WQ0016247_Regional Office Historical File Pre 2018 (14)

I L E
vts
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory Donald van der Vaart
Governor Secretary
May 6, 2015
Synagro Central, LLC
284 Boger Road
Mocksville, North Carolina 27028-7619
Attn: Marshall Puryear
Subject: Acknowledgement'of Receipt of the 2014 Annual Report
Synagro Central, LLC - Permit No.: WQ0016247
Synagro Western Piedmont RLAP
Land Application of Residual Solids (503)
Alexander County
Dear Mr. Puryear:
The Mooresville Regional Office (MRO) received and reviewed the 2014 Annual Report for the
above permit. The information submitted appears to meet permit requirements. This permit was
recently modified for an additional residual source and renamed to Synagro Western Regional
RLAP to avoid confusion with other city of Statesville in-house permits.
I may be reached by phone at [phone] or email (maria.schutte(a-).ncdenr.gov) should you
have questions.
Sincerely,
Maria Schutte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
CC: Mr. Andy Smith, Town of Statesville (email)
Mr. Todd Norman, Town of Statesville (email)
Ed Hardee, LAU Compliance, CO -Raleigh (email)
Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115
Phone: [phone] / Fax:[phone] / Customer Service:1-877-623-6748
Internet: www.ncdenr.gov
An Equal Opportunity %Affirmative Acton Employer — Made in part by recycled paper

RECEIVED/NCDENR/DWR
MAR 10 2015
WQROS
MOORESVILLE REGIONAL OFFICE
CITY OF STATESVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. W00016247
2014 ANNUAL REPORT

City of Statesville, IBC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and Land
Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR
Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

ANNUAL LAN® APPLICATION CERTIFICATION FORM
WQ Permit #: W00016247 County Iredell Year 2014
Facility Name (as shown on permit) City of Statesville, Third Creek WWTP & Fourth Creek WWTP
NPDES No. NCO020591 & NCO031836
Land Application Operator S�nagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 31
Total number of fields utilized for land application during the year: 11
Total amount of dry tons applied during the year for all application sites: 639.01
Total number of acres utilized for land application during the year: 225.8
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of m_ y kno led 'e and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false in i i g nes and imprisonment for
knowing violations."
Todd ar n. O erations Director PODS`
Per itte lame d Tithe ype or print) na r o mi Date
2015
Signatur of Preparer* Date Shgnature of Land Applier Date
(if differbrit from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2014 ANNUAL OPERATIONS SUMMARY e LAND APPLICATION
STATESVILLE, NC
STATESVILLE, NC FOURTH CREEK CAKE
MONTHNEAR
February 2014
March 2014
June 2014
October 2014
YEARLY TOTAL
AMOUNT UNIT
704.00
Y
384.00
Y
1,056.00
Y
325.00
Y
2,469.00
Y
STATESVILLE, SIC THIRD CREEK CAKE
MONTHNEAR
January 2014
February 2014
March 2014
June 2014
October 2014
YEARLY TOTAL
AMOUNT UNIT
DRY METRIC
DRY TONS
UNIT
TONS
87.93
D
79.76
47.97
D
43.50
126.03
D
114.30
40.89
D
37.09
302.82 D
DRY TONS UNIT
640.00
Y
76.49 D
544.00
Y
65.02 D
160.00
Y
19.12 D
928.00
Y
120.21 D
400.00
Y
55.35 D
2,672.00
Y
336.19 D
274.65
DRY METRIC
TONS
69.37
58.96
17.34
109.03
50.21
304.91
1 /26/2015

2014 ANNUAL REPORT
PROJECT:
FACILITY:
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
City of Statesville, NC
Third Creek WWTP
NCO020591
Todd Norman, Residuals
Superintendent
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Todd Norman, Third Creek WWTP Supt.
Town of Statesville
P.O. Box 1111
Statesville, NC 28677.
[phone]
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

2014 ANNUAL REPORT
PROJECT:
FACILITY:
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
City of Statesville, NC
Fourth Creek WWTP
NCO031836
Andy Smith, Residuals Superintendent
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Andy Smith, Fourth Creek WWTP Supt.
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type
CAx
CAx
CAx
Date Sampled (grab) or 01/09/14
05/11/14
09/26/14
Date Composited
Percent Solids
14.83
14.17
14.94
PARAMETERS (mg/kg dry weight)
Arsenic
5
5
4
Cadmium
5
5
4
Mercury
1.3
0.5
<0.4
Chromium
48
56
42
Copper
364
308
370
Lead
36
32
30
Molybdenum
14
12
11
Nickel
34
46
22
Selenium
5
<5
<5
Zinc
709
704
458
Total Phosphorus
25800
23300
29600
TKN
54600
59600
50500
Ammonia -Nitrogen
9510
15100
7760
Nitrate and Nitrite
12.1
<2
. <2
Laboratory
A&L Eastern Laboratories Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed $o assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submjtting false information, including the possibility of fines and imprisonment for knowing violations."
X
Date Dom-
DENR FORM RSSF (5/2003) Printed: Tuesday - January 27, 2015 at 11:03:55 for: 2084 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type CAx
CAx
CAx
Date Sampled (grab) or 01/09/14
05/11/14
09/26/14
Date Composited
Percent Solids 14.83
14.17
14.94
PARAMETERS (mg/kg dry weight)
Aluminum 26200
20900
30100
Calcium 10600
29200
6750
Magnesium 2590
3970
1620
pH 6.42
7.98
5.67
Potassium 2960
4130
2260
Sodium 843
862
881
Laboratory
A&L Eastern Laboratories Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant PAnalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
ft
(SIGNATRE OF—PREPARER)
NR - Data Not Reported or Data Not Required
Date ::2- ( s l
DENR FORM RSSF-B (7/2002) Printed: Tuesday - January 27 2015 at 11:04:28 for: 2084 01

Page: 1 of 2
Report Number: 14-010-0201
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97420
Sample Id : 4TH CK
A&L EasternLaboratories, Inc.
@P.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wrwwaleastern.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/9/2014 09:20:00
Date Received: 01/10/2014 00:00
Date Reported: 01/15/2014
Total Solids *
14.83
148300
100.0
JM
01/10/2014 14:19
SM-2540G
Moisture *
85.17
100.0
JM
01/10/2014 14:19
SM-2540G
Total Kjeldahl Nitrogen
5.46
54600
10.0
JM
01/13/2014 08:30
SM-4500-NH3C-TKN
Total Phosphorus
2.58
25800
100
KM
01/13/2014 11:35
SW 6010C
Total Potassium
0.30
2960
100
KM
01/13/2014 11:35
SW 6010C
Total Sulfur
0.88
8800
100
KM
01/13/2014 11:35
SW 6010C
Total Calcium
1.06
10600
100
KM
01/13/2014 11:35
SW 6010C
Total Magnesium
0.26
2590
100
KM
01/13/2014 11:35
SW 6010C
Total Sodium
0.08
843
100
KM
01/13/2014 11:35
SW 6010C
Total Iron
25300
100
KM
01/13/2014 11:35
SW 6010C
Total Aluminum
26200
100
KM
01/13/2014 11:35
SW 6010C
Total Manganese
1580
5
KM
01/13/2014 1-1:35
SW 6010C
Total Copper
364
5
KM
01/13/2014 11:35
SW 6010C
Total Zinc
709
5
KM
01/13/2014 11:35
SW 6010C
Ammonia Nitrogen
0.95
9510
10.0
JM
01/13/2014 08:30
SM-4500-NH3C
Organic N
4.51
45090
10.0
01/13/2014 08:30
CALCULATION
Nitrate+Nitrite-N
12.1
2.00
JM
01/13/2014 08:30
SM-450ONO3F
Total Cadmium
5.0
2.0
KM
01/13/2014 11:35
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made C�m
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-010-0201
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer.
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97420
Sample Id: 4TH CK
A&L Eastern Laboratories, Inc.
aLid
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/9/2014 09:20:00
Date Received: 01/10/2014 00:00
Date Reported: 01/15/2014
Total Chromium
48
5
KM
01/13/2014 11:35
SW 6010C
Total Nickel
34
5
KM
01/13/2014 11:35
SW 6010C
Total Lead
36
5
KM
01/13/2014 11:35
SW 6010C
Total Arsenic
5.0
3.0
KM
01/13/2014 11:35
SW 6010C
Total Mercury
1.3
0.4
KM
01/13/2014 09:00
SW-7471B
Total Selenium
5.0
5.0
KM
01/13/2014 11:35
SW 6010C
pH (Standard Units) *
6.42
2.00
JM
01/13/2014 08:30
SW-9045D
Total Molybdenum
14
5
KM
01/13/2014 11:35
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N" AND "Se". THE MATRIX SPIKE WAS OUT OF. LIMITS FOR "As" AND "S".
ALL OTHER QC
DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
Debbie Holt

,SAMPLING LOG #
ST �I�I�I�IIIIIfII�IIIIIIIIIIILIIIIII�IIIIIIIIIIII�Ii 46493
CUSTOMER.- SYNAGRO SOUTHEA S)'b1AGq0CENT.RALL CISTATESVILLE- G 1''l 0-2014
STATES.VqLLE 4TH. CK. 12;57.06
PROJECT -MANAGER: 1146
3 3�') J. 7
�CHARN. OF CUSTODY
'R,ECORUZ ANALYSIS
RECORD-,
per field sampling procedures
1,70 QalleCUOO of MOSe samples.
SAMI�ktR
A&L• CUSTOMER.
SAMPLING-
SAMPLE
OF
SAMPLING
METHOD
METHOD
LAB' SAMPLE I.D.
LOCATION
TYPE.
CONTAINERS
DATE TIME
PRESERVED
SHIPPED
RIP
Relinquished by SaMplen/
Date •/Zl Time
Recieved by:
REMAFW&
Relinquished, by:
Datt7l Time
Redeved
'[Ps 1Z_S;2929?2-trj
2,L4Q1z-
-7- -or
Relinquished by;
Dqfe .1 Time
Reclev'ed bT�
SPECIAL INSTRUCTIONS:
For
monitoring purposes.
P 0
ANALY-SISREQUEST
SAMPLE
:SLj
NH'-_'�
47-
WO 3--N
Organic
N
Od.
01,
Pb-
As:
H q
Se
PH
aCO �
e Uiv!
Voliatile
Solids.,
[NO2_�N
mow
;-00f
A,0.0,
bow
P10r
pw
1.4011'
tow
A-000
Pw
tog
POW
L/
-SLI: Total:S-611d' -(Mbl!§tUrd):,'Total-Kj'oldeihiNitro on Phosphorus, and Potassium
SL2; 5asiaTest;SLI plus. Sulfur.'Calclom,,. Magnesium, Sodium,.Iroq,:Aluminum'..MEirfganese,'Cbpp.or and Zinc
WhIfe—A-&L. - Canary— MANAGER COPY

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 1/9/2014 111/2014-3/31/2014 0.7309
Na mg/I = (Na mg/kg x % Solids) + 100 = (843 x 14.8300) + 100 = 125.017
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (10600 x 14.8300) + 100 = 1571.98
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2590 x 14.8300) _ 100 = 384.097
Na meq = Na mg/I + Molec.Wgt.Na = 125.017 + 23 = 5.43552
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1571.98 + 20 = 78.599
Mg meq = Mg mg/I + Molec.Wgt.Mg = 384.097 + 12 = 32.0081
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.43552 + SgrRoot[0.5(78.599+32.0081)] = 0.730911
Printed: 1/27/2015
Page 1 11:11

Page: 1 of 2
Report Number: 14-133-0206
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55320
Sample ld : STATESVILLE 4TH CK
99YY A L Eastern Laboratories, Inc.
F9 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com -
Project: STATESVILLE 4TH CK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 5/11/2014 11:15:00
Date Received: 05/13/2014 00:00
Date Reported: 05/16/2014
Total Solids *
14.17
141700
100.0
JM
05/13/2014 13:59
SM-2540G
Moisture *
85.83
100.0
JM
05/13/2014 13:59
SM-2540G
Total Kjeldahl Nitrogen
5.96
59600
10.0
JM
05/14/2014 08:24
SM-4500-NH3C-TKN
Total Phosphorus
2.33
23300
100
KM
05/14/2014 12:42
SW 601OC
Total Potassium
0.41
4130
100
KM
05/14/2014 12:42
SW 661OC
Total Sulfur
0.76
7610
100
KM
05/14/2014 12:42
SW 601OC
Total Calcium
2.92
29200
100
KM
05/14/2014 12:42
SW 601 OC
Total Magnesium
0.40
3970
100
KM
05/14/2014 12:42
SW 601OC
Total Sodium
0.09
862
100
KM
05/14/2014 12:42
SW 601OC
Total Iron
20300
100
KM
05/14/2014 12:42
SW 6010C
Total Aluminum
20900
100
KM
05/14/2014 12:42
SW 6010C
Total Manganese
1490
5
KM
05/14/2014 12:42
SW 601OC
Total Copper
308
5
KM
05/14/2014 12:42
SW 601OC
Total Zinc
704
5
KM
05/14/2014 12:42
SW 6010C
Ammonia Nitrogen
1.51
15100
10.0
JM
05/14/2014 08:24
SM-4500-NH3C
Organic N
4.45
44500
10.0
05/14/2014 08:24
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
05/14/2014 08:25
SM-450ONO3F
Total Cadmium
5.0
2.0
KM
05/14/2014 12:42
SW 601OC
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-133-0206
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55320
Sample Id : STATESVILLE 4TH CK
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com
Project; STATESVILLE 4TH CK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 5/11/2014 11:15:00
Date Received: 05/13/2014 00:00
Date Reported: 05/16/2014
Total Chromium
56
5
KM
05/14/2014 12:42 _
SW 6010C
Total Nickel
46
5
KM
05/14/2014 12:42
SW 6010C
Total Lead
32
5
KM
05/14/2014 12:42
SW 6010C
Total Arsenic
5.0
3.0
KM
05/14/2014 12:42
SW 6010C
Total Mercury
0.5
0.4
KM
05/14/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
05/14/2014 12:42
SW 6010C
pH (Standard Units) *
7.98
2.00
JM
05/14/2014 08:30
SW-9045D
Total Molybdenum
12
5
KM
05/14/2014 12:42
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr", "Fe", "Ni", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

. v��!•t.sa_e � tF�l tli �l��.� iiewi[V i✓L��FI�.dE'C� akMt
Product Code Product Name .Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAFE 5/11/2014 4/112014-6130/2014 0.4715
Na mg/I = (Na mg/kg x % Solids) _ 100 = (862 x 14.1700) + 100 = 122.145
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (29200 x 14.1700) + 100 = 4137.64
Mg mg/I = (mg mg/kg x % Solids) + 100 = (3970 x 14.1700) = 100 = 562.549
Na meq = Na mg/I _ Molec.Wgt.Na = 122.145 = 23 = 5.31067
Ca meq = Ca mg/1 + Molec.Wgt.Ca = 4137.64 = 20 = 206.882
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 562.549 _ 12 = 46.8791
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.31067 = SgrRoot[0.5(206.882+46.8791)] = 0.471468
Printed: 1 /27/2015
Page 1 11:12

Page: i of 2
Report Number: 14-273-0211
y Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 57857
Sample Id : STATESVILLE 4TH CK
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 9/26/2014 13:25:00
Date Received: 09/30/2014 00:00
Date Reported: 10/06/2014
Total Solids *
14.94
149400
100.0
BW
09/30/2014 14:15
SM-2540G
Moisture *
85.06
100.0
BW
09/30/2014 14:15
SM-2540G
Total Kjeldahl Nitrogen
5.05
50500
10.0
JM
10/01/2014 08:44
SM-4500-NH3C-TKN
Total Phosphorus
2.96
29600
100
KM
10/01/2014 12:04
SW 6010C
Total Potassium
0.23
2260
100
KM
10/01/2014 12:04
SW 6010C
Total Sulfur
0.83
8250
100
KM
10/01/2014 12:04
SW 6010C
Total Calcium
0.68
6750
100
KM
10/01/2014 12:04
SW 6010C
Total Magnesium
0.16
1620
100
KM
..1.0/01/2014 12:04
SW 6010C.
Total Sodium
0.09
881
100
KM
10/01/2014 12:04
SW 6010C
Total Iron
27100
100.
KM
10/01/2014 12:04
SW 6010C
Total Aluminum
30100
100
KM
10/01/2014 12:04
SW 6010C
Total Manganese
853
5
KM
10/01/2014 12:04
SW 6010C
Total Copper
370
5
KM
10/01/2014 12:04
SW 6010C
Total Zinc
458
5
KM
10/01/2014 12:04
SW 6010C
Ammonia Nitrogen
0.78
7760
10.0
JM
10/01/2014 08:44
SM-4500-NH3C
Organic N
4.27
42740
10.0
10/01/2014 08:44
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
10/01/2014 08:45
SM-450ONO3F
Total Cadmium
4.0
2.0
KM
10/01/2014 12:04
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , L�dg
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-273-021'1 �L
A&L Eastern Laboratories, Inc.
Account Number: 46493 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Submitted By: ERIC THOMPSON www.aleasteni.com
Send To: SYNAGRO CENTRAL LLC/STATESVILLE Project: STATESVILLE 4TH CK
Mary Brewer NC CERT#257
284 BOGER RD
MOCKSVILLE , NC 27028 '
Lab Number: 57857
Sample Id : STATESVILLE 4TH CK
REPORT OF ANALYSIS Date Sampled: 9/26/2014 13:25:00
Date Received: 09/30/2014 00:00
Date Reported: 10/06/2014
Total Chromium
42
5
KM
10/01/2014 12:04
SW 6010C
Total Nickel
22
5
KM
10/01/2014 12:04
SW 6010C
Total Lead
30
5
KM
10/01/2014 12:04
SW 6010C
Total Arsenic
4.0
3.0
KM
10/01/2014 12:04
SW 6010C
Total Mercury
<0.4
0.4
KM
09/30/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/01/2014 12:04
SW 6010C
pH (Standard Units) *
5.67
2.00
JM
10/01/2014 08:50
SW-9045D
Total Molybdenum
11
5
KM
10/01/2014 12:04
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE AND
MSD WERE OUT OF LIMITS FOR "Mg".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

A. Col L. dl 4�l ! C�� t... � ! �,.
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 9/26/2014 9/1/2014-10/31/2014 0.9632
Na mg/I = (Na mg/kg x % Solids) = 100 = (881 x 14.9400) _ 100 = 131.621
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (6750 x 14.9400) _ 100 = 1008.45
Mg mg/I = (mg mg/kg x % Solids) = 100 = (1620 x 14.9400) = 100 = 242.028
Na meq = Na mg/I _ Molec.Wgt.Na = 131.621 + 23 = 5.72267
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 1008.45 + 20 = 50.4225
Mg meq = Mg mg/I + Molec.Wgt.Mg = 242.028 + 12 = 20.169
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.72267 _ SgrRoot[0.5(50.4225+20.169)] = 0.963247
Printed: 1 /27/2015
Page 1 11:12

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: W00016247 Laboratory
Facility Name: STATESVILLE, NC A&L Eastern Laboratories Inc.
NPDES# : NCO020591
or WQ# (residual only)
WWTP Name: THIRD CREEK
Residuals Analysis Data
Product Type
CAK
CAx
CAE{
CAR
Date Sampled (grab) or 01/09/14
05/11/14
09/26/14
01/29/15 i
Date Composited
Percent Solids
14.19
15.38
16.43
15.49
PARAMETERS (mg/kg dry weight)
Arsenic
5
3
3
4
Cadmium
12
11
15
17
Mercury
0.4
<0.4
<0.4
0.6
Chromium
88
85
101
109
Copper
438
369
453
417
Lead
99
82
127
107
Molybdenum
23
16
19
20
Nickel
55
54
47
52
Selenium
<5
<5
<5
<5
Zinc
1090
1230
965
1150
Total Phosphorus
19300
18100
20400
17300
TKN
49300
53400
39700
34100
Ammonia -Nitrogen
4580
5330
4020
1940
Nitrate and Nitrite
14.8
7.15
21.9
444
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed assure that qualified pers nnel properly gathered and evaluated the information submitted. I am aware that there are
significa pe Ities for submitting fa information, including the possibility of fines and imprisonment for knowing violations."
75
X Date 2_ty_( .
(SIGNATURE OF PREPARER)
DENR FORM RSSF (5/2003)
Printed: Tuesday - February 10 2015 at 13.55:28 for: 2084 02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247 Laboratory
Facility Name: STATESVILLE, NC A&L Eastern Laboratories Inc.
NPDES# : NCO020591
or WQ# (residual only)
WWTP Name: THIRD CREEK
Residuals Analysis Data
Product Type
cAK
cAK
cAK
cAK
Date Sampled (grab) or 01/09/14
05/11/14
09/26/14
01/29/15
Date Composited
Percent Solids
14.19
15.3E
16.43
15.49
PARAMETERS (mg/kg dry weight)
Aluminum
15800
15800
19900
16800
Calcium
10600
10700
12200
16300
Magnesium
2460
3300
2150
2180
pH
5.96
8.09
6.07
5.10
Potassium
2940
3770
2050
2180
Sodium
1140
1450
1440
568
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to ss a that qualified per onnel properly gathered and evaluated the information submitted. I am aware that there are
significa-en-s for su mitting f Ise information, including the possibility of fines and imprisonment for knowing violations."
XDate O� �J1C DDCDADCD\
NR - Data Not Reported or Data Not Required
I
DENR FORM RSSF-B (712002) Printed: Tuesday - FebruarV 10 2015 at 13:55:57 for: 2084 02

Page: 1 of 2
Report Number: 14-010-0200
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97419
Sample Id : 3RD CK
A&L Eastern Laboratories, Inc.
@P. 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleasterii.com
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/9/2014 09:15:00
Date Received: 01/10/2014 00:00
Date Reported: 01/15/2014
Total Solids "
14.19
141900
10b.0
JM
01/10/2014 14:19
SM-2540G
Moisture*
85.81
100.0
JM
;01/10/201414:19
SM-2540G
Total Kjeldahl Nitrogen
4.93
49300
10.0
JM
01/13/2014 08:30
SM-4500-NH3C-TKN
Total Phosphorus
1.93
19300
100
KM
01/13/2014 11:35
SW 6010C
Total Potassium
0.29
2940
100
KM
01/13/2014 11:35
SW 6010C
Total Sulfur
0.91
9070
100
KM
01/13/2014 11:35
SW 6010C
Total Calcium
1.06
10600
100
KM
01/13/2014 11:35
SW 6010C
Total Magnesium
0.25
2460
100
KM
01/13/2014 11:35
SW 6010C
Total Sodium
0.11
1140
100
KM
01/13/2014 11:35
SW 6010C
Total Iron
24000
100
KM
01/13/2014 11:35
SW 6010C
Total Aluminum
15800
100
KM
01/13/2014 11:35
SW 6010C
Total Manganese
531
5
KM
01/13/2014 11:35
SW 6010C
Total Copper
438
5
KM
01/13/2014 11:35
SW 6010C
Total Zinc
1090
5
KM
01/13/2014 11:35
SW 6010C
Ammonia Nitrogen
0.46
4580
10.0
JM
01/13/2014 08:30
SM-4500-NI3C
Organic N
4.47
44720
10.0
01/13/2014 08:30
CALCULATION
Nitrate+Nitrite-N
14.8
2.00
JM
01/13/2014 08:30
SM-450ONO3F
Total Cadmium
12.0
2.0
KM
01/13/2014 11:35
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-010-0200
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97419
Sample Id : 3RD CK
99, A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 7434401 Fax [phone]
www.aleastern.com
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/9/2014 09:15:00
Date Received: 01/10/2014 00:00
Date Reported: 01/15/2014
Total Chromium
88
5
KM
01/13/2014 11:35
SW 6010C
Total Nickel
55.
5
KM
01/13/2014 11:35
SW 6010C
Total Lead
99
5
KM
01/13/2014 11:35
SW 6010C
Total Arsenic
5.0
3.0
KM
01/13/2014 11:35
SW 6010C
Total Mercury
0.4
0.4
KM
01/13/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
01/13/2014 11:35
SW 6010C
pH (Standard Units) *
5.96
2.00
JM
01/13/2014 08:30
SW-9045D
Total Molybdenum
23
5
KM
01/13/2014 11:35
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N" AND "Se". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As" AND "S".
ALL OTHER QC
DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made%�-
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

SAMPLINGLOG '4' ik& °��
OFCUSTODY7 IIIIIIIIIIIII 14­01P-6200 RDA NALI46M93 _ RECORD
LLC'STATESVILLE. 14.
CUSTOMER: SYNAGRO SOUTHEAST 804 :S-rA7SV,)LLE 3R . D CK
[..s2mpjfi7g procedures,
PRGJECT MANAGER, -ction of these samples.
Phone: _7(
SAME 4-R
A;&:L CUSTWER
SAMPLING
SAMPLE
#--OF' SAPAPLINd
ME-11HOD
9ETHOD
_LAB* SAMPLE`I.1j.*._
DaCATION.
TYPE
CONTAINERS DATE' TIME!
PRESERVED
SHIPPtO.
Rel[rijuished7bg S
Date. Time,
'.Recieved by:
REMARKS:
- ampler'.
-4.2
Relinquished by-
Dirt, rima
Recieved
PS
Refin'quished,by!
Dqie- I '.'Time!
Recieved*.,
SPECIAL INSTRUCTIONS:
For i
monitoring purposes::
PO#,
SAMPLE
ANALYSIS -REQUEST
SLI
`�SL2
NH4_N
NO,,-N
'Orga 111C
N
'Cd
-,
Cr
Hi
[' Pb
AS
Hg
so.
III
e-quiv.
Solids
mc,
C1
N.O,-N'
C
9.9r
too,
100
P10
too
SL-1: Total Solids (Moisture):,.Tow.1 Rjenldahl-(4itrqgen, Phosphorus, and Potassium
SL121: Basic Test,S1_1 plus Sulfur,"Calcium, Maories-I'LIM, Sodium, Iron, Aluminum, Manganese, Copper arid -Zinc-.
Wbite;"A & L Canary­MANAGER'COPY

�• /'1 � � t . r'M-� fl� � 1 � r� +. � x• • ri a l I.!' n - r'� t�~ �-, r t - i � ,--� r�
�1 1. / 1 t o•„f .,i i ., t/ . d `�i. `i •� �..3 ��f . V i t� F"l �F" 1 e .� �1 • �i ;
E
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 1/9/2014 111/2014-3/31/2014 0.9740
Na mg/I = (Na mg/kg x % Solids) _ 100 = (1140 x 14.1900) _ 100 = 161.766
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (10600 x 14.1900) + 100 = 1504.14
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2460 x 14.1900) + 100 = 349.074
Na meq = Na mg/I + Molec.Wgt.Na = 161.766 _ 23 = 7.0333
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1504.14 + 20 = 75.207
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 349.074 _ 12 = 29.0895
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.0333 + SgrRoot[0.5(75.207+29.0895)] = 0.973956
Printed: 1 /27/2015
Page 1 11:12

Page: 1 of 2
Report Number: 14-133-0205
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55319
Sample Id: STATESVILLE 3RD CK
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleasterii.com
Project: STATESVILLE 3RD CK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 5/11/2014 11:10:00
Date Received: 05/13/2014 00:00
Date Reported: 05/16/2014
Total Solids *
15.38
153800
100.0
JM
05/13/2014 13:59
SM-2540G
Moisture *
84.62
100.0
JM
05/13/2014 13:59
SM-2540G
Total Kjeldahl Nitrogen
5.34
53400
10.0
JM
05/14/2014 08:24
SM-4500-NH3C-TKN
Total Phosphorus
1.81
18100
100
KM
05/14/2014 12:42
SW 6010C
Total Potassium
0.38
3770
100
KM
05/14/2014 12:42
SW 6010C
Total Sulfur
0.80
7950
100
KM
05/14/2014 12:42
SW 6010C
Total Calcium
1.07
10700
100
KM
05/14/2014 12:42
SW 6010C
Total Magnesium
0.33
3300
100
KM
05/14/2014 12:42
SW 6010C
Total Sodium
0.15
1450
100
KM
05/14/2014 12:42
SW 6010C
Total Iron
20400
100
KM
05/14/2014 12:42
SW 6010C
Total Aluminum
15800
100
KM
05/14/2014 12:42
SW 6010C
Total Manganese
592
5
KM
05/14/2014 12:42
SW 6010C
Total Copper
369
5
KM
05/14/2014 12:42
SW 6010C
Total Zinc
1230
5
KM
05/14/2014 12:42
SW 6010C
Ammonia Nitrogen
0.53
5330
10.0
JM
05/14/2014 08:24
SM-4500-NH3C
Organic N
4.81
48070
10.0
05/14/2014 08:24
CALCULATION
Nitrate+Nitrite-N
7.15
2.00
JM
05/14/2014 08:25
SM-450ONO3F
Total Cadmium
11.0
2.0
KM
05/14/2014 12:42
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made�—
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-133-0205
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55319
Sample Id : STATESVILLE 3RD CK
g"t A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: STATESVILLE 3RD CK/NC CERT#257
REPORT OFANALYSIS Date Sampled: 5/11/2014 11:10:00
Date Received: 05/13/2014 00:00
Date Reported: 05/16/2014
Total Chromium
85
5
KM
05/14/2014 12:42
SW 6010C
Total Nickel
54
5
KM
05/14/2014 12:42
SW 6010C
Total Lead
82
5
KM
05/14/2014 12:42
SW 6010C
Total Arsenic
3.0
3.0
KM
05/14/2014 12:42
SW 6010C
Total Mercury
<0.4
0.4
KM
05/14/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
05/14/2014 12:42
SW 6010C
pH (Standard Units) * 8.09
2.00
JM
05/14/2014 08:30
SW-9045D
Total Molybdenum
16
5
KM
05/14/2014 12:42
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr", "Fe",
"Ni", AND "Se".
ALL OTHER
QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made9,&U. ` 69
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 6/11/2014 411/2014-6/30/2014 1.2285
Na mg/I = (Na mg/kg x % Solids) + 100 = (1450 x 15.3800) + 100 = 223.01
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (10700 x 15.3800) _ 100 = 1645.66
Mg mg/I = (mg mg/kg x % Solids) + 100 = (3300 x 15.3800) + 100 = 507.54
Na meq = Na mg/I + Molec.Wgt.Na = 223.01 + 23 = 9.69609
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1645.66 + 20 = 82.283
Mg meq = Mg mg/I + Molec.Wgt.Mg = 507.54 + 12 = 42.295
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 9.69609 + SgrRoot[0.5(82.283+42.295)] = 1.22854
Printed: 1 /27/2015
Page 1 11:13

Page: 1 of 2
Report Number: 14-273-0210
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 57856
Sample Id: STATESVILLE 3RD CK
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (8041743-9401 Fax [phone]
www.aleasterii.com
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 9/26/2014 13:35:00
Date Received: 09/30/2014 00:00
Date Reported: 10/06/2014
Total Solids '
16.43
164300
100.0
BW
09/30/2014 14:15
SM-2540G
Moisture *
83.57
100.0
BW
09/30/2014 14:15
SM-2540G
Total Kjeldahl Nitrogen
3.97
39700
10.0
JM
10/01/2014 08:44
SM-4500-NH3C-TKN
Total Phosphorus
2.04
20400
100
KM
10/01/2014 12:04
SW 6010C
Total Potassium
0.21
2050
100
KM
10/01/2014 12:04
SW 6010C
Total Sulfur
0.89
8920
100
KM
10/01/2014 12:04
SW 6010C
Total Calcium
1.22
12200
100
KM
10/01/2014 12:04
SW 6010C
Total Magnesium
0.22
2150
100
KM
10/01/2014 12:04
SW 6010C
Total Sodium
0.14
1440
100
KM
10/01/2014 12:04
SW 6010C
Total Iron
29000
100
KM
10/01/2014 12:04
SW 6010C
Total Aluminum
19900
100
KM
10/01/2014 12:04
SW 6010C
Total Manganese
420
5
KM
10/01/2014 12:04
SW 6010C
Total Copper
453
5
KM
10/01/2014 12:04
SW 6010C
Total Zinc
965
5
KM
10/01/2014 12:04
SW 6010C
Ammonia Nitrogen
0.40
4020
10.0
JM
10/01/2014 08:44
SM-4500-NH3C
Organic N
3.57
35680
10.0
10/01/2014 08:44
CALCULATION
Nitrate+Nitrite-N
21.9
2.00
JM
10/01/2014 08:45
SM-450ONO3F
Total Cadmium
15.0
2.0
KM
10/01/2014 12:04
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made�—
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-273-0210
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 57856
Sample Id: STATESVILLE 3RD CK
@P. A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project; STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 9/26/2014 13:35:00
Date Received: 09/30/2014 00:00
Date Reported: 10/06/2014
Total Chromium
101
5
KM
10/01/2014 12:04
SW 6010C
Total Nickel
47
5
KM
10/01/2014 12:04
SW 6010C
Total Lead
127
5
KM
10/01/2014 12:04
SW 6010C
Total Arsenic
3.0
3.0
KM
10/01/2014 12:04
SW 6010C
Total Mercury
<0.4
0.4
KM
09/30/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/01/2014 12:04
SW 6010C
pH (Standard Units) *
6.07
2.00
JM
10/01/2014 08:50
SW-9045D
Total Molybdenum
19
5
KM
10/01/2014 12:04
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE AND MSD WERE OUT OF LIMITS FOR "Mg". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in. any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorpti®n Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE . 9/26/2014 911/2014-1013112014 1.2776
Na mg/I = (Na mg/kg x % Solids) + 100 = (1440 x 16.4300) =100 = 236.592
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (12200 x 16.4300) + 100 = 2004.46
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2150 x 16.4300) + 100 = 353.245
Na meq = Na mg/I = Molec.Wgt.Na = 236.592 _ 23 = 10.2866
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2004.46 + 20 = 100.223
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 353.245 _ 12 = 29.4371
SAR = Na meq _ SgrRoot[0.5 x (Ca`meq + Mg meq)] = 10.2866 _ SgrRoot[0.5(100.223+29.4371)] = 1.27757
Page 1 Printed: 1/27/2015
11:13

Page: 1 of 2
Report Number: 15-030-0200
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59938
Sample Id: 3RD CK
@P.
A&LEastern Laboratories, Ifac.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.alerstem.com
Project: 3RD CHECK/NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 1/29/2015 09:30:00
Date Received: 01/30/2015 00:00
Date Reported: 02/05/2015
Total Solids °
15.49
154900
100.0
RD
01/30/2015 14:19
SM-2540G
Moisture "
84.51
100.0
RD
01/30/201514:19
SM-2540G
Total Kjeldahl Nitrogen
3.41
34100
10.0
JM
02/02/2015 08:24
SM-4500-NH3C-TKN
Total Phosphorus
1.73
17300
100
KM
02/02/2015 13:08
SW 6010C
Total Potassium
0.22
2180
100
KM
02/02/2015 13:08
SW 6010C
Total Sulfur
0.76
7630
100
KM
02/02/2015 13:08
SW 6010C
Total Calcium
1.63
16300
100
KM
02/02/2015 13:08
SW 6010C
Total Magnesium
0.22
2180
100
KM
02/02/2015 13:08
SW 6010C
Total Sodium
0.06
568
100
KM
02/02/2015 13:08
SW 6010C
Total Iron
22700
100
KM
02/02/2015 13:08
SW 6010C
Total Aluminum
16800
100
KM
02/02/2015 13:08
SW 6010C
Total Manganese
509
5
KM
02/02/2015 13:08
SW 6010C
Total Copper
417
5
KM
02/02/2015 13:08
SW 6010C
Total Zinc
1150
5
KM
02/02/2015 13:08
SW 6010C
Ammonia Nitrogen
0.19
1940
10.0
JM
02/02/2015 08:24
SM-4500-NH3C
Organic N
3.22 ,
32160
10.0
02/0212015 08:24
CALCULATION
Nitrate+Nitrite-N
444
2.00
im
02/02/2015 08:25
SM-450ONO3F
Total Cadmium
17.0
2.0
KM
02/02/2015 13:08
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
and letters are for the exclusive and confidential use orourclients, and ma not be reproduced in
Ourreporls, Y
whole or art, nor may an reference be made
P Y Y
8�-
to the wodc, the results, or the company in any advertising, news release, orother public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-030-0200
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59938
Sample Id: 3RD CK
99 A&L Eastern Laboratories, Inc.
7621 Whitopine Road Richmond, Virginia 23237 (804) T43.9401 Fax [phone]
www.aleasteni.com
Project: 3RD CHECK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/29/2015 09:30:00
Date Received: 01/30/2015 00:00
Data Reported: 02/05/2015
Total Chromium
109
5
KM
02/02/201513:08
SW 6010C
Total Nickel
52
5
KM
02/02/2015 13:08
SW 6010C
Total Lead
107
5
KM
02/02/2015 13:08
SW 6010C
Total Arsenic
4.0
3.0
KM
02/02/2015 13:08
SW 6010C
Total Mercury
0.6
0.4
KM
02/03/201613:35
SW-7471 B
Total Selenium
<5.0
5.0
KM
02/02/2015 13:08
SW 6010C
pl-I (Standard Units) *
5.10
2.00
JM
02/02/2015 08:24
SW-9045D
Total Molybdenum
20
5
KM
02/02/2015 13:08
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT
FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "AI" AND "Se". ALL OTHER QC DATA
IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the wort; the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. .
Debbie Holt

/'1 � c P � t \ C. C \ 1'i l 4l � '..' P • !� ' � i '� '' l � A r�l E
��r ��a L a .7 i-i e�. / :� 4 � ��J 4 ice. C: d , � 1 ;� 4 : � i. • �• 1 � 1�1 � �,
Product Code Product Name Sample Date ReportRange Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 1/29/2015 11 - 1 1 0.4354
Na mg/I = (Na mg/kg x % Solids) -=100 = (568 x 15.4900) = 100 = 87.9832
Ca mg/I = (Ca mg/kg x % Solids) =100 = (16300 x 15.4900) =100 = 2524.87
Mg mg/I = (mg mglkg x % Solids) =100 = (2180 x 15.4900) _ 100 = 337.682
Na meq = Na mg/I _ Molec.Wgt.Na = 87.9832 _ 23 = 3.82536
Ca meq = Ca mg/I = Molec.Wgt.Ca = 2524.87 _ 20 = 126,244
Mg meq = Mg mg/I z- Molec.Wgt.Mg = 337.682 =12 = 28.1402
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.82536 - SgrRoot[0.5(126.244+28.1402)] = 0.435398
it
Printed: 2/10/2015
Page 1
14:08

SAMPLING LOG.1#
A & L.EASTEI
7621 Whit'ep'in
ousioMER: .`�'NAGRO ;Richmond', VA
IL
804r43-9401,
PROJECT MANAGER:
Phone: y�(G.). 77 f
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1IIIIII11111111111�ILI�II111111�11111111�111111�1111111'IAII �Q,S I��a
MAGR4 CENTRAL LWISTATESUILLE
•$RD CHECK/NC CERT#25.7 12-56:26
►eedures
vverQ,7usea aurrrag the conearron or mess samples. i
CUSTOMER.
LAB -it SAMPLE ].D.
SAMPUN'Cu
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TYPE
CONTAINERS. DdATE'. TIME'
Relinquished by:
SPECIAL ;I N STRU C.TI Q:I+JS:
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V3 Far- �srnr� aFAT monitoring purposes,
O5eS.
SAMPLE
B.D'.
Y�� 6A
Time Recieved by:.
va_te. Time Recieved by;
Date' Tiche Recleved by:
)METHOD
PRESERVED
L ° eS)
REMARKS:
P.ol;.:
ANALYSl;a REQUEST
SL1 SI.2 6VI t-N NO3-IV �r iic Cd Cr ful Pb. As jig 1. Se pig.
SL't: Tota('Salids:(Maist.ure),•Tgtai Kjeldahl:Nitrncdon, Phosphorus., and Potassium
SL2: I3asia'Tost SL1 Pius Sulfur,:,Galciurn,'Magnesium, Sodium, :Iron, Aluminum,. Man
ganese,.Copper and Zinc
Mo. I G9
METHOD
SNIPPED
4
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mmm
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ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: RHODISS
OWNER: TIMOTHY PAYNE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 13.84
SITE #: NC AL 00014 FIELD# : AL 00014 0001 A OPERATOR: TIMOTHY PAYNE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 19.20 ACRES PERMITTED: 19.20
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
0/0Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/9/14
100.00 (CY)
5.208
16.43
0.721
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
39,700. p
4,020.00 p
21.90 p
1 12716
WHEAT
Oct-14
100.00 (CY)
5.208
1
I offal �_uuic I usir�c: �,LL
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.004
0.022
0.146
0.653
0.183
<.001
0.027
0.068
0.007
1391
29.41
18
Cumulative lbs/acre
0.004
0.022
1 0.146
1 0.653
1 0.183
<.001
0A27
1 0.068
0.007 -
1391
Permit PAN Limit (lbs/acre) 1stCrop/2nd Crop
--
85
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
t 375.0
89.0
2500.0
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X
(SIGNAT ' OF L ' APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: STATESVILLE, NC
OWNER: TIMOTHY PAYNE
SITE #: NC AL 00014 FIELD# : AL 00014 0001 B
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 82.41
OPERATOR: TIMOTHY PAYNE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 22.70 ACRES PERMITTED: 22.70
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Total
Per Acre
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
m
(pp )
Cro p
MONTH
10/8/14
325.00 (CY)
14.317
14.94
1.802
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
50,500. p
7,760.00 p
2.00 p
16 004
WHEAT
Oct-14
325.00 (CY)
14.317
10/8/14
50.00 (CY)
2.203
16.43
0.305
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
39,700. p
4,020.00 p
21.90 p
12736
I WHEAT
10/9/14
250.00 (CY)
11.013
16.43
1.524
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
39,700. p
4,020.00 p
21.90 p
12736
WHEAT
Oct-14
300.00 (CY)
13.216
7^+„ l r'„LGn VAIA,.•
avw. vuvav a..wa ay. L/.JJ
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Amnuallbs/acre
107
0.025
0.069
0.521
2.990
0.573
0.003
0.109
0.251
0.036
5.180
181.26
Cumulative Ibs/acre
0.025
0.069
0.521
2.990
0.573
0.003
0.109
0.251
0.036
5.180
Permit PAN Limit (lbs/acre) 1st Crop/2ud Crop
i
120
._
a
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 t i 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X - v�-r x t S
(SIGNATURE OF APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for lniowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/hncorporation 1.0
r Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: STATESVILLE, NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0004 A
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 142.19
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 44.20 ACRES PERMITTED: 44.20
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zatiott
zatiott
TKN
Nitrogen
and
(pptm)
Crop
1/27/14
224.00 (CY)
5.068
14.19
0.606
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
49,300.p
4,580.00 p
14.80 p1
15721
I FESCUE
1/28/14
416.00 (CY)
9.412
14.19
1.125
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
49,300. p
4,580.00 p
14.80 p
15721
FESCUE
Jan-14
1 640.00 (CY)
14.480
2/27/14
416.00 (CY)
9.412
14.19
1.125
STTCC
MOIST
0-<1/2"
SUR
0.5
0.30
49,300. p
4,580.00 p
14.80 p
15721
FESCUE
Feb-14
416.00 (CY)
9.412
3/1/14
128.00 (CY)
2.896
14.83
0.362
STFCC
MOIST
0-<I/2"
SUR
0.5
0.30
54,600. p
9,510.00 p
12.10 p
18294
FESCUE
Mar-14
128.00 (CY)
2.896
Total Cubic Yds/Ac• 2G 79
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
103
0.032
0.072
0.537
2.765
0.591
0.003
.0.441
0.339
0.032
6.738
128-.88
Cumulative lbs/acre
0.131 1
0.197
1.649
10.616
1.704
0.039
0.393
1.070
0.109
21.923
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
STTCC = STATESVILLE, NC THIRD CREEI{ CAKE
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X all 3 1)
(SIGNATURE 0 AND AP ' R) DATE
"I certify, under enalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for lutowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
r Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: ,. STATESVILLE, NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0007
RESIDUAL SOURCE(S):*;See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HELENA
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 35.28
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 13.90 ACRES PERMITTED: 13.90
Page
Lune Applied ***
Date
LWAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
2/28/14
160.00 (CY)
11.511
14.83
1.438
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
54,600. p
9,510.00 p
12.10 p
18294
FESCUE
Feb-14
160.00 (CY)
11.511
2/27/14
128.00 (CY)
9.2091
14.19
1.101
STTCC
MOIST
0-<1/2"
SUR
0.5
0.30
49,300. p
4,580.00 p
14.80 p
11721
FESCUE
Feb-14
128.00 (CY)
9.209
I
1
T„a..1 n.. L:,. 11A_1A
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
87
0.025
0.041
0.332
2.011
0.321
0.005
0.091
0.219
0.025
4.438
116.67
Cumulative Ibs/acre
0.113
0.124
1.143
8.154
1.012
0.044
0.299
0.759
0.125
15.288
(
1
1
1
r* I
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
'�
3
!s
188
{
FD Cu nulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
i i
15.0 Y
375.0
89.0
2500.0
P
a
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X I ®2- t3 1 �
(SIGNATURE LAND PLIER) DATE
"I certify, and penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, . Injection/Incorporation 1.0
e Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: STATESVILLE, NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0008
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: APPLING
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 27.98
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.20 ACRES PERMITTED: 11.20
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
DATE or
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
2/28/14
224.00 (CY)
20.000
14.83
2.498
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
54,600. p
9,510.00 p
p
18294
FESCUE
Feb-14
1 224.00 (CY)
20.000
F2.10
Total Cubic Yds/Ac• . 2000
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
91
0.025
0.025
0.240
1.819
0.180
0.006
0.070
0.170
0.025
3.542
128.90
Cumulative lbs/acre
0.113
0.161
1.353
9.838
1.333
0.042
0.331
0.871
0.159
17.787
r�
a
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
r h
g
i
` &
,
- }
6 µ
216
;;
r
1
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
P
1339.0
267.9
15.0
?
375.0
89.0
2500.0
>,
d
e.
6
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
x i
(SIGNATURE 0 AND XPI IER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for !mowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0
Application Method: SUR - Surface, INJ - h»jection, SURIN- Incorporation *** See Site pH & Lune Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: STATESVILLE, NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0009
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 43.79
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 12.20 ACRES PERMITTED: 12.20
Page
Lune Applied ***
Date
LWAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
2/28/14
320.00 (CY)
26.230
14.83
3.276
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
54,600. p
9,510.00 p
12.10 p
18294
FESCUE
Feb-14
320.00 (CY)
26.230
311114
1 32.00 (CY)
2.6231
14.19
0.313
STTCC
MOIST
1 0-<1/2"
SUR
0.5
0.30
49,300. p
4,580.00 p
14.80 p
15721
FESCUE
Mar-14
32.00 (CY)
2.623
1
Total Cubic Yds/Ac• 28 85
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Amnuallbs/acre
130
0.036
0.040
0.370
2.660
0.298
0.009
0.106
0.257
0.036
5.329
181.15
Cumulative lbs/acre
0.121
0.194
1.613
10.909
1.635
0.046
0.390
0.999
0.164
20.661
`
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
e6
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0�
375.0
89.0
2500.0
(
r
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X r��✓ f i
(SIGNATURE OFj AND LIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Ic nowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: STATESVILLE, NC
OWNER: LORANE PAGE
SITE #: NC IR 00023 FIELD# : IR 00023 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 66.37
OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 17.20 ACRES PERMITTED: 17.20
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner-
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
(ppni)
Crop
Total
Per Acre
3/1/14
256.00 (CY)
14.884
14.83
1.859
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
54,600. p
9,510.00 p
12.10 p
18294
FESCUE
Mar-14
1 256.00 (CY)
14.884
3/1/14
128.00 (CY)
7.442
14.19
0.889
STTCC
MOIST
0-<I/2"
SUR
0.5
0.30
49,300. p
4,580.00 p
14.80 p
15721
FESCUE
Mar-14
128.00 (CY)
7.442
6/23/14
160.00 (CY)
9.3021
14.17
1.110
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,600.p
15,100.00 p
2.00 p
20902
FESCUE
Jun-14
160.00 (CY)
9.302
Total Cubic Yds/Ac• 31 63
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
142
0.039
0.051
0.459
2.816
0.381
0.007
0.120
0.326
0.039
6.138
181.99
Cumulative lbs/acre
0.144
0.240
2.079
14.219
2.374
0.053
0.507
1.180
0.158
25.500
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEI{ CAKE
STTCC = STATESVILLE, NC THIRD CREEI{ CAKE
x 3
(SIGNATURE OF L APP R) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR -Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, Lijection/Incorporation 1.0
r Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 103.63
SITE #: NC IR 00023 FIELD# : IR 00023 0002 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 32.40 ACRES PERMITTED: 32.40
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppnm)
Crop
MONTH
Total
Per Acre
Solids
6/17/14
448.00 (CY)
13.827
15.38
1.791
STTCC
DRY
0-<I/2"
SUR
0.5
0.30
53,400. p
5,330.00 p
7.15 p
17093
FESCUE
6/18/14
352.00 (CY)
10.864
15.38
1.407
STTCC
DRY
0-<1/2"
SUR
.0.5
0.30
53,400. p
5,330.00 p
7.15 p
17093
FESCUE
.dun-14
1 800.00 (CY)
24.691
a-1- _.0 ♦ ­. LY.VJ
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Aimimuallbs/acre
109
0.019
0.070
0.544
2.360
0.525
0.003
0.102
0.345
0.032
7.868
115.78
Cumulative lbs/acre
0.130
0.295
2.373
14.420
2.811
0.046
0.540
1.298
0.156
29.304
J,
'
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X
(SIGNATURE O AND PLIER) DATE
"I certify, under,13enalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg Volatilization Rate: Surface 0.5, Injection/hmcorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: STATESVILLE, NC
OWNER: LORANE PAGE
SITE #: NC IR 00023 FIELD# : IR 00023 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 42.01
OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 23.00 ACRES PERMITTED: 23.00
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WI) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
D ,
D Wet
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TICN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
6/23/14
160.00 (CY)
6.957
14.17
0.830
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,600.p
15,100.00 p
2.00 p
20902
I FESCUE
6/24/14
192.00 (CY)
8.348
14.17
0.996
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,600.p
15,100.00 p
2.00 p
21912
FESCUE
Jun-14
352.00 (CY)
15.305
1
Total Cubic Vdc/An• tc 2n
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
76
0.018
0.018
0.205
1.125
0.117
0.002
0.044
0.168
0.018
2.572
85.11
Cumulative lbs/acre
0.066
0.063
0.844
5.759
0.485
0.032
0.205
0.528
0.087
10.893
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
IIR
t
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
(
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEI{ CAKE
4 X '�L > S
(SIGNATU F LAN APPLIER) DATE
"I certify, under penalty of law, that this document -was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %=percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 34.37
SITE #: NC IR 00023 FIELD# : IR 00023 0004 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 1-3.70 ACRES PERMITTED: 13.70
Page: 1
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY).
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
or
DATE%
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppin)
Crop
Total
Per Acre
6/20/14
288.00 (CY)
21.022
14.17
2.509
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,600.p
15,100.00 p
2.00 p
20902
FESCUE
Jun-14
288.00 (CY)
21.022
T..t..1 !'..I.:.. V.I../A-
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
105
0.025
0.025
0.281
1.545
0.161
0.003
0.060
0.231
0.025
3.532
116.91
Cumulative lbs/acre
0.093
0.109
1.183
8.295
0.889
0.037
0.314
0.775
0.125
16.670
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
C
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEIC CAICE
X 13, LA li
(SIGNATURJ F LAPI, R) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface Q..S Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITYNAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 47.13
SITE #: NC IR 00023 FIELD# : IR 00023 0005 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.10 ACRES PERMITTED: 16.10
Page
Lime Apphed ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
or Wet Tons (WT) (specify)
o�o
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pprn)
Crop
Total
Per Acre
6/19/14
256.00 (CY)
15.901
14.17
1.898
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,600. p
15,100.00 p
2.00 p
20902
FESCUE
Jun-14
256.00 (CY)
15.901
6/19/14 1
128.00 (CY)
7.9501
15.38
1.030
STTCC
DRY
0-<I/2"
SUR
0.5
0.30
53,400.p
5,330.00 p
7.15 p
17093
FESCUE
Jmr-14
128.00 (CY)
7.950
I
1
1
1
1
1 1
1
1
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annua I lbs/acre
115
0.025
0.042
0.388
1.929
0.290
0.003
0.079
0.286
0.029
5.205
125.71
Cumulative lbs/acre
0.108
0.154
1.583
10.020
1.419
0.046
0.392
0.960
0.130
20.403
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
;
1339.0
267.9
15.0 ' 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEI{ CAKE
X)f OLr� li
(SIGNATURE ZAND PLIER) DATE
"I certify, under penal of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/Icg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

Sunmtit Environmental Technologies, Inc.
" t'P Y "+�` f 1 2bt4 # 1 -7 3310 WinSt.
0N rl-rr31.11,1ENT,1LT CH `,,0tJ3C,=53; Pci?; Cuyahoga Falls, Ohio 44223
r ra iicaP 1 3rttnlfa TEL: [phone] FAX.- [phone]
Website: http://www.setiekcont
January 21, 2014
Edward Stephens
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Statesville
Dear Edward Stephens:
Order No.: 14010514
Summit Environmental Technologies, Inc. received 2 sample(s) on 1/10/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, WashingtonC891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 8

Summit Environmental Technologies, hic. W ' T
)i�L�
R
�1, La
8 WV 0�ll•��11•
�r1� 3310WinSt.
t d,rls3t7td1,1EM iAL 1`� C�rSLdGta , Inc;, Cuyahoga Falls, Ohio 44223 Sal mple Summary1._ q__ _ rlrsi; tfi�F1 I:atiar.�P it}e ; TEL: [phone] FAX. • [phone] WO#: 14010514
Website: h1tP.1Avmv.settelccom 21_Jan-14
CLIENT: Synagro
Project: Statesville
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
14010514-001 Statesville 3rd CK 1/9/2014 9:15:00 AM 1/10/2014 9:52:00 AM Sludge
14010514-002 Statesville 4th CK 1/9/2014 9:20:00 AM 1/10/2014 9:52:00 AM Sludge
Page 2 of 8

h ri
( �-
Su it Enrironn:ervtal Technologies, Inc.
g
3310 Win Sr.
WO#:
14010514
aL
f--NVIRONJlEN0tLt`2CSt,QLrGi s,➢Pdc'
Cuyahoga Falls, Ohio44223 Date Reported:
1/21/2014
Arraflre°ca11 L.u,elara?oI-feS
TEL: [phone] FAX.• [phone]
Company:
Synagro
Website: httD:/hviviv.settek cons
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/10/2014
Project#:
Statesville
TCLP Metals Analysis (6010)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd CK
001
1/9/2014
TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/15/2014
WK
Statesville 3rd CK
001
1/9/2014
TCLP Barium(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
1/15/2014
WK
Statesville 3rd CK
001
1/9/2014
TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/15/2014
WK
Statesville 3rd CK
001
1/9/2014
TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/15/2014
WK
Statesville 3rd CK
001
1/9/2014
TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
, 1
5.0
1/15/2014
WK
Statesville 3rd CK
001
1/9/2014
TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/15/2014
WK
Statesville 3rd CK
001
1/9/2014
TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/15/2014
WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Statesville 3rd CK 001 1/9/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 1/15/2014 ALJ
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd CK
001
1/9/2014
Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
1/15/2014
JBN
Statesville 3rd CK
001
1/9/2014
Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1.
0.50
1/15/2014
JBN
Statesville 3rd CK
001
1/9/2014
Enddn
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
1/15/2014
JBN
Statesville 3rd CK
001
1/9/2014
gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
1/15/2014
JBN
Statesville 3rd CK
001
1/9/2014
Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/15/2014
JBN
Statesville 3rd CK
001
1/9/2014
Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/15/2014
JBN
Statesville 3rd CK
001
1/9/2014
Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
1/15/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd CK
001
1/9/2014
1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/15/2014
MES
Statesville 3rd CK
001
1/9/2014
1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
Statesville 3rd CK.
001
1/9/2014
Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
Statesville 3rd CK
001
1/9/2014
Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
Statesville 3rd CK
001
1/9/2014
Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
1/15/2014
MES
Statesville 3rd CK
001
1/9/2014
Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
1/15/2014
MES
Statesville 3rd CK
001
1/9/2014
Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/15/2014
MES
Statesville 3rd CK
001
1/9/2014
Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
Statesville 3rd CK
001
1/9/2014
Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
1/15/2014
MES
Statesville 3rd CK
001
1/9/2014
MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
1/15/2014
MES
Page 3 of 8

j
t
# -, .1 Lk Summit Environmental Technologies, b:c.
i i ,` �' 3310 Win
WO#:
14010514
!.� 1 7 t! L l
l 1
St.
5
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r•t4'd19rSk�lllEhll,'tL
T C
Gz�"s�i'�'r�L�3GtE S, 9;dc`,
Cuyahoga Falls, Ohio 44223
Date Reported:
p
1/21/2014
Imo,
rt'ra:yti s,° t.yi oxatot;e
TEL: [phone] FAX.- [phone]
Company:
Synagro
Website: htto://wwiv.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/10/2014
Project#:
Statesville
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd CK
001
1/9/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Sludge.
EPA 8270 C
1
0.13
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
Cresols, Total
5.0
ND mg/L
Sludge .
EPA 8270 C
1
200
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
1/15/2014
AKE
butadiene
Statesville 3rd CK
001
1/9/2014
Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
Nitrobenzene
- 0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
1/15/2014
AKE
Statesville 3rd CK
001
1/9/2014
Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
1/15/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd CK
001 1/9/2014 2,4-D
5.0 ND mg/L
Sludge
EPA 8321 A
1
10
1/15/2014
AMZ
Statesville 3rd CK
001 1/9/2014 2,4,5-TP
0.50 ND mg/L
Sludge
EPA 8321 A
1
1.0
1/15/2014
AMZ
TCLP Metals Analysis (6010)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th CK
002
1/9/2014 TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/15/2014
WK
Statesville 4th CK
002
1/9/2014 TCLP Barium(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
1/15/2014
WK
Statesville 4th CK
002
1/9/2014 TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/15/2014
WK
Statesville 4th CK
002
1/9/2014 TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/15/2014
WK
Statesville 4th CK
002
1/9/2014 TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/15/2014
WK
Statesville 4th CK
002
1/9/2014 TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/15/2014
WK
Statesville 4th CK
002
1/9/2014 TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/15/2014
WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Statesville 4th CK 002 1/9/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 1/15/2014 ALJ
Wage 4 of 8

Summit Environmental Technologies, Inc.
3310 Win St.
Mwc; Cuyahoga Falls, Ohio44223
Ara:,uN` .sa i=.TEL: [phone] FAX.- [phone]
Website: http://ivivw.settekcom
WO#: 14010514
Date Reported: 1/21/2014
Company: Synagro
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 1/10/2014
Project#: Statesville
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th CK
002
1/9/2014
Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
1/15/2014
JBN
Statesville 4th CK
002
1/9/2014
Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
1/15/2014
JBN
Statesville 4th CK
002
1/9/2014
Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
1/15/2014
JBN
Statesville 4th CK
002
1/9/2014
gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
1/15/2014
JBN
Statesville 4th,CK
002
1/9/2014
Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/15/2014
JBN
Statesville 4th CK
002
1/9/2014
Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/15/2014
JBN
Statesville 4th CK
002
1/9/2014
Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
1/1'5/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th CK
002
1/9/2014
1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/15/2014
MES
-tatesville 4th CK
002
1/9/2014
1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
tatesville 4th CK
002
1/9/2014
Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
Statesville 4th CK
002
1/9/2014
Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
Statesville 4th CK
. 002
1/9/2014
Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
1/15/2014
MES
Statesville 4th CK
002
1/9/2014
Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
1/15/2014
MES
Statesville 4th CK
002
1/9/2014
Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/15/2014
MES
Statesville 4th CK
002
1/9/2014
Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
Statesville 4th CK
002
1/9/2014
Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
1/15/2014
MES
Statesville 4th CK
002
1/9/2014
MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
1/15/2014
MES
SVOC 8270 TCLP BNA List
Client ID#
Lab EN Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th CK
002
1/9/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
1/15/2014
AKE
butadiene
Statesville 4th CK
002
1/9/2014
Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
. 1
100
1/15/2014
AKE
Statesville 4th CK
002
1/9/2014
Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
1/15/2014
AKE
Page 5 of 8

0 L
Summit Environmental Technologies,
WO#:
14010514
3310 Win St.
Cuyahoga Falls, Ohio
Date Reported:
p
1/21/2014
r
TEL: [phone] FAX.- [phone]
Company:
Synagro
Website: htto://iviviv.settekcou:
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 1/10/2014
Project#: Statesville
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th CK
002 1/9/2014 2,4-D
5.0 ND mg/L
Sludge
EPA 8321 A
1
10
1/15/2014
AMZ
Statesville 4th CK
002 1/9/2014 2,4,5-TP
0.50 ND mg/L
Sludge
EPA 8321 A
1
1.0
1/15/2014
AMZ
Page 6 of 8

Smnn:it Environmental Technologies, Inc.
I 3310
WO#: 14010514
Win St.
rt:dlnritd6tElr;'SL'E•FCPHOLaGscs�i.ic
Cioahoga Falls, Ohio 44223
Date Reported: 1/21/2014
•—
/s atyti,af L,Earal.at,tc�.. TEL: [phone] FAX. • [phone]
Company: Synagro
Website: hap.-lAm.iv.setfek.com
Address: 284 Boger Rd.
Mocksville.NC 27028
Received: 1/10/2014
Project#: Statesville
Client ID# Lab ID# Collected Analyte
Result Units
Matrix Method DF RL
Run Analyst
Statesville 3rd CK 001 1/9/2014 Flashpoint (140°F)
>140 T
Sludge EPA 1010 1
1/13/2014 TAH
Statesville 3rd CK 001 1/9/2014 Cyanide, Reactive
ND ppm
Sludge EPA 9014 1 0.50
1/13/2014 TIR
Statesville 3rd CK 001 1/9/2014 pH
6.0 s.u.
Sludge EPA 9045 D 1
1/13/2014 AYS
Statesville 3rd CK 001 1/9/2014 Sulfide, Reactive
ND ppm
Sludge EPA 9034 1 25
1/13/2014 TIR
Client ID#
Lab ID# Collected Analyte
Result Units
Matrix
Method
DF RL
Run
Analyst
Statesville 4th CK
002
1/9/2014
Flashpoint (140T)
>140 T
Sludge
EPA 1010
1
1/13/2014
TAH
Statesville 4th CK
002
1/9/2014
Cyanide, Reactive
ND ppm
Sludge
EPA 9014
1 0.50
1/13/2014
TIR
tatesville 4th CK
002
1/9/2014
pH
5.9 s.u.
Sludge
EPA 9045 D
1
1/13/2014
AYS
Statesville 4th CK
002
1/9/2014
Sulfide, Reactive
ND ppm
Sludge
EPA 9034
1 25
1/13/2014
TIR
Page 7 of 8

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
Town of Statesville
WQ Permit Number:
WWTP Name: Fourth Creek WWTP NPDES Number:
Monitoring Period: From Jan 1, 2014 To Dec 31, 2014
WQ 00016247
NCO031836
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlicable to alternative nerformed (Class A or Class R) comnlete the followinu manitorina data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6h
MPN
Coliform
power per gram
96
6363
70,485
MPN/g
0
quarterly
grab
SM92210E
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Mt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) XX
Option/Mt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
AnddSrAh, Residuals Superintendent
Pre, rer me title type or print) f Land Applier Name and Title (if applicable) (type or print)
Signatur t
f Preparer'r Date Signature of Land Applier (if applicable) Date
"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 1114/2014
Reported: 1/22/2014
For: 4th Creek -Statesville
Date
Sample ID
Parameter
Cust ID
Result
Units
Method
Analyzed Analyst
140114-14.1
% Solids
1
30.1
%
SM2540B-1997
1115/14
CL
140114-14.1
Fecal Coliform MTF
1
9302
MPNIg
SM9221 CE-2006
1116/14
CL
140114-14.1
Geometric Mean
1
6363
MPNIg
dry wt. basis
1/17/14
CL
140114-14.2
% Solids
2
21.9
%
SM2540B-1997
1116/14
CL
140114-14.2
Fecal Coliform MTF
2
22,831
MPNIg
SM92210E 2006
1/15/14
CL
140114-14.3
% Solids
3
25.7
%
SM2640B-1997
1/15/14
CL
140114-14.3
Fecal Coliform MTF
3
1167
MPNIg
SM9221 CE 2006
1116114
CL
140114-14.4
0/c Solids
4
32.6
%
SM25408-1997
1116/14
CL
140114-14.4
Fecal Coliform MTF
4
27,607
MPNIg
SM92210E 2006
1115/14
CL
140114-14.6
% Solids
5
41.5
%
SM2540B-1997
1115114
CL
140114-14.5
Fecal Coliform MTF
5
96
MPN/g
SM92210E 2006
1/15/14
CL
140114-14.6
% Solids
6
22.7
%
SM254OB-1997
1115/14
CL
140114-14.6
Fecal Coliform MTF
6
70,485
MPNIg
SM92210E 2006
1115/14
CL
140114-14.7
% Solids
7
32.9
%
SM2540B-1997
1116/14
CL
140114-14.7
Fecal Coliform MTF
7
9119
MPN/g
SM92210E 2006
1116/14
CL
P.O. Box 228 a Statesville, North Carolina 28687.704/872/4697

Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 1/14/2014
Reported: 1/22/2014
For:
Date
Sample ID Parameter - Cust ID Result Units Method Analyzed Analyst
Respectfully submitted,
Dena Myers
f.}
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 a Statesville, North Carolina 28687.7041872/4697

rl(— —7.
j
Address: r— t
.... •? STATE SVILLE ANALYTICAL
122 Court Street • P 0. $ox 228
ft\ 4 s h, �� r ✓ S
Statesville,NC 28687
(704) 87244597
�� 6
Contact Person: ,r _ ' ' Phone # — ,
— C"`I t '`iC�.S'_
FAX#3�,l �qy gq_50
Chi of
PO # J r;� r Requisitioned by: / j j v
f�' s Jt�'
(Time' ��� Date)w
'
Custody �eCOx'd'
Customer Lab -ID # Time Sampled
Sample 1D!!# (Grab Only)
Date Sampled i
(Grab Only)
{�v`<%i''JAt
Matrix
slu9Bo vuw Parameters requested for analysis
#,�f �'. It � i L
/
,
F% • ; .:
.
}
it
1
k
/V
v
%
Relinquished by: �*'� ✓�
Gi v
Time
am„Date
Sampled b rfi %,
Received by:
Time i z . G arri, pm Date ./:r �'°
�=--�
Transported by:
✓
Relinquished by:
Time
am, pm Date
Holding times met:
/
Received by:
Y
Time
am, pm Date
••
Compliance work:
Composite Sampling #1:
Time begin am, pm Date _/ /
Non-compliance work:
Time end am, pm Date �//
Lab Comments:
Composite Sampling #2:
Time begin am, pm' Date ! /�
Time end am, pm Date �% J

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1/6/2014
13.8.
1/6/14 9:24AM
LC
1/6/14 9:31 AM
BJ
300
1.3
13.8
14.2
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
5.59
1
5.57
2
5.58
3
5.58
4
5.61
5
5.63
6
5.65
7
5.68
8
5.65
9
5.61
10
5.59
11
5.58
12
5.55
13
5.55
14
5.54
15
5.51
Slope: 0.0
Intercept: 5.6
Correlation Coefficient: 0.4
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.24 mg Oxygen/hr
0.06 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.09 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.6
7.63
7.67
7.64
7.63
7.54
7.51
7.48
7.51
7.49
7.48
7.44
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1/7/2014
12.9
117/14 2:30 PM
1/7/14 2:38 PM
300
1.34
13.4
13.6
0.0
7.7
0.9
liliters
Dry Solids
arees Celsius
frees Celsius
0.94 mg Oxygen/hr
0.23 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.3I- mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WW
Biosolids Permit Number:
Date:
1/8/2014
Digester Temperature:
11.5
Sampling Date/Time:
1/8/14 1:00 PM
Sampled By:
LC
Analysis Date/Time:
1/8/14 1:12 PM
Analyzed By:
BJ
Sample Volume:
300
Total Solids:
1.5
Beginning Temperature:
11.7
End Temperature:
12.8
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.4
1
8.43
2
8.39
3
8.36
4
8.34
5
8.29
6
8.26
7
8.25
8
8.23
9
8.18
10
8.15
11
8.09
12
8.04
13
7.99
14
7.92
15
7.88
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.5
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
2.15 mg Oxygen/hr
0.48 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1 0.82 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. .

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/l)
8.45
8.4
8.39
9.34
8.32
8.26
8.2
8.23
8.21
8.2
8.17
8.14
8.13
8.1
8.07
8.05
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
1 /9/2014
10.2
1/9/14 1:14 PM
AS
1/9114 1:25 PM
BJ
300
1.3
10.7
12.4
ti
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
2.30 mg Oxygen/hr
0.59 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 1.01 mg Oxygen/g/hr
. _ _ _ - _ _
"'' iistructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically:

Specific Oxygen Uptake Rate
SOUR
Facility Name:jFou
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 1/
Sampled By:
Analysis Date/Time: 1,
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
6.98
6.94
6.93
6.93
6.92
6.91
6.95
6.9
6.83
6.82
6.8
6.77
6.76
6.75
6.74
6.71
Slope:
Intercept:
Correlation Coefficient:
11.9
RG
4 1:06 PiV
300 milliliters
1.4 % Dry Solids
12.2 degrees Celsius
13 degrees Celsius
0.0
7.0
1.0
Oxygen Uptake Rate: 1.08 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.26 mg Oxygen/g/hr
Average Temperature: 13 degrees Celsius
Temperature Correction Factor: 1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.41 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.31
6.07
5.88
5.72
5.56
5.45
5.4
5.38
5.25
5.22
5.17
5.15
5.12
5.1
5.07
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
ourth Creek
0.1
6.0
0.9
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4.33 mg Oxygen/hr
0.90 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 1.18 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
_ 6.45
1
6.31
2
6.3
3
6.21
4
6.21
5
6.12
6
6.05
7
6.12
8
6.11
9
6.12
10
6.13
11
6.13
12
6.16
13
6.18
14
6.14
15
6.15
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTPW
1/14/2014
15.3
1/14/14 12:51 PM
1/14/14 1:02 PM
BJ
300
1.5
16.9
0.0
6.3
0.6
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.78 mg Oxygen/hr
0.17 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.23 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Third Creek WWTP NPDES Number: NCO020591
Monitoring Period: From Jan 1, 2014 To Mar 31, 2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Anaerobic Digestion
Composting Aerobic Digestion
.Li applicaule LU alternative PeFlurineu %-
ass A or %-lass l5 complete ine ionowing monitoring
tiara:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dances
Analysis
Fecal
2x10 to the 6'h
MPN
Coliform
power per gram
30,488
59,351
100,000
MPN/g
0
quarterly
grab
SM92210E
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Mt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) XX
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Mt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Anh Smith, Residuals Su erintendent
Pr pare ame Title (y e or print) Land Applier Name and Title (if applicable) (type or print)
-r3�s
Signatur of Preparer* Date Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 1/14/2014
Reported: 1/22/2014
For: 3rd Creek -Statesville
Sample ID
Parameter ' Cust ID
Result
Units
Method
Date
Analyzed Analyst
140114-13.1
% Solids
1
15.4
%
SM254OB-1997
1116/14
CL
140114-13.1
Fecal Coliform MTF
1
32,468
MPN/g
SM92210E 2006
1/16114
CL
140114-13.1
Geometric Mean
1
59,351
MPNIg
dry wt. basis
1117114
CL I
140114-13.2
% Solids
2
15.7
%
SM2640B-1997
1115/14
CL
140114-13.2
Fecal Coliform MTF
2
57,325
MPN/g
SM92210E-2006
1115/14
CL
140114-13.3
% Solids
3
16.0
%
SM2540B-1997
1116/14
CL
140114-13.3
Fecal Coliform MTF
3
100,000
MPN/g
SM92210E-2006
1/16114
CL
140114-13.4
% Solids
4
21.0
%
SM254OB-1997
1/15114
CL i
i
140114-13.4
Fecal Coliform MTF
4
76,190
MPNIg
SM92210E 2006
1115114
CL
140114-13.5
% Solids
5
16.4
%
SM2540B-1997
1116114
CL
140114-13.5
Fecal Coliform MTF
5
30,488
MPNIg
SM92210E 2006
1116114
CL
140114-13.6
% Solids
6
15.0
%
SM2540B-1997
1115/14
CL
140114-13.6
Fecal Coliform MTF
6
60,000
MPNIg
SM92210E 2006
1116/14
CL
140114-13.7
% Solids
7
16.0
%
SM2540B-1997
1115/14
CL
140114-13.7
Fecal Coliform MTF
7
100,000
MPNIg
SM92210E-2006
1115114
CL
P.O. Box 228 9 Statesville, North Carolina 28687.704/872/4697

Synagro
284 Boger Rd.
Mocksville
Entered 1/14/2014
Reported: 1/22/2014
For:
NC 27028
Sample ID Parameter Cust ID Result Units ©ate
Method - Analyzed Analyst
Respectfully submitted,
Dena Myers �J
NC Cert #440,
NCDW Cert #37756,
EPA NCOO909
P.O. Box 228 s Statesville, North Carolina 28687 0 704/872/4697

Myl-011t. I
ocA 01, ��rc
Address: I r era a
STATESVILLE, ANALYTICAL
122 Court Street - P.O. Box 228
AA
Statesville. NC 28687
(704) 8724697
Contact Person: Phone
sa/k 17
�q
FAX#
� - -11
(Chain of
Requisitionecl by: (Time /41� x Date)
Custody Record -
Customer
La
Sample 10# Lab -ID 0 Time Sampled
(Grab Only)
—Date —Sampled aMaim
(Grab Only) 2
studgo ["'fq ww Parameters requested for analysis
'Kosvo�("
e.
130 '"'V\
tz/
if
t
eK
/v
V
I
Af
Relinquished by: VC
Time
a Date
M"
Sampled by: 'V
Received by:
Time am, P'm Date /M/!�
Transported by:
Relinquished by: ✓
Time
am, pm Date
Holding times met:
Received by:
Time
am, pm Date
Composite Sampling 41:
Compliance work:
Time begin_ am, pm Date
Non-compliance work:
Time end am, pm Date
.
Lab Comm ents:
Composite Sampling #2:
Time begin— am, pm' Date
Time end— am, pm Date

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.23
1
8.17
2
8.15
3
8.11
4
8.08
5
8.02
6
8
7
7.98
8
7.91
9
7.85'
10
7.81
11
7.76
12
7.76
13
7.75
14
7.73
15
7.69
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1/2/2014
12.7
1/2/14 8:43
SA
1/2/14 8:51
SA
300
1.9
12.3
12.8
0.0
8.2
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.22 mg Oxygen/hr
0.39 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.63 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
1 /3/2014
Digester Temperature:
10.8
Sampling Date/Time:
1/3/1413:23
Sampled By:
SA
Analysis Date/Time:
1/3/14 13:32
Analyzed By:
SA
Sample Volume:
300
milliliters
Total Solids:
1.9
% Dry Solids
Beginning Temperature:
11.1
degrees Celsius
End Temperature:
11.9
degrees Celsius
Time Dissolved Oxygen Level
(minutes)
(mg/l)
0
9.53
1
9.48
2
9.4
3
9.34
4
9.28
5
9.23
6
9.15
7
9.11
8
9.04
9
8.97
10
8.9
11
8.85
12
8.79
13
8.74
14
8.68
15
8.65
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
9.5
1.0
3.62 mg Oxygen/hr
0.64 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 1.09 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
.7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1 /6/2014
11.3
1/6/14 10:19
SA
1/6/14 10:24
SA
300
milliliters
1.8
% Dry Solids
11.4
degrees Celsius
11.8
degrees Celsius
0.0
9.6
1.0
2.81 mg Oxygen/hr
0.52 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: �0.89 �mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
1 /14/2014
12.8
1/14114 12:27
SA
1/14/14 12:32
SA
300
1.7
12.6
13.2
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.6.
1.0
2.91 mg Oxygen/hr
0.57 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 1 0.91 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
1 /15/2014
Digester Temperature:
11.4
Sampling Date/Time:
1/15/14 10:32
Sampled By:
SA
1/15/14 10:38
Analysis Date/Time:
Analyzed By:
SA
Sample Volume:
milliliters
300
Total Solids:
1.7
% Dry Solids
Beginning Temperature:
degrees Celsius
11.7
12.3
End Temperature:
degrees Celsius
Dissolved Oxygen Level
(mg/1)
7.08
7.03
7.02
6.97
6.94
6.88
6.8
6.76
6.71
6.68
6.63
6.58
6.55
6.53
6.5
6.48
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.1
1.0
2.58 mg Oxygen/hr
0.51 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 1 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Nam(
Biosolids Permit Numbe
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
7.52
7.47
7.43
7.36
7.32
7.25
7.21
7.14
7.12
7.08
7.06
7.02
6.97
6.93
6.86
6.82
Slope:
Intercept:
Correlation Coefficient:
Third Creek WWTP
1/16/2014
11.5
1/16/14 10:08
SA
1/16/14 10:14
300
1.7
11.7
0.0
7.5
1.0
Aliliters
o Dry Solids
egrees Celsius
egrees Celsius
. Oxygen Uptake Rate: 2.73 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.53 mg Oxygen/g/hr
Average Temperature: 12 degrees Celsius
Temperature Correction Factor: 1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.92 �mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
1 /17/2014
11.5
1/17/14 12:26
SA
1/17/14 12:31
SA
300
1.8
13
13.9
Dissolves! Oxygen Level
7.13
7.03
6.99
6.94
6.88
6.84
6.81
6.79
6.74
6.67
6.58
Slope:
0.0
Intercept:
7.2
Correlation Coefficient:
1.0
Oxygen Uptake Rate:
2.45 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.45 mg Oxygen/g/hr
Average Temperature:
13 degrees Celsius
Temperature Correction Factor:
1.605781476
Temperature Corrected Specific
Oxygen Uptake Rate: 0�73� mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Third Creek WWTP NPDES Number: NCO020591
Monitoring Period: From Apr 1, 2014 To Jun 30, 2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13(Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Al UPPUCKVIC w aueniauve eriormeu %.Pass
A or %.lass is complete ine ionowing monnorm
aaia:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6a'
MPN
Coliform
power per gram
3106
16,593
53,892
MPN/g
0
quarterly
grab
SM92210E
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) XX
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(A1k Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Andy SAnith,Residuals Su erintendent
Pr ar Nam d Title'(ty e or print) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagr®
284 Boger Rd.
Mocksville NC 27028
Entered 5/1/2014
Reported: 5/5/2014
For: 3rd Creek City of Statesville
®ate
Sample ID
Parameter
Cust ID
Result
Units
Method
Analyzed Analyst
140501-7.1
% Solids
1
15.5
%
SM2540B-1997
511/14
CL
)501-7.1
Fecal Coliform MTF
1
19,355
MPN/g
SM92210E-2006
5/1/14
CL
1-+0501-7.1
Geometric Mean
1
16,593
MPN/g
dry wt. basis
5/5/14
CL
140501-7.2
% Solids
2
14.7
%
SM2540B-1997
5/1/14
CL
140501-7.2
Fecal Coliform MTF
2
34,014
MPN/g
SM92210E-2006
5/1/14
CL
140501-7.3
% Solids
3
16.7
%
SM2540B-1997
511114
CL
140501-7.3
Fecal Coliform MTF
3
53,892
MPN/g
SM92210E-2006
511114
CL
140501-7.4
% Solids
4
14.3
%
SM2540B-1997
5/1114
CL
140501-7.4
Fecal Coliform MTF
4
16,783
MPN/g
SM92210E-2006
5/1114
CL
140501-7.5
% Solids
5
16.1
%
SM2540B-1997
5/1/14
CL
140501-7.5
Fecal Coliform MTF
5
3106
MPN/g
SM92210E-2006
511/14
CL
140501-7.6
% Solids
6
17.8
%
SM2540B-1997
5/1/14
CL
140501-7.6
Fecal Coliform MTF
6
9551
MPN/g
SM92210E-2006
5/1/14
CL
140501-7.7
% Solids
7
15.3
%
SM2540B-1997
511/14
CL
140501-7.7
Fecal Coliform MTF
7
19,608
MPN/g
SM92210E-2006
5/1/14
CL
P.O. Box 228 o Statesville, North Carolina 28687 o 704/872/4697

Synagro
284 Boger Rd.
Nlocksville NC 27028
±`ered 5/1/2014
Reported: 5/5/2014
For:
Date
Sampie ID Parameter Cust 10 Result Units Method Analyzed Analyst
Respectfully submitted,
Dena Myers v
NC Cert #440,
NCDW Cert #37755,
FDA NC00909
P.O. Box 228 o Statesville, North Carolina 28687 o 7041872/4697

Client: <
Address.
STATES 87MUI�'ANALYTICAL
122 Court
Street - P.O. Box 228
Statesville, NC 28687
[phone]
Contact Person: Phone #V,,/ FAX#, Chain of
PO # _ "-10 Requisitioned by:
(Time Custody Record
"
Customer
yj
IKS CAM,
Lab -ID # Time Sampled
Sample lD# (Grab Only)
Date Sampled
(Grab Only)
CL x
E I .
, I 3ludge W Matrix Parameters requested for analysis
/6 1I
Relinquished by:
Time )q �a7m, prn Date Sampled by: -..7, 'i
-A, I Q _D�
Received by:
Time
(am� pm
Date Transported by:
Relinquished by:
Time
am, pm
Date
Holding times met:
Received by:
Time
am, pm
Date _—Z
Compliance work:
Composite Sampling #11:
Time begin— am, pm Date
Non-compliance work:
Time end am, pm Date
Lab Comments:
Composite Sampling #2:
Time begin— am, pm Date
C" -
JO
Time end am, pm Date

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
'.Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total;.Solids'
Beginning Temperature:
End Temperature:
Third C
WQ
01
411
411
Dissolved Oxygen Level
9.47
9.43
9.36
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
f01 /14
12.8
a
14 8:2
0.1
9.8
1.0
milliliters
Dry Solids'
degrees Celsius
degrees Celsius
3.12 mg Oxygen/hr
0.58 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.93 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
TotalSolids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7
a
91
8.77
8.73
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
14 8:
SA
300 milliliters
8 0/0 Solids
13.9 degrees Celsius
14.6 degrees Celsius
0.1
9.5
1.0
3.21 mg Oxygen/hr
0.59 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.89 jmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Thirc
Biosolids Permit Number: V
Date:
Digester Temperature:
Sampling Date/Time-
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids
Beginning Temperature:
End Temperature:
rl
Dissolved Oxygen Level
9.52
a
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
14 I
SA
5.4
0.1
9.6
1.0
iilliliters
1W Dry Solids,.
egrees Celsius
egrees Celsius
3.49 mg Oxygen/hr
0.61 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.86 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes) �
1
2
3
4
5
O
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
BioaoidaPermit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
AnolyoisOate/Tima:
Analyzed By:
Sample Volume:
` ����
/;' k�1i
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.77
8.32
8.22
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
"._ ���U����
1degreesCelsiva
SA
300
'
161
3.38mg r
0.63mgOxygen/g/hr
18degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:mg Oxxoen/o/hr
Instructions: Enter Data inthe Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
1
2
3
4
5
0
7
8
8
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Nome:
Bi000UdsPermit Number:
Digester Temperature:
Sampling Date/Time:
8onnp|ed By:
AmokmiaDate/Time:
Analyzed By:
Sample Volume:
��zn^�U�l:-
ds:
�'o `
BeginningTemperature:
End Temperature:
Dissolved Oxygen Level
8.25
8.22
7.98
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
%'Dr lift
1�� Celsius
417� Idearees Celsius
1.94 mg
0.36 nngOxygen/o/hr
17degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rote:Onmoen/g/r
Instructions: Enter Data inthe Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Nam
Biosolids Permit Numbe
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total,Solids
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.5
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
300 milliliters
1°9 %:Dry Solids,;..
16.3 degrees Celsius
16.8 degrees Celsius
0.0
8.7
1.0
2.98 mg Oxygen/hr
0.52 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.64 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR .
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.76
9.7
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
04/09/14
14.1
4/9/14 8:01
SA
4/9/14 8:09
SA
300
14.2
15
0.0
9.9
1.0
milliliters
Dry Solids
degrees Celsius
degrees Celsius
2.74 mg Oxygen/hr
0.51 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.71 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville
WQ Permit Number: WQ 00016247
WWTP Name: Third Creek WWTP NPDES Number: NCO020591
Monitoring Period: From Jul 1, 2014 To Sep 30, 2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Anaerobic Digestion
Composting Aerobic Digestion
If applicable to alternative performed Class A or Class B complete the following monitorin data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6`h
MPN
Coliform
power per gram
369
52,945
305,343
MPN/g
0
quarterly
grab
SM92210E
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) XX
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Anhy With, Residuals S erintendent
Pr are me itle or print) Land Applier Name and Title (if applicable) (type or print)
Signatur to
f Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Analytical Result
s ynagro
284 Boger Rd.
Mocksville NC 27028
Entered 7/28/2014
Reported: 7/30/2014
For: 3rd Creek
Date
Sample ID
Parameter
Cust ID
Result
Units
Method
Analyzed Analyst
140728-6.1
% Solids
1
61.7
%
SM2540B-1997
7/28/14
CL
A^728-6.1
Fecal Coliform MTF
1
35,656
MPN/g
SM92210E-2006
7/28/14
CL
728-6.1
Geometric Mean
1
52,945
MPN/g
dry wt. basis
7/30114
CL
140728-6.2
% Solids
2
61.3
%
SM2540B-1997
7128/14
CL
140728-6.2
Fecal Coliform MTF
2
261,011
MPN/g
SM92210E-2006
7/28/14
CL
140728-6.3
% Solids
3
32.7
%
SM2540B-1997
7128/14
CL
140728-6.3
Fecal Coliform MTF
3
91,743
MPN/g
SM92210E-2006
7/28/14
CL
140728-6.4
% Solids
.4
50.7
%
SM2540B-1997
7/28/14
CL
140728-6.4
Fecal Coliform MTF
4
47,337
MPN/g
SM92210E-2006
7/28/14
CL
140728-6.5
% Solids
5
54.2
%
SM2540B-1997
7128/14
CL
140728-6.5
Fecal Coliform MTF
5
369
MPN/g
SM92210E-2006
7/28114
CL
140728-6.6
% Solids
6
62.5
%
SM2540B-1997
7/28/14
CL
140728-6.6
Fecal Coliform MTF
6
256,000
MPN/g
SM92210E-2006
7/28/14
CL
140728-6.7
% Solids
7
52.4
%
SM2540B-1997
7/28/14
CL
140728-6.7
Fecal Coliform MTF
7
305,343
MPN/g
SM92210E-2006
7/28/14
CL
P.O. Box 228 ,DStatesville, North Carolina 28687 o 704/872/4697

Synagro
284 Boger Rd.
Mocksville
Fered
.sported:
For:
Sam le ID
7/28/2014
7/30/2014
NC 27028
Date
p esu Units memod Analyzed Analyst
Parameter
Respecffully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
Cust i® R It
P.O. Box 228 0 Statesville, North Carolina 28687 0 704/872/4697

Client:
STATESVILLE ANALYTICAL
122 Court Street - P.O. Box 228
�. Q\ :1
Address: ,)
Statesville, NC 28687
[phone]
Chain
(Custody Record
Contact Person: Phone C;n <_ FAX -
`
PO # Si., Requisitioned by'%l „14 +n : '.,; (Time, 1 % rrDate)
Customer Lab -ID #
Sample ID#
Time Sampled
Date Sampled
m E
Matrix Parameters requested
for analysis
(Grab Only)
(Grab Only)
6
Sludgel w I ww
�,t •°tF':_ j�`,+,.O
�.C71
3
,
•�ifl ;
JJ S{
l�l t
/,
+
I
+
I
I
Relinquished by: ' '; Irk;`!' 1 ~! r ✓ n
Time g.rf,.�
;
am ,, m Date �' uy:
9 r:=/Ir
Sampled b
Received by: by: - - ��
_�_ ,.
% ;�r;r --- _
_ —
Time
1 r -'am; pm)Date °`
Transported by.:
if
Relinquished by:
Time
am, pm Date _/ /
Golding times met:-''
Received by:
Time
am, pm Date
Compliance work:
Composite Sampling #1:
Time begin am, pm Date
/_/_
Non-compliance work:
Time end am, pm Date _/_/
Lab Comments:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date _/
/_

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
.14
15
Specific Oxygen Uptake Rate
SOUR -
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
3.3
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
300 milliliters
1.9. %Dry Solids:.
22.9 degrees Celsius
22.1 degrees Celsius
0.0
3.4
1.0
2.37 mg Oxygen/hr
0.42 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 0.36 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

C
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR .
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
:Total,Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Third Creek WWTP
WQ0016247
07/09/14
23
7/9/1413:38
SA
7/9/14 13:46
SA
300
L
21
20.6
Slope: 0.0
Intercept: 3.6
Correlation Coefficient: 1.0
rilliliters
'/o bry Solids:
iegrees Celsius
legrees Celsius
Oxygen Uptake Rate: 2.35 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.46 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.44 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12_
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
16W Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
4.35
v
4.31
4.27
Third Creek WWTP
W00016247
07/10/14
21.7
7/10/14 8:34
SA
7/10/14 8:43
SA
300
;1 :7
21.4
21.1
milliliters
Yo Dry S61ift
iegrees Celsius
iegrees Celsius
Slope: 0.0
Intercept: 4.6
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.84 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids,
Beginning Temperature
End Temperature
Dissolved Oxygen Level
74
6.52
46 8
0
6.45
6.42
Third Creek WWTP
W Q0016247
07/11/14
21.7
7/11/14 8:25
SA
7/11 /14 8:30
SA
300
17,
20.5
20.3
milliliters
Drs/ Solids
legrees Celsius
legrees Celsius
Slope: 0.0
Intercept: 6.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.69 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.53 mg Oxygen/g/hr
Average Temperature: 20 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate: 0.53 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total, Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.83
6.26
6.2
6.17
Third Creek WWTP
WQ0016247
07/14/14
22.5
7/14/14 9:56
SA
7/14/14 10:04
SA
300
17
21.6
21.1
Slope: 0.1
Intercept: 8.0
Correlation Coefficient: 0.6
-milliliters
Dry Solids :`a
legrees Celsius
legrees Celsius
Oxygen Uptake Rate: 8.37 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.64 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 1.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility P
Biosolids Permit Nu
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids.
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.08
6.51
6.47
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
300 milliliters
1 7. 0io Y. Solids
20.9 degrees Celsius
20.4 degrees Celsius
0.1
7.2
1.0
3.00 mg Oxygen/hr
0.59 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
6.57
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
07/16/14
21.2
7/16/14 7:08
SA
7/16/14 7:11
SA
300
17
21.1
19.8
0.0
6.5
1.0
-nilliliters
'/o 1. 1Dry Solids;
legrees Celsius
legrees Celsius
2.20 mg Oxygen/hr
0.43 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.43 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Third Creek WWTP NPDES Number: NCO020591
Monitoring Period: From Oct 1, 2014 To Dec 31, 2014
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
xr apPlICRDle ro airernar►ve periormea r;iass
A or Maass ps complete ine iouowing monirorm
aara:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6ch
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
1260
4230
8780
CFU/g
0
quarterly
grab
9222D-MF
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. l
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) XX
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction_
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
And S ' h Residuals Superintendent
Pr arer ame itle or print) Land Applier Name and Title (if applicable) (type or print)
Signature f Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing SeMces., Inc.
Laboratory Report
Synagrr®
. C 5
Statesville
4 ��gt�latorr
=
tample
Information
amgled +
E. Thom son wMR
Dae 3;
P-..,
01/29/15 Re et e
ROB ;
Analyses
.and Results
NC DENR 4654
NC PHHS #37799
US EPA #NC01918
ISOM
t
SY
Yes
vw�gg
C: Cameron �=Datr 01/29/15
0
150132 01
a
Sludge. Gr Fec. Coliform-S <8780
CFUig
8780 01/30/15 SB 9222D - MF
b _
<1260
CFU1g
1260
G
_ - <1290
CF01g
1290
d
- <7750
CFUI9
7750
e
<7700
CFU/g .
7700
f
<7150
CFU/g
7150
9
<3970
C.FU/a
3970
Geomean <4230
150132 `:01 a
3]udge Gr TS (%} 11,2
1.
o,m 01130/15 S13 2540 G -TS
b
'
78.6
%
c,oi
C
o
77.0
%
0.01
d
12.2
�
0.01
ev
12.6
%
0.01
r
f
13.0
%
0.01
9
21.4
%
0.01
Data'
Review aZ—Mpl,,-�
L echnician Date
Report
Review
Lab Director Date1
i
i
219 S. Steele Str. 919-209-4240
Sanford NC 17330 [e-mail]

219 S. Steele Str.
Sanford, NC 27330 Cameron- Testing Inc..
Phone; 919-208-4240 NC VVVVIGW Cert;-#654 NC PHHS:Cert #-37799- US EPA NG01418
Chain- of Custody
Page t of /
Cqmp�any*
71
Samoa,
-Tali use only
'Phone ,.-
TZp�(C).
-Address`T
`284 Bober Rd. Fax xf.
Blank
(YININA)
Arrive:
10)
MOC 9VilleNC 27028, Notes
- , --
4'
q4 f, /k_-Regp�a­oy
i
,-
Due---
Due
:
Project:
,
V1 t.
-Rdsh, i
(YIN)4
(YIN)
Collected:
Nanv: rxelz_ . —64 s
Signature:
-.-Sam le —Information
1,
:- ,,Nu rof-b .Iles; —
Lu
M
1- 11 z 0. V)
a3 a)
Ca Y
S'kmple ID CL LO Requested Analysis
0
. U 4 SludgeFecail/%Solids
- - -- ----- -- -------
T
Rd§hrwork-�ill requjre'..pejbr approval. Addifionalcharges.\Mll -apply
ID
0

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
. End Temperature
Dissolved Oxygen Level
7.94
7.87
7.47
7.45
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
09/02/14
18.7
9/2/14 8:04
JW
9/2/14 8:11
SA
300
18.8
18.6
0.0
7.9
1.0
milliliters
Dry Solids
legrees Celsius
legrees Celsius
2.52 mg Oxygen/hr
0.47 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.50 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By:
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.12
7.09
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
09/03/14
18.7
9/3114 8:08
JW
9/3/14 8:15
SA
300
19
18.6
0.1
7.2
1.0
milliliters
Dry Solids
legrees Celsius
legrees Celsius
3.00 mg Oxygen/hr
0.56 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.59 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total,.5olids
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.38 .
4.82
4.73
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
35
300 milliliters
DIry.Solids.
21 degrees Celsius
20.7 Idearees Celsius
0.1
5.4
1.0
3.48 mg Oxygen/hr
0.61 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:j 0.58 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
09/05/14
20.2
9/5/14 9:19
SA
9/5/14 9:26
SA
300
1:9
19.6
19.1
0.1
8.0
1.0
rilliliters
Dry Solids.
legrees Celsius
legrees Celsius
5.17 mg Oxygen/hr
0.91 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.97 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Third Creek
Biosolids Permit Number: WO001F
Date: 09/097
Digester Temperature: 19.7
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids
Beginning Temperature:
End Temperature:
9/9/1Z
. S.
9/9/12
S,
3(
1:
19
18
Dissolved Oxygen Level
7.7
0
7.67
7.62
7.46
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
%'DF Solids
degrees Celsius
decrees Celsius
0.0
7.8
1.0
1.66 mg Oxygen/hr
0.29 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:' 0.31 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
'Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.05
a
7.98
7.75
7.75
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
09/10/14
19
9/10/14 9:24 -
SA
9/10/14 9:29
SA
300
19
18.9
18.4
0.0
8.1
0.9
'milliliters
ji
' D, $olIds,.;
legrees Celsius
legrees Celsius
1.97 mg Oxygen/hr
0.35 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.37 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation'and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
1 WQ0016247 I
Digester Temperature:
Sampling Date/Time: f
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total ;Solids
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.87
0
7.82
i
7.79
7.6
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
f14 8:20
SA
i00 milliliters
% Dry Solid$
9.2 degrees Celsius
8.7 degrees Celsius
0.0
7.9
1.0
1.44 mg Oxygen/hr
( 0.25 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 11 0.27 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Agricultural Lime Application Log
2014
Project: City of Statesville
Field
Soil
��Tlac.(frorn
Lime Requirement 11
Tons/Acre
- Date Applied
(state -county -site -field)
pH
soil analysis
Applied
(invoice date)
AL-14-1A
6.0
N/AN/A..
_�,
N
AL-14-1 B
5.6
0.8
IR-20-4A
7.1
N/A
N/A
R-20-07
6.7
N/A
IR-20-08
6.2
N/A
IR-20-09
7.1
N/A
_ nN/Q_a_.
R-23-01
6.2
N/A
IR-23-02
6.3
N/A
N/A
I R-23-03
6.2
N/A
IR-23-04
6.7
N/AN/AN/A�
R-23-05
6.1
N/A
* = Lime to be applied when weather and/or crop removal allows

Page 1 of 1 -
Report Number: 15-013-0601�
Account Number: 46493
Send To: SYNAGRO CENTRAL LLC/STATESVILLE aleastertt.com
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 01/13/2015 Date Of Analysis: 01/14/2015
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower:
T PAYNE
STATESVILLE ANNUAL
SOIL ANALYSIS REPORT
Date Of Report: 01/14/2015
Submitted By: ERIC THOMPSON
Farm ID: AL 14
Analytical Method(s):
Mehlich 3
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
o ENR
/o Rate
Mehlich 3
Re serve
K
Mg
Ca
Na
Soil
Buffer
H
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
' '
. - Rate
ppm Rate
P H
Index
meq/100g
meq/100g
1A
237 VH
147 H
182 H
1211
M
13 VL
05098
5.9 H 150
6.0
6.78
1.5
9.5
NC=197
NC=75
Percent
Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
Field ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mti
Fe
Cu
B
SS
Cl
Al
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
1A
19 M
24.3 VH
26 H
188 VH
7.7 VH
0.6 M
0.12 VL
4.0
16.0
63.7
0.6
15.3
NC = 40
NC = 607.5
NC = 163
NC = 385.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by; paµric me
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

NCDA&CS A..._..-)mic Division Phone: [phone]
Website: WWW.nL.U..uov/agronomi/
Report No. FY15-OLU 14603
��i_
Client: Tim L. Payne
Advisor: Synagro Central
Predictive
c/o Superior Jersey FarmAttn:Eric
Thompson
r�!
1265 Payne Dairy Rd.
284 Boger Rd
,.5, ;,
ti- , , �. _ + S ®l l Report
Mehlich-3 Extraction
Taylorsville, NC 28681
Mocksville, NC 27028
Sampled County: Alexander
Sampled: 10/01/2014 Received:
11/07/2014
Completed: 11/26/2014
Farm: AZ-14
Links to Helpful Information
Sample ID: 1 B
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O6
K2O Mg S Mn
Zn
Cu B
Information
Lime History:
1 -Small Grain (SG)
0.8
80-100 0
0 0 0 0
0
0 0
Note: 3
2-Soybean
0.0
0 0
0 0 0 0
0
0 0
Note:3
Test Results [units - W/v in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.46 1.07 9.7 81 1.9 5.6
186 88
61 16
45 210 136 136 473
473
230 0.1 1
North Carolina
�9iah:�t�o aru>; Fund Ct;mrifrsltau
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Ate. _..mimic Division Phone: [phone] Website: www.ntayr.yovlagronomi/ Report No. FY15-aLu-i4603
Tim L. Payne Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncaar.pov/apronomi/obpart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
'rest Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaaraov/aaronomi/uyrst.htm
for more information.
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-I
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-AI1
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P206
phosphate
S-1
sulfur index
SS-1
soluble salt index
W1V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

NCDA&CS A-_ _
mic Division Phone: [phone]
Website: www.nc-,,,,:�.-)v/agronomi/
Report No. FY14-' __ ,2424
Lru�r
Client: Dennis Phillips
201 Barry Oak Rd
Advisor: Synagro Central
Attn:Eric Thompson
off.;,
Predictive
��(I "• a
}' �I
�''��' ` -'��,�>��.•!�i
Soil Report Mehlich-3 Extraction
Statesville, NC 28625
Sampled Count Iredell
284 Boger Rd
Mocksville, NC 27028
Sampled: Received: 04/07/2014 Completed: 04/16/2014
Farm: IR-20
Links to Helpful Information
Sample ID: 4A
Recommendations: Lime
- Nutrients (Ib/acre)
More
Crop (tons/acre)
N P206
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1 0.0
120-200 0
60 0 0
pH$
0
0 0
Note: 12 Note:
2-Fescue/OGrass/Tim, 0.0
120-200 0
60 0 0
pH$
0
0 0
Note: 12 Note:
Test Results [units - WN in g/crrr3; CEC and Na 'in meq/100 cd; NO3-N in mg/drrP]:
Soil Class:
Mineral
NM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-I Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 0.96
16.3 98 0.3 7.1 206 39
80 17
43 127 76 76
486
486
346 0.1 1
Sample ID: 413
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.0
120-200 0
50 0 0
pH$
0
0 0
Note: 12 Note:
2-Fescue/OGrass/Tim, 0.0
120-200 0
50 0 0
pH$
0
0 0
Note: 12 Note:
Test Results [units -WIV in g/crril; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WN
Co BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.13 0.94
3f 4 100 0.1 7.4 192 42
83 16
80 154 88 88
449
449
272 0..2. 1
Sample ID: 7
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
pH$
0
0 0
Note: 12 Note:
2- Fescue/OGrass/Tim, 0.0
120-200 0
0 0 0
pH$
0
0 0
Note: 12 Note:
Test Results [units - WN in glcrrt?; CEC and Na in meq/100 cm3; NO3-N in mg/dnf]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 0.98
15.9 95 0.8 , 6.7 484 197
75 14
61 586 358 358
759
759
423 0.1 1
forth Carolna
y 4jjb
3tiai�a«[a 7n�st 1'utcJ �t<<yil�si05�i�:rte
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS A_
mic Division Phone: [phone]
Website: www.ntuy.,jv/agronomi/
Report No.
FY14-oL-vo2424
Dennis Phillips
Page 2 of 3
Sample ID: 8
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0
0
0
0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, 0.0
120-200 0
0
0
0
0
0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-1
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 0.90
16.6 92 1.3 6.2 314 168
70 17 64
365
234
234
785
785
469 0.1
1

NCDA&CS E_-.___-)mic Division Phone: [phone] Website: www.n�.!j..zjov/agronomi/ ReportNo. FY14-oLu,32424
Dennis Phillips Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations ::
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for yield crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per.acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-O
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micron utrients.. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you. cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncapr.gov/apronomi/obpart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer.
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
Zn-I
zinc index
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaargov/apronomi/uvrsthtm
for more information.

Page 1 of 1
Report Number: 15-013-0597
Account Number:46493
n
�
www.aleasterii.com
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 01/13/2015 Date Of Analysis: 01/14/2015
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower:
D PHILLIPS
STATESVILLE ANNUAL
SOIL ANALYSIS REPORT
Date Of.Report: 01/14/2015
Submitted By: ERIC THOMPSON
Farm ID: 1 R-20
Analytical Method(s):
Mehlich 3
Organic Matter
Phosphorus
Potassium
Magnesium
- Calcium
.----Sodium
pH- ...
AcidIty
C.E.0
Sample ID
Lab
Field ID
Number
ENR
% Rate
Mehlich 3
Reserve
K-
Mg
Ca
Na
Soil
Buffer.
H
Ibs/A
ppm 'Rate
ppm Rate
ppm Rate
ppm Rate-
ppm
Rate
ppm Rate `
PH
Index
meq/100g
meq/100g
9
342 VH
207 H
281 M
3256
H
14 VL
05089
13.0 VH 150
71
0.0
19.2
9
NC = 285
NC = 106
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
"' Copper
Boron
Soluble.Salts
Chloride
-Aluminum
Sample ID
'
Field ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
CI
Al
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
9
29 H
22.2 VH
62 VH
196
VH
8.5 VH
1.0 M
0.25 VL
2.8
12.2
84.8
0.3
0.0
9
NC = 60
NC = 555.0
NC = 388
NC = 425.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by; �ptfia,
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary
E
t YYt�

NCDA&CS A,.—..,)mic Division Phone: [phone]
Predictive
461
,.rr ' .L� R w 1 +11
■
l Report
Website: www.nuagr.gov/agronomi/
Client: Eddie Porter
351 Gantt Horn Rd.
Statesville, NC 28625
Mehlich-3 Extraction
Sampled County: Iredell
Report No. FY14-si_u i2426
Advisor: Synagro Central
Attn:Eric Thompson
284 Boger Rd
Mocksville, NC 27028
Sampled: Received: 04/07/2014
Completed: 04/16/2014
Farm: IR-23
Links to Helpful Information
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
60
0
0
0
0
0 0
Note: 12
2-Fescue/OGrass/Tim, 0.0
120-200 0
60
0
0
0
0
0 0
Note:12
Test Results [units - W/V in g/cO; CEC and Na in meg1100 crrP; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 0.97
12.3 91 1.2 6.2 287 38
76 13
49 154
107
107
435
435
315 0.1 1
tNorth Carolina
Iti5{YIL(i) �j 11U1 FUILI) C(17111SIiS:•{iY19
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS � )mic Division Phone: [phone] Website: www.n- ov/agronomi/ Report No. FY1d. ___J2426
Eddie Porter Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations I Report Abbreviations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncacir.pov/aaronomi/oboart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncacirgov/apronomi/uvrsthtm
for more information.
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-AI1
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/v
weight per volume
Zn-AI
zinc availability index
Zn-1
zinc index

NCDA&CS Fry..;.:jmic Division Phone: [phone]
Website: vv war.na.ay..uov/agronomi/
ReportNo. FY15-aLUU6893
�r �'l` Y1�i
Predictive
Client: Shane Porter
351 Gantt Horn Rd.
Advisor: Synagro Central
Attn:Eric Thompson
I�s
Statesville, NC 26677
Boger Rd
284 Bo 9
Soil Report Mehlich-3 Extraction
Sampled County: Iredell
Mocksville, NC 27028
Sampled: Received: 09/25/2014
Completed: 10/06/2014
Farm: IR-23
Links to Helpful Information
Sample ID: 2
Recommendations: Lime
Nutrients (Ib/acre )
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
0
0
0 0
Note: 12
2-Fescue/OGrass/Tim, 0.0
120-200 0
0 0 0
0
0
0 0
Note: 12
Test Results [units -WIV in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-Al2
Zn-1
Zn-Al
Cu-I Na ESP SS-1 NO3-N
0.27 0.93
20.2 94 1.1 6.3 369 151
78 12 , 80
315 202 202
629
629
362 0.1 1
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, 0.0
120-200 0
0 0 0
0
0
0 0
Note: 12
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 cO; NO3-N in mg/drrP]:
Soil Class:
Mineral
HM% W/V .
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.18 1.05
14.7 94 0.9 6.2 361 110
77 13
79
232 153 153
431
431
237 0.1 1
Sample ID: 4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
pH$
0
0 0
Note: 12 Note:.
2- Fescue/OGrass/Tim, 0.0
120-200 0
0 0 0
pH$
0
0 0
Note: 12 Note:
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WIV
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.13 1.04
18.5 97 0.6 6.7 365 124
83 10
68
183 116 116
504
504
320 0.1 1
1!,Iarth Carolina
y rt?tia �.
90'tra co This: I-uiul Coannilssiviz
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS i _
- ►mic Division Phone: [phone]
Website: www.nL.�-.__.ovlagronomil
Report No.
FY1° ----- 6893
Shane Porter
Page 2 of 3
Sample ID: 5
Recommendations: Lime
Nutrients (lb/acre)
more
Crop (tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
30
0
0
0
0
0 0
Note: 12
2-Fescue/OGrass/Tim, 0.0
120-200 0
30
0
0
0
0
0 0
Note: 12
Test Results (units - WIV in 'g/cd; CEC and Na in meq/100 crn3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WIV
CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I Na
ESP SS-1 NO3-N
0.32 1.02
13.1 90 1.3 6.1 266 58
74 14 60
440
279
279
469
469
266 0.1
1

NCDA&CS AT____mic Division Phone: [phone]
Shane Porter
Website: www.nt.°,.:,',dv/agronomi/
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an. excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Report No. FY1E ___6893
Page 3 of 3
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-I
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
Mn-All
Mn-AI2
Mn-I
M-O
N
Na
NO3-N
ORG
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot pH
find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htm#fs to find P-1
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P205
S-1
Test Results SS-1
W/V
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not Zn-I
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagrgov/agronomi/uvrst.htm
for more information.
manganese
Mn-availability index for crop 1
Mn-availability index for crop 2
manganese index
mineral -organic soil class
nitrogen
sodium
nitrate nitrogen
organic soil class
current soil pH
phosphorus index
phosphate
sulfur index
soluble salt index
weight per volume
zinc availability index
zinc index

RECEIVED/NCDENR/DWR
MAR 10 2015
WQROS
MOORESVILLE REGIONAL OFFICE
STANLY COUNTY UTILITIES, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0005387
2014 ANNUAL REPORT

Stanly County Utilities, NC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Page
3. Annual Land Application Field Summary Form
4. TCLP Analysis -
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analysis

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00005387 County Stanly Year 2014
Facility Name (as shown on permit) Town of Oakboro WWTP NPDES No. NC0043532
Land Application Operator Svnagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 14
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 32.84
Total number of acres utilized for land application during the year: 24.1
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
II. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
Doug Burgess, Mayor
Pee7p4 e Name an i pe or p t)
l nnr �—� -f'JG' s X
Sit ature of Pr er Date
(i different from Permittee)
G � ��
ue i ae_
2015 s
giMiature of Land Applier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and -15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
STANLY COUNTY UTIL., NC (FKA OAKBOR
STANLY COUNTY UTIL.,
NC QUEST STANLY WVVTi P AEROBICALLY DIGESTED LIQUID
DRY
METRIC
MONTH/YEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
September 2014
254,200.00 G
15.48
D
14.04
October 2014
285,200.00 G
17.36
D
15.75
.YEARLY TOTAL
539,400.00 G
32.84
D
29.79
1 /26/2015

2014 ANNUAL REPORT
PROJECT: Stanly Co. Utilities, NC
FACILITY: West Stanly WWTP
24939-B Barbees Grove Road
Oakboro, NC 28129
704-485-4613
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
NCO043532
Doug Burgess, Mayor
109-A N Main St
PO Box 610
Oakboro, NC 28129
252-753-5774
James Amaral, ORC/Town
Administrator
109-A N Main St
PO Box 610
Oakboro, NC 28129
704-485-8322
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0005387 Laboratory
Facility Name: STANLY COUNTY UTIL., NC (FKA OAKBORO) A&L Eastern Laboratories Inc.
NPDES# : NCO043532
or WQ# (residual only)
WWTP Name: WEST STANLY WWTP (FKA OAKBORO WWTP)
Residuals Analysis Data
Product Type
LIQ
Date Sampled (grab) or 07/31/14
Date Composited
Percent Solids
1.46
PARAMETERS (mg/kg dry weight)
Arsenic
7
Cadmium
<2
Mercury
1.6
Chromium
48
Copper
369
Lead
28
Molybdenum
17
Nickel
30
Selenium
8
Zinc
849
Total Phosphorus
19000
TKN
47300
Ammonia -Nitrogen
4790
Nitrate and Nitrite
9040
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gath(,Paq and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, incj4dino the possibility of fines and imprisonment for knowing violations."
x
(SI
Date 2
DENR FORM RSSF (5/2003) Printed: Monday - January 26 2015 at 13:21:09 for: 2170 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0005387 Laboratory
Facility Name: STANLY COUNTY UTIL., NC (FKA OAKBORO) A&L Eastern Laboratories Inc.
NPDES# : NCO043532
or WQ# (residual only)
WWTP Name: WEST STANLY WWTP (FKA OAKBORO WWTP)
Residuals Analysis Data
Product Type
LIQ
Date Sampled (grab) or 07/31/14
Date Composited
Percent Solids
1.46
PARAMETERS (mg/kg dry weight)
Aluminum
17000
Calcium
24500
Magnesium
4330
pH
5.96
Potassium
4690
Sodium
3600
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered arLq evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, includin h possibility of fines and imprisonment for knowing violations."
x
UREeOF P
NR - Data Not Reported or Data Not Required
Date 2 2 57
DENR FORM RSSF-B (7/2002) Printed: Monday - January 26 2015 at 13.21:40 for: 2170 01

Page: 1 of 2
Report Number: 14-213-0201
Account Number: 46477
Submitted By: DREW CULP
Send To: SYNAGRO CENTRAL LLC/OAKBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE . NC 27028
Lab Number: 56810
Sample Id : OAKBORO 2014
9A&L Eastern Laboratories, Inc.
90 7621 Whitepine Road Richmond, Mr9inla23237 [phone] Fax[phone] .
wwwaleastern.com
Project: OAKBORO
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 7/31/2014 08:45:00
Date Received: 08/01/2014 00:00
Date Reported: 08/08/2014
Total Solids '
I A6
14600
100.0
JM
08101 /201415:04
SM-2540G
Moisture `
98.54
100.0
JM
08101/201415:04
SM-254OG
Total Kjeldahl Nitrogen
4.73
47300
0
tw
08/04/2014 08:39
SM-4500-NH3C-TKN
Total Phosphorus
1.90
19000
100
KM
08/04/2014 14:50
SW 6010C
Total Potassium
0.47
4690
100
KM
08/04/2014 14:50
SW 6010C
Total Sulfur
1.05
10500
100
KM
08/04/2014 14:50
SW 6010C
Total Calcium
2A5
24500
100
KM
08/04/2014 14:50
SW 6010C
Total Magnesium
0.43
4330
100
KM
08/04/2014 14:50
. SW 6010C
Total Sodium
0.36
3600
100
KM
08/04/2014 14:50
SW 6010C
Total Iron
24300
100
KM
08/04/2014 14:50
SW 6010C
Total Aluminum
17000
100
KM
08/04/2014 14:50
SW 6010C
Total Manganese
680
5
KM
08104/201414:50
SW 6010C
Total Copper
::
369
5
KM
08/04/2014 14:50
SW 6010C
Total Zinc
849
5
KM
08/04/2014 14:50
SW 6010C
Ammonia Nitrogen
0.48
4790
10.0
MW
. 08/04/2014 08:39
SM-4500-NH3C
Organic N
4.25
42510
10.0
08/04/2014 08:39
CALCULATION
Nitrate+Nitrite-N
9040
2.00
TW
08104/2.01410:20
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
08/04/2014 14:50
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. ((/
. .. ... ... � i u, . �.rar; : �r ,nr: : rur ^r.::• rv,; :rrr:� •r nr:. ir. /�J�u/"�'-- `;'���wl.
r. ;;o-•...vh :nr r::::u::. .. .... ...: gt,;rrrc �n :tr:: :rJv.:.. ,, ., r: x.: reloa:. u•Rum, ;I:.. rr:<:;,J.-.. r:! •,rr ,r:r!.;:rr:n,, ur:, ,ern•. .:rIN. nti!4i at.7.drr.�
Debbie Holt

Page: 2 of 2
Report Number: 14-213-0201
Account Number: 46477
Submitted By: DREW CULP
Send To: SYNAGRO CENTRAL LLC/OAKBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
A&L EasternLaboratories, Inc.@P.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastem.com
Project: OAKBORO
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 7/31/2014 08:45:00
Lab Number: 56810
- -
Date Received: 08/01/2014 00:00
Sample Id: OAKBORO 2014
LIMIT
Date Reported: 08/08/2014
ANALYSIS METHOD
ARAM_
48
5
KM
■. ­rErrIME
08104/201414:50 SW 6010C
Total Chromium
Total Nickel
30
5
KM
08/04/2014 14:50 SW 6010C
Total Lead
28
5
KM
08104/201414:50 SW 6010C
Total Arsenic
7.0
3.0
KM
08/04/2014 14:50 SW 6010C
Total Mercury
1.6
0.4
KM
08/04/2014 14:00 SW-7471 B
Total Selenium
8.0
5.0
KM
08/04/2014 14:50 SW 6010C
pH (Standard Units) "
5.96
2.00
MW
0810412014 10:05 SW-9045D
Total Molybdenum
17
5
KM
08/04/2014 14:50 SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
"Ca", THE MATRIX SPIKE DUPLICATE WAS
OUT OF LIMITS FOR NO3+NO2-N, ALL OTHER
QUALIFIER: THE MATRIX SPIKE WAS OUT
OF LIMITS FOR
QC DATA WAS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
.., ..n.l ; .�•.,.. .n.... MA: 'A 411i,7011,I.,! :1s,::1; .!:r !•in:: aI,;! rr>;ry !:I , „J III '!I,1 ..,!:rr 1:7.'r:!,. .., ir, !f❑ q.,. 'll.l rmArn:II ,; :W;
,.: d':. ..:, a: •. ,.. .a.,.,..n ar.. ,nJJ':r,,::,; u„ n.r:v;. u:b:..<. . ,„'• .,...:f orlrr,: .rtrr,::rr;i.,:pnnr: D. ,:'l: n: :: a' u..::r. :o:.:.+nr ; :n.' ::•r::.:':!I .::U:, •!:Z:,;," .
Debbie Holt

SAMPLING LOG.# -A& =,02bi
M;i .
702! '1KOFOU1
OMI-2014 i STODY
:Filch• 3-RDAAKA
cusT-omm. -.SY.,NAGAn::.-Qn*I'IT14=.A.k�*r- Raw'. . dD '804Y. OAKSORCINC.CERT*257 RE00RD-
-PROJE5CT.MMA(3ER: _> _j-_g _.e
Phone;
A & L OU�OUWR
LAB # SAMPLEi.o.
.90--,,4470 "r"'fJ W I w TP
017
fleflinquisphAd by Sampi
r'e
Relinquished by.
Relinquished by.;
SPECIAL INSTRUCTIONS:
SAMPLE
J.D. SU
SL2 NHe;N,.NC):r.W
Of •koo A00'r
.1,000 t'oor i.01V
were used.duringthe collechon of these. samples.
SAMPLE
0 OF
SAWNIPUNG
TYPE
CONTAINERS
DATE TIME
Uy 12,:.ela
'Date Time,
(il"I.-LI
,-
Reic I Wed, bk
7clw
D%te Time
Hecievedby.
Date Time
Recievedby:
ANALYSIS -REQUEST
garlic "N °����1/r-;00f
Cd Cr Ni , Pb I As. Hg 1. Se pH.
Iboor loor
.......... I .......... . ...... . . ...... . . ...
SL . afal'solids (Moisture), -'Tow IqpIdMI Nitrogen, Phosphorus, and Potassium
SL2: BasserTest SLI plus -Sulfur,, Caldiulp. -Magn661YM, Sbdium, Iron, Aluminum, Manganese, Copper and Zinc
1Nhiti3—A & L Canary— MANAGER COPY
RM, . Go.
PRESEFWW
METHOD
SHIPPED
.7ZA-11

; .� .s � :�
t .. E *
Product Code Product Name Sample Date Report Range Ratio
2170-01-LIQ-NC STANLY COUNTY UTIL., NC WEST STANLY 7/31/2014 111/2014-1213112014 0.6716
WWTP AEROBICALLY DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (3600 x 1.4600) + 100 = 52.56
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (24500 x 1.4600) _ 100 = 357.7
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (4330 x 1.4600) + 100 = 63.218
Na meq = Na mg/I + Molec.Wgt.Na = 52.56 + 23 = 2.28522
Ca meq = Ca mg/I + Molec.Wgt.Ca = 357.7 _ 20 = 17.885
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 63.218 _ 12 = 5.26817
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.28522 _ SgrRoot[0.5(17.885+5.26817)] = 0.671641
Printed: 1/26/2015
Page 1 13:22

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: BADIN
OWNER: ROBERT RIDENHOUR PERMIT #: W00005387 ANNUAL DRY TONS APPLIED: 32.84
SITE #: NC ST 00003 FIELD# : ST 00003 0003 OPERATOR: ROBERT RIDENHOUR CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 24.10 ACRES PERMITTED: 24.10
Page: 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
9/10/14
49,600.00 (G)
2058.091
1.46
0.125
SCUWSAE
MOIST
0-<I/2"
SUR
0.5
0.30
47,300. p
4,790.00 p
9,040.00 p
24188
I FESCUE
9/11/14
124,000.00 (G)
5145.228
1.46
0.313
SCUWSAE
MOIST
0-<I/2"
SUR
0.5
0.30
47,300. p
4,790.00 p
9,040.00 p
24188
FESCUE
9/12/14
80,600.00 (G)
3344.398
1.46
0.204
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0:30
47,300. p
4,790.00 p
9,040.00 p
24188
FESCUE
Sep-14
254,200.00 (G)
10,547.717
10/2/14
124,000.00 (G)
5145.228
1.46
0.313
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
47,300. p
4,790.00 p
9,040.00 p
24188
I FESCUE
10/3/14
74,400.00 (G)
3087.137
1.46
0.188
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
47,300. p
4,790.00 p
9,040.00 p
24188
I FESCUE
10/6/14
86,800.00 (G)
3601.660
1.46
0.219
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
47,300. p
4,790.00 p
9,040.00 p
24188
FESCUE
Oct-14
285,200.00 (G)
11,834.025
Total Gallons/Ac: 22,381.74
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
66
Annual lbs/acre
0.019
0.005
0.131
1.006
0.076
0.004
'.0.:046
0.082
0.022
2.314 -
51.73
Cumulative lbs/acre
0.052
1 0.024
0.476
1 4.773
1 0.382
0.012
0.170
0.303
0.069
11.529
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
163
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROBICALLY DIGESTED LIQU11
X 0 _0 1 c `j r
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
r. Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

3UN:47"I
��
August 12, 2014
Drew Culp
Synagro, NC 28134
12701 Lancaster Hwy
Pineville, NC 28134
TEL: [phone]
FAX: [phone]
RE: Oakboro WWTP
Dear Drew Culp:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.• [phone]
Website: httu://ivwtv.settek.corn
Order No.: 14080126
Summit Enviromnental Technologies, fiic. received 1 sample(s) on 8/1/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank)
3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099,
New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma
9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5,
Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West
Virginia 248 and 9957C and E87688, Wisconsin 399013010
Page 1 of 10

� _ i t 1 Sununit Enrironmental Technologies, Inc. Workordej^
3310 Win St.J� l " Sample SSumm
ary OVAL .,NMI Cuyahoga Falls, Ohio 44223
.4',rafy foal tl borail rl�,,� TEL: [phone] FAX. [phone] WO#: 14080126
Website: hho:/Aviviv.senekcoin 12 Aug-14
CLIENT: Synagro, NC 28134
Project: Oakboro WWTP
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
14080126-001 Oakboro (50-2170) 2014
7/31/2014 8:45:00 AM 8/l/2014 9:50:00 AM Non -Potable
Water
Page 2 of 10

ice% —t Summit Environmental Technologies, Inc. Case Narrafive
3310 Win St.
ENIVIn(MMEN AL 12C1ir'0LGG1 5, ;itq_ Cuyahoga Falls, Ohio 44223 WO#: 14080126
r1r�f;:ticai f;;ai or'��ok'1t=rt TEL: [phone] FAX.- [phone]
Website: h�://iviviv.settekconr Date: 8/12/2014
CLIENT: Synagro, NC 28134
Project: Oakboro WWTP
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports•and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 10

Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
14080126
Cc'JIROhIGTEt•1fJiL7'�CS �`:r3,Lc7� i^t
Cuyahoga Falls, Ohio44223
Date Reported:
8/12/2014
__!
traiyln,ai L .at�fo+;4:
TEL: [phone] FAX.- [phone]
Company:
Synagro, NC 28134
A'ebsite: httw1Avwiv.settekcom
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received: 8/1/2014
Project#: Oakboro WWTP
TCLP Metals Analysis (6010)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Oakboro (50-2170)
001
7/31/2014 TCLP Arsenic(As)
0.50
ND mg/L
Non-
EPA 6010 C
1
5.0
8/5/2014
WK
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 TCLP Ba6um(Ba)
5.0
ND mg/L
Non-
EPA 6010 C
1
100
8/5/2014
WK
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 TCLP Cadmium(Cd)
0.10
ND mg/L
Non-
EPA 6010 C
1
1.0
8/5/2014
WK
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 TCLP Chromium(Cr)
0.20
ND mg/L
Non-
EPA 6010 C
1
5.0
8/5/2014
WK
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 TCLP Lead(Pb)
0.50
ND mg/L
Non-
EPA 6010 C
1
5.0
8/5/2014
WK
2014
Potable
Water
�akboro (50-2170)
001
7/31/2014 TCLP Selenium(Se)
0.50
ND mg/L
Non-
EPA 6010 C
1
1.0
8/5/2014
WK
D14
Potable
Water
Oakboro (50-2170)
001
7/31/2014 TCLP Silver(Ag)
0.50
ND mg/L
Non-
EPA 6010 C
1
5.0
8/5/2014
WK
2014
Potable
Water
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Oakboro (50-2170) 001 7/31/2014 TCLP Mercury 0.0020 ND mg/L Non- EPA 7470 A 1 0.20 8/5/2014 ALJ
2014 Potable
Water
Page 4 of 10

F `
j 1 � t a
�J-
Summit Em,ironn:ental'Techrsologies, Inc.
3310 l3�in St.
WO#:
14050126
4
Fi'S'dl RotlPalEhlP tL T'cCi rdrj LOG.=
,9i1
Cuyahoga Falls, Ohio 44223
Date Reported:
8/12/2014
If
)hJf
�iralyt^ i t:=ac,alan =s
TEL: [phone] FAX. • [phone]
Company:
Synagro, NC 28134
Wehsite: httn://ivivrv.settek.com
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
8/1/2014
Project#:
Oakboro WWTP
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DI♦
RegLVI
Run
Analyst
Oakboro (50-2170)
001
7/31/2014 Chlordane, total
0.010
ND mg/L
Non-
EPA 8081 B
1
0.030
8/6/2014
JBN
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Toxaphene
0.10
ND mg/L
Non-
EPA 8081 B
1
0.50
8/6/2014
JBN
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Endrin
0.0020
ND mg/L
Non-
EPA 8081 B
1
0.020
8/6/2014
JBN
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 gamma-BHC
0.0020
ND mg/L
Non-
EPA 8081 B
1
0.40
8/6/2014
JBN
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Heptachlor
0.0020
ND mg/L
Non-
EPA 8081 B
1
0.0080
8/6/2014
JBN
2014
Potable
Water
akboro (50-2170)
001
7/31/2014 Heptachlor epoxide
0.0020
ND mg/L
Non-
EPA 8081 B
1
0.0080
8/6/2014
JBN
)14
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Methoxychlor
0.0020
ND mg/L
Non-
EPA 8081 B
1
10
8/6/2014
JBN
2014
Potable
Water
Page 5 of 10

JG
%
f , -� ' J�
i I• I j���%
Summit Envi/'olimerltal Technologies, Inc.
3310 Win St.
WO#:
14080126
Is
�.�il�. t J L !
Date Reported:
8/12/2014
t=NVIR0HMEh11'itL;IecY.nr1L0G1 tilt';
Cuyahoga Falls, Ohio44223
(_;--
rstyt.,cof La_barai* e:-!
TEL: [phone] FAX. • [phone]
Company:
Synagro, NC 28134
Website: httD://iviviv.settek.eorn
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
8/1/2014
Project#:
Oakboro WWTP
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyse
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Oakboro (50-2170)
001
7/31/2014 1,1-Dichloroethene
0.10
ND mg/L
Non-
EPA 8260 B
1
0.70
8/5/2014
MES
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 1,2-Dichloroethane
0.10
ND mg/L
Non-
EPA 8260 B
1
0.50
8/5/2014
MES
2014
Potable
Watery ,
Oakboro (50-2170)
001
7/31/2014 Benzene
0.10
ND mg/L
Non-
EPA 8260 B
1
0.50
8/5/2014
MES
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Carbon tetrachloride
0.10
ND mg/L
Non-
EPA 8260 B
1
0.50
8/5/2014
MES
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Chlorobenzene
0.10
ND mg/L
Non-
EPA 8260 B
1
100
8/5/2014
MES
2014
Potable
Water
akboro (50-2170)
001
7/31/2014 Chloroform
0.10
ND mg/L
Non-
EPA 8260 B
1
6.0
8/5/2014
MES
)14
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Tetrachloroethene
0.10
ND mg/L
Non-
EPA 8260 B
1
0.70
8/5/2014
MES
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Trichloroethene
0.10
ND mg/L
Non-
EPA 8260 B
1
0.50
8/5/2014
MES
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Vinyl chloride
0.20
ND mg/L
Non-
EPA 8260 B
1
0.20
8/5/2014
MES
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 MEK
2.0
ND mg/L
Non-
EPA 8260 B
1
200
8/5/2014
MES
2014
Potable
Water
Page 6 of 10

Summit Environmental Technologies, Inc.
3310 IVin St.
WO#:
14080126
e r;'dlnr�hUd EhJfALI Y+''�3Lci c,.3CdG Cuyahoga Falls, Ohio 44223
Date Reported:
8/12/2014
AnSi fi-rr-1 b.-borahvies
TEL: [phone] FAX: [phone]
Company:
Synagro, NC 28134
Website: htto://wwrv.setmkcon:
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
8/1/2014
Project#:
Oakboro WWTP
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte Rep Lmt Result Units
Matrix
Method DF RegLvl Run Analyst
Oakboro (50-2170)
001
7/31/2014 1,4-Dichlorobenzene
0.10
ND mg/L
Non-
EPA 8270 C
1
7.5
8/8/2014
AKE
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 2,4,5-Trichlorophenol
0.25
ND mg/L
Non-
EPA 8270 C
1
400
8/8/2014
AKE
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 2,4,6-Trichlorophenol
0.25
ND mg/L
Non-
EPA 8270 C
1
2.0
8/8/2014
AKE
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 2,4-Dinitrotoluene
0.10
ND mg/L
Non-
EPA 8270 C
1
0.13
8/8/2014
AKE
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Cresols, Total
5.0
ND mg/L
Non-
EPA 8270 C
1
200
8/8/2014
AKE
2014
Potable
Water
akboro (50-2170)
001
7/31/2014 Hexachloro-1,3-
0.10
ND mg/L
Non-
EPA 8270 C
1
0.50
8/8/2014
AKE
)14
butadiene
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Hexachlorobenzene
0.10
ND mg/L
Non-
EPA 8270 C
1
0.13
8/8/2014
AKE
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Hexachloroethane
0.10
ND mg/L
Non-
EPA 8270 C
1
3.0
8/8/2014
AKE
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Nitrobenzene
0.10
ND mg/L
Non-
EPA 8270 C
1
2.0
8/8/2014
AKE
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Pentachlorophenol
0.25
ND mg/L
Non-
EPA 8270 C
1
100
8/8/2014
AKE
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 Pyridine
0.25
ND mg/L
Non-
EPA 8270 C
1
5.0
8/8/2014
AKE
2014
Potable
Water
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lint Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Oakboro (50-2170)
001
7/31/2014 2,4-D
5.0
ND mg/L
Non-
EPA 8321 A
1
10
8/6/2014
AMZ
2014
Potable
Water
Oakboro (50-2170)
001
7/31/2014 2,4,5-TP
0.50
ND mg/L
Non-
EPA 8321 A
1
1.0
8/6/2014
AMZ
2014
Potable
Water
Page 7 of 10

Summit Environmental Technologies, Inc.
�"
3310 Win St.
WO#: 14080126
'
LJ
Date Reported: 8/12/2014
ti
F�:'dlr2t�hlFiSc,l�i?L3_�S'C�7LQC,t ,i•.�:
C aho a Falls, Ohio 44223
uJ g
_�_,
arrr r�iiraf 1 s? a �iorts. TEL: [phone] FAX. [phone]
Company: Synagro, NC 28134
Website: httn:/Aviviv.settek.com
Address: 12701 Lancaster Hwy
Pineville NC 28134
Received: 8/1/2014
Project#: Oakboro WWTP
Client ID# Lab ID# Collected Analyte
Result Units
Matrix Method DT RL
Run Analyst
Oakboro (50-2170) 001 7/31/2014 Flashpoint (200T)
>200 T
Non- EPA 1010 1
8/5/2014 TAH
2014
Potable
Water
Oakboro (50-2170) 001 7/31/2014 Cyanide, Reactive
ND ppm
Non- EPA 9014 1 0.50
8/4/2014 TIR
2014
Potable
Water
Oakboro (50-2170) 001 7/31/2014 pH
' ` 5.2 pH Units Non- SM 4500 1 0
8/4/2014 AYS
2014
Potable H+B
Water
Oakboro (50-2170) 001 7/31/2014 Sulfide, Reactive
ND ppm
Non- EPA 9034 1 25
8/4/2014 TIR
2014
Potable
Water
Page 8 of 10

Analysi's Request / Chain of Custody
rj E NVIRONNIUNTAL *1 ECHNOLOGIr-S. INC.
:13 10 Win Strew For SwrimR,Environmental Technologies, Inc. use only
CUY01,00a Faks. OhIG4,122.3
eoc-va-ol :a
Page
—:prCkjCCT lVDIIIII[calioof SET No.-
C!iIz,11 �Niww ll
Synagro Central 04 1/-13 0 /1-0 w W—Tr Anal.}U'C"al Para -meters
C-'FLutAudrtcti'and ,.Method
12701,Lancaster Hwy Pineville NIC, 28134 70
Client 111101IL: TTI- T-11
II
704-752-8673 lz F- W Llnt,t
Client j to Rcccivu Rcmills by. Fax 110 Numlicr
704-752-8736
Contact Florsuit C. Quoic Numbur
S,-j(nl)lcd By
if Ohio-VAP Samplias
Sa,iilAeldentificalioll
67131 /J
x
Votes
Reffillitfished by:- Date Thne I R i�, I it I
it
(2
12
'eceived in L 1) by:
Date
Time
Rush Requestic!d:
be,"riproved by LzIbilvingiagel-
1,1V
-J— I
Page 1 of 2

r
Rev. 12 C11
Date: 07/27/13
ttt
SurnmN Environmental TCchl'1010gies, ritc,
C©Oler Receipt Forma f
fnitiats of person inspecting cooler and samples:_ i
OrderNumber;
Date Received:_ Time Rece4eed� U _ pate cao)er[s) opened and �4
samples Inspected; U ��•-{�
Number Co" er
s fie.
r WA
Shipper; / ED UPS
bHL Airborne rS Postal VLlattS-in Plckup Other:
PaC§agirSg:
Peanut��_u6'
bbieVJrap Paper Foam Iqone ether:
I- pe on cooleribox;
Y NI
�.-�
iV;A
Custody Seals Intact
fJ
rr
C-O-C in plastic
Gr' r�
Ice- Blue ice
present ! - sent' / malted`
NIA,
/
Sample Temperature IP, Gun #1 020�59 CFi �` ^C =C
N/A
Radipioglcai Testing Instrument
serial t#'SJ 127 Y N
. ^ 1
(see page 2 fat scan'resultsj
"Use i sheet per'sample for
Immediately.
Radiological Testing. if sample is HOT, uiQ Radiological
Safety Officer must be notified
C-O-C filled out properly
,
N
N/A
Samples in separate bags
'
N
NIA
Sample containers intact`
N
C j
NIA
-If no, list brok-en samale,$):
Sample labei(s) complete (ID, date, eic.)
`�� N
NIA
Label(s) agree with C-O-C
f hf
NIA
Collect containers used
N
NIA
Sufficient sample received
N
N/A
Subbles absent from 40 mL vials"
Y NC-1JiA
I
"Samples with bubbles <6mm are acceptable.
Indicate bubble size if >6mm.
Was dent contacted about samples
Y N
Will cti=_nt send new samples
Y N
Client contact
Lodged in
Comment
GAQC SNARED\Document Control Templates - Tracking',Cooler receipt f-s" Rev. 12 07-27.13.doc gaga 1 of 2
Paige 10 of 10

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Oakboro WQ Permit Number: WQ0005387
WWTP Name: Town ofOakboro WWTP NPI3ES Number: NCO043532
Monitoring Period: From 07/31/14 To 12/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2/B (AlkTreatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ' Air Drying Composting Aerobic Digestion
Anaerobic Digestion
-A /d'•1...... A -- d-1-- M tl.n Fnlln n mnni4n rena rlafa•
Parameter
Allowable level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x 10 to the 6'
Coliform
power per gram
MPN
109,650.57
125,852
135,075.94
MPN/g
0
Annual
grab
SM 9221E
of total solids
CFU
CFU/g
0
annual
grab
9222D
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu offeeal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. I
Option/Alt.2
Option/Alt. 3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt_ 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
Phis determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Jim Amaral, WWTP O oro
parer ame a {type or pr' it) Land Applier Name and Title (if applicable) (type or print)
of Preparers ate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1 102 (26)

PRONIPT. A CC U RATE -RE LIABLE
I tAB0RATORII;S, INC
N'\ WAIARLABS.C'0\i
RtEPORT OF AtiAT.YSE:S
ALIri: DREDJ CULT'
SYNAGRO
12701 LANCASL'ER HWY
PINEVILA.,E, NC 28134-
PROJECT NAME: LlUL, '14
DATE: 08/29/14
SA14PLE NUMBER-
115.139
SAMPLE ID- 0AM30RO
50-2170 2014
SAMPLE t4A`CRIX- SO
DATE SAMP1.1VID-
07/31 / 1 a
TIME SAMPLED- 0830
DATE RECEIVED-
0 7/31 / 14
SAMPLER- DC
RECEIVED BY-- Di
TIME REC;r.IVED-
1255
DELIVEREDBY- DC'
TYPE SAMPLE- Grab
Page 1 of I
ANALYSIS
ANALYSTS
METHOD
DA'L'L: 'DIME BY
RESULT UNITS
FECAL. COLIFORM (GEOM. MlEAN) SM 9221 E
08/01 / 14 1020 RE
1 25, 852. MPN/g
L.AF3ORA'i'OR`! DIRECTOR
lwa-
1�(). 13m-111-W3, - C'h.ulutte, NC 353.11-1483
Phone: (70-1) 58ti-8333 • I'ux: (704) )588-8335
f'I'A,. iil:pi Y;.„)If `.i ��Y:/•�iiji;jji(/!1

PROMPT- Ar-66RATE- RELIAEILE
LA]3i7INC,
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
!�[hIa!►'1e��`' a
{11i'
t07/31/14
SYNAGRO
OAKBORO 50-2170 2014
FECAL COLIFORM, GEOMETRIC MEAN
SM 9221 E
155139
2.19%
133,801.82
1
2,930
2
3,093
2.29%
135,075.94
3
2,819
2.33%
121,006.13
4
3,105
2.34%
132,674.90
5
2,882
2.28%
126,411.26
6
2,785
2.240%
124,331.02
7
2,533
2.31%
109,650.57

PAR
LABORATORIES INC.
www.par/abs.com
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
GNAW OF CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Mailing:
PO Box 411483
Charlotte, NC 28241.1483
It is essential that all Information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc, and the North
Company Name (billing) Comments/ Special Instructions
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State Et zip code
PINEVILLE NC 28134
Point of Contact It Telephone Number
PR-GW CUL10 70y- 57y-sz7l
Taken By: SIGNATURE
r"1\II1 1 LV IYHwyl"
ARE SAMO ES FOR STATE or EPA REPORTING? YES _x NO
*Sample Type: DW Ww GWMW HW Soil Other Bivso
Sample Temp at time of sampling: a C Sample Temp upon receipt: _ ° C
*Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes _No u n/a
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN):
Client Sample I.O. _
(Sample Location I Number)
Comp
Grab
Preserv.
Set
Dateffime
Collection
Dateffime
nalyses
Requested
61+1C400 a o y
5o - 9.1'70
07 3I IY
�'30
FSy cA-1- &Fvtem
RqQnquished by: DaterTime Received y uarer l rme
_ r
11 )J! K. L/ L ZLi�U lLl !. / Z S S
mquished by: Daiern e� Received by: I Dateffime
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste "See
Other Side

Aft
- 'm
PL mk- FZ
PROM PT•ACCU RATE- RE L I A BLE
LABORATORIES, INC
REPORT OF ANALYSES
Attn: DREW CULP
SYNAGRO PROJECT NAME: JUL 14
12701 LANCASTER HWY DATE: 08/29/14
PINEVILLE, NC 28134-
SAMPLE NUMBER- 1I5138 SAMPLE ID- OAR_30RO 50-2170 20.14_
DATE SAlviPLED- 07/31 /14
DATE RECEIVED- 07/31/14 SAMPLER-- DC
TIME RECEIVED- 1255 DELIVERED BY- DC
Page 1 of 1
ANALYSIS
30 DAY BENCH SCALE `PEST
SAMPLE MATRIX- SO
TIME SAMPLED- 0830
RECEIVED BY- DJ
TYPE SAMPLE- Grab
ANALYSIS .
METHOD DATE TIME BY RESULT UNITS
VAR 08/01/14 RE ATTACHED
LAI30I:ATORY DIRECTOR
P.O. Box 411453 ^ Charlotte. NC 28241-1483
Phow: (70.1) 533-8333 • Fax: [phone]

Am
P./Z-X R
PROM PT•ACCURATE- RELIABLE_
1-AFC)r riTORIES, ZNC
WWW.PARLABS.COM
30 ®ay Bench Scale_ Extended Aeration Test
Percent Volatile Solids reduction
r
SYNAGRO
OAKBORO 50-2170 2014
115138
08101 /14
08/29114
Start: End:
TS
0.2243
0.2251
TS%
1.47%
1.47%
VS
0.1442
0.1430
VS%
64.29%
63.53%
yIN
0.00332
yOUT
0.00339959
FSVR (Mass Balance)
-2.41 %
FSVR (Van Kleeck)
3.25%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
l .O. Bo,c=111483 m Charlotte, NC 28241-1433
Phone: [phone] e Fax: [phone]

�A
MSCRATCRIES, INC.
wwwpariabs.com
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN N OF CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Carolina Deoartment of Environmental and Natural Resources.
Company Name (billing)
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State & zip code
PINEVILLE NC 28134
Point of Contact a Telephone Number
PRE Cut-P. 74,q- 57Y- X27/
Taken By: SIGNATURE
Comments/ Special Instructions
b,e, d;A,
PRINTED NAME
I ARE SAMPLES FOR STATE or EPA REPORTING? YES X NO
*Sample Type: DW WW GWMW HW Soil other 4cos-I.'
Sample Temp at time of sampling: ° C Sample Temp upon receipt: J ° C
"-ield Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
:sidual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN):
Client Sample I.D.
(Sample Location / Number)
Camp
Grab
Preserv.
Set Up
Date/time
Collection
Datefrime
nalyses
Requested
I
rqursnea py: ua[e/ r rme tteceivea y Dateffime
quished by: Datefriniie Received by: ( DaterTime
` C=Composite G=Grab DW=Drinking VVaterWW=UVastewater G�VNIW=Groundwater Monitoring Well HW=Hazardous Waste "See
Other Side

Liming was not necessary, as the field pH value was 6.0 or greater.

Page 1 of 1
Report Number: 14-336-0609
�
Account Number: 46477
R
aleasterll.com
Send To: SYNAGRO CENTRAL LLC/OAKBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
n-f- De.-oc—A- 1')10"W'�-r11A n.tn of -i9msr9n1A
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower:
ROBERT RIDENHOUR
NC-ST-03
OAKBORO 50-2170
SOIL ANALYSIS REPORT
nnte Of Renort 12/03/2014
Submitted By: DREW CULP
Farm ID:
Analytical Method(s):
Mehlich 3
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
% Rate Ibs/A
ppm
Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
P H'
Index
meq/100g
meq/100g
3
03827
5.1 H 141
33
M
53 VL
266 VH
986 M
6.5
0.6
7.9
NC=27
NC=27
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
Field ID
%
6/0
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
3
1.7
28.1
62.4
7.4
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil, Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: �aµlic me 60w�
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc, v
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

I
�a-C�l�%E®
'9!V!SlON OF 11VATEq QUALITY
FEB 2 4 20114
-11" ,.c �.Tauv
MOOE:ESi1.LL;� 4�a=CiO AL OFFISE
CITY OF STATESVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0016247
2013 ANNUAL REPORT

City of Statesville, NC
Residuals Land Application Program
2013 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and Land
Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR
Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

:-��-1W .41,LA.ND PzP-L[CO.TION CERTIFICATION FORM
WQ Permit #: W00016247 County Iredell Year 2013
Facility Name (as shown on permit) City of Statesville, Third Creek WWTP & Fourth Creek WWTP
NPDES No. NCO020591 & NCO031836
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part Band proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summ
Total number of application fields in the permit: 31
Total number of fields utilized for land application during the year: 7
Total amount of dry tons applied during the year for all application sites: 456.91
Total number of acres utilized for land application during the year: 158.2
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2013 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil ,pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. ]
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." ��qq
Todd Larson, Operations Director
Pe ittee me and itle (tyke or rrit) SignatVre of Permittee Date
—
JhWW 1�k
7J
Signature of P eparer* Date
(if different fr&n Permittee)
Signature of Land Applier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2013 ANNUAL OPERATIOINS -SUM MARY v LAND APPLICATION
STATESVILLE, NC
STATESVILLE, NC FOURTH CREEK CAKE
MONTHNEAR
April 2013
May 2013
November 2013
December 2013
YEARLY TOTAL
AMOUNT UNIT
1,184.00
Y
448.00
Y
820.00
Y
320.00
Y
2,772.00
Y
STATESVILLE, NC THIRD CREEK CAKE
MONTHNEAR
April 2013
YEARLY TOTAL
AMOUNT UNIT
1,088.00 Y
1,088.00 Y
DRY TONS
UNIT
141.40
D
53.50
D
100.08
D
39.05
D
334.03
D
DRY TONS UNIT
122.88 D
122.88 D
DRY METRIC
TONS
128.26
48.53
90.77
35.42.
302.98
DRY METRIC
TONS
111.45
111.45
0
1/22/2014

2013 ANNUAL REPORT
PROJECT:
FACILITY:
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
City of Statesville, NC
Third Creek WWTP
NCO020591
Todd Norman, Residuals
Superintendent
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Todd Norman, Third Creek WWTP Supt.
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

2013 ANNUAL REPORT
PROJECT:
FACILITY:
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
City of Statesville, NC
Fourth Creek WWTP
NC0031836
Andy Smith, Residuals Superintendent
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Andy Smith, Fourth Creek WWTP Supt.
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Laboratory
Facility Name: STATESVILLE, NC
A&L EASTERN LABORATORIES, INC.
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type CAK
CAI{ CAK CAR
Date Sampled (grab) or 01/10/13
04/24/13 08/22/13 11/20/13
Date Composited
Percent Solids 18.92
14.18 16.54 14.49
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
4
3
5
5
3
3
3
3
1.9
1.7
1.2
1.9
45
39
50
39
435
338
356
325
32
25
27
26
12
12
12
9
29
27
33
30
<5
<5
<5
<5
745
614
499
573
26300
23300
25000
22500
51800
66400
52800
55400
6340
10400
9370
8140
19.6
<2
23
32.4
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant,pen* ies for submitting false Oformation, including the possibility of fines and imprisonment for knowing violations."
X
Date C�` J (
DENR FORM RSSF (5/2003) Printed: Wednesday - January 22, 2014 at 14:44:52 for: 2084 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type CAK CAK CAK
Date Sampled (grab) or 01/10/13 , 04/24/13 08/22/13
Date Composited
Percent Solids 18.92 14.18 16.54
PARAMETERS (mg/kg dry weight)
Laboratory
A&L EASTERN LABORATORIES, INC.
CAK
11/20/13
14.49
Aluminum
21300
17900
26400
28000
Calcium
12700
12400
14200
18500
Magnesium
2820
3060
2180
2430
pH
6.65
6.04
6.96
7.84
Potassium
3210
3350
2540
2470
Sodium
717
917
804
783
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significanpenties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date
(SIGNATURE F PREPARER)
NR - Data Not ported or Data Not Required
DENR FORM RSSF-B (712002) Printed: Wednesday - January 22 2014 at 14:45:18 for: 2084 01

Page: l of 2
Report Number: 13-011-0213
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 91287
Sample Id : STATESVILLE 4TH
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (8p4) 743-9401 Fax [phone]
wwwaleastem.com
Project: STATESVILLE 4TH
NC CERT #257
REPORT" OF ANALYSIS Date Sampled: 1/10/2013 09:45:00
Date Received: 01/11/2013 00:00
Date Reported: 01/17/2013
Total Solids *
18.92
189200
100.0
KM
01/11/2013 14:44
SM-2540G
Moisture *
81.08
100.0
KM
01/11/2013 14:44
SM-2540G
Total Kjeldahl Nitrogen
5.18
51800
10.0
JM
01/14/2013 09:29
SM-4500-NH3C-TKN
Total Phosphorus
2.63
26300
100
KM
01/14/2013 12:21
SW 6010C
Total Potassium
0.32
3210
100
KM
01/14/2013 12:21
SW 6010C
Total Sulfur
0.94
9360
100
KM
01/14/2013 12:21
SW 6010C
Total Calcium
1.27
12700
100
KM
01/14/2013 12:21
SW 6010C
Total Magnesium
0.28
2820
100
KM
01/14/2013 12:21
SW 6010C
Total Sodium
0.07
717
100
KM
01/14/2013 12:21
SW 6010C
Total Iron
24000
100
KM
01/14/2013 12:21
SW 6010C
Total Aluminum
21300
100
KM
01/14/2013 12:21
SW 6010C
Total Manganese
1750
5
KM
01/14/2013 12:21
SW 6010C
Total Copper
435
5
KM
01/14/2013 12:21
SW 6010C
Total Zinc
745
5
KM
01/14/2013 12:21
SW 6010C
Ammonia Nitrogen
0.63
6340
10.0
JM
01/14/2013 09:29
SM-4500-NH3C
Organic N
4.55
45460
10.0
01/14/2013 09:29
CALCULATION
Nitrate+Nitrite-N
19.6
2.00
JM
01/14/201311:25
SM-450ONO3F
Total Cadmium
3.0
2.0 .
KM
01/14/2013 12:21
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
i&u
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , A
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
I

Page: 2 of 2
Report Number: 13-011-0213
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 91287
Sample Id : STATESVILLE 4TH
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-940t Fax (804) 271,6446
wwwaleastern.cam
Project: STATESVILLE 4TH
NC CERT #257
REPORT OF ANALYSIS Date Sampled: 1/10/2013 09:45:00
Date Received: 01/11/2013 00:00
Date Reported: 01/17/2013
Total Chromium
45
5
KM
01/14/2013 12:21
SW 6010C
Total Nickel
29,
5
KM
01/14/2013 12:21
SW 6010C
Total Lead
32
5
KM
01/14/2013 12:21
SW 6010C
Total Arsenic
4.0
3.0
KM
01/14/2013 12:21
SW 6010C
Total Mercury
1.9
0.4
KM
01/14/2013 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
01/14/2013 12:21
SW 6010C
pH (Standard Units) *
6.65
2.00
JM
01/14/2013 08:05
SW-9045D
Total Molybdenum
12
5
KM
01/14/2013 12:21
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "P". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining our, prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 1/10/2013 1/112013-3/31/2013 0.6501
Na mg/I = (Na mg/kg x % Solids) + 100 = (717 x 18.9200) + 100 = 135.656
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (12700 x 18.9200) = 100 = 2402.84
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2820 x 18.9200) + 100 = 533.544
Na meq = Na mg/I + Molec.Wgt.Na = 135.656 + 23 = 5.8981
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2402.84 + 20 = 120.142
Mg meq = Mg mg/I + Molec.Wgt.Mg = 533.544 + 12 = 44.462
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.8981 + SgrRoot[0.5(120.142+44.462)] = 0.650141
Printed: 1/22/2014
Page 1 15:16

Page: 1 of 2
Report Number: 13-116-0206
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 93319
Sample Id : STATESVILLE 4TH CK
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Yir&W 23237 [phone] Fax (804) 771.W6
www.aleastem.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/24/2013 13:45:00
Date Received: 04/26/2013 00:00
Date Reported: 05/02/2013
Total Solids *
14.18
141800
100.0
MW
04/29/2013 08:24
SM-2540G
Moisture *
85.82
100.0
MW
04/29/2013 08:24
SM-2540G
Total Kjeldahl Nitrogen
6.64
66400
10.0
JM
04/29/2013 08:39
SM-4500-NH3C-TKN
Total Phosphorus
2.33
23300
100
KM
04/29/2013 13:56
SW 6010C
Total Potassium
0.34
3350
100
KM
04/29/2013 13:56
SW 6010C
Total Sulfur
0.89
8850
100
KM
04/29/2013 13:56
SW 6010C
Total Calcium
1.24
12400
100
KM
04/29/2013 13:56
SW 6010C
Total Magnesium
0.31
3060
1.00
KM
04/29/2013 13:56
SW 6010C
Total Sodium
0.09
917
100
KM
04/29/2013 13:56
SW 6010C
Total Iron
18900
100
KM
04/29/2013 13:56
SW 6010C
Total Aluminum
17900
100
KM
04/29/2013 13:56
SW 6010C
Total Manganese
1450
5
KM
04/29/2013 13:56
SW 6010C
Total Copper
338
5
KM
04/29/2013 13:56
SW 6010C
Total Zinc
614
5
KM
04/29/2013 13:56
SW 6010C
Ammonia Nitrogen
1.04
10400
10.0
JM
04/29/2013 08:39
SM-4500-NH3C
Organic N
5.60
56000
10.0
04/29/2013 08:39
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
04/29/2013 08:30
SM-450ONO3F
Total Cadmium
3.0
2.0
KM
04/29/2013 13:56
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 13-116-0206
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 93319
Sample Id : STATESVILLE 4TH CK
�L AFL Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Vlrginia.23237 [phone] Fax [phone]
www.aleastern.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/24/2013 13:45:00
Date Received: 04/26/2013 00:00
Date Reported: 05/02/201'3
Total Chromium
39
5
KM
04/29/2013 13:56
SW 6010C
Total Nickel
27
5
KM
04/29/2013 13:56
SW 6010C
Total Lead
25
5
KM
04/29/2013 13:56
SW 6010C
Total Arsenic
3.0
3.0
KM
04/29/2013 13:56
SW 6010C
Total Mercury
1.7
0.4
KM
04/30/2013 08:05
SW-7471 B
Total Selenium
<5.0
5.0
KM
04/29/2013 13:56
SW 6010C
pH (Standard Units) *
6.04
2.00
JM
04/29/2013 08:30
SW-9045D
Total Molybdenum
12
5
KM
04/29/2013 13:56
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR) - -
Product Code Product Name Sample Date ReportRange Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 4/24/2013 4/1/2013-6/30/2013 0.7178
Na mg/I = (Na mg/kg x % Solids) =100 = (917 x 14.1800) =100 = 130.031
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (12400 x 14.1800) =100 = 1758.32
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3060 x 14.1800) = 100 = 433.908
Na meq-= Na mg/I _ Molec.Wgt.Na = 130.031 = 23 = 5.6535
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 1758.32 _ 20 = 87.916
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 433.908 + 12 = 36.159
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.6535 + SgrRoot[0.5(87.916+36.159)] = 0.717779
Printed: 1 /22/2014
Page 1 15:17

Page: 1 of 2
Report Number: 13-235-0209
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 95163
Sample Id : STATESVILLE 4TH CK
�L A&L Eastern Laboratories, Inc:
7621 Whitepine Road Richmond, Virginia.23237 [phone] Fax [phone]
wwwaleastern.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 8/22/2013 10:45:00
Date Received: 08/23/2013 00:00
Date Reported: 08/28/2013
Total Solids *
16.54
165400
100.0
JM
08/23/2013 14:15
SM-2540G
Moisture *
83.46
100.0
JM
08/23/2013 14:15
SM-2540G
Total Kjeldahl Nitrogen
5.28
52800
10.0
JM
08/26/2013 08:10
SM-4500-NH3C-TKN
Total Phosphorus
2.50
25000
100
KM
08/26/2013 14:21
SW 6010C
Total Potassium
0.25
2540
100
KM
08/26/2013 14:21
SW 6010C
Total Sulfur
0.91
9100
100
KM
08/26/2013 14:21
SW 6010C
Total Calcium
1.42
14200
100
KM
08/26/2013 14:21
SW 6010C
Total Magnesium
0.22
2180
100
KM
08/26/2013 14:21
SIN 6010C
Total Sodium
0.08
804
100
KM
08/26/2013 14:21
SW 6010C
Total Iron
25200
100
KM
08/26/2013 14:21
SW 6010C
Total Aluminum
26400
100
KM
08/26/2013 14:21
SW 6010C
Total Manganese
953
5
KM
08/26/2013 14:21
SW 6010C
Total Copper
356
5
KM
08/26/2013 14:21
SW 6010C
Total Zinc
499
5
KM
08/26/2013 14:21
SW 6010C
Ammonia Nitrogen
0.94
9370
10.0
JM
08/26/2013 08:10
SM-4500-NH3C
Organic N
4.34
43430
10.0
08/26/2013 08:10
CALCULATION
Nitrate+Nitrite-N
23.0
2.00
JM
08/26/2013 08:10
SM-450ONO3F
Total Cadmium
3.0
2.0
KM
08/26/2013 14:21
SW 6010C
AII'values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made A&U8�
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 13-235-0209
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 95163
Sample ld : STATESVILLE 4TH CK
@P.
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 8/22/2013 10:45:00
Date Received: 08/23/2013 00:00
Date Reported: 08/28/2013
Total Chromium
50
5
KM
08/26/2013 14:21
SW 6010C
Total Nickel
33
5
KM
08/26/2013 14:21
SW 6010C
Total Lead
27
5
KM
08/26/2Q13 14:21
SW 6010C
Total Arsenic
5.0
3.0
KM
08/26/2013 14:21
SW 6010C
Total Mercury
1.2
0.4
KM
08/26/2013 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
08/26/2013 14:21
SW 6010C
pH (Standard Units) *
6.96
2.00
JM
08/26/2013 08:10
SW-9045D
Total Molybdenum
12
5
KM
08/26/2013 14:21
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr" AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculate n JSAM--
Product Code Product Name Sample Date ReportRange Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 8/22/2013 911/2013-10/3112013 0.6733
Na mg/I = (Na mg/kg x % Solids) + 100 = (804 x 16.5400) + 100 = 132.982
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (14200 x 16.5400) + 100 = 2348.68
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2180 x 16.5400) + 100 = 360.572
Na meq = Na mg/I + Molec.Wgt.Na = 132.982 + 23 = 5.78181
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2348.68 + 20 = 117.434
Mg meq = Mg mg/I + Molec.Wgt.Mg = 360.572 + 12 = 30.0477.
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.78181 + SgrRoot[0.5(117.434+30.0477)] = 0.673302
Printed: 1 /22/2014
Page 1 15:17

Page: 1 of 2
Report Number: 13=325-0211
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 96706
Sample Id : STATESVILLE 4TH CK
A&L Eastern Laboratories, Inc.
7.621 Whitepine Road Richmond, Virginia 23237 (804) 743-94Q1 Fax [phone]
-www aleastern.com
Project: STATESVILLE 4TH CHECK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 11/20/2013 10:25:00
Date Received: 11/21/2013 00:00
Date Reported: 11/27/2013
Total Solids *
14.49
144900
100.0
JM
11/22/2013 09:09
SM-2540G
Moisture *
85.51
100.0
JM
11/22/2013 09:09
SM-2540G
Total Kjeldahl Nitrogen
5.54
55400
10.0
JM
11/22/2013 10:20
SM-4500-NH3C-TKN
Total Phosphorus
2.25
22500
100
KM
11/22/2013 12:11
SW 6010C
Total Potassium
0.25
2470
100
KM
11/22/2013 12:11
SW 6010C
Total Sulfur
0.84
8390
100
KM
11/22/2013 12:11
SW 6010C
Total Calcium
1.85
18500
100
KM
1.1/22/2013 12:11
SW 6010C
Total Magnesium
0.24
2430
100
KM
11/22/2013 12:11
SW 6010C
Total Sodium
0.08
783
100
KM .
11/22/2013 12:11
SW 6010C
Total Iron
24300
100
KM
11/22/2013 12:11,
SW 6010C
Total Aluminum
28000
100
KM
11/22/2013 12:11
SW 6010C
Total Manganese
1450
5
KM
11/22/2013 12:11
SW 6010C
Total Copper
325
5
KM
11/22/2013 12:11
SW 6010C
Total Zinc
573
5
KM
11/22/2013 12:11
SW 6010C
Ammonia Nitrogen
0.81
8140
10.0
JM
11/22/2013 09:00
SM-4500-NH3C
Organic N
4.73
47260
10.0
11/22/2013 09:00
CALCULATION
Nitrate+ N itrite-N
32.4
2.00
JM
11/26/201313:45
SM-450ONO3F
Total Cadmium
3.0
2.0
KM
11/22/2013 12:11
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 13-325-0211
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 96706
Sample Id : STATESVILLE 4TH CK
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-M6
www.aleastern.com
Project: STATESVILLE 4TH CHECK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 11/20/2013 10:25:00
Date Received: 11/21/2013 00:00
Date Reported: 11/27/2013
Total Chromium
39
5
KM
11/22/2013 12:11
SW 6010C
Total Nickel
30
5
KM
11/22/2013 12:11
SW 6010C
Total Lead
26
5
KM
11/22/2013 12:11
SW 6010C
Total Arsenic
5.0
3.0
KM
11/22/2013 12:11
SW 6010C
Total Mercury
1.9
0.4
KM
11/22/2013 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
11/22/2013 12:11
SW 6010C
pH (Standard Units) *
7.84
2.00
JM
11/22/2013 09:00
SW-9045D
Total Molybdenum
9
5
KM
11/22/2013 12:11
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

A-.=6 law%
SAMPLING LOGJ# 7621: Whitepid
.CUSTOMER: SYNAGRO SOUTH EAST SYNA, GMCCNTRAUE&iTATMMI 16
STAtESVILE 4tH PHEdK
PIOUECTMAN&GEW
7 1-
Phone-.
A& L CUSTOWItIR
LABI ZAMPLEILD,
SAIPLANG
LOCATION
TYPE
1# OF
CONTAINERS-
DATE TIME
ou 9,
ANALY318
.464 3
11_ 21 �-2013'
12:5214.3
METROD METHOD
PRESERVED SHIPPED
.
-n Rigoleved'byz REMARKS,
hv, Rqmnlen. Date., n1p
Titne R66evedjvyw
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Reirriqulshed,O)r.
SPECIAL INSTRW-111ONS"
v-_­ ..ifr,rlhev -M-1 frnnl.qpq*.. Pc)#_ .
'ANALYSIS REQUEST
SAMPLE
SLI'
NI
Pb
AA
HS
Se:PH
; ,
V Ili
S1011861
Mo
Cl
14o'N
loo
' PJ&
Pow
xq
LZ
SL1:'Tbtai:Sbr1d . s:!(MWqture)- Tot.3UKjdlchAh11Nj1f!(j9Bn, Phoppborus,.and Potasg!UM
SL2, Basic Test 81-1 plus SU'IW-,- - Calclum, $,adlum, [ror!., Aluminum, *LngarISSe, Dapper andZina.
. . I ; ! I
- OPY Cay)ary— MANAGER C

-Sodium Absorption Ratio Calculation (SA) --- --
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 11/20/2013 111112013-12/3112013 0.5458
Na mg/l = (Na mg/kg x % Solids) + 100 = (783 x 14.4900) =100 = 113.457
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (18500 x 14.4900) + 100 = 2680.65
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2430 x 14.4900) + 100 = 352.107
Na meq = Na mg/I + Molec.Wgt.Na = 113.457 + 23 = 4.9329
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2680.65 + 20 = 134.033
Mg meq = Mg mg/I + Molec.Wgt.Mg = 352.107 + 12 = 29.3422
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.9329 + SgrRoot[0.5(134.033+29.3422)] = 0.545789
Printed: 1 /22/2014
Page 1 15:18

ANNUAL. RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO020591
or WQ# (residual only)
WWTP Name: THIRD CREEK
Residuals Analysis Data
Product Type CAK CAK CAK
Date Sampled (grab) or 01/10/13 04/24/13 08/22/13
Date Composited
Percent Solids 14.56 13.41 13.71
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
Laboratory
A&L EASTERN LABORATORIES, INC.
CAK
11/20/13
13.65
3
3
4
4
14
13
8
4
<0.4
<0.4
0.4
1.4
89
88
98
39
416
399
418
321
115
113
98
26
20
21
20
11
47
49
53
32
5
<5
<5
<5
1240
1100
729
665
19600
20200
19500
23800
49600
51200
58800
56000
5150
8950
12400
5490
20.6
26.8
48.1
24.2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant pen"ies for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1:1
,TURE PF PREPARER)
Date C� I
DENR FORM RSSF (5/2003) Printed: Wednesday - January 22, 2014 at 14:44:58 for: 2084 02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Laboratory
Facility Name: STATESVILLE, NC
A&L EASTERN LABORATORIES, INC.
NPDES# : NCO020591
or WQ# (residual only)
WWTP Name: THIRD CREEK
Residuals Analysis Data
Product Type CAR
CAx
CAx
CAx
Date Sampled (grab) or 01/10/13
04/24/13
08/22/13
11/20/13
Date Composited
t
Percent Solids 14.56
13.41
13.71
13.65
PARAMETERS (mg/kg dry weight)
f
Aluminum 15000
16700
15900
21900
Calcium 10500
11200
18600
21800
Magnesium 2530 .
2360
2540
2890
pH 6.96
6.70
7.84
7.55
Potassium 2790
2980
2490
2670
Sodium 1910
1740
1100
790
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted.. I am aware that there are
significantAenaAes for submitting false information, including the possibility of fines and imprisonment for knowing violations."
n
(SION4TURE (PF P
NR - Data Not Reported or Data Not Required
Date �), � 1 "- f
N
DENR FORM RSSF-B (7/2002) Printed: Wednesday - January 22 2014 at 14:45:25 for: 2084 02

Page: 1 of 2
Report Number: 13-011-0212
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 91286
Sample Id : STATESVILLE 3RD
AL A-&L Eastern Laboratories, Inc.
7621.Whitepine Road Richmond, Virginia.23237 [phone] Fax (804) 271.W6
www aleastern.com
Project: STATESVILLE 3RD
NC CERT#257
REPORT OFANALYS/S
Date Sampled: 1/10/2013 09:30:00
Date Received: 01/11/2013 00:00
Date Reported: 01/17/2013
Total Solids *
14.56
145600
100.0
KM
01/11/2013 14:44
SM-2540G
Moisture *
85.44
100.0
KM
01/11/2013 14:44
SM-2540G
Total Kjeldahl Nitrogen
4.96
49600
10.0
JM
01/14/2013 09:29
SM-4500-NH3C-TKN
Total Phosphorus
1.96
19600
100
KM
01/14/2013 12:21
SW 6010C
Total Potassium
0.28
2790
100
KM
01/14/2013 12:21
SW 6010C
Total Sulfur
0.95
9540
100
KM
01/14/2013 12:21
SW 6010C
Total Calcium
1.05
10500
100
KM
01/14/2013 12:21
SW 6010C
Total Magnesium
0.25
2530
100
KM
01/14/2013 12:21
SW 6010C
Total Sodium
0.19
1910
100
KM
01/14/2013 12:21
SW 6010C
Total Iron
19600
100
KM
01/14/2013 12:21
SW 6010C
Total Aluminum
15000
100
KM
01/14/2013 12:21
SW 6010C
Total Manganese
596
5
KM
01/14/2013 12:21
SW 6010C
Total Copper
416
5
KM
01/14/2013 12:21
SW 6010C
Total Zinc
1240
5
KM
01/14/2013 12:21
SW 6010C
Ammonia Nitrogen
0.52
5150
10.0
JM
01/14/2013 09:29
SM-4500-NH3C
Organic N
4.44
44450
10.0
01/14/2013 09:29
CALCULATION
Nitrate+Nitrite-N
20.6
2.00
JM
01/14/201311:25
SM-450ONO3F
Total Cadmium
14.0
2.0
KM
01/14/2013 12:21
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 13-011-0212
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 91286
Sample Id : STATESVILLE 3RD
� L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-Ml Fax (804) 271-W6
a
www.ale-astem.com
Project: STATESVILLE 3RD
NC CERT#257
1 »:Z•]ar•]y'l�'Trfjr --FBI
Total Chromium
89
5
Total Nickel
47
5
Total Lead
115
5
Total Arsenic
3.0
3.0
Total Mercury
<0.4
0.4
Total Selenium
5.0
5.0
pH (Standard Units) * 6.96
2.00
Total Molybdenum
20
5
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "P".
ALL OTHER QC DATA IS ACCEPTABLE.
Date Sampled: 1/10/2013 09:30:00
Date Received: 01/11/2013 00:00
Date Reported: 01/17/2013
KM
01/14/2013 12:21
SW 6010C
KM
01/14/2013 12:21
SW 6010C
KM
01/14/2013 12:21
SW 6010C
KM
01/14/2013 12:21
SW 6010C
KM
01/14/2013 09:00
SW-7471 B
KM
01/14/2013 12:21
SW 6010C
JM
01/14/2013 08:05
SW-9045D
KM
01/14/2013 12:21
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

SDdium Absorption Ratio Calculation (SAR)-°
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 1/10/2013 111/2013-313112013 1.6520
Na mg/I = (Na mg/kg x % Solids) =100 = (1910 x 14.5600) =100 = 278.096
Ca mg/I = (Ca mg/kg x % Solids) =100 = (10500 x 14.5600) + 100 = 1528.8
Mg mg/I = (mg mg/kg x % Solids) : 100 = (2530 x 14.5600) + 100 = 368.368
Na meq = Na mg/I + Molec.Wgt.Na = 278.096 _ 23 = 12.0911
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1528.8 + 20 = 76.44
Mg meq = Mg mg/I + Molec.Wgt.Mg = 368.368 _ 12 = 30.6973
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 12.0911 + SgrRoot[0.5(76.44+30.6973)] = 1.65201
Printed: 1 /22/2014
Page 1 15:17

Page: 1 of 2
Report Number: 13-116-0205
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 93318
Sample ld : STATESVILLE 3RD CK
A&L Eastern Laboratories, Inc.
A 7621 Y1lhitepine Road Richmond, Virginia23237 [phone] Fax [phone]
wwwaleas.tern.com
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 4/24/2013 13:40:00
Date Received: 04/26/2013 00:00
Date Reported: 05/02/2013
Total Solids *
13.41
134100
100.0
MW
04/29/2013 08:24
SM-2540G
Moisture *
86.59
100.0
MW
04/29/2013 08:24
SM-254OG
Total Kjeldahl Nitrogen
5.12
51200
10.0
JM
04/29/2013 08:39
SM-4500-NH3C-TKN
Total Phosphorus
2.02
20200
100
KM
04/29/2013 13:56
SW 6010C
Total Potassium
0.30
2980
100
KM
04/29/2013 13:56
SW 6010C
Total Sulfur
0.96
9570
100
KM
04/29/2013 13:56
SW 6010C
Total Calcium
1.12
11200
100
KM
04/29/2013 13:56
SW 6010C
Total Magnesium
0.24
2360
100
KM
04/29/2013 13:56
SW 6010C
Total Sodium
0.17
1740
100
KM
04/29/2013 13:56
SW 6010C
Total Iron
19500
100
KM
04/29/2013 13:56
SW 6010C
Total Aluminum
16700
100
KM
04/29/2013 13:56
SW 6010C
Total Manganese
460
5
KM
04/29/2013 13:56
SW 6010C
Total Copper
399
5
KM
04/29/2013 13:56
SW 6010C
Total Zinc
1100
5
KM
04/29/2013 13:56
SW 6010C
Ammonia Nitrogen
0.90
8950
10.0
JM
04/29/2013 08:39
SM-4500-NI3C
Organic N
4.22
42250
10.0
04/29/2013 08:39
CALCULATION
Nitrate+Nitrite-N
26.8
2.00
JM
04/29/2013 08:30
SM-450ONO3F
Total Cadmium
13.0
2.0
KM
04/29/2013 13:56
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 13-116-0205
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE ; NC 27028
Lab Number: 93318
Sample Id : STATESVILLE 3RD CK
s A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia.23237 (804) 743-94Qt Ea (804) 271-MG
www.aleastem.com
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 4/24/2013 13:40:00
Date Received: 04/26/2013 00:00
Data Reported: 05/02/2013
Total Chromium
88
5
KM
04/29/2013 13:56
SW 6010C
Total Nickel
49
5
KM
04/29/2013 13:56
SW 6010C
Total Lead
113
5
KM
04/29/2013 13:56
SW 6010C
Total Arsenic
3.0
3.0
KM
04/29/2013 13:56
SW 6010C
Total Mercury
<0.4
0.4
KM
04/30/2013 08:05
SW-7471 B
Total Selenium
<5.0
5.0
KM
04/29/2013 13:56
SW 6010C
pH (Standard Units) *
6.70
2.00
JM
04/29/2013 08:30
SW-9045D
Total Molybdenum
21
5
KM
04/29/2013 13:56
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Oodium Absorption Ratio Caicui 'doa-,(GAR)
Product Code Product Name Sample Date ReportRange Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 4/24/2013 41112013-6/30/2013 1.4243
Na mg/I = (Na mg/kg x % Solids) _ 100 = (1740 x 13.4100) _ 100 = 233.334
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (11200 x 13.4100) _ 100 = 1501.92
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2360 x 13.4100) + 100 = 316.476
Na meq = Na mg/I + Molec.Wgt.Na = 233.334 = 23 = 10.145
Ca meq = Ca mg/I = Molec.Wgt.Ca = 1501.92 _ 20 = 75.096
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 316.476 = 12 = 26.373
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 10.145 '= SgrRoot[0.5(75.096+26.373)] = 1.42429
Printed: 1 /22/2014
Page 1 15:17

Page: 1 of 2
Report Number: 13-235-0208
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 95162
Sample Id : STATESVILLE 3RD CK
A&L Eastern Laboratories, Inc.
AFL 7621 Whitepine Road Richmond, Virginia.23237 [phone]. Fax (804) 271,6446
wwm aleastern.cbm
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 8/22/2013 10:30:00
Date Received: 08/23/2013 00:00
Date Reported: 08/28/2013
Total Solids *
13.71
137100
100.0
JM
08/23/2013 14:15
SM-2540G
Moisture *
86.29
100.0
JM
08/23/2013 14:15
SM-2540G
Total Kjeldahl Nitrogen
5.88
58800
10.0
JM
08/26/2013 08:10
SM-4500-NH3C-TKN
Total Phosphorus
1.95
19500
100
KM
08/26/2013 14:21
SW 6010C
Total Potassium
0.25
2490
100
KM
08/26/2013 14:21
SW 6010C
Total Sulfur
0.94
9430
100
KM
08/26/2013 14:21
SW 6010C
Total Calcium
1.86
18600
100
KM
08/26/2013 14:21
SW 6010C
Total Magnesium
0.25
2540
100
KM
08/26/2013 14:21
SW 6010C
Total Sodium
0.11
1100
100
KM
08/26/2013 14:21
SW 6010C
Total Iron
22600
100
KM
08/26/2013 14:21
SW 6010C
Total Aluminum
15900
100
KM
08/26/2013 14:21
SW 6010C
Total Manganese
417
5
KM
08/26/2013 14:21
SW 6010C
Total Copper
418
5
KM
08/26/2013 14:21
SW 6010C
Total Zinc
729
5
KM
08/26/2013 14:21
SW 6010C
Ammonia Nitrogen
1.24
12400
10.0
JM
08/26/2013 08:10
SM-4500-NI3C
Organic N
4.64
46400
10.0
08/26/2013 08:10
CALCULATION
Nitrate+Nitrite-N
48.1
2.00
JM
08/26/2013 08:10
SM-450ONO3F
Total Cadmium
8.0
2.0
KM
08/26/2013 14:21
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may -not be reproduced in whole or part, nor may
any reference be made
to the work, the results, or the company in any advertising, news release, or other
public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 13-235-0208
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
A&L Eastem Laboratories, Inc;
7621 whitepine Road Richmond, Virginia.23237 (804) 743-P401 Fax (804) 27t-6446
www.ale.astem.com
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 8/22/2013 10:30:00
Lab Number: 95162 Date Received: 08/23/2013 00:00
Sample Id : STATESVILLE 3RD CK Date Reported: 08/28/2013
Total Chromium
at$
o
11111vl
U0l/-o/LUl.3 "14:CI
JVV UU IUI,
Total Nickel
53
5
KM
08/26/2013 14:21
SW 6010C
Total Lead
98
5
KM
08/26/2013 14:21
SW 6010C
Total Arsenic
4.0
3.0
KM
08/26/2013 14:21
SW 6010C
Total Mercury
0.4
0.4
KM
08/26/2013 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
08/26/2013 14:21
SW 6010C
pH (Standard Units) *
7.84
2.00
JM
08/26/2013 08:10
SW-9045D
Total Molybdenum
20
5
KM
08/26/2013 14:21
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr" AND "Ni". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Oodiurn
Product Code Product Name Sample Date ReportRange Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 8/22/2013 9/1/2013-10/31/2013 0.7412
Na mg/I = (Na mg/kg x % Solids) _ 100 = (I 100 x 13.7100) _ 100 = 150.81
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (18600 x 13.7100) _ 100 = 2550.06
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2540 x 13.7100) z- 100 = 348.234
Na meq = Na mg/I + Molec.Wgt.Na = 150.81 _ 23 = 6.55696
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2550.06 _ 20 = 127.503
Mg meq = Mg mg/I + Molec.Wgt.Mg = 348.234 _ 12 = 29.0195
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.55696 _ SgrRoot[0.5(127.503+29.0195)] = 0.741189
Printed: 1/22/2014
Page 1 15:18

Page: 1 of 2
Report Number: 13-325-0210
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 96705
Sample Id : STATESVILLE 3RD CK
�L A&L Eastem Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271.WG
0
wwwaleastim.com
Project: STATESVILLE 3RD CHECK
NC CERT#257
REPORT OF ANALYSIS Data Sampled: 11/20/2013 10:15:00
Date Received: 11/21/2013 00:00
Date Reported: 11/27/2013
Total Solids *
13.65
136500
100.0
JM
11/22/2013 09:09
SM-2540G
Moisture *
86.35
100.0
JM
11/22/2013 09:09
SM-2540G
Total Kjeldahl Nitrogen
5.60
56000
10.0
JM
11/22/2013 10:20
SM-4500-NH3C-TKN
Total Phosphorus
2.38
23800
100
KM
11/22/2013 12:11
SW 6010C
Total Potassium
0.27
2670
100
KM
11/22/2013 12:11
SW 6010C
Total Sulfur
0.81
8050
100
KM
11/22/2013 12:11
i SW 6010C
Total Calcium
2.18
21800
100
KM
11/22/2013 12:11
SW 6010C
Total Magnesium
0.29
2890
100
KM
11/22/2013 12:11
SW 6010C
Total Sodium
0.08
790
100
KM
11/22/2013 12:11
SW 6010C
Total Iron
23300
100
KM
11/22/2013 12:11
SW 6010C
Total Aluminum
21900
100
KM
11/22/2013 12:11
SW 6010C
Total Manganese
1600
5
KM
11/22/2013 12:11
SW 6010C
Total Copper
321
5
KM
11/22/2013 12:11
SW 6010C
Total Zinc -
665
5
KM
11/22/2013 12:11
SW 6010C
Ammonia Nitrogen
0.55
5490
10.0
JM
11/22/2013 09:00
SM-4500-NH3C
Organic N
5.05
50510
10.0
11/22/2013 09:00
CALCULATION
Nitrate+Nitrite-N
24.2
2.00
JM
11/26/201313:45
SM-450ONO3F
Total Cadmium
4.0
2.0
KM
11/22/201.3 12:11
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
4&U
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made -aid
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 13-325-0210
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 96705
Sample Id: STATESVILLE 3RD CK
A�. A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia23237 [phone] Fax [phone]
.a
www.aleastem.com
Project: STATESVILLE 3RD CHECK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 11/20/2013 10:15:00
Date Received: 11/21/2013 00:00
Date Reported: 11/27/2013
Total Chromium.
39.
5
KM
11/22/2013 12:11
SW 6010C
Total Nickel
32
5
KM
11/22/2013 12:11
SW 6010C
Total Lead
26
5
KM
11/22/2013 12:11
SW 6010C
Total Arsenic
4.0
3.0
KM
11/22/2013 12:11
SW 6010C
Total Mercury
1.4
0.4
KM
11/22/2013 09:00
SW-7471B
Total Selenium
<5.0
5.0
KM
11/22/2013 12:11
SW 6010C
pH (Standard Units) *
7.55
2.00
JM
11/22/2013 09:00
SW-9045D
Total Molybdenum
11
5
KM
11/22/2013 12:11
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or otherpublic announcements without obtaining our prior written authorization.
Debbie Holt

4 EAt
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Sodium AiysoTption Ratio Calculation (SAR) 3
Product Code Product Name Sample Date Report Range 'Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 11/20/2013 1111/2013-12/3112013 0.4919
Na mg/I = (Na mg/kg x % Solids) = 100 = (790 x 13.6500) = 100 = 107.835
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (21800 x 13.6500) = 100 = 2975.7
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2890 x 13.6500) = 100 = 394.485
Na meq = Na mg/I _ Molec.Wgt.Na = 107.835 _ 23 = 4.68848
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 2975.7 _ 20 = 148.785
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 394.485 = 12 = 32.8738
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.68848 _ SgrRoot[0.5(148.785+32.8738)] = 0.491947
Printed: 1 /22/2014
Page 1 15:18

FACILITY NAME: STATESVILLE,NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0004 A
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 87.87
OPERATOR: DENNIS .PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 44.20 ACRES PERMITTED: 44.20
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
11/22/13
140.00 (CY)
3.167
14.49
0.387
STFCC
MOIST
0-<I/2"
SUR
0.5
0.30
55,400. p
8,140.00 p
32.40 p
280FESCUE
11/23/13.
160.00 (CY)
3.620
14.49
0.442
STFCC
MOIST
0-<I/2"
SUR
0.5
0.30
55,400.p
8,140.00 p
32.40 p
F18280
I FESCUE
11/25/13
100.00 (CY)
2.262
14.49
0.276
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
55,400.p
8,140.00 p
32.40 p
18280
FESCUE
Nov-13
400.00 (CY)
9.049
12/3/13
320.00 (CY)
7.240
14.49
0.884
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
F7T1140.00
p
32.40 p
18280
FESCUE
1Dee-13
320.00 (CY)
7.240
Total Cubic Yds/Ac: 16.29
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
0.020
0.012
0.155
1.292
0.103
0.008
0.036
0.119
0.020
2.278
89.46
73 ;
1
Cumulative lbs/acre
0.099
0.125
1.112
7.851
1.112
0.036
0.251
0.731
0.077
15.186
i=-
�w .
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
l:
`'-
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500 0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X
(SIGNA OF 4ZAPPLIER) DATE
"I certi y,, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injectioi /Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014

FACILITY NAME: STATESVILLE, NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0004 B
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 51.26
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.60 ACRES PERMITTED: 11.60
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
till-
zation
Miner -
all-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
`
•..,
Crop
MONTH
Total
Per Acre
Solids
11/19/13
40.00 (CY)
3.448
14.49
0.421
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
55,400.p
8,140.00 p
32.40 p
18280
I FESCUE
11/20/13
160.00 (CY)
13.793
14.49
1.683
STFCC
MOIST
0-<I/2"
SUR
0.5
0.30
55,400.p
8,140.00 p
32.40 p
18280
I FESCUE
11/21/13
200.00 (CY)
17.241
14.49
2.104
STFCC
MOIST
0-<I/2"
SUR
0.5
0.30
55,400.p
8,140.00 p
32.40 p
18280
I FESCUE
11/22/13
20.00 (CY)
1.724
14.49
0.210
STFCC
MOIST
0-- I/2"
SUR
0.5
0.30
55,400.p
8,140.00 p
32.40 p
18280
FESCUE
Nov-13
420.00 (CY)
36.206
'
P
70tffi I:UC)1C YnS!AC: 36.21
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAx'j�I
TOTALS:
162
Annuallbs/acre
.0.044
0.027
0.345
2.872
0.230
0.017
0.080
0.265
0.044
5.064
198.84
Cumulative lbs/acre
0.124
0.170
1.619
10.784
1 1.714
0.046
0.352
1.000
0.092
21.090
;
k
,
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
;
t
,
216
FD Cumulative Pollutant LoadingRate Limit Ibs/acre
( )
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X
(SIGNA�FAPPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false informatipn, including the possibility of fines and imprisonment for laiowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
s Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014

FACILITY NAME: STATESVILLE, NC
OWNER: LORANE PAGE
SITE #: NC IR 00023 FIELD# : IR 00023 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 52.67
OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 17.20 ACRES PERMITTED: 17.20
Page: 1
Lune Applied **0
Date
L&Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
k
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp in )
Crop
p
MONTH
Total
Per Acre
Solids
4/25/13
288.00 (CY)
16.744
14.18
2.000
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
66,400. p
10,400.00 p
2.00 p
002
I FESCUE
4/26/13
32.00 (CY)
1.860
14.18
0.222
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
66,400. p
10,400.00 p
2.00 p
F22102
FESCUE
Apr-13
320.00 (CY)
18.604
4/24/13
128.00 (CY)
7.4421
13.41
0.841
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
51,200. p
8,950.00 p
26.80 p
1 17177
FESCUE
Apr-13
128.00 (CY)
7.442
1 VL¢l I..UU1N lUJ/AV. LU.VJ
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
127
0.018
0.035
0.321
2.173
0.301
0.008
0.089
0.202
0.031
4.578
137.50
Cumulative lbs/acre
0.105
0.189
1.620
11.403
1.993
0.047
0.388
0.854
0.119
19.362
t
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
.,.t
..,tit
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1
1339.0
267.9
15.0 375.0
89.0
2500.0 I
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
:� I Ll
X � .
(SIGNAT OF L APPLIER) DATE
"I certi nder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I ant aware that there are significant penalties for submitting false'information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014

FACILITY NAME: STATESVILLE, NC
OWNER: LORANE PAGE
SITE #: NC IR 00023 FIELD# : IR 00023 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 119.89
OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 32.40 ACRES PERMITTED: 32.40
Page: , 1
Lune Applied **"
Date
LLs/Ac
allons (G) or Cubic Yards (CY)
Dry,
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/24/13
32.00 (CY)
0.988
14.18
0.118
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
66,400. p
10,400.00 .p
2.00 p
22002
FESCUE
4/25/13
64.00 (CY)
1.975
14.18
0.236
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
66,400. p
10,400.00 p
2.00 p
22002
FESCUE
Apr-13
96.00 (CY)
2.963
4/23/13
480.00 (CY)
14.815
13.41
1.673
STTCC
DRY
0-<I/2"
SUR
0.5
0.30
51,200. p
8,950.00 p
26.80 p
17177
I FESCUE
4/24/13
480.00 (CY)
14.815
13.41
1.673
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
51,200. p
8,950.00 p
26.80 p
17177
FESCUE
Apr-13
960.00 (CY)
29.630
I Oral 1.1101c Y as�nc: 3"L.59
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.022
0.089
0.617
2.910
0.774
0.004
0.149
0.347
0.037
7.797
151.69
131
Cumulative lbs/acre
0.111 1
0.224
1 1.829
1 12.059
1 2.286
0.043
0.438
1 0.952
0.124
21.436
F
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
I
r
;' ' �,
• 1 i'
16
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
C "
1339.0
267.9
15.0 375.0
89.0
2500 0 �'
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X c i
(SIGNAT OF LAND PLIER) DATE
"I certify, nder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for lcnowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
K Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 53.50
SITE #: NC IR 00023 FIELD# : IR 00023 0003 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 23.00 ACRES PERMITTED: 23.00
Page
Lune Applied ***
Date
I Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pptn)
Crop
MONTH
Total
Per Acre
Solids
5/1/13
128.00 (CY)
5.565
14.18
0.665
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
66,400. p
10,400.00 p
2.00 p
22002
I FESCUE
5/2/13
256.00 (CY)
11.130
14.18
1.329
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
66,400.p
10,400.00 p
2.00 p
22002
I FESCUE
5/3/13
64.00 (CY)
2.783
14.18
0.332
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
66,400. p
10,400.00 p
2.00 p
22002
FESCUE
May-13
448.06 (CY)J
19.478
Total uubic Yas/Ac: 19.48
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.014
0.014
0.181
1.573
0.116
0.008
0.056
0.126
0.023
2.857
108.40
102
Cumulative Ibs/acre
0.048
1 0.044
1 0.640
1 4.634
1 0.369
0.030
1 0.161
1 0.360
0.069
8.321
=
Permit PAN Limit (lbs/acre) 1st Crop/2nd� Crop
t
.. -
r-.
;
i
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
r
1339.0
267.9
15.0 ) 375.0
89.0
2500.0`
STFCC = STATESVILLE, NC FOURTH CREEI{ CAKE
X & i16.;' Lly
(SIGN OF L APPLIER) DATE
"I certi , under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for lcnowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation "** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 42.04
SITE #: NC IR 00023 FIELD# : IR 00023 0004 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.70 ACRES PERMITTED: 13.70
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
THIN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
32.00(CY)
21.693
14.18
3
CC
"
SUR
0.5
0.3
6,400. p
10,400.00 p
2.00 p
22002
FESCUE4/26/13
Apr-13
352.00 (CY)
25.693
iotat t uoic Yas/ac: 25.69
As
Cd
Cr
Cu
Ph
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.018
0.018
0.239
2.074
0.153
0.010
0.074
0.166
0.031
3.768
142.99
135
r7..-.— - -lf
_ k
Cumulative lbs/acre
0.068
0.084
' 0.902
1 6.750
1 0.729
0.035
0.254
0.544
0.100
13.138
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
ry,
i
-
r
- l,r
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X J� l
(SIGNA OF L APPLIER) DATE
"I certify, nder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 -
Application Method: SUR - Surface, IN7 -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014
i
P

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 49.68
SITE #: NC IR 00023 FIELD# : IR 00023 0005 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.10 ACRES PERMITTED: 16.10
Page
Lune Applied
***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/25/13
192.00 (CY)
11.925
14.18
1.424
STFCC
DRY
0-<I/2"
SUR
0.5
0.30
66,400. p
10,400.00 p
2.00 p
22002
I FESCUE
4/26/13
224.00 (CY)
13.913
14.18
1.662
STFCC
DRY
0-<I/2"
SUR
0.5
0.30
66,400. p
10,400.00 p
2.00 p
22002
FESCUE
Apr-13
1 416.00 (CY)
1 25.838
1
1 ULc l I.UULL; I UW,'IV,. 43.84
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annuallbs/acre
136
0.019
0.019
0.241
2.086
0.154
0.010
0.074
0.167
0.031
3.789 143.80
Cumulative Ibs/acre
0.083
0.113
1.195
8.091
1.128
0.043
0.314
0.674
0.101
15.198
Permit PAN Limit (Ibs/acre) Ist Crop/2nd Crop
i i rz n 1
i xa ;
a �'
216 -
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
;
1339.0
267.9
15.0 ; i 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
r
2
X
(SIGNA OF L PLIER) DATE
"I certi , under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2014 '
r

S mo M MIT
ENVInONMEN IAL TECHNOLOGIES, INC.
Analytici
Client
Synagro Southeast
284 Boger Rd.
Mocksville, NC 27028
Order Number
1300640
Project Number
Statesville
Issued
Friday, January 25, 2013
Total Number of Pages
7 (excluding C.O.C. and cooler receipt form)
Approved By:
QA Manager
Certifications. A21-AIDOD 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-W05,
Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana
C-01-1-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and
LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Michigan (Reg.S), Minnesota 409711,
Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and
631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island
LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 5 WG-15J, Region
8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, Wast Virginia 248 and 9957C and E87688, Wisconsin 399013010
"Analytical Int6gilty" • EPA Certified • Ni°LAP Certified
3310 Win Street • Cuyahoga Falls, Ohio 411223 m Phone: [phone],11 - Fax: [phone]
Web .site: wwwsettek.com

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
R �..-- !)cllytical d aboratorie
Sample Summary
Client: Svnagro Southeast
Order Number: 1300640
Laboratory ID Client ID
1300640-01 Statesville 3rd CK
1300640-02 Statesville 4th CK
Matrix
4
Sampling Date
Sludge 1/10/2013
Sludge 1/10/2013
"Analytical Integrity" • EPA Certified • NELAP Certified
3910 Win street • Cuphoga Falls, Ohio 44223 0 Phone. [phone]'11 -Fax: [phone]
Web Site: www..S;elteiGcoil)

SUMMIT
€i ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories 3
Report [Narrative
Client: Synagro Southeast
Order Number: 1300640
No problems were encountered during analysis of this order number, except as noted.
Data Qualifiers:
B = Analyte found in the method blank
J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)
C = Analyte has been confirmed by another instrument or method
E = Analyte exceeds the upper limit of the calibration curve.
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate out of control limits
U = Undetected
a = Not Accredited by NELAC
ND = Non Detected at LOQ
DF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor)
Limit Of Detection (LOD) = Method Detection Limit
Practical Quantitation Limit (PQL) = (same as LOQ)
Method Detection Limit (MDL) = (same as LOD)
Reporting Detection Limit (RDL) = (same as LOD)
Estimated uncertainty values are available upon request.
Matrices:
A = Air
C = Cream
DW = Drinking Water
L = Liquid
O = Oil
St. = Sludge
SO = Soil
S = Solid
T = Tablet
TO = TCLP Extract
WW = Waste Water
W = Wipe
The test results meet the requirements of the NELAC standard, except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this
report was issued. The results contained in this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not
responsible for use or interpretation of the data included herein.
"Analytical Integ11ty" • EPA Certified • NELAP Certified
3319 Win treat - Cuyahoga Falls, t 1do 44223 m PlIono: 330-253-8211 • Fax: [phone]
Web Site: www.sellek.00111

SUMMor
ENVIRONMEN IAL TECHNOLOGIES, INC. January 25, 2013
Analy foal l iborato os Client: Synagro Southeast
Address: 284 Boger Rd.
A4ocksville, NC 27028
Received:1/11/2013
Project 9: Statesville
TCLP Volatites
Client Ill#
Lab 1D#
Collected Analyte
Rep Lmf Result
Units
T•latrix Method
DF
Re Lvl
Run Amlyst
Statesville 3rd CK
1300640-01
10 Jan-13 1,2-Dichloroethane
0.1 ND
mg/L
SL
1311
1
0.5
15 Jan-13 MS
Statesville 3rd CK
1300640-01
10-Jan-13 Benzene
0.1 ND
mg/L
SL
1311
1
0.5
15-Jan-13 MS
Statesville 3rd CK
1300640-01
10-Jan-13 Carbon tetrachloride
0.1 ND
mg/L
SL
1311
1
0.5
15-Jan-13 MS
Statesville 3rd CK
1300640-01
10-Jan-13 Trichloroethene
0.1 ND
mg/L
SL
1311
1
0.5
15-Jan-13 MS
Statesville 3rd CK
1300640-01
10 Jan-13 1,1-Dichloroethene
0.1 ND
mg/L
SL
1311
1
0.7
15-Jan-13 MS
Statesville 3rd CK
1300640-01
10-Jan-13 Tetrachloroethene
0.1 ND
mg/L
SL
1311
1
0.7
15-Jan-13 MS
Statesville 3rd CK
1300640-01
10-Jan-13 Chlorobenzene
0.1 ND
mg/L
SL
1311
1
100
IS-Jan-13 MS
Statesville 3rd CK
1300640-01
10-Jan-13 2-Butanone (MEK)
2 ND
mg/L
SL
1311
1
200
15-Jan-13 MS
Statesville 3rd CK
1300640-01
10-Jan-13 Chloroform
0.1 ND
mg/L
SL
1311
1
6
15-Jan-13 MS
Statesville 3rd CK
1300640-01
10-Jan-13 Vinyl Chloride
0.2 ND
mg/L
SL
1311
1
0.2
15-Jan-13 MS
TCLP BNA
Client ID#
I-ab ID#
Collected Anal&
Rep Lmt Result
Units
Matrix Method
DF
Re9Lvl
Run Analyst
Statesville 3rd CK
1300640-01
10-Jan-13 Hexachlorobenzene
0.1 ND
mg/L
SL
1311
1
0.13
17 Jan-13 AE
Statesville 3rd CK
1300640-01
10-Jan-13 Pyridine
0.25 ND
mg/L
SL
1311
1
5
17 Jan-13 AE
Statesville 3rd CK
1300640-01
10-Jan-13 2,4,5-Tdchlorophenol
0.25 ND
mg/L
SL
1311
1
400
17-Jan-13 AE
Statesville 3rd CK
1300610-01
10-Jan-13 Hexachloroethane
0.1 ND
mg/L
SL
1311
1
3
17-Jan-13 AE
Statesville 3rd CK
1300640-01
10-Jan-13 Cresols.
5 ND
mg/L
SL
1311
1
200
17-Jan-13 AE
Statesville 3rd CK
1300640-01
10-Jan-13 Nitrobenzene
0.1 ND
mg/L
SL
1311
1
2
17-Jan-13 AE
Statesville 3rd CK
1300640-01
10-Jan-13 2,4,6--Tdchlorophenol
0.25 ND
mg/L
SL
1311
1
2
17-Jan-13 AE
Statesville 3rd CK
1300640-01
10-Jan-13 Hexachloro-1,3-butadiene
0.1 ND
mg/L
SL
1311
1
0.5
17 Jan-13 AE
Statesville 3rd CK
1300640-01
10 Jan-13 1,4-Dichlorobenzene
0.1 ND
mg/L
SL
1311
1
7.5
17-Jan-13 AE
Statesville 3rd CK
1300640-01
10-Jan-13 2,4-Dinitrotoluene
0.1 ND
mg/L
SL
1311
1
0.13
17-Jan-13 AE
Statesville 3rd CK
1300640-01
10-Jan-13 Pentachlorophenol
0.25 ND
mg/L
SL
1311
1
100
17-Jan-13 AE
TCLP Pesticides
Client IN
Lib ID#
Collected Anal�4e
R_ ep Lmt Result
Units
Tdntrix Method
DF
R_ egLyl
Run Analyst
Statesville 3rd CK
1300640-01
10-Jan-13 Gamma-BHC
0.002 ND
mg/L
SL
1311
1
0.4
16-Jan-i3 KMG
Statesville 3rd CK
1300640-01
10-Jan-13 Methoxychlor
0.002 ND
mg/L
SL
1311
1
10
16-Jan-13 KMG
Statesville 3rd CK
1300640-01
10-Jan-13 Toxaphene
0.1 ND
mg/L
SL
1311
1
0.5
16-3an-13 KMG
Statesville 3rd CK
1300640-01
10-Jan-13 Endrin
0.002 ND
mg/L
SL
1311
1
0.02
16-Jan-13 KMG
Statesville 3rd CK
1300640-01
10-Jan-13 Heptachlor Epoxide
0.002 ND
mg/L
SL
1311
1
0.008
16-Jan-13 KMG
Statesville 3rd CK
1300640-01
10-Jan-13 Heptachlor
0.002 ND
mg/L
SL
1311
1
0.008
16 Jan-13 KMG
Statesville 3rd CK
1300640-01
10-Jan-13 Chlordane
0.01 ND
mg/L
SL
1311
1
0.03
16 Jan-13 MG
TCLP Herbicides
Client ID#
Lab ID#
Collected Analyle
Rep Lmt Result
Units
Matrix Method
DF
RegLvl
Run Analyst
Statesville 3rd CK
1300640-01
10-Jan-13 2,4,5-TP(Silvex)
0.5 ND
mg/L
SL
1311
1
1
21-Jan-13 KMG
Statesville 3rd CK
1300640-01
10-Jan-13 2,4,D
5 ND
mg/L
SL
1311
1
10
21-Jan-13 KMG
TCLP
Arsenic
Client ID#
Ub ID#
Collected Anal�4e
Reg) Lmt Result
Units
Aig& Method
DF
RL'4Lyi
Run Malys(
Statesville 3rd CK
1300640-01
10-3an-13 TCLP Arsenic
0.5 ND
mg/L
SL
1311
1
5
16-Jan-13 CXS
Page 4
"Anolytical h7legrity" • EPA Certified • NELAP Certified
3310 Irvin Street - CI..4l,1c1i7oga Falls, Ohio 1422,9 o Phone: [phone] • Fax: 330-253-d489
Web Site: wwlv.Sellel xoni

M IT
ENVIRONMENTAL TECHNOLOGIES, INC. January25, 2013
Analytical Laboratories Client: Spiagro Southeast
Address: 284 Boger Rd.
Mocksville, NC 27028
Received: 1 /11 /2013
Project #: Statesville
TCLP (Barium
Client ID#
Lab ID#
Collected Anal51e
Rep Lmt Result
Units
Matrix Method
DF
RepLyl
1Run Analvsl
Statesville 3rd CK
1300640-01
10-Jan-13 TCLP Barium
5 ND
mg/L
SL 1311
1
100
16 Jan-13 CXS
TCLP Cadmium
Client ID#
1-ab ID#
Collected anal 4e
Rep Lmt Result
Units
Matrix Method
DF
ReaLyl
Run An„ 811'st
Statesville 3rd CK
1300640-01
10-Jan-13 TCLP Cadmium
0.1 ND
mg/L
SL 1311
1
1
16-Jan-13 CXS
TCLP Chromium
Client ID#
Lab iDt1
Collected Awlk'1e
Rep Lmt Result
Units
Matrix Method
DF
ReQLvI
Run Analyst
Statesville 3rd CK
1300640-01
10-Jan-13 TCLP Chromium
0.2 ND
mg/L
SL 1311
1
5
16-Jan-13 CXS
TCLP Lead
Client ID#
Lab 1D#
Collected Anal54e
Rep Lm Result
Units
Matrix Method
DF
Ree Lvl
Run Analyst
Statesville 3rd CK
1300640-01
10-Jan-13 TCLP Lead
0.5 ND
mg/L
SL 1311
1
5
16-Jan-13 CXS
-
TCLP Mercury
Client IN
Lah IN
Collected Ann11_e
Rep Lmt Result
Units
Matrix Method
DF
Reotyl
Run Analyst
Statesville 3rd CK
1300640-01
10-Jan-13 Mercury
0.002 ND
mg/L
SL 1311
1
0.2
16-Jan-13 AU
TCLP Selenium
Client IN
Lab ID#
Collected Ail%-Ie
Rep Lmt Result
Units
Matrix Method
DF
R_ egLyi
Run Analyst
Statesville 3rd CK
1300640-01
10-Jan-13 TCLP Selenium
0.5 ND
mg/L
SL 1311
1
1
16-Jan-13 CXS
TCLP Silver
Client Ill#
Lab ID#
Collected Annlvle
Rep Lmt Result
Units
Matrix Method
DF
RegLvl
Run Anal ys
Statesville 3rd CK
1300640.01
10-Jan-13 TCLP Silver
0.5 ND
mg/L
SL 1311
1
5
16-Jan-13 CXS
Client ID#
Lab 1D9
Collected Ana1�Ke
Result
Units
Matrix Method
DF
LO�C
Run Anaivst
Statesville 3rd CK
1300640-01
10-Jan-13 Flash Point
>140
OF
SL 1010
1
18-Jan-13 TAH
Client ID#
Statesville 3rd CK
Lab ID#
1300640-01
Collected Annl)�te
10-Jan-13 pH
Result
7.65 @ 19AC
Units '
S.U.
Matrix Method
SL 9010
DF
1
LQQ
0.01
Run Analyst
15-Jan-13 SML
Client ID#
Lab ID#
Collected An -,%le
Result
Unils
Matrix Mettod
DF
LOQ
lR n Analyst
Statesville 3rd CK
1300640-01
10-Jan-13 Reactive Cyanide
ND
mg/kg
SL 7.3.3.2
1
0.5
14 Jan-13 TIR
Client ID#
Lab ID#
Collected AnsINI
Result
Units
Matrix Method
DF
LOQ
Run Analvsl
Statesville 3rd CK
1300640-01
10-Jan-13 Reactive Sulfide
ND
mg/kg
SL 7.3.4.2
1
25
14-Jan-13 TIR
Page 5
"Analytical Integrity" . ERA Certified • INELAP Certified
3310 Will Situ,,, - Cuyahoga F-9I1s, Ohio 44223 o Pi1©11o: 330-253-8211 • Fax: [phone]
Web Site: www.sef okxonl

'M
` SUMMMY
ENVIRONMENTAL. TECHNOLOGIES, INC. January25, 2013
�_. .... At3afyffcaf ,(.,��borafQi-le Client: Synagro Southeast
Address: 284 Boger Rd,
Mocksville, NC 27028
Received: 1/l 1/2013
Project #: Statesville
TCLP Volatiles
Client ID#
Lab ID#
Collected Attal��le
Rep Lmt Result
Units
Matrix
Method
DF
RegLvl
Rw► Analyst
Statesville 4th CK
1300640-02
10-Jan-131,2-Dichloroethane
0.1 ND
mg/L
SL
1311
1
0.5
15Jan-13 MS
Statesville 4th CK
1300640-02
10-Jan-13 Benzene
0.1 ND
mg/L
SL
1311
1
0.5
15 Jan-13 MS
Statesville 4th CK
1300640-02
10-Jan-13 Carbon tetrachloride
0.1 ND
mg/L
SL
1311
1
0.5
15-Jan-13 MS
Statesville 4th CK
1300640-02
10-Jan-13 Trichloroethene
0.1 ND
mg/L
SL
1311
1
0.5
15-Jan-13 MS
Statesville 4th CK
1300640-02
10-3an-13 1,1-Dichloroethene
0.1 ND
mg/L
SL
1311
1
0.7
15-Jan-13 MS
Statesville 4th CK
1300640-02
10-Jan-13 Tetrachloroethene
0.1 ND
mg/L
SL
1311
1
0.7
15-Jan-13 MS
Statesville 4th CK
1300640-02
10-3an-13 Chlorobenzene
0.1 ND
mg/L
SL
1311
1
100
15-Jan-13 MS
Statesville 4th CK
1300640-02
10-3an-13 2-Butanone (MEK)
2 ND
mg/L
SL
1311
1
200
15Jan-13 MS
Statesville 4th CK
1300640-02
10-3an-13 Chloroform
0.1 ND
mg/L
SL
1311
1
6
15-Jan-13 MS
Statesville 4th CK
1300640-02
10 Jan-13 Vinyl Chloride
0.2 ND
mg/L
SL
v
1311
1
0.2
15-Jan-13 MS
TCLP BNA
Client ID#
Lab ID #
Collected AualZe
Rep Lint Resn t
Units
Matrix
Method
DF
ReqLvI
Run Analyst
Statesville 4th CK
1300640-02
10-Jan-13 Hexachlorobenzene
0.1 ND
mg/L
SL
1311
1
0.13
17-Jan-13 AE
Statesville 4th CK
1300640-02
10-3an-13 Pyridine
0.25 ND
mg/L
SL
1311
1
5
17-Jan-13 AE
Statesville 4th CK
1300640-02
10-Jan-13 2,4,5-Ttichlorophenol
0.25 ND
mg/L
SL
1311
1
400
17-Jan-13 AE
Statesville 4th CK
1300640-02
10 Jan-13 Hexachloroethane
0.1 ND
mg/L
SL
1311
1
3
17-Jan-13 AE
Statesville 4th CK
1300640-02
10 Jan-13 Cresols
5 ND
mg/L
SL
1311
1
200
17-Jan-13 AE
Statesville 4th CK
1300640-02
10-Jan-13 Nitrobenzene
0.1 ND
mg/L
SL
1311
1
2
17-3an-13 AE
Statesville 4th CK
1300640-02
10-Jan-13 2,4,6-Trichlorophenol
0.25 ND
mg/L
SL
1311
1
2
17 Jan-13 AE
Statesville 4th CK
1300640-02
10-Jan-13 Hexachloro-1,3-butadiene
0.1 ND
mg/L
SL
1311
1
0.5
17 Jan-13 AE
Statesville 4th CK
1300640-02
10-Jan-13 1,4-Dichlorobenzene
0.1 ND
mg/L
SL
1311
1
7.5
17-Jan-13 AE
Statesville 4th CK
1300640-02
10-Jan-13 2,4-Dinitrotoluene
0.1 ND
mg/L
SL
1311
1
0.13
17 Jan-13 AE
Statesville 4th CK
1300640-02
10-Jan-13 Pentachlorophenol
0.25 ND
mg/L
SL
1311
1
100
17 Jan-13 AE
TCLP Pesticides
Client IDN
Lab ID#
Collected Anal lee
Rep Lmt Restdt
Units
Matrix
Method
DF
RegLvl
Run Analyst
Statesville 4th CK
1300640-02
10-3an-13 Gamrna-BHC
0.002 ND
mg/L
SL
1311
1
0.4
25-Jan-13 KMG
Statesville 4th CK
1300640-02
10 Jan-13 Methoxychlor
0.002 ND
mg/L
SL
1311
1
10
25-Jan-13 KMG
Statesville 4th CK
1300610-02
10-Jan-13Toxaphene
o.i Nb
mg/L
SL
1311
1
0.5
25-Jan-13 KMG
Statesville 4th CK
1300640-02
10-Jan-13 Enddn
0.002 ND
mg/L
SL
1311
1
0,02
25-Jan-13 KMG
Statesville 4th CK
1300640-02
10-Jan-13 Heptachlor
0.002 ND
mgfL
SL
1311
1
0.008
25-Jan-13 KMG
Statesville 4th CK
1300640-02
10-Jan-13 Heptachlor Epoxide
O.OD2 ND
mgfL
SL
1311
1
0.008
25-Jan-13 KMG
Statesville 4th CK
1300640-02
10-Jan-13 Chlordane
0.01 ND
mg/L
SL
1311
1
0.03
25 Jan-13 KMG
_
TCLP Herbicides
Client ID#
Lab ID#
Collected Anal�4c
R, en Lmt Result
Units
Matrix
Method
DF
R- egLvl
Run. Analyst
Statesville 4th CK
1300640-02
10-Jan-13 2,4,5-TP(Silvex)
0.5 ND
mgfL
SL
1311
1
1
24-Jan-13 KMG
Statesville 4th CK
1300640-02
10-Jan-13 2,4,D
5 ND'
mg/L
SL
1311
1
10
24-Jan-13 KMG
~ TCLP
Arsenic
Client IDN
Lab IDN
Collected Anable
Rep Lmf Result
Units
Matrix
Method
DF
RegLvl
Run Analyst
Statesville 4th CK
1300640-02
10-Jan-13 TCLP Arsenic
0.5 ND
mg/L
SL
1311
1
5
17-Jan-13 JRK
Page 8
"Analytical Infeyrfty" - EPA Certified - NIEL.AP Certified
3310 I/ilin stYtr t • Cuphog,i Rills, Olilo 44223 a Phone. [phone] •Rix: 330-263-4,489
Web Site: www.sellek.com

1
W,
- - - - - - - - - -
� U11 M M my
ENVIRONMENTAL TECHNOLOGIES, INC.
Jiililtary 25, 2013
Client: Synagro Southeast
Address: 284 Boger Rd.
Mocksville, NC 27028
Received:1/11/2013
Project #: Statesville
TCLP Barium
Client ID#
Lab ID#
Collected Anal%
Rep Lmt Result
Units
Matrix Method
DF
R, pgLvl
Rna Analyst
Statesville 4th CK
1300640-02
10-Jan-13 TCLP Barium
5 ND
mg/L
SL 1311
1
100
17-1an-13 JRK
TCLP Cadmium
Client ID#
Lab ID#
Collected Anal ate
Rep Lmt Result
Units
Matrix Method
DF
RegLvl
ILtm Analyst
Statesville 4th CK
1300640-02
10-Jan-13 TCLP Cadmium
0.1 ND
mg/L
- SL 1311
1
1
17-Jan-13 JRK
TCLP Chromium
Client IDH
Lab ID#
Collected AnalLI
Rep Lmt Result
Units
Matrix Method
DF
RegLvl
Run Analyst
Statesville 4th CK
1300640-02
10-Jan-13 TCLP Chromium
0.2 ND
mg/L
SL 1311
1
5
17-Jan-13 JRK
TCLP Lead
Client ]DO Lab ID# Collected Analti1e R• eo Lmt Result Units Matrix Method DF RegLvl Run Analyst
Statesville 4th CK 1300640-02 10 Jan-13 TCLP Lead 0.5 ND, mg/L SL 1311 1 5 17-Jan-13 JRK
TCLP Mercury
Client IDH
Lab ID#
Collected An. a1�1e
Rep Lmt Result
Units
Matrix Method
DF
Re Lvl
Run Anti\,sl
Statesville 4th CK
1300640-02
10-Jan-13 Mercury
0.002 ND
mg/L
SL 1311
1
0.2
16-Jan-13 AL3
TCLP Selenium
Client IDH
I.ab ID#.
Collected Analyze
Rep Lmt Result
Units
Matrix Method
DF
RegLvl
Ran Analyst
Statesville 4th CK
1300640-02
10 Jan-13 TCLP Selenium
0.5 ND
tng/L
SL 1311
1
1
17-Jan-13 JRK
TCLP Silver
Client ID#
Lab ID#
Collected Annhl
Rep Lmt Result
Units
Matrix Method
DF
RegLvl
Run Analyst
Statesville 4th CK
1300640-02
10-Jan-13 TCLP Silver
0.5 ND
mg/L
SL 1311
1
5
17-Jan-13 JRK
Client ID# Lab IN Collected Anal-Je
Statesville 4th CK 1300640-02 10-Jan-13 Flash Point
Client ID# Lab iD# Collected An,11 �11
Statesville 4th CK 1300640-02 10-Jan-13 pH
Result Units Matrix Method DF LQQ Run Analyst
> 140 OF SL 1010 1 18-Jan-13 TAH
Result Units Matrix Method DF LOQ Run Analyst
7.04 @ 19.1C S.U. SL 9040 1 0.01 15-Jan-13 SML
Client ID# Lab IDH Collected Analrle Result Units Matrix Method DF LCIQ Run Analyst
Statesville 4th CK 1300640-02 10-Jan-13 Reactive Cyanide ND mg/kg SL 7.3.3.2 1 0.5 14 Jan-13 TIR
Client IDH Lab IDH Collected Anah4e
Statesville 4th CK 1300640-02 10-Jan-13 Reactive Sulfide
Result Units Matrix Method DF LOB Run Analyst
ND mg/kg SL 7.3.4.2 1 25 14-Jan-13 TIR
Page 7
"Analytical Integrity" • IPA Certified - NELAP Certified
3310 Win Street , Cuyahoga Falls, Ohio 44— 23 ® Phone: [phone] = Fax: [phone]
Web Sit;;: wwwsettek,corrl

unit Environmental Technologies, Iuc. ..alysis Request/43310
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Win Street
Cuyahoga Falls Ohio 44223
Tel: [phone] Fax: [phone]
For Summit Environmental '
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Company Name (Please Print)
Project Name
Order ID: 13ow4Q CDC
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Company Address
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Project Address
Client Phone No.
33
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Client Fax No. Please Fax es I-t _✓ El
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Check if Ohio VAP samples ✓
w c v.
# Sample identification
Date TTimeI's
Collected Collected
Q
E
a G°) � m
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Plmie Cheek Andl
'cal Box
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Relin hed by: Date Time
Received b : I Date I
Tithe
Notes/Comments:
a
Received in lab by: D to Time
Rush Requested By: Must be approved
la
Date by lab manager
White and yellow pages should accompany samples to the laboratory. The
client retains the pink page.
587 2 5

Summit Environmental Technologies, Inc.
Cooler Receipt Form
order IM,o COOLER
Client, �i 1� Order ID:
IJ Log in initials:
Date Received: 1 Time Received:. jrQM Date opened:
Number of o iers Boxes: N/A Unpacked by:
Shipper: FED EX UPS DHL Airborne US Postal Walk-in Pickup Other:
Packaging: Peanuts [e Wra Paper Foam None Other:
Tape o cools ox: rY N N/A
Custody Seals Intact 0 N NIA
C-0•C In plastic 0Y N N/A
Coolant: Ice, Blue ice Vater,_,None_ Sample Temperature r °C
C-O-C filled out properly by N NIA
Samples in separate bags Y N N/A
Sample containers Intact N NIA
'if no, list broken sample($):
Semple label(s) complete (ID, date, etc.) 0) N N/A
Label(s) agree with C-O-C cy N N/A
Correct containers used Y N N/A
Sufficient sample received Y N N/A
Samples at correct pH? pls(below) Y N
Bubbles absent from 40 mL vials*" Y N
°' Samples vilth bubbles less than the size of a pea are acceptable.
Client contact: pateMme:
Comments:
Sample ID pH Sample ID all `--1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Town of Statesville
Fourth Creek W WTP
WQ Permit Number: WQ 00016247
NPDES Number: NCO031836
Monitoring Period: From Jan. 1, 2013 To Mar. 31, 2013
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamins Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tr I:__�I- a,.A 19,1—c A — CInc o Y2\ nmmnlnfn fha fnllnwina mnnifnrina dafn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10to the 6th
MPN
Coliform
power per gram
17,600
35,052
124,031
MPN/g
0
quarterly
sludge
SM92210E
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
02 XX
(VS reduction)
(40-day bench)
(30-day bench) (Spec. uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." -
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Residuals
print)
�,I-i
Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 1/22/2013
Reported: 1 /29/2013
For: 4th Creek
Sample ID
Parameter Cust ID
Result
Units
Method
Date Analyzed
Analyst
130122-7.1
% Solids 4-1
12
%
SM2540B
1123/13
MD
130122-7.1
Fecal Coliform MTF 4-1
18,333
MPN/g
SM92210E
1/23113
MD
130122-7.2
% Solids 4 2
12.5
%
SM2540B
1/23/13
MD
130122-7.2
Fecal Coliform MTF 4-2
72,000
MPN/g
SM92210E
1/23/13
MD
i30122-7.3
% Solids 4-3
12.5
%
SM2540B
1/23/13
MD
30122-7.3
Fecal Coliform MTF 4-3
17,600
MPN/g
SM92210E
1/23113
MD
130122-7.4
% Solids 4-4
13.4
%
SM2540B
1/23113
MD
130122-7.4
Fecal Coliform MTF 4-4
22,388
MPN/g
SM92210E
1/23/13
MD
130122-7.5
% Solids 4-5
12.2
%
SM2540B
1/23113
MD
130122-7.5
Fecal Coliform MTF 4-5
24,590
MPN/g
SM9221 CE
1123/13
MD
130122-7.6
% Solids 4-6
12.2
%
SM2540B
1/23/13
MD
130122-7.6
Fecal Coliform MTF 4-6
40,984
MPNIg
SM92210E
1123/13
MD
130122-7.7
% Solids 4-7
12.9
%
SM2540B
1/23/13
MD
130122-7.7
Fecal Coliform MTF 4-7
124,031
MPN/g
SM92210E
1123/13
MD
130122-7.7
Geometric Mean 4-7
35,052
MPN/g
dry wt. basis
1/24/13
MD
Respectfully submitted,
Dena Myers r
NC Cert #440,
NCDW Cert #37755,
EPA NC00909
P.O. Box 228 a Statesville, North Carolina 28687 0 704/872/4697

Client: C ,
`D i/
STATES'VILLE ANALYTICAL
122 Court Street • P.O. Box 229
Mw
Address: `� ' /,' r
Statesville, NC 28687
[phone]
Chain of
I Custody Record
Contact Person: ,. 1 .� Phone # nL
t ,� (Time Date
PO # t Requisitioned by:, j1 ,r'v�fi
._0i 4 �j �c,2 .�'(f
I
Customer
Sample ID#
Lab -ID #
Time Sampled
(Grab Only)
Date Sampled (
(Grab Only)
�
a
-
Matrix
Parameters requested for analysis
swaeo
w
I ww
�
t
/j
1
4
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Relinquished by:�.`V`
Time t amp Date
Sampled by:
Received by: 1 • , \ j w:
Time am, 'm ®ate
Transported by, M
1%��{,'
Relinquished by:
Time am, pm. Date/ /
Holding times met:7-,,,-,,
Received by:
Time am, pm Date _,/--/_
Compliance work:
Composite Sampling #'I:
Time begin am, pm Date _/ /
Non-compliance work: r•
Time end am, pm Date
Lab Comments:
IF
i
Composite Sampling #2:
Time begin am, pm Date.:_,/ /
Time end am, pm Date

9pec�lfic,Q)gfgen, !Qlptake, Rate _..
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
I_ _.,... tobl f'Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.28
1 .
8.51
2
8.71
3
8.63
4
8.75
5
8.8
6
8.64
7
8.6
8
8.46
9
8.36
10
8.27
11
8.42
12
8.36
13
8.21
14
8.16
15
8.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
1 /2/2013
12.7
1/2/13 1:35 PM
RG
1/2/13 1:42 PM
BJ
300
12.8
13.3
0.0
8.7
0.7
milliliters
%Dry Solids
legrees Celsius
legrees Celsius
1.92 mg Oxygen/hr
0.43 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.69 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Srarifr. QxvgQn Untak?.Rte,
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
� -� Total'Solids
Beginning Temperature
End Temperature
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/I)
8.61
8.55
8.43
8.43
8.37
8.38
8.3
8.32
8.47
8.48
8.43
8.34
8.25
8.15
8.04
7.95
Fourth Creek WWTP
1 /3/2013
14.3
1/3/13 1:00 PM
LC
1/3/13 1:05 PM
BJ
300
14.2
14.6
Slope: 0.0
Intercept: 8.6
Correlation Coefficient: 0.8
milliliters
Dry S"olI S
iegrees Celsius
legrees Celsius
Oxygen Uptake Rate: 1.81 mg Oxygen/hr
'Ambient Specific Oxygen Uptake Rate: 0.41 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:1 0.61 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

x .......... Specific Oxvaen Uptake Rate
SOUR
Facility Name: FOL
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total _Solids-:
Beginning Temperature:
End Temperature:
- Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
10.21
10.18
10.05
9.91
9.87
9.79
9.65
9.6
9.54
9.54
9.54
9.51
9.46
9.39
9.39
9.32
1 /4/2013
12.6
1/4/13 1:50 PM
LC
1/4/13 1:55 PM
BJ
300
12.8
14
milliliters
%_Dry Solids
degrees Celsius
degrees Celsius
Slope: 0.1
Intercept: 10.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 3.45 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.75 mg Oxygen/g/hr
Average Temperature: 13 degrees Celsius
Temperature Correction Factor: 1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 1.21 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
- Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
1 1/7/2013 1
1 1/7/13 12:40 PM 1
1 1/7/13 12:48 PM 1
(minutes) (mg/1)
0
9.75
1
9.83
2
9.83
3
9.72
4
9.78
5
9.71
6
9.68
7
9.51
8
9.47
9
9.42
10
9.35
11
9.31
12
9.27
13
9.12
14
9.09
15
9.04
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
300 milliliters
148 %o_Dry Solids
13.2 degrees Celsius
13.6 Idearees Celsius
0.1
9.9
1.0
3.36 mg Oxygen/hr
0.76 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 1.21 1mg Oxygen/g/hr
i
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

9perific.Oxyaen
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling DatelTime
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Tofa_L.Solid_s
Beginning Temperature
End Temperature
Fourth Creek WWTP
1 /8/2013
13.3
1/8/13 12:38 PM
LC
1/8/13 12:47 PM
BJ
300
13.6
13.8
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
9.64
1
9.75
2
9.89
3
9.74
4
9.52
5
9.92.
6
9.68
7
9.78
8
9.65
9
9.54
10
9.4
11
9.26
12
9.17
13
9.08
14
8.98
15
8.9
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
0.1
9.9
0.9
-milliliters
%.DCy S_ol�ds..
legrees Celsius
legrees Celsius
3.54 mg Oxygen/hr
0.76 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:1 1.14 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
_� T t � Solids
Beginning Temperature
End Temperature
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
8.95
9.02
8.91
8.85
8.81
8.76
8.72
8.68
8.43
8.54 .
8.61
8.43
8.39
8.28
8.23
8.16
rp�ifia_Q,x!gen.Uptake Rate
SOUR
jhr/e WWTP
13
9 PM
8 PM
300
�149
13.4
15
Slope: 0.1
Intercept: 9.0
Correlation Coefficient: 1.0
milliliters
S; kidsq
degrees Celsius
degrees Celsius
Oxygen Uptake Rate: 3.30 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.74 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352*
Temperature Corrected Specific Oxygen Uptake Rate:1 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total`:_Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
9.6
1
9:57
2
9.43
3
9:41
4.
9.33
5
9.29
6
9.19
7
9.08
8
8.99
9
8.91
10
8.87
11
8.79
12
8.71
13
8.73
14
8:67
15
8.65
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Fourth Creek WWTP
1 /10/2013
13.9
1/10113 1:00 PM
RG
1/10113 1:12 PM
BJ
300
13.8
15.4
0.1
9.6
1.0
rilliliters
Pry, _ I_ S' I
legrees Celsius
legrees Celsius
4.13 mg Oxygen/hr
0.93 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 1.30 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AyNND,1MC-TOR A TTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Fourth Creek WWTP NPDES Number: NCO031836
Monitoring Period: From Apr. 1, 2013 To June 30, 2013
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
_c__u_ .._ _u-.._..a:..,...,...0 ........7 //'`L..... A .... !`L.�� 32\ ...,m.,lo4n Oho fnllnwino mnni4nrina rya+a'
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6 1h
MPN
Coliform
power per gram
21,127
71,607
111,888
MPN/g
0
quarterly
sludge
SM92210E
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) XX
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
*Preparer is
d—I 1
Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

t
Analytical Results
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 4/15/2013
Reported: 4/25/2013
For: Fourth Creek
Date
Sample ID
Parameter Cust ID
Result
Units
Method
Analyzed Analyst
130415-5.1
% Solids
1
14.3
%
SM2540B-1997
4/16/13
MD
130415-5.1
Fecal Collform MTF
1
111,888
MPN/g
SM92210E-2006
4/16113
MD
130415-5.2
% Solids
2
14.2
%
SM254OB-1997
4116113
MD
130415-5.2
Fecal Cofiform MTF
2
21,127
MPN/g
SM92210E-2006
4116/13
MD
130415-5.3
% Solids
3
14.3
%
SM264OB-1997
4/16/13
MD
130415-5.3
Fecal Coliform MTF
3
34,965
MPN/g
SM92210E-2006
4116113
MD
130415-5.4
% Solids
4
15.4
%
SM2540B-1997
4/16/13
MD
130415-6.4
Fecal Coliform MTF
4
108,896
MPN/g
SM92210E-2006
4/16/13
MD
130415-5.5
% Solids
5
17.1
%
SM2540B-1997
4/16113
MD
130415-5.5
Fecal Coliform MTF
5
93,567
MPN/g
SM92210E-2006
4/116/13
MD
130415-5.6
% Solids
6
14.3
%
SM254OB-1997
4/16/13
MD
130415-5.6
Fecal Coliform MTF
6
111,888
MPN/g
SM92210E-2006
4/16113
MD
130415-5.7
% Solids
7
14.9
%
SM254OB-1997
4116/13
MD
130415-5.7
Fecal Coliform MTF
7
107,383
MPN/g
SM92210E-2066
4/16113
MD
130415-5.7
Geometric Mean
7
71,607
MPN/g
dry wt. basis
4/17A3
MD
P.O. Box 228 o Statesville, North Carolina 28687.704/872/4697

Synagro
284 Boger Rd.
"nocksville
Entered 4/15/2013
Reported: 4/25/2013
For:
NC 27028
': a-3_,..,
Date
Sample ID Parameter Cust ID Result Units Method Analyzed Analyst
Respectfully submitted,
al-111�
Dena Myers
NC Cert #440,
NCDW Cert #37755,
ZPA NCO0909
PO. Box 228 o Statesville, Noith Carolina 28687 0 704/872/4697

Client:
S,1 `11 Cx Ok "'r)
"'' w`
STATESVILLE ANALYTICAL
122 Court street • P.O. Boy. 228
Statesville.NC 28687
[phone]
Address: 1 ' -I L` r;
yy / C.``++1J v^Y•
Contact Person:
Phone # r _ C FAX# f cr
3�C� -mot i t �tJ�� , 3-..� q - � o
I
Chain of
,
Custody Record
P
PO Requisitioned by: {llme Date} a
. 1 � - r� !� � t-t��cLt% �w. `'t '\ � r� �v ��i'n •tl -1 j /�
Customer
Sample Ib#
Lab-10 #
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
Matrix
Parameters requested
for analysis i
§R5
w
ww
4
I/
t
t
§
s
`f J 5- i 3
Relinquished by: fl.Lrr; r
•' .''f / � ,(
r
Time r �y an j�. Date sr / /, %�
Sampled b
p Y L:tG`
Received by: s /
% �?� '
Time��,� am,07bate ? /�.f
.Ll
Transported by:
Relinquished by:
Time am, pm Date /
Holding times met:
Received by:
Time am, pm Date —/_�
Compliance work:
Composite Sampling 01:
Time begin am, pm
Date/ /
Non-compliance work:
Time —'end —am, pm
Date —/_--J
Lab Comments:
Composite Sampling #2,
Time begin am, pm
Date
Time end am, pm
Date _/,_-_/

Time
(minutes)
0
. 1
2
3
4
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake_Rate.._._ ._
SOUR
Facility Name:1 Fourth Creek WWTP
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids
Beginning Temperature:
- End Temperature:
Dissolved Oxygen Level
6.38
6.15
17.8
'1/13 12:42 PM
LC
11/13 12:50 PM
BJ
300 milliliters
17 Idegrees Celsius
17.6 Idearees Celsius
Slope: 0.0
Intercept: 6.5
Correlation Coefficient: 0.7
Oxygen Uptake Rate: 2.37 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Average Temperature: 17 degrees Celsius
Temperature Correction Factor: 1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.69 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Y Total,�S®lids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.22
1
7.7
2
7.83
3
7.67
4
7.45
5
7.47
6
7.58
7
7.64
8
7.6
9
7.53
10
7.5
11
7.39
12
7.38
13
7.37
14
7.36
15
7.28
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
SOUR
17.9
4/2/13 12:38 PM
BJ
300 milliliters
17.2 degrees Celsius
17.5 degrees Celsius
0.0
7.6
0.5
1.03 mg Oxygen/hr
0.24 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.29 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Fourth Creek
4/3/201
18.4
4/3/13 12:7
LC
4/3/13 12:,r
BJ
300
TotalSolrcJs
13
Beginning Temperature:
17.3
End Temperature:
17.5
Time
Dissolved Oxygen Level
(minutes)
(mg/I)
0
7.31
1
7.38
2
7.5-
-3
7.64
4
7.67 .
5
7.72
6
7.72
7
7.69
8
7.75
9
7.85
10
7.7
11
7.62
12
7.58
13
7.48
14
7-.41
15
7.28
Slope: 0.0
Intercept: 7.6
Correlation Coefficient: 0.0
milliliters
degrees Celsius
degrees Celsius
Oxygen Uptake Rate: 0.07 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.02 mg Oxygen/g/hr
Average Temperature: 17 degrees Celsius
Temperature Correction Factor: 1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.02 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen UptmlUe,Rate -..
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
. _ ._Yota_I Solid
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/I)
0
8.8
1
8.78
2
8.86
3
8.84
4
8.67
5
8.57
6
8.42
7
8.34
8
8.38
9
8.35
10
8.21
11
8.14
12
8
13
8.21
14
8.2
15
8.22
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
4/4/2013
12.5
4/4/13 12:41 PM
RG-
4/4/13 12:51 PM
BJ
300
13
13.1
14.3
0.1
8.8
0.9
'milliliters
®ry Solids
Degrees Celsius
Degrees Celsius
3.23 mg Oxygen/hr
0.83 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:F 1.24 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
���_ Totalt=Solid
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
7.35
7.35
7.41
7.4
7.33
7.26
7.24
7.18
7.12
7.02
6.93
6.8
6.7
6.64
6.57
SOUR
Fourth. Creek WWTP
4/5/2013
12.6
E
9:51 AM
4/5/13 45 13
G0:00 AM
J00
2.8
11
3.9
Slope: 0.1
Intercept: 7.5
Correlation Coefficient: 1.0
milliliters
% Dly Solidsz,,,
Degrees Celsius
legrees Celsius
- Oxygen Uptake Rate: 3.51 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.89 mg Oxygen/g/hr
Average Temperature: 13 degrees Celsius
Temperature Correction Factor: 1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 1:42 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1,
2
3
4
5
6
7
9
10
11
12
13
14
15
Facility
Biosolids Permit N
Digester Temp(
Sampling Dat(
Samr
Analysis Dati
Analy;
Sample v
Beginning Temp(
End Temp(
Oxygen 11pt@ke Rate-,...
SOUR
Name:
umber:
Date:
�rature:
:/Time:
led By:
/Time:
:ed By:
olume:
Fourth Creek WWTP
milliliters
4/8/2013
19
4/8/13 1:39 PM
RG
418/13 1:45 PM
BJ
300
lids
434.
oo Dry,
!rature:
�rature:
19.1
degrees
degrees
19.2
Dissolved Oxygen Level
m
7.06
7.08
7.12
7.15
7.12
7.07
7.05
6.93
6.89
6.82
6.8
6.72
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.2
0.9
Solid`s,
Celsius
-elsius
2.10 mg Oxygen/hr
0.52 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.56 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Sp-e-ci_fic_Oxven Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total: Solids
Beginning Temperature
End Temperature
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.04
1
5.96
2
5.96
3
5.92
4
5.84
5
5.86
6
5.81
7
5.89
8
5.85
9
5.84
10
5.81
11
5.83
12
5.78
13
5.79
14
5.77
15
5.78
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Fourth Creek WWTP
4/9/2013
19
4/9113 1:00 PM
RG
4/9/13 1:10 PM
BJ
-300'
1 31
19
18.4
milliliters
%.VVDry Solids: V
_._
degrees Celsius
degrees Celsius
0.86 mg Oxygen/hr
0.22 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.23 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Town of Statesville WQ Permit Number:
Fourth Creek WWTP NPDES Number: _
00016247
NCO031836
Monitoring Period: From July 1 , 2013 To Sept. 30, 2013
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirnhle to alternative ne.rfnrmed !Class A or Class Bl comnlete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Co
N o land application occurred during this monitoring
period
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench) _
(30-day bench)
(Spec. 02 uptake) XX
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
—AAidy Smith,Residuals Superintendent
P par Name anitle (type o rint) Land Applier Name and Title (if applicable) (type or print)
Signature f Preparer* Date Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

. . i • i t It'd R
Analytical Results
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 7/15/2013
Reported: 7/22/2013
For: City of Statesville
Sample ID
Parameter Cust ID
Result
Units
Method
Date
Analyzed Analyst
130715-5.1
% Solids
4th Creek 1
16.1
%
SM254OB-1997
7/15/13
MD
10715-5.1
Fecal Coliform MTF
41h Creek 1
13,664
MPNlg
SM92210E-2006
7/15113
MD
130715-5.2
% Solids
2
16
%
-SM2540B-1997
7115113
MD
130715-5.2
Fecal Coliform MTF
2
18,750
MPN/g
SM92210E-2006
. 7/15113
MD
130715-5.3
% Solids
3
15.6
%
SM25408-1997
7/15113
MD
130715-5.3
Fecal Coliform MTF
3
57,692
MPN/g
SM92210E-2006
7/15/13
MD
130715-5.4
% Solids
4
15.8
%
SM254OB-1997
7115113
MD
130715-5.4
Fecal Coliform MTF
4
18,987
MPN/g
SM92210E-2006
7115/13
MD
130715-5.5
% Solids
5
12.4
%
SM254OB-1997
7115113
MD
130715-5.5
Fecal Coliform MTF
5
24,193
MPN/g
SM92210E-2006
7/15113
MD
130715-5.6
% Solids
6
15.7
%
SM254OB-1997
7115113
MD
130715-5.6
Fecal Coliform MTF
6
19,108
MPN/g
SM92210E-2006
7/15113
MD
130715-5.7
% Solids
7
16.1
%
SM254OB-1997
7/15113
MD
130715-5.7
Fecal Coliform MTF
7
18,633
MPN/g
SM92210E-2008
7115/13
MD
130715-5.7
Geometric Mean
7
21,902
MPN/g
dry wt. basis
7116/13
MD
P.O. Box 228 * Statesville, North Carolina 28687 o 704//872/4697

Synagro-
284 Boger Rd.
'llocksville
Entered 7/15/2013
Reported: 7/22/2013
For:
NC 27028
Sample ID Parameter Cust ID Result Units
Respectfully submitted,
1
C� �c
Dena Myers
NC Cert #440,
NCDW Cert #37755,
.PA NC00909
v 1 ( 1 t FI Y fl- F-n3n —1 f
Method
Date
Analyzed Analyst
P.O. Box 228 • Statesville, North Carolina 28687 © 704/872/4697

Client:
STATESVILL, ANALYTICAL,,
Address:
!e�
122 Court Street - P.O. Box22K,
R Statesville. NC 286S7 e.
ag
[phone]
Contact Person: Phone #
FAX#.);, 941J
Chain of
Custody Record
PO# Requisitioned by: (TimefYl
111 V\IQ U
Customer
Sample IDO
Lab -ID #
Sampled
(Grab Only)
Date Sampled
amp0
(Grab Only)
mat
x
Parameters requested for analysis
Is 10901
/W1
WW
0
Relinquished by: J
Time pm Date! /Z��/
Ll OM
Sampled by:
Received by:
L-5
m Date(Transported
4'
b
Relinquished by:
Time
am, pm Date _J_/—
Holding times met:
Received by:
Time
am, pm Date
Compliance work:
Composite Sampling fl-
Time begin am, pm
Date
Non-compliance work,
Time end am, pm
Date
Lab Comments-.*
Composite Sampling #2:
Time begin am, pm
Date
Time end am, pm
Date

Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
-4.5
1
4.43
2
4.35
3
4.27
4
4.25
5
4.14
6
4
7
3.94
8
3.88
9
3.76
10
3.61
11
3.59
12
3.54
13
3.51
14
3.49
15
3.39
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Rate
SOUR
Fourth Creek WWTP
7/1/2113
24.2
7/1/13 12:20 PM
RG
7/1/13 12:32 PM
BJ
300 r
1:_69 .
24.5 c
24.4 c
0.1
4.5
1.0
nilliliters
/o 10ry Solids
legrees Celsius
legrees Celsius
4.65 mg Oxygen/hr
0.92 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.75771mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically

Facility Nary
Biosolids Permit Numbi
Da
Digester Temperatui
Sampling Date/Tirr
Sampled E
Analysis Date/Tirr
Analyzed E
Sample Volurr
Beginning Temperatu
End Temperatu
Rate
SOUR
ree
:r:
:e:
7/2/2013
,e:
25
e:
7/2/13 10:09 AM
ly:
RG
ie:
7/2/13 10:17 AM
ly:
BJ
ie:
300
ss
1.4'.
,e:
24.9
e:
23
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/I)
4.75
4.66
4.72
4.67
4.67
4.6
4.54
4.49
4.48
4.33
4.19
4.21
4.19
4.15
4.1
4.06
Slope: 0.1
Intercept: 4.8
Correlation Coefficient: 1.0
m
o
dE
dE
Ililiters
Dry Solids
grees Celsius
grees Celsius
Oxygen Uptake Rate: 3.01 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.68 mg Oxygen/g/hr
Average Temperature: 24 degrees Celsius
Temperature Correction Factor: 0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
�_�_ Total Sold"s�
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Fourth Creek WWTP
7/3/2013
23.8
7/3/13 9:57 AM
RG
7/3/13 10:04 AM
BJ
300
1 fi3 --
23.9
23.5
Slope: 0.1
Intercept:. 5.5
Correlation Coefficient: 1.0
rilliliters
%-,0ry s_o4_,
legrees Celsius
legrees Celsius
Oxygen Uptake Rate: 3.36 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:. 0.69 mg Oxygen/g/hr
Average Temperature: 24 degrees Celsius
Temperature Correction Factor: 0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.57 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation'and the Spreadsheet execute automatically.

Specific Oxygen Uptake. Rate —
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
T&al.Solfi
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
6.44
1
6.38
2
6.34
3
6.26
4
6.23
5
6.19
6
6.12
7
6.08
8
5.92
9
5.89
10
5.8
11
5.73
12.
5.69
13
5.62
14
5.58
15
5.54
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
7/5/2013
24.5
7/5/13 9:50 AM
RG
7/5/13 10:00 AM.
BJ
300
1.45
24.5
24.4
0.1
&5
1.0
-milliliters
%_D ry_So I ids`
legrees Celsius
Degrees Celsius
3.82 mg Oxygen/hr
0.88 mg Oxygen/g/hr
- 24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.72 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Sne£ific,O� pa.Uptake-Rate
SOUR
Facility Name:
Fourth Creek WW-
Biosolids Permit Number:
-
Date:
7/8/2013
Digester Temperature:
26
Sampling Date/Time:
7/8/13 12:57 PM
Sampled By:
LC
Analysis Date/Time:
7/8/13 1:02 PM
Analyzed By:
BJ
Sample Volume:
300
Total>Solids
1'4
Beginning Temperature:
26
End Temperature:
24.8
Time
Dissolved Oxygen Level
(minutes)
(mg/l)
0
5.29
1
5.2
2
5.18
3
5.0.6
4
5.15
5
5.12
6
5.07
7
5.01
8
4.95
9
4.91
10
4.85
11
4.78
12
4.73
13
4.67
14
4.67
15
4.56
iilliliters
a Dry Solids
egrees Celsius
egrees Celsius
Slope: 0.0
Intercept: 5.3
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.73 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.65 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 0.51 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

,ppcitic 0-xyge-n-Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
_ Total -Solids:
Beginning Temperature:
End Temperature:
Fourth Creek 1
7/9/201
26
7/9/13 12:5,
LC
7/9/13 1:02
BJ
300
1.48
26
25.4
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.09
1
T05
2
7.07
3
7.07
4
7.09
5
7.04
6
6.92
7
6.83
8
6.79
9
6.72
10
6.64
11
6.61
12
6.57
13
6.5
14
6.48
15
6.45
Slope:
I ntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
illiliters
-®r_y S6 .ids-,
agrees Celsius
:orees Celsius
0.0
7.2
1.0
2.98 mg Oxygen/hr
0.67 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate:1 0.50 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0,
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fou
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 7/
Sampled By:
Analysis Date/Time: 7
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/I)
6.89
6.9
6.94
6.95
6.95
6.96
6.98
6.96
6.92
6.88
6.9
Slope:
Intercept:
Correlation Coefficient:
26.8
3 12:55 PM
300 milliliters
134 %_Dry -Solids j
25.7 degrees Celsius
24 degrees Celsius
0.0
7.0
0.8
Oxygen Uptake Rate: 1.36 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.34 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:1 0.27 mg Oxygen/g/hr
Instructions: * Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

u,,,, ,—*.Isdl`1TJAL:p�mo-GEN.AND. W—CTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Fourth Creek WWTP NPDES Number: NCO031836
Monitoring Period: From Oct. 1, 2013 To Dec. 31, 2013
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If a licable to alternative performed Class A or Class B com lete the following monitoring data:
VV
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2xl0 to the 6'h
MPN
Coliform
power per gram
97
124
133
MPN/g
0
quarterly
sludge
SM92210E
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/9
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Mt. 3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) XX
Option/Mt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 8
(Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
Xa reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
—ArASrAlth, Residuals Superintendent
JP�are e and �itie"( e or print) /
i
Signature f
f Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 10/22/2013
Reported:. 10/31/2013
For: Fourth Ck.
Date
Sample ID
Parameter Cust ID
Result
Units
Method
Analyzed Analyst
131022-7.1
% Solids
15.5
%
SM2540B-1997
10/22/13
MD
,31022-7.1
Fecal Coliform MTF
<129
MPN/g
SM92210E-2006
10/22/13
MD
131022-7.2
% Solids
15
%
SM2540B-1997
10/22/13
MD
131022-7.2
Fecal Coliform MTF
<133
MPN/g
SM92210E-2006
10/22/13
MD
131022-7.3
% Solids
16.4
%
SM2540B-1997
10/22/13
MD
131022-7.3
Fecal Coliform MTF
<122
MPN/g
SM92210E-2006
10/22/13
MD
131022-7.4
% Solids
15.1
%
SM2540B-1997
10/22/13
MD
131022-7.4
Fecal Coliform MTF
<132
MPN/g
SM92210E-2006
10/22/13 _
MD
131022-7.5
% Solids
20.6
%
SM2540B-1997
10/22/13
MD
131022-7.5
Fecal Coliform MTF
<97
MPN/g
SM92210E-2006
10/22/13
MD
131022-7.6
% Solids
15.3
%
SM2540B-1997
10/22/13
MD
131022-7.6
Fecal Coliform MTF
<131
MPN/g
SM92210E-2006
10/22/13
MD
131022-7.7
% Solids
15.2
%
SM2540B-1997
10/22/13
MD
131022-7.7
Fecal Coliform MTF
<132
MPN/g
SM9221 CE-2006
10/22/13
MD '
131022-7.7
Geometric Mean
<124
MPN/g
dry wt. basis
10/22/13
MD
P.O. Box 228 o Statesville, North Carolina 28687 s 704187214697

SynAgro
284 Boger Rd.
Aocksville NC 27028
Entered 10/22/2013
Reported: 10/31/2013
For:
. ':: �.rc rs.a •SR�i
Date
Sample ID Parameter Cust ID Result Units Method Analyzed Analyst
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert-#37755,
=PA NCO0909
P.Q. Box 228 a Statesville, Norm Carolina 28687 0 704187214697

Client: S
STATES'VILLE ANALYTICAL
122 Court Street - P.O. Box 228
Statesville, NC 28687
[phone]
(Chain o
Custody Record
Address: �y Q n _ (�
OfLlS �7G`i �"�
_ _
� ��.
.�
Contact Person: C � Phone #-33 � ,� C FAX#3 c g.—�y �
C'
I
PO # n �Q Requisitioned by: (rime Date) j
50 —4910 6vw \ V'0 a 6 1 . 7
Customer
Sample ID#
P
Lab -ID #
r
Time Sampled
Grab Only)
( Y)
Date Sampled
(Grab Only)
a
�8
n
Matrix
Parameters requested for analysis
NludgoL.W
I
ww
�f
1 1
l
JI
�K
j dL
4�f
Relinquished by:AW/ 0141A,Time
Received by:
Relinquished b •
q Y•
0t
Received by: ~yr,� l\`�/
Composite Sampling #1:
Time begin am, pm Date /
Time end am, .pm Date _J—/—
Composite Sampling #2:
Time begin am, pm Date ,, )
Time end am, pm Date/_/
T
�y� // am,am,40 Date d/��� Sampled by: O'l
Time am, pm Date AZ/A/L Transported by:
Time am, pm Date / Ll
Holding times met:
l r' \
Tim�a/ ` ( a , pm al L-16 L2S Compliance work:
Non-compliance work:
Lab comments:

i
Condition of Receipt
SampleID 131022-6 Client Synam
Temp on Arrival 1
pH upon Arrival Parameter Schedule
%Solids
❑
HNO3
❑
Ho
❑
NaOH
❑
19280
❑
Na2S20
❑
Dechlorinated
pH upon Arrival
Parameter Schedule
El
El
El
El
Fecal COlW= MTF
HNO3
HCI
NaOH
H2SO
Na2S20
Declilorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
'IV Received on Ice
C J Samples chilled upon receipt
❑ Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
SA Received on Ice
❑ Samples chilled upon receipt
L�l Chemicals in containers, lab
Page 1 of 1

Condition of Receipt
Sample ID 131022-7 Client Synagro
Temp on Arrival 1
pH upon Arrival
pH upon Arrival
Parameter Schedule %Solids
❑
HNO3
El
Hcl
❑
NaOH
❑
H2S0
❑
Na2S20
Dechlorinated
Parameter Schedule
recal colifonn M'fr
El
HNO3
❑
HCl
11
NaOH
❑
11280
Na2S20
❑
Dechlorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
Wei Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
❑ Chemicals in containers, client
Chemicals upon receipt
'v Received on Ice
❑ Samples chilled upon receipt
Rl Chemicals in containers, lab
Page 1 of 1

Time
(minutes)
0
1
2
3
4
5
6.
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Fourth Creek V
10/1 /201 i
20.4
10/1/13 2:30
LC
10/1/13 2:38
Analyzed By:
Sample Volume:
=Total Solids
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.83
6.79
6.73
76 8
6.76
681
6.84
6.71
300 milliliters
2_ %',Dry Solids .�
20.3 degrees Celsius
20.1 degrees Celsius
Slope: 0.0
Intercept: 7.1
Correlation Coefficient: 0.9
Oxygen Uptake Rate: 1.91 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.32 mg Oxygen/g/hr
Average Temperature: 20 degrees Celsius
Temperature Correction Factor: 1
Temperature Corrected Specific Oxygen Uptake Rate:1 0.32 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
TotalSolids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.15
1
7.11
2
7.12
3
7.04
4
6.99
5
6.94
6
6.93
7
6.9
8
6.97
9
6.92
10
6.88
11
6.85
12
6.85
13
6.79
14
6.77
15
6.76
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
1212013
19.8
3 12:32 PM
LC
3 12:41 PM
BJ
300
20
0.0
7.1
1.0
milliliters
Dry Solids
degrees Celsius
dearees Celsius
1.49 mg Oxygen/hr
0.33 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.33 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake -,Rate --,
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids`
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/l)
0
7.53
1
7.56
2
7.5
3
7.43
4
7.37
5
7.37
6
7.4
7
7.32
8
7.28
9
7.26
10
7.23
11
7.21
12
7.19
13
7.15
14
7.16
15
7.14
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/3/2013
20.1
10/3/13 9:56 AM
RG
10/3/13 10:01 AM
BJ
300
20.1
18.5
0.0
7.5
1.0
milliliters
Yo Dry S;olld-S
legrees Celsius
legrees Celsius
1.71 mg Oxygen/hr
0.38 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.41 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

rre rK'.;!.r r1 9 fi Fir KN ,
Specific Oxygen Uptake Rate
SOUR
Facility Name;
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids_
Beginning Temperature
End. Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.41
1
. 6.62
2
6.63
3
6.51
4
6.56
5
6.56
6
6.49
7
6.53
8
6.5
9
6.47
10
6.45
11
6.4
12
6.37
13
6.31
14
6.2
15
6.12
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Fourth Creek WWTP
10/4/2013
20
10/4/13 10:15 AM
RG
1014/13 10:23 AM
BJ
300
20
19.8
milliliters
Dly Solids' _j
iegrees Celsius
legrees Celsius
1.44 mg Oxygen/hr
0.29 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:1 0.29 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

, Specific Oxygen Uptake Rate
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
SOUR
Facility Name: Fourth Creek WWTP
Biosolids Permit Number:
Date: 10/7/2013
Digester Temperature: 21
Sampling Date/Time: 10/7/13 12:33 PM
Sampled By: RG
Analysis Date/Time: 10/7/13 12:38 PM
Analyzed By: BJ
Sample Volume: 300 milliliters
I Total S0l1ds 1 `55 % ®ry solids
Beginning Temperature: 21.2 degrees Celsius
End Temperature: 19.8 degrees Celsius
Dissolved Oxygen Level
7.63
7.65
7.51
7.59
7.56
7.46
Slope: 0.1
Intercept: 7.8
Correlation Coefficient: 0.9
Oxygen Uptake Rate: 3.30 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.71 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.68 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen iUptake-Rate -
SOUR
Facility Name.
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
_ Total �Sol�dsp'
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
6.39
6.38
6.26
6.34
6.32
6.36
6.32
6.33
6.29
6.27
6.24
6.18
6.13
6.11
6.09
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/8/2013
20.1
10/8/13 12:37 PM
RG
10/8/13 12:42 PM.
BJ
300
16
20.1
19.5
0.0
6.4
0.9
milliliters
Dry Solids_
Degrees Celsius
Degrees Celsius
1.10 mg Oxygen/hr
0.23 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:1 0.23 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Spec fic Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
t _
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mgll)
0
6.79
1
6.75
2
6.81
3
6.73
4
6.71
5
6.71
6
6.63
7
6.57
8
6.67
9
6.59
10
6.57
11
6.56
12
6.53
13
6.49
14
6.47
15
6.44
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/9/2013
19.6
10/9113 12:53 PM
RG
10/9/13 1:02 PM
BJ
300
16
19.7
19.1
0.0
6.8
1.0
milliliters
°V" SolidsN
Degrees Celsius
Degrees Celsius
1.41 mg Oxygen/hr
0.29 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:j 0.31 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

f , , z , � ANNUAL, P-A.THO..G N.A.ND.N T —rTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Third Creek WWTP NPDES Number: NCO020591
Monitoring Period: From Jan. 1, 2013 To Mar. 31, 2013
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class B complete the followin monitorin data:
Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo. Mean Maximum Units dances Analysis
Fecal 2x10 to the 6` MPN
Coliform power per gram 2054 4085 10,377 MPN/g 0 quarterly sludge SM92210E
of total solids
CFU CFU/g
1000 MPN per gram of MPN/g
total solids (dry weight)
Salmonella 3 MPN per 4 grams total
bacteria (in solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 2
(40-day bench)
Option/Alt. 3 Option/Alt. 4
(30-day bench) (Spec. 02 uptake) XX
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(In"ection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Pr arer m and�lo�type r print) Land Applier Name and Title (if applicable) (type or print)
�I N
Signature o Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is�deflned in 40 CFR Part 503.9(r) and 15ANCAC 2T.1102 (26)

Synagro
284 Boger Rd.
Mocksville
Entered 1/22/2013
Reported: 1/29/2013
For: 3rd Creek
Analytical Results
NC 27028
Sample ID Parameter Cust ID
Result
Units
Method
Date Analyzed
Analyst
130122-6.1 % Solids 3-1
10.9
%
SM2540B
1/23/13
MD
130122-6.1 Fecal Coliform MTF 3-1
2,752
MPN/g
SM92210E
1/23/13
MD
130122-6.2 % Solids 3-2
11.4
%
SM2540B
1/23/13
MD
130122-6.2 Fecal Coliform MTF 3 2
2,632
MPN/g
SM92210E
1/23/13
MD
130122-6.3 % Solids 3-3
11.2
%
SM2540B
1123/13
MD
-130122-6.3 Fecal Coliform MTF 3-3
2,054
MPN/g
SM92210E
1/23113
MD
130122-6.4 % Solids 3-4
10.8
%
SM2540B
1/23113
MD
130122-6.4 Fecal Coliform MTF 3-4
2,778
MPN/g
SM92210E
1/23/13
MD
130122-6.5 % Solids 3-5
10.6
%
SM2540B
1/23/13
MD
130122-6.5 Fecal Coliform MTF 3-5
10,377
MPN/g
SM92210E
1/23/13
MD
130122-6.6 % Solids 3-6
11.1
%
SM2540B
1/23/13
MD
130122-6.6 Fecal Coliform MTF 3-6
6,306
MPN/g
SM92210E
1/23113
MD.
130122-6.7 % Solids 3-7
11.4
%
SM2540B
1123/13
MD
130122-6.7 Fecal Coliform MTF 3-7
7,017
'MPN/g
SM92210E
1/23/13
MD
130122-6.7 Geometric Mean 3-7
4,085
MPN/g
dry wt. basis
1124113
MD
-Respectfully submitted,
/ V
Dena Myers rl
NC Cert #440, s
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 o Statesville, Noith Carolina 28687 © 704f872/4697

Client: c: , /-
- D l( yea � v
STATES'VILLE ANALYTICAL
122 Court Street • P.O. Box 229
Address: ' d /!
L fr a 1
Statesville, NC 28697
[phone]
Chain of
Custody Record
-
Contact Person: �. ;�� f i Phone # ' �� r"'r-^ FAX#imm
."��Giv�, pca ' ✓` - /� - Cc7r7, .. -t j " '�?5 G'
I
PO # JrG Li i Requisitioned by.; 1 t (Time / r Date
1,\��V\ i� �L'1!l'�l� f��%� /�
Customer
Sample ID#
Lab -ID #
Time Sampled
(Grab Only)
Date Sampled
(Grab Oniy)
°
.,��fl�IvQ(J"'il
Matrix
parameters requested for analysis
sfua¢o
W
WW
f
{
11 f J
!
1
Z
131� C\C)2
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f�Tj�— ✓
y
��
t�Cr�L��iUchJ�a
Relinquished by:
q
Time 1 1 a
am, p�rra Date_/�� /?
Sampled by:
f
Received b -�=
Y: J �-
/'
f ! G
Time am, '• m Date /�/
Trans
orted b"
p Y:
Relinquished by:
Time am pm Date /
Holding times met: r ;!
Received by:
Time am, pm Date ^/_/
✓ '
Compliance work:
Composite Sampling #1^
Time begin am, pm Date _1 /
Non-compliance work:
Time end am, pm Date _/ /
Lab Comments:
COMRosite Sampling #2:
Time begin am, pm Date,,•,.) /
F
Time end am, pm Date/ /

Condition of Receipt
Sample ID 130122-6.I-6.7
Client Synagro
Teinp on Arrival 6
pH upon Arrival
Parameter Scheduled
% Solids
❑
HNO3
❑ Chemicals in containers, client
❑
HCI
❑ Chemicals upon receipt
❑
NaOH
LV] Received on Ice
❑
H2SO4
❑ Samples chilled upon receipt
❑
Na2S20
❑ Chemicals in containers, lab
❑
Dechlorinated
pH upon Arrival
Parameter Scheduled
Fecal Colifonn MTF
❑
HNO3
❑ Chemicals in containers, client
❑
HCl
❑ Chemicals upon receipt
❑
NaOH
EV] Received on Ice
❑
H2SO4
❑ Samples chilled upon receipt
❑
Na2S20
❑ Chemicals in containers, lab
❑ Dechlorinated
Page I of I

Condition of Receipt
Sample ID 130122-7.1-7.7 Client Synagro
Temp on Arrival 6
pH upon Arrival Parameter Scheduled %Solids
❑
HNO3
❑
HCl
❑
NaOH
❑
H2SO4
❑
Na2S20
❑
Dechlorinated
pH upon Arrival Parameter Scheduled
Fecal Colifomi MTF
❑
HNO3
❑
HCI
❑
NaOH
❑
H2SO4
Na2S20
❑
Dechlorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
1] Received on lee
❑ Samples chilled upon receipt
❑ ChemicaIs in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
',] Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
Page 1 of 1

=u _ Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
_ `Tota k$-, 1 -0
Beginning Temperature
End Temperature
Time
Dissolved Oxygen Level
(minutes)
(mg/l)
0
8.71
1
8.69
2
8.62
3
8.57
4
8.51
5
8.48
6
8.43
7
8.37
8
8.34
9
8.26
10
8.24
11
8.2
12
8.17
13
8.16
14
8.09
15
8.08
Third Creek WWTP
WQ0016247
1 /2/2013
10.5
1/2/13 8:31am
SA
1/2/2013 8:36am
SA
300
10.5
11.3
milliliters
DY
Dry}Solids
legrees Celsius
Degrees Celsius
Slope: 0.0
Intercept: 8.7
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.63 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.52 mg Oxygen/g/hr
Average Temperature: 11 degrees Celsius
Temperature Correction Factor: 1.838459212
Temperature Corrected Specific Oxygen Uptake Rate:1 0.95 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
_ 'IT, otal£ Soo ds
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/l)
0
6.97
1
6.98
2
6.97
3
6.96
4
6.93
5
6.92
6
6.88
7
6.86
8
6.83
9
6.78
10
6.72
11
6.65
-12
6.58
13
6.49
14
6.38
15
6.36
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1 /3/2013
14.2
1/3/13 8:23am
SA
1/3/2013 8:27am
SA
300
r 5�g
14.4
14.7
0.0
7.1
0.9
rilliliters
%��Dry�S_ollds,a
Degrees Celsius
legrees Celsius
2.55 mg Oxygen/hr
0.47 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 0.66 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature.
Sampling Date/Time.
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
9.33
1
9.31
2
9.27
3
9.26
4
9.25
5
9.23
6
9.23
7
9.25
8
9.2
9
9.16
10
9.13
11
9.08
12
9.05
13
9.02
14
9
15
8.98
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1 /4/2013
11.2
1 /4/13 9:18am
SA
1/4/2013 9:26am
SA
300
1r 8
11.3
13.5
0.0
9.3
1.0
-milliliters
Solads
legrees Celsius
legrees Celsius
1.40 mg Oxygen/hr
0.26 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: r 0.45 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

.,., ,....,... Specific Oxygen.Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
TotaL,Sol1.
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.54
1
7.52
2
7.51
3
7.49
4
7.45
5
7.42
6
7.38
7
7.33
8
7.26
9
7.19
to
7.13
11
7.05
12
6.96
13
6.83
14
6.78
15
6.69
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1 /7/2013
11.2
117/13 10:35am
SA
1/7/2013 10:39am
SA
300
14.4
14.8
0.1
7.7
1.0
,milliliters
°Io.Dry� Solids.
Degrees Celsius
legrees Celsius
3.49 mg Oxygen/hr
0.65 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 0.91 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
r Total;Solds
Beginning Temperature
End Temperature
Third Creek WWTP
WQ0016247
1 /8/2013
11.8
1 /8/13 1:42am
SA
1 /8/2013 1:46am
SA
300
18;
11.8
12.6
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.28
1
8.16
2
8.02
3
7.95
4
7.88
5
7.82
6
7.79
7
7.75
8
7.73
9
7.69
10
7.64
11
7.64
12
7.61
13
7.58
14
7.55
15
7.52
Slope: 0.0
Intercept: 8.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
rilliliters
-:Dry: Solids j
legrees Celsius
legrees Celsius
2.66 mg Oxygen/hr
0.49 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1 0.85 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
� Total";Solids-
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.84
7.81
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
1/9/2013
14.6
1/9/13 9:05am
SA
1/9/2013 9:11am
SA
300
19
14.9
15.2
0.0
7.9
1.0
milliliters
%Dry�S:olids,,�
iegrees Celsius
legrees Celsius
2.21 mg Oxygen/hr
0.39 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 0.54 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

L Specific Oxygen Uptake..R to—, <..
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.12
1
8.09
2
8.07 -
3
8.03
4
8.01
5
8
6
8
7
7.97
8
7.96
9
7.95
10
7.94
11
7.92
12
7.9
13
7.87
14
7.84
15
7.82
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Third Creek WWTP
WQ0016247
1 /10/2013
13.4
1/10/13 8:51am
SA
1/10/2013 8:59am
SA
300
13.6
14.5
0.0
8.1
1.0
milliliters
Dry solids a
degrees Celsius
Degrees Celsius
1.08 mg Oxygen/hr
0.19 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.28 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

t 2t1�1_.:J1'SY.'S'. T+1-o :•1]e �,-ANIVJJA IL•.PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)... - •.R .•--..=W
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Third Creek WWTP NPDES Number: NCO020591
Monitoring Period: From Apr. 1, 2013 To June 30, 2013
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
7f �nnl:oohln +n al+nroa+ivn nnrf--A Wlace A nr Clace R\ emmnla+a +hn fnllnwina mnnifnrina dOn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
Coliform
power per gram
5517
21,802
106,667
MPN/g
0
quarterly
sludge
SM92210E
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Mt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) XX
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Mt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
V
anVi
e�or p nt Land Applier Name and Title (if applicable) (type or print)
Of reparer* Date Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro -
284 Boger Rd.
Mocksville NC 27028
Entered 4/15/2013
Reported: 4/25/2013
For: Third Creek
Sample ID
Parameter Cust ID
Result
Units
Method
Date
Analyzed Analyst
130415-4.1
% Solids
1
15.1
%
SM254OB-1997
4/16/13
MD
,130415-4.1
Fecal Coliform MTF
1
19,868
MPN/g
SM92210E-2006
4/16/13
MD
130415-4.2
% Solids
2
14.8
%
SM254OB-1997
4116/13
MD
130415-4.2
Fecal Coliform MTF
2
14,865
MPN/g
SM92210E-2006
4116/13
MD
130415-4.3
% Solids
3
16
%
SM254OB-1997
4116/13
MD
130415-4.3
Fecal Coliform MTF
3
18,750
MPN/g
SM92210E-2006
4/16/13
MD
130415-4.4
% Solids
4
14.5
%
SM254OB-1997
4/16/13
MD
130415-4.4
Fecal Coliform MTF
4
5,517
MPN/g
SM92210E-2006
4116/13
MD
130415-4.5
% Solids
5
15
%
SM254OB-1997
4/16/13
MD
130415-4.5
Fecal Coliform MTF
5
106,667
MPN/g
SM92210E-2006
4116113
MD
130415-4.6
% Solids
6
14.7
%
SM254OB-1997
4/16/13
MD
130415-4.6
Fecal Coliform MTF
6
20,408
MPN/g
SM92210E-2006
4/16113
MD
130415-4.7
% Solids
7
14.2
%
SM254OB-1997
4I16/13
MD
130415-4.7
Fecal Coliform MTF
7
35,211
MPN/g
SM92210E-2006
-4116113
MD
130415-4.7
Geometric Mean
7
21,802
MPN/g
dry wt. basis
4117/13
MD
P.O. Box 228 a Statesville, North Carolina 28687 . 7041872/4697

Synayro
284 Boger Rd.
Mocksville
Entered 4/15/2013
Reported: 4/25/2013
For:
NC 27028
Sample ID Parameter Cust ID Result Units
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NC00909
Date
Method Analyzed Analyst
P.O. Box 228 a Statesville, North Carolina 28687 o 704/872/4697

Client
Sk 1 A a G\ C, n
. _
s 9a r
STATESVILLE ANALYTICAL
122 Court Street • P.O. Box. 214
Statesville. NC 28687 ,
[phone]
Address: 1 ` -' r, n
Contact Person:
�-^<
Phone
# �� _(�`rs FAX#��_�;
Chain of
Custody Record
I
PO # � Requisitioned by: �1� ('171i e 3C f Date) r�
,.�`
J�— n t
Customer
Sample ID#
Lab -ID #
Time Sampled
Grab Only)
( y)
Date Sampled
(Grab Only)
a
m
Matrix
Parameters requested for analysis
swaec
w
ww
�
v
r
_
����
�
��`4�f
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t ��✓`f�
%
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F
P
k
e
Relinquished b
G Y
r' ;' �l (
'i; It, r, 1
Time �0 a�Date 41 � )%r' 3
f
Sampled b a:t 1 `=
p y: ;
rP
.� -AAA
Received by:
Time/� am, m Date // ? /��
�
Transported by: � ,SQL/ ✓E�`Ii'/
.
t
Relinquished by:
Time am, pm Date _/ /
Holding times met:
Received by:
Time am, pm Date �_/
Compliance work: •
Composite Sampling
01:
Time begin
am, pm
Date —/--J—
Non-compliance work:
Time"end
am, pm
Date �_ _J
Lab. Comments:
Composite Sampling
#2:.
Time begin
am, pm
Date ___ —J
Time end
am, pm
Date ___j_

-__Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By.
Sample Volume
_ Tot4l'.861ids:
Beginning Temperature
End Temperature
Time
Dissolved Oxygen Level
(minutes) (mg/1)
0
8.07
1
7.96'
2
7.92
3
7.85
4
7.8
5
7.76
6
7.72
7
7.68
8
7.64
9
7.58
10
7.58
11
7.55
12
7.48
13
7.45
14
7.4
15
7.82
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient
Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/1 /2013
14.7
4/1113 9:23am
SA
4/1/13 9:28am
SA
300
_ 1:7
15.2
16.1
milliliters
°_/o Dry Solids.
degrees Celsius
degrees Celsius
2.00 mg Oxygen/hr
0.39 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.51 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
...

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
...Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date
Digester'Temperature
Sampling Date/Time
Sampled By -
Analysis Date/Time
Analyzed By
Sample Volume
( To461"So11d_s
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
8.25
8.14
8.07
8.02
7.99
7.97 -
7.95
7.93
7.9
7.86
7.83
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
4/2/2013
12.1
4/2/13 7:26am
SA
4/2/13 7:32am
SA
300
12.2
14.5
0.0
8.2
1.0
rilliliters _
wy Solids
legrees .Celsius
legrees Celsius
1.88 mg Oxygen/hr
0.35 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
8
0
11
12
13
14
15
Spedfic axy en .Uptanke_Pate_--'
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
_ Total Solid"s;
Beginning Temperature
End Temperature
Dissolved Oxygen Level
;..
::.
8.73
8.66
8.58
8.57
8.55
8.57
8.47
8.46
8.45
8.46
8.43
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/3/2013
12.6
4/3/13 8:16am
SA
4/3/13 8:25am
SA
300
1`7 .
13.1
14.4
,milliliters
O y;Sollds.
Degrees Celsius
legrees Celsius
2.15 mg Oxygen/hr
0.42 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:1 0.63 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen.Uptake Rate....,,,.....,
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
�~ �Totaf=Solids'
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/l)
0
7.64
1
7.64
2
7.62
3
7.61
4
7.59
5
7.57
6
7.56
7
7.55
8
. 7.55
9
7.53
10
7.52
11
7.51
12
7.49
13
7.46
14
7.45
15
7.45
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/4/2013
14.4
4/4/13 8:04am
SA
4/4/13 8:12am
SA
300
14.9
15.9
0.0
7.6
1.0
milliliters
Dry S.olids��
legrees Celsius
legrees Celsius
0.80 mg Oxygen/hr
0.16 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 0.22 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen: Uptake-R-ate—..,
SOUR
Facility Name;
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By
Sample Volume
Total�:Sollds'
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/I)
0
8.17
1
8.18
2
8.13
3
8.11
4
8.06
5
8.08
6
8.08
7
8.02
8
7.88
9
7.86
10
7.86
11
7.81
12
7.81
13
7.79
14
7.74
15
7.72
- Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/5/2013
14.1
4/5/13 9:31 am
SA
4/5/13 9:36am
SA
300
14.3
15.1
0.0
8.2
1.0
milliliters
% Dry Solids^�
degrees Celsius
degrees Celsius
1.99 mg Oxygen/hr
0.39 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 0.55 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxyga-m ke_Rate—... _ --- -- _._--- -
SOUR
Facility Name;
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
_ Total SolIds"
Beginning Temperature
End Temperature
Time . Dissolved Oxygen Level
(minutes) (mg/1)
0
7.38
1
7.41
2
7.43
3
7.43
4
7.42.
5
7.44
6
7.42
7
7.43
8
7.41
9
7.42
10
7.4
11
7.37
12
7.36
13
7.36
14
7.34
15
7.33
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/8/2013
18.3
4/8/13 1:26pm
SA
4/8/13 1:33pm
SA
300
18.3
18
0.0
7.4
0.7
milliliters
�_/o }Dry�'So�ids
legrees Celsius
legrees Celsius
0.32 mg Oxygen/hr
0.06 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate:1 0.07 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name;
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
_ TotaL Solid_s�
~Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.72
1
7.68
2
7.64
3
7.63
4
7.62
5
7.62
6
7.63
7
7.64
8
7.65
9
7.65
10
7.64
11
7.63
12
7.59
13
7.55
14
7.51
15
7.48
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
- Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/9/2013
18.3
4/9/13 8:40pm
SA
4/9/13 8:46pm
SA
300
16.4
16.8
0.0
7.7
0.8
nilliliters
'/C r Solids
legrees Celsius
Degrees Celsius
0.61 mg Oxygen/hr
0.12 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.15 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION EORM (02T I:.
Facility Name:
WWTP Name:
Town of Statesville
Third CreekWWTP
WQ Permit Number: WQ 00016247
NPDES Number: NCO020591
Monitoring Period: From July 1, 2013 To Sept. 30, 2013
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
_a__�_a i�i__- ♦ _ /'9.. ., a\ .. ..1..�.. Fho f nn ;+.A.. A.fa•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
No land application occurred during this monitoring
period
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
(VS reduction)
Option/Alt. 2
(40-day bench)
Option/Alt. 3 Option/Alt. 4
(30-day bench) (Spec. 02 uptake) XX
Option/Alt. 5
(14-Day Aerobic)
Option/Mt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Infection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
AndA Smi liResiduals Su erinte dent
Pr er and atlb'(typa or p t) % Land Applier Name and Title (if applicable) (type or print)
- -. �-, /tf
Siginature f Preparer* Date I Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 7/15/2013
Reported: 7/22/2013
For: City of Statesville
Date
Sample ID Parameter Cust ID �ResultUnits Method Analyzed Analyst
-130715-4.1 % Solids 3rd Creek 1J 20.4 % SM2540B-1997 7115/13 MD
30715-4.1 Fecal Coliform MTF 3rd Creek 1 >78,4�31 MPN/g SM92210E-2006 7/15/13 MD
130715-4.2 % Solids 2 27.3 %` SM2540B-1997 7/15113 MD
130715-4.2 Fecal Coliform MTF 2 >58,608 MPN/g SM92210E-2006 7/15/13 MD
130715-4.3 % Solids 3 17.2 % SM2540B-1997 7/15/13 MD
130715-4.3 Fecal Coliform MTF 3 93,023 MPN/g SM92210E-2006 7/15113 MD
%
130715-4.4 % Solids 4 19.1 +' SM2540B-1997 7/15/13 MD
130715-4.4 Fecal Coliform MTF 4 >83,769 MPN/g SM92210E-2006 7/15113 MD
130715-4.5 % Solids 5 27.3 °� SM2540B-1997 7/15113 MD
130715-4.6 Fecal Coliform MTF 5 >58,608 PN/g SM92210E-2006 7/15/13 MD
1307154.6 % Solids 6 ° 17.2 J% SM2540B-1997 7/15/13 MD
130715-4.6 Fecal Coliform MTF 6 .4f4 >93,023 MPN/g SM92210E-2006 7/15/13 MD
130715-4.7 % Solids 7 `, 20.8 /% SM2540B-1997 7/15/13 MD
130715-4.7 Fecal Coliform MTF 7 >76,923 /� MPN/g SM92210E-2006 7/15113 MD
130715-4.7 Geometric Mean 7 >76,276 MPN/g dry wt. basis 7/16/13 MD
r
P.O. Box 228 • Statesville, North Carolina 28687 ° 7041872/4697

284 Boger Rd.
Mocksville NC 27028
Entered 7/15/2013
Reported: 7/22/2013
For:
Date
Sample ID Parameter Cust ID Result Units Method Analyzed Analyst
Respectfully, submitted,
y�
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 • Statesville, North Carolina 28687 o 704/872/4697

Client:.
. -�) C.
STATESVILLE ANALYTICAL
- P.0.Boy 228
Address: L
122 Court Street
Statesville, NC 2S687
... ...... .
[phone]
Chain of
Record
Contact Person: Phone# 2 FAXII 5 0
PO# Requisitioned by:Custody
(Time�'O
Customer
Lab -ID
Tlme Sampled
Date Sampled f
t
C.
Matrix
Parameters requested for analysis
Slvdgol/w
IyQy
Sample lD#
(Grab Only)
(Grab Only)
C
U
1-15
'A
Relinquished by:
Time prn Date r.12
Sampled
Received by: A
Tim rn Date7
Transported by.k
Relinquished by:
Time am, pm Date
Holding times met:
Received by:
Time am, pm Date
Compliance work:
Composite Sampling #11:
Time begin -am, pmDate
Non-compliance work:
Time end_ am, pm -Date
Lab Comments:
Composite Sampling #2,
Time begin am, pm Date
Time end am, prin Date

Condition of Receipt
Sample ID 130715-4 Client Swam
Temp on Arrival
pH upon Arrival
pH upon Arrival
Parameter Schedule %Solids
❑
HNO3
❑
HCl
❑
NaOH
❑
H2SO
❑
Na2S20
❑
Dechlorinated
Parameter Schedule
Fecal Colifomi MTF
❑
HNO3
❑
HCl
❑
NaOH
❑
H2SO
R1
Na2S20
❑
Dechlorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
RJ Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
Wl Received on Ice
❑ Samples chilled upon receipt
vI Chemicals in containers, Iab
Page i of i

Analytical Result
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 7/29/2013
Reported: 8/6/2013
For: Statesville-3rd Creek
Date
Sample ID
Parameter Cust ID
Result
Units
Method
Analyzed Analyst
130729-6.1
% Solids
1
15.1
%
SM254OB-1997
7/30/13
CL
130729-6.1
Fecal Coliform MTF
1
105,960
MPN/g
SM92210E 2006
7/30/13
CL
130729-6.2
% Solids
2
14.1
%
SM254OB-1997
7/30/13
CL
130729-6.2
Fecal Coliform MTF
2
113,475
MPN/g
SM92210E-2006
7130113
CL
130729-6.3
% Solids
3
14.3
%
SM264OB-1997
7/30/13
CL
130729-6.3
Fecal Coliform MTF
3
62,937
MPN/g
SM92210E-2006
7130113
CL
130729-6.4
% Solids
4
13.5
%
SM2540B-1997
7130/13
CL
130729-6.4
Fecal Coliform MTF
4
66,667
MPNIg
SM92210E-2006
7130113
CL
130729-6.5
% Solids
5
14.8
%
SM2540B-1997
7/30/13
CL
130729-6.6
Fecal Collform MTF
5
2027
MPN/g
SM92210E-2006
7130113
CL
130729-6.6
% Solids
6
15.1
%
SM254OB-1997
7/30/13
CL
130729-6.6
Fecal Coliform MTF
6
105,960
MPN/g
SM92210E-2006
7130/13
CL
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 o Statesville, North Carolina 28687 o 704/872/4697

M
Client:
STATESVFLLE ANALYfICAL
Address: 'k(1
122CourtStreet - P.O.Box 229
Statesville. NC 28687
[phone] -
Contact Person- Phone # -71
7A
F
Chain of
y Record
Custod
Requisitioned b DatV Cane
PO# 50 ?
-) 01/
Customer
Sample lD#
1-ab-ID 4
Time Sampled
(Grab 0 r*)
Date Sampled
(Grab Only)
Isluagal
mat
'Parameters requested for analysis
W I
WW
V�
Relinquished bye
/
Time 111._Yi j J am; 3p Date
Sampled by:
Received by:
-/a ate _Lgt:;"
Time Nprrl
Transported by- V\
Relinquished by:
Time am, pm Date
Holding times met:
Received by:
Time am, pm Date
Compliance work:
Composite Sampling #1
Time begin am, pm Date--/
Non-compliance work:
Time end am, pm Date
Lab Comments:
Composite Sampling #2
Time begin am, pm Date
Time end am, pm Date

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
--.Total-Solid's
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
P23
WWTP
6247
13
:14pm
2:20pm
(minutes) (mg/1)
0
6.79
1
6.7
2
6.7
3
6.59
4
6.56
5
6.42
6
6.32
7
6.24
8
6.15
9
6.05
10
5.97
11
5.89
12
5.78
13
5.72
14
5.62
15
5.54
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.8
1.0
milliliters
Dry Solids _
degrees Celsius
degrees Celsius
5.18 mg Oxygen/hr
1.02 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.97 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4, - _..Specific Oxygen. Upt@ka Rate----- ---
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
7/2/2013
Digester Temperature:
22.4
Sampling Date/Time:
7/2/13 9:46
Sampled By:
SA
Analysis Date/Time:
7/2/2013 9:50am
Analyzed By:
SA
Sample Volume:
300 milliliters
_. Total Soled"s
1 7 %Dry Solids
Time
(minutes)
0
1
2
3
4
5
7
8
9
10
11
12
13
14
15
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
mgn
20.8 degrees Celsius
20.3 degrees Celsius
Slope: 0.0
Intercept: 6.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.92 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.57 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.55 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue.Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total -Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(mg/1)
7
6.98
6.97
6.94
6.94
6.86
6.83
6.79
6.72
6.68
6.64
.6.6
6.55
6.46
6.41
6.35
SOUR
Third Creek WWTP
ml
WQ0016247
7/3/2013
22.3
7/3/13 8:12
SA
7/3/2013 8:20am
SA
300
1,.7
22.1
de
de
20.9.
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.1
1.0
Ililiters
pry_Solids.
grees Celsius
grees Celsius
2.67 mg Oxygen/hr
0.52 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: 0.48 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Facility Nat
Biosolids Permit Numl
D;
Digester Temperatt
Sampling Date/Tii
Sampled
Analysis Date/Tii
Analyzed
Sample Volui
.- Total ,Sol�c
Beginning Temperate
End Temperati
Specific Oxygen -Uptake Rate
SOUR
ne:
ier:
ite:
ire:
ne:
By:
ne:
By:
ne:
Third Creek WWTP
WQ0016247
7/5/2013
21
7/5/13 8:05
SA
7/5/2013 8:12am
SA
300
ire:
ire:
20.9
20.6
Time Dissolved Oxygen Level
(minutes) (mg/I)
0
7.13
1
7.09
2
7.04
3
6.97
4
6.94
5
6.9
6
6.83
7
6.79
8
6.76
9
6.7
10
6.67
11
6.61
12
6.57
13
6.56
14
6.55
15
6.53
Slope:.
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.1
1.0
milliliters
'/ovDry Solids.,_
legrees Celsius
legrees Celsius
2.54 mg Oxygen/hr
0.50 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.47 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
3
5
6
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
`SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
'; _ `Total ��olids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
6.13
6.11
6.07
6.06
6.03
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
7/8/2013
21
7/8/13 9:58
SA
7/8/2013 10:06am
SA
300 rr
22.3 d
21.6 d
0.0
6.6
1.0
illiliters
i Day
:grees Celsius
:grees Celsius
2.63 mg Oxygen/hr
0.51 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:1 0.47 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

_.Specific Oxygen Uptake Rate
SOUR
Facility Name:1 Third Creek WWTP
Biosolids Permit Numberl WO0016247
Digester Temperature:
21.8
Sampling Date/Time:
7/9/13 8:14
Sampled By:
SA
Analysis Date/Time:
7/9/2013 8:19am
Analyzed By:
SA
Sample Volume:
300
Tot_al__Solids:
1..6
__
Beginning Temperature:
21.8
End Temperature:1
21.1
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
6.49
1
6.47
2
6.42
3
6.39
4
6.38
5
6.36
6
6.35
7
6.3
8
6.3
9
6.27
10
6.25
11
6.24
12
6.23
13
6.2
14
6.18
15
6.14
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.5
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.29 mg Oxygen/hr
0.27 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.26 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WW
Biosolids Permit Number:
WQ0016247 -
Date:
7/10/2013
Digester Temperature:
21.9
Sampling Date/Time:
7110/13 7:08
Sampled By:
SA
Analysis Date/Time:
7/10/2013 7:16,
Analyzed By:
SA
Sample Volume:
300 -
Total solids
1_5.
Beginning Temperature:
21.5
End Temperature:
20.7
Dissolved Oxygen Level
Ililiters
_Dry
grees~Celsius
grees Celsius
Slope: 0.0
Intercept: 6.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.68 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.60 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.57 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND 1.7N-- TO,1<- ATTRE A CYT_ON TREDKC—T-10l`T
Facility Name: _
WWTP Name:
Monitoring Period
Town of Statesville
Third Creek VOM
From Oct. 1, 2013
WQ Permit Number:
NPDES Number: _
To Dec. 31, 2013
WQ 00016247
NCO020591
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
TC _-��l-..Ll.. l.. .. LL......,.t:-.........F ........7 19 1— A — Cl— Rl ...,mn1a+a +ha fn11nwina mnnitnrina dnfn-
Paraeter
m
Al lowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6'h
MPN
Coliform
power per gram
59
98
146
MPN/g
0
quarterly
sludge
SM92210E
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) XX
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
• (Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
and
Signature cif Preparer*
Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville NC 27028
Entered 10/22/2013
Reported: 10/31/2013
For: Third Ck.
Date
Sample ID
Parameter Cust ID
Result
Units
Method
Analyzed Analyst
' 31022-6.1
% Solids
33.7
%
SM254OB-1997
10/22/13
MD
31022-6.1
Fecal Coliform MTF
<59
MPN/g
SM92210E-2006
10122/13
MD
131022-6.2
% Solids
13.7
%
SM254013-1997
10/22/13
MD
131022-6.2
Fecal Coliform MTF
146
MPN/g
SM92210E-2006
10/22/13
MD
131022-6.3
% Solids
2Q.7
%
SM254OB-1997
10122/13
MD
131022-6.3
Fecal Coliform MTF
<97
MPN/g
SM92210E-2006
10/22/13
MD
131022-6.4
% Solids
20.4
%
SM254OB-1997
10/22/13
MD
131022-6.4
Fecal Coliform MTF
<98
MPNIg
SM92210E-2006
10/22/13
MD
131022-6.5
% Solids
16.5
%
SM25408-1097
10/22/13
MD
131022-6.5
Fecal Coliform MTF
<121
MPN/g
SM92210E-2006
10/22/13
MD
131022-6.6
% Solids
22.1
%
SM2540B-1997
10/22/13
MD
131022-6.6
Fecal Coliform MTF
<91
MPN/g
SM92210E-2006
10/22/13
MD
131022-6.7
% solids -
20.9
%
SM2540B-1997
10/22/13
MD
131022-6.7
Fecal Coliform MTF
<96
MPN/g
SM9221 CE-2006
10/22/13
MD
131022-6.7
Geometric Mean
98
MPN/g
dry wt. basis
10/22/13
MD
P.O. Box 228 9 Statesville, North CaroIuia 28687 o 704187214697

Synig o `
284 Boger Rd.
locksville NC 27028
Entered " 10/22/2013
Reported: 10/31/2013
For:
Date
Sample ID Parameter Cust ID Result Units Method Analyzed Analyst
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCOO909
P.O. Box 228 o Statesville, forth Carolina 28687 . 704/872/4697

Client:
�
'
STATESVILLE ANALYTICAL
122 courtstreet • P.o. Box 228
Statesville, NC 28687
(704)87»�697
Chanu of
Custody Record
Address- �(� t1_ fZ _ (�
15 C t.7C�3n
(�"` n
`\��V \�\C/ (�LCi
Contact Person: L Phone #33xa- 8S 5AX#3� (�c&_' fg5O
PO # JT—© 7 Requisitioned by: �i.,U1� (Time` Date)
Customer
Sample1D#
Lab -ID #
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
matrix
Parameters requested for analysis
mdaa
w I
ww
t l (/ izWOR
,(�
L
1
Relinquished by:
Received b :
c y
y. Relinquished b •
q
Received by: 01
Composite Sampling #i:
Time begin am, pm
Time end am, pm
Composite Sampling #z:
Time begin am, pm
Time end am, pm
�-�V
Date __J__/
Date ____�_J
Date _J_1
Date
Time /ki am,10 Date 1�, /� Sampled by: (�
Time am, pm Date NIAL-3 Transported by: :
�
Time am, pm Date
\ Holding times met:
Tim�� a , pm atCompliance work:
Non-compliance work:
Lab Comments:
r
r

,Specific --Oxygen Uptake,. I�lvtes acs sr a Fer r c c r_
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
r __ Total Solids
TBeginning Temperature
End Temperature
Time . Dissolved Oxygen Level
(minutes) (mg/1)
0
7.79
1
7.97
2
7.92
3
7.91
4
7.87
5
7.84
6
7.84
7
7.83
8
7.82
9
7.82
10
7.81
11
7.76
12
7.7
13
7.67
14
7.62
15
7.59
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
10/1 /2013
19.6
10-1-13 11:52am
SA
10/1/13 11:58
SA
300
1:8
19.6
19.8
0.0
7.9
0.9
-milliliters
% Dry Solids
legrees Celsius
legrees Celsius
1.16 mg Oxygen/hr
0.22 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.22 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
4
5
6
8
9
10
11
12
13
14
15
Specific 0xw,&'wq,Uptake R,atev. i,
SOUR
Facility Name
Biosolids Permit Number
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
T®tal-^Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.12
8.11
8.09
8.06
8.05
8
7.98
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
rd Creek WWTP
WQ0016247
10/2/2013
19.6
10/2/13 13:43
SA
10/2/13 13:47
300 milliliters
oo Dry Solids
19.5 degrees Celsius
19.4 Idearees Celsius
0.0
8.2
1.0
1.64 mg Oxygen/hr
0.30 mg Oxygen/g/hr
19 degrees Celsius
1:07
Temperature Corrected Specific Oxygen Uptake Rate:j 0.33 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
TOUT -Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.77
7.74
7.73
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
10/3/2013
19.3
10/3/13 9:03
SA
10/3/13 9:10
SA
300 r
19.4 c
19.2 c
0.0
8.0
1.0
nilliliters
/o Dry, Solids,
legrees Celsius
legrees Celsius
1.64 mg Oxygen/hr
0.30 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.33 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
10/4/2013
Digester Temperature:
19.3
Sampling Date/Time:
10/4113 12:23
Sampled By:
SA
Analysis Date/Time:
10/4/13 12:31
Analyzed By:
SA
Sam le Volume:
p
300
milliliters
f Total, Solids.:
, 1.8
0/6_D Solids
Beginning Temperature:
19.5
degrees Celsius
End Temperature:
19.3
degrees Celsius
Dissolved Oxygen Level
7.91
Slope: 0.0
Intercept: 7.9
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 1.72 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.32 mg Oxygen/g/hr
Average Temperature: 19 degrees Celsius
Temperature Correction Factor: 1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.34 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Spe�y_Ox3yer UptaI<e.Rate:..:..:-
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
� _ �otai�.souas
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.9
s
7.87
7.85
7.77
7.75
7.74
m
7.7
7.66
7.63
7.6
7.56
7.52
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
10/6/2013
19.8
10/6/13 10:03
SA
10/6/13 10:12
SA
300
1.8
19.8
19.5
0.0
7.9
1.0
milliliters
Yd Dry S®lids,
legrees Celsius
legrees Celsius
1.45 mg Oxygen/hr
0.27 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.27 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Nam
Biosolids Permit Numb(
Dal
Digester Temperatur
Sampling Date/Tim
Sampled E
Analysis Date/Tirr
Analyzed E
Sample Volurr
Total'Solid
Beginning Temperatui
End Temperatui
Specific Oxygen Uptake Rate
SOUR
e:
Third Creek WWTP
r:
WO0016247
e:
10/7/2013
e:
19.1
e:
10/7/13 9:48
y:
SA
e:
10/7/13 9:57
y:
SA
e:
300
e:
19
e:
18.7
Dissolved Oxygen Level
(mg/1)
8.03
8
7.96
7.94
7.9
7.88
7.86
7.55
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.0
1.0
-milliliters
®ry Solids
9egrees Celsius
Degrees Celsius
1.94 mg Oxygen/hr
0.36 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.38 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

(Yvp.e--ti�rt[CY.1'fi f roc �i
Time
(minutes)
0
2
3
4
5
6
7
9
10
11
12
13
14
15
Specific Oxygen -Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
_ � Total Solids
Beginning Temperature
End Temperature
Dissolves! Oxygen Level
7.93
7.9
7.86
F&I
7.76
7.74
7.72
7.71
67 8
7..65
7.61
7.56
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
10/9/2013
19.2
10/9/13 8:52
SA
1019/13 9:03
SA
300
19
18.8
0.0
7.9
1.0
rilliliters
%Dry Solids
legrees Celsius
legrees Celsius
1.40 mg Oxygen/hr
0.26 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.28 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Agricultural Lime Application Log
2013
Project: City of Statesville
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date Applied
(invoice date)
NC-IR-20-4A
6.8
N/A
N/A
N/A . .
NC-IR-20-4B
7.0
N/A
N/A
N/A_
NC-IR-23-1
6.4
N/A
N/A
N/A
NC-IR-23-2
5.9
0.0
N/A
N/A
NC-IR-23-3
7.0
N/A
N/A
N/A
NC-IR-23-4
6.8
N/A
N/A
N/A
NC-IR-23-5
6.2
N/A
N/A
N/A

NCDA&C--,,.anomIc Division - —= -Phone: ,(919)_=733.2655-
,Website:"www.ncagr.gov/agronomi
, "
Report'No. FY14-5LOZ6059'
Client: Dennis Phillips
Advisor:
Synagro Central
Predictive
201 Barry Oak Rd
Statesville, NC 28625
Attn:Eric Thompson
284 Boger Rd
j
Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
r
N
Sampled County: Iredell
N..lyic5i
Sampled: Received: 12/09/2013
Completed: 02/06/2014
Farm: 1 R-20
Links to Helpful Information
Sample ID: 4A
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1 0.0
120-200 0
90 0 0
pH$
0
0
0
Note: 12 Note:
2 - Fescue/OGrass/Tim, 0.0
120-200 0
90 0 0
pH$
0
0
0
Note: 12 Note:
Test Results [units - WN in g/crrrii; CEC and Na in meq/100 cm3; NO3-N in mg/drri]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.36 0.98
11.9 95 0.6 6.8 169 24
78 16
43 763 463 463
391
391
249
0.1 1
Sample ID: 4B
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim,1 0.0
120-200 0
70 0 0
pH$
0
0
0
Note: 12 Note:
2 - Fescue/OGrass/Tim, 0.0
120-200 0
70 0 0
pH$
0
0
0
Note: 12 Note:
Test Results [units - WN in g/crr?; CEC and Na in meq/100 cmP; NO3-N in mg/drrr3]:
. Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.27 0.94
27.0 98 0.6 7.0 319 33
85 13
77 146 90 90
697
697
345
0.1 0
North .Carollnai.
ob:icq:o Trust njul CwaniwsNkm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS A ,_
�mic Division Phone: [phone]
Website: www.nc
_ Dv/agronomi/
Report No. FY12 . 10607 .
Client:
Shane Porter
Advisor.
Synagro Central
g„u,Tc'.ur.
f E'
Predictive
351 Gantt Horn Rd.
STATESVILLE, NC 28677
Attn:Eric Thompson
284 Boger Rd
.r �..1
Mehlich-3
Soil i I Report
Extraction
Mocksville, NC 27028
-
County:
-Jredell
Links to
Helpful Information
Sampled. 04/13/2013 Received:04130/2013
Completed:05/06/2013
IFarm:
Sample ID: 1
Recommendations: Lime
Nu t ients (lb/acre)
( )
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fes/OG/Tim,M 0.0
120-200 0
70
0 0
0
0
0
0
Note: 12
2 - Fes/OG/Tim, M 0.0
120-200 0
70
0 0
0
0
0
0
Note: 12
Test Results [units - WN in g/criti3; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil -Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.46 0.98
11.1 91 1.0 6.4 138 34
77 13
38
141
96 96
225
225
190
0.1 1
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fes/OG/Tim,M 0.0
120-200 0
0
0 0
0
0
0
0
Note: 12
2 - Fes/OG/Tim,M 0.0
120-200 0
0
0 0
0
0
0
0
Note: 12
Test Results [units - WN in g/cd; CEC and Na in meg1100 cirt3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac rpH -1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.51 1.00
11.8 87 1.6 t 5.9 453 146
67 14
56
376
243 243
283
283
213
0.1 1
Sample ID: 4
Recommendations- Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg S
Mn
Zn
Cu
B Information
Lime History:
1-Fes/OG/Tim,M 0.0
120-200 0
0
0 0
pH$
0
0
0 Note: 12 Note:
2- Fes/OG/Tim,M 0.0
120-200 0
0
0 0
pH$
0
0
0 Note: 12 Note: $
Test Results [units - WN in g/crrr3; CEC and Na in meg1100 crrr3; NO3-N in mg/dnr3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-14
0.41 1.08
16.4 97 0.5 6.8 294 97
82 12
49
233
145 145
414
414
249
0.1 1
,-I orth Cat -at na
Tobacco Trust PwtdCi m 1wisslc,a.
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS k.._..imic Division Phone: [phone]
Website: www.n6-,..yov/agronomi/
Report No.
FY1i,-:,--�10607 '
Shane Porter
Page 2 of 3
Sample ID: 5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6 K2O
Mg
S
Mn
Zn
Cu B
Information l
Lime History:
1-Fes/OG/Tim,M 0.0
120-200 0 0
0
0
0
0
0 0
Note: 12
2 - Fes/OG/Tim, M 0.0
120-200 0 0
0
0
0
0
0 0
Note: 12
Test Results [units - WN in 9/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dni]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-I
Ca% Mg% S-1 Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-H
0.46 0.93 14.4 91 1.3 6.2 309 198
71 13 46 166
113
113
471
471
252 0.1
1

NCDA&CS �_�___ )mic Division
Phone: [phone] Website: www.n.,..y..yov/agronomi/
Client: Shane Porter
Predictive 351 Gantt Horn Rd.
Soil
Statesville, NC 28677
S ®i l Report Mehlich-3 Extraction
County: Iredell
Sampled: Received:07/15/2013 completed:07/17/2013 Farm: IR-23
Sample ID: 3 Recommendations: Lime Nutrients (lb/acre)
Report No.. FY1d. _-_J0592
Advisor. Synagro/J Blackwell
284 Boger Rd
Mocksville, NC 27028
Links to Helpful Information
More
Crop
(tons/acre) N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fes/OG/Tim,M
0.0 120-200 0
0
0
0
pH$
0
0 0
Note: 12 Note:I
2 - Fes/OG/Tim,M
0.0 120-200 0
0
0
0
pH$
0
0 0
Note: 12 Note: _.
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dnf]:
Soil Class:
Mineral
d
HM% W/V
CEC BS% Ac pH
P-1 K-1 Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-Al
Cu-I Na ESP SS-1 NO3-F;I
d
0.36 1,03
16.2 99 0.2 7.0
325 121 82 13 53
334
203
203
427
427
211 0.1 1 _
,Aaah Carolina
-L„
16bacco Trust Pwid Comniisslon
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture