WQ0016247_Regional Office Historical File Pre 2018 (12)

Schutte, Maria
From: Schutte, Maria
Sent: Friday, June 08, 2018 8:20 PM
To: 'Robert Roth'
Cc: '[e-mail]'; 'Erik Bruce'; Gregory, Sonia; Doby, Troy; Pitner, Andrew
Subject: RE: [External] RE: WQ0016247 Synagro Western Piedmont Regional-2017 Annual Report
Additional Information Request
Hello Note,
I just copied you on a response to Charlotte Water, as I made a similar inquiry for new land they applied to last year; and,
received the same comments/concerns you relayed to me.
Based on your responses and my additional reading (which I will detail in a separate email on the topic of CPLRs), I have no
further questions related to the referenced annual report.
Sincerely,
Maria Schutte
From: Schutte, Maria
Sent: Wednesday, May 02, 2018 11:19 AM
To:'Robert Roth' <[e-mail]>
Cc: '[e-mail]' <[e-mail]>; Erik Bruce <[e-mail]>; Gregory, Sonia
<[e-mail]>; Doby, Troy <[e-mail]>; Pitner, Andrew <[e-mail]>
Subject: RE: [External] RE: WQ0016247 Synagro Western Piedmont Regional-2017 Annual Report Additional Information
Request
Good Morning Nate,
Per our phone conversation last night, your response for the "ESP" is acceptable for this report, but future soils results will be
presented in -line with NCDA specifications. I just spoke with Troy Doby in our Central Office concerning the baseline metals
question. Troy and I agree that when we have total metals results for a new field, that baseline should be included in the CPLRs
for that field.
I would request you first verify you have total metals data for the new fields, if not, reply as such and that will serve as the
response for this inquiry. We do NOT intend to request additional sampling, just will note the oversight on our part for future
land addition. Otherwise, please include the baseline metals history in the CPLR totals and email me the updated forms, ONLY if
the resulting totals dictate updates are necessary.
Thank you and please call should you have further questions,
Maria (704-235-2184)
From: Robert Roth [mailto:[e-mail]]
Sent: Tuesday, May 01, 2018 3:13 PM
To: Schutte, Maria <[e-mail]>
Subject: [External] RE: WQ0016247 Synagro Western Piedmont Regional-2017 Annual Report Additional Information Request
V�Fr.�Jo' r 7 L "�s f,° �7{ s r C u ^fit .,.^�±�r r m rr ^ f" t,. , n s l r, ° !' i' c t i���0 G L S X3�71.
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Maria,
Hope all is well. I will be the primary contact for this permit. To address each item:

Waypoint analytical reports "ESP" as Na % under percent base saturation. The items are interchangeable and
mean the same thing. However, if you request I can have the lab report rewritten to mirror the NCDA specs.
(Waypoint has already tested for the parameters).
To date CPLRs have not used heavy metals concentrations as a baseline. It has been interpreted in the past that
heavy metals samples will be pulled to insure the fields do not have concentrations above the permitted limits.
Once permitted, the cumulative concentrations have been calculated each year to account for the applied
residuals. I have reviewed the state and EPA requirements that are somewhat loosely constructed and do not
feel they instruct to use the heavy metals results as a baseline. I feel a better approach would be monitoring the
soil reports and cumulative CPLRs (as they are now) to predict when an issue may arise.
Please let me know your thoughts.
Nate
From: Schulte, Maria[mailto:[e-mail]]
Sent: Tuesday, May 01, 2018 11:31 AM
To: Todd Larson
Cc: Robert Roth; Erik Bruce; Gregory, Sonia
Subject: WQ0016247 Synagro Western Piedmont Regional-2017 Annual Report Additional Information Request
Mr. Larson,
I have addressed this item to you, since you signed as permittee on the Annual Land Application Certification form; however, our
data base shows Nate Roth as having signature authority. Please clarify, so we may update our data base accordingly. In
addition, Mr. Roth is currently listed as the ORC and Erik Bruce the BU-ORC.
This email will serve as the Acknowledgement of Receipt of the 2017 Annual Report for the referenced residuals permit. A
report copy was received in the Mooresville office on March 5th, 2018. Upon review, the following additional information is
requested:
Please send calculations/results for, or request an amended Soils Report from your contract lab to include, the
Exchangeable Sodium Percentage (ESP) parameter in accordance with permit condition IV.S. of your permit (copied
below for your convenience), for each field affected. It is the permittees responsibility to ensure all parameters are
sampled, requested on the COC and reported as required, including the appropriate units of measure, in -line with the
North Carolina Department of Agriculture and Consumer Services recommendations.
Recalculate cumulative pollutant loading rates to include baseline metals for any new field land applied and email the
updated Field Summary Forms; Or, explain why this is unnecessary (ex: data conversion results in numbers outside
the current 3 decimal ("0.000" lbs/acre), significant figures reported). I only reviewed field NC-AL-00013-0001A, but
did not locate a baseline metals analysis iri my copy of the permit modification.
Please email the requested information to me or contact me with any questions.
Sincerely,
Maria Schutte

5Pvi annual. representative soils analysis (i.e., Standard Soil Fertility Analysis) shall. be conducted on
each land application site listed in Attachment B on which a residuals land application event will occur
in the respective calendar year. This analysis shall be in accordance with the "Guidanee on Soil
Sampling" located in the Sampling Instructions Section of the NC Department of Agriculture &
consumer Services' website The Permittee shall maintain
these results and a description of t-hesampling methodologies used to determine soil fertility for a period
of no less than five years, and.diall be made available to the Division upon request. At a minimum, the
Stand,ud Soil Fertility Analysis shall include the following parameters -
Acidity
Exchangeable Sodium Percentage
Phosphorus
Base Saturation (by calculation)
Magnesium
Potassium
Calcium
Manganese
Sodium
Cation Er change Capacity
Percent Humic. Nlatter
Zinc
Copper
PH
I 5A NC AC 02T .01 0.8(c), 15 A CAC 02T . ll t I (d))
Maria Schuffe
Environmental Specialist
Water Quality Regional Operations Section
Division of Water Resources
North Carolina Department of Environmental Quality
704 663 1699 office
704 235 2184 direct
Maria. sch ufte(5-ncdenr.gov
610 East Center Avenue
Suite 301
Mooresville, NC 28115
�" Nothing Comparcs.—%--,-
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

RECEIVED/NDDENRiDWR
WQRQS,
MOORESVILLE PEt3lC7r`IAL OFFICE
Western Piedmont Regional, NC
Class B Residuals Land Application Program
Permit No. WQ0016247
2017 ANNUAL REPORT
WWI

Western Piedmont Regional, NC
Class B Residuals Land Application Program
2017 Annual Report
TABLE OF CONTENTS
1. Certification Form
2. City of Statesville
3. Stanly County Utilities
4. Town of Columbus

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00016247 County Alexander Year 2017
Facility Name (as shown on permit) West Stanly WWTP, City of Statesville, Third Creek WWTP, Fourth Creek WWTP, Columbus
WWTP, Granite Falls WWTP, & Granite Falls WTP NPDES No. NC0043532, NC0020591, NC0031836, NC0021369,
NC0021890, & NCO082546
Land Application Operator Snagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 55
Total number of fields utilized for land application during the year: 14
Total amount of dry tons applied during the year for all application sites: 437.42
Total number of acres utilized for land application during the year: 204.8
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2017 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Todd Larson, Operations Director
Permittee Name and Title (type or print)
Signatur Of Permittee I 1
Signature of Preparer* Date Signature of Land Applier ,
(if different from Permittee) (if different from Permittee and Preparl,
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF,

2017 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
STATESVILLE, NC
STATESVILLE, NC FOURTH CREEK CAKE
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
April 2017
905.00 Y
1,15.01
D
December 2017
340.00 Y
40.32
D
YEARLY TOTAL
1,245.00 Y
155.33
D
STATESVILLE, NC THIRD CREEK CAKE
MONTHNEAR
April 2017
December 2017
YEARLY TOTAL
AMOUNT UNIT
795.00 Y
160.00 Y
955.00 Y
DRY TONS
UNIT
93.47
D
18.81
D
112.28
D
DRY METRIC
TONS
104.32
36.57
140.89
DRY METRIC
TONS
84.78
17.06
101.84
2/1 /2018

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type
CisK
CAx
CAx
Date Sampled (grab) or 01/04/17
04/10/17
10/04/17
Date Composited
Percent Solids
13.90
15.09
14.08
PARAMETERS (mg/kg dry weight)
Arsenic
4.72
4.32
3.13
Cadmium
3.37
5.13
2
Mercury
1.15
<0.4
0.601
Chromium
37.9
60.8
35.1
Copper
266
261
242
Lead
20
35.2
18.9
Molybdenum
10.7
11.7
9.9
Nickel
25
26.5
19.5
Selenium
6.58
<5
<5
Zinc
642
579
307
Total Phosphorus
25900
21600
23600
TKN
53400
57200
48800
Ammonia -Nitrogen
4740
10100
9510
Nitrate and Nitrite
40.1
<2. 03
<2. 39
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significanIenAes for submitti7g fAe information, including the possibility of fines and imprisonment for knowing violations."
X VZ Y& ( U(i(f_NL Date ! vtvi V
(SIGNATU E OF PREPARER)
DENR FORM RSSF (5/2003) Printed: Thursday - February 1, 2018 at 11:54:32 for: 2084 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
WQ0016247
Facility Name
STATESVILLE, NC
NPDES#
NCO031836
or WQ# (residual only)
WWTP Name
FOURTH CREEK
Residual Analysis Data
Product Type
CAK
CAK
CAK
Date Sampled
01/04/17
04/10/17
10/04/17
Date Composited
Percent Soilds
13.90
15.09
14.08
PARAMETERS (mg/kg dry weight)'
Aluminium
31200
16900
22700
Calcium
8830
14800
3440
Magnesium
2490
2280
1160
pH
6.65
8.23
5.11
Potasium
3480
3000
1770
Sodium
669
876
311
PAN
17008
19182
16544
SAR
0.602003
0.686111
0.437766
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure tha ual' d personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitti als i formation, includpg le possibility of fines and imprisonment for knowing violations."
X Date
(SI NATURE F PREPARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/6/2018 1:39:49 PM

Page: 1 of 2
Report Number: 17-006-0208
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61533
Sample Id : Statesville 4th Creek
D
Waypoin(t,M
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OF ANALYSIS Date Sampled: 1/4/2017 13:15:00
Date Received: 01/06/2017 00:00
Date Reported: 01/13/2017
Total Solids *
13.90
139000
100.0
BW1
01/06/2017 15:00
SM-2540G
Moisture *
86.09
100.0
BW1
01/06/2017 15:00
SM-2540G
Total Kjeldahl Nitrogen
5.34
53400
10.0
SJB
01/12/2017 09:00
SM-4500-NH3C-TKN
Total Phosphorus
2.59
25900
100
JTR
01/10/2017 21:03
6010C
Total Potassium
0.35
3480
1000
JTR
01/10/2017 21:08
6010C
Total Sulfur
0.65
6460
100
JTR
01/10/2017 21:03
6010C
Total Calcium
0.88
8830
100
JTR
01/10/2017 21:03
6010C
Total Magnesium
0.25
2490
100
JTR
01/10/2017 21:03
6010C
Total Sodium
0.07
669
100
JTR
01/10/2017 21:03
6010C
Total Iron
22600
100
JTR
01/10/2017 21:03
6010C
Total Aluminum
31200
100
JTR
01/10/2017 21:03
6010C
Total Manganese
2260
5.00
JTR
01/10/2017 21:03
6010C
Total Copper,
266
5.00
JTR
01/10/2017 21:03
6010C
Total Zinc
642
5.00
JTR
01/10/2017 21:03
6010C
Ammonia Nitrogen
0.47
4740
10.0
SJB
01/09/2017 09:55
SM-4500-NH3C
Organic N
4.87
48660
10.0
01/09/2017 09:55
CALCULATION
Nitrate+Nitrite-N
40.1
1.98
SJB
01/11/201714:02
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
Debbie Holt
Laboratory Supervisor

Page: 2 of 2
Report Number: 17-006-0208
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61533
Sample Id : Statesville 4th Creek
Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OFAMALYSIS Date Sampled: 1/4/2017 13:15:00
Date Received: 01/06/2017 00:00
Date Reported: 01/13/2017
Total Cadmium
3.37
2.00
JTR
01/10/2017 21:03
6010C
Total Chromium
37.9
5.00
JTR
01/10/2017 21:03
6010C
Total Nickel
25.0
5.00
JTR
01/10/2017 21:03
6010C
Total Lead
20.0
5.00
JTR
01/10/2017 21:03
6010C
Total Arsenic
4.72
3.00
JTR
01/10/2017 21:03
6010C
Total Mercury
1.15
0.400
JM
01/12/2017 13:00
SW-7471B
Total Selenium
6.58
5.00
JTR
01/10/2017 21:03
6010C
pH (Standard Units) *
6.65
1.00
SJB
01/09/2017 09:55
SW-9045D
Total Molybdenum
10.7
5.00
JTR
01/10/2017 21:03
6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 1/4/2017 1/1/2017-313112017 0.6020
Na mg/I = (Na mg/kg x % Solids) + 100 = (669 x 13.9000) + 100 = 92.991
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (8830 x 13.9000) _ 100 = 1227.37
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2490 x 13.9000) _ 100 = 346.11
Na meq = Na'mg/I = Molec.Wgt.Na = 92.991 - 23 = 4.04309
Ca meq = Ca mg/1 = Molec.Wgt.Ca = 1227.37 _ 20 = 61.3685
Mg meq = Mg mg/1= Molec.Wgt.Mg = 346.11 _ 12 = 28.8425
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.04309 _ SgrRoot[0.5(61.3685+28.8425)] = 0.602003
Printed: 2/1/2018
Page 1 12:02

Page: 1 of 2
Report Number: 17-101-0204
Account Number: 46493
Submitted By: Erik Bruce
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
•
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OFANALYSIS
Date Sampled: 4/10/2017 08:30:00
Lab Number: 63307
Date Received:
04/11/2017 00:00
Sample Id : Statesville 4th Creek
Date Reported:
04/17/2017
RESULT
RESULT
QUANTITATION LIMIT
ANALYSISMETHOD
PARAMETER
N
.
D,
Total Solids *
15.09
150900
100.0
JM
04/11/2017 15:40
SM-2540G
Moisture *
84.90
100.0
JM
04/11/2017 15:40
SM-254OG
Total Kjeldahl Nitrogen
5.72
57200
50.0
JM
04/12/2017 09:55
SM-4500-NH3C-TKN
Total Phosphorus
2.16
21600
100
MOS
04/13/2017 11:52
6010C
Total Potassium
0.30
3000
100
MOS
04/13/2017 11:52
6010C
Total Sulfur
0.78
7770
100
MOS
04/13/2017 11:52
6010C
Total Calcium
1.48
14800
100
MOS
04/13/2017 11:52
6010C
Total Magnesium
0.23
2280
100
MOS
04/13/2017 11:52
6010C
Total Sodium
0.09
876
100
MOS
04/13/2017 19:23
6010C
Total Iron
17800
100
MOS
04/13/2017 11:52
6010C
Total Aluminum
16900
100
MOS
04/13/2017 19:23
6010C
Total Manganese
1420
5.00
MOS
04/13/2017 11:52
6010C
Total Copper
261
5.00
MOS
04/13/2017 11:52
6010C
Total Zinc
579
5.00
MOS
04/13/2017 11:52
6010C
Ammonia Nitrogen
1.01
10100
50.0
JM
04/12/2017 10:00
SM-4500-NH3C
Organic N
4.71
47100
50.0
04/12/2017 09:55
CALCULATION
Nitrate+Nitrite-N
<2.03
2.03
SJB
04/14/201714:59
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made ,
to the work, the results, or the company in any advertising,, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Page: 2 of 2
Report Number: 17-101-0204
Account Number: 46493
Submitted By: Erik Bruce
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 63307
Sample ld : Statesville 4th Creek
Waypdlont(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
NC Cert#257
REPORT OFANALYSIS Date Sampled: 4/10/2017 08:30:00
Date Received: 04/11/2017 00:00
Date Reported: 04/17/2017
Total Cadmium
5.13
2.00
MOS
04/13/2017 11:52
6010C
Total Chromium
60.8
5.00
MOS
04/13/2017 11:52
6010C
Total Nickel
26.5
5.00
MOS
04/13/2017 11:52
6010C
Total Lead
35.2
5.00
MOS
04/13/2017 11:52
6010C
Total Arsenic
4.32
3.00
MOS
04/13/2017 11:52
6010C
Total Mercury
<0.400
0.400
SJB
04/17/2017 11:03
SW-7471 B
Total Selenium
<5.00
5.00
MOS
04/13/2017 11:52
6010C
pH (Standard Units) *
8.23
1.00
JM
04/12/2017 09:55
SW-9045D
Total Molybdenum
11.7
5.00
MOS
04/13/2017 11:52
6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
I ,r
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 4/10/2017 4/l/2017-6/30/2017 0.6861
Na mg/1 = (Na mg/kg x % Solids) _ 100 = (876 x 15.0900) = 100 = 132.188
Ca mg/1 = (Ca mg/kg x % Solids) _ 100 = (14800 x 15.0900) + 100 = 2233.32
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2280 x 15.0900) _ 100 = 344.052
Na meq = Na mg/I = Molec.Wgt.Na = 132.188 = 23 = 5.74732
Ca meq = Ca mg/I = Molec.Wgt.Ca = 2233.32 = 20 = 111.666
Mg meq = Mg mg/I = Molec.Wgt.Mg = 344.052 t- 12 = 28.671
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.74732 _ SgrRoot[0.5(111.666+28.671)] = 0.686111
Printed: 2/1 /2018
Page 1 12:03

Page: 1 of 2
Report Number: 17-278-0211
Account Number: 46493
Submitted By: Erik Bruce
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 56512
Sample Id : Statesville 4th Creek
(2)
WaypRintAYTICAL .
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
REPORT OF ANALYSIS Date Sampled: 10/4/2017 08:00:00
Date Received: 10/05/2017 00:00
Date Reported: 10/12/2017
Total Solids *
14.08
140800
100.0
R D
10/05/2017 14:50
SM-2540G
Moisture *
85.91
100.0
R D
10/05/2017 14:50
SM-254OG
Total Kjeldahl Nitrogen
4.88
48800
50.0
R D
10/06/2017 08:40
SM-4500-NH3C-TKN
Total Phosphorus
2.36
23600
100
MOS
10/10/2017 14:12
6010C
Total Potassium
0.18
1770
100
MOS
10/10/2017 14:12
6010C
Total Sulfur
0.66
6600
100
MOS
10/10/2017 14:12
6010C
Total Calcium
0.34
3440
100
MOS
10/10/2017 14:12
6010C
Total Magnesium
0.12
1160
100
MOS
10/10/2017 14:12
6010C
Total Sodium
0.03
311
100
MOS
10/10/2017 14:12
6010C
Total Iron
19900
100
MOS
10/10/2017 14:12
6010C
Total Aluminum
-
22700
100
MOS
10/10/2017 14:12
6010C
Total Manganese
849
5.00
MOS
10/10/2017 14:12
6010C
Total Copper
242
5.00
MOS
10/10/2017 14:12
6010C
Total Zinc
307
5.00
MOS
10/10/2017 14:12
6010C
Ammonia Nitrogen
0.95
9510
50.0
R D
10/06/2017 08:40
SM-4500-NH3C
Organic N
3.93
39290
50.0
10/06/2017 08:40
CALCULATION
Nitrate+Nitrite-N
<2.39
2.39
SJB
10/10/201714:57
4500NO3F-2011
All values are on a dry weight
basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
?OfZ4
#IC 60wr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in
whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 17-278-0211
Account Number: 46493
Submitted By: Erik Bruce
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 56512
Sample Id : Statesville 4th Creek
(2)
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Project : Statesville 4th Creek
REPORT OF ANALYSIS Date Sampled: 10/4/2017 08:00:00
Date Received: 10/05/2017 00:00
Date Reported: 10/12/2017
Total Cadmium
2.00
2.00
MOS
10/10/2017 14:12
6010C
Total Chromium
35.1
5.00
MOS
10/10/2017 14:12
6010C
Total Nickel
19.5
5.00
MOS
10/10/2017 14:12
6010C
Total Lead
18.9
5.00
MOS
10/10/2017 14:12
6010C
Total Arsenic
3.13
3.00
MOS
10/10/2017 14:12
6010C
Total Mercury
0.601
0.400
SJB
10/10/2017 14:24
SW-7471B
Total Selenium
<5.00
5.00
MOS
10/10/2017 14:12
6010C
pH*
5.11
1.00
R D
10/06/2017 08:40
SW-9045D
Total Molybdenum
9.90
5.00
MOS
10/10/2017 14:12
6010C
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made pori4 Kc 60wr
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 10/4/2017 1011/2017-12/3112017 0.4378
Na mg/1= (Na mg/kg x % Solids) - 100 = (311 x 14.0800) _ 100 = 43.7888
Ca mg/1= (Ca mg/kg x % Solids) _ 100 = (3440 x 14.0800) _ 100 = 484.352
Mg mg/I = (mg mg/kg x % Solids) + 100 = (1160 x 14.0800) _ 100 = 163.328
Na meq = Na mg/1 = Molec.Wgt.Na = 43.7888 _ 23 = 1.90386
Ca meq = Ca mg/1 = Molec.Wgt.Ca = 484.352 _ 20 = 24.2176
Mg meq = Mg mg/1 = Molec.Wgt.Mg = 163.328 _ 12 = 13.6107
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.90386 _ SgrRoot[0.5(24.2176+13.6107)] = 0.437766
Printed: 2/1/2018
Page 1 12:03

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO020591
or WQ# (residual only)
WWTP Name: THIRD CREEK
Residuals Analysis Data
Product Type CAx
Date Sampled (grab) or 01/04/17
Date Composited
Percent Solids 13. 96
PARAMETERS (mg/kg dry weight)
Arsenic
3.34
Cadmium
13.2
Mercury
<0.4
Chromium
141
Copper
327
Lead
84.6
Molybdenum
19.4
Nickel
53.3
Selenium
6.87
Zinc
1020
Total Phosphorus
16300
TKN
43100
Ammonia -Nitrogen
2 650
Nitrate and Nitrite
159
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant en ties for submittin false information, including the possibility of fines and imprisonment for knowing violations."
X r
Date
(SIGNAT RE OF PREPARER)
DENR FORM RSSF (5/2003) Printed: Thursday - February 1, 2018 at 11:54:45 for: 2084 02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
Facility Name
NPDES#
or WQ# (residual only)
WWTP Name
Residual Analysis Data
WQ0016247
STATESVILLE, NC
NC0020591
THIRD CREEK
Product Type CAK
Date Sampled 01/04/17
Date Composited
Percent Solids 13.96
PARAMETERS (mg/kg dry weight)'
Aluminium
14400
Calcium
14300
Magnesium
3280
pH
6.61
Potasium
3490
Sodium
1310
PAN
13619
SAR
0.957303
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure th t qualied personnel properly thered and evaluated the information submitted. I am aware that there are significant penalties for
submitti fals nformati includNig t possibility of fines and imprisonment for knowing violations."
X f
f, Date
(SI NATURE F PREPARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/6/2018 1:51:55 PM

Page: 1 of 2
Report Number: 17-006-0207
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61532
Sample Id : Statesville 3rd Creek
D
Waypoin(t,M
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 3rd Creek
NC Cert#257
REPORT OFANALYSIS Date Sampled: 1/4/2017 13:00:00
Date Received: 01/06/2017 00:00
Date Reported: 01/13/2017
Total Solids '
13.96
139600
100.0
BW1
01/06/2017 15:00
SM-2540G
Moisture *
86.03
100.0
BW1
01/06/2017 15:00
SM-2540G
Total Kjeldahl Nitrogen
4.31
43100
10.0
SJB
01/12/2017 09:00
SM-4500-NH3C-TKN
Total Phosphorus
1.63
16300
100
JTR
01/10/2017 20:54
6010C
Total Potassium
0.35
3490
1000
JTR
01/10/2017 20:59
6010C
Total Sulfur
0.79
7930
100
JTR
01/10/2017 20:54
6010C
Total Calcium
1.43
14300
100
JTR
01/10/2017 20:54
6010C
Total Magnesium
0.33
3280
100
JTR
01/10/2017 20:54
6010C
Total Sodium
0.13
1310
100
JTR
01/10/2017 20:54
6010C
Total Iron
18900
100
JTR
01/10/2017 20:54
6010C
Total Aluminum
14400
100
JTR
01/10/2017 20:54
6010C
Total Manganese
593
5.00
JTR
01/10/2017 20:54
6010C
Total Copper
327
5.00
JTR
01/10/2017 20:54
6010C
Total Zinc
1020
5.00
JTR
01/10/2017 20:54
6010C
Ammonia Nitrogen
0.27
2650
10.0
SJB
01/09/2017 09:55
SM-4500-NH3C
Organic N
4.04
40450
10.0
01/09/2017 09:55
CALCULATION
Nitrate+Nitrite-N
159
2.00
SJB
01/11/201714:01
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ,
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Page: 2 of 2
Report Number: 17-006-0207
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 3rd Creek
NC Cert#257
REPORT OF ANALYSIS Date Sampled: 1/4/2017 13:00:00
Lab Number: 61532 Date Received: 01/06/2017 00:00
Sample Id : Statesville 3rd Creek Date Reported: 01/13/2017
Total Cadmium
Chromium
L13.2Total
Total Nickel
53.3
Total Lead
84.6
Total Arsenic
3.34
Total Mercury
<0.400
Total Selenium
6.87
pH (Standard Units) *
6.61
Total Molybdenum
19.4
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
2.00
JTR
01/10/2017 20:54
6010C
5.00
JTR
01/10/2017 20:54
6010C
5.00
JTR
01/10/2017 20:54
6010C
5.00
JTR
01/10/2017 20:54
6010C
3.00
JTR
01/10/2017 20:54
6010C
0.400
JM
01/12/201713:00
SW-7471B
5.00
JTR
01/10/2017 20:54
6010C
1.00
SJB
01/09/2017 09:55
SW-9045D
5.00
JTR
01/10/2017 20:54
6010C
asis except as noted by asterisk. Detection limit on all N series is on a wet basis.
ntial use of our clients, and may not be reproduced in whole or part nor may any reference be made
ng, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 1/4/2017 111/2017-12131/2017 0.9573
Na mg/I = (Na mg/kg x % Solids) = 100 = (1310 x 13.9600) - 100 = 182.876
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (14300 x 13.9600) = 100 = 1996.28
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3280 x 13.9600) = 100 = 457.888
Na meq = Na mg/I - Molec.Wgt.Na = 182.876 - 23 = 7.95113
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 1996.28 _ 20 = 99.814
Mg meq = Mg mg/I = Molec.Wgt.Mg = 457.888 _ 12 = 38.1573
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.95113 - SgrRoot[0.5(99.814+38.1573)] = 0.957303
Printed: 2/1 /2018
Page 1 12:15

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
�-CILITYNAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: PACOLET
VNER: ARLENE MILLSAPS PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 18.81
rE #: NC AL 00013 FIELD# : AL 00013 0001 A OPERATOR: DANNY MILLSAPS CATION EXCHANGE CAPACITY (NON-503):
"sSIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 14.70 ACRES PERMITTED: 14.70
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
SATE or
dONTH
Total
Per Acre
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TIN
Nitrogen
and
(ppm)
Crop
[2/28/17
160.00 (CY)
10.884
13.96
1.280
STTCC
MOIST
0- 1/2"
SUR
0.5
0.30
43,100. p
2,650.00 p
159.00 p
13619
FESCUE PASTURE
Dec-17
160.00 . (CY)
10.884
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
nnual lbs/acre
35
0.009
0.034
0.361
0.837
0.217
0.001
0.050
0.136
0.018
2.611
41.72
emulative lbs/acre
0.009
0.034
0.361
0.837
0.217
0.001
0.050
0.136
0.018
2.611
rmit PAN Limit (lbs/acre) 1st Crop/2nd Crop
:' ' 3
�:
�;
{
;��;
r
!
- I
J;
D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
CTCC = STATESVILLE, NC THIRD CREEK CAKE
X
(SIGNA T' "—
AVI
,AND APPLIER) DATE
Ity of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
Fion submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
t Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

FACILITY NAME: STATES VILLE, NC
OWNER: ARLENE MILLSAPS
SITE #: NC AL 00013 FIELD# : AL 00013 0001 B
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 40.32
OPERATOR: DANNY MILLSAPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 15.10 ACRES PERMITTED: 15.10
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
DATE or
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
12n1I7
340.00 (CY)
22.517
14.08
2.670
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
48,800. p
9,510.00 p
2.39 p
16544
Dec-17
340.00 (CY)
1 22.517
1
IFESCUEPASTURE
'P..4..1 n. :_ --A _.
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
gg
0.017
0.011
0.187
1.292
0.101
0.003
0.053
0.104
0.027
1.639
126.03
Cumulative lbs/acre
0.017
0.011
0.187
1.292
0.101
0.003
0.053
0.104
0.027
1.639
1 a
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
162
m
a
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
i '
1339.0
267.9
15.0 ; ._, 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X l
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
iWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 101.04
ITE #: NC IR 00023 FIELD# : IR 00023 0002 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
.ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 32.40 ACRES PERMITTED: 32.40
Page
Lune Applied ***
Date:T
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
THIN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
4/10/17
535.00 (CY)
16.512
15.09
2.099
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
57,200. p
10,100.00 p
2.03 p
19182
I FESCUE PASTURE
4/I1/17
260.00 (CY)
8.025
15.09
1.020
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
57,200. p
10,100.00 p
2.03 p
19182
FESCUE PASTURE
Apr-17
795.00 (Cl)
24.537
i- vua •... ". A. .JY
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
P
PAN
TOTALS:
knnuallbs/acre
F3.61
120
0.027
0.032
0.379
1.628
0.220
0.003
0.073
0.165
0.031
134.72
3umulativelbs/acre
0.190
0.350
3.223
18.886
3.255
0.053
0.727
1.728•
0.228
37.787
,
ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
' '
" ``
N }
:
V
12
6
-------------------
"`
'D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
25�0 0
t
r
3TFCC = STATESVILLE, NC FOURTH CREEK CAKE
(SIGNATURE OF LAND APPLIER) DATE `
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 52.32
SITE #: NC IR 00023 FIELD# : IR 00023 0004 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.70 ACRES PERMITTED: 13.70
Page
Lime Applied ***
Date
Lbs/Ac
or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PANDATE
(ppm)
Crop
Total
Per Acre
4/13/17
90.00 (CY)
6.569
13.96
0.772
1 STTCC
DRY
0-<1/2"
SUR
0.5
0.30
43,100. p
2,650.00 p
159.00 p
13619
I FESCUE PASTURE
4/14/17
355.00 (CY)
25.912
13.96
3.047
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
43,100.p
2,650.00 p
159.00 p
13619
FESCUE PASTURE
Apr-17
445.00 (CV)
32.481
1
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
104
0.026
0.101
1.077
2.498
0.646
0.003
0.148
0.407
0.052
7.791
124.50
Cumulative lbs/acre
0.123
0.213
2.334
11.219
1.570
0.041
0.479
1.223
0.184
25.149
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
:;
s
162
4
iY
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0 i
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X ��I
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 55.13
SITE #: NC IR 00023 FIELD# : IR 00023 0005 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.10 ACRES PERMITTED: 16.10
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acre
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
4/11/17
110.00 (CY)
6.832
115.09
0.868
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
57,200. p
10,100.00 p
2.03 p
19182
FESCUE PASTURE
Apr-17
110.00 (Cl)
6.832
4/13/17
350.00 (CY)
21.7391
13.96
2.556
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
43,100. p
2,650.00 p
159.00 p
13619
1 FESCUE PASTURE
Apr-17
350.00 (CY)
21.739
I
1
1
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se _
Zn
P
PAN
Annual lbs/acre
103
0.025
0.076
0.826
2.125
0.494
0.003
0.119
0.318
0.044
6.220
120.84
Cumulative lbs/acre
0.170
0.267
3.010
15.588
2.194
0.057
0.655
1.614
0.227
32.536
a
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
162
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 t 375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X _' ViVI
r�
(SIGNATURE OF LAND APPLIER) DATE I
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

sumfort
t:hf'r�Ri-'ilJ&SEt:Y?tL a�::ttit]L���:=5;'itc:
/dnaFyrc3f L�t�rAic;�FS
February 03, 2017
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Statesville
Dear Erik Bruce:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: httD:/hvivtv.settek.com
Order No.: 17010157
Summit Environmental Technologies, Inc. received 2 sample(s) on 1/5/2017 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North
Dakota R-201, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001,
Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 9957C
Page 1 of 44

G
S to Af(I *4 1
Summit Environmental Technologies, Inc.
3310 Win St.
Case Narrative
I rVIftONMEN'ML Y_t INOLGGJE5, iNc_
Cuyahoga Falls, Ohio 44223
WO#: 17010157
Ap,alifU,al Ls[rerafor pS
TEL: [phone] FAX: [phone]
Website: hQ.-1Avww.settekcon:
Date: 2/3/2017
CLIENT:
Synagro
Project:
Statesville
WorkOrder Narrative:
17010157: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vaiy at different
times and at different sampling conditions. Summit Envirommental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Comments:
17010157-002ams 1054985: Analytical Comments for tclp-VOC-MSTR_tclp(8260), Sample 17010157-
002ams, Batch ID R64004 : Due to instrument error, the VOC MS and MSD were analyzed outside of
12 hour tune. The LCS exhibited control.
17010157-002amsd 1054986: Analytical Comments for tclp-VOC-MSTR_tclp(8260), Sample
17010157-002ainsd, Batch ID R64004 : Due to instrument error, the VOC MS and MSD were analyzed
outside of 12 hour tune. The LCS exhibited control.
Original
Page 2 of 44

w- Summit Environmental Technologies, In Qualifiers and Acronyms
. 3310 Win 5
r-.`:t�IRnhffriEhli',9L"€_tY,tJOU-1 a=st!NC. Cuyahoga Falls, Ohio4421 pd09: 17010157
M-Hifytical Lsboraforip: TEL: [phone] FAX. (330.) 253-446
Website: httn:/hviviv.settekco Date: 2/3/2017
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
x The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
BM+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
s The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
M1nCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 44

SummitEnvironn:entaZTechnologies, Inc. Workorder
Mp SUMN&I'l- 3310 Win St.
FUVIROMMENY_'iL?IICIiNOLaI:cc, 1,114. CuyahogaFaZls, Ohio44223 Sample Summary
ArrHbfUcal Lb beraiur e . TEL: [phone] FAX.• [phone] WO#: 17010157
Website: hQ.*1 vwrv.settekcom 03-Feb-17
CLIENT: Synagro
Project: Statesville
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
17010157-001 Statesville 4th Creek 1/4/2017 8:30:00 AM 1/5/2017 9:45:00 AM Solid
17010157-002 Statesville 3rd Creek 1/4/2017 9:00:00 AM 1/5/2017 9:45:00 AM Solid
Page 4 of 44

o =
Summit Environmental Technologies, Inc.
� 3310 Win St.
Analytical Report
a
f WlRntlh1EK1rN!L T-2CW' )LOCI o, iNQ.
Cuyahoga Falls, Ohio 44223
(base report)
gnat;: tir_al Lr baraiarie s
TEL: (330)
253-8211 FAX.- [phone]
WO#: 17010157
Website: hM.-Ilwivw.settek.coni
Date Reported: 2/3/2017
CLIENT: Synagro
Tag Number:
Matrix: SOLID
Collection Date:
1/4/2017 8:30:00 AM
Lab ID: 17010157-OOIA
Project: Statesville
Client Sample ID Statesville 4th Creek
Analyses Result
PQL
Qual Units
DF
Date Analyzed
TCLP METALS ANALYSIS (SW846 1311130101601017470)
SW7470A
SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (1311/7470)
TCLP Mercury
ND
0.00200
mg/L
1
1/6/20174:35:00 PM
TCLP METALS ANALYSIS (SW846 1311/3010/601017470)
SW601OC
SW3010A Analyst: VVK
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
1/6/2017 3:55:11 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
1/6/2017 3:55:11 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
1/6/2017 3:55:11 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
1/6/2017 3:55:11 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
1/6/2017 3:55:11 PM
TCLP Selenium(Se)
ND
0.500
mg/L
1
1/6/2017 3:55:11 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
1/6/2017 3:55:11 PM
TCLP SVOC ANALYSIS (SW846 13111351018270)
SW8270C
SW351 OC Analyst: MSM
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
1/10/2017 12:48:00 AM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
1/10/2017 12:48:00 AM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
1/10/2017 12:48:00 AM
2,4-Dinitrotoluene
ND
0.0400
mg/L
2
1/10/2017 12:48:00 AM
o-Cresol
ND
0.200
mg/L
2
1/10/2017 12:48: 00 AM
m/p-Cresol(s)
ND
0.200
mg/L
2
1/10/2017 12:48:00 AM
Cresols, Total
ND
4.00
mg/L
2
1/10/2017 12:48:00 AM
Hexachloro-1,3-butadiene
ND
0.0160
mg/L
2
1/10/2017 12:48: 00 AM
Hexachlorobenzene
ND
0.0400
mg/L
2
1/10/2017 12:48:00 AM
Hexachloroethane
ND
0.0800
mg/L
2
1/1012017 12:48:00 AM
Nitrobenzene
ND
0.0800
mg/L
2
1/10/2017 12:48:00 AM
Pentachlorophenol
ND
0.200
mg/L
2
1/10/2017 12:48:00 AM
Pyridine
ND
0.200
mg/L
2
1/10/2017 12:48:00 AM
Surr: 2-Fluorophenol
63.8
10 - 109
%Rec
2
1/10/2017 12:48:00 AM
Surr: Phenol-d6
64.1
10 - 109
%Rec
2
1/10/2017 12:48:00 AM
Surr: Nitrobenzene-d5
68.7
19 - 120
%Rec
2
1/10/2017 12:48:00 AM
Surr: 2,4,6-Tribromophenol
67.8
10 - 120
%Rec
2
1/10/2017 12:48:00 AM
Surr: 2-Fluorobiphenyl
70.8
22 - 117
%Rec
2
1/10/2017 12:48:00 AM
Surr: p-Terphenyl-d14
94.2
34 - 116
%Rec
2
1/10/2017 12:48:00 AM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 5 of 44

Sunrafftour
SummitEnvir•onmental Technologies, Inc. Analytical report
fn 3310 Win St.
F;-;'O D N hl EMIT L : Er> UD La si -IN C- Cuyahoga Falls, Ohio 44223 (base report)
lir3;irtrs! La erai�rae5 TEL: [phone] FAX: [phone] W04: 17010157
Website: hgo.-11wiviv.settelccon: Date Reported: 2/3/2017
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/4/2017 8:30:00 AM
Lab ED: 17010157-001A
Project: Statesville
Client Sample ID Statesville 4th Creek
Analyses Result PQL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
58.3
Surr: DCB
78.8
SW8081A SW3510C Analyst: JBN
0.0100
mg/L
1
1/9/2017 9:31:00 PM
0.0200
mg/L
1
1/9/2017 9:31:00 PM
0.00100
mg/L
1
1/9/2017 9:31:00 PM
0.00100
mg/L
1
1/9/2017 9:31:00 PM
0.00100
mg/L
1
1/9/2017 9:31:00 PM
0.00100
mg/L
1
1/9/2017 9:31:00 PM
0.00100
d mg/L
1
1/9/2017 9:31:00 PM
10 - 119
%Rec
1
1/9/2017 9:31:00 PM
10 - 119
%Rec
1
1/9/2017 9:31:00 PM
TCLP HERBICIDES ANALYSIS (SW846 131118151)
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D ND 1.00 mg/L
2,4,5-TP ND 0.500 mg/L
TCLP VOC ANALYSIS (SW846 131118260)
VOC BY GC/MS (8260)-TCLP
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Bromofluorobenzene
Surr: Dibromof] uoromethane
Surr: Toluene-d8
RCI
REACTIVE CYANIDE (9014/7.3.3.2)
SW8151A SW8151A Analyst: JBN
SW8260B
1 1/18/2017 3:16:00 AM
1 1/18/2017 3:16:00 AM
Analyst: MES
ND
0.100
mg/L
1
1/6/2017 7:28:00 PM
ND
0.100
mg/L
1
1/6/2017 7:28:00 PM
ND
2.00
mg/L
1
1/6/2017 7:28:00 PM
ND
0.100
mg/L
1
1/6/2017 7:28:00 PM
ND
0.100
mg/L
1
1/6/2017 7:28:00 PM
ND
0.100
mg/L
1
1/6/2017 7:28:00 PM
ND
0.100
mg/L
1
1/6/2017 7:28:00 PM
ND
0.100
mg/L
1
1/6/2017 7:28:00 PM
ND
0.100
mg/L
1
1/6/2017 7:28:00 PM
ND
0.200
mg/L
1
1/6/2017 7:28:00 PM
93.3
70 - 130
%Rec
1
1/6/2017 7:28:00 PM
98.1
70 - 130
%Rec
1
1/6/2017 7:28:00 PM
96.9
70 - 130
%Rec
1
1/6/2017 7:28:00 PM
SW9014 Analyst: MS
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 6 of 44

f Sunnnit Environmental Technologies, Inc.
a { Analytical Report
3310 Win St.
e= 4:r1`;OWMEKml- �c etiOLe•�;es: trtc_ Cuyahoga Falls, Ohio44223 (base report)
ri.rraf; ricai Lsberai�r'h==, TEL: [phone] FAX.- [phone] WO#: 17010157
Website: &W.-I/rviviv.settekcom Date Reported: 2/3/2017
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/4/2017 8:30:00 AM
Lab ID: 17010157-OOIA
Project: Statesville
Client Sample ID Statesville 4th Creek
Analyses Result
PQL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)
Cyanide, Reactive ND
0.500 mg/Kg
1
1/10/2017 12:17:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030) '
SW1030
Analyst: RMT
Ignitability Non-flammable.
1
2/1/2017 9:30:00 AM
RCI
SW9045D
Analyst: DHC
PH (SW9045D)
pH 6.67
s.u.@19.3C
1
1/9/2017 4:59:00 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND
25.0 mg/Kg
1
1/10/2017 12:17:00 PM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 7 of 44

A
sumbulf
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
f1rin.C�hlhSEi�PtkLtc�Yi�:rjLO�: ��dC.
Cuyahoga
Falls, Ohio44223
(base report)
A?Talyficaf Lzi;oraiQ ec,
TEL: (330)
253-8211 FAX. [phone]
WO#: 17010157
Website: htt12:1Av1viv.settek.com
Date Reported: 2/3/2017
CLIENT: Synagro
Tag Number:
Matrix: SOLID
Collection Date:
1/4/2017 9:00:00 AM
Lab ID: 17010157-002A
Project: Statesville
Client Sample ID Statesville 3rd Creek
Analyses Result
PQL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (131117470)
TCLP Mercury
ND
0.00200
mg/L
1
1/6/2017 4:36:00 PM
TCLP METALS ANALYSIS (SW846 1311/30101601017470)
SW6010C
SW3010A Analyst: VVK
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
1/6/2017 3:55:11 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
1/6/2017 3:55:11 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
1/6/2017 3:55:11 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
1/6/2017 3:55:11 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
1/6/2017 3:55:11 PM
TCLP Selenium(Se)
ND
0.500
mg/L
1
1/6/2017 3:55:11 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
1/6/2017 3:55:11 PM
TCLP SVOC ANALYSIS (SW846 1311/351018270)
SW8270C
SW3510C Analyst: MSM
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
1/10/2017 1:18:00 AM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
1/10/2017 1:18:00 AM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
Ill0/2017 1:18:00 AM
2,4-Dinitrotoluene
ND
0.0400
mg/L
2
1/10/2017 1:18:00 AM
o-Cresol
ND
0.200
mg/L
2
1/10/2017 1:18:00 AM
m/p-Cresol(s)
ND
0.200
mg/L
2
1/10/2017 1:18:00 AM
Cresols, Total
ND
4.00
mg/L
2
1/10/2017 1:18:00 AM
Hexachloro-1,3-butadiene
ND
0.0160
mg/L
2
1/10/2017 1:18:00 AM
Hexachlorobenzene
ND
0.0400
mg/L
2
1/10/2017 1:18:00 AM
Hexachloroethane
ND
0.0800
mg/L
2
1/10/2017 1:18:00 AM
Nitrobenzene
ND
0.0800
mg/L
2
1/10/2017 1:18:00 AM
Pentachlorophenol
ND
0.200
mg/L
2
1/10/2017 1:18:00 AM
Pyridine
ND
0.200
mg/L
2
1/10/2017 1:18:00 AM
Surr: 2-Fluorophenol
64.2
10 - 109
%Rec
2
1/10/2017 1:18:00 AM
Surr: Phenol-d6
63.6
10 - 109
%Rec
2
Ill 0/2017 1:18:00 AM
Surr: Nitrobenzene-d5
72.3
19 - 120
%Rec
2
1/10/2017 1:18:00 AM
Surr: 2,4,6-Tribromophenol
64.2
10 - 120
%Rec
2
1/10/2017 1:18:00 AM
Surr: 2-Fluorobiphenyl
75.6
22 - 117
%Rec
2
1/10/2017 1:18:00 AM
Surr: p-Terphenyl-d14
91.6
34 - 116
%Rec
2
1/10/2017 1:18:00 AM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 8 of 44

summur
Summit Environmental Technologies, Inc.ED 3310 Win St.
Analytical Report
a�tS'dfR�Nh9Eh�P�'ILT=r�P�oL�Glc�;iPtc_
Cuyahoga Falls, Ohio44223
(base report)
S r3P;rtecai Lofinraiorjle
TEL: (330)
253-8211 FAX: [phone]
WO#: 17010157
Website: http://iviviv.settek.com
Date Reported: 2/3/2017
CLIENT: Synagro
Tag Number:
Matrix: SOLID
Collection Date:
1/4/2017 9:00:00 AM
Lab ID: 17010157-002A
Project: Statesville
Client Sample ID Statesville 3rd Creek
Analyses Result
PQL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081A
SW3510C Analyst: JBN
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total
ND
0.0100
mg/L
1 1/9/2017 9:58:00 PM
Toxaphene
ND
0.0200
mg/L
1 1/9/2017 9:58:00 PM
Endrin
ND
0,00100
mg/L
1 1/9/2017 9:58:00 PM
gamma-BHC
ND
0.00100
mg/L
1 1/9/2017 9:58:00 PM
Heptachlor
ND
0.00100
mg/L
1 1/9/2017 9:58:00 PM
Heptachlor epoxide
ND
0.00100
mg/L
1 1/9/2017 9:58:00 PM
Methoxychlor
ND
0.00100
mg/L
1 1/9/2017 9:58:00 PM
Surr: TCMX
87.1
10 - 119
%Rec
1 1/9/2017 9:58:00 PM
Surr: DCB
96.7
10 - 119
%Rec
1 1/9/2017 9:58:00 PM
TCLP HERBICIDES ANALYSIS (SW846131118151)
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
2,4,5-TP
ND 1.00 mg/L
ND 0.500 mg/L
SW8151A SW8151A Analyst: JBN
1/18/2017 3:45:00 AM
1/18/2017 3:45:00 AM
TCLP VOC ANALYSIS (SW846 1311/8260)
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
1,1-Dichloroethene
ND
0.100
mg/L
1
1/9/2017 11:44:00 AM
1,2-Dichloroethane
ND
0.100
mg/L
1
1/9/2017 11:44:00 AM
MEK
ND
2.00
mg/L
1
1/9/2017 11:44:00 AM
Benzene
ND
0.100
mg/L
1
1/9/2017 11:44:00 AM
Carbon tetrachloride
ND
0.100
mg/L
1
1/9/2017 11:44:00 AM
Chlorobenzene
ND
0.100
mg/L
1
1/9/2017 11:44:00 AM
Chloroform
ND
0.100
mg/L
1
1/9/2017 11:44:00 AM
Tetrachloroethene
ND
0.100
mg/L
1
1/9/2017 11:44:00 AM
Trichloroethene
ND
0.100
mg/L
1
1/9/2017 11:44:00 AM
Vinyl chloride
ND
0.200
mg/L
1
1/9/2017 11:44:00 AM
Surr: 4-Bromofluorobenzene
92.3
70 - 130
%Rec
1
1/9/2017 11:44:00 AM
Surr: Dibromofluoromethane
105
70 - 130
%Rec
1
1/9/2017 11:44:00 AM
Surr: Toluene-d8
101
70 - 130
%Rec
1
1/9/2017 11:44:00 AM
RCI SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 9 of 44

Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
r:``srin�?P1FetENPL €ems' oL�,l ,�tr_ Cuyahoga Falls, Ohio44223 (base report)
TISUMMIT
Anaglrrcai Labe-rai!:wm,, TEL: [phone] FAX.- [phone] WO#: 17010157
Website: htto://tvivw.settek.com Date Reported: 2/3/2017
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/4/2017 9:00:00 AM
Lab ID: 17010157-002A
Project: Statesville
Client Sample ID Statesville 3rd Creek
Analyses Result PQL Qual Units DF Date Analyzed
RCI
REACTIVE CYANIDE (9014/7.3.3.2)
Cyanide, Reactive ND
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability Non-flammable.
RCI
PH (SW9045D)
pH 6.42
RCI
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND
SW9014
0.500 mg/Kg
SW1030
SW9045D
s.u.@19.4C
SW9034
25.0 mg/Kg
Analyst: MS
1 1/10/2017 12:17:00 PM
Analyst: RMT
1 2/1/2017 9:30:00 AM
Analyst: DHC
1 1/10/2017 3:15:00 PM
Analyst: MS
1 1/10/2017 12:17:00 PM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode .
Original
Page 10 of 44

! Summit Environmental Technologies, Inc.
�"i�� t '- 331oYVinst. QC SUMMARY REPORT
cr;,vlHa�t9tU�NIA, w i;I-'NNuut GI!:b, ittw Cuyahoga Falls, Ohio 44223 WO#: 17010157
iknadl,Ucaf Laboiworles TEL: [phone] FAX.- [phone]
Website: htto.•/hvww.settelccom 03-Feb-17
Client: Synagro
Project: Statesville BatchED: 24817
Sample ID MB-24817
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/6/2017
RunNo: 63973
�lient ID: PBW
Batch ID: 24817
TestNo: SW6010C SW3010A
Analysis Date: 1/6/2017
SegNo: 1054297
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-24817
SampType: LCS
TestCode:
Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/6/2017
RunNo: 63973
;lient ID: LCSW
Batch ID: 24817
TestNo:
SW6010C SW3010A
Analysis Date: 1/6/2017
SegNo: 1054298
\nalyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
_ %RPD RPDLimit Qua[
TCLP Arsenic(As)
1.99
0.500
2.000
0
99.5
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
99.5
80
120
,TCLP Cadmium(Cd)
2.01
0.100
2.000
0
101
80
120
TCLP Chromium(Cr)
1.99
0.200
2.000
0
99.5
80
120
TCLP Lead(Pb)
1.99
0.500
2.000
0
99.5
80
120
TCLP Selenium(Se)
2.00
0.500
2.000
0
100
80
120
TCLP Silver(Ag)
0.990
0.500
1.000
0
99.0
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J A ialyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 11 of 44

h Summit Environmental Technologies, Inc. � C SUMMARY RY REPORT
,, 4.... lVJ �1�1111��1L-Li� i 1eL1 li
., 3310 Win St.
e summmeff
RI JKC, Cuyahoga Falls, Ohio44223 W09: 17010157
kr r1t V':ccst L abo;ratoae� TEL: [phone] FAX.- [phone]
Website: htty:/hvrvw.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: 24817
Sample ID 17010147-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/6/2017
RunNo: 63973
lient ID: BatchQC
Batch ID: 24817
TestNo: SW6010C SW3010A
Analysis Date: 1/6/2017
SegNo: 1054300
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Arsenic(As) -
2.04
0.500
2.000
0
102
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0
99.5
70
130
TCLP Cadmium(Cd)
1.94
0.100
2.000
0
97.0
70
130
TCLP Chromium(Cr)
1.94
0.200
2.000
0
97.0
70
130
TCLP Lead(Pb)
1.96
0.500
2.000
0
98.0
70
130
TCLP Selenium(Se)
2.08
0.500
2.000
0
104
70
130
TCLP Silver(Ag)
0.980
0.500
1.000
0
98.0
70
130
Sample ID 17010147-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/6/2017
RunNo: 63973
client ID: BatchQC
Batch ID: 24817
TestNo: SW6010C SW3010A
Analysis Date: 1/6/2017
SegNo: 1054301
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.03
0.500
2.000
0
102
70
130
2.040
0.491
20
TCLP Barium(Ba)
ND
5.00
2.000
0
100
70
130
0
0
20
TCLP Cadmium(Cd)
1.93
0.100
2.000
0
96.5
70
130
1.940
0.517
20
TCLP Chromium(Cr)
1.93
0.200
2.000
0
96.5
70
130
1.940
0.517
20
TCLP Lead(Pb)
1.95
0.500
2.000
0
97.5
70
130
1.960
0.512
20
TCLP Selenium(Se)
2.06
0.500
2.000
0
103
70
130
2.080
0.966
20
TCLP Silver(Ag)
0,080
0.500
1.000
0
98.0
70
130
0.9800
0
20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 12 of 44

Summit Environmental Technologies, Inc.
,,,, _ g
� �C SUMMARY REPORT
N a �';.:p'�11a 3310 Win St.
�n:vl+r+r�rni;ni�t1_�r:r �ruL�tsai s.JriC;. Cuyahoga Falls, Ohio44223 WO#: 17010157
ff
r f6 zd,4, t.caf C.Ti)o,r9rrarier< TEL: [phone] FAX- [phone]
Website: hgp://www.setlelc.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: 24826
Sample ID MB-24826
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/6/2017
RunNo: 63984
Client ID: PBW
Batch ID: 24826
TestNo: SW7470A SW7470A
Analysis Date: 1/6/2017
SegNo: 1054456
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
CLP Mercury
ND 0.00200
Sample ID LCS-24826
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/6/2017
RunNo: 63984
Client ID: LCSW
Batch ID: 24826
TestNo: SW7470A SW7470A
Analysis Date: 1/6/2017
SegNo: 1054457
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD . RPDLimit Qual
CLP Mercury
0.00405 0.00200 0.00400
0 101 80 120
Sample ID 17010096-001AMS
SampType: MS
TestCode: HG TCLP(74 Units: PPM
Prep Date: 1/6/2017
RunNo: 63984
Client ID: BatchQC
Batch ID: 24826
TestNo: SW7470A SW7470A
Analysis Date: 1/6/2017
SegNo: 1054462
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
CLP Mercury
0.00371 0.00200 0.00400 0 92.8 75 125
Sample ID 17010096-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/6/2017
RunNo: 63984
Client ID: BatchQC
Batch ID: 24826
TestNo: SW7470A SW7470A
Analysis Date: 1/6/2017
SegNo: 1054463
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00368 0.00200
0.00400 0 92.0 75
125
0.00371 0.812 20
Qualifiers: " Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit Original
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 13 of 44

a« h Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Moo
o�� 3310 Win St. `�
t:n!V1K Nrni,N I Al, R a + Md�uLusuhs, n ti. Cuyahoga Falls, Ohio 44223 WO#: 17010157
z A !1,z- fVfl.afff LzborafurieF TEL: [phone] Ff1X.• [phone]
Website: httv://wivw.settelc.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: 24826
Sample ID 17010096-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/6/2017
RunNo: 63984
Client ID: BatchQC
Batch ID: 24826
TestNo: SW7470A SW7470A
Analysis Date: 1/6/2017
SegNo: 1054463
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: :k Value exceeds Maximum Contaminant Level. _ B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 14 of 44

[ ` Summit Environmental Technologies, Inc. QC SUMMARY REPORT
r 6;;�L}�� �f.'� l 3310 Win St. SUMMARY i 1
L?4MW.V,Nrnt:ni:u.4ia"r4cauat;1!:S,JnC. Cuyahoga Falls, Ohio44223 WO#: 17010157
_ 4r TEL: [phone] FAX.- [phone]
Website: http://ivivw.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: 24860
Sample ID mb-24860
SampType: mblk
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 1/9/2017
RunNo: 64072
Client ID: PBW
Batch ID: 24860
TestNo: SW8081A SW3510C
Analysis Date: 1/9/2017
SegNo: 1055931
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00500
Toxaphene
ND
0.0100
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500 d
Surr: TCMX
7.77
10.00 77.7 10 119
Surr: DCB
9.09
10.00 90.9 10 119
Sample ID Ics-24860
SampType: Ics
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 1/9/2017
RunNo: 64072
Client ID: LCSW
Batch ID: 24860
TestNo: SW8081A SW3510C
Analysis Date: 1/9/2017
SegNo: 1065932
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.00449
0.000500
0.00500
0
89.9
20
157
gamma-BHC
0.00371
0.000500
0.00500
0
74.1
22
137
Heptachlor
0.00394
0.000500
0.00500
0
78.9
24
121
Heptachlor epoxide
0.00419
0.000500
0.00500
0
83.8
27
152
Methoxychlor
0.00521
0.000500
0.00500
0
104
10
199
Surr: TCMX
7.38
10.00
73.8
10
119
Surr: DCB
7.09
10.00
70.9
10
119
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to detennine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 15 of 44

Sunvnit Environmental Technologies, Inc.
g QC SUMMARY REPORT
t 1� 3310 Wire St.
er;r ix4 rare;n i ai, s t: .zsz,L uu�z s; ir: �. Cuyahoga Falls, Ohio 44223 WO#: 17010157
_� ! .i1,.ii C.31' L.rtacar9ioric 5 TEL: [phone] FAY- [phone]
Websile: http:AAww.settekcom 03-Feb-17
Client: Synagro
Project: Statesville BatchID: 24860
Sample ID 17010154-001ams
SampType: ms
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 1/9/2017
RunNo: 64072
Client ID: BatchQC
Batch ID: 24860
TestNo: SW8081A SW3510C
Analysis Date: 1/9/2017
SegNo: 1055933
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.0113
0.00100
0.0100
0
113
20
157
gamma-BHC
0.00897
0.00100
0.0100
0
89.7
22
137
Heptachlor
0.00975
0.00100
0.0100
0
97.5
24
121
Heptachlor epoxide
0.0105
0.00100
0.0100
0
105
27
152
Methoxychlor
0.0133
0.00100
0.0100
0
133
10
199
Sum TCMX
19.4
20.00
97.1
10
119
Surr: DCB
19.1
20.00
95.3
10
119
Sample ID 17010154-001amsd
SampType: msd
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 1/9/2017
RunNo: 64072
;lient ID: BatchQC
Batch ID: 24860
TestNo: SW8081A SW3510C
Analysis Date: 1/9/2017
SegNo: 1055934
analyte
Result
'PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.00828
0.00100
0.0100 0 82.8
20
157
0.0113 31.0
30 R
gamma-BHC
0.00670
0.00100
0.0100 0 67.0
22
137
0.00897 29.0
30
Heptachlor
0.00728
0.00100
0.0100 0 72.8
24
121
0.00975 29.0
30
Heptachlor epoxide
0.00764
0.00100
0.0100 0 76.4
27
152
0.0105 31.4
30 R
Methoxychlor
0.00995
0.00100
0.0100 0 99.5
10
199
0.0133 28.6
30
Surr: TCMX
14.0
20.00 69.9
10
119
0
Surr: DCB
13.5
20.00 67.6
10
119
0
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7 Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
Original
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 16 of 44

Summit Environmental Technologies, Inc.
sa"�
w a 3310 win St. QC SUMMARY REPORT
iHvF16U:NIAkfti:ONULUi31tS.INC Cuyahoga Falls, Ohio44223 WO#: 17010157
Arratyfl-caf LzbP)rato,,,,es TEL: [phone] FAX.- [phone]
Website: httv:/hvlpw.settelc.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: 24862
Sample ID MB-24862
SampType: MBLK
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 1/9/2017
RunNo: 64062
client ID: PBW
Batch ID: 24862
TestNo: SW8270C SW3510C
Analysis Date: 1/9/2017
SegNo: 1055779
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0200
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0100
o-Cresol
ND
0.0500
m/p-Cresol(s)
ND
0.0500
Cresols, Total
ND
1.00
Hexachloro-1,3-butadiene
ND
0.00400
Hexachlorobenzene
ND
0.0100
Hexachloroethane
ND
0.0200
Nitrobenzene
ND
0.0200
Pentachlorophenol
ND
0.0500
Pyridine
ND
0.0500
Surr: 2-Fluorophenol
0.272
Surr: Phenol-d6
0.275
Surr: Nitrobenzene-d5
0.304
Surr: 2,4,6-Tribromophenol
0.284
Surr: 2-Fluorobiphenyl
0.311
Surr: p-Terphenyl-d14
0.421
Qualifiers: ,k Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
0.5000
54.4
10
109
0.5000
55.1
10
109
0.5000
60.7
19
120
0.5000
56.8
10
120
0.5000
62.2
22
117
0.5000
84.2
34
116
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
m
Original
Page 17 of 44

S _
' !
Summit Environmental Technologies,lnc.
3310 Win St.
QC SUMMARY REPORT['
er4,YIKV'rgN1ar41 A I t;tt WLrJU1�s, INC
Cuyahoga Falls, Ohio 44223
WO#: 17010157
_.
A.!?all-,Uzaf i.abcy.girarre
TEL: [phone] FAX.- [phone]
Website: http://wivmv.sette%conz
03-Feb-17
Client:
Synagro
Project:
Statesville
BatchID: 24862
Sample ID LCS-24862
SampType: LCS
TestCode: svoc-BNA T Units: mg/L
Prep Date: 1/9/2017
RunNo: 64062
Client ID: LCSW
Batch ID: 24862
TestNo: SW8270C SW3510C
Analysis Date: 1/9/2017
SegNo: 1055780
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.0924
0.0200
0.2000
0
46.2
19.1
126
2,4,5-Trichlorophenol
0.106
0.0500
0.2000
0
53.0
11.7
151
2,4,6-Trichlorophenol
0.104
0.0500
0.2000
0
51.8
12.4
150
2,4-Dinitrotoluene
0.111
0.0100
0.2000
0
55.4
20.6
140
o-Cresol
0.0923
0.0500
0.2000
0
46.2
13.8
137
m/p-Cresol(s)
0.0968
0.0500
0.2000
0
48.4
10
134
Cresols, Total
ND
1.00
0.4000
0
47.3
10
129
Hexachloro-1,3-butadiene
0.0872
0.00400
0.2000
0
43.6
14.7
137
Hexachlorobenzene
0.0959
0.0100
0.2000
0
48.0
12
139
Hexachloroethane
0.0882
0.0200
0.2000
0
44.1
14.8
132
Nitrobenzene
0.0980
0.0200
0.2000
0
49.0
15.6
138
Pentachlorophenol
0.109
0.0500
0.2000
0
54.7
10
156
Pyridine
0.0376
0.0500
0.2000
0
18.8
10
126
Surr: 2-Fluorophenol
0.288
0.5000
57.5
10
147
Surr: Phenol-d6
0.296
0.5000
59.1
10
140
Surr: Nitrobenzene-d5
0.316
0.5000
63.3
10
169
Surr: 2,4,6-Tribromophenol
0.299
0.5000
59.8
10
185
Surr: 2-Fluorobiphenyl
0.327
0.5000
65.4
10
169
Surr: p-TerphenyW14
0.391
0.5000
78.1
10
179
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
m
m
Original
Page 18 of44

a r ^ M Summit Environmental Technologies, Inc. QC SUMMARY REPORT
'�• ' , &I hl 3310 Win St.
t: 74N It C 1) ! T-4 M I , N I AL I L-CH?4LILrJaI-,S. Jrq C Cuyahoga Falls, Ohio 44223 WO#: 17010157
;'4nj4xfi.cm L.Tlaofalo,fip4 TEL: [phone] FAX [phone]
Website: hgp:/hvivw.settek.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: 24862
Sample ID 17010154-002AMS
SampType: MS
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 1/9/2017
RunNo: 64062
Client ID: BatchQC
Batch ID: 24862
TestNo: SW8270C SW3510C
Analysis Date: 1/9/2017
SegNo: 1055782
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.204
0.0800
0.4000
0
51.1
29
112
2,4,5-Trichlorophenol
0.227
0.200
0.4000
0
56.8
53
123
2,4,6-Trichlorophenol
0.216
0.200
0.4000
0
54.1
50
125
m
2,4-Dinitrotoluene
0.234
0.0400
0.4000
0
58.4
57
128
o-Cresol
0.1996
0,200
0.4000
0
49.9
30
117
m/p-Cresol(s)
0.210
0.200
0.4000
0
52.5
29
110
Cresols, Total
0.4096
4.00
0.8000
0
51.2
20
125
Hexachloro-1,3-butadiene
0.192
0.0160
0.4000
0
48.1
22
124
Hexachlorobenzene
0.236
0.0400
0.4000
0
59.1
53
125
Hexachloroethane
0.194
0.0800
0.4000
0
48.5
21
115
Nitrobenzene
0.214
0.0800
0.4000
0
53.4
45
121
Pentachlorophenol
0.298
0.200
0.4000
0
74.4
35
138
Pyridine
0.0564
0.200
0.4000
0
14.1
10
126
m
Surr: 2-Fluorophenol
0.640
1.000
64.0
10
147
m
Surr: Phenol-d6
0.655
1.000
65.5
10
140
Surr: Nitrobenzene-d5
0.716
1.000
71.6
10
169
Surr: 2,4,6-Tribromophenol
0.634
1.000
63.4
10
185
Surr: 2-Fluorobiphenyl
0.755
1.000
75.5
10
169
Surr: p-Terphenyl-d14
0.840
1.000
84.0
10
179
Qualifiers: :k Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation
or analysis exceeded
J Analyte detected
below quantitation limits
M Manual Integration used to determine
Original
MC Value is below Minimum
Compound Limit.
ND Not Detected at
the Reporting
Limit
0 RSD is greater than RSDlimit
P Second column confirmation
exceeds
PL Permit Limit
R RPD outside accepted recovery limits
Page 19 of 44

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
` , `rd.P
1I, 3310 Win St.
LNNIKUIFVAt.NIAkI ,INC. Cuyahoga Falls, Ohio44223 WO#: 17010157
dkrt tliti,caf C.�2aar atarir� TEL: [phone] TAX.- [phone]
Website: http:113vivw.settek.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: 24862
Sample ID 17010154-002AMSD
SampType: MSD
TestCode:
svoc-BNA_T Units: mg/L
Prep Date: 1/9/2017
RunNo: 64062
Client ID: BatchQC
Batch ID: 24862
TestNo:
SW8270C SW3510C
Analysis Date: 1/9/2017
SegNo: 1055783
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
0.224
0.0800
0.4000
0
56.1
29
112
0.2044
9.33
30
2,4,5-Trichi orophenol
0.260
0.200
0.4000
0
64.9
53
123
0.2272
13.3
30
2,4,6-Trichi orophenol
0.248
0.200
0.4000
0
61.9
50
125
0.2164
13.4
30
2,4-Dinitrotoluene
0.265
0.0400
0.4000
0
66.3
57
128
0.2336
12.7
30
o-Cresol
0.218
0.200
0.4000
0
54.5
30
117
0.1996
8.81
30
m/p-Cresol(s)
0.231
0.200
0.4000
0
57.7
29
110
0.2100
9.44
30
Cresols, Total
0.4488
4.00
0.8000
0
56.1
20
125
0
0
30
Hexachloro-1,3-butadiene
0.219
0.0160
0.4000
0
54.7
22
124
0.1924
12.8
30
Hexachlorobenzene
0.255
0.0400
0.4000
0
63.7
53
125
0.2364
7.49
30
Hexachloroethane
0.220
0.0800
0.4000
0
55.0
21
115
0.1940
12.6
30
Nitrobenzene
0.235
0.0800
0.4000
0
58.7
45
121
0.2136
9.46
30
Pentachlorophenol
0.316
0.200
0.4000
0
79.0
35
138
0.2976
6.00
30
Pyridine
0.0628
0.200
0.4000
0
15.7
10
126
0
0
30
Surr: 2-Fluorophenol
0.686
1.000
68.6
10
147
0
Surr: Phenol-d6
0.694
1.0D0
69.4
10
140
0
Surr: Nitrobenzene-d5
0.768
1.000
76.8
10
169
0
Surr: 2,4,6-Tribromophenol
0.708
1.000
70.8
10
185
0
Surr: 2-Fluorobiphenyl
0.804
1.000
80.4
10
169
D
Surr: p-Terphenyl-d14
0.930
1.000
93.0
10
179
0
Qualifiers: 'k Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
m
Original
Page 20 of 44

^� Summit Environmental Technologies, Inc.
SUM&INT3310 Win St. C SUMMARY REPORT
LMVIKar•NNINIAI,I1;i;H?4Q1LrJUits.,Ir.0 Cuyahoga Falls, Ohio44223
WO#: 17010157
An;37¢�li:crta L:rbnratorie4 TEL: [phone] FAX.- [phone]
Website: htta://wwiv.settelc.cont 03-Feb-17
Client: Synagro
Project: Statesville BatchID• 25012
Sample ID MB-25012
SampType: mblk
TestCode: telp-SVOC-H Units: mg/L
Prep Date: 1/11/2017
RunNo: 64421
Client ID: PBW
Batch ID: 25012
TestNo: SW8151A SW8151A
Analysis Date: 1/1712017
SegNo: 1061565
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Sum DCAA 392 500.0 78.3 20 140
nple ID LCS-25012
SampType: Ics
TestCode: telp-SVOC-H Units: mg/L
Prep Date: 1/11/2017
RunNo: 64421
.nt ID: LCSW
Batch ID: 25012
TestNo: SW8151A SW8151A
Analysis Date: 1/17/2017
SegNo: 1061566
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D
364 1.00
0.500
0 72.8
62.6
125
2,4,5-TP
325 0.500
0.500
0 65.0
52.5
128
Surr: DCAA
431
500.0
86.2
20
140
Sample ID 17010164-001AMS
SampType: MS
TestCode: telp-SVoC-H Units: mg/L
Prep Date: 1/11/2017
RunNo: 64421
Client ID: BatchQC
Batch ID: 25012
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2017
SegNo: 1061636
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 340 1.00 0.500 0 68.1 37 105
2,4,5-TP 308 0.500 0.500 0 61.7 38 106
Surr: DCAA 388 500.0 77.7 2D 140
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 44

_ Summit Environmental Technologies, Inc.
�`}�+,�1��' 'I 3310 Win St. Qd�t � SUMMARY REPORT
LWOIHV�NT-II:A IA6 a r4 3tF ULU10I-�S: INC:, Cuyahoga Falls, Ohio 44223 WO#: 17010157
! ,tl.nwi4`Plaat L-T5a,rq!Dnvs TEL: [phone] FAX.- [phone]
Website: http://ivivw,settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville Batch][D: 25012
Sample ID 17010154-001AMSD
SampType: msd
TestCode: telp-SVoC-H Units: mg/L
Prep Date: 1/1112017
RunNo: 64421
Client ID: BatchQC
Batch ID: 25012
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2017
SegNo: 1061637
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D 337 1.00 0.500 0 67.4 37 105 0 0 30
2,4,5-TP 308 0.500 0.500 0 61.6 38 106 0 0 30
Surr: DCAA 386 500.0 77.2 20 140 0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 22 of 44

ff
�� �5�'� �i , t�
Suann:itEnvironmental Technologies, Inc.
3310 10 Win St.
QC SUMMARY REPORT
� .+'Ir 4:rarnr;n t at. a trCaiiaJUY�t�5, INC. Cuyahoga Falls, Ohio 44223
k allYLca/ C:�iaaastnrre� TEL: [phone] FAX.- [phone]
WO#: 17010157
Website: http://www.settek.com
03-Feb-17
Client:
Synagro
Project:
Statesville
BatchID: R63970
Sample ID LCS-R63970
SampType: LCS
TestCode: FlashPt_S(10 Units: °F
Prep Date:
RunNo: 63970
;lient ID: LCSS
Batch ID: R63970
TestNo: SW1010
Analysis Date: 1/6/2017
SegNo: 1054227
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Flashpoint (140T) 84.0 77.00 0 109 100 110
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 23 of 44

Sul
Summit Environmental Technologies, Inc.
` .;�. - 3310Win St. QC SUMMARY REPORT
�bVIFi4'FJNI:h I ESL M%C"NQLFJU)!:S, JrqC Cuyahoga Falls, Ohio 44223 WO#: 17010157
a 4.rrJ.ti.+t t Aa' CzTk:t ,r,niordc ,r TEL: [phone] FAX- [phone]
Website: ham://imww.settek conz 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64004
Sample ID 17010157-002ams
SampType: MS
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 64004
client ID: Statesville 3rd Cree
Batch ID: R64004
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1054986
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDL'imit Qual
1,1-Dichloroethene
0.102
0.100
0.200
0
51.2
39.9
160
1,2-Dichloroethane
0.103
0.100
0.200
0
51.6
42.5
157
MEK
ND
2.00
1.00
0
66.0
16.6
227
Benzene
0.118
0.100
0.200
0
59.0
38.1
155
Carbon tetrachloride
ND
0.100
0.200
0
49.8
40.8
162
Chlorobenzene
0.120
0.100
0.200
0
59.8
35.7
168
Chloroform
0,112
0.100
0.200
0
55.8
18.3
199
Tetrachloroethene
0.106
0.100
0.200
0
53.0
10
261
Trichloroethene
0.109
0.100
0.200
0
54.4
23.8
175
Vinyl chloride
ND
0.200
0.200
0
62.5
10
165
Surr: 4-Bromofluorobenzene
460
500.0
92.1
84.6
130
Surr: Dibromofluoromethane
628
500.0
126
71.4
127
Surr: Toluene-d8
500
500.0
100
74.6
127
Sample ID 17010157-002amsd
SampType: MSD
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 64004
-lient ID: Statesville 3rd Cree
Batch ID: R64004
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1054986
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.163
0.100
1,2-Dichloroethane
0.150
0.100
MEK
ND
2.00
Benzene
0.176
0.100
Qualifiers: k
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
P
Second column confirmation exceeds
0.200
0
81.6
39.9
0.200
0
75.2
42.5
1.00
0
89.2
16.6
0.200
0
87.9
38.1
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
160
0.102
45.7
157
0.103
37.2
227
0
0
155
0.118
39.4
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
25 R
25 R
25 R
25 R
Original
Page 24 of 44

Summit Environmental Technologies, Inc.
z -
3310Win St. QC SUMMARY REPORT
r .:vIK4�rrrai;r i:�r r;;+ p;iU�trar s .liar Cuyahoga Falls, Ohio44223 WO#: 17010157
_ jl.K.44.1fliad Cataar loripe TEL: [phone] FAX.- [phone]
Website: http:/hviow.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatehID: R64004
Sample ID 17010157-002amsd
SampType: MSD
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 64004
lient ID: Statesville 3rd Cree
Batch ID: R64004
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1054986
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Carbon tetrachloride
0.150
0.100
0.200
0
75.0
40.8
162
0.0996
40.3
25 R
Chlorobenzene
0.169
0.100
0.200
0
84.3
35.7
168
0.120
34.0
25 R
Chloroform
0.168
0.100
0.200
0
83.8
18.3
199
0.112
40.3
25 R
Tetrachloroethene
0.142
0.100
0.200
0
70.8
10
261
0.106
28.8
25 R
Trichloroethene
0.151
0.100
0.200
0
75.4
23.8
175
0.109
32.4
25 R
Vinyl chloride
0.201
0.200
0.200
0
101
10
165
0.125
46.7
25 R
Surr:4-Bromofluorobenzene
488
500.0
97.6
84.6
130
0
25
Surr: Dibromofluorom ethane
501
500.0
100
71.4
127
0
25
Surr: Toluene-d8
509
500.0
102
74.6
127
0
25
Sample ID Ics 20ppb L0104/
SampType: LCS
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 64004
client ID: LCSW
Batch ID: R64004
TestNo: SW8260B
Analysis Date: 1/6/2017
SegNo: 1054989
%nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.217
0.100
0.200 0 108
79.4
131
1,2-Dichloroethane
0.214
0.100
0.200 0 107
73.6
137
MEK
1.12
1.00
1.00 0 112
55.1
163
Benzene
0.225
0.100
0.200 0 113
73.1
132
Carbon tetrachloride
0.209
0.100
0.200 0 104
63.7
139
Chlorobenzene
0.220
0.100
0.200 0 110
72.3
139
Chloroform
0.213
0.100
0.200 0 107
79.3
129
Tetrachloroethene
0.209
0.100
0.200 0 104
56.2
187
Qualifiers:
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
IIolding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
0 RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits Page 25 of 44

Summit Environmental Technologies, Inc. QC SUMMARY RE PORT
f 3310 Win St.
Lr_+'IKQNr,u:NIAl- a.irrc Cuyahoga Falls, Ohio44223
1k.n3,f1 f1..3! t,T2apr9rorie� TEL: [phone] FAX.- [phone] WO#: 17010157
Website: http://ivww.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64004
Sample ID Ics 20ppb L0104/
SampType: LCS
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 64004
lient ID: LCSW
Batch ID: R64004
TestNo: SW8260B
Analysis Date: 1/6/2017
SegNo: 1054989
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Trichloroethene
0.222 0.100
0.200
0 111
64.1
138
Vinyl chloride
0.209 0.200
0.200
0 105
22.1
147
Surr:4-Bromofluorobenzene
498
500.0
99.6
80.4
126
Surr: Dibromofluoromethane
502
500.0
100
70.3
125
Surr: Toluene-d8
510
500.0
102
82
117
;ample ID mbik
SampType: MBLK
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 64004
lient ID: PBW
Batch ID: R64004
TestNo: SW8260B
Analysis Date: 1/6/2017
SegNo: 1054990
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
ND
0.100
1,2-Dichloroethane
ND
0.100
MEK
ND
2.00
Benzene
ND
0.100
Carbon tetrachloride
ND
0.100
Chlorobenzene
ND
0.100
Chloroform
ND
0.100
Tetrachloroethene
ND
0.100
Trichloroethene
ND
0.100
Vinyl chloride
ND
0.200
Surr:4-Bromofluorobenzene
495
500.0 98.9 70
130
Surr: Dibromofluoromethane 494
500.0 98.9 70
130
Qualifiers: k
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Page 26 of 44

,r
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
"'+�,� 1*�', I .4 i � - 3310 Win St.
L-MYiRUJIMUNIa%[,, I a�adc�tu 3r�s, M.C. Cuyahoga Falls, Ohio44223 WO#: 17010157
t1 Jtkth i L;Tborasori"6 TEL: [phone] FAX., [phone]
Website: httU://ivrviv.settelccom 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64004
Sample ID mblk
SampType: MBLK
TestCode: tclp-VOC-MS Units: mg/L
Prep Date:
RunNo: 64004
client ID: PBW
Batch ID: R64004
TestNo: SW8260B
Analysis Date: 1/6/2017
SegNo: 1054990
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Surr: Toluene-d8
466
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
500.0
93.2 70 130
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 27 of 44

S
SummitEnvironmental Technologies, Inc. t`�,_�,� � QC SUMMARY REPORT
�st ill #,• 3310 Win St.
L-Pu� irc�a.rarni r F4I. 1a�ar�t�UC.;r�s, INC. Cuyahoga Falls, Ohio 44223 WO#: 17010157
...
4r f4'.t/caP C,Ttatorwtoriec TEL: [phone] FAK- [phone]
Website: httv:llivivw.settek.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64008
Sample ID 17010164-001ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: s.u.@19.00
Prep Date:
RunNo: 64008
client ID: BatchQC
Batch ID: R64008
TestNo: SW9045D
Analysis Date: 1/9/2017
SegNo: 1055456
gnalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDUrnit Qual
pH
6.32
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
6.320 0 10
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 28 of 44

SumntitEnvironmental Technologies, Inc. SUMMARY REPORT
U(�C S
I?r 3310 Win St. `C
Lr;AINVr W I.-N IA1. a r;r Nt �L4't3 5; JPtC . Cuyahoga Falls, Ohio 44223
l7aatt fl-ra CzTbarareric: TEL: [phone] FAX. [phone] WO#: 17010157
Website: http://www.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64008
Sample ID LCS-R64008
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@19.9C
Prep Date:
RunNo: 64008
Client ID: LCSW
Batch ID: R64008
TestNo: SW9045D
Analysis Date: 1/9/2017
SegNo: 1055038
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH 7.01 7.000 0 100 98.6 101.4
Sample ID 17010115-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@20.7C
Prep Date:
RunNo: 64008
Client ID: BatchQC
Batch ID: R64008
TestNo: SW9045D
Analysis Date: 1/9/2017
SegNo: 1065040
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.32 7.320 0 5
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 29 of 44

rs Summit Environmental Technolo ies, Inc.
331g0WinSt. QC SUMMARY REPORT
P
�rr,irsr�.rarer;r�iAl.rk:crcaaciLst�i�s,;rt Cuyahoga Falls, Ohio44223 WO#: 17010157
r'k1Ylt4�Ci'c�1 �.rbar4lo ies TEL: [phone] FAX.• [phone]
Website: http://ivivw.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64054
Sample ID 17010179-001ams
SampType: MS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 64054
client ID: BatchQC
Batch ID: R64054
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1055666
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
D.116
0.0200
0.100
0
116
39.9
160
1,2-Dichloroethane
0.0995
0.0200
0.100
0
99.5
42.5
157
MEK
0.527
0.100
0.500
0
105
16.6
227
Benzene
0.108
0.0200
0.100
0
108
38.1
155
Carbon tetrachloride
0.112
0.0200
0.100
0
112
40.8
162
Chlorobenzene
D.104
0.0200
0.100
0
104
35.7
168
Chloroform
0.109
0.0200
0.100
0
109
18.3
199
Tetrachloroethene
0.103
0.0200
0.100
0
103
10
261
Trichloroethene
0.101
0.0200
0.100
0
101
23.8
175
Vinyl chloride
0.0992
0.0200
0.100
0
99.2
10
165
Surr:4-Bromofluorobenzene
523
500.0
105
84.6
130
Surr: Dibromofluoromethane
491
500.0
98.2
71.4
127
Surr: Toluene-d8
506
500.0
101
74.6
127
Sample ID 17010179-001amsd
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 64054
,lient ID: BatchQC
Batch ID: R64054
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1055667
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.112
0.0200
0.100 0 112
39.9
160
0.116 3.50
25
1,2-Dichloroethane
0.100
0.0200
0.100 0 100
42.5
157
0.0995 0.501
25
MEK
0.558
0.100
0.500 0 112
16.6
227
0.527 5.77
25
Benzene
0.106
0.0200
0.100 0 106
38.1
155
0.108 1.77
25
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
MC
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
J
ND
Analyte detected below quantitation limits
Not Detected at the Reporting Limit
M
0
Manual Integration used to determine
RSD is greater than RSDlimit
Original
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 30 of 44

Summit Environmental Technologies, Inc.
sumh1lot 3310 Win St. QC SUMMARY REPORT
LNA-I Kr.J NW UN IP.I- 11:C4!T-AJ LUi31"8, INC Cuyahoga Falls, Ohio 44223 WO#: 17010157
S An3il; Ucai babongta,rip� TEL: [phone] FAX.- [phone]
Website: http://lvww.settefc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64054
Sample ID 17010179-001amsd
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 64054
client ID: BatchQC
Batch ID: R64054
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1055667
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.106
0.0200
0.100
0
106
40.8
162
0.112
4.59
25
Chlorobenzene
0.102
0.0200
0.100
D
102
35.7
168
0.104
2.05
25
Chloroform,
0.107
0.0200
0.100
0
107
18.3
199
0.109
1.48
25
Tetrachloroethene
0.0999
0.0200
0.100
0
99.9
10
261
0.103
3.44
25
Trichloroethene
0.100
0.0200
0.100
0
100
23.8
175
0.101
1.19
25
Vinyl chloride
0.0948
0.0200
0.100
0
94.8
10
165
0.0992
4.54
25
Surr:4-Bromofluorobenzene
514
500.0
103
84.6
130
0
25
Surr: Dibromofluoromethane
498
500.0
99.6
71.4
127
0
25
Surr: Toluene-d8
504
500.0
101
74.6
127
0
25
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit,
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 31 of 44

Summit Environmental Technologies, Inc. C SUMMARY REPORT
IL
_ f SUMJj4JJ0J 3310 Win St. `� (�
ecwv�rxr�.wraiar;inI�aM.C. Cuyahoga Falls, Ohio44223 W09: 17010157
_ ?k.n:3t4tidcaP C:s27�1'9ro.rle TEL: [phone] FAX.- [phone]
Website: http://ivivw.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64054
Sample ID Ics 10ppb L01041
SampType: LCS
TestCode: voc-mstr_np Units: mg/L
Prep Date:
RunNo: 64054
:lient ID: LCSW
Batch ID: R64054
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1055654
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.0109
0.00500
0.0100
0
109
71
138
Benzene
0.0105
0.00500
0.0100
0
105
75
137
Chlorobenzene
0.0101
0.00500
0.0100
0
101
77
132
Trichloroethene
0.0102
0.00500
0.0100
0
102
64
119
Surr: 4-Bromofluorobenzene
50.7
50.00
101
70
130
Surr: Dibromofluorom ethane
50.0
50.00
99.9
70
130
Surr: Toluene-d8
49.7
50.00
99.5
70
130
Sample ID mblk
SampType: MBLK
TestCode: voc-mstr_np Units: mg/L
Prep Date:
RunNo: 64054
client ID: PBW
Batch ID: R64054
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1055656
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
ND 0.00500
1,2-Dichloroethane
ND 0.00500
MEK
ND 0.0250
Benzene
ND 0.00500
Carbon tetrachloride
ND 0.00500
Chlorobenzene
ND 0.00500
Chloroform
ND 0.00500
Tetrachloroethene
ND 0.00500
Trichloroethene
ND 0.00500
Vinyl chloride
ND 0.00200
Qualifiers: k
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Page 32 of 44

Grp d-� mr Summit Environmental Technologies, Inc. QC SUMMARY R l'PORT
' 3310 Win St.
r r;wlHoraru;rJIRL a trsC;. Cuyahoga Falls, Ohio44223 WO#: 17010157
" n lyfl,ff/ Cabnrafo,r/es TEL: [phone] FAX: [phone]
Website: http:llivivw.settelc.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64054
Sample ID mblk
SampType: MBLK
TestCode: voc-mstr_np Units: mg/L
Prep Date:
RunNo: 64054
client ID: PBW
Batch ID: R64054
TestNo: SW8260B
Analysis Date: 1/9/2017
SegNo: 1055656
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Surr: 4-Bro mofluo ro benzene 45.8 50.00 91.5 70
Surr: Dibromofluoromethane 52.2 50.00 104 70
Surr: Toluene-d8 49.7 50.00 99.4 70
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
130
130
130
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 33 of 44

SUMMI'l,
SummitEnvironmental Technolo ies, Inc.g QC sulVIIVIAR�' 1L�EP®1��
'3310 Win St.
�r::vlrrvrar,uinla,l-rt�taaat��t�itis;�r?w. Cuyahoga Falls, Ohio44223 WO#: 17010157
_� A �a14,tl.cal L<Tboj'9lorJe4 TEL: [phone] FAX.- [phone]
Website: htto:Uwww.settelr.com 03-Feb-17
Client: Synagro
Project: Statesville BatchlD: R64094
Sample ID LCS-R64094
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@20.8C
Prep Date:
RunNo: 64094
Client ID: LCSW
Batch ID: R64094
TestNo: SW9045D
Analysis Date: 1/1012017
SegNo: 1056114
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.04 7.000 0 101 98.6 101.4
Sample ID 17010363-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@20.9C
Prep Date:
RunNo: 64094
Client ID: BatchQC
Batch ID: R64094
TestNo: SW9045D
Analysis Date: 1/10/2017
SegNo: 1056116
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH 7.73 7.730 0 5
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 34 of 44

Summit Envionmental Technologies, Inc.
IMAT 3310WinSt. QC SUMMARY REPORT
tr;,vikVr r,11. rani. at:+r:atrauu i o, r;.ti Cuyahoga Falls, Ohio44223 WO#: 17010157
!6riatyUcaS LTbongfuriv4 TEL: [phone] FAX.- [phone]
Website: ham://www.settek.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64094
Sample ID 17010303-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@19.2C
Prep Date:
RunNo: 64094
Client ID: BatchQC
Batch ID: R64094
TestNo: SW9045D
Analysis Date: 1/1012017
SegNo: 1056568
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDUrnit Qua[
pH
7.76
7.760 0 5
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 35 of 44

t
z r
f
SunvnitEnvironmental Technologies, Inc.
3310 Win St.
11.E 6J 1V1 1 K li, 1( J
QC SUMMARYRE, PORT
-ir
tr;vlKVNroll.6JlAl-W4a,ta790LUti3LS.INC
Cuyahoga Falls, Ohio44223
WO#: 17010157
;t,rr321 tf.cal C;Tna,ratFrif
TEL: [phone] FAX..• [phone]
Website: hQ.-Iliv)vw.settelc.coni
03-Feb-17
Client:
Synagro
Project:
Statesville
BatchID: R64153
Cyanide, Reactive ND 0.500
Cyanide, Reactive 1.02 0.500 1.000 0 102 85 110
Cyanide, Reactive 1.04 0.500 1.000 0 104 81.6 122
Sample ID 17010234-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 64153
Client ID: BatchQC
Batch ID: R64153
TestNo: SW9014
Analysis Date: 1/10/2017
SegNo: 1057118
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive
1.01 0.500
1.000 0 101 81.6
122
1.045 3.41 5
Qualifiers:
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7 Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 36 of 44

Summit Environmental Technologies, Inc.
M it —tin? a I v 3310 Win St. QC SUMMARY REPORT
t: NV I HE," N N1 I., rJ I %. I IA.W.-ULUO I �:St INC; Cuyahoga Falls, Ohio 44223
L-aijoraxorie!7 TEL: [phone] FAX.- [phone] WO#: 17010157
Website: hQ.-Iliviviv.settelfcom 03-Feb-I 7
Client: Synagro
Project: Statesville Batch1l): R64153
Sample ID 17010234-001AMSD
SampType: MSD
TestCode: Cyanicle,Rea Units: mg/Kg
Prep Date:
RunNo: 64153
Client ID: BatchQC
Batch ID: R64153
TestNo: SW9014
Analysis Date: 1/1012017
SeqNo: 1057118
Analyte
Result
PQL SPK value SPKRef Val
%REC Lowl-imit HighLimit RPDRef Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 37 of 44

�a, �-
Summit Environmental Technologies, Inc.�,
Win St.Gr;A
QC SUMMARY REP®RT
t�—
LItj�'�+'��3310
Ixra nlratr N I AI G J,�.m�,1ULcti31 sar ��.
Cuyahoga Falls, Ohio 44223
WW#: 17010157
?6t2Yi4Ci:G3i' C;Ti�u�r �loe/r s
TEL: [phone] FAX.- [phone]
Website: httl2J/www.settefc.com
03-Feb-17
Client:
Synagro
Project:
Statesville
BatchID: R64203
Sample ID MB-R64203
SampType: MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 64203
Client ID: PBS
Batch ID: R64203
TestNo: SW9034
Analysis Date: 1/1012017
SegNo: 1057883
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive ND 25.0
Sample ID LCS-R64203
SampType: LCS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 64203
Client ID: LCSS
Batch ID: R64203
TestNo: SW9034
Analysis Date: 1/10/2017
SegNo: 1057884
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive 2980 25.0 2990 0 99.7 85 130115
Sample ID 17010234-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 64203
Client ID: BatchQC
Batch ID: R64203
TestNo: SW9034
Analysis Date: 1/10/2017
SegNo: 1057885
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 2850 25.0 2990 0 95.3 80 120
Sample ID 17010234-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 64203
Client ID: BatchQC
Batch ID: R64203
TestNo: SW9034
Analysis Date: 1/10/2017
SegNo: 1057886
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2910 25.0
2990 0 97.3 80
120
2850 2.08 30
Qualifiers: " Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 38 of 44

<=x as Summit Environmental Technologies, Inc.
� QC SUMMARY' RE PORT
� 3310 Win St.
r:,t IrcV rrraun I 'I ra it, canus�t s .,r;%. Cuyahoga Falls, Ohio 44223 WO#: 17010157
TEL: [phone] FAX [phone]
Website: http:IAvwiv.settelc.com 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64203
Sample ID 17010234-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mglKg
Prep Date:
RunNo: 64203
client ID: BatchQC
Batch ID: R64203
TestNo: SW9034
Analysis Date: 1/10/2017
SegNo: 1057886
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 39 of 44

12. Summit Environmental Technologies, Inc. QC SUMMARY REPORT
" f�,� 3310 Win St. SUMMARY 1V11.1 I REPORT
- ✓1 �: il" L}�4�rr ,
Le, 1KVNrnr.MIA a+-.i.H?aULUGI s INC Cuyahoga Falls, Ohio44223 WO#: 17010157
i4r 4,61-aaf i abor:aforip TEL: [phone] FAX- [phone]
Website: htto:/hvww.settelc.com 03-Feb-17
Client: Synagro
Project: Statesville BatchED: R64990
Sample ID 17010178-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070823
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010178-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070824
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010179-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070826
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010179-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070827
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 40 of 44

f++ G 3 [ x �� Summit Environmental Technologies, Inc.
��
k f � N P.� �� 1 f1 3310 Win St. C SUMMARY REPORT
} tr.:VlrtV'N614N 116 A t:�:�ts",!L�Ltf€II�S, 1P;� Cuyahoga Falls, Ohio 44223
t ,<6nait`1i•c.�f-miaar�ra�TeS TEL: [phone] FAX.- [phone] WO#: 17010157
Website: http://ivivml.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64990
Sample ID 17010179-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070827
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 17010177-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070829
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability Ion -flammable. 0 0 20
Sample ID 17010177-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070830
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010154-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070832
Analyte
.Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Jon -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 41 of 44

/
C w
,r
r '+ L,RR t� H
Summit Environmental Technologies, Inc.
33I0 lf�irt St.
r�
r SUMMARY
tTT p �T REPORT
QC SdJMMARY R POR
LNNIko N7,11.n t.u, r t:� a�tauut�t�s; Jr;,:
Cuyahoga Falls, Ohio 44223
I_.
_
r1.7t1y'L:ca1 Labor9ront:s
TEL: [phone] FIX- [phone]
WO#: 17010157
Website: htty:/hviviv.settelc.coni
03-Feb-17
Client:
Synagro
Project:
Statesville
BatchID: R64990
Sample ID 17010154-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070833
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
itability Jon -flammable. - 0 0 20
mple ID 17010154-002ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
ent ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070835
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability Ion -flammable. 0 0 20
Sample ID 17010154-002ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070836
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability Jon -flammable. 0 0 20
mple ID 17010157-001ADUP
SampType: DUP.
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
ent ID: Statesville 4th Cree
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070838
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: ;k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 42 of 44

Saanmit Environmental Technologies, Inc.
SUMMINtQC SUMMARY ]i�EP®R7i 3310 Win St.
�rwiY.o•r•:rai;rvIALIa:i��uLdt�ts ,JRC. Cuyahoga Falls, Ohio44223 WO#: 17010157
1. _ _ Ar:tg.,U�f L:7bor-gYPfiP,,. TEL: [phone] FAX.- [phone]
Website: httn:/Avwiv.seuek.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchID: R64990
Ignitability Ion -flammable. 0 0 20
Ignitability Ion -flammable. 0 0 20
Ignitability Ion -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 43 of 44

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
R1 ' 3310 lVin St.
+.�;tIk�.�FrrnraN1AL4•I:t:'KmJLuCi1!:5,7lfgc Cuyahoga Falls, Ohio44223 WO#: 17010157.
?4.r, �/xfi ci' C a2aar9toFie� TEL: [phone] FAX.- [phone]
'Website: http://lvivn,.settelc.coni 03-Feb-17
Client: Synagro
Project: Statesville BatchED: R64990
Sample ID 17010234-001ADUP
SampType: DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo:
SW1030
Analysis Date: 2/1/2017
SegNo: 1070844
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17010234-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 64990
Client ID: BatchQC
Batch ID: R64990
TestNo: SW1030
Analysis Date: 2/1/2017
SegNo: 1070845
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability Ion -flammable. 0 0 20
Qualifiers: Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 44 of 44

Sntnrnit Environmental Technologies, Inc,
3310 Win Street
Cuyahoga Faits, Ohio 44223
,.naysi s Request/Chain of Custody
For Summit Emwironaental -rechnologies, Irc. use only
Page of
of 2

N
_ 4—
O
N
d)
00-7 E:1faclmc I)aic 0/+1471E
f?•:v. 16
. uLlr:ti:i �L.Ji�,F't:-Ft.•Ilt:�� iC:t:.it€:GiQ�IG':i, liCiC:.
initials of person inspectin
cooler and samples::
Client:
Order Number:_._-�
� . Ole + ---
Date Received:~
Time Received:l�j Date coolers) opened and
samples inspocied:_.
I' 7
Number of CoolerslBoxes:
_ NIA
Shipper. Foo UPS
DH[- Airborne US Postal Walk-in Pickup Other:
Packaging:
Peanuts eau ble V' ap Paper Foam None Other:
Tape on cooierlbox:
I\
WA
Custody Seals inioct
u
Y N
1 l
C-O-C in plastic
N
ltitfr-.
/1
Ice Blue ice f
1 absent ! melted
"NIA
Sample Temperature IR Gun
16{120h5a CF_& °C .°C
ft
N/A
Radiological Testing Instrument serial V35127 Y N
Q5
(see page 2 for scan results)
"*Use 1 shoot persample for Radiological Tc=sting. 0 sample is HOT, the Radiological Safety Officer must
be nofff.,cct
immedEately.
C-O-G filled out properly
�j N
WA
Samples in separate bags
L•Y N
N/A
Sample containers intact'
LY N
NIA
"It no, list broken sampla(s):,_Y__
��
Sample labal(s) complete (ID, date. etc.)
1 Y
N
NIA
Label(s) agree with C-O•C
N
v!A
Correct containers used
Y
N
NI1A
Sufficient sample raceWd
N
N/A
Samples received within holding time
Y
N
Bubbles absent from 40 mL vials""
Y
N
OfA
— Samples with bubbles <omm are acceptable.
indicate bubble size if'6mm.
.
Was client contacted about samples
Y Nl
Will client send new samples
Y N
Client contact:
Logged Sn by:,
Page 1 of 2

STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
LABORATORY CERTIFICATION BRANCH
in accordance with the prc
)(10) and NCAC 2H.0800.
Summit Environmental Technologies, Inc.
Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data to DEQ for
compliance with NPDES effluent, surface water, groundwater, and pretreatment regulations.
Byrefemnce W NCAC 2H.0800Is made a part ofthis certificate.
This certificate does not guarantee validity of data generated, but Indicates the methodology, equipment, quality control procedures,
records, and proficiency ofthe laboratory have been LAamined and found to be acceptable.
This certificate shall be valid until 12/31/2017
Certificate No. 631
Dana B. Satt wte

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Summit Environmental Technologies, Inc.
Certificate Number: 631
Address: 3310 Win Street
Effective Date: 1/1/2017
Cuyahoga Falls, OH 44223-
Expiration Date: 12/31/2017
Date of Last Amendment: 1/5/2016
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
INORGANIC
SILICA
BOD
EPA 2D0.7, Rev. 4.4, 1994 (Aqueous)
SM 521 D B-2001 (Aqueous)
SW-848 6010 D (Aqueous)
CHLORIDE
, SULFATE
SW-846 9D56 A (Aqueous)
EPA 30D.0, Rev. 2.1, 1993 (Aqueous)
COD
SW-846 9056 A (Aqueous)
SM 5220 CA997 (Aqueous)
SULFIDE
FLUORIDE
SW-846 9034 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
METAL
SW-846 9056 A (Aqueous)
TCLP METALS
INORGANIC PHENOLS
SW-846 1311 (Aqueous)
EPA420,1, Rev. 1978 (Aqueous)
ALUMINUM
NITROGEN, NITRATE
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
N
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
SW-846 6010 D (Aqueous)
0
SW-846 9056 A (Aqueous)
EPA 20D.8, Rev, 5.4, 1994 (Aqueous)
-h
NITROGEN, NITRITE
SW-846 6020 B (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
ANTIMONY
SW-846 9056 A (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
NITROGEN, NO3 + NO2
SW-846 6010 D (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
EPA 200.8, Rev, 5.4, 1994 (Aqueous)
SW-846 9055 A (Aqueous)
SW-846 6020 B (Aqueous)
NITROGEN, TOTAL KJELDAHL
ARSENIC
SM 4500 Norg B-1997 (SM 4500 NH3 D-1997) (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
OIL & GREASE
SW-846 6010 D (Aqueous)
EPA 1664 Rev. B (Aqueous)
EPA 20D.8, Rev. 5.4, 1994 (Aqueous)
SW-846 9071 B (Non -Aqueous)
SW-846 602D B (Aqueous)
PHOSPHORUS, TOTAL
BARIUM
EPA 200.7, Rev. 4.4 (1994) (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Aqueous)
RESIDUE, DISSOLVED 180 C
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SM 2540 C-1997 (Aqueous)
SW-846 6020 B (Aqueous)
RESIDUE, SUSPENDED
BERYLLIUM
SM 2540 0-1997 (Aqueous)
EPA 200.8, Rev, 5A, 1994 (Aqueous)
RESIDUE, TOTAL
SW-B46 6020 B (Aqueous)
SM 2540 B-1997 (Aqueous)
BORON
This certification requires maintanee of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboralodes are subject to civil etwdo
as set forth In 15A NCAC 21-1.0807.

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Summit Environmental Technologies, Inc.
Certificate Number: 631
Address: 3310 Win Street
Effective Date: 1/112017
Cuyahoga Falls, OH 44223-
Expiration Date: 12/31/2017
Date of Last Amendment: 1/5/2015
The above named laboratory, having duly met the requirements of 15A NCAC 2H.01300, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 5010 D (Aqueous)
SW-846 6D20 B (Aqueous)
MAGNESIUM
CADMIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 5010 D (Aqueous)
SW-846 6D10 D (Aqueous)
MANGANESE
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
EPA 200.7, Rev, 4.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 5010 D (Aqueous)
CALCIUM
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 6010 D (Aqueous)
MERCURY
CHROMIUM TOTAL
EPA 245.1, Rev, 3.0, 1994 (Aqueous)
EPA 200.7, Rev, 4.4, 1994 (Aqueous)
SW-846 7470 A (Aqueous)
SW-846 6D10 D (Aqueous)
EPA 1631 E (Aqueous)
W
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
MOLYBDENUM
0
SW-846 6020 B (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
*
COBALT
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6020 B (Aqueous)
EPA 200.8, Rev, 5.4, 1994 (Aqueous)
NICKEL
SW-846 6020 B (Aqueous)
EPA 20D.7, Rev. 4.4, 1994 (Aqueous)
COPPER
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6020 B (Aqueous)
EPA 200.8, Rev, 5.4, 1994 (Aqueous)
POTASSIUM
SW-846 6020 B (Aqueous)
EPA 200.7, Rev, 4.4, 1994 (Aqueous)
IRON
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1904 (Aqueous)
SELENIUM
SW-846 6010 D (Aqueous)
EPA 20D.7, Rev, 4.4, 1994 (Aqueous)
LEAD
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 2018, Rev. 5.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6020 B (Aqueous)
EPA 200.8, Rev. 6.4, 1994 (Aqueous)
SILVER
SW-846 6020 B (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
LITHIUM
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
This certification requires maintance of an acceptable qualityassurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penalties and or catamn�tian im 7nfrPrt•9nD
as set forth In 15A NCAC 21-1.0807.

North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Summit Environmental Technologies, Inc.
Certificate Number: 631
Address: 3310 Win Street
Effective Date: 1/1/2017
Cuyahoga Falls, OH 44223-
Expiration Date: 12/31/2017
Date of Last Amendment: 1/6/2016
The above named laboratory, having duly met the requirements of 15A NCAC 2H.08DD, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
SW-846 6020 B (Aqueous)
CHLORINATED PHENOLICS
SODIUM
EPA 1653, Rev. A, 1997 (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EXTRACTABLE PETROLEUM HYDROCARBONS
SW-846 6010 D (Aqueous)
MADEP, May 2004, Rev. 1.1 (Aqueous)
STRONTIUM
NONHALOGENATED VOLATILE, ORGANICS
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 8015 C (Aqueous)
SW-846 6010 D (Aqueous)
PESTICIDES, ORGANOCHLORINE
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
EPA BOB (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 8081 B (Aqueous)
THALLIUM
POLYCHLORINATED BIPHENYLS (PCBs)
EPA 20D.7, Rev. 4.4, 1994 (Aqueous)
EPA 608 (Aqueous)
v
SW-846 8010 D (Aqueous)
SW-846 8082 A (Aqueous)
EPA 200.8, Rev_ 5.4, 1994 (Aqueous)
PURGEABLE, ORGANICS
Cn
-P
SW-846 6020 B (Aqueous)
EPA 624 (Aqueous)
TIN
SW-846 8260 B (Aqueous)
—�
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
TOTAL ORGANIC HALIDES
SW-846 6010 D (Aqueous)
SW-846 9020 B (Aqueous)
VANADIUM
TPH DIESEL RANGE, ORGANICS
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 8015 C (Aqueous)
SW-846 6020 B (Aqueous)
TPH GASOLINE RANGE, ORGANICS
ZINC
SW-846 8015 C (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
VOLATILE PETROLEUM HYDROCARBONS
SW-846 6010 D (Aqueous)
MADEP, May 2004, Rev. 1.1 (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
ORGANIC
TCLP ORGANICS
SW-846 1311 (Aqueous)
ADSORBABLE ORGANIC HALIDES
EPA 1650, Rev. C, 1997 (Aqueous)
BASE NEUTRAUACID, ORGANICS
EPA 625 (Aqueous)
SW-946 8270 D (Aqueous)
CHLORINATED ACID HERBICIDES
SW-B46 8151 A (Aqueous)
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penaltiss en 3ftiir dei�rtttca1F7f1(f f hlfftlGtiulia•
as set forth In 15A NCAC 21-1.0607.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP WQ Permit Number
WWTP Name: Statesville Fourth Creek WWTP NPDES Number:
WQ 0016247
NC 0031836
Monitoring Period: From 01/01/17 To 12/31/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf nnnlirahle. to alternative nerformed (Class A or Class B) comalete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6
MPN
<123.5
<131
<140.8
MPN/g
0
Annual
Grab
Sm9221ce
Coliform
power per gram
- 2006
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for f Ise certification' including fine and
imprisonment."
®��--b Lever-C �� 1"Ze�tt�
Pr r m nd Tille type or print) Land Applier Name and itle (if applicable _(type or print)
�.4?L_L1
Si natur of Preparer* a Signatu d ppli (if applicabl7e)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
02/02/2017
Reported:
02/03/2017
For:
4th Creek
Comments:
Geometric Mean <131 MPNIg
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
170202-14-01
Fecal Coliforms
1
<134.2
MPN/g
SM92210E-2006
02/02/2017
WC
170202-14-01
Percent Solids
1
14.9
%
SM25498-1997
02/02/2017
WC
170202-14-02
Fecal Coliforms
2
<123.5
MPN/g
sM92210E-2005
02/02/2017
WC
170202-14-02
Percent Solids
2
16.2
%
SM254OB-1997
02/0212017
WC
170202-14-03
Fecal Coliforms
3
<135
MPNIg
SM92210E-2006
02/02/2017
WC
170202-14-03
Percent Solids
3
14.8
%
SM254OB-1997
02/02/2017
WC
170202-14-04
Fecal Coliforms
4
<133.1
MPN/g
sM922'cE-2006
02/02/2017
WC
170202-14-04
Percent Solids
4
15.03
%
SM254OB-1997
02/02/2017
WC
170202-14-05
Fecal Coliforms
5
<125.8
MPNIg
SM92210E-2006
02/02/2017
WC
170202-14-05
Percent Solids
5
15.9
%
SM254OB-1997
02/02/2017
WC
170202-14-06
Fecal Coliforms
6
<140.8
MPN/g
SM92210E-2006
02/02/2017
WC
170202-14-06
Percent Solids
6
14.2
%
SM25405-1997
02/02/2017
WC
170202-14-07
Fecal Coliforms-
7
<124.2
MPN/g
SM92210E-2006
02/02/2017
WC
170202-14-07
Percent Solids
7
16.1
%
SM254OB-1997
02/02/2017
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 a Statesville, NC 28687 0 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 170202-14-01 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosuffate Received on Ice
Sample Number 170202-14-02 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-14-03 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-14-04 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosuffate Received on Ice
Sample Number 170202-14-05 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-14-06 Temp on Arrival: 3
PC Box 228 • Statesville, NC 28687. 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on ice
Sample Number 170202-14-07 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 . Statesville, NC 28687 • 704/872/4697
Page 3 of 4

by.
Parameters mquested fotanaWs
Relinquished by;
Time (9Pm Date
Received by;
Time pm Date �Z /� 7
Relinquished by;
Received by;
CoMpos;te Samol_ __ in_a #y,
Time begin_
am, pm pate __/�
Time end_
ampm Date
Campo f 4�t,,..iirra
ire
Time begin.
am. Pm Dated r
Ttme end__
am, Pm Date�l /
Time �- am, Pm Date
lime am, Pm Date
Lab Comments;
STATESVtLLEANALYTTCAL
'22 CO- Street • PO, Box 228
S=svillr= 28687
[phone]
Chain of
Custody Retard
Sampled by. —kw Vlq-11
Transported by.
Holding times met;
Compliance wok. ✓
Non-compliance work;
r`
rn
N p
r0 �}
00 �
Vj- o�
CD tL
00
Q0
00
41
U
ai
.j
41
N
s
00
N
N
X
O
0
a

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
8.25
8.2
8.17
8.06
7.96
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1 1/3/17 2:15 PM 1
1 1/3/17 2:22 PM 1
300
1.72
13.1
14.7
0.1
8.3
1.0
iilliliters
o Dry Solids
egrees Celsius
egrees Celsius
5.12 mg Oxygen/hr
0.99 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:1 1.49 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
7.61
7.52
7.41
7.37
7.21
7.15
Slope:
Intercept:
Correlation Coefficient:
Oxygen. Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek WWTP
1 1 /4/2017 1
13
1/4/2017 100 PM
EA
1/4/17 107 PM
300
71 6
13.2
0.1
7.6
1.0
illiliters
Dry Solids
;grees Celsius
:grees Celsius
5.04 mg Oxygen/hr
0.95 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:1 1.43 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9.21
9.26
9.21
9.11
9.02
8.98
8.87
8.74
8.67
8.63
58 8
8.41
8.32
8.26
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
(Fourth Creek VW1/TP
1 /5/2017
12.4
1/5/2017 100 PM
RG
1/5/17 108 PM
BJ
300
1.6
12.7
0.1
9.3
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
4.37 mg Oxygen/hr
0.9.1 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate:j 1.46 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility
Biosolids Permit N
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes) (mg/l)
0
8.49
1
8.47
2
8.43
3
8.31
4
8.26
5
8.24
6
8.13
7
8.1
8
8.06
9
7.99
10
7.94
11
7.9
12
7.84
13
7.72
14
7.67
15
7.61
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WQ0016247
1/6/2017
1 1/6/2017 100 PM 1
1 1/6/2017 110 PM 1
300
1.72
15.8
16.7
0.1
8.5
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
3.54 mg Oxygen/hr
0.69 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.90 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
9.67
1
9.69
2
9.62
3
9.57
4
9.51
5
9.55
6
9.5
7
9.39
8
9.34
9
9.27
10
9.15
11
9.06
12
8.99
13
8.89
14
8.86
15
8.82
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
WO0016247
1 /9/2017
14.9
1/9/2017 138 PM
RG
1/9/2017 147 PM
300
1.8
15.1
15.5
0.1
9.8
1.0
Aliliters
o Dry Solids
egrees Celsius
egrees Celsius
3.77 mg Oxygen/hr
0.70 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.98 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
=1
9.52
9.43
9.35
9.21
9.19
9.14
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
W Q 0016247
1/10/2017
15.7
1/10/2017 150 PM
RG
1/10/2017 200 PM
BJ
300
1.81
15.8
16.5
0.1
10.2
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4.04 mg Oxygen/hr
0.74 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.98 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
2
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9.08
9.01
8.91
8.83
8.74
8.65
8.55
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
WQ0016247
1/11/2017
13.7
1/11/2017 135 PM
1 1/11/2017 148 PM 1
300
1.7
14.5
15.7
0.1
9.9
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
5.26 mg Oxygen/hr
1.03 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 1.45 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville
WQ Permit Number: WQ 0016247
WWTP Name: Statesville Third Creek WWTP NPDES Number: NC 0020591
Monitoring Period: From 01/01/17 To 12/31/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: ❑
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf ..h�ohlo +n of+pr ot:c prfnrmprl /f lace A nr ('hee Rl emmnipfp fhn fnllnwina mnnitnrinv rinf5k-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6 th
MPN
<123.5
<129
<141.8
MPN/g
0
Annual
Grab
SM9221 C
Coliform
power per gram
E-2006
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Mt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-daybench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Mt. 6
Option/Ah. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable) _
Option/Mt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate t e information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are si is t penalties for false certifigation including fine and imprisonment."
P p 1 r Name and Title ( type or print) l $at,
y Land Applier
b'na•
Si e of Pre arer* Signature o ]
P
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Applier
e or print)
'- -21
ate

1
Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 02/02/2017
Reported: 02/03/2017
For: 3rd Creek
Comments: Geometric Mean <129 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
170202-13-01
Fecal Coliforms
1
<123.5
MPN/g
sM92210E-2006
02/02/2017
WC
170202-13-01
Percent Solids
1
16.2
%
SM254OB-1997
02102/2017
WC
170202-13-02
Fecal Coliforms
2
<125.8
MPNIg
SM92210E-2006
02/02/2017
WC
170202-13-02
Percent Solids
2
15.9
%
SM254OB-1997
02/02/2017
WC
170202-13-03
Fecal Coliforms
3
<135
MPN/g
SM92210E-2006
02/02/2017
WC
170202-13-03
Percent Solids
3
14.8
%
SM254OB-1997
02/02/2017
WC
170202-13-04
Fecal Coliforms
4
<127.4
MPN/g
SM92210E-2006
02/02/2017
WC
170202-13-04
Percent'Solids
4
15.7
%
SM2540B-1997
02/02/2017
WC
110202-13-05
Fecal Coliforms
5
<141.8
MPN/g
SM92210E-2005
02/02/2017
WC
170202-13-05
Percent Solids
5
14.1
%
8M2540e4997
02/02/2017
WC
170202-13-06
Fecal Coliforms
6
<126.6
MPN/g
SM92210E-2006
02/02/2017
. WC
170202-13-06
Percent Solids
6
15.8
%
SM254OB-1997
02/02/2017
WC
170202-13-07
Fecal Coliforms
7
<125
MPN/g
SM9221cE-2006
02/02/2017
WC
170202-13-07
Percent Solids
7
16.0
%
SM254OB-1997
02/02/2017
WC.
Respectfully submitted,
D? -WO-J-07t,
Dena Myers
NC Cert #440,
NCDW Cert#37755,
EPA #NC00909
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 1 of 4 .

Condition of Receipt
Sample Number 170202-13-01 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-13-02 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-13-03 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-13-04 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-13-05 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-13-06 Temp on Arrival: 3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 170202-13-07 Temp on Arrival: 3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Contact Person;
PO #
Phone #
Customer
Requisiti
Sample IAA
Lab-11) N
'rime Sampled
(Grab Only)
nets Sal
•�--
(Gmbor
t
-QFO
n --7
SPAnSVZLEANALYTICAL
122 Court street • pa, Bax 228
Slarasvllle, NC 28687
(704) 872-d697
Chain of
Date) Custody Record
Parameters mquimted for anatyats
Refinquished by.
Received by:
Time I Pm Date 1 J
—�
Sampiedby; 41
64r�
Relinquished by:
Time 17W 0. Pm Date I? /� �
L�
Transported by.
Received by:
Time am, pm Date „/
Molding times rnet
Corhnos;t�gam fin #�:
Tfine am, Pm Date__Time
Compliance
begin_am.
pm Date �/ �
work
-�.-�
Time end,
am m
P Date �/�
Non-compliance work:
Cgmgo-"� °Y�==�P�Q�-
Lab Comments:
Time begin_
am m Date
Time endue_
am Pm bate
r\
tn
IM
N o
C�)
� C1.
00
W
(.O
co
N
U
z
aD
00
N
N
X
0
m
0

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.89
8.84
881
8.76
8.65
8.6
8.54
8.44
8.38
8.33
8.29
8.2
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1/3/2017
13.4
1/3/17 14:09
SA
1/3/17 14:19
300
1.8
138
15.7
0.0
8.9
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.78 mg Oxygen/hr
0.51 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.72 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
. M,
5.96
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
1 /4/2017
11.1
1/4/17 9:02
SA
1/4/17 9:10
SA
300
1.9
11.4
12.6
0.1
6.8
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
3.55 mg Oxygen/hr
0.62 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1 1.07 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.97
1
6.93
2
6.87
3
6.84
4
6.79
5
6.73
6
6.68
7
6.64
8
6.6
9
6.57
10
6.52
11
6.48
12
6.44
13
6.41
14
6.35
15
6.29
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1 Third Creek WWTP 1
1/5/2017
10.8
1/5/17 8:57
1/5/17 9:08
SA
300
1.9
2.3
0.0
7.0
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
2.65 mg Oxygen/hr
0.46 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1 0.80 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
1 /612017
11.1
1/6117 8:48
SA
1/6/17 8:56
SA
300
1.9
11.3
12.6
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.48
1
7.45
2
7.4
3
7.36
4
7.31
5
7.27
6
7.22
7
7.18
8
7.13
9
7.1
10
7.05
11
7
12
6.97
13
6.94
14
6.91
15
6.85
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.5
1.0
2.53 mg Oxygen/hr
0.44 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:j 0.76 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
8.91
8.86
8.81
8.77
8.69
8.61
8.58
8.54
8.51
8.46
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP I
1/12/2017
10.6
1/12/17 9:03
SA
1/12/17 9:11
SA
300
1.9
11.6
0.0
8.9
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.56 mg Oxygen/hr
0.45 mg Oxygen/g/hr
11 degrees Celsius
1.838459212
Temperature Corrected Specific Oxygen Uptake Rate: 0.83 jmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
1 /13/2017
Digester Temperature:
10.6
Sampling Date/Time:
1/13/17 7:12
Sampled By:
SA
Analysis Date/Time:
1/13/17 7:21
Analyzed By:
SA
Sample Volume:
300
milliliters
Total Solids:
1.9
% Dry Solids
Beginning Temperature:
11.8
degrees Celsius
End Temperature:
13.1
degrees Celsius
Dissolved Oxygen Level
(mg/1)
8.64
8.58
8.53
8.47
8.42
8.35
8.31
8.27
8.24
8.19
8.13
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
8.6
1.0
3.09 mg Oxygen/hr
0.54 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate: 0.93 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Agricultural Lime Application Log
Year: 2017
Project: Statesville
Field
Soil
Lime Requirement
Tons/Acre
Date Applied
11 (state -county -site -field)
pH
(from soil analysis)
Applied(CCE Eq.)
AL-13-1 A
6.9
O.OT/Ac.
AL-1 3-1 B
6.9
O.OT/Ac.
I R-23-02
6.1
O.OT/Ac.
IR-23-04
6.8
O.OT/Ac.
I R-23-05
6.2
O.OT/Ac.
`Lime will be applied when conditions improve.

Page 1 of 2
Report Number: 17-341-0865
Account Number: 46488
Send To: SYNAGRO CENTRAL LLC/SALISBURY
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 12/07/2017
Date Of Analysis: 12/08/2017
"Every acre... Every year. "rM
SOIL ANALYSIS REPORT
Date Of Report: 12/11/2017
Grower: Danny Millsaps
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
%
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pp m Rate
pp m Rate
ppm Rate
p H
Index
meq/100g
meq/100g
1A
15900
6.5
150
343 VH
237 VH
323 H
1661 M
43 VL
6.9
0.2
12.0
I MIN
H
NC = 286
NC = 121
1 B
15901
6.3
150
315 VH
85 L
268 H
1556 H
24 VL
6.9
0.1
10.4
HH
NC = 262
NC = 43
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO, N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pp Rate
ppm m Rate
ppm Rate
mslcm Rate
1A
5.1
22.4
69.2
1.6
1.7
20 M
26.6 VH
18 M
182 VH
18.6 VH
1.0 M
0.18 VL
NC=42
NC=665.0
NC=113
NC=930.0
1B
2.1
21.5
74.8
1.0
1.0
7 VL
23.8 VH
20 M
258 VH
14.3 VH
0.9 M
VL
0.177
1
5
NC=595.0
NC=1,
NC
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: � r`
C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm.
Analysis prepared by: Waypoint Analytical Virginia, Inc.
Pauric McGroary

Page 2 of 2
Report Number: 17-341-0865
Account Number:46488
Send To: SYNAGRO CENTRAL LLC/SALISBURY
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 12/07/2017
Date Of Report: 12/11/2017
"Every acre... Every year. "r
SOIL FERTILITY RECOMMENDATIONS
Grower: Danny Millsaps
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
VA
Ib/A
1A
Adjust pH to 6.0
0
0.0
0
2
0
1B
Adjust pH to 6.0
0
0.0
0
2
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

NCDA&CS A.. _—mic Division Phone: [phone]
Website: www.nc.u..uov/agronomi/
Report No. FY17-oi-W5002
`-'I•,.�11;�
Predictive
Client:
Shane Porter
351 Gantt Horn Rd.
Advisor:
Synagro
_•.I
I,
Statesville, NC 28677
284 Boger Rd
Mocksville, NC 27028
a
�Iti:4 "fir ®i Report Mehlich-3 Extraction
c
Sampled County : Iredell
_Links to Helpful Information
Client ID: 420431
Advisor
ID: 404711
Sampled:04/20/2017 Received: 06/01/2017 completed: 06/12/2017
Farm: IR-23
Sample ID: 23-02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
0
0
0
0
Note: 12
2-
Test Results [units - W/V in g/crrt3; CEC and Na in meq/100 ca; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.56 0.99 14.0 90 1.4 6.1 328 143
72 13
63
372
238
618
618
389
0.1 1
Sample ID: 23-04
Recommendations: Lime
Nutrients (Ib/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
pH$
0
0
0
Note: 12 Note:
2-
Test Results [units - WfV in g/cm3; CEC and Na in meq/100'cO; NO3-N in mg/dO]:
Soil Class.
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-1
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.46 0.98 14.7 96 0.6 6.8 333 123
80 12
55
280
174
406
406
305
0.1 1.
Sample ID: 23-05
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
0
0 0
0
0
0
0
Note: 12
2-
Test Results [units -WN in g/cm3; CEC and Na in meq/100 c0; NO3-N in mg/do]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-AI1 Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.41 0.99 14.2 91 1.2 6.2 438 156
74 12
63
296
191
499
499
360
0.1 1
or h Cardirla
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS A_ mic Division Phone: [phone]
Website: www.n(.-,,..,3v/agronomi/
Report No. FY17-OLUo5002
Shane Porter
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on(
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50: If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www ncagr gov/agronomi/oboart4 htrMWsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilize
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility�measurement. Visit www.ncagr.c1ov1agronomWuyrst.htm
Page 2 of 2
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P206
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

2017 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
STANLY COUNTY UTIL., NC (FKA OAKBOR
STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
DRY METRIC
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
March 2017
403,000.00
G
40.83
D
37.05
April 2017
365,800.00
G
37.07
D
33.63
October 2017
415,400.00
G
42.10
D
38.19
YEARLY TOTAL
1,184,200.00
G
120.00
D
108.87
2/1 /2018

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0005387 Laboratory
Facility Name: STANLY COUNTY UTIL., NC (FKA OAKBORO) Waypoint Analytical Virginia Inc.
NPDES# : NCO043532
or WQ# (residual only)
WWTP Name: WEST STANLY WWTP (FKA OAKBORO WWTP)
Residuals Analysis Data
Product Type LIQ
Date Sampled (grab) or 01/31/17
Date Composited
Percent Solids 2.43
PARAMETERS (mg/kg dry weight)
Arsenic
8.15
Cadmium
<2
Mercury
1.08
Chromium
55.7
Copper
261
Lead
23.7
Molybdenum
13.9
Nickel
30.7
Selenium
8.43
Zinc
883
Total Phosphorus
17800
TKN
50000
Ammonia -Nitrogen
6560
Nitrate and Nitrite
1550
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X Date 2 / ( Ct /i
(SIGNATURE OF P ER)
DENR FORM RSSF (5/2003) Printed: Thursday - February 1, 2018 at 11:23:33 for: 2170 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
WQ0005387
Facility Name
STANLY COUNTY UTIL., NC (FICA
NPDES#
NC0043532
or WQ# (residual only)
WWTP Name
WEST STANLY WWTP (FKA
Residual Analysis Data
Product Type
LIQ
Date Sampled
01/31/17
Date Composited
Percent Soilds
2.43
PARAMETERS (mg/kg dry weight)'
Aluminium
12300
Calcium
16400
Magnesium
13400
pH
6.84
Potasium
3630
Sodium
2020
PAN
17862
SAR
0.439961
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
X Date
(SIGNATURE REPARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/6/2018 12:44:41 PM

Page: 1 of 2
Report Number: 17-032-0201
Account Number: 46477
Submitted By: Clay Fisackerly
Send To: Synagro Central LLC/ Stanly County Utilities
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61986
Sample Id : West Stanly Utilities
Waypoint0 (2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : West Stanly Utilities
NC Cert#257
REPORT OF ANALYSIS Date Sampled: 1/31/2017 09:45:00
Date Received: 02/01/2017 00:00
Date Reported: 02/07/2017
Total Solids *
2.43
24300
100.0
R D
02/01/2017 14:00
SM-2540G
Moisture *
97.56
100.0
R D
02/01/2017 14:00
SM-254OG
Total Kjeldahl Nitrogen
5.00
50000
10.0
JM
02/04/2017 11:00
SM-4500-NH3C-TKN
Total Phosphorus
1.78
17800
100
JTR
02/06/2017 18:39
6010C
Total Potassium
0.36
3630
1000
JTR
02/06/2017 18:44
6010C
Total Sulfur
0.94
9370
100
JTR
02/06/2017 18:39
6010C
Total Calcium
1.64
16400
100
JTR
02/06/2017 18:39
6010C
Total Magnesium
1.34
13400
100
JTR
02/06/2017 18:39
6010C
Total Sodium
0.20
e
2020
100
JTR
02/06/2017 18:39
6010C
Total Iron
19000
100
JTR
02/06/2017 18:39
6010C
Total Aluminum
12300
100
JTR
02/06/2017 18:39
6010C
Total Manganese
580
5.00
JTR
02/06/2017 18:39
6010C
Total Copper
261
5.00
JTR
02/06/2017 18:39
6010C
Total Zinc
883
5.00
JTR
02/06/2017 18:39
6010C
Ammonia Nitrogen
0.66
6560
10.0
JM
02/04/2017 10:50
SM-4500-NH3C
Organic N
4.34
43440
10.0
02/04/2017 10:50
CALCULATION
Nitrate+Nitrite-N
1550
2.45
SJB
02/02/201714:35
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Page: 2 of 2
Report Number: 17-032-0201
Account Number: 46477
Submitted By: Clay Fisackerly
Send To: Synagro Central LLC/ Stanly County Utilities
Mary. Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 61986
Sample Id : West Stanly Utilities
(2)
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : West Stanly Utilities
NC Cert#257
REPORT OF ANALYSIS Date Sampled: 1/31/2017 09:45:00
Date Received: 02/01/2017 00:00
Date Reported: 02/07/2017
Total Cadmium
<2.00
2.00
JTR
02/06/2017 18:39
6010C
Total Chromium
55.7
5.00
JTR
02/06/2017 18:39
6010C
Total Nickel
30.7
5.00
JTR
02/06/2017 18:39
6010C
Total Lead
23.7
5.00
JTR
02/06/2017 18:39
6010C
Total Arsenic
8.15
3.00
JTR
02/06/2017 18:39
6010C
Total Mercury
1.08
0.400
SJB
02/02/2017 10:45
SW-7471 B
Total Selenium
8.43
5.00
JTR
02/06/2017 18:39
6010C
pH (Standard Units) *
6.84
1.00
R D
02/02/2017 08:30
SW-9045D
Total Molybdenum
13.9
5.00
JTR
02/06/2017 18:39
6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2170-01-LIQ-NC STANLY COUNTY UTIL., NC WEST STANLY 1/31/2017 111/2017-12/3112017 0.4400
WWTP AEROB DIG LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (2020 x 2.4300) + 100 = 49.086
Ca mg/1= (Ca mg/kg x % Solids) + 100 = (16400 x 2.4300) + 100 = 398.52
Mg mg/I = (mg mg/kg x % Solids) + 100 = (13400 x 2.4300) + 100 = 325.62
Na meq = Na mg/I + Molec.Wgt.Na = 49.086 + 23 = 2.13417
Ca meq = Ca mg/I + Molec.Wgt.Ca = 398.52 = 20 = 19.926
Mg meq = Mg mg/I + Molec.Wgt.Mg = 325.62 + 12 = 27.135
SAR = Na meq : SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.13417 + SgrRoot[0.5(19.926+27.135)] = 0.439961
Printed: 2/1 /2018
Page 1 11:25

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAIOO PREDOMINANT SOIL SERIES: GOLDSTON
WNER: ROBERT RIDENHOUR PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 11.94
iTE #: NC ST 00003 FIELD# : ST 00003 0004 OPERATOR: ROBERT RIDENHOUR CATION EXCHANGE CAPACITY (NON-503):
ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.40 ACRES PERMITTED: 8.40
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
3/24/17
68,200.00 (G)
8119.048
2.43
0.823
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
3/25/17
18,600.00 (G)
2214.286
2.43
0.224
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
3/27/17
24,800.00 (G)
2952.381
2.43
0.299
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
3/29/17
6,200.00 (G)
738.095
2.43
0.075
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000.p
6,560.00 p
1,550.00 p
17862
FESCUE
Mar-17
117,800.00 (G)
14,023.810
Total Gallons/Ac: 14,023.81
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
lnnuallbs/acre
51
0.023
0.006
0.158
0.742
0.067
0.003
0.040
0.087
0.024
2.510
50.59
:umulative Ibs/acre
0.023
0.006
0.158
0.742
0.067
0.003
0.040
0.087
0.024
2.510
runt PAN Limit (lbs/acre) 1st Crop/2nd Crop
;­77 7 11
a t
i
152
'D Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
t
1339.0
267.9
15.0 i J
375.0
89.0
2500.0
}
ICUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
r
X Z _/1-/F
(S URE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/lcg k* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
'" Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: GOLDSTON
IWNER: ROBERT RIDENHOUR PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 25.13
ITE #: NC ST 00003 FIELD# : ST 00003 0005 OPERATOR: ROBERT RIDENHOUR CATION EXCHANGE CAPACITY (NON-503):
.ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 12.40 ACRES PERMITTED: 12.40
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
3/25/17 .
37,200.00 (G)
3000.000
2.43
0.304
SCUWSAE
MOIST
0-<I/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
3/27/17
68,200.00 (G)
5500.000
2.43
0.557
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
FESCUE
Mar-17
105,400.00 (G)
8,500.000
4/10/17
31,000.00 (G)
2500.000
2.43
0.253
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
4/13/17
37,200.00 (G)
3000.000
2.43
0.304
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
4/14/17
74,400.00 (G)
6000.000
2.43
0.608
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
11162
FESCUE
Apr-17
142,600.00 (G)
11,500.000
Total Gallons/Ac: 20,000.00
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zu
P
PAN
TOTALS:
�tmual lbs/acre
72
0.033
0.008
0.226
1.058
0.096
0.004
0.056
0.124
0.034
3.579
72.15
3umulative lbs/acre
0.033
0.008
0.226
1.058
0.096
0.004
0.056
0.124
0.034
3.579
^�
ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
i
F
:?
b
152
l f
--D Cumulative
Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
F
1339.0
267.9
15.0 375.0
l,.
89.0
2500.0
i
3CUWSAEDL= STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X
2-/y-/S
(SI�NP7URE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
?ACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: BADIN
DWNER: ROBERT RIDENHOUR PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 40.84
iITE #: NC ST 00003 FIELD# : ST 00003 0007 OPERATOR: ROBERT RIDENHOUR CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 18.10 ACRES PERMITTED: 18.10
Page
Lime Applied ***
Date::T
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Total
Per Acre
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
3/29/17
99,200.00 (G)
5480.663
2.43
0.555
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
3/30/17
80,600.00 (G)
4453.0391
2.43
0.451
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
FESCUE
Mar-17
179,800.00 (G)
9,933.702
4/3/17
43,400.00 (G)
2397.790
2.43
0.243
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
4/10/17
43,400.00 (G)
2397.790
2.43
0.243
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
4/11/17
93,000.00 (G)
5138.122
2.43
0.521
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
4/13/17
43,400.00 (G)
2397.790
2.43
0.243
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
FESCUE
Apr-17
223,200.00 (G)
12,331.492
Total Gallons/Ac: 22,265.19
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
81
0.037
0.009
0251
1.178
0.107
0.005
0.063
0.139
0.038
3.984
8032
Cumulative lbs/acre
0.037
0.009
0.251
1.178
0.107
0.005
0.063
0.139
0.038
3.984
?ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
�a
°
P ' _
1 ;'' 1
3`l
'' ' a
t
163
.f
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0 267.9
15.0 375.0
89.0
2500 0
7
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X M-4
(SIMIKE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation "** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
4CILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: BADIN
WNER: ANDERSON LIVING TRUST PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 16.34
TE #: NC ST 00004 FIELD# : ST 00004 0001 OPERATOR: HINRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 26.80 ACRES PERMITTED: 26.80
Page: 1
Lune Applied ***
Date Lbs/Ac
SATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pprm)
Crop
MONTH
Total
Per Acre
Solids
10/10/17
6,200.00 (G)
231.343
2.43
0.023
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
10/11/17
117,800.00 (G)
4395.522
2.43
0.445
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
FESCUE
10/13/17
37,200.00 (G)
1388.060
2.43
0.141
SCUWSAE
DRY
0-<I/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
FESCUE
Oct-17
161,200.00 (G)
6,014.925
Total Gallons/Ac: 6,014.93
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Lnnual lbs/acre
22
0.010
0.002
0.068
0.318
0.029
0.001
0.017
0.037
0.010
1.076
21.70
;umulative lbs/acre
0.073
1 0.045
0.758
8.279
0.562
0.021
0.274
0.413
0.095
16.803
1
1
JJ
1
f
t
122
;rmit PAN Limit (lbs/acre) 1st Crop/2nd Crop
4
;
'D Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
i
1339.0
267.9
15.0 375.0
89.0
2500.0 I
ICUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X
(SIG40T11URE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: BADIN
WNER: ANDERSON LIVING TRUST PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 20.10
[TE #: NC ST 00004 FIELD# : ST 00004 0004 OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90
Page: 1
Lune Applied ***
Date Lbs/Ae
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/6/17
62,000.00 (G)
6966.292
2.43
0.706
SCUWSAE
MOIST
0-<I/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
10/10/17
49,600.00 (G)
5573.034
2.43
0.565
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17862
I FESCUE
10/12/17
86,800.00 (G)
9752.809
2.43
0.988
SCUWSAE
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
6,560.00 p
1,550.00 p
17812
FESCUE
Oct-17
198,400.00 (G)
22,292.135
Total Gallons/Ac: 22,292.13
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
annual lbs/acre
81
0.037
0.009
0.252
1.179
0.107
0.005
0.063
0.139
0.038
3.989
80.42
3umulative lbs/acre
0.037
0.009
1 0.252
1.179
1 0.107
0.005
0.063
0.139
0.038
3.989
+
ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
z''
i ?
,
,
122
��
iD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
¢
1339.0
267.9
15.0 i 375.0
..,
89.0
2500.0
'CUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X
(SIG RE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ACILITY NAME: STANLY COUNTY UTIL., NC (FKA OAKBO PREDOMINANT SOIL SERIES: MISENHEIIvIER
WNER: ANDERSON LIVING TRUST PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 5.65
TE #: NC ST 00004 FIELD# : ST 00004 0005 OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.70 ACRES PERMITTED: 6.70
Page
Lane Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
SATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
m
(pp )
Crop
Total
Per Acre
10/10/17
55,800.00 (G)
8328.358
2.43
0.844
SCUWSAE
MOIST
0-<1/2"
SUR
0.5
6,560.00 p
1,550.00 p
17862
FESCUE
Oct-17
55,800.00 (G)
8,328.358
750,000.p
1
Total Gallons/Ac: 8,328.36
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
annual lbs/acre
30
0.014
0.003
0.094
0.441
0.040
0.002
0.023
0.052
0.014
1.490
30.04
;umulative lbs/acre
0.014
0.003
0.094
0.441
0.040
0.002
0.023
0.052
0.014
1.490
'
rmit PAN Limit 1st Crop/2nd Crop
P
Y
t , '
-
k
110
(lbs/acre)
+k
a
l
�D Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1
y
1339.0
267.9
15.0 y 375.0
89.0
2500.0
!CUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X
(SI -ARE OF LAND APPLIER) DATE
" certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

msummu
fh{t'IRCrtJf�iEtv1'I.L = '4oLri,:_5; T G
�rrdl�`rCsJ'!'ni70fe�Ci i'7P5
March 01, 2017
Clay Fisackerly
Synagro, NC 28134
12701 Lancaster Hwy
Pineville, NC 28134
TEL: [phone]
FAX: [phone]
RE: West Stanly Utilities
Dear Clay Fisackerly:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: htto:/Avivtv.settekcorn
Order No.: 17020619
Summit Environmental Technologies, Inc. received 1 sample(s) on 2/10/2017 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Proj ect Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North
Dakota R-201, Olio Drinking Water 4170, Olio VAP CL0052, Oklahoma 9940, Oregon 0112O0001, Rhode Island LA000317, South Carolina 92016001,
Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
WashingtonC891, West Virginia 9957C
Page 1 of 28
Page 1 of 33

Summit Environmental Technologies, Inc. Case Narrative
IT
SUMM 3310 Win St.
f=h{ ROMMENITALTEGHUOLGGI_S; 7NQ,- Cuyahoga Falls, Ohio44223 WO#: 17020619
An-Hlytira1 Lsbaratore5 TEL: [phone] FAX: [phone]
Website: ham.-1Avww.settek.con: Date: 3/1/2017
CLIENT: Synagro, NC 28134
Project: West Stanly Utilities
This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical
Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler
Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Comments for tclp-voc-mstr_telp(8260), Sample 17020619-001a, Batch ID R66034
Sample exhibited outlying recovery for Surrogate: 4-Bromofluoroberrzene - likely due to dilution. There
are no compounds associated with this surrogate.
Analytical Comments for SVOC-BNA_TCLP(8270), Sample MB-25652, Batch ID 25652: The
Method Blank (Batch 25652) exhibited high recovery for Surrogate: 2,4,6-Tribromophenol; MB was
ND for all analytes of interest.
Original
Page 2 of 28
Page 2 of 33

Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win 5
Era'I^nEDMAENTd.L EC-1JN]La!t_5,INC. Cuyahoga Falls, Ohio442� WO#: 17020619
rirarvClcal L�bor:3rur{�; TEL: [phone] FAX: [phone]
Website: hQ.-1wvviv.settekco. Date: 3/1/2017
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
x The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GUMS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
s The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
-MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 28
Page 3 of 33

z Summit Environmental Technologies, Inc. Workorder
Av 3310 Win St.
ErtVIRONMENTAL :=G Crr,L�Gt s, t t�. Cuyahoga Falls, Ohio 44223 Sample Summary
,Anst,•iicsl Lsboratorfes TEL: [phone] FAX.- [phone] WO#: 17020619
Website: hqp://wivw.settek.com 01 Mar-17
CLIENT: Synagro, NC 28134
Project: West Stanly Utilities
Lab SampleID Client Sample ID
17020619-001 West Stanly TCLP 2017
Tag No Date Collected
2/9/2017 10:00:00 AM
0
Date Received Matrix
2/10/2017 9:40:00 AM Sludge
Page 4 of 28
Page 4 of 33

r Summit Environmental Technologies, Inc. DATES REPORT
Surmaly 3310 Win St.
ENVIRoN:olrWALTECHW00E6F ;rdc. Cuyahoga Falls, Ohio44223 WO#: 17020619
A .IJ41tdraP b3borai`Drh,s TEL: [phone] FAX.- [phone]
Website: hI&11ww1v.settek.com 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
17020619-OOIA West Stanly TCLP 2017 2/9/2017 10:00:00 AM Sludge Ignitability of Solids (SW-846: 1030) 2/15/2017 8:00:00 AM
pH (SW9045D) 2/22/2017 3:15:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid 2/21/2017 10:47:00 AM
Reactive Sulfide (9034) 2/21/2017 10:47:00 AM
SVOC 8270 TCLP BNA List 2/21/2017 4:44:39 PM 2/23/2017 8:00:00 AM 2/24/2017 4:50:00 PM
SVOC SW-846: 8081-TCLP Pesticide! 2/21/2017 4:44:39 PM 2/28/2017 8:30:00 AM 2/28/2017 2:58:00 PM
SVOC SW-846: 8151 Herbicides-TCL2/21/2017 4:44:39 PM 2/23/2017 12:10:00 PM 2/28/2017 8:09:00 PM
TCLP Mercury Analysis (1311/7470) 2/21/2017 4:44:39 PM 2/22/2017 10:00:00 A 2/22/2017 4:13:00 PM
�R
TCLP Metals Analysis (6010) 2/21/2017 4:44:39 PM 2/22/2017 10:17:05 A 2/23/2017 11:47:32 AM
�2
VOC by GC/MS (8260)-TCLP 2/23/2017 5:35:00 PM
Original
Page 5 of 28
Page 5 of 33

Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
Y
t=. fttl iOfJhlEhT4Lu3 P•t�L�l�s; srtr_
Cuyahoga Falls, Ohio 44223
(base report)
A;-alytical Laberatooes
TEL: (330)
253-8211 FAX: [phone]
W04: 17020619
Website: http://wivw.settekeoni
Date Reported: 3/1/2017
CLIENT: Synagro, NC 28134
Tag Number:
Matrix: SLUDGE
Collection Date:
2/9/2017 10:00:00 AM
Lab ID: 17020619-OOIA
Project: West Stanly Utilities
Client Sample ID West Stanly TCLP 2017
Analyses Result
PQL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (1311/7470)
TCLP Mercury
ND
0.00200
mg/L
1
2/22/2017 4:13:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010C
SW3010A Analyst: VVK
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
2/23/2017 11:47:32 AM
TCLP Barium(Ba)
ND
5.00
mg/L
1
2/23/2017 11:47:32 AM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
2/23/2017 11:47:32 AM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
2/23/2017 11:47:32 AM
TCLP Lead(Pb)
ND
0.500
mg/L
1
2/23/2017 11:47:32 AM
TCLP Selenium(Se)
ND
0.500
mg/L
1
2/23/2017 11:47:32 AM
TCLP Silver(Ag)
ND
0.500
mg/L
1
2/23/2017 11:47:32 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270C
SW3510C Analyst: CxA
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
2/24/2017 4:50:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
2/24/2017 4:50:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
2/24/2017 4:50:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
2/24/2017 4:50:00 PM
Cresols, Total
ND
4.00
mg/L
2
2/24/2017 4:50:00 PM
Hexachloro-1,3-butadiene
ND
0.100
mg/L
2
2/24/2017 4:50:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
2/24/2017 4:50:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
2/24/2017 4:50:00 PM
Nitrobenzene
ND
0.0800
mg/L
2
2/24/2017 4:50:00 PM
Pentachlorophenol
ND
0.200
mg/L
2
2/24/2017 4:50:00 PM
Pyridine
ND
0.200
mg/L
2
2/24/2017 4:50:00 PM
Surr: 2-Fluorophenol
61.4
10 - 109
%Rec
2
2/24/2017 4:50:00 PM
Surr: Phenol-d6
57.4
10 - 109
%Rec
2
2/24/2017 4:50:00 PM
Surr: Nitrobenzene-d5
75.6
19 - 120
%Rec
2
2/24/2017 4:50:00 PM
Surr: 2,4,6-Tribromophenol
91.0
10 - 120
%Rec
2
2/24/2017 4:50:00 PM
Surr: 2-Fluorobiphenyl
74.6
22 - 117
%Rec
2
2/24/2017 4:50:00 PM
Surr: p-Terphenyl-d14
85.0
34 - 116
%Rec
2
2/24/2017 4:50:00 PM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
RL Reporting Detection Limit W Sample container temperature is out of limit as specified at testcode
Original
Page 6 of 28
Page 6 of 33

Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
r tF rl i 1hIPilEA'I'a1L Ei �fi Cdr3L1G1_5; WC- Cuyahoga Falls, Ohio 44223 (base report)
Arralt+tic31 L iharatorlez. TEL: [phone] FAX: [phone] WO#: 17020619
Website: h=.-11wivw.settekcom Date Reported: 3/1/2017
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 2/9/2017 10:00:00 AM
Lab ID: 17020619-OOIA
Project: West Stanly Utilities
Client Sample ID West Stanly TCLP 2017
Analyses
Result
PQL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081A
SW3510C Analyst: JBN
SVOC SW-846: 8081-TCLP PESTICIDES
Chlordane, total
ND
0.0100
mg/L
1
2/28/2017 2:58:00 PM
Toxaphene
ND
0.0200
mg/L
1
2/28/2017 2:58:00 PM
Endrin
ND
0.00100
mg/L
1
2/28/2017 2:58:00 PM
gamma-BHC
ND
0.00100
mg/L
1
2/28/2017 2:58:00 PM
Heptachlor
ND
0.00100
mg/L
1
2/28/2017 2:58:00 PM
Heptachlor epoxide
ND
0.00100
mg/L
1
2/28/2017 2:58:00 PM
Methoxychlor
ND
0.00100
mg/L
1
2/28/2017 2:58:00 PM
Surr: Tetrachloro-m-xylene
84.6
10 - 119
%Rec
1
2/28/2017 2:58:00 PM
TCLP HERBICIDES ANALYSIS (SW846 131118151)
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
2,4,5-TP
Surr: DCAA
SW8151A SW8151A Analyst: JBN
ND 1.00 mg/L 1 2/28/2017 8:09:00 PM
ND 0.500 mg/L 1 2/28/2017 8:09:00 PM
73.8 20 - 140 %Rec 1 2/28/2017 8:09:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
M-Dichloroethene
ND
0.100
mg/L
1
2/23/2017 5:35:00 PM
1,2-Dichloroethane
ND
0.100
mg/L
1
2/23/2017 5:35:00 PM
MEK. _- . t
ND
2.00
mg/L
1
2/23/2017 5:35:00 PM
Benzene
ND
0.100
mg/L
1
2/23/2017 5:35:00 PM
Carbon tetrachloride
ND
0.100
mg/L
1
2/23/2017 5:35:00 PM
Chlorobenzene -
ND
0.100
mg/L
1
2/23/2017 5:35:00 PM
Chloroform
ND
0.100
mg/L
1
2/23/2017 5:35:00 PM
Tetrachloroethene
ND
0.100
mg/L
1
2/23/2017 5:35:00 PM
Trichloroethene
ND
0.100
mg/L
1
2/23/2017 5:35:00 PM
Vinyl chloride
ND
0.200
mg/L
1
2/23/2017 5:35:00 PM
Surr: 4-Bromofluorobenzene
69.8
70 - 130
S %Rec
1
2/23/2017 5:35:00 PM
Surr: Dibromofluoromethane
105
70 - 130
%Rec
1
2/23/2017 5:35:00 PM
Surr: Toluene-d8
110
70 - 130
%Rec
1
2/23/2017 5:35:00 PM
RCI SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
RL Reporting Detection Limit W Sample container temperature is out of limit as specified at testcode
Original
Page 7 of 28
Page 7 of 33

S
U. r Summit Environmental Technologies, Inc. Analytical report
MA IT 3310 Win St.
f. WIFIONNIENTaAL :'= 3 Pdt5Li7G,_5; mc- Cuyahoga Falls, Ohio 44223 (base report)
Ap.71.fi,,al Laberaio0c TEL: [phone] FAX.- [phone] WO#: 17020619
Website: hQ.-Iliviviv.settek.com Date Reported: 3/1/2017
CLIENT:
Synagro, NC 28134 Tag Number:
Matrix:
SLUDGE Collection Date: 2/9/2017 10:00:00 AM
Lab ID:
17020619-OOIA
Project:
West Stanly Utilities
Client Sample ID West Stanly TCLP 2017
Analyses Result
PQL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND
0.500 mg/Kg
1
2/21/2017 10:47:00 AM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SWI030
Analyst: RMT
Ignitability Non-flammable.
1
2/15/2017 8:00:00 AM
RCI
SW9045D
Analyst: DHC
PH (SW9045D)
pH 7.0
s.u.@20.4C
1
2/22/2017 3:15:00 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND
25.0 mg/Kg
1
2/21/2017 10:47:00 AM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
RL Reporting Detection Limit W Sample container temperature is out of linvt as specified at testcode
Original
Page 8 of 28
Page 8 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
,4 ma to
3310 Win St.
t,"I cUNMUNLAl- i t;LHwLQCiu:s, irkc, Cuyahoga Falls, Ohio 44223 WO#: 17020619
1.n3.i'ilid;r+3f CrTiap,r ainfide6 TEL: [phone] FAX.- [phone]
Website: h1W.-1 wivw.settek.com 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25622
Sample ID MB-25622
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 212212017
RunNo: 65964
'lient ID: PBW
Batch ID: 25622
TestNo: SW6010C SW3010A
Analysis Date: 2/23/2017
SegNo: 1087954
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-25622
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/22/2017
RunNo: 65964
lient ID: LCSW
Batch ID: 25622
TestNo: SW6010C SW3010A
Analysis Date: 2/23/2017
SegNo: 1087955
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.11
0.500
2.000
0
106
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
104
80
120
TCLP Cadmium(Cd)
2.08
0.100
2.000
0
104
80
120
TCLP Chromium(Cr)
2.08
0.200
2.000
0
104
80
120
TCLP Lead(Pb)
2.07
0.500
2.000
0
104
80
120
TCLP Selenium(Se)
2.10
0.500
2.000
0
105
80
120
TCLP Silver(Ag)
1.05
0.500
1.000
0
105
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 9 of 28
Page 9 of 33

Summit Environmental Technologies, Inc.
`��`� 3310 Win St. QC SUMMARY' REPORT
/nsum4 �� _.
CRa01KUflT,1 N I Ah r Y LHNfJLtt33 S, AKC� Cuyahoga Falls, Ohio 44223 WO#: 17020619
A mar 1{2lcaf Labor-9tvrioc, TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 01 Mat-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchlD: 25630
Sample ID MB-25630
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/22/2017
RunNo: 65943
Client ID: PBW
Batch ID: 25630
TestNo: SW7470A SW7470A
Analysis Date: 2/22/2017
SegNo: 1086913
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Mercury ND 0.00200
Sample ID LCS-25630
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/22/2017
RunNo: 65943
Client ID: LCSW
Batch ID: 25630
TestNo: SW7470A SW7470A
Analysis Date: 2/22/2017
SegNo: 1086914
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00417 0.00200 0.00400 0 104 80 120
Sample ID 17020617-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/2212017
RunNo: 65943
Client ID: BatchQC
Batch ID: 25630
TestNo: SW7470A SW7470A
Analysis Date: 2/2212017
SegNo: 1086918
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury 0.00415 0.00200 0.00400 0 104 75 125
Sample ID 17020617-001AMSD
SampType: MSD
TestCode: HG TCLP(74 Units: PPM
Prep Date: 2/22/2017
RunNo: 65943
Client ID: BatchQC
Batch ID: 25630
TestNo: SW7470A SW7470A
Analysis Date: 2/22/2017
SegNo: 1086919
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowL]mit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00416 0.00200 0.00400 0 104 75 125 0.00415 0.241 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 10 of 28
Page 10 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
PORT
fn summifft
3310 Win St.
LMN IRUIN ro71:NIAI a'LCHNULUOILs,iNC. Cuyahoga Falls, Ohio44223 WO#: 17020619
An311, Era1 LaboratoFies TEL: [phone] FAX.- [phone]
Website: httl2:/hvww.settelc.coni 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities
BatchID: 25630
Sample ID 17020617-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/22/2017
RunNo: 65943
Client ID: BatchQC
Batch ID: 25630
TestNo: SW7470A SW7470A
Analysis Date: 2/2212017
SegNo: 1086919
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 11 of 28
Page 11 of 33

summil-
Summit Environmental Technologies, Inc. C�•r SUMMARY
Tn �� /� � 7� Y 7� �T 3310 Win St. Ql.. S V l�'Yl�lri�t i REPORT
w L b lxr,rarti,M JAI. s IA;Ht,uuttiit s; tray:. Cuyahoga Falls, Ohio 44223 WO#: 17020619
s: dRai{�f .�or a,d-8211 FX (330) 253-44891A
Website: http://ivivw.settelc.com 01-Mar-17
I
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25652
Sample ID M13-25652
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/23/2017
RunNo: 66076
Client ID: PBW
Batch ID: 25652
TestNo: SW8270C SW3510C
Analysis Date: 2/24/2017
SegNo: 1089446
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0200
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0100
Cresols, Total
ND
1.00
Hexachloro-1,3-butadiene
ND
0.00400
Hexachlorobenzene
ND
0.0100
Hexachloroethane
ND
0.0200
Nitrobenzene
ND
0.0200
Pentachlorophenol
ND
0.0500
Pyridine
ND
0.0500
Surr: 2-Fluorophenol
0.411
Surr: Phenol-d6
0.387
Surr: Nitrobenzene-d5
0.465
Surr: 2,4,6-Tribromophenol
0.641
Surr: 2-Fluorobiphenyl
0.483
Surr: p-Terphenyl-d14
0.524
0.5000
82.2
10
109
0.5000
77.4
10
109
0.5000
93.0
19
120
0.5000
128
10
120
0.5000
96.6
22
117
0.5000
105
34
116
S
Sample ID LCS-25652
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/23/2017
RunNo: 66076
Client ID: LCSW
Batch ID: 25652
TestNo: SW8270C SW3510C
Analysis Date: 212412017
SegNo: 1089447
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 12 of 33
Original
Page 12 of 28

Summit Environmental Technologies, Inc. REPORT
ffrJ-e
�_;. �' � ��` ��' +� '" 1 3310 Win St. � � SUMMARY
U �,�:�
E .+'IFcVNTo1N +l1Ak Ua. ?'"LUGI� a; Jr; Cuyahoga Falls, Ohio 44223 WO#: 17020619
;4.�3t1atF.u31 C2aAf rQ�dc_ TEL: [phone] FAX.- [phone]
Website: http:/hvlvwl.settelc.com 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25652
Sample ID LCS-25652
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/23/2017
RunNo: 66076
:.lient ID: LCSW
Batch ID: 25652
TestNo: SW8270C SW3510C
Analysis Date: 2/24/2017
SegNo: 1089447
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.150
0.0200
0.2000
0
74.8
19.1
126
2,4,5-Trichlorophenol
0.167
0.0500
0.2000
0
83.3
11.7
151
2,4,6-Trichlorophenol
0.176
0.0500
0.2000
0
88.1
12.4
150
2,4-Dinitrotoluene
0.176
0.0100
0.2000
0
88.2
20.6
140
Cresols, Total
ND
1.00
0.4000
0
73.0
10
129
Hexachloro-1,3-butadiene
0.179
0.00400
0.2000
0
89.3
14.7
137
Hexachlorobenzene
0.195
0.0100
0.2000
0
97.3
12
139
Hexachloroethane
0.151
0.0200
0.2000
0
75.3
14.8
132
Nitrobenzene
0.144
0.0200
0.2000
0
72.0
15.6
138
Pentachlorophenol
0.108
0.0500
0.2000
0
54.0
10
156
Pyridine
0.0529
0.0500
0.2000
0
26.4
10
126
Surr: 2-Fluorophenol
0.357
0.5000
71.3
10
147 .
Surr: Phenol-d6
0.340
0.5000
68.0
10
140
Surr: Nitrobenzene-d5
0.405
0.5000
80.9
10
169
Stlrr: 2,4,6-Tribromophenol
0.551
0.5000
110
10
185
Surr: 2-Fluorobiphenyl
0.416
0,5000
83.2
10
169
Surr: p-Terphenyl-d14
0.437
0.5000
87.3
10
179
Sample ID 17021057-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg[L
Prep Date: 2/23/2017
RunNo: 66076
Client ID: BatchQC
Batch ID: 25652
TestNo: SW8270C SW3510C
Analysis Date: 2/24/2017
SegNo: 1089451
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 13 of 28
Page 13 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
w� fiv, t e 1 7 3310 Win St.
MVIKV, arnnra ln.rt R JN . Cuyahoga Falls, Ohio 44223 WO#: 17020619
,aLr,a 4eU of Labor9to6ev7 TEL: [phone] FAX: [phone]
Website: http://Www.settek.conz 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25652
Sample ID 17021057-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 212312017
RunNo: 66076
Client ID: BatchQC
Batch ID: 25652
TestNo: SW8270C SW3510C
Analysis Date: 212412017
SegNo: 1089451
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
0.407
0.0800
0.4000
0
102
29
112
2,4,5-Trichlorophenol
0.454
0.200
0.4000
0
114
53
123
2,4,6-Trichlorophenol
0.467
0.200
0.4000
0
117
50
125
2,4-Dinitrotoluene
0.462
0.0400
0.4000
0
116
57
128
Cresols, Total
ND
4.00
0.8000
0
99.2
20
125
Hexachloro-1,3-butadiene
0.463
0.0160
0.4000
0
116
22
124
Hexachlorobenzene
0.498
0.0400
0.4000
0
125
53
125
Hexachloroethane
0.394
0.0800
0.4000
0
98.5
21
115
Nitrobenzene
0.396
0.0800
0.4000
0
99.0
45
121
Pentachlorophenol
0.369
0.200
0.4000
0
92.2
35
138
Pyridine
ND
0.200
0.4000
0
29.7
10
126
Surr: 2-Fluorophenol
0.908
1.000
90.8
10
147
Surr: Phenol-d6
0.891
1.000
89.1
10
140
Surr: Nitrobenzene-d5
0.971
1.000
97.1
10
169
Surr: 2,4,6-Tribromophenol
1.36
1.000
136
10
185
Surr: 2-Fluorobiphenyl
0.994
1.000
99.4
10
169
Surr: p-Terphenyl-d14
1.17
1.000
117
10
179
Sample ID 17021057-001AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/23/2017
RunNo: 66076
Client ID: BatchQC
Batch ID: 25652
TestNo: SW8270C SW3510C
Analysis Date: 2/24/2017
SegNo: 1089452
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 14 of 28
Page 14 of 33

Sul
- Summit Environmental Technologies, Inc. QC SUMMARY REPORT
u 3310 Win St. SUMMARY l�ll�il i 1
IHUTA511,N IAl, a i-,A.HUM LuG 'a, INC. Cuyahoga Falls, Ohio 44223 W04: 17020619
P],,na?.k.,H-coif Lkxborararar� TEL: [phone] FAX- [phone]
Website: htty://wivw.settelc.com 01-Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25652
Sample ID 17021057-001AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/23/2017
RunNo: 66076
Client ID: BatchQC
Batch ID: 25652
TestNo: SW8270C SW3510C
Analysis Date: 2/24/2017
SegNo: 1089452
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
0.382
0.0800
0.4000
0
95.5
29
112
0.4068
6.29 30
2,4,5-Trichlorophenol
0.438
0.200
0.4000
0
109
53
123
0.4540
3.68 30
2,4,6-Trichlorophenol
0.477
0.200
0.4000
0
119
50
125
0.4668
2.20 30
2,4-Dinitrotoluene
0.446
0.0400
0.4000
0
ill
57
128
0.4624
3.70 30
Cresols, Total
ND
4.00
0.8000
0
98.7
20
125
0
0 30
Hexachloro-1,3-butadiene
0.432
0.0160
0.4000
0
108
22
124
0.4632
6.97 30
Hexachlorobenzene
0.499
0.0400
0.4000
0
125
53
125
0.4984
0.160 30
Hexachloroethane
0.381
0.0800
0.4000
0
95.2
21
115
0.3940
3.41 30
Nitrobenzene
0.389
0.0800
0.4000
0
97.3
45
121
0.3960
1.73 30
Pentachlorophenol
0.368
0.200
0.4000
0
92.0
35
138
0.3688
0.217 30
Pyridine
ND
0.200
0.4000
0
28.1
10
126
0
0 30
Surr: 2-Fluorophenol
0.778
1.000
77.8
10
147
0
Surr: Phenol-d6
0.758
1.000
75.8
10
140
0
Surr: Nitrobenzene-d5
0.872
1.000
87.2
10
169
0
Surr: 2,4,6-Tribromophenol
1.13
1.000
113
10
185
0
Surr: 2-Fluorobiphenyl
0.869
1.000
86.9
10
169
0
Surr: p-Terphenyl-dl4
0.941
1.000
94.1
10
179
0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit. 9 ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 15 of 28
Page 15 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ff 3310 Win St.
N tM,%-1KQNroJ1.I hUHNULDG1�:S1 INC. Cuyahoga Falls, Ohio 44223 WO#: 17020619
TEL: [phone] FAX.• [phone]
Website: http://www.settelf.coi?i 01-Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25682
Sample ID 17011001-001ams
SampType: rns
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 2/23/2017
RunNo: 66212
:;lient ID: BatchQC
Batch ID: 25682
TestNo: SW8151A SW8151A
Analysis Date: 2/2812017
SeqNo: 1091776
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 91.8 37 106
2,4,5-TP ND 0.500 0.500 0 78.7 38 106
Surr: DCAA 1190 500.0 238 20 140
Sample ID 17011001-001amsd
SampType: rnsd
Client ID: BatchQC
Batch ID: 25682
Analyte
Result
2,4-D
ND
2,4,5-TP
ND
Surr: DCAA
1340
TestCode: tclp-svoc-her Units: mg/L
TestNo: SW8151A SW8151A
PQL SPK value SPK Ref Val
1.00 0.500 0
0.500 0.500 0
500.0
Prep Date:
2123/2017
Analysis Date:
2/2812017
%REC
Lowl-imit Highl-imit
RPD Ref Val
103
37
105 0
84.4
38
106 0
269
20
140
mH
mH
SH
RunNo: 66212
SeqNo: 1091777
%RPD RPDLimit Qual
0 30 mH
0 30 H
0 SH
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit
P Second column confirmation exceeds Pl, Permit Limit R RPD outside accepted recovery limits Page 16 of 28
Page 16 of 33

1, Summit Environmental Technologies, Inc.
'1 g �C SUMMARY REPORT
sumharr 3310 Win St.
i_ IFEQNr+ii N i lk w N� r�aacauts�r=s; rrtiw. Cuyahoga Falls, Ohio 44223 WO#: 17020619
Iti ,_ Anaty2l.m f C:atra,r9irneFf-� TEL: [phone] FAX.- [phone]
Website: hQ.-11ivww.settek.com 01-Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25682
Sample ID mb-25682
SampType: mblk
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 2/23/2017
RunNo: 66131
Client ID: PBW
Batch ID: 25682
TestNo: SW8151A SW8151A
Analysis Date: 2/27/2017
SegNo: 1090510
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Surr: DCAA 451 500.0 90.1 20 140
Sample ID Ics-25682
SampType: Ics
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 2/23/2017
RunNo: 66131
Client ID: LCSW
Batch ID: 25682
TestNo: SW8151A SW8151A
Analysis Date: 2/27/2017
SegNo: 1090511
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit . Qua[
2,4-D 0.449 0.100 0.500 0 89.8 62.6 125
2,4,5-TP 0.457 0.100 0.500 0 91.4 52.5 128
Surr: DCAA 567 500.0 113 20 140
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 17 of 28
Page 17 of 33

Summit Environmental Technologies, Inc. REPORT
3310 Win St. QC SUMMARY 1tL' P®�T
r-NA-Irc4��T01UNIAl. a ti.a�F.araL.ct r� ;ARC, Cuyahoga Falls, Ohio44223 WO#: 17020619
TiSUMMIT
Agay kFtl-aaf Labar.-Arbrif,- TEL: [phone] FAX.- [phone]
Website: hgp.-Ilwivw.settelc.com 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25719
Sample ID mb-25719
SampType: mblk
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 2/28/2017
RunNo: 66212
client ID: PBW
Batch ID: 25719
TestNo: SW8081A SW3510C
Analysis Date: 2/28/2017
SegNo: 1091768
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-init HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Chlordane, total
ND
0.00500
Toxaphene
ND
0.0100
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500 m
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500 d
Surr: TCMX
7.65
10.00 76.5 10 119
Surr: DCB
11.1
10.00 ill 10 119
Sample ID Ics-25719
SampType: Ics
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 2/28/2017
RunNo: 66212
client ID: LCSW
Batch ID: 25719
TestNo: SW8081A SW3510C
Analysis Date: 2/28/2017
SegNo: 1091769
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00436
0.000500
0.00500
0
87.3
20
157
gamma-BHC
0.00406
0.000500
0.00500
0
81.2
22
137
Heptachlor
0.00423
0.000500
0.00500
0
84.6
24
121
Heptachlor epoxide
0.00454
0.000500
0.00500
0
90.7
27
152
Methoxychlor
0.00428
0.000500
0.00500
0
85.5
10
199
Surr: TCMX
8.11
10.00
81.1
10
119
Surr: DCB
9.51
10.00
95.1
10
119
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 18 of 28
Page 18 of 33

w SunsmitEnvironmental Technologies, Inc.
� �, f- C SUMMARY REPORT
^. y o 3310 Win St.
cc+lrr�rarrsirvi�r r+�a�rlULttti�s,af4�. Cuyahoga Falls, Ohio44223 WO#: 17020619
I .,?;4,(Vf?,Paf LaboraLosie5i TEL: [phone] FAX- [phone]
Website: httv:/hvww.settelc.com 01-Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: 25719
Sample ID 17021124-008ams
SampType: ms
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 2/28/2017
RunNo: 66212
Client ID: BatchQC
Batch ID: 25719
TestNo: SW8081A SW3510C
Analysis Date: 212812017
SegNo: 1091770
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00886
0.00100
0.0100
0
88.6
20
157 m
gamma-BHC
0.00660
0.00100
0.0100
0
66.0
22
137
Heptachlor
0.00524
0.00100
0.0100
0
52.4
24
121
Heptachlor epoxide
0.00602
0.00100
0.0100
0
60.2
27
152
Methoxychlor
0.00535
0.00100
0.0100
0
53.5
10
199
Surr: TCMX
9.72
20.00
48.6
10
119
Surr: DCB
9.87
20.00
49.4
10
119
Sample ID 17021124-008amsd
SampType: msd
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 212812017
RunNo: 66212
Client ID: BatchQC
Batch ID: 25719
TestNo: SW8081A SW3510C
Analysis Date: 2/28/2017
SegNo: 1091771
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00856 0.00100
0.0100 0 85.6
20
157
0.00886 3.47
30 m
gamma-BHC
0.00712 0.00100
0.0100 0 71.2
22
137
0.00660 7.60
30
Heptachlor
0.00549 0.00100
0.0100 0 54.9
24
121
0.00524 4.73
30
Heptachlor epoxide
0.00638 0.00100
0.0100 0 63.8
27
152
0.00602 5.81
30
Methoxychlor
0.D0557 0.00100
0.0100 0 55.7
10
199
0.00535 4.13
30
Surr: TCMX
10.6
20.00 52.8
10
119
0
Surr: DCB
10.8
20.00 53.8
10
119
0
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 19 of 28
Page 19 of 33

Summit Environmental Technologies, Inc.
._ QC SUMMARY REPORT
��,"
' �` 3310 Win St.
tr 1ffVNiAI n I AL s t Qu*a,ULD1113t�:s:, artw. Cuyahoga Falls, Ohio 44223 W04: 17020619
A!m,(VHcaP L„bor3fDfiv-5 TEL: [phone] FAX.- [phone]
Website: htto://ivww.settelc.coni 01-Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchlD: R65854
Sample ID MB-R65854
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 65854
Client ID: PBS
Batch ID: R65854
TestNo: SW9014
Analysis Date: 212112017
SegNo: 1085485
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive ND 0.500
Sample ID LCS-R65854
SampType: LCS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 65854
Client ID: LCSS
Batch ID: R65854
TestNo: SW9014
Analysis Date: 2/2112017
SegNo: 1085486
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive 1.08 0.500 1.000 0 108 85 110
Sample ID 17020768-009AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 65854
Client ID: Batch=
Batch ID: R65854
TestNo: SW9014
Analysis Date: 2/21/2017
SegNo: 1085488
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.05 0.500 1.000 0.08300 96.3 81.6 122
Sample ID 17020758-009AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 65854
Client ID: BatchQC
Batch ID: R65854
TestNo: SW9014
Analysis Date: 2/21/2017
SegNo: 1085489
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
1.08 0.500
1.000 0.08300 99.2 81.6
122
1.046 2.73 5
Qualifiers: *
Value exceeds Maximum, Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 20 of 28
Page 20 of 33

sum"IN't
Summit Environmental Technologies,Inc. QC SUMMARY REPORT1.VL�1\ i lul1 3310 Win St.
tc IHr: runr N i ni a ht:" rJLf C3itS5. INC Cuyahoga Falls, Ohio 44223 WO#: 17020619
ll:.qa;-vf?,ca1 Labor lorieS TEL: [phone] FAX.- [phone]
Website: hgp.Ilivivw.settelc.com 01-Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R65854
Sample ID 17020758-009AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 65854
Client ID: BatchQC
Batch ID: R65854
TestNo: SW9014
Analysis Date: 2/2112017
SegNo: 1085489
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 28
Page 21 of 33

r Summit Environmental Technologies, Inc. REPORT
t��� Iiy�' � Lhi 3310 Win St. QC SUMMARY
ffl Lr:vIKVTJ411.N 1:jl= 4 fA;HNUL.UG]t :St aKC. Cuyahoga Falls, Ohio 44223 WO#: 17020619
; 4,rzrtP!'.u31 Ca7�a�,rt.o,r,+e5 TEL: [phone] FAX.- [phone]
Website: hgp:Ilwivw.settelc.com 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R65855
Sample ID MB-R65855
SampType: MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 65855
Client ID: PBS
Batch ID: R65855
TestNo: SW9034
Analysis Date: 212112017
SegNo: 1085555
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDL]mit Qual
Sulfide, Reactive ND 25.0
Sample ID LCS-R65855
SampType: LCS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 65855
Client ID: LCSS
Batch ID: R65855
TestNo: SW9034
Analysis Date: 2/21/2017
SegNo: 1085556
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2490 25.0 2500 0 99.6 85 130115
Sample ID 17020758-009AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 65855
Client ID: BatchQC
Batch ID: R65855
TestNo: SW9034
Analysis Date: 2/21/2017
SegNo: 1085557
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 2390 25.0 2500 0 95.6 80 120
Sample ID 17020758-009AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 65855
Client ID: BatchQC
Batch ID: R65855
TestNo: SW9034
Analysis Date: 2/21/2017
SegNo: 1085558
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive 2460 25.0 2500 0 98.4 80 120 2390 2.89 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 22 of 28
i
Page 22 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
EPOR S
` 3310 Win St.
tN%IHU;F4r,11hI16abi,!nNULG997 5S,JKC Cuyahoga Falls, Ohio44223 WO#: 17020619
TEL: [phone] FAX: [phone]
Website: http:/hvivm).settelf.com 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchED: R65855
Sample ID 17020758-009AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 65855
client ID: BatchQC
Batch ID: R65855
TestNo: SW9034
Analysis Date: 2/21/2017
SegNo: 1085558
Analyte
Res uit
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD- RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to detennine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 23 of 28
Page 23 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
sumnINT 3310 Win St.
t:rV.-IHQ,raroII.NI Ak :rnC. CaryahogaFalls, Ohio 44223 WO#: 17020619
A.r?M Ural Lab4a,r�rorie g TEL: [phone] F9X [phone]
Website: hgp.11Www.settelc.com OI Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R65902
Sample ID LCS-R65902
SampType: LCS
TestCode: pH_DW(4500- Units: s.u.@21.00
Prep Date:
RunNo: 65902
lient ID: LCSW
Batch ID: R65902
TestNo: SW9045D
Analysis Date: 2/22/2017
SegNo: 1086417
%nalyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.0 7.0 0 100 98.6 101.4
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 24 Of 28
Page 24 of 33

Summit Environmental Technologies, Inc.
t< mp � .s 3310Win St.
QC SUMMARY REPORT
C_.r4N1HU1Nn11;NIPJ= 9t:a,:.„-�ayi�,aLUt3i�s; JKC, Cuyahoga Falls, Ohio44223 WO#: 17020619
+6 Er1J,,Uc i L;-ibor910 if,-5 TEL: [phone] FAX.- [phone]
Website: hQ://www.settefc.can 01-Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R66034
Sample ID Ics 5-50ppb L021
SampType: LCS
TestCode: voc-mstr_np Units: mg/L
Prep Date:
RunNo: 66034
client ID: LCSW
Batch ID: R66034
TestNo: SW8260B
Analysis Date: 2/23/2017
SegNo: 1088573
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.00457
0.00100
0.00500
0
91.4
71
138
1,2-Dichloroethane
0.00457
0.00100
0.00500
0
91.4
50
150
MEK
0.0257
0.00500
0.0250
0
103
50
150
Benzene
0.00477
0.00100
0.00600
0
95.4
75
137
Carbon tetrachloride
0.00498
0.00100
0.00500
0
99.6
50
150
Chlorobenzene
0.00459
0.00100
0.00500
0
91.8
77
132
Chloroform
0.00462
0.00100
0.00500
0
92.4
50
150
Tetrachloroethene
0.00513
0.00100
0.00500
0
103
50
150
Trichloroethene
0.00508
0.00100
0.00500
0
102
64
119
Vinyl chloride
0.00475
0.00100
0.00500
0
95.0
50
150
Surr:4-Bromofluorobenzene
51.8
50.00
104
70
130
Surr: Dibromofluorom ethane
50.1
50.00
100
70
130
Surr: Toluene-d8
48.1
50.00
96.3
70
130
Sample ID mblk
SampType: MBLK
TestCode: voc-mstr_np Units: mg/L
Prep Date:
RunNo: 66034
client ID: PBW
Batch ID: R66034
TestNo: SW8260B
Analysis Date: 212312017
SegNo: 1088579
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 25 of 28
Page 25 of 33

summkie
_ Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
LN%'1HVTJr+u;NIAl. a r.LtPd' ULUG11:E�, 3fgc Cuyahoga Falls, Ohio 44223 WO#: 17020619
t_Rbo,rw1ofie6z TEL: [phone] FAX.- [phone]
Website: htty://wivw.settek.com 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R66034
Sample ID mblk
SampType: MBLK
TestCode: voc-mstr_np Units: mg/L
Prep Date:
RunNo: 66034
:lient ID: PBW
Batch ID: R66034
TestNo: SW8260B
Analysis Date: 2/23/2017
SegNo: 1088679
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
41.4
Surr: Dibromofluoromethane
51.8
Surr: Toluene-d8
54.0
50.00 82.8 70 130
50.00 104 70 130
50.00 108 70 130
Qualifiers: x Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 26 of 28
Page 26 of 33

a SunsnsitEnvironmentalTechnologies,Inc . QC SUMMARY REPORT %$� ` 3310 Win St. �J REPORT
1
Lr IFcVNI" n 1 AI. A.f i;HNULUUtws., JNG Cuyahoga Falls, Ohio 44223 WO#: 17020619
?k 3tt ti;caP �ra2aorsica,r,e TEL: [phone] FAX.- [phone]
Website: http://wivw.settekeont 01 Mar-17
Client: Synagro, NC 28134
Project: West Stanly Utilities BatchID: R66034
Sample ID 17021021-001ams
SampType: MS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 66034
client ID: BatchQC
Batch ID: R66034
TestNo: SW8260B
Analysis Date: 2/2412017
SegNo: 1088626
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.0479
0.00200
0.0500
0
95.8
39.9
160
H
1,2-Dichloroethane
0.0497
0.00200
0.0500
0
99.4
42.5
157
H
MEK
0.257
0.00500
0.250
0
103
16.6
227
H
Benzene
0.0470
0.00200
0.0500
0
94.0
38.1
155
H
Carbon tetrachloride
0.0553
0.00200
0.0500
0
111
40.8
162
H
Chlorobenzene
0.0475
0.00200
0.0500
0
95.0
35.7
168
H
Chloroform
0.0478
0.00200
0.0500
0
95.6
18.3
199
H
Tetrachloroethene
0.0523
0.00200
0.0500
0
105
10
261
H
Trichloroethene
0.0515
0.00200
0.0500
0
103
23.8
175
H
Vinyl chloride
0.0473
0.00200
0.0500
0
94.6
10
165
H
Surr:4-Bromofluorobenzene
516
500.0
103
84.6
130
H
Surr: Dibromofluoromethane
500
500.0
100
71.4
127
H
Surr: Toluene-d8
527
500.0
105
74.6
127
H
Sample ID 17021021-001ams
SampType: MS
TestCode: telp-voc-mstr Units: mg/L
Prep Date:
RunNo: 66034
;lient ID: BatchQC
Batch ID: R66034
TestNo: SW8260B
Analysis Date: 2/24/2017
SegNo: 1088627
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.0466 0.00200
0.0500 0 93.2
39.9
160
H
1,2-Dichloroethane
0.0476 0.00200
0.0500 0 95.2
42.5
157
H
MEK
0.264 0.00500
0.250 0 106
16.6
227
H
Benzene
0.0457 0.00200
0.0500 0 91.4
38.1
155
H
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
7 Analyte detected below quantitation limits
M
Manual Integration used to determine
Ol'lglllal
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 27 of 28
Page 27 of 33

x � Summit Environmental Technologies, Inc.
IT3310 Win St.
�u;vik�:rar�isNiai. s t ��aa��aut�r�a, 1K. Cuyahoga Falls, Ohio 44223
_ I4d+t.cr? Catatar airaFFas TEL: [phone] FAX.- [phone]
Website: htty:Ilivww.settelc.coni
Client: Synagro, NC 28134
Project: West Stanly Utilities
QC SUMMARY REPORT
WO#: 17020619
01 Mar-17
BatchID: R66034
Sample ID 17021021-001ams
SampType: MS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 66034
Client ID: BatchQC
Batch ID: R66034
TestNo: SW8260B
Analysis Date: 2/24/2017
SegNo: 1088627
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Carbon tetrachloride
0.0519
0.00200
0.0500
0
104
40.8
162 H
Chlorobenzene
0.0444
0.00200
0.0500
0
88.8
35.7
168 H
Chloroform
0.0493
0.00200
0.0500
0
98.6
18.3
199 H
Tetrachloroethene
0.0489
0.00200
0.0500
0
97.8
10
261 H
Trichloroethene
0.0496
0.00200
0.0500
0
99.2
23.8
175 H
Vinyl chloride
0.0480
0.00200
0.0500
-0
96.0
10
165 H
Surr: 4-Bromofluorobenzene
507
500.0
101
84.6
130 H
Surr: Dibromofluoromethane
510
500.0
102
71.4
127 H
Surr: Toluene-d8
555
500.0
111
74.6
127 H
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to detennine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 28 of 28
Page 28 of 33

IT Aysis-Request / Chain ref CustodENYEPi'QNMENTrAL TECHNOLOGI,
3310 Win sneer For Sunmik EuvirctnmcnW Technologies,1w. use only
�1lYPhoQP FPlIs, Obro 44223
aen.�rn ,Mlt
M
SU
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©0-7
Rev, to
Summit Environmental Technologies, Inc.
Cooler Receipt Form
FffoctiVo ❑atu 07/14115
Initials of person Inspecting cooler and sample - -.-
Client: SY� aj-, Order Number:
Date Received LQ Time Received: C40 Date cooler(s) opened and samples Inspected:
Number of axes: _ __-- -- `. _ _ _ ...- _-. NIA
Sflippe ; FED E UPS OHL Airborne US Postal Walk-in Pickup Other.
Packaging: Peanuts Bubbl.Wra Paper roam None Other:
Tape on cooler/box-, N NIA
Custody Seals intact Y N NIA
C-��r
Y N NIA.ice prese I sent I melted NIA
Sample Temperature IR Gun # §Q204. 9 CF 0, 0 °C � -'i °C NIA
Radiological Testing Instrument serial Q027 Y N N1A
(see page 2 for scan reaults)
Use 1 sheet per sample for Radiological Testing. If sample is NOT, the Radiological Safety Officer must be notified
Immediately.
C-O-C filled out properly Y N NIA
Samples in separate bags Y N NIA
Sample containers intact* Y N NIA
*If no, list broken sample(s):� _R
Sample label(&) complete (ID, date, etc.)
Label(s) agree with C-0-C
Correct containers used
Y N NIA,
Y; r .' t N N/A
r N NIA
Sufficient sample received N NIA
Samples received within holding time Y N
Bubbles absent from 40 mL vials- Y N
— Samplesvdth bubbles <6mm are acceptable- Indicate bubble size if>6mm.
Was Client contacted about samples Y N
Will client send new samples Y N
Client contact
Datefrime:
Logged in
Page I of 2
Page 30 of 33

(D
0
NoNi Car!olina Wastewal:erfGrotrldwater LaboratRty GerrIficaVoo
Cortlfi,ed Pwaratneters Listing
1.1112 llamo: iirt.
Addresq: :M 10 Win strud
Qxeahooa ratia. 03A 442 n--
Trin T�.l d 15ANICAC 3.I,0E10W:,,i9 or .he t�klLyn
CERTIFIED PARAMETERS
WORGANIC
RrSJr.HJF. NLl.%Pr-Xl13PD
SM 254 0 0-1997 iAquuou 2)
5210 0-2C01 ',.6,qutjvLjqj)
RES[IDLIE, TOTAL
C P Li RIDP
VA 254 F, U-1 n.T (Aquurju*)
SV,,'-h4 5 90133A j)'+,Qwuus.I
SILICA
Qu,
EPA 2003, Rem. 4 A t 9 P e IAqxouF
SM-5220 C-K,97 rALI-Jectml
$W4450-10 (3-lAquemw
FLUORII'lz
&ULFATE
r-11A 7111O.C. Rev. 2.1, 193a(Aquccusj
EPA 30-3.0, Rixv. 2 1 i-V3 tAq-,cea us�
S'Vi-e-i 5 lUBS A f�Nqueousj
F,VV4,AB Oil SGA (Aqvpr,,1-:5i
IGN11TA3ILIT4'
S'A" ?"q 1113D
G'VV-a4g 0-134 (Aquco-.,31
wor--.Oac PHEriaLs
METAL
EmsA42111.r Rev- I Q78,',Aqu-ecuE,)
TOW fArTA!,
NITRCIGEN', N1 L
SW440 1311 (Aqueous)
LIA -NC-Q. RrAv. 2.1, 1993 (AcIveous)
ic-LUMINUM
±'0-54G �3W, A rAqueousj
LPA 2DU.7, Ne?j4A, 1 �94 (AcIur-OuS.:
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VAr-W5 WO'D {Aqur,,oL,,j
[-'A !-On. 0. Rov 2 1. 199: (AqA,)ul'Q
E0.4200-8, Rew- 5A, 1 19W ?AqUeDLJS:
BM6 A (AqdL-jjs)
ITLY-Wi 6,020 B;(Apehl is)
MTRCGEN rNxm , wv
ANTMII)MY
F"A 300. C. Ruv. ZA. 1991 ( Aqmuus)
EPA 2DO-7, Rey,q.+ I U(N 4Aquunuus:
5;A,-Z4G DUN A (AIUROLJF.)
M%Y,441i fin'I'll 11 (AquFcjL.--nI
N-'ITRC,GFN, 70TAL KIELMHL
FPA 200.5. Rp,-v-5 4, 1
1,1A 4 WE' NQlw V-1 Z-137 tZW 45014110 D,l 0971 CALIULMUS)
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OIL & GREASE
ARc;ENIf,
EPIA 166d Rev. B eAgvctokgsIt
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S'A' PA er 9071 Ell
3W'-84Pj6Q1-D D (Anpum.ni
PH
EPA REV. 5A, 19141+, AqklfLf)WB I
VN-846
W66AF5 0020 L! L*)
PHOSPHORUS, 1'DrAl-
BARIUM,
EPA 2160.7 Rov. 4.41 (AcIucaq),
EPA 200-7, Rey. 4.4, 1004 (Aquentr.:
51.0,1-04 6 SO 10 0 (AqUe U, USJ
-a .1,j 6 610 r,) ,p ,
NL'S:IJlJL uk;ll;(jLVIQ lb"I (7
EPA 2,1UNH, R". 5k 1904 ,Aqueous,I
'r'I`-r,25LQ C-lq97 ?Aquuou*);
SW-6A6 6020 .9 (Agueum',,
clel0caw Nwalv.-w 051
E',fmul,f- Da w IW2017
Expiral,ion Date. 1213'1r20 17
-Dare of Last III 212,P2011 7
m;irTIango,7.f.!fLagr",Az?rep,,il.fr zqawpmn lcagrarr, 1re of arrinwpj L,Mftrplwirje ote, 3u17Nf;tio fw- g'GwMQ,� Rfla"), !",flrfrpoions
5-el kl;V, ,, 15A NC%C 21-113,1417

North Carolina Wastma,WIG round wa N? r Laboratory Ceriffico[tiopq
CQrtjfj'0d'para'fj0.teLrS Listfrig
U113 h Mrltu: 50mmil EnvimnmanW 7W- mafqqje.5,'Int
Addmms: 1;11rc*QL
Falls, CH
rh- Lboua normi tabir-,it-re. hzyinr. 111f Mt IM r0qulrermrts af I-M NICAC 211 1--b!iut7y u;,:jfjw fgr!M meajuremnl of Me pa,imc-1— 6,19.1 hlop,
CERTIMIED F14RAMETERS
BERYLLIUM
EPA 2firi 5. RLAY 5.4, 19 !114 (.rkqvoUuzj
5'A',945 6020 8 ±pqueaj.F,)
50ROW
EPA 21S0 6, Rev. F�.c -1 Q�i4 j;kQupol.,,.s.,
$Q11'-54t5 GU20 B l;Rqunauq:
LADMIUM
EPAMJ. R4Y.4.4. 1:s04 (rmjiiarjmqj
-".V-J413,001 OD (Atpjemw,, 1
EPA Z 00.6, Rev, J1A, 1 i1q4 (Aijuvoin)
SlOV_8413002013 (AqUem-si
CAUDUM
EPA M-7. Rev- 4.4. 199,4 VA7,unauS)
CHRONVQ NJ -'OTAL
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t:r-4 200.7, hew. j 4, 19ti-I
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MANGANESE
EPA2%.7, Rev. 4 4, 11JN (Aclueakis)
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51,r -S46 eid)20
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$110 -644y 5r1'7 D JAVIU00LIG)
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'; W-846 ULIZU 13 jAquuolii.[
Curtifiziflu Number
6117
Effeciivri Dale
W20 9 7
Exi,4ak1411 DL1W.
IZCM,f) -17
Date of 4L2,5t Amenarrem,
MV20 17
This CeMlle tlan rcollmes memie,,m. 01 37 lruEgly a:S7Jrxzm 5:fcgr.L-q. U'c 0.1 "QVINKI nert-1 _.Wc. a, vMlimuban eLO;ed la CkIP,
PH QPD7,

North Carollria Certification
Car` frimed Palra'rleters Listing
ub llume St�rtirii4 Er�fitt:rsrnen!al 'I'eetanolr~gsr s. Iniu
Carf.•il cafe Njmb er
031
'Adc'ress 'saBflil im82r". ,
'EfffCIFveDaIG
M,''2Q17
:'uyphnff Fills. taFl 4a22'.s-
expiration Dote;
1:0144017
Data of Last, mendmeril:
20212017
Tl* a!zvm rapier~ lel:cr�A:ry, hnviny —ly mct Lfit requitom.,rit, el i 5A. NCAZ 214.1'aba, is ilvpi wb wmlllora ror IPA mslaswi iert of Itrtr I}3rntrie[ei5 let-_u LFAI i
---------
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11-b"1. LIli GI
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svv-E:4BbuIQ 17 (Af-,U"vs)
0 (.d,fguC;I zl
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as sot P<:•¢'n in 1 �rS R? :7+ : 91-1L'S,`.v

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: West Stanly
WWTP WQ Permit Number: WQ0016247
WWTP Name: West Stanly
WWTP NPDES Number: NC
Monitoring Period: From
01/01/17 To 12/31/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp)
Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test)
Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed
(Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying Heat Treatment Thermophilic
Beta Ray
Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Air Drying Composting Aerobic Digestion
Anaerobic Digestion
It applicable to alternative pertormedl l lass
A or mass is com fete the ionowing momtorm
aata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
MPN/g
Coliform
power per gram
of total solids
CFU/g
0
Annual
Grab
SM 9221E
CFU
400,000
409,930
420,000
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
Option/Mt. 3
(30-day bench) X
Option/Alt. 7
(Drying — Stable)
No vector attraction reduction alternatives were performed N/A Industrial CFR Part 257
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Mt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inlcluding fine and imprisonment."
71 e� ��� �s��cc.. O(LC LUS- wt 710 claw (� r�'`�n2G�rl 7 S
Preparer Name And Title Land A plie Name and Title (if applicable) (type or print)
Signature of reparer* Date Si Land Applier (if applicable) Date

j 1`z
a�::
z NC Certification No.402
Full -Service Analytical & NC Drinking Water Cert No. 37735
yEnvironmental SolutionsSC Certification No. 99012
Aaaffinwte- $``
LABORATORIES, INC.
Synagro
Clay Fisackerly
12701 Lancaster Hwy.
Pineville, NC 28134
Project: 2017 Production
Lab Submittal Date: 01/31/2017
Prism Work Order: 7010454
2.
r
Case Narrative
02/02/2017
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative dotes:
This report contains a total of 4 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Cara C. Rusmisell
Project Manager
Data Qualifiers Key Reference:
Reviewed By Cara C. Rusmisell
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 24-0643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]

,. _-,.�_=_-ram::___ ________________:.,•a-.=-�.-:_:.::�_: _________r_ _..-.--r.:�=. =__z= _`�-____ :..: __� ..____________: _..4=>_.:_«._.,r.� .____z.==;'_=a�,a.:_...:-try,:... _., .--•-zc._.:.- ,�________.:r__.. _. _,,.
i
IFu iron ice al Solutions
Environmental Solutions
`'LABORAWRM
Sample Receipt Summary
02/02/2017
Prism Work Order: 7010454
Client Sample I®
Lab Sample 1®
Matrix
®ate Sampled
®ate Received
West Stanly Fecals 2017 - 01
7010454-01
Solid
01/31/17
01/31/17
West Stanly Fecals 2017 - 02
7010454-02
Solid
01/31/17
01/31/17
West Stanly Fecals 2017 - 03
7010454-03
Solid
01/31/17
01/31/17
West Stanly Fecals 2017 - 04
7010454-04
Solid
01/31/17
01/31117
West Stanly Fecals 2017 - 05
7010454-05
Solid
01/31/17
01/31/17
West Stanly Fecals 2017 - 06
7010454-06
Solid
01/31/17
01/31/17
West Stanly Fecals 2017 - 07
7010454-07
Solid
01/31/17
01/31/17
Samples were received in good condition at 5.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone. [phone] -Toll Free Dumber: 1-8001529.6364 - Fax: [phone]

G=,
�y Ism
`LABORATORIES, INC<
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Client Name: Synagro
Sample DatelTime Collected:
Sample Date/Time Submitted:
Full -Service Analytical &
Environmental Solutions
449 Springbrook Rd.
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
Fax: [phone]
Project Name: West Stanly Utilities
1/31117 09:42 Project ID: West Stanly Fecals 2017
1/31117 11:14 C®C Group: 7010464
Sample
ID
Client
Sample ID
Solidsr(cfulg$
SM9222 D
Deporting
Limit
%m Solids SM2540 G
Analysis Date/Time
7010454-01
West Stanly
420000A
420000
2.38
1/31/1712:27
7010454-02
West Stanly
410000 A
410000
2.43
1 /31/17 12:27
0454-03
West Stanly
410000 A
410000
2.44
1/31117 12:27
0454-04
E
West Stanly
400000 A
400000
2.47
1131 /17 12:27
7010454-05
West Stanly
400000 A
400000
2.52
1 /31 /17 12:27
7010454-06
West Stanly
420000 A
420000
2.40
1131M 7 12:27
7010454-07
West Stanly
410000 A
410000
____T_
2.45
1 /31 /17 12:27
Geometric Mean Calculation:
Prism Sample ID: 7010454 Geometric Mean: 409930 A cfu/g
Reporting Limit: 409930
Note: All results are reported on a dry -weight basis.
A: The result is less than the reportinb limit. At the request of the client, the value reported equals the value of the reporting
limit. f
Al
Data Reviewed By: l o �` � roject Manager: C. Rusmisell
E
Review Date: 2-2-17 Approval Date: 2-2-17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

F... r.,..,r �,�.,.�.....�_....i....,��..i.,:�".. ��. r....�....r. r..�d��, r,,.,�rr,�,�r.�.,.,r,.....,� r., .,rr.�.r. ,� .��.�.r.. ................... ............ .. ..
E� 1 CHAIN OF CUSS'® Y RE®® m
Full -Service Analytical &
t Il e, Environmental Solutions P6AGE 0 OF QUOTE O TO ENSURE PROPER BILLING:. fain es 1 ,Y
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] - Fax: [phone]
Cllent Company Name:
Report To/Contact Name: srn, cJ--,fit
Re orting Address:
rev % �It .kr.
Project Name: ' i K)e* SACS
Short Bold Analysis: (Yes) (No) ­� UST, Project: (Yes) (NO)
*Please ATTACH any project specific reporting (GEC LEVEL. I II III IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone: ��fax (Yes)
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: r Q%�c�t «' y Requested Due Date O 1 Day O 2 Days El 3 Days © 4 Days El 5 Days
��'�' R�
Ceo�ta$uca�l®ov: NCI_AC D®®
ti
6"0_. NC X
EDD Type- POF Y Excel Ot r
"Working Days" ® 6-9 Days ® Standard 10 days ® RushWork Must Be
Site Location Name: 'g'b��i3��� q �i'�^e
pproved
d:'� QS Samples received after 14:00 will be processed neat business day.
SC OTHER
N/A
Site Location physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO �
(SEE REVERSE FOR TERMS E CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES
5' NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
—
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
REMARKS
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
*TYPE
NO.
SIZE
TIVES
ID NO.
HOURS
SLUDGE)
SEC BELOW
kk
-
r
r�
p
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Upon relinquishing, this Chai f Custody is your aut or ation for Prism to proceed with t e analyses as requested above. Any change oast be '
o
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relinq TNed By: (Signature)
Received By: (Signature) Date r MllitarylHours Additional Comments:
:SlierArlilh111Tt1i`tA -.,i
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Relinquis ed By: (Snatur �'
Received By: (Signature) Date
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Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITHTIL TODY SEALS FOR TRANSPORTATION TO THE LABORATORY. OC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED
AGAINST COC RECEIVED AT THE LABORATORY.
J 11
7D o✓� 1''
❑ Fed Ex ❑ UPS ❑ Hand -delivered ❑ Prism Field Service
❑ Other i
NP®Es: I UST: GROUNDWATER:
DRINKINGWATER: SOLIDWASTE: RC
RA: cERCLA LAN®FILL OTHER:®
NC ® SC El NC ® SC ® NC D SC
D NC ❑ SC I] NC ® SC ® NC O SC ® NC D SC ® NC D SC ® NC D SC
D ®
® ® ® ® D D
t)
alfe.i
*CONTAIN PE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Ct A = Volatile Organics Analysis (Zero Head Space)

PA
PROM PT•ACCUR ATE -RE LIABLE
LABORATORIES, INC
tV1F'W ARLABS.COM
REPOPT Or ANALY'SFS
Altn: CLA'`' 1`ISACXERLY
SYNAGRO
12701 LANCASTER HkY
PINEV-1I.1E, NC 28134-
PROjE::T NAME: jAN 17
DATE: 02/22/17
SAMPLE NUM;=:Ec'.
128355
5: 1.1"t'__._ 17,_ WEST
STANLY
SAMPLE MATRIX- SO
AT=: SAP+IPI EL-
01 / 1 °/ 1 7
MIME SAMPLED- 1 1 30
DATE RECEIVED-
01 / 1 9/ 1 7
5.A -!PL =R- CF
RECEIVED BY- DJ
TIME RECEIVED-
1320
DEL7V"7ReD SY- __
TYPE SAMPLE- Grab
Page i of 1
ANALYSIS
ANALYSIS
I'll ET1iC"`
DATE
TIME. BY RESULT UNITS
30 DAY BENCH SCALE EST ..
VA,
0 1 / 1 °/ 1 7
RE A`T'TAC IED
�ABORn.TOPY DIRECTOR
P.O. Box 411483 • Charlotte, SIC 28241-1483
Phone: [phone] - Fax: [phone]
IN
r

RAF;Z
PROMPT -ACCURATE -RELIABLE
LAB4DRATORIES, ZNC
WWW. PAP,LASS. COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
Start: End:
TS ()
0.1786
0.1793
TS%
1.37%
1.39%
VS )
0.1258
0.1208
VS%
70.44%
67.37%
IN
0.00389
OUT
0.0037509
FSVR (Mass Balance)
3.57%
FSVR Van Kleeck)
13.33%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] Fax: [phone]
r

PAR
LABORATORIES. INC.
www.parlabs.com
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that alt information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Carolina Department of Environmental and Natural Kesources.
Company Name (billing)
SYNAGRO CENTRAL
Address
12701 LANCASTER HVVY
City, State Et zip code
PINEVILLE NC 28134
Point of Contact Et Telephone Number
CLAY FISACKERLY 704-574-5291
Sample
Taken By:
SIGNATURE U r
Comments/ Special Instructions
PRINTED NAME
�-tUe€\-�-
1cA-2ct
ARE SAMPLES FOR STATE or EPA REPORTING? YF-S x NO
*Sample Type: DW WW n GWMW HW Soil Other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
**Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No — n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
Client Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date/Time
Collection
Date[Time
Analyses
Requested
Vies-� S-Fvo� l 10,101—�
jC
1 ��
t -tom► - t�
- C� �3 �
R wisheAb uatei I ime rceceivCu y. •••�
Relinqui d by: Datell tme Received by: Date/Time
* C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See
Other Side

Agricultural Lime Application Log
2017
Project: West Stanly Utilities
Field 11
(state -county -site -field)
Grower
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acr
Applied
Date
Applied
Total
Acres
NC-ST-03-04
Robert Ridenhour
6.1
0.0
0.0
X
NC-ST-03-05
Robert Ridenhour
6.0
0.0
0.0
X
NC-ST-04-01
HenryAnderson
6.1
0.0
0.0
X
NC-ST-04-04
Henry Anderson
5.1
1.4
1.5
12/1517
8.9
NC-ST-04-05
HenryAnderson
5.1
1.4
1.5
12/15/17
6.7
NC-ST-04-07
I Robert Ridenhour
6.2
0
0.0
X
* lime has been ordered but not spread
X No Lime Needed

Page 1 of 1
Report Number: 17-082-0509
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville NC 28134
Waypoint.
ANALYTICAL
"Every acre —Every year. "TM
Date Received: 03/23/2017 Date Of Analysis: 03/24/2017
Farm ID: NC-ST-03
SOIL ANALYSIS REPORT
Date Of Report: 03/24/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Robert Ridenhour
West Stanley 50-2170
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
°
�°
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
04
06832
6.7
150
123 VH
87 L
194 H
995 M
14 VL
6.1
6.82
1.1
8.0
H
IMIN
NC = 102
NC = 45
05
06833
5.3
148
39 M
58 L
139 H
672 M
6 VL
6.0
6.84
0.9
5.6
MIN
H
NC = 32
NC = 30
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
%
Mg
%
Ca
%
Na
%
H
%
NON
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
04
2.8
20.2
62.2
0.8
13.8
2 VL
5.8 H
66 VH
119 VH
2.9 H
0.3 VL
NC=4
NC=145.0
NC=413
NC=145.0
05
2.7
20.7
60.0
0.5
16.1
1 VL
3.2 M
42 H
74 VH
2.1 H
0.2 VL
NC=2
NC=80.0
NC=263
NC=105.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: 1 wio IV Ge—r
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc.
Pauric McGroary

Page 1 of 1
Report Number: 18-026-0503
Account Number: 46441
Send To: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypoint(D
ANALYTICAL
'Every acre... Every year. "rM
Farm ID/Name: NC-ST-03
SOIL ANALYSIS REPORT
Date Received: 01/26/2018 Date Of Analysis: 01/29/2018 Date Of Report: 01/29/2018
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Robert Ridenhow
West Stanly-2170
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
°
�°
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
3-07
21747
5.0
133
214 VH
33 VL
237 H
1667 M
26 VL
6.2
1.5
12.0
H
I MIN
NC = 178
NC = 17
Percent
Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO, N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
3-07
0.7
16.5
69.5
0.9
12.5
10 L
12.7 VH
138 VH
234 VH
7.5 VH
0.7 M
NC=21
NC=317.5
NC=863
NC=375.0
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoi nt Analytical Virginia, Inc.
Salts ms/cm x 640 = ppm.
by: ?AWi . mF 60wr
Pauric McGroary

NCDA&CS Agronomic Division Phone: [phone] Website: www.neagr.gov/agronomi/
Report No. FY18-SL016346
G,GULTUI��d Predictive Client:
Henry Anderson
Advisor:
Synagro'
°r. `10
109 Oak Hill Ln
12701 Lancaster Hwy
Mehlich-3 Extraction
Soil Report
New Bern, NC 28562
Pineville, NC 28134
Sampled County: Stanly
Links to Helpful Information Sampled: Not Provided
Received: 11 /09/2017
Farm: NC-ST-04 Completed: 12/07/201.7
Client ID: 314192
Advisor ID: 449334
Sample ID: 04-01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6
K2O Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0 120-200 0
10 0
0
0
0
0 0
Note: 12
2-
Test Results [units -W/V in g/c0; CEC and Na in meq/100 cn�; NO3-N in mg/dnft
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 1.00 10.3 86 1.4 6.1 208 72 70 13
54 146 103
167
167
445 0.2 2
Sample ID: 04-04
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6
K2O Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.4 120-200 40
20 0
0
0
0
0 0
Note: 12
2-
Test Results [units - W/V in g/c0; CEC and NN crrr�; NO3-N in mg/drrr�]:
Soil Class:
Mineral
,n�mpq1110
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-AI1
Mn-AI2 -Zn-I
Zn-AI
Cu-I Na ESP ISS-I NO3-N
0.51 0.98 5.7 59 2.3 5.1 i� 40 67 39 15
87 197 135
34
34
135 0.3 5 .
Sample ID: 04-05
Recommendations: Lime
h��
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6
K2O Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 1.4 120-200 50
20 0
0
0
0
0 0
Note: 12
2-
Test Results [units - WN in g/cO; CEC and Ni inme q/100 crrr; NO3-N in mg/drrr3]:
Soil Class:
Mineral
n
HM% WiV CEC BS% Ac f pH j P-1 K-1 Ca% Mg%
S-1 Mn-1 Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na :' ESP SS -I NO3-N
0.46 0.99 5.7 58 2.4 5.1 f 37 66 38 14
87 230 155
35
35
130 0.3 + 5 J
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FYI 8-SL015345
Henry Anderson Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat(
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $/Vote: Secondary Nutrients and Micronutrients_ In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htm1" fsFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizes
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine)
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagrgov/agronomVuvrsthtm
Report Abbreviations
AG
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-I
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-1
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-1
zinc index

2017 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
,COLUMBUS, NC
COLUMBUS, NC WWTF AEROBICALLY DIGESTED LIQUID
MONTHNEAR
August 2017
YEARLY TOTAL
AMOUNT UNIT
241,800.00 G
241,800.00 G
DRY TONS
49.81
49.81
DRY METRIC
UNIT TONS
D 45.17
D 45.17
2/5/2018

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
Facility Name: COLUMBUS, NC
NPDES#:
or WQ# (residual only)
WWTP Name: COLUMBUS WWTF
Residuals Analysis Data
Product Type AEDLTQ
Date Sampled (grab) or 10/11/17
Date Composited
Percent Solids 4.94
PARAMETERS (mg/kg dry weight)
Arsenic
3.06
Cadmium
<2
Mercury
0.44
Chromium
32.7
Copper
553
Lead
28.1
Molybdenum
<5
Nickel
14.6
Selenium
<5
Zinc
730
Total Phosphorus
13200
TKN
33900
Ammonia -Nitrogen
8280
Nitrate and Nitrite
80
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submi ' g alse informa ' n, including the possibility of fines and imprisonment for knowing violations."
X Date
(SIGNATURE OF PREPARER)
DENR FORM RSSF (5/2003) Printed: Monday - February 5, 2018 at 10:52:14 for: 2143 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
Facility Name
NPDES#
or WQ# (residual only)
WWTP Name
Residual Analysis Data
Product Type
Date Sampled
Date Composited
Percent Soilds
COLUMBUS, NC
COLUMBUS WWTF
PARAMETERS (mg/kg dry weight)'
Aluminium
Calcium
Magnesium
pH
Potasium
Sodium
PAN
SAR
AEDLIQ
10/11/17
4.94
196000 ,/
162000
7740
11.99
1770
851
11906
0.124366
Laboratory
Waypoint Analytical Virginia Inc.
e
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualifie -pe I perl er d evaluated the information submitted. I am aware that there are significant penalties for
subm' se fo t' g t . e possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF PREPARER)
Date
0
NR - Data Not Reported or Data Not Required Report Run Date:- 2/6/2018 12:42:17 PM

Page: 1 of 2
Report Number: 17-285-0206
Account Number: 90024
Send To: Synagro SW LLC/ Columbus MS
C Simmons- 56-2994
501 Woodall Road
Decatur, AL 35601
Lab Number: 56591
Sample Id : Columbus WWTP
D
Waypoint..(
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Columbus WWTP
REPORT OFANALYSIS Date Sampled: 10/11/2017 10:00:00
Date Received: 10/12/2017 00:00
Date Reported: 10/19/2017
Total Solids *
4.94
49400
100.0
JM
10/12/2017 15:00
SM-2540G
Moisture *
95.05
100.0
JM
10/12/2017 15:00
SM-2540G
Total Kjeldahl Nitrogen
3.39
33900
50.0
JM
10/13/2017 10:10
SM-4500-NH3C-TKN
Total Phosphorus
1.32
13200
100
MOS
10/16/2017 15:37
6010C
Total Potassium
0.18
1770
100
MOS
10/16/2017 15:37
6010C
Total Sulfur
0.61
6120
100
MOS
10/16/2017 15:37
6010C
Total Calcium
16.20
162000
100
MOS
10/16/2017 15:37
6010C
Total Magnesium
0.77
7740
100
MOS
10/16/2017 15:37
6010C
Total Sodium
0.09
851
100
MOS
10/16/2017 15:37
6010C
Total Iron
12000
100
MOS
10/16/2017 15:37
6010C
Total Aluminum
19600
100
MOS
10/16/2017 15:37
6010C
Total Manganese
221
5.00
MOS
10/16/2017 15:37
6010C
Total Copper
553
5.00
MOS
10/16/2017 15:37
6010C
Total Zinc
730
5.00
MOS
10/16/2017 15:37
6010C
Ammonia Nitrogen
0.83
8280
50.0-
JM
10/13/2017 10:10
SM-4500-NH3C
Organic N
2.56
25620
50.0
10/13/2017 10:10
CALCULATION
Nitrate+Nitrite-N
80.0
2.31
SJB
10/16/201714:56
4500NO3F-2011
All values are on a dry weight basis except as noted
by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and
may not be reproduced in
whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 17-285-0206
Account Number: 90024
Send To: Synagro SW LLC/ Columbus MS
C Simmons- 56-2994
501 Woodall Road
Decatur, AL 35601
Lab Number: 56591
Sample Id : Columbus WWTP
(2)
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Columbus WWTP
REPORT OF ANALYSIS Date Sampled: 10/11/2017 10:00:00
Date Received: 10/12/2017 00:00
Date Reported: 10/1912017
Total Cadmium
<2.00
2.00
MOS
10/16/2017 15:37
6010C
Total Chromium
32.7
5.00
MOS
10/16/2017 15:37
6010C
Total Nickel
14.6
5.00
MOS
10/16/2017 15:37
6010C
Total Lead
28.1
5.00
MOS
10/16/2017 15:37
6010C
Total Arsenic
3.06
3.00
MOS
10/16/2017 15:37
6010C
Total Mercury
0.440
0.400
SJB
10/17/2017 14:20
SW-7471B
Total Selenium
<5.00
5.00
MOS
10/16/2017 15:37
6010C
pH*
11.99
1.00
R D
10/16/2017 08:45
SW-9045D
Total Molybdenum
<5.00
5.00
MOS
10/16/2017 15:37
6010C
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not he reproduced in whole or part, nor may any reference he made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
pw�c #IC 60wr
Pauric McGroary
Agronomist

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2143-01-AEDLIQ-NC COLUMBUS, NC WWTF AEROBICALLY 10/11/2017 1/112017-12131/2017 0.1244
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (851 x 4.9400) _ 100 = 42.0394
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (162000 x 4.9400) _ 100 = 8002.8
Mg mg/I = (mg mg/kg x % Solids) = 100 = (7740 x 4.9400) + 100 = 382.356
Na meq = Na mg/I + Molec.Wgt.Na = 42.0394 _ 23 = 1.8278
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 8002.8 = 20 = 400.14
Mg meq = Mg mg/I + Molec.Wgt.Mg = 382.356 _ 12 = 31.863
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.8278 + SgrRoot[0.5(400.14+31.863)] = 0.124366
Printed: 2/5/2018
Page 1 10:54

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
�ACILITY NAME: COLUMBUS, NC PREDOMINANT SOIL SERIES: CECIL
)WNER: ROBERT & LINDA HOLBERT PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 12.77
IITE #: NC PO 00006 FIELD# : PO 00006 0001 OPERATOR: BILL DAVIS CATION EXCHANGE CAPACITY (NON-503):
tESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.10 ACRES PERMITTED: 8.10
Page: 1
Lune Applied ***
Date Lbs/Ac
::::F
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
8/18/17
62,000.00 (G)
7654.321
4.94
1.577
COLAEDL
DRY
0- 1/2"
SUR
0.5
0.30
33,900. p
8,280.00 p
80.00 p
11906
FESCUE PASTURE
Aug-17
62,000.00 (G)
7,654.321
Total Gallons/Ac: 7,654.32
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.010
0.006
0.103
1.744
0.089
0.001
0.016
0.046
0.016
2.302
41.63
38
Cumulative Ibs/acre
0.010
1 0.006
1 0.103
1.744
1 0.089
0.001
0.016
0.046
0.016
2.302
'ermit PAN Limit 1st Crop/2nd Crop
;• !'
_
156
(lbs/acre)
jPYI
;
y- ;,
y
}
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
J
COLAEDL = COLUMBUS, NC WWTF AEROBICALLY DIGESTED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable '", = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
?ACILITY NAME: COLUMBUS, NC PREDOMINANT SOIL SERIES: CECIL
DWNER: ROBERT & LINDA HOLBERT PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 21.71
>ITE #: NC PO 00006 FIELD# : PO 00006 0002 OPERATOR: BILL DAVIS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.20 ACRES PERMITTED: 16.20
Page: 1
Lune Applied
***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
MONTH
8/17/17
37,200.00 (G)
2296.296
4.94
0.473
COLAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
33,900. p
8,280.00 p
80.00 p
11906
I FESCUE PASTURE
8/18/17
68,200.00 (G)
4209.8771
4.94
0.867
COLAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,900. p
8,280.00 p
80.00 p
11906
FESCUE PASTURE
Aug-17
105,400.00 (G)
6,506.173
1
Total Gallons/Ac: 6,506.17
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
32
0.008
0.005
0.088
1.482
0.075
0.001
0.013
0.039
0.013
1.957
35.38
Cumulative lbs/acre
0.008
0.005
0.088
1.482
0.075
0.001
0.013
0.039
0.013
1.957
?ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
, F,_
a
; ;
s
a
4 4 i
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
COLAEDL = COLUMBUS, NC WWTF AEROBICALLY DIGESTED LIQUID
x
1
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
?ACILITY NAME: COLUMBUS, NC PREDOMINANT SOIL SERIES: CECIL
)WNER: DALE EDWARDS PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 15.33
>ITE #: NC PO 00006 FIELD# : PO 00006 0003 OPERATOR: BILL DAVIS CATION EXCHANGE CAPACITY (NON-503):
3ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.20 ACRES PERMITTED: 7.20
Page
Lane Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
site
Inches
Appli-
Vola-
Miner -
or
or Wet Tons (WT) (specify)
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Total
Per Acre
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
8/17/17
74,400.00 (G)
10333.333
4.94
2.129
COLAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
33,900. p
8,280.00 p
80.00 p
11906
FESCUE PASTURE
Aug-17
74,400.00 (G)
10,333.333
I otal Gallons/Ac: 10,333.33
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
51
0.013
0.009
0.139
2.354
0.120
0.002
0.021
0.062
0.021
3.108
56.20
Cumulative lbs/acre
0.013
0.009
0.139
2.354
0.120
0.002
0.021
0.062
0.021
3.108
; .
{
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
i �r C� +
156
�x
_..��
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
rs a
1339.0
267.9
15.0 .� 375.0
89.0
2500 0
COLAEDL = COLUMBUS, NC WWTF AEROBICALLY DIGESTED LIQUID
x -Z(A
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or m)kg ** Volatilization Rate: Surface 0.5, InjectioiVIncorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018

M itt t.
rw
trNVIR NFoIERJITA.L "aft ,-: s[3L� !25; NC
1��
May 05, 2017
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Columbus WWTP
Dear Erik Bruce:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://lviviv.settek.com
Order No.: 17041258
Summit Environmental Technologies, Inc. received 1 sample(s) on 4/21/2017 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North
Dakota R-201, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001,
Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 9957C
Page 1 of 31
Page 1 of 33

SUMN&EUN
Summit Environmental Technologies, Inc. Case Narrative
R7, 3310 Win St.
t.; VIn.0NMENIT L E r_hU0LOG , 'ONC. Cuyahoga Falls, Ohio 44223 WO#: 17041258
Amgrytir_sl Lo_barafonpti TEL: [phone] FAX: [phone]
Website: htm://wwiv.settek.com Date: 5/5/2017
CLIENT: Synagro
Project: Columbus WWTP
WorkOrder Narrative:
17041258: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
WorkOrder Comments:
17041258: Sample Receipt Temperature = 3.6C
Analytical Sequence QC Comments:
40ng CCV Mix A 1133478: Analytical Comments for SVOC-MSTR_NPW(8270), Sample 40ng CCV
Mix A, Batch ID R68632 : The SVOC CCV (R68632) exhibited poor recovery for several analytes; All
CCCs except Hexachlorocyclopentadiene are within acceptance limits; All associated samples are ND
for all analytes of interest.
17041258-OOIAMS 1134086: Analytical Comments for SVOC-BNA_TCLP(8270), Sample 17041258-
001AMS, Batch ID 26625 : Sample MS exhibited high recovery for Pentachlorophenol; All other
Original
Page 2 of 31
Page 2 of 33

Summit Environmental Technologies, Inc.
U 3310 Win St. Case Narrative
SARMN'T
:i t�l9��blhiEF'i�tL3c "'oLz� NQ. Cuyahoga Falls, Ohio44223 WO#: 17041258
s :. P3i rt:5731 Ley ei TEL: [phone] FAX[phone]
Website: htto://iviviv.settek.com Date: 5/5/2017
CLIENT: Synagro
Project: Columbus WWTP
analytes exhibited recoveries within acceptance limits.
17041258-001AMSD 1134087: Analytical Comments for SVOC-BNA_TCLP(8270), Sample
17041258-001AMSD, Batch ID 26625 : Sample MSD exhibited high recovery for Pentachlorophenol;
MS/MSD pair exhibited high RPDs for Pentachlorophenol and Pyridine; All other analytes exhibited
recoveries within acceptance limits.
ccv-00000 1134172: Analytical Comments for svoc-cpest_npw(8081), Sample ccv-00000, Batch ID
R68670 : The SVOC midpoint CCV (R68670) exhibited marginally high recovery for Surrogate:
TCMX; All other analytes exhibit recoveries within acceptance limits.
ccv 20ppb p04241 1135313: Analytical Comments for voc-mstr_npw(8260), Sample ccv 20ppb
p04241, Batch ID R68738 : The VOC CCV (Batch R68738) exhibited high recovery for Acetone and
Bromomethane; All reported samples were below RL . All Method -Specified CCCs and SPCCs
exhibited control.
17041258-001ams 1135333: Analytical Comments for tclp-voc-mstr_tclp(8260), Sample 17041258-
001ams, Batch ID R68738: The VOC MS was analyzed outside of 12 hour tune. The LCS and LCSD
all exhibited control.
Original
Page 3 of 31
Page 3 of 33

Summit Environmental Technologies, In
�( � Qualifiers and Acronyms
vi— M M E L� 3310 Win S
a NWIRONfolENTAL s'E-CJ1 tF`+LrnGI r— Cuyahoga Falls, Ohio442; WO#: 17041258
ffis
rtcal Lsi aratut'is; TEL: [phone] F,4X• (330) 253-445
Website: htto:11ivww.settek.co. Date: 5/5/2017
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinC'L
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextracfron
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 31
Page 4 of 33

r, ti Summit Environmental Technologies, Inc.
� �1� ��
ti -+ � f 3310 Win St.
P¢.I�i�hlifEi'PitL:_cc.;�Lo�fes. t Cuyahoga Falls, Ohio44223
h.r;w; th-al Ca_,pr�r rid TEL: [phone] F - [phone]
Website: htty.,1Avww.settek.com
CLIENT: Synagro
Project: Columbus WWTP
Lab SampleID Client Sample ID Tag No Date Collected
17041258-001 Columbus WWTP 4/19/2017 12:00:00 PM
Workorder
Sample Summary
WO#: 17041258
0s May-17
Date Received Matrix
4/21/2017 10:05:00 AM Sludge
Page 5 of 31
Page 5 of 33

msumma
Summit Environmental Technologies, Inc. Analytical Report
3310 Win St. (base report)
R1,fIz0N&1E11!I 7L V''ChN OLLIG1 :. WQ. Cuyahoga Falls, Ohio 44223
Arafy6 al L aaraPur e+ TEL: [phone] FAX: [phone] W04: 17041258
Website: httD://wwiv.settek.com Date Reported: 5/5/2017
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 4/19/2017 12:00:00 PM
Lab ID:
17041258-OOIA
Project:
Columbus WWTP
Client Sample ID Columbus WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
SW7470A SW7470A Analyst: ALJ
mg/L 1 4/26/2017 4:13:00 PM
SW6010C SW3010A Analyst: CM
TCLP Arsenic(As)
ND
0.500
mg/L
1
4/26/2017
TCLP Barium(Ba)
ND
5.00
mg/L
1
4/26/2017
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
4/26/2017
TCLP Chromium(Cr)
ND
0.200
mg/L
1
4/26/2017
TCLP Lead(Pb)
ND
0.500
mg/L
1
4/26/2017
TCLP Selenium(Se)
ND
0.500
mg/L
1
4/26/2017
TCLP Silver(Ag)
ND
0.500
mg/L
1
4/26/2017
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270C
SW3510C Analyst: CxA
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
4/26/2017 5:12:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
4/26/2017 5:12:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
4/26/2017 5:12:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
4/26/2017 5:12:00 PM
Cresols, Total
ND
4.00
mg/L
2
4/26/2017 5:12:00 PM
Hexachloro-1,3-butadiene
ND
0.100
mg/L
2
4/26/2017 5:12:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
4/26/2017 5:12:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
4/26/2017 5:12:00 PM
Nitrobenzene
ND
0.0800
mg/L
2
4/26/2017 5:12:00 PM
Pentachlorophenol
ND
0.200QM-QMRmg/L
2
4/26/2017 5:12:00 PM
Pyridine
ND
0.200
QMR ' mg/L
2
4/26/2017 5:12:00 PM
Surr: 2-Fluorophenol
51.2
10 - 109
%Rec
2
4/26/2017 5:12:00 PM
Surr: Phenol-d6
57.6
10 - 109
%Rec
2
4/26/2017 5:12:00 PM
Surr: Nitrobenzene-d5
75.5
19 - 120
%Rec
2
4/26/2017 5:12:00 PM
Surr: 2,4,6-Tribromophenol
52.6
10 - 120
%Rec
2
4/26/2017 5:12:00 PM
Surr: 2-Fluorobiphenyl
81.7
22 - 117
%Rec
2
4/26/2017 5:12:00 PM
Surr: p-Terphenyl-d14
101
34 - 116
%Rec
2
4/26/2017 5:12:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected at the Reporting Limit
0 RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 6 of 33

- summgv
Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
F`,'rl t NbIEhPuL12CHN01-00J , t ;. Cuyahoga Falls, Ohio44223 (base report)
A,Tar,:'tir al Lsborsiork::; TEL: [phone] FAX.. [phone] WO#: 17041258
Website: hQ.-Iliviviv.settek.com Date Reported: 5/5/2017
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 4/19/2017 12:00:00 PM
Lab ED:
17041258-OOIA
Project:
Columbus WWTP
Client Sample ID Columbus WWTP
Analyses Result
RL Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081A
SW3510C
Analyst: JBN
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total ND
10.0
pg/L
1
4/26/2017 4:50:00 PM
Toxaphene ND
20.0
pg/L
1
4/26/2017 4:50:00 PM
Endrin ND
1.0
pg/L
1
4/26/2017 4:50:00 PM
gamma-BHC ND
1.0
pg/L
1
4/26/2017 4:50:00 PM
Heptachlor ND
1.0
pg/L
1
4/26/2017 4:50:00 PM
Heptachlor epoxide ND
1.0
pg/L
1
4/26/2017 4:50:00 PM
Methoxychlor ND
1.0
pg/L
1
4/26/2017 4:50:00 PM
Surr: TCMX 96.9
10 - 119
%Rec
1
4/26/2017 4:50:00 PM
Surr: DCB 90.4
10 - 119
%Rec
1
4/26/2017 4:50:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8151A
SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D ND
11300
pg/L
1
5/1/2017 7:34:00 PM
2,4,5-TP ND
11300
pg/L
1
5/1/2017 7:34:00 PM
Surr: 2,4-Dichlorophenylacetic aci 88.6
20 - 140
%Rec
1
5/1/2017 7:34:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B
Analyst: MES
TCLP VOLATILES ANALYSIS (SW1311/8260)
1,1-Dichloroethene ND
100
pg/L
1
4/27/2017 6:54:00 PM
1,2-Dichloroethane ND
100
pg/L
1
4/27/2017 6:54:00 PM
MEK ND
2000
pg/L
1
4/27/2017 6:54:00 PM
Benzene ND
100
pg/L
1
4/27/2017 6:54:00 PM
Carbon tetrachloride ND
100
pg/L
1
4/27/2017 6:54:00 PM
Chlorobenzene ND
100
pg/L
1
4/27/2017 6:54:00 PM
Chloroform ND
100
pg/L
1
4/27/2017 6:54:00 PM
Tetrachloroethene ND
100
pg/L
1
4/27/2017 6:54:00 PM
Trichloroethene ND
100
pg/L
1
4/27/2017 6:54:00 PM
Vinyl chloride ND
200
pg/L
1
4/27/2017 6:54:00 PM
Surr: 4-Bromofluorobenzene 101
70 - 130
%Rec
1
4/27/2017 6:54:00 PM
Surr: Dibromofluoromethane 99.9
70 - 130
%Rec
1
4/27/2017 6:54:00 PM
Surr: Toluene-d8 97.5
70 - 130
%Rec
1
4/27/2017 6:54:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected at the Reporting Limit
0 RSD is greater than RSDlimit
P Second column confrnnation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 7 of 33

Summit Environmental Technologies, Inc.
- 3310 Win St. J Analpticallae Report
�� ARM *� p
i fVI:0[4flENIT T L2C .40LLIGIE 1Kc. Cuyahoga Falls, Ohio44223 (base report)
,mar"", ticai Lai prat :rtr ,_•. TEL: [phone] FAX [phone] WO#: 17041258
Website: htW.-Iliviviv.settek.com Date Reported: 5/5/2017
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 4/19/2017 12:00:00 PM
Lab ID:
17041258-001A
Project:
Columbus WWTP
Client Sample ID Columbus WWTP
Analyses Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.500 mg/Kg
1
4/25/2017 1:48:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: RMT
Ignitability Non-flammable.
1
4/25/2017 8:00:00 AM
RCI
SW9045D
Analyst: DHC
PH (SW9045D)
pH 6.9
s.u.@19.00
1
5/2/2017 3:02:00 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND
25.0 mg/Kg
1
4/25/2017 1:48:00 PM
Qualifiers: * -
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 33

SUMMIT -
Summit Environmental Technologies, Inc. � /�� /� A � 3310 Win St. QC SU1WJLl:lt1.1�Y REPORT
L-RL IKUNNI nL.u__a.r.4.,nabrJW31LS,INC Cuyahoga Falls, Ohio44223 WO#: 17041258
A naiyfl-gai L bo.ratoriee.z TEL: [phone] FAX.' [phone]
Website: htip:/hvww.settelc.coni 05 May-17
Client: Synagro
Project: Columbus WWTP BatchID: 26619
Sample ID MB-26619
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 412612017
RunNo: 68625
lient ID: PBS
Batch ID: 26619
TestNo: SW6010C SW3010A
Analysis Date: 4/2612017
SegNo: 1134001
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-26619
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/26/2017
RunNo: 68625
;lient ID: LCSS
Batch ID: 26619
TestNo: SW6010C SW3010A
Analysis Date: 4/26/2017
SegNo: 1134002
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Arsenic(As)
1.90
0.500
2.000
0
95.1
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
95.6
80
120
TCLP Cadmium(Cd)
1.92
0.100
2.000
0
96.2
80
120
TCLP Chromium(Cr)
1.92
0.200
2.000
0
96.0
80
120
TCLP Lead(Pb)
1.91
0.500
2.000
0
95.6
80
120
TCLP Selenium(Se)
1.94
0.500
2.000
0
96.8
80
120
TCLP Silver(Ag)
0:966
0.500
1.000
0
96.6
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 9 of 31
Page 9 of 33

Summit Environmental Technologies, Inc. QC SUMMARY MMARY REPORT
4 3310 Win St.
L IXV rarou;N 1 U1 B tV t�s�rj Wags, �N.t . Cuyahoga Falls, Ohio 44223 WO#: 17041258
f4 dal hlcal L Tbor9frnlp!F TEL: [phone] FAX.• [phone]
Wehsite: http:/hvww.settelc.com OS May-17
Client: Synagro
Project: Columbus WWTP BatchID: 26619
Sample ID 17041275-002AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/26/2017
RunNo: 68625
client ID: BatchQC
Batch ID: 26619
TestNo: SW6010C SW3010A
Analysis Date: 4/26/2017
SegNo: 1134020
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
0.1600
0
120
70
130
TCLP Barium(Ba)
ND
5.00
0.2000
0.1798
98.4
70
130
TCLP Cadmium(Cd)
ND
0.100
0.04000
0
97.8
70
130
TCLP Chromium(Cr)
ND
0.200
0.1600
0
95.2
70
130
TCLP Lead(Pb)
ND
0.500
0.4000
0
89.9
70
130
TCLP Selenium(Se)
ND
0.500
0.04000
0
121
70
130
TCLP Silver(Ag)
ND
0.500
0.04000
0
108
70
130
>ample ID 17041275-002AMSD
SampType: MSD
TestCode:
Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/26/2017
RunNo: 68625
:lient ID: BatchQC
Batch ID: 26619
TestNo:
SW6010C SW3010A
Analysis Date: 412612017
SegNo: 1134021
analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Arsenic(As)
ND
0.500
0.1600
0
126
70
130
0
0
20
TCLP Barium(Ba)
ND
5.00
0.2000
0.1798
106
70
130
0
0
20
TCLP Cadmium(Cd)
ND
0.100
0.04000
0
104
70
130
0
0
20
TCLP Chromium(Cr)
ND
0.200
0.1600
0
101
70
130
0
0
20
TCLP Lead(Pb)
ND
0.500
0.4000
0
94.2
70
130
0
0
20
TCLP Selenium(Se)
ND
0.500
0.04000
0
126
70
130
0
0
20
TCLP S]Iver(Ag)
ND
0.500
0.04000
0
118
70
130
0
0
20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 10 of 31
Page 10 of 33

S
u� Summit Environmental Technologies, Inc.
I�t,g QC SUMMARY REPORT
rT ,� �3310 Win St.
INIA[,;JA.'11?4rJLiJUQ:S,,Jrv�: Cuyahoga Falls, Ohio44223 WO#: 17041258
a4.nytisfl.�1 L, borftifieu TEL: [phone] FAX.- [phone]
YPebsite: httv:/livww.settelc.com 05-May-17
Client: Synagro
Project: Columbus WWTP BatchED: 26624
Sample ID mb-26624
SampType: mblk
TestCode: tclp-svoc-cpe Units: pg/L
Prep Date: 4/2612017
RunNo: 68670
Client ID: PBS
Batch ID: 26624
TestNo: SW8081A SW3510C
Analysis Date: 4/2612017
SegNo: 1134166
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Chlordane, total
ND
10.0
Toxaphene
ND
20.0
Endrin
ND
1.0
gamma-BHC
ND
1.0
Heptachlor
ND
1.0
Heptachlor epoxide
ND
1.0
Methoxychlor
ND
1.0
Surr: TCMX
0
20.00 0 10 119 S
Surr: DCB
0
20.00 0 10 119 S
Sample ID Ics-26624
SampType: Ics
TestCode: tclp-svoc-cpe Units: pg/L
Prep Date: 4/26/2017
RunNo: 68670
Client ID: LCSS
Batch ID: 26624
TestNo: SW8081A SW3510C
Analysis Date: 4/26/2017
SegNo: 1134167
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Endrin
8.48
1.0
10.00
0
84.8
20
157
gamma-BHC
7.98
1.0
10.00
0
79.8
22
137
Heptachlor
8.82
1.0
10.00
0
88.2
24
121
Heptachlor epoxide
8.19
1.0
10.00
0
81.9
27
152
Methoxychlor
10.2
1.0
10.00
0
102
10
199
Surr: TCMX
16.7
20.00
83.6
10
119
Surr: DCB
18.6
20.00
93.1
10
119
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte, detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 11 of 31
Page 11 of 33

i 4 Sunlnl11Environn9ental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
tMN1KVruP0I1.'N IRI, 9 �.tnr �aLtrs�t �; �rt�. Cuyahoga Falls, Ohio 44223
l d4r�ttttG:c.3r C.a?ara ❑rTer TEL: [phone] FAX.- [phone] WO#: 17041258
Website: httv:/hvivw.settelf..coni OS May-17
Client: Synagro
Project: Columbus WWTP BatchID: 26624
Sample ID 17041260-001ams
SampType: ms
TestCode: tclp-svoc-cpe Units: pg/L
Prep Date: 4/26/2017
RunNo: 68670
Client ID: BatchQC
Batch ID: 26624
TestNo: SW8081A SW3510C
Analysis Date: 4/26/2017
SegNo: 1134168
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
4.77
1.0
10.00
0
47.7
20
157
gamma-BHC
6.59
1.0
10.00
0
65.9
22
137
Heptachlor
3.38
1.0
10.00
0
33.8
24
121 QMR
Heptachlor epoxide
4.51
1.0
10.00
0
45.1
27
152
Methoxychlor
4.39
1.0
10.00
0
43.9
10
199 QMR
Surr: TCMX
8.57
20.00
42.8
10
119
Surr: DCB
7.70
20.00
38.5
10
119
Sample ID 17041260-001amsd
SampType: msd
TestCode: tclp-svoc-cpe Units: Ng/L
Prep Date: 4/26/2017
RunNo: 68670
Client ID: Batch QC
Batch ID: 26624
TestNo: SW8081A SW3510C
Analysis Date: 4/26/2017
SegNo: 1134169
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
6.14
1.0
10.00 0 61.4
20
157
4.771 25.1
30
gamma-BHC
7.10
1.0
10.00 0 71.0
22
137
6.588 7.43
3D
Heptachlor
5.13
1.0
10.00 0 51.3
24
121
3.380 41.1
30 R
Heptachlor epoxide
5.96
1.0
10.00 0 59.6
27
152
4.509 27.6
30
Methoxychlor
6.40
1.0
10.00 0 64.0
10
199
4.393 37.1
30 R
Surr: TCMX
11.2
20.00 56.0
10
119
0
Surr: DCB
11.2
20.00 55.9
10
119
0
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 12 of 31
Page 12 of 33

`tea Summit Environmental Technologies, Inc.
g� QC SUMMARY REPORT
}£i ¢ 3310 Win St.
Ikc�r�rnar l �l A t;a:raa�oLruts; INC.Cuyahoga Falls, Ohio44223 WO#: 17041258
^lr t r[i raP C.7 h4�r �1ra lar TEL: [phone] FAX.- [phone]
Website: http:/hvivw.settekconi 05 May-17
Client: Synagro
Project: Columbus WWTP
BatchID: 26625
Sample ID MB-26625
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 4/26/2017
RunNo: 68632
Client ID: PBS
Batch ID: 26625
TestNo: SW8270C SW3510C
Analysis Date: 4/26/2017
SegNo: 1134083
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighL[mit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Trichlorophenol
ND
0.100
2,4-Dinitrotoluene
ND
0.0200
o-Cresol
ND
0.100
m/p-Cresol(s)
ND
0.100
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenol
ND
0.100
Pyridine
ND
0.100
Surr: 2-Fluorophenol
0.578
Surr: Phenol-d6
0.647
Surr: Nitrobenzene-d5
0.805
Sum 2,4,6-Tribromophenol
0.580
Surr: 2-Fluorobiphenyl
0.831
Surr: p-Terphenyl-d14
0.943
1.000
57.8
10
109
1.000
64.7
ID
109
1.000
80.5
19
120
1.000
58.0
10
120
1.000
83.1
22
117
1.000
94.3
34
116
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 13 of 31
Page 13 of 33

SUMIM111-
SunsmitEnvironmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
L-RA W,r:rar NN N L�J, a bUHT-AULUG1 :51 JK . Cuyahoga Falls, Ohio 44223 WO#: 17041258
^6:nz. y csf LaborWo rie6 TEL: [phone] FAX.- [phone]
Website: httv:/hvww.settelc.coni 05-May-17
Client: Synagro
Project: Columbus WWTP
BatchID: 26625
Sample ID LCS-26625
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 4/26/2017
RunNo: 68632
Client ID: LCSS
Batch ID: 26625
TestNo: SW8270C SW3510C
Analysis Date: 4126/2017
SegNo: 1134084
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.284
0.0400
0.4000
0
70.9
19.1
126
2,4,5-Trichlorophenol
0.212
0.100
0.4000
0
52.9
11.7
151
2,4,6-Trichlorophenol
0.196
0.100
0.4000
0
49.0
12.4
150
2,4-Dinitrotoluene
0.380
0.0200
0.4000
0
95.0
20.6
140
o-Cresol
0.293
0.100
0.4000
0
73.2
13.8
137
m/p-Cresol(s)
0.281
0.100
0.4000
0
70.4
10
134
Cresols, Total
ND
2.00
0.8000
0
71.8
10
129
Hexachloro-1,3-butadiene
0.297
0.00800
0.4000
0
74.2
14.7
137
Hexachlorobenzene
0.377
0.0200
0.4000
0
94.2
12
139
Hexachloroethane
0.285
0.0400
0.4000
0
71.2
14.8
132
Nitrobenzene
0.358
0.0400
0.4000
0
89.6
15.6
138
Pentachlorophenol
ND
0.100
0.4000
0
18.2
10
156
Pyridine
0.110
0.100
0.4000
0
27.6
10
126
Surr: 2-Fluorophenol
0.509
1.000
50.9
10
147
Surr: Phenol-d6
0.622
1.000
62.2
10
140
Surr: Nitrobenzene-d5
1.17
1.000
117
10
169
Surr: 2,4,6-Tribromophenol
0.557
1.000
55.7
10
185
Surr: 2-Fluorobiphenyl
1.13
1.000
113
10
169
Surr: p-Terphenyl-d14
1.43
1.000
143
10
179
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
m
Original
Page 14 of 31
Page 14 of 33

1si
'
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
k
i
c.r;:vIKr-"NrnP;N1-A1. E9;k�H?,.9LFJGI1:S1INC
Cuyahoga Falls, Ohio44223
WO#: 17041258
ram-
PYrta(vg,c+3P
LxTl77Y 4so ic,
TEL: [phone] F.9X [phone]
Website: httyJ/ivivw.settelc.coni
05-May-17
Client: Synagro
Project: Columbus WWTP BatchID: 26625
Sample ID 17041258-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 4/26/2017
RunNo: 68632
Client ID: Columbus WWTP
Batch ID: 26625
TestNo: SW8270C SW3510C
Analysis Date: 4/26/2017
SegNo: 1134086
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDL]mit Qua]
1,4-Dichlorobenzene
0.238
0.0800
0.4000
0
59.5
29
112
2,4,5-Trichlorophenol
0.250
0.200
0.4000
0
62.4
53
123
2,4,6-Trichlorophenol
0.256
0.200
0.4000
0
64.0
50
125
2,4-Dinitrotoluene
0.276
0.0400
0.4000
0
69.1
57
128
o-Cresol
0.275
0.200
0.4000
0
68.8
30
117
m/p-Cresol(s)
0.271
0.200
0.4000
0
67.8
29
11 D
Cresols, Total
ND
4.00
0.8000
0
68.3
20
125
Hexachloro-1,3-butadiene
0.254
0.0160
0.4000
0
63.4
22
124
Hexachlorobenzene
0.313
0.0400
0.4000
0
78.3
53
125
Hexachloroethane
0.232
0.0800
0.4000
0
58.0
21
115
Nitrobenzene
0.296
0.0800
0.4000
0
74.1
45
121
Pentachlorophenol
ND
0.200
0.4000
0
6.40
35
138
QMRS
Pyridine
0.228
0.200
0.4000
0
56.9
10
126
mQMR
Surr: 2-Fluorophenol
0.869
1.000
86.9
10
147
Surr: Phenol-d6
0.936
1.000
93.6
10
140
Surr: Nitrobenzene-d5
1.25
1.000
125
10
169
Surr: 2,4,6-Tribromophenol
0.883
1.000
88.3
10
185
Surr: 2-Fluorobiphenyl
1.31
1.000
131
10
169
Surr: p-Terphenyl-d14
1.45
1.000
145
10
179
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte, detected in the associated
Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M Manual Integration used to determine
Original
MC Value is below Minimum
Compound Limit.
ND Not Detected at
the Reporting
Limit
0 RSD is greater than RSDlimit
,
P Second column confirmation
exceeds
PL Permit Limit
R RPD outside accepted recovery limits
Page 15 of 31
Page 15 of 33

_-� Summit Environmental Technologies, Inc.
I( 3310 Win St.
Cuyahoga Falls, Ohio 44223
�r5olH4nrol1.NIAl F1r6�tNrJL1JeJ1 SS,iP,,�.,
y ttr tt4tdi l?5pxatnrFr.:s TEL: [phone] FAX.' [phone]
Website: htty•/hvrvw settek.com
Client: Synagro
Prnierf' Columbus WWTP
Sample ID 17041258-001AMSD
SampType: MSD
TestCode:
SVOC-BNA T
Units: mg/L
Client ID: Columbus WWTP
Batch ID: 26625
TestNo:
SW8270C
SW3510C
Result
PQL
SPK value SPK
Ref Val
Analyte
0.204
0.0800
0.4000
0
1,4-Dichlorobenzene
0.210
0.200
0.4000
0
2,4,5-Trichlorophenol
0.212
0.200
0.4000
0
2,4,6-Trichlorophenol
0.229
0.0400
0.4000
0
2,4-Dinitrotoluene
0.226
0.200
0.4000
0
o-Cresol
0.226
0.200
0.4000
0
m/p-Cresols)
ND
4.00
0.8000
0
Cresols, Total
0.2
0.0
0.4000
0
Hexachloro-1,3-butadiene
0.0400 0
0.4000
0
Hexachlorobenzene
0.267
0.208
0.0800
0.4000
0
Hexachloroethane
0.248
0.0800
0.4000
0
Nitrobenzene
ND
0.200
0.4000
0
Pentachlorophenol
ND
0.200
0.4000
0
Pyridine
0.834
-
1.000
Surr: 2-Fluorophenol
1.000
Surr: Phenol-d6
0 .899
1.000
Surr: Nitrobenzene-d5
1.18
1.18
1.000
Surr: 2,4,6-Tribromophenol
0.854
Surr: 2-Fluorobiphenyl
1.23
1.000
Surr: p-Terphenyl-d14
1.41
1.000
SUMMARY REPORT
W04: 17041258
05 May-17
26625
Prep Date:
4/26/2017
KunNO: nunaA
Analysis Date:
4/26/2017
SegNo: 1134087
%REC
Lowl-imit Highurnit
RPD Ref Val
%RPD RPDLimit
50.9
10
112
0.2380
15.6
30
52.4
10
123
0.2496
17.4
30
53.0
10
125
0.2560
18.8
30
57.3
18
128
0.2764
18.7
30
56.5
10
117
0.2752
19.6
30
56.6
10
110
0.2712
18.0
30
56.6
10
125
0
0
30
53.0
13
124
0.2536
1
30
66.8
10
125
0.3132
15.9 .9
30
52.0
10
115
0.2320
10.9
30
62.0
10
121
0.2964
17.8
30
0
10
138
0
0
30
29.3
10
126
0.2276
200
30
83.4
10
147
0
89.9
10
140
0
118
10
169
0
85.4
10
185i
0
123
10
169I
0
141
10
179
0
Qual
RS
mR
E Value above quantitation range
B Analyte detected in the associated Method Blank M Manual Integration used to determine
Qualifiers: * Value exceeds Maximum Contaminant Level. original
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits 0 RSD is greater than RSDlimit
t
ND Not Detected at the Reporting Limit p r page 16 of 31
MC Value is below Minimum Compound Limit. R RPD outside accepted recovery limits g
P Second column confirmation exceeds PL Permit Limit
Page 16 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM01- 3310 Win St.
r, inr, rartu ry i Ai a ra HN(JLtt1Jt s, JNr;. Cuyahoga Falls, Ohio 44223 WO#: 17041258
f� �'--_ k�.iSrt:cai L.Tiati i;�rrariE TEL: [phone] FAX.- [phone]
Website: httl2 ww.settek.com OS-May-17
Client: Synagro
Project: Columbus WWTP BatchID: 26630
)ample ID MB-26630
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/26/2017
RunNo: 66650
;lient ID: PBS
Batch ID: 26630
TestNo: SW7470A SW7470A
Analysis Date: 4/26/2017
SegNo: 1133739
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-26630
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/26/2017
RunNo: 68650
Client ID: LCSS
Batch ID: 26630
TestNo: SW7470A SW7470A
Analysis Date: 4/26/2017
SegNo: 1133740
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
FCLP Mercury 0.00404 0.00200 0.00400 0 lu1 bu i/-u
)ample ID 17041276-002AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/26/2017
RunNo: 68650
;lient ID: BatchQC
Batch ID: 26630
TestNo: SW7470A SW7470A
Analysis Date: 4/26/2017
SegNo: 1133755
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
FCLP Mercury 0.00395 0.00200 0.00400 0.0000401 97.8 75 Izo
Sample ID 17041275-002AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/26/2017
RunNo: 68650
Client ID: BatchQC
Batch ID: 26630
TestNo: SW7470A SW7470A
Analysis Date: 4/26/2017
SegNo: 1133756
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Mercury
0.00390
0.00200 _ 0.00400 0.0000401
96.5 75 125 0.00395
1.27 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 17 of 31
Page 17 of 33

4� Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
tra:vIWflWI.-h111.1t.1;HN.QWCW:S!artti Cuyahoga Falls, Ohio44223 WO#: 17041258
AFNV!rUca' LS'00rainfie�, TEL: [phone] FAX.- [phone]
Website: httD:/hvivii,.settelc.com 05-May-17
Client: Synagro
Project: Coltunbus WWTP BatchID: 26630
Sample ID 17041275-002AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/26/2017
RunNo: 68650
Client ID: BatchQC
Batch ID: 26630
TestNo: SW7470A SW7470A
Analysis Date: 4/26/2017
SegNo: 1133756
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 18 of 31
Page 18 of 33

_ x Summit Environmental Technologies, Inc. QC SUMMARY REPORT
T
� U � f� �� � 3310 Win St.
ai-
rMVIR,VNT,1uNIPJ.;:�a�aat�Lctt3t�sINC. Cuyahoga Falls, Ohio44223 W04: 17041258
?4,�4ayllmgT Lzborvir.1,rie6 TEL: [phone] FAX.• [phone]
Website: http://ivww.settek.com 05-May-17
Client: Synagro
Project: Columbus WWTP BatchID: 26662
Sample ID mb-26662
SampType: mblk
TestCode: tclp-svoc-her Units: pg/L
Prep Date: 4/27/2017
RunNo: 68793
client ID: PBS
Batch ID: 26662
TestNo: SW8151A SW8151A
Analysis Date: 4/28/2017
SegNo: 1136093
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 10.0 0 0
2,4,5-TP ND 5.00 0 0
Surr: DCAA 3.96 5.000 79.2 20 140
Sample ID
Ics-26662 SampType: Ics
TestCode: tclp-svoc-her Units: lig/L
Prep Date:
4/27/2017 RunNo: 68793
Client ID:
LCSS
Batch ID: 26662
TestNo: SW8151A SW8151A
Analysis Date:
4/2812017 SegNo: 1136094
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D
ND
10.0 5.000 0 89.9
62.6
125
2,4,5-TP
ND
5.00 5.000 0 87.7
52.5
128
Surr: DCAA
4.72
5.000 94.3
20
140
Sample ID
Icsd-26662 SampType: Icsd
TestCode: tclp-svoc-her Units: Ng/L
Prep Date:
4/27/2017 RunNo: 68793
Client ID:
LCSS02
Batch ID: 26662
TestNo:'SW8151A SW8151A
Analysis Date:
4/28/2017 SegNo: 1136095
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua]
2,4-D
ND
10.0 5.000 0 91.4
62.6
125 0 0 30
2,4,5-TP
ND
5.00 5.000 0 88.5
52.5
128 0 0 30
Surr: DCAA
4.66
5.000 93.3
20
140 0
Qualifiers:
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method
Blank
E Value above quantitation range
H
Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
M Manual Integration used to determine
Original
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Page 19 of 31
Page 19 of 33

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
U M 11'a I MT 3310 Win St.
t:741A- I FEVN M N N I AR t;-L:HwU Lu'Jil: �1 ;Fqc Cuyahoga Falls, Ohio 44223 W09: 17041258
TEL: [phone] FAX- [phone]
Website: http://ivivii,.settek.coni 05-May-I 7
Client: Synagro
Project: Columbus WWTP BatehID: R68540
Ignitability not propagate. 0 0 20
Ignitability not propagate. 0 0 20
Ignitability Ion -flammable. 0 0 20
Ignitability Jon -flammable. 0 0 20
Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 20 of 31
Page 20 of 33

Irsuat
Summit Environmental Technologies, Inc. QC SUMMARY n i'.PORT
�,�3310 Win St.
e ±ti lxc�r�dn Mist, I 1-.t:z1NfJLUt31�:S,, VC; Cuyahoga Falls, Ohio 44223 WO#: 17041258
lrat tt.caf C rta4�,rsrn+ie TEL: [phone] FAX.- [phone]
Website: http:/hvww.settelc.com 05-May-17
Client: Synagro
Project: Columbus WWTP BatchID: R68540
Sample ID 17041075-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 68540
Dlient ID: BatchQC
Batch ID: R68540
TestNo: SW1030
Analysis Date: 4/25/2017
SegNo: 1131778
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 17041075-003ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 68540
client ID: BatchQC
Batch ID: R68540
TestNo: SW1030
Analysis Date: 4/25/2017
SegNo: 1131780
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Sample ID 17041075-003ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 68540
'lient ID: BatchQC
Batch ID: R68540
TestNo: SW1030
Analysis Date: 4/25/2017
SegNo: 1131781
Malyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability Ion -flammable. 0 0 20
Sample ID 17041255-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 68540
,lient ID: BatchQC
Batch ID: R68540
TestNo: SW1030
Analysis Date: 4/25/2017
SegNo: 1131783
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability Ion -flammable. 0 0 20
Qualifiers: 'r Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 31
Page 21 of 33

W�
t*
`�=ws ari ����jj��
Summit Environmental Technolo ies, Inc.
3310WinSt.
QC SUMMARY REPORT
�P
LR;: I1-fQ NDlQN I `'I 1'1; C 41 N;.1 LSIr0i S, JP,U
Cuyahoga Falls, Ohio 44223
WO#: 17041258
_. .,
,4;r�at1•tdc�i L7bt�,ratra,ri�;r
TEL: [phone] FAX.• [phone]
Website: htty:/hvivw.settelc.com
05-May-17
Client:
Synagro
Project:
Columbus WWTP
BatchID: R68540
Ignitability Ion -flammable. 0 0 20
Ignitability Ion -flammable. 0 0 20
Sample ID 17041258-001ATRIP SampType: DUP TestC6de: Ignitability_S Units: Prep Date: RunNo: 68540
Client ID: Columbus WWTP Batch ID: R68540 TestNo: SW1030 Analysis Date: 4/26/2017 SegNo: 1131787
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual
Ignitability Jon -flammable. 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 22 of 31
Page 22 of 33

SUMM13-
Summit Environmental Technologies, Inc.
3310Win St.
QC SUMMA RY itl'�.[ OR 1
tR%1Wi nrn;o-, I iU w i:� tBd �LJ 37 �; INC
Cuyahoga Falls, Ohio 44223
WO#: 17041258
k_t_
•
?t t..1/.csl C Taar�torle
TEL: [phone]i FAX [phone]
Website: htII2://www.settelfconi
05-May-17
Client:
Synagro
Project:
Columbus WWTP
BatchID: R68626
Sample ID MB-R68626
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 68626
Client ID: PBS
Batch ID: R68626
TestNo: SW9014
Analysis Date: 4/25/2017
SegNo: 1133390
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive ND 0.500
Sample ID LCS-R68626
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 68626
Client ID: LCSS
Batch ID: R68626
TestNo: SW9014
Analysis Date: 4/26/2017
SegNo: 1133391
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 0.972 0.500 1.000 0 97.2 85 115
Sample ID 17041323-004AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 68626
Client ID: BatchQC
Batch ID: R68626
TestNo: SW9014
Analysis Date: 4/26/2017
SegNo: 1133393
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive 1.05 0.500 1.000 0 105 81.3 118
Sample ID 17041323-004AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 68626
Client ID: BatchQC
Batch ID: R68626
TestNo: SW9014
Analysis Date: 412612017
SegNo: 1133394
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive 1.03 0.500 1.000 0 103 81.3 118 1.048 1.83 5
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 23 of 31
Page 23 of 33

Summit Environmental Technologies, Inc. T �� � ,� 7�REPORT
sualwAIT 3310Win St.
QC SUMMARY
tWOIWIN rnreNIAl. w I;CM?'JLUG ,!S, INC. Cuyahoga Falls, Ohio44223 WO#: 17041258
,4n,alyfli .3f L bo,r.gXu P,� TEL: [phone] FAX.- [phone]
Website: hgp://www.settelc.conz OS May-17
Client: Synagro
Project: Columbus WWTP BatchED: R68626
Sample ID 17041323-004AMSD
SampType:-MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 68626
Client ID: Batch=
Batch ID: R68626
TestNo: SW9014
Analysis Date: 4/25/2017
SegNo: 1133394
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Original
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 24 of 31
Page 24 of 33

Summit Environmental Technologies, Inc. �T REPORT
.9SUMMOT 3310Win St.
QC SUMMARY
r LNNIKV,NrolUNIAl1 a4-C.HNULUGI'=s;.lr;.ti. Cuyahoga Falls, Ohio44223
E...�_ _ WO#: 17041258
nzriyF 4aal L uboratn, e,,F TEL: [phone] FAX.- [phone]
al
Website: htto://www.settelcconi 05 May-17
Client: Synagro
Project: Columbus WWTP BatchID: R68631
Sulfide, Reactive ND 25.0
Sulfide, Reactive 4780 25.0 4800 0 99.6 85 115
Sample ID 17041323-004AMS
SampType: MS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 68631
Client ID: BatchQC
Batch ID: R68631
TestNo: SW9034
Analysis Date: 4/25/2017
SegNo: 1133467
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4650 25.0 4800 0 96.9 75 125
Sample ID 17041323-004AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 68631
Client ID: BatchQC
Batch ID: R68631
TestNo: SW9034
Analysis Date: 4/25/2017
SegNo: 1133468
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4700 25.0
4800 0 97.9 75
125
4650 1.07 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 25 of 31
Page 25 of 33

Sun2mit Environmental Technologies, Inc.
lue i�ff 3310 Win St. QC SUMli�I�i R�' REPORT
sv lrscJ r:rni:N ML A #:19�P•dUL4}i ir�t ; INC Cuyahoga Falls, Ohio 44223 WO#: 17041258
<Y,.nalyU,ca! L Thn,raloriar. TEL: [phone] FAX.- [phone]
Website: hup://wwiv.settek.com OS May-17
Client: Synagro
Project: Columbus WWTP BatchlD: R68631
Sample ID 17041323-004AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 68631
Client ID: BatchQC
Batch ID: R68631
TestNo: SW9034
Analysis Date: 4/26/2017
SegNo: 1133468
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 26 of 31
Page 26 of 33

S t^ Summit Environmental Technologies, Inc. SUMMARY
�/ M A RAT REPORT
r Y u?E��f��l�''1H . 3310Win St.
QC �7U1�11�ltilti i�1�POi\T
tr ulxP.ra{:u.-N 11l- 9 t;a.:HNULFJ',36_` , lhti Cuyahoga Falls, Ohio 44223 WO#: 17041258
m dt.�r3lt i ,i .T1aar�rraFies TEL: [phone] FAX.- [phone]
Website: hQ.-1Avww.settekcon: 05-May-17
Client: Synagro
Project: Columbus WWTP BatchlD: R68738
Sample ID Ics 20ppb s04241
SampType: LCS
TestCode: voc-mstr_np Units: pg/L
Prep Date:
RunNo: 68738
Client ID: LCSS
Batch ID: R68738
TestNo: SW8260B
Analysis Date: 4/27/2017
SegNo: 1135314
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
23.9
5.00
20.00
0
119
71
138
Benzene
21.7
5.00
20.00
0
108
75
137
Chlorobenzene
21.0
5.00
20.00
0
105
77
132
Trichloroethene
21.9
5.00
20.00
0
110
64
119
Surr:4-Bromofluorobenzene
49.5
50.00
99.0
70
130
Surr: Dibromofluoromethane
49.8
50.00
99.7
70
130
Surr: Toluene-d8
50.1
50.00
100
70
130
Sample ID Icsd 20ppb s0424
SampType: LCSD
TestCode: voc-mstr_np Units: pg/L
Prep Date:
RunNo: 68738
Client ID: LCS302
Batch ID: R68738
TestNo: SW8260B
Analysis Date: 4/27/2017
SegNo: 1135316
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
M-Dichloroethene
24.8
5.00
20.00
0
124
71
138
23.86
3.70
30
Benzene
20.6
5.00
20.00
0
103
75
137
21.66
4.87
30
Chlorobenzene
20.8
5.00
20.00
0
104
50
150
21.04
1.34
30
Trichloroethene
21.0
5.00
20.00
0
105
64
119
21.94
4.57
30
Surr:4-Bromofluorobenzene
48.8
50.00
97.5
70
130
0
0
Surr: Dibromofluoromethane
50.7
50.00
101
70
130
0
0
Surr: Toluene-d8
50.1
50.00
100
70
130
0
0
Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 27 of 31
Page 27 of 33

Summit Environmental Technologies, Inc. C SUMMARY REPORT
vof i 3310 Win St. `�
er,NIrsVNWQNIAkR't-.4:11 ULvG1a:1K Cuyahoga Falls, Ohio44223 WO#: 17041258
pl,n; kr.l,:czl L,:rbm,ratr�,ie5 TEL: [phone]l1 FAX [phone]
Website: http://4vww.settelc.coni 05-May-17
Client: Synagro
Project: Columbus WWTP BatchID: R68738
Sample ID mblk
SampType: MBLK
TestCode: voc-mstr_np Units: pg/L
Prep Date:
RunNo: 68738
-lient ID: PBS
Batch ID: R68738
TestNo: SW8260B
Analysis Date: 4/27/2017
SegNo: 1135318
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
5.00
1,2-Dichloroethane
ND
5.00
MEK
ND
25.0
Benzene
ND
5.00
Carbon tetrachloride
ND
5.00
Chlorobenzene
ND
5.00
Chloroform
ND
5.00
Tetrachloroethene
ND
5.00
Trichloroethene
ND
5.00
Vinyl chloride
ND
2.00
Surr: 4-Bromofluorobenzene
49.7
Surr: Dibromofluoromethane
50.9
Surr: Toluene-d8
49.3
50.00 99.5 70 130
50.00 102 70 130
50.00 98.7 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 28 of 31
Page 28 of 33

is Summit Environmental Technologies, Inc. C SUMMARY REPORT
�t
3310 Win St.
easvlrr4.r•�rnr;M in,t F i;r rtea�Lttcit s, INC, Cuyahoga Falls, Ohio 44223 WO#: 17041258
tb14t1.caf CaTiaararorre TEL: [phone] FAX.- [phone]
Website: hup.-Ilwww.settek.com 05 May-17
Client: Synagro
Project: Columbus WWTP BatchED: R68738
Sample ID 17041258-001ams
SampType: MS
TestCode: tclp-voc-mstr Units: pg/L
Prep Date:
RunNo: 68738
Client ID: Columbus WWTP
Batch ID: R68738
TestNo: SW8260B
Analysis Date: 4/2712017
SegNo: 1135333
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
217
10.0
200.0
0
108
39.9
160
1,2-Dichloroethane
224
10.0
200.0
0
112
42.5
157
MEK
1050
50.0
1000
0
105
16.6
227
Benzene
215
10.0
200.0
0
108
38.1
155
Carbon tetrachloride
227
10.0
200.0
0
113
40.8
162
Chlorobenzene
219
10.0
200.0
0
110
35.7
168
Chloroform
220
10.0
200.0
0
110
18.3
199
Tetrachloroethene
217
10.0
200.0
0
109
10
261
Trichloroethene
229
10.0
200.0
0
114
23.8
175
Vinyl chloride
200
10.0
200.0
0
100.0
10
165
Surr:4-Bromofluorobenzene
498
500.0
99.6
84.6
130
Surr: Dibromofluoromethane
508
500.0
102
71.4
127
Surr: Toluene-d8
498
500.0
99.6
74.6
127
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 29 of 31
Page 29 of 33

Summit Environmental Technologies, Inc. 7� 7�
ri �'+��"`-.U,(.� �Il� �� ����� m Lf 3310 Win St. �� SUMl0A�i�Y 1�1�P®�T
( LNN IMPTJ Tol U N IAl-4 H--H?-JULtrfat S, IN . Cuyahoga Falls, Ohio 44223 WO#: 17041258
a 'lr3l4P1,c�1 Czzhta,rinaak: TEL: [phone] FAX.- [phone]
Website: hi4p:/hvww.settelc.com 05 May-17
Client: Synagro
Project: Columbus WWTP BatchdD: R68851
Sample ID LCS-R68851
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@20.5C
Prep Date:
RunNo: 68851
Client ID: LCSS
Batch ID: R68851
TestNo: SW9045D
Analysis Date: 5/2/2017
SegNo: 1137169
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH 7.0 7.0 0 100 90 110
Sample ID 17050033-001ADUP
SampType: DUP
TestCode: pH_Oil(9045 Units: s.u.@20.3C
Prep Date:
RunNo: 68851
Client ID: BatchQC
Batch ID: R68851
TestNo: SW9045D
Analysis Date: 5/2/2017
SegNo: 1137171
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 6.2 0 0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
Page 30 of 33
6.2 0.5 10
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 30 of 31

Summit Environmental Technologies, Inc.
- fan a - . 7 3310 Win St. QC SUMMARY RE'
c ,"OIH Q.rarnGN I AJ, u 4a kEd L LUi3t a. INC Cuyahoga Falls, Ohio 44223 WO#: 17041258
+6 a. vfdc,ii LdTbo vforif- TEL: [phone] FAX [phone]
Website: htU2.Ilivwiv.settelc.com 05 May-17
Client: Synagro
Project: Columbus WWTP BatchID: R68851
Sample ID 17041323-004ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@19.8C
Prep Date:
RunNo: 68851
,lient ID: BatchQC
Batch ID: R68851
TestNo: SW9045D
Analysis Date: 6/2/2017
SegNo: 1137443
%nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
pH
6.4
6.3 0.3 5
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 31 of 31
Page 31 of 33

SummitMMOM Env�>r�un> entail Technologies,Inc. Analysis Request/Chtain of Custody
Ui3310 Witt StrwA For 5unma Environmental lbe idol ies, Inc. use only
Guyallaga Falls, Ohio 44223 Tel: [phone] Fax: [phone] page i ..-of L— SEi No.
Analytical Parameters and Methods
mpenyName (Pleaael'tint)
PmicctName
Mur5
WW
om yAMMS
0
Pmlect eAddreSs
M �M
life tom- Z70 8
Client Throne No. -703 " X V
Rt port.to
pent Fax No.
PUB
Client Emai] Please
Quote No.
Contact Person.
Sampled by
Check if OWo VAP samples , [�
Sample ldemtiHesatnA
Date 15me
Collected Collected
Vt t-P
9,
p
c�
z
$L I tce
NotesfCorauu ats.-
Rush Requested DY: Must be approved `
-Da—to by lab msnaM
lWte aad Yellow pales should accompany eawptes to the labDmtary. The client ratains the pink pale.
4

DC, L+iradvu lair. :�� f14755
IzLv 16
SLtlTiij-,1t Technologies, Irie.
Cooler Receipt Form
Initials of person inspecting cooler
jand
}samrplles-:____t_,,__
Client ,, VAII fa Order Number:
Date Received: Time Received_ db Date cooler(s) opened and samples inspected:_
Number of CoolersJ3oxes: NIA
Shipper- FI& UPS DHL Airborne US Postal Walk-in Pickup Other,
Packaging: Peanuts B ble ap Paper Foam None Other.
Tape on cooler/box. N NA
Custody Seats intact
Y N
C-O-C in last.
�Y N
NIJa
Ica glue ice
res t J absent I melted NIA
Sample Temperature IR Gun #F1607-G459 CF�s-
Z,_°C 1(1 'c
NIA
Radiological Testing Instrument serial'35127.
Y
(see page 2 for scan results)
'Use 1 sheet per sample for Radiological Testing. If sample
is HOT, the Radiological Safety Officer must be notified
immediately.
CA-C filled out properly
N
eyy
NIA
Samples in separate bags
N
NIA
Sample containers intact'
N
LY
NJA
`If no, list broken sample(s):
Sample lalrel(s) CoMplete (ID, date. eta.)
U
Id NIA
Label(s) agree tirith C-0-0
Gy
N N/A
Correct containers used
N NIA
Sufficient sample received
N NIA
Samples received within holding time
(Y-1
N
Bubbles absent from 40 mL vials"
Y
N IiA
x• Samples with bubbles -�crrim are acceptable. indicate babble size if >Smrn.
Was client contacted about samples Y N
Will Client send new samples Y N
Client contact: / Q rl
Detefrime: I- ( - _
Logged in by: /-
('nmmPnrc- l .tl+ t$u�
Page 1 of 2
N
v—
O
N
N
n
Page 33 of 33

Facility Name:
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Columbus NC
WWTP Name: Columbus WWTP
WQ Permit Number: WQ 0016247
NPDES Number: NC 0021369
Monitoring Period: From 01/01/17 To 12/31/2017
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens x
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
li applicable to alternative pertormecal c lass
A or l lass xs coin fete the ionowina monnonn
aata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
(VS reduction)
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization) x
Option/Mt. 9
Option/Alt. 10
(Injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certificationud' e a d imprisonment."
Todd Larson, Regional Director ca, 0
Prep r la d tle int) Land Applier Name arAT' e ( applica e or print)
�l (a
Signa re of Preparer* 1 Dle Signature of d Applier (if a pficable) bate 1
*Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 2T.1102 (26)

o l -7
TOWN OF COLUMBUS WWTP
VECTOR ATTRACTION REDUCTION
OPTION 6- 503 BEGS.
24 HOUR TEST OF ADDITION OF ALKALINE MATERIAL FOR LAND APPLIED SLUDGE
TEST: FS� 16 111 G r o�'i r� u' / ©. oo f 1q1 j 2 ! T f ._._-
Temu°C
t
INITIAL p H i Z 10�.� TIME O TEMP Z4 DATE
P H @ 2 HOURS )L2LN TIME lJ2 TEMPoZ .7 DATE?LI&1�
cGc�hra�6 rt6�&r j1-- 0-?JO 7,00l lt7.00112.s1S C
P H@ 22 HOURS
L TIME og3D TEMPO , DATE` )_ 17
S 2.3Y
30% LIME SLURRY PRODUCT
-GALLONS OF ALKALINE MATERIAL ADDED i 000
i
SIGNATURE 4-0 DATE_Li C
40
39
38
37
36
35
34
33
32
31
30
79
23
27
26
25
24
23
2�
21
20
19
18
17
16
15
14
13
12
.11
]0
Correction Factor
Plus 0.45
Plus 0.42
Plus 039
Plus 0.36
Plus 0.33
Plus 0.30
Plus 0.27
Plus 0.24
Plus 0.21
Plus 0.1s
Plus 0.15
Plus 0.12
Plus 0.09
Plus 0.06
Plus 0.03
0.00
Minus 0.03
Minus 0.06
Minus 0.09
Minus 0.12
Minus 0.15
kinus0.18inus 0.?1
inus 0.24
Minus 0.27
Minus 0.30
Minus 0.33
Minus 0.36
Minus 0.39
Minus 6.42
.Minus 0.45

Agricultural Lime Application Log
Year: 2017
Project:
Columbus NC WWTP
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied(CCE Eq.)
Date Applied
PO-06-01
6.5
O.T/Ac.
PO-06-02
6.7
OT/Ac
PO-06-03
6.7
O.OT/Ac.
*Lime will be applied when conditions improve.

NCDA&CS Age—..-.,ric Division Phone: [phone] Website: www.ncay..u_v/agronomi/ Report No. FY17------ 656
u1JU
Client: Synagro Advisor: Synagro
�- Heavy Metals 284 Boger Rd 284 Boger Rd
='r Mocksville, NC 27028 Mocksville, NC 27028
Soil Re r)®rt Mehlich-3 Extraction
4: • .,� Sampled County Polk
Links to Helpful Information
Client ID: 404711 Advisor ID: 404711
Sampled: 06/06/2017 Received: 06/27/2017 Completed: 06/30/2017 Farm: PO-06/Bill Davis
Agronomist's Comments:
This report contains both routine soil test information as well as heavy metals data in a section labeled as Heavy Metals under soil test lab results. Using Mehlich 3 as a soil test
extractant, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic (As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium (Cr)- 0.2 ppm, lead (Pb)-
4.2 ppm, nickel (Ni)- 0.8 ppm, & selenium (Se)- 0.2 ppm (FY2005-2007). Although the above metals here are not believed to pose a concern for plant growth, continue to monitor these and
note where elevated above background levels.Note any lime and fertilizer recommendations. Tissue testing is advised where soil pH is elevated and are of concern as in samples found
here.Ja athi Kamalakanthan 6/30/2017
Sample ID: 06-01
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0 50 0 0 pH$ 0 0 0
Note: 12 Note:
2-
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 crnP; NO3-N in mg/da]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N
0.71 1.05 9.2 88 1.1 6.6 94 47 56 29 41 94 65 68 68 31 0.1 1
Heavy Metals (parts per million): Arsenic, 0.2 Cadmium, 0.1 Nickel, 0.5 Chromium, 0.2 Lead, 5.3 Selenium, 0.0
� rth C ro1i)»
' 'jtitilti;i[a4p 7YutiC FI�fkLi �:C6T�71Gfk551f�1q
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agrununlic Division Phone: [phone] Website: www.ncagr.guv/agronomi/ Report No. FY17-__ J656
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronami/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htm[ sFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS-1, Na, ESP, SS-1, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-1
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P206
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

NCDA&CS Ac nic Division Phone: [phone] Website: www.nc�-....jv/agronomi/ Report No. FY17---- ,3657
Client: Bill Davis Advisor: S na ro
y'O.j,% Heavy Metals 315 Timberbrook Lane 284 Boger Rd
Tryon, NC 28782 Mocksville, NC 27028
Soil Report Mehlich-3 Extraction
r w.Sampled County: Polk
Links to Helpful Information
Client ID: 428800 Advisor ID: 404711
Sampled: 06/21/2017 Received: 06127/2017 completed: 06/30/2017 Farm: PO-06
Agronomist's Comments:
This report contains both routine soil test information as well as heavy metals data in a section labeled as Heavy Metals under soil test lab results. Using Mehlich 3 as a soil test
extractant, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic (As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium (Cr)- 0.2 ppm, lead (Pb)-
4.2 ppm, nickel (Ni)- 0.8 ppm, & selenium (Se)- 0.2 ppm (FY2005-2007). Note elevated lead (Pb) in both the samples. Although the above metals here are not believed to pose a concern
for plant growth, continue to monitor these and note where elevated above background levels. Note any lime and fertilizer recommendations. Where soil test phosphorus (P) is very high (P-1
> 100), crops will not res and to additional P applied.Tissue testing is advised where soil pH is elevated and are of concern as in samples found here.Ja athi Kamalakanthan 6/30/2017
Sample ID: 06-02
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0 30 0 0 pH$ 0 0 0
Note: 12 Note:
2-
Test Results [units - WN in g/crap; CEC and Na in meq/100 cnr ; NO3-N in mg/da]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N
0.76 1.00 11.9 92, 1.0 6.7 105 60 59 30 48 175 112 103 103 40 0.1 1
Heavy Metals (parts per million): Arsenic, 0.1 Cadmium, 0.1 Nickel, 0.3 Chromium, 0.2 Lead, 6.5 Selenium, 0.3
Sample ID: 06-03
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0 40 0 0 pH$ 0 0 0
Note: 12 Note:
2-
Test Results [units - WN in g/cnr ; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N
0.81 1.00 11.1 91 1.0 6.7 96 51 60 29 43 158 101 84 84 36 0.1 1
Heavy Metals (parts per million): Arsenic, 0.1 Cadmium, 0.1 Nickel, 0.3 Chromium, 0.2 Lead, 5.9 Selenium, 0.0
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T4+1r KCL: IILA FuialJ L':csaivuih551t is
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Ac nic Division Phone: [phone] Website: www.ncw...,jv/agronomi/ Report No. FY17---- ,3657
Bill Davis Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at on
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat(
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htrn[sfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizei
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomWuvrst.htm
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-I
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index