WQ0016247_Regional Office Historical File Pre 2018 (15)

Schutte, Maria
From: Schutte, Maria
RECEIVED/NCDENR/DWR
Sent: Monday, May 01, 2017 5:08 PM MAY 1 20V
To: 'Erik Bruce'
Cc: - '[e-mail]'; '[e-mail]' WQROS
Subject: RE: Synagro Class B annual report MOORESVILLE REGIONAL OFFICE
Erik,
Upon review the attachments and your response adequately meet the additional information request. I have no further
questions.
Maria
From: Erik Bruce [mailto:[e-mail]]
Sent: Monday, May 01, 2017 3:39 PM
To: Schutte, Maria <[e-mail]>
Subject: Synagro Class B annual report
Enclosed is the missing Sour Test reports for Statesville 4th Creek, the ESP results for Stanly soil tests, and the bench
sheet for Stanlys 30 day bench test. After speaking with Patrick Mitchell today, the CEC levels on these soil reports are
normal for the region and soil types, and have no bearing on land application. Lime will be purchased for Statesville as
soon as the lime vendors are done spreading.cropland fertilizer. Any further questions feel free to contact me.
Thanks,
Erik
Your Partner for a cleanser, greener world
Erik Bruce
Technical Services Specialist
284 Boger Road Mocksville, NC 27028
0: 1-336-790-1610 1 M: 1-336-703-8681
[e-mail] I www.synagro.com
Facebook I Twitter I Linkedin
1

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling: Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
4/8/2016
19
4/8/16 1:00 PM
RW
4/8/16 1:11 PM
BJ
300 milliliters
17.5 degrees Celsius
17.4 degrees Celsius
Time Dissolved Oxygen Level
(minutes)
0-
1 -:
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Slope: 0.0 0
Intercept: 9.6
Correlation Coefficient: 0.9
Oxygen Uptake. Rate:. 1.48 mg.Oxygen/hr
Ambient Specific Oxygen Uptake Rate:. 0:27 mg Oxygen/g/hr
-Average Temperature: 17 degrees Celsius
Temperature Correction. Factor: 1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.33 m"Img Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End. Temperature:
r
h Creek WWTP
4/11/2016
19.3
1/16 1:00 PM
LC
1/16 1:09 PM
BJ
.300 milliliters
1.9.5 degrees Celsius
17.8 degrees Celsius
Time. Dissolved Oxygen Level
(minutes) (mg/1)
0 5.64
1 5.82
2 6.07
3 6.18
4 6.18
5 6.16
6 6.14
..7 6.08
8 6.06
9 5.93
10 5.89
11 5.86
12 5.76
13 5.79
14 5.71
15 5.69
Slope:
- 0.0
Intercept:
6.1
Correlation Coefficient:
0.4
.Oxygen Uptake.Rate:
1.04 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.21 mg Oxygen/g/hr
Average Temperature:
19 degrees Celsius
Temperature Correction Factor:
1.07
Temperature Corrected Specific
Oxygen Uptake Rate: 0`22 mg Oxygen/g/hr. .
Instructions: Enter. Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
-Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
a
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
10/10/2016
17.7
10/10/16 12:36 PM
LC
10/10/16 12:44 PM
BJ -
300 milliliters
i
17.2 degrees Celsius
18 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/1)
0 8.97
1 8.94
2 8.89
3 8.85
4 8.83
5 8.78
6 8.76
7 8.72
8 8.68
9 8.65 ...
10 8.62
11 8.6
12 8.58
13 8.55
14 8.53
15 8.51
Slope:
0.0
Intercept:.
8.9
Correlation Coefficient:
1.0
Oxygen Uptake Rate:
1.87 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.42 mg Oxygen/g/hr
Average Temperature:
18 degrees Celsius
Temperature Correction Factor:
1.1449
Temperature Corrected. Specific
Oxygen Uptake Rate:1 0.48 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
10/11/2016
16.3
10/11/16 1:06 PM
LC
10/11/16 1:11. PM
BJ
300 Imilliliters
16.4 degrees Celsius
17.5 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/1)
0 8..75
1 8.67
2 8.6
3 8.56
4 8.51
5. 8.46
6 8.41
7 8.38
8 8.33
9 8.29
10 8.23
11 8.2
12 8.18
13 8.13
14 8.07
15 8.01
Slope:. 0.0
Intercept: 8.7
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.75 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.59 mg Oxygen/g/hr
Average Temperature: 17 degrees Celsius
Temperature Correction Factor: 1.225043.
Temperature Corrected Specific Oxygen Uptake Rate:1 0.73 - mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

PAR
LABORATORIES, INC
W W W.PARLABS.COM
Crucible
Tare VJt (g)
Sample(g)
Dried Wt(g)
Burned Wt(g)
TS%
VS%
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
�•' SYNAGRO
WEST STANLEY UTILITIES 50-2170
122419
• 02/23/16
03122/16
As Received Day 0 Day 7 Day 14 Day 21
X9
X18
X35
X24
21.4728
21.5536
27.8390
21.2210
35.3923
35.3751
41.3580
34.4846
21.6371
21.7181
27.9999
21.3802
21.5211
21.6021
27.8892
21.2715
#DIV/01
1.18%
1.19%1
1.19%1
1.20%
70.60 %
70.52 %
68.80 %
68,28
0.003277549
x
0,001364704
TS (g
0.1643
VS g
0.116
Volatile Fraction In 0.59815
Na If.. 411483 •Chsstatta NC:8241-1493
Me- [phone] 6 Fax: [phone]
Volatile Fraction Out
Day 28
03/22/16
X9
21.4714
35.3633
21.6367
21.5241
1.19%
68.12
0.003184092
0.001490246
0.1653
0.1126
0.57247

Fj
nr�
P FiOMPT• AC G U RATE • i2E1..lAF] i_E.
LA.130RATaRIES, INC _. .
W W W. PARLABS.COM
Crucible
Tare Wt (g)
Sample(g)
Dried Wt(g)
Burned Wt(g)
TS%
VS%
30 ®ay Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
WEST STANLEY UTILITIES 50-2170
122419
02123/16
03/22/16
As Received Day 0 Day 7 Day 14 Day 21
02/23116 03/01/16 03108116 03/15116
X9
X18
X36
X24
21.4728
21.5536
27.8390
21.2210
35.3923
35.3751
41.3580
34.4846
21.6371
21.7181
27.9999
21.3802
21.5211
21.6021
27.8892
21.2715
#DIV/0!
1.18%
1.19%
1.19%
1.20%
70.60%
70.52%
68.80%
68.28%
0.003277549
x
0.001364704
TS
0.1643
VS
0.116
Volatile Fraction In 0.59815
PO.11ax 41141?3 * Oariotm NC; 28241,148,
Phone: [phone] ra.- [phone]
x
TS
VS
Volatile Fraction Out

Day 28
03122/16
X9
21.4714
35.3633
21.6367
21.5241
1.19%
68.12%
0.003184092
0.001490246
0.1653
0.1126
0.57247

West Stanly Utilities 2016 Soil ESP
Field Na (PPM) Na (meq/100g) CEC (meq/100g) ESP
NC-ST-03 19 0.1 6.4 1.3
Equations: Na (meq/100g)= (Na PPM x 2)/460
ESP=((Na meq/100g)/CEC) x 100

Schutte, Maria
Fro;.:: Schutte, Maria
Sent: Thursday, April 13, 2017 7:44 PM
To: [e-mail]'
Cc: '[e-mail]'
Subject: WQ0016247 Synagro Western Regional Residuals 2016 Annual Report - Receipt and
Request for Additional Information
Nate,
The Mooresville Office received a copy of the referenced Annual Report on March 6th, 2017. Please email me the
additional information:
• The ESP (Exchangeable Sodium Percentage) is not being reported on the Waypoint Labs soil reports. Please
send the data for each affected field and make a note to correct this in future reports.
• Some soils reports show elevated CECs. It is recommended you discuss sites at 15% or above with a soil scientist
or agronomist for evaluation. Please forward their findings to me. A once/permit cycle evaluation of this type
of situation is acceptable for each field.
• Has lime been applied? Please send your updated lime application log for years 2015 & 2016 (to include Iredell
and Stanly county land).
• Verify the 30day bench for the West Stanly plant meets the lab procedure, as the testing dates reported appear
to be less than 30days.
• Verify all the SOUR testing from Statesville was included. The copy received has 7 sample results for some qtrs.,
5 for another and 3 for yet another.
Please contact me with any questions.
Sincerely,
Maria
Maria Schutte
Environmental Specialist
Water Quality Regional Operations Section
Division of Water Resources
North Carolina Department of Environmental Quality
704 663 1699 office
704 235 2184 direct
Maria.schutteCc7ncdenr.gov
610 East Center Avenue
Suite 301
Mooresville, NC 28115
-�5--Nothlng Compares,.,-

Email correspondence to and from this address is subject to the
North Carolina Public records Lair and may he disclosed to third parties.

RECEIVED/NCDENR/DWF;
MAR - 6 2017
WQROS
MOORESVILLE REGIONAL OFFICE
V
Pr,
0 2®1,
lrf�f> j�tion Fir
°C,qg UricCn
Western Piedmont Regional, NC
Class B Residuals Land Application Program
Permit No. WQ0016247'
2016 ANNUAL REPORT

Western Piedmont Regional, NC
Class B Residuals Land Application Program
2016 Annual Report
TABLE OF CONTENTS
1. Certification Form
2. City of Statesville
3. Stanly County Utilities

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00016247 County Alexander Year 2016
Facility Name (as shown on permit) West Stanly WWTP, City of Statesville, Third Creek WWTP & Fourth Creek WWTP NPDES
No. NC0043532, NC0020591, & NCO031836
Land Application Operator S nagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summ
Total number of application fields in the permit: 55
Total number of fields utilized for land application during the year: 7
Total amount of dry tons applied during the year for all application sites: 434.25
Total number of acres utilized for land application during the year: 184.2
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2016 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached:
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, ' 1 * g e possib' i es and imprisonment for
knowing violations."
Todd Larson, Operations Director
Permittee Name and Title (type or print) Signature of Permittee Date
Signature of Preparer*
(if different from Permittee)
Date Signature of Land Applier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2016 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
STATESVILLE, NC
STATESVILLE, NC
FOURTH CREEK CAKE
DRY METRIC
MONTHNEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
January 2016
1,530.00
Y
165.20
D
149.83
April 2016
1,347.00
Y
145.43
D
131.91
October 2016
960.00
Y
103.66
D
94.01
YEARLY TOTAL
3,837.00
Y
414.29
D
375.75
2/1 /2017

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
FacmtyNUmber: WQ0016247
Np Name: STATESVILLE, NC
orVV* :
QNCO031836
*V�1'p (residual only)
Name: FOURTH CREEK
�pat�SUctt4ap0Analysis Data
Pete 0o�ple0 (grab) or
r
oeht SPNted
CAK CAK
01/06/16 12/28/16
P gas
A1�
caq�i METERS (mg/kg dry weight)
erg urn
U
Cola hrorn.
keaPerurn
cl
S cke de/Vih4rh
Trnceh�4fi
9 �ti phis
\ p o
r48
\`aha � �r9en
12.82 14.32
Laboratory
Waypoint Analytical Virginia Inc.
WAYPOINT ANALYTICAL
CAK CAK
12/29/16 12/30/16
13.23 13.70
4
5.47
4.45
4.62
3
2.73
2.97
3.16
0.6
1.25
1.19
<0.4
62
34.2
41.3
36.6
360
252
266
269
29
20.9
20.5
20.5
14
9.18
11.2
10.5
35
22.2
26.5
25.4
<5
<5
5.22
6.28
582
576
633
644
29300
24400
25700
26100
59400
49500
54300
53800
7720
5440
5210
5470
<2
<11
26.4
<2.04
of law, that this document was prepared under my direction or supervision in accordance with a system
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
ubmitting false information, including the possibility of fines and imprisonment for knowing violations."
Date 0)/ / -111
03)
Printed: Wednesday - February 1 2017 at 10:20.31 for: 2084 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type CAK CAK
Date Sampled (grab) or 01/06/16 12/28/16
Date Composited
Percent Solids 12.82 14.32
PARAMETERS (mg/kg dry weight)
Laboratory
Waypoint Analytical Virginia Inc.
WAYPOINT ANALYTICAL
CAK CAK
12/29/16 12/30/16
13.23 13.70
Aluminum
27000
29300
33800
32700
Calcium
10600
7710
8770
8740
Magnesium
2260
2130
2390
2410
pH
7.14
6.04
6.95
6.90
Potassium
2710
2950
3640
3490
Sodium
749
605
620
668
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
A .�
MW
PREPARER)
NR - Data Not Reported or Data Not Required
Date �// 3�(
DENR FORM RSSF-B (7/2002) Printed: Wednesday*- February 1, 2017 at 10:21:03 for: 2084 01

Page: 1 of 2
Report Number: 16-007-0218
Account Number: 46493
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 66081
Sample Id: STATESVILLE 4TH CREEK
o
Waypoint,�
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: STATESVILLE 4TH CREEK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/6/2016 12:00:00
Date Received: 01/07/2016 00:00
Date Reported: 01/14/2016
Total Solids *
12.82
128200
100.0
JM
01/07/2016 15:00
SM-2540G
Moisture *
87.18
100.0
JM
01/07/2016 15:00
SM-2540G
Total Kjeldahl Nitrogen
5.94
59400
10.0
JM
01/11/2016 08:30
SM-4500-NH3C-TKN
Total Phosphorus
2.93
29300
100
KM
01/08/2016 11:19
SW 6010C
Total Potassium
0.27
2710
100
KM
01/08/2016 11:19
SW 6010C
Total Sulfur
0.91
9140
100
KM
01/08/2016 11:19
SW 6010C
Total Calcium
1.06
10600
100
KM
01/08/2016 11:19
SW 6010C
Total Magnesium
0.23
2260
100
KM
01/08/2016 11:19
SW 6010C
Total Sodium
0.07
749
100
KM
01/08/2016 11:19
SW 6010C
Total Iron
24100
100
KM
01/08/2016 11:19
SW 6010C
Total Aluminum
.27000
100
KM
01/08/2016 11:19
SW 6010C
Total Manganese
954
5
KM
01/08/2016 11:19
SW 6010C
Total Copper
360
5
KM
01/08/2016 11:19
SW 6010C
Total Zinc
582
5
KM
01/08/2016 11:19
SW 6010C
Ammonia Nitrogen
0.77
7720
10.0
JM
01/11/2016 08:30
SM-4500-NI3C
Organic N
5.17
51680
10.0
01/11/2016 08:30
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
01/08/2016 08:50
SM-4500NO3F
Total Cadmium
3.0
2.0
KM
01/08/2016 11:19
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ,
to the work: the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 16-007-0218
Account Number: 46493
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 66081
Sample Id : STATESVILLE 4TH CREEK
D
Waypoin(t,"
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: STATESVILLE 4TH CREEK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/6/2016 12:00:00
Date Received: 01/07/2016 00:00
Date Reported: 01/14/2016
Total Chromium
62
5
KM
01/08/2016 11:19
SW 6010C
Total Nickel
35
5
KM
01/08/2016 11:19
SW 6010C
Total Lead
29
5
KM
01/08/2016 11:19
SW 6010C
Total Arsenic
4.0
3.0
KM
01/08/2016 11:19
SW 6010C
Total Mercury
0.6
0.4
KM
01/08/2016 09:00
SW-7471B
Total Selenium.
<5.0
5.0
KM
01/08/2016 11:19
SW 6010C
pH (Standard Units) *
7.14
2.00
JM
01/08/2016 08:50
SW-9045D
Total Molybdenum
14
5
KM
01/08/2016 11:19
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE V6/2016 1/1/2016-12/31/2016 0.6152
Na mg/I = (Na mg/kg x % Solids) _ 100 = (749 x 12.8200) = 100 = 96.0218
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10600 x 12.8200) = 100 = 1358.92
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2260 x 12.8200) = 100 = 289.732
Na meq = Na mg/I = Molec.Wgt.Na = 96.0218 = 23 = 4.17486
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 1358.92 _ 20 = 67.946
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 289.732 = 12 = 24.1443
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.17486 = SgrRoot[0.5(67.946+24.1443)] = 0.615248
Printed: 2/1/2017
Page 1 11:44

Page: 1 of 2
Report Number: 17-003-0207
Account Number: 46493
Submitted By: Erik Bruce
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61397
Sample Id : Statesville 4th Creek
•
Waypoin(2t,M
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OF ANALYSIS Date Sampled: 12/28/2016 09:00:00
Date Received: 01/03/2017 00:00
Date Reported: 01/11/2017
Total Solids *
14.32
143200
100.0
BW1
01/03/2017 16:30
SM-254OG
Moisture *
85.67
100.0
BW1
01/03/2017 16:30
SM-254OG
Total Kjeldahl Nitrogen
4.95
49500
10.0
JM
01/04/2017 11:35
SM-4500-NH3CJKN
Total Phosphorus
2.44
24400
100
JTR
01/06/2017 02:19
6010C
Total Potassium
0.30
2950
1000
JTR
01/06/2017 02:24
6010C
Total Sulfur
0.61
6060
100
JTR
01/06/2017 02:19
601.00
Total Calcium
0.77
7710
100
JTR
01/06/2017 02:19
601 OC
Total Magnesium
0.21
2130
100
JTR
01/06/2017 02:19
601 OC
Total Sodium
0.06
605
100
JTR
01/06/2017 02:19
601 OC
Total Iron
23300
100
JTR
01/06/2017 02:19
601 OC
Total Aluminum
29300
100
JTR
01/06/2017 02:19
601 OC
Total Manganese
1980
5.00
JTR
01/06/2017 02:19
601 OC
Total Copper
252
5.00
JTR
01/06/2017 02:19
601 OC
Total Zinc
576
5.00
JTR
01/06/2017 02:19
601 OC
Ammonia Nitrogen
0.54
5440
10.0
JM
01/04/2017 09:50
SM-4500-NH3C
Organic N
4.41
44060
10.0
01/04/2017 09:50
CALCULATION
Nitrate+Nitrite-N
<11.0
11.0
SJB
01/05/201712:38
450ONO3F-2011
All values are on a dry weight basis•except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced In whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Page: 2 of 2
Report Number: 17-003-0207
Account Number: 46493
Submitted By: Erik Bruce
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61397
Sample Id : Statesville 4th Creek
•
Waypoin(2t,w
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OF ANALYSIS Date Sampled: 12/28/2016 09:00:00
Date Received: 01/03/2017 00:00
Date Reported: 01/11/2017
Total Cadmium
2.73
Total Chromium
34.2
Total Nickel
22.2
Total Lead
20.9
Total Arsenic
5.47
Total Mercury
1.25
Total Selenium
<5.00
pH (Standard Units) *
6.04
Total Molybdenum
9.18
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
2.00
JTR
01/06/2017 02:19
6010C
5.00
JTR
01/06/2017 02:19
6010C
5.00
JTR
01/06/2017 02:19
6010.0
5.00
JTR
01/06/2017 02:19
6010C
3.00
JTR
01/06/2017 02:19
6010C
0.400
JM
01/10/201713:00
SW-7471B
5.00
JTR
01/06/2017 02:19
6010C
1.00
JM
01/04/2017 09:50
SW-9045D
5.00
JTR
01/06/2017 02:19
6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 12/28/2016 / / - / / 0.5933
Na mg/I = (Na mg/kg x % Solids) _ 100 = (605 x 14.3200) = 100 = 86.636
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (7710 x 14.3200) = 100 = 1104.07
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2130 x 14.3200) _ 100 = 305.016
Na meq = Na mg/I _ Molec.Wgt.Na = 86.636 _ 23 = 3.76678
Ca meq = Ca mg/I = Molec.Wgt.Ca = 1104.07 _ 20 = 55.2036
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 305.016 _ 12 = 25.418
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.76678 _ SgrRoot[0.5(55.2036+25.418)] = 0.59328
Printed: 2/1/2017
Page 1 11:45

Page: 1 of 2
Report Number: 17-006-0205
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61530
Sample Id : Statesville 4th Creek
•
Waypdin(2t.�
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OFANALYSIS Date Sampled: 12/29/2016 13:00:00
Date Received: 01/06/2017 00:00
Date Reported: 01/13/2017
Total Solids *
13.23
132300
100.0
BW1
01/06/2017 15:00
SM-2540G
Moisture *
86.76
100.0
BW1
01/06/2017 15:00
SM-2540G
Total Kjeldahl Nitrogen
5.43
54300
10.0
SJB
01/12/2017 09:00
SM-4500-NH3C-TKN
Total Phosphorus
2.57
25700
100
JTR
01/10/2017 20:26
6010C
Total Potassium
0.36
3640
1000
JTR
01/10/2017 20:31
6010C
Total Sulfur
0.64
6380
100
JTR
01/10/2017 20:26
6010C
Total Calcium
0.88
8770
100
JTR
01/10/2017 20:26
6010C
Total Magnesium
0.24
2390
100
JTR
01/10/2017 20:26
6010C
Total Sodium
0.06
620
100
JTR
01/10/2017 20:26
6010C
Total Iron
23000
100
JTR
01/10/2017 20:26
6010C
Total Aluminum
33800
100
JTR
01/10/2017 20:26
6010C
Total Manganese
2190
5.00
JTR
01/10/2017 20:26
6010C
Total Copper
266
5.00
JTR
01/10/2017 20:26
6010C
Total Zinc
633
5.00
JTR
01/10/2017 20:26
6010C
Ammonia Nitrogen
0.52
5210
10.0
SJB
01/09/2017 09:55
SM-4500-NI3C
Organic N
4.91
49090
10.0
01/09/2017 09:55
CALCULATION
Nitrate+Nitrite-N
26.4
2.11
SJB
01/11/201713:56
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, orother public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Page: 2 of 2
Report Number: 17-006-0205
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61530
Sample Id : Statesville 4th Creek
Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OFANALYSIS Date Sampled: 12/29/2016 13:00:00
Date Received: 01/06/2017 00:00
Date Reported: 01/13/2017
Total Cadmium
2.97
Total Chromium
41.3
Total Nickel
26.5
Total Lead
20.5
Total Arsenic
4.45
Total Mercury
1.19
Total Selenium
5.22
pH (Standard Units) *
6.95
Total Molybdenum
11.2
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
2.00
JTR
01/10/2017 20:26
6010C
5.00
JTR
01/10/2017 2026
6010C
5.00
JTR
01/10/2017 20:26
6010C
5.00
JTR
01/10/2017 20:26
6010C
3.00
JTR
01/10/2017 20:26
6010C
0.400
JM
01/12/201713:00
SW-7471B
5.00
JTR
01/10/2017 20:26
6010C
1.00
SJB
01/09/2017 09:55
SW-9045D
5.00
JTR
01110/2017 20:26
6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
i
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 12/29/2016 / / - / / 0.5491
Na mg/I = (Na mg/kg x % Solids) = 100 = (620 x 13.2300) = 100 = 82.026
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (8770 x 13.2300) _ 100 = 1160.27
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2390 x 13.2300) _ 100 = 316.197
Na meq = Na mg/I _ Molec.Wgt.Na = 82.026 = 23 = 3.56635
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 1160.27 _ 20 = 58.0135
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 316.197 _ 12 = 26.3498
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.56635 _ SgrRoot[0.5(58.0135+26.3498)] = 0.549113
Printed: 2/1/2017
Page 1 11:45

Page: i of 2
Report Number.: 17-006-0206
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61531
Sample Id : Statesville 4th Creek
D
Waypoin(trM
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OFANALYSIS Date Sampled: 12/30/2016 10:00:00
Date Received: 01/06/2017 00:00
Date Reported: 01/13/2017
Total Solids *
13.70
137000
100.0
BW1
01/06/2017 15:00
SM-2540G
Moisture *
86.29
100.0
BW1
01/06/2017 15:00
SM-2540G
Total Kjeldahl Nitrogen
5.38
53800
10.0
SJB
01/12/2017 09:00
SM-4500-NH3C-TKN
Total Phosphorus
2.61
26100
100
JTR
01/10/2017 20:49
6010C
Total Potassium
0.35
3490
1000
JTR
01/10/2017 20:36
601 OC
Total Sulfur
0.65
6510
100
JTR
01/10/2017 20:49
601 OC
Total Calcium
0.87
8740
.100
JTR
.01/10/2017 20:49
6010C
Total Magnesium
0.24
2410
100
JTR
01/10/2017 20:49
6010C
Total Sodium
0.07
668
100
JTR
01/10/2017 20:49
601 OC
Total Iron
22800
100
JTR
01/10/2017 20:49
6010C
Total Aluminum
32700
100
JTR
01/10/2017 20:49
601 OC
Total Manganese
2210
5.00
JTR
01/10/2017 20:49
601 OC
Total Copper
269
5.00
JTR
01/10/2017 20:49
601 OC
Total Zinc
644
5.00
JTR
01/10/2017 20:49
6010C
Ammonia Nitrogen
0.55
5470
10.0
SJB
01/09/2017 09:55
SM-4500-NI3C
Organic N
4.83
48330
10.0
01/09/2017 09:55
CALCULATION
Nitrate+Nitrite-N
<2.04
2.04
SJB
01/11/201714:00
450ONO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Page: 2 of 2
Report Number: 17-006-0206
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61531
Sample Id : Statesville 4th Creek
D
Waypoint(
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OF ANALYSIS Date Sampled: 12/30/2016 10:00:00
Date Received: 01/06/2017 00:00
Date Reported: 01/13/2017
Total Cadmium
3.16
2.00
JTR
01/10/2017 20:49
6010C
Total Chromium
36.6
5.00
JTR
01/10/2017 20:49
6010C
Total Nickel
25.4
5.00
JTR
01/10/2017 20:49
6010C
Total Lead
20.5
5.00
JTR
01/10/2017 20:49
6010C
Total Arsenic
4.62
3.00
JTR
01/10/2017 20:49
6010C
Total Mercury
<0.400
0.400
JM
01/12/201713:00
SW7-7471B
Total Selenium
6.28
5.00
JTR
01/10/2017 20:49
6010C
pH (Standard Units) *
6.90
1.00
SJB
01/09/2017 09:55
SW-9045D
Total Molybdenum
10.5
5.00
JTR
01/10/2017 20:49
6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 12/30/2016 / / - / / 0.6020
Na mg/1 = (Na mg/kg x % Solids) + 100 = (668 x 13.7000) + 100 = 91.516
Ca mg/1= (Ca mg/kg x % Solids) + 100 = (8740 x 13.7000) + 100 = 1197.38
Mg mg/1 = (mg mg/kg x % Solids) + 100 = (2410 x 13.7000) + 100 = 330.17
Na meq = Na mg/1 + Molec.Wgt.Na = 91.516 + 23 = 3.97896
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1197.38 + 20 = 59.869
Mg meq = Mg mg/I + Molec.Wgt.Mg = 330.17 + 12 = 27.5142
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.97896 + SgrRoot[0.5(59.869+27.5142)] = 0.601964
Printed: 2/1/2017
Page 1 11:46

FACILITYNAME: STATESVILLE,NC
DWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0004 A
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 95.02
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 44.20 ACRES PERMITTED: 44.20
Page
Lnne Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
all-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
10/25/16
460.00 (CY)
10.407
12.82
1.124
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
FESCUE HAY
10/26/16
420.00 (CY)
9.502
12.82
1.026
STFCC
DRY
0-<1/2"
1 SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
FESCUE HAY
Oct-16
880.00 (CY)
19.909
ToW ('.11hir..Y(IR/Ac• io ni
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs/acre
83
0.017
0.013
0.267
1.548
0.125
0.003
0.060
0.150
0.022
2.502-
125.97
Cumulative Ibs/acre
0.148
0.210
1.915
12.163
1.829
0.041
0.453
1.221
0.130
24.425
4
�'
'ermit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
4 r"
f }
r �x
d
9 a
t
216
,`
n
k
i t
k .:A
3
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
I
1` '
{
1339.0
267.9
15.0 375.0
k.+7�
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X
(SIGNATURE F LAND APPLIER) DATE
"I certify unde. penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

FACILITY NAME: STATESVILLE, NC
DWNER: DENNIS PHU-LIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0004 B
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 8.64
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.60 ACRES PERMITTED: 11.60
Page : 1
Lane Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acre
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-) .
Crop
10/26/16
80.00 (CY)
6.897
12.82
0.745
STFCC
DRY
0-<1/2"
SUR
0.5
0.30[7�17,720.00
p
2.00 p
FESCUE HAY
Oct-16
80.00 (CY)
6.8971
1
1
11
1
F366
Total Cubic Yds/Ac: 6.90
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annual lbs/acre 29
0.006 0.004 0.092 0.536 0.043 <.001 0.021 0.052 0.007 0.867 43.64
Cumulative lbs/acre. 0.130 0.175 1.711 11.320 1.757 0.047 0.373 1.052 0.099 21.957 t
?ermit PAN Limit (lbs/acre) 1st Crop/2nd Cropff
°
121
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
r r
1339.0
267.9
x
15.0 7 375.0
89.0
2500.0 L M
"'l
a
i
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
(SIGNATURE OF L APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS PHILLIPS PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 145.44
SITE #: NC IR 00020 FIELD# : IR 00020 0011 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 41.60 ACRES PERMITTED: 41.60
Page: 1
Lune Applied ***
Date Lbs/Ac
DATE or
DATE
MONTH
allons (G) or Cubic Yards (CY)
Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
m
(pp )
Crop
p
Total
Per Acre
4/25/16
225.00 (CY)
5.409
12.82
0.584
STFCC
DRY
0-<I/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
I FESCUE
4/26/16
330.00 (CY)
7.933
12.82
0.857
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
I FESCUE
4/27/16
330.00 (CY)
7.933
12.82
0.857
STFCC
DRY
0-<I/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
Ij FESCUE
4/28/16
279.00 (CY)
6.707
12.82
0.724
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
I FESCUE
4/29/16
183.00 (CY)
4.399
12.82
0.475
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
FESCUE
Apr-16
1,347.00 (CY)
1 32.381
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
135
0.028
0.021
0.434
2.517
0.203
0.004
0.098
0.245
0.035
4.070
204.88
Cumulative lbs/acre
0.105
0.108
1.273
8.719
0.851
0.045
0.334
0.890
0.111
14.776
y
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
t' %i
1;
216
r
t
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
r
1339.0
267.9
15 0
375.0
89.0
2500.0
5
STFCC = STATESVILLE, NC FOURTH CREEK CAFE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACILTTY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
)WNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 110.67
;ITE #: NC IR 00023 FIELD# : IR 00023 0002 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
tESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 32.40 ACRES PERMITTED: 32.40
Page: 1
Lune Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or
or Wet Tons (WT) (specify)
Solids
Dry
Tons
Per
Residual
Site
Cond,
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
MONTH
Per Acre
1/13/16
300.00 (CY)
9.259
12.82
1.000
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
I FESCUE
1/14/16
725.00 (CY)
22.377
12.82
2.416
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
FESCUE
Jan-16
1 1,025.00 (CY)
31.636
1
i-_. 1 ivai
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
132
0.027
0.021
0.424
2.459
0.198
0.004
0.096
0.239
0.034
3.976
200.17
Cumulative lbs/acre
0.163
0.318
2.844
17.258
3.035
0.051
0.654
1.563
0.197
34.176
$
`
'ermit PAN Limit lbs/acre /2nd
F
o- {
3 x
a
21G
1st Cro Crop
( ) P p
Ip
lk
s
t
9
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
x
1339.0
267.9
15.0 375.0
89.0
2500 0
'
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X 243-O i
(SIGNATURE APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 8.10
SITE #: NC IR 00023 FIELD# : IR 00023 0004 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.70 ACRES PERMITTED: 13.70
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
DATE or
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
1/20/16
75.00 (CY)
5.474
12.82
0.591
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
p
2.00 p
19366
FESCUE
Jan-16
75.00 (CY)
5.474
[7�7,720.00
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
23
0.005
0.004
0.073
0.426
0.034
<.001
0.017
0.041
0.006
0.688
34.64
Cumulative lbs/acre
0.097
0.112
1.257
8.721
0.923
0.038
0.330
0.816
0.131
17.358
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
h (1
216
3
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
�P 1
71
s
t
;
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X Z-13.12
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

FACILITY NAME: STATESVILLE, NC
OWNER: LORANE PAGE
SITE #: NC IR 00023 FIELD# : IR 00023 0005
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 46.43
OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 16.10 ACRES PERMITTED: 16.10
Page: I
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
1/15/16
130.00 (CY)
8.075
12.82
0.872
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19366
I FESCUE
1/20/16
300.00 (CY)
18.634
12.82
2.012
STFCC
MOIST
0-<I/2"
SUR
0.5
0.30
59,400. p
7,720.00 p
2.00 p
19316
FESCUE
Jan-16
1 430.00 (CY)
1 26.709
1
Total Cubic Yds/Ac: 26.71
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.023 0.017 0.358 2.076 0.167 0.003 0.081 0.202 0.029 3.357 168.99 112
Cumulative lbs/acre 0.145 0.191 2.184 13.463 1.701 0.054 0.535 1.295 0.183 26.316 y ,
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
a t;°'
`av
J :
g 1
r 9 t ti 1 k
216
_
r
44
. i .-mac.]. �
i .4 o r_
.Ji': }
n .�.✓ � . ,i
,�;' �. ..W
{ ', ^ +r
i
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
(
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X 2�13vP 7
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be.applied in 2017

F6s"rIRC?tJfaSE1d5'ftLS_�i-f€�fSLi�st=�; �td�,
ArraPf,i;ca1 LSe :7r2tpr'!'e5
January 19, 2016
Marshall Puryear
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Statesville 4th Creek
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Dear Marshall Puryear: Order No.: 16010277
Summit Environmental Technologies, Inc. received 1 sample(s).on 1/7/2016 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
r
Bachar Najm
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank)
3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099,
New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma
9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L,
USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 9

Summit Environmental Technologies, Inc. N
S U £ 3310Win St.
Case Narrative
MVIROWNiEtdluLI-ECH4OWGiEs,;etc_ Cuyahoga Falls, Ohio44223 WO#: 16010277
rr3f,,frcal La aarairpe s TEL: [phone] FAX.- [phone]
Website: http://wwiv.setiek.com Date: 1/19/2016
CLIENT: Synagro
Project: Statesville 4th Creek
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway
Haddock, GA 31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vaiy at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency.
Any comments or problems with the analytical events associated with this report are noted below.
Analytical Comments for tclp-svoc-herb_tclp(8151), Sample lcs-18001, Batch ID 18001 : The TCLP
Herbicides LCS (Batch 18001) exhibited slightly high recovery for 2,4-D; All samples were ND.
Original
Page 2 of 9

Summit Environmental Technologies, Inc.
3310WinSt. Case Narrative
arrative
if
FIVIRONMEK,rAL _ �teer�La�tcs, wr_ Cuyahoga Falls, Ohio 44223 WO#: 16010277
Ar.,Hllytirsl' LaharaiDr�- TEL: [phone] FAX.- [phone]
Website: httD://wwiv.settek.com Date: 1/19/2016
CLIENT: Synagro
Project: Statesville 4th Creek
Analytical Comments for telp-svoc-epest telp(8081), Sample les-18072, Batch ID 18072 :Sample
exhibited poor recovery for Surrogate: DCB due to spiking error; Surrogate: TCMX exhibited control.
Analytical Comments for telp-svoc-cpest telp(8081), Sample 16010277-001a, Batch ID 18072 :
Sample exhibited poor recovery for Surrogate: DCB due to spiking error; Surrogate: TCMX exhibited
control.
Analytical Comments for telp-svoc-cpest tclp(8081), Sample mb-18072, Batch ID 18072: Sample
exhibited outlying recovery for Surrogate: DCB due to spiking error; Surrogate: TCMX exhibited
control.
Analytical Comments for svoc-epest_s(8081), Sample lcs-17673, Batch ID 17673 : Sample exhibited
poor recovery for Surrogate: DCB due to spiking error; Surrogate: TCMX exhibited control.
Analytical Comments for svoc-cpest_s(8081), Sample mb-17673, Batch ID 17673 : Sample exhibited
poor recovery for Surrogate: DCB due to spiking error; Surrogate: TCMX exhibited control.
Analytical Comments for SVOC-bna_tclp(8270), Sample mb-18101, Batch ID 18101 : The 8270 TCLP
MB (batch 1810) exhibited a high recovery for surrogate p-Terphenyl-d14. The MB was non -detect for
analytes.
Analytical Comments for telp-svoc-herb_telp(8151), Sample lcs-18139, Batch ID 18139 : The TCLP
Herbicides LCS (Batch 18139) exhibited slightly high recovery for 2,4-D; All samples were ND.
Original
Page 3 of 9

suftammor
Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win S
e_`YIrIzOMMENTAL:tsv. Cuyahoga Falls, Ohio4422 j WO#: 16010277
ArrHlyr;'cal TEL: [phone] FAX.' (330) 253-446
Website: httD://wivw.settek.co. Date: 1/19/2016
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MIB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLv1
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 9

M9Sub", WAIRt
F.iWRLNIAEN'MLTrov; ,'OLGG '=5:ih1M.
R.ratittr�at L�_�eraT,�rle�
CLIENT: Synagro
Project: Statesville 4th Creek
Lab SampleID Client Sample ID
16010277-001 Statesville 4th Creek
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://Vww.settek.com
Tag No Date Collected
1/6/2016 5:00:00 PM
Workorder
Sample Summary
WO#: 16010277
19-Jan-16
Date Received Matrix
1/7/2016 10:25:00 AM Solid
Page 5 of 9

Summit Environmental Technologies, Inc. Analytical Report
KIµ'
IT 3310 Win St.
i-uviFiowwwr L I_Ci:l OL IG, s, Inc- Cuyahoga Falls, Ohio 44223 (base report)
Arral,vffoal L at Clrarurfe—� TEL: [phone] FAY- [phone] WO#: 16010277
Website: hM.-Ilwivw.settek.com Date Reported: 1/19/2016
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/6/2016 5:00:00 PM
Lab ID: 16010277-001A
Project: Statesville 4th Creek
Client Sample ID Statesville 4th Creek
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 6.86 s.u.@19.8C 1 1/7/2016 3:50:00 PM
Qualifiers: *
Value exceeds Maximum Contaminant LeveL
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column con5rmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
U
Samples with CalcVal <MDL
J
Analyte detected below quantitation limits Page 6 of 9

Summit Environmental Technologies, Inc.
WO#:
16010277
RUVIRONFAEN`rAL V--CPV,0LQGJE5, INN
ETS"Mmoir
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported:
1/19/2016
Analytical LsSaratories
TEL: [phone] FAX. [phone]
Company:
Synagr0
Website: httD://www.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/7/2016
Project#:
Statesville 4th Cr
TCLP Metals Analysis (6010)
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Creek
001
1/6/2016
TCLP Arsenic(As)
0.500
ND mg/L
Solid
EPA 6010 C
1
5.00
1/11/2016
WK
Statesville 4th Creek
001
1/6/2016
TCLP Barium(Ba)
5.00
ND mg/L
Solid
EPA 6010 C
1
100
1/11/2016
WK
Statesville 4th Creek
001
1/6/2016
TCLP Cadmium(Cd)
0.100
ND mg/L
Solid
EPA 6010 C
1
1.00
1/11/2016
WK
Statesville 4th Creek
001
1/6/2016
TCLP Chromium(Cr)
0.200
ND mg/L
Solid
EPA 6010 C
1
5.00
1/11/2016
WK
Statesville 4th Creek
001
1/6/2016
TCLP Lead(Pb)
0.500
ND mg/L
Solid
EPA 6010 C
1
5.00
1/11/2016
WK
Statesville 4th Creek
001
1/6/2016
TCLP Selenium(Se)
0.500
ND mg/L
Solid
EPA 6010 C
1
1.00
1/11/2016
WK
Statesville 4th Creek
001
1/6/2016
TCLP Silver(Ag)
0.500
ND mg/L
Solid
EPA 6010 C
1
5.00
1/11/2016
WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Qtatesville 4th Creek 001 1/6/2016 TCLP Mercury 0.0100 ND mg/L Solid EPA 7470 A 1 0.200 1/12/2016 MFW
SVOC SW-846: 8081-TCLP Pesticides
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Creek
001
1/6/2016
Chlordane, total
0.0250
ND mg/L
Solid
EPA 8081 B
1
0.0300
1/12/2016
JBN
Statesville 4th Creek
001
1/6/2016
Toxaphene
0.0500
ND mg/L
Solid
EPA 8081 B
1
0.500
1/12/2016
JBN
Statesville 4th Creek
001
1/6/2016
Endrin
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.0200
1/12/2016
JBN
Statesville 4th Creek
001
1/6/2016
gamma-BHC
0.00250
ND mg1L
Solid
EPA 8081 B
1
0.400
1/12/2016
JBN
Statesville 4th Creek
001
1/6/2016
Heptachlor
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.00800
1/12/2016
JBN
Statesville 4th Creek
001
1/6/2016
Heptachlor epoxide
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.00800
1/12/2016
JBN
Statesville 4th Creek
001
1/6/2016
Methoxychlor
0.00250
ND mg/L
Solid
EPA 8081 B
1
10.0
1/12/2016
JBN
SVOC
SW-846: 8151 Herbicides-TCLP
Client ID# Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Creek
001
1/6/2016
2,4-D
1.00
ND mg/L
Solid
EPA 8151 A
1
10.0
1/15/2016
JBN
Statesville 4th Creek
001
1/6/2016
2,4,5-TP
0.100
ND mg/L
Solid
EPA 8151 A
1
1.00
1/15/2016
JBN
Page 7 of 9

,:
Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
16010277
v
f NIVIFIONMENTAL :FCC d0LaGJ=S, IBC
Cuyahoga Falls, Ohio44223
Date Reported:
1/19/2016
__na,yti"ca} LsEaoratort
TEL: [phone] F,4X.- [phone]
Company:
Synagro
Website: http://www.settekcom
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/7/2016
Project#:
Statesville 4th Cr
VOC by GC/MS (8260)-TCLP
Client ID# Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Creek
001
1/6/2016
1,1-Dichloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.700
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
1,2-Dichloroethane
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
MEK
2.00
ND mg/L
Solid
EPA 8260 B
1
200
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
Benzene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
Carbon tetrachloride
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
Chlorobenzene
0.100
ND mg/L
Solid
EPA 8260 B
1
100
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
Chloroform
0.100
ND mg/L
Solid
EPA 8260 B
1
6.00
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
Tetrachloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.700
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
Trichloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
1/11/2016
MES
Statesville 4th Creek
001
1/6/2016
Vinyl chloride
0.200
ND mg/L
Solid
EPA 8260 B
1
0.200
1/11/2016
MES
SVOC 8270 TCLP BNA List
Vent ID# Lab IN
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Creek
001
1/6/2016
1,4-Dichlorobenzene
0.500
ND mg/L
Solid
EPA 8270 C
5
7.50
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
2,4,5-Trichlorophenol
1.25
ND mg/L
Solid
EPA 8270 C
5
400
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
2,4,6-Trichlorophenol
1.25
ND mg/L
Solid
EPA 8270 C
5
2.00
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
2,4-Dinitrotoluene
0.500
ND mg/L
Solid
EPA 8270 C
5
0.130
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
Cresols, Total
25.0
ND mg/L
Solid
EPA 8270 C
5
200
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
Hexachloro-1,3-
0.500
ND mg/L
Solid
EPA 8270 C
5
0.500
1/16/2016
MO
butadiene
Statesville 4th Creek
001
1/6/2016
Hexachlorobenzene
0.500
ND mg/L
Solid
EPA 8270 C
5
0.130
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
Hexachloroethane
0.500
ND mg/L
Solid
EPA 8270 C
5
3.00
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
Nitrobenzene
0.500
ND mg/L
Solid
EPA 8270 C
5
2.00
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
Pentachlorophenol
1.25
ND mg/L
Solid
EPA 8270 C
5
100
1/16/2016
MO
Statesville 4th Creek
001
1/6/2016
Pyridine
1.25
ND mg/L
Solid
EPA 8270 C
5
5.00
1/16/2016
MO
Page 8 of 9

Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
16010277
ffisummipt
€KVIR01QoIEWI'bL€LCHNOLaGiasrINQ
Cuyahoga Falls, Ohio44223
Date Reported:
1/19/2016
r paryPica1 Laboratur{es TEL:
[phone] FAX.- [phone]
Company:
Synagro
Website: hM2.-Ilwwiv.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/7/2016
Project#:
Statesville 4th Cr
Client ID# Lab ID# Collected Analyse
Result Units
Matrix
Method DF RL Run Analyst
Statesville 4th Creek
001
1/6/2016
Flashpoint (140°F)
>140 °F
Solid
EPA 1010
1
1/8/2016
TAH
Statesville 4th Creek
001
1/6/2016
Cyanide, Reactive
ND mg/Kg
Solid
EPA 9014
1
0.500 1/7/2016
MS
Statesville 4th Creek
001
1/6/2016
Sulfide, Reactive
ND mg/Kg
Solid
EPA 9034
1
25.0 1/7/2016
MS
Page 9 of 9

ti- un'11111t 1*nvironment,,1l 'Fechn1 logojes, IFIC.
,�) Will stt•eet CtyahCa F,IE , (}hir44w23 Tcl: 330.?Si.82'I I Fax: �ectlnteucsnitltll 7CLchhnualai,licl ,4f
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Prnet Nome
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\'t'Iriic and )�'llutr rages shuntd urconip:ms' .,)wpleS 14 dtr lablrrittore.'r
.Te •e

DG7
Rev. 14
0511 15
i
Summit Envlronmentel Technologies, Inc.
Cooler R"Pt Form
Infifals of person tns t
petting cooler and samples:
J
Omer Number,_ (`� I
Date Received: i EI �� t0 •11nje Ruefved: /� Date coeler(s)
— L�
opened and sam les in (�
P spatted:
Number of Coolers/Boxes:
f
WA
Shlpper. FED EX f> DHL
/
i Airborne US Postal
Waik-in pickup Other:
Packaging; Peak
uts Bu le p Paper Foam None Other.
Tape on cooled/box
N NIA
Custody Seals intact
Y N
C-O-C In plastic
CY--
Ice Iue Ice
NWA
wit
I absent / melted WA
Sample Temperature IR Gun #1602�p46q
CF• ` D -C
L , b oC
Radiological TeWng instruments
(see page 2 for scan results)
"Use 1 sheet per tampie for. Fdlaiogfcal
rial #3 2
Testing.
WA
Y N
NIA
lnimedlatefy.'If
sample
Is HOT, the Radiological Safety Officer must be notified ,
(-'4-C filled out properly I
Samples in separate bags
N N/A
N WA
Samp''e containers Intaet' N
WA
'If no, list broken sample(s):
• - i •
Sampis labal(s) complete (ID, date, eta)
i .
Y N WA
Labeks) agree with C-o-C
�, Y J N WA
�.
Correct containers used
Y/ N NIA
Sufficient sample received
Y N N/A
Samples received within holding time4
lJ N
Bubbles absent from 40 mL vials"
Y N WA
" Samples with bubbles <emm are a =0Ptabla- Indicate bubble size if >6mm.
Was cbnt contacted about samples Y N
V011 client send new samples Y N
Client contact
DateMms:
Logged in by:.
Page t of

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP WQ Permit Number:
WWTP Name: Statesville Fourth Creek WWTP NPDES Number: _
WQ 0016247
NC 0031836
Monitoring Period: From 01/01/16 To 3/31/2016
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf � .,1;..ahlo t., al+.—+;— —f--1 (('lace A nr Clace M rmmnlPfP the fnllnwinv mnnifnrinv data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Exece-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10to the 6 1h
MPN
1769
23872
123077
MPN/g
0
Quarterly
Grab
Sm9221ce
Coliform
power per gram
- 2006
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
tidy Sk6,t+k ze skdv,�S 53'U v*4'e-(,4.64
P pair N m n Title( type or print) Land Applier Name and Title (if applicable) (type or print)
Signa re of Preparer* ate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
Reported:
For:
Comments:
Analytical Results
01/12/2016
12/28/2016
COS 4th Creek
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
160112-20-01
Fecal Coliforms
1
31,250
MPN/g
sM9221cE-2006
01/12/2016
WL
160112-20-01
Percent Solids
1
16
%
SM254OB-1997
01/12/2016
WL
160112-20-02
Fecal Coliforms
2
106,667
MPN/g
SM92210E-2006
01/12/2016
WL
160112-20-02
Percent Solids
2
15
%
SM254OB-1997
01/12/2016
WL
160112-20-03
Fecal Coliforms
3
114,286
MPN/g
sM92210E-2006
01/12/2016
WL
160112-20-03
Percent Solids
3
14
%
sM254OB-1997
01/12/2016
WL
160112-20-05
Fecal Coliforms
5
123,077
MPN/g
SM92210E-2006
01/12/2016
WL
160112-20-05
Percent Solids
5
13
%
SM254OB-1997
01/12/2016
WL
Respectfully submitted,
LPZw10(-'
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 1

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 01/14/2016
Reported: 12/28/2016
For: City of Statesville 4th Creek
Comments: Geometric mean 17,180 MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
160114-17-01
Fecal Coliforms
1
1,769
MPN/g
SM92210E-2006
01/14/2016
WL
160114-17-01
Percent Solids
1
13
%
SM254OB-1997
01/14/2016
WL
160114-17-02
Fecal Coliforms
2
23,077
MPN/g
SM92210E-2005
01/14/2016
WL
160114-17-02
Percent Solids
2
13
%
SM2540B-1997
01/14/2016
WL
160114-17-03
Fecal Coliforms
3
2,308
MPN/g
SMMlCE-2006
01/14/2016
WL
160114-17-03
Percent Solids
3
13
%
SM254OB-1997
01/14/2016
WL
Respectfully submitted,
to
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

Condition of Receipt
Sample Number 160114-17-01 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Chemicals in containers, lab
Received on Ice
Sample Number 160114-17-02 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Chemicals in containers, lab
Received on Ice
Sample Number 160114-17-03 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 2

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 1/5,
Sampled By:
Analysis Date/Time: 1/5,
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.74
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5/i 2
12.4
6
LC
6 1:�10
BJ
300 milliliters
1.69 % Dry Solids
12.6 degrees Celsius
13.5 degrees Celsius
0.0
7.9
0.1
0.15 mg Oxygen/hr
0.03 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.05 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.86
7.93
8.08
8.09
08 8
8.09
7.95
7.86
7.84
7.78
7.71
7.65
7.62
7.57
7.57
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
ou
1 /6/2016
10.7
1/6/16 1:00 PM
1/6/16 1:09 PM
BJ
300
1.75
13.1
0.0
8.1
0.8
liliters
Dry Solids
arees Celsius
frees Celsius
2.01 mg Oxygen/hr
0.38 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.61 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
0
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1/7/2016
16
1/7/16 1:00 PM
RG
1/7/16 1:03 PM
BJ
300
1.73
16.2
17.1
Dissolved Oxygen Level
7.52
7.42
7.3
7.24
7.18
7.13
7.06
7
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
7.5
1.0
3.45 mg Oxygen/hr
0.66 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.81 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
0
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WW
1 /8/2016
14.3
1/8/16 1:03 PM
RG
1/8/16 1:12 PM
BJ
300
1.7
14.4
14.2
Dissolved Oxygen Level
8.32
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
deqrees Celsius
0.87 mg Oxygen/hr
0.17 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.26 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
5 .
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.4
7.36
Slope:
Intercept:
Correlation Coefficient:
(Fourth Creek WWTPI
1/11/2016 .
13.3
1/11/16 1:29 PM
RG
1/11/16 1:42 PM
BJ
300
1.87
13.9
0.0
7.6
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
Oxygen Uptake Rate: 0.82 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.15 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.22 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.69
1
8.69
2
8.58
3
8.72
4
8.8
5
8.82
6
8.73
7
8.66
8
8.64
9
8.69
10
8.68
11
8.63
12
8.54
13
8.49
14
8.49
15
8.45
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek VW11TP
1/12/2016
14.8
1/12/16 1:07 PM
RG
1/12/16 1:13 PM
BJ
300
1.78
15
14.5
Ililiters
Dry Solids
grees Celsius
grees Celsius
0.96 mg Oxygen/hr
0.18 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.25 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.85
1
8.78
2
8.74
3
8.77
4
8.72
5
8.72
6
8.66
7
8.64
8
8.57
9
8.59
10
8.56
11
8.45
12
8.47
13
8.44
14
8.45
15
8.42
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
I-ourtn ureeK VVVV I N
1/13/2016
13.1
1/13/16 1:03 PM
RG
1/13/16 1:11 PM
BJ
300
1.95
13.7
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.74 mg Oxygen/hr
0.30 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.45 jmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP WQ Permit Number: WQ 0016247
WWTP Name: Statesville Fourth Creek WWTP NPDES Number: NC 0031836
Monitoring Period: From 04/01/16 To 6/30/2016
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf nnnlirahln fn alfarnnfivP narfnrmrrl ff'lncc A nr (9acc R) rmmnlnfe fhe fnllnwina mnnifnrina rintn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
127
1567
10400
MPN/g
0
Quarterly
Grab
Sm9221
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Mt. 4
(VS reduction)
(40-day bench)
(3 0-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
W
itle ( type or print) -WW1
of Preparer* bad
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results.
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
04/26/2016
Reported:
12/28/2016
For:
4th Creek
Comments:
Geometric Mean 1567 MPN/g
Sample Number
Parameter Sample ID
Result
Unit Method
Analyzed
Analyst
160426-09-01
Fecal Coliforms
3480
MPN/100 ml SM9221
04/26/2016
DM
160426-09-01
Percent Solids
86.2
% SM254OB-1997
04/26/2016
DM
160426-09-02
Fecal Coliforms
924
MPN/100 ml sM9221
04/26/2016
DM
160426-09-02
Percent Solids
86.6
% SM254OB-1997
04/26/2016
DM
160426-09-03
Fecal Coliforms
10400
MPN/100 ml sM9221
04/26/2016
DM
160426-09-03
Percent Solids
86.5
% SM254OB-1997
04/26/2016
DM
160426-09-04
Fecal Coliforms
3460
MPN/100 ml sM9221
04/26/2016
DM
160426-09-04
Percent Solids
86.7
% SM254OB-1997
04/26/2016
DM
160426-09-05
Fecal Coliforms
5730
MPN/100 ml SM9221
04/26/2016
DM
160426-09-05
Percent Solids
87.2
% SM254OB-1997
04/26/2016
DM
160426-09-06
Fecal Coliforms
275
MPN/100 ml SM9221
04/26/2016
DM
160426-09-06
Percent Solids
87.4
% SM254OB-1997
04/26/2016
DM
160426-09-07
Fecal Coliforms
127
MPN/100 ml SM9221
04/26/2016
DM
160426-09-07
Percent Solids
86.5
% SM254OB-1997
04/26/2016
DM
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 3

Condition of Receipt
Sample Number 160426-09-01 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 160426-09-02 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 160426-09-03 Temp on Arrival: 2,0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 160426-09-04 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 160426-09-05 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 3

Parameter Schedule:
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 160426-09-06 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 160426-09-07 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 3

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4/1 /2016
20
4/1/16 1:20 PM
KG
4/1/16 1:28 PM
BJ
300
1.6
19.9
20.3
Dissolved Oxygen Level
mg/1
5.62
5.57
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
5.6
1.0
4.91 mg Oxygen/hr
1.02 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 1.02 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4/4/2016
20.6
4/4/16 1:13 PM
RG
4/4/16 1:20 PM
BJ
300
1.76
20.5
20.1
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
9.02
8.26
18 8
8.1
7.93
7.85
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
9.1
1.0
4.80 mg Oxygen/hr
0.91 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.91 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek VWI/TP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4/5/2016
16.5
415/16 2:OOPM
KG
4/5/16 2:10 PM
BJ
300
1.8
16.4
17.1
Dissolved Oxygen Level
6.75
6.65
6.58
6.41
6.23
6.14
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
7.3
1.0
4.23 mg Oxygen/hr
0.78 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.96 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek
4/6/201
15.3
4/6/16 1:7
KG
4/6/16 1:G
BJ
300
1.68
15.5
15.7
Dissolved Oxygen Level
(mg1l)
7.8
7.81
7.88
8.04
8.16
8.15
8.09
8.04
7.97
7.93
7.84
7.71
7.72
7.63
7.58
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
deorees Celsius
1.35 mg Oxygen/hr
0.27 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:j 0.35 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4/7/2016
18.4
4/7116 2:45 PM
KG
4/7/16 2:51 PM
BJ
300
1.82
18.2
18.3
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.5
1
6.46
2
6.45
3
6.43
4
6.54
5
6.51
6
6.45
7
6.44
' 8
6.41
9
6.34
10
6.26
11
6.23
12
6.22
13
6.19
14
6.11
15
6.04
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1.76 mg Oxygen/hr
0.32 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate:1 0.37 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP
WWTP Name: Statesville Fourth Creek WWTP NPDES Number:
Monitoring Period: From 07/01/16 To 09/30/2016
WQ Permit Number:
WQ 0016247
NC 0031836
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf nnnlirnhlP to nitrrnntivP. nrrfnrmPd (( N.RR A nr Cincc M rmmnlrte the fallnwinu monitorin¢ data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2xl0to the 6th
MPN
<1333
<1488
<1961
MPN/g
0
Quarterly
Grab
Sm9221ce
Coliform
power per gram
- 2006
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
I
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there/dare significant penalties for false certification including fine and imprisonment."
of S ✓,a1 -�° 9 1`" al
N e d Title ( type or print) /
of Preparer* a
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
09107/2016
i
Reported:
12128/2016
For:
4th Creek
Comments:
Geometric Mean <1,488 MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
160907-15-01
Fecal Coliforms
1
<1,961
MPN/g
sm9221cE-2006
09/07/2016
WC
160907-15-01
Percent Solids
1
10.2
%
SM2540B-1997
09/07/2016
WC
160907-15-02
Fecal Coliforms
2
<1,471
MPN/g
sm9221cE-2006
09/07/2016
WC
160907-15-02
Percent Solids
2
13.6
%
SM254OB-1997
09/07/2016
WC
160907-15-03
Fecal Coliforms
3
<1,739
MPN/g
SM92210E-2006
09/07/2016
WC
160907-15-03
Percent Solids
3
11.5
%
sM2540B-1997
09/07/2016
WC
160907-15-04
Fecal Coliforms
4
<1,351
MPN/g
SM92210E-2006
09/07/2016
WC
160907-15-04
Percent Solids
4
14.8
%
SM2540B-1997
09/07/2016
WC
160907-15-05
Fecal Coliforms
5
<1,333
MPN/g
SM922-ICE-2006
09/07/2016
WC
160907-15-05
Percent Solids
5
15.0
%
SM2540B-1997
09/07/2016
WC
160907-15-06
Fecal Coliforms
6
<1,333
MPN/g
SM92210E-2006
09/07/2016
WC
160907-15-06
Percent Solids
6
15.0
%
SM2540B-1997
09/07/2016
WC
160907-15-07
Fecal Coliforms
7
<1,342
MPN/g
SM92210E-2006
09/07/2016
WC
160907-15-07
Percent Solids
7
14.9
%
SM2540B-1997
09/07/2016
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 160907-15-01 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 160907-15-02 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 160907-15-03 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 160907-15-04 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 160907-15-05 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 160907-15-06 Temp on Arrival: 3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Scheduler Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 160907-15-07 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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0
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(D
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Client: Q
5'I'A'1'IiSVlt,l.li ANALYTICAL
122 Court Street • P.0. Box 228
Address:
Shuesville, NC 28687
004)872.4697
Contact Person:
/ Phone # 431 goGZ
r
FAX#
Chain of
PC It
Requisitioned by:
(Time Dalo)
Custody Recoi-d
cuslamer
Sample IDr+
p
Lah-ID rr
Time Sampled
(Grate Only)
Dale Sampled
(Grate Only)
t°
7
u
-
Matrix
siwv w ww
Paramalets requested [or analysis
h k
lk �''l 15
01
3 G
1/
02
:, 1
/
U5
s:j�
Relinquished by:
Ma/� �
1,1 , f y r
Time Lc)_; o
G' pm Date g/3 / I �
Sampled by:
Received by:
`{7II
ITV �j
Time 0
(m pm Dale � /-7 / � �
Transported by:
Relinquished by:
Time
am, pm Date _/_/
Holding times met:
Received by:
Time
am, pm Dale _/_/_
Compliance work:
Composite Sampling
#7:
Time begin am, pm Date _/_/_
Non-compliance work:
Time end am, pm Date _/_/_
Lab comments;
Com osite Sampling
#2•
Time begin am, pm Date
Time end am, pm Date —/—/_

Specific Oxygen Uptake Rate
SOUR
Facility Name:1Fourth Creek WW
Biosolids Permit Number:
Date:
7/5/2016
Digester Temperature:
25.8
Sampling Date/Time:
7/5/16 1:58 PM
Sampled By:
LC
Analysis Date/Time:
7/5/16 2:00 PM
Analyzed By:
BJ
Sample Volume:
300
milliliters
Total Solids:
1.46
% Dry Solids
Beginning Temperature:
25.9
Idegrees Celsius
End Temperature:
23.4
Idegrees Celsius
Time Dissolved Oxygen Level
(minutes)
(mg/I)
0
6.7
1
6.71
2
6.72
3
6.78
4
6.77
5
6.73
6
6.74
7
6.71
8
6.64
9
6.62
10
6.59
11
6.49
12
6.5
13
6.41
14
6.36
15
6.32
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
t.1
1.70 mg Oxygen/hr
0.39 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:1 0.30 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/l)
6.65
6.61
6.49
6.4
6.33
6.22
6.19
6.1
6.05
5.89
5.86
5.71
65 85.63
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
IFourth Creek WWTPI
7/6/2016
25.4
7/6/16 1:20 PM
1 716116 1:27 PM 1
300
1.56
25.3
0.1
6.6
1.0
Aliliters
16 Dry Solids
egrees Celsius
egrees Celsius
4.16 mg Oxygen/hr
0.89 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:1 0.70 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fou
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.36
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
24.7
7/7/16 1:07 PM
RG
7/7/16 1:13 PM
300 milliliters
1.74 % Dry Solids
24.5 degrees Celsius
24 Idearees Celsius
0.1
7.2
1.0
3.39 mg Oxygen/hr
0.65 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.53 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
6.73
6.67
6.61
6.59
6.55
6.51
6.45
6.42
6.37
6.29
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
7/8/2016
26.1
7/8/16 1:09 PM
RG
7/8/16 1:13 PM
BJ
300
1.69
25.8
24.6
0.1
6.7
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.12 mg Oxygen/hr
0.61 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:1 0.48 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
7/11/2016
24.2
7111/16 1:05 PM
RG
7/11/16 1:13 PM
BJ
300
1.66
24.6
24.8
Dissolved Oxygen Level
6.17
6.07
95 85.91
5.54
5.42
Slope: 0.1
Intercept: 6.2
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 3.38 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.68 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:1 0.53 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
2
3
4
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.51
6.48
6.41
6.31
6.26
6.17
6.1
5.92
5.87
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
F-ourtn ureeK VVVV I N
7/12/2016
24.9
7/12/16 1:52 PM
7/12/16 2:01 PM
milliliters
% Dry Solids
Idegrees Celsius
lde.qrees Celsius
BJ
300
1.67
24.8
24
0.1
6.8
1.0
3.41 mg Oxygen/hr
0.68 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:jFourth Creek
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
7/13/20
24.9
7/13/16 7
RG
7/13/16 1:1
BJ
300
1.49
24.7
23.9
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.01
1
7
2
6.94
3
6.87
4
6.8
5
6.72
6
6.69
7
6.63
8
6.59
9
6.52
10
6.41
11
6.37
12
6.31
13
6.29.
14
6.22
15
6.16
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.1
7.0
1.0
3.55 mg Oxygen/hr
0.79 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.65 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP WQ Permit Number: WQ 0016247
WWTP Name: Statesville Fourth Creek WWTP
Monitoring Period
NPDES Number: NC 0031
From 10/01/16 To 12/31/2016
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying
Anaerobic Digestion
Composting Aerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitorine data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6
MPN
797
2026
35461
MPN/g
0
Quarterly
Grab
Sm9221cc
Coliform
power per gram
- 2006
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-daybench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
P p r a e(a Title ( type or print) ILand Applier Name and Title (if applicable) (type or print)
Signatfre of Preparer* Signature of Land A Tier if applicable) Date
g Pp ( pp )
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
10/11/2016
Reported:
12/28/2016
For:
4th Creek City of Statesville
Comments:
Geometric Mean 2,026 MPN/100ML
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
161011-20-01
Fecal Coliforms
1
<1379
MPN/g
SM92210E-2006
10/11/2016
WC
161011-20-01
Percent Solids
1
14.5
%
SM2WB-1997
10/11/2016
WC
161011-20-02
Fecal Coliforms
2
<1389
MPN/g
SM92210E-2006
10/11/2016
WC
161011-20-02
Percent Solids
2
14.4
%
sM254OB-1997
10/11/2016
WC
161011-20-03
Fecal Coliforms
3
797
MPN/g
SM92210E-2005
10/11/2016
WC
161011-20-03
Percent Solids
3
25.1
%
SM254OB-1997
10/11/2016
WC
161011-20-04
Fecal Coliforms
4
<1361
MPN/g
SM92210E-2006
10/11/2016
WC
161011-20-04
Percent Solids
4
14.7
%
SM2540B-1997
10/11/2016
WC
161011-20-05
Fecal Coliforms
5
<1399
MPN/g
SM92210E-2006
10/11/2016
WC
161011-20-05
Percent Solids
5
14.3
%
SM2540B-1997
10/11/2016
WC
161011-20-06
Fecal Coliforms
6
<1361
MPN/g
SM92210E-2006
10/11/2016
WC
161011-20-06
Percent Solids
6
14.7
%
SM254OB-1997
10/11/2016
WC
161011-20-07
Fecal Coliforms
7
35461
MPN/g
SM92210E-2006
10/11/2016
WC
161011-20-07
Percent Solids
7
14.1
%
SM2540B-1997
10/11/2016
WC
Respectfully submitted,
hO
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 161011-20-01 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate- Received on Ice
Sample Number 161011-20-02 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 161011-20-03 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 161011-20-04 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 161011-20-05 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 161011-20-06 Temp on Arrival: 2
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 161011-20-07 Temp on Arrival: 2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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STATESVILLE ANALYTICAL
Address: L yl� � f o/�
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122 Coun Street • P.O. Box 228
Statesville,NC 28687
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f'Tt • GA S i// �r Ci ;7a,?- 5.!
[phone]
Contact Person:Phone
# FAX# 3 �,©
Chain of
Custody Record
PO # Q 4 Requisitioned by: f% (Time Date)
Customer
Samle ID#
p
Lah•ID #
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
'�
a
Maldx
Parameters requested for analysis
so
w
vrn
0
Relinquished by: �,, (fir ,�
Received by: --
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date _/ /_
Time end am, pm Date _J�l—
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date / !_
Time 6?pm Date �� /_.A�
Time d ara~pm Dataf_4_�Jf� /%
Time am, pm Date _
Time am, pm Date_/_/
Lab Comments:
Sampled by: fi— - (�
Transported by: 1, (t�frrs
Holding times met: /
Compliance work:
Non-compliance work:

Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.9
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/3/2016
20.6
10/3/16 1:50 PM
RG
10/3/16 1:55 PM
BJ
300
1.59
20.6
20.8
0.0
8.3
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
2.82 mg Oxygen/hr
0.59 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected'Specific Oxygen Uptake Rate:j 0.56 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
4
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time-
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level:
8.05
8.04
8.02
8
7.98
7.96
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/4/2016
19.4 .
1014/16 12:55 PM
RW
10/4/16 12:59 PM
300
1.77
19.6
19.8
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.0
8.4
1.0
2.07 mg Oxygen/hr
0.39 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:1 0.39 wm�mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.22
8.14
8.11
8.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
ou
10/5/2016
18.5
10/5116 1:10 PM
1 10/5/16 1:13 PM 1
300
1.72
18.5
19
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
0.0
8.2
1.0
1.88 mg Oxygen/hr
0.36 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.39 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WW-
Biosolids Permit Number:
Date:
10/6/2016
Digester Temperature:
18.8
Sampling Date/Time:
10/6/16 1:117 prr
Sampled By:
LC
Analysis Date/Time:
10/6/16 1:23 PM
Analyzed By:
BJ
Sample Volume:
300
Total Solids:
1.66
Beginning Temperature:
18.9
End Temperature:
19.5
Dissolved Oxygen Level
(mg/1)
8
7.98
7.94
7.9
7.86
7.84
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.0
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
1.83 mg Oxygen/hr
0.37 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.39 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
7.98
7.95
7.95
7.92
7.9
7.88
7.86
7.81
7.77
7.73
7.7
7.67
7.65
7.62
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
10/7/2016
18.6
10/7/16 1:07 PM
10/7/16 1:12 PM
BJ
300
1.62
18.6
19.6
0.0
8.0
1.0
milliliters
% Dry Solids
degrees Celsius
deorees Celsius
1.61 mg Oxygen/hr
0.33 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.35 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Third Creek WWTP WQ Permit Number: WQ 0016247
WWTP Name: Statesville Third Creek WWTP NPDES Number: NC 0020591
Monitoring Period: From 01/01/16 To 12/31/2016
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 31C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
P p N a Title ( type or print) Land Applier Name and Title (if applicable) (type or print)
Signa re of Preparer* to Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Agricultural Lime Application Log
Year: 2016
Project:
Statesville Fourth Creek
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied(CCE Eq.)
Date Applieu
IR-204A
6.8
O.OT/Ac.
I R-20-4B
7.1
O.OT/Ac.
I R-20-11
6.7
0.OT/Ac.
I R-23-2
5.5
1.OT/Ac.
I R-23-4
6.8
O.OT/Ac.
I R-23-5
6.5
O.OT/Ac.
*Lime will be applied when conditions improve.

NCDA&CS Ag. _.._.,nic Division Phone: [phone] Website: www.nc.u..yov/agronomi/
Report No. FY17-��� �3550
Client:
Dennis Phillips
Advisor: Synagro
Predictive
201 Barry Oak Rd
Statesville, NC 28625
284 Boger Rd
Mocksville, NC 27028
I� '8$' S o i I Report Mehlich-3 Extraction
r w
Sampled County: Iredell
Sampled: 11/03/2016 Received: 11/18/2016 completed: 12/15/2016
Farm: IR-20
Links to Helpful Information
Sample ID: 20-4a
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
80
0 0
pH$
0
0 0
Note: 12 Note:
2-
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 cnr3; NO3-N in mg/dO]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 0.99 16.7 97 0.5 6.8 183 29 82 14
34
170
107
376
376
294 0.1 1
Sample ID: 20-4b
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
80
0 0
pH$
0
0 0
Note: 12 Note:
2-
Test Results [units - W!V in g/cO; CEC and Na in meq/100 cnr3; NO3-N in mg/do]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.27 1.01 22.9 98 0.4 7.1 270 31 82 16
43
104
63
621
621
355 0.2 1
Sample ID: 20-11
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
20
0 0
pH$
0
0 0
Note: 12 Note:
2-
Test Results [units - WfV in g/cO; CEC and Na in meq/100 cO; NO3-N in mg/drrt3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 0.92 15.7 95 0.8 6.7 268 64 81 11
41
277
173
543
543
329 0.1 1
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Trox

NCDA&CS k mic Division Phone: [phone] Website: www.nc_.._)v/agronomic Report No. FY17 ..�., .3550
Dennis Phillips Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat(
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.aov/agronomi/obpart4.htmY fsFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizei
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-1, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov1agronomi1uMt.htm
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P206
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

NCDA&CS Ac nic Division Phone: [phone] Website: www.nc_,..,-)v/agronomi/
Report No.
FY17- __...3482
-;hrout
Client: Eddie Porter
Advisor:
Predictive
351 Gantt Horn Rd.
Statesville, NC 28625
I�' n'x�4�6a1 Soil Report Mehlich-3 Extraction
.�t'4• 1nvsy'_
Sampled County: Iredell
Sampled: 10/28/2016 Received: 11/18/2016 Completed: 12/16/2016
Farm: 1 R-23
Links to Helpful Information
Sample ID: 23-02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.0 120-200 0
0 0 0
0
0
0 0
Note: 12
2-
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-Al
Cu-1 Na ESP
SS-1 NO3-N
0.56 0.95 13.2 82 2.3 5.5 287 170 64 12
82 285 188
522
522
262 0.1
1
Sample ID: 23-04
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
0 0 0
pH$
0
0 0
Note: 12 Note:
2-
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-1
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.22 0.87 17.5 96 0.6 6.8 404 215 76 14
81 362 223
545
545
.305 0.1
1
Sample ID: 23-05
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P2O6
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
0 0 0
pH$
0
0 0
Note: 12 Note:
2-
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/do]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 0.99 17.2 94 1.1 6.5 398 165 77 12
73 299 189
570
570
350 0.2
1
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Trox

NCDA&CS Ag._.._mic Division Phone: [phone] Website: www.nc _ _ >v/agronomi/ Report No. FY17 _� .3482
Eddie Porter Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Report Abbreviations
Ac
B
BS%
Ca%
e CEC
Cu-I
ESP
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncapr.pov/agronomi/obpart4.htrnl sFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizel
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine[
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncaaraov/agronomi/uyrst.htm
HM%
K-1
K20
Mg%
MIN
Mn
Mn-All
Mn-AI2
Mn-1
M-O
N
Na
NO3-N
ORG
pH
P-1
P205
S-1
SS-1
W/V
Zn-AI
Zn-I
exchangeable acidity
boron
• CEC occupied by basic cations
• CEC occupied by calcium
cation exchange capacity
copper index
exchangeable sodium percent
percent humic matter
potassium index
potash
% CEC occupied by magnesium
mineral soil class
manganese
Mn-availability index for crop 1
Mn-availability index for crop 2
manganese index
mineral -organic soil class
nitrogen
sodium
nitrate nitrogen
organic soil class
current soil pH
phosphorus index
phosphate
sulfur index
soluble salt index
weight per volume
zinc availability index
zinc index

2016 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
STANLY COUNTY UTIL., NC (FKA OAKBOR
STANLY COUNTY UTIL.; NC WEST STANLY WWTP AEROBICALLY DIGESTED LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
June 2016
YEARLY TOTAL
443,300.00 G 19.96
443,300.00 G 19.96
D 18.12
D 18.12
1 /27/2017

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
i Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0005387 Laboratory
Facility Name: STANLY COUNTY UTIL., NC (FKA OAKBORO) WAYPOINT ANALYTICAL
NPDES# : NCO043532
or WQ# (residual only)
WWTP Name: WEST STANLY WWTP (FKA OAKBORO WWTP)
Residuals Analysis Data
Product Type
L1Q
Date Sampled (grab) or 02/23/16
Date Composited.
Percent Solids
1.08
PARAMETERS (mg/kg dry weight)
Arsenic
6
Cadmium
<2
Mercury
2
Chromium
44
Copper
329
Lead
22
Molybdenum
17
Nickel
23
Selenium
7
Zinc
874
Total Phosphorus
17700
TKN
57400
Ammonia -Nitrogen
3700
Nitrate and Nitrite
8850
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant pl ItiP�for submitting false information, including the possibility of fines and imprisonment for knowing violations."
:A9
3)
Date l3
Printed: Friday - January 27, 2017 at 12:15:15 for: 2170 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0005387 Laboratory
Facility Name: STANLY COUNTY UTIL., NC (FKA OAKBORO) WAYPOINT ANALYTICAL
NPDES# : NCO043532
or WQ# (residual only)
WWTP Name: WEST STANLY WWTP (FKA OAKBORO WWTP)
Residuals Analysis Data
Product Type LIQ
Date Sampled (grab) or 02/23/16
Date Composited
Percent Solids 1.08
PARAMETERS (mg/kg dry weight)
Aluminum
11700
Calcium
20900
Magnesium
4830
pH
6.41
Potassium
3690
Sodium
3520
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
x
SIGNATUREOF PREP
NR - Data Not Reported or Data Not Required
Date Z /-/ 3/
DENR FORM RSSF-B (7/2002) Printed: Friday - January 27, 2017 at 12:22:56 for: 2170 01

.cHth"�a. utG �sv�a:vYMWI,tl • • •-.••Je_ULMJCYIVC.CmI.PoImM,;eaw"-Mfiabmnesuelrsun.eru9x1,!wMnm
Page: 1 of 2
Report Number: 16-055-0211
Account Number: 46477 7621 Whitepine Road, Richmond, VA 23237
Submitted By: DREW CULP Waypoint. Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Send To: SYNAGRO CENTRAL LLC/OAKBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27D28
Lab Number: 55207
Sample Id : 2016
Project: WEST STANLY UTILITIES
NC CERT#257
REPORT OF ANALYSIS Date sampled: 2/23/2016 09:45:00
Date Received: 02/24/2016 00:00
Date Reported: 03/0112DIS
Total Solids *
1.08
10800
100.0
JM
02/24/2016 15:35
SM-2540G
Moisture *
98.92
100.0
JM
02/24/2016 15:35
8M-2540G
Total Kjeldahl Nitrogen
5.74
57400
10.0
JM
02/25/2016 09:09
SM-4500-NHSC-TKN
Total Phosphorus
1.77
17700
100
KM
02/25/2018 12:50
SW 60100
Total Potassium
0,37
3690
100
KM
02/25/2018 12:59
SW 6010C
Total Sulfur
1.08
10800
100
KM
02/25/2016 12:59
SW 6010C
Total Calcium
2.09
2090D
100
KM
02/25/2016 12:59
SW 6010C
Total Magnesium
0.48
4830
100
KM
02/26/2016 12:59
SW 6010C
Total Sodium
D.35
3520
100
KM
02/26/2016 12:59
SW 6010C
Total Iron
18800
100
KM
02/25/2016 12:59
SW 6010C
Total Aluminum
11700
100
KM
02/26/2016 12:59
SW 6010C
Total Manganese
415
5
KM
02/25/2016 12:59
SW 6010C
Total Copper
329
5
KM
02/25/2016 12:59
SW 6Di0C
Total Zinc
874
5
KM
0212512016 12:59
SW 6010C
Ammonia Nitrogen
0.37
3700
10.0
JM
02/25/2016 09:09
SM-4500-NH3C
Organic N
5.37
63700
10.0
02/25/2016 09:09
CALCULATION
Nitrate+Nitrite-N
8850
2.00
JM
02/25/2016 09:1D
SM-460ONO3F
Total Cadmium
<2.0
2.0
KM
02/25/2016 12:59
SW 6010C
Ali values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. A&U-ft'
J//�/`J-Our re orts and letters are or th exclusive d o d alusecfourcllents and ma notbere roduced in wholeor art nor ma an reference be made -" "'
p f e an c nfl entl y p p y y
to the work, the results, or the company In any advertising, news release, orother public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 16-055-0211 a
Account Number: 46477 7621
Waypoin-1.
Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
Submitted By: DREW CULP ANALYTICALwww.waypointanalytical.com
Send To: SYNAGRO CENTRAL LLC/OAKBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55207
Sample Id : 2016
Total Chromium
Total Nickel
Total Lead
Total Arsenic
Total Mercury
Total Selenium
pH (Standard Units)
Total Molybdenum
Comments:
Project: WEST STANLY UTILITIES
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 2/23/2016 09:45:00
Date Received: 02/24/2016 00:00
Date Reported: 03/01/2016
44
5
KM
02/25/2016 12:59
SW 6010C
23
5
KM
02/26/2016 12:69
SW 6010C
22
5
KM
02/25/2016 12:59
SW 6010C
6.0
3.0
KM
021251201612:59
SW 6010C
2.0
0.4
KM
02/25/2016 09:00
SW-7471 B
7.0
5.0
KM
021251201612:59
SW 6010C
6.41
2.00
JM
02/25/2016 09:09
SW-9045D
17
5
KM
02/25/2016 12:59
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series Is on a wet basis.
Ourreports and letters are for the exclusive and confidenSal use of our clients, and may not be reproduced In whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, orother public announcements without obtelning our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2170-01-LIQ-NC STANLY COUNTY UTIL., NC WEST STANLY 2/23/2016 3/1/2016-12/31/2016 0.5912
WWTP AEROBICALLY DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (3520 x 1.0800) _ 100 = 38.016
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (20900 x 1.0800) _ 100 = 225.72
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (4830 x 1.0800) _ 100 = 52.164
Na meq = Na mg/I = Molec.Wgt.Na = 38.016 = 23 = 1.65287
Ca meq = Ca mg/I = Molec.Wgt.Ca = 225.72 _ 20 = 11.286
Mg meq = Mg mg/I = Molec.Wgt.Mg = 52.164 _ 12 = 4.347
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.65287 = SgrRoot[0.5(11.286+4.347)] = 0.591197
Printed: 1 /27/2017
Page 1
12:17

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: BADIN
OWNER: ROBERT RIDENHOUR PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 19.96
SITE #: NC ST 00003 FIELD# : ST 00003 0003 OPERATOR: ROBERT RIDENHOUR CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 24.60 ACRES PERMITTED: 24.60
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
6/1/16
148,800.00 (G)
6048.780
1.08
0.272
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
57,400. p
3,700.00 p
8,850.00 p
26810
I FESCUE
6/2/16
130,200.00 (G)
5292.683
1.08
0.238
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
57,400. p
3,700.00 p
8,850.00 p
26810
I FESCUE
6/8/16
86,800.00 (G)
3528.455
1.08
0.159
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
57,400. p
3,700.00 p
8,850.00 p
26810
I FESCUE
6/14/16
77,500.00 (G)
3150.407
1.08
0.142
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
57,400. p
3,700.00 p
8,850.00 p
26811
FESCUE
Jun-16
443,300.00 (G)
18,020.325
Total Gallons/Ac: 18,020.33
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
44
0.010
0.003
0.071
0.534
0.036
0.003
0.028
0.037
0.011
1.419 28.73
Cumulative lbs/acre
0.062
0.027
0.547
5.307
0.417
0.015
0.198
0.340
0.080
12.948 i
x
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
163
r
11
t
FD Cumulative Pollutant Loading Rate Limit (lbs/acre )
36.6
34.8
1339.0
267.9
15.0 ; � 375.0
89.0
2500.0
i
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROBICALLY DIGESTED LIQUII
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017

F.UVIRCN41EP1T L
IL. _.-_ _ _ lyJf31�tRCni i,4i'rcI: AYL�r1G.5
March 14, 2016
Drew Culp/Reports&Invoices
Synagro, NC 28134
12701 Lancaster Hwy
Pineville, NC 28134
TEL: [phone]
FAX: [phone]
RE: West Stanly Utilities
Dear Drew Culp/Reports&Invoices:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] F.9X.• [phone]
Website: http://www.settek.com
Order No.: 16021626
Summit Environmental Technologies, Inc. received 1 sample(s) on 2/25/2016 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943,
Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana
04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New
Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001,
Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Region 8 8TMS-L, USDAIAPHIS P330-11-00244, Utah OH009232011-1,
Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010
Page 1 of 29

Summit Environmental Technologies, Inc. Narrative
S IF 3310Win St.
Case 1\`arr`cll�ve
F.fFVl��7td&9ENP,�L`_�kttr�LOG�;;raG Cuyahoga Falls, Ohio44223 WO#: 16021626
ArrafyhUcal Lafaaraiurie TEL: [phone] FAX: [phone]
Website: httn://wwii,.settek.com Date: 3/14/2016
CLIENT: Synagro, NC 28134
Project: West Stanly Utilities
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway
Haddock, GA 31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency.
Any comments or problems with the analytical events associated with this report are noted below.
Prep Comments for SVPrep_PCB NPW(3510), Sample 16021626-OOIA: Prep Method hold time was
exceeded by 2.177 days, Sample was multi phased
Original
Page 2 of 29

Summit Environmental Technologies, Inc.
3310 Win St. Case Narrative
fn S L
N=` VI .ONMEhTAL 1eG-3:td4L0M s, i tr,_ Cuyahoga Falls, Ohio 44223 WO#: 16021626
Arra,;rtrcral L: hcraillrle a TEL: [phone] FAX: [phone]
Website: hyp✓hviviv.settek.com Date: 3/14/2016
CLIENT: Synagro, NC 28134
Project: West Stanly Utilities
Analytical Comments for SVOC-PCB_NPW(8082), Sample 16021626-001A, Batch ID 19078 : Sample
was extracted past hold time for PCB Analysis.
Analytical Comments for SVOC-PCB_NPW(8082), Sample 16021626-001A, Batch ID 19078 : Sample
was extracted past hold time for PCB Analysis. Analytical Sequence's Prep Method hold time was
exceeded by 2.177 days.
Analytical Comments for TCLP-SVOC-Herb_TCLP(8321), Sample 16021626-001AMSD, Batch ID
R50630 : The TCLP Herbicides MSD (Batch R50630) exhibited high recoveries; All samples were ND.
Analytical Comments for TCLP-SVOC-Herb_TCLP(8321), Sample 16021626-001AMS, Batch ID
R50630 : The TCLP Herbicides MS (Batch R50630) exhibited high recoveries; All samples were ND.
Analytical Comments for TCLP-SVOC-Herb_S(8321), Sample LCSD-R50630, Batch ID R50630 : The
TCLP Herbicides LC SD (Batch R50630) exhibited high recoveries; All samples were ND.
Analytical Comments for TCLP-SVOC-Herb_S(8321), Sample LCS-R50630, Batch ID R50630: The
TCLP Herbicides LCS (Batch R50630) exhibited high recoveries; All samples were ND.
Analytical Comments for tclp-svoc-cpest tclp(8081), Sample ccv-19164, Batch ID R50893 : Matrix
influence affecting instrument calibration demonstrated by repeated analysis.
Sample results may be biased but beyond laboratory control.
Original
Page 3 of 29

Summit Environmental Technologies, In
g� S Qualifiers and Acronyms
summan 3310 Win
F IVIRONMENTdLTECli 40La�m_s; INC. Cuyahoga Falls, Ohio 4422 WO#: 16021626
Aj—.7lv fcal Lzbongfo e,, TEL: [phone] FAX. [phone]
Website: httD://www.settekco. Date: 3/14/2016
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
A The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/1VIB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quamitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 29

i4 Summit Environmental Technologies, Inc.
a 1 I v 3310 Win St.
E':I1VI3WAIEWAL TECW80LGG:_a, 3mr,. Cuyahoga Falls, Ohio 44223
AmT,'yt,caP Lzbaratorie i TEL: [phone] FAX.- [phone]
Website: httn://wivw.settek.com
CLIENT: Synagro, NC 28134
Project: West Stanly Utilities
Lab SampleID Client Sample ID
16021626-001 West Stanly Utilities
Tag No Date Collected
2/23/2016 9:45:00 AM
Workorder
Sample Summary
WO#: 16021626
14-Mar-16
Date Received Matrix
2/25/2016 MOM AM Waste
Page 5 of 29

r Summit Environmental Technologies, Inc.
3310 Win St. Analytical Report
ffj U-SWMITtr{:�I�t�fJktE;b]„L €c aoLc��.�c l,ar__ Cuyahoga Falls, Ohio44223 (base report)
Ana.,wth al Lahexafori s TEL: [phone] FAX. [phone] WO#: 16021626
Website: hQ.-Ilivwiv.settek.com Date Reported: 3/14/2016
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: WASTE Collection Date: 2/23/2016 9:45:00 AM
Lab ID: 16021626-OOIA
Project: West Stanly Utilities
Client Sample ID West Stanly Utilities
Analyses _ Result RL Qual Units DF Date Analyzed
RCI
PH (SM4500-H+ B)
pH
A4500-H+B Analyst: DHC
6.00 s.u.@19.2C 1 3/1/2016 3:40:00 PM
Qualifiers:
Value exceeds Maximum Contaminant Level.
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Mnmum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
U
Samples with CalcVal<MDL
Page 6 of29

' ` -
S U Im,
Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
16021626
.
RrinCNPAENMLI1ECtNOLQGIP51inc
Cuyahoga Falls, Ohio44223 Date Reported:
3/14/2016
ATraiyHral Laboratonez
TEL: [phone] FAX.- [phone]
Company:
Synagro, NC 28134
Website: httm://ww,v.settek.com
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
2/25/2016
Project#:
West Stanly Utili
TCLP Metals Analysis (6010)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly Utilities
001
2/23/2016 TCLP Arsenic(As)
0.500
ND mg/L
Waste
EPA 6010 C
1
5.00
3/4/2016
VVK
West Stanly Utilities
001
2/23/2016 TCLP Barium(Ba)
5.00
ND mg/L
Waste
EPA 6010 C
1
100
3/4/2016
VVK
West Stanly Utilities
001
2/23/2016 TCLP Cadmium(Cd)
0.100
ND mg/L
Waste
EPA 6010 C
1
1.00
3/4/2016
VVK
West Stanly Utilities
001
2/23/2016 TCLP Chromium(Cr)
0.200
ND mg/L
Waste
EPA 6010 C
1
5.00
3/4/2016
VVK
West Stan ly,Utilities
001
2/23/2016 TCLP Lead(Pb)
0.500
ND mg/L
Waste
EPA 6010 C
1
5.00
3/4/2016
VVK
West Stanly Utilities
001
2/23/2016 TCLP Selenium(Se)
0.500
ND mg/L
Waste
EPA 6010 C
1
1.00
3/4/2016
VVK
West Stanly Utilities
001
2/23/2016 TCLP Silver(Ag)
0.500
ND mg/L
Waste
EPA 6010 C
1
5.00
3/4/2016
VVK
TCLP Mercury Analysis (1311/7470)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly Utilities
001
2/23/2016 TCLP Mercury
0.0100
ND mg/L
Waste
EPA 7470 A
1
0.200
3/4/2016
MFW
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DIT
RegLvl
Run
Analyst
West Stanly Utilities
001
2/23/2016 Chlordane, total
0.0250
ND mg/L
Waste
EPA 8081 B
1
0.0300
3/11/2016
JBN
West Stanly Utilities
001
2/23/2016 Toxaphene
0.0500
ND mg/L
Waste
EPA 8081 B
1
0.500
3/11/2016
JBN
West Stanly Utilities
001
2/23/2016 Endrin -
0.00250
ND mg/L
Waste
EPA 8081 B
1
0.0200
3/11/2016
JBN
West Stanly Utilities
001
2/23/2016 gamma-BHC
0.00250
ND mg/L
Waste
EPA 8081 B
1
0.400
3/11/2016
JBN
West Stanly Utilities
001
2/23/2016 Heptachlor
0.00250
ND mg/L
Waste
EPA 8081 B
1
0.00800
3/11/2016
JBN
West Stanly Utilities
001
2/23/2016 Heptachlor epoxide
0.00250
ND mg/L
Waste
EPA 8081 B
1
0.00800
3/11/2016
JBN
West Stanly Utilities
001
2/23/2016 Methoxychlor
0.00250
ND mg/L
Waste
EPA 8081 B
1
10.0
3/11/2016
JBN
VOC by GC/MS (8260)-TCLP
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly Utilities
001
2/23/2016 1,1-Dichloroethene
0.100
ND mg/L
Waste
EPA 8260 B
1
0.700
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 1,2-Dichloroethane
0.100
ND mg/L
Waste
EPA 8260 B
1
0.500
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 MEK
2.00
ND mg/L
Waste
EPA 8260 B
1
200
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 Benzene
0.100
ND mg/L
Waste
EPA 8260 B
1
0.500
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 Carbon tetrachloride
0.100
ND mg/L
Waste
EPA 8260 B
1
0.500
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 Chlorobenzene
0.100
ND mg/L
Waste
EPA 8260 B
1
100
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 Chloroform
0.100
ND mg/L
Waste
EPA 8260 B
1
6.00
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 Tetrachloroethene
0.100
ND mg/L
Waste
EPA 8260 B
1
0.700
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 Trichloroethene
0.100
ND mg/L
Waste
EPA 8260 B
1
0.500
3/4/2016
MES
West Stanly Utilities
001
2/23/2016 Vinyl chloride
0.200
ND mg/L
Waste
EPA 8260 B
1
0.200
3/4/2016
MES
Page 7 of 29

Suffimlar
Summit Environmental Technologies,Inc.
3310 WinSt.FUVIRL�NPolENITAL7cC3?r
WO#:
16021626
r)LaG;cs, �tG
Cuyahoga Falls, Ohio 44223
Date Reported:
3/14/2016
/iyralytival L23haratorie.,
TEL: [phone] FAX.- [phone]
Company:
Synagro, NC 28134
Website: htta://wiviv.settekcom
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
2/25/2016
Project#:
West Stanly Utili
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly Utilities
001
2/23/2016 1,4-Dichlorobenzene
0.200
ND mg/L
Waste
EPA 8270 C
2
7.50
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 2,4,5-Trichlorophenol
0.500
ND mg/L
Waste
EPA 8270 C
2
400
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 2,4,6-Trichlorophenol
0.500
ND mg/L
Waste
EPA 8270 C
2
2.00
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 2,4-Dinitrotoluene
0.200
ND mg/L
Waste
EPA 8270 C
2
0.130
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 Cresols, Total
10.0
ND mg/L
Waste
EPA 8270 C
2
200
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 Hexachloro-1,3-
0.200
ND mg/L
Waste
EPA 8270 C
2
0.500
3/8/2016
CxA
butadiene
West Stanly Utilities
001
2/23/2016 Hexachlorobenzene
0.200
ND mg/L
Waste
EPA 8270 C
2
0.130
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 Hexachloroethane
0.200
ND mg/L
Waste
EPA 8270 C
2
3.00
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 Nitrobenzene
0.200
ND mg/L
Waste
EPA 8270 C
2
2.00
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 Pentachlorophenol
0.500
ND mg/L
Waste
EPA 8270 C
2
100
3/8/2016
CxA
West Stanly Utilities
001
2/23/2016 Pyridine
0.500
ND mg/L
Waste
EPA 8270 C
2
5.00
3/8/2016
CxA
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly Utilities
001
2/23/2016 2,4-D
5.00
ND mg/L
Waste
EPA 8321 A
1
10.0
3/4/2016
BJH
West Stanly Utilities
001
2/23/2016 2,4,5-TP
0.500
ND mg/L
Waste
EPA 8321 A
1
1.00
3/4/2016
BJH
Page 8 of 29

Environmental Technologies, Inc.
INT 3310 Win St.
Analytical Report
TSUMNSummit
FFf,tl1RONMEN"UtL 1_Ci;t40LdclE5, wq+
Cuyahoga Falls, Ohio 44223
(consolidated)
Arrslyti.^.al Labarafaf/pc TEL: [phone] FAX.- [phone]
WO#: 16021626
Website: &W.-Ihviviv.settek.com
Date Reported: 3/14/2016
CLIENT: Synagro, NC 28134
Collection Date:
2/23/2016 9:45:00 AM
Project: West Stanly Utilities
Lab ID: 16021626-001
Matrix:
WASTE
Client Sample ID West Stanly Utilities
Analyses Result
RL Qual Units
DF Date Analyzed
RCI
SW1010
Analyst: TAH
FLASHPOINT (EPA 1010)
Flashpoint (200°F) >200
°F
1 3/4/2016 3:53:24 PM
PCB-LIQUID-8082
SW8082
SW3510C Analyst: BJH
SVOC PCB (EPA 8082)
Total PCBs ND
0.00100 H mg/L
1 3/7/2016 10:53:00 AM
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)
Cyanide, Reactive ND
0.500 mg/L
1 2/26/2016 12:44:00 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (EPA 9034)
Sulfide, Reactive ND
25.0 mg/L
1 2/26/2016 12:44:00 PM
Qualifiers: * Value exceeds Maximum Contaminant LeveL
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected at the Reporting Limit
0 RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
U Samples with CalcVa1 <MDL
Page 9 of 29

Summit Environmental Technologies, Inc.
msumnan- 3310 Win St. QC SUMMARY REPORT
tr4NIKUNrou-N JRl- F t;t;!H?4rJLUi:.it:�, JR. . Cuyahoga Falls, Ohio 44223 WO#: 16021626
? FWD ,rV-raf La borsilDfFer TEL: [phone] FAX: [phone]
Website: htW.-Ilivww.settelc.coni 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities Batchll): 19078
Sample ID MB-19078
SampType: MBLK
TestCode: SVOC-PCB_ Units: mg/L
Prep Date: 3/3/2016
RunNo: 50615
Client ID: PBW
Batch ID: 19078
TestNo: SW8082 SW3510C
Analysis Date: 3/4/2016
SegNo: 795301
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Total PCBs ND 0.000100
Sample ID LCS-19078
SampType: LCS
TestCode: SVOC-PCB_ Units: mg/L
Prep Date: 3/3/2016
RunNo: 50615
Client ID: LCSW
Batch ID: 19078
TestNo: SW8082 SW3510C
Analysis Date: 3/4/2016
SegNo: 795302
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Total PCBs 0.00834 0.000100 0.0100 0 83.4 10 124
Sample ID LCSD-19078
SampType: LCSD
TestCode: SVOC-PCB_ Units: mg/L
Prep Date: 3/3/2016
RunNo: 50615
Client ID: LCSS02
Batch ID: 19078
TestNo: SW8082 SW3510C
Analysis Date: 3/4/2016
SegNo: 795303
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Fotal PCBs 0.00755 0.000100 0.0100 0 75.5 10 124 0.00834 9.92 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 10 of 29

Summit Environmental Technologies, Inc.
MIT 3310 Win St. QC SUMMARY REPORT
Ica+Ikr-JrJI.NI:'tLar�a�r�ruLut;i�s,art+ Cuyahoga Falls, Ohio44223 WO#: 16021626
_ Anaf,vUcal' L:Ti�o,r�lorlr e TEL: [phone] FAX.- [phone]
Website: htto:/hvww.settelc.com 14 Mm'-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID• 19080
iample ID MB-19080
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/3/2016
RunNo: 50581
lient ID: PBW
Batch ID: 19080
TestNo: SW6010C SW3010A
Analysis Date: 3/4/2016
SegNo: 794446
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-19080
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 3/3/2016
RunNo: 50581
;lient ID: LCSW
Batch ID: 19080
TestNo: SW6010C SW3010A
Analysis Date: 3/4/2016
SegNo: 794447
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.01
0.500
2.000
0
101
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
101
80
120
TCLP Cadmium(Cd)
2.01
0.100
2.000
0
101
80
120
TCLP Chromium(Cr)
2.02
0.200
2.000
0
101
80
120
TCLP Lead(Pb)
2.01
0.500
2.000
0
100
80
120
TCLP Selenium(Se)
2.00
0.500
2.000
0
100
80
120
TCLP Silver(Ag)
0.960
0.500
1.000
0
96.0
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 11 of 29

01- Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
dui �
I:c<NIF6VNT,II:N IAII IvUHNOLUOILS, INN. Cuyahoga Falls, Ohio 44223Sur WO#: 16021626
P �tr rr�+N.ca1 Labpr lorlr6 TEL: [phone] FAX.- [phone]
Website: hgp:/hvivmv.settelc.coni 14-Mat'-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchlD: 19092
Sample ID 16021794-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/4/2016
RunNo: 50586
Client ID: BatchQC
Batch ID: 19092
TestNo: SW7470A SW7470A
Analysis Date: 3/4/2016
SegNo: 795002
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00461 0.00200 0.00400 0 115 75 125
Sample ID 16021794-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 3/4/2016
RunNo: 50586
Client ID: BatchQC
Batch ID: 19092
TestNo: SW7470A SW7470A
Analysis Date: 3/4/2016
SegNo: 795003
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
FCLP Mercury 0.00459 0.00200 0.00400 0 115 75 125 0.00461 0.435 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 12 of 29

ZF1,14-MIA-117
Summit Environmental Technologies, Inc.
3310Win St. QC SUMMARY REPORT
cr4,v1KVNr,1i.N1,61,Jhtti Cuyahoga Falls, Ohio44223 WO#: 1602162G
?4.na4"11aaif Laboraro,�iv� TEL: [phone] FAX.- [phone]
Website: http://lvirtiv.settel(.com 14-Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID• 19159
Sample ID MB-19159
SampType: MBLK
TestCode: svoc-BNA T Units: mg/L
Prep Date: 3/8/2016
RunNo: 50725
client ID: PBW
Batch ID: 19159
TestNo: SW8270C SW3510C
Analysis Date: 3/8/2016
SegNo: 797708
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichi orophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0200
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Sample ID LCS-19169
SampType: LCS
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 3/8/2016
RunNo: 50725
:lient ID: LCSW
Batch ID: 19159
TestNo: SW8270C SW3510C
Analysis Date: 3/8/2016
SegNo: 797710
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene 0.893
0.100
1.000 0 89.3
10
134
2,4,5-Trichlorophenol 0.985
0.250
1.000 0 98.5
27
154
2,4,6-Trichlorophenol 1.03
0.250
1.000 0 103
27
154
2,4-Dinitrotoluene 1.01
0.0200
1.000 0 101
29
149
Cresols, Total ND
5.00
3.000 0 58.5
20
125
Hexachloro-1,3-butadiene 0.842
0.0200
1.000 0 84.2
14
126
Qualifiers: :" Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit Original
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Page 13 of 29

Summit Environmental Technologies, Inc.
"�"', g
'� � � iQC SUMMARY' REPORT
�,, �+� ��'� 3310 Win St.
a;:vlrr:r.�;r•�Gn;N IAL s ;-.C,11 IOLoJI!:Ia, ;rtr: Cuyahoga Falls, Ohio 44223 WO#: 16021626
^k.t3f� i1.caP C:T��ar9tarlE TEL: [phone] FAX.' [phone]
Website: Iattp://wtvw.settekcan 14-Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 19159
Sample ID LCS-19159
SampType: LCS
TestCode: svoc-BNA T Units: mg/L
Prep Date:. 3/8/2016
RunNo: 50725
client ID: LCSW
Batch ID: 19159
TestNo: SW8270C SW3510C
Analysis Date: 3/8/2016
SegNo: 797710
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Hexachlorobenzene
0.944
0.0200
1.000
0
94.4
1
162
Hexachloroethane
0.862
0.100
1.000
0
86.2
30
123
Nitrobenzene
0.890
0.100
1.000
0
89.0
25
190
Pentachlorophenol
0.983
0.250
1.000
0
98.2
4
186
Pyridine
0.361
0.250
1.000
0
36.1
5
130 m
Sample ID 16030149-001AMS
SampType: MS
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 3/8/2016
RunNo: 50725
lient ID: BatchQC
Batch ID: 19159
TestNo: SW8270C SW3510C
Analysis Date: 3/8/2016
SegNo: 798149
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene 0.937
0.200
1.000
0
93.7
10
134
2,4,5-Trichlorophenol 1.04
0.500
1.000
0
104
27
154
2,4,6-Trichi orophenol 1.08
0.500
1.000
0
108
27
154
2,4-Dinitrotoluene 1.05
0.0400
1.000
0
105
29
149
Cresols, Total ND
10.0
3.000
0
66.5
20
125
Hexachloro-1,3-butadiene 0.896
0.0400
1.000
0
89.6
14
126
Hexachlorobenzene 1.04
0.0400
1.000
0
104
1
162
Hexachloroethane 0.930
0.200
1.000
0
93.0
30
123
Nitrobenzene 0.919
0.200
1.000
0
91.9
25
190
Pentachlorophenol 1.12
0.500
1.000
0
112
4
186
Pyridine ND
0.500
1.000
0
20.5
5
130
mQMR
Qualifiers: k Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected
below quantitation limits
M Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting
Limit
O RSD is greater than RSDlimit
Original
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
Page 14 of 29

SuMmInt
Summit Environmental Technologies, rnc.
3310 Win St. QC SUMMARY REPORT
rr;.t'IkVNrnr;Nltt.IL-C NOLU101--s,JNC Cuyahoga Falls, Ohio44223 WO#: 16021626
l.t3dStii caf C.�hn.r9torie5 TEL: [phone] FAX.- [phone]
Website: hQ.-1Avivw.settekcont 14-Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 19159
Sample ID IB030149-001AMSD
SampType: MSD
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 3/8/2016
RunNo: 50725
Client ID: BatchQC
Batch ID: 19159
TestNo: SW8270C SW3510C
Analysis Date: 3/8/2016
SegNo: 798151
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene
0.824
0,200
1.000
0
82.4
10
134
0.9370
12.8
30
2,4,5-Trichlorophenol
0.977
0.500
1.000
0
97.7
27
154
1.037
5.96
30
2,4,6-Trichlorophenol
1.01
0.500
1.000
0
101
27
154
1.085
7.06
30
2,4-Dinitrotoluene
1.02
0.0400
1.000
0
102
29
149
1.050
2.60
30
Cresols, Total
ND
10.0
3.000
0
58.9
20
125
0
0
30
Hexachloro-1,3-butadiene
0.835
0.0400
1.000
0
83.5
14
126
0.8960
7.05
30
Hexachlorobenzene
1.02
0.0400
1.000
0
102
1
162
1.043
1.94
30
Hexachloroethane
0.817
0.200
1.000
0
81.7
30
123
0.9300
12.9
30
Nitrobenzene
0.836
0.200
1.000
0
83.6
25
190
0.9190
9.46
30
Pentachlorophenol
1.10
0.500
1.000
0
110
4
186
1.120
1.98
30
Pyridine
0.556
0.500
1.000
0
55.6
5
130
0.2050
92.2
30 R
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit,
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 15 of 29

¢ 2
�} �, ���1
Summit Environmental Technologies, Inc.
3310 win St.
QC SUMMARY REPORT
tr-A'IH NWI.NIALw;lrtc
Cuyahoga Falls, Ohio44223
WO#: 16021626
A.naIWI.P�aS Lab4orarafie.5
TEL: [phone] FAX.- [phone]
websiie: httv:1Avivw.settelccom
14 Mar-16
Client:
Synagro, NC 28134
Project:
West Stanly Utilities
BatchED: 19189
Sample ID mb-19189
SampType: mblk
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/9/2016
RunNo: 50893
lient ID: PBW
Batch ID: 19189
TestNo: SW8081A SW3510C
Analysis Date: 3/1112016
SegNo: 801224
�nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Chlordane, total
ND
0.0250
Toxaphene
ND
0.0500
Endrin
ND
0.00250
gamma-BHC
ND
0.00250
Heptachlor
ND
0.00250
Heptachlor epoxide
ND
0.00250
Methoxychlor
ND
0.00250
Sample ID Ics-19189
SampType: Ics
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/9/2016
RunNo: 50893
client ID: LCSW
Batch ID: 19189
TestNo: SW8081A SW3510C
Analysis Date: 3/11/2016
SegNo: 801225
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.0305
0.00250
0.0250
0
122
20
157
gamma-BHC
0.0257
0.00250
0.0250
0
103
22
137
Heptachlor
0.0279
0.00250
0.0250
0
111
24
121
Heptachlor epoxide
0.0252
0.00250
0.0250
0
101
27
152
Methoxychlor
0.0317
0.00250
0.0250
0
127
1
199
Qualifiers: :" Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 16 of 29

"� aLL 1 Y Su limit Environmental Technologies, Inc.
3310 Win St. QC SUMMARY REPORT
tr •aIRVINMUNIAL Af;tZHNULrJ131�s,M.C. Cuyahoga Falls, Ohio44223
FT
,� rwil!ii.cal Labor:at.rarfe� TEL: [phone] FAX.- [phone] WO#: 16021626
Website: http✓hvivw.settek.com 14-Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 19189
Sample ID 16030034-002ams
SampType: ms
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 3/9/2016
RunNo: 50893
Dlient ID: BatchQC
Batch ID: 19189
TestNo: SW8081A SW3510C
Analysis Date: 3/11/2016
SegNo: 801226
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.0168
0.00250
0.0250
0
67.3
20
157
gamma-BHC
0.0179
0.00250
0.0250
0
71.7
22
137
Heptachlor
0.0164
0.00250
0.0250
D
65.5
24
121
Heptachlor epoxide
0.0166
0.00250
0.0250
0
66.2
27
152
Methoxychlor
0.0173
0.00260
0.0250
0
69.3
1
199
Sample ID 16030034-002amsd
SampType: msd
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 3/9/2016
RunNo: 50893
;lient ID: BatchQC
Batch ID: 19189
TestNo: SW8081A SW3510C
Analysis Date: 311112016
SegNo: 801227
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Endrin
0.0127
0.00250
0.0250
0
50.8
20
157
0.0168
27.9 30
gamma-BHC
0.0136
0.00250
0.0250
0
54.6
22
137
0.0179
27.1 30
Heptachlor
0.0127
0.00250
0.0250
0
50.8
24
121
0.0164
25.3 30
Heptachlor epoxide
0.0127
0.00250
0.0250
0
50.8
27
152
0.0166
26.4 30
Methoxychlor
0.0131
0.00250
0.0250
0
52.5
1
199
0.0173
27.5 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 17 of 29

Summit Environmental Technologies, Inc.
plot 3310 Win St. QC SUMMARY REPORT
cr,;vlRV N411INi 1. 9 t;tiMUL U1!:S, JNU Cuyahoga Falls, Ohio 44223 WO#: 16021626
!X.7�tttt[dcal Lzrtaoratgri TEL: [phone] FAX.- [phone]
Website: http:/hvww.settelacom 14-Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50283
Sample ID MB-R50283
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: PBW
Batch ID: R50283
TestNo: SW9034
Analysis Date: 2/2612016
SegNo: 788524
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive ND 25.0
Sample ID LCS-R50283
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: LCSW
Batch ID: R50283
TestNo: SW9034
Analysis Date: 2/26/2016
SegNo: 788525
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 81.8 25.0 86.00 0 95.1 85 115
Sample ID 16021626-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: West Stanly Utilities
Batch ID: R50283
TestNo: SW9034
Analysis Date: 2/26/2016
SegNo: 788526
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 84.6 25.0 86.00 0 98.4 75 125
Sample ID 16021626-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: West Stanly Utilities
Batch ID: R50283
TestNo: SW9034
Analysis Date: 212612016
SegNo: 788527
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 82.6 25.0 86.00 0 96.0 75 125 84.60 2.39 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 18 of 29

_ Summit Environmental Technologies,lnc. QC SUMMARY REPORT
?I 1 3310 Win St.
r_r:v H�a r� Gn; ry i Al. w rarada aLu r s, .inr �. Czryahoga Falls, Ohio 44223 WO#: 16021626
__. A4r t/y L ua! L:7 7pf 9IOFA�' TEL: [phone] FAX.- [phone]
Website: htto✓%vww.settelc.coni 14-Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50283
Sample ID
16021626-001AMSD SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
-lient ID:
West Stanly Utilities Batch ID: R50283
TestNo: SW9034
Analysis Date: 2/26/2016
SegNo: 788527
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 19 of 29

y r� �� Sunrrriit Environmental Technologies, Inc.
U � s 3310 Win St. QC SUMMARY REPORT
tr,;vIRVNrni;Niah +aa a�rauLuc;t�s, trvti Cuyahoga Falls, Ohio44223 W09: 16021626
_a rra(vii.cz1 TEL: [phone] FAX.- [phone]
Website: hgg.-111vww.settekcoin 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50284
nple ID MB-R50284
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 50284
ant ID: PBW
Batch ID: R50284
TestNo: SW9014
Analysis Date: 212612016
SegNo: 788536
Ilyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua
Cyanide, Reactive ND 0.500
Cyanide, Reactive 1.04 0.500 1.000 0 104 85 110
Cyanide, Reactive 1.01 0.500 1.000 0 101 85 110
Cyanide, Reactive
0.965 0.500
1.000 0 96.5 85
110
1.010 4.56 20
Qualifiers: :k
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
Ii
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 20 of 29

rr
._ Summit Environmental Technologies, Inc.
:,- � i
33Win St. QC SUMMARY REPORT
�N'wIH-Q-N UN I Al, Ito epi 4L4C3P�S; Mc Cuyahoga Falls, Ohio 44223 WO#: 16021626
lk�Bi4Ei.r.�f CzTURr9dO,rj�5 TEL: [phone] FAX.- [phone]
Website: http:/hvipw.settelf.coni 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50284
Sample ID
16021626-001AMSD SampType: MSD
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 50284
Client ID:
West Stanly Utilities Batch ID: R50284
TestNo:
SW9014
Analysis Date: 2/26/2016
SegNo: 788540
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 29

Summit Environmental Technologies, Inc.
ir 3310 Win St. QC SUMMARY REPORT
�MVIRV Ntolr:n i RL R 7aA1?4 )LUUU s; ]KC. Cuyahoga Falls, Ohio 44223 WO#: 16021626
Email l.ca.t C:Tbcr,ralnrifrs TEL: [phone] FAX.• [phone]
website: http://lyww.settelc.coni 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50411
Sample ID LCS-R50411
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@20.8C
Prep Date:
RunNo: 50411
lient ID: LCSW
Batch ID: R50411
TestNo: A4500-H+B
Analysis Date: 3/1/2016
SegNo: 791013
analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH
7.04
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
7.000 0 101 90 110
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 22 of 29

:Ky mt Summit Environmental Technologies, Inc. C SUMMITRY REPORT
3310 Win St. `�
t r VIKU'Nrnr:N I Al. I I.L;MNJLIJUI�:'i:, 'KC Cuyahoga Falls, Ohio 44223 WO#: 16021626
A 4: ralyUcrri TEL: [phone] FAX.- [phone]
Website: ham:/Avivw.settek..com 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50598
Sample ID LCS-R50598
SampType: LCS
TestCode: FlashPt_NP Units: T
Prep Date:
RunNo: 50598
client ID: LCSW
Batch ID: R50598
TestNo: SW1010
Analysis Date: 3/4/2016
SegNo: 794917
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Flashpoint (200T)
115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
.MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
120.0 0 95.8 90 110
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 23 of 29

sumaomlwt
SunarnitEnvironmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
LNiVIRVNmr,N191.gh-CHNULui71tL�,IIVlG Cuyahoga Falls, Ohio44223 WO#: 1602162G
_. _ /4ratrClcaf L rbei,ratoFit:S TEL: [phone] FAX.- [phone]
Website: httv://iviviv.settelccom 14-Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50630
Sample ID
16021626-001AMS SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 50630
Client ID:
West Stanly Utilities Batch ID: R50630
TestNo: SW8321A
Analysis Date: 3/4/2016
SegNo: 798230
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
57.6
5.00
50.00
0
115
37
105
S
2,4,5-TP
61.8
0.500
50.00
0
124
38
106
S
Sample ID 16021626-001AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 50630
Client ID: West Stanly Utilities
Batch ID: R50630
TestNo: SW8321A
Analysis Date: 3/4/2016
SegNo: 798231
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D 57.1 5.00 50.00 0 114 10 150 57.56 0.855 30
2,4,5-TP 6.1.7 0.500 50.00 0 123 10 150 61.78 0.190 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 24 of 29

C� -'� Sztmmit Environmental Technologies, Inc.ffl QC SUMMARY REPORT
y,_ - �`� " 3310 Win St.
er; 41 KV N ra l:N I Al, I I-VHNU LUUU:11 , 1R C. Cuyahoga Falls, Ohio 44223 WO#: 16021626
4w t1,Uu,3f Lab, ralurieS TEL: [phone] FAX.• [phone]
Website: htty.-Mvivw.settek.can 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchED: R50630
2,4-D ND 5.00
2,4,5-TP ND 0.500
2,4-D
56.9
5.00
50.00
0
114
37
105
S
2,4,5-TP
59.2
0.500
50.00
0
118
38
106
S
2,4-D 56.4 5.00
50.00 0 113 37
105
56.92 0.912
30 S
2,4,5-TP 62.0 0.500
50.00 0 124 38
106
59.23 4.61
30 S
Qualifiers: k Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
Original
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 25 of 29

tF Summit Environmental Technologies, Inc. QC SUMMARY REPORT
}
�C:rdIH�Vr+M�;M I..u, a 1,6Hz4oLuU1!:s:, ar,r-. Cuyahoga Falls, Ohio 44223 WO#: 16021626
ff
_ 3310 Ilrin St. lkrt�'i�,//lafff Laboraforipu TEL: [phone] FAX.- [phone]
Website: http:/hvwtv.settelc.com 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchED: R50635
Sample ID Ics 20ppb voc-s-
SampType: LCS
TestCode: VOC-mstr_np Units: mg/L
Prep Date:
RunNo: 50635
Client ID: LCSW
Batch ID: R50635
TestNo: SW8260B
Analysis Date: 3/4/2016
SegNo: 795649
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.0188
0.00500
0.0200
0
93.9
71
138
Benzene
0.0192
0.00500
0.0200
0
95.8
75
137
Chlorobenzene
0.0191
0.00500
0.0200
0
95.7
77
132
Trichloroethene
0.0186
0.00500
0.0200
0
92.8
64
119
Sample ID lesd 20ppb voc-s
SampType: LCSD
TestCode: VOC-mstr_np Units: mg[L
Prep Date:
RunNo: 50635
Client ID: LCSS02
Batch ID: R50635
TestNo: SW8260B
Analysis Date: 3/4/2016
SegNo: 795650
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0206
0.00500
0.0200
0
103
71
138
0.0188
9.34 30
Benzene
0.0202
0.00500
0.0200
0
101
75
137
0.0192
5.48 30
Chlorobenzene
0.0199
0.00500
0.0200
0
99.6
50
150
0.0191
4.00 30
Trichloroethene
0.0198
0.00500
0.0200
0
99.0
64
119
0.0186
6.46 30
Sample ID mblk
SampType: MBLK
TestCode: VOC-mstr_np Units: mg/L
Prep Date:
RunNo: 50635
Client ID: PBW
Batch ID: R50635
TestNo: SW8260B
Analysis Date: 3/4/2016
SegNo: 795651
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
1,2-Dichloroethane
ND 0.00500
ND 0.00500
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 26 of 29

4 Summit Environmental Technologies, Inc. QC SUMMARY REPORT
1 3310 Win St.
tr.,vlrsVNMUNJ;kk ai:�rad�ouar�i�s; ar Cuyahoga Falls, Ohio44223 WO#: 16021626
Are yfi' a.f Lzbor9tofie,5 TEL: [phone] FAK- [phone]
Website: hgp:Ilivivw.settelc.coni 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50635
Sample ID mblk
SampType: MBLK
TestCode: VOC-mstr_np Units: mg/L
Prep Date:
RunNo: 50635
client ID: PBW
Batch ID: R50635
TestNo: SW8260B
Analysis Date: 3/4/2016
SegNo: 795651
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
MEK
ND
D.0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetra chloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
B Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 27 of 29

Tsumwun-
Summit Environmental Technologies, Inc.
3310WinSt. QC SUMMARY REP®RT
LMVIKV VANNIIAl. r Ft;HuUL1i1:S, rr,..c. Cuyahoga Falls, Ohio 44223WO#: 16021626
;X.rw� l,,ti.caf L..Tbq,rotnrh,-u TEL: [phone] FAX.- [phone]
Website: http://lvivw.settelc.cotit 14 Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchYD: R50635
Sample ID 16021680-002ams
SampType: MS
TestCode: tclp-VOC-mst Units: mg/L
Prep Date:
RunNo: 50635
lient ID: BatchQC
Batch ID: R50635
TestNo: SW8260B
Analysis Date: 3/4/2016
SegNo: 795670
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.198
0.100
0.200
0
99.0
39.9
160
1,2-Dichloroethane
0.198
0.100
0.200
0
99.1
42.5
157
MEK
ND
2.00
1.00
D
107
16.6
227
Benzene
0.198
0.100
0.200
0
99.2
38.1
155
Carbon tetrachloride
0.193
0.100
0.200
0
96.5
40.8
162
Chlorobenzene
0.199
0.100
0.200
0
99.7
35.7
168
Chloroform
0.183
0.100
0.200
0
91.7
18.3
199
Tetrachloroethene
0.194
0.100
0.200
0
97.0
10
261
Trichloroethene
0.193
0.100
0.200
0
96.7
23.8
175
Vinyl chloride
0.220
0.200
0.200
0
110
10
165
Sample ID 16021680-002amsd
SampType: MSD
TestCode: telp-VOC-mst Units: mg/L
Prep Date:
RunNo: 50635
;lient ID: BatchQC
Batch ID: R50635
TestNo: SW8260B
Analysis Date: 3/4/2016
SegNo: 795671
%nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1, 1 -Dichloroethene
0.212
0.100
0.200 0 106
39.9
160
0.198 7.02
25
1,2-Dichloroethane
0.200
0.100
0.200 0 99.9
42.5
157
0.198 0.804
25
MEK
ND
2.00
1.00 0 108
16.6
227
0 0
25
Benzene
0.208
0.100
0.200 0 104
38.1
155
0.198 4.67
25
Carbon tetrachloride
0.207
0.100
0.200 0 104
40.8
162
0.193 7.10
25
Chlorobenzene
0.203
0.100
0.200 0 101
35.7
168
0.199 1.59
25
Chloroform
0.191
0.100
0.200 0 95.4
18.3
199
0.183 4.01
25
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 28 of 29

Sum
Summit Environmental Technologies, Inc. _ °S�:+ 3 . ._ 3310 win St. QC SUMMARY REPORT
V IRUT-4 611 N I Ak R fvumuriLucil s, m.c . Cuyahoga Falls, Ohio 44223 W09: 16021626
pt.n�ttlri':w�!' C:a r9r.vrFes TEL: [phone] FAX.- [phone]
Website: htto:/hvw").settelf.coni 14-Mar-16
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R50635
Sample ID 16021680-002amsd
SampType: MSD
TestCode: tclp-VOC-mst Units: mg/L
Prep Date:
RunNo: 50635
Client ID: BatchQC
Batch ID: R50635
TestNo: SW8260B
Analysis Date: 3/4/2016
SegNo: 195671
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Tetra chloroethene 0.198 0.100 0.200 0 99.0 10 261 0.194 2.04 25
Trichloroethene 0.203 0.100 0.200 0 102 23.8 175 0.193 4.94 25
Vinyl chloride 0.234 0.200 0.200 0 117 10 165 0.220 6.29 25
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 29 of 29

Ii n
Summit Environmental Technologies, le,u,
Cooler Receipt Form
Initials Ji pEfSC Ins n C
sfarrples:
tin,
Omar !Jumar: 1
rco'-.)erla(nd.
V • I ( [�'W
Date r._Cahved: '~.. v i irie Riceivad:
,� ..
!Y" c._ '73t8 coDle:4s} Cper:e9 arld s3mpleS
IDSG?'[2d;
1Jur ber of CoolerSJjC);�" 1
"-
NA
Jr I1LID_� FED -}�
1 P_sicl '�'at}; i:1 Pic';up Other:
Paci,aging_ peanut_ �ubbk ll'rF Paoer =Darn None c `-
t`
art•= n� cool�rloOx;
It `` N
NIA
cusm'-v Seals inzaCt
ti' rJ
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C-O.-C in plastic
1J
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Ice Blue ice
r�r�G FF I i meltad
fufA,
Sample i �mpe-atur IP Bun a18320459 CF
(absent
l�, 'C
NA
Radiologicaf T=_sting Instrument serial �3512 i
y x,
fssa page 2 for scan results)
n;n
"Use 1 sheat per sample ror Radiological Testing_ If sample is HOT, the Radiological
immediately.
Safety
Officer must be notified
C-O-- flled out P. Dparly
Y tJ
c%
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samples i-1 sepamt-s )bags
S
Y
l.J
N/A
Sample Containers ir2act'
_ r
J
NIA
'I no. list Groe arl Sa Dt391:
Sampls labelfs; compute (ID. date. etc,)
Y
fJ
Label(:) acres with C-O-C
v Y
COME tcntrinersused
Y
hi
N!A
Surteient sample ra�eivad
•�
I`,
,`frt
Samples recewL-i V;:tniri hclding time
Y
I'J
Bubbles absel-.t from 40 mt_ vials^
Y
!J
N!A
" S311MAS?.h bubbles co"tnm are as pt<tble.
Indicate bubble si=s if>6mm.
'A'as client contacted about samples
Y tJ
Will dleril send re"sr samples
Y N
Client conlec
Date,ri'h�ie.-
Lociged it by:
Page 1 of 71

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name West Stanly WWTP Permit Number WQ0016247
WWTP Name West Stanly WWTP NPDES # NC
Monitoring Period: From 01 / 01 / 16 To 12 / 31 / 16
Pathogen Reduction (40 CFR 503.32) — Please indicate level achieved and alternative performed
Class A
Alternative 1 Alternative 2 Alternative 3
Alternative 4 Alternative 5 Alternative 6
Class B X
Alternative 1 X Alternative 2 Alternative 3
If applicable to alternative performed (Class B only) indicate " Process To Significantly Reduce Pathogens ".
Aerobic Digestion Air Drying Anaerobic Digestion Composting Lime Stabilization
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable
Pathogen Density
Number of
Frequency
Sample
Analytical
Parameter
Level inSludge
Minimum
GeoMn.
Maximum
Units
Exceedences
of Analysis
Type
Technique
Fecal
2 x 106 MPN
Coliform
per gram of total
8,448
13,193
18,993
MPN/g
0
Annual
Grab
SM 9221 E
solids or 2 x 106
CFU per gram
of total solids
1000 IvIPN
per gram of
total solid
weight)
Salmonella
3MPNper4
Bacteria (in
grams total solid
lieu of fecal
(dry weight)
coliform)
Vector Attraction Reduction (40 CFR 503.33) — Please indicate option performed
Option 1 Option 2 Option 3 X Option 4 Option 5,
Option 6 Option 7 Option 8 Option 9 Option 10
No vector attraction reduction options were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
X " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
" I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." ( Please note if you check this statement
attach an explanation why you have not met one or both ofthe requirements)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print)
�3 /
ignature of Preparer Date
Signature of Land Applier (if applicable) Date

PAAM mmulm
mummm
9-44 FiL.
PROMPT•ACOU RATE• RELIABLE
LABORATOR.IESa INC
WWNV.PARLABS.00,1I
REPORT OF ANALYSES
Attn: DREW CULP
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: FEB 16
DATE: 03/.17/16
SAMPLE NUMBER- 122420 SAMPLE ID- WEST STANLY UTILITIES 50-2170 SWPLE MATRIX- SO
DATE SAMPLED- 02/23/16 TIME SAMPLED- 0948
DATE RECEIVED- 02/23/16 SAMPLER- DC RECEIVED BY- DJ
TIME RECEIVED-- 1242 DELIVERED BY- DC TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 02/23/16 1500 RE < 13,193 MPN/g
LABORATORY DIRECTOR
P.O. Box 411483 • Charlotte, NC 28241-1483
P[ione: [phone] • Fax: [phone]

RALF;Z
PROMPT-ACOURATE• RE:LIAF]LE
LABOiZATORi�Sa INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
SYNAGRO
WEST STANLEY UTILITIES 60-2170
e 4 02/23/16
FECAL COLIFORM, GEOMETRIC MEAN
• e SM 9221 E
122420
1
< 209
1.19%
< 17,655.52
2
< 129
1.19%
< 10 825.94
3
< 98
1.15%
< 8,647,76
4
< 100
1.18%
< 8,447,54
5
< 185
1.16%
< 15,926.90
6
< 195
1.17%
< 16,667.33
7
< 224
1.18%
< 18,992.78
��I"ec�i Co1lfo�rri :� ,
Geametr�cJVleat�, •

PAR CHAIN OF CUSTODY
M8ORaTORIES,INC. PAR Laboratories, Inc
�. Phone [phone]
www.parlabs.com Eax [phone]
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded an this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North
uarouna ue anment or tnvlronmental and Natural ResonrCe8,
Company Name (billing) Comments/ Special Instructions
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State Ft zip code
PINEVILLE NC 28134
Point of Contact Et Telephone Number
DREW C(/L-P 7,04-574-52?J
Sample
taken By: SIGNATURE
ft
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES X NO
*Sample Type: DW ww GVVMW Hw $all Other AIDS.,.
Sample Temp at time of sampling: a C Sample Temp upon receipt: ° C
**Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No _ n/a
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (Y/N):
Client Sample I.D.
(Sample locatlon I Number)
Comp
Grab
Preserv.
Set Up
Datemme
Collection
DataMme
Analyses
Requested
'
X
5'0 — oZ! -0 0-016
rceunqufsnua DX. vale/ I me Ke a oy: Uatei I ime
zas
Relinquished by: ate lme Received by: Datefrime
* C=Composite G=Grab DW=Drinking Water WW=Wastawater GWMW=Groundlvater Monitoring Well HW=Hazardous Waste "See
Other Side

A
PROM PT•ACCU RATE• REL I A BLE
LABORA'FORIESY INC
WWWPARLABS.CONi
REPORT Or ANALYSES
Attn: DREW CULP
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: PEB 16
DATE: 03/24/16
SAMPLE NUMBER- 122419 SAMPLE `_+D- WEST STANLY UTILITIES 50-2170 SAMPLE MATRIX- SO
DATE SAMPLED- 02/23/16 TIME SAMPLED- 0945
DATE RECEIVED- 02/23/16 SAIMPLER- DC RECEIVED BY- DJ
TIME RECEIVED- 1242 DELIVERED BY- DC TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS 'METHOD
30 DAY BENCH SCALE TEST VAR
ANALYSIS
DATE TIME BY RESULT UNITS
02/23/16 1400 RE ATTACHED
LABORATORY DIRECTOR
P.O. Box 411483 - Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]
e

PAAF;Z
PROM PT•ACOU RATE• RELIABLE
LABORATORIES, IWC
WWW.PARLABS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
Start: End:
TS )
0.1643
0.1653
TS%
1.18%
1.19%
VS
0.1160
0.1126
VS%
70.60%
68.12%
i N
0.003278
OUT
0.00318409
FSVR (Mass Balance)
2.85%
FSVR an Kleeck)
11.04%
FSVR Mass Balance <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Boa 411483 r Charlotte, NC 28241-1483
Phone: [phone] Fax: [phone]

fo:ATRORES'INC.
www.pariabs.com
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Company Name (billing)
Comments/ Special Instructions
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State i} zip code
PINEVILLE NC 28134
Point of Contact It Telephone Number
'DREW C"L-P 7e-1-574-5M
sample
Taken By:
SIGNATURE
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES _)�_NO
*Sample Type: DW Ww GWMVV HW Soil Other 9.11SO(If
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
**Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
Client Sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date/rime
Collection
DateMme
Analyses
Requested
G,IGs� l (!t 1't i -h ems`
X
o.? - 2 3 - / 6
6-7: q5
3 o - y
0 / -0
e,,5
elingwsnea I Ifrl@ RCl C tv V / i vawr i uiic
612101
Relinquished by: Dalef re Received by: DateRme
C=Composite G=Grab DW--Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste "See
Other Side

Agricultural Lime Application Log
2016
Project: West Stanley Utilities
Field
(state -county -site -field)
Grower
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date
Applied
Total
Acres
NC-ST-03-03
Robert Ridenhour
6.3
0 tons/acre
N/A
N/A
TOTAL
0.0
* lime will be spread when crop and field conditions are suitable

Page 1 of 1
Report Number: 17-011-0514
Account Number:46477
Send To: Synagro Central LLC/ Oakboro
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypointo
ANALYTICAL
"Every acre... Every year. "Tu
Date Received: 01/11/2017 Date Of Analysis: 01/12/2017
Submitted By: Clay Fisackerly
Farm ID: NC-ST-03
SOIL ANALYSIS REPORT
Date Of Report: 01/17/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Robert Ridenhour
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
%
Soil
M3
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
Rate
Class
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
03
09575
5.0
141
53 H
38 VL
194 VH
774 M
19 VL
6.3
0.7
6.4
H
I MIN
NC = 44
NC = 19
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
NH4-N
Sample ID
K
Mg
Ca
Na
H
NO, N
S
Zn
Mn
Fe
Cu
B
SS
Field ID
ova
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm
03
1.5
25.3
60.5
1.3
10.9
1 VL
8 VL
4.7 H
35 H
155 VH
2.2 H
0.2 VL
2
NC=17
NC=117.5
NC=219
NC=110.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
by: Pauria W Ge-r
Pauric McGroary

x
�2-
(6
(j
RECeIVED/NCDENR/DWR
MA; 12016
WQROS
MOORESVILLE REGIONA . L OFFICE
RECEIVED/NCDEQ/DWR
FEB 19 2016
Nan-018oharge
POrmiffing Unit
Western Piedmont Regional, NC
Class B Residuals Land Application Program
Permit No. WQ0016247
2015 ANNUAL REPORT

Western Piedmont Regional, NC
Class B Residuals Land Application Program
2015 Annual Report
TABLE OF CONTENTS
1. Certification Form
2. City of Statesville
3. Stanly County Utilities

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00016247 County Alexander Year 2015
Facility Name (as shown on permit) West Stanly WWTP, City of Statesville, Third Creek WWTP & Fourth Creek WWTP NPDES
No. NC0043532, NC0020591, & NCO031836
Land Application Operator Svnagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 31
Total number of fields utilized for land application during the year: 7
Total amount of dry tons applied during the year for all application sites: 344.76
Total number of acres utilized for land application during the year: 108.1
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2015 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. ]
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Marshall Purvear. Technical Services Manager
Permittee Name and Title (type or print) Sigl f Per'11117& Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2015 ANNUAL REPORT
PROJECT:
FACILITY:
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
City of Statesville, NC
Third Creek WWTP
NCO020591
Todd Norman, Residuals
Superintendent
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Todd Norman, Third Creek WWTP Supt.
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

2015 ANNUAL OPERATIONS SUMMARY- LAND APPLICATION.
ATATESVILLE, NC
.;TATESVILLE, NC FOURTH CREEK CAKE
MONTH/YEAR
AMOUNT UNIT
DRY TONS
UNIT
May 2015
850.00 Y
93.41
D
June 2015
375.00 Y
41.22
D
YEARLY TOTAL
1,225.00 Y
134.63
D
STATESVILLE, NC THIRD CREEK CAKE
MONTH/YEAR
AMOUNT UNIT
DRY TONS
UNIT
May 2015
1,100.00 Y
194.38
D
YEARLY TOTAL
1,100.00 Y
194.38
D
DRY METRIC
TONS
84.75
37.38
122.13
DRY METRIC
TONS
176.30
176.30
2/5/2016

2015 ANNUAL REPORT
PROJECT:
FACILITY:
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
City of Statesville, NC
Fourth Creek WWTP
NC0031836
Andy Smith, Residuals Superintendent
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Andy Smith, Fourth Creek WWTP Supt.
Town of Statesville
P.O. Box 1111
Statesville, NC 28677
[phone]
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type
CAx
CAx
CAx
Date Sampled (grab) or 03/26/15
04/23/15
09/21/15
Date Composited
Percent Solids
14.20
13.05
13.87
PARAMETERS (mg/kg dry weight)
Arsenic
<3
3
4
Cadmium
3
4
3
Mercury
0. 9
1
1.2
Chromium
35
51
48
Copper
273
286
333
Lead
21
24
26
Molybdenum
12
13
14
Nickel
21
28
26
Selenium
<5
<5
<5
Zinc
524
535
596
Total Phosphorus
24200
24900
28100
TKN
64600
68600
54400
Ammonia -Nitrogen
9790
11600
5620
Nitrate and Nitrite
18.3
<2
<2
Laboratory
WAYPOINT ANALYTICAL
A&L Eastern Laboratories Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant,penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF PREPARER)
Date �wb— Icle
DENR FORM RSSF (5/2003) Printed: Friday - February 5, 2016 at 10:58:49 for: 2084 01

AI NNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type CAx
CAx
CAx
Date Sampled (grab) or 03/26/15
04/23/15
09/21/15
Date Composited
Percent Solids 14.20
13.05
13.87
PARAMETERS (mg/kg dry weight)
Aluminum 17700
18200
24700
Calcium 8030
10700
6660
Magnesium 2870
2990
1860
pH 7.21
7.81
6.26
Potassium 3570
3400
2500
Sodium 731
685
801
Laboratory
WAYPOINT ANALYTICAL
A&L Eastern Laboratories Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significanj pepalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
,TUJRE OF PREPARER)
NR - Data Not Reported or Data Not Required
Date �(� —�0
DENR FORM RSSF-B (7/2002) Printed: Friday - February 5, 2016 at 10:59:25 for: 2084 01

Page: 1 of 2
Report Number: 15-086-0202
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 60953
Sample Id : STATESVILLE 4TH CK
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwmaleastern.com
Project: STATESVILLE 4TH CK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/26/2015 11:25:00
Date Received: 03/27/2015 00:00
Date Reported: 04/01/2015
Total Solids *
14.20
142000
100.0
JM
03/30/2015 09:24
SM-2540G
Moisture *
85.80
100.0
JM
03/30/2015 09:24
SM-2540G
Total Kjeldahl Nitrogen
6.46
64600
10.0
JM
03/30/2015 09:00
SM-4500-NH3C-TKN
Total Phosphorus
2.42
24200
100
KM
03/30/2015 15:22
SW 6010C
Total Potassium
0.36
3570
100
KM
03/30/2015 15:22
SW 6010C
Total Sulfur
0.77
7680
100
KM
03/30/2015 15:22
SW 6010C
Total Calcium
0.80
8030
100
KM
03/30/2015 15:22
SW 6010C
Total Magnesium
0.29
2870
100
KM
03/30/2015 15:22
SW 6010C
Total Sodium
0.07
731
100
KM
03/30/2015 15:22
SW 6010C
Total Iron
17300
100
KM
03/30/2015 15:22
SW 6010C
Total Aluminum
17700
100
KM
03/30/2015 15:22
SW 6010C
Total Manganese
1320
5
KM
03/30/2015 15:22
SW 6010C
Total Copper
273
5
KM
03/30/2015 15:22
SW 6010C
Total Zinc
524
5
KM
03/30/2015 15:22
SW 6010C
Ammonia Nitrogen
0.98
9790
10.0
JM
03/30/2015 09:00
SM-4500-NI3C
Organic N
5.48
54810
10.0
03/30/2016 09:00
CALCULATION
Nitrate+Nitrite-N
18.3
2.00
JM
03/30/2015 09:00
SM-450ONO3F
Total Cadmium
3.0
2.0
KM
03/30/2015 15:22
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-086-0202
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
99. A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: STATESVILLE 4TH CK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/26/2015 11:25:00
Lab Number: 60953 Date Received: 03/27/2015 00:00
Sample Id : STATESVILLE 4TH CK Date Reported: 04/01/2015
Total Chromium
35
Total Nickel
21
Total Lead
21
Total Arsenic
<3.0
Total Mercury
0.9
Total Selenium
<5.0
pH (Standard Units) *
7.21
Total Molybdenum
12
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
5
KM
03/30/2015 15:22
SW 6010C
5
KM
03/30/2015 15:22
SW 6010C
5
KM
03/30/2015 15:22
SW 6010C
3.0
KM
03/30/2015 15:22
SW 6010C
0.4
KM
03/30/2015 09:00
SW-7471 B
5.0
KM
03/30/2015 15:22
SW 6010C
2.00
JM
03/30/2015 09:00
SW-9045D
5
KM
03/30/2015 15:22
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption ' Ratio Calculation (SAR)
Product Code - Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 3/26/2015 1/112015-4130/2016 0.6692
Na mg/I = (Na mg/kg x % Solids) -= 100 = (731 x 14.2000) = 100 = 103.802
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (8030 x 14.2000) _ 100 = 1140.26
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2870 x 14.2000) = 100 = 407.54
Na meq = Na mg/I - Molec.Wgt.Na = 103.802 + 23 = 4.51313
Ca meq = Ca mg/I - Molec.Wgt.Ca = 1140.26 + 20 = 57.013
Mg meq L Mg mg/I - Molec.Wgt.Mg = 407.54 _ 12 = 33.9617
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.51313 = SgrRoot[0.5(57.013+33.9617)] = 0.669164
Printed: 2/5/2016
Page 1 11:02

Page: 1 of 2
Report Number: 15-114-0201
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 61587
Sample Id: STATESVILLE 4TH CK
A&L Eastern Laboratories, Inc.
@P. 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 4/23/2015 09:45:00
Date Received: 04/24/2015 00:00
Date Reported: 04/29/2015
Total Solids *
13.05
130500
100.0
BW
04/24/2015 15:00
SM-254OG
Moisture *
86.95
100.0
BW
04/24/2015 15:00
SM-2540G
Total Kjeldahl Nitrogen
6.86
68600
10.0
JM
04/27/2015 09:24
SM-4500-NH3C-TKN
Total Phosphorus
2.49
24900
100
KM
04/27/2015 13:15
SW 6010C
Total Potassium
0.34
3400
100
KM
04/27/2015 13:15
SW 6010C
Total Sulfur
0.82
8150
100
KM
04/27/2015 13:15
SW 6010C
Total Calcium
1.07
10700
100
KM
04/27/2015 13:15
SW 6010C
Total Magnesium
0.30
2990
100
KM
04/27/2015 13:15
SW 6010C
Total Sodium,
0.07
685
100
KM
04/27/2015 13:15
SW 6010C
Total Iron
17800
100
KM
04/27/2015 13:15
SW 6010C
Total Aluminum
18200
100
KM
04/27/2015 13:15
SW 6010C
Total Manganese
1210
5
KM
04/27/2015 13:15
SW 6010C
Total Copper
286
5
KM
04/27/2015 13:15
SW 6010C
Total Zinc
535
5
KM
04/27/2015 13:15
SW 6010C
Ammonia Nitrogen
1.16
11600
10.0
JM
04/27/2015 09:24
SM-4500-NH3C
Organic N
5.70
57000
10.0
04/27/2015 09:24
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
04/27/2015 09:25
SM-450ONO3F
Total Cadmium
4.0
2.0
KM
04/27/2015 13:15
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-114-0201
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 61587
Sample Id: STATESVILLE 4TH CK
A&L Eastern Laboratories, Inc.
99.
7621 Whitepfne Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleasteril.com
Project: STATESVILLE 4TH CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/23/2015 09:45:00
Date Received: 04/24/2015 00:00
Date Reported: 04/29/2015
Total Chromium
51
5
KM
04/27/2015 13:15
SW 6010C
Total Nickel
28
5
KM
04/27/2015 13:15
SW 6010C
Total Lead
24
5
KM
04/27/2015 13:15
SW 6010C
Total Arsenic
3.0
3.0
KM
04/27/2015 13:15
SW 6010C
Total Mercury
1.0
0.4
KM
04/28/2015 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
04/27/2015 13:15
SW 6010C
pH (Standard Units) * 7.81
2.00
JM
04/27/2015 09:24
SW-9045D
Total Molybdenum
13
5
KM
04/27/2015 13:15
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE RPD WAS OUT OF LIMITS FOR "NO3/NO2-N".
THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al",
"Cr", AND "Ni". ALL OTHER QC DATA
IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

SAMPLING LOG #'
�L=
COST. iMER: S.YNAGRO
15-114-0201
I IIIIII�IIII IIICIIIIII IIIII IIIILIIII �IIII II I IIIII IIIILIIII IIIL4649�
SYNAGRO G.ENTRAL LW/sT.AT.ESVILLE,, 04 242015
STATESVILLE 4rH CPC 1$:31:07
PROJECT MANAGER: 1 I7��t,±ram �t J ff
Phone: �•� �.�,.) �`� j � � 0 � ,�" _ �4� ��
ECO)RD
am Wng roeedures
tiVerQ;Cl5 a raurrrry urn C ijirr t� o(7;of X.Pr.5.MP,es
A-& L CUSTOMER:
SAMPLING
SAMPLE
W'OP SAMPLING
METNOb
MET oij
1AI3.:lt SAMPLE I.D.:
LOCATION
TYPE
CONTAINERS DATE TIME
PRESERVED
SFIII?.PED
44
Relinquished by Sam I r:
Date Timm
Recieved by;
REMARKS:
—`� . / Date Ti ..� Recleved h
Relihquiishe.d'by; Y
;19e.ICn.quf"sh©d'by_ Date Tit•ne Recleaned by,
SPECIAL INSTRUCTID"NS:
P9[.` For
1.6
monito.6ng purposes,
Pail,"
SAMPLEANALYSIS
REQUEST
I C
SL:t
SL2
N14,41
1�C� _NFIN
taic
cd
Cr
NI
Erb
As:
GIB,
Se .'
PH
equiv. v
Sollitl's
M'o
Cl
Nof N:
S'f f{.1'vj'
:-. •;
:
1
1
PO.
.
.'
eAl +
SLf- Total Solids:(Molsture),. Total, Kjeldahl •Nitrogen, Phosphorus, :and Potassi m
SL2: Basic Test'SL1 plus Sulfur, Calcium, Magnesium, Sodium,, Iron, Aluminum., Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 4/23/2015 51112016-613012016 0.5433
Na mg/I = (Na mg/kg x % Solids) : 100 = (685 x 13.0500) =100 = 89.3925
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10700 x 13.0500) _ 100 = 1396.35
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2990 x 13.0500) _ 100 = 390.195
Na meq = Na mg/I = Molec.Wgt.Na = 89.3925 -= 23 = 3.88663
Ca meq = Ca mg/I = Molec.Wgt.Ca = 1396.35 _ 20 = 69.8175
Mg meq = Mg mg/I = Molec.Wgt.Mg = 390.195 _ 12 = 32.5162
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.88663 = SgrRoot[0.5(69.8175+32.5162)] = 0.543349
Printed: 2/5/2016
11:01
Page 1

Page: 1 of 2
Report Number: 15-266-0200
Account Number: 46493
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
D
Waypoint(
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237 -
Main 804-743-9401 ° Fax [phone]
www.waypo inta nalytica I.com
Project: STATESVILLE 4TH CREEK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 9/21/2015 15:30:00
Lab Number: 64373 Date Received: 09/23/2015 00:00
Sample Id : STATESVILLE 4TH CREEK Date Reported: 09/28/2015
Total Solids *
13.87
138700
100.0
JM
o9/z3/zuI5 Ib:zu
5Avi-/-01+uo
Moisture *
86.13
100.0
JM
09/23/2015 15:20
SM-254OG
Total Kjeldahl Nitrogen
5.44
54400
10.0
JM
09/24/2015 09:24
SM-4500-NH3C-TKN
Total Phosphorus
2.81
28100
100
KM
09/24/2015 10:03
SW 6010C
Total Potassium
0.25
2500
100
KM
09/24/2015 10:03
SW 6010C
Total Sulfur
0.83
8300
100
KM
09/24/2015 10:03
SW 6010C
Total Calcium
0.67
6660
100
KM
09/24/2015 10:03
SW 6010C
Total Magnesium
0.19
1860
100
KM
09/24/2015 10:03
SW 6010C
Total Sodium
0.08
801
100
KM
09/24/2015 10:03
SW 6010C
Total Iron
21800
100
KM
09/24/2015 10:03
SW 6010C
Total Aluminum
24700
100
KM
09/24/2015 10:03
SW 6010C
Total Manganese
766
5
KM
09/24/2015 10:03
SW 6010C
Total Copper
333
5
KM
09/24/2015 10:03
SW 6010C
Total Zinc
596
5
KM
09/24/2015 10:03
SW 6010C
Ammonia Nitrogen
0.56
5620
10.0
JM
09/24/2015 09:24'
SM-4500-NH3C
Organic N
4.88
48780
10.0
09/24/2015 09:24
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
09/24/2015 09:25
SM-450ONO3F
Total Cadmium
3.0
2.0
KM
09/24/2015 10:03
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for th
e exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-266-0200
Account Number: 46493
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 64373
Sample Id : STATESVILLE 4TH CREEK
Waypoint-(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-§401 ° Fax [phone]
www.waypointanalytical.com
Project: STATESVILLE 4TH CREEK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 9/21/2015 15:30:00
Date Received: 09/23/2015 00:00
Date Reported:.09/28/2015
Total Chromium
48
5
KM
09/24/2015 10:03
SW 6010C
Total Nickel
26
5
KM
09/24/2015 10:03
SW 6010C
Total Lead
26
5
KM
09/24/2015 10:03
SW 6010C
Total Arsenic
4.0
3.0
KM
09/24/2015 10:03
SW 6010C
Total Mercury
1.2
0.4
KM
09/23/2015 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
09/24/2015 10:03
SW 6010C
pH (Standard Units) * 6.26
2.00
JM
09/24/2015 09:24
SW-9045D
Total Molybdenum
14
5
KM
09/24/2015 10:03
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Na".
THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL
OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

iii
L l 1r�� ��< l 4 !�i ; �1 J i\ C•% k l s+t I e .� $ 3 i �, 2
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 9/21/2015 / / - / / 0.8303
Na mg/I = (Na nI x % Solids) - 100 = (801 x 13.8700) _ 100 = 111.099
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (6660 x 13.8700) = 100 = 923.742
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1860 x 13.8700) = 100 = 257.982
Na meq = Na mg/I _ Molec.Wgt.Na = 111.099 _ 23 = 4.83038
Ca meq = Ca mg/I = Molec.Wgt.Ca = 923.742 _ 20 = 46.1871
Mg meq = Mg mg/I + Molec.Wgt.Mg = 257.982 = 12 = 21.4985
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.83038 _ SgrRoot[0.5(46.1871+21.4985)] = 0.830325
Printed: 2/5/2016
Page 1 11:03

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO020591
or WQ# (residual only)
WWTP Name: THIRD CREEK
Residuals Analysis Data
Product Type
CAK
CAK
CAK
Date Sampled (grab) or 01/29/15
03/26/15
04/23/15
Date Composited
Percent Solids
15.49
14.78
20.98
PARAMETERS (mg/kg dry weight)
Arsenic
' 4
3
4
Cadmium
17
10
22
Mercury
0.6
0.4
0.6
Chromium
109
75
248
Copper
417
344
381
Lead
107
68
80
Molybdenum
20
17
18
Nickel
52
41
104
Selenium
<5
<5
<5
Zinc
1150
1180
965
Total Phosphorus
17300
17800
13100
TKN
34100
55000
33600
Ammonia -Nitrogen
1940
3040
1950
Nitrate and Nitrite
444
473
270
Laboratory
A&L Eastern Laboratories Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significantoenalps for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date
DENR FORM RSSF (5/2003) Printed: Friday - February 5 2016 at 10:58.59 for: 2084 02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO020591
or WQ# (residual only)
WWTP Name: THIRD CREEK
Residuals Analysis Data
Product Type cAx
cAx
cAx
Date Sampled (grab) or 01/29/15
03/26/15
04/23/15
Date Composited
Percent Solids 15.49
14.78
20.98
PARAMETERS (mg/kg dry weight)
Aluminum 16800
13700
26000
Calcium 16300
11900
12000
Magnesium 2180
3220
3510
pH 5.10
6.18
6.92
Potassium 2180
3700
3430
Sodium 568
1840
1400
Laboratory
A&L Eastern Laboratories Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significan penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(SPGNATURC OF PREPARER)
NR _ Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Friday - February 5 2016 at 10.59.33 for 2084 02

Page: 1 of 2
Report Number: 15-030-0200
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
A&L Eastern Laboratories, Inc.
99, 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: 3RD CHECK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/29/2015 09:30:00
Lab Number - 59938 Date Received: 01/30/2015 00:00
Sample Id: 3RD CK Date Reported: 02/05/2015
Total Solids *
15.49
154900
100.0
Ku
u1/3u/Lu10 14:'iy
NVI-L04UU
Moisture *
84.51
100.0
RD
01/30/2015 14:19
SM-2540G
Total Kjeldahl Nitrogen
3.41
34100
10.0
JM
02/02/2015 08:24
SM-4500-NH3C-TKN
Total Phosphorus
1.73
17300
100
KM
02/02/2015 13:08
SW 6010C
Total Potassium
0.22
2180
100
KM
02/02/2015 13:08
SW 6010C
Total Sulfur
0.76
7630
100
KM
02/02/2015 13:08
SW 6010C
Total Calcium
1.63
16300
100
KM
02/02/2015 13:08
SW 6010C
Total Magnesium
0.22
2180
100
KM
02/02/2015 13:08
SW 6010C
Total Sodium
0.06
568
100
KM
02/02/2015 13:08
SW 6010C
Total Iron
22700
100
KM
02/02/2015 13:08
SW 6010C
Total Aluminum
16800
100 .
KM
02/02/2015 13:08
SW 6010C
Total Manganese
509
5
KM
02/02/2015 13:08
SW 6010C
Total Copper
417
5
KM
02/02/2015 13:08
SW 6010C
Total Zinc
1150
5
KM
02/02/2015 13:08
SW 6010C
Ammonia Nitrogen
0.19
1940
10.0
JM
02/02/2015 08:24
SM-4500-NH3C
Organic N
3.22
32160
10.0
02/02/2015 08:24
CALCULATION
Nitrate+Nitrite-N
444
2.00
JM
02/02/2015 08:25
SM-450ONO3F
Total Cadmium
17.0
2.0
KM
02/02/2016 13:08
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and
letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-030-0200
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59938
Sample Id: 3RD CK
A&L Eastern Laboratories, Inc.
IL 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleasterii.com
Project: 3RD CHECK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/29/2015 09:30:00
Date Received: 01/30/2015 00:00
Date Reported: 02/05/2015
Total Chromium
109
Total Nickel
52
Total Lead
107
Total Arsenic
4.0
Total Mercury
0.6
Total Selenium
<5.0
pH (Standard Units) *
5.10
Total Molybdenum
20
Comments:
SULFUR AND ORGANIC NITROGEN NOT
FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Se".
5
KM
02/02/2015 13:08
SW 6010C
5
KM
02/02/2015 13:08
SW 6010C
5
KM
02/02/2015 13:08
SW 6010C
3.0
KM
02/02/2015 13:08
SW 6010C
0.4
KM
02/03/2015 13:35
SW-7471 B
5.0
KM
02/02/2016`13:08
SW 6010C
2.00
JM
02/02/2015 08:24
SW-9045D
5
KM
02/02/2015 13:08
SW 6010C
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 1/29/2015 / / - / / 0.4354
Na mg/I = (Na mg/kg x % Solids) + 100 = (568 x 15.4900) + 100 = 87.9832
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (16300 x 15.4900) + 100 = 2524.87
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2180 x 15.4900) s- 100 = 337.682
Na meq = Na mg/I _ Molec.Wgt.Na = 87.9832 + 23 = 3.82536
Ca meq = Ca mg/1 + Molec.Wgt.Ca = 2524.87 _ 20 = 126.244
Mg meq = Mg mg/I + Molec.Wgt.Mg = 337.682 _ 12 = 28.1402
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.82536 = SgrRoot[0.5(126.244+28.1402)] = 0.435398
Printed: 2/5/2016
Page 1 11:17

Page: 1 of 2
Report Number: 15-086-0201
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 60952
Sample Id : STATESVILLE 3RD CK
y A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
c�
www.aleastern.com
Project: STATESVILLE 3RD CK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/26/2015 11:15:00
Date Received: 03/27/2015 00:00
Date Reported: 04/01/2015
Total Solids *
14.78
147800
100.0
JM
03/30/2015 09:24
SM-254OG
Moisture *
85.22
100.0
JM
03/30/2015 09:24
SM-2540G
Total Kjeldahl Nitrogen
5.50
55000
10.0
JM
03/30/2015 09:00
SM-4500-NH3C-TKN
Total Phosphorus
1.78
17800
100
KM
03/30/2015 15:22
SW 6010C
Total Potassium
0.37
3700
100
KM
03/30/2015 15:22
SW 6010C
Total Sulfur
0.76
7640
100
KM
03/30/2015 15:22
SW 6010C
Total Calcium
1.19
11900
100
KM
03/30/2015 15:22
SW 6010C
Total Magnesium
0.32
3220
100
KM
03/30/2015 15:22
SW 6010C
Total Sodium
0.18
1840
100
KM
03/30/2015 15:22
SW 6010C
Total Iron
17000
100
KM
03/30/2015 15:22
SW 6010C
Total Aluminum
13700
100
KM
03/30/2015 15:22
SW 6010C
Total Manganese
491
5
KM
03/30/2015 15:22
SW 6010C
Total Copper
344
5
KM
03/30/2015 15:22
SW 6010C
Total Zinc
1180
5
KM
03/30/2015 15:22
SW 6010C
Ammonia Nitrogen
0.30
3040
10.0
JM
03/30/2015 09:00
SM-4500-NI3C
Organic N
5.20
51960
10.0
03/30/2015 09:00
CALCULATION
Nitrate+Nitrite-N
473
2.00
JM
03/30/2015 09:00
SM-450ONO3F
Total Cadmium
10.0
2.0
KM
03/30/2015 15:22
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-086-0201
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 60952
Sample Id: STATESVILLE 3RD CK
o
www.aleastern.com
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: STATESVILLE 3RD CK/NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/26/2015 11:15:00
Date Received: 03/27/2015 00:00
Date Reported: 04/01/2015
Total Chromium
75
5
KM
03/30/2015 15:22
SW 6010C
Total Nickel
41
5
KM
03/30/2015 15:22
SW 6010C
Total Lead
68
5
KM
03/30/2015 15:22
SW 6010C
Total Arsenic
3.0
3.0
KM
03/30/2015 15:22
SW 6010C
Total Mercury
0.4
0.4
KM
03/30/2015 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
03/30/2015 15:22
SW 6010C
pH (Standard Units)
6.18
2.00
JM
03/30/2015 09:00
SW-9045D
Total Molybdenum
17
5
KM
03/30/2015 15:22
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

SAMPUNa,LOG: t A&:L,E
7621 �W
OUSTOMER::SGRO.
YNA804174
P
2
Phone-
4 S486-0201
E�NTRALLLC14TA
ZfYNAGF�O.0 TESVILLE P-27 2015
VrATV3VILLE 3Pb dKONG CEPMA257' 1.3;58.57
F'OUSTO)DY
&ANALY-sRs.
CON.D
Ling, Procedures
Me-ge gamples
A-&-L CIJSTQMF-R 'SAMPLING SAMPLE--#
' :OF S PILING METHOD. METHOD
LARO SAMPLELD.. LOCATION, TYpr: CONTAINERS PATE TIME PRESERVEP SHIPPEU
3fw L< b L3j-1,
<-7A-
Relinquished by Sampler - Ql�fe Time, RedievQd by: REMARX8:
o -24/1
Relinquished-4y; Date, Time: Reclewd by-
For monitoring purposes. pot ;
-SAMPLE
ANALYSIS REQUEST
SO
mqew
dd;
Cr
NI
Pb-
As
pH
, ICOAds,
Sol Volat�loj:
MO
Cl
NO,N
P007
POO
kjo
too
P041*
kow
POO'
koo
1.40
.1140
Par
1,001
50-1?nA
SLI: Total Solids '(Moisture.), Tdtal*.1qeldah1 Nitrogen,. Phosphorus, and ,Potasziurn
SL2: 13a6ic.Tb6t SLI plus Sulfur, -Calolum, Magnesium, Sodium,,, Iron, Ajumlhum, Mhnganerso, Capper and' Zno
m

Sodium Absorption Ratio Calculation (SAR)
Product.Code Product Name Sample Date ReportRange Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 3/26/2015 11112015-4130/2015 1.4803
Na mg/I = (Na mg/kg x % Solids) + 100 = (1840 x 14.7800) + 100 = 271.952
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (11900 x 14.7800) + 100 = 1758.82
Mg mg/I = (mg mg/kg x % Solids) + 100 = (3220 x 14.7800) + 100 = 475.916
Na meq = Na mg/I + Molec.Wgt.Na = 271.952 + 23 = 11.824
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1758.82 + 20 = 87.941
Mg meq = Mg mg/I + Molec.Wgt.Mg = 475.916 + 12 = 39.6597
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 11.824 + SgrRoot[0.5(87.941+39.6597)] = 1.48031
Printed: 2/5/2016
Page 1 11:05

c
Page: 1 of 2
Report Number: 15-114-0200
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 61586
Sample Id: STATESVILLE 3RD CK
y A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/23/2015 09:40:00
Date Received: 04/24/2015 00:00
Date Reported: 04/29/2015
Total Solids *
20.98
209800
100.0
BW
04/24/2015 15:00
SM-2540G
Moisture *
79.02
100.0
BW
04/24/2015 15:00
SM-2540G
Total Kjeldahl Nitrogen
3.36
33600
10.0
JM
04/27/2015 09:24
SM-4500-NH3C-TKN
Total Phosphorus
1.31
13100
100
KM
04/27/2015 13:15
SW 6010C
Total Potassium
0.34
3430
100
KM
04/27/2015 13:15
SW 6010C
Total Sulfur
0.77
7680
100
KM
04/27/2015 13:15
SW 6010C
Total Calcium
1.20
12000
100
KM
04/27/2015 13:15
SW 6010C
Total Magnesium
0.35
3510
100
KM
04/27/2015 13:15
SW 6010C
Total Sodium
0.14
1400
100
KM
04/27/2015 13:15
SW 6010C
Total Iron
19800
100
KM
04/27/2015 13:15
SW 6010C
Total Aluminum
26000
100
KM
04/27/2015 13:15
SW 6010C
Total Manganese
610
5
KM
04/27/2015 13:15
SW 6010C
Total Copper
381
5
KM
04/27/2015 13:15
SW 6010C
Total Zinc
965
5
KM
04/27/2015 13:15
SW 6010C
Ammonia Nitrogen
0.20
1950
10.0
JM
04/27/2015 09:24
SM-4500-NH3C
Organic N
3.16
31650
10.0
04/27/2015 09:24
CALCULATION
Nitrate+Nitrite-N
270
2.00
JM
04/27/2015 09:25
SM-450ONO3F
Total Cadmium
22.0
2.0
KM
04/27/2015 13:15
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made9'&ak��
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 15-114-0200
Account Number: 46493
Submitted By: ERIC THOMPSON
Send To: SYNAGRO CENTRAL LLC/STATESVILLE
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 61586
Sample Id: STATESVILLE 3RD CK
A� Y¢ A&L Eastem Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wiv%aleastern.com
Project: STATESVILLE 3RD CK
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/23/2015 09:40:00
Date Received: 04/24/2015 00:00
Date Reported: 04/29/2015
Total Chromium
248
5
KM
04/27/2015 13:15
SW 6010C
Total Nickel
104
5
KM
04/27/2015 13:15
SW 6010C
Total Lead
80
5
KM
04/27/2015 13:15
SW 6010C
Total Arsenic
4.0
3.0
KM
04/27/2015 13:15
SW 6010C
Total Mercury
0.6
0.4
KM
04/28/2015 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
04/27/2015 13:15
SW 6010C
pH (Standard Units) " 6.92
2.00
JM
04/27/2015 09:24
SW-9045D
Total Molybdenum
18
5
KM
04/27/2015 13:15
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE RPD WAS OUT OF LIMITS FOR "NO3/NO2-N".
THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al",
"Cr", AND "Ni". ALL OTHER QC DATA
IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 4/23/2016 511/2016-6130/2015 1.3198
Na mg/1= (Na mg/kg x % Solids) = 100 = (1400 x 20.9800) = 100 = 293.72
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (12000 x 20.9800) = 100 = 2517.6
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3510 x 20.9800) 100 = 736.398
Na meq = Na mg/I = Molec.Wgt.Na = 293.72 _ 23 = 12.7704
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 2517.6 _ 20 = 125.88
Mg meq = Mg mg/I + Molec.Wgt.Mg = 736.398 _ 12 = 61.3665
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 12.7704 = SgrRoot[0.5(125.88+61.3665)] = 1.31982
Printed: 2/5/2016
Page 1 11:17

ANNUAL LAND APPLICATION FIELD SUMMARY EOM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: APPLING
OWNER: DENNIS PHILLIPS PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 83.93
SITE #: NC IR 00020 FIELD# : IR 00020 0001 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON 503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.40 ACRES PERMITTED: 11.40
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
THIN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
MONTH
5/27/15
225.00 (CY)
19.737
20.98
3.488
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
33,600. p
1,950.00 p
270.00 p
10740
I FESCUE
5/28/15
250.00 (CY)
21.930
20.98
3.875
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
33,600. p
1,950.00 p
270.00 p
10740
FESCUE
May-15
1 475.00 (CY)
41.667
Total Gallons/Ac:
1 VL61 ­1 11J/AV. I41.0 /
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Za
P
PAN
TOTALS:
Annual lbs/acre
158
0.059
0.324
3.652
5.610
1.178
0.009
0.265
1.531
0.074
14.210
192.90
Cumulative lbs/acre
0.128
0.402
4.551
12.656
1.785
0.050
0.489
2.182
0.127
26.096F
�_Ii
Permit PAN Limit lbs/acre 1st Cro /2nd Crop!
9 .
''
_-
237
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
`
i
1339.0
267.9
15.0
375.0
89.0
2500.0
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X
(SIGNATURE F LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the in onnation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or ing/lcg k'" Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
'J` Application Method: SUR - Surface, INJ - hijection, SURIN - Incorporation *'k'r See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS PHILLIPS PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 58.40
SITE #: NC IR 00020 FIELD# : IR 00020 0002 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.20 ACRES PERMITTED: 13.20
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/28/15
175.00 (CY)
13.258
13.05
1.457
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
68,600. p
11,600.00 p
2.00 p
22902
I FESCUE
5/29/15
75.00 (CY)
5.682
13.05
0.625
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
68,600. p
11,600.00 p
2.00 p
22902
FESCUE
May-15
250.00 (CY)
1 18.940
5/28/15
175.00 (CY)
13.2581
20.98
2.343
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
33,600. p
1,950.00 p
270.00 p
10740
FESCUE
May-15
175.00 (CY)
1 13.258
I
1
1
1
1
1
Total Gallons/Ac:
I UU11 l.UUll: IUWt-W.
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
146
0.031
0.120
1.374
2.976
0.475
0.007
0.138
0.604
0.044
6.749
165.04
Cumulative lbs/acre
0.096
0.205
2.303
9.695
1.217
0.047
0.364
1.246
0.094
18.408
Pennit PAN Limit (ibs/acre) 1st Crop/2nd Crop'
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
R.�
2500.0 r
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
x IN/P2_ /� ,6
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of f nes and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or rng/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

FACILITY NAME: STATESVILLE, NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 79.52
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.60 ACRES PERMITTED: 11.60
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/27/15
450.00 (CY)
38.793
20.98
6.855
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
33,600. p
1,950.00 p
270.00 p
10740
FESCUE
May-15
450.00 (ClA
38.793
Total Gallons/Ac:
imaiwuic Yus/lic:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.055
0.302
3.400
5.223
1.097
0.008
0.247
1.426
0.069
13.230
179.59
147
Cumulative lbs/acre
0.169
0.483
4.927
14.971
2.873
0.063
0.589
2.308
0.180
31.840
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant LoadingRate Limit lbs/acre1
( )
36.6
E34.8]}
1339.0
267.9
15.0
375.0
89.0
2500.0
STTCC = STATESVILLE, NC THIRD CREEI{ CAKE
X/IX//// 0'/l (e
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0
k Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

FACILITY NAME: STATESVILLE, NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# :1R 00020 0008
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: APPLING
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 32.97
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.20 ACRES PERMITTED: 11.20
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (VM (specify)
"�o
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/29/15
300.00 (CY)
26.786
13.05
2.944
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
68,G00. p
11,600.00 p
2.00 pF72902
FESCUE
May-15
300.00 (Cl)
26.786
Total Gallons/Ac:
1 OUR l.uOlc rOS/EiG: LU.lJ
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.018
0.024
0.300
1.684
0.141
0.006
0.077
0.165
0.029
3.150
146.61
135
Cumulative Ibs/acre
0.130
0.184
1 1.653
1 11.522
1 1.475
0.048
0.408
1 1.036
0.188
20.937
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X
(SIGNAT OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS PHILLIPS PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 32.97
SITE #: NC IR 00020 FIELD# : IR 00020 0009 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 12.20 ACRES PERMITTED: 12.20
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
0
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/29/15
300.00 (CY)
24.590
13.05
2.703
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
68,600. p
11,600.00 p
2.00 p
12902
FESCUE
May-15
300.00 (CY)
24.590
1
Total Gallons/Ac:
i Mai
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
124
0.016
0.022
0.276
1.546
0.130
0.005
0.070
0.151
0.027
2.892 134.60
Cumulative lbs/acre
0.137
0.216
1.889
12.455
1.765
0.051
0.460
1.151
0.191
23.553
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
(
L
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEI{ CAKE
x
(SIG ATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 18.51
SITE #: NC IR 00023 FIELD# : IR 00023 0002 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 32.40 ACRES PERMITTED: 32.40
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/14/15
62,000.00 (G)
1913.580
1.15
0.092
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600. p
2,610.00 p
4,100.00 p
23402
I FESCUE
5115115
99,200.00 (G)
3061.728
1.15
0.147
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600. p
2,610.00 p
4,100.00 p
23402
I FESCUE
5/16/15
62,000.00 (G)
1913.580
1.15
0.092
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600. p
2,610.00 p
4,100.00 p
23402
I FESCUE
5/18/15
62,000.00 (G)
1913.580
1.15
0.092
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600.p
2,610.00 p
4,100.00 p
23402
I FESCUE
5/19/15
43,400.00 (G)
1339.506
1.15
0.064
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600.p
2,610.00 p
4,100.00p
23402
FESCUE
May-15
328,600.00 (G)
10,141.974
6/1/15
25.00 (CY)
0.7721
13.05
0.085
STFCC
DRY
0-<1/2"
SUR
0.5
1 0.30
1 68,600. p
1 11,600.00 p
1 2.00 p
22902
FESCUE
Jun-15
25.00 (CY)
0.772
I
1
Total Gallons/Ac: 10,141.98
Total Cubic Yds/Ac: 0.77
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
27
Annual lbs/acre
0.006
0.003
0.048
0.379
0.026
0.001
0.019
0.026
0.007
0.896
22.32
Cumulative lbs/acre
0.136
0.297
1 2.421
1 14.799
1 2.837
0.047
0.559
1.324
0.163
30.200
r •,
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
TI
(
°
162
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
; ,
1339.0
267.9
15.0
375.0
89.0
2500.0
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROBICALLY DIGESTED LIQUII
STFCC = STATESVILLE, NC FOURTH CREEI{ CAKE
X D2 /G /(
(SIGNATURf OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - hijection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

FACILITY NAME: STATESVILLE, NC
OWNER: LORANE PAGE
SITE #: NC IR 00023 FIELD# : IR 00023 0005
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL, LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 38.47
OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 16.10 ACRES PERMITTED: 16.10
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
0
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
6/1/15
350.00 (CY)
21.739
13.05
2.389
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
68,600. p
11,600.00 p
1 2.00 p
22902
FESCUE
Jun-15
350.00 (CY)
21.739
Total Gallons/Ac:
Total Cubic Yds/Ac: 21.74
As
Cd
Cr
Cu.
Pb
Fig
Mo
Ni
Se
Zn
P
PAN
TOTALS:
109
Annual lbs/acre
0.014
0.019
0.244
1.367
0.115
0.005
0.062
0.134
0.024
2.557
118.99
Cumulative lbs/acre
0.122
0.174
1.826
11.387
1.533
0.051
0.454
1.094
0.154
22.960
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
:
•`
2
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEI{ CAKE
X ©ZZ�� Z"-�
(SIGNAT OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for luiowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or rmg/lcg * * Volatilization Rate: Surface 0.5, bijection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SUR1N -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

t ttttjjVU
`tijJl
April 11, 2015
Eric Thompson
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Statesville
Dear Eric Thompson:
SununitEnvironmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: ham:1Av1vw.settek.cont
Order No.: 15032606
Summit Environmental Technologies, Inc. received 2 sample(s) on 3/27/2015 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3,
Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940,
Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8
8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia248 and
9957C and E87688, Wisconsin 399013010
Page 1 of 12

SunnnitEnvironmental Technologies, Inc.
3310Win St.
Workorder
Sample Summary
kkR
�[;',IR�hlflEtl111L�P p'rtLtu3! rl`ir_
Cuyahoga Falls, Ohio44223
i
--
A.,riat;it c. P Laboraiorie-s
TEL: [phone] FAX. [phone]
WO#: 15032606
Website: httn:/Aviviv.settek.com
12 Apr-15
CLIENT: Synagro
Project: Statesville
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
15032606-001 Statesville 3rd Ck 3/26/2015 11:15:00 AM 3/27/2015 12:00:00 PM Solid
15032606-002 Statesville 4th Ck 3/26/2015 11:25:00 AM 3/27/2015 12:00:00 PM Solid
Page 2 of 12

G SunmritEnvironnrental Technologies, Inc.
guiInv }�Cage l�TarrativeL't 1'�� l 3310 Win St.
I P.1'Ih��ilfal_t11itL nc%'Y:&IIOLLL 2l_,,, ahzr_ Cuyahoga Falls, Ohio 44223 WO#: 15032606
_ n."?yfer=l Ltitia;:gfuifes TEL: [phone] FAX: [phone]
Website: h0:1Anmv.settekcom Date: 4/11/2015
CLIENT: Synagro
Project: Statesville
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control
Summary Reports, and copies of the Chain of Custody Documents are supplied with this sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Lunt (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM, VRM, or SG were performed at Summit Labs 2704 Eatonton Highway
Haddock, GA 31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Suminit Enviroiunental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency.
Any comments or problems with the analytical events associated with this report are noted below.
Prep Comments for TCLP-Ext_S(1311), Sample 033115FL1-A: QC BLANK
Analytical Comments for TCLP-SVOC-CPEST_TCLP(8081), Sample LCS-12028, Batch ID 12028
The TCLP Pesticide LCS (Batch 12028) exhibited low recoveries for Endrin, gamma-BHC, Heptachlor, .
Original
Page 3 of 12

�s
y
rD (F rT l I
��1t���;E�r
S:m:mft Environmental Technologies, Inc.
Case Narrative
r�
ILLJ3310WinSt.
UL11
Cuyahoga Falls, Ohio44223
WO#: 15032606
AraPy,. fff --i
TEL: [phone] FAX.- [phone]
Website: hM:1Avivmseffekconr
Date: 4/11/2015
CLIENT: Synagro
Project: Statesville
and Heptachlor epoxide; The MS and MSD exhibited control.
Analytical Comments for TCLP-SVOC-Herb TCLP(8321), Sample R35035CCV3, Batch ID R35035
The TCLP Herbicide CCV(3) exhibited high recovery for all analytes; All samples were ND.
Original
Page 4 of 12

SvmmitEnvironmental Technologies, Inc.
3310 Win St. Analytical Report
3VL1iJ JL tk I breport)
{ �h,1rlRtsAlfdBhJlltLl ,fly_ CayahogaFalls,Ohio44223 (base
An TEL: [phone] FAX.- [phone] WO#: 15032606
Website: hW:/Atntnv.settekcom Date Reported: 4/11/2015
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 3/26/2015 11:15:00 AM
Lab ID: 15032606-OOIA
Project: Statesville
Client Sample ID Statesville 3rd Ck
Analyses Result RI., Qual Units DF Date Analyzed
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 5.54 s.u.@21.4C 1 4/7/2015 1:30:00 PM
Qualifiers•• `
Value exceeds Maximum Contaminant Level.
C
Value is below Minimum Compound Limit
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
U
Samples with CalcVal <MDL
J
Analyte detected below quantitation limits Page 5 of 12

i%I
(seSi
L—� {
SwinnitEnvironmental Technologies, Inc.
3310WinSt.
1! Report
Analytical
i
5 tll(�¢tJ k
h,1rIF t1IIPICi�IF1LJ€Y`va LC��-�,a
L�
t;_
Cuyahoga Falls, Ohio44223
(base report)
uv
I ��
Ikr "j ftt sl i §t at �:lL ^i
TEL: [phone] FAX: [phone]
WO#: 15032606
Website: hQ. :1Ai-,ivro.settek.com
Date Reported: 4/11/2015
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 3/26/2015 11:25:00 AM
Lab ID: 15032606-002A
Project: Statesville
Client Sample ID Statesville 4th Ck
Analyses Result RL Qual Units D)F Date Analyzed
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 7.12 s.u.@21.3C 1 4/7/2015 1:30:00 PM
Qualifiers• °
•
Value exceeds Maximum Contaminant Level.
C -
Value is below Minimum Compound Limit.
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
U
Samples with CalcVal a MDL
J
Analyte detected below quantitation limits Page 6 of 12

—
Summit Etl Technologies, Inc.
nvironmenaecnoo es, g
3310 Win St..
WO#:
15032606
( '?
,',rint��.11e9Eh�'1,1L �tC :+7t3L mil_ INC,
Cuyahoga Falls, Ohio 44223
Date Reported
4/11/2015
TEL: [phone] FAY [phone]
Company:
Synagro
Website: hQ. :/hmvw.settekcom
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
3/27/2015
Project#:
Statesville
TCLP Metals Analysis (6010)
Client IN
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd Ck
001
3/26/2015 TCLP Arsenic(As)
0.500
ND mg/L
Solid
EPA 6010 C
1
5.00
4/1/2015
WK
Statesville 3rd Ck
001
3/26/2015 TCLP Barium(Ba)
5.00
ND mg/L
Solid
EPA 6010 C
1
100
4/1/2015
WK
Statesville 3rd Ck
001
3/26/2015 TCLP Cadmium(Cd)
0.100
ND mg/L
Solid
EPA 6010 C
1
1.00
4/1/2015
WK
Statesville 3rd Ck
001
3/26/2015 TCLP Chromium(Cr)
0.200
ND mg/L
Solid
EPA 6010 C
1
5.00
4/1/2015
WK
Statesville 3rd Ck
001
3/26/2015 TCLP Lead(Pb)
0.500
3.16 mg/L
Solid
EPA 6010 C
1
5.00
4/1/2015
WK
Statesville 3rd Ck
001
3/26/2015 TCLP Selenium(Se)
0.500
ND mg/L
Solid
EPA 6010 C
1
1.00
4/1/2015
WK
Statesville 3rd Ck
001
3/26/2015 TCLP Silver(Ag)
0.500
ND mg/L
Solid
EPA 6010 C
1
5.00
4/1/2015
WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Statesville 3rd Ck 001 3/26/2015 TCLP Mercury 0.00200 ND mg/L Solid EPA 7470 A 1 0.200 4/1/2015 ALJ
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd Ck
001
3/26/2015 Chlordane, total
0.0250
ND mg/L
Solid
EPA 8081 B
1
0.0300
4/5/2015
AMZ
Statesville 3rd Ck
001
3/26/2015 Toxaphene
0.0500
ND mg/L
Solid
EPA 8081 B
1
0.500
4/5/2015
AMZ
Statesville 3rd Ck
001
3/26/2015 Endrin
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.0200
4/5/2015
AMZ
Statesville 3rd Ck
001
3/26/2015 gamma-BHC
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.400
4/5/2015
AMZ
Statesville 3rd Ck
001
3/26/2015 Heptachlor
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.00800
4/5/2015
AMZ
Statesville 3rd Ck
001
3/26/2015 Heptachlor epoxide
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.00800
4/5/2015
AMZ
Statesville 3rd Ck
001
3/26/2015 Methoxychlor
0.00250
ND mg/L
Solid
EPA 8081 B
1
10.0
4/5/2015
AMZ
Statesville 3rd Ck
001
3/26/2015 Surr: Tetrachloro-m-
5-119
88.4 %REC
Solid
EPA 8081 B
1
4/5/2015
AMZ
xylene
Page 7 of 12

�-
S:nnmitEnvironraental Technologies, Inc.
3310 Win St.
WO#:
15032606
i+iVlnOhlfatEh:'I'}1L IEC�tt'd0WGIeS; W
CVahogaFalls, Ohio 44223
Date Reported
4/11/2015
i
!
Amin. tiro'] Lo'bor.3lor.ie",
TEL: [phone] FAX. [phone]
( ) ( )
Company:
Synagro
Website: hM:1Av w.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
3/27/2015
Project#:
Statesville
VOC by GC/MS (8260)-TCLP
Client II3#
Lab 1D# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd Ck
001
3/26/2015 1,1-Dichloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.700
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 1,2-Dichloroethane
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 MEK
2.00
ND mg/L
Solid
EPA 8260 B
1
200
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 Benzene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 Carbon tetrachloride
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 Chlorobenzene
0.100
ND mg/L
Solid
EPA 8260 B
1
100
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 Chloroform
0.100
ND mg/L
Solid
EPA 8260 B
1
6.00
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 Tetrachloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.700
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 Trichloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 Vinyl chloride
0.200
ND mg/L
Solid
EPA 8260 B
1
0.200
4/1/2015
JCR
Statesville 3rd Ck
001
3/26/2015 Surr: 4-
70-130
82.9 %REC
Solid
EPA 8260 B
1
4/1/2015
JCR
Bromofluorobenzene
Statesville 3rd Ck
001
3/26/2015 Surr:
70-130
105 %REC
Solid
EPA 8260 B
1
4/1/2015
JCR
Dibrom ofluoromethane
esville 3rd Ck
001
3/26/2015 Surr: Toluene-d8
70-130
102 %REC
Solid
EPA 8260 B
1
4/1/2015
JCR
SVOC 8270 TCLP BNA List
Client ID#
Lab )D# Collected Analyte Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd Ck
001
3/26/2015 1,4-Dichlorobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
7.50
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 2,4,5-Trichlorophenol
0.250
ND mg/L
Solid
EPA 8270 C
1
400
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 2,4,6-Trichlorophenol
0.250
ND mg/L
Solid
EPA 8270 C
1
2.00
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 2,4-Dinitrotoluene
0.100
ND mg/L
Solid
EPA 8270 C
1
0.130
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Cresols, Total
5.00
ND mg/L
Solid
EPA 8270 C
1
200
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Hexachloro-1,3-
0.100
ND mg/L
Solid
EPA 8270 C
1
0.500
4/6/2015
JBN
butadiene
Statesville 3rd Ck
001
3/26/2015 Hexachlorobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
0.130
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Hexachloroethane
0.100
ND mg/L
Solid
EPA 8270 C
1
3.00
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Nitrobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
2.00
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Pentachlorophenol
0.250
ND mg/L
Solid
EPA 8270 C
1
100
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Pyridine
0.250
ND mg/L
Solid
EPA 8270 C
1
5.00
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Surr: 2-Fluorophenol
5-109
33.9 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Surr: Phenol-d6
5-109
30.9 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Surr: Nitrobenzene-d5
19-120
39.9 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Surr: 2,4,6-
10-120
89.9 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Tribromophenol
Statesville 3rd Ck
001
3/26/2015 Surr: 2-Fluorobiphenyl
22-117
43.0 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Statesville 3rd Ck
001
3/26/2015 Surr: p-Terphenyl-d14
34-116
59.8 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Page 8 of 12

IRE
v F'$VIROHI9EWfAL2'EL"§-NOLOGIE iTIC
Arra, rJ mll l r seat i s
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Tfrebsite: hh:/Avww.settek.con:.1Avivw.settek.con:
i
WO#:
15032606 '
Date Reported
4/11/2015 \\
Company:
Synagro \
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 3/27/2015
Project#: Statesville
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab II)# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 3rd Ck
001
3/26/2015 2,4-D
5.00 ND mg/L
Solid
EPA 8321 A
1
10.0
4/1/2015
AMZ
Statesville 3rd Ck
001
3/26/2015 2,4,5-TP
0.500 ND mg/L
Solid
EPA 8321 A
1
1.00
4/1/2015
AMZ
TCLP Metals Analysis (6010)
Client ID#
Lab EW Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Ck
002
3/26/2015 TCLP Arsenic(As)
0.500 ND mg/L
Solid
EPA 6010 C
1
5.00
4/1/2015
WK
Statesville 4th Ck
002
3/26/2015 TCLP Barium(Ba)
5.00 ND mg/L
Solid
EPA 6010 C
1
100
4/1/2015
WK
Statesville 4th Ck
002
3/26/2015 TCLP Cadmium(Cd)
0.100 ND mg/L
Solid
EPA 6010 C
1
1.00
4/1/2015
WK
Statesville 4th Ck
002
3/26/2015 TCLP Chromium(Cr)
0.200 ND mg/L
Solid
EPA 6010 C
1
5.00
4/1/2015
WK
Statesville 4th Ck
002
3/26/2015 TCLP Lead(Pb)
0.600 15.4 mg/L
Solid
EPA 6010 C
1
5.00
4/1/2015
WK
Statesville 4th Ck
002
3/26/2015 TCLP Selenium(Se)
0.500 ND mg/L
Solid
EPA 6010 C
1
1.00
4/1/2015
WK
esville 4th Ck
002
3/26/2015 TCLP Silver(Ag)
0.500 ND mg/L
Solid
EPA 6010 C
1
5.00
4/1/2015
WK
TCLP Mercury Analysis (1311/7470)
Client EN Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run. Analyst
Statesville 4th Ck 002 3/26/2015 TCLP Mercury 0.00200 ND mg/L Solid EPA 7470 A 1 0.200 4/1/2015 ALJ
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Ck
002
3/26/2015 Chlordane, total
0.0250
ND mg/L
Solid
EPA 8081 B
1
0.0300
4/5/2015
AMZ
Statesville 4th Ck
002
3/26/2015 Toxaphene
0.0500
ND mg/L
Solid
EPA 8081 B
1
0.500
4/5/2015
AMZ
Statesville 4th Ck
002
3/26/2015 Endrin
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.0200
4/5/2015
AMZ
Statesville 4th Ck
002
3/26/2015 gamma-BHC
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.400
4/5/2015
AMZ
Statesville 4th Ck
002
3/26/2015 Heptachlor
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.00800
4/5/2015
AMZ
Statesville 4th Ck
002
3/26/2015 Heptachlor epoxide
0.00250
ND mg/L
Solid
EPA 8081 B
1
0.00800
4/5/2015
AMZ
Statesville 4th Ck
002
3/26/2015 Methoxychlor
0.00250
ND mg/L
Solid
EPA 8081 B
1
10.0
4/5/2015
AMZ
Statesville 4th Ck
002
3/26/2015 Surr: Tetrachloro-m-
5-119
56.8 %REC
Solid
EPA 8081 B
1
4/5/2015
AMZ
xylene
Page 9 of 12

UJII�.�i$Z,l��rrC1�i-, - L�-
� (( �f;'JIR[�hlPelEhl'Ii1L'0'cCi�tl�L7:�1��, iit�
S:mrmitEnvironmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX. [phone]
Website: ha.-M�vivw.settekconr
W09: 15032606
Date Reported 4/11/2015
Company: Synagro
Address: 284 Boger Rd.
Mocksville NC 27028
VOC by GC/MS (8260)-TCLP
Received: 3/27/2015
Project#: Statesville
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method DF
RegLvl
Run
Analyst
Statesville 4th Ck
002
3/26/2015 1,1-Dichloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.700
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 1,2-Dichloroethane
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 MEK
2.00
ND mg/L
Solid
EPA 8260 B
1
200
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 Benzene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 Carbon tetrachloride
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 Chlorobenzene
0.100
ND mg/L
Solid
EPA 8260 B
1
100
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 Chloroform
0.100
ND mg/L
Solid
EPA 8260 B
1
6.00
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 Tetrachloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.700
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 Trichloroethene
0.100
ND mg/L
Solid
EPA 8260 B
1
0.500
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 Vinyl chloride
0.200
ND mg/L
Solid
EPA 8260 B
1
0.200
4/1/2015
JCR
Statesville 4th Ck
002
3/26/2015 Surr: 4-
70-130
82.2 %REC
Solid
EPA 8260 B
1
4/1/2015
JCR
Bromofluorobenzene
Statesville 4th Ck
002
3/26/2015 Surr:
70-130
107 %REC
Solid
EPA 8260 B
1
4/1/2015
JCR
Dibromofluoromethane
lesville 4th Ck
002
3/26/2015 Suer: Toluene-d8
70-130
102 %REC
Solid
EPA 8260 B
1
4/1/2015
JCR
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Ck
002
3/26/2015 1,4-Dichlorobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
7.50
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 2,4,5-Trichlorophen ol
0.250
ND mg/L
Solid
EPA 8270 C
1
400
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 2,4,6-Trichlorophen ol
0.250
ND mg/L
Solid
EPA 8270 C
1
2.00
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 2,4-Dinitrotoluene
0.100
ND mg/L
Solid
EPA 8270 C
1
0.130
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Cresols, Total
5.00
ND mg/L
Solid
EPA 8270 C
1
200
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Hexachloro-1,3-
0.100
ND mg/L
Solid
EPA 8270 C
1
0.500
4/6/2015
JBN
butadiene
Statesville 4th Ck
002
3/26/2015 Hexachlorobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
0.130
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Hexachloroethane
0.100
ND mg/L
Solid
EPA 8270 C
1
3.00
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Nitrobenzene
0.100
ND mg/L
Solid
EPA 8270 C
1
2.00
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Pentachlorophenol
0.250
ND mg/L
Solid
EPA 8270 C
1
100
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Pyridine
0.250
ND mg/L
Solid
EPA 8270 C
1
5.00
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Surr: 2-Fluorophenol
5-109
39.9 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Surr: Phenol-d6
5-109
36.3 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Surr: Nitrobenzene-d5
19-120
45.5 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Surr: 2,4,6-
10-120
92.2 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Tribromophenol
Statesville 4th Ck
002
3/26/2015 Surr: 2-Fluorobiphenyl
22-117
51.1 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Statesville 4th Ck
002
3/26/2015 Surr: p-Terphenyl-04
34-116
71.8 %REC
Solid
EPA 8270 C
1
4/6/2015
JBN
Page 10 of 12

-3 -1
#��
Summit Environmental Technologies, Inc.
3310Win St.
�(j��P•f'dIflDPIPa1EM1',1L
5c�:r+Lr1GI'ca; irtC
CtryahogaFalls, Ohio 44223
Date Reported
4/11/2015
LL�_���
Jr7 iir.':=i f 7i�pra7t7r`,a .
TEL: [phone] FAX.- [phone]
Company:
Synagro
Website: htto.11www.settek.cou+
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 3/27/2015
Project#: Statesville
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Statesville 4th Ck
002 3/26/2015 2,4-D
5.00 ND mg/L
Solid
EPA 8321 A
1
10.0
4/1/2015
AMZ
Statesville 4th Ck
002 3/26/2015 2,4,5-TP
0.500 ND mg/L
Solid
EPA 8321 A
1
1.00
4/1/2015
AMZ
Page 11 of 12

Summ Environmental Technologies, Inc.
iv1_
3310Win St.
WO#: 15032606
��
6 i.JIRtlhllalEh!'I,.tL��Ct?tdnL�Gl=_•, 1PiG
Cuyahoga Falls, Ohio44223
Date Reported 4/11/2015
J nyi, frr.::P [_=avrai4ih:.5 TEL: (330)
253-8211 FAX [phone]
Company: Synagro
Website: hawlAnviv.settek.con:
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 3/27/2015
Project#: Statesville
Client ID# Lab EN Collected Analyte
Result Units
Matrix Method DF RL
Run Analyst
Statesville 3rd Ck 001 3/26/2015 Flashpoint (140T)
>140 °F
Solid EPA 1010 1
4/5/2015 TAH
Statesville 3rd Ck 001 3/26/2015 Cyanide, Reactive
ND ppm
Solid EPA 9014 1 0.500
3/30/2015 SG
Statesville 3rd Ck 001 3/26/2015 Sulfide, Reactive
ND ppm
Solid EPA 9034 1 25.0
3/30/2015 TIR
Client ID# Lab E D# Collected Analyte Result Units Matrix Method DF RL Run Analyst
Statesville 4th Ck
Statesville 4th Ck
Statesville 4th Ck
002
3/26/2015
Flashpoint (140°F)
>140 °F
002
3/26/2015
Cyanide, Reactive
ND ppm
002
3/26/2015
Sulfide, Reactive
ND ppm
Solid
EPA 1010
1 4/5/2015
TAH
Solid
EPA 9014
1 0.500 3/30/2015
SG
Solid
EPA 9034
1 25.0 3/30/2015
TIR
Page 12 of 12

s-
Sulmmlit Euvironmentalleehnologies,_Inc. , Iialysis Request/Chain -of Custody
3310•Win-Street For Summit Environmental Technolggies, Inc. use only
Cuyahoga Falls, Ohio 44223 Tel: [phone] Fax: 330.253,4489 Page f of SET No,
Company Name (Please Print)
Project Name
Analytical Parameters and Methods
Company Address
Project Address
DLY4 V t it s J.1
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.° 7:
Y
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Client Phone No. 7 7 t Q
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Report to G�st
Client Fax No. WAS Fax Resuits-✓
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Sample Idenffleaition
Da-'
Time
Colic
eoileetea
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Rev. 12
Date: 07/27/13
Summit Environmental Technologies, Inc,
Cooler Receipt Form
Initials of person inspecting cooler and samples:
Client: ��ll order Number: /5-O .S G �<"
Date Received:) Time Received: V Date cooler(s) opened and samples inspected:
Number of oole ox NIA
Shipper. ED EX UPS DHL Airborne US Postal Walk-in Pickup other
Packaging: Peanuts ubbte Wr Paper Foam None Other. -
Tape on do
Y N NIA
Custody Seals intact N NIA
C-o-C in plastic Y N N/A
ice Slue ice _ resen ! bsent / melted NIA
Sample Temperature IR Gun 416020459 CF o0 oC N/A
Radiological Testing Instrument serial 9 5127 Y N
(see page 2 for scan results)
Use 7 sheet per sample for Radiological Testing, If sample is HUT, the Radiological safe
cer must be notified
C-U-C filled out properly N NIA
Samples in separate bags N NIA
Sample containers intact' N N/A
*If no, list broken sample(s):
Sample label(s) complete (ID, date, etc.) Y N N/A
Label(s) agree with C-0-C N NIA
Correct containers used i Y N NIA
Sufficient sample received /v' 1 N N/A
Bubbles absent from 40 mL vials* y N !A
** Samples with bubbles <6mm are acceptable. Indicate bubble size if >6mm.
Was client contacted about samples Y N
Will client send new samples Y N
Client contact
Datemme:
Logged in by:
GMC SHAREDIDocument Control Templates - TraekinglCooler receipt form Rey, 12 W-27-13,doe Page 1 of 2

ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Fourth Creek WWTP NPDES Number: NCO031836
Monitoring Period: From 01/01/2015 To 12/31/2015 .
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class B complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo. Mean Maximum Units dences Analysis
Fecal 2x10 to the 6` MPN
Coliform power per gram 576 1960 6351 MPN/g 0 quarterly grab SM92210E
of total solids
CFU CFU/g
1000 MPN per gram of MPN/g
total solids (dry weight)
Salmonella 3 MPN per 4 grams total
bacteria (in solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) XX
Option/Mt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable)
Option/Alt. 9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
Andy Smith Residuals Superintendent
"ofreparer*
type or print) Land Applier Name and Title (if applicable) (type or print)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 01/2112015
Reported: 01/23/2015
For: 4th Creek- COS
Comments:
Sample Number Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
150121-09-01
Fecal Coliforms
1
2,246
MPN/g
SM92210E-2006
01/22/2015
WL
150121-09-01
Percent Solids
1
13.36
%
SM254OB-1997
01/22/2015
WL
150121-09-02
Fecal Coliforms
2
1,714
MPN/g
SM92210E-2006
01/22/2015
WL
150121-09-02
Percent Solids'
2
14.00
%
SM254OB-1997
01/22/2016
WL
150121-09-03
Fecal Coliforms
3
676
MPN/g
SM92210E-2006
01/22/2015
WL
150121-09-03
Percent Solids
3
13.89
%
SM254OB-1997
01/22/2015
WL
150121-09-04
Fecal Coliforms
4
1,533
MPN/g
SM92210E-2006
01/22/2015
WL
150121-09-04
Percent Solids
4
14.35
%
SM264OB-1997
01/22/2015
WL
150121-09-05
Fecal Coliforms
5
6,351
MPN/g
SM92210E-2008
01/22/2015
WL
150121-09-05
Percent Solids
5
14.17
%
SM254OB-1997
01/22/2015
WL
150121-09-06
Fecal Coliforms
6
831
MPN/g
SM92210E-2006
01/22/2015
WL
150121-09-06
Percent Solids
6
15.64
%
SM254OB-1997
01/22/2015
WL
150121-09-07
Fecal Coliforms
7
6,186
MPN/g
SM92210E-2006
01/22/2015
WL
150121-09-07
Percent Solids
7
14.55
%
SM254OB-1997
01/22/2016
WL
Respectfully
submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 o Statesville, NC 28687 •704/872/4697
Page 1 of 3

Client:
'3 n C\C );
STATESVILLE ANALYTICAL
122 Court Street • P.O. Box 228
Address: / )
Statesville, NC 28687
[phone]
of
Custody Record
J
Contact Person: Phone #�^ c,i ` v I=AX# _L�t _ �; Sc7Chain
I
PO # 70 _ 0�6) Requisitioned by e^�1 r t � ( �� ;11 �YD Fa}e)
Customer
Sample !D#
Lab -ID #
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
Matrix
Parameters requested for analysis
siutleo
w
ww
C'
L� ��Li,i .0
i
.✓
f
w
k.
1 U 121. ON
t
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Relinquished by: � f . L
Time r� a �� !wpm Date ! IL / 1E
Sampled by: GC11_f
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Cl
. by:
Received l; ; \
Time � 1,.r �.1
rl
gg 4" y 3 �'
a� pm Date t l=l �
A t �
Transported by:
,
Relinquished by:
Time
am, pm Date / !
Holding times met:
Received by:
Time
am, pm Date
Compliance work: "✓
Composite Sampling 99:
Time begin am, pm Date /
Non-compliance work:
Time end am, pm Date _/ /
Lab Comments:
-Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date �_ 1

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mgll)
0
8.55
1
8.44
2
8.32
3
8.28
4
8.23
5
8.19
6
8.1
7
8.06
8
8
9
7.93
10
7.88
11
7.8
12
7.71
13
7.64
14
7.57
15
7.51
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Fourth Creek WWTP
1/5/2015
13.1
1/5/15 12:55 PM
LC
1/5115 1:04 PM
BJ
300
1.57
13.3
14.8
0.1
8.5
1.0
milliliters
Yo Dry Solids
legrees Celsius
legrees Celsius
3.94 mg Oxygen/hr
0.84 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1.26 Jmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
1 /6/2015
12.6
1/6/15 12:55 PM
LC
1/6/15 1:03 PM
BJ
300
1.48
11.7
13.3
0.1
10.8
1.0
milliliters
1/6 Dry Solids
legrees Celsius
legrees Celsius
4.10 mg Oxygen/hr
0.92 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate:, 1. 8 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 1/7�
Sampled By:
Analysis Date/Time: 1/T
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
10.25
10.1
9.95
9.86
9.77
9.69
9.61
9.57
9.51
9.42
9.37
9.32
9.22
9.17
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
7/2015
12.6
5 1:05 PM
5 1:15 PM
BJ
300
milliliters
1.52
% Dry Solids
12.8
degrees Celsius
14.1
degrees Celsius
0.1
10.1
1.0
3.94 mg Oxygen/hr
0.86 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 1.39 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
Dissolved Oxygen Level
(mg/1)
10.65
10.56
10.47
10.39
10.3
10.25
10.22
10.12
10.09
9.95
9.9
9.82
9.77
9.75
II 1 /8/2015 li
1 1/8/15 12:51 PM I
1 1/8/15 1:02 PM p
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
300
1.54
12
12.8
0.1
10.6
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.74 mg Oxygen/hr
0.81 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 1.39 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
NFourth Creek WWTPB
1 /9/2015
13.5
1/9/15 9:55 AM
RG
1/9/15 10:10 AM
300
1.59
13.2
14.8
0.1
8.7
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
3.46 mg Oxygen/hr
0.72 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1.09 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR

Specific Oxygen Uptake Rate
SOUR
Facility Name;
Biosolids Permit Number;
Date;
Digester Temperature
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By.
Sample Volume
Total Solids:
Beginning Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
10.5
1
10.43
2
10.35
3
10.26
4
10.19
5
10.11
6
10.05
7
9.96
8
9.98
9
9.83
10
9.74
11
9.67
12
9.56
13
9.51
14
9.46
15
9.41
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
13.5
1/12/15 12:54 PM
RW
1/12/15 1:05 AM
BJ
300
1.47
14.3
15.3
0.1
10.5
.1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
4.47 mg Oxygen/hr
1.01 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 1.42 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fou
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1 1/13/2015 A
1 1/13/15 1:00 PM n
1 1/13/15 1:09 PM I
300
1.52
15.8
16.5
0.1
8.2
1.0
milliliters
% Dry Solids
degrees Celsius
decrees Celsius
3.85 mg Oxygen/hr
0.84 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 1.11 - mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
Fourth Creek WW
2/2/2015
12.3
2/2/15 1:10 PM
LC
2/2/15 1:23 PM
BJ
300
1.49
12.3
13.6
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
0.1
9.1
1.0
3.64 mg Oxygen/hr
0.81 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
w
Temperature Corrected Specific Oxygen Uptake Rate: 1.31 11mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
Dissolved Oxygen Level
10.96
10.96
10.87
10.82
10.74
10.66
OFourth Creek WWTPA
10.49
10.36
10.26
10.33
10.36
10.37
10.29
10.22
10.14
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
2/4/2015
11.7
2/4/15 12:58 PM
LC
2/4/15 1:10 PM
BJ
300 milliliters
1.47 % Dry Solids
11 degrees Celsius
12.2 degrees Celsius
0.1
10.9
1.0
3.33 mg Oxygen/hr
0.75 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:lr— 1.36 �mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
Fourth Creek V
2/5/2015
11.7
2/5/15 12:58
RG
2/5/15 1:09
BJ
300
1.3
14.2
14.9
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
0.1
9.7
1.0
3.42 mg Oxygen/hr
0.88 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rater 1.23 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWTP
Biosolids Permit Number:
Date:
2/6/2015
Digester Temperature:
14.4
Sampling Date/Time:
2/6/15 12:58 PM
Sampled By:
RW
Analysis Date/Time:
2/6/15 1:13 PM
Analyzed By:
BJ
Sample Volume:
300
milliliters
Total Solids:
1.4
% Dry Solids
Beginning Temperature:
14.9
Idearees
degrees Celsius
15.4
Celsius
Dissolved Oxygen Level
8.74
e
8.68
8.6
8.66
8.64
8.56
8.46
8.32
8.12
8.07
8.01
7.94
7.88
7.83
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
8.8
1.0
3.89 mg Oxygen/hr
0.93 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: f A1., !mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
2/9/2015
15.9
2/9/15 1:00 PM .
9 2/9/15 1:12 PM H
300 milliliters
1.49 % Dry Solids
15.4 degrees Celsius
17 degrees Celsius
0.1
8.1
1.0
4.27 mg Oxygen/hr
0.95 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:1.25 1 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWTP
Biosolids Permit Number:
Date:
2/10/2015 -
Digester Temperature:
17.9
Sampling Date/Time:
2/10/15 1:00 PM
Sampled By:
TR
Analysis Date/Time:
2/10/14 1:07 PM
Analyzed By:
BJ
Sample Volume:
300
milliliters
Total Solids:
1.47
% Dry Solids
Beginning Temperature:
18.4
degrees Celsius
End Temperature:
18.9
degrees Celsius
Dissolved Oxygen Level
(mg/1)
6.31
6.27
6.16
6.04
5.95
5.85
5.76
5.69
5.51
5.46
0
5.39
5.32
5.27
5.19
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.3
1.0
4.85 mg Oxygen/hr
1.10 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: �1.18 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time - Dissolved Oxygen Level
1 2/11/2015 1
1 2/11/15 10:02 AM 1
(minutes)
(mg/1)
0
6.93
1
6.86
2
6.78
3
6.7
4
6.61
5
6.52
6
6.42
7
6.38
8
6.29
9
6.21
10
6.12
11
6.06
12
5.95
13
5.88
14
5.81
15
5.76
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
2/11/15 10:13 AM
BJ
300
1.52
15
0.1
6.9
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
4.80 mg Oxygen/hr
1.05 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 1.48 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
3/2/2015
13.4
3/2/15 1:02 PM
LC
3/2/15 1:10. PM
BJ
300
1.77
12.8
14
0.1
7.0
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.05 mg Oxygen/hr
0.57 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate:11 0.92 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Digester Temperature
Sampling Date/Time
Sampled %
Analysis Date/Time
Analyzed %
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
ree
3/3/2015
9.8
3/3/15 1:07 PM
3/3/15 1:14 PM
BJ
300
1.93
10
0.1
8.9
1.0
milliliters
% Dry Solids
degrees Celsius
degrees. Celsius
3.49 mg Oxygen/hr
0.60 mg Oxygen/g/hr
11 degrees Celsius
1.838459212
Temperature Corrected Specific Oxygen Uptake Rate: 1.11mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WW
Biosolids Permit Number:
Date:
3/4/2015
Digester Temperature:
16.2
Sampling Date/Time:
3/4/15 1:12 PM
Sampled By:
JJ
Analysis Date/Time:
3/4/15 1:21 PM
Analyzed By:
BJ
Sample Volume:
300
Total SolidsA
1.59
Beginning Temperature:
15.9
End Temperature:
15.2
Dissolved Oxygen Level
6.83
6.78
m
6.71
6.62
s
6.54
6.49
6.4
6.36
6.22
6.17
6.1
6.04
5.97
5.89
5.84
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.8
1.0
milliliters
% Dry Solids
degrees Celsius
decrees Celsius
3.98 mg Oxygen/hr
0.83 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: � 1.09 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
16.5
3/5/15 1:30 PM
milliliters
% Dry Solids
degrees Celsius
Celsius
RG
3/5/15 1:37 PM
BJ
300
1.66
16.4
17.1 jdegrees
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
5.5
1.0
5.47 mg Oxygen/hr
1.10 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 1.35 �� mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Nam
Biosolids Permit NumbE
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek
17.1
3/6/15 1:09 PM
5 3/6/15 1:12 PM R
300 milliliters
1.5 % Dry Solids
17.2 degrees Celsius
17.1 dearees Celsius
0.1
7.3
1.0
4.67 mg Oxygen/hr
1.04 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 1V27 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.16
1
8.09
2
7.98
3
7.91
4
7.86
5
7.74
6
7.64
7
7.59
8
7.53
9
7.44
10
7.32
11
7.29
12
7.25
13
7.28
14
7.19
15
7.12
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
3/10/2015
19
3/10/15 1:05 PM
1 3/10/15 1:10 PM H
300 milliliters
1.62 % Dry Solids
19 degrees Celsius
19.8 degrees Celsius
0.1
8.1
1.0
4.21 mg Oxygen/hr
0.87 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:. 0.9mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
mgn
7.37
7.32
7.21
7.16
7.05
6.69
Q
6.61
6.56
6.48
6.38
6.27
6.22
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
3/11/2015
19.5
3/11/15 1:07 PM
RG
3/11/15 1:12 PM
BJ
300
1.56
19.7
20
0.1
7.4
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4.70 mg Oxygen/hr
1.00 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:,, 1.00 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Analytical Results
tynagr®
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
04/08/2015
1
Reported:
04/09/2015
� i
3
For:
47H Creek
Comments:
Geometric Mean 5,906 MPN/g
Sample Number Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
150408-13-01
Fecal Coliforms
1
11,644
MPN/g
SM92210E-2006
04/08/2015
CL
150408-13-01
Percent Solids
1
14.6
%
SM2540B-1997
04/08/2015
CL
150408-13-02
Fecal Coliforms
2
6,670
MPN/g
SM92210E-2006
04/08/2016
CL
150408-13-02
Percent Solids
2
13.7
%
SM254OB-1997
04/08/2015•
CL
160408-13-03
Fecal Coliforms
3
7,639
MPN/g
SM92210E-2006
04/08/2015
CL
150408-13.03
Percent Solids
3
14A
%
SM254OB-1997
04/08/2015
CL
150408-13-04
Fecal Coliforms
4
2,128
MPN/g
SM92210E-2006
04/08/2015
CL
150408-13-04
Percent Solids
4
14.1
%
SM2540B-1997
04/08/2015
CL
150408-13-05
Fecal Coliforms
5
9,032
MPN/g
SM92210E-2006
04/08/2015
CL
150408-13-05
Percent Solids
5
15.5
%
SM25408-1997
04/08/2015
CL
150408-13-06
Fecal Coliforms
6
3,621
MPN/g
SM92210E-2006
04/08/2016
CL
150408-13-06
Percent Solids
6
14.2
%
SM254OB-1997
04/08/2015
CL
150408-13-07
Fecal Coliforms
7
6,338
MPN/g
SM92210E-2006
04/08/2015
CL
150408-13-07
Percent Solids
7
14.2
%
SM254OB-1997
04/08/2015
CL
Respectfully
submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 e Statesville, NC 28687 e 704/872/4697
Page 1 of 3

Client:
J a tGS�C 0 V
STA.TESVMLF ANALYTICAL
122 Court Street • P.O. Box 228 Statesville, NC 28687
3,
(704) 8724697
Address: n 0
Contact Person: 1--T Phone # G
FAX,,fi-
3� � ^c �� v
Chain of
Custody Record
PO # Requisitioned by: A c (Time
tj
D tee
Customer
Sample 1D#
Lab -ID #
Time Sampled
(Grab Only)
Date Sampled +
(Grab Only)
Matrix
parameters requested for analysis
studao
wI
ww
7
Inn
.4
0
8'
S
elinquished by: '/-1ifr,(g r
Time �9G�{�
arr', pm pate
Sampled by:�L tiVG
Received by: i '{ i ,�,_----71
Time
m„i pm Date -�5'IJ r�.
Transported by:r
Relinquished by:
Time
am, pm Date , j/
1
Holding times met:
Received by:
Time
am, pm Date �J_/
CompEiance work:
Composite Sampling #1:
Time begin am, pm Date / /
Non-compliance work:
Time end am, pm Date
Lab comments:
Composite Sampling 92:
Time begin am, pm Date
Time -end - am, pm Date_(

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.46
6.65
6.63
6.8
6.87
6.77
56 8
a
6.49
m
6.36
6.29
6.18
6.12
6.01
5.94
5.85
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
18.6
M
LC
BJ
300 milliliters
1.54 % Dry Solids
18.2 degrees Celsius
18 Idearees Celsius
0.1
6.9
0.9
3.99 mg Oxygen/hr
0.86 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate:j0.99 11mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek W'
4/2/2015
17.4
4/2/15 1:03 P
RG
4/2/15 1:11 P
BJ
300
1.51
17
17.8
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.1
6.1
1.0
3.81 mg Oxygen/hr
0.84 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:11 1.03 _ D mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fo
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/l)
6.16
6.07
6
5.97
5.94
5.91
5.85
5.83
5.81
5.78
5.75
5.72
5.65
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
4/6/2015
4/6/15 1:06 PM
BJ
300
1.6
20
iilliliters
16 Dry Solids
egrees Celsius
egrees Celsius
0.0
6.1
1.0
1.89 mg Oxygen/hr
0.39 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 1 0.39 11mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
4.9
1
4.98
2
4.91
3
4.97
4
4.9
5
4.8
6
4.76
7
4.74
8
4.68
9
4.63
10
4.53
11
4.49
12
4.44
13
4.37
14
4.3
15
4.22
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
4/7/2015
19.6
4/7/15 12:59 PM
RG
4/7/15 1:10 PM
BJ
300
1.56
19.1
19
0.1
5.0
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.04 mg Oxygen/hr
0.65 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: .69 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WW-
Biosolids Permit Number:
Date:
4/8/2015
Digester Temperature:
21
Sampling Date/Time:
4/8/15 12:57 PM
Sampled By:
RG
Analysis Date/Time:
4/8/15 1:06 PM
Analyzed By:
BJ
Sample Volume:
300
Total Solids:
1.5
Beginning Temperature:
19.4
End Temperature:
19.4
Dissolved Oxygen Level
(mg/1)
4.49
4.46
4.41
4.34
4.25
4.12
4.03
3.97
3.91
3.86
6.74
3.6
3.52
3.47
3.39
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
4.5
0.3
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
2.68 mg Oxygen/hr
0.60 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: . .. 7,---Img Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWTP
Biosolids Permit Number:
Date:
4/9/2015
Digester Temperature:
19.9
Sampling Date/Time:
4/9/15 12:53 PM
Sampled By:
LC
Analysis Date/Time:
4/915 1:03 PM
Analyzed By:
BJ
Sample Volume:
300
milliliters
Total Solids:
1.53
% Dry Solids
Beginning Temperature:
19.8
degrees Celsius
End Temperature:
20
degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.3
1.0
3.75 mg Oxygen/hr
0.82 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.82 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek WWT
Biosolids Permit Number:
Date: 4/10/2015
Digester Temperature: 20.9
Sampling Date/Time: 4/10/15 12:53 PM
Sampled By:
LC
Analysis Date/Time:
4/10/15 1:C
Analyzed By:
BJ
Sample Volume:
300
Total Solidsl
1.46
Beginning Temperature:
20.9
End Temperature:
20.6
Dissolved Oxygen Level
5.77
5.67
5.56
5.49
5.37
5.31
5.26
4'1M
5.09
4.92
4.87
4.81
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
0.1
5.8
1.0
3.94 mg Oxygen/hr
0.90 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.01
1
6.15
2
6.07
3
5.93
4
5.9
5
5.75
6
5.63
7
5.55
8
5.42
9
5.34
10
5.23
11
5.12
12
5
13
4.88
14
4.77
15
4.63
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0 5/4/2015 1
1 5/4/151:19PM S
H 5/4/15 1:25 PM EI
300
1.53
18.9
18.9
Ililiters
Dry Solids
grees Celsius
grees Celsius
0.1
6.2
1.0
6.10 mg Oxygen/hr
1.33 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 1.42 R�mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Na
Biosolids Permit Num
D
Digester Temperat
Sampling Date/Ti
Sampled
Analysis Date/Ti
Analyzed
Sample Volu
Total Soli
Beginning Temperat
End Temperat
DE
Specific Oxygen Uptake Rate
SOUR
me:
ber:
Fourth Creek WWTP
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
6.3
1.0
-milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.77 mg Oxygen/hr
0.84 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rater 0.84 �Jmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
ourm GreeK vvvv
5/6/2015
20.6
5/6/15 12:56 PM
RG
5/6/15 1:10 PM
300
1.49
20.6
20.8
0.1
6.1
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
4.37 mg Oxygen/hr
0.98 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: . I mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
5/7/2015
20.9
5/7/15 12:49 PM
LC
5/7115 12:59 PM
BJ
300
1.47
20.8
20.5
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.57
1
6.56
2
6.56
3
6.5
4
6.45
5
6.37
6
6.32
7
6.22
8
6.18
9
6.16
10
6.1
11
6.02
12
5.94
13
5.88
14
5.81
15
5.74
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
0.1
6.6
1.0
3.49 mg Oxygen/hr
0.79 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.75 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
5/8/2015
21.1
5/8/15 1:24 PM
LC
5/8/15 1:36 PM
BJ
300
1.52
20.9
20.8
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.36
1
7.29
2
7.21
3
7.18
4
7.09
5
7.04
6
6.98
7
6.91
8
6.85
9
6.77
10
6.66
11
6.58
12
6.52
13
6.44
14
6.39
15
6.32
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
0.1
7.4
1.0
4.22 mg Oxygen/hr
0.93 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rater 0.88 . mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
5/11 /2015
23.6
5/11/15 12:59 PM
LC
5/11/15 1:07 PM
BJ
300
1.61
23.3
22.8
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
5.7
1.0
4.35 mg Oxygen/hr
0.90 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: r� 0.78 1Img Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time:
Sampled By,
Analysis Date/Time;
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.53
6.47
6.41
6.36
6.3
6.27
6.3
6.22
6.1
6.01
5.95
5.84
5.78
5.73
5.62
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
5/12/2015
23.8
5112/15 1:09 PM
LC
5/12/15 1:15 PM
BJ
300
1.57
23.2
22.5
0.1
6.6
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.47 mg Oxygen/hr
0.74 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 0.64=mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
(mg/1)
5.74
5.62
5.59
5.47
5.32
5.27
5.19
5.12
5.06
5.02
4.96
4.83
4.7
4.62
4.56
4.47
Slope:
Intercept:
Correlation Coefficient:
23
6/1/15 1:09 PM
5 1:15 PM
milliliters
% Dry solids
degrees Celsius
degrees Celsius
BJ
300
1.8
22.7
22.5
0.1
5.7
1.0
Oxygen Uptake Rate: 4.94 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.91 mg Oxygen/g/hr
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 0.79 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time,
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
6/2/2015
24.6
6/2/15 12:55 PM
RW
612/15 1:01 PM
BJ
300
1.8
23.6
23
Time Dissolved Oxygen Level
(minutes)
(moll)
0
4.89
1
4.83
2
4.68
3
4.56
4
4.48
5
4.4
6
4.37
7
4.22
8
4.16
9
4.1
10
4.07
11
4.02
12
3.99
13
3.93
14
3.89
15
3.8
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
0.1
4.8
1.0
4.21 mg Oxygen/hr
0.78 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 0.67 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
6/3/2015
21
RW
15 12:57 PM
BJ
300
1.72
20.9
20.8
0.1
6.2
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4.85 mg Oxygen/hr
0.94 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:y 0.89 �j mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.61
55 8
5.53
5.44
5.42
5.36
5.3
Fourth Creek WWTP
mi
%
de
de
6/4/2015
20.8
6/4/15 1:14 PM
LC
614/15 1:20 PM
BJ
300
1.7
20.7
20.6
5.16
5.08
5
4.95
4.89
4.84
4.78
4.73
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
5.6
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
3.70 mg Oxygen/hr
0.73 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.69 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
6/8/2015
23.6
618/15 1:09 PM
LC
6/8115 1:13 PM
BJ
300
1.71
23.5
22.6
0.1
5.2
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.95 mg Oxygen/hr
0.77 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 �mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
6/9/2015
24.3
6/9/15 1:06 PM
RW
BJ
300 milliliters
1.81 % Dry Solids
23.7 degrees Celsius
23.4 degrees Celsius
0.1
8.6
1.0
4.64 mg Oxygen/hr
0.85 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:0.70 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 07/09/2015
Reported, 07/13/2015
For: City of Statesville 4th Creek
Comments: Geometric Mean 95,428 MPNIg
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
150709-17-01
Fecal Coliforms
1
29,661
MPNIg
SM92210E-2006
07/10/2015
WL
150709-17-01
Percent Solids
1
11.8
%
SM254OB-1997
07/10/2015
WL
160709-17-02
Fecal Coliforms
2
96,386
MPNIg
SM92210E-2006
07/10/2015
WL
150709-17-02
Percent Solids
2
16.6
%
SM254OB-1997
07/10/2015
WL
150709-17-03
Fecal Coliforms
3
123,077
MPN/g
SM92210E-2006
07/10/2015
WL
150709-17-03
Percent Solids
3
13.0
%
SM2540B-1997
07/10/2015
WL
160709-17-04
Fecal Coliforms
4
131,148
MPNIg
SM92210E-2006
07/10/2015
WL
150709-17-04
Percent Solids
4
12.2
%
SM254OB-1997
07/10/2015
WL
150709-17-05
Fecal Coliforms
5
120,300
MPNIg
SM92210E-2006
07/10/2015
WL
150709-17-05
Percent Solids
5
13.3
%
SM254OB-1997
07110/2016
WL
150709-17-06
Fecal Coliforms
6
110,346
MPNIg
SM92210E-2006
07/10/2015
WL
150709-17-06
Percent Solids
6
14.6
%
SM254OB-1997
07/10/2015
WL
150709-17-07
Fecal Collforms
7
117,647
MPNIg
SM92210E-2006
07/10/2015
WL
160709-17-07
Percent Solids
7
13.6
%
SM2540B-1997
07/10/2015
WL
Respectfully
submitted,
Dena Myers
NC Cert 9440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 6704/872/4697
Page 1 of 3

Client:
STATE,
122 Court Street v P.O. Box 229
Address: '' b�J 7C �� GG
Statesville, NC 28687
( ,;,, "r% (704) S72-4697
Chainof
Custody Record
�qC_ a'lo g
Contact Person: C�� _ ;O��n��v� Phone #33& _ _ �S- FAX#-� �'14S/-
PO # S� _ ��! �� Requisitioned by: ''� J (rir�}� /, ,^ c,Date
Yttiti St'L\t 1 % 3`
c`\
J/S411V1
Customer
Sample 1D#
Lab 1D #
Time Sampled
Grab Only
) y)
Date Sampled
{Grab Only)
a
Matrix
Parameters requested for analysis
sWdOo,
w
ww
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s
lr
f
2
3
I
j�LUl.1 I
t
i
a
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Relinquished b-✓�L{��
q Y i�'C' ,
r � C�J ~
Time n - am,pm Date a %/ /
Sampled by:
Received by: +�-�� I J
Time t C m Date 1
LAP
r:
Transported by: L(5
-J--/
v�
Relinquished by:
Time am, pm Date __j
Holding times met:
,Received by:
Time am, pm Date /�/
Compliance work:
Composite Sampling #1:
Time begin am, pm Date
Non-compliance work:
Time end am, pm Date —f�
Lab Comments:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date _/�

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.75
1
7.75
2
7.7
3
7.68
4
7.63
5
7.61
6
7.56
7
7.51
8
7.45
9
7.4
10
7.34
11
7.29
12
7.22
13
7.17
14
7.1
15
7.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
7/1/2015
23.3
7/1/15 1:26PM
7/1115 1:32 PM
BJ
1.52
23
22.5
0.0
7.8
1.0
Ililiters
Dry Solids
grees Celsius
arees Celsius
2.92 mg Oxygen/hr
0.64 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: r mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids;
Beginning Temperature
End Temperature
Dissolved Oxygen Level
(MO/1)
E7.86
.91
.92
.91
.89
7.79
7.69
7.64
7.6
7.56
7.52
7.45
7.4
7.31
7.26
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
7/2/2015
22.6
7/2/15 1:06 PM
LC
7/2/15 1:10 PM
BJ
300
1.53
22.6
22.1 .
0.0
8.0
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.75 mg Oxygen/hr
0.60 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:.054 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWTP
Biosolids Permit Number:
Date:
7/6/2015
Digester Temperature:
24.9
Sampling Date/Time:
716/15 12:59 PM
Sampled By:
LC
Analysis Date/Time:
7/6/15 1:06 PM
Analyzed By:
BJ
Sample Volume:
300
milliliters
Total Solids:
1.48
% Dry Solids
Beginning Temperature:
24.7
degrees Celsius
End Temperature:
23.2
degrees Celsius
Dissolved Oxygen Level
7.38
e
7.44
7.48
7.5
0
7.48
7.49
7.49
7.48
7.45
7.42
7.38
7.4
7.39
7.36
7.35
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.5
0.6
0.40 mg Oxygen/hr
0.09 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.07 �mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.55
7.51
7.47
7.43
7.37
7.33
7.29
7.27
7.23
7.24
7.24
7.25
7.28
27 8
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTPI
24.8
BJ
300 milliliters
1.53 % Dry Solids
24.5 degrees Celsius
23.7 Idegrees Celsius
0.0
7.5
0.8
1.09 mg Oxygen/hr
0.24 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.20 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
7/8/2015
24.6
7/8/15 1:00 PM
LC
7/8115 1:09 PM
BJ
300
1.55
24.3
22.6
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.1
0.2
0.30 mg Oxygen/hr
0.07 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 0.06 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1 7/13/2015 1
7/13/15 1:02 PM
AS
7/13/15 1:14 PM
BJ
300
1.71
24
23.8
0.1
8.2
1.0
Aliliters
'o Dry Solids
egrees Celsius
egrees Celsius
4.00 mg Oxygen/hr
0.78 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.64 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WW"
Biosolids Permit Number:
Date:
7/14/2015
Digester Temperature:
23.7
Sampling Date/Time:
7/14/15 1:10 PM
Sampled By:
AS
Analysis Date/Time:
7/14/15 1:22 PM
Analyzed By:
BJ
Sample Volume:
300
Total Solids:
1.65
Beginning Temperature:
23.4
End Temperature:
23.1
Dissolved Oxygen Level
8.13
8.04
7.99
7.95
7.88
7.76
7.72
7.64
7.57
7.48
7.41
7.31
s
7.25
7.16
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
8.1
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.82 mg Oxygen/hr
0.77 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 0.67 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
10/5/2015
18.8
10/5/15 9:56 AM
RG
10/5/15 10:04 AM
BJ
300
1.46
18.9
19.3
Dissolved Oxygen Level
9.33
9.15
9.1
::•
8.58
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
9.2
1.0
2.70 mg Oxygen/hr
0.62 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.66 S mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
10.1
9.96
9.83
9.74
9.66
9.56
9.48
9.41
9.36
9.32
9.22
9.11
09 6
s
9.03
0
9.01
Slope:
Intercept:
Correlation Coefficient:
IFourth Creek WWTP1
20.5
10/6/15 3:01 PM
RG
10/6/15 3:10 AM
300
milliliters
% Dry Solids
degrees Celsius
decrees Celsius
1.5
20.5
20.7
0.1
10.0
1.0
Oxygen Uptake Rate: 4.27 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.95 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/I)
0
7.88
1
7.89
2
7.94
3
7.94
4
8.04
5
8.04
6
8.03
7
8
8
8.03
9
8.02
10
8.02
11
7.99
12
7.96
13
7.94
14
7.9
15
7.84
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
10/7/2015
22.6
10/7/15 12:48 PM
RG
10/7/15 12:55 PM
BJ
300
1.59
21
0.0
8.0
0.1
milliliters
% Dry Solids
Degrees Celsius
Degrees Celsius
0.07 mg Oxygen/hr
0.01 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: 0.01 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
21.1
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.13
8.06
8
7.95
7.92
7.9
7.84
7.779
7.77
7.76
7.75
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
)urth Creek WWTP
10/8/2015
22.6
10/8/15 12:30 PM
RG
10/8/15 12:37 PM
BJ
300 milliliters
1.57 % Dry Solids
20.3 degrees Celsius
19.8 dearees Celsius
0.0
8.2
1.0
1.93 mg Oxygen/hr
0.41 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.41 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fou
Biosolids Permit Number:
21.1
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.18
8.17
8.26
8.21
8.26
8.3
8.3
0
8.36
0
8.29
8.12
8.1
8.02
8.05
Slope:
Intercept:
Correlation Coefficient:
10/9/2015
21.6
10/9/15 1:00 PM
RG
15 1:08 PM
milliliters
% Dry Solids
Idegrees Celsius
lde.qrees Celsius
BJ
300
1.55
21.4
19.9
0.0
8.3
0.4
Oxygen Uptake Rate: 0.49 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.10 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:0.10 4 _ _ mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR "
Facility Name: Fourth Creek
Biosolids Permit Number:
Date:
Digester Temperature
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
10/12/2015
21.6
10/12/15 12:58 PM
I;I 10/12/15 1:05 PM n
300 milliliters
1.5 % Dry Solids
19.3 degrees Celsius
19.3 degrees Celsius
0.0
8.0
0.5
0.91 mg Oxygen/hr
0.20 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rater 0.22 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
10/13/2015
20.6
10/13/15 12:59 PM
LC
10/13/15 1:07 PM
BJ
300
1.48
20.8
20.4
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
2.27 mg Oxygen/hr
0.51 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.49 .11mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Statesville WQ Permit Number: WQ 00016247
WWTP Name: Third Creek WWTP NPDES Number: NCO020591
Monitoring Period: From 01/01/2015 To 12/31/2015
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. VA (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density XX Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlicahle to alternative nerformed (Class A or Class R) comnlete the fnllnwinu monitorinu data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dances
Analysis
Fecal
2x10to the 6 th
MPN
Coliform
power per gram
1,149
2282
5333
MPN/g
0
quarterly
grab
SM92210E
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) XX
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
XX reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
And mith Residuals Superintendent
Pteanprint) ✓
Signature of P eparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 01/21/2015
Reported: 01/22/2015
For: 3rd Creek- COS
Comments: Geometric Mean 2,282 MPNg
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
150121-08-01
Fecal Coliforms
1
1,149
MPNIg
SM92210E-2006
01/21/2015
WL
150121-08-01
Percent Solids
1
14.8
%
SM254OB-1997
01/2112015
WL
150121-08-02
Fecal Coliforms
2
3,327
MPNIg
SM92210E-2006
01/21/2016
WL
160121-08-02
Percent Solids
2
15.03
%
SM254OB-1997
01/21/2015
WL
150121-08-03
Fecal Coliforms
3
5,263
MPNIg
SM92210E-2006
01/2112015
WL
150121-08-03
Percent Solids
3
15.2
°lo
SM254OB-1997
01/21/2015
WL
160121-08-04
Fecal Coliforms
4
1,381
MPN/g
SM92210E-2006
01121/2015
WL
160121-08-04
Percent Solids
4
15.2
%
SM254OB-1997
01/21/2016
WL
160121-08-05
Fecal Coliforms
5
1,513
MPNIg
SM92210E-2006
01/21/2016
WL
150121-08-05
Percent Solids
5
15.2
%
SM2540B-1997
01/21/2015
WL
150121-08-06
Fecal Coliforms
6
5,333
MPNIg
SM92210E-2006
01/21/2015
WL
150121-08-06
Percent Solids
6
15
%
SM254OB-1997
01/21/2015
WL
150121-08-07
Fecal Coliforms
7
1,438
MPN/g
SM92210E-2006
0112112015
WL
150121-08-07
Percent Solids
7
16
%
SM254OB-1997
01/21/2016
WL
Respectfully
submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 •704/872/4697
Page 'I of 3
y

Client:^1 ngr G ^
STATESVILLEANALY'Z'ICAL
122 Court Street - PO- Sox 228
Address: 1 �-'� J
J
1 `"Cr �'sJ ,1 ;\i �r'4 �i 7 �'
Statesville, NC 28687
.[phone]
Contact Person, C; ; C l� w` � Phone
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FAM, , �� �
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Chainof
# 4—G, y, ��y¢, Requisitioned b
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Crime
Date)
Custody 3' R�CO�'(�
Customer Lab -ID # Time Sampled
Sample ID# (Grab Only)
Date Sampled / m
(Grab Only)
Matrix
sioago w I ww
Parameters requested for analysis
1
4 3
9Ir JV. �;
%
ii✓ilyf�5
i�q�u• ��
? �ry
k,
r
Gi v i
1
}
s
8
I
rr
Relinquished by: .I1',f�
Time J 3!Jpm Date `�/� ,s 1S
Sampled by:
Received by:U
Time ° '�
am,'pm Date J� /
Transported by:
v
L\1A
Relinquished by:
Time
am, pm Date
//
/
Holding times met: V
Received by:
Time
am, pm Date
/
Composite Sampling #1:
_/
Compliance work:
Time begin am, pm Date _/ /_
Non-compliance work:
Time end am, pm Date ^/ /
Lab Comments:
.Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date _/

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
10.71
10.66
10.61
10.54
10.58
10.57
10.54
10.51
10.45
10.4
10.38
10.36
10.31
10.22
10.18
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
10.8
1/5/15 10:18
SA
1/5/15 10:25
300
1.7
11.6
0
12.4
0.0
10.7
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
1.87 mg Oxygen/hr
0.37 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.63 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Nam
Biosolids Permit Numb(
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
10
9.95
89 8
9.78
9.72
9.65
9.67
9.59
9.52
9.46
9.35
9.26
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WO0016247
1 /6/2015
1 1/6/15 12:14 1
1 116/15 0:24 1
300
1.7
11�.9
s
13.5
0.1
10.1
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.19 mg Oxygen/hr
0.63 mg Oxygen/g/hr
13 degrees Celsius
1.6057814,76
Temperature Corrected Specific Oxygen Uptake Rate: 1.00 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WV1
WQ0016247
1 /7/2015
10.6
1/7/15 12:09
SA
1/7/15 0:18
SA
300
1.7
11.8
13.2
Dissolved Oxygen Level
9.56
9.53
9.49
9.45
9.41
9.35
e
9.32
9.27
9.25
9.21
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
0.0
9.6
1.0
1.84 mg Oxygen/hr
0.36 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.58 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:1 Third Creek WWTP
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
WQ0016247
1 /9/2015
10.6
1/9/15 14:11
SA
1/9/15 2:23
SA
300
1.7
11.3
13.8
Time Dissolved Oxygen Level
(minutes)
(Mgt[)
0
10.28
1
10.24
2
10.2
3
10.15
4
10.07
5
10.03
6
10.01
7
9.99
8
9.94
9
9.9
10
9.86
11
9.83
12
9.79
13
9.79
14
9.76
15
9.72
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
10.3
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.23 mg Oxygen/hr
0.44 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: = 0.70 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WQ0016247
1/12/2015
10.6
1/12/15 12:50
1 1/12/1513:04 M
300 milliliters
1.7 % Dry Solids
11.1 degrees Celsius
12.8 degrees Celsius
0.0
10.2
1.0
2.54 mg Oxygen/hr
0.50 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.85 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
9.57
1
9.53
2
9.5
3
9.47
4
9.45
5
9.43
6
9.4
7
9.4
8
9.41
9
9.39
10
9.38
11
9.36
12
9.33
13
9.31
14
9.27
15
9.26
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WQ0016247
1/13/2015
10.5
1/13/15 13:49
SA
1/13/15 14:01
SA
300 milliliters
1.7 % Dry Solids
11.1 degrees Celsius
13.1 degrees Celsius
0.0
9.5
1.0
1.08 mg Oxygen/hr
0.21 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.37 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.04
7.99
7.92
7.86
7.81
7.78
7.75
s
7.72
7.68
7.66
7.61
7.58
7.55
7.53
7.52
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
2/2/2015
11.8
2/2/15 12:19
SA
2/2/15 12:27
SA
300
1.8
12.1
13.9
0.0
8.0
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.99 mg Oxygen/hr
0.37 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.59 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
2/4/2015
10.9
2/4/15 13:05
SA
2/4/15 13:12
SA
300
1.9
11.2
13.5
Dissolved Oxygen Level
9.3
9.29
9.27
9.26
9.23
9.2
9.1
9.05
s
9
8.93
8.75
8.65
8.6
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
9.4
0.9
2.89 mg Oxygen/hr
0.51 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.87 ] mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14 ..
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WV)
WO0016247
2/5/2015
10.9
2/5/15 12:58
SA
2/5/15 13:11
SA
300
1.9
11.7
12.8
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
0.0
7.7
1.0
2.73 mg Oxygen/hr
0.48 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.82 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
2/6/2015
10.9
SA
2/6/15 13:35
SA
300
1.9
11.1
0.0
8.7
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.57 mg Oxygen/hr
0.45 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1, mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
2/10/2015
10.9
2/10/15 12:50
SA
2/10/15 13:03
SA
300
1.9
11.8
13.3
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
7.8
1.0
3.64 mg Oxygen/hr
0.64 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 1 1.03 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
2/11 /2015
10.7
2/11/15 14:10
9 2/11/15 14:16 1
300
s
1.9
11.4
s
12.3
0.1
8.7
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.24 mg Oxygen/hr
0.57 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: ^^ 0.98 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number;
Date=
Digester Temperature:
Sampling Date/Time:
Sampled By,
Analysis Date/Time
Analyzed By:
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
2/12/2015
10.5
2/12/15 13:48
SA
2/12/15 13:56
SA
300
1.9
11.2
13.1
0.1
9.5
1.0
milliliters
% Dry Solids
Degrees Celsius
Degrees Celsius
3.68 mg Oxygen/hr
0.65 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 1.11 =1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name;
Biosolids Permit Number
Date;
Digester Temperature
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature.
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.0
10.3
1.0
1.59 mg Oxygen/hr
0.28 mg Oxygen/g/hr
11 degrees Celsius
1.838459212
Temperature Corrected Specific Oxygen Uptake Rate: 0.51 1,mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
3/3/2015
10.8
3/3/15 10:12
JW
3/3/15 10:21
SA
300
1.9
11.1
12.5
0.0
8.3
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.21 mg Oxygen/hr
0.21 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.36 =7J mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
-
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
3/4/2015
11.8
3/4/15 13:24
JW
3/4/15 13:30
SA
300
1.9
12.2
13.8
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.8
1.0
1.14 mg Oxygen/hr
0.20 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 32 1 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.68
6.64
6.59
6.54
6.49
6.44
a
6.4
6.33
6.26
6.2
6.15
6.09
6.04
6.01
5.94
5.88
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
3/5/201s
12.8
3/5/15 6:50
SA
3/5115 6:58
300 milliliters
1.9 % Dry Solids
12.5 degrees Celsius
13.8 dearees Celsius
0.1
6.7
1.0
3.26 mg Oxygen/hr
0.57 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rater 0.92 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W00016247
3/6/2015
3/6/15 13:33
SA
3/6/15 13:41
300 milliliters
1.9 % Dry Solids
11.8 degrees Celsius
13.3 degrees Celsius
0:0
8.6
1.0
2.59 mg Oxygen/hr
0.45 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.73 �mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek VM
Biosolids Permit Number:
WQ0016247
Date:
315/2015
Digester Temperature:
11.6
Sampling Date/Time:
3/9/15 10:18
Sampled By:
SA
Analysis Date/Time:
3/9/15 10:27
Analyzed By:
SA
Sample Volume:
300
Total Solids:
1.9
Beginning Temperature:
12.2
End Temperature:
13.8
Time
Dissolved Oxygen Level
(minutes)
(mg/I)
0
9.69
1
9.68
2
9.62
3
9.6
4
9.56
5
9.52
6
9.49
7
9.45
8
9.46
9
9.42
10
9.38
11
9.34
12
9.3
13
9.26
14
9.23
15
9.17
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
0.0
9.7
1.0
2.01 mg Oxygen/hr
0.35 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.57 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By.
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
12.37
1
12.33
2
12.28
3
12.25
4
12.21
5
12.17
6
12.11
7
12.03
8
11.97
9
11.93
10
11.9
11
11.88
12
11.83
13
11.78
14
11.75
15
11.71
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
3/10/2015
11.1
3/10/15 12:14
SA
3/10/15 12:20
SA
300
1.9
11.5
13.1
0.0
12.4
1.0
milliliters
% Dry Solids
legrees Celsius
legrees Celsius
2.73 mg Oxygen/hr
0.48 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.0 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 04/08/2015
Reported: 04/09/2015
For: 3RD Creek
Comments: Geometric Mean 17,211 MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
160408-12-01
Fecal Coliforms
1
40,909
MPN/g
SM92210E-2006
04/08/2015
CL
150408-12-01
Percent Solids
1
22.0
%
SM254OB-1997
04/08/2015
CL
150408-12-02
Fecal Coliforms
2
15,957
MPN/g
SM92210E-2006
04/08/2015
CL
150408-12-02
Percent Solids
2
18.8
%
SM254OB-1997
04/08/2015
CL
150408-12-03
Fecal Coliforms
3
17,722
MPN/g
SM92210E-2006
04/08/2015
CL
150408-12-03
Percent Solids
3
15.8
%
SM254OB-1997
04/08/2015
CL
150408-12-04
Fecal Coliforms
4
6,468
MPN/g
SM9221 CE-2006
04/08/2015
CL
150408-12-04
Percent Solids
4
20.1
%
SM254OB-1997
04/08/2015
CL
150408-12-05
Fecal Coliforms
5
7,556
MPN/g
SM92210E-2006
04/08/2015
CL
150408-12-05
Percent Solids .
5
22.5
°%
SM2540B-1997
04/08/2015
CL
150408-12-06
Fecal Coliforms
6
11,719
MPN/g
SM92210E-2006
04/08/2016
CL
150408-12-06
Percent Solids
6
25.6
%
SM254OB-1997
04/08/2015
CL
150408-12-07
Fecal Coliforms
7
67,511
MPN/g
SM92210E-2006
04/08/2016
CL
150408-12-07
Percent Solids
7
23.7
%
SM2540B-1997
04/08/2015
CL
Respectfully
submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37756,
EPA #NC00909
PO Box 228.Statesville, NC 28687. 704/872/4697
Page 1 of 3

Client: S\111GLCC mi
STATES VILLE ANALYTICAL
i I22 CourtStreet • P.Q. Box 228
Address: ;1)
Statesville. NC 28687
(704) 872- 697
On©
Contact Person: - Phone #
3.� '9 1 � ` �rf.�S
FAX#
3.3CD
Chain of
Custody Record.
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PO # �-, _ �4 i�( ` Requisitioned by ! 1�lti S V1 i `c�` ��%O✓ �'�p� '�� -Y ��S
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Customer
Sample [DO
Lab -ID #
Time Sampled
(Grab Only)b
Date Sampled !
(Grab Only)
Matrix
Parameters requested for analysis
siudgo
, w
ww
6 -iCj
C-14
+
j
l
7`
C7 6
elinquished by:
Time=� a , pm Date t} //
Sampled
Received by: �} Y - ,L r Time s % (m,;� pm Date fi�.�
Transported by:
Relinquished by:
Time
am, pm Date _J_J
Molding times met:
Received by:
Time
am, pm Date ,/ /
Compliance work:
Composite Sampling #i;
Time begin am, pm Date _ J/
Non-compliance work:
Time end am, pm Date T/-_/
Lab Comments:
Composite Sampling #2:
Time begin am, pm Date
Time' end am, pm Date_/

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Datdt
, 4/1/2015
Digester Temperature:
13.7
Sampling Date/Time:
4/1/15 8:38
Sampled By:
JW
Analysis Date/Time:
4/1/15 8:47
Analyzed By:
SA
Sample Volume:
300
milliliters
Total Solids:
1.9
% Dry Solids
Beginning Temperature:
13.9
degrees Celsius
End Temperature:
15.2
degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.2
1.0
2.57 mg Oxygen/hr
0.45 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:E0.63 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
4/2/2015
12.7
4/2/15 8:35
SA
412/15 8:42
SA
300
1.9
12.8
14.3
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.97
1
6.92
2
6.89
3
6.86
4
6.82
5
6.79
6
6.73
7
6.7
8
6.67
9
6.62
10
6.59
11
6.56
12
6.51
13
6.48
14
6.43
15
6.39
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
0.0
7.0
1.0
2.29 mg Oxygen/hr
0.40 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
IM

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.75
1
7.7
2
7.68
3
7.64
4
7.61
5
7.56
6
7.49
7
7.43
8
7.37
9
7.31
10
7.26
11
7.22
12
7.16
13
7.12
14
7.06
15
7.02
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
-4/20/20151:S'
17.6
4/20/15 11:28
SA
4/20/15 11:36
SA
300
1.5
17.5
17.8
0.1
7.8
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.05 mg Oxygen/hr
0.68 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate: �0.7 �} mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
4/21 /20151
17.3
4/21/15 8:55
SA
4/21/15 9:04
SA
300
1.5
17.1
16.5
Dissolved Oxygen Level
(mg/1)
7.41
7.35
7.29
7.27
7.24
7.2
7.15
7.12
7.09
7.03
7
6.97
6.92
6.9
6.87
6.82
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.4
1.0
2.28 mg Oxygen/hr
0.51 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.62jimg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Na
Biosolids Permit Num
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
4/22/2015
4/22/15 8:39
SA
4/22/15 8:45
300
1.5
16.8
0.0
7.7
1.0
Milliliters
6 Dry Solids
egrees Celsius
egrees Celsius
2.00 mg Oxygen/hr
0.44 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 54 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
4/23/2015
Digester Temperature:
15.9
Sampling Date/Time:
4/23/15 8:28
Sampled By:
SA
Analysis Date/Time:
4/23/15 8:36
Analyzed By:
SA
Sample Volume:
300
milliliters
Total Solids:
1.5
% Dry Solids
Beginning Temperature:
15.8
degrees Celsius
End Temperature:
15.5
degrees Celsius
Dissolved Oxygen Level
8.32
8.31
8.28
8.24
8.2
18 8
8.15
8.11
8.07
8.05
8
7.95
7.91
7.89
7.86
Slope: 0.0
Intercept: 8.3
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 1.93 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.43 mg Oxygen/g/hr
Average Temperature: 16 degrees Celsius
Temperature Correction Factor: 1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:L0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WO0016247
5/1/2015
13.8
5/1/15 11:06
SA
5/1/15 11:15
SA
300
1.5
14.1
15.2
Dissolved Oxygen Level
7.49
7.41
7.35
7.3
7.27
7.2
7.14
7.1
7.07
6.98
6.9
6.83
6.79
6.73
6.69
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
7.5
1.0
3.12 mg Oxygen/hr
0.69 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.97 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
5/4/2015
17.4
5/4/15 13:09
SA
5/4/15 13:14
SA
300
1.5
16
16.8
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.74
1
7.67
2
7.62
3
7.58
4
7.55
5
7.49
6
7.41
7
7.36
8
7.32
9
7.28
10
7.22
11
7.16
12
7.11
13
7.08
14
7.05
15
7.01
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
0.0
7.7
1.0
2.97 mg Oxygen/hr
0.66 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: �u0.87 � mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Nam
Biosolids Permit Numb(
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.79
7.75
7.7
7.66
7.61
7.53
7.45
7.41
s
7.36
7.32
7.3
7.27
7.18
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
16.2
5/5/15 12:10
0 5/5/1512:17 N
300 milliliters
1.5 % Dry Solids
15.7 degrees Celsius
16.4 decrees Celsius
0.0
7.8
1.0
2.42 mg Oxygen/hr
0.54 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:11 0.70 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.22
8.17
8.09
8.05
8.02
.8
7.92
s
7.89
7.81
7.7
7.76
7.66
7.6
7.48
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
5/6/2015
15
5/6/15 8:11
SA
5/6/15 8:18
SA
300
1.5
15.3
15.9
0.1
8.2
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
3.02 mg Oxygen/hr
0.67 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: L_ 0.88___Jlmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
� Third Creek WWTP 0
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5/7/2015
15.7
5/7/15 8:21
SA
5/7/15 8:31
SA
300
1.5
16
16.8
0.0
7.7
1.0
liliters
Dry Solids
3rees Celsius
frees Celsius
2.69 mg Oxygen/hr
0.60 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.78�mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number.
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.0
6.4
1.0
2.70 mg Oxygen/hr
0.60 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.74� mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
5/11 /2015
17.8
5/11/15 13:21
SA
5/11/15 13:30
SA
300
1.5
17.6
18.5
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.3
1.0
2.21 mg Oxygen/hr
0.49 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Analytical Results
g-�
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 07/09/2015
Reported: 07/10/2016
For: City of Statesville 3rd Creek
Comments: Geometric Mean 261 MPN/g
Sample Number Parameter Sample 1D Result Unit Method Analyzed Analyst
150709-16-01
Fecal Coliforms
1
1,061
MPN/g
SM92210E-2006
07/09/2015
WL j
160709-16-01
Percent Solids
1
13.2
0/0
SM254OB-1997
07/09/2015
WL
150709-16-02
Fecal Conforms
2
155
MPN/g
SM92210E-2006
07/09/2016
WL
150709-16-02
Percent Solids
2
26.8
%
SM254OB-1997
07/09/2016
WL
150709-16-03
Fecal Coliforms
3
1,619
MPN/g
SM92210E-2006
07/09/2015
WL
150709-16-03
Percent Solids
3
14.2
%
SM254OB-1997
07/09/2015
WL
150709-16-04
Fecal Coliforms
4
177
MPNIg
SM92210E-2006
07/09/2015
WL
150709-16-04
Percent Solids
4
11.3
%
SM254OB-1997
07/0912015
WL
150709-16-05
Fecal Coliforms
5
<167
MPN/g
SM9221 CE-2006
07/09/2015
WL
150709-16-05
Percent Solids
5
12
%
SM254OB-1997
07/09/2015
WL
150709-16-06
Fecal Coliforms
6
<95
MPN/g
SM92210E-2006
07/09/2015
WL
150709-16-06
Percent -Solids
6
21
%
SM254OB-1997
07/09/2016
WL
150709-16-07
Fecal Coliforms
7
<110
MPN/g
SM92210E-2006
07/09/2015
WL
150709-16-07
Percent Solids
7
18.2
%
SM254OB-1997
07/09/2015
WL
Respectfully
submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37766,
EPA #NC00909
PO Box 228 • Statesville, NC 28687.704/872/4697
Page 1 of 2

Client: t r,,.
STATESYY1.Y.lE ANALYTICAL
122 CStre.e - Px 228
Address: ' t u �� f\ � OG
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Stat 23687
i704) 872-4697
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PO # ? ` Requisitioned b : ," crr�}G rr Date
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Customer
Sample ID# p
Sam
Lab -ID #
The Sampled
(Grab Only)
Date Sampled
(Grab Only)
a
Matrix
Parameters requested for analysis
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41
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Relinquished by: � i''j'�; ��
Time E �-��
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Sampled by: >?iE•�
Received by: �--- +� �' i
Time i' ' '
_
� pm Date l
Transported AV�k-j S�1••`��i
by:
Relinquished by:
Time
am, pm Date _f�
Holding times met:
Received by:
Time
am, pm Date _/�
Compliance work:
Composite Sampling ##1:
Time begin am, pm Date �/_ _/
Non-compliance work:
Time end am, pm Date �/_/
Lab Comments:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
s Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
6/1 /2015
19.8
6/1/15 12:48
1 611/15 12:55 M
300
1.5
19.6
20.3
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.1
6.7
1.0
3.00 mg Oxygen/hr
0.67 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.67= mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name: Third Creek WWTP
Biosolids Permit Number: WQ0016247
Date: 6/4/2015
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
18.3
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
6/4/15 8:31
SA
6/4/15 8:40
SA
300
1.5
18.2
18.9
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.98
1
6.93
2
6.89
3
6.84
4
6.8
5
6.76
6
6.71
7
6.67
8
6.63
9
6.6
10
6.57
11
6.52
12
6.49
13
6.45
14
6.41
15
6.38
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.0
1.0
2.39 mg Oxygen/hr
0.53 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.57 D mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Facility Na
Biosolids Permit Numb
Da
Digester Temperatu
Sampling Date/Ti
Sampled
Analysis Date/Ti
Analyzed
Sample Volu
Total Solid
Beginning Temperatu
End Temperatu
Specific Oxygen Uptake Rate
SOUR
m
m
me: Third -Creek WWTP
er: WQ0016247
te: 6/5/2015
re: 17.9
e: 6/5/15 10:05
By: SA
e: 6/5/15 10:15
By: SA
me: 300 mi
s: 1.5 %
re: 17.6 de
re: 18.4 de
Time Dissolved Oxygen Level
(minutes) (mg/1)
0 6.83
1 6.79
2 6.76
3 6.71
4 6.68
5 6.64
6 6.61
7 6.58
8 6.55
9 6.5
10 6.47
11 6.43
12 6.4
13 6.36
14 6.32
15 6.29
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.8
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
2.15 mg Oxygen/hr
0.48 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate:0.55 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Time Dissolved Oxygen Level
(minutes) (mg/1)
0 6.83
1 6.79
2 6.76
3 6.71
4 6.68
5 6.64
6 6.61
7 6.58
8 6.55
9 6.5
10 6.47
11 6.43
12 6.4
13 6.36
14 6.32
15 6.29
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.8
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
2.15 mg Oxygen/hr
0.48 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate:0.55 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
0.0
6.8
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
2.15 mg Oxygen/hr
0.48 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate:0.55 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Nam
Biosolids Permit NumbE
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WQ0016247
6/8/2015
19.6
618115 9:25
SA
SA
300 milliliters
1.5 % Dry Solids
19.5 degrees Celsius
19.2 degrees Celsius
0.1
7.4
1.0
3.10 mg Oxygen/hr
0.69 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: �J0.74 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
WQ0016247
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
6/9/2015
21
6/9115 13:03
SA
6/9/15 13:07
SA
300
I
20.9
20.8
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.23
1
7.17
2
7.11
3
7.07
4
7.02
5
6.98
6
6.93
7
6.88
8
6.85
9
6.79
10
6.73
11
6.69
12
6.59
13
6.61
14
6.55
15
6.5
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.2
1.0
2.90 mg Oxygen/hr
0.64 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: j9.61 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:N Third Creek WWTP
Biosolids Permit Number:1 WQ0016247
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:1
19.8
6/10/15 9:57
SA
6/10/15 10:06
SA
300
1.5
20.4
20.2
Dissolved Oxygen Level
7.23
7.17
7.11
7.07
. •:
6.88
6.85
6.79
6.73
6.69
6.59
6.61
0
6.55
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.0
7.2
1.0
2.90 mg Oxygen/hr
0.64 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:i�0.64 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
6/11 /2015
21
6/11/15 10:46
SA
6/11115 10:55
SA
300
1.5
20.9
20.4
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.1
1.0
2.77 mg Oxygen/hr
0.62 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:11 0.59 7 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
7/1 /2015
Digester Temperature:
20.1
Sampling Date/Time:
7/1/15 10:53
Sampled By:
SA
Analysis Date/Time:
7/1/15 11:01
Analyzed By:
SA
Sample Volume:
300
Total Solids:
1.4
Beginning Temperature:
19.9
End Temperature:
19.7
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.6
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
2.09 mg Oxygen/hr
0.50 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.50 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
3.:

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WQ0016247
712/2015
19.8
7/2/15 9:15
SA
7/2/15 9:24
SA
300
1.4
20.1
19.9
0.0
7.6
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.44 mg Oxygen/hr
0.58 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate f 0.58 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
7/6/2015
210.6
7/6/15 11:58
SA
7/6/15 12:06
SA
300
1.4
21
20.8
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.84
1
7.8
2
7.76
3
7.71
4
7.67
5
7.6
6
7.57
7
7.51
8
7.47
9
7.43
10
7.38
11
7.35
12
7.3
13
7.26
14
7.22
15
7.18
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.8
1.0
2.69 mg Oxygen/hr
0.64 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 1 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:1 Third Creek WU1
Biosolids Permit Number:1 WO0016247
- Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
7/7/2015
19.6
7/7/15 8:10
SA
7/7/15 8:19
SA
300
1.4
19.7
20.1
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.0
8.0
1.0
2.18 mg Oxygen/hr
0.52 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.52 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
7/7/2015
22.1
7/8/15 7:03
SA
7/8/15 7:10
SA
300
1.4
20.8
21.2
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.64
1
7.61
2
7.59
3
7.55
4
7.5
5
7.46
6
7.43
7
7.39
8
7.34
9
7.31
10
7.27
11
7.24
12
7.19
13
7.14
14
7.09
15
7.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.7
1.0
2.37 mg Oxygen/hr
0.56 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.54Mmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:1
Third Creek WWTP
Biosolids Permit Number:V
WQ0016247
Date:
7/9/2015
Digester Temperature:
21.2
Sampling Date/Time:
719/15 13:23
Sampled By:
SA
Analysis Date/Time:
7/9/15 13:29
Analyzed By:
SA
Sample Volume:
300
milliliters
Total Solids:
1.4
% Dry Solids
Beginning Temperature:
21.1
degrees Celsius
End Temperature:q
20.9
degrees Celsius
Dissolved Oxygen Level
7.56
7.54
7.5
7.46
7.44
7.39
7.36
7.28
7.24
7.2
7.17
7.11
7.07
7.05
7.01
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.6
1.0
2.27 mg Oxygen/hr
0.54 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:1 _ _ _0.5_ `�mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:1 Third Creek WWTP
Biosolids Permit Number: WQ0016247
Date: 7/10/2015
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis .Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
22.1
6�
SA
300 milliliters
1.4 % Dry Solids
21.7 degrees Celsius
21.5 Idegrees Celsius
0.0
7.5
1.0
1.92 mg Oxygen/hr
0.46 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: LV 0.41 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Agricultural Lime Application Log
2014
Project: City of Statesville
Field
Soil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pFl
T/ac.(from soil analysis)
Applied
(invoice date)
I 20-01
6.5
N/A
N/A
N/A
I 20-03
6.3
N/A
N/A
N/A
IR-20-08
6.6
N/A
N/A
N/A
IR-20-09
6.6
N/A
N/A
N/A
IR-23-02
6.0
N/A
-N/A
N/A.
IR-23-05
5.9
No lime addition recommended
N/A
N/A
* = Lime to be applied when weather and/or crop removal allows

NCDA&CS comic Division Phone: [phone]
Website: www.i
gov/agronomi
Report No. FY' 136273
Client:
Dennis Phillips
Advisor: Synagro Central
y F
Predictive
201 Barry Oak Rd
Attn:Eric Thompson
t
^�
Statesville, NC 28625
284 Boger Rd
ti �
Mehlich-3 Extraction
Soil Report
Mocksville, NC 27028
Sampled County: Iredell
Sampled:- 05/01/2016 Received: 06/18/2015
Completed: 06/26/2015
Farm: IR-20
Links to Helpful Information -
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0
0 0
0
0
0 0
Note: 12
2-Fescue/OGrass/Tim, 0.0
120-200 0
0
0 0
0
0
0 0
Note: 12
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.36 0.87
16.3 95 0.8 6.5 377 ' 134
73 18
45
383
240 240
548
548
308 0.0
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0
0 0
pH$
0
0 0
Note: 12 Note:
2-Fescue/OGrass/Tim, 0.0
120-200 0
0
0 0
pH$
0
0 0
Note: 12 Note:
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All Mn-Al2
Zn-1
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.36 0.83
15.7 96 0.6 6.6 326 156
75 16
46
366
227 227
491
491
291 0.0
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P206
K20
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
20
0 0
0
0
0 0
Note: 12
2-Fescue/OGrass/Tim, 0.0
120-200 0
20
0 0
0
0
0 0
Note: 12
Test Results [units - WN in g/crrt3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-I K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 0.92
10.7 90 1.1 6.3 291 62
68 19
37
246
160 160
595
595
315 0.0
Nonh Carolina
To11. C0TrU%I1'fVfCaa7ipikAois
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS comic Division Phone: [phone]
Website: vwwv.i
gov/agronomi/
Report No.
FY' 136273
Dennis Phillips
Page 2 of 3
Sample ID: 8
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-FescuelOGrass/Tim, 1 0.0
120-200 0
0
0
0
pH$
0
0
0
Note: 12 Note:
2-Fescue/OGrass/Tim, 0.0
120-200 0
0
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - W/V in
g/cO; CEC and Na in meq/100 cm3; NO3-N in mgldo]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I Na
ESP SS-1 NO3-N
0.32 0.85 20.6
97 0.6 6.6 363 126
81 12
63
261
165
165
761
761
405 0.0
Sample ID: 9
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0
0
0
pH$
0
0
0
Note: 12 Note:
2-Fescue/OGrass/Tim, 0.0
120-200 0
0
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - W/V in
g/ctrr3; CEC and Na in meq/100 cm3; NO3-N in mg/do]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I Na
ESP
SS-1 NO3-N
0.27 0.82 23.6
97 0.6 6.6 407 173
80 14
71
319
199
199
965
965
581 0.0

NCDA&CS omic Division Phone: [phone]
Website: www.r
]ov/agronomi/
Report No. FY1 36293
Client: Shane Porter
Gantt Horn Rd.
Advisor:
Synagro Central
Attn:Eric Thompson
Predictive
351
y
^sv,)�
Statesville, NC 28677
284 Boger Rd
' Y�X,t�,
�ReportMehlich-3
Extraction
Soil I
Mocksville, NC 27028
++ -�
Sa+
Sampled County: Iredell
k I.
Sampled: 05/01/2015 Received: 06/19/2015 Completed: 06/29/2015
Farm: IR-23
Links to Helpful Information
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
0
0
0
0
Note: 12
2-Fescue/OGrass/Tim, 0.0
120-200 0
0 0 0
0
0
0
0
Note: 12
Test Results [units - WIV in g/crrP; CEC and Na in meq/100 cmP; NO3-N in mg/dnr3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.51 0.79
15.4 89 1.8 6.0 292 129
68 17
49 339 220 220
950
950
403
0.1 1
Sample ID: 5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, 0.0
120-200 0
0 0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cnr ; CEC and Na in meq/100 crrr3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WIV
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.46 0.84
15.0 89 1.7 5.9 377 138
69 15
48 222 150 150
637
637
338
0.0
North Carolina
8i?I7:�lCtF Trust fmd Cwniwh%%ik*
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

STANLY COUNTY UTILITIES, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQQ0016247
2015 ANNUAL REPORT

2015 ANNUAL OPERATIONS SUMMARY - LAN® APPLICATION
RTANLY COUNTY UTIL., NC (FKA OAKBOR
.:TANLY COUNTY UTIL., NC WEST STANLY WWTP AEROBICALLY DIGESTED LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
May 2015 328,600.00 G 15.75 D 14.30
YEARLY TOTAL 328,600.00 G 15.75 D 14.30
2/5/2016

2015 ANNUAL REPORT
PROJECT: Stanly Co. Utilities, NC
FACILITY: West Stanly WWTP
24939-B Barbees Grove Road
Oakboro, NC 28129
704-485-4613
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARIER OF LAND
APPLICATION ANNUAL REPORT:
NC0043532
Doug Burgess, Mayor
109-A N Main St
PO Box 610
Oakboro, NC 28129
252-753-5774
James Amaral, ORC/Town
Administrator
109-A N Main St
PO Box 610
Oakboro, NC 28129
704-485-8322
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0005387 Laboratory
Facility Name: STANLY COUNTY UTIL., NC (FKA OAKBORO) A&L Eastern Laboratories Inc.
NPDES# : NCO043532
or WQ# (residual only)
IAWTP Name: WEST STANLY WWTP (FKA OAKBORO WWTP)
Residuals Analysis Data
Product Type
L1Q
Date Sampled (grab) or 03/02/15
Date Composited
Percent Solids
1.15
PARAMETERS (mg/kg dry weight)
Arsenic
6
Cadmium
<2
Mercury
1
Chromium
40
Copper
340
Lead
23
Molybdenum
17
Nickel
22
Selenium
6
Zinc
828
Total Phosphorus
18600
TKN
62 600
Ammonia -Nitrogen
2 610
Nitrate and Nitrite
4100
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
91
(SIGNATURE OF PREPARER)
Date a�— !G - / 6
DENR FORM RSSF (5/2003) Printed: Friday - February 5 2016 at 13:19.17 for: 2170 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0005387 Laboratory
Facility Name: STANLY COUNTY UTIL., NC (FKA OAKBORO) A&L Eastern Laboratories Inc.
NPDES# : NCO043532
or WQ# (residual only)
WWTP Name: WEST STANLY WWTP (FKA OAKBORO WWTP)
Residuals Analysis Data
Product Type
LIQ
Date Sampled (grab) or 03/02/15
Date Composited
Percent Solids
1.15
PARAMETERS (mg/kg dry weight)
Aluminum
14500
Calcium
21600
Magnesium
3730
pH
6.60
Potassium
3780
Sodium
3580
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
FLI
(SIGNATURE OF PREPARER)
NR - Data Not Reported or Data Not Required
Date oq- /( `/
DENR FORM RSSF-B (7/2002) Printed: Friday - February 5 2016 at 13:19:38 for: 2170 01

Page: 1 of 2
Report Number: 15-062-0205
Account Number: 46477
Submitted By: DREW CULP
Send To: SYNAGRO CENTRAL LLC/OAKBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
�L
www.aleastem.com
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond. Virginia 23237 [phone] Fax [phone]
Project: WEST STANLEY WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/2/2015 09:15:00
Lab Number • 60458 Date Received: 03/03/2015 00:00
Sample Id: WS 2015 Date Reported: 03/06/2015
Total Solids *
1.15
11500
100.0
JM
03/03/2015 13:59
gg 85
100.0
JM
03/03/2015 13:59
Moisture
Total Kjeldahl Nitrogen
6.26
62600
10.0
JM
03l04/2015 15
Total Phosphorus
1.86
18600
100
KM
12:
03/04/2015 12:2299
Total Potassium
0.38
3780
100
KM
03/04/2015 12:29
1.00
9960
100
KM
03/04/2015 12:29•
Total Sulfur
2.16
21600
100
KM
03/04/2015 12:29
Total Calcium
0.37
3730
100
KM
03/04/2015 12:29
Total Magnesium
0.36
3580
100
KM
03/04/2015 12:29
Total Sodium
18700
100
KM
03/04/2015 12:29
Total Iron
14500
100
KM
03/04/2015 12:29
Total Aluminum
529
5
KM
03/04/2015 12:29
Total Manganese
5
KM
03/04/2015 12:29
Total Copper
340
828
5
KM
03/04/2015 12:29
Total Zinc
0.26
2610
10.0
JM
03/04/2015 08:15
Ammonia Nitrogen
10.0
03/04/2015 08:15
Organic N
6.00
59990
4100
2.00
JM
03/04/2015 08:15
Nitrate+Nitrite-N
<2.0
2.0
KM
03/04/2015 12:29
Total Cadmium
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Oc;r rr prirrs rind totters are fnr tlto ','xrhrsn-e and' onitdent;ril use a! vor clients. zinc may nol be rerrnrfur.E>rr rrn vviinio or prui, nor an, z!ny refercirrN be nm..dc
to the 1-vo:k. the rC,culLS, <u't)ut comn,imJ rn.any 1'IGV:'rt,sino. nr:.-v.4z orotherj,u;Irc announcomr_-Ms wilb ul Obtrrntn,..; nt;rhnnro-rnttcn authorrritrnn
SM-2540G
SM-254OG
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 60100
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SM-450ONO3F
SW 6010C
Debbie Holt

Page: 2 of 2
Report Number: 15-062-0205
Account Number: 46477
Submitted By: DREW CULP
Send To: SYNAGRO CENTRAL LLC/OAKBORO
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
� L A&L Eastem Laboratories, Inc.
7621 Whttepine Road Richmond, Virginia 23237 [phone] Fax [phone]
e�
www.aleastem.com
Project: WEST STANLEY WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/2/2015 09:15:00
Lab Number: 60458 Date Received: 03/03/2015 00:00
Sample Id • WS 2015 Date Reported: 03/06/2015
Total Chromium
Total Nickel
40
22
o
5
nfvt
KM
VQIWYfGV lJ I--
03/04/2015 12:29
�••
SW 6010C
Total Lead
Total Arsenic
Total Mercury
Total Selenium
PH (Standard Units)
Total Molybdenum
23
6.0
1.0
6.0
6.60
17
5
3.0
0.4
5.0
2.00
5
KM
KM
KM
KM
JM
KM
03/04/2015 12:29_
03/04/2015 12:29
03/04/2015 09:00
03/04/2015 12:29
03/04/2015 08:15
03/04/2015 12:29
SW 6010C
SW 6010C
SW-7471 B
SW 6010C
SW-9045D
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr "Fe", "P", AND "Se". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Oar tepnns and lrs;!er s .ire fry ;fro .exclusn,o .-ind rnnhdont:al ose of our rrienfs .rnd rrny : r-,l be rrp:ncLlrr N. rn ,:•Hu;e rrp,r nnr rsn, : ury r�! rrnre i�^ rtrraf;
to the work, the rNSu!fs, or the :on'±pany in any ndvrrlrsrnG, news release, or�nnn;rrtrornon!s oll:,rrrnr, q: our pn-�r wnflon :iu!I:ona:rLgn.
Debbie Holt

"LING LOG P A'& L EAQ---'kl
V _ -ICF CUSTODY
7621 W, {�j } Q(}�j j�jl j N ` `! q� osz azo5 ) 8s ANALYSIS
Richman �1fU]I�HIi`illltl�ul�`I�t11�11►'"� 003Z01.5 ECOIW
�n
'OMER: SYNAGRO SOUTHEAST 8041743 S"AGRQCWj'RALL C10A10ORO 12394s
wVss srANLEY'�-TP pling procedures
►ECT MANAGER: -bRyw _ of these samples.
e: (7aq ) s 7 Y- S Z 4 I
SAMPLER
N & L CUSTOMER SAMPUNG SAMPLE # Of SAMPLING METHOD METHOD
.AB # SAMPLE LD. LOCATION TYPE CONTAINERS 'DATE TIME PRESERVED SHIPPED
1Neg¢ Sf4,jJ7 WwnP
6a-2.170 tzars 1N�N' Al G Q i o 02 +�`I.'t5 rc6' cic3e
elinquished by Saritple .
elinquished by:
elinquished by:
aIAL INSTRUCTIONS:
-02--IS
S : ad T-*,,("
Time
1.0
Time
Date Time
Recieved b
Recieved by:
Recieved by:
ANALYSIS REQUEST
WIPLE
[.D. SL1 SL2 XHy N NO3 N .OrgNa* Cd Cr W1 Pb i As Hg Se pH
Total Solids {Moisture), Total Keldahl Nitrogen, Phosphorus, and Potassium.
Basic Test SLI plus Sulfur, Calcium, Magnesium, Sodium, iron; Aluminum. Manganese, Copper and Zinc
White — A & L Canary — MANAGER COPY
REMARKS:
Mo I CI I NOeN
mmm
4

T ' f 9b
a, �� ✓' . J i. �� : y 'f. S L A ,, 1 Y +. 1 C i t .� i I S � 1 :. l 5 1!! l�E
Product Code Product Name' Sample Date ReportRange Ratio
2170-01-LIQ-NC STANLY COUNTY UTIL., NC WEST STANLY 3/2/2015 311/2015-12/3112016 0.6330
WWTP AEROBICALLY DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (3580 x 1.1500) _ 100 = 41.17
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (21600 x 1.1500) _ 100 = 248.4
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3730 x 1.1500) + 100 = 42.895
Na meq = Na mg/I + Molec.Wgt.Na = 41.17 _ 23 = 1.79
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 248.4 + 20 = 12.42
Mg meq = Mg mg/I + Molec.Wgt.Mg = 42.895 _ 12 = 3.57458
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.79 + SgrRoot[0.5(12.42+3.57458)] = 0.632968
Printed: 2/5/2016
Page 1 13:21

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 18.51
SITE #: NC IR 00023 FIELD# : IR 00023 0002 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 32.40 ACRES PERMITTED: 32.40
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/14/15
62,000.00 (G)
1913.580
1.15
0.092
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600.p
2,610.00 p
4,100.00 p
3412
I FESCUE
5115115
99,200.00 (G)
3061.728
1.15
0.147
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600. p
2,610.00 p
4,100.00 p
F23402
I FESCUE
5/16/15
62,000.00 (G)
1913.580
1.15
0.092
SCUWSAE
MOIST
0-<I/2"
SUR
0.5
0.30
62,600. p
2,610.00 p
4,100.00 p
23402
I FESCUE
5/18/15
62,000.00 (G)
1913.580
1.15
0.092
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600. p
2,610.00 p
4,100.00 p
23402
I FESCUE
5119115
43,400.00 (G)
1339.506
1.15
0.064
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
62,600. p
2,610.00 p
4,100.00 p
23402
FESCUE
May-15
328,600.00 (G)
10,141.974
611115
25.00 (CY)
- 0.7721
13.05
0.085
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
68,600. p
11,600.00 p
2.00 p
1 22902
FESCUE
Jun-15
25.00 (CY)
0.772
I
1
Total Gallons/Ac: 10,141.98
IL)LaL%­uei� IUWh�­ U.
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
27
0.006
0.003
0.048
0.379
0.026
0.001
0.019
0.026
0.007
0.896
22.32
Cumulative Ibs/acre
0.136
1 0.297
1 2.421
1 14.799
1 2.837
0.047
0.559
1 1.324
0.163
30.200
Permit PAN Limit (ibs/acre) 1st Crop/2nd Crop
162
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
G .k
f
1339.0
267.9
15.0
375.0
89.0
2500.0
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROBICALLY DIGESTED LIQUII
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
x Z
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2016

NAN—
ArT 31p"r". rz i' .L;i l`'9J afCJ'ih'�';7
March 11, 2015
Drew Culp
Synagro, NC 28134
12701 Lancaster Hwy
Pineville, NC 28134
TEL: [phone]
FAX: [phone]
RE: West Stanly WWTP
Dear Drew Culp:
Summit Environmental Technologies, btc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: httcr:/Amvtv.settek.com
Order No.: 15030093
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/3/2015 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Ptsklr
A'6-� U
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC
E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank)
3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099,
New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma
9940, Oregon OH2O0001, Pennsylvania 68-01335; Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5,
Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West
Virginia 248 and 9957C and E87688, Wisconsin 399013010
Page 1 of 8

NY a Summit Environmental Technologies, bic.
j it [ �, a (,1 , (41- 3310 Win St.
L�_r G RtsllPtEl�hL�d�s Clr5L4 ,iic. Cuyahoga Falls, Ohio44223
l _J r:yu, r r-a Li- TEL: [phone] FAX.- [phone]
Website: httD:/hvwiv.settek.com
CLIENT: Synagro, NC 28134
Project: West Stanly WWTP
Lab SampleID Client Sample ID
15030093-001 West Stanly WWTP 2015
Tag No Date Collected
3/2/2015 9:30:00 AM
Workorder
Sample Summary
WO#: 15030093
11-Mar-15
Date Received Matrix
3/3/2015 10:45:00 AM Sludge
Page 2of8

g E
�; � � � rat � �- jj
SunnnitEnviromnental Technologies, Inc.
Narrative
���NarrativeJ�
3310 Win St.
�P'b's�In�h1h1E'11l1L7E '2a�Lfltit _
Cuyahoga Falls, Ohio44223
WO#: 15030093
TEL: [phone] FAX. [phone]
Date: 3/11/2015
Website: httu:/Avww.settek.cons
CLIENT: Synagro, NC 28134
Project: West Stanly WWTP
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM were performed at Summit Labs 2704 Eatonton Highway Haddock, GA
31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry' designation on the reporting units.
Summit Envirommental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 8

L x
oummmu
Summit Environmental Technologies, Inc.
3310WinSt.S�
tl
Analytical y-}3 eport
s
fN °dIROmmEwrPL'i
ti t 3Lac;1 ,sax ;_
Cuyahoga Falls, Ohio 44223
(base report)
s-.agftit
,T1 ti4-fb rafo;,Iir--s
TEL: [phone] FAX: [phone]
WO#: 15030093
Website: htto:Uwwiv.settek.con:
Date Reported: 3/11/2015
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 3/2/2015 9:30:00 AM
Lab ID: 15030093-OOIA
Project: West Stanly WWTP
Client Sample ID West Stanly WWTP 2015
Analyses Result RL Qual Units DF Date Analyzed
RCI A4500-H+B Analyst: DHC
PH (SM4500-H+ B)
pH 5.49 s.u.@20.4C 1 3/4/2015 10:30:00 AM
Qualifiers: "
Value exceeds Maximum Contaminant Level.
C
Value is below Minimum Compound Limit.
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
U
Samples with CAVA <MDL
Page 4 of 8

Summit Environmental , Inc. Technologies, g
3310WinSt.
WO#:
15030093
Date Reported:
3/11/2015
I
Et"dlft0tIUt 111.Ii7L" 241-'P J0L0r ,: 5, jPtC'.
CzryahogaFalls, Ohio 44223
stir=;;
TEL: [phone] FAX.- [phone]
Company:
Synagro, NC 28134.
Website: huy.-Ilivlviv.settek.con:
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
3/3/2015
Project#:
West Stanly WW
TCLP Metals Analysis (6010)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly WWTP
001
3/2/2015
TCLP Arsenic(As)
0.500
ND mg/L
Sludge
EPA 6010 C
1
5.00
3/5/2015
WK
2015
West Stanly WWTP
001
3/2/2015
TCLP Badum(Ba)
5.00
ND mg/L
Sludge
EPA 6010 C
1
100
3/5/2015
WK
2015
West Stanly WWTP
001
3/2/2015
TCLP Cadmium(Cd)
0.100
ND mg/L
Sludge
EPA 6010 C
1
1.00
3/5/2015
WK
2015
West Stanly WWTP
001
3/2/2015
TCLP Chromium(Cr)
0.200
ND mg/L
Sludge
EPA 6010 C
1
5.00
3/5/2015
WK
2015
West Stanly WWTP
001
3/2/2015
TCLP Lead(Pb)
0.500
ND mg/L
Sludge
EPA 6010 C
1
5.00
3/5/2015
WK
2015
West Stanly WWTP
001
3/2/2015
TCLP Selenium(Se)
0.500
ND mg/L
Sludge
EPA 6010 C
1
1.00
3/5/2015
WK
2015
West Stanly WWTP
001
3/2/2015
TCLP Silver(Ag)
0.500
ND mg/L
Sludge
EPA 6010 C
1
5.00
3/5/2015
WK
2015
TCLP Mercury Analysis (1311n470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
West Stanly WWTP 001 3/2/2015 TCLP Mercury 0.00200 ND mg/L Sludge EPA 7470 A 1 0.200 3/5/2015 ALJ
2015
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly WWTP
001
3/2/2015
Chlordane, total
0.0250
ND mg/L
Sludge
EPA 8081 B
1
0.0300
3/6/2015
AMZ
2015
West Stanly WWTP
001
3/2/2015
Toxaphene
0.0500
ND mg/L
Sludge
EPA 8081 B
1
0.500
3/6/2015
AMZ
2015
West Stanly WWTP
001
3/2/2015
Endrin
0.00250
ND mg/L
Sludge
EPA 8081 B
1
0.0200
3/6/2015
AMZ
2015
West Stanly WWTP
001
3/2/2015
gamma-BHC
0.00250
ND mg/L
Sludge
EPA 8681 B
1
0.400
3/6/2015
AMZ
2015
West Stanly WWTP
001
3/2/2015
Heptachlor
0.00250
ND mg/L
Sludge
EPA 8081 B
1
0.00800
3/6/2015
AMZ
2015
West Stanly WWTP
001
3/2/2015
Heptachlor epoxide
0.00250
ND mg/L
Sludge
EPA 8081 B
1
0.00800
3/6/2015
AMZ
2015
West Stanly WWTP
001
3/2/2015
Methoxychlor
0.00250
ND mg/L
Sludge
EPA 8081 B
1
10.0
3/6/2015
AMZ
2015
Page 5 of 8

Summit EnvironmentalTechnolo Technologies, g
WO#:
15030093
L
�f r' ti7L�5�
f 1
3310Win St.
Date Reported:
3/11/2015
F{',Irtr)11PaiED�P,'ILarL"3;'t'r�Urtdl=`_,v
c;
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Company:
Synagro, NC 28134
Website: htro://iviviv.settek.com
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
3/3/2015
Project#:
West Stanly WW
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly WWTP
001
3/2/2015
1,1-Dichloroethene
0.100
ND mg/L
Sludge
EPA 8260 B
1
0.700
3/5/2015
JCR
2015
West Stanly WWTP
001
3/2/2015
1,2-Dichloroethane
0.100
ND mg/L
Sludge
EPA 8260 B
1
0.500
3/5/2015
JCR
2015
West Stanly WWTP
001
3/2/2015
Benzene
0.100
ND mg/L
Sludge
EPA 8260 B
1
0.500
3/5/2015
JCR
2015
West Stanly WWTP
001
3/2/2015
Carbon tetrachloride
0.100
ND mg/L
Sludge
EPA 8260 B
1
0.500
3/5/2015
JCR
2015
West Stanly WWTP
001
3/2/2015
Chlorobenzene
0.100
ND mg/L
Sludge
EPA 8260 B
1
100
3/5/2015
JCR
2015
West Stanly WWTP
001
3/2/2015
Chloroform
0.100
ND mg/L
Sludge
EPA 8260 B
1
6.00
3/5/2015
JCR
2015
West Stanly WWTP
001
3/2/2015
Tetrachloroethene
0.100
ND mg/L
Sludge
EPA 8260 B
1
0.700
3/5/2015
JCR
2015
West Stanly WWTP
001
3/2/2015
Trichloroethene
0.100
ND mg/L
Sludge
EPA 8260 B
1
0.500
3/5/2015
JCR
5
st Stanly WWTP
001
3/2/2015
Vinyl chloride
0.200
ND mg/L
Sludge
EPA 8260 B
1
0.200
3/5/2015
JCR
__.5
West Stanly WWTP
001
3/2/2015
MEK
2.00
ND mg/L
Sludge
EPA 8260 B
1
200
3/5/2015
JCR
2015
SVOC 8270 TCLP BNA List
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
West Stanly WWTP
001
3/2/2015
1,4-Dichlorobenzene
0.100
ND mg/L
Sludge
EPA 8270 C
1
7.50
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
2,4,5-Trichlorophenol
0.250
ND mg/L
Sludge
EPA 8270 C
1
400
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
2,4,6-Trichlorophenol
0.250
ND mg/L
Sludge
EPA 8270 C
1
2.00
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
2,4-Dinitrotoluene
0.100
ND mg/L
Sludge
EPA 8270 C
1
0.130
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
Cresols, Total
5.00
ND mg/L
Sludge
EPA 8270 C
1
200
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
Hexachloro-1,3-
0.100
ND mg/L
Sludge
EPA 8270 C
1
0.500
3/7/2015
AKE
2015
butadiene
West Stanly WWTP
001
3/2/2015
Hexachlorobenzene
0.100
ND mg/L
Sludge
EPA 8270 C
1
0.130
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
Hexachloroethane
0.100
ND mg/L
Sludge
EPA 8270 C
1
3.00
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
Nitrobenzene
0.100
ND mg/L
Sludge
EPA 8270 C
1
2.00
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
Pentachlorophenol
0.250
ND mg/L
Sludge
EPA 8270 C
1
100
3/7/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
Pyridine
0.250
ND mg/L
Sludge
EPA 8270 C
1
5.00
3/7/2015
AKE
5
Page 6 of 8

t
ssue�mwn3310
Summit Environmental Technologies, Inc.
Win St.
WO#:
15030093
tf
FKVIRONMEN1s1L 9t % b L�tic a <<w
�
Cu)ahogaFalls, Ohio44_23
Date Reported:
3/11/2015
EI
,
ARaf t„ ,
TEL: [phone] FAX.- [phone]
Company:
Synagro, NC 28134
Wehsite: htty.111vwiv.settekcotn
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received: 3/3/2015
Project#: West Stanly WW
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID# Collected Analyse Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
West Stanly WWTP 001 3/2/2015 2,4-D 5.00 ND mg/L Sludge EPA 8321 A 1 10.0 3/6/2015 AMZ
2015
West Stanly WWTP 001 3/2/2015 2,4,5-TP 0.500 ND mg/L Sludge EPA 8321 A 1 1.00 3/6/2015 AMZ
2015
Page 7 of 8

as
C771-
HI I
Summit Environmental Technologies, Inc.
3310 Win St.
VItO#:
15030093
�1
(
CNRIRC) N bl E WmL I E-,- HUOLn ?•_ 4N0
Cuyahoga Falls, Ohio44223
Date Reported:
3/11/2015
AF,H(vf z L:, Im ?ru
TEL: [phone] FAX.- [phone]
Compan y;
Synagro, NC 28134
Website: httn:/hvivw.settek.com
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
3/3/2015
Project#:
West Stanly WW
Client ID#
Lab ID# Collected Analyse
Result Units
Matrix
Method
DF
I2L
Run
Analyst
West Stanly WWTP
001
3/2/2015
Flashpoint (200°F)
>200 °F
Sludge
EPA 1010
1
3/10/2015
TAH
2015
West Stanly WWTP
001
3/2/2015
Total PCBs
ND mg/L
Sludge
EPA 8082
1
0.000200
3/9/2015
AKE
2015
West Stanly WWTP
001
3/2/2015
Cyanide, Reactive
ND ppm
Sludge
EPA 9014
1
0.500
3/4/2015
TIR
2015
West Stanly WWTP
001
3/2/2015
Sulfide, Reactive
ND ppm
Sludge
EPA 9034
1
25.0
3/4/2015
TIR
2015
Page 8 of 8

Rev. 12
Date: 07/27/13
summit Environmental Technologies, Inc.
Cooler Receipt Form
C• Initials of person inspecting COOlf4 and samples 'a C-
Clienl Order IJumher: ji: c� y; l
_. l
❑ate Received: - `� Time,R-ceiveri "3
—�)L�— Date cootE•r(s) OPened and samples inspected:
Number of Cc OIL rs/Boxes:__ _ NIA
Shipper: -ED EY.)JPS DHL Airbofn US Postal Walk-in Pickup Other_ ____ —
Packaging' Peanuts ble%Nra� Paper Foam None O:her.___
T.,pc on cooledboz:
N NA
Custody Seats intact Y N NfPJ IA
C-C-C In plastic
CD N N'A
Blue ice _ present I absent 1 melted NIA
SambleTemperature IRGun *16020.5g CFS 0 `C r'j� ()
-C NIA
Radiological Testing Instrument serial ,"-3512% yNIA
(see page 2 for scan results) i
Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety officer must be notified
Immediately.
C-D-C filled out properiy
N N'A
Samples In sepaiate.bags Y N NIA
Sarrole containers intact' N N1A
�.
'If no, list broken samole(sl:
Sample label(s) complete (ID, date, etc.)
Y
N
NIA
Labe.(s) agree with C-r:)-C
�i
Y
N
N+A
Corect containers used
Y
~y
N
MIA
Sufficient samplereceived
j
N
NIA
Bubbles absent from 40 mL virls"
Y
N
WA
" Samples with bubbles <6mm are acceptable.
Indicate bubble size it>6mm.
Was client contacted about samples
Y N
Will client send new samples
Y N
ClientconIact:_
Logged in by:
(31W. SHARE DIDocument Control Templates - Tra&jrglCooler receipt form Rev, 12 07-27-13.doc Page 1 of 2

ANNUAL, PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: West Stanly WWTP WQ Permit Number: W00016247
WWTP Name: West Stanly WWTP NPDES Number: NC 0043532
Monitoring Period: From 01/01/2015 To 12/31/2015
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirahle to alternative nerformed (Class A or Class B) complete the followinE monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
.Fecal
Coliform
2x10 to the 6th
power per gram
MPN
8,588
13,672
25,153
MPN/g
0
Annual
Grab
SM 9221 E
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench) X
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
'Do norx L-DAUtS , U���iylEs�,reG�o�
P prer Name and Title ( e or print) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

pF PROMPT -ACC. R 'Tr--RrLIAFALF-
LABORA-1-OR.IES, INC
NVNN'%%'TA RLABS.COM
REPORT OF i\NALYSES
Attn: DREW CULP F Al'--11
SYNAGRO. PROJECT N : MAR -5 12701 LANCASTER HWY DATE: 04/10/15
PT NEVILLE, NC 28134
SAMPLE NUMBER- '1117952 SAMPLE ID- WEST STANLY WWTP 50-2170 2015 SAMPLE MA'l'RIX- SO
DATE: SAIMPT..ED- 03/02/15 TIME SAMIPLED- 0925
DATE RECEIVED- 03/02/15 SAMPLER- D,'-- RECFTVED BY- DJ
TTNjE RECEIVED- 1120 DELIVERED BY- DC TYPE SAMPLE- Grab
Page I o f
ANALYSIS
FECAL COLIFORM (GEOM. MEAN)
ANALYSIS
iAETHOD DATE TIME BY RESULT UNITS
SM 9221 E 03/02115 1430 RE < 13,672 MPN/g
j
LA20RATORY DIRECTOR
P.O. Box 411483 - 0wi-lolic, N(' 28241-1 -1 X3
Nione: (704) 588-,,333 - I`.tx: (70-1) 58',35-8335
F 7

P "i
1,7 FZ
PROMPT•ACCURATE • RELIABLE
LABORATORIES., INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
-
®
r
•
SYNAGRO
WEST STANLEY WWTP 50-2170 2015
03/02/15
FECAL COLIFORM, GEOMETRIC MEAN
SM 9221 E
< 12,618.11
< 12,618.11
117952
1
< 146
1.16%
2
143
1.17%
12,190.86
3
110
1.16%
9,515.11
4
100
1.16%
8,588.23
5
< 185
1.15%
< 16,052.52
6
< 208
1.18%
< 17,596.71
7
< 294
1.17%
< 25,153.06
Fecal��oR�'orrrl'
eo etrc'1►�ien _13,672

[RAR CHAIN OF CUSTODY
r1,so,R,voa,Es,/Pic. PAR Laboratories, Inc
Phone [phone]
www.parlabs.com Fax [phone]
Shipping: Mailing:
2217 Graham Park Drive PD Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc and the North
k-.aruuna ueparnuent ur r=nvuunmemai dnu rvawrdi musuurces.
Company Name (billing)
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State Et zip code
PINEVILLE NC 28134
Point of Contact tz Telephone Number
DREW CULP 704-574-5291
Comments/ Special Instructions
Sample
Taken By: SIGNATURE �I---, _�-�---�J PRINTED NAME1�
ARE SAMPLES FOR STATE or EPA REPORTING? YES __NO
"Sample Type: DW _ WW GWMW HW Soil Other l?o osa I•�6_
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No _ n/a _
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (Y/N):
Client Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
DaterTime
Collection
Daterrime
nalyses
Requested —
We-sf- 5t&n I WV/777'
a-0 iS
r`C'
o3-oL—rS
09a-S
L r�GA-1-- cot/for
CS
Relinquished
Re tnquished by: Dateffime Received by: t Daterrime 1
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste "See
Other Side

p AIL
PROMPT• A CC.0 RATE• RCl_IAMI-E
LA130I.A.T0I2TES, INC
11'11'WI'AItLABS.00.11
REPORT OF ANALYSES
Attn: DREW CULP
SYNAGRO
12701 LANCASTER HWY
PINT VILLE, NC 281 ;'-
PROJECT NAME: MAR 15
DATE: 04/10/ 15
SAMPLE NUMBER-- 1 17951 SAMPLE ID- `,d ST STANLY WR'J'PP 50- 2170 2015 SAMPLE MATRIX- SC
DATE SAMPLED- 03/02./15 TIME: SAMPLED- 0930
DATE RECEIVED- 03/02./15 SAMPLER- DC RECEIVED BY- DJ
TIME RECEIVED- 1120 DELIVERED BY- DC TYPE SAMPLE Grab
Page 1 or 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCE SCALE TEST VAR 031104/15 RE ATTACHED
LA} ORATORY DIRECTOR
F..__Iiox 411453 • Chadollc, iN 282:I~1-1483 --- -
Phone: [phone] Pax: (70.1) SS ;-5335

Aft
RAA R'
PROM PT•ACOU RATE• RELIA6 LE
I ABOR.ATOPIES, INC
WWW.PAPLABS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
•1 j
SYNAGRO
WEST STANLEY WWTP 50-2170 2015
1 -
117951
-
r
03/04/15
04/01115
Start: End:
TS
0.1602
0.1643
TS%
1.16%
1.15%
VS
0.1125
0.1135
VS%
70.22%
69.08%
yIN
0.003513
yOUT
0.00349304
FSVR (Mass Balance)
0.57%
FSVR (Van Kleeck)
5.27%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box411483 o Charlotte, NC 28241-1483
Phone: [phone] a Fax: [phone]

[RAR CHA OF CUSTODY
L,LaoR.troRfes.1NC. PAR Laboratories, Inc
Phone [phone]
wwmparlabs.com Fax [phone]
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc and the North
Garoiina uepanmenl ul Cnvuu-ntllnd, auu 1-1-oi-
Company Name (billing)
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State Er zip code
PIN_EVILLE NC 28134
Point of Contact @ Telephone Number
DREW CULP 704-574-5291
Sample
Taken By: SIGNATURE
Comments/ Special
Instructions
ClC4riA'`e,, �441aen 4-
Pf0 v,de-J /'i e-
van/¢- 50
bell w
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES x NO
`Sample Type: DW WW GWMW HW Soil Other Bi'sa/'J
Sample Temp at time of sampling: _ ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes —No _ n1a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (Y/N):
Client Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date rime
Collection l
Date/Time
II
nalyses
Requested
6Ve-5-f .51'4-1 fWwT?0
X
- o-/s
offa
09 - 30
3o - DA4 Y
5-0 - Lj 7a�/S
flofo/Tima
tiennquisneu uy: —1— 71_
,;Imquished by ate ime Received by: / DateTfime
' C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well IiW=Hazardous Waste "See
Other Side

Liming was not necessary, as the field pH value was 6.0 or greater.

NCDA&CS nomic Division Phone: [phone]
Website: www.
gov/agronomil
ReportNo. FY )36293
+;,ti
Predictive
Client: Shane Porter
351 Gantt Horn Rd.
Advisor:
Synagro Central
Attn:Eric Thompson
F'I
EfU Ia�
Statesville, NC 28677
284 Boger Rd
�}
l`-?+
Mehlich-3
�ilReport
Extraction
Sampled County Iredell
Mocksville, NC 27028
P.
Sampled: 05/01/2015 Received: 06/19/2015
Completed: 06/29/2015
Farm: IR-23
Links to Helpful Information
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, 0.0
120-200 0
0 0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cd; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 ' Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.51 0.79
15.4 89 1.8 6.0 292 129
68 17
49 339 220 220
950
950
403
0.1 1
Sample ID: 5.
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
0
0
0
0
Note: 12
2-Fescue/OGrass/Tirn, 0.0
120-200 0
0 0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/crrt3; CEC and Na in meq/100 crtr3; NO3-N in mg/dnt ]:
Soil Class:
Mineral
HM% WIV
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-1 Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.46 0.84
15.0 89 1.7 5.9 377 138
69 15
48 222 150 150
637
637
338
0.0
North Carolina
' �S?li;iCOP �iU>i (Ufuil {..itityldi�SSi{�i9
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&C,c nomic Division Phone: [phone] Website: www -.gov/agronomi/ Report No. FY 036293
Shane Porter Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/acironomi/obpart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to For
Test Results
The first seven values [soil class, HM%, WA/, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS-1, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagrgov/agronomi/uyrsthtm
for more information.
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter I
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS -I
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index