NC0005177_Regional Office Historical File Pre 2018

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FMC Corporation
Lithium Division
Highway 161
Box 795
Bessemer City North Carolina 28016
704 868 5300 Fax [phone]
+FWC
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
April 3, 1996
Mr. David A. Goodrich
Permits and Engineering Unit
Water Quality Section
Division of Environmental Management
P.O. Box 29535
Raleigh, NC 27626-0535
Re: Renewal Application
NPDES No. NC0005177 & NCS000002
Dear Mr. Goodrich:
In accordance with the provisions of Part II, Item 10 of NPDES
Permit No. NC0005177, FMC Corporation's Lithium Division facility
in Bessemer City, Gaston County ("FMC") is herewith requesting
renewal of NPDES Permit No. NC0005177 and submitting three copies
of the completed, signed application form and a processing fee of
$300.00. The processing fee is based on a total flow of 1M-10M
Gal/day, as per 15A NCAC 2H .0104. This renewal application is
being submitted 180 days prior to expiration of the current
permit on September 30, 1996; FMC requests that should a new
permit not be issued by that date that the current permit remain
in force until superceded by a new permit.
Please note that this permit renewal application package includes
discharges from Outfall 001, which has been permitted under NPDES
No. NC0005177, Outfall 004, which has been permitted under NPDES
No. NCS000002, and the toe drain discharge from the Lower Pond
Dam, as discussed in the report entitled "Evaluation of
Stormwater and Regulated Discharges" which was submitted to
DEM/Water Quality Section pursuant to the requirements of NPDES
No. NCS000002 on August 15, 1995. FMC has discussed this report
with DEM/Water Quality Section and wishes to explore combining
the two NPDES permits in order to streamline administration of
the NPDES program and clarify the regulatory status of the toe
drain discharge. Given this streamlining, FMC proposes to adjust
its upstream sampling location to reflect the unnamed tributary
to which flows are discharged; the current permit language is
sufficient to allow this adjustment.

V.-
FMC Corp - NPDES No. NC0005177
Mr. David Goodrich
April 3, 1996 - Page 2
Additionally, FMC is requesting that the NPDES permit address
alternate flow rates which would correspond with alternate
chronic bioassey dilution factors, considering flows from the
western canal, as provided in the current permit structure. In
addition to the flows provided in NPDES No. NC0005177 currently,
FMC also requests that the permit address a higher flow rates
from Outfall 001. This would allow increase in the rate of
siphon withdrawl from the Lower Pond and would allow FMC better
control of water levels in the Lower Pond, and is requested given
1995's experience in very high levels of precipitation. FMC
requests addtional flow rates of "less than or equal to 0.700 MGD
but greater than 0.615 MGD" which would correspond to a chronic
bioassey dilution of 80%; "less than or equal to 0.800 MGD but
greater than 0.700 MGD" which would correspond to a chronic
bioassey dilution of 82%; and "less than or equal to 0.900 MGD
but greater than 0.800," which would correspond to a chronic
bioassey dilution of 84%.
Additionally, as was discussed with DEM/Water Quality Section in
December 1995, FMC is building a pilot plant on some newly
aquired property west of Highway 161. Stormwater runoff from
this property and boiler blowdown, cooling water, and steam
condensate will be managed in the same manner as those waters
associated with FMC's existing development west of Highway 161,
i.e., they will be directed into the western canal stormwater
conveyance system and discharged via Outfall 004. These flows,
anticipated to commence late in 1996, are included in this
renewal application.
Finally, FMC has initiated retesting for mercury, cyanide and oil
and grease at outfalls 001 and 004; the values reported by the
lab in the March 1996 priority pollutant analyses included with
this permit application are believed to be in error as they are
not consistent with historical observations. FMC will forward
the supplemental analyses as soon as they are available.
FMC looks forward to further discussions with DEM/Water Quality
Section on the NPDES programs at this facility. If you have any
questions, please call me at 704/868-0806.
Ve truly yours
Barbara E. itchie
Environm tal Manager

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State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
g Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. Paul Schroeder
FMC Corporation - Lithium Division
Post Office Box 795
Highway 274
Tryon School Road
Bessemer City, North Carolina 28016
Dear Mr. Schroeder:
4 • •
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September 30, 1996 N.C.DEPT.
aP PdA.WRAL R c:..
AMON Of ENVIROPll?@INTA! � 011',k:: [V
K81 UVILE-REMNAL OFFICE
Subject: NPDES Permit Issuance
Permit No. NC0005169
Hallman Beam Mine
Gaston County
In accordance with the application for a discharge permit received on March 11, 1996 the Division is
forwarding herewith the subject NPDES permit. This permit is issued pursuant to the requirements of North
Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the
U.S. Environmental Protection Agency dated December 6, 1983.
An investigation of the NPDES facility site indicated that a residence is using well water adjacent to
Pond F. Presently, there are no groundwater monitoring wells in the vicinity of Pond F. Lithium has been
detected in groundwater samples collected from monitoring wells at other locations on the FMC site. The
State requires that a groundwater monitoring well be installed between Pond F and the residence well to
identify and track the movement of any potential contamination.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30)
days following receipt of this letter. This request must be in the form of a written petition, conforming to
Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings,
Post Office Drawer 27447, Raleigh, North Carolina 27611-7447. Unless such demand is made, this
decision shall be final and binding.
Please take note that this permit is not transferable. Part II, E.4. addresses the requirements to be
followed in case of change in ownership or control of this discharge.
This permit does not affect the legal requirements to obtain other permits which may be required by
the Division of Water Quality or permits required by the Division of Land Resources or any other Federal or
Local governmental permit that may be required.
f;
i
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

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September 30. 1996
Page 2
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If you have any questions concerning this permit, please contact Paul B. Clark at telephone number
[phone]. extension 580.
Sincerely,
Gigawj by
A. Preston Howard. Jr., P.E.
Enclosures
cc: Central Files
Mooresville Regional mice, Water Quality Section
Mr. Roosevelt Childr EPA
Permits and Engineer. Unit
Facility Assessment U,
Aquatic Survey and Tox- -logy Unit
L.

Permit No. NC0005169
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
FMC Corporation, Lithium Division
is hereby authorized to discharge wastewater from a facility located at
NCSR 1474
east of Tryon
Gaston County
to receiving waters designated as an unnamed tributary to Long Creek in the Catawba River Basin
in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I,
II, III, and IV hereof.
The permit shall become effective November 1, 1996
This permit and the authorization to discharge shall expire at midnight on September 30, 2001
Signed this day September 30, 1996
Original Signed By
David A. Goodrich
A. Preston Howard, Jr., P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission
1

SUPPLEMENT TO PERMIT COVER SHEET
FMC Corporation, Lithium Division
is hereby authorized to:
Permit No. NC0005169
1. Continue to discharge from FMC treatment system which consists of several ponds. Ponds
C, D, and F (Polymer addition included in Pond F) receive tailings (or pit dewatering) waste
and either discharge directly through outfall 002 or discharge to Pond A. Pond A (in addition
to receiving tailings waste from ponds C, D, and F) also receives process wastewater. Pond
A discharges through outfall 001. Outfalls 001 and 002 are located in close proximity of
each other and their flows combine a short distance from the two outfall locations. These
treatment systems are located at NCSR 1474, east of Tryon, Gaston County (See Part III of
this permit), and
2. Discharge from said treatment system at the location specified on the attached map into an
unnamed tributary to Long Creek (Class C) in the Catawba River Basin.

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ROAD CLASSIFICATION
PRIMARY HIGHWAY LIGHT-DUrY ROAD, HARD OR
HARD SURFACE IMPROVED SURFACE
SECONDARY HIGHWAY
HARD SURFACE r__jwNN= U NMPROVED ROAD
Latitude-35°20'20" Longitude 81 °18'40"
Map # F13SE Sub -basin 030836
Stream Class C
Discharge Class
Receiving Stream Long Creek / Catawba River
Design Qyariahlt, Permit expires 9/30/01
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$27
QUAD LOCATION FMC Corp. - Lithium Division
NC0005169
% Gaston County
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A. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Permit No. NC0005169
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from outfall(s) serial number
001. Such discharges shall be limited and monitored by the Permittee as specified below:
EFFLUENT CHARACTERISTICS
LIMITS
MONITORING REQUIREMENTS
Monthly
Average
Weekly
Average
Daily
Maximum
Measurement
Frequency
Sample.
Type
Sample
Location'
Flow
Continuous
Recording
I or E
TSS
50.0 m /I
90.0 m /I
2/month
Composite
E
Turbidity 2
Monthly
Grab
U, D
MBAS
500.0 u /I
2/month
Composite
E
Chloride
Monthly
Composite
E
Sulfate
Monthly
Composite
E
Lithium
,-Monthly
Composite
E
Total Nitrogen (NO2+ NO3 + TKN)
-Monthly
Composite
E
Total Phosphorus
-Monthly
Composite
E
Acute Toxicity 3
Quarterly
Composite
E
Notes:
' Sample locations: E - Effluent, I - Influent, U - Upstream approximately 50 feet upstream of discharge, D - Downstream approximately 100 feet downstream of
discharge. Upstream and Downstream samples shall be grab samples.
2 The discharge shall not cause the turbidity of the receiving water to exceed 50 NT}J. If the turbidity exceeds these levels due to natural background
conditions, the discharge level cannot cause any increase in the turbidity of the receiving water.
3 Acute Toxicity (Daphnis ulex , 24-hour, no significant mortality at 90 %; February, May, August, and November; See Part III, Condition E.
The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units and shall be monitored 2/month at the effluent by grab sample.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
L.
A

F
A. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Permit No. NC0005169
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from outfall(s) serial number
002. Such discharges shall be limited and monitored by the Permittee as specified below (these limits apply only when discharging pit dewatering wastewater):
EFFLUENT CHARACTERISTICS
LIMITS
MONITORING REQUIREMENTS
Monthly
Average
Weekly
Average
Daily
Maximum
Measurement
Ere uenc
Sample
T e �j
Sample
Location'
Flow
Monthly
Instantaneous
E
TSS
50.0 m /I
90.0 m /I
2/month
Grab
E
Notes:
' Sample locations: E - Effluent.
Best Management Practices (BMP) Conditions
1. The permittee shall operate the facilities in a manner which will minimize the impact on the receiving waters.
2. The permittee shall utilize sound management practices to ensure that contaminants do not enter the surface water as a result of blasting at this site.
The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units and shall be monitored 2/month at the effluent by grab sample.
There shall be no discharge of floating solids or visible foam in other than trace amounts.

PART
TM • t z• • • . k.
1. The permittee shall comply with Final Effluent Limitations specified for discharges in accordance
with the following schedule:
Permittee shall comply with Final Effluent Limitations by the effective date of the permit unless
specified below.
2. Permittee shall at all times provide the operation and maintenance necessary to operate the
existing facilities at optimum efficiency.
3. No later than 14 calendar days following a date identified in the above schedule of compliance,
the permittee shall submit either a report of progress or, in the case of specific actions being
required by identified dates, a written notice of compliance or noncompliance. In the latter case,
the notice shall include the cause of noncompliance, any remedial actions taken, and the
probability of meeting the next schedule requirements.

Part II
Page 1 of 14
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
WeR 14 2h! •
I . Permit Issuing Authority
The Director of the Division of Water Quality.
43VEWUM
Means the Division of Water Quality, Department of Environment, Health and Natural Resources.
a.�
Used herein means the North Carolina Environmental Management Commission.
4. Actor "the Act"
The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended, 33 USC
1251, et. seq.
5. Mass/Day Measurements
a . The "monthly average discharge" is defined as the total mass of all daily discharges sampled
and/or measured during a calendar month on which daily discharges are sampled and
measured, divided by the number of daily discharges sampled and/or measured during such
month. It is therefore, an arithmetic mean found by adding the weights of the pollutant found
each day of the month and then dividing this sum by the number of days the tests were
reported. The limitation is identified as "Monthly Average" in Part I of the permit.
b. The "weekly average discharge" is defined as the total mass of all daily discharges sampled
and/or measured during the calendar week (Sunday - Saturday) on which daily discharges are
sampled and measured, divided by the number of daily discharges sampled and/or measured
during such week. It is, therefore, an arithmetic mean found by adding the weights of
pollutants found each day of the week and then dividing this sum by the number of days the
tests were reported. This limitation is identified as "Weekly Average" in Part I of the permit.
c. The "maximum daily discharge" is the total mass (weight) of a pollutant discharged during a
calendar day. If only one sample is taken during any calendar day the weight of pollutant
calculated from it is the "maximum daily discharge." This limitation is identified as "Daily
Maximum," in Part I of the permit.
d. The "average annual discharge" is defined as the total mass of all daily discharges sampled
and/or measured during the calendar year on which daily discharges are sampled and
measured, divided by the number of daily discharges sampled and/or measured during such
year. It is, therefore, an arithmetic mean found by adding the weights of pollutants found each
day of the year and then dividing this sum by the number of days the tests were reported. This
limitation is defined as "Annual Average" in Part I of the permit.

Part II
Page 2 of 14
a . The "average monthly concentration," other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges sampled and/or measured during a calendar month on
which daily discharges are sampled and measured, divided by the number of daily discharges
sampled and/or measured during such month (arithmetic mean of the daily concentration
values). The daily concentration value is equal to the concentration of a composite sample or in
the case of grab samples is the arithmetic mean (weighted by flow value) of all the samples
collected during that calendar day. The average monthly count for fecal coliform bacteria is
the geometric mean of the counts for samples collected during a calendar month. This
limitation is identified as "Monthly Average" under "Other Limits" in Part I of the permit.
b. The "average weekly concentration," other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges sampled and/or measured during a calendar week
(Sunday/Saturday) on which daily discharges are sampled and measured divided by the
number of daily discharges sampled and/or measured during such week (arithmetic mean of the
daily concentration values). The daily concentration value is equal to the concentration of a
composite sample or in the case of grab samples is the arithmetic mean (weighted by flow
value) of all the samples collected during that calendar day. The average weekly count for
fecal coliform bacteria is the geometric mean of the counts for samples collected during a
calendar week. This limitation is identified as "Weekly Average" under "Other Limits" in
Part I of the permit.
C. The "maximum daily concentration" is the concentration of a pollutant discharge during a
calendar day. If only one sample is taken during any calendar day the concentration of
pollutant calculated from it is the "Maximum Daily Concentration". It is identified as "Daily
Maximum" under "Other Limits" in Part I of the permit.
d. The "average annual concentration," other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges sampled and/or measured during a calendar year on
which daily discharges are sampled and measured divided by the number of daily discharges
sampled and/or measured during such year (arithmetic mean of the daily concentration
values). The daily concentration value is equal to the concentration of a composite sample or in
the case of grab samples is the arithmetic mean (weighted by flow value) of all the samples
collected during that calendar day. The average yearly count for fecal coliform bacteria is the
geometric mean of the counts for samples collected during a calendar year. This limitation is
identified as "Annual Average" under "Other Limits" in Part I of the permit.
e. The "daily average concentration" (for dissolved oxygen) is the minimum allowable amount of
dissolved oxygen required to be available in the effluent prior to discharge averaged over a
calendar day. If only one dissolved oxygen sample is taken over a calendar day, the sample is
considered to be the "daily average concentration" for the discharge. It is identified as "daily
average" in the text of Part 1.
The "quarterly average concentration" is the average of all samples taken over a calendar
quarter. It is identified as "Quarterly Average Limitation" in the text of Part I of the permit.
g. A calendar quarter is defined as one of the following distinct periods: January through March,
April through June, July through September, and October through December.

Part II
Page 3 of 14
7. Other Measurements
a. Flow, (MGD): The flow limit expressed in this permit is the 24 hours average flow, averaged
monthly. It is determined as the arithmetic mean of the total daily flows recorded during the
calendar month.
b. An "instantaneous flow measurement" is a measure of flow taken at the time of sampling, when
both the sample and flow will be representative of the total discharge.
c. A "continuous flow measurement" is a measure of discharge flow from the facility which occurs
continually without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for
infrequent maintenance activities on the flow device.
8. Types of Samples
a. Composite Sample: A composite sample shall consist of:
(1) a series of grab samples collected at equal time intervals over a 24 hour period of discharge
and combined proportional to the rate of flow measured at the time of individual sample
collection, or
(2) a series of grab samples of equal volume collected over a 24 hour period with the time
intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow
recorder and totalizer, and the present gallon interval between sample collection fixed at
no greater than 1 /24 of the expected total daily flow at the treatment system, or
(3) a single, continuous sample collected over a 24 hour period proportional to the rate of flow.
In accordance with (1) above, the time interval between influent grab samples shall be no
greater than once per hour, and the time interval between effluent grab samples shall be no
greater than once per hour except at wastewater treatment systems having a detention time of
greater than 24 hours. In such cases, effluent grab samples may be collected at time intervals
evenly spaced over the 24 hour period which are equal in number of hours to the detention time
of the system in number of days. However, in no case may the time interval between effluent
grab samples be greater than six (6) hours nor the number of samples less than four (4) during a
24 hour sampling period.
b. Grab Sample: Grab samples are individual samples collected over a period of time not
exceeding 15 minutes; the grab sample can be taken manually. Grab samples must be
representative of the discharge or the receiving waters.
a Arithmetic Mean: The arithmetic mean of any set of values is the summation of the individual
values divided by the number of individual values.
b. Geometric Mean: The geometric mean of any set of values is the Nth root of the product of the
individual values where N is equal to the number of individual values. The geometric mean is
equivalent to the antilog of the arithmetic mean of the logarithms of the individual values.
For purposes of calculating the geometric mean, values of zero (0) shall be considered to be one
(1).
c. Weighted by Flow Value: Weighted by flow value means the summation of each concentration
times its respective flow divided by the summation of the respective flows.

Part II
Page 4 of 14
10. Calendar Day
A calendar day is defined as the period from midnight of one day until midnight of the next day.
However, for purposes of this permit, any consecutive 24-hour period that reasonably represents
the calendar day may be used for sampling.
11. Hazardous Substance
A hazardous substance means any substance designated under 40 CFR Part 116 pursuant to Section
311 of the Clean Water Act.
12. Toxic Pollutant
A toxic pollutant is any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
SECTION B. GENERAL CONDITIONS
The permittee must comply with all conditions of this permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit renewal application.
a . The permittee shall comply with effluent standards or prohibitions established under section
307(a) of the Clean Water Act for toxic pollutants and with standards for sewage sludge use or
disposal established under section 405(d) of the Clean Water Act within the time provided in
the regulations that establish these standards or prohibitions or standards for sewage sludge
use or disposal, even if the permit has not yet been modified to incorporate the requirement.
b. The Clean Water Act provides that any person who violates a permit condition is subject to a
civil penalty not to exceed $25,000 per day for each violation. Any person who negligently
violates any permit condition is subject to criminal penalties of $2,500 to $25,000 per day of
violation, or imprisonment for not more than 1 year, or both. Any person who knowingly
violates permit conditions is subject to criminal penalties of $5,000 to $50,000 per day of
violation, or imprisonment for not more than 3 years, or both. Also, any person who violates a
permit condition may be assessed an administrative penalty not to exceed $10,000 per violation
with the maximum amount not to exceed $125,000. [Ref: Section 309 of the Federal Act 33
U.S.C. 1319 and 40 CFR 122.41 (a)]
c. Under state law, a civil penalty of not more than ten thousand dollars ($10,000) per violation
may be assessed against any person who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit. [Ref: North Carolina General Statutes § 143-215.6A]
d. Any person may be assessed an administrative penalty by the Administrator for violating
section 301, 302, 306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation
implementing any of such sections in a permit issued under section 402 of the Act.
Administrative penalties for Class I violations are not to exceed $10,000 per violation, with
the maximum amount of any Class I penalty assessed not to exceed $25,000. Penalties for Class
II violations are not to exceed $10,000 per day for each day during which the violation
continues, with the maximum amount of any Class II penalty not to exceed $125,000.

Part II
Page 5 of 14
2. Duty to Mitigate
The permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or
disposal in violation of this permit which has a reasonable likelihood of adversely affecting
human health or the environment.
It_ .. Eqn-In \
Except as provided in permit conditions on "Bypassing" (Part II, C-4) and 'Tower Failures" (Part II,
C-7), nothing in this permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309 of
the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for consequential damages,
such as fish kills, even though the responsibility for effective compliance may be temporarily
suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities, or penalties to which the permittee is or may
be subject to under NCGS 143-215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321.
Furthermore, the permittee is responsible for consequential damages, such as fish kills, even
though the responsibility for effective compliance may be temporarily suspended.
The issuance of this permit does not convey any property rights in either real or personal property,
or any exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights, nor any infringement of Federal, State or local laws or regulations.
�1�_ • • fit i • •• • •_ � q� •
This permit does not authorize or approve the construction of any onshore or offshore physical
structures or facilities or the undertaking of any work in any navigable waters.
7. Severability
T
The provisions of this permit are severable, and if any provision of this permit, or the application
of any provision of this permit to any circumstances, is held invalid, the application of such
provision to other circumstances, and the remainder of this permit, shall not be affected thereby.
The permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any
information which the Permit Issuing Authority may request to determine whether cause exists for
modifying, revoking and reissuing, or terminating this permit or to determine compliance with this
permit. The permittee shall also furnish to the Permit Issuing Authority upon request, copies of
records required to be kept by this permit.
If the permittee wishes to continue an activity regulated by this permit after the expiration date of
this permit, the permittee must apply for and obtain a new permit.

Part II
Page 6 of 14
10. Expiration of Permit
The permittee is not authorized to discharge after the expiration date. In order to receive
automatic authorization to discharge beyond the expiration date, the permittee shall submit such
information, forms, and fees as are required by the agency authorized to issue permits no later than
180 days prior to the expiration date. Any permittee that has not requested renewal at least 180
days prior to expiration, or any permittee that does not have a permit after the expiration and has
not requested renewal at least 180 days prior to expiration, will subject the permittee to enforcement
procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. Sign tort' Kwuirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed
and certified.
a . All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a
responsible corporate officer means: (a) a president, secretary, treasurer or vice president
of the corporation in charge of a principal business function, or any other person who
performs similar policy or decision making functions for the corporation, or (b) the manager
of one or more manufacturing production or operating facilities employing more than 250
persons or having gross annual sales or expenditures exceeding 25 million (in second quarter
1980 dollars), if authority to sign documents has been assigned or delegated to the manager
in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive
officer or ranking elected official.
b. All reports required by the permit and other information requested by the Permit Issuing
Authority shall be signed by a person described above or by a duly authorized representative of
that person. A person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
responsibility, or an individual or position having overall responsibility for environmental
matters for the company. (A duly authorized representative may thus be either a named
individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Permit Issuing Authority.
c. Certification. Any person signing a document under paragraphs a. or b. of this section shall
make the following certification:
"I certify, under penalty of law, that this document and all attachments were prepared under
my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering
the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."

Part II
Page 7 of 14
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request
by the permittee for a permit modification, revocation and reissuance, or termination, or a
notification of planned changes or anticipated noncompliance does not stay any permit condition.
13. Permit Modification Revocation and Reissuance or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and
modifying the permit, revoking and reissuing the permit, or terminating the permit as allowed by
the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122 and
123; Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North
Carolina General Statute 143-215.1 et. al.
14. Previous Permits
All previous National Pollutant Discharge Elimination System Permits issued to this facility,
whether for operation or discharge, are hereby revoked by issuance of this permit. [The exclusive
authority to operate this facility arises under this permit. The authority to operate the facility
under previously issued permits bearing this number is no longer effective. ] The conditions,
requirements, terms, and provisions of this permit authorizing discharge under the National
Pollutant Discharge Elimination System govern discharges from this facility.
1. Certified Operator
Pursuant to Chapter 9OA-44 of North Carolina General Statutes, and upon classification of the
facility by the Certification Commission, the permittee shall employ a certified wastewater
treatment plant operator in responsible charge (ORC) of the wastewater treatment facilities. Such
operator must hold a certification of the grade equivalent to or greater than the classification
assigned to the wastewater treatment facilities by the Certification Commission. The permittee
must also employ a certified back-up operator of the appropriate type and any grade to comply
with the conditions of Title 15A, Chapter 8A .0202. The ORC of the facility must visit each Class I
facility at least weekly and each Class II, III, and IV facility at least daily, excluding weekends
and holidays, and must properly manage and document daily operation and maintenance of the
facility and must comply with all other conditions of Title 15A, Chapter 8A .0202. Once the
facility is classified, the permittee shall submit a letter to the Certification Commission which
designates the operator in responsible charge within thirty days after the wastewater treatment
facilities are 50% complete.
The permittee shall at all times properly operate and maintain all facilities and systems of
treatment and control (and related appurtenances) which are installed or used by the permittee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also
includes adequate laboratory controls and appropriate quality assurance procedures. This provision
requires the operation of back-up or auxiliary facilities or similar systems which are installed by a
permittee only when the operation is necessary to achieve compliance with the conditions of the
permit.

Part H
Page 8 of 14
It shall not be a defense for a permittee in an enforcement action that it would have been necessary
to halt or reduce the permitted activity in order to maintain compliance with the condition of this
permit.
4. Bypassing of Treatment Facilities
a. Definitions
(1) "Bypass" means the known diversion of waste streams from any portion of a treatment
facility including the collection system, which is not a designed or established or operating
mode for the facility.
(2) "Severe property damage" means substantial physical damage to property, damage to the
treatment facilities which causes them to become inoperable, or substantial and permanent
loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage does not mean economic loss caused by delays in
production.
b. Bypass not exceeding limitations.
The permittee may allow any bypass to occur which does not cause effluent limitations to be
exceeded, but only if it also is for essential maintenance to assure efficient operation. These
bypasses are not subject to the provisions of Paragraphs c. and d. of this section
c. Notice
(1) Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall
submit prior notice, if possible at least ten days before the date of the bypass; including an
evaluation of the anticipated quality and affect of the bypass.
(2) Unanticipated bypass. The permittee shall submit notice of an unanticipated bypass as
required in Part 11, E. 6. of this permit. (24 hour notice).
d. Prohibition of Bypass
(1) Bypass is prohibited and the Permit Issuing Authority may take enforcement action against
a permittee for bypass, unless:
(A) Bypass was unavoidable to prevent loss of life, personal injury or severe property
damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment
facilities, retention of untreated wastes or maintenance during normal periods of
equipment downtime. This condition is not satisfied if adequate backup equipment should
have been installed in the exercise of reasonable engineering judgment to prevent a bypass
which occurred during normal periods of equipment downtime or preventive maintenance;
and
(C) The permittee submitted notices as required under Paragraph c. of this section.
(2) The Permit Issuing Authority may approve an anticipated bypass, after considering its
adverse affects, if the Permit Issuing Authority determines that it will meet the three
conditions listed above in Paragraph d. (1) of this section.

Part II
Page 9 of 14
5. Upsets
a. Definition.
"Upset " means an exceptional incident in which there is unintentional and temporary
noncompliance with technology based permit effluent limitations because of factors beyond the
reasonable control of the permittee. An upset does not include noncompliance to the extent
caused by operational error, improperly designed treatment facilities, inadequate treatment
facilities, lack of preventive maintenance, or careless or improper operation.
b. Effect of an upset.
An upset constitutes an affirmative defense to an action brought for noncompliance with such
technology based permit effluent limitations if the requirements of paragraph c. of this
condition are met. No determination made during administrative review of claims that
noncompliance was caused by upset, and before an action for noncompliance, is final
administrative action subject to judicial review.
c. Conditions necessary for a demonstration of upset.
A permittee who wishes to establish the affirmative defense of upset shall demonstrate,
through properly signed, contemporaneous operating logs, or other relevant evidence that:
(1) An upset occurred and that the permittee can identify the cause(s) of the upset;
(2) The permittee facility was at the time being properly operated; and
(3) The permittee submitted notice of the upset as required in Part 11, E. 6. (b) (B) of this permit.
(4) The permittee complied with any remedial measures required under Part II, B. 2. of this
permit.
d. Burden of prof.
In any enforcement proceeding the permittee seeking to establish the occurrence of an upset has
the burden of proof.
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of
wastewaters shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such
as to prevent any pollutant from such materials from entering waters of the State or navigable
waters of the United States. The permittee shall comply with all existing federal regulations
governing the disposal of sewage sludge. Upon promulgation of 40 CFR Part 503, any permit issued
by the Permit Issuing Authority for the utilization/disposal of sludge may be reopened and
modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR Part 503. The
permittee shall comply with applicable 40 CFR Part 503 Standards for the Use and Disposal of
Sewage Sludge (when promulgated) within the time provided in the regulation, even if the permit
is not modified to incorporate the requirement. The permittee shall notify the Permit Issuing
Authority of any significant change in its sludge use or disposal practices.
7. Power Failures
The permittee is responsible for maintaining adequate safeguards as required by DEM Regulation,
Title 15A, North Carolina Administrative Code, Subchapter 2H, .0124 Reliability, to prevent the
discharge of untreated or inadequately treated wastes during electrical power failures either by
means of alternate power sources, standby generators or retention of inadequately treated effluent.

Part II
Page 10 of 14
Samples collected and measurements taken, as required herein, shall be characteristic of the
volume and nature of the permitted discharge. Samples collected at a frequency less than daily
shall be taken on a day and time that is characteristic of the discharge over the entire period
which the sample represents. All samples shall be taken at the monitoring points specified in this
permit and, unless otherwise specified, before the effluent pins or is diluted by any other
wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to and the approval of the Permit Issuing Authority.
Monitoring results obtained during the previous month(s) shall be summarized for each month and
reported on a monthly Discharge Monitoring Report (DMR) Form (DEM No. MR 1, 1.1, 2, 3) or
alternative forms approved by the Director, DEM, postmarked no later than the 30th day
following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case
of a new facility, on the last day of the month following the commencement of discharge.
Duplicate signed copies of these, and all other reports required herein, shall be submitted to the
following address:
Division of Water Quality
Water Quality Section
ATTENTION: Central Files
Post Office Box 29535
Raleigh, North Carolina 27626-0535
Appropriate flow measurement devices and methods consistent with accepted scientific practices
shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges. The devices shall be installed, calibrated and maintained to ensure that the
accuracy of the measurements are consistent with the accepted capability of that type of device.
Devices selected shall be capable of measuring flows with a maximum deviation of less than + 10%
from the true discharge rates throughout the range of expected discharge volumes. Once -through
condenser cooling water flow which is monitored by pump logs, or pump hour meters as specified in
Part I of this permit and based on the manufacturer's pump curves shall not be subject to this
requirement.
Test procedures for the analysis of pollutants shall conform to the EMC regulations published
pursuant to NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations
published pursuant to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as
Amended, and Regulation 40 CFR 136; or in the case of sludge use or disposal, approved under 40
CFR 136, unless otherwise specified in 40 CFR 503, unless other test procedures have been specified
in this permit.
To meet the intent of the monitoring required by this permit, all test procedures must produce
minimum detection and reporting levels that are below the permit discharge requirements and all
data generated must be reported down to the minimum detection or lower reporting level of the
procedure. If no approved methods are determined capable of achieving minimum detection and

Part II
Page 11 of 14
reporting levels below permit discharge requirements, then the most sensitive (method with the
lowest possible detection and reporting level) approved method must be used.
5. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders
inaccurate, any monitoring device or method required to be maintained under this permit shall,
upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for
not more than two years per violation, or by both. If a conviction of a person is for a violation
committed after a first conviction of such person under this paragraph, punishment is a fine of not
more than $20,000 per day of violation, or by imprisonment of not more than 4 years, or both.
6. Records Retention
Except for records of monitoring information required by this permit related to the permittee's
sewage sludge use and disposal activities, which shall be retained for a period of at least five
years (or longer as required by 40 CFR 503), the permittee shall retain records of all monitoring
information, including all calibration and maintenance records and all original strip chart
recordings for continuous monitoring instrumentation, copies of all reports required by this permit,
for a period of at least 3 years from the date of the sample, measurement, report or application.
This period may be extended by request of the Director at any time.
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the permittee
shall record the following information:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f . The results of such analyses.
The permittee shall allow the Director, or an authorized representative (including an authorized
contractor acting as a representative of the Director), upon the presentation of credentials and other
documents as may be required by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or
conducted, or where records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions
of this permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control
equipment), practices, or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as
otherwise authorized by the Clean Water Act, any substances or parameters at any location

Part H
Page 12 of 14
�Ixq • ,4:; welav10 mZ4*9181 1._
1. mange in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit.
The discharge of any pollutant identified in this permit more frequently than or at a level in excess
of that authorized shall constitute a violation of the permit.
The permittee shall give notice to the Director as soon as possible of any planned physical
alterations or additions to the permitted facility. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for determining
whether a facility is a new source in 40 CFR Part 122.29 (b); or
b. The alteration or addition could significantly change the nature or increase the quantity of
pollutants discharged. This notification applies to pollutants which are subject neither to
effluent limitations in the permit, nor to notification requirements under 40 CFR Part 122.42 (a)
(1).
c. The alteration or addition results in a significant change in the permittee's sludge use or
disposal practices, and such alternation, addition or change may justify the application of
permit conditions that are different from or absent in the existing permit, including notification
of additional use or disposal sites not reported during the permit application process or not
reported pursuant to an approved land application plan.
3. AnticiFated Noncompliance
The permittee shall give advance notice to the Director of any planned changes in the permitted
facility or activity which may result in noncompliance with permit requirements.
4. Transfers
This permit is not transferable to any person except after notice to the Director. The Director may
require modification or revocation and reissuance of the permittee and incorporate such other
requirements as may be necessary under the Clean Water Act.
Monitoring results shall be reported at the intervals specified elsewhere in this permit.
a . Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part H. D. 2
of this permit) or forms provided by the Director for reporting results of monitoring of sludge use
or disposal practices.
b. If the permittee monitors any pollutant more frequently than required by the permit, using test
procedures specified in Part II, D. 4. of this permit or in the case of sludge use or disposal,
approved under 40 CFR 503, or as specified in this permit, the results of this monitoring shall be
included in the calculation and reporting of the data submitted in the DMR.
c. Calculations for all limitations which require averaging of measurements shall utilize an
arithmetic mean unless otherwise specified by the Director in the permit.

Part II
Page 13 of 14
6. Twenty-four Hour R=rting
a . The permittee shall report to the central office or the appropriate regional office any
noncompliance which may endanger health or the environment. Any information shall be
provided orally within 24 hours from the time the permittee became aware of the
circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances. The written submission shall contain a
description of the noncompliance, and its cause; the period of noncompliance, including exact
dates and times, and if the noncompliance has not been corrected, the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence
of the noncompliance.
b. The following shall be included as information which must be reported within 24 hours under
this paragraph:
(1) Any unanticipated bypass which exceeds any effluent limitation in the permit.
(2) Any upset which exceeds any effluent limitation in the permit.
(3) Violation of a maximum daily discharge limitation for any of the pollutants listed by the
Director in the permit to be reported within 24 hours.
C. The Director may waive the written report on a case -by -case basis for reports under paragraph
b. above of this condition if the oral report has been received within 24 hours.
7. Other Noncompliance
The permittee shall report all instances of noncompliance not reported under Part II. E. 5 and 6. of
this permit at the time monitoring reports are submitted. The reports shall contain the information
listed in Part II. E. 6. of this permit.
Where the permittee becomes aware that it failed to submit any relevant facts in a permit
application, or submitted incorrect information in a permit application or in any report to the
Director, it shall promptly submit such facts or information.
The permittee shall report by telephone to either the central office or the appropriate regional
office of the Division as soon as possible, but in no case more than 24 hours or on the next working
day following the occurrence or first knowledge of the occurrence of any of the following:
a. Any occurrence at the water pollution control facility which results in the discharge of
significant amounts of wastes which are abnormal in quantity or characteristic, such as the
dumping of the contents of a sludge digester; the known passage of a slug of hazardous substance
through the facility; or any other unusual circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of
adequate wastewater treatment such as mechanical or electrical failures of pumps, aerators,
compressors, etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass
directly to receiving waters without treatment of all or any portion of the influent to such
station or facility.

Part II
Page 14 of 14
Persons reporting such occurrences by telephone shall also file a written report in letter form within
5 days following first knowledge of the occurrence.
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the
Federal Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for
public inspection at the offices of the Division of Water Quality. As required by the Act, effluent
data shall not be considered confidential. Knowingly making any false statement on any such
report may result in the imposition of criminal penalties as provided for in NCGS 143-215.1(b)(2) or
in Section 309 of the Federal Act.
fili;" :, . . . ..
The Clean Water Act provides that any person who knowingly makes any false statement,
representation, or certification in any record or other document submitted or required to be
maintained under this permit, including monitoring reports or reports of compliance or
noncompliance shall, upon conviction, be punished by a fine of not more than $10,000 per violation,
or by imprisonment for not more than two years per violation, or by both.

PART III
OTHER REQUIREMENTS
No construction of wastewater treatment facilities or additions to add to the plant's treatment
capacity or to change the type of process utilized at the treatment plant shall be begun until Final
Plans and Specifications have been submitted to the Division of Water Quality and written approval
and Authorization to Construct has been issued.
The permittee shall, upon written notice from the Director of the Division of Water Quality, conduct
groundwater monitoring as may be required to determine the compliance of this NPDES permitted
facility with the current groundwater standards.
C. Changes in Discharges of Toxic Substances
The permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe:
a.That any activity has occurred or will occur which would result in the discharge, on a routine or
frequent basis, of any toxic pollutant which is not limited in the permit, if that discharge will
exceed the highest of the following "notification levels";
(1) One hundred micrograms per liter (100 ug/1);
(2)Two hundred micrograms per liter (200 ug/1) for acrolein and acrylonitrile; five hundred
micrograms per liter (500 ug/1) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol; and
one milligram per liter (1 mg/1) for antimony;
(3) Five (5) times the maximum concentration value reported for that pollutant in the permit
application.
b. That any activity has occurred or will occur which would result in any discharge, on a non -routine
or infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will
exceed the highest of the following "notification levels';
(1) Five hundred micrograms per liter (500 ug/1);
(2) One milligram per liter (1 mg/1) for antimony;
(3) Ten (10) times the maximum concentration value reported for that pollutant in the permit
application.
The permittee shall continually evaluate all wastewater disposal alternatives and pursue the most
environmentally sound alternative of the reasonably cost effective alternatives. If the facility is in
substantial non-compliance with the terms and conditions of the NPDES permit or governing rules,
regulations or laws, the permittee shall submit a report in such form and detail as required by the
Division evaluating these alternatives and a plan of action within sixty (60) days of notification by the
Division.

M
1
Part III Permit No. NCO005169 I
i
E. ACUTE TOXICITY PASS/FAIL PERMIT LIMIT (QUARTERLY)
The permittee shall conduct acute toxicity tests on a -quarterly basis using protocols defined in the North
Carolina Procedure Document entitled "Pass/Fail Methodology For Determining Acute Toxicity In A
Single Effluent Concentration." The monitoring shall be performed as a Daphnia pulex 24 hour static test,
using effluent collected as a 24 hour composite. The effluent concentration at which there may be at no
time significant acute mortality is 90 % (defined as treatment two in the North Carolina procedure
document). Effluent samples for self -monitoring purposes must be obtained during representative effluent
discharge below all waste treatment. The first test will be performed after thirty days from the effective
date of this permit during the months of February, May, August, and November. {
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the month in which it was performed, using the parameter code TGE6C.
Additionally, DWQ Form AT-2 (original) is to be sent to the following address:
Attention: Environmental Sciences Branch
North Carolina Division of
Water Quality
4401 Reedy Creek Road
Raleigh, N.C. 27607
Test data shall be complete and accurate and include all supporting chemical/physical measurements
performed in association with the toxicity tests, as well as all dose/response data. Total residual chlorine
of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of
the waste stream.
Should any single quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring
will begin immediately until such time that a single test is passed. Upon passing, this monthly test
requirement will revert to quarterly in the months specified above.
Should any test data from either these monitoring requirements or tests performed by the North Carolina
Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened
and modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control
organism survival and appropriate environmental controls, shall constitute an invalid test and will require
immediate retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will
constitute noncompliance with monitoring requirements.

PART IV
ANNUAL ADMINISTERING AND COMPLIANCE MONITORING FEE REQUIREMENTS
A. The permittee must pay the annual administering and compliance monitoring fee within 30
(thirty) days after being billed by the Division. Failure to pay the fee in a timely manner in
accordance with 15A NCAC 2H .0105(b)(4) may cause this Division to initiate action to
revoke the permit.

State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
DEHNR
DIVISION OF WATER QUALITY
October 4, 1996
Mr. Paul Schroeder
FMC Corporation - Lithium Division
Post Office Box 795
Highway 274
Tryon School Road
Bessemer City, North Carolina 28016
Subject:
Dear Mr. Schroeder:
r
NPDES Permit No. NCO05169
Hallman Beam Mine
Gaston County, NC
Our records indicate that NPDES Permit No. NCO05169 was issued
on September 30, 1996 for the discharge of wastewater to the
surface waters of the State from your facility. The purpose of
this letter is to advise you of the importance of the Permit and
the liabilities in the event of failure to comply with the terms
and conditions of the Permit. If you have not already done so, it
is suggested that you thoroughly read the Permit. Of particular
importance are Pages 4-5.
Pages 4-5 set forth the effluent limitations and monitoring
requirements for your discharge. Your discharge must not exceed
any of the limitations set forth. The section headed "Monitoring
Requirements" describes the measurement frequencies, sample types
and sampling locations. Upon commencement of your discharge (or
operation), you must initiate the required monitoring. The
monitoring results must be entered on reporting forms furnished or
approved by this Agency. If you have not received these forms,
they should be arriving shortly. If you fail to receive the forms,
please contact this Office as quickly as possible. I have enclosed
a sample of the "Effluent" reporting form (DEM Form MR-1), plus
instructions for completing the form. It is imperative that all
applicable parts be completed, and the original and one copy be
submitted as required.
Please be advised that an annual administering and compliance
monitoring fee may be required for your facility. You will soon be
receiving a statement from our Raleigh Office. It is imperative
that the fee be paid in a timely manner so as to prevent
enforcement action or possible revocation of your permit.
919 North Main Street, 4 FAX [phone]
Mooresville, North Carolina 28115 C An Equal Opportunity/Affirmative Action Employer
Voice 704-663-1699 1. ITr am. - 500% recycled/l0% post -consumer paper

Mr. Paul Schroeder
October 4, 1996
Page Two
The remaining Parts of the Permit set forth definitions,
general conditions and special conditions applicable to the
operation of wastewater treatment facilities and/or discharge(s).
The conditions include special reporting requirements in the event
of noncompliance, bypasses, treatment unit/process failures, etc.
Also addressed are requirements for a certified wastewater
treatment plant operator if you are operating wastewater treatment
facilities. Any changes in operation of wastewater treatment
facilities, quantity and type of wastewater being treated or
discharged, expansions and/or upgrading of wastewater treatment
facilities must be permitted or approved by this Agency.
Failure to comply with the terms and conditions of an NPDES
Permit subjects the Permittee to enforcement action pursuant to
Section 143-215.6 of the North Carolina General Statutes. A civil
penalty of up to $10,000 per violation (and/or criminal penalties)
may be assessed for such violations. If you find at any time that
you are unable to comply with the terms and conditions of the
Permit, you should contact this Office immediately. A Consent
Order may be necessary while pursuing action to obtain compliance.
As a final note, an NPDES Permit is normally issued for a
five-year period. Permits are not automatically renewed. Renewal
requests must be submitted to this Agency no later than 180 days
prior to expiration. Please make note of the expiration date of
your Permit. This date is set forth on Page 1 of the Permit. Also
note that NPDES Permits are not automatically transferable. If
you, as the Permittee, cease to need this Permit, then you should
request that the Permit be rescinded or transferred to another
party, if necessary.
As mentioned previously,
advise you of the importance of
Permit and contact this Office
you have any questions or need
providing any assistance.
Enclosure
DRG:ls
the purpose of this letter is to
your NPDES Permit. Please read the
at 704/663-1699 in Mooresville if
clarification. We look forward to
Sincerely,
VD. Rex AGeason, P. E.
Water Quality Regional Supervisor

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Ms. Barbara E. Ritchie
Environmental Manager
FMC Corporation, Lithium Division
Highway 161
Box 795
Bessemer City, North Carolina 28016
Dear Ms. Ritchie:
l(PI"
OEHNR
April 15, 1996
N.C. DEPT. OF
� MRONMENT, TIF, ^ r.rt;
LY tiATURAL REgr?t i r l
(L c
OR 17 11996 7,
ON 64F EMMENTAL MANAGEMENT
N01811VUEAE61OAAL OFFICE
Subject: Permit Renewal Acknowledgment
NPDES: NC0005177
FMC Corp., Lithium Division
Gaston County
This letter is to acknowledge receipt of your request for a permit renewal for NPDES Penn::
No. 1•N'C0005177 and fee of $300.00 received April 4, 1996.
I aril, by copy of this letter, requesting that our Regional Office Supervisor prepare a staff
report and recommendations with regard to this discharge.
You will be advised of any comments, recommendations, questions or other information
necessary for the review of the application. If you have questions regarding this renewal, please
contact me at [phone] ext. 516.
Sincerely, 7
Steven D. Pellei
Environmental Engineer, NPDES Group
cc:
Permits and Engineering Unit/Permit File
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

STANDARD FORM C - MANUFACTURING AND COMMERCIAL
SECTION II. BASIC DISCHARGE DESCRIPTION
s to municipal sewerage systems In
Complete this section for each discharge Indicated In Section I, Hems 9,r to belnntgghat Is to surface waters This Includes dischargIlls must be es described
which the ywater does not
watrged to surface waters. Discharges to w4
enofroom this a treatment works facility. SEPARATEbDESCRIAP ONS OF EACH DISCHARGE ARE R IRED EVEN IFS VERAL DI CHA DISCHARGES
also dischargesshould be reprosentatNe of " twelve previous months of operation. I this Is a proposed
ORIGINATE IN THE SAME FACILITY. All values for an existing discharge
discharge, values should rotted best engineering estimates.
ADDITIONAL TINS OUT THESE RUCTIONS ORS LECTED ITEMS APPEAR IN SEPARATE INSTRUCTION BOOKLET AS INDICATED. REFER TO BOOKLET
BEFORE FILLING
1' Serial No and
a Discharge Serial No. Name
201a
(see instructions)
b. Discharge Name
201b
Give the name of discharge, if
any (see instructions)
c. Previous Discharge Serial No
201c
If a previous permit
application was made for this dis
charge (Item 4, Section 11 provide
previous discharge serial
number.
2 Discharge Operating Dates
a Discharge Began Date
2
If the discharge described below
is in operation, give the date
(within best estimate) the
discharge began
b. Discharge to Begin Date
202b
If the discharge has never
occurred but is planned for some
future date, give the date the
discharge will begin.
c. Discharge to End Date If the
202C
discharge is scheduled to be
discontinued within the next 5
years, give the date (within best
estimate) the dscharge will and.
3 Engineering Report Available
Check if an engineering report is
available to reviewing agency
upon request (see instructions)
203
4. Discharrgge Location Name the
political within which
the point of dsdmig. is located:
State
204a
County
204b
(If applicable) City or Town
204c
5 Discharge Point Description
(see instructions)
Discharge into (check one)
Stream (includes ditches, arroyos,
205a
and other watercourses
take
Ocean
Municipal Sanitary Wastewater
Transport System
Municipal Combined Sanitary
and Storm Transport System
001
Discharge from Lower Pond
001 / NPDES Permit NC0005177
1954 Plant Discharge Began
1971 Lower Pond Dam Constructed
YR MO
YR MO
0
Agency_ Use
North Carolina 204d
Gaston 234e
Near Bessemer City 204f
USTR
❑LKE
❑ OCE
(] MTS
0 MCS

Municipal Stone Water Transport
System
Well (injection)
Other
tf'othee is checked, specify type
6. Discharge Point - Iat/lnng.
Give the pprecise location of the
paint of discharge to the nearest
second.
latitude
Longitude
7. Discharge Receiving Water Name
Name the waterway at the point of
discharge. (see instructions)
If the discharge is through an outfa9 that extends
beyond the shoreline or is below the mean low
water line, complete item S.
a? A2aUse ..
N!&� wz I Sub
ForAoen Use
8. Offshore Discharge
a Discharge Distance from Shore
b. Discharge Depth Below Water
9 Discharge Type and Occurrence
a Type of Discharge Check
whether the discharge is
continuous or intermittent
(See instructions)
b. Discharge Occurrence Days
per Week. Enter the average
number of days per week
(during periods of discharge)
this discharge occurs.
c. Discharge Occurrence- Months
If this discharge normally oper-
ates (either intermittently or
continuously) on less than a yea
around basis (excluding shut-
downs for routine maintenance)
check the months during the yet
when the discharge is operating
(see instructions)
Complete Items 10 and 11 if 'intermittent' is
checked in Item 9.a. Otherwise, proceed to
Item 12
10. Intermittent Discharge Quantity
State the average volume per dis-
charge occurrence in thousands of
gallons
11. Intermittent Discharge Duration
and Frequency
a Intermittent Discharge Duration
Per Day State the average
numberof hoursperday the
discharge is operating
b. Intermittent Discharge
Frequency State the average
number of discharge occurreno
per day during days when
discharging
12 Maximum Flow Period Give the
time period in which the maximum
flow of this discharge occurs
DISCHARGE SERIAL NUMBER
001
p STS
p WEL
p OTH
i
206a 35 DEG. 16 MIN. SEC
206b 81 DEG. 18 MIN. SEC
207a Unnamed tributarizto
Ahp nath3,z Crpoll
2M
1 X7c 1
20Ba
feet
2pgb
feet
209a
® (con) Continuous
p (int) Intermittent
2pgb
7 days per week
209c
® JAN ® FEB]
MAR
© APR ® MAY
JUN
® JUL ® AUG]
SEP
® OCT ® NOV
DEC
210
thousand gallons per
day
21la
cum per day
211b
discharge occurrences per day
Flow is generally
212
From to
month month
constant.

I& Activity Description Give a 213a
narrative description of activity
producing this discharge (see
instructions)
DISCHARGE SERIAL NUMBER
001
Manufacturing and processing of inorganic
chemicals, primarily lithium and—UMPounds.
Manufacture and prOCess nQ of oreanlc
chemical primarilynrganolitbi„ma and derivatives.
a
Dom sti l
RpwngP treAmPnfi_
Steam / Electric cogeneration utility boilers.
Research and Development actMrieR_
Stormwater runoff,
14. Activity Causing Discharge For each SIC Code which
describes the activity causing this discharge, supply the
type and maximum amount of either the raw material
consumed (Item 14a) or the product produced (Item 14b)
in the units s fled in Table 1 of the Instruction Booldet.•
For SIC es not fisted in Table I, use raw material or
production units normally used for measuring production
(see instructions)
a Raw Materials
h Products
21
n
(*) A portion of the Industrial Inorganic Chemical manufacture includes
the manufacture of Lithium Carbonate, subject to the Categorical
Effluent Standard at 40 CFR 415.450 et. seq. (Subpart AS)
(**) A portion of the Industrial Organic Chemical manufacture includes
expansion anticipated within the next five years.

1s Waste Abatement
a Waste Abatement Practices
Describe the waste abatement
practices used on this dis-
charge with a brief narrative
(see instructions)
b. Waste Abatement Codes
Using the codes listed in Table
II of the Instruction Booklet
describe the waste abatement
processes for this discharge in
the order in which they occur
if possible.
DISCHARGE SERIAL NUMBER
001
215a Narrative• Wastewaters are recovered and rP1lCP(1.
LiCl process wastewaters are recovered via
reverse osmosis Domestic sewage is treated
in package biological treatment units.
Process waters are neutralized, as reauired,
and equalized in the Lower Pond.
Hypochlorite wastewaters are treated with
hydrogen peroxide prior to discharge.
215b (1) RECOVE (2) RECYCL (3)
(4) (5) (6)
(71 ESEGRE (g) MREVER (g)
0 BAGS—(11) (12)
(13) (14) (15)
(16) 07) (18)
(19) rNEU13 (20) PEQUAL (21)
(�) (23) (24)
(25) COTHER (H2O2 treatment)

DISCHARGE SERIAL NUMBER
001
16. Wastewater Characteristics
Check the box beside each constituent which is present in the effluent (discharge Ovate rj. This determination is to be
based an actual analysis or best estimate.(see instructions)
Specify substances, compounds and/or elements in Item 26 _
in n
tal Protection Agency,
Pesticides (insecticides, fungicides, and rodenticides) must be reported in terms of the acceptable common names Washington, ingto 20250, June 97Z as
and Chemicat names /orOe in redfent Statement on PesBdde Labels'. 2nd Edition, Environmen
required by Subsection 162.7(b) of the Regulations for the Enforcement of the Federal Insecticide, Fungicide, and Rodenticide Act.
x = present
A - Absent
ND = Not detected; see attached analytical report
* = Reported as present in attached analytical report; re -testing has been initiated.

ond-
c iv:
umhi
DISCHARGE SERIAL NUMBER
001
17. Description of Intake and Discharge a
For each of the parameters listed below, enter in the appropriate box the value or code letter answer called for (see instructions)
In adddon, enter the parameter name and code and all required values for any of the following parameters I they ere checked in Item 16:
ammonia, cyanide, aluminum, arsenic, beryllium, cadmium, chromium, copper, lead mercury, nickel, selenium, zinc, phends, oil and grease, and
chlorine (residual).
Innuent
Effluent
Parameter and Code
Untreated
Intake
n-
Treated
ar y
Average
minimum
Value
maximum
Value
mquencyr
of Analysis
Numbero
Analyses
5ample
Type
Water
Intake
Observed or
Observed or
217
(Daily
Water
Expected
Expected
average)
(Daily
During
During
average)
Discharge
Discharge
Activity
Activity
1)
2)
(3
4
(5)
(6)
(7)
8
0.504
0.622
Contin
ously
Gallon°Nr
00056 per day
0056
----
----
MGD
0
MGD
Mon'
tored
P
Units
00400
----
----
7.2
8.5
1 /wk
104
Grab
Temperature (venter)
OF
----
----
48
36
64
1/wk
52
Grab
74028
Temperature (summer)
OF
----
----
73
57
84
1/wk
52
Grab
74W
Biochernmal Oxygen
Demand
----
----
3.0
42.0
6.0
1/mon
27
Grab
(800 5-Day)
mgA
00310
—Chemical xygen
permit
Demand (COD)
—__—
_---
---_
28
28
renewal
1
Grab
m gn
00340
—ToW 6uspenced
(nonfilterable) Solids
MgA
005M
----
----
5.0
L1
8
2/mon
54
Grab
.tyiicromhosbnzt45t2x
----
----
1,400
2,100
1 /wk
104
Grab
Sealeaole Manor
(residue)
----
----
__--
BDL
BDL
permit
1
Grab
MIA
00545
renewal
Other discharges sharing intake flow (serial numbers) (see instructions)
.I
(11/1 — 4/30)
(5/1 — 10/30)
—DATA COLLECTED DURING TERM OF CURRENT PERMIT (3/1/94 through 3/1/96) PRESENTED HERE.
—Current NPDES permit requires collection of conductivity, not specific conductance
—BDL - Below detection limit; see attached analytical report.

r
r�n:r_caactynty��
17. (Contd)
parameterand Code
217 See Notes
Below
Bromodichlormethane
Dibromochloromethane
Bromoform (u /1
Chloroform (ug/1)
chromium (m /1
copper (mg/1)
Ammonia NH -N m
DISCHARGE SERIAL NUMBER
001
InIluerit
en
n
Intake
n
Treated
ar y
Average
minimum
Value
maximum
Value
of Analysis
Number
of
bamPle
Type
Water
Intake
Observed or
Observed or
Analyses
(Daily
average)
Water
(Daily
ExpectedExpected
During
t .
During
average)
Discharge
Discharge
activity
Activity8)
7
8)
(1
2)
3
-----
---
1.8
c'1.0
3.5
1 mon
27
rab
!Grab
-----
-----
2.5
41.0
4.0
1/mon
27
Grab
-----
-----
4.0
.C1.0
10.0
1 mon
27
-----
-----
3.0
41.0
5.3
1/mon
27
Grab
-----
-----
0.012
40.005
0.022
1/mon
1 27'
Grab
-----
-----
0.003
<0.002
0.010
1/mon
27
1
Grab
-----
1.0
4 0.10
4.0
1/mon
27
Grab
-_--_
n nt"I
1 /Tnnn
27
Grab
Zinc (mg/1) ----- ----- 0.024 < 0.010
18. plant Controls Check if the following
plant controls are available for this �8
discharge
Altemate power source for major
pumping facility ❑ APS
Alarm or emergency procedure for
power or equipment failure ❑ ALM
Complete Item 19 if discharge is tmrr
cooling andtor steam water
generation and water treatment
additives are used
19. Water Treatment Additives If the
discharge is treated with any
conditioner, inhibitor, or algrcide,
answer the following:
(ug/1)
(ug/1)
(ug/1)
(ug/1)
(mg/ 1)
(mg/1)
(mg/1)
(mg/1)
a. Name of Materials) 219a SEE ATTACHMENT 6 - WATER TREATMENT CHEMICALS
b. Name and address of
manufacturer
c, Quantity (pounds added per
million gallons of water treated)
219b
I 219c
_DATA COLLECTED RUING TERM OF CURRENT PERMIT (3/l/94 — 3/1/96) PRESENTED HERE.
_ AS WITH MONTHLY DISCHARGE MONITORING REPORT INSTRUCTIONS, AVERAGE VALUES
DO NOT INCLUDE RESULTS REPORTED AS BELOW DETECTION LIMIT.

d Chemical oomposition of these I
219d
ee I
additives (sinstructions)
Complete Items 20-251 there is a thermal discharge
(e.g., associated with a steam and/or power generation
plant, steel mill, petroleum refinery, or any other
manufacturing process) and the total dscharge flow is
10 million gallons per day or more. (see instructions)
20. Thermal Discharge Source -Check 220
the appropriate hem(s) indicating
the source of the discharge (see
instructions)
Boiler Slowdown
Boiler Chemical Cleaning
Ash Pond Overflow
Boiler Water Treatment -
Evaporator Slowdown
Oil and Coal Fred Plants -Effluent
from Air Pollution Control Devices
Condense Cooling Water
Cooling Tower Slowdown
Manufacturing Process
Other
21. Discharge/Receiving Water
Temperature Difference
Give the maximum temperature
difference between the discharge
and receiving waters for summer
and winteroperating conditions
(see instructions)
ummer 221a
Winter 221b
22. Discharge Temperature, Rate of 222
Change Per Hour
Give the maximum possible rate of
temperature change per hour of
discharge under operating
conditions (see instructions)
23. Water Temperature, Percentile
Report(Frequency of Occurrence)
In the table below, enter the
temperature which is exceeded 10%
of the year, 5°/a of the year, 1 % of
the year and not at all (maximum
yearty temperature). (see
instructions)
Frequency of occurrence
a. Intake Water Temperature 223a
(subject to natural changes
b. Discharge Water Temperature 223b
24. Water Intake Velocity 224
(see instructions)
25. Retention Time Give the length of 225
time, in minutes, from start of
water temperature rise to discharge
of cooling water. (see instructions)
DISCHARGE SERIAL NUMBER
001
BLBD
0 BCCL
APOF
❑ EPBD
0 OCFP
s
[d COND
p CTSD
MFPR
OTHR
OF
OF
°Ffiour
t /Y
%
t o
axrmu
OF
.F
OF
OF
OF
OF
OF
OF
feetfsec.
minutes
a

H AU
DISCHARGE SERIAL NUMBER
26. AdcftrsW Information

P
STANDARD FORM C - MANUFACTURING AND COMMERCIAL
SECTION II. BASIC DISCHARGE DESCRIPTION
In
Complete this section for each discharge Indicated In Section 1. Items 9,r to ntghat Is to aurtacs waters This includesdischargesto wells
to must
bemunicdescribed where there al sewerage systems a
Which tM s tosurfacewaters from this faeHlty. SEPARATE a treatment works DESCRIed to surface wat*n
PT ONS OF EACH DISCHARGE ARE REQUIRED EVEN S SEVERAL DISCHARGES
Is a proposed
�
also discharg should be representative of tt» twelve previous months of opsration. a this Is a proposed
ORIGINATE IN THE SAME FACILITY. All values for an existing discharge
discharge, values should reflect best engineering estimates.
BEFORE FAWNG ORUT THESE IF'OfEM ELECTED ITEMS APPEAR IN SEPARATE INSTRUCTION BOOKLET AS INDICATED. REFER TO BOOKLET
t. Serial No and
a Dischischarge Serial No. Name
(see instructions)
b. Discharge Name
Give the name of discharge, if
any (see instructions)
c. previous Discharge Serial No
If a previous permit
application was made for this cgs
charge (Item 4, Section 1) provide
previous discharge serial
number.
2 Discharge Operating Dates
a Discharge Began Date
If the discharge described below
is in operation, give the date
(within best estimate) the
discharge began
b. Discharge to Begin Date
If the discharge has never
occurred but is planned for some
future date, give the date the
discharge will begin.
c. Discharge to End Date If the
discharge is scheduled to be
discontinued within the next 5
years, give the date (within best
estimate) the discharge will end.
3. Engineering Report Available
Check if an engineering report is
available to reviewing agency
upon request (see instructions)
4, Discharrgge Location Name the
politicalboundaries within which
the point of discharge is boated:
State
County
(If applicable) City or Town
5, Discharge Point Description
(see instructions)
Discharge into (check one)
Stream (includes ditches, arroyos,
and other watercourses
lake
Ocean
Municipal Sanitary Wastewater
Transport System
Municipal Combined Sanitary
and Storm Transport System
201a
201b
2D1c
202b
202c
Toe Drain Discharge
Discharge from Toe Drain in Lower Pend Dam
Associated with Outfall 001 / NPDES No. NC0005177
Plant Operations Began 1954
Lower Pond Dam Constructed 1971
YR MO
YR MO
IN
North Carolina 2�4d
Gaston 204e
Near Bessemer City 2041
® STR
❑ LKE
OCE
NITS
MCS
Agency Use

FA
Municipal Storm Water Transport
System
Well (injection)
Other
ff'othee is checked, specify type
Discharge Point - LattLong.
Give the precise location of the
point of discharge to to nearest
second.
Latitude
Lon&de
7. Discharge Receiving Water Name
Name the waterway at the point of
discharge. (see instructions)
ff the discharge is through an outfall that extends
beyond the shoreline or is below the mean low
water line, complete hem 8,
I sub
In
For Aa*mev Use
& Offshore Discharge
a. Discharge Distance from Shore
b. Discharge Depth Below Water
9 Discharge Type and Occurrence
a. Type of Discharge Check
whether the discharge is
continuous or intermittent
(See instructions)
b. Discharge Occurrence Days
per Week. Enter the average
number of days per week
(during periods of discharge)
this discharge occurs.
c. Discharge Occurrence- Months
If this discharge normally oper-
ates (either intermittently or
continuously) on less than aye
around basis (excluding shut-
downs for routine maintenance),
check the months during the yea
when the discharge is operating
(see instructions)
Complete Items 10 and 11 If 'intermittent' is
checked in Item 9.a. Otherwise, proceed to
Item 12.
10. Intermittent Discharge Quantity
State the average volume per dis-
charge occurrence in thousands of
gallons
it. Intermittent Discharge Duration
and Frequency
a Intermittent Discharge Duration
Per Day State the average
number of hours per day the
discharge is operating
b, Intermittent Discharge
Frequency State the average
number of discharge occurrana
per day during days when
discharging
12. Maximum Flow Period Give the
time period in which the maximum
flow of this discharge occurs
r_ _07"
208a
208b
M
M
2090
210
211a
211b
212
DISCHARGE SERIAL NUMBER
- Top Drain nischarge
STS
0 WEL
C] OTH
15
DEG.
_ 16 _MIN.
_JSEC
81
DEG.
tributary
_1.8
MIN.
to
SEC
Unnamed
Abernathy
Creek
Jeet
Jeet
(con) Continuous
(Int) Intermittent
I_days perweek
JAN
Z FEB
MAR
APR
MAY
JUN
E@ JUL
AUG
SEP
@ OCT
NOV
DEC
thousand gallons per day
ours perday
_discharge ocou rrenoes per day
From - to
month month Flow is relatively
constant.

P,
AUhN(.;Y W
DISCHARGE SERIAL NUMBER
Toe Drain Discharge
13. Activity Description Give a 213a Drainage from _'F-rgjnPP-rjng s*sXzm—
narrative description of activity inherent
producirig this discharge (see in dam c ngt-ruct-ion T-war P
cjj-,rhnrcrPe3 vi-a outfall (2-epsg
instructions) e
dA :6
io i� 8 44r��
through the Toe Drain and-di-Srh-qrged
Via the Toe Drain nisrbarge-
14. Activity Causing Discharge For each SIC Code which
describes the activity causing this discharge, supply the
type and ma)dmum amount of either the raw material N/A See Outfall 001 otherwise
consumed (Item 14a) or the product produced (Item 14b) associated with Lower Pond Dam.
in the units specified. in Table I of the Instruction Booldet.
For SIC Codes not fisted in Table 1, use raw material or
production units normally used for measuring production
(306 Instructions)
a Raw Materials
b. Products
1 Wt Shared Discharges
n

1s Waste Abatement
a Waste Abatement Practices
Describe the waste abatement
practices used on this dis-
charge with a brief narrative
(see instructions)
b. Waste Abatement Codes
Using the codes listed in Table
II of the Instruction Booklet,
describe the waste abatement
processes for this discharge in
the order in which they occur
if possible.
DISCHARGE SERIAL NUMBER
TnP Drain III charge
215a I Narrative
215b (1) -
(2) 131
I (4)
(5) (6)
(7)
(6) (9)
(13)
(14) f15)
(16)
0 1 08)
(19)
(20) (21)
(22)
(23) (24)
(2

r
DISCHARGE SERIAL NUMBER
Toe Drain Discharge
16. Wastewater Characteristics
Check the box beside each constituent which is present in the effluent (discharge water). This determination is to be
based on actual analysis or best estimate.(see instructions)
arameter
Present
arameter
Present
216
216
Color
00080
x
01042 r
ND
onia
r0n
01045
00610
�icro n
5
x
Lead
01051
A
gnesium
X
Nitrate
00620
rk 7
A
�itnte
ime
00615
Phos
00665Molybdenum
rcury�°�xA
71900
Sultale
00945
x
01052
bultide007450107
x
ice
A
-Selenium
rite
01147
00740
A
romiae
x
ever
01077
A
711870
x
Potassium
X
Chloride
00940
37
009ru
ism
anioe
00720
A
00929
muon e
x
Thallium
01059
A
00951
uminum
i ism
01105
Antimony
A
Tin
01102
A
01097
nc
X
rsenic
01092
01002
-Beryllium
gig s
A
74051
01012
-Banum
A
Chlorinated organic compou
A
74052
01007
Pesticides'
non
A
74053
boron
Oil and grease
A
Cadmium
x
00550
01007
A
icium
lnrm
00916
is
A
3g'reo
A
01037
Total residual
-1: A
Chromium
5=
01034
I Hadioactiviry
Fecal i orm bacteria
A
174050
74055
Specify substances, compounds and/or elements in ftem 26. CommNames
Pesticides (insecticides, fungicides, and rodentiades) must be reported in terms of the acceptable common names specified � Juneon 1972, as
and chemical names lorMe In relent StatemWashington,
on Fesdafde Labels, 2nd Edition, Environmental Protection Agency,
required by Subsection 162.7(b) of the Regulations for the Enforcement of the Federal Insecticide, Fungicide, and Rodenticide Act
Characterization is based on relation of this stream to Outfall 001 and
its characterization, supplemented by limited chemical analyses.
x = present
A - Absent
ND = Not detected in laboratory analysis; see attached report.

■tee :I_<<1a►[el'L�b'f�
DISCHARGE SERIAL NUMBER
Toe Drain Discharge
17. Description of Intake and Discharge a
For each of the parameters fisted below, enter in the appropriate box the value or code letter answer called for (see instructions)
In addition, enter the parameter name and code and a9 required values for any of the following parameters it they era checked in Item 16:
ammonia, cyanide, aluminum, arsenic, beryllium, cadmium, chromium, copper, lead, mercury, nickel, selenium, zinc, phenols, o7 and grease, and
chlorine (residual).
Influent
hmuent
Parameter and Code
Untreated
Intake
n-
Treated
at y
Average
Minimum
Value
Maximum
Value
Frequency
of Analysis
Numberoi
Analyses
bample
Type
Water
Intake
Observed or
Observed or
217
(Daily
average)
Water
(Daily
Expected
During
E�ted
During
average)
Discharge
Discharge
Actim
Activity
1)
2)
(3
4
(5)
(6)
(7)
6)
Flow'
Gallons per day
00056
_____
___--
4,00
4?000
8,000
Estimated
P
Units
00400
_
_____
6.0
9.0
Estim
ted
--Temperature (winter)
OF
— __--
—----
Ambient
74026
Temperature (summer)
OF
-----
-----
Ambient
74027
-Biocriemcial Oxygen
Demand
(BOD 5-Day)
-----
-----
mgA
03310
--Chemical Oxygen
Demand (COO)
-----
-----
mg/I
00340
otar spenoed
(nonfilterable) Solids
-----
_____
12
12
ermit
1
Grab
mg/I
00530
Renewal
--Specific Conductance
micromhos/crn at 25°C
—Seftlearile Matter
(residue)
MIA
00545
Other discharges sharing intake flow (serial numbers) (see instructions)

T
DISCHARGE SERIAL NUMBER
Tne nrain Discharge
(ruonra)
ParameterandCode
217
Zinc m 1
Influent
en
i
n
Intake
Water
(Daily
average)
(1(2)
-------
n- an
Treated
Intake
Water
(Dail
avverage)
-----
ar y
Average
3
--
inimum aximum
Value Value
Observed or Observed or
x Expected
Expected
During During
Discharge Discharge
activity 5 tivity
—Permit
requenry
ofAnafysrs
(61
renewal
um er
d
Analyses
7
1
e
Type
8)
Grab
18. Plant Controls Check if the following
plant controls are available for this
discharge
Attemate power source for major
pumping facility
Alarm or emergency procedure for
power or equipment failure
Complete Item 19 if discharge is frorr
coding and/or steam water
generation and water treatment
additives are used
19. Water Treatment Additives If the
discharge is treated with any
conditioner, inhibitor, oralgrcide,
answer the following:
a Name of Materials)
b. Name and address of
manufacturer
C. Quantity (pounds added per
million gallons of water treated)
218
APS
�] ALM
N/A
219a
219b
2190
E

d Chemical composition of these i
219d I
additives (see instructions)
Complete Items 20-25 if there is a thermal discharge
(e.g., associated with a steam and/or power generation
plant, steel mill, petroleum refinery, or any other
manufacturing process) and the total discharge flow is
10 million gallons per day or more. (see instructions)
20. Thermal P h� So umea tineck M
the approthe source of the discharge (see
instructions)
Boiler Blowdown
Boiler Chemical Cleaning
Ash Pond Overflow
Boiler Water Treatment -
Evaporator Blowdown
Oil and Coal Fred Plants -Effluent
from Air Pollution Control Devices
Condense Cooling Water
Cooling Tower Blowdown
Manufacturing Process
Other
21. Discharge/Reosiving Water
Temperature Difference
Give the maximum temperature
difference between the discharge
and receiving waters for summer
and winteroperating conditions
(see instructions)
Summer 221a
Winter 221b
22 Discharge Temperature, Rate of
Change Per Hour 222
Give the maximum possible rate of
temperature change per hour of
discharge under operating
conditions (see instructions)
23. Water Temperature, Percentile
Report(Frequency of Occurrence)
In the table below, enter the
temperature which is exceeded 10%
of the year, S% of the year, 1 % of
the year and not at all (maximum
yearly temperature). (see
instructions)
Frequency of occurrence
a. Intake WaterTemperature 223a
(subject to natural changes
b. Discharge Water Temperature 223b
24. Water Intake Velocity 224
(see instructions)
25. Retention Time Give the length of 225
time, in minutes, from start of
water temperature rise to discharge
of cooling water. (see instructions)
DISCHARGE SERIAL NUMBER
Toe Drain Discharge
BLBD
BCCL
APOF
EPBD
OCFP
[� COND
CTSD
MFPR
OTHR
'F
'F
°FJhour
.r
1 /o
/.
1%
axrmum
.F
OF
OF
OF
OF
OF
OF
OF
teel/sec.
minutes
e

m I
H AU N%.,T WQr.
DISCHARGE SERIAL NUMBER
25. Addfional Infomiation
Tna n—i-a DLscharge

STANDARD FORM C - MANUFACTURING AND COMMERCIAL
SECTION 11. BASIC DISCHARGE DESCRIPTION
Is 10 tems In
Complete this section for each discharge Indicated In Section I. Items
bel that
dtiseharged tosurfacewaters. Discharges watem This Includes to r�reeitstmust beddescribed al where there are
GES
Which the waste water does not go through a Vestment works prior nnggOF EACH
also discharges to surface waters from this IacUtry. SEPARATE DESCRge should d be representat DISCHARGE
the twelve prseloous months of ops2U�on. Da thins Is proposed
ORIGINATE IN THE SAME FACILITY. Ali values for an existing discharge
discharge, values should reflect best engineering estimates.
ADDITIONAL
FAWNG ORUCTIONS UT THESE ITEMS.
SELECTED
�S APPEAR IN SEPARATE INSTRUCTION BOOKLET AS INDICATED. REFER TO BOOKLET
1, Discharge Serial No. and Name
a Discharge Serial No.
(see instructions)
b. Discharge Name
Give the name of discharge, if
any (see instructions)
c. Previous Discharge Serial No
If a pprevious permit
application was made for this dis
charge (Item 4, Section 1) provide
previous discharge serial
number.
2 Discharge Operating Dates
a Discharge Began Date
If the discharge described below
is in operation, give the date
(within best estimate) the
discharge began
b. Discharge to Begin Date
if the discharge has never
occurred but is planned for some
future date, give the date the
discharge will begin.
c. Discharge to End Date If the
discharge is scheduled to be
discontinued within the next 5
years, give the date (within best
estimate) the discharge will end.
g, Engineering Report Available
Check if an engineering report is
available to reviewing agency
upon request (see instructions)
4. Discharge Location Name the
political boundaries within which
the point of discharge is located:
State
County
(if applicable) City or Town
g, Discharge Point Description
(see instructions)
bischarge into (check one)
Stream (includes ditches, arroyos,
and other watercourses
Lake
Oman
Municipal Sanitary Wastewater
Transport System
Municipal Combined Sanitary
and Storm Transport System
201a 1 004 —
201b
201c
202a
202b
202c
Discharge from Western Canal System
__924_L NPDES Permit No. NCS000002
1954 Plant Discharge Began
—t9/r' I wen Pond Dam Constructed
1978 Western Canal System Constructed to divert
flows around Lower Pond
YR MO
YR MO
D
North Carolina 204d
Gast'nn — 204e
Near Bessemer City - 204f
BSTR
❑ LKE
❑ OCE
MTS
MCS

Municipal Storm Water Transport
System
Well (injection)
Other
rothee is checked, specify type
6. Discharge Point - Lat(Iong-
Give the precise location of the
pant
discharge to the nearest
Latitude
Lon4tuda
7. Discharge Receiving Water Name
Name the waterway at the point of
discharge. (see instructions)
If the discharge is through an outfall that extends
beyond the shoreline or is below the mean low
water line, complete item 8.
r Or Me.. Se
Wei M^yI stA
X. . . . . . . . . . .
1 X7C 1
For Aces Use
& offshore Discharge
a. Discharge Distance from Shore
b. Discharge Depth Below Water
9 Discharge Type and Occurrence
a. Type of Discharge Check
whether the discharge is
continuous or intermittent.
(See instructions)
b. Discharge occurrence Days
per Week. Enter the average
number of days per week
(during periods of discharge)
this discharge occurs.
c. Discharge Occurrence- Months
If this discharge normally oper-
ates (either intermittently or
continuously) on less than a yea
around basis (excluding shut-
downs for routine maintenance),
check the months during the yez
when the discharge is operating
(see instructions)
Complete Items 10 and 11 if 'intermittent' is
checked in Item 9,a. Otherwise, proceed to
Item 12.
10. Intermittent Discharge Ouan
State the average volume per
occurrence in thousands of
gallons
it. Intermittent Discharge Duration
and Frequency
a Intermittent Discharge Duration
Per Day State the average
numberof hours perday the
discharge is operating
b. Intermittent Discharge
Frequency State the average
number of discharge occurrena
ddydg days when
12. Maximum Flow Period Give the
time period in which the maximum
flow Of this discharge occurs
7-9rz .1
206a
M
207a
2M
K- 1.22
210
21 la
211b
212
DISCHARGE �RAL NUMBER
STS
WEL
0 OTH
_2-5DEG. 16 MIN. SEC
_1DEG. _18_MIN. SEC
feet
feet
jgc(oon) Continuous
C] (int) Intermittent
_days perwe k
JAN @ FEB
:aMAR
APR 20 MAY
Q JUN
JUL 2] AUG
Q SEP
OCT ED NOV
E3 DEC
thousand gallons Per day
hours per day
_discharge occurrences per day
Maximum flows occur
From m during heavy storm events.
month month

13. Activity Description Give a 213a
narrative description of activity
producing this discharge (see
instructions)
DISCHARGE SERIAL NUMBER
004
Manufacture and prnrcccing ofxnnz4�nic
chemir 1, nrim ri13� lirhim^ and nm
rpounds.
M fart- ira and nrnraino n_f nr ,�,n�C
rhPmiralg *ri +ti V and
Domestic Serge ire^tment (� narlraap units.)
croam / F1e - ^};^^ "r=lity boilers
14. Activity Causing Discharge For each SIC Code which
describes the activity causing this discharge, supply the
type and maximum amount of either the raw material
consumed (item 14a) or the product produced (Item 14b)
in the units specified in Table I of the Instruction Booldet.-
For SIC Codes not listed in Table I, use raw material or
production units normally used for measuring production
(see instructions)
a. Raw Materials
214
b. Products
SIC Code
214 (t)
2819
2869
Maximum
Name
Ind. Inoraaa-L----ZLd—(±
Ind.Organic 100,000 (
r tnlr
Shared Discharges
Unit Shared Discharges
Table 1) (Serial Number)
on/dav Drain
lb/day�00�1,004,Toe Drain
(*) A portion of the Industrial Inorganic Chemical manufacture includes
the manufacture of Lithium Carbonate, subject to the Categorical
Effluent Standard at 40 CFR 415.450 et. seq. (Subpart AS)
(**) A portion of the Industrial Organic Chemical manufacture includes
expansion anticipated over the next five years.

15 Waste Abatement
a Waste Abatement Practices
Describe to waste abatement
practices used on this dis-
charge with a brief narrative
(see instructions)
b. Waste Abatement Codes
Using the codes listed in Table
II of the Instruction Booklet,
describe the waste abatement
processes for this discharge in
the order in which they occur
if possible.
215a
215b
DISCHARGE SERIAL NUMBER
004
Narrative. Waters are recovered and reused_
West Canal System includes sedimentation
pond and polishing pond.
(1) RF.COVF (2) RECYCL. (3) PSEDTM_
(4) PSEDIM (5) BPOLIS (6)
(7) (8) (9)
(t6) (17) (18)
(19) (20) (21)
(�) (23) (24)
(25)

r.
DISCHARGE SERIAL NUMBER
004
16. Wastewater Characteristics
waie This dejennination is to be
Check the box beside each constituent which is present in the effluent (drscharge �• +
based an actual analysis or best estimate.(see instructions)
- Specify substances, compounds and/or elements in Item 26.
Washington, D.C. 20250, June 197Z as
Pesticides ('insecticides, fungicides, and rodenticdes) must be reported in terms of the acceptable common names specified in Acceptable Common amen
and Chemrcalnames forthe In redOnt Statement on PestSdde Labels, 2nd Edition, Environmental Protection Agency,
required by Subsection 162.7(b) of the Regulations for the Enforcement of the Federal Insectiade, Fungicde, and Rodentiade Act
x = Present
A = Absent
ND = Non detected; see attached analytical report.
* = Reported as present in attached analytical report; re -testing has been initiated.

.P
ondu
tivi
(uhn
DISCHARGE SERIAL NUMBER
004
17. Description of Intake and Dischargs s
For each of the parameters listed below, enter in the appropriate box the value or code letter answer called for (see instructions)
In addtion, enter the parameter name and code and all required values for any of the following parameters it they ere checked in Item 16:
ammonia, cyanide, aluminum, arsenic, beryllium, cadmium, chromium, copper, lead, mercury, nickel, selenium, zinc, phends, of and grease, and
chlorine (residual).
InIluent,
Effluent
Parameter and Code
Untreated
Intake
n-
Treated
of y
Average
Minimum
Value
maximum
Value
requenry
of Analysis
Numbero
Analyses
bample
Type
Water
Intake
Observed or
Observed or
217
(Daily
Water
Expected
Expected
average)
(Daily
During
During
average)
Discharge
Discharge
Activity
Activity
1)
2)
(3
4
(5)
(6)
(7)
8
Flow'
Gallons per day
-----
-----
N/A
0
2.842
Estimated
00056
MGD
P
Units
004M
_____
6.5
8.5
Estim
ted
emperature (winter)
`F
-----
— ----
48
34
66
1/wk
57
Grab
74M
—Temperature (summer)
°F
-----
-----
72
50
91
1/wk
51
Grab
74o27
BK=emcial Uxygen
Permit
Demand
D
(BOD 5-Day)
-----
-----
---
BDL
BDL
Renewal.
1
Grab
mgll
00310
Chemical Oxygen
Demand (COD)
Permit
m9/1
00340
_____
-----
__--
17
17
Renewal.
1
Grab
—Totalspen
(nonCilterable) Solids
Permit
mgA
00530
_____
-----
—__
2
2
Renewal.
1
Grab
t
-----
-----
420
1,100
1/wk
54
Grab
e r
Permit
(residue)
-----
-----
---
BDL
BDL
Renewal.1
Grab
ml�
00545
Other discharges sharing intake flow (serial numbers) (see instructions)
(11/1 — 5/1)
(5/1 — 11/1)
- Data collected druing term of current permit (3/1/94-3/1/96) presented here.
- Current NPDES Permit requires collection of conductivity, not specific conductance.
- BDL= Below Detection limit; see attached analytical report.
- Data collected at a frequency greater than permit renewal has been reported as
upstream data pursuant to NC0005177 requirments.

tiZel: /_le_1a►ty l�l'f �
1
Ammon:
Cyanic
Cadmii
Mercu
Zinc
Chlc
T.D.
DISCHARGE SERIAL NUMBER
00
�, �t;onrafInfluent
parameter and Code
217 See
Notes Below
en
a
Untreatedn
Intake
Water
(Daily
average)
(1
Treated
Intake
Water
(Daily
average)
2)
fai
age
3
inimum
Value
Observed or
F
During
Discharge
activity
MaximValue um
Observed or
� .
During
Discharge
Activity- -
Fr And
6)
m er
Analyses
7
T�5ampe
8)
-----
-----
-----
---
---
0.011
0.011
Permit
Renewal
1
Grab
_a (NH3-N m 1
le mg/1
-----
_____
___
0.002
0.002
1
Grab
>m mg/1
__
0. 0077
1
Grab
_____
____
___
-----
---
0.023
0.023
1•
Grab
mg/1
--
14
487
8
360
20
680
1/mon
1/mon
48
48
Grab
Grab
Retest initiated
is. plant Controls Check if the following
plant controls are available for this 218
d��
Alternate power source for major
.pumping facility ❑ APS
Alarm or emergency procedure for ❑ ALM
power or equipment failure
Complete Item 19 if discharge is frorr
cooling andtor steam water
generation and water treatment
additives are used
19. Water TreatmentAddrtives If the See Attachment 6 — Water Treatment Chemicals
dscharge is treated with any
conditioner, inhibitor, or algicde,
answer the following
a Name of Materials) 219a
b. Name and address of 219b
manufacturer
c, Quantity (pounds added per 219c
million gallons of water treated)
- Data collected during term of current permit (3/1/94-3/1/96) presented here.
- Data collected at a frequency greater than permit renewal has been reproted as upstream
data pursuant to NC0005177 requirements.
0

■gel:/c(eta.[yNt.-t
d Chemical composition of these i
219d I
additives (see instructions)
Complete Items 20-25 if there is a thermal discharge
(e.g., associated with a steam andlor power generation
plant, steel mill, petroleum refinery, or any other
manufacturing process) and the total discharge flow is
10 million gallons per day or more. (see instructions)
20. Thermal Discharge Source -Check 220
the appropriate item(s) indicating
the source of the discharge (see
instructions)
Boiler Slowdown
Boiler Chemical Cleaning
Ash Pond Overflow
Boiler Water Treatment -
Evaporator Blowdown
Oil and Coal Fred Plants-Etfhuent
from Air Pollution Control Devices
Condense Cooling Water
Cooling Tower Blowdown
Manufacturing Process
Other
21. Discharge/Receiving Water
Temperature Difference
Give the maximum temperature
difference between the discharge
and receiving waters for summer
and winter operating conditions
(see instructions)
Summer 221a
Winter 221b
22 Discharge Temperature, Rate of
Change Per Hour 222
Give the maximum possible rate of
temperature change per hour of
discharge under operating
conditions (see instructions)
23. Water Temperature, Percentile
Report(Frequency of Occurrence)
In the table below, enter the
temperature which is exceeded 10'/.
of the year, 5% of the year, 1 % of
the year and not at all (maximum
yearly temperature). (see
instructions)
Frequency of oocurence
a. Intake Water Temperature 223a
(subject to natural changes
b. Discharge Water Temperature 223b
24. Water Intake Velocity 224
(see instructions)
25. Retention Time Give the length of 225
time, in minutes, from start of
water temperature rise to discharge
of cooling water. (see instructions)
DISCHARGE SERIAL NUMBER
004
BLBD
BCCL
APOF
EPBD
OCFP
C] COND
CTSD
MFPR
OTHR
OF
OF
°FJhour
1 /.
/e
1 .
Maximum
OF
.F
.F
OF
OF
OF
OF
OF
feettsec.
minutes
a

FUH AUr-MT W
DISCHARGE SERIAL NUMBER
26. Adclifional information

'J
NORTH CAROLINA DEPT. OF ENVMONMENT, HEALTH, AND NATURAL RESOURCES
ENVIRONMENTAL MANAGEMENT COMMISSION
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
STANDARD FORM C - MANUFACTURING AND COMMERCIAL
i
SECTION I. APPLICATION AND FACILITY DESCRIPTION
Unless otherwise spectiled on this form all items are to be completed. It an Rem Is not applicable Indicate 'NA'.
ADDITIONAL INSTRUCTIONS FOR SELECTED ITEMS APPEAR IN SEPARATE INSTRUCTION BOOKLET AS INDICATED. REFER TO BOOKLET
BEFORE FILLING OUT THESE ITEMS.
Please Print or Type
1. Legal Name of Applicant
101 FMC Corporation
(see instructions)
Lithium Division
2. Mailing Address of Applicant
(see Instructions)
Numbert£ Street
102a Highway 161, Box 795
City
102b Bessemer City
North Carolina
State
102c
Zip Code
102d 28016
3. Applicant's Authorized Agent
(see Instructions)
Barbara E. Ritchie
Nameandrtie
103d
Environmental Manager
Number & Street
103b Highway 161
Box 795
City
103c Bessemer City
sty
103d North Carol i na
ZIP Code
103e 28016
Telephone
103f 704 868-0806
Area Number
4, Previous Application
code
If a previous application for a
a under the National
rpe
Potlutant Discharge Elimination
System has been made, give
the date of application.
104 1991 March 7
YR MO DAY
I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete,
and accurate.
Quentin G. Hopkins 102e Plant Manager
4 Printed Name t Person SI ring Title'Jali.L 102tq(-o
signature o Applicant or uthorized Agent YR MO DAY
Date Application Signed
North Carolina General Statue 143-215.6 (b)(2) provides that Any person who knowingly makes any false statement representation, or certification in any
application, record, report, plan, or other dorxrment files or required to be maintained under Article 21 or regulations of the Environmental Management
Commission implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required
to be operated or maintained un der Article 21 or regulations of the Environmental Management Commission implementing that Article, shall be guilty of a
misdemeanor punishable by a fine not to exceed Siopo0, or by imprisonment not to exceed sit months, or by both. 18 U.S.C. Section 1o01 provides a
punishment by a fine or not more than $10,000 or imprisonment not more than 5 years, or both, for a similar oNense.1

5, Facility (see instructions)
Give the name, ownetshi and
physical location of thttoy plant or
other operating
presently xaiKs)
em
discharge() P
or will occur.
Name
Ownership (Public, Private
or both Pubic and Private)
Check block if a Federal
facility
and give GSA Inventory
Control Number
Location.
Number 3 Street
City
County
State
6. Nature of Business State the nature
of the business conducted at the
plant or operating facility.
7. Facility Intake Water (see
instructions) Indicate water intake
volume per day by sources.
Estimate averagevolume per day
in thousand gans perday.
Municipal or private water system
Surface water
Groundwater
Other'
Total Item 7
If there is intake water from'othee
specify thg source.
8. Facility Water Use Estimate averag4
volume per day in thousand gallons
per day for the following types of
water usage at the facility.
(See instructions)
Noncontact cooing water
Baler feed water
Process water (including contact
cooing water]
Sanitary water
Other'
Total Item 8
If there are discharges to'othee,
specify
If there is'Sanitan/ water
use,
give the number of people
10Eb
105c
to5d
105e
105f
1059
105h
106a
tTsy
107a
107b
107c
107d
107e
1a7f
lo8a
108b
108c
toed
108e
108f
1089
108h
FMC Corporation
Lithium Division
------
Bessemer City Plant i
19PUS PRV 0 aPP
m
Chemical Manufactnring�
Research and Development
AGENCY USE
F7=
737 thousand gallons per day
thousand gallons per day
thousand gallons per day
284Z _thousand gallons per day
3579 thousand gallons per day
Sto-rmwater
188 thousand gallons per day
432 thousand gallons per day
246 thousand gallons per day
12 thousand gallons per day
2701 thousand gallons per day
thousand gallons per day
See Attachment 1
approx 450 people served
11

-FUR AUhNUY
9. All Facility Discharges and other Losses. Number
and Discharge (See instructions)Volume Specify the
number of disduirge points and the volume of water
discharged, or lost1rorn the facility according lo the
categones below. Estimate average volume per day in
Ihousand gallons per day Number of Total Volume Discharged,
Discharge Points Million GallonsPer DE
Surface Water 109a1 oe ijra'ln joW —7-727—
Sanitary wastewater trwsport systen 109b1 1 109t2 nil
Storm water transport system 109c1 109c2
Combined sanitary and storm water 109d1 109d2
im
it.
12.
transport system
Surface impoundment with no 10981 2 109e2 N/A - Makeup to recirculating system
tnclMd as evaporation
effluent
Underground percolation
109f1
10912
Well injection
109g1
109ga
x
0.004
Waste acceptance firm
109h1
109h2
Evaporation
109i1
Y
109i2
0,250
x
nil
Consumption
109i1
10%2
Other'
109k1
10910.
Facility dischargers and volume
Total Item 9
10911
10912
T them are dischargesto'other',
109m1
specify.
Permits, Licenses and Applications
List all existing, pending or denied permits,
licenses and applications related to discharges from this facility (see
Issuing
For
Type
'ito
Date
I
Date
Expirai
Agency
Agency
P= r
Filed
I
Issued
I
Denied
Date
Use
License
ID Number
YR/MOIDA
YDaRtB
MO,,A
, YR/MO/DA
YRIMC
Maps and Drawings
Attach all required maps and drawings to the back of this application. (see instructions)
Additional Information
9
instructions)
Item
112 Number
Information
Attachmt
I
Narrative Explanation of Specified items
Attachmt
2
Location Map
Attachmt
3
outfall Map
Attachmt
4
ISchematic of Water Flow
I

FMC Corporation
Lithium Division
Bessemer City, NC
NPDES Permit No. NC0005177
Renewal Application
April 1996
ATTACHMENT 1
Item 8 - Facility Water Usage - Other (108e)
Other water usage estimate includes stormwater which enters the
FMC collection system and is combined with other flows prior to
discharge.
Item 9 - Facility Discharges and Other Losses
Discharge points to surface water include:
- Outfall 001, the siphoned discharge from FMC's Lower Pond,
- Outfall 004, cooling water, boiler blowdown, condensate, and
stormwater discharged through FMC's system of stormwater
conveyances, and
- Drainage from the Toe Drain of the Lower Pond Dam
FMC currently has one restroom which is connected to the city of
Bessemer City Municipal treatment works. This sanitary facility
supplies 3-5 employees and discharge to the Bessemer City
treatment works from this facility is negligible. Nonetheless,
FMC is exploring directing all sanitary wastes to the Bessemer
City municipal system at some future date. This would increase
the discharge to a sanitary wastewater transport system to
approximately 12-15 K gal/day.
Item 10 - Permits, Licenses and Applications
Agency Type Number Term
NCDEHNR
Water
NCDEHNR
Stormwater
NCDEHNR
Recycle System
NCDEHNR
Air
NCDEHNR
Haz Waste
US EPA
Haz Waste
NCDEHNR
Solid Waste
No permits have been denied.
NC0005177
NCS000002
WQ0008149
3560R30
NCD000771964
NCD000771964
36-05
3/1/94-9/30/96
2/1/95-12/31/99
1/17/95-5/31/99
2/6/96-7/31/96
8/14/90-9/14/00
9/14/90-9/14/00
4/28/78

Attachment 3 FMC Corporation
NPDES Renewal 4/96 NPDES No. NC0005177
t !
,0
e7.
Z
Soo
3,
ry
X
79r—� OUTFALL 001
8 .9
0UTFALL 004
16.32 � G
S82 10_ 7 > -pig Z
� 800
'SIBL
EIEL
810
WE o
WER 70
,7
o
X 86 7
SCALE
1 INCH = 160 FEET
FIGURE 3.
FMC — DETAIL OF FMC EFFLUENT
LITHIUM FACILITY The ADVENT Group, Inc. CHANNEL AND CONFLUENCE
L WITH UN -NAMED TRIBUTARY
AUGUST 1995 64580TW�FIGS.PPE

FMC Corporation
NPDES Renewal 4/96
NC0005177
ATTACHMENT 4
Schematic of Water Flows
Water Purchased from Bessemer City 737 K gpd (1)
Rainfall Draining through FMC property 2,842 K gpd (2) I
I
I
I I
I 12 K gpd sanitary usage
I 725 K gpd process/boiler/cooling waters I
I -> 432 K gpd boiler feed I
I -> 122 K gpd non -contact cooling (Cogen) I
I -> 171 K gpd process and other cooling I
I I
I 2701 K gpd stormwater treated/discharged
I 10 K gpd stormwater to kiln pond/scrubber water I
I I
I 131 K gpd to R&D pond/cooling & process water
I I
--> 600 K gpd outfall 001 / treated sanitary, process, cooling
--> 125 K gpd outfall 004 / cooling water, boiler, condensate
--> 2600 K gpd outfall 004 / treated stormwater
--> 4 K gpd shipped offsite for treatment
--> 250 K gpd evaporation
--> discharge to Bessemer City POTW - nil
--> Consumption in products - nil
--> Seepage from Lower Pond Toe Drain system - nil
(1) Estimate based on 1995 annual purchases from Bessemer City / 365
(2) Estimate based on average rainfall of 42.8"/year, over 1.4 sq mi / 365

s
V
FMC Corporation
Lithium Division
NDPES No. NC0005177
Permit Renewal 4/96
ATTACHMENT 6
WATER TREATMENT CHEMICALS
APR 17 1996
V1£10N ?F(yF
Plant uses these trade name products, or equivalent products, available through
commercial water treatment service firms. Data presented here is 1995 usages.
MSDSs for these materials are attached.
PERFORMAX 401
sodium molybdate 1-10%
organic salt 1-10%
sodium tolyltriazone 1-10%
organic salt 1-10%
sodium hyroxide 1-10%
BIOSPERSE 250
magnesium nitrate 1-10%
5-chloro-2-methyl-4-
isothiazoline-3-one 1.15-1.42%
cupric nitrate <1%
magnesium chloride 1-10%
2-methyl-4-isothiazolin-3-one 0.35-0.47%
MEKOR 70
methyl ethyl ketone oxime 85-100%
WRICO OXY 11
sodium sulfite 1-10%
DREWAMINE CORROSION INHIBITOR
morpholine 40-55%
DREWPHOS 2300
sodium hexametaphosphate 1-10%
acrylic acid polymer, acid salt 1-10%
sodium hydroxide 3%
DREWPLEX 1621
acrylic acid polymer, sodium salt 10-25%
acrylic acid polymer, sodium salt 1-10%
sodium hydroxide 1-10%
CAUSTIC SODA (25%)
sodium hydroxide pellets 98-100%
AMERTROL 1123
Tetrapotassium pyrophosphate 40-55%
acrylic polymer 1-10%
CATALYZED SULFITE
sodium sulfite 85-100%
benzoic acid 1-10%

FMC Corporation - Lithium Division
NDPES No. NC0005177 - Permit Renewal 4/96
ATTACHMENT 6, PAGE 2
WATER TREATMENT APPLICATION SPECIFICS
(1) Turbine Generator #1 Cooling Tower
5 gal. Performax 401 corrosion inhibitor
1 gal. Biosperse 250 microbiocide
Weekly feed automatic; Discharge drain from Cogen to Lower pond/001
(2) Turbine Generator #2 Cooling tower
11 gal. Performax 401 corrosion inhibitor
2 gal. Biosperse 250 microbiocide
Weekly feed automatic; Discharge drain from Cogen to Lower Pond/001
(3) B.Q. Metal Cooling Tower
4 gal. Performax 401 corrosion inhibitor
1 gal. Biosperse 250 microbiocide
Weekly feed automatic; Discharge from north drain to Lower Pond/001
(4) R&D Cooling Tower
1 gal. Performax 401 corrosion inhibitor
1 gal. Biosperse 250 microbiocide
Weekly shock; Circulate through R&D Lake/001,004
(5) Shipping Air Comp. Cooling Tower
1 gal. Performax 401 corrosion inhibitor
1 gal. Biosperse 250 microbiocide
Weekly shock; Discharge from north drain to Lower Pond/001
(6) Organic Plant Cooling Tower
1 gal. Performax 401 corrosion inhibitor
1 gal. Biosperse 250 microbiocide
Weekly shock; Discharge to West Canal/004
(7) Cogen Boiler
3 qt. Mekor 70 corrosion inhibitor
3 gal. Wrico Oxy 11 corrosion inhibitor
3 qt. Drewamine corrosion inhibitor
100 ml. Drewphos 2300 deposit control agent
1 qt. Drewplex 1621 cleaner conditioner
Daily feed automatic; Discharge drain from Cogen to Lower Pond/001
Demineralization System
1 gal. Wrico oxy 11 corrosion inhibitor
Daily feed automatic; Discharge drain from Cogen to Lower Pond/001

FMC Corporation - Lithium Division
NDPES No. NC0005177 - Permit Renewal 4/96
ATTACHMENT 6, PAGE 3
WATER TREATMENT APPLICATION SPECIFICS
(8) Organic Boiler
16 oz. Wrico Oxy 11 corrosion inhibitor
16 oz. Drewamine corrosion inhibitor
16 oz. Caustic Soda 25%
16 oz. Amertrol 1123 boiler water treatment
16 oz. Catalyzed Sulfite
Weekly feed automatic; Discharge to West Canal/004
(9) Old Boilers
60 lb. Ametrol 1125 deposit inhibitor
60 lb. Caustic Soda 25%
3 lb. Drewamine corrosion inhibitor
1 qt. Mekor 70 corrosion inhibitor
Daily feed automatic; Circulate through R&D Lake/001,004

Drew Divisions
Emergency -Telephone
t
ASHLAND CHEMICAL INC.
One Drew Plaza. Boonton. New Jersey 07005
1 [phone] or
MATERIAL SAFETY
t
263-7600/Telex 136444 FAX [phone]
1(800) 274-5263
DATA SHEET
. Phone (201)
PERFORMAX 401 CORROSION INHIBITOR
l Ua Page:
003804
1910.1200 (THE HAZARD CCMMUNICATION STANDARD)
THIS MSOS COMPLIES WITH 29 CFR
affassf sssiaasasaf sfsifffif of iffifiif if sffifisifaafiasfaif iaf afsaif aasasaasasafiafaa
i iisf iff ifffsif ssf aiafsfsaaf
Product Name: PERFORMAX 401 CORROSION INHIBITOR
Data Sheet No:
0197353-007.000
OD 10 124 31860-063
Supearsedes: 05/12/93
FMC CORP. / LITHIUM DIVISION
449 NORTH COX ROAD ATTN: A/P PRODUCT: 4641
p, 0. BOX 3925 INVOICE- 389071
GASTONIA INVOICE DATE: 06/21/93
NC 28016
T0: 449 CORP.ORCOX OADM DIVISION
GAS'i ONIA
General or Generic ID: CORROSION INHIBITOR
DOT Hazard Classification: CORROSIVE MATERIAL (173.240)
SHA IIICINOGENS SECTION 3113 AARREMIDENTIFIEDEIN THIS SECTIONREPORT
IF TO THE
NTP AND
TIT
SEE DEFINITION PAGE FOR CLARIFICATION
% (by WT) PEL TLV
Note
INGREDIENT 5 MG/M3
1-10 5 MG/M3
SODIUM MOLYBOATE
CAS 0: 7631-95-0
( 1)
1-10
ORGANIC SALT a
( 2)
SODIUM TOLYLTRIAZOLE 1-10
CAS 0: 64665-57-2
( 3) ,
1-10
ORGANIC SALT f
1-10 2 MG/M3 - CEILING 2 MG/M3 - CEILING
SODIUM HYDROXIDE
CAS 0: 1310-73-2
Notes:
( 1) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
( 2) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
( 3) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
f THE SPECIFIC CHEMICAL NAME OF THIS COMPONENT IS BEING WITHHELD AS A TRADE SECRET.
212.00 Deg F
Boiling Point for COMPONENT( 70-85%)
( 100.00 Deg C)
@ 760.00 mm Fig
17.50 mmHq
Vapor Pressure for COMPONENT( 70-85%)
@ 68.00 Deg
( 20.00 Deg C)
Specific Vapor Density UNAVAILABLE 1.180
Specific Gravity @ 7725..00 Deg F
( 00 Deg C)
70-85%
Percent Volatiles
Evaporation Rate UNAVAILABLE 11.7
pH CLEAR YELLOW
Appearance LIQUID
State
FLASH POINT NOT APPLICABLE
EXPLOSIVE LIMIT UNAVAILABLE
EXTINGUISHING MEDIA: REGULAR FOAM OR WATER FOG OR CARBON DIOXIDE OR DRY CHEMICAL NITROGEN COMPOUNDS,
HAZARDOUS CITpMPOUNDS.AAND/OR THERMAL C" DIOXIDE DECOMPOSITION
CARBON OR MONOXIDE Y PRODUCE:.
PIECE OPERATED IN THE POSITIVE
FIREFI PRESSNG RE PROCEDURES- 'WEAR
FULL COE FIGHTINGNTAINEDBREAT IING APPARATUS WITH A FULL FACE
DEMAND MODE AND
CONTINUED ON PAGE: 2

Drew Divisions Emergency Telephone
ASHLAND CHEMICAL. INC.
MATERIAL SAFETY I
One Drew Plaza, Boonton. New Jersey 07005 1(606) 324-1133 or
DATA SHEET Phone [phone]rfelex 136444 FAX [phone](800) 274— 263
003804 PERFORMAX 401 CORROSION INHIBITOR Page: 2 -
• ' '
NFPA CODES: HEALTH- 3 FLAMMABILITY- 0 REACTIVITY- 1
•
PERMISSIBLE EXPOSURE LEVEL: NOT ESTABLISHED FOR PRODUCT. SEE SECTION II.
EFFECTS OF ACUTE OVEREXPOSURE:
SKIN - CAUSES BURNS.
EYES - CAUSES BURNS.
BREATHING - CANSCAUSEIDAMAGERTO NASAL AND REPIRATORYAPASSAGES DEEP TISSU
FIRST AID: _
IF ON SKIN-
IMMEDDICLOTHI FLU LAUNDER CONTAMINATED AREA IWITEDWATER FOR
ING BEFORE LEAST
MINUTES. GET MEDICAL ATTENTION. REMOVE
REMOVE CONTAMINATED SHOES PROMPTLY. DISCARD SHOES SATURATED WITH THIS PRODUCT.
IF INEYIOGETESIMMEDIATELY FLUSH WITH IMMEDIATE MLARGE
AMOUNTS OF WATER FOR AT LEAST 15 MINUTES, LIFTING UPPER AND LOWER LIDS
IF PHYSICIAN IS NOT IMMEDIATELY AVAILABLE, CONTINUE FLUSHING WITH WATER.
IF SWALLOWED GIVNOT IE MILK"OFCMAGNESIA"G KEEPHWARMG QUIETWILL �USE GETFURTHER MEDICAL ATTGE TO THE ENTION IMMEDIATELY.
BY GIVING
EN. IF
IF BREATHED:
IFHAAFFECTED,
DR�VE ARTIFICIAL TO FREATIONSH R KEEP PERSONNWARM,IS DQUIET. AND GET NMEEDDICALL ATTENTION.
PRIMARY ROUTE(S) OF ENTRY:
INHALATION, SKIN CONTACT
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMPATIBILITY: AVOID CONTACT WITH:, STRONG MINERAL ACIDS.
STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED:
SMALL SPILL: ABSORB LIQUID ON VERMICULITE, FLOOR ABSORBENT, OR OTHER ABSORBENT MATERIAL AND TRANSFER TO H000.
LARGESPILL:EEN COMPLETED. NOTSTOWEAiINGLL ATPROTECTIVE
URCE DIEI REATOF SHOULD BE
PREVENT SPREADFROM ING,EA OPUMP ILIQUID LL ITO SALVAGE
L CLEAN-UP �S
TANK. REMAINING LIQUIDMAERSE TAKEN UP ON SAND, CLA
Y• EARTH, FLOOR ABSORBENT, OR OTHER ABSORBENT MATERIAL
AND
OVELED
NOTIFY PROPER AUTHORITIES
PREVENT RRUN-OFFiTA SPILL OSEWERS,HSTREAMS
OR OTHER BODIES OF WATER. IF RUN-OFF OCCURS
.
AS
WASTE DISPOSAL METHOD:
OF WATER IN ACCORDANCE WITH APPLICABLE REGULATIONS.
SMALL SPILL: FLUSH DOWN DRAIN WITH LARGE AMOUNTS
LARGE SPILL: DISPOSE OF IN ACCORDANCE WITH ALL APPLICABLE LOCAL, STATE AND FEDERAL REGULATIONS.
madmalk SEE
CTION
RESPIRATORY PROTECTION: IF WORKPLACE EXPOIUREED RESPIT(S) OISPRODU E OR ANY
ABSENCE QFNPROPER ENVIRONMENTAL CONTROL-
:). CONTROL.
II), A NIOSH/MSHA APPROVED AIR SUP
OSHA REGULATIONS ALSO PERMIT OTHER NIOSH/MSI` RESPIRATORS (NEGATIVE PRESSURE TYPE) UNDER SPECIFIED
TO DITIONSREbuCE E(SEE YOUR INDUSTRIAL HYGIENIST). ENGINEERING OR ADMINISTRATIVE CONTROLS SHOULD BE IMPLEMENTED
L EXHAUST) VENTILATION TO MAINTAIN EXPOSURE
VENTILATION: PRO IDE SUFFICIENT MECHANICAL (GENERAL AND/OR LOCA
B
PROTECTIVE GLOVES: WEAR RESISTANT GLOVES SUCH AS:, NEOPRENE
4CE WITH OSHA GI IARE
FACE
SHIELD
BNIN CGL
EYE PROTECION:EGOGGLES SAFETY GLASSES. (CONSULT YOUR DUSTRAL
ADVISED- CEVR�OSHA REGULATIONS ALSO R
HYGIENIST).
OTHER PROTECTIVE EQUIPMENT: TO PREVENT SKIN CONTACT, WEAR IMPERVIOUS CLOTHING AND B�00T T'TT
�r■z�r�rr,r*r��Ti � �
KEEP FROM FREEZING.
CONTAINERS OF THIS MATERIAL MAY BE HAZARDOUS W PRECAUTIONS GIVEN INPTHIS DTIED ATASHEETMUST NERS IBEPOBSERVED.
ESIDUES
(VAPOR, LIQUID, AND/OR SOLID),
THE IyNjIFTTHTTHEOCOMPANYUOR NOT. RECIPIENTSLAREEADVIISED TO CONFIRMBUT
INIADVANCEWAR
OFANEED NTED TTHAT ETHHE�IHNFORMATIONAISD
CURRENT, APPLICABLE, AND SUITABLE TO THEIR CIRCUMSTANCES.
LAST PAGE --SEE ATTACHMENT PAGE ENCLOSED --LAST PAGE

7 J 24-HOUR
.�. Drew Industrial Division ►O Emergency
ASHLMO CHEMKAL WC. Telephone
MATERIAL SAFETY One Drew Plaza, Boonton, New Jersey 07005 1(800) 274-5263 or
DATA SHEET Phone [phone]/Telex 136444 1(800) ASHLAND
e
- 000134 BIOSPERSE 250 MICROBIOCIDE Page: 1
_ THIS MSDS COMPLIES WITH 29 CFR 1910.1200 (THE 14AZARD COMMUNICATION STANDARD)
ssssassssssssssssssssssssssssssssssssssssssssss:ssssssssssssssssssssssssssssssssssss:ssssssss:s:ssssssssssssssss
Product Name: BIOSPERSE 25O MICROSIOCIDE
Data Sheet No: 0137221-003.000
OD 10 124 31860-063 Prepared: 05/31/88
FMC CORP. / LITHIUM DIVISION Supersedes: 09/10/86
449 NORTH COX ROAD ATTN: A/P PRODUCT: 1551
G 0. BOX 3925 INVOICE• 375717
ASTONIA NC 28016 INVOICE DATE: 02/05/93
T0: NLITHIUM DIVISION
OTH COX ROAA�/P
GASTONIA
General or Generic ID: MICROBIOCIDE
DOT Hazard Classification: CORROSIVE MATERIAL (173.240)
- - s•rarr�•�Tlr.7
IF PRESENT IARC, NTP AND OSHA CARCINOGENS AND CHEMICALS SUBJECT TO THE REPORT-
ING REQUIREMENTS OF SEE TITLE
IDEFINIII
SECTION
PAGE 31 3 ARIFICATION ARE IDENTIFIED IN THIS SECTION.
INGREDIENT % (by WT) PEL TLV Note
MAGNESIUM NITRATE 1-10 ( 1)
CAS 0: 10377-60-3
5-CHLORO-2-METHYL-4-ISOTHIAZOLIN-3-ONE 1.15-1.42 ( 2)
CAS 0: 26172-55-4
CUPRIC NITRATE <1 1 MG/M3 1 MG/M3 ( 3)
CAS #: 3251-23-8
MAGNESIUM CHLORIDE 1-10 ( 4)
CAS *: 7786-30-3
2-METHYL-4-ISOTHIAZOLIN-3-ONE 0.35-0.47 ( 5)
CAS x: 2682-20-4
Notes:
( 1) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
( 2) 5PCHLORO-2CMETHYD54AISOTHIAZOLIN-3-ONE, 2AMEETHYLL04 ISOTHIAZOLIN 9 ONE.IOTMIAZOLONES.
( 3) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
( 4) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
( 5) (5PCHLOORROR2CM ETHYDLS4ATWA ISOTHIAZOLIN-3--ONE,D2AME L-4 OISOTHIAZOLIN 3-OMETHYL
85-100%) 212.00 Deg F
for COMPONENT(
Boiling Point ( 100.00 Deg C)
@ 760.00 mmHg
for COMPONENT( 85-100%) 18Deg
.50 mmHg
Vapor Pressure ®
20.00 P
( 20.00 Deg C)
HEAVIER THAN AIR
Specific Vapor Density
1.010 - 1.030
Specific Gravity Q 77.00 Deg F
( 25.00 Deg C)
85-100%
Percent Volatiles
SLOWER THAN ETHER
Evaporation Rate
2.0 - 5.0
pH
CLEAR, LIGHT GREEN YELLOW
Appearance LIQUID
State HOMOG SOLN
Form
FLASH POINT NOT APPLICABLE
EXPLOSIVE LIMIT NOT APPLICABLE
EXTINGUISHING MEDIA: NOT APPLICABLE
CONTINUED ON PAGE: 2

24-HOUR
Drew Industrial Division Emergency
ASHLASO CNEWAI INC. Telephone
MATERIAL SAFETY One Drew
Plaza, Bo nNew T ex ton, Jersey
07005 1(800) 274-5263 or
Phone2011
DATA SHEETVA. 1(800) ASHLAND
000134 BIOSPERSE 250 MICROBIOCIDE Page: 2
HAZARDOUS DECOMPOSITION PRODUCTS: THERMAL DECOMPOSITION OR COMBUSTION MAY PRODUCE:, OXIDES OF SULFUR, HYDROGEN
CHLORIDE
FIREFIGHTING PROCEDURES: NOT APPLICABLE
WEAR SELF-CONTAINED BREATHING
WHENNG APPARATUS
FIGHFIR
WITH A
FULL FACEPIECE OPERATED IN THE POSITIVE PRESSURE DEMAND
BODY
MODE FULL
WATER MAY BE USED TO KEEP FIRE -EXPOSED CONTAINERS COOL UNTIL FIRE IS OUT.
NFPA CODES: HEALTH- 3 FLAMMABILITY- 0 REACTIVITY- 0
PERMISSIBLE EXPOSURE LEVEL: NOT ESTABLISHED FOR PRODUCT. SEE SECTION II.
EFFECTS OF ACUTE OVEREXPOSURE:
EYES - CAUSES SEVERE IRRITATION AND CORNEAL INJURY.
SKIN - CAUSES SEVERE IRRITATION.
SKIN - REPEATED CONTACT MAY CAUSE SENSITIZATION.
BCAN BE REATHINGS OFDMIN ISTTCANCCAUSENIRRITATIONAOFYFROM NASAL ANDLRESPIRAATTORYPEATED PASSAGESD�RE.
SWALLOWING - CAN CAUSE DEATH
FIRST AID:
IF ON SKIN: IMMEDIATELY FLUSH EXPOSED AREA WITH WATER FOR AT LEAST 15 MINUTES. GET MEDICAL ATTENTION. REMOVE
CONTAMINATED CLOTHING. LAUNDER CONTAMINATED CLOTHING BEFORE RE -USE.
IF IN EYES: IMMEDIATELY
IMMEDIATE MEDICAL AMOUNTS OF WATER FOR AT LEAST 15 MINUTES, LIFTING UPPER AND LOWER LIDS
IF SWIFLTHESE ARENNOTIAVAILABOLE, DRINK LAIRGE QUANTITIES OFGWATEER . AVOIDFAMCOHbLE CALLIA PHYSICIANNIMMEDIATTEELY.
AGAINST CIRCULATORY PSHOCK. RESPIRATORYADEPRESSIONOA D CONVULSIONSEMAY BEFNEEEDEDIC LAVAGE. MEASURES
IF BRB EEAATTHINGFHASFSTOPPEDRGMEEARTIFICIIALLRESPIRATTIION. kEEP PERSONIWARM, QUIETCAND.GET MEDICAL ATTENTION•
PRIMARY ROUTE(S) OF ENTRY:
INHALATION, SKIN ABSORPTION. SKIN CONTACT
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMPATIBILITY: NOT APPLICABLE
• .•��r-.ram � �=^r7r�-�' � � •
STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED:
SMALL SPILL: ABSORB LIQUID ON VERMICULITE, FLOOR ABSORBENT OR OTHER ABSORBENT MATERIAL.
LARGE SPILL: PERSONS NOT WEARING PROTECTIVE EQUIPMENT SHOULD BE EXCLUDED FROM AREA OF SPILL UNTIL CLEAN-UP HAS
BEEN COMPLETED. STOP SPILL AT SOURCE. DIKE TO PREVENT SPREADING. ABSORB WITH INERT MATERIAL. THE
ABSORBENT(AND SURFACE SOIL TO A DEPTH SUFFICIENT TO REMOVE ALL MICROBIOCIDE) IS THEN SHOVELED INTO A PAIL
OR DRUM AND TREATED WITH ENOUGH DECONTAMINANT SOLUTION TO WET THE SOLID THOROUGHLY. LET THESE CONTAINERS
STAND OPEN FOR 48 HOURS TO AVOID THE BUILDUP OF PRESSURE, THEN SEAL AND DISPOSE OF BY BURYING AS LANDFILL.
R DECONTAMINATED AREA IS
CLTDANNARNIAND
FLUSHED INTO
OMUICIIPPALSEWER DO NOT DISCHARGE SPILLSANCLEAIINGUNOFFS ITOPENBODIE OWATR
CLOTHING PROMPTLY; LAUNDER BEFORE REUSE. WASH SKIN WITH SOAP AND WATER.
DECONTAMINANT SOLUTION: SODIUM SISULFITE SOLUTIONS (ABOUT 11% SOLIDS CONTENT) DECOMPOSE D WITHIN 30
250
COMPLETELY DEACTIVA
MINUTES LABORATORY
WITHSATNLEASTE4 EQUIVALENTS OFIDECONTAMINA�NG SOLUTION. A VOLUME RATIO OF20/1
DECONTAMINANT/ACTIVE MICROBIOCIDE IS RECCMMENDED. THE FOLLOWING SOLUTIONS ARE ACCEPTABLE DECONTAMINANTS:
INGREDIENT: SODIUM METABISULFITE (WEIGHT = 1 POUND) + WATER(WEIGHT = 8 POUNDS). TOTAL 9 POUNDS. SOLIDS
CONTENT = 11.1%. PH = 4.2. INGREDIENT: SODIUM SISULFITE (WEIGHT 1 POUND + WATER (WEIGHT 8.3 POUNDS).
TOTAL 9.3 POUNDS. SOLIDS CONTENT = 10.7%. PH = 4.2. INGREDIENT: SODIUM SULFITE (WEIGHT = 1 POUND) +
WATER (WEIGHT = 7 POUNDS) + HYDROCHLORIC ACID(37%) (WEIGHT= 0.67 POUNDS). TOTAL 8.67 POUNDS. SOLIDS
CONTENT = 9.5%. PH = 5-5.5.
NOTE: DECONTAMINANT SOLUTION MUST HAVE PH ON THE ACID SIDE• SINCE IT IS MUCH LESS EFFECTIVE WHEN
ALKALINE. IN CONVERTING SODIUM SULFITE TO THE BISULFITE, DfSSOLVE THE SALT IN WATER AND SLOWLY ADD THE
ACID WITH GOOD AGITATION TO PREVENT LIBERATION OF SULFUR DIOXIDE CAUSED BY LOCAL EXCESS OF OXIDACIDE
INET
CONTAINERS OF DECONTAMINANT SOLUTION CLOSED OR COVERED TO REDUCE ACCUMULATION OF SULFUR DITHE OXIDE IN THE
MAKING UP(OR HANDLING LIMIT VAAMINANTISOLUTION$ SHOULD WEAURIOUGOGGLES,OR LD BE
SHIELD MADE AND RURBERRGLOVEESSSONNEL
WASTE DISPOSAL METHOD:
SMALL SPILL: DEPOSIT IN A LANDFILL IN ACCORDANCE WITH LOCAL, STATE AND FEDERAL REGULATIONS.
LARGE SPILL: DEPOSIT IN A LANDFILL IN ACCORDANCE WITH LOCAL, STATE AND FEDERAL REGULATIONS.
CONTINUED ON PAGE: 3

' 24-HOUR
Drew Industrial Division Emergency
ASHLAW CHEMICAL WW_ Telephone
MATERIAL SAFETY One Draw
Plaza, Boonton,
New Telexersey 07005 1(800) 274-5263 or
Phone DATA SHEET4. 1(800) ASHLAND
y._ 000134 BIOSPERSE 250 MICROBIOCIDE Page: 3
RESPIRATORY PROTECTION: IF OVEREXPOSURE HAS BEEN DETERMINED OR DOCUMENTED, A NIOSH/MSHA JOINTLY APPROVED AIR
SUPPLIED RESPIRATOR IS ADVISED IN ABSENCE OF PROPER ENVIRONMENTAL CONTROL. OSHA REGULATIONS ALSO PERMIT
OR ER NIOSH/MSIAVERCSONTRATTOROLS S UNDEULD BE SPECIFIED
DNCONTED CONDITIONS.
(SEE
URESAFETY EQUIPMENT SUPPLIER). ENGINEERING
VENTILATION:
PROVIDE
EVEL OF OSUUFFICIENT MECHANICOM AL
(GENERAL, SUSPECTED
LOCAL
OC APPARENT ADVERSE VENTILATION
FFECTS TO MAINTAIN EXPOSURE
PROTECTIVE GLOVES: WEAR RESISTANT GLOVES SUCH AS:, NEOPRENE
EYE PROTECTION: CHEMICAL SPLASH GOGGLES AND FACE SHIELD (8" MIN.) IN COMPLIANCE WITH OSHA REGULATIONS ARE
ADVISED• HOWEVER, OSHA REGULATIONS ALSO PERMIT OTHER TYPE SAFETY GLASSES. (CONSULT YOUR SAFETY EQUIPMENT
SUPPLI Eft )
OTHER PROTECTIVE EQUIPMENT: TO PREVENT SKIN CONTACT, WEAR IMPERVIOUS CLOTHING AND BOOTS.
•'EYEWASH STATION, EMERGENCY SHOWER -
CONTAINERS FTHIS MATERIAL MAY BE LIQUID , AND/OR SOLID),HALLR�SRD PRECAUTIONS GIVWHEN EMPTIED. EN INPTIED THIS DATASHEETSMUSTABE POBBSERVED. DUES
THE INFORMATION ACCUMULATED HEREIN IS BELIEVED TO BE ACCURATE BUT IS NOT WARRANTED TO BE WHETHER ORIGINATING
WITH APPLICABLE,
THE COMPANY OR
NOT. SUITABLE RECIPIENTS ARE ADVISED TO CONFIRM IN ADVANCE OF NEED THAT THE INFORMATION IS
CURRENT,

` Drew Industrial Division EmermerHOUR
gency
ASHLA o CHEMICAL 01_ Telephone
MATERIAL SAFETY One Drew Plaza, Boonton, New Jersey 07005
DATA SHEET Phone [phone]/Telex 136444 1(800) 1(800) SHLAND ASHLAND or
DEFINITIONS This definition page is intended for use with Material Safety Data Sheets supplied by the Drew Chemical Corporation.
Recipients of these data sheets should consult the OSHA Safety and Health Standards (29 CFR 1910). particularly
subpart G — Occupational Health and Environmental Control, and subpart I — Personal Protective Equipment, for
General guidance on control of potential Occupational Health and Safety Hazards.
SECTION 1
PRODUCT IDENTIFICATION
GENERAL OR GENERIC ID: Chemical family or product
description.
DOT HAZARD CLASSIFICATION: Product meets DOT
criteria for hazards listed.
-SECTION II
COMPONENTS
Components are listed in this section if they present a
physical or health hazard and are present at or above
1 % in the mixture. If a component is identified as a
CARCINOGEN by NTP. IARC, or OSHA as of the date
on the MSDS, it will be listed and footnoted in this
section when present at or above 0.1 % in the product
Negative conclusions concerning carcinogenicity are not
reported. Additional health information may be found in
Section V. Components subject to the reporting
requirements of Section 313 of SARA Title III are
identified in the footnotes in this section, along with
typical percentages. Other components may be listed if
deemed appropriate.
Exposure recommendations are for components. OSHA
Permissible Exposure Limits (PELS) and American
Conference of Governmental Industrial Hygienists
(ACGIH) Threshold Limit Values (TLVs) appear on the
line " with the component identification. Other
recommendations appear as footnotes.
SECTION III
PHYSICAL DATA
BOILING POINT: Of product if known. The lowest
value of the components is listed for mixtures.
VAPOR PRESSURE: Of product if known. The highest
value of the components is listed for mixtures.
SPECIFIC VAPOR DENSITY: Compared to AIR = 1. If
the Specific Vapor Density of a product is not known,
the value is expressed as lighter or greater than air.
SPECIFIC GRAVITY. Compared to WATER = 1. If
Specific Gravity of product is not known, the value is
expressed as less than or greater than water.
pH: If applicable.
PERCENT VOLATILES: Percentage of material with
initial boiling point below 425 degrees Fahrenheit and
vapor pressure above 0.1 mm Hg at 68 F.
EVAPORATION RATE: Indicated as faster or slower
than ETHYL ETHER, unless otherwise stated.
SECTION IV
FIRE AND EXPLOSION DATA
FLASH POINT: Method identified.
EXPLOSION LIMITS: For product if known. The lowest
value of the components is listed for mixtures.
HAZARDOUS DECOMPOSITION PRODUCTS: Known or
expected hazardous products resulting from heating,
burning or other reactions.
ECTION IV (cont.)
EXTINGUISHING MEDIA: Following National Fire
Protection Association criteria.
FIREFIGHTING PROCEDURES: Minimum equipment to
protect firefighters from toxic products of vaporization.
combustion or decomposition in fire situations. Other
firefighting hazards may also be indicated.
SPECIAL FIRE AND EXPLOSION HAZARDS: States
hazards not covered by other sections.
NFPA CODES: Hazard ratings assigned by the National
Fire Protection Association.
SECTION V
HEALTH HAZARD DATA
PERMISSIBLE EXPOSURE LIMIT: For product
THRESHOLD LIMIT VALUE For product
EFFECTS OF ACUTE OVEREXPOSURE: Potential local
and systemic effects due to single or short term
overexposure to the eyes and skin or through inhalation
or ingestion.
EFFECTS OF CHRONIC OVEREXPOSURE: Potential local
and systemic effects due to repeated or long term
overexposure to the eyes and skin or through inhalation
or ingestion.
FIRST AID: Procedures to be followed when dealing
with accidental overexposure.
PRIMARY ROUTE OF ENTRY: Based on properties and
expected use.
SECTION VI
REACTIVITY DATA
HAZARDOUS POLYMERIZATION: Conditions to avoid to
prevent hazardous polymerization resulting in a large
release of energy.
STABILITY: Conditions to avoid to prevent hazardous or
violent decomposition.
INCOMPATIBILITY: Materials and conditions to avoid to
prevent hazardous reactions.
SECTION VII
SPILL OR LEAK PROCEDURES
Reasonable precautions to be taken and methods of
containment, clean—up and disposal. Consult federal,
state and local regulations for accepted procedures and
any reporting or notification requirements.
SECTION VIII
PROTECTIVE EQUIPMENT TO BE USED
Protective equipment which may be needed when
handling the product
SECTION IX
SPECIAL PRECAUTIONS OR OTHER COMMENTS
Covers any relevant points not previously mentioned.
ADDITIONAL COMMENTS
Containers should be either reconditioned by CERTIFIED firms or properly disposed of by APPROVED firms. Disposal of
containers should be in accordance with applicable laws and regulations. "EMPTY" drums should not be given to
individuals. Serious accidents have resulted from the misuse of "EMPTIED" containers (drums,pails,etc.). Refer to Sections
IV and IX.

MATERIAL SAFETY
DATA SHEET
_ Drew Divisions - I;) V 1 Emergency Telephone
ASHLAND CHEMICAL INC.
One Drew Plaza, Boonton. Jersjj FAX [phone]=4482 1(800) 274-5263 or
Phone [phone]W/T
Page:
MEKOR..70.CORROSION:INHIBITOR
000080. _ 1910.1200 (THE HAZARD COMMUNICATION STANDARD)
,.
MSOS COMPLIES WITH 29 CFR .,..--•--.•._--.---
'•- ttsststtttststatttttsttttssssssssassststtstsssssssstssttssttsssstssttattsstsstssssttstststastssstsssssstsssstsss ^
FOR 70 CORROSION INHIBITOR
• - D oduct Nana: Data Sheet No: 0015516-006.006 _
CAS NUMBER:. .. 96-29-7
_ FMCP, /LITHIUM DIVISION
- ATTN: A/P
449 NORTH COX ROAD
PP.0. 13r.ASTONIOAX 3925
Nc . 28016 : • .
Prepared: 12/22/94
OD 10 001 31860-063 _ �persedes: 09/30/94
Print Date: 01/14/95
PRODUCT: =:` 4115 _ ♦h
INVOICE: 334906 Llt111U'il
INVOICE DATE. 10/12/94 r
TO: FM NORTH COXIROAD DCORPATTTN: A/P ! _
GASTONIA .. • FFR 1 3 =1945_
Kedth Services
General or Generic ID: CORROSION INHIBITOR
DOT Hazard Classification: COMBUSTIBLE , •
REPORT -
IF PRESENT IARC. NTP AlD OSHA IIICSECTION 3113 ARE IDENTILS FIEDCT I
N THIS THE
ON'
ING REQUIREMENTS OF SEE DRA EFINITION PAGE FOR CLARIFICATION nV Note
Percent PEL ( 1)
INGREDIENT 85-100
METHyL ETHYL KETONE OXIME
CAS: 96-29-7
Notes:
( 1) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
THE AIHA HAS ESTABLISHED A WORKPLACE ENVIRONMENTAL EXPOSURE LEVEL (WEEL) OF 10 PPM. 8-HOUR TIME WEIGHTED
AVERAGE.
306.00 Deg F
for PRODUCT ( 152.22 Deg C)
s.
Boiling Point @ 760.00 mm Hg
10.00 mm Hg
for PRODUCT @ 115.00 Deg FF
f
Vapor Pressure ( 46.11 Deg C)
3.00
Specific Vapor Density AIR = 1 .916 - .924
@ 77.00 Deg F
Specific Gravity ( 25.00 Deg C)
>95%
Percent Volatites < 1.00
Evaporation Rate (N-BUTYL ACETATE = 1) COLORLES: UNPLEASANT AROM ODOR
LIQUID
Appearance
FIOMO(' SDLN
State
Form
• 145.0 Deg F ( 62.8 Deg C)
FLASH POINT(PMCC )
EXPLOSIVE LIMIT UNAVAILABLE
EXTINGUISHING MEDIA: ALCOHOL FOAM OR CARBON DIOXIDE OR DRY CHEMICAL METHYL ETHYL KETONE.
HAZARDOUS DECOMPOSITION PRODUCTS: THERMAL DECOMPOSITION OR COMBUSTION MAY PRODUCE:.
NITROGEN OXIDES. CARBON DIOXIDE AND CARBON MONOXIDE, SUBSTITUTED AMIDES
FIREFIGHTING PROCEDURES: EARSFI�N TAINED BREATH
APPARATUS WITH A FULL FACEPIECE OPERATED IN THE POSITIVE
PRESSURE DEMAND MODE
WATER MAY BE USED TO KEEP FIRE -EXPOSED CONTAINERS COOL UNTIL FIRE IS OUT•
-' TAD BY HEAT, PILOT LIGHTS. OTHER FLAMES AND IGNITION SOURCES AT LOCATIONS DISTANT FROM
SPECIAL FIRE 3 EXPLOSIONHAZARDS:VAPORS ARE HEAVIER THAN AIR AND MAY TRAVEL ALONG THE GROUND I BE MOVED B
VENTILATION AND IGNITED
MATERIAL HANDLING POINT.
R DRUM (EVEN EMPTY) BECAUSE PRODUCT (EVEN JUST RESIDUE) CA
NEVER USE WELDING OR CUTTING TORCH ON OR NEA
IGNITE EXPLOSIVELY. REACTIVITY- 0
.� NFPA CODES: HEALTH-3 FLAMMABILITY- 2
02.
CONTINUED :ON PAGE: 2

24—HOUR
Drew Divisions Emergency Telepjonrer
ASHLANO CHEMICAL. INC.
MATERIAL SAFETY One Drew Plaza. Boonton, New Jersey 07005 .1(606) 324-113DATA SHEET Phone [phone]relex 136444 FAX [phone](800) 274-526
MEKOR 70 CORROSION INHIBITOR
000080
PERMISSIBLE EXPOSURE LEVEL: NOT ESTABLISHED FOR PRODUCT. SEE SECTION II.
EFFECTS OF ACUTE OVEREXPOSURE:
MAY INCLUDE $TINGING. TEARING. REDNESS. SWELLING AND
EYES - EXPOSURE CAUSES SEVERE EYE IRRITATION. SYMPTOMS
EYE DAMAGE.
SKIN - EXPOSURE MAY CAUSE MILD SKIN IRRITATION. SYMPTOMS MAY INCLUDE REDNESS AND THE BRRNIN .
SKIN ABSORPTION IS POSSIBLE AND MAY CONTRIBUTE TO SYMPTOMS OF TOXICITY FROM OTHER ROUTES OF EXPOSURE.
BREATHING - EXPOSURE TO VAPbR OR MIST IS POSSIBLE.
SHORT-TERM INHALATION TOXICITY IS MODE EXPOSURE MAY BE HARMFUL. SYMPTOMS OF
SYMPTOMS ARE MORE TYPICALLY SEEN AT AIR CONCENTRATIONS EXCEEDING THE RECOMMENDED EXPOSURE LIMITS.
EXPOSURE MAY INCLUDE:
DERS. E.G. ASTHMA -LIKE CONDITION
IRRITATION (NOSE. THROAT RESPIRATORY TRACT)- PRE-EXISTING LUNG DISOR
MAY BE AGGRAVATED BY EXPOSURE TO THIS MATERIAL.HE
-CENTRAL NERVOUS SYSTEM DEPRESSION (DIZZINESS. DROWSINESS. WEAKNESS, FATIGUE. NAUSEA. HEADA
UNCONSCIOUSNESS-
-RESPIRATORY FA LURE BLUISH TINT THE -
GGRAVVATE ABYNEREA�BSDOOGACONDITION SENSSIITIVE TONAA DECREASE IN AVAILABLEKOXYGEN SUCH S CHRONICTLUNG�
DISEASE. CORONARY ARTERY DISEASE OR ANEMIAS-
COMA- - SINGLE DOSE ORAL TOXICITY IS MODERATE• SWALLOWING; MAY BE HARMFUL.
SYMPTOMS MAY INCLUDE: _
-GASTROINTESTINAL IRRITATION NAUSEA. VOMITING DIARRHEA)OUS ATE
(BLLOOOIDNG CONDITION SENSITIVEOTIN ADECREASBLU E IN AVAILABLEKOXYGEN, SUCH AAS�CHRONIC LUNG'
DISEASE. CORONARY ARTERY DISEASE OR ANEMIAS -
ADDITIONAL OF SKIN COACT MAY INCLUDE:
Afi
FIRST AID: PERSIST. SEEK
IF ON SKIN: REMOVE CONTAMINATED CLOTHING. WASH EXPOSED AREA WITH SOAP AND WATER. IF SYMPTOMS
MEDICAL ATTENTION. LAUNDER CLOTHING BEFORE REUSE.
IF INEYES-kK�IF S MPTOMSMATER FOR IMMEDIATELY
EDIMINLUTEMMOM�E INDIVIDUAL AWA' HOLDING EYELIDSAPART; SEEPOSURE K IMMEDIAINTO TEEMMEEDICAL ATTEENTTIOFLUSH ONN-
IF SWALLOWED:
SEEK
KUMEDIC THEFT SIDE IF INDIVIDUHE AL
IDOWN DROWSY
F OR IVIDUALIOIUSSL�ONSCIOUSDO NOT GAND ALERT IVE ININDUCBY E�H•
VOMITING BY GIVING SYRUP OF IPECAC OR BY GENTLY PLACING TWO FINGERS AT THE BACK OF THE THROAT. IF
POSSIBLE. DO NOT LEAVE INDIVIDUAL UNATTENDED-
•c en�.Taa�y; •F SY4ir CEVE O^ I?�� IIATELY VnVE I!:'JIVIDUAL A'!AY FROM EXoDS�RE AND INTO FRESH AIR. SEEK
M RMMPDEATONEDICCAALBATAENTION-S KEEP
RESPIRATION. ADMINIAND STER QUIET.
OXYGEN.
PERSON IS NOT BREATHING. BEGIN ARTIFICIAL
PRIMARY ROUTE(S) OF ENTRY:
INHALATION. SKIN ABSORPTION
Page: 2
EFFECTS OF CHRONIC OVEREXPOSURE: HAS
OVEREXPOSURE
TO THIS MATLS ERNOLM(OR
AY ITS
COMEPRE-EXISTINGEDISORDERS OF THESE EN SUGGESTED AS A �ORGANS USE FIN HUMATHE NS- BLOOD
IN
ABNORMALITIES
SS.PRELIMINARYL THE SRESULTUDY IS FROMCOMPATLIFETIMEED WE 00 STUDYNOT IN IFTTHESE EFS AND FECTS WILLEBEE RELEVANTTOHUJMANTERM
HEALTH. UNTIL SUCH TIME, EXPOSURE SHOULD BE KEPT AS LOW AS REASONABLY ACHIEVABLE.
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMPATIBILITY: AVOID CONTACT WITH:. STRONG OXIDIZING AGENTS. STRONG ORGANIC ACIDS. STRONG ALKALIES.
EXCESSIVE HEAT
STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED: AND ELECTRICAL
SMALL SPILL: ELIMINATE ALL SOURCES OF IGNITION SUCH AS FLARES. FLAMES (INCLUDING PILOT LIC+iTS).
SPARKS.
. OR OTHER ABSORBENT MATERIAL AND TRANSFER TO FOOD.
ABSORB LIQUID ON VERMICULITE. FLOOR ABSORBENT
VENTILATE AREA. LUDNG PILOT
LARGE
NOT SPILL:
ELIMINATE
TECALL
IGNITION
SOURCES
(FL RES,FLAMES
INEXCLUDED FROM AREAIOF SPI!'L UNTIL SOLEAN-UPIK
HAS BEENCOMPLETED.
WEAING
SPREADIOM
STOP NG. AIFSOURCE. PREVENT FROM ENTERING DRAINS
TIES REQUSEWEIRED . PUMP OR VACUUM STREAMS OR OTHER BTRANSFER SPODIES OF ILLEDRPRODUCT EVENT RTO
CLEAN CONTAINERS FOR REOCCURSCOVERY. ABSORB UNRECOVERABLE PRODUCT TRANSFER CONTAMINATED ABSORBENT, SOIL AND
OTHER MATERIALS TO CONTAINERS FOR DISPOSAL.
PREVENT RUN RUN-OFF
TOASEWERS.HST STREAMS OR OTHER BOGIES OF WATER. IF RUN-OFF OCCURS, NOTIFY PROPER AUTHORITIES
AS
OCCU
WASTE DISPOSAL METHOD:
SMALL SPILL: DISPOSE OF IN ACCORDANCE WITH ALL LOCAL. STATE AND FEDERAL REGULATIONS.
LARGE SPILL: DISPOSE OF IN ACCORDANCE WITH ALL APPLICABLE LOCAL, STATE AND FEDERAL REGULATIONS.

MATERIAL SAFETY
DATA SHEET
000080
Drew DIVISIOfis Emergency Telephone
ASHLAND CHEMICAL. INC.
or
One Drew e01263-7
za, Boonton. New Jersey 0700
Phone (600frelex 1136444 FAX [phone] [phone]
MEKOR 70 CORROSION INHIBITOR
RESPIRATORY PROTECTION: NOT REQUIRED UNDER NORMAL CONDITIONS OF IS,EXCEEDED(SEE SECTION II). A NIOSH/MSHA
IF WORKPLACE EXPOSURE LIMIT UORF PRODUCT OR ANY COMPONABSENCE
APPROVED AIR SUPPLIED LIMI, IS ADVISED IN ABSENCE OF PROPER ENVIRONMENTAL ED CONDICONTROL.TIONSS EXPOSURE
ALSO PERMIT OTHER SUPPLIED
NIOREMSHA RESPIRATORS (NEGATIVE PRESSURE TYPE�__UNDER SPECIFIED CONTO DITIONS (SEE YOUR
INDUSTRIAL HYGIENIST). ENGINEERING OR ADMINISTRATIVE CONTROLS S LD BE IMPLEMENTED
VENTILATION: PROVIDE SUFFICIENT MECHANICAL (GENERAL AND/OR LOCAL EXHAUST) VENTILATION TO MAINTAIN EXPOSURE
BELOW TLV(S).
PROTECTIVE GLOVES: NATURAL RUBBER COMPLIANCE WITH HOWEVER- OSHA
EYE P�uO.ECIEILHGOESCONSULT YRSAEYPRENTAtI
PROTECTION.
ALSO CHEMICAL TYPE SAFETY
TO PREVENT REPEATED OR PROLONGED SKIN CONTACT, WEAR IMPERVIOUS CLOTHING AND BOOTS.
OTHER PROTECTIVE EQUIPMENT: �.
LE INTERNAL PRESSURE. NEVER USE PRESSURE TO EMPTY.
WHEN OPENING.REMOVE CLOSURES CAREFULLY TO RELIEVE POSSIB
CONTAINERS �.FL HIS MATERIAL
A AND/OR SOLIBE D).HAAZARLL DOUS WEN EMPTI1 PRECAUTIONS GIVEN IINCE N T�tiIS ED DRAT AISHEET MUSTNERS IBEPOBSERRVVEDESIDUES
TING
THE INFORMATION
ACCUMULATEDMPANY OR ED HEREIN IS BELITS EVED
ADVIBE SED TOCCONFIRM INBUT IADVANCEAOFANEED TOBE
THEEIN�FORMATIONAIS
CURRENT. APPLICABLE. AND SUITABLE TO THEIR CIRCUMSTANCES.
Page: 3
ENCLOSED --LAST PAGE
LAST PAGE --SEE ATTACHMENT PAGE

MATERIAL SAFETY
DATA SHEET
Drew Divisions 24—HOUR
ASHLAND CHEMICAL. INC. Emergency Telephcne
t One Drew ((201) 263P7600..Telextoor
136444 FAX (20 ) 263.4482 1 [phone]
Phone
:n
DEFINITIONS
is intended for use with Material Safety Data Sheets supplied by the Drew Chemical Corporation.
This definition page
Recipients of these data sheets should consult the OSHA Safety
and Health Standards (29 CFR 1910). particularly
I — Personal Protective Equipment. for
subpart G — Occupational Health and Environmental Control, and subpart
Occupational Health and Safety Hazards
general guidance on control of potential
SECTION IV (cont)ECT10N
1
PRODUCT IDENTIFICATION
EXTINGUISHING MEDIA: Following National Fire
Protection Association criteria.
GENERAL OR GENERIC ID: Chemical family or product
FIREFIGHTING PROCEDURES: Minimum equipment to
description.
protect firefighters from toxic products of vaporization.
DOT HAZARD CLASSIFICATION: Product meets DOT
combustion or decomposition in fire situations. Other
criteria for hazards listed
firefighting hazards may also be indicated.
SECTION II
SPECIAL FIRE AND EXPLOSION HAZARDS: States
COMPONENTS
hazards not covered by other sections.
Components are listed in this section if they present a
NFPA CODES: Hazard ratings assigned by the National
Fire Protection Association.
physical or health hazard and are present at or above
1 % in the mixture. if a component is identified as a
V
CARCINOGEN by NTP. IARC, or OSHA as of the date
be listed and footnoted in this
sSECTION
HEALTH HAZARD DATA
on the MSDS. it will
section when present at or above 0.1 % in the product
PERMISSIBLE EXPOSURE LIMIT.• For product
Negative conclusions concerning carcinogenicity are not
THRESHOLD LIMIT VALUE For product
reported Additional health information may be found in
subject to the reporting
EFFECTS OF ACUTE OVEREXPOSURE: Potential local
Section V. Components
requirements of Section 313 of SARA Title III are
and systemic effects due to single or short term
the and skin or through inhalation
identified in the footnotes in this section, along with
may be listed if
overexposure to eyes
or ingestion
typical percentages. Other components
deemed appropriate.
EFFECTS OF CHRONIC OVEREXPOSURE Potential local
Exposure recommendations are for components. OSHA
and systemic effects due to repeated or long term
the eyes and skin or through inhalation
Permissible Exposure Limits (PELS) and American
overexposure to
Conference of Governmental Industrial Hygienists
or ingestion.
(ACGIH) Threshold Limit Values (TLVs) appear on the .
identification. Other
FIRST AID: Procedures to be followed when dealing
line with the component
recommendations appear as footnotes.
with accidental overexposure.
PRIMARY ROUTE OF ENTRY: Based on properties and
SECTION III
expected use.
PHYSICAL DATA
SECTION VI
BOILING POINT. Of product if known. The lowest
BEAr'TIVITY DATA
value of the components is listed for mixtures.
HAZARDOUS POLYMERIZATION: Conditions to avoid to
VAPOR PRESSURE: Of product if known. The highest
prevent hazardous polymerization resulting in a large
value of the components is listed for mixtures.
release of energy.
SPECIFIC VAPOR DENSITY: Compared to AIR = 1. If
STABILITY: Conditions to avoid to prevent hazardous or
the Specific Vapor Density of a product is not known,
violent decompositiom
the value is expressed as lighter or greater than air.
INCOMPATIBILITY: Materials and conditions to avoid to
SPECIFIC GRAVITY: Compared to WATER = I. If
prevent hazardous reactions.
Specific Gravity of product is not known, the value is
SECTION VII
expressed as less than or greater than water.
SPILL OR LEAK PROCEDURES
pH: If applicable.
PEFZCENT VOLATILES: Percentage of material with
425 degrees Fahrenheit and
Reasonable precautions to be taken and methods of
and disposal. Consult federal,
initial boiling point below
vapor pressure above 0.1mm Hg at 68 F.
containment, clean—up
state and local regulations for accepted procedures and
EVAPORATION RATE Indicated as faster or slower
any reporting or notification requirements.
than ETHYL ETHER, unless otherwise stated
SECTION VIII
§ICIIO_NI V
PROTECTIVE EQUIPMENT TO BE USED
FIRE AND EXPLOSION DATA
Protective equipment which may be needed when
FLASH POINT: Method identified
handling the product
EXPLOSION LIMITS: For product if known. The lowest
SECTION IX
value of the components is listed for mixtures.
SPECIAL PRECAUTIONS OR OTHER COMMENTS
HAZARDOUS DECOMPOSITION PRODUCTS: Known or
from heating.
Covers any relevant points not previously mentioned
expected hazardous products resulting
burning or other reactions.
ADDITIONAL COMMENTS
Containers should be either reconditioned by CERTIFIED
firms or properly disposed of by APPROVED firms. Disposal of
containers should be in _accordance
fr applicable
,�� with
misuse of aEMPTIED� containers (drums pailshetc.). Referbto Sections

a
MATEnIAL SAFETY
DATA SHEET
Drew Divisions Eme: gency Telephone
ASHLAND CHE(-tiCAL. INC
one -Drew Plaza. Boonton. New Jersey 07005 1 [phone] or
Phone [phone]Telex 136s4A FAX [phone] (800) 2-74-5263
WRICO OXY-11 CORROSION INHIBITOR Page:
000115
THIS MSOS COMPLIES WITH 29 CFR 1910.1200 (THE HAZARD COMMUNICATION STANDARD
sssaasassssssssassssaassssssssagassssssssssasaasssaasssssasasssaassssssssassssasasssssasassssassssssssssssassss
Product Name: WRICO OXY-11 CORROSION INHIBITOR
FMC CORP. / LITHIUM DIVISION
449 NORTH COX ROAD ATTN: A/P
P. 0. BOX 3925
GASTONIA NC 28016
Data Sheet No• 0218084-004.0O2
00 10 001 31860-063 Supersedes: 05/23/94
Print Date: 10/15/94
PRODUCT: 8267
INVOICE: 324776
INVOICE DATE: 07/05/94
T0: 449 CORP. COXIROADM DIVISION
GASTONIA
General or Generic ID: CORROSION INHIBITOR
IF
INGPREQUIREMENTS,OFTSARADTIIT E IIICSECTION 31,3 AARRE{IDENTIFIEDE N THIS ESERCTEPIOONR
ECTION•
SEE DEFINITION PAGE FOR CLARIFICATION Note
Percent PEL TLV
INGREDIENT ( 1)
1-10
SODIUM SULFITE
CAS x: 7757-83-7
Notes:
( 1) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
.
212.00 Deg F
Boiling Point for COMPONENT( 85-100%)
( 100.00 Deg C)
@ 760.00 = H9
17.50 — Hg
Vapor Pressure for COMPONENT( 85-100%)
@ 68.00 Deg.?
` ='!.=: ^=S Ci
> 1.00
Specific 'vapor Density AIR = 1
NOV1 7 � � @ Deg F �
Specific Gravity
1994 25.00
ii��1iJJ t7 ( 25.00 Deg C)
85-100%
Percent Vclatiles
Co 0
SLOWER THAN ETHER
Evaporation Rate
8.1
pH
CLEAR, LIGHT- PINK LIQUID
Appearance
LIQUID
State �-■� r,r
rmS3'TJI�i r i ter■ ra^r�T7^ nm
FLASH POINT NOT APPLICABLE
EXPLOSIVE L:MIT NOT APPLICABLE
EXTINGUISH:NG MEDIA: WATER FOG
AL DECOMPOSITION OR COMBUSTION MAY PRODUCE:. TOXIC FUMES, SULFUR
HAZARDOUS DECOMPOSITION PRODUCTS: THERM
OIOX:OE, CARBON DIOXIDE AND CARBON MONOXIDE
FIREFIIG WITH
TINGE ROCEDUREES: WEAR FULL BODYAPROTECREAT IING AFPA(RATUS FIRES.
FULL FACEPIECE OPERATED IN THE POS:TINE
DEMAND
AND
NFPA CODES: HEALTH- 1 FLAMMABILITY- 0 REACTIVITY- 0
PERMISSIBLE EXPOSURE LEVEL: NOT ESTABLISHED; SEE SECTION VIII.
EFFECTS OF ACUTE OVEREXPOSURE:
SYMPTOMS MAY INCLUDE STINGING. TEARING REDNESS. AND SWELLING.
EYES - EXPOSURE CAUSES EYE IRRITATION.
BREATHING - OF MIST BY SULFITE SENSITIVE INDIVIDUALS MAY CAUSE AN ALLERGIC REAETION SIMILAR TO THAT DESCR:BEO
UNDER INGESTING. EXPERIENCE AN
EO
SULFITE -SENSITIVE UILS.UPON
INGESTION OF
VES IACUTODASTFMAYA TACK(POSSIBLYALIFEGITIIREATENING) C REACTION LOSS OF�Z
CONSC:OUSNESS OR ANAPHYLACTIL� SHOCK. LARGE DOLES MAY PRODUCE VIOLENT GASTROINTESTINAL COLIC AND DEPRESSION
OF THE CENTRAL NERVOUS SYSTEM. MAY
SKIN SKINPOSURE CAUSES SKINAIIRRITATIO BY EXPOS1. URE INCLUDE
To THIS MATERIAL.
BURNING, AND SKIN DAMAGE. PRE-EXISTIN
DISOR
ERS
FIRST AID:
ON
IMMEDICLOTHIFLUSH WITH
REAUSE,FOR AT LEAST 15 MINUTES. REMOVE CONTAMINATED CLOTHING. LAUNDER
IF

MATERIAL SAFE i Y
DATA SHEET
000115
24-HOUR
Drew Divisions Emergency Telephone
AS`+LANC C-i•_MICAL .tiC
rt ne Grew P+aza. B_,="ton. New _ersey 07,=0= 1 (806) 324- 263 or
C
/Pnone [phone]Telex 136444 FAX [phone] (00) 274-53
WRICO OXY-11 CORROSION INHIBITOR
IF IN EYES10jMMEDIATELY IMMEDIATE MEDICAL AMOUNTSOFWATER FOR AT LEAST 15 MINUTES, LIFTING UPPER AND LOWER LIDS
OCC
ING IPECAC
UP OR
IF PLACING IMMEDIATELY TWO NEVEROGIVETANYTHINGAND NBY MOUCE �ITONANBUNCONSCIOUSVPERSON. GET MEDICAL BY
ATTENTION IMMEDIATELY.
IF BREATHED: REMOVE INDIVIDUAL TO FRESH AIR.
PRIMARY ROUTE(S) OF ENTRY:
SKIN CONTACT, INHALATION
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMPATIBILITY: AVOID CONTACT WITH:. STRONG OXIDIZING AGENTS, STRONG MINERAL ACIDS., STRONG ORGANIC ACIDS
IL
r�� �-Jr-7f�T"1■ � � �
STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED:
SMALL SPILL: ABSORB LIQUID ON VERMICULITE. FLOOR ABSORBENT OR OTHER ABSORBENT MATERIAL.
LARGE BEPE1NtCOMPLET COMPLETED. NOT STOPWSPILLGATRSOU PROTECTIVE
DIKEPMENT AREAOF SPILL LD BE O PREVENT SPREADFROM ING. G.EA OPUMPSPILL
LIQUIDUNTIL
TOCSALVAGE HAS
TANK
SHREMAININGLIQUID
MAY
BE TAKEN UP ON SAND. CLAY. EARTH , FLOOR ABSORBENT, OR OTHER ABSORBENT MATERIAL
AND
fbVELED INTO
Page: 2
WASTE DISPOSAL METHOD:
E WITH ALL LOCAL, STATE AND FEDERAL REGULATIONS.
SMALL SPILL: DISPOSE OF IN ACCORDANC
E WITH ALL APPLICABLE LOCAL, STATE AND FEDERAL REGULATIONS.
LARGE SPILL: DISPOSE OF IN ACCORDANC
RESPIRATORY D RESC RATORIIS ORVAASPTDEVOESANEPROPERTINENVRONMENTALTCONiR_OL100 M REGULATIONSADLSOVPERMIR
pROTHER N
gpMNNTSST/RA7VERCONTROLSRSHOULDRBEPIMPLEMENT ODTOIREDUCESEXPOSRESrctY EwIrnscNT SUPPLIEecJ. Et:GlnecKinu
VENTIBBELOWNLEVELPROVIDE
OVEREXPOSUREMECHANICAL (FROM KNOWN, SUSPECTED/OR OR LOCAL
PP RENTiADVERSEEEFFECTSjN TO MAINTAIN EXPOSURE
PROTECTIVE GLOVES: NATURAL RUBBER
COMPLIANCE IN OREGULATIONS RE
EYE PABEEGL FSHIELD
BN
IONS ALSOPERMOTHERTYPESAFETYGLAASSES. (CONSULT YOUR INDUSTRIAL
VISED HOWEVER. REU
HYGIENIST).
ENT REPEATED OR PROLONGED SKIN CONTACT, WEAR IMPERVIOUS CLOTHING AND B00 S.
OTHER PROTECTIVE EQUIPMENT: TO PREV
KEEP FROM FREEZING.
CONTAINERS OF THIS MATERIAL MAY BE HAZARDOUS ARD PRECAUTIONS GIVEN EMPTIED
DATAASHEET MUST BEPOBSERVEDESIDUE
(VAPOR, LIQUID. AND/OR SOLID), ~AE_
BE WHETHER
ORIGINATING
&LATHELET ACCURATE LIA_
THE INFORMATIONACCUBE SINADVNCEOFNED THAT THE INFORMATION THE COMPANY OR NOT.
CURRENT, APPLICABLE, AND SUITABLE TO THEIR CIRCUMSTANCES.

Drew Divisions l v "/ 24-HOER
, reWD CHE'.�Si n Emergency Telephone ,
--MATERIAL SAFETY � t One Crew Plaza. Boonton.. New ,,e-sey 07005 1(606) 324-1133 o r
DATA SHEET pPhone (20'. 263-76007elex 1364—'4 =4X (201! 263-»182 1 (800) -274-5263
000733 DREWAMINE 1791 CORROSION INHIBITOR
Page: 1
THIS MSDS COMPLIES WITH 29 CFR 1910.1200 (THE HAZARD COMMUNICATION STANDARD)
s•ssssssssssssssssssssesssssasassssssassssssassasssssssasssasssssssasssasssasssssssssssssssssssssssssstssssessss
Product Name: DREWAMINE 1791 CORROSION INHIBITOR
Data Sheet No: 0193535-004.002
OD 10 120 31860-063 Prepared: 08/17/94
FMC CORP. / LITHIUM DIVISION Sursedes: /15/94
"S NORTH COX ROAD ATTN: A/P Prpeint Date: 10//94
P. 0. BOX 3925 PRODUCT: 4534
GASTONIA INVOICE: 329992
NC 28016 INVOICE DATE: 08/24/94
T0: SION
49 NORTH COX LITHIUM
DA�VINN.A/P
GASTONIA
• I
General or Generic ID: CORROSION INHIBITOR
IF PRESENT, IARC. NTP AND OSHA CARCINOGENS AND CHEMICALS SUBJECT TO THE REPORT-
ING REQUIREMENTS OF SSEE TITLE III SP TIOFORICLARIFICATION3 ARE DENTIFIED IN THIS SECTION.
DEFININGREDIENT Percent PEL TLV Note
MORpHOLINE 40-55 20'PPM - SKIN 20 PPM - SKIN ( 1)
CAS 0: 110-91-8
Notes:
( 1) TAKENATO PREVENTMABSORPTION�So TTFHATTTTHEVETRALLV ANDBSORRPELOAREFNOTTHIS
INVALIDATED. APPROPRIATE
SECTIONMV.
EASURES SHOULD BE
OSHA/ACGIH SHORT TERM EXPOSURE LIMIT (STEL) FOR MORPHOLINE IS 30 PPM.
for COMPONENT( 55-70%) 22.00 Deg F
Boiling Point ( 1
00.00 Deg C)
@ 760:00 mm Fig
Vapor Pressure NOT APPLICABLE
LIGHTER THAN AIR
Specific Vapor Density
1.002
Specific Gravity @ 77.00 Deg F
E►..0 LJL' (::l D:' stv►t
." ( 25.00 Deg C) \
>95%
Percent Velatiles
Evaporation Rate NOT APPLICABLE
12.5
pH a CLEAR TO SIGHTLY HAZY
Appearance LIQUID
State
FLASH FOIN- NOT APPLICABLE
EXPLOSIVE LIMIT (LOWEST VALUE OF COMPONEN-) LOWER - 1.8% UPPER - 1C.8%
EXTINGUISHING MEDIA: ALCCHOL FOAM OR WATER FOG OR CARBON DIOXIDE OR DRY CHEMICAL
HAZARDOUS DECOMPOSITION PRODUCTS: MAY FORM 'OXIC MATERIALS:. CARBON DIOXIDE AND CARBON MONOXIDE, NITROGEN
COMPOUNDS, ETC.
FIREFIIGHTING PROCEDURES:
WEAR FULL CONTAINEDDY BREATCTION IwNG APPARATUSWITH FIGHTING FULL FACEPIECE OPERATED 1N THE POSITIVE
PRESSUR
DEMAND
AND
NFPA CODES: HEALTH- 3 FLAMMABILITv- 0 REACTIVITY- 1
PERMISSIBLE EXPOSURE LEVEL: NOT ESTABLISHED FOR PRODUCT. SEE SECTION Ii.
EFFECTS OF ACUTE OVEREXPOSURE:
EYES - EXPOSURE CAUSES IRREVERSIBLE EYE DAMAGE. SYMPTOMS MAY 1NCLLDE STINGING. TEARING. REDNESS. SWELLING,
CORNEAL DAMAGE AND BLINDNESS.
BREATHING - EXCESSIVE INHALATION OF VAPORS CAN CAUSE NASAL AND RESPIRATORY :RRITATION.
SWALLOWING - CAN CAUSE SEVERE GASTROINTESTINAL IRRITATION. VOMITING. DIARRHEA. SWEATING. WEAKNESS. HEADACHE.
SKIN INCLUDSUREDCAUSESBSEV RE SKINDRYIRRITATION.NG AND PROLONNG GEDBRNSEFANDESEVERESSKIN OAMAGE.URE MAY DRY �PRE�EXISTI GIN PSK:N MAY
DISORDERS MAY BE AGGRAVATED BY EXPOSURE TO THIS MATERIAL.
FIRST AID:
IF ON SKIN:
IMMEDIATELYINGUSLAUNOEEXPOSED
AREAA WITH
T WATER
FOR AT LEAST
ORE 15MINUTES. GET MEDICAL ATTENTION. REMOVE
CONTINUED ON PAGE: 2

•f /.-:Jnf*n
MATERIAL SAFETY
DATA SHEET
Drew Divisions Emergency Telephone
cJ,_&
ASHL%+ND-ir-`N11CA` 'N 1 (606) 324-113-3 or
\One Drew Plaza. Boonton. New Jersey
7005 �so2 1 [phone]
Phone [phone] i_i_x 136z--
DREWAMINE 1791 CORROSION INHIBITOR
000733 CEEESM
REMOVE CONTAMINATED SHOES PROMPTLY. DISCARD SHOES SATURATED WITH THIS PRODUCT.
IF INa�SIOIMMMEDIIMMEDIATE FLUSH WITH TE MEDICAL LARGE
AMOUNTS
OF WATER FOR AT LEAST 15 MINUTES, LIFTING UPPER AND LOWER LIDS
NALLY
IF SWALLOWED: DONOTVOMITING.
IMMEDIATELCIAN OR TRANSIINK TWOO AN SSES OF WAFACILINY� GIVE ANYTHING BY MOUTH TO
AN UNCONSCIOUS
IF
IF BREATHED: IF
FHAFFEECTED REMOVE
IVE ARTIFICI�ALLTO RESPIRATION. KEEP IF PERSONIWARM. QUIET NG IS CAND�GET ADMINISTER OXYGEN.
ATTENTION.
PRIMARY ROUTE(S) OF ENTRY:
INHALATION. SKIN CONTACT. SKIN ABSORPTION
EFFECTS OF CHRONIC OVEREXPOSURE:
OVEREXPOSURE OTTO RY THIS MLAATERIALS AND I,1(OR
AY I�AVATEPRE EXISTING S) HAS EDISORDERS OF THESE ORGANS EN SUGGESTED AS A CAUSE FIN HUMANS:, LIVER
THE FOLLOWING FECTS IN
ABNORMALITIES. KIDNEY DAMAGE. EYE DAMAGE
.r��t rlr�riTi � ■ �'�'��
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMPATIBILITY: AVOID CONTACT WITH:. STRONG OXIDIZING AGENTS. STRONG ALKALIES. STRONG ORGANIC ACIDS
.-
■ •■•li �i30 ■ ■9
fi
Page: 2
S RELEASED OR SPILLED:
STEPS TO BE TAKEN IN CASE MATERIAL I
ABSORBENT OR OTHER ABSORBENT MATERIAL.
SMALL SPILL: ABSORB LIQUID ON VERMICULITE, FLOOR ,
LARGE SPILL: PERSONS NOT WEARING PROTECTIVE EQUIPMENT SHOULDLL TO PREVENT ABSORBENFROM T, OR OTHER LIQUID
TOESOF SPILL UNTIL ALVAGERIAL
BEEN COMPLETED. STOP SPILL AT SOURCE. DIKE AREA OF SPILL TO PREVENT SPREADING. PUMP LIQUID TO SALVAGE
TANK
SIIREE REMED AINING
LIQUID MAY
NERSE TAKEN UP ON SANG. CLAY,
AND
WASTE DISPOSAL M_E1`HOD:
SMALL SPILL: DISPOSE OF IN ACCORDANCE WITH ALL LOCAL. STATE AND FEDERAL REGULATIONS.
, STATE AND FEDERAL REGULATIONS.
LARGE SPILL: DISPOSE OF IN ACCORDANCE WITH ALL APPLICABLE LOCAL
ED
CTION
RESPIRATORY PROTECTION -
IF WORKPLACE
SUPPSURERESPIT(S) OISPRODUCT OR IN ABSENCE ANY
COMO F PROPERXENVDIRONMENTALECONTROL.
II). RESPIRATORS (NEGATIVE PRESSURE TYPE) UNDER SPECIFIED
OSHA REGULATiONS ALSO PERMIT OTHER NIOSH/MSHA
CONDITIONS (SEE YOUR INDUSTRIAL HYGIENIST). ENGINEERING OR ADMINISTRA IVE CONTROLS SHOULD BE IMPLEMENT
TO REDUCE EXPOSURE.
ON- PRS)IDE SUFFICIENT MECHANICAL (GENERAL AND/OR LOCAL E.XFiAUST) '%EN ILATION TO MAINTAIN EXPOSURE
VENTILATION-
BELO)
PROTECTIVE GLOVES: WEAR RESISTANT GLOVES SUCH AS:. AA'.URAL RUBBER
SH:ELD
BNIN CLCEWITH �GINARE
EYE PROTECTION:
AICIO:ALASHGOGGLENDFY(CONSULT
DVNHOWEVER,OSHAREGULATIONS ALSO PERM RAGSSES
HYG1ENitT).
OTHER PROTECTIVE EQUIPMENT: TO PREVENT' SKIN CON'AC'. WEAR IMPERVIOUS CLO'H;NG AND BOOTS.
IN
CONTAINERS OF THIS MATERIAL MAY BE HAZARDOUS WARD PRECAUTIONS GIVEN INPTHES CAhASHEETSMUST ABE OBSERVED.
(VAPOR. (VAPOR. LIQUID, AND/OR SOLID),
THE I2�MATOCrPAYJTNHEEREA�BE NIBUT
IAAANEDTEWHETHER
ANG
RMINADVNCEOFETHATTHE NFORMATIONIS
wTHT1EONOROTRECIPINgSAEOVSED TO COF
CURRENT. APPLICABLE. AND SUITABLE TO THEIR CIRCUMSTANCES.
- - __ —. r•e•

MATERIAL SAFETY
DATA SHEET
Drew Divisions 304-
ASHLANDCHEN11C-L.!NC
% Emergency TeIephor
r�One Drew Plaza. Boonton. New Jersey 07005 1 [phone] 0
/Phone [phone]Telex 136444 FAX [phone] [phone]
oo178D DREWPHOS 2300 DEPOSIT CONTROL AGENT Page:
THIS MSOS COMPLIES WITH 29 CFR 1910.1200 (THE HAZARD COMMUNICATION STANDARD)
sassasasasssaasssaassssasaasassssastiasasassasaassaasasasaaasaaaaaassaassasssaassaasasasssssasaasssasasaasasasssa
Product Name: DREWPHOS 2300 DEPOSIT CONTROL AGENT
Data Sheet No: 0221077-004.001
OD t0 124 31860-063 Prepared: 05/25/94
Supersedes: 06/08/93
FMC CORP. / LITHIUM DIVISION Print Date: 08/13/94
449 NORTH COX ROAD ATTN: A/P PRODUCT: 4827
P. 0. BOX 3925 INVOICE: 302107
GASTONIA NC 28016 INVOICE DATE: 11/02/93
70: 9 LITHIUM DIVISION 44CORP.TCOXROAN:A/P
GASTONIA
sn aa.rsssrr� r^mra attrT3'Td E:m ■ -Till ■ T'
General or Generic ID: DEPOSIT CONTROL AGENT
�zsa•�^rn�■ri! i i ■
IF PRESENT, IARC. NTP AND OSHA CARCINOGENS AND CHEMICALS SUBJECT TO THE REPORT-
ING REQUIREMENTS OF SARA TITLE III SECTION 313 ARE IDENTIFIED IN THIS SECTION.
SEE DEFINITION PAGE FOR CLARIFICATION
TLV Note
INGREDIENT
SODIUM HEXAMETAPHOSPHATE
CAS 0: 10124-56-8
ACRYLIC ACID POLYMER. SODIUM SALT
CAS 0: 9003-04-7
SODIUM HYDROXIDE
CAS 0: 1310-73-2
Percent PEL
1-10 15 MG/M3
1-10
3 2 MG/M3 - CEILING
10 MG/M3 ( 1)
2 MG/M3 - CEILING
( 2)
Notes:
( 1) PEL AND TLV ARE FOR TOTAL NUISANCE PARTICULATES.
THE PEL/TLV FOR RESPIRABLE DUST IS 5 AG/CUib.
( 2) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
ENT( 70-85%)
for COMPONENT( Boiling Point
20.00 Deg F
( 7060.00 Deg C).
@ 760.00 mmHg
Vapor Pressure for COMPONENT( 70-85%)
17.50 mmHg
@ 68.CO Deg F
( 20.00 Deg C)
HEAVIER THAN AIR
Specific Vapor Density
I
Specific Gravity
@ 77.00 Deg F
( 25.CO Deg C)
70-85%
Percent Volatiles
SLOWER THAN ETHER
Evaporation Rate
13.1
pH
CLEAR. PALE STRAW
Appearance
LIQUID
State �T� �■-T twf Y3�TT,
■
FLASH POINT NOT APPLICABLE
EXPLOSIVE LIMIT NOT APPLICABLE
EXTINGUISHING MEDIA: REGULAR FOAM OR WATER FOG OR CARBON DIOXIDE OR DRY CHEMICAL
CARBON DIOXIDE AND CARBON
HAZARDOUS DECOMTHERMAL DECOMPOSITION OR COMBUSTION MAY PRODUCE:.
IDE. TOSITIOMONOMEDUCTS:
FACEPIECE
OPERATED IN THE POSITIVE
IG
FIREFIIG ROCETINDURES:DEMAND WEAR FULL CCONTAINEDPROTBTION W1IENAFIAGHTING FIRESS WITH FULL
AND
SSURE
HAZARDS: CAN REACT WITH CHEMICALLY REACTIVE METALS SUCH AS
AIR.
ALUMINUM. ZINC. MAGNESIUM.
SPECIAL FIRE S EXPLOSION
COPPER ETC. TO RELEASE HYDROGEN GAS WHICH CAN FORM EXPLOSIVE MIXTURES WITH
NFPA CODES: HEALTH- 3 FLAMMABILITY- 0 REACTIVITY- 1
AUU 2 9 1994
�
+.11{.
Vr.S..I'VIY3S
CONTINUED ON PAGE: 2

w Drew Divisions `4_HuuK
ASHLAND CHEM1CAL.INC Emergency Telephone
MATERIAL SAFETY t One Drew Plaza. Boonton. New Jersey 07005 1 [phone] or
DATA SHEET Phone t201) 263-7600 Telex 136 =44 FAX [phone] [phone]
001780 DREWPHOS 2300 DEPOSIT CONTROL AGENT Page: 2
PERMISSIBLE EXPOSURE LEVEL: NOT ESTABLISHED FOR PRODUCT. SEE SECTION II.
EFFECTS OF ACUTE OVEREXPOSURE:
EYES - EXPOSURE TO LIQUID OR VAPOR CAUSES IRREVERSIBLE EYE DAMAGE. SYMPTOMS MAY INCLUDE STINGING, TEARING,
REDNESS SWELLING CORNEAL DAMAGE AND BLINDNESS.
SKIN - CAUSES BURNS. pbSSIBLE DEEP ULCERATION.
BREATHING - MIST CAN CAUSE DAMAGE TO NASAL AND RESPIRATORY PASSAGES.
SWALLOWING - RESULTS IN SEVERE DAMAGE TO MUCOUS MEMBRANES AND DEEP TISSUES.
FIRST AID: ATER FOR AT
IF ONCS�NN:IMMEDIATEOTHINGu LAUNDER OSED AREA
IWITH
TEDWC CLOTHING BEFORE RE�USEINUTES. GET MEDICAL ATTENTION. REMOVE
REMOVE CONTAMINATED SHOES PROMPTLY. DISCARD SHOES SATURATED WITH THIS PRODUCT.
IF IN EYES: IMMEDIATELY
IMMEDIATE MEDICAL AMOUNTS OF WATER FOR AT LEAST 15 MINUTES, LIFTING UPPER AND LOWER LIDS
IF PHYSICIAN IS NOT IMMEDIATELY AVAILABLE, CONTINUE FLUSHING WITH WATER.
DO NOT USE CHEMICAL ANTIDOTE.
IF SWALLOWED: DO NOT INDUCE VOMITING. VOMITING WILL CAUSE FURTHER DAMAGE TO THE THROAT. DILUTE BY GIVING
WATER. GIVE MILK OF MAGNESIA. KEEP WARM, QUIET. GET MEDICAL ATTENTION IMMEDIATELY.
IF
IF BREATHED: EANGFHASFSTOPPEDRGGIVEEARTIFICIALLRESPIRATTIiON. AIR.
EEP PERSONIF ING IS WARM, QUIETCAND,GET ADMINISTER
EDICAL OXYGEN.
PRIMARY ROUTE(S) OF ENTRY:
INHALATION. SKIN CONTACT
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMPATIBILITY: AVOID CONTACT WITH: STRONG MINERAL ACIDS.. REACTIVE METALS SUCH AS ALUMINUM AND MAGNESIUM,
ORGANIC MATERIALS, STRONG ORGANIE ACIDS. COPPER
STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED:
SMALL SPILL: ABSORB LIQUID ON VERMICULITE, FLOOR ABSORBENT OR OTHER ABSORBENT MATERIAL.
LARGE SPILL: PERSONS NOT WEARING PROTECTIVE EQUIPMENT SHOULD BE EXCLUDED FROM AREA OF SPILL UNTIL CLEAN-UP HAS
BEEN COMPLETED. STOP SPILL AT SOURCE. DIKE AREA OF SPILL TO PREVENT SPREADING. PUMP LIQUID TO SALVAGE
TANK. REMAINING LIQUID MAY BE TAKEN UP ON SAND, CLAY. EARTH. FLOOR ABSORBENT, OR OTHER ABSORBENT MATERIAL
AND SHOVELED INTO CONTAINERS.
WASTE DISPOSAL ME1-00:
SMALL SPILL: DISPOSE OF IN ACCORDANCE WITH ALL LOCAL, STATE AND FEDERAL REGULATIONS.
LARGE SPILL: DISPOSE OF IN ACCORDANCE WITH ALL APPLICABLE LOCAL. STATE AND FEDERAL REGULATIONS.
RESPIRATORY PROTECTION: IF WORKPLACE EXPOSURE LIMITS) OF PRODUCT OR ANY COMPONENT IS EXCEEDED (SEE SECTION
II). A NIOSH/MSHA APPROVED AIR SUPPLIED RESPIRATOR IS ADVISED IN ABSENCE OF PROPER ENVIRONMENTAL CONTROL.
OSHA REGULA-IONS ALSO PERMIT OTHER NIOSH/MSHA RESPIRATORS (NEGATIVE PRESSURE TYPE) UNDER SPECIFIED
CONDITIONS (SEE YOUR INDUS RIAL HYGIENIST). ENGINEERING OR ADMINIS RATIVE CONTROLS SHOULD BE IMPLEMENTED
TO REDUCE EXPOSURE.
VENTILATION:
PROVIDE SUFFICIENT MECHANICAL (GENERAL AND/OR LOCAL EXHAUST) VENTILATION TO MAINTAIN EXPOSURE
E
PROTECTIVE GLOVES: WEAR RESISTANT GLOVES SUCH AS:
EYE PROTECTION: CHEMICAL SPLASH GOGGLES IN COMPLIANCE WITH OSHA REGULATIONS ARE ADVISED: HOWEVER. OSHA
REGULATIONS ALSO PERMIT OTHER TYPE SAFETY GLASSES. CONSULT YOUR SAFETY REPRESENTATIVE.
OTHER PROTECTIVE EQUIPMENT: TO PREVENT REPEATED OR PROLONGED SKIN CONTACT. WEAR IMPERVIOUS CLOTHING AND BOOTS.
CONTAINERS OF THIS MATERIAL MAY BE HAZARDOUS WHEN EMPTIED. SINCE EMPTIED CONTAINERS RETAIN PRODUCT RESIDUES
(VAPOR. LIQUID. ANDIOR SOLID). ALL WIZARD PRECAUTIONS GIVEN IN THIS DATA SHEET MUST BE OBSERVED.
THE INFORMATION ACCUMULATED HEREIN IS BELIEVED TO BE ACCURATE BUT IS NOT WARRANTED TO BE WHETHER ORIGINATING
WITH THE COMLICABLOR NOT. RECIPIENTS ARE ADVISED TO CONFIRM IN ADVANCE OF NEED THAT THE INFORMATION IS

Drew Divisions 24—HOUR
ASHLAND CHEMICAL. INC. Emergency Telephonf
MATERIAL SAFETY 1 One Drew Plaza, Boonton, New Jersey 07005 1(606) 324-1133 or
DATA SHEET Phone [phone]/Telex 136444 FAX [phone] [phone]
000262 DREWPLEX 1621 BOILER WATER TREATMENT Page:
THIS MSDS COMPLIES WITH 29 CFR 1910.1200 (THE HAZARD COMMUNICATION STANDARD)
sssssssssssssssssssssssssssassssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssss
Product Name: DREWPLEX 1621 BOILER WATER TREATMENT
Data Sheet No: 0246766-002.002
OD 10 935 - Prepared: 04/11/94
DREW INDUSTRIAL DIVISION Supersedes: 03/09/94
309 WEST BELT LINE BLVD. PRODUCT: 5408 Print Date: 04/23/94
ANDERSON INVOICE:
SC 29625 INVOICE DATE:
TO: DREW INDUSTRIAL DIVISION
309 WEST BELT LINE BLVD.
DISTRICT MANAGER ANDERSON
SC 29625
General or Generic ID: BOILER WATER TREATMENT
IF PRESENT IARC, NTP AND OSHA CARCINOGENS AND CHEMICALS SUBJECT TO THE REPORT-
ING REQUIRlzMENTS OF SEE DEFINITIONTITLE III
FOR ICLARIFICATIONIED IN THIS SECTION.
INGREDIENT Percent PEL TLV Note
ACRYLIC ACID POLYMER, SODIUM SALT 10-25 ( 1)
CAS 0: 9003-04-7
ACRYLIC ACID POLYMER. SODIUM SALT 1-10 ( 2)
CAS s: 9003-04-7
SODIUM HYDROXIDE ' 1-10 2 MG/M3 - CEILING 2 MG/M3 - CEILING ( 3)
CAS 0: 1310-73-2
Notes:
( 1) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
cl r•c, i,a ,vvi ajiAuLixiEw rim Aha.a A—'r—AL.
( 3) AS SODIUM HYDROXIDE. NIOSH RECOMMENDS 2 MG/CUM - 15 MINUTE CEILING.
Boiling Point for PRODUCT > 2 0.00 Deg F
( 100.00 Deg C)
® 760.00 mm Hg
Vapor Pressure for PRODUCT < 17.50 mm Hg
@ 68.00 Deg FF
( 20.00 Deg C)
Specific Vapor Density AIR = 1 .60
Specific Gravity @ 77.002Deg F
( 25.00 Deg C)
70-85%
Percent Volatiles
Evaporation Rate SLOWER THAN ETHER
13.2
PH
CLEAR, LIGHT YELLOW
Appearance LIQUID
State
HOMOG SOLN
Form
FLASH POINT NOT APPLICABLE
EXPLOSIVE LIMIT NOT APPLICABLE
EXTINGUISHING MEDIA: WATER FOG
HAZARDOUS DECOMPOSITION PRODUCTS: MAY FORM TOXIC MATERIALS:, CARBON DIOXIDE AND CARBON MONOXIDE, TOXIC MONOMER
FUMES
FIREFIGHTING SURE DEMAND AND FULL CCOONTAINEDDY BREATCTIONHING
WHEAPPARATUSIGHTING WITH A FULL FACEPIECE OPERATED IN THE POSITIVE
WATER MAY BE USED TO KEEP FIRE -EXPOSED CONTAINERS COOL UNTIL FIRE IS OUT.
SPECICOOPPIERREETC.TEXPLOSION ELLASE HYDROGENNGREACT WITH AS WHICH CANNFORMM EEXPLOSIVICALLY VEEIMIXTURES WALS ITH AICH R,ALUMINUM, ZINC. MAGNESIUM,
ACRYLIC EMULSIONS WILL NOT BURN. THEY MAY SPATTER IF TEMPERATURE EXCEEDS BOILING POINT (212 DEG.F).
DRIED POLYMER FILMS ARE CAPABLE OF BURNING.
CONTINUED ON PAGE: 2

Drew Divisions 24—HOUR
ASHLAND CHEMICAL. INC. Emergency Telephone -
MATERIAL SAFETY VAO
One Drew Plaza, Boonton, New Jersey 07005 1(606) 324-1133 or
DATA SHEET Phone [phone]/Telex 136444 FAX [phone](800) 274-5263
000262 DREWPLEX 1621 BOILER WATER TREATMENT Page: 2
NFPA CODES: HEALTH- 3 FLAMMABILITY- 0 REACTIVITY- 1
PERMISSIBLE EXPOSURE LEVEL: SEE SECTION II
EFFECTS OF ACUTE OVEREXPOSURE:
EYES - CAN CAUSE SEVERE IRRITATION, REDNESS, TEARING, BLURRED VISION: LIQUID CAN CAUSE SEVERE OR PERMANENT EYE
DAMAGE.
SKIN - CAN CAUSE SEVERE IRRITATION AND EXCESSIVE OR PROLONGED CONTACT CAN RESULT IN BLISTERS AND BURNS.
BREATHINGSUREFIMIEXTENSDUST CAN
AAY CAUSE SEVERE
IRRITSUE ATION
TO THE RESPIRATORY TRACT AND MUCOUS MEMBRANES AND IF
EXPSWALLOWING - CAN CAUSE NAULEA, VOMITING, DIARRHEA, IRRITATION AND BURNS TO STOMACH, MOUTH, THROAT, ETC.
FIRST AID:
IF ONCSNI�IMMMEEDDICLOTHINGFLUSH
EXPOSED
UNDER AREA
IWITH
TEDWC 0 FOR
ING AT BEFORE T 15 MINUTES, GET MEDICAL ATTENTION. REMOVE
ONTDE.
REMOVE CONTAMINATED SHOES PROMPTLY. DISCARD SHOES SATURATED WITH THIS PRODUCT.
IF INOCEYES:
IMMEDIATELY
ILLUUFLUSHMEDICAL ION.
WITH
AMOUNTS WATER FOR AT LEAST 15 MINUTES, LIFTING UPPER AND LOWER LIDS
SIO
IF SWALLOWED: DO UNCONSCIOUS VULLINNG. IMMEDIATELYICIAN OR DRIPORTO AN SSERGENCYAF R. NEVER GIVE ANYTHING BY MOUTH TO
Y.
IF BRBBREATHINGFHASFSTO PELDRGIIVVE ARTIFICVE IALLTO RESPIRATTIiON. KEEP PERSONIF IWARM, QUIET IS DIFFICULT,
MEDICAL ATTENTION•
PRIMARY ROUTE(S) OF ENTRY:
INHALATION, INGESTION, SKIN CONTACT
EFFECTS OF CHRONIC OVEREXPOSURE:
OVEREXPOSURE TO THIS MATERIAL (OR ITS COMPONENTS) HAS BEEN SUGGESTED AS A CAUSE OF THE FOLLOWING EFFECTS IN
HUMANS:, LUNG DAMAGE, EYE DAMAGE
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMTEMPERAATURES OVER 120NF. COPPER,'TEMPESSIVE ERATUREHEAT REACTIVE EXTkEM S , STRONG METALS
AS ALUMINUM AND MAGNESIUM,
STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED:
SMALL SPILL: PERSONS NOT WEARING PROPER PERSONAL PROTECTIVE EQUIPMENT SHOULD BE EXCLUDED FROM AREA OF SPILL.
ABSORB LIQUID ON VERMICULITE, FLOOR ABSORBENT OR OTHER ABSORBENT MATERIAL.
SWEEP UP MATERIAL FOR DISPOSAL OR RECOVERY.
LARGE
BEENLCOMPLEED. STOPWS ILLGATRSOU SOURCE, DIKE AREAEQUIPMENT
OF SHOULD BE
PREVENT SPREADOM ING. G. PUEA OF MPILIQUIDITOCSALVAGE �S
TANK. REMAINING LIQUID MAY BE TAKEN UP ON SAND, CLAY, EARTH, FLOOR ABSORBENT, OR 07HER ABSORBENT MATERIAL
AND SHOVELED INTO CONTAINERS.
WASTE DISPOSAL METHOD:
SMALL SPILL: DISPOSE OF IN ACCORDANCE WITH ALL LOCAL, STATE AND FEDERAL REGULATIONS.
LARGE SPILL: DISPOSE OF IN ACCORDANCE WITH ALL APPLICABLE LOCAL, STATE AND FEDERAL REGULATIONS.
W T
RESPIRATORY PROTECTION: IF WORKPLACE EXPOSURE LIMIT(S) OF PRODUCT OR ANY COMPONENT IS EXCEEDED (SEE SECTION
II), A NIOSH/MSHA APPROVED AIR SUPPLIED RESPIRATOR IS ADVISED IN ABSENCE OF PROPER ENVIRONMENTAL CONTROL.
OSHA REGULATIONS ALSO PERMIT OTHER NIOSH/MSHA RESPIRATORS (NEGATIVE PRESSURE TYPE) UNDER SPECIFIED
CONDITIONS (SEE YOUR INDUSTRIAL HYGIENIST). ENGINEERING OR ADMINISTRATIVE CONTROLS SHOULD BE IMPLEMENTED
TO REDUCE EXPOSURE.
VENTILATION: PROVIDE SUFFICIENT MECHANICAL (GENERAL AND/OR LOCAL EXHAUST) VENTILATION TO MAINTAIN EXPOSURE
BELOW TLV(S).
PROTECTIVE GLOVES: WEAR RESISTANT GLOVES SUCH AS:, NEOPRENE
EYE PROTECTION: CHEMICAL SPLASH GOGGLES AND FACE SHIELD (8- MIN.) IN COMPLIANCE WITH OSHA REGULATIONS ARE
ADVISED• HOWEVER, OSHA REGULATIONS ALSO PERMIT OTHER TYPE SAFETY GLASSES. (CONSULT YOUR INDUSTRIAL
HYGIENIST).
OTHER PROTECTIVE EQUIPMENT: TO PREVENT SKIN CONTACT. WEAR IMPERVIOUS CLOTHING AND BOOTS.
EYEWASH STATION, EMERGENCY SHOWER.
roNTINUED ON PAGE: 3

-' - Drew Divisions L4—HOUR
ASHLAND CHEMICAL, INC. Emergency Telephone
MATERIAL SAFETY One Drew Plaza, Boonton, New Jersey 07005 1(606) 324-1133 or
DATA SHEET © Phone [phone](relex 136444 FAX [phone](800) 274-5263
000262 DREWPLEX 1621 BOILER WATER TREATMENT Page:
CONTAINERS OF THIS MATERIAL MAY BE HAZARDOUS *IEN EMPTIED. SINCE EMPTIED CONTAINERS RETAIN PRODUCT RESIDUES
(VAPOR. LIQUID. AND/OR SOLID). ALL HAZARD PRECAUTIONS GIVEN IN THIS DATASHEET MUST BE OBSERVED.
THE INFORMATION ACCUMULATED HEREIN IS BELIEVED TO BE ACCURATE BUT IS NOT WARRANTED TO BE WITHER ORIGINATING
WITH THE COMPANY OR NOT. RECIPIENTS ARE ADVISED TO CONFIRM IN ADVANCE OF NEED THAT THE INFORMATION IS
CURRENT, APPLICABLE. AND SUITABLE TO THEIR CIRCUMSTANCES.
rsem v1r_7--Q7V ATTACHMENT PAGE ENCLOSED --LAST PAGE

Drew Divisions 24—HOUR
Emergency Telephone
ASHLAND CHEMICAL. INC.
MATERIAL SAFETY One Drew Plaza, Boonton, New Jersey 07005 1(606) 324-1133 or
DATA SHEET o Phone [phone]/Telex 136444 FAX [phone](800) 274-5263
DEFINITIONS
This definition page is intended for use with Material Safety Data Sheets supplied by the Drew Chemical Corporation.
Recipients of these data sheets should consult the OSHA Safety and Health Standards (29 CFR 1910), particularly
subpart G — Occupational Health and Environmental Control, and subpart I — Personal Protective Equipment, for
general guidance on control of potential Occupational Health and Safety Hazards.
SECTION I
PRODUCT IDENTIFICATION
GENERAL OR GENERIC ID: Chemical family or product
description.
DOT HAZARD CLASSIFICATION: Product meets DOT
criteria for hazards listed.
SECTION II
COMPONENTS
Components are listed in this section if they present a
physical or health hazard and,.are presept,.at . or above
1% in the mixture. If a component' is identified as a
CARCINOGEN by NTP, IARC, or OSHA as of the date
on the MSDS, it will be listed and footnoted in this
section when present at or above 0.1 % in the product
Negative conclusions concerning carcinogenicity are not
reported. Additional health information may be found in
Section V. Components subject to the reporting
requirements of Section 313 of SARA Title III are
identified in the footnotes in this section, along with
typical percentages. Other components may be listed if
deemed appropriate.
Exposure recommendations are for components. OSHA
Permissible Exposure Limits (PELS) and American
Conference of Governmental Industrial Hygienists
(ACGIH) Threshold Limit Values (TLVs) appear on the
line with the component identification. Other
recommendations appear as footnotes.
SECTION III
PHYSICAL DATA
BOILING POINT: Of product if known. The lowest
value of the components is listed for mixtures.
VAPOR PRESSURE: Of product if known. The highest
value of the components is listed for mixtures.
SPECIFIC VAPOR DENSITY: Compared to AIR = 1. If
the Specific Vapor Density of a product is not known,
the value is expressed as lighter or greater .than air.
SPECIFIC GRAVITY. Compared to WATER = 1. If
Specific Gravity of product is not known, the value is
expressed as less than or greater than water.
pH: If applicable.
PERCENT VOLATILES: Percentage of material with
initial boiling point below 425 degrees Fahrenheit and
vapor pressure above 0.1 mm Hg at 68 F.
EVAPORATION RATE: Indicated as faster or slower
than ETHYL ETHER, unless otherwise stated.
SECTION IV
FIRE AND EXPLOSION DATA
FLASH POINT: Method identified.
EXPLOSION LIMITS: For product if known. The lowest
value of the components is listed for mixtures.
HAZARDOUS DECOMPOSITION PRODUCTS: Known or
expected hazardous products resulting from heating,
burning or other reactions.
SECTION IV (cont)
EXTINGUISHING MEDIA: Following National Fire
Protection Association criteria
FIREFIGHTING PROCEDURES: Minimum equipment to
protect firefighters from toxic products of vaporization,
combustion or decomposition in fire situations. Other
firefighting hazards may also be indicated.
SPECIAL FIRE AND EXPLOSION HAZARDS: States
hazards not covered by other sections.
NFPA CODES: Hazard ratings assigned by the National
'Fire Protection- Association.
SECTION V
HEALTH HAZARD DATA
PERMISSIBLE EXPOSURE LIMIT. For product
THRESHOLD LIMIT VALUE: For product
EFFECTS OF ACUTE OVEREXPOSURE: Potential local
and systemic effects due to single or short term
overexposure to the eyes and skin or through inhalation
or ingestion.
EFFECTS OF CHRONIC OVEREXPOSURE: Potential local
and systemic effects due to repeated or long term
overexposure to the eyes and skin or through inhalation
or ingestion.
FIRST AID: Procedures to be followed when dealing
with accidental overexposure.
PRIMARY ROUTE OF ENTRY: Based on properties and
expected use.
SECTION VI
REACTIVITY DATA
HAZARDOUS POLYMERIZATION: Conditions to avoid to
prevent hazardous polymerization resulting in a large
release of energy.
STABILITY: Conditions to avoid to prevent hazardous or
violent decomposition.
INCOMPATIBILITY: Materials and conditions to avoid to
prevent hazardous reactions.
SECTION VII
SPILL OR LEAK PROCEDURES
Reasonable precautions to be taken and methods of
containment, clean—up and disposal. Consult federal,
state and local regulations for accepted procedures and
any reporting or notification requirements.
SECTION VIII
PROTECTIVE EQUIPMENT TO BE USED
Protective equipment which may be needed when
handling the product
SECTION IX
SPECIAL PRECAUTIONS OR OTHER COMMENTS
Covers any relevant points not previously mentioned.
ADDITIONAL COMMENTS
Containers should be either reconditioned by CERTIFIED firms or properly disposed of by APPROVED firms. Disposal of
containers should be in accordance with applicable laws and regulations. "EMPTY" drums should not be given to
individuals. Serious accidents have resulted from the misuse of "EMPTIED" containers (drums,pails,etc.). Refer to Sections
IV and IX

J.T.SAKER INC. 222 RED SCHOOL LANE, PHILLIPSBURG, NJ 08865
' M A T E R I A L S A F E T Y D A T A S H E E T
24-HOUR EMERGENCY TELEPHONE -- 19081 859-2151 /
CHEMTREC 0 t 800) 424-9300 -- NATIONAL RESPONSE CENTER # (800 ) 424-8802
S4034 -06 SODIUM HYDROXIOE,PELLETS PAGE: 1
EFFECTIVE: 11/18/94 ISSUED: 01/03/95
J.T.BAKER INC., 222 RED SCHOOL- LANE• PHILL-IPSBURG, NJ 08365
SECTION I - PRODUCT IDENTIFICATION
PRODUCT NAME: SODIUM HYDROXIDE,PELLETS
COMMON SYNONYMS: CAUSTIC SODA; SODIUM HYDRATE; LYE
CHEMICAL FAMILY: INORGANIC SODIUM COMPOUNDS
FORMULA: NAOH
FORMULA WT.: 40.00
CAS NO.: 1310-73-2
NIOSH/RTECS NO»: W34900000
PRODUCT USE: LABORATORY REAGENT
PRODUCT CODES: 5104,5312,3730,5045*372393736v372993734t5565v5O22,3726,3728
37180721,3722
----------------- -----------
PRECAUTIONARY LABELING
BAKER SAF-T-DATA* SYSTEM
HEALTH - 3 SEVERE tPOISON)
FLAMMABILITY - 0 NONE
% REACTIVITY - 2 MODERATE
CONTACT - 4 EXTREME 1CORR OSIVE)
.- LABORATORY PROTECTIVE EQUIPMENT
GOGGLES; LAB COAT; VENT HOOD; PROPER GLOVES
U.S. PRECAUTIONARY LABELING
POISON DANGER
HARMFUL IF INHALED. CAUSES SEVERE BURNS. MAY BE FATAL IF SWALLOWED. REACTS
VIOLENTLY WITH WATER ANO ACIDS.
DO NOT GET IN EYES, ON SKIN, ON CLOTHING. AVOID SPATTERING BY SLOWLY ADDING
TO SOLUTION. AVOID BREATHING DUST- KEEP IN TIGHTLY CLOSED CONTAINER. USE
WITH ADEQUATE VENTILATION- WASH TH7RCUGHL•Y AFTER HANDLING.
INTERNATIONAL LABELING
CAUSES SEVERE BURNS.,
KEEP OUT OF REACH OF CHILDREN- IN CASE OF CONTACT WITH EYES, RINSE IMMEDIATELY
WITH PLENTY OF WATER AND SEEK MEDICAL ADVICE. WEAR SUITABLE GLOVES AND
EYE/FACE PROTECTION.
CONTINUED ON PAGE: Z
FIE Lithium Division
FEB 1 3:1995
Health Services

J.T.BAKER INC. 222 RED SCHOOL LANE, PHILLIPSB'JRGv NJ 08865
M A T E R I A L S A F E T Y D A T A S H E E T
24-HOUR EMERGENCY TELEPHONE -- I908) 859-2151
CHEMTREC # [phone] -- NATIONAL, RESPONSE CENTER # 18(D) 424-8802
S4034 -06 SODIUM HYDROXIDE,PELLETS PAGE: 2
EFFECTIVE: 11/18/94 ISSUED: 01/03/95
PRECAUTIONARY LABELING ICONTINUEDI
SAF-T-DATA* STORAGE COLOR CODE: WHITE STRIPE ( STORE SEPARATELY)
----- ------------------
SECTION II - COMPONENTS
COMPONENT CAS NO. WEIGHT x OSHA/PEL ACGIH/TLV
SODIUM HYDROXIDE 1310-73-2 98-100 2 MG/M ? M!G/M
THE TLV AND PEL LISTED DE':OTE CEILING LIMITS.
----------------- ----------
SECTION III - PHYSICAL DATA
801-LING POINT: 1390 C t 2534 F)
( AT 760 MM! HG)
MELTING POINT:B C 1604 F)
tAT 760 MM H )
SPECIFIC GRAVITY: 2.13
(H20=1)
SOLUBILITY(H20): APPRECIABLE (>lOb)
- PH: 14.0 (I.OM; SOLUTION)
ODOR THRESHOLD (P.P.M.): N/A
COEFFICIENT WATER/OIL DISTRIBUTION: N/A
VAPOR PRESSURE I MMHGI: <1
(20 C)
VAPOR DENSITY (AIR=1 ): N/A
EVAPORATION RATE: N/A
% VOLATILES BY VOLUME: 0
(21 C)
PHYSICAL STATE: SOLID
APPEARANCE C ODOR: WHITE PELLETS OR FLAKES. ODORLESS.
-----------------------------
SECTION IV - FIRE AND EXPLOSION HAZARD DATA
FLASH POINT ICLOSED CUP)-- N/A NFPA 704M RATING: 3-0-1
AUTOIGNITION TEMPERATURE: N/A
CONTINUED ON PAGE: 3

J.T.BAKER INC. 222 RED SCHOOL LANE. PHIL LIPSBURG• NJ 08865
M A T E R I A L S A F E T Y D A T A S H E E T
24—HOUR EMERGENCY TELEPHONE -- [phone]
• CHEMTREC # [phone] -- NATIONAL RESPONSE CENTER 4 [phone]
S4034 —06 SODIUM HYDROXIDEsPELLETS PAGE: 3
EFFECTIVE: 11/18/94 ISSUED: 01/03/95
SECTION IV — FIRE AND EXPLOSION HAZARD DATA (CONTINUED)
FLAMMABLE LIMITS: UPPER — N/A LOWER — N/A
FIRE EXTINGUISHING MEDIA
USE EXTINGUISHING MEDIA APPROPRIATE FOR SURROUNDING FIRE.
SPECIAL FIRE —FIGHTING PROCEDURES
FIREFIGHTERS SHOULD WEAR PROPER PROTECTIVE EOUIPMENT AND SELF—CONTAINED
BREATHING APPARATUS WITH FULL FACEPIECE OPERATED IN POSITIVE PRESSURE
MODE, FLOOD WITH WATER SPRAY TO PREVENT SPLASHING OF MATERIAL -
UNUSUAL FIRE E EXPLOSION HAZARDS
CONTACT WITH j'OISTURE OR WATER MAY GENERATE SUFFICIENT HEAT TO IGNITE
COMBUSTIBLE MATERIALS. REACTS WITH MOST M=TALS TO PRODUCE HYDROGEN GAS9
WHICH CAN FORM AN EXPLOSIVE MIXTURE WITH AIR.
TOXIC GASES PRODUCED
NONE IDENTIFIED
EXPLOSION DATA—NSITIVITY TO MECHANICAL IMPACT
NONE I DENT I• I EO-
EXPLOSION DATA —SENSITIVITY TO STATIC DISCHARGE
NONE IDENTIFIED -
SECTION V — HEALTH HAZARD DATA
THRESHOLD LIMIT VALUE ( TLV/"f'WA) = 2 MG/M
TLV LISTED DENOTES CEILING LIMIT.
SHORT—TERM EXPOSURE LIMIT ISTEL): NOT ESTABLISHED
PERMISSIBLE EXPOSURE LIMIT IPEL): 2 MG/M
PEL LISTED DENOTES CEILING LIMIT.
TOXICITY OF COMPONENTS
INTRAPERITONEAL MCUSE LD50 FOR SODIUM HYDROXIDE 40 M G/KG
CONTINUED ON .PAGE: 4

` J.T.BAKER INC. 222 RED SCHOOL LANEY PHILLIPSSURGY NJ 08865
M A T E R I A L S A F E T Y D A T A S H E E T
24-HOUR EMERGENCY TELEPHONE -- [phone]
CHEMTREC m [phone] -- NATIONAL RESPONSE CENTER # [phone]
S4034 -06 SODIUM HYDROXIDEYPELLETS PAGE: 4
EFFECTIVE: 11/18/94 ISSUED: 01/03/95
----------- ------------------
----------
SECTION V - HEALTH HAZARD DATA ;CONTINUED)
CARCINOGENICITY: NTP: NO IARC: NO Z LIST: NO OSHA REG: NO
CARCINOGENICITY
NONE IDENTIFIEn.
REPRODUCTIVE EFFECTS
NONE IDENTIFIED.
EFFECTS OF OVEREXPOSURE
INHALATION: SEVERE IRRITATION OR BURNS OF RESPIRATORY SYSTEMv
PULMONARY EDEMAS LUNG INFLAMMATIONS MAY CAUSE RESPIRATORY
SYSTEM DAMAGE
SKIN CONTACT_ SEVERE IRRITATION OR BURNS
EYE CONTACT: SEVERE IRRITATION OR BURNS, PERMANENT EYE DAMAGE
SKIN ABSORPTI N: NONE IDENTIFIED
INGESTION: IS HARMFUL AND MAY BE FATAL. SEVERE BURNS TO MOUTHY
THROATY AND STOMACH, NAUSEA, VOMITING
CHROMIC EFFECTS: NONE IDENTIFIEDD
TAOET ORGANS
EYES, SKINY RESPIRATORY SYSTEMS LUNGS
MEDICAL CONDITIONS GENERALLY AGGRAVATED BY EXPOSURE
DAMAGED SKIN
PRIMARY ROUTES OF ENTRY
INHALATION• INGESTION, EYE CONTACTY SKIN CONTACT
EMERGENCY AND FIRST AID PROCEDURES
_ INGESTION: CALL A PHYSICIAN. IF SWALLOWED• DO NOT INDUCE IOMITING. IF
CONSCIOUS, GIVE LARGE AMOUNTS OF WATER. FOLLOW WITH DILUTED
VINEGARY FRUIT JUICE OR WHITES OF EGGS BEATEN WITH WATER.
INHALATION= IF INHALED, REMOVE TO FRESH AIR. IF NOT BREATHING, GIVE
ARTIFICIAL RESPIRATION. IF 3REATHING IS DIFFICULT. GIVE
OXYGEN. PROMPT ACTION IS ESSENTIAL.
CONTINUED ON PAGE: 5

J.T.BAKER INC. 2?2 RED SCHOOL LANE, PHILLIPSBURG, NJ 08865
M A T E R I A L S A F E T Y D A T A S H E E T
24-HOUR EMERGENCY TELEPHONE -- t9081 859-2151
CHEMTREC : I830) 424-9300 -- NATIONAL RESPONSE CENTER 4 (8001 424-8802
S4034 -06 SODIUM HYDROXIDE,PELLETS PAGE: 5
EFFECTIVE: 11/18/94 ISSUED: 01/03/95
-------------------------------
SECTION V - HEALTH HAZARD DATA lCONTINUED)
SKIN CONTACT: IN CASE OF CONTACT, IMMEDIATELY FLUSH SKIN WITH PLENTY OF
WATER FOR AT LEAST 15 MINUTES WHILE REMOVING CONTAMINATED
CLOTHING AND SHOES. WASH CLOTHING BEFORE RE -USE.
EYE CONTACT: IN CASE OF EYE CONTACT, IMMEDIATELY FLUSH WITH PLENTY OF
WATER FOR AT LEAST 15 MINUTES.
NOTES TO PHYSICIAN
IN CASES OF SEVERE ESOPHAGEAL CORROSION, THE USE OF THERAPEUTIC DOSES OF
STEROIDS SHOULD BE CONSIDERED. GENERAL SUPPORTIVE MEASURES WITH CONTINUAL
MONITORING OF GAS EXCHANGE, ACID -BASE BALANCE, ELECTROLYTES, AND FLUID
INTAKE ARE ALSO REQUIRED.
SARA/TITLE III HAZARD CATEGORIES AND LISTS
ACUTE: YES . CHRONIC: YES FLAMMABILITY: NO PRESSURE: NO REACTIVITY: NO
t EXTREMELY HAZARDOUS SUBSTANCE: NO
CERCLA HAZARDOUS SUBSTANCE: YES CONTAINS SODIUM HYDROXIDE t RQ = 1000 LBS)
SARA 313 TOXIC .(.HEMTCALS: YES CONTAINS SODIUM HYDROXIDE
GENERIC CLASS: GENERIC CLASS REMOVED FROM CFR: 7!1/9i
TSCA INVENTORY: YES
----------------------
_ SECTION VI - REACTIVITY DATA
STABILITY: STABLE HAZARDOUS POLYMERIZATION: WILL NOT OCCUR
CONDITIONS TO AVOID: MOISTURE
INCOMPATIBLES: WATER• STRONG ACIDS, MOST COMMON METALS, COMBUSTIBLE
!MATERIALS, ORGANIC 'MATERIALS, ZINC, ALUMINUM,
PEROXIDES, HALOGENATED HYDROCARSONS
DECOMPOSITION PRODUCTS: NONE IDENTIFIED
CONTINUED ON PAGE: 6

J.T.BAKER INC. 222 RED SCHOOL LANE, PHILLIPSBURG, NJ 08865
' M A T E R I A L S A F C T Y 0 A T A S H E E T
24-HOUR EMERGENCY TELEPHONE -- (9081 859-2151
CHEMTREC # 1800) 424-9300 -- NATIONAL• RESPONSE CENTER # t80D) 424-8802
S4034 -06 SODIUM HYDROXIDE,PELLETS PAGE: 6
EFFECTIVE= 11/18/94 ISSUED: 01/03/95-
--------------
SECTION VII - SPILL S DISPOSAL PROCEDURES
STEPS TO BE TAKEN IN THE EVENT OF A SPILL OR DISCHARGE
WEAR SELF-CONTAINED BREATHING APPARATUS A40 FULL PROTECTIVE CLOTHING, WITH
CLEAN SHOVELv CAREFULLY PLACE MATERIAL INTO CLEAN, DRY CONTAINER 440
COVER; REMOVE FROM AREA. FLUSH S°ILL AREA WITH WATER.
DISPOSAL PROCEDURE
DISPOSE IN ACCORDANCE WITH ALL APPLICABLE FEDERAL, STATE, AND LOCAL
ENVIRONMENTAL REGULATIONS.
EPA HAZARDOUS WASTE NUMBER- D0029 D003 iCORROSIVE, REACTIVE WASTE)
SECTION VIII - INDUSTRIAL PROTECTIVE EQUIPMENT
VENTILATION= USE GENERAL OR LOCAL EXHAUST VENTILATION TO MEET TLV
REQUIREMENTS.
RESPIRATORY PROTECTION: RESPIRATORY PROTECTION REQUIRED IF AIRBORNE
CONCENTRATION EXCEEDS TLV. AT CONCENTRATIONS UP TO
100 PPM, A HIGH -EFFICIENCY PARTICULATE RESPIRATOR IS
RECOMMENDED, ABOVE THIS LEVEL, A SELF-CONTAINED
BREATHING APPARATUS IS ADVISED-
EYE/SKIN PROTECTION: SAFETY GOGGLES, UNIFORPi, APRON, NEOPRENE GLOVESARE
.� RECOMMENDED.
---------------------------------
SECTION IX - STORAGE AND HANDLING PRECAUTIONS
SAF-T-DATA* STORAGE COLOR CODE: WHITE STRIPE t STORE SEPARATELY)
STORAGE REQUIREMENTS
KEEP CONTAINER TIGHTLY CLOSED. STORE IN CORROSION -PROOF AREA. STORE IN A
DRY AREA. ISOLATE FRO4 INCOMPATIBLE MATERIALS.
CONTINUED ON PAGE: 7

J.T.BAKER INC. 222 RED SCHOOL LANE, PHILLIPSBURG? NJ 08865
M A T E R I A L S A F E T Y D A T A S H E E T
24-HOUR EMERGENCY TELEPHONE -- [phone]
CHEMTREC 9 [phone] -- NATIONAL RESPONSE CENTER t (800) 424--8802
S4034 -06 SODIUM HYDROXIDErPELLETS PAGE: 7
EFFECTIVE: 11/18/94 ISSUED: 01/03/95
------ ---------------
SECTION X - TRANSPORTATION DATA AND AD')ITIONAL INFORMATION
'3
DOMESTIC (D.O.T.)
PROPER SHIPPING NAME: SODIUM HYDROXIDES SOLID
HAZARD CLASS: 8
UN/NA: UN1823 REPORTABLE QUANTITY: lODO Lg S. PACKAGING 'GROUP: II
LABELS: 8 CORROSIVE
REGULATORY REFERENCES: 49CFR 172.101
INTERNATIONAL ( I . M.O. )
PROPER SHIPPING -NAME: SODIUM HYDROXIDE? SOLID
I.M.O. PAGE: 8225
HAZARD CLASS: 8
UN: UN1823 MARINE POLLUTANTS: NO PACKAGING GROUP: II
LABELS: 8 CORROSIVE
REGULATORY REFERENCES: 49CFR PART 176; IMDG CODE
AIR (I.C.A.O.)
PROPER SHIPPING.-IIIAME:
SODIUM HYDROXIDE, SOLID
HAZARD CLASS:
8
UN: UN1823
PACKAGING GROUa: II
LABELS: 8 CORROSIVE
_
REGULATORY REFERENCES:
49CFR PART 175; ICAO WE BELIEVE THE TRANSPORTATION
DATA AND REFERENCES CONTAINED HEREIN TO BE FACTUAL AND
�
THE OPINION OF QUALIFIED EXPERTS. THE DATA IS MEANT AS
A GUIDE TO THE OVERALL CLASSIFICATION OF THE PRODUCT
AND IS NOT PACKAGE SIZE SPECIFIC? NOR SHOULD T_T BE
TAKEN AS A WARRANTY OR REPRESENTATION FOR w".-iICH THE
COMPANY ASSUMES LEGAL RESPONSIBILITY.=== THE
INFORMATION IS OFFERED SOLELY FOR YOUR CONST.DERATION•
INVESTIGATION, AND VERIFICATION. ANY USE OF T`iE
INFORMATION 'LUST BE 1DETERMINP-0 9Y THE USER TO BE IN
ACCORDANCE WITH APPLICABLE FE'_',ERAL, STATE, ANO LOCAL
LAWS AND REGULATIONS. SEE SHIPPER REQUIREMENTS 49CFR
171.2t CERTIFICATION 172.2049 AND EMPLOYEE TRAINING 49
CFR 173.1t51.
U.S. CUSTOMS HARMCNIZATION NUMBER: 28151100003
CONTINUED ON PAGE: 8

J.T.BAKER INC. 222 RED SCHOOL LANE, PHILLIPSBURG, NJ 08865
M A T E R I A L S A F E T Y D A T A S H E E T
24-HOUR EMERGENCY TELEPHONE -- [phone]
CHEMTREC 0 [phone] -- NATIONAL RESPONSE CENTER # [phone]
S4034 -06 SODIUM HYDROXIDE,PELLETS PAGE: 8
EFFECTIVE: 11/18/94 ISSUED: 01/03/95
NOTE: WHEN HANDLING LIQUID PRODUCTS, SECONDARY PROTECTIVE CONTAINERS MUST BE
USED FOR CARRYING.
-N/A = NOT APPLICABLE, OR NOT AVAILABLE;
N/E = NOT ESTABLISHED. -
THE INFORMATION IN THIS MATERIAL SAFETY DATA SHEET MEETS THE
REQUIREMENTS OF THE UNITED STATES OCCUPATIONAL SAFETY AND HEALTH ACT A40
REGULATIONS PROMULGATED THEREUNDER (29 CFR 1910.1200 ET. SEQ.1 AND THE
CANADIAN WORKPLACE HAZARDOUS MATERIALS INFORMATION SYSTEM. THIS DOCUMENT
IS INTENDED ONLY AS A GUIDE TO THE APPROPRIATE PRECAUTIONARY HANDLING OF
THE MATERIAL BY A PERSON TRAINED IN, OR SUPERVISED BY A PERSON TRAINED
IN, CHEMICAL HANDLING. THE USER IS RESPONSIBLE FOR DETERMINING THE
PRECAUTIONS AND DANGERS OF THIS CHEMICAL FOR HIS OR HER PARTICULAR
APPLICATION. DEPENDING ON USAGE, PROTECTIVE CLOTHING INCLUDING EYE AND
FACE GUARDS AND RESPIRATORS MUST BE USED TO AVOIb CONTACT WITH MATERIAL
OR BREATHING CHEMICAL VAPORS/FUMES.
EXPOSURE TO THIS PRODUCT MAY HAVE SERIOUS ADVERSE HEALTH EFFECTS. THIS
CHEMICAL MAY INTERACT WIT-i OTHER SUBSTANCES. SINCE THE POTENTIAL USES
ARE SO VARIED• BAKER CANNOT WARN OF ALL OF THE POTENTIAL DANGERS OF USE
OR INTERACTION WITH OTHER CHEMICALS OR MATERIALS. BAKER WARRANTS THAT
THE CHEMICAL MEETS THE SPECIFICATIONS SET FORTH ON THE LABEL.
BAKER DISCLAIMS ANY OTHER WARRANTIES, EXPRE-SSED OR IMPLIED WITH REGARD
TO THE PRODUCT .6—UPPLIED HEREUNDER, ITS MERCHANTABILITY OR ITS FITNESS
FOR A PARTICULAR PURPOSE.
THE USER SHOULD RECOGNIZE THAT THIS PRODUCT CAN CAUSE SEVERE INJURY AND
EVEN DEATH, ESPECIALLY IF IMPROPERLY HANDLED OR THE KNOWN DANGERS OF USE
ARE NOT HEEDED. READ ALL PRECAUTIONARY INFORMATION. AS NEW DOCUIPENTED
GENERAL SAFETY INFORMATION BECOMES AVAILABLE, BAKER WILL PERIODICALLY
REUSE THIS MATERIAL SAFETY DATA SHEET.
NOTE: CHEMTREC, CANUTEC, AND NATIONAL RESPONSE CENTER EMERGENCY TELEPHONE
NUMBERS ARE TO BE USED ONLY IN THE EVENT OF CHEMICAL EMERGENCIES INVOLVING
A SPILL, LEAK, FIRE, EXPOSURE, OR ACCIDENT INVOLVING CHEMICALS. ALL
NON -EMERGENCY QUESTIONS SHOULD BE DIRECTED TO CUSTOMER SERVICE
t 1-800-JTBAKER) FCR ASSISTANCE.
COPYRIGHT 1995 J.T.BAKER INC.
* TRADEMARKS OF J.T.3AKER INC.
AP?°OVED BY QUALITY ASSURANCE DEPARTMENT.
-- LAST PAGE --
"ISSUED 3Y VWR 02/04/95"

Drew Divisions 24-xoux
Emergency Telephone.
ASHLAND CHEMICAL, INC.
005 1(606) 324-1133 or
MATERIAL SAFETY t One Drew Plaza, Boonton, New Jersey 07
DATA SHEET O Phone [phone]o%relex 136444 FAX [phone](800) 274-5263
003576 AMERTROL 1123 DEPOSIT INHIBITOR Page:
THIS MSDS COMPLIES WITH 29 CFR 1910.1200 ('THE HAZARD COMMUNICATION STANDARD)
sssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssssassssssss
Product Name: AMERTROL 1123 DEPOSIT INHIBITOR
Data Sheet No: 0006724-002.001
OD 10 935 - Prepared: 02/10/95
DREW INDUSTRIAL DIVISION Supersedes: 02/02/95
Print Date: 02/18/95
309 WEST BELT LINE BLVD.
PRODUCT: 5214
ANDERSON INVOICE: -
SC 29625 INVOICE DATE:
TO: DREW INDUSTRIAL DIVISION
309 WEST BELT LINE BLVD.
DISTRICT MANAGER ANDERSON
SC 29625
• •• • •
General or Generic ID: DEPOSIT INHIBITOR
DOT Hazard Classification: NOT APPLICABLE
IF PRESENT IARC, NTP AND OSHA CARCINOGENS AND CHEMICALS SUBJECT TO THE REPORT-
ING REQUIR&ENTS OF SE TITLE
IT EIII SECTION
AGE 313 CLARIFICATION
IN THIS SECTION.
INGREDIENT % (by WT) PEL TLV Note
TETRAPOTASSIUM PYROPHOSPHATE 40-55 15 MG/M3 10 MG/M3 ( 1)
CAS 0: 7320-34-5
ACRYLIC POLYMER 1-10 ( 2)
CAS x: 9003-04-7
Notes:
( 1) PEL AND TLV ARE FOR TOTAL NUISANCE PARTICULATES.
( 2) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
• a.■• -.
Boiling Point for COMPONENT( 40-55%)
212.00 Deg F
( 100.00 Deg C)
@ 760.00 mm Hg
Vapor Pressure for COMPONENT( 40-55%)
17.50 mm Hg
Q 68.00 Deg'
( 20.00 Deg C)
HEAVIER THAN AIR
Specific Vapor Density
1.595
Specific Gravity
@( 77.00 Deg F
25.00 Deg C)
40-55%
Percent Volatiles
SLOWER THAN ETHER
Evaporation Rate
10.5
PH
CLEAR TO SLIGHTLY HAZY
Appearance
LIQUID
State
HOMOG SOLN
Form
•APMM7• • �'
FLASH POINT NOT APPLICABLE
EXPLOSIVE LIMIT NOT APPLICABLE
EXTINGUISHING MEDIA:
HAZARDOUS DECOMPOSITION PRODUCTS: MAY FORM:, pF10SPHDROUS COMPOUNDS, TOXIC MONOMER FUMES
FIREFIGHTING PROCEDURES: WEAR A SELF-CONTAINED BREATHING APPARATUS WITH A FULL FACEPIECE
NOF�S�MSDSESISTANT
OPERATED IN THE
PERSONAL PROTECTIVE
PRESSURE TDEMAND O THE PPERSONALHPAROTECTIVE APPROPRIATE
SECTIONEAR
EQUIPMENT.
SPECIAL FIRE & EXPLOSION HAZARDS: NO SPECIAL FIRE HAZARDS ARE KNOWN TO BE ASSOCIATED WITH THIS PRODUCT.
NFPA CODES: HEALTH- 2 FLAMMABILITY- 1 REACTIVITY- 0
Fat• •• ••
PERMISSIBLE EXPOSURE LEVEL: NOT ESTABLISHED FOR PRODUCT. SEE SECTION II.
EFFECTS OF ACUTE OVEREXPOSURE:
EYES - EXPOSURE MAY CAUSE MILD EYE IRRITATION. SYMPTOMS MAY INCLUDE STINGING. TEARING, AND REDNESS.
CONTINUED ON PAGE: 2

Drew Divisions 24—HOUR
• ASHLANDCHEMICAL INC. Emergency Telephone
MATERIAL SAFETY t One Drew Plaza, Boonton, New Jersey 07005 1(606) 324-1133 or
DATA SHEET Phone [phone]irelex 136444 FAX [phone] [phone] .
003576 AMERTROL 1123 DEPOSIT INHIBITOR Page: 2
SKIN - EXPOSURE MAY CAUSE MILD SKIN IRRITATION. PROLONGED OR REPEATED EXPOSURE MAY DRY THE SKIN. SYMPTOMS MAY
INCLUDE REDNESS, BURNING DRYING AND CRACKING, AND SKIN BURNS. PRE-EXISTING SKIN DISORDERS MAY BE
AGGRAVATED BY EXPOSURE Tb THIS MATERIAL.
BREATHING - EXPOSURE TO VAPOR OR MIST IS POSSIBLE.
SYMPTOMS MAY INCLUDE:
-IRRITATION (NOSE, THROAT RESPIRATORY TRACT)- PRE-EXISTING LUNG DISORDERS, E.G. ASTHMA -LIKE CONDITIONS,
MAY BE AGGRAVATED BY EXPOSURE TO THIS MATERIAL.
SWALLOWING - SINGLE DOSE ORAL TOXICITY IS LOW. SWALLOWING SMALL AMOUNTS DURING NORMAL HANDLING IS NOT LIKELY
TO CAUSE HARMFUL EFFECTS; SWALLOWING LARGE AMOUNTS MAY BE HARMFUL.
SYMPTOMS MAY INCLUDE•
-GASTROINTESTINAL IRRITATION (NAUSEA, VOMITING, DIARRHEA) -
FIRST AID:
IF ON SKIN: REMOVE CONTAMINATED CLOTHING. WASH EXPOSED AREA WITH SOAP AND WATER. IF SYMPTOMS PERSIST, SEEK
MEDICAL ATTENTION. LAUNDER CLOTHING BEFORE REUSE.
IF IN EYES: IF SYMPTOMS DEVELOP IMMEDIATELY MOVE INDIVIDUAL AWAY FROM EXPOSURE AND INTO FRESH AIR. FLUSH EYES
GENTLY WITH WATER FOR AT LAST 15 MINUTES WHILE HOLDING EYELIDS APART; SEEK IMMEDIATE MEDICAL ATTENTION.
IF SWALLOWED: IF SWALLOWED, SEEK MEDICAL ATTENTION. IF INDIVIDUAL IS DROWSY OR UNCONSCIOUS DO NOT GIVE
ANYTHING BY MOUTH PLACE INDIVIDUAL ON THE LEFT SIDE WITH THE HEAD DOWN. IF INDIVIDUAL IS CONSCIOUS AND
ALERT INDUCE VOMITING BY GIVING SYRUP OF IPECAC OR BY GENTLY PLACING TWO FINGERS AT THE BACK OF THE
THROAt. IF POSSIBLE, DO NOT LEAVE INDIVIDUAL UNATTENDED.
IF BREATHED: IF SYMPTOMS DEVELOP, IMMEDIATELY MOVE INDIVIDUAL AWAY FROM EXPOSURE AND INTO FRESH AIR. SEEK
IMMEDIATE MEDICAL ATTENTION- KEEP PERSON WARM AND QUIET. IF PERSON IS NOT BREATHING, BEGIN ARTIFICIAL
RESPIRATION. IF BREATHING fS DIFFICULT, ADMINISTER OXYGEN.
PRIMARY ROUTE(S) OF ENTRY:
SKIN CONTACT
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMPATIBILITY: AVOID CONTACT WITH:, STRONG MINERAL ACIDS., STRONG ORGANIC ACIDS
STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED:
SMALL SPILL: ABSORB LIQUID ON VERMICULITE, FLOOR ABSORBENT OR OTHER ABSORBENT MATERIAL.
LARGE SPILL: E55 NOT WEARING
EQUIPMENT SHOULD
REAREA OIIU ICHas
BEEN
COMPLETED. PSLLATSOUCE. DIKE OFSPILL BE EXCLUDED
SPREADING,PUMP LQDTOSALVAGE
TANK. REMAINING LIQUID MAY BE TAKEN UP ON SAND, CLAY, EARTH, FLOOR ABSORBENT, OR OTHER ABSORBENT MATERIAL
AND SHOVELED INTO CONTAINERS.
WASTE DISPOSAL METHOD:
SMALL SPILL: DISPOSE OF IN ACCORDANCE WITH ALL LOCAL, STATE AND FEDERAL REGULATIONS.
LARGE SPILL: DISPOSE OF IN ACCORDANCE WITH ALL APPLICABLE LOCAL, STATE AND FEDERAL REGULATIONS.
RESPIRATORY PROTECTION: IF OVEREXPOSURE HAS BEEN DETERMINED OR DOCUMENTED. A NIOSH/MSHA JOINTLY APPROVED AIR
SUPPLIED RESPIRATOR IS ADVISED IN ABSENCE OF PROPER ENVIRONMENTAL CONTROL. OSHA REGULATIONS ALSO PERMIT
OTHER NIOSH/MSHA RESPIRATORS UNDER SPECIFIED CONDITIONS. (SEE YOUR SAFETY EQUIPMENT SUPPLIER). ENGINEERING
OR ADMINISTRATIVE CONTROLS SHOULD BE IMPLEMENTED TO REDUCE EXPOSURE.
VENTILATION: PROVIDE SUFFICIENT MECHANICAL (GENERAL AND/OR LOCAL EXHAUST) VENTILATION TO MAINTAIN EXPOSURE
BELOW LEVEL OF OVEREXPOSURE (FROM KNOWN, SUSPECTED OR APPARENT ADVERSE EFFECTS).
PROTECTIVE GLOVES: WEAR RESISTANT GLOVES (CONSULT YOUR SAFETY EQUIPMENT SUPPLIER).
EYE PROTECTION: CHEMICAL SPLASH GOGGLES IN COMPLIANCE WITH OSHA REGULATIONS ARE ADVISED• HOWEVER, OSHA
REGULATIONS ALSO PERMIT OTHER TYPE SAFETY GLASSES. CONSULT YOUR SAFETY REPRESENTAtIVE.
OTHER PROTECTIVE EQUIPMENT: TO PREVENT REPEATED OR PROLONGED SKIN CONTACT, WEAR IMPERVIOUS CLOTHING AND BOOTS.
CONTAINERS OF THIS MATERIAL MAY BE HAZARDOUS WHEN EMPTIED.SINCE EMPTIED CONTAINERS RETAIN PRODUCT RESIDUES
(VAPOR, LIQUID, AND/OR SOLID), ALL HAZARD PRECAUTIONS GIVEN IN THE DATA SHEET MUST BE OBSERVED.
THE INFORMATION ACCUMULATED HEREIN IS BELIEVED TO BE ACCURATE BUT IS NOT WARRANTED TO BE WHETHER ORIGINATING
WITH THE COMPANY OR NOT. RECIPIENTS ARE ADVISED TO CONFIRM IN ADVANCE OF NEED THAT THE INFORMATION IS
CURRENT, APPLICABLE, AND SUITABLE TO THEIR CIRCUMSTANCES.
LAST PAGE --SEE ATTACHMENT PAGE ENCLOSED --LAST PAGE

•
Drew Divisions 24-HOUR
ASHLAND CHEMICAL. INC. Emergency Telephone
MATERIAL SAFETY t One Drew Plaza. Boonton. New Jersey 07005 1(606) 324-1133 or
DATA SHEET . Phone [phone]!Telex 136444 FAX [phone](800) 274-5263
001585 CATALYZED SULFITE CORROSION INHIBITOR Page: 1
THIS MSDS COMPLIES WITH 29 CFR 1910.1200 (THE HAZARD COMMUNICATION STANDARD)
ssssssssas:sssssssssasssssssasasassasssassssssassssssssssssssssassasssssssssssssssssssssssasssssssssssssssssssss
Product Name: CATALYZED SULFITE CORROSION INHIBITOR
Data Sheet
No: 0006719-003.001
OD 10 120 31860-074
Prepared:
05/23/94
FMC LITHIUM CORPORATION
Supersedes:
11/11/92
ATTN: B. TUMBLESON
Print Date:
08/13/94
HIGHWAY 161
PRODUCT: 5247
BESSEMER CITY
INVOICE: 327021
NC 28016
INVOICE DATE: 07/26/94
TO: FMC LITHIUM CORPORATION
ATTN• B. TUMBLESON
BESSEMER CITY
SECTI ON I -PRODUCT IDENTIFICATION
General or Generic ID: CORROSION INHIBITOR
IF PRESENT IARC, NTP AND OSHA CARCINOGENS AND CHEMICALS SUBJECT TO THE REPORT-
ING REQUIREMENTS OF SARA TITLE III SECTION 313 ARE IDENTIFIED IN THIS SECTION.
SEE DEFINITION PAGE FOR CLARIFICATION
INGREDIENT
SODIUM SULFITE
CAS 0: 7757-83-7
BENZOIC ACID
CAS 0: 65-85-0
Notes:
( 1) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
( 2) PEL/TLV NOT ESTABLISHED FOR THIS MATERIAL
Boiling Point NOT APPLICABLE
Vapor Pressure NOT APPLICABLE
Percent PEL
85-100
1-10
TLV
Note
( 1)
( 2)
Specific Vapor Density NOT APPLICABLE
Specific Gravity
77.00 Deg F
( 25.00 Deg C)
Percent Volatiles NOT APPLICABLE
Evaporation Rate NOT APPLICABLE
Appearance WHT-LT TAN/PINK SPECS/POWDER
State SOLID
Form POWDER
FLASH POINT NOT APPLICABLE
EXPLOSIVE LIMIT NOT APPLICABLE
EXTINGUISHING MEDIA:
HAZARDOUS DECOMPOSITION PRODUCTS: MAY FORM TOXIC MATERIALS:, TOXIC FUMES, SULFUR DIOXIDE
FIREFIGHTING PROCEDURES: WEAR SELF-CONTAINED BREATHING APPARATUS WITH A FULL FACEPIECE OPERATED IN THE POSITIVE
PRESSURE DEMAND MODE WHEN FIGHTING FIRES.
SPECIAL FIRE & EXPLOSION HAZARDS: NOT APPLICABLE
NFPA CODES: HEALTH- 1 FLAMMABILITY- 0 REACTIVITY- 0
DATA
PERMISSIBLE EXPOSURE LEVEL: NOT ESTABLISHED; SEE SECTION VIII.
EFFECTS OF ACUTE OVEREXPOSURE:
EYES - EXPOSURE TO LIQUID OR VAPOR CAUSES EYE IRRITATION. SYMPTOMS MAY INCLUDE STINGING, TEARING, REDNESS, AND
SWELLING.
SKIN - CAN CAUSE IRRITATION.
SULFITE -SENSITIVE INDIVIDUALS UPON INHALATION OF THIS PRODUCT MAY EXPERIENCE AN ALLERGIC REACTION SIMILAR TO
THAT DESCRIBED UNDER INGESTION.
SULFITE-SENSITIVE
NAUSEA, DIARRHEA, ITCHING SWEUPON LL NG, HIVES STION OF THIS
ASTiMACT YATTTTACK(POSSIBLYENCE AN ALIFEGTHREATEIC NINNGG);�LOSS OFIZED
CONSCIOUSNESS OR ANAPHYLACTIE SHOCK. LARGE DOPES MAY PRODUCE VIOLENT GASTROINTESTINAL COLIC AND DEPRESSION
OF THE CENTRAL NERVOUS SYSTEM.
CONTINUED ON PAGE: 2

Drew Divisions 24-xo(rR
Emergency Telephone
ASHLANDCHEMICAL.INC.
MATERIAL SAFETY t One Drew Plaza. Boonton. New Jersey 07005 1(606) 324-1133 or
DATA SHEET . Phone [phone],Telex 136444 FAX [phone](800) 274-5263
001585 CATALYZED SULFITE CORROSION INHIBITOR Page: 2.
FIRST AID:
IF ON SKIN:
THOROUGHLY
C LY WASH
EXPOSED
AREA WITH SOAP AND WATER. REMOVE CONTAMINATED CLOTHING. LAUNDER
CONTAMINATED
IF IN EYES: FLUSH WITH LARGE AMOUNTS OF WATER, LIFTING UPPER AND LOWER LIDS OCCASIONALLY, GET MEDICAL ATTENTION.
IF SWALLOWED:
FINGERIATEBACKROFKTTWO HROAT. NEVERES OGIVE ANYTHIR ANDINDUCEGMUTHVOMTONANBUNC SCCIIOUSVPERSON- GETNG IPECAC SMEDICUP ARL BY
ATTENTION IMMEDIATELY.
IF BREATHED: REMOVE INDIVIDUAL TO FRESH AIR.
PRIMARY ROUTE(S) OF ENTRY:
SKIN CONTACT, INHALATION
HAZARDOUS POLYMERIZATION: CANNOT OCCUR
STABILITY: STABLE
INCOMPATIBILITY: AVOID CONTACT WITH:. STRONG MINERAL ACIDS., STRONG ORGANIC ACIDS, STRONG OXIDIZING AGENTS
STEPS TO BE TAKEN IN CASE MATERIAL IS RELEASED OR SPILLED:
SMALL SPILL: SWEEP UP MATERIAL FOR DISPOSAL OR RECOVERY.
LARGE SPILL: SHOVEL MATERIAL INTO CONTAINERS. THOROUGHLY SWEEP AREA OF SPILL TO CLEAN UP ANY RESIDUAL MATERIAL.
WASTE DISPOSAL METHOD:
SMALL SPILL: DISPOSE OF IN ACCORDANCE WITH ALL LOCAL, STATE AND FEDERAL REGULATIONS.
LARGE SPILL: DISPOSE OF IN ACCORDANCE WITH ALL APPLICABLE LOCAL, STATE AND FEDERAL REGULATIONS.
RESPIRATORY PROTECTION: IF OVEREXPOSURE HAS BEEN DETERMINED OR DOCUMENTED, A NIOSH/MSHA JOINTLY APPROVED AIR
SUPPLIED RESPIRATOR IS ADVISED IN ABSENCE OF PROPER ENVIRONMENTAL CONTROL. OSHA REGULATIONS ALSO PERMIT
OTHER NIOSH/MSHA RESPIRATORS UNDER SPECIFIED CONDITIONS. (SEE YOUR SAFETY EQUIPMENT SUPPLIER). ENGINEERING
OR ADMINISTRATIVE CONTROLS SHOULD BE IMPLEMENTED TO REDUCE EXPOSURE.
VENTILATIOON: PROVIDE SUFFICIENT MECHANICAL (GENERAL AND/OR LOCAL EXHAUST) VENTILATION TO MAINTAIN EXPOSURE
BELOW
PROTECTIVE GLOVES: WEAR RESISTANT GLOVES SUCH AS:. NATURAL RUBBER
EYE PROTECTION:
REGULAT REGULATIONS PERMIT OTHER TYPE SAFETY GIANCE WITH LASSES. CONSULTRYOOUUR SAFNETYAREPRESENTAtIVEWEVER. OSHA
OTHER PROTECTIVE EQUIPMENT: TO PREVENT REPEATED OR PROLONGED SKIN CONTACT, WEAR IMPERVIOUS CLOTHING AND BOOTS.
CONTAINERS OF THIS MATERIAL MAY BE HAZARDOUS WHEN EMPTIED.SINCE EMPTIED CONTAINERS RETAIN PRODUCT RESIDUES
(VAPOR, LIQUID, AND/OR SOLID). ALL HAZARD PRECAUTIONS GIVEN IN THE DATA SHEET MUST BE OBSERVED.
THE INFORMATION ACCUMULATED HEREIN IS BELIEVED TO BE ACCURATE BUT IS NOT WARRANTED TO BE WHETHER ORIGINATING
WITH THE COMPANY OR NOT. RECIPIENTS ARE ADVISED TO CONFIRM IN ADVANCE OF NEED THAT THE INFORMATION IS
CURRENT, APPLICABLE, AND SUITABLE TO THEIR CIRCUMSTANCES.
LAST PAGE --SEE ATTACHMENT PAGE ENCLOSED --LAST PAGE

r *** Attachment 5 ***
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
FMC Corporation
LithiumDivision
NPDES No. NC0005177
Permit Renewal
March 26, 1996
Mr. Joe Morrison
FMC Corporation - Lithium Division
P.O. Box 3925
Gastonia, NC 28053-3925
RE: PACE Project No. 660228.517
Client Reference: NPDES Renewal Application
Dear Mr. Morrison:
APR
Enclosed is the report of laboratory analyses for samples received
February 28 - March 04, 1996.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
La"��
Clevecia M. Harris
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
withni it the written mncent of Pace Analytical Services. Inc.

Pace Analytical Services, Inc.
9800 ICincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
FMC Corporation - Lithium Division
P.O. Box 3925
Gastonia, NC 28053-3925
Attn: Mr. Joe Morrison
Client Reference: NPDES Renewal Application
PACE Sample Number:
Date Collected:
Date Received:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand, 05 Day
Calcium
Chemical Oxygen Demand
Color
Cyanide, Total
Fluoride, Total
Units
March 26, 1996
PACE Project Number: 660228517
92 0559894
02/28/96
02/28/96
001
MDL Outfall DATE ANALYZED
mg/L
2.0
4
mg/L
0.50
154
mg/L
10
28
Pt -Co
Unit 5
30-PH 7
mg/L
0.002
0.002
mg/L
0.2
0.62
03/01/96
03/06/96
03/11/96
02/29/96
03/13/96
03/13/96
Nitrogen, Ammonia
mg/L
0.1
0.16
03/08/96
Nitrogen, Kjeldahl
mg/L
1.0
1.2
03/05/96
Nitrogen, Nitrate plus Nitrite
mg/L
0.1
ND
03/14/96
Oil & Grease
mg/L
1.0
62
03/14/96
Phenol, Low Level
mg/L
0.005
ND
03/05/96
Phosphorus, Total
mg/L
0.010
0.05
03/11/96
Potassium
mg/L
1.0
22
03/06/96
Sodium
mg/L
0.50
193
03/06/96
Solids, Settleable
ml/L
0.1
ND
03/01/96
Solids, Total Dissolved
mg/L
1
1400
03/05/96
Solids, Total Suspended
mg/L
1.0
12
03/04/96
Sulfate
mg/L
200
590
03/11/96
Sulfide
mg/L
0.10
0.90
03/05/96
Surfactants
mg/L
0.30
ND
03/01/96
Total Organic Carbon
mg/L
2.0
95
03/07/96
Zirconium
mg/L
0.5
ND
03/21/96
PRIORITY POLLUTANT METALS - FORM "A"
Aluminum
mg/L
0.10
0.10
03/06/96
Antimony
mg/L
0.003
ND
03/01/96
Arsenic
mg/L
0.005
ND
03/04/96
Beryllium
mg/L
0.002
ND
03/05/96
Cadmium
mg/L
0.001
0.002
03/05/96
Chromium
mg/L
0.005
ND
03/08/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
....a��....V� .....w�...... ---# -f 0� On2"r21 Sdbrviras. Inc_

t+
Pace Analytical Services, Inc.
9800 Kncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison March 26, 1996
Page 2 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number: 92 0559894
Date Collected: 02/28/96.
Date Received: 02/28/96
Client Sample ID: 001
Parameter Units MDL Outfall DATE ANALYZED
INORGANIC ANALYSIS
PRIORITY POLLUTANT METALS
- FORM "A"
Copper
mg/L
0.01
NO
03/06/96
Lead
mg/L
0.005
NO
03/04/96
Mercury
mg/L
0.0002
0.0065
03/06/96
Nickel
mg/L
0.05
ND
03/06/96
Selenium
mg/L
0.010
ND
03/05/96
Silver
mg/L
0.010
NO
03/04/96
Zinc
mg/L
0.01
0.024
03/06/96
Barium
mg/L
0.10
ND
03/06/96
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Cyclohexane
ug/L
5.0
ND
03/13/96
BASE/NEUTRALS & ACIDS -REPORTING
FORM "A"
N-Nitrosodimethylamine
ug/L
1.0
NO
03/08/96
bis(2-Chloroethyl) ether
ug/L
1.3
NO
03/08/96
Phenol
ug/L
1.2
NO
03/08/96
2-Chlorophenol
ug/L
1.1
ND
03/08/96
1,3-Dichlorobenzene
ug/L
1.2
ND
03/08/96
1,4-Dichlorobenzene
ug/L
1.2
NO
03/08/96
1,2-Dichlorobenzene
ug/L
1.1
NO
03/08/96
bis(2-Chloroisopropyl) ether
ug/L
1.8
NO
03/08/96
Hexachloroethane
ug/L
1.3
NO
03/08/96
N-Nitrosodi-n-propylamine
ug/L
1.7
ND
03/08/96
Nitrobenzene
ug/L
1.3
ND
03/08/96
3,5,5-Trimethyl-2-cyclohexanone
ug/L
1.7
ND
03/08/96
2-Nitrophenol
ug/L
1.4
NO
03/08/96
2,4-Dimethylphenol
ug/L
1.9
NO
03/08/96
bis(2-Chloromethoxy)methane
ug/L
1.6
NO
03/08/96
Z,4-Dichlorophenol
ug/L
1.4
NO
03/08/96
1,2,4-Trichlorobenzene
ug/L
1.4
NO
03/08/96
Naphthalene
ug/L
1.7
NO
03/08/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
..:u.....� ��� .... we.....,n.e..0 ..f 0— Ann"irnl Ranrirna Inc

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison
Page 3
Client Reference: NPDES Renewal Application
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
Units MDL
March 26, 1996
PACE Project Number: 660228517
92 0559894
02/28/96
02/28/96
001
Outfall DATE ANALYZED
BASE/NEUTRALS & ACIDS -REPORTING
Hexachlorobutadiene
FORM "A"
ug/L
1.6
ND
03/08/96
4-Chloro-3-methylphenol
ug/L
1.2
ND
03/08/96
Hexachlorocyclopentadiene
ug/L
1.5
ND
03/08/96
2,4,6-Trichlorophenol
ug/L
1.3
ND
03/08/96
2-Chloronaphthalene
ug/L
1.7
ND
03/08/96
Acenaphthylene
ug/L
1.8
ND
03/08/96
Dimethyl phthalate
ug/L
1.0
ND
03/08/96
2,6-Dinitrotoluene
ug/L
1.1
ND
03/08/96
Acenaphthene
ug/L
1.8
ND
03/08/96
2,4-Dinitrophenol
ug/L
1.9
ND
03/08/96
2,4-Dinitrotoluene
4-Nitrophenol
ug/L
ug/L
1.0
0.3
ND
ND
03/08/96
03/08/96
Fluorene
ug/L
1.6
ND
03/08/96
4-Chlorophenyl phenyl ether
ug/L
1.7
ND
03/08/96
Diethyl phthalate
ug/L
1.0
ND
03/08/96
1,2-Diphenylhydrazine
4,6-Dinitro-o-cresol
ug/L
ug/L
1.5
1.0
ND
ND
03/08/96
03/08/96
N-Nitrosodiphenylamine
ug/L
1.8
ND
03/08/96
4-Bromophenyl phenyl ether
Hexachlorobenzene
ug/L
ug/L
1.0
1.0
ND
ND
03/08/96
03/08/96
Pentachlorophenol
Phenanthrene
ug/L
ug/L
1.4
1.0
ND
ND
03/08/96
03/08/96
Anthracene
Di-n-butyl phthalate
ug/L
ug/L
1.0
1.2
ND
ND
03/08/96
03/08/96
Fluoranthene
Benzidine
ug/L
ug/L
1.0
16.4
ND
ND
03/08/96
03/08/96
Pyrene
Butyl benzyl phthalate
ug/L
ug/L
1.0
1.0
ND
ND
03/08/96
03/08/96
3,3-Dichlorobenzidine
ug/L
ug/L
2.6
1.0
ND
ND
03/08/96
03/08/96
Benz[a]anthracene
Chrysene
ug/L
1.0
ND
03/08/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax [phone]
Mr. Joe Morrison March 26, 1996
Page 4 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number:
92 0559894
Date Collected:
02/28/96
Date Received:
02/28/96
Client Sample ID:
Parameter
Units
MDL
001
Outfall
DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS & ACIDS -REPORTING FORM "A"
bis(2-Ethylhexyl) phthalate
ug/L
1.0
NO
03/08/96
Di-n-octyl phthalate
Benzo[b]fluoranthene
ug/L
ug/L
1.4
1.0
NO
NO
03/08/96
03/08/96
Benzo[k]fluoranthene
ug/L
1.0
NO
03/08/96
Benzo[a]pyrene
Indeno[1,2,3-cd]pyrene
ug/L
ug/L
1.0
1.0
NO
NO
03/08/96
03/08/96
Dibenz[a,h]anthracene
ug/L
1.0
NO
03/08/96
Benzo[g,h,i]perylene
ug/L
1.0
NO
03/08/96
Surrogate - 2-Fluorophenol
%
28
19
03/08/96
03/08/96
Surrogate - Phenol-d6
Surrogate - Nitrobenzene-d5
%
%
78
03/08/96
Surrogate - 2-Fluorobiphenyl
%
64
03/08/96
Surrogate - 2,4,6-Tribromophenol
%
62
75
03/08/96
03/08/96
Surrogate - Terphenyl-d14
Date Extracted, Base/Neutrals and Acids
%
Date
030596
03/05/96
PESTICIDES AND PCBS - REPORTING FORM "A"
Aldrin
ug/L
0.05
NO
03/12/96
alpha-BHC
ug/L
0.05
NO
03/12/96
beta-BHC
ug/L
0.05
NO
03/12/96
delta-BHC
ug/L
0.1
NO
03/12/96
gamma-BHC (Lindane)
ug/L
ug/L
0.05
0.2
NO
NO
03/12/96
03/12/96
Chlordane (tech)
4,4-DDD
4,4-DDE
ug/L
ug/L
0.1
0.1
NO
NO
03/12/96
03/12/96
4,4-DDT
Dieldrin
ug/L
ug/L
0.1
0.02
NO
NO
03/12/96
03/12/96
Endosulfan I
Endosulfan II
ug/L
ug/L
0.1
0.1
NO
NO
03/12/96
03/12/96
Endosulfan sulfate
ug/L
ug/L
0.7
0.06
NO
NO
03/12/96
03/12/96
Endrin
Endrin aldehyde
ug/L
0.2
NO
03/12/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
----a--.—._._u----------to--A—khi—IC--Arse Inr

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. [phone]
Fax: [phone]
Mr. Joe Morrison March 26, 1996
Page 5 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number: 92 0559894
Date Collected: 02/28/96
Date Received: 02/28/96
Client Sample ID:
01
Parameter Units MDL Outfall DATE ANALYZED
ORGANIC ANALYSIS
PESTICIDES AND PCBS - REPORTING FORM "A"
Heptachlor
ug/L
0.05
ND
03/12/96
Heptachlor epoxide
ug/L
0.8
ND
03/12/96
Methoxychlor
ug/L
0.5
ND
03/12/96
Toxaphene
ug/L
2.4
ND
03/12/96
Mirex
ug/L
0.2
ND
03/12/96
Aroclor-1016
ug/L
1.0
ND
03/12/96
Aroclor-1221
ug/L
1.0
ND
03/12/96
Aroclor-1232
ug/L
1.0
NO
03/12/96
Aroclor-1242
ug/L
1.0
ND
03/12/96
Aroclor-1248
ug/L
1.0
NO
03/12/96
Aroclor-1254
ug/L
1.0
ND
03/12/96
Aroclor-1260
ug/L
1.0
ND
03/12/96
Date Extracted, Pesticides
Date
030696
03/06/96
VOLATILE ORGANICS - REPORTING FORM "A"
Chloromethane
ug/L
1.2
ND
03/06/96
Chloroethene (Vinyl chloride)
ug/L
1.0
NO
03/06/96
Bromomethane
ug/L
1.0
NO
03/06/96
Chloroethane
ug/L
1.0
ND
03/06/96
Trichlorofluoromethane
ug/L
1.0
NO
03/06/96
Acrolein
ug/L
41
ND
03/06/96
1,1-Dichloroethene
ug/L
1.0
ND
ND
03/06/96
03/06/96
Acrylonitrile
Dichloromethane
ug/L
ug/L
36
3.3
ND
03/06/96
1,2-Dichloroethene, trans-
ug/L
1.0
ND
ND
03/06/96
03/06/96
1,1-Dichloroethane
Chloroform
ug/L
ug/L
1.0
1.1
5.2
03/06/96
1,1,1-Trichloroethane
ug/L
1.5
ND
NO
03/06/96
03/06/96
1,2-Dichloroethane
Carbon tetrachloride
ug/L
ug/L
1.0
1.0
ND
03/06/96
Benzene
ug/L
1.0
NO
03/06/96
Trichloroethene
ug/L
1.0
ND
03/06/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. [phone]
Fax:[phone]
Mr. Joe Morrison March 26, 1996
Page 6 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number: 92 0559894
Date Collected: 02/28/96
Date Received: 02/28/96
Client Sample ID:
01
Parameter Units MDL Outfall DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS - REPORTING FORM "A"
1,2-Dichloropropane
ug/L
1.0
ND
03/06/96
Bromodichloromethane
ug/L
1.0
3.4
03/06/96
2-Chloroethoxyethene
ug/L
1.8
ND
03/06/96
cis-1,3-Dichloropropene
-
ug/L
ug/L
1.1
1.0
ND
ND
03/06/96
03/06/96
Toluene
trans-1,3-Dichloropropene
ug/L
1.0
ND
03/06/96
1,1,2-Trichloroethane
ug/L
1.0
ND
03/06/96
Dibromochloromethane
ug/L
1.0
5.8
03/06/96
Tetrachloroethene
ug/L
1.0
ND
03/06/96
Chlorobenzene
ug/L
1.0
ND
03/06/96
Ethylbenzene
ug/L
1.0
ND
03/06/96
Bromoform
ug/L
1.0
5.5
03/06/96
1,1,2,2-Tetrachloroethane
ug/L
1.1
ND
03/06/96
Surrogate - Dibromofluoromethane
%
95
96
03/06/96
03/06/96
Surrogate - Toluene-d8
Surrogate - Bromofluorobenzene
%
%
95
03/06/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace A n a l Xti c a l Huntersville, NC 28078
Tel: [phone]
Fax [phone]
Mr. Joe Morrison March 26, 1996
Page 7 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number: 92 0559924
Date Collected: 02/28/96
Date Received: 02/28/96
Client Sample ID: 004
Parameter Units MDL Outfall DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand, 05 Day
mg/L
2.0
ND
03/01/96
Calcium
mg/L
0.50
88
03/06/96
Chemical Oxygen Demand
mg/L
10
17
03/11/96
Chlorine, Residual
mg/L
0.1
ND
02/29/96
Color
Pt -Co
Unit 5
15-PH 6
02/29/96
Cyanide, Total
mg/L
0.002
0.011
03/13/96
Fluoride, Total
mg/L
0.2
0.31
03/13/96
Nitrogen, Ammonia
mg/L
0.1
0.10
03/08/96
Nitrogen, Kjeldahl
mg/L
0.10
0.35
03/05/96
Nitrogen, Nitrate plus Nitrite
mg/L
0.1
ND
03/14/96
Oil & Grease
mg/L
1.0
ND
03/14/96
Phenol, Low Level
mg/L
0.005
ND
03/05/96
Phosphorus, Total
mg/L
0.010
0.04
03/11/96
Potassium
mg/L
1.0
3.53
03/06/96
Sodium
mg/L
0.50
8.90
03/06/96
Solids, Settleable
ml/L
0.1
ND
03/01/96
Solids, Total Dissolved
mg/L
1.0
620
03/06/96
Solids, Total Suspended
mg/L
1.0
2
03/04/96
Sulfate
mg/L
40
330
03/11/96
Sulfide
mg/L
0.10
1.4
03/05/96
Surfactants
mg/L
0.30
NO
03/01/96
Total Organic Carbon
mg/L
1.0
79
03/07/96
Zirconium
mg/L
0.5
NO
03/21/96
PRIORITY POLLUTANT METALS - FORM "A"
Aluminum
mg/L
0.10
ND
03/06/96
Antimony
mg/L
0.003
0.003
03/01/96
Arsenic
mg/L
0.005
ND
03/04/96
Beryllium
mg/L
0.002
ND
03/05/96
Cadmium
mg/L
0.001
0.002
03/05/96
Chromium
mg/L
0.005
ND
03/08/96
Copper
mg/L
0.01
ND
03/06/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. [phone]
Fax [phone]
Mr. Joe Morrison March 26, 1996
Page 8 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number: 92 0559924
Date Collected: 02/28/96
Date Received: 02/28/96
Client Sample ID:
04
Parameter Units MDL Outfall DATE ANALYZED
INORGANIC ANALYSIS
PRIORITY POLLUTANT METALS
- FORM "A"
Lead
mg/L
0.005
NO
03/04/96
Mercury
mg/L
0.0002
0.0077
03/06/96
Nickel
mg/L
0.05
ND
03/06/96
Selenium
mg/L
0.005
ND
03/05/96
Silver
mg/L
0.010
ND
03/04/96
Zinc
mg/L
0.01
0.023
03/06/96
Barium mg/L 0.010 ND 03/06/96
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Cyclohexane
ug/L
5.0
NO
03/13/96
BASE/NEUTRALS & ACIDS -REPORTING FORM
N-Nitrosodimethylamine
"A"
ug/L
1.0
NO
03/08/96
bis(2-Chloroethyl) ether
ug/L
1.3
NO
03/08/96
Phenol
ug/L
1.2
ND
03/08/96
2-Chlorophenol
ug/L
1.1
NO
03/08/96
1,3-Dichlorobenzene
ug/L
ug/L
1.2
1.2
NO
ND
03/08/96
03/08/96
1,4-Dichlorobenzene
1,2-Dichlorobenzene
bis(2-Chloroisopropyl) ether
ug/L
ug/L
1.1
1.8
ND
ND
03/08/96
03/08/96
Hexachloroethane
N-Nitrosodi-n-propylamine
ug/L
ug/L
1.3
1.7
NO
ND
03/08/96
03/08/96
Nitrobenzene
3,5,5-Trimethyl-2-cyclohexanone
ug/L
ug/L
1.3
1.7
NO
NO
03/08/96
03/08/96
2-Nitrophenol
2,4-Dimethylphenol
ug/L
ug/L
1.4
1.9
NO
ND
03/08/96
03/08/96
bis(2-Chloromethoxy)methane
ug/L
1.6
ND
NO
03/08/96
03/08/96
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
ug/L
ug/L
1.4
1.4
NO
03/08/96
Naphthalene
ug/L
1.7
ND
03/08/96
Hexachlorobutadiene
ug/L
1.6
NO
03/08/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
_ _....'--- --------- • � n--- w--I.Ai-.J Qw..;i In&

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison March 26, 1996
Page 9 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number: 92 0559924
Date Collected: 02/28/96
Date Received: 02/28/96
Client Sample ID: 004
Parameter Units MDL Outfall DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS & ACIDS -REPORTING FORM
"A"
4-Chloro-3-methylphenol
ug/L
1.2
ND
03/08/96
Hexachlorocyclopentadiene
ug/L
1.5
ND
03/08/96
2,4,6-Trichlorophenol
ug/L
1.3
ND
03/08/96
2-Chloronaphthalene
ug/L
1.7
ND
03/08/96
Acenaphthylene
ug/L
1.8
ND
03/08/96
Dimethyl phthalate
ug/L
1.0
ND
03/08/96
2,6-Dinitrotoluene
ug/L
1.1
ND
03/08/96
Acenaphthene
ug/L
1.8
ND
03/08/96
2,4-Dinitrophenol
ug/L
1.9
ND
03/08/96
2,4-Dinitrotoluene
ug/L
1.0
ND
03/08/96
4-Nitrophenol
ug/L
0.3
ND
03/08/96
Fluorene
ug/L
1.6
ND
03/08/96
4-Chlorophenyl phenyl ether
ug/L
1.7
ND
03/08/96
Diethyl phthalate
ug/L
1.0
ND
03/08/96
1,2-Diphenylhydrazine
ug/L
1.5
ND
03/08/96
4,6-Dinitro-o-cresol
ug/L
1.0
ND
03/08/96
N-Nitrosodiphenylamine
ug/L
1.8
ND
03/08/96
4-Bromophenyl phenyl ether
ug/L
1.0
ND
03/08/96
Hexachlorobenzene
ug/L
1.0
ND
03/08/96
Pentachlorophenol
ug/L
1.4
ND
03/08/96
Phenanthrene
ug/L
1.0
ND
03/08/96
Anthracene
ug/L
1.0
ND
03/08/96
Di-n-butyl phthalate
ug/L
1.2
ND
03/08/96
Fluoranthene
ug/L
1.0
ND
03/08/96
Benzidine
ug/L
16.4
ND
03/08/96
Pyrene
ug/L
1.0
ND
03/08/96
Butyl benzyl phthalate
ug/L
1.0
ND
03/08/96
3,3-Dichlorobenzidine
ug/L
2.6
ND
03/08/96
Benz(a]anthracene
ug/L
1.0
ND
03/08/96
Chrysene
ug/L
1.0
ND
03/08/96
bis(2-Ethylhexyl) phthalate
ug/L
1.0
ND
03/08/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
...:�_... .�� .....Mew-----.J -8 D..s Aw-"d 1 Cann -a Ine

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. [phone]
Fax: [phone]
Mr. Joe Morrison March 26, 1996
Page 10 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number:
92 0559924
Date Collected:
02/28/96
Date Received:
02/28/96
Client Sample ID:
Parameter
Units
MDL
004
Outfall
DATE ANALYZED
ORGANIC ANALYSIS
BASE/NEUTRALS & ACIDS -REPORTING FORM "A"
Di-n-octyl phthalate
ug/L
1.4
ND
03/08/96
Benzo[b]fluoranthene
ug/L
1.0
ND
03/08/96
Benzo[k]fluoranthene
ug/L
1.0
ND
03/08/96
Benzo[a]pyrene
ug/L
1.0
ND
03/08/96
Indeno[1,2,3-cd]pyrene
ug/L
1.0
ND
03/08/96
Dibenz[a,h]anthracene
ug/L
1.0
ND
03/08/96
Benzo[g,h,i]perylene
ug/L
1.0
ND
03/08/96
Surrogate - 2-Fluorophenol
%
49
34
03/08/96
03/08/96
Surrogate - Phenol-d6
Surrogate - Nitrobenzene-d5
%
%
85
03/08/96
Surrogate - 2-Fluorobiphenyl
%
76
82
03/08/96
03/08/96
Surrogate - 2,4,6-Tribromophenol
%
Surrogate - Terphenyl-d14
Date Extracted, Base/Neutrals and Acids
%
Date
75
030596
03/08/96
03/05/96
PESTICIDES AND PCBS - REPORTING FORM "A"
ug/L
0.05
ND
03/12/96
Aldrin
alpha-BHC
ug/L
0.05
ND
03/12/96
beta-BHC
delta-BHC
ug/L
ug/L
0.05
0.1
ND
ND
03/12/96
03/12/96
gamma-BHC (Lindane)
ug/L
ug/L
0.05
0.2
ND
ND
03/12/96
03/12/96
Chlordane (tech)
4,4-DDD
ug/L
0.1
ND
03/12/96
4,4-DDE
ug/L
0.1
ND
03/12/96
4,4-DDT
ug/L
0.1
ND
03/12/96
Dieldrin
Endosulfan I
ug/L
ug/L
0.02
0.1
ND
ND
03/12/96
03/12/96
Endosulfan II
ug/L
0.1
ND
03/12/96
Endosulfan sulfate
ug/L
ug/L
0.7
0.06
ND
ND
03/12/96
03/12/96
Endrin
Endrin aldehyde
ug/L
0.2
ND
03/12/96
Heptachlor
ug/L
0.05
ND
03/12/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
w7fhni at fhwriffnn rnnRant of Para AnaMral Services. Inc.

pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison March 26, 1996
Page 11 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number: 92 0559924
Date Collected: 02/28/96
Date Received: 02/28/96
Client Sample ID: 004
Parameter Units MDL Outfall DATE ANALYZED
ORGANIC ANALYSIS
PESTICIDES AND PCBS - REPORTING FORM "A"
Heptachlor epoxide
ug/L
0.8
NO
03/12/96
Methoxychlor
ug/L
0.5
NO
03/12/96
Toxaphene
ug/L
2.4
NO
03/12/96
Mirex
ug/L
0.2
NO
03/12/96
Aroclor-1016
Aroclor-1221
ug/L
ug/L
1.0
1.0
NO
NO
03/12/96
03/12/96
Aroclor-1232
ug/L
ug/L
1.0
1.0
NO
NO
03/12/96
03/12/96
Aroclor-1242
Aroclor-1248
ug/L
1.0
NO
03/12/96
Aroclor-1254
ug/L
ug/L
1.0
1.0
NO
ND
03/12/96
03/12/96
Aroclor-1260
Date Extracted, Pesticides
Date
030696
03/06/96
VOLATILE ORGANICS - REPORTING FORM "A"
Chloromethane
ug/L
1.2
NO
03/06/96
Chloroethene (Vinyl chloride)
ug/L
1.0
1.0
NO
NO
03/06/96
03/06/96
Bromomethane
Chloroethane
ug/L
ug/L
1.0
NO
03/06/96
Trichlorofluoromethane
ug/L
1.0
NO
NO
03/06/96
03/06/96
Acrolein
ug/L
41
1,1-Dichloroethene
ug/L
ug/L
1.0
36
NO
NO
03/06/96
03/06/96
Acrylonitrile
Dichloromethane
ug/L
3.3
NO
03/06/96
1,2-Dichloroethene, trans-
ug/L
1.0
ND
NO
03/06/96
03/06/96
1,1-Dichloroethane
Chloroform
ug/L
ug/L
1.0
1.1
NO
03/06/96
1,1,1-Trichloroethane
ug/L
1.5
NO
NO
03/06/96
03/06/96
1,2-Dichloroethane
Carbon tetrachloride
ug/L
ug/L
1.0
1.0
NO
03/06/96
Benzene
Trichloroethene
ug/L
ug/L
1.0
1.0
2.0
NO
03/06/96
03/06/96
1,2-Dichloropropane
ug/L
1.0
NO
03/06/96
Bromodichloromethane
ug/L
1.0
NO
03/06/96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
...:fA..,,f fk. —r4fan enneanf of Parr, Analvtical Services. Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison March 26, 1996
Page 12 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PACE Sample Number: 92 0559924
Date Collected: 02/28/96
Date Received: 02/28/96
Client Sample ID:
04
Parameter Units MDL Outfall DATE ANALYZED
ORGANIC ANALYSIS
VOLATILE ORGANICS - REPORTING FORM "A"
2-Chloroethoxyethene
ug/L
1.8
ND
03/06/96
cis-1,3-Dichloropropene
ug/L
1.1
ND
03/06/96
Toluene
ug/L
1.0
ND
03/06/96
trans-1,3-Dichloropropene
ug/L
1.0
ND
03/06/96
1,1,2-Trichloroethane
ug/L
1.0
ND
03/06/96
Dibromochloromethane
ug/L
1.0
ND
03/06/96
Tetrachloroethene
ug/L
1.0
ND
03/06/96
Chlorobenzene
ug/L
1.0
ND
03/06/96
Ethylbenzene
ug/L
1.0
ND
03/06/96
Bromoform
ug/L
1.0
ND
03/06/96
1,1,2,2-Tetrachloroethane
ug/L
1.1
ND
95
03/06/96
03/06/96
Surrogate - Dibromofluoromethane
%
Surrogate - Toluene-d8
%
93
94
03/06/96
03/06/96
Surrogate - Bromofluorobenzene
%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
.-;#k... , ft,...,ae... —neon* of Paeva Analytical Services_ Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax 70"75-9091
Mr. Joe Morrison
Page 13
Client Reference: NPDES Renewal Application
March 26, 1996
PACE Project Number: 660228517
PACE Sample Number:
92 0561414
Date Collected:
03/04/96
Date Received:
03/04/96
Client Sample ID:
001
Parameter
Units
MDL
Outfall
DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chlorine, Residual
mg/L
0.1
0.2
03/04/96
Coliform, Fecal by MF
col/100ml
2
2
03/04/96
Sulfite
mg/L
2.0
ND
03/05/96
PACE Sample Number:
92 0561422
Date Collected:
03/04/96
Date Received:
03/04/96
Client Sample ID:
004
Parameter
Units
MDL
Outfall
DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chlorine, Residual mg/L 0.1 ND 03/04/96
Coliform, Fecal by MF col/100ml 2 5 03/04/96
Sulfite mg/L 2.0 ND 03/05/96
These data have been reviewed and are approved for release.
Margaret S. Harding
Manager, Laboratory Operations
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
...:u.�..a u.� ...tea-- .... ---- * —$ D..— A..hAL—1 Q--i— Ine

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace A n a lyt i s l Huntersville, NC 28078
Tel. 70"75-9092
Fax: [phone]
Mr. Joe Morrison FOOTNOTES March 26, 1996
Page 14 for pages 1 through 13 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
MOIL Method Detection Limit
ND Not detected at or above the MDL.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
...ati.,, it the written r neant of Pace Analytical Services. Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. 70"75-9092
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 15 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
Biochemical Oxygen Demand, 05 Day
Batch: 92 44456
Samples: 92 0559894, 92 0559924
METHOD BLANK AND SAMPLE DUPLICATE:
920559924 Duplicate
Method 004 of
Parameter Units MDL Blank Outfall 92 0559924 RPD
Biochemical Oxygen Demand, 05 Day mg 2.0 ID — dD — ND �NC
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units MDL Value Recv
-TiFo- TM
Biochemical Oxygen Demand, 05 Day mg T.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

0
Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace A n a l yt" c a l Huntersville, NC 28078
Tel: 70"75-9092
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 16 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
Chemical Oxygen Demand
Batch: 92 44607
Samples: 92 0559894, 92 0559924
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method
of
Parameter
—Oxygen
Units
mg
MDL
Tu-
Blank 920559460
Nuu— 0
92 0559460 RPD
13
Chemical Demand
SPIKE:
Spike
Parameter
Units
MDL
920559460 SS*ke
Recv
98%
C emica Oxygen Demand
mg
TF
30 500
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units MDL Value Recv
Chemical Oxygen Demand mg/L 10 500 —TO-22-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
...ate..... .�� ....:Mew ---- m of Dorm Anah fieoi CYMPP__l Inc_

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytcal
Huntersville, NC 28078
Tel. [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA
Page 17
Client Reference: NPDES Renewal Application
Chlorine, Residual
Batch: 92 44373
Samples: 92 0559924
March 26, 1996
PACE Project Number: 660228517
SAMPLE DUPLICATE:
920559894 Duplicate
001 of
Parameter Units MDL Outfall 92 0559894 RPD
Chlorine, Residual m9 0� UM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA
Page 18
Client Reference: NPDES Renewal Application
Chlorine, Residual
Batch: 92 44608
Samples: 92 0561414, 92 0561422
SAMPLE DUPLICATE:
Parameter Units
C orine, Residual m9
March 26, 1996
PACE Project Number: 660228517
920561422 Duplicate
004 of
MDL Outfall 92 0561422 RPD
p, �' Nam— Nam— N�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
. ;fk—d N.s,.niMnn ernaanf of Pnea Analvfiral Services. Inc.

Pace Analytical Services, Inc.
9800 Mncey Avenue, Suite 100
Pace An a lyti ca I Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA
Page 19
Client Reference: NPDES Renewal Application
Col iform, Fecal by MF
Batch: 92 44402
Samples: 92 0561414, 92 0561422
METHOD BLANK AND SAMPLE DUPLICATE:
March 26, 1996
PACE Project Number: 660228517
920561422 Duplicate
Method 004 of
Parameter Units MDL Blank Outfall 92 0561422 RPD
o i orm, Fecal by MF coTT00m1 T— ND
Coliform, Fecal by MF col/100ml 2 5 2 86%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA
Page 20
Client Reference: NPDES Renewal Application
Color
Batch: 92 44372
Samples: 92 0559894, 92 0559924
March 26, 1996
PACE Project Number: 660228517
METHOD BLANK AND SAMPLE DUPLICATE:
920559894 Duplicate
Method 001 of
Parameter Units MDL Blank Outfall 92 0559894 RPD
0 or t- o Unit T— ND- -IR-6 3-0-- MT7— 10-PH 7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA
Page 21
Client Reference: NPDES Renewal Application
Cyanide, Total
Batch: 92 44708
Samples: 92 0559894, 92 0559924
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter Units
Cyanide, Total m9
LABORATORY CONTROL SAMPLE:
Parameter Units
yani e, Total m9
March 26, 1996
PACE Project Number: 660228517
Duplicate
Method of
MDL Blank 920564120 92 0564120 RPD
(�. 0-02 NU— 0.014 0—.014— 0%
Reference
MOIL Value Recv
0.002 �•02�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
—ifk—f n,. writtwn nnnnant of Pae* AnaNtiCA Services. Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: 70"75-9091
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 22 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
Fluoride, Total
Batch: 92 44702
Samples: 92 0559894, 92 0559924
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method
of
Parameter
Units
MDL
Blank 920560590
92 0560590 RPD
Fluoride, Total
mg
0.2
IVY Nam—
ND NC
SPIKE:
Spike
Parameter
Units
MDL
920560531 S ike
Recv
Fl uori e, Total
mg/L
0.2
0.28 T .00
29
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units MDL Value Recv
Fl
uori e, Total mg 02 .00 Oa
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
..s.....� ewe .....we.. nn -# of 0.&a On9IV4V`ml Aarvi[`PQ Inc_

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace A n a l xt I C aI Huntersville, NC 28078
Tel: 70"75-9092
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 23 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
Nitrogen, Nitrate plus Nitrite
Batch: 92 44759
Samples: 92 0559894, 92 0559924
METHOD BLANK AND SAMPLE
DUPLICATE:
Duplicate
Method
of
Parameter
Units
MDL
Blank 920557123
92 0557123
itrogen,
Nitrate plus
Nitrite
mg
0.T
0—
Nitrogen,
Nitrate plus
Nitrite
mg/L
2.5
9.60
9.25
SPIKE:
Spike
Parameter
Units
MDL
920557123 Spike
Recv
itrogen,
Nitrate plus
Nitrite
mg
T.-S
9.60 —
88%
LABORATORY
CONTROL SAMPLE:
Reference
Parameter
Units
MDL
Value
Recv
Nitrogen,
Nitrate plus
Nitrite
mg
0.1
0.20
9
RPD
4%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
within it the written ransent of Pace Analytical Services. Inc.

Pace Analytical Services, Inc.
9800 Kncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA
Page 24
Client Reference: NPDES Renewal Application
Oil & Grease
Batch: 92 44745
Samples: 92 0559894, 92 0559924
March 26, 1996
PACE Project Number: 660228517
METHOD BLANK:
Method
Parameter Units MDL Blank
iUr—ease m9 1—.0 �—
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units MDL Value Recv
O & Grease mg 10 so 102%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
--------4 of 0— A-1� 4i—1 Ine

Pace Analytical Services, Inc.
9800 Kncey Avenue, Suite 100
Pace Analyt"cal Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY.CONTROL DATA March 26, 1996
Page 25 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
Solids, Total Dissolved
Batch: 92 44536
Samples: 92 0559894, 92 0559924
METHOD BLANK
AND SAMPLE DUPLICATE:
920559894
Duplicate
Method 001
of
Parameter
Units
MDL
Blank Outfall
92 0559894. RPD
Solids —,Total
Dissolved
m9
T.—O
Wa
Solids, Total
Dissolved
mg/L
1
1400
1300 7%
Solids, Total
Dissolved
mg/L
1.0
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Solids, Total
Dissolved
Units
mg/
MDL
�
Value —
Recv
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
..dB.... b N,e —A4+.. rnnrnn} of Pne-P Analvtical Services_ Inc_

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. 70"75-9092
Fax:[phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 26 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
Solids,,Total Suspended
Batch: 92 44352
Samples: 92 0559894, 92 0559924
METHOD BLANK AND SAMPLE DUPLICATE:
Duplicate
Method of
Parameter Units MDL Blank 920559193 92 0559193 RPD
Solids —,—Total Suspended m9 �0 N[T 2 —
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units MDL Value Recv
So i s, otal Suspended mg T 0 00 9-89
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
rnneanf of Parr Analytical Services. Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA
Page 27
Client Reference: NPDES Renewal Application
Sulfite
Batch: 92 44853
Samples: 92 0561414, 92 0561422
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter Units
u i to m91C
March 26, 1996
PACE Project Number: 660228517
920561414 Duplicate
Method 001 of
MDL Blank Outfall 92 0561414 RPD
2.O NF— Nam— ND NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
withm it tha writtan cnnsant of P2Ca Analvtical Semices. Inc.

Pace Analytical Services, Inc.
9800 I incey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 28 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
Surfactants
Batch: 92 44376
Samples: 92 0559894, 92 0559924
METHOD BLANK AND SAMPLE DUPLICATE:
920559894
Duplicate
Method
001
of
Parameter
Units
MDL
Blank
Outfall
92 0559894 RPD
ur actants
mg
030
Nt3—
�—
�—NC
SPIKE:
920559894
001
Spike
Parameter
Units
MDL
Outfall
Spike
Recv
ur actants
mg�
�0
Ate—
1.00
�6%
LABORATORY CONTROL SAMPLE:
Reference
Parameter
ur actants
Units
mg/L
MDL
U-.30
Value
.00
Recv
9-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Pace Analytical Services, Inc.
9800 l incey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA
Page 29
Client Reference: NPDES Renewal Application
Cyclohexane
Batch: 92 44737
Samples: 92 0559894, 92 0559924
March 26, 1996
PACE Project Number: 660228517
METHOD BLANK:
Method
Parameter Units MDL Blank
yc o exane u9 S—.O ND
LABORATORY CONTROL SAMPLE:
Reference
Parameter Units MDL Value Recv
yc o exane u9— 9°
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace AnaWcal Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 30 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
BASE/NEUTRALS & ACIDS -REPORTING FORM "A"
Batch: 92 44671
Samples: 92 0559894, 92 0559924
METHOD BLANK:
Method
Parameter
- itrosodimethylamine
Units
u9
MDL
T 0
Blank
�-
bis(2-Chloroethyl) ether
ug/L
1.3
ND
Phenol
ug/L
1.2
ND
2-Chlorophenol
ug/L
1.1
ND
1,3-Dichlorobenzene
ug/L
1.2
ND
1,4-Dichlorobenzene
ug/L
1.2
ND
1,2-Dichlorobenzene
ug/L
1.1
ND
bis(2-Chloroisopropyl) ether
ug/L
1.8
ND
Hexachloroethane
ug/L
1.3
ND
N-Nitrosodi-n-propylamine
ug/L
1.7
ND
Nitrobenzene
ug/L
1.3
ND
3,5,5-Trimethyl-2-cyclohexanone
ug/L
1.7
ND
2-Nitrophenol
ug/L
1.4
ND
2,4-Dimethylphenol
ug/L
1.9
ND
bis(2-Chloromethoxy)methane
ug/L
1.6
ND
2,4-Dichlorophenol
ug/L
1.4
ND
1,2,4-Trichlorobenzene
ug/L
1.4
ND
Naphthalene
ug/L
1.7
ND
Hexachlorobutadiene
ug/L
1.6
ND
4-Chloro-3-methylphenol
ug/L
1.2
ND
Hexachlorocyclopentadiene
ug/L
1.5
ND
2,4,6-Trichlorophenol
ug/L
1.3
ND
2-Chloronaphthalene
ug/L
1.7
NO
Acenaphthylene
ug/L
1.8
NO
Dimethyl phthalate
ug/L
1.0
ND
2,6-Dinitrotoluene
ug/L
1.1
ND
Acenaphthene
ug/L
1.8
ND
2,4-Dinitrophenol
ug/L
1.9
ND
2,4-Dinitrotoluene
ug/L
1.0
ND
4-Nitrophenol
ug/L
0.3
ND
Fluorene
ug/L
1.6
ND
4-Chlorophenyl phenyl ether
ug/L
1.7
ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 31 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
BASE/NEUTRALS & ACIDS -REPORTING FORM "A"
Batch: 92 44671
Samples: 92 0559894, 92 0559924
METHOD BLANK:
Method
Parameter
Units
MDL
Blank
�e6 t yyT phthalate
u97U-
T-6
RD-
1,2-Diphenylhydrazine
ug/L
1.5
NO
4,6-Dinitro-o-cresol
ug/L
1.0
NO
N-Nitrosodiphenylamine
ug/L
1.8
NO
4-Bromophenyl phenyl ether
ug/L
1.0
NO
Hexachlorobenzene
ug/L
1.0
ND
Pentachlorophenol
ug/L
1.4
NO
Phenanthrene
ug/L
1.0
NO
Anthracene
ug/L
1.0
NO
Di-n-butyl phthalate
ug/L
1.2
NO
Fluoranthene
ug/L
1.0
NO
Benzidine
ug/L
16.4
NO
Pyrene
ug/L
1.0
NO
Butyl benzyl phthalate
ug/L
1.0
NO
3,3-Dichlorobenzidine
ug/L
2.6
NO
Benz[a]anthracene
ug/L
1.0
NO
Chrysene
ug/L
1.0
NO
bis(2-Ethylhexyl) phthalate
ug/L
1.0
NO
Di-n-octyl phthalate
ug/L
1.4
NO
Benzo[b]fluoranthene
ug/L
1.0
1.4
Benzo[k]fluoranthene
ug/L
1.0
1.7
Benzo[a]pyrene
ug/L
1.0
1.9
Indeno[1,2,3-cd]pyrene
ug/L
1.0
2.0
Dibenz[a,h]anthracene
ug/L
1.0
1.8
Benzo[g,h,i]perylene
ug/L
1.0
1.7
Surrogate - 2-Fluorophenol
%
23
Surrogate - Phenol-d6
%
34
Surrogate - Nitrobenzene-d5
%
92
Surrogate - 2-Fluorobiphenyl
%
90
Surrogate - 2,4,6-Tribromophenol
%
29
Surrogate - Terphenyl-d14
%
91
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
.Athn. t ti.a unittwn rnnee-nt of Pam AnaMcal Services. Inc.

Pace Analytical Services, Inc.
98M lGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA MarchP26, 199PACE ct Number: 660228517
Page 32
Client Reference: NPDES Renewal Application
BASE/NEUTRALS & ACIDS -REPORTING FORM "A"
Batch: 92 44671
Samples: 92 0559894, 92 0559924
LABORATORY CONTROL SAMPLE AND CONTROL
SAMPLE DUPLICATE:
Reference
Dupl
Parameter
Units
ug
MOIL
T.0
Value
-
Recv
Recv
62
RPD
�91
N- itrosodimethylamine
ug/L
1.3
50
50
88%
88%
94%
7%
bis(2-Chloroethyl) ether
ug/L
1.2
50
46%
46%
0%
Phenol
2-Chlorophenol
ug/L.
1.1
50
50
82%
68%
80%
76%
2%
11%
1,3-Dichlorobenzene
ug/L
ug/L
1.2
1.2
50
70%
78%
11%
1,4-Dichlorobenzene
1,2-Dichlorobenzene
ug/L
1.1
50
50
76%
90%
86%
94%
12%
4%
bis(2-Chloroisopropyl) ether
ug/L
ug/L
1.8
1.3
50
62%
70%
12%
Hexachloroethane
N-Nitrosodi-n-propylamine
ug/L
1.7
50
96%
100%
4%
Nitrobenzene
ug/L
1.3
1.7
50
50
86%
84%
92%
86%
7%
2%
3,5,5-Trimethyl-2-cyclohexanone
ug/L
2-Nitrophenol
ug/L
1.4
50
50
90%
82%
92%
82%
2%
0%
2,4-Dimethylphenol
ug/L
ug/L
1.9
1.6
50
90%
92%
2%
bis(2-Chloromethoxy)methane
ug/L
1.4
50
86%
86%
0%
2,4-Dichlorophenol
1,2,4-Trichlorobenzene
ug/L
1.4
50
70%
78%
11%
Naphthalene
ug/L
1.7
50
80%
88%
10%
Hexachlorobutadiene
ug/L
ug/L
1.6
1.2
50
50
58%
86%
66%
82%
13%
5%
4-Chloro-3-methylphenol
ug/L
1.5
50
32%
36%
12%
Hexachlorocyclopentadiene
ug/L
1.3
50
86%
90%
5%
2,4,6-Trichlorophenol
ug/L
1.7
50
80%
86%
7%
2-Chloronaphthalene
ug/L
1.8
50
84%
92%
9%
Acenaphthylene
Dimethyl phthalate
ug/L
1.0
1.1
50
50
20%
102%
22%
108%
10%
6%
2,6-Dinitrotoluene
ug/L
ug/L
1.8
50
86%
92%
7%
Acenaphthene
2,4-Dinitrophenol
ug/L
1.9
50
78%
94%
88%
104%
12%
10%
2,4-Dinitrotoluene
ugg/L
11.0
50
50
38%
38%
0%
4-Nitrophenol
Fluorene
ug/L
1.6
50
50
92%
90%
100%
98%
8%
9%
4-Chlorophenyl phenyl ether
ug/L
1.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,

Pace Analytical Services, Inc.
9800 ICincey Avenue, Suite 100
Pace An alyti c a I Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 33 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
BASE/NEUTRALS & ACIDS -REPORTING FORM "A"
Batch: 92 44671
Samples: 92 0559894, 92 0559924
LABORATORY CONTROL SAMPLE AND
CONTROL SAMPLE DUPLICATE:
Reference
Dupl
Parameter
Units
MDL
Value
Recv
Recv
RPD
Diethyl —phthalate
u9
T—.O
-
50
1,2-Diphenylhydrazine
ug/L
1.5
50
82%
86%
5%
4,6-Dinitro-o-cresol
ug/L
1.0
50
94%
102%
8%
N-Nitrosodiphenylamine
ug/L
1.8
50
92%
96%
4%
4-Bromophenyl phenyl ether
ug/L
1.0
50
90%
94%
4%
Hexachlorobenzene
ug/L
1.0
50
90%
98%
9%
Pentachlorophenol
ug/L
1.4
50
90%
102%
13%
Phenanthrene
ug/L
1.0
50
92%
98%
6%
Anthracene
ug/L
1.0
50
96%
102%
6%
Di-n-butyl phthalate
ug/L
1.2
50
84%
90%
7%
Fluoranthene
ug/L
1.0
50
98%
106%
8%
Benzidine
ug/L
16.4
50
19%
15%
24%
Pyrene
ug/L
1.0
50
100%
112%
11%
Butyl benzyl phthalate
ug/L
1.0
50
78%
86%
10%
3,3-Dichlorobenzidine
ug/L
2.6
50
92%
94%
2%
Benz[a]anthracene
ug/L
1.0
50
94%
100%
6%
Chrysene
ug/L
1.0
50
96%
104%
8%
bis(2-Ethylhexyl) phthalate
ug/L
1.0
50
98%
104%
6%
Di-n-octyl phthalate
ug/L
1.4
50
106%
114%
7%
Benzo[b]fluoranthene
ug/L
1.0
50
100%
106%
6%
Benzo[k]fluoranthene
ug/L
1.0
50
94%
100%
6%
Benzo[a]pyrene
ug/L
1.0
50
96%
102%
6%
Indeno[1,2,3-cd]pyrene
ug/L
1.0
50
100%
104%
4%
Dibenz[a,h]anthracene
ug/L
1.0
50
108%
110%
2%
Benzo[g,h,i]perylene
ug/L
1.0
50
98%
100%
2%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
within it thw written consent of Pace Analvtical Services. Inc.

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: 70"75-9092
Fax: 70"75-9091
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 34 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PESTICIDES AND PCBS - REPORTING FORM "A"
Batch: 92 44698
Samples: 92 0559894, 92 0559924
METHOD BLANK:
Method
Parameter
Units
MDL
Blank
u T
D05
NU
alpha-BHC
ug/L
0.05
ND
beta-BHC
ug/L
0.05
ND
delta-BHC
ug/L
0.1
ND
gamma-BHC (Lindane)
ug/L
0.05
ND
Chlordane (tech)
ug/L
0.2
ND
4,4-DDD
ug/L
0.1
ND
4,4-DDE
ug/L
0.1
ND
4,4-DDT
ug/L
0.1
ND
Dieldrin
ug/L
0.02
ND
Endosulfan I
ug/L
0.1
ND
Endosulfan II
ug/L
0.1
ND
Endosulfan sulfate
ug/L
0.7
ND
Endrin
ug/L
0.06
ND
Endrin aldehyde
ug/L
0.2
ND
Heptachlor
ug/L
0.05
ND
Heptachlor epoxide
ug/L
0.8
ND
Methoxychlor
ug/L
0.5
ND
Toxaphene
ug/L
2.4
ND
Mirex
ug/L
0.2
ND
Aroclor-1016
ug/L
1.0
ND
Aroclor-1221
ug/L
1.0
ND
Aroclor-1232
ug/L
1.0
ND
Aroclor-1242
ug/L
1.0
ND
Aroclor-1248
ug/L
1.0
ND
Aroclor-1254
ug/L
1.0
ND
Aroclor-1260
ug/L
1.0
ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 IClncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. [phone]
Fax: 70"75-9091
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 35 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
PESTICIDES AND PCBS - REPORTING FORM "All
Batch: 92 44698
Samples: 92 0559894, 92 0559924
LABORATORY CONTROL SAMPLE
AND CONTROL SAMPLE DUPLICATE:
Reference
Dupl
Parameter
Units
u�
MDL
-6-.05
Value
0.16-
Recv
lb%
Recv
-M
RPD
ATZ[ri n
alpha-BHC
ug/L
0.05
0.16
94%
75%
22%
beta-BHC
ug/L
0.05
0.16
106%
94%
12%
delta-BHC
ug/L
0.1
0.16
113%
100%
12%
gamma-BHC (Lindane)
ug/L
0.05
0.16
119%
94%
23%
4,4-DDD
ug/L
0.1
0.16
131%
113%
15%
4,4-DDE
ug/L
0.1
0.16
125%
106%
16%
4,4-DDT
ug/L
0.1
0.16
150%
125%
18%
Dieldrin
ug/L
0.02
0.16
125%
106%
16%
Endosulfan I
ug/L
0.1
0.16
81%
69%
16%
Endosulfan II
ug/L
0.1
0.16
119%
88%
30%
Endosulfan sulfate
ug/L
0.7
0.16
125%
106%
16%
Endrin
ug/L
0.06
0.16
125%
106%
16%
Endrin aldehyde
ug/L
0.2
0.16
100%
88%
13%
Heptachlor
ug/L
0.05
0.16
94%
75%
22%
Heptachlor epoxide
ug/L
0.8
0.16
106%
94%
12%
Methoxychlor
ug/L
0.5
0.40
133%
110%
19%
Mirex
ug/L
0.2
0.40
90%
78%
14%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
...fti....f N.-.-Afton cnnennt of Par-^ Analvtical Services. Inc.

Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 36 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
VOLATILE ORGANICS -
Batch: 92 44678
Samples: 92 0559894,
REPORTING FORM "A"
92 0559924
METHOD BLANK:
Method
Parameter
Units
MDL
-Z
Blank
Chloromethane
ug
r
0
Chloroethene (Vinyl chloride)
ug/L
1.0
NO
Bromomethane
ug/L
1.0
NO
Chloroethane
ug/L
1.0
NO
Trichlorofluoromethane
ug/L
1.0
NO
Acrolein
ug/L
41
NO
1,1-Dichloroethene
ug/L
1.0
NO
Acrylonitrile
ug/L
36
NO
Dichloromethane
ug/L
3.3
NO
1,2-Dichloroethene, trans-
ug/L
1.0
NO
1,1-Dichloroethane
ug/L
1.0
NO
Chloroform
ug/L
1.1
NO
1,1,1-Trichloroethane
ug/L
1.5
NO
1,2-Dichloroethane
ug/L
1.0
NO
Carbon tetrachloride
ug/L
1.0
NO
Benzene
ug/L
1.0
NO
Trichloroethene
ug/L
1.0
NO
1,2-Dichloropropane
ug/L
1.0
NO
Bromodichloromethane
ug/L
1.0
NO
2-Chloroethoxyethene
ug/L
1.8
NO
cis-1,3-Dichloropropene
ug/L
1.1
NO
Toluene
ug/L
1.0
NO
trans-1,3-Dichloropropene
ug/L
1.0
NO
1,1,2-Trichloroethane
ug/L
1.0
NO
Dibromochloromethane
ug/L
1.0
NO
Tetrachloroethene
ug/L
1.0
NO
Chlorobenzene
ug/L
1.0
NO
Ethylbenzene
ug/L
1.0
NO
Bromoform
ug/L
1.0
NO
1,1,2,2-Tetrachloroethane
ug/L
1.1
NO
Surrogate - Dibromofluoromethane
%
99
Surrogate - Toluene-d8
%
97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel. [phone]
Fax:[phone]
Mr. Joe Morrison
Page 37
QUALITY CONTROL DATA PMarch 26
ACEProj9 Project Number: 660228517
Client Reference: NPDES Renewal Application
VOLATILE ORGANICS - REPORTING FORM "A"
Batch: 92 44678
Samples: 92 0559894, 92 0559924
METHOD BLANK: Method
Parameter Units MDL Blank
Surrogate - Bromofluorobenzene y—
SPIKE AND SPIKE DUPLICATE:
920559924
Spike
004
Spike
Dupl
Parameter
Units
u9
MDL
1.2
Outfall
Nam-
Spike
20
Recv
-7-0%
Recv
80
RPD
iW
C oromethane
Chloroethene (Vinyl chloride)
ug/L
1.0
ND
20
100%
95%
5%
Bromomethane
ug/L
1.0
1.0
NO
NO
20
20
95%
80%
100%
85%
5%
6%
Chloroethane
Trichlorofluoromethane
ug/L
ug/L
1.0
NO
20
90%
95%
5%
7%
Acrolein
ug/L
41
NO
200
86%
92%
1,1-Dichloroethene
ug/L
1.0
36
NO
NO
20
200
90%
66%
90%
60%
0%
10%
Acrylonitrile
ug/L
ug/L
3.3
ND
20
60%
65%
8%
Dichloromethane
1,2-Dichloroethene, trans-
ug/L
1.0
NO
20
85%
90%
90%
95%
6%
5%
1,1-Dichloroethane
ug/L
ug/L
1.0
1.1
NO
NO
20
20
95%
100%
5%
Chloroform
1,1,1-Trichloroethane
ug/L
1.5
1.0
ND
NO
20
20
105%
95%
110%
100%
5%
5%
1,2-Dichloroethane
Carbon tetrachloride
ug/L
ug/L
1.0
NO
20
100%
105%
5%
Benzene
ug/L
ug/L
1.0
1*.0
2.0
NO
20
20
85%
100%
90%
105%
6%
5%
Trichloroethene
1,2-Dichloropropene
ug/L
1.0
NO
20
95%
100%
5%
Bromodichloromethane
ug/L
1.0
NO
20
95%
105%
10%
2-Chloroethoxyethene
ug/L
ug/L
1.8
1.1
NO
NO
20
100%
105%
5%
cis-1,3-Dichloropropene
ug/L
1.0
NO
20
95%
100%
5%
Toluene
trans-1,3-Dichloropropene
ug/L
1.0
NO
20
95%
95%
105%
95%
10%
0%
1,1,2-Trichloroethane
ug/L
1.0
ND
20
Dibromochloromethane
ug/L
1.0
NO
20
20
95%
105%
100%
110%
5%
5%
Tetrachloroethene
ug/L
1.0
ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
-;*k # ►tie —io.n nnnewnt of Pace Analytical Services. Inc.

4.
Pace Analytical Services, Inc.
9800 Kncey Avenue, Suite 100
Pace Analytical Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Mr. Joe Morrison QUALITY CONTROL DATA March 26, 1996
Page 38 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
VOLATILE ORGANICS - REPORTING FORM "A"
Batch: 92 44678
Samples: 92 0559894, 92 0559924
SPIKE AND SPIKE DUPLICATE:
920559924
Spike
004
Spike
Dupl
Parameter
Units
MDL
Outfall •
Spike
Recv
Recv RPD
oro enzene
ug
I.0
ND
L�'
�
TM
Ethylbenzene
ug/L
1.0
ND
20
100%
105% 5%
Bromoform
ug/L
1.0
ND
20
90%
95% 5%
1,1,2,2-Tetrachloroethane
ug/L
1.1
ND
20
90%
95% 5%
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
MDL
Value
Recv
oromethane
ug
T 2
20
Chloroethene (Vinyl chloride)
ug/L
1.0
20
90%
Bromomethane
ug/L
1.0
20
100%
Chloroethane
ug/L
1.0
20
85%
Trichlorofluoromethane
ug/L
1.0
20
95%
Acrolein
ug/L
41
200
84%
1,1-Dichloroethene
ug/L
1.0
20
100%
Acrylonitrile
ug/L
36
200
58%
Dichloromethane
ug/L
3.3
20
85%
1,2-Dichloroethene, trans-
ug/L
1.0
20
90%
1,1-Dichloroethane
ug/L
1.0
20
90%
Chloroform
ug/L
1.1
20
100%
1,1,1-Trichloroethane
ug/L
1.5
20
110%
1,2-Dichloroethane
ug/L
1.0
20
100%
Carbon tetrachloride
ug/L
1.0
20
100%
Benzene
ug/L
1.0
20
95%
Trichloroethene
ug/L
1.0
20
105%
1,2-Dichloropropane
ug/L
1.0
20
90%
Bromodichloromethane
ug/L
1.0
20
95%
2-Chloroethoxyethene
ug/L
1.8
20
90%
cis-1,3-Dichloropropene
ug/L
1.1
20
95%
Toluene
ug/L
1.0
20
95%
trans-1,3-Dichloropropene
ug/L
1.0
20
95%
1,1,2-Trichloroethane
ug/L
1.0
20
90%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

V
Pace Analytical
Pace Analytical Services, Inc.
9800 IGncey Avenue, Suite 100
Huntersville, NC 28078
Tel: 70"75-9092
Fax: [phone]
Mr. Joe Morrison
QUALITY CONTROL
DATA
March 26, 1996
Page 39
PACE Project Number: 660228517
Client Reference: NPDES Renewal
Application
VOLATILE ORGANICS - REPORTING FORM "A"
Batch: 92 44678
Samples: 92 0559894, 92 0559924
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
MDL
Value Recv
i romoc loromethane
ugh -
T
9
Tetrachloroethene
ug/L
1.0
20 105%
Chlorobenzene
ug/L
1.0
20 100%
Ethylbenzene
ug/L
1.0
20 100%
Bromoform
ug/L
1.0
20 85%
1,1,2,2-Tetrachloroethane
ug/L
1.1
20 105%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace AnaNtical Services, Inc.

* ' Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Pace Analytical
Huntersville, NC 28078
Tel. 70"75-9092
Fax: 70"75-9091
Mr. Joe Morrison FOOTNOTES March 26, 1996
Page 40 for pages 15 through 39 PACE Project Number: 660228517
Client Reference: NPDES Renewal Application
MDL Method Detection Limit
NC No calculation due to value below detection limit.
ND Not detected at or above the MDL.
RPD Relative Percent Difference
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

ce,
I N C O R P O R A T E D
*** Attachment 9 ***
REPORT OF LABORATORY ANALYSIS
FMC Corporation
NPDES No. NC0005177
Permit Renewal 4/96
February 02, 1996
Mr. Joe Morrison
FMC Corporation - Lithium Division
P.O. Box 3925
Gastonia, NC 28053-3925
RE: PACE Project No. 660117.507
Client Reference: Effluent/Toe Drain Analysis
Dear Mr. Morrison:
Enclosed is the report of laboratory analyses for samples received
January 17, 1996.__
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
C"� kago
Clevecia M. Harris
Project Manager
Enclosures
98M &9 Avenue Suite 100 An Equal opportunfty anPbYer
HuntersviNe, NC 28078
TEL 704415-M
FAX [phone]

amnonuucuTAL LARMATORIE3
FMC Corporation - Lithium Division
P.O. Box 3925
Gastonia, NC 28053-3925
REPORT OF LABORATORY ANALYSIS
Attn: Mr. Joe Morrison
Client Reference: Effluent/Toe Drain Analysis
February 02, 1996
PACE Project Number: 660117507
PACE Sample Number:
92 0536703
Date Collected:
01/17/96
Date Received:
01/17/96
Client Sample ID:
Effluent
Units MDL DATE ANALYZED
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Solids, Total Suspended
mg/L 1 1.0 01/19/96
PACE Sample Number:
92 0536711
Date Collected:
01/17/96
Date Received:
01/17/96..
Client Sample ID:
Toe Drain
Units MOL DATE ANALYZED
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand, 05 Day
mg/L
2.0
NA (1)
02/02/96
Chromium
mg/L
0.01
NO
02/01/96
Copper
mg/L
mg/L
0.01
0.1
NO
NO
02/01/96
O1/23/96
Nitrogen, Ammonia
Solids, Total Suspended
mg/L
1
12
01/19/96
Zinc
mg/L
0.05
0.06
02/01/96
ORGANIC ANALYSIS
PURGEABLE HALOCARBONS
Dichlorodifluoromethane
ug/L
1.0
NO
O1/19/96
Chloromethane
Chloroethene (Vinyl chloride)
ug/L
ug/L
1.0
1.0
NO
NO
O1/19/96
O1/19/96
Bromomethane
ug/L
ug/L
1.0
1.0
NO
NO
O1/19/96
O1/19/96
Chloroethane
Trichlorofluoromethane
ug/L
1.0
NO
O1/19/96
1,1-Dichloroethene
ug/L
1.0
NO
NO
O1/19/96
O1/19/96
Dichloromethane
trans-1,2-Dichloroethene
ug/L
ug/L
1.0
1.0
NO
O1/19/96
1,1-Dichloroethane
ug/L
1.0
NO
O1/19/96
9800 KmM Avenue Suite 100
An E�W oppmu* DOW
Hunwvile, NC 28078
TE L- 70447S9092
FAX: [phone]

( p I 'r
' REPORT OF LABORATORY ANALYSIS
EMnWMU&, TAL LABOR MMES
Mr. Joe Morrison
Page 2
Client Reference: Effluent/Toe Drain Analysis
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
ORGANIC ANALYSIS
Units MDL
February 02, 1996
PACE Project Number: 660117507
92 0536711
01/17/96
01/17/96
Toe Drain
DATE ANALYZED
PURGEABLE HALOCARBONS
Chloroform
ug/L
1.0
NO
01/19/96
1,1,1-Trichloroethane
ug/L
ug/L
1.0
1.0
NO
NO
01/19/96
01/19/96
Carbon tetrachloride
1,2-Dichloroethane
ug/L
1.0
NO
01/19/96
1,1,2-Trichloroethene
ug/L
ug/L
1.0
1.0
NO
NO
01/19/96
01/19/96
1,2-Dichloropropane
Bromodichlormethane
ug/L
ug/L
1.0
1.0
NO
NO
01/19/96
01/19/96
2-Chloroethoxyethene
cis-1,3-Dichloropropene
ug/L
1.0
NO
01/19/96
trans-1,3-Dichloropropene
ug/L
ug/L
1.0
1.0
NO
NO
01/19/96
01/19/96
1,1,2-Trichloroethane
Tetrachloroethene
ug/L
1.0
NO
01/19/96
Dibromochloromethane
ug/L
ug/L
1.0
1.0
NO
NO
01/19/96
01/19/96
Bromoform
1,1,2,2-Tetrachloroethane
ug/L
1.0
NO
01/19/96
01/19/96
Chlorobenzene
1,3-Dichlorobenzene
ug/L
ug/L
1.0
1.0
NO
NO
01/19/96
1,4-Dichlorobenzene
ug/L
1.0
NO
01/19/96
1,2-Dichlorobenzene
ug/L
1.0
NO
01/19/96
9800 K" Avenue Suite 100 An Equal OW * EffPb➢f
HunWsvik, NC 28M
TEL [phone]M
FAX: [phone]

W4a
O R P e, O R A T E DD
Mr. Joe Morrison
Page 3
REPORT OF LABORATORY ANALYSIS
Client Reference: Effluent/Toe Drain Analysis
These da a have been reviewed and are approved for release.
Dan H. Jones
Inorganic Department
Margaret S. Harding
Manager, Organic Chemistry
February 02, 1996
PACE Project Number: 660117507
9800 Kincey Avenue Suite 100 An Equal opportunity foyer
HuntersviYe. NC 28078
TEL [phone]
FAX:[phone]

•
r A or
=3
wunnonuYFYTAL LABORATORIES
Mr. Joe Morrison
Page 4
REPORT OF LABORATORY ANALYSIS
FOOTNOTES
for pages 1 through
Client Reference: Effluent/Toe Drain Analysis
MDL Method Detection Limit
NA Not analyzed due to laboratory accident.
ND Not detected at or above the MDL.
(1) Sample depleated , resample requested.
February 02, 1996
3 PACE Project Number: 660117507
9800 Kncey Averwe suite 100 An Equal OPPorlurNry foyer
HunterwHe, NC 28078
TEL [phone]
FAX: [phone]

rr 3
�.nnn�uu�vr�� 1 �wAO�T[]iilE9
REPORT OF LABORATORY ANALYSIS
Mr. Joe Morrison QUALITY CONTROL DATA
Page 5
Client Reference: Effluent/Toe Drain Analysis
Solids, Total Suspended
Batch: 92 42970
Samples: 92 0536703, 92 0536711
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
So—li3s, Total Suspended
LABORATORY CONTROL SAMPLE:
Parameter
So i s, otal Suspended
Units
mg/L
Units
mg/L
February 02, 1996
PACE Project Number: 660117507
Duplicate
Method 920536703 of
MDL Blank Effluent 92 0536703 RPD
1 NO 1.0 2.0 67%
MDL
1
Reference
Value Recv
100 98%
98W KmM Avenue Suite 100 An Equal CPPoftnih EnooYer
Huntersvile, NC 28078
TEL [phone]
FAX:[phone]

ce,
O R 4 i E 0
Mr. Joe Morrison
Page 6
REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA
Client Reference: Effluent/Toe Drain Analysis
Zinc
Batch: 92 43380
Samples: 92 0536711
METHOD BLANK:
Parameter
Units
MDL
Barium
mg/L
0.02
Cadmium
mg/L
0.01
Chromium
mg/L
.0.01
Copper
mg/L
0.01
Lithium
mg/L
0.01
Manganese
mg/L
0.01
Nickel
Zinc
February 02, 1996
PACE Project Number: 660117507
Method
Blank
ND
NO
ND
ND
NO
ND
mg/L 0.01 NO
mg/L 0.01 NO
LABORATORY
CONTROL SAMPLE AND CONTROL SAMPLE
DUPLICATE:
Reference
Dupl
Parameter
Units
MDL
Value
Recv Recv RPD
arium
mg/L
0.02
2.0
109%
Cadmium
mg/L
0.01
2.0
97%
Chromium
mg/L
0.01
2.0
96%
Copper
mg/L
0.01
2.0
100%
Lithium
mg/L
0.01
2.0
92%
Manganese
mg/L
0.01
2.0
99%
Nickel
mg/L
0.01
2.0
99%
Zinc
mg/L
0.01
2.0
97%
9800 WmM Avenue Suite 100 An Equal Opp" EmOco w
Hunteniville. NC 28078
TEL 704475-M
FAX:[phone]

ce.,
...
0 O R P ORATED
Mr. Joe Morrison
Page 7
REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA February 02, 1996
PACE Project Number: 660117507
Client Reference: Effluent/Toe Drain Analysis
PURGEABLE HALOCARBONS
Batch: 92 43041
Samples: 92 0536711
METHOD BLANK:
Method
Parameter
Units
MDL
Blank
is oro ifluoromethane
ug/L
1.0
NO
Chloromethane
ug/L
1.0
ND
Chloroethene (Vinyl chloride)
ug/L
1.0
NO
Bromomethane
ug/L
1.0
ND
Chloroethane
ug/L
1.0
NO
Trichlorofluoromethane
ug/L
1.0
NO
1,1-Dichloroethene
ug/L
1.0
NO
Dichloromethane
ug/L
1.0
ND
trans-1,2-Dichloroethene
ug/L
1.0
NO
1,1-Dichloroethane
ug/L
1.0
ND
Chloroform
ug/L
1.0
ND
1,1,1-Trichloroethane
ug/L
1.0
ND
Carbon tetrachloride
ug/L
1.0
ND
1,2-Dichloroethane
ug/L
1.0
ND
1,1,2-Trichloroethene
ug/L
1.0
NO
1,2-Dichloropropane
ug/L
1.0
ND
Bromodichlormethane
ug/L
1.0
ND
2-Chloroethoxyethene
ug/L
1.0
NO
cis-1,3-Dichloropropene
ug/L
1.0
NO
trans-1,3-Dichloropropene
ug/L
1.0
ND
1,1,2-Trichloroethane
ug/L
1.0
NO
Tetrachloroethene
ug/L
1.0
NO
Dibromochloromethane
ug/L
1.0
NO
Bromoform
ug/L
1.0
ND
1,1,2,2-Tetrachloroethane
ug/L
1.0
NO
Chlorobenzene
ug/L
1.0
ND
1,3-Dichlorobenzene
ug/L
1.0
ND
1,4-Dichlorobenzene
ug/L
1.0
ND
1,2-Dichlorobenzene
ug/L
1.0
ND
9800 IOncey Avenue Suite 100 An EQuw Cppw" Envlow
HunteisviBe, NC 28078
TEL [phone]M
FAk 704.875-9091

ace.,
I N C O R P O R A T E D
�..� ...Tjj..#JNW
Mr. Joe Morrison
Page 8
REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA FebrPACE uProject Number: 660117507
Client Reference: Effluent/Toe Drain Analysis
PURGEABLE HALOCARBONS
Batch: 92 43041
Samples: 92 0536711
LABORATORY CONTROL SAMPLE:
Reference
Parameter
Units
MDL
Value
20
Recv
427.
Dichlorodifluoromethane
ug/L
1.0
20
60%
Chloromethane
Chloroethene (Vinyl chloride)
ug/L
ug/L
1.0
1.0
20
0
Bromomethane
ug/L
1.0
20
20
125%
65%
Chloroethane
Trichlorofluoromethane
ug/L
ug/L
1.0
1.0
20
330%
R1
1,1-Dichloroethene
ug/L
1.0
20
20
95%
60/
Dichloromethane
ug/L
ug/L
1.0
1.0
20
90%
trans-1,2-Dichloroethene
ug/L
1.0
20
100%
1,1-Dichloroethane
ug/L
1.0
20
65%
Chloroform
1,1,1-Trichloroethane
ug/L
1.0
20
95%
Carbon tetrachloride
ug/L
1.0
20
20
55%
80%
1,2-Dichloroethane
ug/L
1.0
20
135%
1,1,2-Trichloroethene
ug/L
1.0
20
60%
1,2-Gichloropropane
ug/L
1.0
20
47%
Bromodichlormethane
ug/L
1.0
20
110%
cis-1,3-Dichloropropene
ug/L
1.0
trans-1,3-Dichloropropene
ug/L
1.0
20
20
145%
50%
1,1,2-Trichloroethane
ug/L
1.0
20
115%
Tetrachloroethene
ug/L
1.0
20
125%
Dibromochloromethane
ug/L
1.0
20
60%
Bromoform
1,1,2,2-Tetrachloroethane
ug/L
ug/L
1.0
1.0
20
115%
Chlorobenzene
ug/L
1.0
20
20
100%
95%
1,3-Dichlorobenzene
ug/L
1.0
20
100%
1,4-Dichlorobenzene
ug/L
1.0
20
95%
1,2-Dichlorobenzene
ug/L
1.0
9800 09 Avenue Suite 100 An Equal CPP f
Kmwsv&, NC 28078
TEL 704.87S4M
FAX: [phone]

rmmlm�.Ru- M. REPORT OF LABORATORY ANALYSIS
WML LAWMTOMM
Mr. Joe Morrison
Page 9
FOOTNOTES February 02, 1996
for pages 5 through 8 PACE Project Number: 660117507
Client Reference: Effluent/Toe Drain Analysis
MDL Method Detection Limit
ND Not detected at or above the MDL.
ntrol limit, however, this compound is not
R1 Recovery falls outside the quality co
detected in the associated sample(s).
RPD Relative Percent Difference
9800 IGncey Avenue Suite 100 An Equal opportunity Employer
Huntersvitle, NC 28078
TEL [phone]M
FAX:[phone]

IEA Project #:
Client Name:
r
*** Attachment 8 ***
Eli v
IEA LABORATORY RESULTS C,,y
990-022
EBASCO Services
APR 17
FMC Corporation
Permit Renewal 4/96
NPDES No. NC0005177
Date
Results Analyzed
Sample # Client ID Parameter _ ���
�-__
TOTAL METALS:
<0.02
mg/L
03/05/92
Sample
Set
I
Copper
<0.02
mg/L
03/05/92
Sample
Set
II
Copper
<0.005
mg/L
02/29/92
Sample
Set
I
Selenium
<0.005
mg/L
02/29/92
Sample
Set
II
Selenium
Demand
2,0
mg/L
02/26/92
Sample
Set
I
Biochemical Oxygen
Demand
3,4
mg/L
02/26/92
Sample
Set
II
Biochemical Oxygen
<25
m /L
02/26/92
Sample
Set
I
Chemical Oxygen Demand
<25
mg/L
03/12/92
Sample
Set
II
Chemical Oxygen Demand
17
mg/L
03/12/92
Sample
Set
I
Chloride
15
mg/L
03/03/92
Sample
Set
II
Chloride
0.5
mg/L
03/03/92
Sample
Set
I
Fluoride
0.5
mg/L
03/03/92
Sample
Set
II
Fluoride
<0.02
mg/L
02/28/92
Sample
Set
I
Nitrate/Nitrite
0.0
mg/L
8
02/28/92
Sample
Set
II
Nitrate/Nitrite
2
0,06
mg/L
0/ /92
Sample
Set
I
Total Phosphorus
0.0
mg/L
3/10/92
00/10/92
Sample
Set
II
Total Phosphorus
36
mg/L
Sample
Set
I
Sulfate
340
mg/L
02/28/92
Sample
Set
II
Sulfate
<1.0
mg/L
03/02/92
Sample
Sample
Set
Set
I
I
Sulfide
Total Suspended Solids
5.0
32
mg/L
m /L
02/28/92
02/28/92
Sample
Set
II
Total Suspended Solids
7
mg/L
g
02/28/92
Sample
Set
I
i
Oil•& Grease (Gravmetric)
✓� 4 ) q Z �j �I�l� i
A-Ot 1 c-A9D L5 D S
NO, NC�C,00000Z
,5-mr��

7
IEA LABORATORY RESULTS
Attachment 8, Page 2
FMC Corporation
NPDES Renewal 4/96
NPDES No. NC0005177
IEA Project #: 990-022(S)
Client Name: EBASCO Services
Date
Results Analyzed
le # Client ID Parameter ____________
<0.2 mg/L 02/27/92
1 Sample Set I Total Kjeldahl Nitrogen <0.2 mg/L 02/27/92
2 Sample Set II Total Rjeldahl Nitrogen

FMC CORPORATION
LITHIUM DIVISION
NPDES No. NC0005177
Permit Renewal 4/96
ATTACHMENT 7
APR 17 1996
NARRATIVE DESCRIPTION OF TREATMENT WORKS SLUDGE MANAGEMENT PLAN
FMC Corporation's Lithium Division facility in Bessemer City ("FMC") operated
two aerobic digestion sewage treatment plants. One has a capacity of 5,000
gallons/day and the other a capacity of 10,000 gallons/day. Both discharge to
FMC's Lower Pond and ultimately to outfall 001. Periodically, accumulated
solids are pumped from the system by a commercial septic management firm for
treatment and disposal elsewhere.
FMC is actively exploring the potential to collect sanitary wastes managed in
these package treatment units and discharge these wastes to the City of Bessemer
City's municipal treatment works. Implementation of this project would
eliminate management of sanitary wastes at this facility.