMPLE
GU-I ® UCL RO.UNIT AND CONDENSATE(0-90 GPM)(0 EAR COLLECTED AT {g5
W O F CIA LAB COOLING WATER(-15-50GPM) S
im Q, 7,AUTO SAMPLERUQ.;y y PLANT EFF.Ea001 H_01 ULFURIC r
. NW i Tip 1 ADDmoN,PH CONTROL
•kb
.!±2,
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PLANT PROCESS SEWER
FLUME
O South Drain NOT IN USE
. M-IA CONDENSATE FROM
EXPOSED PHARMACEUTICAL CARBONATE
�/ •
FACILITY BOILER BLOW DOWN
LL -20 GPM(I)
1W-- HY9FLQW.E SBUBBER.A A n-
Q ROOF DRAIN °I n MAG.
--METER FLOW
O -1 GPM(I)COMPRESSOR CONDENSATE MH
47 EXPOSED T�
'
WEST PLANT SITE SURFACE OUTN DRAIN SAMPLE EON
AND ROOF DRANAGE ^ LITHIUM HYDROXIDE CIRCUIT RO y COLLECTED AT eT
7 w LEGEND PERMHA IE UNIT 0-70 ppD)(I) g O
STORM WATERS FROM PERIMETER SURFACE STORMWATER FLOWS
OF R&D POND AND SOUTHERN y' ly
PORTION OF KILO LAB ir ir
_EAST CANAL STORMWATER CONVEYANCE ; PROCESS WASTE WATER FLOWS
2 5TOFIN'W t YsFRO EA5T)R i1OF-NANT
(I)INTERMITTENTFLOW
n @o
m STORMWATERS MANHOLE OR
$ O STORM DRAIN
STORMWATERS n 3 INLET
9R AREA
POND A SIPHON SYSTEM
95,1989p ILL
l.
•
PLANT INCLUDES ROOF DIVERSION PIPE LINE TO LOWER POND
HEADER � AND RETENTION EMERGENCY SPILLWAY OVER FLOW
��__l___�I� DRAINSSEDIMENTATION
DIVERSION DIVERSION '
�� GATE DIVERSION i---.I___L_� t
GATE \ / • ,
OVERFLOW(I) -� GROUNDWATER I ___:„...........„---""'-----
1 -. CHARGE 'V'NOTCH
DIVERSION WIER BOX J— F
I __ O FLOW,0-0.815 MGD
` I GATE
1
1 1 } -� f - - _ POINT
GROUNDWATER •R&D SEDIMENT POLISHING SOURCE
GE gkRE94EA P_MARMV.AT t3_110sT_D_F1nKC1e_lt—, OUTFACE 001
POND MANUF.PARKING LOT,AND AREA 4 BLUE BLDG. POND PONDere
• STORMWATER -4wg1-
WEST CANAL STORMWATER CONVEYANCE OUTFACE 004
RECTANGULAR UNNAMED TRIBUTARY
TO ABERNETHY CREEK
• WIER
•
• fMC MC Corporation
Lithium Division
Bessemer City,NC
PERRE a DRAWN NPDES Renewal 2005
POINT AND STORMWATER
• DISCHARGE FLOW SHEET
Reference Form 2C II.A and II.B DAI.,,-µACNE OM-DATE
APPROVED- JOS NO-OFE
of NPDES Permit application .PRINT µD Al tt SCALE-SCALE 0 r* DESIGN/ENC.
y� OF., °qr�ado DRAWING NO 1 REV.

I
EPA 1.0. NUMBER (copy from Item 1 of Form I) 1
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of
��0���'q��
this information on separate sheets(use the same format)instead of completing these pages.
SEE INSTRUCTIONS.
.....+..Ir,N.I 26 t t 'Y'1( I F It pI 1,ky41�1'I 1111 C'1 p L pppp!qqIy y1p5I F yt!!I 7 Ik p { IN
p ,
VI k )�I lill. IF��i l EI[II' E� I .�i1{Ii17I��}+ Il'i 7`!. � f -y..Ili 9WId I� 9 i14�IIjIIII �Itl �.,'l II •
OVT FALL NO.
1111 ! 't�l'� .u` p� .�:r, �I�r,1. .I 11". ''� L1 1 i & ,.I,I�,•I t',i�.�I� ils
V. INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-0 + 1 p' /�/�I
PART A-You must provide the results of at least one analysis for every pollutant in.this table. Complete one table for each outfall. See instructions for additional details. V�/
2. EFFLUENT l 3. UNITS 4. INTAKE (optional)
I. POLLUTANT a. MAXIMUM DAILY VALUE MAXI M 3p PAY VALUE C.LONG11 f.}�M y{[R�a VALUE I (specify I/blank) a. LONG TERM
z auailabl¢) Itl aValfable) d, NO.OF AVERAGE VAl U b. NO. OF
1 a.CONCEN-
( ) (z) MAls (I) (x)MASS (a) (t) MAss ANALYSE$ TRATION b.MASS (I) � (x) . ANALYSE
CONCENTRATION CONCENTRATION CONCENTRATION CONCENTRATION
Oxygena.
Demand I
q ...gin—� ' ,II?b.Chemical i CIZ
(COD)n Demand RIEI tirlaal , I ! — ( `f</IN/
e.Total Organic �/ i — /V.
Carbon(TOC) Y Ifl-1 :.� ��
S.Total Suspended er.a -- _- �� �� 16 P�
Solids(TSS) — 4J , �
e.Ammonia(as N) 014.4.
-�__ I
a- I --..
1w ,!r _
VALUE/_ VALUEe VALUE VALUE
t. Flow Q Goo M`.`��r.© I%I r` t) .....� .
® '+�. ..IM..
y.Temperature VALUE VALUE VALUE VALUE
(winter) 1Z .3.4.
Z .3o la. °C
h. Temperature VALUE VALUE VALUE ° VALUE
(summer) as 6° .�..�' C
MINIMUM MAXIMUM MINIMUM MAXIMUM •
I.PH 1 1' 51 , 4-0
STANDARD UNITS
PART 9- Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant
which is limited either directly,or indirectly but expressly,in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant.For other pollutants for which you mark
column 2a,you must provide quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
1.POt.LUT- 2. MARK'X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
ANT AND a. cc- b. es- a.MAXIMUM DAILY VALUE b.MAXIMtL1M 9A pAY VALUE C.LONG TVRM gYR VALUE a. LONG TERM
CAS NO. LIEVECUEVEC (ItQVaUaOte) (ttaVaitable� dNO.OF8.CONCEN- AVERAGE VALUE b NO.OF
fir available) PRE. aunt II) (x)MACS la) (x)Mws9 (I) ANAL- TRATION b.MASS I.)
ANAL-
GONCENTRATION CONCENTRATION • CONCENTRATION (x) IA ASS YSES CONCENTRATION (t)MASS YSES
a. Bromide
(24959-67-9)
b.Chlorine,
Total Residual
c.Color 5 E E. A --ri-p, 0 4-' ,,,,,b .
PR .com L lot El,e. REppcpp.,:r-
. _
d. Fecal
Collform
e.Fluoride
(18984-48-8)
f.Nltrate—
Nitrite(as N)
PAGE V-i •
EPA Form 3510-2C (8-90) CONTINUE ON REVERSE

ITEM wi a-CONTI.Wu C.FI�v + >Raf�rrt........ •
• • ..
i f;LU.Tr . 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
"Afrt AND a.■e-b,■E- s.MAXIMUM DAILY VALUE b.MAXIS{ M 3y a Y VALUE C.LONG 7 M VALUE
•• ;tAS NO, uEVE Ievco (I0...Rat:, (` availa��e NG g
•eE- As- d.N AL- a.COKCEN- AVt AG ETV ALUE
((favat(able) sENr sENr (�) (;)Mwss (') (,) ANAL- TRATION b. MASS b.NO.OF
ANAL-
coNCENTgA ,,,,, CONCENTRATION (2)MASS CONCENTRATION 0) MASS YSES ('►
flj•Nlt►9Pan� • CONCENTRATION (2) MASS YSES
Tdt'(Organic
(os'A')'
.h.A.il and
Grwis
I,.Phorphorua
(a[Pl,Total
(7723-14-0)
I.ftaidloactivity
(1)'Alpha,
Total
(2)Beta. •
•
Total••
•
•
(3) Radium,
Total
(4) Radium
226,Total
k.Sulfate •
(as SO4)
(14808-79-8)
I.Sulfide
(as 8)
m.Sulfite
(as SO3)
(14265-45.3)
n.Surfactants
o.Aluminum, •
Total
(7429.90-5)
P.Barium,
Total
(7440-39-3)
q.Boron,
Total
(7440-42-8)
r.Cobalt,
Total
(7440-48-4)
L Iron,Total
(7439-89-6)
t.Magnesium,
Total
(7439-95-4)
u.Molybdenum,
Total
(7439-98-7)
v. anganese,
Total
(7439-96-5)
w.Tin,Total
(7440.31.5) .
x.Titanium,
Total
(7440-32-6)
•
•
•
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V•3

EPA 1.0..0 NUMBER \
(copy from Item I of Form I) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C • NCt OOc11 1(
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark"X"in column
2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2-a(secondary industries,nonprocess
wastewater outfalls,and nonrequired GC/MS fractions),mark"X"in column 2-b for each pollutant you know or have reason to believe is present.Mark"X"in column 2-c for each pollutant you
believe is absent.If you mark column 2a for any pollutant,you must provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results
of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein,acrylonitrile,2,4
• dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in
concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to
be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages) for each outfall.See instructions for additional details and requirements.
1.POLLUTANT z.MARK'X' 3. EFFLUENT • 4. UNITS 5. INTAKE (optional)
AND CAS b.MAXI M 3 try'.
NUMBER a.rclT b.■E• G ac- C.MAXIMUM DAILY VALUE ) VALUE C,LONG 7 RM AYR�s VALUE d NO.OF e. LONG TERM b.NO.OF
INC IEVEDLIEVIM au a auto Cllef a. CONCEN- AVERAGE VALUE
(lfauallable) o�lR• ieNrT StHT (II ANAL- b.MASS _ ANAL-
Of CONCENTRATION (_)MASS CONCENTRATIONI tx)_M A!! CONCENTRATION i=)MAS! Y$E$ TRATION (I TRATIONN (Ti MAs! YSES
METALS,CYANIDE,AND TOTAL PHENOLS
1M,Antimony,
Total(7440-36-0) •
2M.Arsenic,Total
(7440-38-2)
3M.Beryllium,
Total,7440.41.7)
4M.Cadmium, .
Total(7440-43-9)
5M.Chromium,
Total(7440-47.3)
5M.Copper,Total
(7440-50-8)
7M.load,Total
(7439-82-1)
8M.Mercury,Total ,
(7439-97-6)
9M..NIokal,Total
(744070210)
10M,Selenium,
Totril'(7782-49-2)
47 �Stiliiar,Total':
12M.Thallium,
Total.(7440-28-0)
13MrZino,Total
(7440-86-6)
14M:Cyanide,
Total(57-12-6)
.15M.Phenols,
Total
•019XINV
2 31 ATetra- DESCRIBE RESULTS
c4iorlidlbinzb-P-
PIo 1n(17B4-91.6)
' EPA Form $510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
p1.POLLUTANT T 2.MARK •X• 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
AND CAS Mu g�
NUMBER ar[rT�b [[-Jun-, a. MAXIMUM DAILY VALUE b•MAXI M b Y VALUE c.LONG TERM AYR VALUE
Ca Icv[p u[v[, aua a [) rt/auatiab(e� d.NO.OF AVERAG.K VALVE b.N0.01
a.CONCEN-
((Javailable) ou e- {sNT {CNT LII (1)NIA" (t) _ 1— ANAL- b, MASS ANAL-
II)GONG[NTN AT ION .CONC[NTT AT ION (1)�^ [ CO N CC N Tf.IO A TION Ill Hwrt ANAL-
YSES TRATION CONC[N• (1 MA{{ YSES
TR nylON )
GC/I11S FRACTION—VOLATILE COMPOUNDS
IV.Acroleln
(107-02-8)
2V.Acrylonitrile
(107-13-1)
3V.Benzene •
(71-43-2)
4V.Ells(Chloro-
methyl)Ether
(542-88-1)
5V.Bromoform
(75-25-2)
6V.Carbon •
—
Tetrachloride
(56.23-5)
7V.Chlorobenzene
(108-90-7)
8V.Chlorodi-
bromomethene
(124-48-1)
•
9V.Chloroethane
(75-00.3)
10V.2-Chloro-
ethylvinyl Ether
(110-75-8)
11V.Chloroform
(67-66-3)
12V.Dichloro-
bromomethene
(75-27-4)
13V.Dichloro-
dif luoromethene
(75-71-8)
14V.1,1-Dichloro-
ethane(75-34-3)
15V.1,2-Dlohioro-
ethane(107-06-2)
16V.1,1-Dlchloro-
ethylene(76-35-4)
17V,1,2-Dichloro- •
propane(78-87-5)
18V.1,3-Dlchloro-
propylene(542.75-8)
19V.Ethylbenzene
(100-41-4) •
20V.Methyl
Bromide(74-83-9)
•
21V.Methyl.
Chloride(74-87-3)
EPA Form 3510-2C (8-00) PAGE V-4
CONTINUE ON PAGE V-I

CONTINUED FROM PAGE V 4 •
1.'POLLUTANT Z.MARK•X• • 3. EFFLUENT 4. UNITS 5, INTAKE (optional)
AND CAS
NUMBER wTcsr' b.i[- C.s[- a. MAXIMUM DAILY VALUE b.MAXIM�ljM 39 pAY VALUE c.LONG T atl AVPG VALUE dNO.OF a. LONG TERM b.NO.OF
IMG uevcw.lcvc� (17 availa0{e) (( avallaDle/ a.CONCEN- ANAL_
ae- /R[• Ate• ANAL- b. MISS
(((available) Dula- s[NT scNr (t). (i) awss (I) (a)mnis (') (a) ..ss YSES TRATION YSES
rO CONCENTRATION CONCENTRATION CONCCNTRATION TPIATION
0C/1S FRACTION—VOLATILE COMPOUNDS(continued)
22V.Methylene •
Chloridi(75-09-2)
23V..1 1,2,2-Tetra-
ch)0rdethene
(79-346)
24V,Tetrachloro-
ethylene(127-18-4)
25V.Toluene
(108=88-3)
•
26 V.'1,2-Trans-
Dichloroethylene
(186-60.5)
•
27V.1,1,1-Tri-
•
chloroethene
(71-56-6)
28V.1,1,2-Trl-
chloroethene
(79-00-5)
29V.Trlchloro-
ethylene(79-01-6)
30V.Trichloro-
fluoromethane
(75-69-4)
31 V.Vinyl
Chloride(75-01-4)
GC/MS FRACTION—ACID COMPOUNDS
•
1A.2-Chlorophenol •
(96.67.8)
•
2A.2r4Dichloro-
'phanol(120-83-2)
•
3A.3;4Dimethyl-
phenol(106.67-9)
4,6-Dinitro-O-
Cresol(534-52-1)
6A't2;4•Dlnitro-
phenol(61-28-5)
•
SA.2-Nitrophenol
(88.75-6) •
•
7A.4-N itrophenol
(100-02-7)
•
8A.P-Chioro-M-
• Cresol(59-50-7)
9A.'1•Pentachioro-
phatioi(87-86-5)
fps;Phenol
z)..
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
1.POLLUTANT 2.MARK 'X' 3. EFFLUENT 4. UNITS 5. INTAKE AND CAS (optional)
NUMBER a.""" b.mac- C•e- a. MAXIMUM DAILY,VALUE i� P
O.MAXIM M 3U pAY VALUE C.LONG T M G.VALUE
ti,ev eo L,evcn '1 bi ) f`� �� c1.NO.OF a. LONG TERM
(lf Qaala e s aua[1a e) a-CONCEN- AVERAGE VALVE h.NO.OF
(if4Vai1,01e) OVIa• aenT serer I,' (2i.,^ss 1,1 ANAL' b. MASS lij ma." V5E5
GO Cone......ror. cencenrNwnon (�) ...ASS CO.,Cr NrlN^T,on (�I••^ss VSES TRATION I,j conce N.
1,1AT10N
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS
1 B.Acenaphthene
(83-32.9)
2B.Acenaphtylene
•• (208-96-8)
3B.Anthrecene •
(120-12-7)
48.BentidIne -
(92-87-5)
58.Benzo(a) — —
Anthracene
(56-55-3)
68, Benzo(a)
Pyrene(50-32-8)
7B.3,48enzc- ,-----r—
fluoranthene
(2054912)
88.Benzo(ghi)
Perylene •
(191:24-2)
98.;¢enz0:(k) r--- I
Fluorinthene
(207-08-9)
1OB;Bit(2-Chloro- --
sthoxy)Methane
(111-91-1)
1113.BIN(2•Chloro-
ethyl)Ether
(111.444)
128.Bit(2-Or/oroiso-
•
ProPM Ether(102.604) •
13B..Bie(2-Ethyl- — -
hexyl).Phthalate
(1.1741-7) •
' ,14 4B!'omo-
. ){(Plifnyl.
4:E{ '(101-55-3) '
-1),IB.rButyl Binzyl •
Al1tfi)ati(86=58-7)
rro
Ifs; ,` 1llo.
'• 12-3)
i 15 f4tiry ene
121841.-9S', '
;19BADIOnzo(a,h)
i`Arithfae4ne
(53-29-3) '
20B.1,2-0lchioro-
benzene(95-50-1)
218.1,3-DIchloro-
benzenei(541-73-1)
EPA Form 3510-2C (8-90)
PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
1"POLLUTANT z.MARK •x•
3. EFFLUENT 4, UNITS 5. INTAKE (op rinna!)
AND CAS b.MAXI M ;, AY VALUE c.LO NG T�jtM y RG•VALUE
NUMBER aTt'T' b rc• c re- e. MAXIMUM DAILY VALUE Y S! ) (I/aValla�(a) J.NO.OF a. LONG TERM b,NO.OF
INo ts:v ea lAev cq. I OUata a a. CONCEN• AVERAGE VALVE
(ifovailable) OY�iR- 1cNT aewT I') ANAL- b. MASS
ANAL-
an Ca NC4NTRATION 1■I s+us coNceRTRATIow I+I ..Ass CONCe!TINATTON 1+1 ..Ass YSES TR ATION ( }coNc eN- I1) .+Ass YSES
TRATIaN
GC/MSFRACTION—BASE/NEUTRAL COMPOUNDS(continued'
ri 7•8:'1;4-bichloro-
1:teniteni(106.46-71
4 f:�j;(3�,3'-DIchloro
P hyl
#y+ •
{' -.Butyl
pinitro •
-
.. •
,021.14.2)
g; N 0a),biitro-
-tolueyla{606-2b-2)
'208.;D1-N-Octyl
-Phthalate
(1`I7.84.0)
3080,2712lpheny(-
6ydg4ifii{as Also-
.bensenej(122-66-71
310;Fluoranthene
---y
(206-44M
328:::Fluorene
•
33e40111,41000b•n2re •
11 . •
34B..Haxe-
•chlorobutedlene
(87.68.3)
358.Hexachloro-
cyalopentadlene
(77-47-4)'
368.Hexachloro-
ethane(67-72-1)
378.Indeno
(1,2,3-cd)Pyrene
(193-39-6)
38B.Isophorone
(78-59-1)
39B.Naphthalene
(91-20-3)
40B.Nitrobenzene
(9B-96-3)
418.N-Nitro-
sodlmethylamine
(62-75-9)
428.N-Nitrosodi-
N-Propylamine
(621.64-7) •
EPA Form 3510-2C (8-90) • PAGE V-7 . . CONTINUE ON REVERSE

•
CONTINUED FROM THE FRONT
—
I.POLLUTANT z.MARK•x• 3. EFFLUENT --� 4. UNITS 5. INTAKE (.,prin,lol)
AND CAS
' NUMBER at..,"' b..E- a•E- a.MAXIMUM DAILY VALUE b. MAXIMUM 3 Y VALUE c.LONG TWa y'(R?+ VALUE
INC LIfV EC LI[V Eft (1/QUQt�gP, (tj QU6llQblBJ d.NO.OF AVa. LONG ERA E VALUE
(�.NO.OF
ANAL- a-CONCEN- b.MASS ALUE(if4Ue110bIC) ou711- M; teat (.IANAL-
(�I .Ass I'1 (rl ..Ass YSES TRATtON (,i CONCEn-
¢o cone ION (2)MASS CONcs:nTOATTON CONCAATOATIOA 1�1..wss 'YSES
YAATion
GC/MS FRACTION—SASE/NEUTRAL COMPOUNDS(continued)
438.N•Nitro-
sodiphenylamine
(86-30-6)
448.Phenanthrene
' 1
(85-01-8)
46B.P.yrene
(.128.00.0)
468:1,2,4-TO-.
bll(gcobsnzene.
f� N FRACTIO PESTICIDES
2.(19 S4) x
( , 6)
(31 x
(68 9-9)C
(68�9=9)
•
1319-86-8) •
(5 Chlordane `i
2(5 3)
(60.29.3) X. '
8P.
(72 55-9) ` '
•
(7 54-4,4'8) `�
10P. DIeldrIn
•
(80-0-67-1)7-1)
•
• ,X
(1P•29-7) alfan X
(115.29.7)
12P.a-Endow(fan X
L
(115-29-7)
13 Endosulfan
Sulfate
(1031-07-5)
14P
(72- Endrin
20-8$)72.
15P. driri
Aldehyde
(7421-93-4)
Heptachlor
(76-44$)
EPA Form 3510-2C (8-90) PAGE v-8 CONTINUE ON PAGE V-9
•
>i

F • - • _
EPA I. NUMBER(COPY from Item I of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-8 I v"'�-�COO—I1 19(Q+ - VO I
1.POLLUTANT 2.MARK •x' 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
AND CAS b.MAXIM id 3 Y VALUE C.LONG TERM A�[RG VALUE NUMBER a rH sr b si- c sa- S.MAXIMUM DAILY VALUE ( (0 0A (`(aaaA R ' J.NO.OF a. LONG TERM b.NO.OF
c uev ea uev erava a ANAL- a,CONCEN- b. MASS AV FRAGg VALVE
(if available) oui°- iiikir sehr (2)i+AssANAL-
(,)Ep CONCENTRATION CONCEN,TRA TION (2)�int5 f.O,+C C',T(anTlOn NI Mn5t VSES TRATION CO CO„N- (2)MAst VSES
GC/MS FRACTION—PESTICIDES(continued)
17P.HeptachlorEpoxide -
- ►(102467-3)
)
18P.PCB-1242 IA`
(53469-21-9)
19P,PCB-1254
(11097-69-1)
20P.PCB-1221 -
(11104-28.2)
21P•PCB-1232 X -- --
(11141-16-5)
22P.PCB-1248
(12672-29-6)
23P.PCB-1260 �/
(1109S-82-5) +Al
24P.PCB-1016
(12674-11-2)
25P.Toxephene
(8001-35-2)
•
PAGE V-9
:PA Form 3510-2C•(8-90)

r
\::\V‘qP`,;'';
sl
ease Narrative.
'" ''LtI�Q 71fR1 MC
Date: 2/28/05
Company: FMC Corp.Lithium Division Client Project 1D: NPDES Renewal 2/9/05
Contact: Rodney Willis Prism COC Group No: G0205278
Address: Seven LakePointe Plaza
2801 Yorkmont Rd.,Suite 300
Charlotte,NC 28208
The attached Laboratory Report contains the analytical results for the project identified above and includes a
Chain-of-Custody copy.
Data qualifiers are flagged individually on each sample. A Key Reference for the data qualifiers appears at the bottom of this page.
Quality control statements and/or sample specific remarks are included in the sample comments section of the
laboratory report for each sample affected.
Please call if you have any questions relating to this analytical report.
Data Reviewed by: C ra Rusmisell Proj' Manager: Whitney Munroe
Signature: i4 d� he Signature: iltite'j Pyt ---
Review Date: 2/28/05 Approval Date: 2/28/05
Data Qualifier Key Reference:
#: Result outside of QC Limits
B: Compound also detected in the method blank
DO: Compound diluted out.
E: Estimated concentration,calibration range exceeded
J: The analyte was positively identified but the value is estimated below the reporting limit
JH: Estimated concentration with a high bias
JL: Estimated concentration with a low bias
M: A matrix effect is present
T: Tentatively identified compound. The concentration is estimated.
Note: This report should not be reproduced,except in its entirety,without the written consent of Prism Laboratories,Inc.
449 Springbrook Road,P.0.Box 240543,Charlotte,NC 28224-0403
Phone: [phone] Toll Free: 800/529-6364 Fax: [phone]
F:\common\casenarrative Revised 4/20/04 Revised 4/20/04

•
NC Certification No.402
SC Certification No.99012 Laboratory Report
NC Drinking Water Cert.No.37735 3/1/05
F8i smvicsAmh 8.EvironmenrtasaWan: FL Certification No.E87519
FMC Corporation Lithium Division Project Name: NPDES Renewal Client Sample ID: 001
Attn: Rodney Willis Sampling Prism Sample ID: 110704
Seven LakePointe Plaza Project ID: NPDES Renewal COC Group: G0205278
2801 Yorkmont Rd.Ste.300 Sample Matrix: Water Time Collected: 02/09/05 9:45
Charlotte,NC 28208 Time Submitted: 02/09/05 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Puroeable Organics by GC/MS
1,1,1-Trichloroethane BRL mg/L 0.0050 0.00075 1 624 02/18/05 14:49 erussell Q03240
1,1,2,2-Tetrachloroethane BRL mg/L 0.0050 0.00062 1 624 02/18/05 14:49 erussell Q03240
1,1,2-Trichloroethane BRL mg/L 0.0050 0.00063 '1 624 02/18/05 14:49 errssell Q03240
1,1-Dichloroethane BRL mg/L 0.0050 0.00039 1 624 02/18/05 14:49 erussell Q03240
1,1-Dichloroethene BRL mg/L 0.0050 0.00065 1 624 02/18/05 14:49 erussell Q03240
1,2-Dichlorobenzene BRL mg/L 0.0050 0.00023 1 624 02/18/05 14:49 erussell Q03240
1,2-Dichloroethane BRL mg/L 0.0050 0.00061 1 624 02/18/05 14:49 erussell Q03240
1,2-Dichioropropane BRL mg/L 0.0050 0.00077 1 624 02/18/05 14:49 erussell Q03240
1,3-Dichlorobenzene BRL mg/L 0.0050 0.00033 1 624 02/18/05 14:49 erussell Q03240
1,,1-Dichlorobenzene BRL mg/L 0.0050 0.00071 1 624 02/18/05 14:49 erussetl Q03240
'-Chloroethyl Vinyl Ether BRL mg/L 0.010 0.00044 1 624 02/18/05 14:49 erussell Q03240
Acrolein BRL mg/L 0.10 0.012 1 624 02/18/05 14:49 erussefi Q03240
Acrylonitrile BRL mg/L 0.10 0.0063 1 624 02/18/05 14:49 erusseit Q03240
Benzene BRL mg/L 0.0050 0.00035 1 624 02/18/05 14:49 erussell 003240
Bromodichloromethane BRL mg/L 0.0050 0.00083 1 624 02/18/05 14:49 erussell Q03240
Bromoform BRL mg/L 0.0050 0.00036 1 624 02/18/05 14:49 erussell Q03240
Bromomethane BRL mg/L 0.010 0.0018 1 624 02/18/05 14:49 erussell Q03240
Carbon Tetrachloride BRL mg/L 0.0050 0.00062 1 624 02/18/05 14:49 erusselt Q03240
Chtorobenzene BRL mg/L 0.0050 0.00023 1 624 - 02/18/05 14:49 erussetl Q03240
Chtoroethane BRL mg/L 0.010 0.00072 1 624 02/18/05 14:49 erussetl Q03240
Chloroform BRL mg/L 0.0050 0.00063 1 624 02/18/05 14:49 erussell Q03240
Chloromethane BRL mg/L 0.010 0.57 1 624 ' 02/18/05 14:49 erusselt Q03240
cis-1,3-Dichloropropene BRL mg/L 0.0050 0.00067 1 624 02/18/05 14:49 erussell Q03240
Dibromochloromethane BRL mg/L 0.0050 0.00072 1 624 02/18/05 14:49 erussell Q03240
Ethylhenzene BRL mg/L 0.0050 0.00031 1 624 02/18/05 14:49 erussell Q03240
rn,p-Xylenes BRL mg/L 0.0050 0.00061 1 624 02/18/05 14:49 erussell Q03240
Methylene Chloride BRL mg/L 0.0050 0.0011 1 624 02/18/05 14:49 erussell Q03240
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Toll Free Number:.1-800/529.6364 - Fax:[phone] Page 1 of 8

i
Ci
NCCertiflcatonNo.402 Laboratory Report
SC Certification No.99012
u • • NC Drinking Water Cert.No.37735 3/1/05
e 1 ' ._.;" FL Certification No.E87519
Fell Service Analytical 8 Environmental Sehtliarm
FMC Corporation Lithium Division Project Name: NPDES Renewal Client Sample ID: 001
Attn: Rodney Willis Sampling Prism Sample ID: 110704
Seven LakePointe Plaza Project ID: NPDES Renewal COC Group: G0205278
2801 Yorkmont Rd.Ste.300 Sample Matrix: Water Time Collected: 02/09/05 9:45
Charlotte,NC 28208 Time Submitted: 02/09/05 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
o-Xylene BRL mg/L 0.0050 0.00026 1 624 02/18/05 14:49 erussell Q03240
Tetrachloroethene BRL mg/L 0.0050 0.00038 1 624 02/18/05 14:49 erussell Q03240
Toluene BRL mg/L 0.0050 0.00024 1 624 02/18/05 14:49 missal! Q03240
trans-i,2-Dichloroethene BRL rng/L 0.0050 0.00081 1 624 02/18/05 14:49 erussell Q03240
trans-1,3-Dlchloropropene BRL mg/L 0.0050 0.00045 1 624 02/18/05 14:49 erussell Q03240
Trichioroethene BRL mg/L 0.0050 0.00079 1 624 02/18/05 14:49 erussell Q03240
Trichiorofluoromethane BRL mg/L 0.010 0.00039 1 624 02/18/05 14:49 erussell Q03240
Vinyl Chloride BRL mg/L 0.010 0.00072 1 624 02/18/05 14:49 erussell Q03240
Surrogate %Recovery Control Limits
Toluene-d8 90 75-121
Dibromofluoromethane 86 74-133
Bromofluorobenzene 70 69-139
Semivolatile Organic Comtzounds by GC/MS
1,2,4-Trichiorobenzene BRL mg/L 0.0098 0.0025 1 625 02/15/05 21:58 kelliot Q03122
1,2-Dichiorobenzene BRL mg/L 0.0098 0.0026 1 625 02/15/05 21:58 kelliot Q03122
1,2-Diphenylhydrazine BRL mg/L 0.010 0.0016 1 625 02/15/05 21:58 kelliot Q03122
1,3-Dichlorobenzene BRL mg/L 0.0098 0.0019 1 625 02/15/05 21:58 kelliot Q03122
1,4-Dichlorobenzene BRL mg/L 0.0098 0.0024 1 625 - .02/15/05 21:58 kelliot Q03122
2.4,6-Trichlorophenol BRL mg/L 0.0098 0.0018 1 625 02/15/05 21:58 kelliot Q03122
2.4-Dichiorophenol BRL mg/L 0.0098 0.0019 1 625 02/15/05 21:58 kelliot Q03122
2,4-Dimethylphenol BRL mg/L 0.0098 0.00066 1 625 02/15/05 21:58 kelliot Q03122
2,4-Dinitrophenol BRL mg/L 0.049 0.0066 1 625 02/15/05 21:58 kelliot Q03122
2,4-Dinitrotoluene BRL mg/L 0.0098 0.0082 1 625 02/15/05 21:58 kelliot Q03122
2,6-Dinitrotoluene BRL mg/L 0.0098 0.0016 1 625 02/15/05 21:58 kelliot Q03122
2-Chloronaphthalene BRL mg/L 0.0098 0.0022 1 625 02/15/05 21:58 kelliot Q03122
2-Chlorophenol BRL mg/L 0.0098 0.0022 1 625 02/15/05 21:58 kelliot Q03122
2-Methyiphenol BRL mg/L 0.0098 0.0018 1 625 02/15/05 21:58 kelliot Q03122
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Toll Free Number 1-800/529-6364 - Fax:[phone] Page 2 of 8

•
: NC Certification No.402 LaboratoryReport
P'' r SC Certification No.99012M
p NC Drinking Water Cert.No.37735 3/1/05
Fun ser,nan®yuoa&EmrNonmonm soiwons FL Certification No.E87519
FMC Corporation Lithium Division Project Name: NPDES Renewal Client Sample ID: 001
Attn: Rodney Willis Sampling Prism Sample ID: 110704
Seven LakePointe Plaza Project ID: NPDES Renewal COC Group: G0205278
2801 Yorkmont Rd.Ste.300 Sample Matrix: Water Time Collected: 02/09/05 9:45
Charlotte,NC 28208 Time Submitted: 02/09/05 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/me ID
2-Nitrophenol BRL mg/L 0.0098 0.0023 1 625. 02/15105 21:58 kelliot Q03122
3&4-Methylphenol BRL mg/L 0.0098 0.0017 1 625 02/15/05 21:58 kelliot Q03122
3.3"-Dichlorobenzidine BRL mg/L 0.049 0.0092 1 625 02/15/05 21:58 kefliot Q03122
4,6-Dinitro-2-methylphenol BRL mg/L 0.049 0.00086 1 625 02/15/05 21:58 kelliot Q03122
4-Bromophenytphenylether BRL mg/L 0.0098 0.0020 1 625 02/15/05 21:58 kelliot Q03122
4-Chloro-3-methylphenol BRL mg/L 0.0098 0.0017 1 625 02/15/05 21:58 kelliot Q03122
4-Chlorophenylphenylether BRL mg/L 0.0098 0.0016 1 625 02/15/05 21:58 keuiot Q03122.
4-Nitrophenol BRL mg/L 0.049 0.00059 1 625 02/15/05 21:58 kelliot Q03122
Acenaphthene BRL mg/L 0.0098 0.0019 1 625 02/15/05 21:58 kelliot Q03122
Acenaphthylene BRL mg/L 0.0098 0.0021 1 625 02/15/05 21:58 kelliot Q03122
Anthracene BRL rng/L 0.0098 0.00096 1 625 02/15/05 21:58 kelliot Q03122
Azobenzene BRL mg/L 0.0098 0.0016 1 625 02/15/05 21:58 kelliot Q03122
Benzidine BRL mg/L 0.049 0.0092 1 625 02/15/05 21:58 kelliot Q03122
Benzo(a)anthracene BRL mg/L 0.0098 0.00092 1 625 02/15/05 21:58 kelliot Q03122
Benzo(a)pyrene BRL mg/L 0.0098 0.00098 1 625 02/15/05 21:58 kelliot Q03122
Benzo(b)fluoranthene BRL mg/L 0.0098 0.0017 1 625 02/15/05 21:58 kelnot Q03122
Benzo(g,h,i)perylene BRL mg/L 0.0098 0.0021 1 625 02/15/05 21:58 kelliot Q03122
8enzo(k)fluoranthene BRL mg/L 0.0098 0.0019 1 625 02/15/05 21:58 kelliot Q03122
Bis(2-chloroethoxy)methane BRL mg/L 0.0098 0.0022 1 625 02/15/05 21:58 kelliot Q03122
Bis(2-chloroethyl)ether BRL mg/L 0.0098 0.0021 1 625 - ' 02/15/05 21:58 kelliot Q03122
Bis(2-chloroisopropyi)ether BRL mg/L 0.0098 0.0024 1 625 02/15/05 21:58 kelliot Q03122
Bis(2-ethylhexyl)phthalate BRL mg/L 0.0098 0.0007 1 625 02/15/05 21:58 keuiot Q03122
Butylbenzylphthalate BRL mg/L 0.0098 0.00069 1 625 02/15/05 21:58 kelliot Q03122
Chrysene BRL mg/L 0.0098 0.00056 1 625 02/15/05 21:58 kelliot Q03122
Di-n-butylphthalate BRL mg/L 0.0098 0.0014 1 625 02/15/05 21:58 kelliot Q03122
Di-n-octylphthalate BRL mg/L 0.0098 0.0022 1 625 02/15/05 21:58 kelliot Q03122
Dibenzo(a,h)anthracene BRL mg/L 0.0098 0.0011 1 625 02/15/05 21:58 kelliot Q03122
Diethylphthalate BRL mg/L 0.0098 0.0011 1 625 02/15/05 21:58 kelliot Q03122
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Toll Free Number.1-800/529.6364 - Fax:[phone] Page 3 of 8

,
NC Certification No.402 LaboratoryReport
; SC Certification No.99012 p
NC Drinking Water Cert.No.37735 3/1/05
roServim Marytkat a Emdtonmenhisektbns FL Certification No.E87519
FMC Corporation Lithium Division Project Name: NPDES Renewal Client Sample ID: 001
Attn: Rodney Willis Sampling Prism Sample ID: 110704
Seven LakePointe Plaza Project ID: NPDES Renewal COC Group: G0205278
2801 Yorkmont Rd.Ste.300 Sample Matrix: Water Time Collected: 02/09/05 9:45
Charlotte,NC 28208 Time Submitted: 02/09/05 15:10
• Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/me ID
Dimethylphthalate BRL mglL 0.0098 0.0014 1 625 02/15/05 21:58 kelliot Q03122
Fluoranthene BRL mg/L 0.0098 0.00092 1 625 02/15/05 21:58 kelliot Q03122
Fluorene BRL mg/L 0.0098 0.0014 1 625 02/15/05 21:58 kelliot Q03122
Hexachlorobenzene BRL mg/L 0.0098 0.0013 1 625 02/15/05 21:58 kelliot Q03122
Hexachiorobutadiene BRL mg/L 0.0098 0.0022 1 625 02/15/05 21:58 kelliot Q03122
Hexachlorocyclopentadlene BRL mg/L 0.0098 0.0024 1 625 02/15/05 21:58 kelliot Q03122
Hexachloroethane BRL mg/L 0.0098 0.0018 1 625 02/15/05 21:58 kelliot Q03122
Indeno(1,2,3-cd)pyrene BRL mg/L 0.0098 0.0017 1 625 02/15/05 21:58 kelliot Q03122
Isophorone BRL mg/L 0.0098 0.0016 1 625 02/15/05 21:58 kelliot Q03122
N-Nitrosodi-n-propylamine BRL mglL 0.0098 0.0022 1 625 02/15/05 21:58 kelliot 003122
N-Nilrosodimethyiamine BRL mg/L 0.0098 0.00098 1 625 02/15/05 21:58 kelliot Q03122
f•I-Nitrosodiphenylamine BRL mg/L 0.0098 0.0015 1 625 02/15/05 21:58 kelliot Q03122
Naphthalene BRL mg/L 0.0098 0.0022 1 625 02/15/05 21:58 kelliot Q03122
Nitrobenzene BRL mg/L 0.0098 0.0019 1 625 02/15/05 21:58 kelliot Q03122
Pentachlorophenol BRL mg/L 0.0098 0.0017 1 625 02/15/05 21:58 kelliot Q03122
Phenanthrene BRL mg/L 0.0098 0.00088 1 625 02/15/05 21:58 kelliot Q03122
Phenol BRL mg/L 0.0098 0.00088 1 625 02/15/05 21:58 kelliot Q03122
Pyrene BRL mg/L 0.0098 0.00089 1 625 02/15/05 21:58 keiriot Q03122
Sample Preparation: 1020 mL / 1 mL 625 02/11/05 13:30 srnanivanh P11779
Surrogate %Recovery Control Limits
Terphenyl-d14 66 10-154
Phenol-d5 22 10-48
Nitrobenzene-d5 71 22-103
2-Fluorophenol 31 10-59
2-Fluorobiphenyl 79 29-112
2,4,6-Tribromophenol 59 27-125
Ammonia Nitrogen by Automated Phenate Method
Ammonia BRL mg/L 0.50 0.013 1 SM4500-NH3 H 02/17/05 10:51 cmatthews Q03208
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Toll Free Number:1-800/529-6364 - Fax:[phone] Page 4 of 8

•
•
NC Certificaon No.992 LaboratoryReport
} ; SC Certification No.99012 „C
NC Drinking Water Cert.No.37735 3/1/05
Fri ServiceAnxyueal&Emwomx,wsautiona FL Certification No.E87519
FMC Corporation Lithium Division Project Name: NPDES Renewal Client Sample ID: 001
Attn: Rodney Willis Sampling Prism Sample ID: 110704
Seven LakePointe Plaza Project ID: NPDES Renewal COC Group: G0205278
2801 Yorkmont Rd.Ste.300 Sample Matrix: Water Time Collected: 02/09/05 9:45
Charlotte,NC 28208 Time Submitted: 02/09/05 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/me ID
Asbestos
Subcontract Report See Attached 1 See Attached
* Analysis Note for Subcontract Report: Subcontracted to EMSL Analytical, Inc.
Biochemical Oxygen Demand
SOD-5 BRL mg/L 3.9 1 405.1 02/10/05 13:23 agibson Q03167
Bromide by Ion Chromatography
Bromide 0.68 mg/L 0.10 0.054 1 300.0 02/10/05 4:25 mlandreth Q03019
Chemical Oxygen Demand
Chemical Oxygen Demand BRL mg/L 50 5.1 1 SM5220 D 02/17/05 10:45 tmaher Q03193
Color by PtCo Visual Comparison
Color 5.0 PtCo Units 5.0 5.0 1 110.2 02/10/05 14:31 mlandreth Q03005
Total Cyanide.Colorimetric Method
Cyanide,Total BRL mg/L 0.0020 0.0016 1 335.2 02/14/05 15:38 cmatthews Q03115
Sample Preparation: 500 mL / 500 mL SM4500-CN C 02/14/05 9:25 cmatthews P11813
Fecal Coliform by Membrane Filter
Fecal Coliform BRL CFU/100 ml 2.0 2.0 1 SM9222 D 02/09/05 15:15 mlandreth Q03013
Fluoride by Ion Chromatography
Fluoride 0.67 mg/L 0.10 0.069 1 300.0 02/10/05 4:25 mlandreth Q02991
Gross Alpha and Gross Beta Radioactivity
Subcontract Report See Attached 1 900.0
* Analysis Note for Subcontract Report: Subcontracted to Florida Radiochemistry Services, Inc.
Methylene Blue Active Substances(MBASI
MBAS BRL mg/L 0.10 0.049 1 SM5540 C 02/10/05 17:30 celfaki Q03251
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Tolf Free Number:1-800/529-6364 - Fax:[phone] Page 5 of 8

b NC Certification No.402
s SC Certification No.99012 Laboratory Report
i .. NC Drinking Water Cert.No.37735 3/1/05
d_"` ''' FL Certification No.E87519
Full Somme Analytical 8 Environmental Solutions
FMC Corporation Lithium Division Project Name: NPDES Renewal Client Sample ID: 001
Attn: Rodney Willis Sampling Prism Sample ID: 110704
Seven LakePointe Plaza Project ID: NPDES Renewal COC Group: G0205278
2801 Yorkmont Rd.Ste.300 Sample Matrix: Water Time Collected: 02/09/05 9:45
Charlotte,NC 28208 Time Submitted: 02/09/05 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/me ID
Mercury by CVAA
Mercury BRL mg/L 0.00020.000044 1 245.1 02/14/05 11:52 mstover Q03083
Sample Preparation: _: 20 mL / 30 mL 245.1 02/14/05 7:05 mstover P11800
metals by ICP
Aluminum BRL mg/L 0.50 0.018 1 200.7 02/23/05 17:58 mcampbell Q03200
Antimony BRL mg/L 0.0050 0.0030 1 200.7 02/23/05 17:58 mcampbell Q03200
Arsenic BRL mg/L 0.010 0.0036 1 200.7 02/17/05 20:39 mcampbell Q03200
Barium BRL mg/L 0.030 0.0015 1 200.7 02/17/05 20:39 mcampbell Q03200
Beryllium BRL mg/L 0.0010 0.0003 1 200.7 02/23/05 17:58 mcampbell Q03200
Boron BRL mg/L 0.50 0.16 1 200.7 02/17/05 20:39 mcampbell Q03200
Cadmium BRL mg/L 0.0050 0.0002 1 200.7 02/17/05 20:39 mcampbell Q03200
Chromium BRL mg/L 0.0050 0.0009 1 200.7 02/17/05 20:39 mcampbell Q03200
Cobalt BRL mg/L 0.0050 0.0006 1 200.7 02/17/05 20:39 mcampbell Q03200
Copper BRL mg/L 0.010 0.0017 1 200.7 02/17/05 20:39 mcampbell Q03200
Iron 0.058 mg/L 0.050 0.0074 1 200.7 02/23/05 17:58 mcampbell Q03200
Lead BRL mg/L 0.0050 0.0011 1 200.7 02/17/05 20:39 mcampbell Q03200
Magnesium 51 mg/L 0.050 0.0081 1 200.7 02/23/05 17:58 mcampbell Q03200
Manganese 0.29 mg/L 0.0050 0.0013 1 200.7 02/17/05 20:39 mcampbell Q03200
Molybdenum BRL mg/L 0.010 0.0032 1 200.7 . ' 02/17/05 20:39 mcampbell Q03200
Nickel BRL mg/L 0.010 0.0009 1 200.7 02/17/05 20:39 mcampbell Q03200
Selenium BRL mg/L 0.010 0.0056 1 200.7 02/23/05 17:58 mcampbell Q03200
Silver BRL mg/L 0.0050 0.0008 1 200.7 02/23/05 17:58 mcampbell Q03200
Thallium BRL mg/L 0:010 0.0048 1 200.7 02/17/05 20:39 mcampbell Q03200
Tin BRL mg/L 0.050 0.0088 1 200.7 02/17/05 20:39 mcampbeD Q03200
Titanium BRL mg/L 0.010 0.0018 1 200.7 02/17/05 20:39 mcampbell Q03200
Zinc BRL mg/L 0.040 0.0027 1 200.7 02/17/05 20:39 mcampbell Q03200
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Toll Free Number.1-800/529-6364 - Fax:[phone] Page 6 of 8

4 NC Certification No.402 Laboratory Report
SC Certification No.99012
NC Drinking Water Cert.No.37735 3/1/05
Service sauu FL Certification No.E87519
Full
FMC Corporation Lithium Division Project Name: NPDES Renewal Client Sample ID: 001
Attn: Rodney Willis Sampling Prism Sample ID: 110704
Seven LakePointe Plaza Project ID: NPDES Renewal COC Group: G0205278
2801 Yorkmont Rd.Ste.300 Sample Matrix: Water lime Collected: 02/09/05 9:45
Charlotte,NC 28208 Time Submitted: 02/09/05 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date>Tme ID
* Analysis Note for Antimony: Initial Calibration Verification (ICV) did not pass within 95-
105% as required by USEPA Method 200.7. Result was 109%. Data should be considered an
estimate.
Sample Preparation: 50 mL / 50 mL 200.7 02/17/05 7:20 cnguyen P11827
Nitrate+Nitrite by Ion Chromatography
Nitrate+Nitrite BRL mg/L 0.20 0.012 1 300.0 02/10/05 4:25 mlandreth Q02993
n-Hexane Extractable Material(HEM:Oil and Grease)
Oil and Grease(HEM) BRL mg/L 5.0 1.4 1 1664A 02/15/05 10:05 tmaher Q03143
Total Recoverable Phenolics,Spectrophotometric,Manual 4-AAp with Distillation
Phenolics,Total BRL mg/L 0.050 0.027 1 420.1 02/14/05 14:05 tmaher Q03091
A Analysis Note for Phenolics, Total: Prep batch P11802 was initiated on 2/9/05 at 12:20.
Sample Preparation: 500 mL / 500 mL 420.1 02/09/05 12:20 tmaher P11802
Total Phosphorus by Automated_Ascorbic Acid Reduction Method
Total Phosphorus BRL mg/L 0.10 0.013 1 SM4500-P F 02/22/05 13:51 cmatthews Q03315
Sample Preparation: 50 mL / 50 mL SM4500-P B5 02/15/05 17:00 celfaki P11824
Residual Chlorine..DPD Colorimetric Method
Residual Chlorine BRL mg/L 0.20 0.0049 1 330.5 02/23/05 9:50 tubbing Q03318
* Analysis Note for Residual Chlorine: Residual chlorine was received and analyzed outside of
holding time.
Sulfate by Ion Chromatography
Sulfate 420 mg/L 10 0.95 10 300.0 02/10/05 4:05 mlandreth Q02994
* Analysis Note for Sulfate: MS/MSD were outside acceptance limits due to matrix interference.
Sulfide by lodometric Method
Sulfide BRL mg/L 2.0 0.094 1 376.1 02/15/05 10:10 cmatthews Q03116
Sulfite Titrimetric Method
Sulfite BRL mg/L 1.0 1 377.1 02/11/05 13:40 cmatthews Q03045
* Analysis Note for Sulfite: Sample was analyzed outside of approximated holding time.
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Toll Free Number.1-800/529-6364 - Fax:[phone] Page 7 of 8

• NC Certification No.402 LaboratoryReport
SC Certification No.99012 p
w4 NC Drinking Water Cert.No.37735 FL Certification No.E87519 3/1105
Fwi service Anaytical&EmAnonnona solutions
FMC Corporation Lithium Division Project Name: NPDES Renewal Client Sample ID: 001
Attn: Rodney Willis Sampling Prism Sample ID: 110704
Seven LakePointe Plaza Project ID:. NPDES Renewal COC Group: G0205278
2801 Yorkmont Rd.Ste.300 Sample Matrix: Water Time Collected: 02/09/05 9:45
Charlotte,NC 28208 Time Submitted: 02/09/05 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/me ID
Total Kieldahi Nitrogen Calorimetric.Semi Automated Block Digester AAIII
Total Kjeldahl Nitrogen BRL mg/L 0.50 0.14 1 351.2 02/14/05 8:00 cmatthews Q03068
Sample Preparation: 50 mL / 50 mL 02/10/05 9:55 cmatthews P11799
Total Organic Carbon
Subcontract Report -See Attached 1 See Attached
'A Analysis Note for Subcontract Report: Sample was subcontracted to NC-Certified laboratory,
Test America, Inc.
Total Nitrogen by Calculation
Total Nitrogen BRL mg/L 0.50 1 N/A
Total Suspended Solids
Total Suspended Solids BRL mg/L 3.0 0.57 1 160.2 02/14/05 9:50 cnguyen Q03084
Sample Comment(s):
BRL= Below Reporting Limit
J=Estimated value between the Reporting Limit and the MDL
Angela D.Overcash, V.P.Laboratory Services
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Toll Free Number:1-800/529-6364 - Fax:[phone] Page 8 of 8

02/1112005 09:29 33E3524175 L=MSL GEENESOPO PAGE 52/03
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prism Laboratories,Inc. CustomerFO:
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Charlotte,NC 28224 EMtLOroer: p20500571-
Fax: [phone] Phone: (704)5Z9-6364 MN,�.g
Project: Ana aiDatz ## 10t2003
Report Date :11112O5
1.
Determination of Asbestos Structures in Weer Performed by the 100.2 Method
(EPA160O1R-941134)
Concentration
R FiberAnalytical. Of Asbestos
.Rampte Prep • #Fibers Non. Tweets)Of Sansitivity Confidence Fibers
• Sample ID pate Asbestos Asbestos Asbestos On FL) . limits (M 3 Comments
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Bdx 29DS4f3•Charlotte,NC 2822A-t75d3 .
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— 'Please ATTACH any pro eats ecilic reporting OC LEVEL III Nf- :; ,, ;gr:- of *e., _-k :�14,•0_;�_:;7 ^I:3- •a
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.,„1. wn" P.rclrfafons and/or QC Requirements " f l 1 x`„'.,^ �a,. .'.' i.: .
Rr#Port•7oiCcntaca Name: — ! 4 if).A.. r,,.,:;,,'''A-"'•`• '
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Phony:�1 ?•s ► Fat((Yes}(Nu)I� � LI�r1 F,urchaseOrder No./Online Reference TO OE FILLED IN Elf CANNY/SAi4'IPLIII .PIRr30t19NII:L
Erma(l(Yes)iNct}Ewalt Addneeg�_ rmquesled Que pate O 1 Day C32£)ay$ 03 Days Ci R Days �W S Days Certitiaatign: NS!AC_ USACE:__._)rL :NC B
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Site Location Name SCE OTHER �NJA
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Stte l.oastiun Phytsia8i Address:— Turnaround time::i based on bushiest;days,excluding weekends and l+.otldars. Water Chlerinated• YES _•_•'t�IO-_
tSF,EPEVER5EF0A31Efl)ASaOOR01TlDN9REGARDINGSEriVICES Sample'Iced Noon GDltection. YES__NO. ••
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submitted.lmwrUtngloUhePdem Protect Fetanag,er.Thera win lechargertorenychanalzsafteranetyses have boeninitlatiked. r,;.r'c . �,:�,•,,-;-..:`:,,1:. !•i:•=
• ET*, nei u'I Iudl tDvy rietdz) - I Daa n tvr sAdditional Comments:l by Sit ��va �hGii ::•'
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,-t SAMMPS Ails 140T AOCEPTFJI AtmO VERIFIED AO.LIteT ode. AlTHE L.ABOIATDAY. f, {{
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NPDt S: UitT: I CiflOINDWATER: Dalt•NI141 WATEitl:. SCUD WASTE! it KRA: I C3RCLA: LANDFILL OTHEFI: . 5 4';atil i, Ct illON
. ClNC QSC'❑NC aSCjjONC USC NC U-SC CI NC •G$0 DNC: uS _ ❑NC Cl SC uNC .USC UNC' USC .
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•
•
02/11/20I35 09:29 3369924175 EMSL GREENSBORO RAGE 01/03
e"
Asbestos r Lead= Environmental.IMaterials&Indoor Air Analysis
7os Ghtlift e
. EMSL
Analytical, Inc Kemersvilte,WC 27284
Rhone:(336)9924025 s„
• Fax (336)992&176
FACSitgliLE TRANSMITTAL SHEE Q
TO: Ei:hittiey Munroe FROM! EMSL Analytical, End.
COMPANY Prism Laberatelies, Inc. DATE: 2/11/2005 9:23:18 AM
FAX [phone] PAGE INCLUDING COVER: 3
PHONE: (704)529,6364
RE: Analysis Results far Order 02050057
The following report covets the analysis performed an samples submitted to EMSL Analytical, Inc. on 2l10/2005.
-
Notice: if you are net the stated recipient cf'MIS fax and have received this in error,please
discard immediately and contact EMSL Analytical at the phone number listed above.
It you have any questions, please do not hesitate to contact us at(336) 2-1625.
VISIT OUR WEBSITE AT
YOU CAN DOWNLOAD AND PRih}T
CERTIFICATIONS OF AOCREOITATION$AND CHAIN OF CUST•OV FORMS

•
-t,
'Florida Radiochemistry Services, Inc.
Contact: Michael J.Naumann
5456 Haffner Ave.,Suite 201 Orlando,FL 32812
Phone: [phone] Fax:[phone]
Certification 1.D.#12709 '
Work Order#: 0502111
Report Date: 02/17/05
Report to:
Prism Laboratories, Inc.
PO Box 240543
Charlotte, NC 28224
Attention: Whitney M1 nroe
I do hereby affirm that this record contains no willful misrepresentations and that this information given by
me is true to the best of my knowledge and belief. I further certify that the methods and quality control
measures used to produce these laboratory results were implemented in accordance with the requirements
of this laboratory's certification and NELAC Standards.
Signed / i(�iYS�l�li� Date 2-/
P esident
Page 1 of 3

9
Florida Radiochemistry Services, Inc.
Sample Login
Client: Prism Laboratories, Inc. Date/Time Work order#
Received
02/11/05 09:05 0502111
Client Contact: Whitney Munroe
Client P.O.
Project I.D. G0205278
Lab Sample I.D. Client Sample I.D. Sample Analysis
Date/Time Requested
0502111-01 110704 02/09/05 09:45 Gross Alpha/Beta
Analysis Results
Gross Alpha 4.8 Gross Beta 11.5
Error+I- 2.2 Error+l- 2.2
MDL 2.9 MDL 3.2
EPA Method 900.0 EPA Method 900.0
Prep Date 02/15/05 Prep Date 02/15/05
Analysis Date 02/16/05 Analysis Date 02/16/05
Analyst MJN Analyst MJN
Units pCi/I Units pCi/l
Page 2 of 3

Florida Radiochemistry Services, Inc.
QA Page
Analyte Sample# Date Sample Amount Spike Spike/Dup Spike Spike Dup
Analyzed Result Spiked Result Result % Rec. % Rpd
Gross Alpha 0502118-02 02/16/05 <0.5 10.2 9.5 9.8 93 3.1
Gross Beta 0502118-02 02M 6/05 <1.0 12.6 14.8 13.1 117 12.2
Quality Control Limits
% RPD % Rec.
Gross Alpha 18.1 68-116
Gross Beta 16.2 78-119
Page 3 of 3

CHAIN OF CUSTODY RECORD
• -•'' `. ,i LAB USE ONLY
LABORgTO Ks;,ti. ;v o F Y'Att / 4 t
•^'.+'� ��'-i''•�''���, ':'.• �:�-I', � PAGE 1 OF QUOTE#TO ENSURE PROPER BILLING: f��x �",1 d t r1 �'��� `t�ir:'Ar���4.� '�f, t�' '� r R'�
yalµl� i1L1 7 u nrr atrSv�I ? E t �i�j � r y .I ryr
Full Service Analytical&Environmental Solutions hf q Write°Mt t aElt '�Y i"y,d4 I'� P +,it e;t1 4 N1
I L oa or-5 `l8 Re rayed 0 li. . dxT �t _€ ,
Project Name: �? S." A' -vA. 3 2,,,ia s + * '` ""
449 6pringbrook Road•P.O,Box 240543•Charlotte,NC 28224-0543 Short Hold Analysis: (ritamdttr.0` Q E )'R' S R `1I�! o-".digp'( n?y��;},aaf!t`y,4.-1. N.;G tits;:
704/529-6364 Fax: [phone] t Y s. (Yes) { o) UST Project (Yes) (No t v ;a,_„ r r3rt y if t r x,3t , s y 0
Client Company Name: r 15 t�t,riS 'I r "Please ATTACH any project specific reporting(QC LEVEL I II III IV) p I T 1 7 , .N.,., 2�(, ' :,� k 4 �/i.e: 1
1,2
j TC9"l,. pSit v,ti4 A •-, 1, ,• k R�r x,x i°r e1
Report To/Contact me:7���t1 yti�� provisions and/or QC Requirements � tadP� k s +fit �yy to,ttl � i � � la
: 10 q� invoice To: ?c P.6111�,ra d,/O lj,111r.4 � „ v k7 s�s r� a
Reporting A,ddres D% asLI65 3 � P iC�tq A 43 � r✓ t� is arr,j. F�'d l�tl( 41 y t
L'V I c o IJC_ 2,�T2 2.. Address: : r? 44. 5��. :,�)-3 ,;.
C 1 ) d � 5; s i+e 1l.t�Y z$.+< t,r.''„ 3l' t, i ;
yf .c.. .....cii. ., �zr+h .� ...6if4� .+! t _ 'k..v..l«k, ...
Phone: ioy)5z1-b3�W Fax(Yes)(No):1704) 52S-0461 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL/
Email(Yes)(No)Email Address Requested Due Date 01 Day 0 2 Days 0 3 Days 0 4 Days 0 5 Days Certification: NELAC USACE FL NC V__
EDD Type:_PDF Excel_Other "Working Days" ❑6.9 Days 0 Standard 10 days 5Tf�N9 V Sr
Site Location Name: SO OTHER N/A
Samples received after 15:00 will be processed next business day, /
Site Location Physical Address: Turnaround time is based on business days,excluding weekends and holidays. Water Chlorinated: YES_ NO V
(SEE REVERSE FOR TERMS&CONDITIONS REGARDING SERVICES Sample le Iced Upon Collection: YES ✓NO
RENDERED BY PRISM LABORATORIES,INC.TO CLIENT) p p
TIME MATRIX SAMPLE CONTAINER . A"ANAL SES REQUESTED PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- {,,,,i��t,\//�4�
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE TIVES tit CF ���� // / / / REMARKS IDLAB
NO.
HOURS SLUDGE) SEE BELOW �p t /
-
110109 2..1cf105— Oct(`i5 w-I ,....- P las. t.- 1 L HNO 3 Y x
i
•
•
Sampler's Signature Sampled By(Print Name) Affiliation 4,
Upon relinquishing,this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above.Any changes must be p,irk s .; y Yi1
submttted in writing to the Prism Project Manager.There will be charges for any changes after analyses have been initialized. 14
7ihep( ure) eiv By: nature) Dale Military/Hours r 1i r
Additional Comments: (elilshed By,(Signature) Received (Signature) V -Fe,: id. its.L.651,24,v4.ag.41kig
"-L" '`{^q "�' "''"'u' "�zu`S a
Y�( 9 ) Date �CET; B � 'j: `�'�?r��,� _
(Signature) art 9�4 fl' '" �:;" �1�.;a•,a,< '' '
RelinquishedBy:( g ) Receive F r Prism Laboratories By: Dat �r' �CAd I fS C rf " `��ch e .d,: ail?1 l
• 02. ) 1 Jul I'�w .� t,i,.
uit
Method of Shipment: NOTE;ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY.. Log-In Group No. Ui'I�11dC•) t' 3�.0��. � Z :(R h �4'4.,*'
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. vv 0 Fad Ex 0 UPS ❑Hand-delivered 0 Prism Field Service 0 Other C 4DI)3 V L—71133
NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑NC 0 SC 0 NC 0 SC 0 NC 0 SC 0 NC 0 SC 0 NC 0 SC 0 NC �.0 SC ❑NC 0 SC 0 NC 0 SC 0 NC 0 SC It � ZtE-
0— 0 ° ---- G o , 0— , 0 0 1] ORIGINAL
'CONTAINER TYPE CODS A=Amber C=Clear G=Glass P=Plastic; TL=Teflon-Lined Cap VOA=Volatile Organics Analysis(Zero Head Space)
8 .

l
Florida Radiochemistry Services
, Inc.
5456'Harmer Ave.,Suite 201 Orlando,FL 32812
Phone: [phone] Fax: [phone]
Radiological Analysis
t � Note:e6ljnm W foron mist be supplied toroomplanee credit
0 [WATER SYSTEM ID #: - -i ` ,a county: t'-'(eCJ ,e {,(2T
Name of Water System: RT\I�P1'esi( Su. ��?�l�-""0"11f IP.R. . �l 10919E
-Sample Type: ❑ Distribution AEntry Point ❑Composite ❑Special/Non-compliance
1\ Collection Data •
Mail Results to(sy,,stiemis-lye�vneesseentaative): p Date time . • Semple Collected
?c l c� r r L4x.i--�C.t O tCt e& single or i �D/YY) (SDsolhdAtorgld) Code Location Sr
x=Qu —J--/--. M
-Po 1 Rf 0,9-4- f-ter-crrri We) -- - - ___
\ ,11 .tf( i•-C9 gS2-;G± • 2"°Qt _J J_- _ _J_NI ___
. Telephone li:( )5 1::)_. - 3"Qtr —J_J__ M
Fax#: Q ,4bG-�p° ----— _--
Qt a/J.2Jss- 1c.:(,,,rd ti 113 Loa- /Z_ _ 4.---446- s-t
LABORATORY ID#: 12 7 0 9 ❑SAMPLE UNSATISFACTORY ❑RESAMPLE REQUIRED
r Required NOT Detected
Con tam Method Reporting Limit (i.e.<R.R.L.) Quantified Counting Allowable
Code Contaminant Code (R.R.L) (X) Results* ErrorJ Limit
,o/ 4000 Gross Alpha 435 3 pCVL /;. ___ —pCi/L —.�L�Q 15 pCVL
4004 Radon —_— 100 pCi/L ❑ --- ......pCVL pCi/L _--- N/A
4006 Uranium 456 2 pCi/L 0 --- __—pCi/L ____ 20.1 pCVL
4999 Uranium --- 3 owl. _,__—0 ,_,_,_Pail- — — 30 pCi/L
4010 Combined Radium N/A N/A N/A ,'270- .--pCi/L ____ 5 •pCi/L
4020 Radium 226 446 1 pCVL e-- -- pCi/L —_ 3 pCl/L
v 4030 Radium 228 452 1 pCi/L )1C _-- --pCi/L —312,3, 2 . pCi/L
4100 Gross Beta 435 4 pCi/L . ❑ . pCi/L 50 pCi/L
4102 Tritium --- 1000 pCi/L 0 --- `—pCVL 20,000 pCi/L
4172 Strontium 89 --- 10 pCi/L ❑ --- pCi/L ••--- N/A
4174 Strontium 90 --- 2 pCi/L 0 .
—PCi/L `—•-- 8 pCi/L
4264 Iodine 131 ——— 1 pCi/L 0 —_ —_ y�p� -- N/A
4270 Cesium 134 --- 10 pCi/L 0 --- `—pCl/L _� _'_— N/A
Note: If result exceeds allowable limit,the laboratory must fax analytical results to the State within 48 hours. .
Date: Time: '
Analyses Begun: Q_J a7J. _40 :c> 7 "km
(MM/DD ) (Specify AM or PM)
Analyses Completed: ' (9 J../__ _a�: -.7 M
(MM/Do/YY) (SpecifyAM or PM)
Laboratory Log#: 657.)301?'O 1 Certified by: Mike Naumann/ . .
i
Comments: >c ' :�� :/X — /727/re /;cs—
Laboratory should mail results to;
• Public Water Supply Section,Attn:Data Entry,1634 Mail Service Center.Raleigh,NC 27699-1634
Fax [phone]
•
Rev.6/30/04
G010512z .V-

Testt meriea
ANALYTICAL TESTMG CORPORATION
2960 FUsmc CREIGHTON DIME•NAyuiiLu.Tscaissss 37209
800-763-0980•615-728-3404 FAX
ANALYTICAL REPORT
PRISM LABORATORIES 5625 , Lab Number: 05-A19312
ANGELA OVERCASH Sample ID: 110704
P.O. BOX 240543 Sample Type: Ground water
CHARLOTTE, NC 28224 Site ID:
Date Collected: 2/ 9/05
Project: G0205278 Time Collected: 9:45
Project Name: Date Received: 2/11/05
Sampler: Time Received: 8:00
Report Dil Analysis Analysis
Analyte Result Units Limit Pactor Date Time Analyst Method Batch
•MISCELLANEOUS CHEMISTRY•
Total Organic Carbon 4.07 mg/1 1.00 1 2/15/05 18:55 S. Pray
ter 9060 7169
LABORATORY COMMENTS:
ND = Not detected at the limit of detection
B = Analyte was detected in the method blank.
J = Estimated Value below Report Limit.
E = Estimated Value above the calibration limit of the instrument.
# = Recovery outside Laboratory historical or method prescribed limits.
•
End of Sample Report.

•
Tests erica
ANMYOCALTES11NOC
2960 Fosrn Cnua rok Dam•Nnsseuut,Tra8688s1 37204
800-765-0080•815-726-8404 Fex
PROJECT QUALITY CONTROL DATA
Project Number: G0205278
Project Name:
Page: 1
Laboratory Receipt Date: 2/11/05
Matrix Spike Recovery
Note: If Blank is referenced as the sample spiked, insufficient volume was received for the defined analytical batch for
MS/MSD analysis on an true sample matrix. Laboratory reagent water was used for QC purposes.
Analyte units Orig. Val. MS Val Spike Conc Recovery Target Range Q.C. Batch Spike Sample
**MISC PARAMETERS**
Total Organic Carbon mg/1 2.08 22.0 20.0 100 80 - 120 7169 05-A19311
Matrix Spike Duplicate
Analyte units Orig. Val. Duplicate RPD Limit Q.C. Batch
Total Organic Carbon mg/1 22.0 22.2 0.90 20 7169
Laboratory Control Data
Analyte units Known Val. Analyzed Val 8 Recovery Target Range Q.C. Batch
**MISC PARAMETERS**
Total Organic Carbon mg/1 200. 183. 92 87 - 110 7169
Duplicates
Analyte units Orig. Val. Duplicate RPD Limit Q.C. Batch Sample Dup'd
Project QC continued . . .

TestAAmerica
ANALYTICAL TESTING CORPORATION
2980 Roans CRTICSTOI.DIME•NeXHra.ut,Mamas 37204
800-763-0980•615-726-3404 FAX
PROJECT QUALITY CONTROL DATA
Project Number: G0205278
Project Name:
Page: 2
Laboratory Receipt Date: 2/11/05
Blank Data
Analyte Blank Value Units Q.C. Batch Date Analyzed Time Analyzed
•*MISC PARAMETERS**
Total Organic Carbon < 1.00 mg/1 7169 2/15/05 18:55
q = Value outside Laboratory historical or method prescribed QC limits.
Bud of Report for Project 406005

Testi&merica
ANALYTICAL TESTING CORPORATION
2960 Fosms Cu rroA DYNE•NASeentIT TICtelt3SES 37204
800-765.0980•615-726.3404 Fnx
2/17/05}
PRISM LABORATORIES 5625
ANGELA OVERCASH
P.Q. BOX 240543
CHARLOTTE, NC 28224
This report includes the analytical certificates of analysis for all
samples listed below. These samples relate to your project identified
below:
Project Name:
Project Number: G0205278.
Laboratory Project Number: 406005_
An executed copy of the chain of custody, the project quality
control data, and the sample receipt form are also included as an
addendum to this report. Any QC recoveries outside laboratory
control limits are flagged individually with an #. Sample specific
comments and quality control statements are included in the Laboratory
notes section of the analytical report for each sample report. If you
have any questions relating to this analytical report, please contact
your Laboratory Project Manager at 1-800-765-0980. Any opinions, if
expressed, are outside the scope of the Laboratory's accreditation.
Page 1
Sample Identification Lab Number Collection Date
110704 05-A19312 2/ 9/05

TestA�merica
ANALYTICAL TESTING CORPORATION
2980 F0877tx CRGiono,DRIVE•NessriLu:,Tsa.vsssss 37209
800-785-0980•816-728-3404 Fax
Page 2
Sample Identification Lab Number Collection Date
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Report Date: 2/17/05
Johnny A. Mitchell, Laboratory Director Gail A. Lage, Senior Project Manager
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Services
Pamela A. Langford, Senior Project Manager Kelly S. Comstock, Technical Services
Eric S. Smith, QA/QC Director Roxanne L. Connor, Senior Project Manage
Sandra McMillin, Technical Services Mark Hollingsworth, Director of Project
Laboratory Certification Number: 387
This material is intended only for the use of the individual(s) or entity to whom it is addressed,
and may contain information that is privileged and confidential. If you are not the intended recipient,
or the employee or agent responsible for delivering this material to the intended recipient, you are
hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited.
If you have received this material in error, please notify us immediately at 615-726-0177.

� F PRISM'. : • CHAIN OF CUSTODY RECORD ILAB uss 4wi .Y .
3 3 LaaoeATonrss INC.r• t°s4 �x41� ak i ' l N/A r
...*-l.".h`$ga��a%9-w.,.e.- :•: : ....... PAGE 1 OF�QUOTE A TO ENSURE PROPER BILLING: SatT1pIQS 1t44CT,',�lp gQa%ai,7 �
Full Service Analytical&Environmental Solutions 1, ,PO
, RecQty' ON; 6Elt1TernQo ,I`I•'r 4 .:.0,:;.:
Project Name: 'y I J-�� �.tx. r:�.; -sr ::,�r;y ,Ff
Phon449 e r704/529 6364brook d••Fax [phone] Charlotte,NC 28224-0543 Short Hold Analysis: .PROPER!PRE�SN" 0 b 1 ,rna�casegi a `' ; l
y (Yes) (No) UST Project: (Yes) (No) 2 )
Y r 1 Received WI IN Q D N94 I E3
Client Company Name: f"J"4� *Please ATTACH any project specific reporting(QC LEVEL I II 111 IV) t pp � � " ` • _ iii (�yt °r i "• ,�, �
CUSTODY SEgLS(l
�� G'1 G�.1,�tt� is provisions and/or QC Requirements ,E o W/T ? n t,` r ���� pYT—
Report To/Contact Name -••
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EDO Type:._PDF Excel V Other Working Days" O 6-9 Days Standard 10 days
Site Location Name: r MG esSd�ay. SC OTHER N/A
11
f a Samples received after 15:00 will be ocessed next business day, -
Site Location Physical Address: -uy I�2 1 Turnaround time Is based on business days,excluding weekends and holidays. Water Chlorinated: YES_ NO I.". rzi
• (SEE REVERSE FOR TERMS 8 CONDITIONS REGARDING SERVICES • Sample Iced Upon Collection: YES
RENDERED BY PRISM:LABORATORIES,INC.TO CLIENT) P P
TIME MATRIX .. SAMPLE CONTAINER ANALYSES QUESTED .v a! . V �� PRISM
CLIENT DATE COLLECTED (SOIL, __ PRESERVA- / ,� �., cry �� LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OFi *TYPE TIVES /�r/
HOURS SLUDGE) SEE BELOW NO. SIZE ti � � A J ID NO.
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Sampler's Signature / • Sampled By(Print Name) alit tr 1 -Ll.viLA-L�- Affiliation 'NlC—'
Upon relinquishing,this Chain of Custody is your authorization for Prism proceed with the analyses as requested above.Any changes must be
submitted In writing to the Prism Project Manager.There will be char fo any changes after analyses have been initialized. • ,, ,,ip ,'
Fitiq heri 3J:(Sig u Receli By:( • tu ) • /1013/4c._ Military/Hours Additional Comments: a � rtY ;T
elinquishedBy:(Signature) eceive ig ature) ; i(e„Q.Qgarlurel`ime;
,Ffeiaeei'Eee•
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M' .- ' hi.•ent: NOTE:ALL Aryl L ••t RS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRAN ORTA ON TO THE LABORATORY. Lo n Oroup No.
/ yileage .
SAMPLE ARE NO ,EPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LAB TO Y.` a
D Fed Ex O UPS ❑Ha 41-delivered ❑Prism Field Service O Wet
NPDES: UST: ` GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER I Illi FIT 111y 1 .1i�
O!dC OSC ONC 0SC ❑NC ❑SC ONC r0SC ❑NC ❑SC 0NC DSC ❑NC 0SC ❑NC ❑SC r0NC ❑SC ����'t�'"rj ")"`ft""" ""'� '"°'
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,°PRISM•:. CHAIN OF CUSTODY RECORD LAfa USE ONLY
15 'LARORAT.ORIESrINC-
¢�� Z 7/ xA :. rf. Gei4T � yr� YE ='NO N/P•
�., i:"�k _..: PAGE_OF_ QUOTE#TO ENSURE PROPER BILLING: i gir tea'RFAfr','TitOi1140.VaI y4 tt. -
Full Service Analytical&Environmental Solutions f s+^ . F h•r L4¢ 4, i
ecePill IC ?Tem '1 x
Project Name: R .h@fl ;. r y1 +�
449 Springbrook Road•P.O.Box 240543•Charlotte,NC 28224-0543 PROQE►�P,RESEPVV TIVE�S'1nd{ca{ed?R
Phone:[phone] • Fax [phone] Short Hold Analysis: (Yes) (No) UST Project (Yes) (No) ' ? ^• -
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Client Company Name: r �✓ , *Please ATTACH any project specific reporting(QC LEVEL III III IV) ,..: , 4
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provisions and/or QC Requirements ¢USTODY;SF�L•$�NIfcOT?I j
Report To/Contact Name: 'ai c>-4 t�)l--tl� PVOLATILES rec d W/OUTI`4EADSPACE? .
Invoice To: xe r
Reporting Address(,- .-_,SC -19 �„ A-M,[ PROPER CcNTAINERS used?
sN► C Ill,Li G G )ollp Address:
Phone: Fax(Yes)(No):
Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
EDD Type: Requested Due Dale 0 1 Day CI Days ❑3 Days ❑4 Days ❑5 Days Certification: NELAC USACE FL NC I/
Emal( 1f No)Email Address
PDF Excel'Y Other "Working Days" 0 6-9 Days 0 Standard 10 days
Site Location Name: F fr1,C" Samples received after 15:00 will be processed next business day. SC_OTHER N/A
Site Location Physical Address:• i I uY-( Vca 1 Turnaround time Is based on business days,excluding weekends and holidays. Water Chlorinated: YES_ NO V-
(SEE REVERSE FOR TERMS&CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES L NO
RENDERED BY PRISM LABORATORIES,INC.TO CLIENT) p
TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED Q PRISM
CLIENT DATE COLLECTED {SOIL, PRESERVA- /�� / / ty)
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE TIVES �1 U REM Ks,/ LAB
HOURS SLUDGE) SEE BELOW NO. SIZE /L.tv�\f /,(b /0 �f � ID NO.
_COI opip5-- ot:tic .usr p 1 . ________
oo1 Z 9 off. tAi " .. P _! _-_ _.._ PC
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Samp led FQ E.•"E -, 1A-'`45 R4C— h ( '
p 9P By(PrintName) Affiliation
Upon relinquishing,this Chain of Custody Is your authorization for Prism to proceed with the analyses as requested above.Any changes must be ptti,$M
submitted in writing to the Prism Project Manager.There will be chart--for any changes a analyses have been initialized. i I
u'j ed y ( at a r Re ed B 1 re Date Military/Hours Additional Comments SIeiArir�JAl Tifne
Relinquished By:(Signature) ' ' - •:y- Ignature) at :SIIBiDepiIture Time ,1'(. -l1
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Relinquished B - u Received For Prism Laboratories By: D to F1el iTech Fee
) (
F•)1 / lC) fIileage'aA
Me • • Ipme. '• •ALLS C S SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. 77 Lo n Oroup No. """' """'4'" "'' ' '
SAMPLES OT EPTED AND VERIFIED AGAINST COO UNTIL RECEIVED AT THE LABORATORY. /
0 Fed Ex G UPS 0 Hand-delivered Prism Field Service , 0 Other • v Oa0SKIe)
NPDES: UST: GROUNDWATER: DRINKING WATER: I SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: I'IA'n z) � f `') '� ,
f]NC OSC II NC OSC GNC C)SC ONC OSC GNC OSC ONC ❑SC ONC ❑SC C!NC 0SC ODIC !DSC I,I1�f""'"' '"
❑ . I o . U . Q , ❑ 0 • .=I ❑ • 0 • ORIGINAL
1 `CONTAINER TYPE CODES: A=Amber C=Clear G=Glass P=Plastic; TL=Teflon-Lined Cap VOA=Volatile Organics Analysis(Zero Head Space) '

EI'A I.D. NUM©ER (copy from Item I of Form 1)
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information on separate sheets fuse the same format)instead of completing these pages. 0C-b000-11 19(0
SEEM INSTRUCTIONS. _
V. INTAKE AND EFFLUENT�CHARACTERISTICS... . . ,,.M-.m...- .. .. ten... ,... i-' ti lII,' ii( , +i ',i Ii ui I71 I�,,��'��I�I1 I' I 1I:I 1 I 1,IF,I 1I'1r1'1 „ 11 ail III IIilfii���I1 Ilik��i1i Pi:l.ouTFALirto.
(continued from page 3 of Form 2-C)
PART A- You must provide the results of at least one analysis for every pollutant in'this table. Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT 3. UNITS 4. INTAKE (optional)
1. POLLUTANT a. MAXIMUM DAILY VALUE MAXIM jjM 3,p p/1Y VALUE c.LONGIT�.}ZM y�[R�i VALUE I (specify i/blank) a. LONG TERM
(II aUQlfaf7le) _ III aUQila blCJ d. NO.OF AVERAGg_V ALUE b, NO. OF •
(I) SS (I) (() ANALYSES a.CONCEN- b. MASS (I) ANALYSES
x
CONCENryTRATION ( )MA CONCENTRATION (�)MASS CONCENTRATION (�) "'wss TRATION CONCENTRATION (,)Mn33
a. Biochemical C.to-1 1
Oxygen Demand I E ,8'—
_
(I30D) I�i451 _—` ----
b.Chemical 135.1-4:3V.3
Oxygen Demand sewizTAf —, - _.-' -
(COD) t-%FAil. _ �-
c. Total Organic T
Carbon(TOC) ' ` —�- _ 1 e® e.,M
S.Total Suspended 14,. r I ____ -^- I,1 _ I )b..d
Solids(TSS) 1
e. Ammonia(as N) t3E..-'ou) ..�
VALUE �p g4�q, VALUE VALUE VALUE
I. Flow I 1 1(0a 1�1d ®'.+
g.Temperature VALUE VALUE VALUE VALUE
(winter) 'C), oC
h. Temperature VALUE VALUE VALUE Sc VALUE
(summer) Z .�t __„�,m, 3
MINIMUM MAXIMUM MINIMUM MAXIMUM
i.pH
STANDARD UNITS
PART B- Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant
which is limited either directly,or indirectly but expressly,in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant.For other pollutants for which you mark
column 2a.you must provide quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
1.POLLUT- 2. MARK 'X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
ANT AND a. a[• b, aE- a.MAXIMUM DAILY VALUE b.MAXI?II M 3, pqY VALUE c.LONG TERM A�tR VALUE d.NO.OF a. LONG TERM b,NO,OF
CAS NO. LIEVCCLIEUE0 (t/QUQ�ble) (fl aVa!!ab(e� a. CONGER- AVERAGE VALUE
(if available) se H U I) (I) (�) ANAL- TRATION b.MASS (I) ANAL-
CONCEN(TRATION (2)MASS CONCENTRATION (_) MASS CONCENTRATION (_) MASs YSES CONCENTRATION (:)MASS YSES
T s
a.Bromide
(24959-67-9)
b.Chlorine,
Total Residual
c.Color 1\41
/1/4
d. Fecal
Collform
a. Fluoride
(16984-48.8)
f.Nltrate—
Nitrite(as N)
EPA Form 3510-2C (8-90)
PAGE V-1 CONTINUE ON REVERSE

.ITEM V•0 CONTINIJEO FFiON1 FRONT
•
:11 •-f.MARK 'X' •
P41i-UT 3. EFFLUENT d. UNITS 5. INTAKE (optional)
•
AT'AND a•ae- 'b.se- b.MAXI M 7 Y VALUE C.LONG 1' t vi A4(RG VALUE L �t E
ctin./Em evco a. MAXIMUM DAILY VALUE is e) (� tl pleJ - a.CO NCEN- AVE PA ETVA%E b.NO.OF
(.''A.$I�t O. d.NO.OF F
asre• ws- _ I oval e t aua a
(t/waLabft) SENT scNr (i) ANAL• b.MASS
CONCe NTR ATION (_)Mwss ('T (�) TRATION ANAL.•
.� CONC GNTR wT10N (2) MASS CONGIf NTRAT40N (2) MATf YSES (t)
�.,�(tro�n; - _ - CONCenTR ATION (2)MA),f YSES
Tilta}torQan iC
(oat•N)
.h,;Qif and
'ant*
L.Pfioaphorus
(aij'),•Tots l
(7723-14-0) •
I. Rsidfoactivity •
(Tr Alpha,
Total
(2)Beta, •
Total,.
(3).Radium,
•
.Total •
(4) Radium
226,Total
k.Sulfate
(as SO4)
(14808-79-8)
I.Sulfide
(as S)
:144
m.Sulfite
I
(as SO3)
(14265-45-3)
n.Surfactants
•
•
o.Aluminum, •
•
Total
(7429-90-5)
p.Barium, "
Total
(7440-39-3)
q.Boron,
Total
(7440-42-8)
r.Cobalt, •
Total
(7440-48-4)
a.Iron,Total
(7439-89-6)
t.Magnesium,
Total
(7439.95.4)
u.Molybdenum,
Total
(7439-98-7)
v.Manganese,
Total
(7439-96-5)
w.Tin,Total
(7440.31-5)
•
x.Titanium,
Total •
(7440-32-6) .
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D. NUM BER(copy
from Item I of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C • 1\ICti(v � 1 ' `( 4- o 4-
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark'"X"in column
2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2-a(secondary industries,nonprocess
wastewater outfalls,and nonrequired GC/MS fractions),mark"X"in column 2-b for each pollutant you know or have reason to believe is present.Mark"X"in column 2-c for each pollutant you
believe is absent.If you mark column 2a for any pollutant,you must provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results
of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein,acrylonitrile,2,4
dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in
concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to
be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages) for each outfall.See instructions for additional details and requirements.
I.POLLUTANT 2.MARK•X• 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
•AND CAS b.MAXIMUM 3 OAYW ALOE C.LONG T M VALUE a. LONG TERM NUMBER B INO b,■a- c ae- 8.MAXIMUM DAILY VALUE or Cp bl fi /��(�6
iNa ilaveo�lavav aaalla eJ • /auW"labtE)• d NO.L- b.NO.L-
_ e.CONCEN- AVERAGE VALVE
ANAL- b.MASS ANAL-
(f/aualta6le) OPO MI; eNT NT (])MAff it)NT (:)MAfS (.1 (])MAST YSES TRATION (1-1 CONta n- I,)Nip YSE$
PO CONGCNTRATION CONCCNTRATION CONCl NTRATION TR ATION .t
METALS,CYANIDE,AND TOTAL PHENOLS
1M.Antimony, •
Total(7440-36-0)
2M.Arsenic,Total
(7440-38-2)
3M.Beryllium,
Total,7440-41.7)
4M.Cadmium, .
Total(7440-43-9)
5M.Chromium,
Total(7440.47.3)
6M.Copper,Total \\\1 /P( •
(7440-50-8)
7M.bed.Total I
(7439-92-1)
•
BM.Mercury,Total
(7438-97-6) .
9M,Nickal,Total,.
.17440 02.0),
1914.Saban film,
Total:(7782-49-2)
11M $11kar;Total':
f.7 ?2.1)
121i1.'Tfialllum,.
Total(7440.28-0)
13M.Zlnc,Total
(7440-66-6)
14M.Cyanide,
Total(57-12-6)
16M;'Phenols,
Total
.DIOXIN
2;3. .8 Tatrat DESCRIBE RESULTS
chl_o, odiben:o-P-
DIo200'(1744-01-e)
• EPA Form .3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
I.POLLUTANT 2.,MARK`X' 3. EFFLUENT — 4. UNITS 5. INTAKE (optional)
AND CAS
NUMBER arRtr- b sc- C•E. a.MAXIMUM DAILY VALUE b, MAXI M 3 Y VALUE C.LONG Z' M VALUE
pp pp//�� A.�[R d,NO.OF a. LONG TERM
INa LIRV RO LICV Rl� aUaliable) �(�aUatW 6iC� ANAL- a,CONCEN• AVERAGE VALUE b.NO.OI
(If available) OU w- :aI; tA*T L11 (a)"Al' YSES b. MASS (11 CONCRN-
a0 CONCCNTRATION (a)ywtt CONCCNITRATOOK (a)a. Co..0 CNTINATION TR ATION TRATION I�l NARt YSE$-
OC/fAS FRACTION—VOLATILE COMPOUNDS
1 V.Acrolaln
(107-02-8)
2V.Acrylonitrlle
(107-13-1)
3V.Benzene
(71.43-2)
•
4V.Bit(Chloro-
—
methyl)Ether
(542-88-1)
5V.Bromoform
(75-26-2)
6V.Carbon
Tetrachloride
(56.23-6)
7V.Chlorobenzene
(108-90-7)
BV.Chlorodl-
bromomethane
(124-48-1)
9V.Chloroethane(75-00-3)
10V.2-Ch loro-
NV1\
ethylvinyl Ether
(110-75-8)
11V.Chloroform
(67-66-3)
•
12V.Dlchloro-
bromomethane
(75-27-4)
13V.Dlchloro-
dffluoromethene
(75.71-(i)
14V.1,1-Dlchloro-
ethane(75-34-3)
15V.1,2-Dichloro-
ethane(107-08-2)
16V.1,1-Dlchloro-
ethylene(75-35-4)
17V.1,2-Dlchloro-
propane(78-87-5)
18V.1,3-Dicbloro-
propylene(542-76-8)
19V.Ethylbenzene
(100-41-4)
20V.Methyl
Bromide(74-83-9)
•
21V.Methyl
Chloride(74-87-3)
EPA. Form. 3510-2C (8-90) PAGE V-4
CONTINUE ON)A(3E V-I

CONTINUED FROM PAGE V-4 R.,...........,o,,A.AAraporoN oltli MeA tlRRIAITTIOIR al' YI RTER llRa Saar
1.'POLLUTANT 2.MARK .x• • 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
' AND CAS '
• NUMBER a.Ta1T b;R;- C aa- E. MAXIMUM DAILY VALUE b.M M 3• Y VALUE c.LONG Tpp M VALUE d NO.OF E. LONG TEAM b.NO.OF
RNG Llavaw.IaVan ^�rtauasQa$r, 1(raoa?a`�e�'
a.CONCEN- AVERAGE Mht.UE._
a- MT At• ANAL- b. MASS - ANAL•
'(IJ aUoilat7l;J- OYIOR- to NT Fa NT' CONC;N'TR ATION i=1 MAff II) ii)ROAST (�I ill xA SS YSES TRATION it)RONCaN-
r coHcaNTR CONCENTRATION GCNTRATION M to
3)mot.. YSES
GC/MS FRACTION—VOLATILE COMPOUNDS(continued)
22V:.Methylene •
Chloride(75-09-2)
•• 23V:1;1,2,2-Tetra-
chloroethane
(79345)
24V;Tetrachloro- •
ethylene(127-18-4)
25V.Toluene .
(108-88-3)
26V.1,2-Tram-
DIchloroethylene •
(156-60-5)
27V.1,1,1-Trl-
chloroethane •
(71-55.8)
28V.1,1,2-Trl-
chioroethane
(79.00.5) •
29V.Trichloro-
ethylene(79-01-6)
30V.Trichloro- 1
fluoromethene
(75-69-4)
•
31V.Vinyl
Chloride(75-01-4)
OC/MS FRACTION—ACID COMPOUNDS
1 A:2•
-Chlorophenol
(95-87.8)
2A,2;4-Dlchloro-
pt riot(120-83-2)
3A;`Z,4-Dimethyl-
phenol.(106-67-9)
4A'4,8-Dihitro-O-
•
ergsol(634-52-1)
.SA:•2;4Dinitro-
Phenol(61-28-5)
8A.2-Nitrophenol
(8875-5)
7A.4-N itrophenoi
(100-02-7)
BA::P-Chloro-M-
Cresol(59-50-7)
9AS Pintaehloro-
phgfb('(87-86-5)
�tj r..henol.
ct1=,4.84).
EPA Form' 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE

ig
CONTINUED FROM THE FRONT
1.POLLUTANT Z.MARK .•b 3. EFFLUENT p �R� a. Co .tionallo.
AND CAS I 1 5. INTAKE (optional)
NUMBER Arcs, b,wc- G we- B.MAXIMUM DAILY VALUE D.MAXIMUM 3e 8AY VALUE C.LONG T) M A VALUE NO.OF B. LONG TERM.nc Ie.c.uevc (t(auala e) (I avalia a AVERAGE VALVE
of
(if available) ai�rt- iin�r AI:, 1,1 ANAL- CEN- b.MASS
c owc cwrrwriow 01,„„„ GONG 1.1 Arlon 1.1 ...ss 1,1 T le)•...• vSES TRATION hi<once., ANAL-
eoneenrnw �o rw•now I:)•+w•e YSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS
18.Acenephthene
(83-32.9)
28.Acenaphtylene■.111__
(208-96-8) -- --.
38.Anthracene • — .----.
(120-12-7)
4B.Benzldine
(92.87.51
El
56.Benzo((a)) IIIIIII
__
Anthracene
56.55-3
BB.Benzo(a) SIM
Pyrene(50-32-8)
(20 -9 Benzo• IIIIIIII_
•fluoraitthene
(19MI
Benzo Oh iJ 11111111111144-2/
��
Perylene
niormill I
IN
Flucirinthene
108<We(Z-Chloro-
011-9)Methane ■■■_ ME •
B.Bi (2-Chloro-■■.__
ethyl)Ether
(11144-4)
128.911(Z-GMorolto- M■■__
pgoy0 Ether(102.60-1)
(l178i-(2
-Et hyl- IIIh40W1Phthalate
•
y1Bromo-
Ell
Il1(1 Pb!nvI
E iis't101.55-3)
19B,:Butyl Benzyl
78tljf'tji'ari(85-68-7
r
tP o iii_
4. fjlolo17
t -72-3)
• 18L l yj rie
218 9r.::.:. •
?19B_OI,snzo(a,h)
°I.tritt%facihe-.
(53.-70'3)
208. 1,2-D Ichioro-
benzene(96-50-1)
218.1,34OIchloro-
benzena(641-73-1
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
1.POLLUTANT 2.MARK •x' 3. EFFLUENT 4, UNITS 5. INTAKE ([peional/
AND CAS b.MAXI M 3 qY VALUE C.LONG T M VALUE NUMBER BT G b..e- e.c- a.MAXIMUM DAILY VALUE 4 g� ER AYRG J.NO.OF a. LONG TERM
we ucv eauc.CC
[ avola e1 (I/auatla6leJ a.CONCEN• b. MASS AVERAGE VALUE bNO.OF
(i/available) OVIM• MI; .CNT I�) ANAL- ANAL-
eoNCENTwSnoN cu•.c c..r..,non le)^+Ass Y5E5 (�I eoneen• I1 YSES
en _ conc Nrn,,rioN ICI"""�* 01 MASS (.I TRATION ) oNce
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued,
;.7?j,B,1,4-Dichloro-
• en.(106-45-7)
01.44.1
Z3'-DIchloro, - [ + r
Yips
Ohyl
i.,. ,yl• •
•
-Butyl
�1� 2.4-DInItro-
,04y (1.21.14-2)
288 413,Initro-to.!Wipe(606-20-2)
'298;DI*1-OctyI —
Phth.lete
(117484-0)
•
300:1,27Dlphenyl-
—
hysr iioi.(cr Azo-
)idnzene)(122-68-71
31 r Fluorenthane 1
(200-M-0)
328Fluorens •
(003.7) .
4/1 -
s•_
348..Hex.-
—
•chlorobu'tadiene
.(87-68-3)
35B.Hexechloro- • — 1
cyolopentadlene
(77-47-4)
•
368.Hexachioro-
ethane(67-72-1)
378.Ind.no -
(1,2,3-cd)Pyrene
(193-39-6)
388.Isophorone
(78-59-1)
39B.Naphthalene
(91-20-3)
408.Nitrobenzene —(98-95-3)
418.N-N Itro-
sodlmethylamIne
(62-75-9)
42B.N-Nltrosodl-
N-Propylamine
(621-64-7) •
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE

a
CONTINUED FROM THE FRONT
I.POLLUTANT 2.MARK'x' 3. EFFLUENT ~_-1,T^•• 4. UNITS 5. INTAKE (optional) 4
AND CAS
NUMBER Ares., b.■c- C ee- a.MAXIMUM 'DAILY VALUE b.MAXIMUM 3p PAY VALUE c,LONG 7 M yL[(� VALUE
INa LliV ed Ll[V e0 (1/available) (7J OUa!!ab(e� d.NO.OF AVa. LONG TERM
ERAGE VALUE b•NO.OF
ANAL- a.TRATION
CONC • b. MASS
Na- ►n a- As- (tl IAA" " ANAL-
Of available) OVIR• MI; st Nr (') 1,1^+-ss YSES III coNcew• I'll•.Ass KSES.
eo GONG ION GONCAINTwAT.ON III owes GONc.!11v A,ioN TR ATION TNAr1ON
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
43B.N-NItro-
sodiphenylamine
(88-30-6)
44B.Phananthrane
(86.01-8)
438.Pyrane
48p 1,2.4';Tr1-
0(10 of nzana.
FRACT10 —PESTICIDES
Okra rn' .
2.P:-c a1�C
(d1$I$k6)•
( C
319 BH 31 7)
4P:''yy-BHC
(68-88.9) N/A
5P.S-811C
(319-86-8) -
6P.Chlordane
(57.74-9)
7P.4,4'-DOT
(60-29-3)
8P.4,4'-ODE
(72-66-9)
•
9P.4,4:-DD D •
•
(72-64-8)
10P.Dleidrin •
(60.67-1)
11P,a-Endosulfan
(115-29-7)
12P.R-Endosulfan
(115-29-7)
13P.Endosulfan
Sulfate
(1031-07-8)
14P.Endrin
(72-20-8)
15P.Endrin
Aldehyde
(7421-93.4) .
16P.Heptachlor
(76-44-8)
EPA Form 35.10-2C (8-90) PAGE V-8 CONTINUE ON PAGE V.9

• EPA 1.0.NUMBER(copy from Item 1 of Form 11 OUTFALL NUMBER •
CONTINUED FROM PAGE V-8 I\1(41 ‘( 1 IJ 9(0 .. ocul-
1.POLLUTANT 2.MARK •X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional/
AND CAS
NUFA6ER aTasT• b •c• C Rc• a•MAXIMUM DAILY VALUE b.MAXIM�.[M 3 pt T VALUE c.LONG TERM At(RG VALUE
iNc Llavaa uavar� (If auculabte) (`/4UnFWDt¢) �.NO.OF AVERAG VALVE a. LONG TERM b,NO.OF
(I/avails blc R¢- ♦Rfi• wR- - ANAL- a.CATION• b.MASS J oV R• fcNr f:NT (') ANAL•
ap CONCENTRATION Ili MAff I`) (Z)Mwft I`I Itl MASC YSES TR ATION I,TRATIONN-
CONGE.NTNATION CONCCNTMATION (il«wff YSES
GC/MS FRACTION—PESTICIDES(continued)
17P.Heptachlor
Epoxide
(1024-67-3)
18P.PCB-1242
(63469-21-9)
19P.PCB-1254
(11097-69-1)
20P,PCB-1221
(11104-28-2)
rt
21P,PC8•1232 • •
(11141.16.5)
22P.PCB-1248 —_
(12672-29-6)
23P.PC8-1260 — — — — —'—
(11096-82.6)
24P.PCB-1016
(12674-11-2)
25P.Toxephene .
(8001-35-2)
PAGE V-9
•
•
•
:PA Form 3510-29 (8-90)
•
mei

0 0 +
: *
Case Narrative RABflRAtOp�s RJG
Date: 3/1/05
Company: FMC Corp.Lithium Division Client Project ID: Weekly WW 2/10/05
Contact: Rodney Willis Prism COC Group No: G0205380
Address: Seven LakePointe Plaza
2801 Yorkmont Rd.,Suite 300
Charlotte,NC 28208
-rhe attached Laboratory Report contains the analytical results for the project identified above and includes a
Chain-of-Custody copy.
Data qualifiers are flagged individually on each sample. A Key Reference for the data qualifiers appears at the bottom of this page.
Quality control statements and/or sample specific remarks are included in the sample comments section of the
laboratory report for each sample affected.
Please call if you have any questions relating to this analytical report.
Data Reviewed by: Cara Rusmisell roject Manager. Whitney Munroe
Signature: __ Signature: k yntr �-e_
Review Date: 3/1/05 Approval Date: 3/1/05 �'
Data Qualifier Key Reference:
#: Result outside of QC Limits
B: Compound also detected in the method blank
DO: Compound diluted out.
E: Estimated concentration,calibration range exceeded
•J: The analyte was positively identified but the value is estimated below the reporting limit
JH: Estimated concentration with a high bias
JL: Estimated concentration with a low bias
M: A matrix effect is present
T: Tentatively identified compound. The concentration is estimated.
•
Note: This report should not be reproduced,except in its entirety,without the written consent of Prism Laboratories,Inc.
449 Springbrook Road,P.0.Box 240543,Charlotte,NC 28224-0403
Phone: [phone] Toll Free: 800/529-6364 Fax: [phone]
Ficommon\casenarrative Revised 4/20/04 Revised 4/20/04

A- t
•
NC Certification No.402 Laboratory Report
SC Certification No.99012
r=ail' NC Drinking Water Cert.No.37735 3/1/05
FL Certification No.E87519
Full Service Analytical R Environmental solutions
FMC Corporation Lithium Division Project Name: Weekly Wastewater Client Sample ID: 004
Attn: Rodney Willis Project ID: Weekly Wastewater Prism Sample ID: 111005
Seven LakePointe Plaza Sample Matrix: Water COC Group: G0205380
2801 Yorkmont Rd.Ste.300 Time Collected: 02/10/05 15:18
Charlotte, NC 28208 Time Submitted: 02/11/05 14:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Ammonia Nitrogen by Automated Phenate Method
Ammonia BRL mg/L 0.50 0.013 1 SM4500-NH3 H 02/17/05 10:51 cmatthews Q03209
Biochemical Oxygen Demand
I30D-5 BRL mg/L 3.2 1 405.1 02/11/05 18:52 agibson Q03206
Chemical Oxygen Demand
Chemical Oxygen Demand BRL mg/L 50 5.1 1 SM5220 D 02/16/05 8:00 tmaher Q03150
Total Organic Carbon
Subcontract Report See Attached 1 See Attached
Analysis Note for Subcontract Report: Sample subcontracted to NC-Certified laboratory, Test
America, Inc.
Total Suspended Solids
Total Suspended Solids BRL mg/L 1.7 0.57 1 160.2 02/15/05 18:05 agibson Q03144
Sample Comment(s):
BRL= Below Reporting Limit
J=Estimated value between the Reporting Limit and the MDL
Z-7:2
Angela D.Overcash, V.P.Laboratory Services
449 Springbrook Road - P.O.Box 240543 - Charlotte,NC 28224-0543
Phone:[phone] - Toil Free Number.1.800/529-6364 - Fax:[phone] Page 1 of 1

Testlmerica
ANAIYTICAI TESTING CORPORATION
2060 Fosssa Csslosson Dies•IVnsseata,17ess$ss 37204
800-765-0080•615-726-3404 FAR
ANALYTICAL REPORT
PRISM LABORATORIES 5625 Lab Number: 05-A20793
ANGELA OVERCASH Sample ID: 111005
P.O. BOX 240543 Sample Type: Water
CHARLOTTE, NC 28224 Site ID:
Date Collected: 2/10/05
Project: Time Collected: 15:18
Project Name: G0205380 Date Received: 2/15/05
Sampler: Time Received: 8:00
Report Dil Analysis Analysis
Analyte Result Units Limit Factor Date Time Analyst Method Batch
•MISCELLANEOUS CHEMISTRY•
Total Organic Carbon ND mg/1 1.00 1 2/23/05 14:56 S. Prayter 415.1 4262
LABORATORY COMMENTS:
ND = Not detected at the limit of detection
B = Analyte was detected in the method blank.
J = Estimated Value below Report Limit.
E = Estimated Value above the calibration limit of the instrument.
# = Recovery outside Laboratory historical or method prescribed limits.
End of Sample Report.

t -Jr .-
•
•
Testlmerica
ANALYTICAL TESTING CORPORATION
2960 Rosrss Ceneiron Dim•%swa.t►,Tew.isssee 37209
800-785-0980•816-726-3404 Fea
PROJECT QUALITY CONTROL DATA
Project Number:
Project Name: G0205380
Page: 1
Laboratory Receipt Date: 2/15/05
•
Matrix Spike Recovery
Note: If Blank is referenced as the sample spiked, insufficient volume was received for the defined analytical batch for
MS/MSD analysis on an true sample matrix- Laboratory reagent water was used for QC purposes.
Analyte units Orig. Val. MS Val Spike Conc Recovery Target Range Q.C. Batch Spike Sample
**MISC PARAMETERS**
Total Organic Carbon mg/1 42.7 62.8 20.0 100 80 - 120 4262 0S-A20560
Matrix Spike Duplicate
Analyte units Orig. Val. Duplicate RPD Limit Q.C. Batch
Total Organic Carbon mg/1 62.8 64.2 2.20 20 4262
Laboratory Control Data
Analyte units Known Val. Analyzed Val 4 Recovery Target Range Q.C. Batch
**MISC PARAMETERS**
Total Organic Carbon mg/1 200. 184. 92 87 - 110 4262
Duplicates
Analyte units Orig. Val. Duplicate RPD Limit Q.C. Batch Sample Duped
•
Project QC continued .

Testlmerica
ANALYTICAL TESTING CORPORATION
2960 Forn s Cxe ceros Dims•NASHVILLE.Ttxrsssss 37204
800.765-0980•615-728-3404 FM
PROJECT QUALITY CONTROL DATA
Project Number:
Project Name: G0205380
Page: 2
Laboratory Receipt Date: 2/15/05
Blank Data
Analyte Blank Value Units Q.C. Batch Date Analyzed Time Analyzed
**MISC PARAMETERS••
Total Organic Carbon c 1.00 mg/1 4262 2/23/05 14:56
$ . Value outside Laboratory historical or method prescribed QC limits.
End of Report for Project 406310

10
•
TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Fusin Cmcxron Dime•NASHVxax.TENSE:RME 37204
800-763.0980•815-726.3404 FAx
2/25/05
PRISM LABORATORIES 5625
ANGELA OVERCASH
P.O. BOX 240543
CHARLOTTE, NC 28224
This report includes the analytical certificates of analysis for all
samples listed below. These samples relate to your project identified
below:
Project Name: G0205380
Project Number: .
Laboratory Project Number: 406310.
An executed copy of the chain of custody, the project quality
control data, and the sample receipt form are also included as an
addendum to this report. Any QC recoveries outside laboratory
control limits are flagged individually with an #. Sample specific
comments and quality control statements are included in the Laboratory
notes section of the analytical report for each sample report. If you
have any questions relating to this analytical report, please contact
your Laboratory Project Manager at 1-800-765-0980. Any opinions, if
expressed, are outside the scope of the Laboratory's accreditation.
Page 1
Sample Identification Lab Number Collection Date
111005 05-A20793 2/10/05

Testlmerica
ANALYTICAL TESTING CORPORATION
2960 Fosrex Cxucaron Daft•Neaueu,u.TaN:IxsSxx 37204 /
800-765-0900•615-726-3404 FAX
Page 2
Sample Identification Lab Number Collection Date
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Report Date: 2/25/05
Johnny A. Mitchell, Laboratory Director Gail A. Lage, Senior Project Manager
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Services
Pamela A. Langford, Senior Project Manager Kelly S. Comstock, Technical Services
Eric S. Smith, QA/QC Director Roxanne L. Connor, Senior Project Manage
Sandra McMillin, Technical Services Mark Hollingsworth, Director of Project
Laboratory Certification Number: 387
This material is intended only for the use of the individual(s) or entity to whom it is addressed,
and may contain information that is privileged and confidential. If you are not the intended recipient,
or the employee or agent responsible for delivering this material to the intended recipient, you are
hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited.
If you have received this material in error, please notify us immediately at 615-726-0177.

'•ir tP .S. t`' LAB USE ONLY
CHAIN OF CUSTODY RECORD
.. ' taA9ARAT0916$IryC i 7 c
. ,, r (( .c 4,�`+�d � ,x* ��1'�, e ' `tYF-----
Full :'IJt7 'NfA"
•+_ - PAGE_.__l_OF_.,..QUOTE lI TO ENSURE PROPER BILLING: 4 Sat 096,( •Ir'J,b" 1 r ( �a :AY', _ _
Service Analytical&Environmental Solutions -• ';.''1
Project Name: kte��Ce
449 Springbrook Road•P.O.Box 240543•Charlotte,NC 28224-0543 �•1.PS�ES '?�"o ® f ��I to '
Phone:[phone] • Fax [phone] Short Hold Analysis: (Yes) (No) UST Project (Yes) (No) s a 'i X-''�" -
o>a sLi-
Client Company Name: Fwc_ *Please ATTACH any project specific reporting(QC LEVEL 111 111 IV) � Fi'�1�4F �z -�' ?
Report To/Contact Name: tT) �`� \ provisions and/or QC Requirements k ^-.a O "-,, 5 T, { Tw I '2 J- __..
Invoice To; �� 1
Reporting Addre j °
E4�,ENt�Izl dJL Z�>�4� Address: ��
Phone: Fax(Yes)(No): Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Emal No)Email Address Requested Due Date Q 1 Day ❑2 Days 0 3 0 4 Days Q 5 Days/ Y DaysY Y Certification: NELAC USACE FL NC X-
EDD Type:__PDF Excel t/ Other "Working Days" Q 6-9 Days 0 Standard 10 days
Site Location Name: -M•� _SC OTHER N/A
Samples received after 15:00 will be processed next business day. —
Site Location Physical Address: NA w 1 UPI Turnaround time is based on business days,excluding weekends and holidays. Water Chlorinated: YES— NO1`-
(SEE REVERSE FOR TERMS&CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES?� NO
-- RENDERED BY PRISM LABORATORIES,INC.TO CLIENT) P
TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED
CLIENT DATE COLLECTED (SOIL, ! , PRISM
PRESERVA- �/
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE TIVES �� /►�!� ///
REMARKS IDLAB
NO.
HOURS SLUDGE) SEE BELOW NO. SIZE v `\ N
C'Q4- 2 t 05 151 W`t` 1 — 00,J5... it(oos
So u 4-- PDF- 1E1E) LA....q IA SO
ti_QA- -)711.D.v Is-P- ttit _Xq ---- tAc L )C _1
_ ,
t r, , C
,,I A PRESS DOWN FIRM Y.,3 COPIES
Sampler's Signature `�.JL.Jis-1CU Sampled By(Print Name) N � V'�u' l-1 `�
p 9 P F Affiliation
Upon relinquishing,this Chain of Custody is your authorization for Prism to proceed with the analyse as requested above.Any changes must be RISE ONLY-:
submitted in writing to the Prism Project Manager.There will be charges f. any gas afterraI es have been initialized.
ishe By Remy 8y:(Sig =tu
D el Militry/lto� Additional Comments 51 sg`I'lit T e 14 3 ''
fri
!qulsIgnaIure) - ec al"" alum) Da v e Depart&e:Time.
Relinquish y:( g ur) / Received For Prism Lab' : -. . n,te Fi !u I
iv hi ent. NbTE:A S Otel4S SHOULD BE TAPED SHUT WITH CUSTODY SEALS FO•T-A :PORTATION TO THE LABORATORY. Log In roue No. m
. SAMP S ARE T ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED ATT E •:ORATORY.
El Fed Ex 0 UPS 0 Hand-delivered sm Field Service O Other Go ao53 So _
N��''DES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: �^ CERCLA LANDFILL OTHER: �1''i(�F 1' 1'1- '.1 ,t I
%-**NC GSC ONC ❑SC ONC OSC ONC 0SC CI NC ❑SC ❑NC QSC ONC GSC ONC ❑SC ONC (USC I li,,r,.>"'`:••'^ " hi"(' ";'ll
,
O _ 0 o_•_._ 0 --i o D o _ o _ ORIGINAL
*CONTAINER TYPE CODkS: A=Amber C=Clear G=Glass P=Plastic; TL=Teflon-Lined Cap VOs.=Volatile Organics Analysis(Zero Head Space)

•
FMC Corporation—Lithium Division
NPDES Permit Renewal, March 2005
Permit No. NC0005177
Sludge Management Plan
In February 1999, FMC discontinued operation of its two sanitary sewer package plants
by directing all sanitary sewer wastewater and laboratory drains to the Bessemer City
POTW. Therefore, no Sludge Management Plan is required.
3lz ©5
oly Weathers Date
f onmental Manager
FMC Corporation—Lithium Division

SOC PRIORITY PROJECT: No
To: Permits and Engineering Unit
Water Quality Section
Attention: Mike Myers
Date: August 21, 2001
NPDES STAFF REPORT AND RECOMMENDATIONS
County: Gaston
NPDES Permit No.: NC0005177
MRO No.: 01-94
PART I -GENERAL INFORMATION
1. Facility and address: FMC Corporation, Lithium Division
Highway 161
Post Office Box 795
Bessemer City,N.C. 28016
2. Date of investigation: August 21, 2001
3. Report prepared by: Michael L. Parker, Environmental Engineer II
4. Person contacted and telephone number: Kimberly Weathers, [phone]
5. Directions to site: The Lithium plant is located on the south(left) side of Hwy. 161 . 0.1
mile west of the jct. of Hwy. 161 and SR 1402,just west of Bessemer City. � 5
� `7 c S I,
6. Discharge point(s), List for all discharge Points: -
Latitude: 35° 15' 44"
Longitude: 81° 17' 57"
Attach a USGS Map Extract and indicate treatment plant site and discharge point on map.
USGS Quad No.: F 13 SE
7. Site size and expansion area consistent with application: Yes. Ample area exists for the
construction of additional WWT facilities, if necessary.
8. Topography (relationship to flood plain included): The site encompasses several hundred
acres with varying topography (3-10%slopes). The main WWT pond is located in a
surface drainage feature, however, it appears to be protected from flooding.
9. Location of nearest dwelling: Approx. 1000± feet from the WWTP site.

Page Two
10. Receiving stream or affected surface waters: U. T. to Abernathy Creek
a. Classification: C
b. River Basin and Subbasin No.: Catawba 030837
c. Describe receiving stream features and pertinent downstream uses: Flow
observed in the receiving stream at the point of discharge. Downstream uses are
primarily agriculture. No other dischargers are known for a reasonable distance
downstream.
PART II -DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
Outfall 001 Outfall 004
1. a. Volume of wastewater: 0.615 MGD Intermittent
b. What is the current permitted capacity: 0.615 MGD (outfall 001)
c. Actual treatment capacity of current facility (current design capacity): 0.615 MGD
d. Date(s) and construction activities allowed by previous ATCs issued in the
previous two years: There have been no ATCs issued in the past two (2)years.
e. Description of existing or substantially constructed WWT facilities: The existing
WWT facilities at outfall 001 consist of two (2) Reverse Osmosis treatment units
followed by a hydrogen peroxide feed for chlorine neutralization, pH adjustment
(H2SO4 acid), and an 18 acre industrial WWT lagoon with a flow meter with
totalizer. Wastewater treated by these treatment processes include discharges of
lithium hydroxide, lithium chloride, and a discharge from a lithium hypochlorite
particulate air scrubber. There is also wastewater entering this outfall from floor
area sumps, boiler blowdown, wet particulate air scrubbers, and stormwater.
There is also a small, earthen pond (referred to as the R&D pond in the renewal
application)that receives condensate, cooling tower overflow, and stormwater.
The water is typically recycled back into the plant,however, if an overflow does
occur,the discharge from this pond will eventually travel through a series of
small, earthen settling ponds prior to reaching the receiving stream and
discharging at outfall 004.
f. Description of proposed WWT facilities: There are no WWT facilities proposed at
this time.
g. Possible toxic impacts to surface waters: This facility has had a consistent
compliance record with respect to toxicity testing.
2. Residual handling and utilization/disposal scheme: As the result of changes in the
manufacturing process,there are essentially no residuals generated at this time.
Previously, residuals were removed from the main treatment pond and stockpiled on-site.
These solids were used throughout the site to fill uneven terrain and stabilize roads.

Page Three
3. Treatment Plant Classification: Class II (no change from previous rating).
4. SIC Code(s): 2819, 2869 Wastewater Code(s): 32, 31, 02
5. MTU Code(s): 50000
PART III- OTHER PERTINENT INFORMATION
1. Is this facility being constructed with Construction Grant Funds or are any public monies
involved(municipals only)?No
2. Special monitoring or limitations (including toxicity)requests: None at this time.
3. Important SOC/JOC or Compliance Schedule dates: N/A
4. Alternative Analysis Evaluation: There are no known on-site or off-site alternatives that
are currently available which would eliminate the need to discharge.
PART IV-EVALUATION AND RECOMMENDATIONS
The permittee, FMC Corporation, Lithium Division(FMC), requests renewal of the
subject Permit. Changes at this facility since the permit was last renewed include the removal
and demolition of the spodumene ore process, and the removal and demolition of the two (2)
package-type WWTPs that treated all of the domestic wastewater generated on-site. The
spodumene ore process moved to a FMC site in South America, and all domestic wastewater is
now diverted to Bessemer City's sewer collection system. All of the changes made at this facility
since the permit was last reissued are documented in the renewal application.
Pending receipt and approval of the WLA, it is recommended that the Permit be renewed
as requested.
7/4"4.e... , c- ,. 4(...._ , / r
2/ °`
Signature of Report Preparer Da
I,/), 14 e.0CS`-4 . Y v/
Water Quality Reg' al Supervisor ate
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CONTOUR iNTER4',�L 20 FEET
NATIONAL GEODETIC VERTICAI DATUM nF 1Q Q Jr

vl'DES WASTE LOAD ALLOCATION ,tee co i.
cin.R.e;007i.a
PERMIT NO.: NC0005177 Modeler Date Rec. #
Corporation
S `liz:q �° _ $`k8 �, ,e,°)
FMC
PERMITTEE NAME:
FACILITY NAME: Lithium Division Drainage Area(mil ) r _ Avg. Streamflow (cfs): I,7
Facility Status: Existing 7Q10 (cfs) (3, 7 Winter 7Q 1 H H (c Cs) o, `r 3 30Q2 (cfs) : -X
Permit Status: Renewal with Modification Toxicity Limits: IWC 7 % Acutero ,
N.C. DEPT. s• -
Major q Minor ENVIRONMENT, H r, rstream Monitoring:
& NATURAL RF SO ' ;C,. /
Pipe No.: 001 Parameters C(w,d E, (ftA) .T r .1 lc, '�1,,:{f (";,,,,'„.7., 4,,
Design Capacity: 0.615 MGD f o.7/p,g/ O.q AUG 30 199 Upstream Y Location v�i` i
Domestic (% of Flow): 3.2 % DIVISION OF ENVIRONMENTAL IAA A EVENT Downstream Y Location-1��1 t 41,11(' ' 515 -fh1 cl
Industrial (% of Flow): 96.8 %
MOORESVIILE RESIONAL OF I — - C-7- -4 t( ,,,,y`^w
U;-(oe,,1.-!4') G Lz k
Monthly Avg. Daily Max. WQ or EL
Comments: Flow (MGD): 0.615
BODS (mg/1): 3 0 4 5 WQ
FMC requests additional flow limits at 0.615 to 0.7 MGD, 0.7 to 0.8 TSS (Ibs/day): 333.9 1001.7 BPT
MGD, and 0.8 to 0.9 MGD. FMC also requests combining 004 DO(mg/1): 5
(stmwtr) and toe drain discharge with existing 001 under one permit. pH (SU): 6-9
NH3-N(mg/1): monitor
RECEIVING STREAM:an unnamed tributary to Abernethy Creek Chlorides (mg/1): monitor
Chromium (µg/1): monitor
Class: C Copper(4/1): monitor
Sub-Basin: 03-08-37 Zinc Olga): monitor
TN(m ): Qrtrly monitor
Reference USGS Quad: F 13 SE (please attach) TP(mom): ly monitor
County: Gaston 1' 1 ` "'
Regional Office: Mooresville Regional Office
Previous Exp. Date: 9/30/96 Treatment Plant Class: Class III
Classification changes within three miles:
none
Requested by: Steve Pellei Date: 4/16/96
Prepared by: `"--17---0, )2rc,�t Date: ,9,27/'/ Comments: f �; / ,,.....a. '��n�tra,t V t,.,, .--
Reviewed by I yl (/ ",u'� , K [. �_. ��U
(z c(.(AAf � Date: , i n :r k-,..-
. ,.,lr, /. 1,)

•
!VPDES WASTE LOAD.ALLOCATION ►eu, co Q
OA:R i F;,wrie)
PERMIT NO.:
NC0005177 Modeler Date Rec. #
FMC Corporation
Sk03 `V-1,1 cto S4g r,e
4 (t, .,o)
PERMITTEE NAME: rP
FACILITY NAME:
Lithium Division Drainage Area(mil ) / ,4 Avg. Streamflow (cfs): 1.7
Facility Status: Existing 7Q10(cfs) 0.27 Winter 7Q1t t (cis) °•4`3 30Q2 (cfs) v. 58
Permit Status: Renewal with Modification Toxicity Limits: IWC J % Acute/(-ironic-
Major �l Minor _
Instream Monitoring:
Pipe No.: 001 . J C,i, J v,d',-�i;,,
Parameters Cl^I w��� T��� s�.��.c� - ,�� �;
Design Capacity: 0.615 MGD/O:'1/o.0/O.ci Upstream Y Location l�r s f( J
Domestic (% of Flow): 3.2 % Downstream \/ Location JL9/1,! I At(' C1u sfi4M f
Industrial (% of Flow): 96.8 % o�i F,tl 7 u +�E,act 7 GEz/c
Monthly Avg. Daily Max. WQ or EL
Comments: Flow (MGD): 0.700
FMC requests additional flow limits at 0.615 to 0.7 MGD,0.7 to 0.8 BODS (mg/1): 26 WQ
MGD, and 0.8 to 0.9 MGD. FMC also requests combining 004 TSS (lbs/day): 333.9 1001.7 BPT
(stmwtr) and toe drain discharge with existing 001 under one permit. DO(mg/1): 5
pH (SU): 6-9
NH3-N (mg/1): monitor
RECEIVING STREAM:an unnamed tributary to Abernethy Creek Chlorides (mg/1): monitor
Class: C Chromium (14/1): monitor
Sub-Basin: 03-08-37 Copper(µg/1): monitor
Zinc (p.g/1): monitor
Reference USGS Quad: F 13 SE (please attach) TN(mom): Qrtrly monitor
County: Gaston TP(mom): Qrtrly monitor
Regional Office: Mooresville Regional Office
Previous Exp. Date: 9/30/96 Treatment Plant Class: Class III
Classification changes within three miles:
none
R ec uested by: Steve Pellei Date: 4/16/96
1 ,,w � ' • e
Prepared by: _,„ °`- / Date: �7 7,Q Comments; �f ��a4 �ti /�n,,, n1� r,:h ��/l
/ g, A %/E /4L ;Nd„J4-,1J/W I-, e;.#7cc 6-1 !/G 414A t,,r++�:i' ✓e 9 • /E c.tt-c_
R e�iewed b � v Date:
79L— i Y

- i
II'DES WASTE LOAD ALLOCATION ,tee co w.
cLAtAitcA'flow)
PERMIT Na:
NC0005177 Modeler Date Rec. # .
I
FMC Corporation S 4 u 1 co ;g4 4 � g' ,c,°)
PE RMITTEE NAME: rP
Lithium Division Drainage Area(mil
F:�CILTTY NAME: ) / ,4 Avg. Streamflow (cfs): I,7
—
Facility Status: Existing 7Q10 (cfs) d•27 Winter 7Q1( (cfs) °•`/3 30Q2 (cfs) v. 58
Permit Status: Renewal with Modification Toxicity Limits: IWC FZ % Acut hrom
Major "1 Minor Instream Monitoring:
Pipe No.: 001 Parameters Cl^10,(<15 7 a) �S f9 'Jci c!"4 L-,d,Ii
DesignCapacity: 0.615 MGD/o.t 0.g O. Upstream Y Location � st
( /
Domestic (% of Flow): 3.2 % Downstream ' Location--DIA't dt 4 t-f/ I.. sfrf.. 1 1L
Industrial (% of Flow): 96.8 % o.Ji-F7tt J I4IoEi;JE y GIA/c
Comments: Monthly Avg. Daily Max. WQ or EL
Flow (MGD): 0.800
FMC requests additional flow limits at 0.615 to 0.7 MGD, 0.7 to 0.8 BODS (mg/1): 23 WQ
MGD, and 0.8 to 0.9 MGD. FMC also requests combining 004 TSS (lbs/day): 333.9 1001.7 BPT
(stmwtr) and toe drain discharge with existing 001 under one permit. DO(mg/1): 5
pH (SU): 6-9
RECEIVING STREAM:an unnamed tributary to Abernethy Creek NH3-N (mg/1):
monitor
Chlorides(mg/1): monitor
Class: C Chromium (14/1): monitor
Sub-Basin: 03-08-37 Copperµ(pg/1): monitor
Cop
monitor
Reference USGS Quad: F 13 SE (please attach) TN(mg/1): Qrtrly monitor
County:
Gaston TP(mg/1): Qrtrly monitor
__.
Regional Office: Mooresville Regional Office
Previous Exp. Date: 9/30/96 Treatment Plant Class: Class III
Classification changes within three miles:
none -
Requested by: Steve Pellei Date: 4/16/96
Prepared by: °`"-`�� � � Date: 3/27 9� Comments: �� 4 V��� -�.� �ti� f� /u- �, 5,.� �l
Reviewed by .f1� A("! Date: - `4 f;l c,,''', '51'"' r' r'�,�' C qpr c.,�-fc / 4 ,,--1 /iv z 4 it,tom::
tn!v�,,� {' ,� vv //V lib v`"i�/fildgli7�l f. 71i,44c ky, f 6,,i1j.,
!D�vJ Z /i'i l j

- 1
Nil DES WASTE LOAD ALLOCATION AeLb t74)e.
UwtRiFC Atlo.)
NC0005177 Modeler Date Rec. #
PERMIT NO.: I
PERMITTEE NAME: FMC Corporation 3 2 �`z� ;�° 841.
(�a,�,c>D)
Lithium Division Drainage Area(mt ) / ,Li_
FACILITY NAME: - Avg. Streamflow (cfs): 1-7
Facility Status: Existing 7Q10 (cfs) 0. 27 Winter 7Q1( (cfs) 0, y-3 30Q2 (cfs) v. 58
Permit Status: Renewal with Modification Toxicity Limits: IWC hi % AcutiiChronic
Major .\l Minor Instream Monitoring: .
Pipe No.: 001 Parameters C w,d is -ritA) . s f4.JJE.J S1,dJ C),,t.,i,,,,-/-)
DesignCapacity: 0.615 MGD o.1 'O. ' r t ,4,,,
� �o•$� � Upstream Y Location � s � /
Domestic (% of Flow): 3.2 % Downstream Y Location-E•im t 4,A fil c:�u..,5fi f4,1 c 1L
Industrial (% of Flow): 96.8 % o-rC7tt ,,7J .4(,(..,c1-4') GEac
Comments: Monthly Avg. Daily Max. WQ or EL
Flow (MGD): ` 0.900
FMC requests additional flow limits at 0.615 to 0.7 MGD, 0.7 to 0.8 BODS (mg/I): 20.5 WQ
MGD, and 0.8 to 0.9 MGD. FMC also requests combining 004 TSS (lbs/day): 333.9 1001.7 BPT
(stmwtr) and toe drain discharge with existing 001 under one permit. DO(mg/1): 5
pH (SU): 6-9
RECEIVING STREAM:an unnamed tributary to Abernethy Creek NH3-N (mg/1): monitor
Chlorides (mg/1): monitor
Class: C Chromium (µg/1): monitor
Sub-Basin: 03-08-37 Copper(1.41): monitor
Zinc (j4/1): monitor
Reference USGS Quad: F 13 SE (please attach) TN(mg/1): Qrtrly monitor
County: Gaston TP(mg/1): Qrtrly monitor
Regional Office: Mooresville Regional Office
Previous Exp. Date: 9/30/96 Treatment Plant Class: Class III
C'ossification changes within three miles:
nc Ong
R ecuested by: Steve Pellei Date: 4/16/96
F-e,tared by: °� / 'Date: ; 27 ,% Comment f 9L 4g /frpN..;d'c /4 7) ' ` c di i,A -�,//
y� /L v,J , t Ldvl/Yi_,S i v ,r4-5 W'LI i E- 4reol . 't4 7t ck1-
F eN iewed b / _ �.; ..# Date: a,� 2. iti /,�%
/'✓EYE. s r

c.. ,
t•
FACT SHEET FOR WASTELOAD ALLOCATION AUG
Requests#
(a,b'c,d)
Facility Name: FMC CORP.-LITHIUM DIV
NPDES No.: NC0005177
Type of Waste: Industrial - 96.8% /Domestic 3.2%
Facility Status: Existing
Permit Status: Renewal with Modification
Receiving Stream: UT Abernethy Creek
Stream Classification: C
Subbasin: 0301837
County: Gaston ,,� Stream Characteristic:
Regional Office: Mooresville) Ji l USGS #
Requestor: Pellei Date:
DLit;of Request: 4/22/96 Drainage Area(mi2): 1.4
Topo Quad: F13SE Summer 7Q10 (cfs): 0.27
Winter 7Q10(cfs): 0.43 Ul
Average Flow(cfs): 1.7
30Q2 (cfs): 0.58
IWC (%): 78
Wasteload Allocation Summary
(approach taken, correspondence with region, EPA,etc.)
Facility requesting renewal with modification of wasteflow to 0.7,0.8, and 0.9 MGD. Facility
requesting the existing stormwater outfalls be incorporated into NPDES process water discharge.
Expansion flows were run in QUAL2e model of Crowders Creek basin dischargers. Results
indicate that if existing permitted loading for BOD5 held the same,expansion flows can be
allowed. Updated raw material information from facility results in higher effluent guidelines (see
attached) for TSS. Chronic toxicity tests recommended for each wasteflow. Reasonable potential
toxicity analysis recommends deletion of limits and monitoring requirements for
dibromochloromethane, bromodichloromethane, bromoform, and chloroform.
Special Schedule Requirements and additional comments from Reviewers:
& re , / /ts
Ct 7,1 f,kK T i,J 4- 5 . P1L4 rid vip/ilc7 77/E ��,c£-c7r,e
prols V-115 N£-c-ess
Recommended by:
`' `�i Date:7/26/96 _
Reviewed by
Instream Assessment: Date:
Regional Supervisor:PA) `� Date: g//9 7‘
/-
Permits &Engineering: �b/171:/ .-- 6/ ----" Date: _ 6
AUG9 'fib RETURN TO TECHNICAL SUPPORT BY:

2
TOXICS/METALS/CONVENTIONAL PARAMETERS
Existing Limit: Chronic Ceriodaphnia Pass/Fail @ 78%
Recommended Limit: 78%
Monitoring Schedule: JAN APR JUL OCT
Existing Limits
Monthly Avg. Daily Max.
Flow (MGD): 0.615
BOD5 (mg/1): 30 45
TSR (lbs/day): 86.91 260.82
DO(mg/1): 5
pH (SU): 6-9
Dibromochloromethane 44
(µg/1)
Bromodichloromethane 28
(;)-gin:
NH3-N (mg/1): monitor
Bromoform WA): Qrtrly monitor
Chloroform (4/1): Qrtrly monitor
Chlorides (mg/1): monitor
Chromium ( 4/1): monitor
Copper(µg/1): monitor
Zinc (14/1): monitor
TN(mg/1): Qrtrly monitor
TP(mg/1): Qrtrly monitor
Recommended Limits for #WLA 8484(a)
Monthly Avg. Daily Max. WQ or EL
Flow (MGD): 0.615
BOD5 (mg/I): 30 45 WQ
TSS (lbs/day): 333.9 1001.7 BPT
DO(mg/1): 5
pH (SU): 6-9
NH3-N (mg/1): monitor
Chlorides (mg/1): monitor
Chromium (1.ig/1): monitor
Copper(µg/1): monitor
Zinc (µg/1): monitor
TN(mg/1): Qrtrly monitor
TP (mg/1): Qrtrly monitor
Limits Changes Due To: Parameter(s) Affected
Change in 7Q10 data
Change in stream classification
Relocation of discharge
Change in wasteflow
Updated facility information TSS
Results of reasonable potential analysis Bromoform, Chloroform,
Dibromochloromethane,
Bromodichloromethane

3
Recommended Limits for #WLA 8484(b)
TOXICS/METALS/CONVENTIONAL PARAMETERS
Existing Limit: Chronic Ceriodaphnia Pass/Fail @ 78%
Recommended Limit: 80% @ 0.700 MGD
Monitoring Schedule: JAN APR JUL OCT
Monthly Avg. Daily Max. WQ or EL
Flow (MGD): 0.700
BOD5 (mg/I): 26 WQ
TSS (lbs/day): 333.9 1001.7 BPT
DO(mg/1): 5
pH (SU): 6-9
NH3-N (mg/1): monitor
Chlorides (mg/1): monitor
Chromium (µg/i). monitor
Copper(41): monitor
Zinc (µg/1): monitor
TN(mg/1): Qrtrly monitor
TP(mg/1): Qrtrly monitor
Limits Changes Due To: Parameter(s) Affected
Change in 7Q10 data
Change in stream classification
Relocation of discharge
Change in wasteflow
Updated facility information TSS
Results of reasonable potential analysis Bromoform, Chloroform,
Dibromochloromethane,
Bromodichloromethane
Recommended Limits for #WLA 8484(c)
TOXICS/METALS/CONVENTIONAL PARAMETERS
Existing Limit: Chronic Ceriodaphnia Pass/Fail @ 78%
Recommended Limit: 82% @ 0.800 MGD
Monitoring Schedule: JAN APR JUL OCT
Monthly Avg. Daily Max. WQ or EL
Flow (MGD): 0.800
BOD5 (mg/1): 23 WQ
TSS (lbs/day): 333.9 1001.7 BPT
DO(mg/1): 5
pH (SU): 6-9
NH3-N (mg/1): monitor
Chlorides (mg/1): monitor
Chromium (µg/1): monitor
Copper(µg/1): monitor
Zinc (4/1): monitor
TN(mg/1): Qrtrly monitor
TP(mg/1): Qrtrly monitor

4
Limits Changes Due To: Parameter(s) Affected
Change in 7Q10 data
Change in stream classification
Relocation of discharge
Change in wasteflow
Updated facility information TSS
Results of reasonable potential analysis Bromoform, Chloroform,
Dibromochloromethane,
Bromodichloromethane
Recommended Limits for #WLA 8484(d)
TOXIC S/METALS/CONVENTIONAL PARAMETERS
Existing Limit: Chronic Ceriodaphnia Pass/Fail @ 78%
Recommended Limit: 84% @ 0.900 MGD
Monitoring Schedule: JAN APR JUL OCT
Monthly Avg. Daily Max. WQ or EL
Flow (MGD): 0.900
BOD5 (mg/I): 20.5 WQ
TSS (lbs/day): 333.9 1001.7 BPT
DO(mg/1): 5
pH (SU): 6-9
NH3-N (mg/1): monitor
Chlorides (mg/1): monitor
Chromium (4/1): monitor
Copper(14/1): monitor
Zinc (4/1): monitor
TN(mg/1): Qrtrly monitor
TP(mg/1): Qrtrly monitor
Limits Changes Due To: Parameter(s) Affected
Change in 7Q10 data
Change in stream classification
Relocation of discharge
Change in wasteflow
Updated facility information TSS
Results of reasonable potential analysis Bromoform, Chloroform,
Dibromochloromethane,
Bromodichloromethane
_X_ Parameter(s) are water quality limited. For some parameters, the available load capacity of
the immediate receiving water will be consumed. This may affect future water quality based
effluent limitations for additional dischargers within this portion of the watershed.
OR
No parameters are water quality limited,but this discharge may affect future allocations.

5
INSTREAM MONITORING REQUIREMENTS
Upstream Location: West Canal
Downstream Location: Immediate downstream of outfall in UT Abernethy Creek
Parameters: Chlorides,Totals# ved Solids, Conductivity
uspemled
Special instream monitoring locations or monitoring frequencies:
MISCELLANEOUS INFORMATION&SPECIAL CONDITIONS
Adequacy of Existing Treatment
Has the facility demonstrated the ability to meet the proposed new limits with existing treatment
facilities? Yes No
If no, which parameters cannot be met?
Would a "phasing in" of the new limits be appropriate? Yes No
If yes, please provide a schedule (and basis for that schedule)with the regional
office recommendations:
If no, why not?
Special Instructions or Conditions
Wasteload sent to EPA? (Major) (Y or N)
(If yes, then attach updated evaluation of facility,including toxics analysis,modeling analysis if
modeled at renewal, and description of how it fits into basinwide plan)
Additional Information attached? (Y or N) If yes,explain with attachments.

Facility Name FMC-Lithium Division Permit# _NC0005177 Pipe#_001
CHRONIC TOXICITY PASS/FAIL PERMIT LIMIT (QRTRLY)
The effluent discharge shall at no time exhibit chronic toxicity using test procedures outlined in:
1.) The North Carolina Ceriodaphni4 chronic effluent bioassay procedure (North Carolina Chronic Bioas.eay
Procedure - Revised *September 1989) or subsequent versions.
The effluent concentration at which there may be no observable inhibition of reproduction or significant mortality
is_78_% (defined as treatment two in the North Carolina procedure document). The permit holder shall
perform quarterkv monitoring using this procedure to establish compliance with the permit condition. The first
test will be performed after thirty days from the effective date of this permit during the months of
_JAN APR JUL OCT .. Effluent sampling for this testing shall be performed at the NPDES permitted
final effluent discharge below all treatment processes.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the month in which it was performed,using the parameter code TGP3B.
Additionally,DEM Form AT-1 (original) is to be sent to the following address:
Attention: Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, N.C. 27607
Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in
association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity
sample must be measured and reported if chlorine is employed for disinfection of the waste stream.
Should any single quarterly monitoring indicate a failure to meet specified limits,then monthly monitoring will
begin immediately until such time that a single test is passed. Upon passing,this monthly test requirement will
revert to quarterly in the months specified above.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of
Environmental Management indicate potential impacts to the receiving stream,this permit may be re-opened and
modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival and appropriate environmental controls, shall constitute an invalid test and will require immediate
retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute
noncompliance with monitoring requirements.
7Q10 0.27 cfs
Permitted Flow _0.615 MGD Recot mended by:
IWC _ 78 °k
Basin & Sub-basin _CTB37
Receiving Stream _UT Abernethy Creek_
County _ Gaston (,Date 7/11/96
QCL P/F Version 9/91

Facility Name FMC-Lithium Division Permit# _NC0005177 Pipe# 001
CHRONIC TOXICITY PASS/FAIL PERMIT LIMIT (QRTRLY)
The effluent discharge shall at no time exhibit chronic toxicity using test procedures outlined in:
1.) The North Carolina Ceriodaphnia chronic effluent bioassay procedure (North Carolina Chronic Bioassay
Procedure - Revised *September 1989) or subsequent versions.
The effluent concentration at which there may be no observable inhibition of reproduction or significant mortality
is_80_% (defined as treatment two in the North Carolina procedure document). The permit holder shall
perform quarterly monitoring using this procedure to establish compliance with the permit condition. The first
test will be performed after thirty days from the effective date of this permit during the months of
_JAN APR JUL OCT .. Effluent sampling for this testing shall be performed at the NPDES permitted
final effluent discharge below all treatment processes.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the month in which it was performed,using the parameter code TGP3B.
Additionally, DEM Form AT-1 (original) is to be sent to the following address:
Attention: Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, N.C. 27607
Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in
association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity
sample must be measured and reported if chlorine is employed for disinfection of the waste stream.
Should any single quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring will
begin immediately until such time that a single test is passed. Upon passing,this monthly test requirement will
revert to quarterly in the months specified above.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of
Environmental Management indicate potential impacts to the receiving stream,this permit may be re-opened and
modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival and appropriate environmental controls, shall constitute an invalid test and will require immediate
retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute
noncompliance with monitoring requirements.
7Q10 0.27 cfs
Permitted Flow _0.700 MGD Recommended by:
IWC 80
Basin & Sub-basin _C11B37 `
Receiving Stream _UT Abernethy Creek_ '
County _ Gaston % Date _ /11/96
I /
QCL P/F Version 9/91

Facility Name_FMC-Lithium Division Permit# _NC0005177 Pipe# 001
CHRONIC TOXICITY PASS/FAIL PERMIT LIMIT (QRTRLY)
The effluent discharge shall at no time exhibit chronic toxicity using test procedures outlined in:
1.) The North Carolina Ceriodaphnia chronic effluent bioassay procedure (North Carolina Chronic Bioassay
Procedure - Revised *September 1989) or subsequent versions.
The effluent concentration at which there may be no observable inhibition of reproduction or significant mortality
is_82_% (defined as treatment two in the North Carolina procedure document). The permit holder shall
perform quarterly monitoring using this procedure to establish compliance with the permit condition. The first
test will be performed after thirty days from the effective date of this permit during the months of
_JAN APR JUL OCT .. Effluent sampling for this testing shall be performed at the NPDES permitted
final effluent discharge below all treatment processes.
All toxicity"testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the month in which it was performed, using the parameter code TGP3B.
Additionally,DEM Form AT-1 (original) is to be sent to the following address:
Attention: Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, N.C. 27607
Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in
association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity
sample must be measured and reported if chlorine is employed for disinfection of the waste stream.
Should any single quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring will
begin immediately until such time that a single test is passed. Upon passing, this monthly test requirement will
revert to quarterly in the months specified above.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of
Environmental Management indicate potential impacts to the receiving stream,this permit may be re-opened and
modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document,such as minimum control organism
survival and appropriate environmental controls,shall constitute an invalid test and will require immediate
retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute
noncompliance with monitoring requirements.
7Q10 0.27 cfs
/72
Permitted Flow 0.800 MGD R mmended by:
8
Basin & Sub-basin 2 CTB37 '/
Receiving Stream _UT Abernethy Creek_ /
County _ Gaston , "Date) 7/11/96
QCL P/F Version 9/91

Facility Name FMC-Lithium Division Permit# _NC0005177 Pipe# 001
CHRONIC TOXICITY PASS/FAIL PERMIT LIMIT (QRTRLY)
The effluent discharge shall at no time exhibit chronic toxicity using test procedures outlined in:
1.) The North Carolina Ceriodaphnia,chronic effluent bioassay procedure (North Carolina Chronic Bioassay
Procedure - Revised *September 1989) or subsequent versions.
The effluent concentration at which there may be no observable inhibition of reproduction or significant mortality
is 84_% (defined as treatment two in the North Carolina procedure document). The permit holder shall
perform quarterly monitoring using this procedure to establish compliance with the permit condition. The first
test will be performed after thirty days from the effective date of this permit during the months of
JAN APR JUL OCT .. Effluent sampling for this testing shall be performed at the NPDES permitted
final effluent discharge below all treatment processes.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the month in which it was performed,using the parameter code TGP3B.
Additionally, DEM Form AT-1 (original)is to be sent to the following address:
Attention: Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, N.C. 27607
Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in
association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity
sample must be measured and reported if chlorine is employed for disinfection of the waste stream.
Should any single quarterly monitoring indicate a failure to meet specified limits,then monthly monitoring will
begin immediately until such time that a single test is passed. Upon passing, this monthly test requirement will
revert to quarterly in the months specified above.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of
Environmental Management indicate potential impacts to the receiving stream,this permit may be re-opened and
modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival and appropriate environmental controls,shall constitute an invalid test and will require immediate
retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute
noncompliance with monitoring requirements.
7Q10 0.27 cfs
Permitted Flow 0.900 MGD Recornmended by:
IWC _ 84 %
Basin & Sub-basin _CTB37 c,1,2.e.s1,_ .
Receiving Stream _UT Abernethy Creek_ /
County _ Gaston ate _ /11/96
QCL P/F Version 9/91

& WA7'F r
Michael F.Easley,Governor
State of North Carolina
Q� William G.Ross,Jr.,Secretary
to . • Depatl fdf Environment andNtlit1rpl Resources
/ / ' /
AND N4, Q
O .,. ` ����, , . Alan afV;Er }`P��E�..,Director
// /J / Divi {�• TY{ 'r Quality
E 1
February 15, 2006
FEB 1 6 2006
Mr. Enrique Berman, Plant Manager
FMC Corporation, Lithium Division
Box 795
Bessemer City, North Carolina 28016 {WATER ,f "• ' -A _ 1
Subject: Draft NPDES Permit
Permit NC0005177
FMC Lithium Corporation
Gaston County
Dear Mr. Berman:
Enclosed with this letter is a copy of the draft permit for your facility. Please review
the draft carefully to ensure thorough understanding of the conditions and
requirements it contains. Changes to your existing permit are summarized below by
outfall.
Outfall 001
• The results of the priority pollutant analysis submitted by your facility detected the
presence of magnesium. The concentration reported was evaluated in the
reasonable potential analysis and was determined to exceed the allowable
concentration for protection of water quality (using EPA's national water quality
criteria). Based on this data, quarterly monitoring for magnesium is recommended
to be included in the permit.
• Deletion of quarterly monitoring for copper and zinc. A review of data indicated
that there was no reasonable potential for the parameters to exceed the water
quality action level standard.
Outfall 004
• The addition of quarterly monitoring for ethylbenzene and methyl chloride.
Information provided in the application indicated the potential discharge of these
constituents through this outfall. Quarterly monitoring is recommended so that an
evaluation of water quality can be done upon next permit renewal.
At this time, the Division is submitting a notice to the newspapers of general
circulation in Gaston County, inviting comments from you or your representative, the
public and other agencies on the draft permit. The notice should be published on or
about February 8, 2006. Following a 30-day comment period, we will review all
pertinent comments received and take appropriate action on the permit issuance.
1617 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1 61 7-TELEPHONE [phone]/FAX [phone]
VISIT US ON THE WEB AT http://h20.enr.5tate.nc.us/NPDES

Permit No. NC0005177
FMC Lithium
1g
Page 2
Please provide written comments on the draft permit no later than March 10,
2006. If you have any questions, please contact me at [phone], extension 512.
Si"erely,
i:
44.1/
Jafft
yn M. jrL
Weste
cc: NPDES File
valooresville Regional Office / Surface Water Protection Section
Aquatic Toxicology Unit
EPA Region IV/Attn. Marshall Hyatt

Permit NC0005177
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
DRAFT PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1,other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission,and the
Federal Water Pollution Control Act,as amended,
FMC Corporation
is hereby authorized to discharge wastewater and stormwater from a facility located at the
FMC Lithium Division
NC Highway 161 west of Bessemer City
Gaston County
to receiving waters designated as an unnamed tributary to Abernethy Creek in the Catawba River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II
III,and IV hereof.
The permit shall become effective xxxxxxxxxx.
This permit and the authorization to discharge shall expire at midnight on August 31, 2010.
Signed this day xxxxxxxxxxxxxxx.
Alan W. Klimek,P.E.,Director
Division of Water Quality
By Authority of the Environmental Management Commission

Part I Permit NC0005177
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility,whether for operation or discharge are hereby revoked,
and as of this issuance,any previously issued permit bearing this number is no longer effective. Therefore,
the exclusive authority to operate and discharge from this facility arises under the permit conditions,
requirements, terms, and provisions included herein.
FMC Corporation is hereby authorized to:
1. Continue operation of an existing 0.615 MGD wastewater treatment facility
consisting of:
• reverse osmosis filtration,
• hydrogen peroxide addition,
• pH adjustment systems, and
• the Lower pond
Facility is located at FMC Corporation's Lithium Division off NC Highway
161 west of Bessemer City in Gaston County;
2. Continue operation of a stormwater conveyance system and two sedimentation
and polishing ponds; and
3. Discharge treated wastewater (outfall 001) and stormwater, boiler blowdown,
and cooling water (004) at the locations specified on the attached map. The
receiving stream is an unnamed tributary to Abernethy Creek, a class C water
in the Catawba River Basin.

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FMC Lithium Division - NC0005177 Facility
•
Location
USGS Quad Name: Bessemer City Lat.: 34°49'53"
Receiving Stream: UT Abernethy Creek Long.: 78°49'23"
Stream Class: C Not to SCALE
Subbasin: Catawba - 030837 North

Part I Permit NC0005177
SECTION A: LIMITATIONS AND CONTROLS
(1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS [001]
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to discharge
treated industrial wastewater from Outfall 001. Such discharges shall be limited and monitored by the Permittee as
specified below:
EFFLUENT LIMITATIONS MONITORING REQUIREMENTS
PARAMETER
Monthly Average Daily Maximum Measurement Sample Type Sample Location
Frequency
Flow 0.615 MGD Continuous Recording Influent or Effluent
BOD5 30.0 mg/L 45.0 mg/L Monthly Grab Effluent
Total Suspended Solids 333.9 pounds/day 1001.7 pounds/day 2/Month Grab Effluent
Dissolved Oxygen Daily Average >_ 5.0 mg/L Weekly Grab Effluent
pH Between 6.0 and 9.0 Standard Units Weekly Grab Effluent
NH3-N Monthly Grab Effluent
Chloride Monthly Grab Effluent
Magnesium Quarterly Grab Effluent
Total Nitrogen Quarterly Grab Effluent
Total Phosphorus Quarterly Grab Effluent
Conductivity Monthly Grab Effluent
Chronic Toxicity' Quarterly Grab Effluent
Footnotes:
1 Chronic Toxicity (Ceriodaphnia) @ 78%,January,April,July,October;see section A. (3) of this permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.

rPart I Permit NC0005177
(2) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS [004]
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to discharge
stormwater, boiler blowdown, steam condensate and non-contact cooling water from Outfall 004. Such discharges
shall be limited and monitored by the Permittee as specified below:
EFFLUENT LIMITATIONS MONITORING REQUIREMENTS
PARAMETER
Monthly Average Daily Maximum Measurement Sample Type Sample Location
Frequency
Flow(MGD)1 Monthly Instantaneous Effluent
Total Suspended Solids Monthly Grab Effluent
pH Between 6.0 and 9.0 Standard Units Monthly Grab Effluent
Conductivity Monthly Grab Effluent
Chloride Monthly Grab Effluent
Ethylbenzene Quarterly Grab Effluent
Methyl Chloride Quarterly Grab Effluent
Footnotes:
1 Where no measurable discharge occurs, "no discharge" shall be clearly noted on the submitted monthly discharge
monitoring report (DMR).
> One set of samples per year shall be collected during a discharge resulting from a representative storm event.
A representative storm shall be any storm event that causes a discharge through outfall 004. Failure to
monitor storm events in accordance with the specified frequency shall constitute a violation of this permit.
For each representative storm event,the total precipitation, storm duration,and total flow shall be recorded.
> Total flow shall be: (a) measured continuously; (b) calculated based on the amount of area draining to the
outfall, the amount of built-upon (impervious) area, and the total amount of rainfall; or (c) estimated by the
measurement of flow at 20 minute intervals during the rain event. "Sample Collected During a Representative
Storm Event" shall be clearly marked on the DMR to indicate the samples were taken during a representative
storm event.
There shall be no chromium,zinc or copper added to the treatment system except as pre-approved
additives to biocidal compounds.
The permittee shall obtain approval from the Division's Aquatic Toxicology Unit prior to the use of any biocide (not
previously approved by the Division) in the effluent discharged under this permit. Approval for use of any biocide
not previously approved should be requested at least 90 days in advance of any planned usage.
Contact the Aquatic Toxicology Unit for detailed instructions on requesting approval of biocides:
NC DENR/DWQ/Aquatic Toxicology Unit
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.
SEE PART I,SECTION C FOR ADDITIONAL STORMWATER REQUIREMENTS.

Part I Permit NC0005177
(3) CHRONIC TOXICITY PERMIT LIMIT (Quarterly)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 78%.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised-February 1998) or subsequent
versions. The tests will be performed during the months of January,April,July, and October. Effluent sampling for
this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit limit,
then multiple-concentration testing shall be performed at a minimum, in each of the two following months as
described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised-February 1998) or
subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised-February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the
pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the
following address:
Attention: NC DENR/DWQ /Environmental Sciences Section
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no later than 30 days
after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity(AT) test form indicating the facility
name,permit number,pipe number, county,and the month/year of the report with the notation of"No Flow"in the
comment area of the form. The report shall be submitted to the Environmental Sciences Branch at the address cited
above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re-opened and modified to include
alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival,
minimum control organism reproduction,and appropriate environmental controls, shall constitute an invalid test and will require
immediate follow-up testing to be completed no later than the last day of the month following the month of the initial monitoring.

rrti
Permit NC0005177
SECTION B: Schedule of Compliance
1. The Permittee shall comply with final effluent limitations by the effective date of the permit.
2. The Permittee shall at all times provide the operation and maintenance necessary to operate the existing
facilities in accordance with Part II.C.2 of this permit.
SECTION C: FINAL Monitoring Requirements FOR STORMWATER DISCHARGES
During the period beginning on the effective date of the permit and lasting until expiration, the permittee is
authorized to discharge stormwater associated with industrial activity from outfall 004. Such discharges shall be
controlled,limited,and monitored as specified below.
1. Stormwater Pollution Prevention Plans
The permittee shall develop and continue to update a Stormwater Pollution Prevention Plan,herein after referred to
as the Plan. The Plan shall be considered public information in accordance with Part II,Section E. 10 of this permit.
The Plan shall include,at a minimum,the following items:
a. Site Plan: The site plan shall provide a description of the physical facility and the potential pollutant
sources which may be expected to contribute to contamination of regulated stormwater discharges.
The site plan shall contain the following:
(1) A general location map (USGS quadrangle map, or appropriately drafted equivalent map),
showing the facility's location in relation to transportation routes and surface waters,and the
name of the receiving water(s) to which the stormwater outfall(s) discharges. If the
discharge is to a municipal separate storm sewer system, the name of the municipality and
the ultimate receiving waters,and accurate latitude and longitude of the point(s) of discharge
must be shown.
(2) A narrative description of storage practices, loading and unloading activities, outdoor
process areas, dust or particulate generating or control processes, and waste disposal
practices.
(3) A site map (or series of maps) drawn to scale with the distance legend indicating location of
industrial activities (including storage of materials, disposal areas,process areas, and loading
and unloading areas), drainage structures, drainage areas for each outfall and activities
occurring in the drainage area, building locations and impervious surfaces, the percentage of
each drainage area that is impervious. For each outfall, a narrative description of the
potential pollutants which could be expected to be present in the regulated stormwater
discharge.
(4) A list of significant spills or leaks of pollutants that have occurred at the facility during the 3
previous years and any corrective actions taken to mitigate spill impacts.
(5) Certification that the stormwater outfalls have been evaluated for the presence of non-
stormwater discharges. The certification statement will be signed in accordance with the
requirements found in Part II,Section B. 11.
b. Stormwater Management Plan: The stormwater management plan shall contain a narrative
description of the materials management practices employed which control or minimize the
exposure of significant materials to stormwater, including structural and non-structural measures.
The stormwater management plan,at a minimum,shall incorporate the following:
(1) A study addressing the technical and economic feasibility of changing the methods of
operations and/or storage practices to eliminate or reduce exposure of materials and

Part I Permit NC0005177
processes to stormwater. Wherever practicable the permittee should consider covering
storage areas, material handling operations, manufacturing or fueling operations to prevent
materials exposure to stormwater. In areas where elimination of exposure is not practicable,
the stormwater management plan shall document the feasibility of diverting the stormwater
runoff away from areas of potential contamination.
(2) A schedule to provide secondary containment for bulk storage of liquid materials, storage of
Section 313 of Title III of the Superfund Amendments and Reauthorization Act (SARA)
water priority chemicals, or storage of hazardous materials to prevent leaks and spills from
contaminating stormwater runoff. If the secondary containment devices are connected
directly to stormwater conveyance systems, the connection shall be controlled by manually
activated valves or other similar devices [which shall be secured with a locking mechanism]
and any stormwater that accumulates in the containment area shall be at a minimum visually
observed prior to release of the accumulated stormwater. Accumulated stormwater shall be
released if found to be uncontaminated. Records documenting the individual making the
observation, the description of the accumulated stormwater and the date and time of the
release shall be kept for a period of five years.
(3) A narrative description of Best Management Practices (BMPs) to be considered such as,but
not limited to, oil and grease separation, debris control, vegetative filter strips, infiltration
and stormwater detention or retention,where necessary. The need for structural BMPs shall
be based on the assessment of potential of sources contributing significant quantities of
pollutants to stormwater discharges and data collected through monitoring of stormwater
discharges.
(4) Inspection schedules of stormwater conveyances and controls and measures to be taken to
limit or prevent erosion associated with the stormwater systems.
c. Spill Prevention and Response Plan: The Spill Prevention and Response Plan shall incorporate a risk
assessment of potential pollutant sources based on a materials inventory of the facility. Facility
personnel (or team) responsible for implementing the plan shall be identified in the plan. A
responsible person shall be on-site at all times during facility operations that have the potential to
contaminate stormwater runoff through spills or exposure of materials associated with the facility
operations.
d. Preventative Maintenance and Good Housekeeping Program: A preventative maintenance program
shall be developed. The program shall document schedules of inspections and maintenance activities
of stormwater control systems, plant equipment and systems. Inspection of material handling areas
and regular cleaning schedules of these areas shall be incorporated into the program.
e. Training schedules shall be developed and training provided at a minimum on an annual basis on
proper spill response and cleanup procedures and preventative maintenance activities for all
personnel involved in any of the facility's operations that have the potential to contaminate
stormwater runoff. Facility personnel (or team) responsible for implementing the training shall be
identified in the plan.
f. The Stormwater Pollution Prevention Plan shall identify a specific position(s) responsible for the
overall coordination, development,implementation, and revision to the Plan. Responsibilities for all
components of the Plan shall be documented and position(s) assignments provided.
g. Plan Amendment: The permittee shall amend the Plan whenever there is a change in design,
construction, operation, or maintenance which has a significant effect on the potential for the
discharge of pollutants via a point source to surface waters. The Stormwater Pollution Prevention
Plan shall be reviewed and updated on an annual basis.
The Director may notify the permittee when the Plan does not meet one or more of the minimum
requirements of the permit. Within 30 days of such notice, the permittee shall submit a time

I Part rPermit NC0005177
schedule to the Director for modifying the Plan to meet minimum requirements. The permittee
shall provide certification in writing(in accordance with Part II, Standard Conditions, Section B.11.)
to the Director that the changes have been made.
h. Facility Inspections: Inspections of the facility and all stormwater systems shall occur at a minimum
on a semiannual schedule, once in the fall (September - November) and once during the spring
(April - June). The inspection and any subsequent maintenance activities performed shall be
documented, recording date and time of inspection, individual(s) making the inspection and a
narrative description of the facility's stormwater control systems, plant equipment and systems.
Records of these inspections shall be incorporated into the Stormwater Pollution Prevention Plan.
Visual monitoring as required in Part II, Section A.2. shall be performed in addition to facility
inspections.
i. Implementation: Implementation of the Plan shall include documentation of all monitoring,
measurements, inspections, maintenance activities and training provided to employees,including the
log of the sampling data.Activities taken to implement BMPs associated with the industrial activities,
including vehicle maintenance activities,must also be recorded. All required documentation shall be
kept on-site for a period of five years and made available to the Director or his authorized
representative immediately upon request.
2. Visual Monitoring
Visual monitoring requires a qualitative visual inspection of each stormwater outfall, regardless of representative
outfall status, for the purpose of evaluating the effectiveness of the Stormwater Pollution Prevention Plan and
assessing new sources of stormwater pollution. No analytical tests are required. Visual monitoring of stormwater
outfalls does not need to be performed during a representative storm event.
Stormwater Discharge Characteristics Frequency' Monitoring Type2 Monitoring Location;
Color Semi-Annual Visual SDO
Odor Semi-Annual Observation SDO
Clarity Semi-Annual Visual SDO
Floating Solids Semi-Annual Visual SDO
Suspended Solids Semi-Annual Visual SDO
Foam Semi-Annual Visual SDO
Oil Sheen Semi-Annual Visual SDO
Other obvious indicators of stormwater Semi-Annual Visual SDO
NOTES:
1 The first visual monitoring event during the term of the permit must be performed during the initial analytical monitoring
event. All subsequent visual monitoring will be performed twice per year,once in the spring and once in the fall.
2 Monitoring requires a qualitative observation of each stormwater outfall. No analytical testing or sampling is required.
3 Stormwater Discharge Outfall(SDO).
SECTION D: STORMWATER DEFINITIONS
1. Best Management Practices (BMPs)
Schedules of activities,prohibitions of practices,maintenance procedures,and other management practices to
prevent or reduce the pollution of waters of the United States. BMPs also include treatment requirements,
operation procedures, and practices to control plant site runoff, spillage or leaks, sludge or waste disposal, or
drainage from raw material storage.

Part I Permit NC0005177
2. Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers having a total storage capacity of greater than 1,320 gallons.
3. Point Source Discharge
Any discernible, confined and discrete conveyance, including but specifically not limited to,any pipe, ditch,
channel, tunnel, conduit, well, discrete fissure, container, rolling stock, or concentrated animal feeding
operation from which pollutants are or may be discharged to waters of the state.
4. Runoff Coefficient
The fraction of total rainfall that is not infiltrated into or otherwise retained by the soil, concrete, asphalt or
other surface upon which it falls that will appear at the conveyance as runoff.
5. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25-year,24-hour storm event.
6. Section 313 Water Priority Chemical
A chemical or chemical category which:
a. Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right-to-
Know Act of 1986;
b. Is present at or above threshold levels at a facility subject to SARA title III, Section 313 reporting
requirements;and
c. That meet at least one of the following criteria:
(1) Is listed in appendix D of 40 CFR part 122 on either Table II (organic priority pollutants),Table III
(certain metals, cyanides, and phenols) or Table IV (certain toxic pollutants and hazardous
substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A)of the CWA at 40 CFR 116.4;or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
7. Significant Materials
Includes, but is not limited to: raw materials; fuels;materials such as solvents, detergents, and plastic pellets;
finished materials such as metallic products; raw materials used in food processing or production;hazardous
substances designated under section 101(14) of CERCLA; any chemical the facility is required to report
pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as ashes, slag
and sludge that have the potential to be released with stormwater discharges.
8. Significant Spills
Includes,but is not limited to: releases of oil or hazardous substances in excess of reportable quantities under
section 311 of the Clean Water Act (Ref: 40 CFR 110.10 and CFR 117.21) or section 102 of CERCLA (Ref:
40 CFR 302.4).
9. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall or as a
result of snowmelt.
10. Total Flow
The flow corresponding to the time period over which the sample collection occurs. The total flow
calculated based on the size of the area draining to the outfall, the amount of the built-upon (impervious)
surfaces within the drainage area,and the total amount of rainfall occurring during the sampling period.
11. Visible Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water,air,gravity,
or ice from its site of origin which can be seen with the unaided eye.

DENR/DWQ
FACT SHEET FOR NPDES PERMIT DEVELOPMENT
NPDES No. NC0005177
Facility Information
Applicant/Facility Name: FMC - Lithium Division
Applicant Address: Box 795 Bessemer City NC 28016
Facility Address: 1115 Bessemer City Kings Mountain Highway Bessemer City NC
Permitted Flow 0.615 MGD
Type of Waste: Industrial
Facility/Permit Status: Existing
County: Gaston
Miscellaneous
Receiving Stream:" UT Abernethy Regional Office: Mooresville
Creek
Stream Classification: C USGS Topo Quad: F13SE
303(d) Listed?: No Permit Writer: Jacquelyn M. Nowell
Subbasin: 03-08-37 Date: January 30, 2006
Drainage Area (mi2): 1.4
Summer 7Q10 (cfs) 0.27
Winter 7Q10 (cfs): 0.43 ,}
Average Flow(cfs): 1.7 -
IWC (%): 78
Primary SIC Code: 2819, 2869
SUMMARY
FMC Corp - Lithium Division is requesting renewal of existing NPDES Permit. The facility does
chemical manufacturing of various Lithium based compounds. Also does research and
development and laboratory analysis.
Plant has two outfalls 001 and 004. Outfall 001 discharges air scrubber wastewater, boiler
blowdown, a/c cooling water, compressor condensate, and combine plant wastewater. Outfall
004 is the stormwater outfall and discharges boiler blowdown, process condensate, and cooling
water.
Facility submitted additional information for the permit, noting the addition of contributing
flow to the wastestream discharged from 001. The additional flow is of comparable
characteristics to existing flow and will be approximately 35 GPM of Lithium Hydroxide Purge.
The additional flow began late in the 3rd quarter of 2005.
•
Application notes that ethylbenzene and methyl chloride would potentially be discharged from
the speciality organics chemical plant through Outfall 004. Will recommend quarterly
monitoring for these parameters at 004.
Existing limit for Outfall 001 are:
Flow= 0.615 MGD,
BOD5 = 30 mg/1,
TSS= 333.9 lbs/day
DO = 5.0 mg/1
PH = 6-9 SU
Monthly monitoring for NH3, Chloride and Conductivity.
Quarterly monitoring for copper, zinc, TN, TP, and chronic toxicity.
Existing limits for Outfall 004:
Monthly monitoring for flow, TSS, pH, Conductivity and Chloride
Conductivity averages over 800-1000 umho from Outfall 004.
F\IC C'i rp-f...irimnf Oirici,n i act Shea
NPI)ES Renewal
Page I

COMPLIANCE INFORMATION
Facility has been in compliance with all limits during this permit cycle. In 2004 and 2005,
facility did not discharge from 001 for 2-3 months mostly during June, July and August.
Average flow discharge at outfall 001 in 2005 - 0.355 MGD;
Average flow discharge at outfall 001 in 2004-0.379 MGD.
TOXICITY TESTING:
Existing: Chronic Quarterly Test @ 78% in January April Jul Oct.
Facility has passed all tests since September 2003. The last test failures were in July and
August 2003. Investigation of the failures showed that copper and zinc discharge levels were
not the cause of the toxicity problems. Problems were more than likely corrected since all
toxicity tests since that time have passed.
Recommendation: Renewal of existing Chronic tox test limit at 78%
INSTREAM MONITORING:
None required
REASONABLE POTENTIAL ANALYSIS
RPA was performed for copper and zinc data based on available data. Results indicated that
there was no reasonable potential for copper to exceed either the acute or the chronic allowable
concentration. For the zinc data, reasonable potential was shown although all the reported
values were below detection. The issue with zinc data is that lab used different detection levels
from month to month from <10 to <50, therefore the analysis showed RP. Since all values were
below detection, will recommend that quarterly monitoring for copper and zinc be dropped.
Data results from the priority pollutant analysis data submitted by FMC.
The following constituents were present in PPA data submitted by FMC. NC Water quality
standards for these constituents are applicable only to streams classified for WS (water supply
usage). The receiving stream for FMC is UT Abernethy Creek and is classified C. Therefore, the
standard is not applicable for this stream. No monitoring or limits will be recommended.
Manganese = 0.29 mg/1
Sulfates = 420 mg/l.
NC water quality standard applies to following reported data:
Fluoride = 0.670 mg/1, the allowable concentration is 5010 ug/1 (5.0 mg/1). No monitoring for
fluoride will be recommended.
Gross alpha = 4.8 pCi/1, the allowable per NC narrative WQ standard is "not greater than 15
pCi/1. No monitoring for Gross alpha will be recommended.
Gross beta = 11.5 pCi/l, the allowable per NC narrative WQ standard is "not greater than 50
pCi/1. No monitoring for Gross beta will be recommended.
NC action level standard applies to following reported data:
Iron = 0.058 mg/1, the allowable concentration is 2783 ug/1 (2.78 mg/1). No monitoring for iron
will be recommended.
No NC water quality standard, action level standard or federal criteria applies to the
following:
Bromide = 0.68 mg/1
Federal Criteria is applicable to the following reported data:
Magnesium= 51 mg/1; the allowable concentration is 556 ug/1. Recommend quarterly
monitoring for magnesium based on this data for full evaluation at next permit renewal.
PROPOSED CHANGES:
• Recommend that quarterly monitoring for copper and zinc be dropped.
• Recommend the addition of quarterly monitoring for ethylbenzene and methyl chloride
at outfall 004.
• Recommend quarterly monitoring for magnesium based on exceedance of allowable
concentration of federal criteria.
PROPOSED SCHEDULE FOR PERMIT ISSUANCE:
Draft Permit to Public Notice: February 1, 2006
J\1C coil) L.ir'rium i)iv icion Fact St;.a
PDI-S Kcnctti al
2`e:

Permit Scheduled to Issue: Est. March 27, 2006
STATE CONTACT:
If you have any questions on any of the above information or on the attached permit, please
contact Jai 'e Nowell at [phone] ext. 512.
NAME: ' ' , , DATE: /36/400cgo
REG O •AL •i /CE COMM NT:
NAME: DATE:
Fmc Corp- Lithium Div°i ion Fact Sheet
NPl.)ES Renewal
Pare

REASONABLE POTENTIAL ANALYSIS
FMC Lithium Corp. Outfall 1
NC0005177 Ow=0.615 MGD
Time Period 0
Ow(MOD) 0.615 WWTP Class 3
7010S(cfs) 0.27 /WC(%)®7010S 77.928
7010W(cis) 0.43 0 7010W 68.914
3002(cfs) 0.58 0 3002 62.172
Avg.Stream Flow,QA(cfs) 1.7 0 QA 35.928
Rec'ving Stream UT Abemethy Creek Stream Class C
STANDARDS&
PARAMETER TYPE CRITERIA(2) POL Units REASONABLE POTENTIAL RESULTS RECOMMENDED ACTION
(11 NCWDS/ KFAV/ n ID.t Ain Prod Cw Allowable Cw
Chronic Acut.
Acute: N/A
Arsenic NC 50 D< ug/L 0 0 N/A
Chronic: 64
Acute: N/A
Beryllium C 6.5 ug/L 0 0 N/A __—_—_—_—_—_—_— __—_-------_
Chronic: 10.5
_ — —
Acute: 15
Cadmium NC 2 15 ug/L 0 0 N/A
Chronic: 2.6----------Acute: 1,022
1,022
Chromium NC 50 1,022 ug/L 0 0 N/A _ _
-- --------- — ----------
Chronic: 64 --------- —
Acute: 7
Copper NC 7 AL 7.3 ugh. 12 0 5.0 __ _ All values below detection. No RP to exceed allowable
Chronic: 9.0 concentrations.
Acute: 22
Cyanide NC 5 N 22 10 ug/L 0 0 N/A
Chronic: 6.4
Acute: N/A
Fluoride NC 1,800 ug/L 1 1 N/A
Note:nc12 Chronic: 2,310 - - ---_—_- ---_-----_- - -----_—
Limited data set
Acute: 34
Lead NC 25 N 33.8 ug/L 0 0 N/A
—__
—___ _—___— -
Chronic: 32.1
J Acute: N/A
'
Mercury NC 0.012 F 0.0002 ug/L 0 0 N/A
Chronic: 0.0154
Acute: N/A
Molybdenum A 3,500 ug/L 0 0 N/A
Chronic: 9,741.804
Acute: 261
Nickel NC 88 261 ugh. 0 0 N/A
Chronic: 112.9 _--
Acute: N/A
Phenols A 1 N [ ug/L 0 0 N/A
Chronic: 2.8
Acute: 56
Selenium NC 5.0 56 ug/L. 0 0 N/A
Chronic: 6.4----------------------------------
Acute: 1
Silver NC 0.06 AL 1.23 ug/L 0 0 N/A
Chronic: 0.08
Acute: 67 Different detection levels used in the past 2.5 years.All vat
Zinc NC 50 AL 67 ug/L 12 0 80.0 below detection but dill.Levels showed max.pred.Above
Chronic: 64 chronic and acute allowables. Facility must use lowest
available detection level consistently.
•Legend: "Freshwater Discharge
C=Carcinogenic
NC=Non-carcinogenic
A=Aesthetic
5177rpa2006,rpa
1/31/2006

REASONABLE POTENTIAL ANALYSIS
5 15
Copper Zinc
Date Data BDL=1/2DL Results Date Data BDL=1/2DL Results
1 Oct-2005 10s 5.0 Std Dev. 0.0000 1 Oct 2005 30 15.0 Std Dev. 7.2169
2 Sep-2005 10 5.0 Mean 5.0000 2 Sep-2005 30 15.0 Mean 10.4167
3 Apr-2005 10 5.0 C.V. 0.0000 3 Apr-2005 30 15.0 C.V. 0.6928
4 Jan-2005 10 5.0 n 12 4 Jan-2005 40 20.0 n 12
5 Oct-2004 ` 10 5.0 5 Oct-2004 10 5.0
6 Sep-2004 10 5.0 Mult Factor= 1.0000 6 Sep-2004 50 25.0 Mult Factor= 3.2000
7 Apr-2004 10 5.0 Max.Value 5.0 ug/L 7 Apr-2004 10 5.0 Max.Value 25.0 ug/L
8 Jan-2004 10 5.0 Max.Pred Cw 5.0 ug/L 8 Jan-2004 10 5.0 Max.Pred Cw 80.0 ug/L
9 Oct-2003'; 10 5.0 9 Oct-2003 10 5.0
10 Jul-2003.',:` ,10 5.0 10 Jul-2003` 10 5.0
11 Apr-2003 I 10 5.0 11 'Apr-2003 10 5.0
12 Jan-2003 10 5.0 12 Jan-2003 10 5.0
13 13
14 14
15 15
16 16
17 17
18 18
19 19
20 20
21 21
22 22
23 23
24 " 24
25 25
26 26
27 27
28 28
29 29
30 30
5177rpa2006,data
-2- 1/31/2006

TOXICANT ANALYSIS
Facility Name FMC Lithium Parameter= Ethylbenzene Parameter= Meth Chloride Parameter= Fluoride Para,
NPDES#NC0005177 Standard= 5201pg/I Standard=I Ipgil Standard=I 1800Ipg/I Star
Ow(MGD) 0.615
7Q10s(cfs) 1.7 n BDL=1/2DL Actual Data RESULTS n3DL=1/2Dbtual Data RESULTS n3DL=1/2Dlctual Da RESULTS
/WC(%) 35.93 1 Std Dev. #DIV/0! 1 Std Dev. #DIV/0! 1 670 670 Std Dev. #DIV/01
Rec'ving Stream UT Abemethy Creek 2 Mean #DIV/0! 2 Mean #DIV/0! 2 Mean 670
Stream Class C 3 C.V. 0.6 3 C.V. #DIV/01 3 C.V. #DIV/01
4 4 4
FINAL RESULTS 5 5 5
Ethylbenzene 6 Mult Facto; 1.511 6 Mult Factor 13.81 6 Mutt Factor{ 11
Max.Pred Cw 0 ugh 7 Max.Value 0 pgA 7 Max.Value 0 pg/I 7 Max.Value 670 pg/I
Allowable Cw 1447.4 ugA 8 Max.Pred, 0 PO 8 Max.Pred C 0 pgA 8 Max.Pred t 670 pg/I
Max.Value 0 9 Allowable C 1447.35 pgA 9 Allowable C #VALUE! pg/I 9 Allowable C 5010.07 pgA
Methyl Chloride 10 10 10
Max.Pred Cw 0 ugh 11 11 11
Allowable Cw #VALUE! ugA 12 12 12
Max.Value 0 13 13 13
Fluoride 14 14 14
Max.Pred Cw 670 ugh 15 15 15
Allowable Cw 5,010.07 ugA 16 16 16
Max.Value 670 17 17 17
Iron 18 18 18
Max.Pred Cw 580 ugh 19 19 19
Allowable Cw 2783.4 ugh 20 20 20
Max.Value 580 21 21 21
Magnesium 22 22 22
Max.Pred Cw 51000 ugh 23 23 23
Allowable Cw 556.7 ugh 24 24 24
Max.Value 51000 25 25 25
1/31/2006

TOXICANT ANALYSIS
meter= Iron Parameter= Magnesium Paran
,Idard=I 1000IpgA Standard=I 2001{10 Stan
n BDL=1/2DLActual Data RESULTS n 3DL=1/2DActual Dat,RESULTS
1 580 580 Std Dev. #DIV/0I 1 51000 51000 Std Dev. #DIV/01
2 Mean 580 2 Mean 51000
3 C.V. #DIV/01 3 C.V. #DIV/01
4 4
5 5
6 Mutt Factor! 11 6 Mutt Facto4 11
7 Max.Value 580{rgA 7 Max.Value 51000 pg/I
8 Max.Pred( 580{rg/1 8 Max.Pred i 51000 pg/I
9 Allowable C 2783.37 pg/I 9 Allowable C 556.67 pg/I
10 10
11 11
12 12
13 13
14 14
15 15
16 16
17 17
18 18
19 19
20 20
21 21
22 22
23 23
24 24
25 25
1/31/2006

•
rif
Q W A 7- ,9 Michael F.Easley
O pG Governor
Uj William G.Ross,Jr.,Secretary
North Carolina Department of Environment and Natural Resources
p 'C Gregory J.Thorpe,Ph.D.,Acting Director
Division of Water Quality
DIVISION OF WATER QUALITY
October 15, 2003
Ms. Kimberly Weathers, Environmental Manager
FMC Corporation, Lithium Division
Highway 161, Box 795
Bessemer City NC 28016
Subject: NPDES Permit No.NC0005177
FMC Corp. Lithium Division
Gaston County,NC
Dear Ms Weathers:
Our records indicate that NPDES Permit No.NC0005177 was issued on October 6,2003 for
the discharge of wastewater to the surface waters of the State from your facility. The purpose of this
letter is to advise you of the importance of the Permit and the liabilities in the event of failure to
comply with the terms and conditions of the Permit. If you have not already done so, it is suggested
that you thoroughly read the Permit. Of particular importance is Pages 4 and 5 .
Pages 4 and 5 set forth the.effluent limitations and monitoring requirements for your
discharge. Your discharge must not exceed any of the limitations set forth. The section headed
"Monitoring Requirements" describes the measurement frequencies, sample types and sampling
locations. Upon commencement of your discharge (or operation), you must initiate the required
monitoring. The monitoring results must be entered on reporting forms furnished or approved by
this Agency. If you have not received these forms, they should be arriving shortly. If you fail to
receive the forms,please contact this Office as quickly as possible. I have enclosed a sample of the
"Effluent" reporting form (DWQ Form MR-1), plus instructions for completing the form. It is
imperative that all applicable parts be completed, and the original and one copy be submitted as
required.
Please be advised that an annual administering and compliance monitoring fee may be
required for your facility. You will soon be receiving a statement from our Raleigh Office. It is
imperative that the fee be paid in a timely manner so as to prevent enforcement action or possible
revocation of your permit.
The remaining parts of the Permit set forth definitions, general conditions and special
conditions applicable to the operation of wastewater treatment facilities and/or discharge(s). The
conditions include special reporting requirements in the event of noncompliance,bypasses,treatment
unit/process failures,etc. Also addressed are requirements for a certified wastewater treatment plant
d
Customer Service Mooresville Regional Office,919 North Main Street,Mooresville,NC 28115 PHONE [phone]
1 800 623-7748 FAX [phone]

Ms. Weathers
October 15, 2003
Page No. 2
operator if you are operating wastewater treatment facilities. Any changes in operation of
wastewater treatment facilities, quantity and type of wastewater being treated or discharged,
expansions and/or upgrading of wastewater treatment facilities must be permitted or approved by
this Agency.
Failure to comply with the terms and conditions of an NPDES Permit subjects the Permittee
to enforcement action pursuant to Section 143-215.6 of the North Carolina General Statutes. A civil
penalty of up to $25,000 per violation (and/or criminal penalties) may be assessed for such
violations. If you find at any time that you are unable to comply with the terms and conditions of
the Permit,you should contact this Office immediately. A Special Order by Consent(SOC)may be
necessary while pursuing action to obtain compliance.
As a final note, an NPDES Permit is normally issued for a five-year period. Permits are Q
automatically renewed. Renewal requests must be submitted to this Agency no later than 180 days
prior to expiration. Please make note of the expiration date of your Permit. This date is set forth on
Page 1 of the Permit. Also note that NPDES Permits are not automatically transferable. If you, as
the Permittee, cease to need this Permit,then you should request that the Division of Water Quality
rescind the Permit or request that DWQ reissue the Permit to another party, if necessary.
As mentioned previously,the purpose of this letter is to advise you of the importance of your
NPDES Permit. Please read the Permit and contact this Office at 704/663-1699 in Mooresville if
you have any questions or need clarification. We look forward to providing any assistance.
'ncerely,
( D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Enclosure
DRG:dee

�� °•AT ,[� ` \ ` Michael F.Easley,Governor
O� QG DER.GF Egviko •State gf North Carolina
AND NAT"`? 'M ss,Jr.,Secretary
.
. • - ( artrnent of Environment and Natural Resources
y )
Alan W.Klimek,P.E.,Director
Division of Water Quality
OCT 1 7nr,•{
October 6, 2003 J
Ms. Kimberly Weathers, Environmental Manager
FMC Corporation, Lithium Division
Highway 161, Box 795
Bessemer City, North Carolina 28016
Subject: NPDES Permit Issuance
Permit No. NC0005177
FMC Corp., Lithium Division
Gaston County
Dear Ms. Weathers:
Division personnel have reviewed and approved your application for renewal of the
subject permit. Accordingly, we are forwarding the attached NPDES discharge permit. This
permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1
and the Memorandum of Agreement between North Carolina and the U.S. Environmental
Protection Agency dated May 9, 1994 (or as subsequently amended).
The attached final permit contains those changes communicated to you in the draft
permit as well as corrections made in accordance with your comments dated September 15,
2003.
Compliance with all terms and conditions of the attached permit is the responsibility
of the Permittee. Please note that T15A 08G .0204 of the North Carolina Administrative Code
has been interpreted to mean that the Operator in Responsible Charge is responsible for
operation of water pollution control systems.
If any parts, measurement frequencies or sampling requirements contained in this
permit are unacceptable to you, you have the right to an adjudicatory hearing upon written
request within thirty (30) days following receipt of this letter. This request must be in the
form of a written petition, conforming to Chapter 150B of the North Carolina General
Statutes, and filed with the Office of Administrative Hearings (6714 Mail Service Center,
Raleigh, North Carolina 27699-6714). Unless such demand is made, this permit shall be final
and binding.
Please take notice that this permit is not transferable. This permit does not affect the
legal requirements to obtain other permits which may be required by the Division of Water
Quality or permits required by the Division of Land Resources, Coastal Area Management Act,
or any other Federal or Local governmental permits which may be required.
If you have any questions or need additional information, please do not hesitate to
contact Mark McIntire of my staff at [phone], extension 508.
Sincerely,
ORIGINAL SIGNED BY
Mark McIntire
Alan W. Klimek, P.E.
cc: Central Files
NPDES Unit Files
1rsflle Regional
Aquatic Toxicology Unit
Roosevelt Childress, EPA Region 4
1617 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1617-TELEPHONE [phone]/FAX [phone]
VISIT US ON THE WEB AT http://h20.enr.state.nc.us/NPDES

Permit NC0005177
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1,other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission,and the
Federal Water Pollution Control Act,as amended,
FMC Corporation
is hereby authorized to discharge wastewater and stormwater from a facility located at the
FMC Lithium Division
NC Highway 161 west of Bessemer City
Gaston County
to receiving waters designated as an unnamed tributary to Abernethy Creek in the Catawba River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II
III, and IV hereof.
The permit shall become effective November 1, 2003.
This permit and the authorization to discharge shall expire at midnight on August 31,2005.
Signed this day October 6, 2003.
ORIGINAL SIGNED BY
Mark McIntire
Alan W.Klimek,P.E.,Director
Division of Water Quality
By Authority of the Environmental Management Commission

Part I Permit NC000S177 • •
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility,whether for operation or discharge are hereby revoked,and as of this issuance,
any previously issued permit bearing this number is no longer effective.Therefore,the exclusive authority to operate and
discharge from this facility arises under the permit conditions,requirements,terms,and provisions included herein.
FMC Corporation is hereby authorized to:
1. Continue operation of an existing 0.615 MGD wastewater treatment facility
consisting of reverse osmosis filtration, and an R & D pond located at FMC's
Lithium Division off NC Highway 161 west of Bessemer City in Gaston
County;
2. Continue operation of a stormwater conveyance system and two sedimentation
and polishing ponds; and
3. Discharge treated wastewater (outfall 001) and stormwater, boiler blowdown,
and cooling water (004) at the locations specified on the attached map. The
receiving stream is an unnamed tributary to Abernethy Creek, a class C water
in the Catawba River Basin.
' f.i T;1FM

. , s.., , , ,, . ,4,N.- , - \. t,- ‘: ;','-,74,t. --_ _ *_ -ii I-ER,:crry ----41 '"0-,' '4' )
f j b' t 7`,r4 fi 'i j'
1 , tf 1 _i- , i b*i' t;ity,t�`alI . --.,a te Jal;` i o
Sys � � '' � ' .� '�� P � ��•
3 l ♦ i 1 ♦t ws.�{}
;3lP.,Z9'""+6. y� i¢� Y t ♦. Y �*�a��lli y w4Y .YyJ.',$
t J • • Pit,
'� s Y
�: , i 4GF tip y ,N..-a„
. t is 4, r
1F ._ t .t �t t Purr) p, * fi ••.,.
•
e 1 1 "k '
. l 6 . , 5 1 ,i(.1rc.�i t
•
, , ti,
Pond ' t.. Outfall 001 ., ,
1°
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J p }fJ t t t s
• 1 1 ' I � , �.
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•
�j f. �y a -,.',.., *�.i i t s �4
•
,.
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P
•
` Outfall004 ' ..,..
q_F # 't p 1
FMC Lithium Division - NC0005177 11 Facility
Location •
USGS Quad Name: Bessemer City Lat.: 35°15'44"
Receiving Stream: UT Abernethy Creek Long.: 81°17'57" $
Stream Class: C North Not to SCALE
Subbasin: Catawba - 030837

Part I Permit NC0005177 '
SECTION A: FINAL LIMITATIONS AND CONTROLS
(1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS [001]
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to discharge
treated industrial wastewater from Outfall 001. Such discharges shall be limited and monitored by the Permittee as
specified below:
EFFLUENT LIMITATIONS MONITORING REQUIREMENTS
PARAMETER
Monthly Average Daily Maximum Measurement Sample Type Sample Location
Frequency
Flow 0.615 MGD Continuous Recording Influent or Effluent
BOD5 30.0 mg/L 45.0 mg/L Monthly Grab Effluent
Total Suspended Solids 333.9 pounds/day 1001.7 pounds/day 2/Month Grab Effluent
Dissolved Oxygen Daily Average >_ 5.0 mg/L Weekly Grab Effluent
pH Between 6.0 and 9.0 Standard Units Weekly Grab Effluent
NH3-N Monthly Grab Effluent
Chloride Monthly Grab Effluent
Copper Quarterly Grab Effluent
Zinc Quarterly Grab Effluent
Total Nitrogen Quarterly Grab Effluent
Total Phosphorus Quarterly Grab Effluent
Conductivity Monthly Grab Effluent
Chronic Toxicityt Quarterly Grab Effluent
Footnotes:
t Chronic Toxicity(Ceriodaphnia) @ 78%,January,April,July,October;see section A. (3)of this permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.

Part I ' Permit NC0005177
(2) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS [004]
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to discharge
stormwater, boiler blowdown, steam condensate and non-contact cooling water from Outfall 004. Such discharges
shall be limited and monitored by the Permittee as specified below:
EFFLUENT LIMITATIONS MONITORING REQUIREMENTS
PARAMETER Measurement
Monthly Average Daily Maximum Sample Type Sample Location
Frequency
Flow(MGD)1 Monthly Instantaneous Effluent
Total Suspended Solids Monthly Grab Effluent
pH Between 6.0 and 9.0 Standard Units Monthly Grab Effluent
Conductivity Monthly Grab Effluent
Chloride Monthly Grab Effluent
Footnotes:
Where no measurable discharge occurs,"no discharge" shall be clearly noted on the submitted monthly discharge monitoring
report(DMR).
➢ One set of samples per year shall be collected during a discharge resulting from a representative storm event. A
representative storm shall be any storm event that causes a discharge through outfall 004. Failure to monitor storm
events in accordance with the specified frequency shall constitute a violation of this permit. For each representative
storm event,the total precipitation,storm duration,and total flow shall be recorded.
➢ Total flow shall be: (a) measured continuously; (b) calculated based on the amount of area draining to the outfall, the
amount of built-upon (impervious) area,and the total amount of rainfall;or(c) estimated by the measurement of flow at
20 minute intervals during the rain event. "Sample Collected During a Representative Storm Event" shall be clearly
marked on the DMR to indicate the samples were taken during a representative storm event.
There shall be no chromium,zinc or copper added to the treatment system except as pre-approved
additives to biocidal compounds.
The permittee shall obtain approval from the Division's Aquatic Toxicology Unit prior to the use of any biocide (not
previously approved by the Division) in the effluent discharged under this permit. Approval for use of any biocide
not previously approved should be requested at least 90 days in advance of any planned usage.
Contact the Aquatic Toxicology Unit for detailed instructions on requesting approval of biocides:
NC DENR/DWQ /Aquatic Toxicology Unit
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.
SEE PART I,SECTION C FOR ADDITIONAL STORMWATER REQUIREMENTS.

Part I Permit NC0005177
(3) CHRONIC TOXICITY PERMIT LIMIT (Quarterly)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 78%.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised-February 1998) or subsequent
versions. The tests will be performed during the months of January,April,July,and October. Effluent sampling for
this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit limit,
then multiple-concentration testing shall be performed at a minimum, in each of the two following months as
described in"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised-February 1998) or
subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised-February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the
pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the
following address:
Attention: NC DENR/ DWQ / Environmental Sciences Branch
1621 Mail Service Center
Raleigh,North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no later than 30 days
after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity(Al) test form indicating the facility
name,permit number,pipe number,county,and the month/year of the report with the notation of"No Flow"in the
comment area of the form. The report shall be submitted to the Environmental Sciences Branch at the address cited
above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re-opened and modified to include
alternate monitoring requirements or limits.
NOTE: Failure to achieve rest conditions as specified in the cited document, such as minimum control organism survival,
minimum control organism reproduction, and appropriate environmental controls, shall constitute an invalid test and will require
immediate follow-up testing to be completed no later than the last day of the month following the month of the initial monitoring.

Part I Permit NC0005177
SECTION B: Schedule of Compliance
1. The Permittee shall comply with final effluent limitations by the effective date of the permit.
2. The Permittee shall at all times provide the operation and maintenance necessary to operate the existing
facilities in accordance with Part II.C.2 of this permit.
SECTION C: FINAL Monitoring Requirements FOR STORMWATER DISCHARGES
During the period beginning on the effective date of the permit and lasting until expiration, the permittee is
authorized to discharge stormwater associated with industrial activity from outfall 004. Such discharges shall be
controlled,limited,and monitored as specified below.
1. Stormwater Pollution Prevention Plans
The permittee shall develop and continue to update a Stormwater Pollution Prevention Plan,herein after referred to
as the Plan. The Plan shall be considered public information in accordance with Part II,Section E. 10 of this permit.
The Plan shall include,at a minimum, the following items:
a. Site Plan: The site plan shall provide a description of the physical facility and the potential pollutant
sources which may be expected to contribute to contamination of regulated stormwater discharges.
The site plan shall contain the following:
(1) A general location map (USGS quadrangle map, or appropriately drafted equivalent map),
showing the facility's location in relation to transportation routes and surface waters,and the
name of the receiving water(s) to which the stormwater outfall(s) discharges. If the
discharge is to a municipal separate storm sewer system, the name of the municipality and
the ultimate receiving waters,and accurate latitude and longitude of the point(s) of discharge
must be shown.
(2) A narrative description of storage practices, loading and unloading activities, outdoor
process areas, dust or particulate generating or control processes, and waste disposal
practices.
(3) A site map (or series of maps) drawn to scale with the distance legend indicating location of
industrial activities (including storage of materials, disposal areas, process areas, and loading
and unloading areas), drainage structures, drainage areas for each outfall and activities
occurring in the drainage area,building locations and impervious surfaces, the percentage of
each drainage area that is impervious. For each outfall, a narrative description of the
potential pollutants which could be expected to be present in the regulated stormwater
discharge.
(4) A list of significant spills or leaks of pollutants that have occurred at the facility during the 3
previous years and any corrective actions taken to mitigate spill impacts.
(5) Certification that the stormwater outfalls have been evaluated for the presence of non-
stormwater discharges. The certification statement will be signed in accordance with the
requirements found in Part II,Section B. 11.
b. Stormwater Management Plan: The stormwater management plan shall contain a narrative
description of the materials management practices employed which control or minimize the
exposure of significant materials to stormwater, including structural and non-structural measures.
The stormwater management plan, at a minimum, shall incorporate the following:
(1) A study addressing the technical and economic feasibility of changing the methods of
operations and/or storage practices to eliminate or reduce exposure of materials and

Part I Permit NC0005177
processes to stormwater. Wherever practicable the permittee should consider covering
storage areas, material handling operations, manufacturing or fueling operations to prevent
materials exposure to stormwater. In areas where elimination of exposure is not practicable,
the stormwater management plan shall document the feasibility of diverting the stormwater
runoff away from areas of potential contamination.
(2) A schedule to provide secondary containment for bulk storage of liquid materials,storage of
Section 313 of Title III of the Superfund Amendments and Reauthorization Act (SARA)
water priority chemicals, or storage of hazardous materials to prevent leaks and spills from
contaminating stormwater runoff. If the secondary containment devices are connected
directly to stormwater conveyance systems, the connection shall be controlled by manually
activated valves or other similar devices [which shall be secured with a locking mechanism]
and any stormwater that accumulates in the containment area shall be at a minimum visually
observed prior to release of the accumulated stormwater. Accumulated stormwater shall be
released if found to be uncontaminated. Records documenting the individual making the
observation, the description of the accumulated stormwater and the date and time of the
release shall be kept for a period of five years.
(3) A narrative description of Best Management Practices (BMPs) to be considered such as, but
not limited to, oil and grease separation, debris control, vegetative filter strips, infiltration
and stormwater detention or retention,where necessary. The need for structural BMPs shall
be based on the assessment of potential of sources contributing significant quantities of
pollutants to stormwater discharges and data collected through monitoring of stormwater
discharges.
(4) Inspection schedules of stormwater conveyances and controls and measures to be taken to
limit or prevent erosion associated with the stormwater systems.
c. Spill Prevention and Response Plan: The Spill Prevention and Response Plan shall incorporate a risk
assessment of potential pollutant sources based on a materials inventory of the facility. Facility
personnel (or team) responsible for implementing the plan shall be identified in the plan. A
responsible person shall be on-site at all times during facility operations that have the potential to
contaminate stormwater runoff through spills or exposure of materials associated with the facility
operations.
d. Preventative Maintenance and Good Housekeeping Program: A preventative maintenance program
shall be developed. The program shall document schedules of inspections and maintenance activities
of stormwater control systems, plant equipment and systems. Inspection of material handling areas
and regular cleaning schedules of these areas shall be incorporated into the program.
e. Training schedules shall be developed and training provided at a minimum on an annual basis on
proper spill response and cleanup procedures and preventative maintenance activities for all
personnel involved in any of the facility's operations that have the potential to contaminate
stormwater runoff. Facility personnel (or team) responsible for implementing the training shall be
identified in the plan.
f. The Stormwater Pollution Prevention Plan shall identify a specific position(s) responsible for the
overall coordination, development,implementation, and revision to the Plan. Responsibilities for all
components of the Plan shall be documented and position(s) assignments provided.
g. Plan Amendment: The permittee shall amend the Plan whenever there is a change in design,
construction, operation, or maintenance which has a significant effect on the potential for the
discharge of pollutants via a point source to surface waters. The Stormwater Pollution Prevention
Plan shall be reviewed and updated on an annual basis.
The Director may notify the permittee when the Plan does not meet one or more of the minimum
requirements of the permit. Within 30 days of such notice, the permittee shall submit a time

Part I Permit NC0005177
schedule to the Director for modifying the Plan to meet minimum requirements. The permittee
shall provide certification in writing (in accordance with Part II, Standard Conditions,Section B.11.)
to the Director that the changes have been made.
h. Facility Inspections: Inspections of the facility and all stormwater systems shall occur at a minimum
on a semiannual schedule, once in the fall (September - November) and once during the spring
(April - June). The inspection and any subsequent maintenance activities performed shall be
documented, recording date and time of inspection, individual(s) making the inspection and a
narrative description of the facility's stormwater control systems, plant equipment and systems.
Records of these inspections shall be incorporated into the Stormwater Pollution Prevention Plan.
Visual monitoring as required in Part II, Section A.2. shall be performed in addition to facility
inspections.
i. Implementation: Implementation of the Plan shall include documentation of all monitoring,
measurements,inspections,maintenance activities and training provided to employees,including the
log of the sampling data.Activities taken to implement BMPs associated with the industrial activities,
including vehicle maintenance activities, must also be recorded. All required documentation shall be
kept on-site for a period of five years and made available to the Director or his authorized
representative immediately upon request.
2. Visual Monitoring
Visual monitoring requires a qualitative visual inspection of each stormwater outfall, regardless of representative
outfall status, for the purpose of evaluating the effectiveness of the Stormwater Pollution Prevention Plan and
assessing new sources of stormwater pollution. No analytical tests are required. Visual monitoring of stormwater
outfalls does not need to be performed during a representative storm event.
Stormwater Discharge Characteristics Frequency) Monitoring Type Monitoring Location3
Color Semi-Annual Visual SDO
Odor Semi-Annual Observation SDO
Clarity Semi-Annual Visual SDO
Floating Solids Semi-Annual Visual SDO
Suspended Solids Semi-Annual Visual SDO
Foam Semi-Annual Visual SDO
Oil Sheen Semi-Annual Visual SDO
Other obvious indicators of stormwater Semi-Annual Visual SDO
NOTES:
1 The first visual monitoring event during the term of the permit must be performed during the initial analytical monitoring
event. All subsequent visual monitoring will be performed twice per year,once in the spring and once in the fall.
2 Monitoring requires a qualitative observation of each stormwater outfall. No analytical testing or sampling is required.
3 Stormwater Discharge Outfall (SDO).
SECTION D: STORMWATER DEFINITIONS
1. Best Management Practices (BMPs)
Schedules of activities,prohibitions of practices, maintenance procedures,and other management practices to
prevent or reduce the pollution of waters of the United States. BMPs also include treatment requirements,
operation procedures, and practices to control plant site runoff, spillage or leaks, sludge or waste disposal, or
drainage from raw material storage.

Part I Permit NC0005177 •
2. Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers having a total storage capacity of greater than 1,320 gallons.
3. Point Source Discharge
Any discernible, confined and discrete conveyance, including but specifically not limited to, any pipe, ditch,
channel, tunnel, conduit, well, discrete fissure, container, rolling stock, or concentrated animal feeding
operation from which pollutants are or may be discharged to waters of the state.
4. Runoff Coefficient
The fraction of total rainfall that is not infiltrated into or otherwise retained by the soil,concrete, asphalt or
other surface upon which it falls that will appear at the conveyance as runoff.
5. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25-year,24-hour storm event.
6. Section 313 Water Priority Chemical
A chemical or chemical category which:
a. Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right-to-
Know Act of 1986;
b. Is present at or above threshold levels at a facility subject to SARA title III, Section 313 reporting
requirements;and
c. That meet at least one of the following criteria:
(1) Is listed in appendix D of 40 CFR part 122 on either Table II (organic priority pollutants),Table III
(certain metals, cyanides, and phenols) or Table IV (certain toxic pollutants and hazardous
substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A)of the CWA at 40 CFR 116.4;or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
7. Significant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents,detergents, and plastic pellets;
finished materials such as metallic products; raw materials used in food processing or production;hazardous
substances designated under section 101(14) of CERCLA; any chemical the facility is required to report
pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as ashes, slag
and sludge that have the potential to be released with stormwater discharges.
8. Significant Spills
Includes,but is not limited to: releases of oil or hazardous substances in excess of reportable quantities under
section 311 of the Clean Water Act (Ref: 40 CFR 110.10 and CFR 117.21) or section 102 of CERCLA (Ref:
40 CFR 302.4).
9. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall or as a
result of snowmelt.
10. Total Flow
The flow corresponding to the time period over which the sample collection occurs. The total flow
calculated based on the size of the area draining to the outfall, the amount of the built-upon (impervious)
surfaces within the drainage area, and the total amount of rainfall occurring during the sampling period.
I I. Visible Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water, air,gravity,
or ice from its site of origin which can be seen with the unaided eye.

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PART II
STANDARD CONDITIONS FOR NPDES PERMITS
Section A. Definitions
2/Month
Samples are collected twice per month with at least ten calendar days between sampling events.
3/Week
Samples are collected three times per week on three separate calendar days.
Act or"the Act"
The Federal Water Pollution Control Act,also known as the Clean Water Act,as amended,33 USC 1251, et. seq.
Annual Average •
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar year. In the case of fecal
coliform,the geometric mean of such discharges.
Arithmetic Mean
The summation of the individual values divided by the number of individual values.
Bypass
The known diversion of waste streams from any portion of a treatment facility including the collection system,which
is not a designed or established or operating mode for the facility.
Calendar Day
The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any
consecutive 24-hour period that reasonably represents the calendar day may be used for sampling.
Calendar Quarter
One of the following distinct periods: January through March, April through June, July through September, and
October through December.
Composite Sample
A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 ml in
such a manner as to result in a total sample representative of the wastewater discharge during the sample period. The
Director may designate the most appropriate method (specific number and size of aliquots necessary, the time
interval between grab samples, etc.) on a case-by-case basis. Samples may be collected manually or automatically.
Composite samples may be obtained by the following methods:
(1) Continuous: a single, continuous sample collected over a 24-hour period proportional to the rate of flow.
(2) Constant time/variable volume: a series of grab samples collected at equal time intervals over a 24 hour
period of discharge and combined proportional to the rate of flow measured at the time of individual sample
collection,or
(3) Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period
with the time intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow recorder and
totalizer, and the preset gallon interval between sample collection fixed at no greater than 1/24 of the
expected total daily flow at the treatment system,or
(4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period at
a constant time interval. This method may only be used in situations where effluent flow rates vary
less than 15 percent. The grab samples shall be taken at intervals of no greater than 20 minutes apart
during any 24-hour period and must be of equal size and of no less than 100 milliliters. Use of this method
requires prior approval by the Director.
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In accordance with (4) above,influent grab samples shall not be collected more than once per hour.
Effluent grab samples shall not be collected more than once per hour except at wastewater treatment systems
having a detention time of greater than 24 hours. In such cases, effluent grab samples may be collected at
intervals evenly spaced over the 24-hour period that are equal in number of hours to the detention time of the
system in number of days. However, the interval between effluent grab samples may not exceed six hours nor
the number of samples less than four during a 24-hour sampling period.
Continuous flow measurement
Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance
activities on the flow device.
Daily Discharge
The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the
calendar day for purposes of sampling. For pollutants measured in units of mass, the "daily discharge" is calculated as
the total mass of the pollutant discharged over the day. The "daily discharge" concentration comprises the mean
concentration for a 24-hour sampling period as either a composite sample concentration or the arithmetic mean of all
grab samples collected during that period. (40 CFR 122.3)
Daily Maximum
The highest"daily discharge"during the calendar month.
Daily Sampling
Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the
permit. The Division expects that sampling shall be conducted on weekdays except where holidays or other
disruptions of normal operations prevent weekday sampling. If sampling is required for all seven days of the week
for any permit parameter(s), that requirement will be so noted on the Effluent Limitations and Monitoring Page(s).
DWQ or"the Division"
The Division of Water Quality, Department of Environment and Natural Resources.
EMC
The North Carolina Environmental Management Commission.
Facility Closure
The cessation of wastewater treatment at a permitted facility,or the cessation of all activities that require coverage
under the NPDES. Completion of facility closure will allow this permit to be rescinded.
Geometric Mean
The Nth root of the product of the individual values where N = the number of individual values. For purposes of
calculating the geometric mean,values of"0" (or"< [detection level]") shall be considered =1.
Grab Sample
Individual samples of at least 100 ml collected over a period of time not exceeding 15 minutes. Grab samples can be
collected manually. Grab samples must be representative of the discharge (or the receiving stream, for instream
samples).
Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
Instantaneous flow measurement
A measure of flow taken at the time of sampling, when both the sample and flow will be representative of the total
discharge.
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Monthly Average (concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar month. In the case of fecal
coliform, the geometric mean of such discharges.
Permit Issuing Authority
The Director of the Division of Water Quality.
Quarterly Average (concentration limit)
The average of all samples taken over a calendar quarter.
Severe property damage
Substantial physical damage to property, damage to the treatment facilities which causes them to become inoperable,
or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage excludes economic loss caused by delays in production.
Toxic Pollutant:
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
Upset
An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance with
permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance caused by
operational error, improperly designed treatment facilities, inadequate treatment facilities, lack of preventive
maintenance,or careless or improper operation.
Weekly Average (concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar week. In the case of fecal
coliform, the geometric mean of such discharges.
Section B. General Conditions
1. Duty to Comply
The Permittee must comply with all conditions of this permit. Any permit noncompliance constitutes a violation
of the Clean Water Act and is grounds for enforcement action; for permit termination,revocation and reissuance,
or modification;or denial of a permit renewal application [40 CFR 122.41].
a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants and with standards for sewage sludge use or disposal established under
section 405(d) of the Clean Water Act within the time provided in the regulations that establish these
standards or prohibitions or standards for sewage sludge use or disposal, even if the permit has not yet been
modified to incorporate the requirement.
b. The Clean Water Act provides that any person who violates section 301,302,306,307, 308,318 or 405 of the
Act, or any permit condition or limitation implementing any such sections in a permit issued under section
402, or any requirement imposed in a pretreatment program approved under sections 402(a)(3) or 402(b)(8)
of the Act,is subject to a civil penalty not to exceed $25,000 per day for each violation. [40 CFR 122.41 (a)
(2)]
c. The Clean Water Act provides that any person who negligently violates sections 301,302, 306,307,308, 318, or
405 of the Act, or any condition or limitation implementing any of such sections in a permit issued under
section 402 of the Act, or any requirement imposed in a pretreatment program approved under section
402(a)(3) or 402(b)(8) of the Act,is subject to criminal penalties of$2,500 to $25,000 per day of violation, or
imprisonment of not more than 1 year, or both. In the case of a second or subsequent conviction for a
negligent violation, a person shall be subject to criminal penalties of not more than $50,000 per day of
violation,or by imprisonment of not more than 2 years,or both. [40 CFR 122.41 (a) (2)]
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d. Any person who knowing violates such sections, or such conditions or limitations is subject to criminal
penalties of$5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. In
the case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal
penalties of not more than $100,000 per day of violation,or imprisonment of not more than 6 years, or both.
[40 CFR 122.41 (a) (2)]
e. Any person who knowingly violates section 301,302,303,306,307,308,318 or 405 of the Act,or any permit
condition or limitation implementing any of such sections in a permit issued under section 402 of the Act,
and who knows at that time that he thereby places another person in imminent danger of death or serious
bodily injury, shall, upon conviction, be subject to a fine of not more than $250,000 or imprisonment of not
more than 15 years, or both. In the case of a second or subsequent conviction for a knowing endangerment
violation,a person shall be subject to a fine of not more than $500,000 or by imprisonment of not more than
30 years, or both. An organization,as defined in section 309(c)(3)(B)(iii) of the CWA, shall, upon conviction
of violating the imminent danger provision,be subject to a fine of not more than$1,000,000 and can be fined
up to$2,000,000 for second or subsequent convictions. [40 CFR 122.41 (a) (2)]
£ Under state law, a civil penalty of not more than $25,000 per violation may be assessed against any person
who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North
Carolina General Statutes § 143-215.6A]
g. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302,
306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such
sections in a permit issued under section 402 of this Act. Administrative penalties for Class 1 violations are
not to exceed$10,000 per violation,with the maximum amount of any Class I penalty assessed not to exceed
$25,000. Penalties for Class II violations are not to exceed $10,000 per day for each•day during which the
violation continues, with the maximum amount of any Class II penalty not to exceed $125,000. [40 CFR
122.41 (a) (3)]
•
2. Duty to Mitigate
The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in
violation of this permit which has a reasonable likelihood of adversely affecting human health or the environment
[40 CFR 122.41 (d)].
3. Civil and Criminal Liability
Except as provided in permit conditions on "Bypassing" (Part II. C. 4), "Upsets" (Part II. C. 5) and "Power
Failures" (Part II. C. 7), nothing in this permit shall be construed to relieve the Permittee from any
responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309
of the Federal Act, 33 USC 1319. Furthermore, the Permittee is responsible for consequential damages, such as
fish kills,even though the responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee
from any responsibilities, liabilities, or penalties to which the Permittee is or may be subject to under NCGS 143-
215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Property Rights
The issuance of this permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor
any infringement of Federal,State or local laws or regulations [40 CFR 122.41 (g)].
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical structures or
facilities or the undertaking of any work in any navigable waters.
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7. Severability
The provisions of this permit are severable. If any provision of this permit, or the application of any provision of thi:
permit to any circumstances,is held invalid, the application of such provision to other circumstances, and the remainder
of this permit, shall not be affected thereby [NCGS 150B-23].
8. Duty to Provide Information
The Permittee shall furnish to the Permit Issuing Authority,within a reasonable time,any information which the
Permit Issuing Authority may request to determine whether cause exists for modifying,revoking and reissuing,or
terminating this permit or to determine compliance with this permit. The Permittee shall also furnish to the
Permit Issuing Authority upon request,copies of records required by this permit [40 CFR 122.41 (h)].
9. Duty to Reapply
If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit,the
Permittee must apply for and obtain a new permit [40 CFR 122.41 (b)].
10. Expiration of Permit
The Permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the Permittee shall submit such information, forms, and
fees as are required by the agency authorized to issue permits no later than 180 days prior to the expiration date.
Any Permittee that has not requested renewal at least 180 days prior to expiration, or any Permittee that does not
have a permit after the expiration and has not requested renewal at least 180 days prior to expiration,will subject
the Permittee to enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and certified
[40 CFR 122.41 (k)].
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible
corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in
charge of a principal business function, or any other person who performs similar policy or decision
making functions for the corporation, or (b) the manager of one or more manufacturing,production, or
operating facilities,provided,the manager is authorized to make management decisions which govern the
operation of the regulated facility including having the explicit or implicit duty of making major capital
investment recommendations, and initiating and directing other comprehensive measures to assure long
term environmental compliance with environmental laws and regulations; the manager can ensure that
the necessary systems are established or actions taken to gather complete and accurate information for
permit application requirements; and where authority to sign documents has been assigned or delegated
to the manager in accordance with corporate procedures .
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,respectively;or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or
ranking elected official [40 CFR 122.22].
b. All reports required by the permit and other information requested by the Permit Issuing Authority shall be
signed by a person described in paragraph a. above or by a duly authorized representative of that person. A
person is a duly authorized representative only if:
1. The authorization is made in writing by a person described above;
2. The authorization specified either an individual or a position having responsibility for the overall
operation of the regulated facility or activity, such as the position of plant manager, operator of a well or
well field, superintendent, a position of equivalent responsibility, or an individual or position having
overall responsibility for environmental matters for the company. (A duly authorized representative may
thus be either a named individual or any individual occupying a named position.);and
3. The written authorization is submitted to the Permit Issuing Authority [40 CFR 122.22]
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c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate
because a different individual or position has responsibility for the overall operation of the facility, a new
authorization satisfying the requirements of paragraph (b) of this section must be submitted to the Director
prior to or together with any reports, information, or applications to be signed by an authorized
representative [40 CFR 122.22]
d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the
following certification [40 CFR 122.22]:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the
Permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned
changes or anticipated noncompliance does not stay any permit condition [40 CFR 122.41 (f)].
13. Permit Modification.Revocation and Reissuance.or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the
permit,revoking and reissuing the permit, or terminating the permit as allowed by the laws, rules,and regulations
contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina
Administrative Code,Subchapter 2H.0100;and North Carolina General Statute 143-215.1 et. al.
14. Annual Administering and Compliance Monitoring Fee Requirements
The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being
billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 2H.0105 (b) (4)
may cause this Division to initiate action to revoke the permit.
Section C. Operation and Maintenance of Pollution Controls
1. Certified Operator
Upon classification of the permitted facility by the Certification Commission, the Permittee shall employ a
certified water pollution control treatment system operator in responsible charge (ORC) of the water pollution
control treatment system. Such operator must hold a certification of the grade equivalent to or greater than the
classification assigned to the water pollution control treatment system by the Certification Commission. The
Permittee must also employ one or more certified Back-up ORCs who possess a currently valid certificate of the
type of the system. Back-up ORCs must possess a grade equal to (or no more than one grade less than) the grade
of the system [15A NCAC 8G.0201].
The ORC of each Class I facility must:
> Visit the facility at least weekly
> Comply with all other conditions of 15A NCAC 8G.0204.
The ORC of each Class II, III and IV facility must:
> Visit the facility at least daily,excluding weekends and holidays
> Properly manage and document daily operation and maintenance of the facility
> Comply with all other conditions of 15A NCAC 8G.0204.
Once the facility is classified, the Permittee shall submit a letter to the Certification Commission designating the
operator in responsible charge:
a. Within 60 calendar days prior to wastewater being introduced into a new system
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b. Within 120 calendar days of:
➢ Receiving notification of a change in the classification of the system requiring the designation of a
new ORC and back-up ORC
➢ A vacancy in the position of ORC or back-up ORC.
2. Proper Operation,and Maintenance
The Permittee shall at all times provide the operation and maintenance resources necessary to operate the existing
facilities at optimum efficiency. The Permittee shall at all times properly operate and maintain all facilities and
systems of treatment and control (and related appurtenances) which are installed or used by the Permittee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the Permittee to install
and operate backup or auxiliary facilities only when necessary to achieve compliance with the conditions of the
permit [40 CFR 122.41 (e)].
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a Permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this permit [40 CFR 122.41
(c)].
4. Bypassing of Treatment Facilities
a. Bypass not exceeding limitations [40 CFR 122.41 (m) (2)]
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but
only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject to the
provisions of Paragraphs b. and c. of this section.
b. Notice [40 CFR 122.41 (m) (3)]
(1) Anticipated bypass. If the Permittee knows in advance of the need for a bypass, it shall submit prior
notice, if possible at least ten days before the date of the bypass; including an evaluation of the
anticipated quality and effect of the bypass.
(2) Unanticipated bypass. The Permittee shall submit notice of an unanticipated bypass as required in Part
II. E. 6. (24-hour notice).
c. Prohibition of Bypass
(1) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for bypass,unless:
(A) Bypass was unavoidable to prevent loss of life,personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment facilities,
retention of untreated wastes or maintenance during normal periods of equipment downtime. This
condition is not satisfied if adequate backup equipment should have been installed in the exercise of
reasonable engineering judgment to prevent a bypass which occurred during normal periods of
equipment downtime or preventive maintenance;and
(C) The Permittee submitted notices as required under Paragraph b. of this section.
(2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for a bypass as provided in any current or future system-wide collection system
permit associated with the treatment facility.
(3) The Permit Issuing Authority may approve an anticipated bypass, after considering its adverse effects,if
the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph c.
(1) of this section.
5. Upsets
a. Effect of an upset [40 CFR 122.41 (n) (2)]: An upset constitutes an affirmative defense to an action
brought for noncompliance with such technology based permit effluent limitations if the requirements of
paragraph b. of this condition are met. No determination made during administrative review of claims that
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noncompliance was caused by upset, and before an action for noncompliance, is final administrative action
subject to judicial review.
b. Conditions necessary for a demonstration of upset: A Permittee who wishes to establish the
affirmative defense of upset shall demonstrate, through properly signed, contemporaneous operating logs, or
other relevant evidence that:
(1) An upset occurred and that the Permittee can identify the cause(s) of the upset;
(2) The Permittee facility was at the time being properly operated;and
(3) The Permittee submitted notice of the upset as required in Part II. E. 6. (b) (B) of this permit.
(4) The Permittee complied with any remedial measures required under Part II. B. 2. of this permit.
d. Burden of proof[40 CFR 122.41 (n) (4)]: The Permittee seeking to establish the occurrence of an
upset has the burden of proof in any enforcement proceeding.
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters
shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant
from such materials from entering waters of the State or navigable waters of the United States. The Permittee
shall comply with all existing Federal regulations governing the disposal of sewage sludge. Upon promulgation of
40 CFR Part 503, any permit issued by the Permit Issuing Authority for the utilization/disposal of sludge may be
reopened and modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR 503. The
Permittee shall comply with applicable 40 CFR 503 Standards for the Use and Disposal of Sewage Sludge (when
promulgated) within the time provided in the regulation, even if the permit is not modified to incorporate the
requirement. The Permittee shall notify the Permit Issuing Authority of any significant change in its sludge use
or disposal practices.
7. Power Failures
The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 2H.0124 —
Reliability) to prevent the discharge of untreated or inadequately treated wastes during electrical power failures
either by means of alternate power sources, standby generators or retention of inadequately treated effluent.
Section D. Monitoring and Records
1. Representative Sampling
Samples collected and measurements taken,as required herein,shall be characteristic of the volume and nature of
the permitted discharge. Samples collected at a frequency less than daily shall be taken on a day and time that is
characteristic of the discharge over the entire period the sample represents. All samples shall be taken at the
monitoring points specified in this permit and, unless otherwise specified, before the effluent joins or is diluted
by any other wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to and the approval of the Permit Issuing Authority [40 CFR 122.41 (j)].
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each month and reported on a
monthly Discharge Monitoring Report (DMR) Form (MR 1, 1.1, 2, 3) or alternative forms approved by the
Director,postmarked no later than the 28th day following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of
these,and all other reports required herein,shall be submitted to the following address:
NC DENR/ Division of Water Quality/Water Quality Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
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3. Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected
and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. The
devices shall be installed, calibrated and maintained to ensure that the accuracy of the measurements is consistent
with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a
maximum deviation of less than 10% from the true discharge rates throughout the range of expected discharge
volumes. Flow measurement devices shall be accurately calibrated at a minimum of once per year and maintained
to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device.
The Director shall approve the flow measurement device and monitoring location prior to installation.
Once-through condenser cooling water flow monitored by pump logs,or pump hour meters as specified in Part I
of this permit and based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations (published pursuant to
NCGS 143-215.63 et. seq.), the Water and Air Quality Reporting Acts, and to regulations published pursuant to
Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act (as Amended), and 40 CFR 136; or in
the case of sludge use or disposal,approved under 40 CFR 136,unless otherwise specified in 40 CFR 503,unless
other test procedures have been specified in this permit [40 CFR 122.41]. •
To meet the intent of the monitoring required by this permit, all test procedures must produce minimum
detection and reporting levels that are below the permit discharge requirements and all data generated must be
reported down to the minimum detection or lower reporting level of the procedure. If no approved methods are
determined capable of achieving minimum detection and reporting levels below permit discharge requirements,
then the most sensitive (method with the lowest possible detection and reporting level) approved method must
be used.
5. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any
monitoring device or method required to be maintained under this permit shall,upon conviction,be punished by
a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or
by both. If a conviction of a person is for a violation committed after a first conviction of such person under this
paragraph, punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not more
than 4 years,or both [40 CFR 122.41].
6. Records Retention
Except for records of monitoring information required by this permit related to the Permittee's sewage sludge
use and disposal activities, which shall be retained for a period of at least five years (or longer as required by 40
CFR 503),the Permittee shall retain records of all monitoring information,including.
> all calibration and maintenance records
> all original strip chart recordings for continuous monitoring instrumentation
> copies of all reports required by this permit
> copies of all data used to complete the application for this permit
These records or copies shall be maintained for a period of at least 3 years from the date of the sample,
measurement,report or application. This period may be extended by request of the Director at any time [40 CFR
122.41].
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the Permittee shall record
the following information [40 CFR 122.41]:
a. The date,exact place,and time of sampling or measurements;
b. The individual(s)who performed the sampling or measurements;
c. The date(s)analyses were performed;
d. The individual(s)who performed the analyses;
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e. The analytical techniques or methods used;and
f. The results of such analyses.
8. Inspection and Entry
The Permittee shall allow the Director, or an authorized representative (including an authorized contractor acting
as a representative of the Director),upon the presentation of credentials and other documents as may be required
by law, to;
a. Enter upon the Permittee's premises where a regulated facility or activity is located or conducted, or where
records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this
permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment),practices,
or operations regulated or required under this permit;and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise
authorized by the Clean Water Act,any substances or parameters at any location [40 CFR 122.41 (i)].
Section E Reporting Requirements
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit. The discharge
of any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall
constitute a violation of the permit.
2. Planned Changes
The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or
additions to the permitted facility [40 CFR 122.41 (1)]. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR
122.29 (b);or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged. This notification applies to pollutants subject neither to effluent limitations in the permit, nor to
notification requirements under 40 CFR 122.42 (a) (1).
c. The alteration or addition results in a significant change in the Permittee's sludge use or disposal practices,
and such alternation, addition or change may justify the application of permit conditions that are different
from or absent in the existing permit, including notification of additional use or disposal sites not reported
during the permit application process or not reported pursuant to an approved land application plan.
3. Anticipated Noncompliance
The Permittee shall give advance notice to the Director of any planned changes to the permitted facility or other
activities that might result in noncompliance with the permit [40 CFR 122.41 (1) (2)].
4. Transfers
This permit is not transferable to any person except after notice to the Director. The Director may require
modification or revocation and reissuance of the permit to document the change of ownership. Any such action
may incorporate other requirements as may be necessary under the Clean Water Act [40 CFR 122.41 (1) (3)].
5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit [40 CFR 122.41 (1) (4)].
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part II. D. 2) or forms
provided by the Director for reporting results of monitoring of sludge use or disposal practices.
b. If the Permittee monitors any pollutant more frequently than required by this permit, the results of such
monitoring shall be included in the calculation and reporting of the data submitted on the DMR.
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6. Twenty-four Hour Reporting
a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that
potentially threatens public health or the environment. Any information shall be provided orally within 24
hours from the time the Permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the Permittee becomes aware of the circumstances. The written
submission shall contain a description of the noncompliance, and its cause; the period of noncompliance,
including exact dates and times, and if the noncompliance has not been corrected, the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the
noncompliance [40 CFR 122.41 (1) (6)].
b. The Director may waive the written report on a case-by-case basis for reports under this section if the oral
report has been received within 24 hours.
c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response
personnel at [phone], [phone] or(919) 733-3300.
7. Other Noncompliance
The Permittee shall report all instances of noncompliance not reported under Part II. E. 5 and 6. of this permit at
the time monitoring reports are submitted. The reports shall contain the information listed in Part II. E. 6. of
this permit [40 CFR 122.41 (1) (7)].
8. Other Information
Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or
submitted incorrect information in a permit application or in any report to the Director,it shall promptly submit
such facts or information [40 CFR 122.41 (1) (8)].
9. Noncompliance Notification
The Permittee shall report by telephone to either the central office or the appropriate regional office of the
Division as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following
a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of
wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge
digester; the known passage of a slug of hazardous substance through the facility; or any other unusual
circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps,aerators,compressors,etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass directly to receiving
waters without treatment of all or any portion of the influent to such station or facility.
Persons reporting such occurrences by telephone shall also file a written report within 5 days following first
knowledge of the occurrence.
10. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act, 33
USC 1318,all reports prepared in accordance with the terms shall be available for public inspection at the offices
of the Division of Water Quality. As required by the Act, effluent data shall not be considered confidential.
Knowingly making any false statement on any such report may result in the imposition of criminal penalties as
provided for in NCGS 143-215.1(b)(2) or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this permit,including
monitoring reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of
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not more than $25,000 per violation, or by imprisonment for not more than two years per violation, or by both
[40 CFR 122.41].
12. Annual Performance Reports
Permittees who own or operate facilities that collect or treat municipal or domestic waste shall provide an annual
report to the Permit Issuing Authority and to the users/customers served by the Permittee (NCGS 143-215.1C).
The report shall summarize the performance of the collection or treatment system, as well as the extent to which
the facility was compliant with applicable Federal or State laws, regulations and rules pertaining to water quality.
The report shall be provided no later than sixty days after the end of the calendar or fiscal year, depending upon
which annual period is used for evaluation.
PART III
OTHER REQUIREMENTS
•
Section A. Construction
The Permittee shall not commence construction of wastewater treatment facilities,nor add to the plant's treatment
capacity,nor change the treatment process(es) utilized at the treatment plant unless the Division has issued an
Authorization to Construct (AtC) permit. Issuance of an AtC will not occur until Final Plans and Specifications for
the proposed construction have been submitted by the Permittee and approved by the Division.
Section B. Groundwater Monitoring
The Permittee shall,upon written notice from the Director of the Division of Water Quality,conduct groundwater
monitoring as may be required to determine the compliance of this NPDES permitted facility with the current
groundwater standards.
Section C. Changes in Discharges of Toxic Substances
The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe (40 CFR 122.42):
a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent
basis, of any toxic pollutant which is not limited in the permit,if that discharge will exceed the highest of the
following "notification levels";
(1) One hundred micrograms per liter(100 µg/L);
(2) Two hundred micrograms per liter (200 µg/L) for acrolein and acrylonitrile; five hundred micrograms
per liter (500 µg/L) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol;and one milligram per liter
(1 mg/L) for antimony;
(3) Five times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge, on a non-routine or
infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the
highest of the following"notification levels";
(1) Five hundred micrograms per liter(500 µg/L);
(2) One milligram per liter(1 mg/L) for antimony;
(3) Ten times the maximum concentration value reported for that pollutant in the permit application.
Section D. Evaluation of Wastewater Discharge Alternatives
The Permittee shall evaluate all wastewater disposal alternatives and pursue the most environmentally sound
alternative of the reasonably cost effective alternatives. If the facility is in substantial non-compliance with the terms
and conditions of the NPDES permit or governing rules,regulations or laws,the Permittee shall submit a report in
such form and detail as required by the Division evaluating these alternatives and a plan of action within 60 days of
notification by the Division.
Section E. Facility Closure Requirements
The Permittee must notify the Division at least 90 days prior to the closure of any wastewater treatment system
covered by this permit. The Division may require specific measures during deactivation of the system to prevent
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adverse impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit
continue at the permitted facility.
PART IV
SPECIAL CONDITIONS FOR MUNCIPAL FACILITIES
Section A. Publicly Owned Treatment Works (POTWs)
All POTWs must provide adequate notice to the Director of the following
1. Any new introduction of pollutants into the POTW from an indirect discharger which would be subject to
section 301 or 306 of CWA if it were directly discharging those pollutants;and
2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger
as influent to that POTW at the time of issuance of the permit.
3. For purposes of this paragraph,adequate notice shall include information on (1) the quality and quantity of
effluent introduced into the POTW,and (2) any anticipated impact of the change on the quantity or quality
of effluent to be discharged from the POTW.
Section B. Municipal Control of Pollutants from Industrial Users.
1. Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs from
industries using the municipal system may be present in the Permittee's discharge. At such time as
sufficient information becomes available to establish limitations for such pollutants, this permit may be
revised to specify effluent limitations for any or all of such other pollutants in accordance with best
practicable technology or water quality standards.
2. Under no circumstances shall the Permittee allow introduction of the following wastes in the waste
treatment system: •
a. Pollutants which create a fire or explosion hazard in the POTW, including, but not limited to,
wastestreams with a closed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees
Centigrade using the test methods specified in 40 CFR 261.21;
b. Pollutants which will cause corrosive structural damage to the POTW, but in no case Discharges
with pH lower than 5.0,unless the works is specifically designed to accommodate such Discharges;
c. Solid or viscous pollutants in amounts which will cause obstruction to the flow in the POTW
resulting in Interference;
d. Any pollutant, including oxygen demanding pollutants (BOD, etc.) released in a Discharge at a flow
rate and/or pollutant concentration which will cause Interference with the POTW;
e. Heat in amounts which will inhibit biological activity in the POTW resulting in Interference, but in
no case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C
(104°F) unless the Division,upon request of the POTW,approves alternate temperature limits;
f. Petroleum oil, nonbiodegradable cutting oil, or products of mineral oil origin in amounts that will
cause interference or pass through;
g. Pollutants which result in the presence of toxic gases, vapors, or fumes within the POTW in a
quantity that may cause acute worker health and safety problems;
h. Any trucked or hauled pollutants,except at discharge points designated by the POTW.
3. With regard to the effluent requirements listed in Part I of this permit, it may be necessary for the
Permittee to supplement the requirements of the Federal Pretreatment Standards (40 CFR, Part 403) to
ensure compliance by the Permittee with all applicable effluent limitations. Such actions by the Permittee
may be necessary regarding some or all of the industries discharging to the municipal system.
4. The Permittee shall require any industrial discharges sending influent to the permitted system to meet
Federal Pretreatment Standards promulgated in response to Section 307(b) of the Act. Prior to accepting
wastewater from any significant industrial user, the Permittee shall either develop and submit to the
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Division a Pretreatment Program for approval per I5A NCAC 2H .0907(a) or modify an existing •
Pretreatment Program per 15A NCAC 2H .0907(b).
5. This permit shall be modified, or alternatively,revoked and reissued, to incorporate or modify an approved
POTW Pretreatment Program or to include a compliance schedule for the development of a POTW
Pretreatment Program as required under Section 402(b)(8) of the Clean Water Act and implementing
regulations or by the requirements of the approved State pretreatment program,as appropriate.
Section C. Pretreatment Programs
Under authority of sections 307(b) and (c) and 402(b)(8) of the Clean Water Act and implementing regulations 40
CFR Part 403, North Carolina General Statute 143-215.3 (14) and implementing regulations 15A NCAC 2H
.0900, and in accordance with the approved pretreatment program, all provisions and regulations contained and
referenced in the Pretreatment Program Submittal are an enforceable part of this permit.
The Permittee shall operate its approved pretreatment program in accordance with Section 402(b)(8) of the Clean
Water Act, the Federal Pretreatment Regulations 40 CFR Part 403, the State Pretreatment Regulations 15A
NCAC 2H .0900, and the legal authorities, policies, procedures, and financial provisions contained in its
pretreatment program submission and Division approved modifications there of. Such operation shall include
but is not limited to the implementation of the following conditions and requirements:
1. Sewer Use Ordinance (SUO)
The Permittee shall maintain adequate legal authority to implement its approved pretreatment program.
2. Industrial Waste Survey (IWS)
The Permittee shall update its Industrial Waste Survey (IWS) to include all users of the sewer collection
system at least once every five years.
3. Monitoring Plan
The Permittee shall implement a Division approved Monitoring Plan for the collection of facility specific
data to be used in a wastewater treatment plant Headworks Analysis (HWA) for the development of
specific pretreatment local limits. Effluent data from the Plan shall be reported on the DMRs (as required
by Part II,Section D,and Section E.5.).
4. Headworks Analysis (HWA) and Local Limits
The Permittee shall obtain Division approval of a Headworks Analysis (HWA) at least once every five
years, and as required by the Division. Within 180 days of the effective date of this permit (or any
subsequent permit modification) the Permittee shall submit to the Division a written technical evaluation
of the need to revise local limits (i.e., an updated HWA or documentation of why one is not needed) [40
CFR 122.42]. The Permittee shall develop,in accordance with 40 CFR 403.5(c) and 15A NCAC 2H .0909,
specific Local Limits to implement the prohibitions listed in 40 CFR 403.5(a) and (b) and 15A NCAC 2H
.0909.
5. Industrial User Pretreatment Permits (IUP)&Allocation Tables
In accordance with NCGS 143-215.1, the Permittee shall issue to all significant industrial users, permits for
operation of pretreatment equipment and discharge to the Permittee's treatment works. These permits
shall contain limitations, sampling protocols, reporting requirements, appropriate standard and special
conditions, and compliance schedules as necessary for the installation of treatment and control
technologies to assure that their wastewater discharge will meet all applicable pretreatment standards and
requirements. The Permittee shall maintain a current Allocation Table (AT) which summarizes the results
of the Headworks Analysis (HWA) and the limits from all Industrial User Pretreatment Permits (IUP).
Permitted IUP loadings for each parameter cannot exceed the treatment capacity of the POTW as
determined by the HWA.
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6. Authorization to Construct(A to C)
The Permittee shall ensure that an Authorization to Construct permit (AtC) is issued to all applicable
industrial users for the construction or modification of any pretreatment facility. Prior to the issuance of
an AtC, the proposed pretreatment facility and treatment process must be evaluated for its capacity to
comply with all Industrial User Pretreatment Permit(IUP)limitations.
7. POTW Inspection&Monitoring of their SIUs
The Permittee shall conduct inspection, surveillance, and monitoring activities as described in its Division
approved pretreatment program in order to determine, independent of information supplied by industrial
users,compliance with applicable pretreatment standards. The Permittee must:
a. Inspect all Significant Industrial Users (SIUs) at least once per calendar year;and
b. Sample all Significant Industrial Users (SIUs) at least twice per calendar year for all permit-
limited pollutants, once during the period from January 1 through June 30 and once during the
period from July 1 through December 31,except for organic compounds which shall be sampled
once per calendar year;
8. SIU Self Monitoring and Reporting
The Permittee shall require all industrial users to comply with the applicable monitoring and reporting
requirements outlined in the Division approved pretreatment program, the industry's pretreatment permit,
or in 15A NCAC 2H .0908.
9. Enforcement Response Plan (ERP)
The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards
promulgated pursuant to section 307(b) and (c) of the Clean Water Act (40 CFR 405 et. seq.), prohibitive
discharge standards as set forth in 40 CFR 403.5 and 15A NCAC 2H .0909, and specific local limitations.
All enforcement actions shall be consistent with the Enforcement Response Plan (ERP) approved by the
Division.
10. Pretreatment Annual Reports (PAR)
The Permittee shall report to the Division in accordance with 15A NCAC 2H .0908. In lieu of submitting
annual reports, Modified Pretreatment Programs developed under 15A NCAC 2H .0904 (b) may be
required to meet with Division personnel periodically to discuss enforcement of pretreatment requirements
and other pretreatment implementation issues.
For all other active pretreatment programs,the Permittee shall submit two copies of a Pretreatment Annual
Report (PAR) describing its pretreatment activities over the previous twelve months to the Division at the
following address:
NC DENR/DWQ/Pretreatment Unit
1617 Mail Service Center
Raleigh,NC 27699-1617
These reports shall be submitted according to a schedule established by the Director and shall contain the
following:
a.) Narrative
A brief discussion of reasons for, status of, and actions taken for all Significant Industrial
Users (SIUs) in Significant Non-Compliance (SNC);
b.) Pretreatment Program Summary(PPS)
A pretreatment program summary(PPS) on specific forms approved by the Division;
c.) Significant Non-Compliance Report(SNCR)
The nature of the violations and the actions taken or proposed to correct the violations on
specific forms approved by the Division;
d.) Industrial Data Summary Forms (IDSF)
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NPDES Permit Requirem.ints
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Monitoring data from samples collected by both the POTW and the Significant Industrial
User (SIU). These analytical results must be reported on Industrial Data Summary Forms
(IDSF) or other specific format approved by the Division;
e.) Other Information
Copies of the POTW's allocation table,new or modified enforcement compliance schedules,
public notice of SIUs in SNC, and any other information, upon request, which in the
opinion of the Director is needed to determine compliance with the pretreatment
implementation requirements of this permit;
11. Public Notice
The Permittee shall publish annually a list of Significant Industrial Users (SIUs) that were in Significant
Non-Compliance (SNC) as defined in the Permittee's Division approved Sewer Use Ordinance with
applicable pretreatment requirements and standards during the previous twelve month period. This list
shall be published within four months of the applicable twelve-month period.
12. Record Keeping
The Permittee shall retain for a minimum of three years records of monitoring activities and results, along
with support information including general records,water quality records, and records of industrial impact
on the POTW.
13. Funding and Financial Report
The Permittee shall maintain adequate funding and staffing levels to accomplish the objectives of its
approved pretreatment program.
14. Modification to Pretreatment Programs
Modifications to the approved pretreatment program including but not limited to local limits
modifications, POTW monitoring of their Significant Industrial Users (SIUs), and Monitoring Plan
modifications, shall be considered a permit modification and shall be governed by 15 NCAC 2H .0114 and
15A NCAC 2H .0907_
•
Version 6/20/2003

OF WAT�c Michael F.Easley,Governor
RPc_ State of North Carolina
am G.Ross,Jr.,Secretary
. ID Department of Environment and Natural Resources
O 'r Alan W.Klimek,P.E.,Director
Division of Water Quality
c
November 6, 2003
�P\I Ms. Kimberly Weathers, Environmental Manager
FMC Corporation, Lithium Division
Highway 161, Box 795
Bessemer City, North Carolina 28016
Subject: NPDES Permit Correction
Permit No. NC0005177
FMC Corp., Lithium Division
Gaston County
Dear Ms. Weathers:
Per your request and our review, the NPDES permit for FMC Corp, Lithium Division
has been corrected to include proper treatment system references on the Supplement to
Permit Cover Sheet.
Please find enclosed the corrected permit page. The corrected page should be inserted
into the respective permit and the old page discarded. All other terms and conditions
contained in the original permit remain unchanged and in full effect. This permit correction is
issued under the requirements of North Carolina General Statutes 143-215.1 and the
Memorandum of Agreement between North Carolina and the U.S. Environmental Protection
Agency.
If you have any questions or need additional information, please do not hesitate to
contact Mark McIntire of my staff at(919) 733-5083, extension 508.
Sincerely
l'Aid#6.. .7L •
*Alan W. Klimek, P.E.
cc: Central Files
NPDES Unit Files
Mooresville Regional Office I�
1617 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1617 -TELEPHONE [phone]/FAX [phone]
VISIT US ON THE WEB AT http://h2o.enr.state.nc.us/NPDES

Permit NC0005177
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility. whether for operation or discharge are hereby revoked,
and as of this issuance, any previously issued permit bearing this number is no longer effective. Therefore,
the exclusive authority to operate and discharge from this facility arises under the permit conditions,
requirements, terms, and provisions included herein.
FMC Corporation
is hereby authorized to:
1. Continue operation of an existing 0.615 MGD wastewater treatment facility consisting of reverse
osmosis filtration, hydrogen peroxide addition, pH adjustment systems, and the Lower Pond located
at FMC's Lithium Division on Highway 161, Bessemer City. Gaston County;
2. Continue operation of a stormwater conveyance system and two sedimentation and polishing
ponds; and
3. Discharge treated wastewater (outfall 001) and stormwater, boiler blowdown, steam condensate, and
non-contact cooling water (004) at the locations specified on the attached map. The receiving stream
is an unnamed tributary to Abernethy Creek. a class C water in the Catawba River Basin.