WQ0016247_Regional Office Historical File Pre 2018 (11)

STANLY COUNTY UTILITIES, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0016247
2019 ANNUAL REPORT
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WQROS
mooRESVILLE REGIONAL OFFICE.

SECTION 1

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
STANLY COUNTY UTIL., NC (FKA OAKBOR
)STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
April 2019
310,000.00
G
25.85
D
May 2019
223,200.00
G
18.62
D
August 2019
68,200.00
G
5.69
D
September 2019
260,400.00
G
21.72
D
YEARLY TOTAL
861, 800.00
G
71.88
D
DRY METRIC
23.44
16.88
5.16
19.70
41B]
1 /30/2020

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0005387 Laboratory
Facility Name: STANLY COUNTY UTIL., NC (FKA OAKBORO) PACE ANALYTICAL SERVICE INC.
NPDES# : NCO043532
or WQ# (residual only)
WWTP Name: WEST STANLY WWTP (FKA OAKBORO WWTP)
Residuals Analysis Data
Product Type
LIQ
Date Sampled (grab) or 01/08/19
Date Composited
Percent Solids
2.00
PARAMETERS (mg/kg dry weight)
Arsenic
<16.7
Cadmium
<1.7
Mercury
0.83
Chromium
NR
Copper
300
Lead
17.7
Molybdenum
27.6
Nickel
31.2
Selenium
<16.7
Zinc
888
Total Phosphorus
12500
TKN
52200
Ammonia -Nitrogen
1320
Nitrate and Nitrite
<95.9
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date
IGNATURE OF PARE )
DENR FORM RSSF (5/2003) Printed: Thursday - February 6. 2020 at 13:05:52 for: 2170 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
WQ0005387
Facility Name
STANLY COUNTY UTIL., NC (FKA
NPDES#
NC0043532
or WQ# (residual only)
WWTP Name
WEST STANLY WWTP (FKA
Residual Analysis Data
Product Type
LIQ
Date Sampled
01/08/19
Date Composited
Percent Soilds
2.00
PARAMETERS (mg/kg dry weight)'
Aluminium
14200
Calcium
14300
Magnesium
10400
pH
6.70
Potasium
<8360
Sodium
<8360
PAN
16020
SAR
1.8279
Laboratory
PACE ANALYTICAL SERVICE INC.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
x (:;; 4.
Date
(SI T RE OF P PARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/6/2020 1:01:38 PM

laceAnalytical"
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 19, 2019
Adam Brigman
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
RE: Project: West Stanley
Pace Project No.: 92413571
Dear Adam Brigman:
Enclosed are the analytical results for sample(s) received by the laboratory on January 10, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Revised Report. The 6010 metals have been redigested and reanalyzed, results are revised.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
Q pCci?-
`9eORAtO��
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 17

laceAnalytical"
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Project: West Stanley
Pace Project No.: 92413571
Charlotte Certification IDs
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
West Stanley
92413571
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92413571001
West Stanley 2019 N+M
EPA 6010D
IDS
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
MFO
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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leAnalytical
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ANALYTICAL RESULTS
Project: West Stanley
Pace Project No.: 92413571
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: West Stanley 2019 N+M Lab ID: 92413571001 Collected: 01/08/19 10:30 Received: 01/10/19 09:38 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7471 Mercury
Mercury
540G Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
14200
mg/kg
167
1
02/18/1911:00
02/18/1916:30
7429-90-5
ND
mg/kg
16.7
1
02/18/1911:00
02/18/1916:30
7440-38-2
ND
mg/kg
1.7
1
02/18/1911:00
02/1811916:30
7440-43-9
14300
mg/kg
167
1
02/18/1911:00
02/18/1916:30
7440-70-2
300
mg/kg
8.4
1
02/18/1911:00
02/18/1916:30
7440-50-8
17.7
mg/kg
8.4
1
02/18/1911:00
02/18/1916:30
7439-92-1
10400
mg/kg
167
1
02/18/1911:00
02/18/1916:30
7439-95-4
27.6
mg/kg
8.4
1
02/18/1911:00
02/18/1916:30
7439-98-7
31.2
mg/kg
8.4
1
02/18/1911:00
02/18/1916:30
7440-02-0
ND
mg/kg
8360
1
02/18/1911:00
02/18/1916:30
7440-09-7
ND
mg/kg
16.7
1
02/18/1911:00
02/18/1916:30
7782-49-2
ND
mg/kg
8360
1
02/18/1911:00
02/18/1 9 16:30
7440-23-5
888
mg/kg
16.7
1
02/18/1911:00
02/18/1916:30
7440-66-6
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
0.83
mg/kg
0.23
1
01/17/1916:00
01/18/1910:54
7439-97-6
Analytical Method: SM 2540G-2011
2.0
%
0.000010
1
01/10/1917:24
Analytical Method: ASTM D2974-87
98.0
%
0.10
1
01/10/1917:18
Analytical Method: EPA 9045D
6.7
Std. Units
0.10
1
01/15/19 11:33
Analytical Method: SM 271 OB-2011
15900
mg/kg
0.12
1
01/15/1917:46
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0
1993 Mod.
1320
mg/kg
414
1
01/12/1910:40
01/12/1915:59
7664-41-7
Analytical Method:
EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2
Rev 2.0 1993
52200
mg/kg
2220
1
01/14/19 11:34
01/15/19 05:03
7727-37-9
Analytical Method: EPA 353.2 Rev 2.0
1993 Preparation
Method: EPA 353.2
Rev 2.0 1993
ND
mg/kg
95.9
1
01 /11 /19 22:50
01 /12/19 03:30
ND
mg/kg
95.9
1
01/11/19 22:50
01/12/19 03:30
14797-55-8
ND
mg/kg
47.9
1
01/11/19 22:50
01/12/19 03:30
14797-65-0
Analytical Method:
EPA 365.1 Rev 2.0
1993 Preparation
Method: EPA 365.1
Rev 2.0 1993
12500
mg/kg
2220
50
01/14/19 19:23
01/14/19 23:24
7723-14-0
H3
N2
Date: 02/19/2019 12:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: West Stanley
Pace Project No.: 92413571
QC Batch: 452998 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Associated Lab Samples: 92413571001
METHOD BLANK: 2475568 Matrix: Solid
Associated Lab Samples: 92413571001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 01/18/1910:36
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2475569
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.068 81 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2475570 2475571
MS MSD
92414199001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
lercury mg/kg ND 0.071 0.071 0.036 0.037 50 50 75-125 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: West Stanley
Pace Project No.: 92413571
QC Batch: 458724 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92413571001
METHOD BLANK: 2500593
Associated Lab Samples: 92413571001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Aluminum
mg/kg
ND
10.0
02/18/1916:23
Arsenic
mg/kg
ND
1.0
02/18/1916:23
Cadmium
mg/kg
ND
0.10
02118/1916:23
Calcium
mg/kg
ND
10.0
02/18/1916:23
Copper
mg/kg
ND
0.50
02/18/1916:23
Lead
mg/kg
ND
0.50
02/18/1916:23
Magnesium
mg/kg
ND
10.0
02/18/1916:23
Molybdenum
mg/kg
ND
0.50
02/18/1916:23
Nickel
mg/kg
ND
0.50
02/18/1916:23
Potassium
mg/kg
ND
500
02/1811916:23
Selenium
mg/kg
ND
1.0
02/18/1916:23
Sodium
mg/kg
ND
500
02/18/1916:23
Zinc
mg/kg
ND
1.0
02/1811916:23
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2500594
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mg/kg
500
493
99
80-120
Arsenic
mg/kg
50
47.9
96
80-120
Cadmium
mg/kg
50
47.8
96
80-120
Calcium
mg/kg
500
491
98
80-120
Copper
mg/kg
50
50.8
102
80-120
Lead
mg/kg
50
48.2
96
80-120
Magnesium
mg/kg
500
469
94
80-120
Molybdenum
mg/kg
50
48.1
96
80-120
Nickel
mg/kg
50
49.1
98
80-120
Potassium
mg/kg
500
ND
99
80-120
Selenium
mg/kg
50
46.6
93
80-120
Sodium
mg/kg
500
502
100
80-120
Zinc
mg/kg
50
47.1
94
80-120
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2500595
2500596
MS
MSD
92413571001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua]
Aluminum mg/kg
14200
8880
8250
24300
23600
113
114
75-125
3
Arsenic mg/kg
ND
888
825
821
758
91
91
75-125
8
Cadmium mg/kg
ND
888
825
824
755
92
91
75-125
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/19/2019 12:57 PM without the written consent of Pace Analytical Services, LLC.
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IeAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: West Stanley
Pace Project No.: 92413571
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2500595
2500596
MS
MSD
92413571001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
14300
8880
8250
22300
21800
90
91
75-125
3
Copper
mg/kg
300
888
825
1180
1110
99
98
75-125
6
Lead
mg/kg
17.7
888
825
834
764
92
91
75-125
9
Magnesium
mg/kg
10400
8880
8250
18400
17600
90
88
75-125
4
Molybdenum
mg/kg
27.6
888
825
850
781
92
91
75-125
9
Nickel
mg/kg
31.2
888
825
863
792
93
92
75-125
9
Potassium
mg/kg
ND
8880
8250
12600
12000
94
95
75-125
5
Selenium
mg/kg
ND
888
825
793
730
88
87
75-125
8
Sodium
mg/kg
ND
8880
8250
10600
9950
95
95
75-125
6
Zinc
mg/kg
888
888
825
1660
1590
87
85
75-125
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: West Stanley
Pace Project No.: 92413571
QC Batch: 451857 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92413571001
SAMPLE DUPLICATE: 2470825
92413658013 Dup
Parameter Units Result Result - RPD Qualifiers
Percent Moisture % 9.9 9.5 4
SAMPLE DUPLICATE: 2470826
92413607001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 36.2 40.1 10
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/19/2019 12:57 PM without the written consent of Pace Analytical Services, LLC.
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Project: West Stanley
Pace Project No.: 92413571
QC Batch: 452172
QC Batch Method: EPA 9045D
Associated Lab Samples: 92413571001
SAMPLE DUPLICATE: 2472426
Parameter - Units
pH at 25 Degrees C Std. Units
SAMPLE DUPLICATE: 2472427
Parameter
pH at 25 Degrees C
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description: 9045 pH
92413563001 Dup
Result Result RPD Qualifiers
5.2 5.3 0 H3
92413312001 Dup
Units Result Result
Std. Units 6.8 6.8
RPD Qualifiers
0 H3
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/19/2019 12:57 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 17

laneAnalytical"
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QUALITY CONTROL DATA
Project: West Stanley
Pace Project No.: 92413571
QC Batch: 452023 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92413571001
METHOD BLANK: 2471582
Associated Lab Samples: 92413571001
Parameter Units
Nitrogen, Ammonia mg/kg
LABORATORY CONTROL SAMPLE: 2471583
Parameter Units
Nitrogen, Ammonia mg/kg
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 8.9 01/12/1915:09
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
472 464 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471584 2471585
MS MSD
92413357001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
litrogen, Ammonia mg/kg 13200 10300 10500 21800 22500 83 89 90-110 3 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471586 2471587
MS MSD
92413358001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg ND 2320 2320 2210 2210 93 93 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Project: West Stanley
Pace Project No.: 92413571
QC Batch: 452219
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92413571001
METHOD BLANK: 2472536
Associated Lab Samples: 92413571001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 01/15/19 04:45
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2472537
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 967 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472538 2472539
MS MSD
92413357001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
litrogen, Kjeldahl, Total mg/kg 62000 21200 19000 74700 74800 60 67 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472540 2472541
MS MSD
92413358001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, Kjeldahl, Total mg/kg 5230 5170 5170 8110 9500 56 83 90-110 16 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02119/2019 12:57 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 17

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QUALITY CONTROL DATA
Project: West Stanley
Pace Project No.: 92413571
QC Batch: 452122 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92413571001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 2472244
Matrix: Solid
Associated Lab Samples: 92413571001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND 2.0
01/12/19 03:27
Nitrogen, Nitrite
mg/kg
ND 0.99
01/12/19 03:27
Nitrogen, NO2 plus NO3
mg/kg
ND 2.0
01/12/19 03:27
LABORATORY CONTROL SAMPLE:
2472245
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mglkg
14.3
15.2
106 90-110
Nitrogen, Nitrite
mg/kg
9.6
10.2
107 90-110
Nitrogen, NO2 plus NO3
mg/kg
23.9
25.4
106 90-110
IATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472246
2472247
MS
MSD
92413583001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qua]
Nitrogen, Nitrate
mg/kg ND
522
529 374
401 72 76
90-110
7
Nitrogen, Nitrite
mg/kg 212
348
351 525
545 90 94
90-110
4
Nitrogen, NO2 plus NO3
mg/kg ND
870
880 899
946 99 103
90-110
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/19/2019 12:57 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 17

leAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: West Stanley
Pace Project No.: 92413571
QC Batch: 452341 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0.1993 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92413571001
METHOD BLANK: 2473119
Associated Lab Samples: 92413571001
Parameter Units
Phosphorus mg/kg
LABORATORY CONTROL SAMPLE: 2473120
Parameter Units
Phosphorus mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 01/14/19 23:27
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
48.1 51.4 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2473121 2473122
MS MSD
92413583001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
'hosphorus mg/kg 2300 1580 1680 3650 3550 85 74 90-110 3 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/19/2019 12:57 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 17

Pace Analytical Services, LLC
aceMalXical o 9800 KinceyAve. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: West Stanley
Pace Project No.: 92413571
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/19/2019 12:57 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 17

laneAnalyfical"
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
West Stanley
92413571
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92413571001
West Stanley 2019 N+M
EPA 3050E
458724
EPA 6010D
458763
92413571001
West Stanley 2019 N+M
EPA 7471 B
452998
EPA 7471 B
453128
92413571001
West Stanley 2019 N+M
SM 2540G-2011
452044
92413571001
West Stanley 2019 N+M
ASTM D2974-87
451857
92413571001
West Stanley 2019 N+M
EPA 9045D
452172
92413571001
West Stanley 2019 N+M
SM 271 OB-2011
452617
92413571001
West Stanley 2019 N+M
EPA 350.1 Rev 2.0 1993
452023
EPA 350.1 Rev 2.0 1993
452144
Mod.
Mod.
92413571001
West Stanley 2019 N+M
EPA 351.2 Rev 2.0 1993
452219
EPA 351.2 Rev 2.0 1993
452403
92413571001
West Stanley 2019 N+M
EPA 353.2 Rev 2.0 1993
452122
EPA 353.2 Rev 2.0 1993
452124
92413571001
West Stanley 2019 N+M
EPA 365.1 Rev 2.0 1993
452341
EPA 365.1 Rev 2.0 1993
452369
Date: 02/19/2019 12:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 17

CHAIN -OF -CUSTODY Analytical Request Document
Analytical'
Chaln-of-Custodyls a LEGAL DONMENi-Complete all relevant fields
3mpaoy: SYNAGRD Billing Intormaxan: Mary Brewer. 2" Boger rd, Mocksv;
Adam
LAB DSEbNLYYfRk Wort WO# a 92413571
A1kSFIA0l 1111111111111111111111111
mntalner Presert�Uve' 92413571
•'Prase—.T .. 'I ro.s:(1)nibicadd,(1)sulfuxcadd,(aJ 7rydmrhlodcadd, (aJ sodium hydroalde, IB)Lnca¢tatG
(BJ methanol, (�sodiVm bisulfate, (e) s.dlum tlUosulfete, (9) M1evne, IN ascmhlcatld, (B).mmonlum saga[.,
- -
Email: [e-mail]
bite/Facll ID #:
50'21%
Compliance Monitoring?
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Collected BY (Print): Adam Brlgman
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Quote it:
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Colle (gnaMe):
Turnaround Data Required:
Immedlately Pad:edon ire:
2 wPtl/f
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'Matrix Codes lklsertin Matrix box helow): Drinking Water(DW),
Gmund Water(GW), Westawatr(WWJ,
Product (P), SaB/Solid
Z
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[SLJ, Oil (OL), Wipe (WO, Air (AR), TIss8
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IABSample7em{i raHlte lrrfo
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Page 16 of 17

Sample ReceivinNon-Conformance Form (NCF)
Data 1 E.'.' d }ayt ,. " r l , '. s�o+
i, Affix Workorder/Login Label Here or List Pace
Client r + Workorder Number or MTJL Log -in Number
Here
1. If Chain-of=Custody (COC) is not received: contact client and if necessary, fill out a COC and indicate that It was filled out by
lab personnel. Note Issues on This NCF
2. If COC Is Incam 10t, check a Ilcable Issues below and add details where a ro riate:
,2 Collection dateAimemissing or - Analyses or analytes: missing or Samples listed on COC do not match samples
aampre Iva on un: ac not
match sample labels Required trip blanks were not received Required signatures are missmg
CommentsfDetalisf0ther Issues not listed above:
N,o a cA (L-0 L) V) Gp fI-6-Q n o f1 -eo e- cjoC_
i Ca nrn Ini-1h, icc nha D ­11ra1Jn c I.nln nA AAA A.,/ens ..,hnr n!late:
Samples: Condition needs to be brought to
-- , Samples: Past holding time
lab ersonnel's attention details below
Preservation: Im m er
Temperature: not within acceptance criteria (typically
_. Samples: Not field filtered
Containers: Broken or compromised
0.6C)-
Samples: Insufficient volume
__. received
Containers: Incorrect
Temperature: Samples arrived frozen
Samples: Cooler damaged or
Custody Seals: Missing or compromised on
_- com romised
samples, trip blanks or coolers
Vials received with Improper heads ece
Samples: contain chlorine or
sulfides
Packing Material: InsllffcientAm ro er
Olher.
uunwmumm�a:
S;jm le ID:
DateMme:
AmounViVpe pres added:
Pieservedb -,
Initlaland Final H:
Lot#of res added:
Sample 10:
Dalefnme:
Amount/type pres added:
Preserved by:
Initial and Final RK
Lot#of les added:
sample ID:
Detemme:
Amount/ a prWs added:'
Preserved by:
Initial and Final H:
Lot#of les added:
5. Client Contact: If client is contacted for anv Issue listed above. fill In details below:
Unent Commentsanstructions: 8' _
1
FALL-C-01 1 -rev.00, 05Ju12018
Page 17 of 17

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2170-01-LIQ-NC STANLY COUNTY UTIL., NC WEST STANLY 1/8/2019 111/2019-12/31/2019 1.8279
WWTP AEROB DIG LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (8360 x 2.0000) _ 100 = 167.2
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (14300 x 2.0000) _ 100 = 286
Mg mg/I = (mg mg/kg x % Solids) = 100 = (10400 x 2.0000) _ 100 = 208
Na meq = Na mg/I _ Molec.Wgt.Na = 167.2 + 23 = 7.26957
Ca meq = Ca mg/I -= Molec.Wgt.Ca = 286 = 20 = 14.3
Mg meq = Mg mg/I = Molec.Wgt.Mg = 208 _ 12 = 17.3333
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.26957 = SgrRoot[0.5(14.3+17.3333)] = 1.82789
Printed: 2/6/2020
Page 1 13:32

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STANLY COUNTY UTIL ., NC (FKA PREDOMINANT SOIL SERIES: BADIN
OWNER: SYLVESTER LITTLE - PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 35.16
SITE #: NC ST 00002 FIELD# : ST 00002 0001 OPERATOR: SYLVESTER LITTLE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 13.00 ACRES PERMITTED: 13.00
Page
Lime Applied ***
Date
Hs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
ova
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acre
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm
Cro) p
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/24/19
93,000.00 (G)
7153.846
2.00
0.597
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
SOYBEANS
4/29/19
117,800.00 (G)
9061.538
2.00
0.756
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
SOYBEANS
4/30/19
99,200.00 (G)
7630.769
2.00
0.636
SCUWSA
MOIST
0-<I/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
SOYBEANS
Apr-19
310,000.00 (G)
23,846.153
5/2/19
111,600.00 (G)
8584.6151
2.00
0.716
SCUWSA
I MOIST
0-<I/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
SOYBEANS
May-19
111,600.00 (G)l
8,584.615
1
1
1
r orai vauons/Ac: s.Z,4JU. ri
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
87
0.090
0.009
NR
1.623
0.096
0.004
0.149
0.169
0.090
4.804
67.62
Cumulative lbs/acre
0.158
0.030
0.579
6.579
0.414
0.020
0.312
0.454
0.164
17.790
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
165
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
L
1339.0
267.9
15.0
1..
375.0
89.0
2500.0
i
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X L �Z G"42G
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Stanly County Utilities Total Dry Tons Applied (Annual):
Permit #: WQ0016247 Cation Exchange Capacity (non 503 only):
erator: Sylvester Little Owner: Sylvester Little Predominant Soil Series:
Acres Used: 13 Acres Permitted: 13 Site #: NC ST 00002 Field #:
35.16
Badin
ST 00002 0001
Residual Analysis Data (Heavy Metals and 'Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
1
1/8/19
2
3
4
5
6
7
8
9
10
11
12
% Solids
2
Arsenic
16.7
Cadmium
1.7
Copper
300
Chromium
0
Lead
17.7
Mercury
0.83
Molyb-
denum
27.6
Nickel
31.2
Selenium
16.7
Zinc
888
Total
Phos-
- [orus
12500
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
U
ME
a
0
W_Wm1
1'1
1 111
1 111
1 111
1 111
1111
1 111
1 111
1 111
1 111
1111
1111
.• •
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1111
1111
1111
1 111
1111
1 11'
•..•
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
i 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®''
1 1'•
1 ill
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•.
1 11�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
•
1 �•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 �•
••�
1 .•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
i 111
1 111
1 .•
1 1' 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1.1
®
:1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� :1�
Total
' •
• •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
. •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisonment for knowing violations".
Signature of La d Applier
MZ L2e-217
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STANLY COUNTY UTIL., NC (FKA PREDOMINANT SOIL SERIES: BADIN
OWNER: SYLVESTER LITTLE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 9.31
SITE #: NC ST 00002 FIELD# : ST 00002 0002 OPERATOR: SYLVESTER LITTLE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 5.60 ACRES PERMITTED: 5.60
Page : 1
Lime Applied ***
Date
LbsAc
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
5/1/19
111,600.00 (G)
19928.571
2.00
1.662
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
SOYBEANS
May-19
111,600.00 (G)
19,928.571
1 otal liallons/Ac: 19,928.57
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
53
0.056
0.006
NR
0.997
0.059
0.003
0.092
0.104
0.056
2.952
41.55
Cumulative llis/acre
0.022
0.375
4.273
0.265
0.015
0.219
0.291
0.098
12.037
I0.103
,
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
165
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
15.0 +
375.0
89.0
2500.0
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X L/L/2
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Stanly County Utilities
Total Dry Tons Applied (Annual): 9.31
Permit #: WQ0016247 Cation Exchange Capacity (non 503 only):
;rator: Sylvester Little Owner: Sylvester Little Predominant Soil Series:
Acres Used: 5.6 Acres Permitted: 5.6 Site #: NC ST 00002 Field #:
Badin
ST 00002 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
1/8/19
2
3
4
5
6
7
8
9
10
11
12
% Solids
2
Arsenic
16.7
Cadmium
1.7
Copper
300
Chromium.
0
Lead
17.7
Mercury
0.83
Molyb-
denum
27.6
Nickel
31.2
Selenium
16.7
Zinc
888
Total
Phos-
`orus
12500
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 1
1 111
1 111
1 111
1 111
KIT, 11
1 111
1 111
1 111
1 111
1 111
ff1 111
1 1 •
.. •
1 11 ml
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11.
•..-
1"
1 111
1 lil
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1"
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 lil
1 1 •
KIM
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1'
� -�
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 1 .
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 Ili
1 111
1 111
KIT, 11
1 1 •
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
1
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1'
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
,I am aware that there are significant penalties for submitting false information, including the possibility of fines and
)risonment for owing violations".
2 /2 12C
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: NORWOOD, NC PREDOMINANT SOIL SERIES: BADIN
OWNER: ANDERSON LIVING TRUST PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 10.22
SITE #: NC ST 00004 FIELD# : ST 00004 0001 OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 26.80 ACRES PERMITTED: 26.80
Page
Lune Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/20/19
117,800.00 (G)
4395.5221
0.61
0.111
NOABL
MOIST
0-<I/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
Aug-19
117,800.00 (G)
4,395.522
I
9/3/19
31,000.00 (G)
1156.716
2.00
0.096
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
9/4/19
55,800.00 (G)
2082.0901
2.00
0.174
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
Sep-19
86,800.00 (G)
3,238.806
i otai liauons/Ac: 7,634.ss
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
12
0.012
0.002
0.020
0.306
0.043
0.001
0.024
0.037
0.014
0.902
11.64
Cumulative lbs/acre
0.085
0.048
0.778
8.585
0.605
0.022
0.298
0.450
0.109
17.705
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
160
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8�
1339.0
267.9
15.0
375.0
89.0
2500.0
NOABL = NORWOOD, NC WWTP AERATION BASIN LIQUID
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X % 12o 2
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Stanly County Utilities/ Norwood, NC Total Dry Tons Applied (Annual):
Permit #: WQ0016247 Cation Exchange Capacity (non 503 only):
rrator: Henry Anderson Owner: Anderson Living Trust Predominant Soil Series:
10.22
Badin
Acres Used: 26.8 Acres Permitted: 26.8 Site #: NC ST 00004 Field #: ST 00004 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
1/8/19
2
8/20/19
3
4
5
6
7
8
9
10
11
12
% Solids
2
0.606
Arsenic
16.7
14
Cadmium
1.7
6.2
Copper
1 300
650
Chromium
0
92
Lead
17.7
150
Mercury
0.83
3
Molyb-
denum
27.6
42
Nickel
31.2
91
Selenium
16.7
22
Zinc
888
1900
Total
Phos-
-orus
12500
22000
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
0100002000100'"
mom
1 11•
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
KITIM
..
1 11
1 11MIT,11
1 111
1 111
1 111
1 111
NOT, 11
MIT, 11
1 111
1 111
1 111
1 11
•..-
1•
1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 111
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
®''
1 1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
FIRM
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 1
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 �
•�
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11'
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1�:1
1�
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1.1
Total
•
• 1
�::�
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
. �'
•.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
.3risonment for knowing violations".
Z/j212ol- e
Signature of an pplier
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: NORWOOD, NC
OWNER: ANDERSON LIVING TRUST
SITE #: NC ST 00004 FIELD# : ST 00004 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: BADIN
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 14.49
OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.90 ACRES PERMITTED: 6.90
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
V27/19
62,000.00 (G)
8985.5071
0.61
0.227
NOABL
MOIST
0-<1/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
Aug-19
62,000.00 (G)
8,985.507
I
8/30/19
68,200.00 (G)
9884.0581
2.00
0.824
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
Aug-19
68,200.00 (G)
9,884.058
I
9/3/19
86,800.00 (G)
12579.7101
2.00
1.049
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
Sep-19
86,800.00 (G)
12,579.710
I
Total Gallons/Ac: 31,449.28
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
67
0.069
0.009
0.042
1.419
0.134
0.004
0.122
0.158
0.073
4.190
56.83
Cumulative lbs/acre
0.069
0.009
0.042
1.419
0.134
0.004
0.122
0.158
0.073
4.190
1
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
163
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
1
NOABL = NORWOOD, NC WWTP AERATION BASIN LIQUID
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
x
(SIGNATURE OF DAP DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Stanly County Utilities/ Norwood, NC Total Dry Tons Applied (Annual):
Permit #: WQ0016247 Cation Exchange Capacity (non 503 only):
erator: Henry Anderson Owner: Anderson Living Trust Predominant Soil Series:
Acres Used: 6.9 Acres Permitted: 6.9 Site #: NC ST 00004 Field #:
14.49
Badin
ST 00004 0003
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 11
1/8/19
1 2
8/20/19
3
4
5
6
7
8
9
10
11
12
% Solids
2 .
0.606
Arsenic
16.7
14
Cadmium
1.7
6.2
Copper
300
650
Chromium
0
92
Lead
17.7
150
Mercury
0.83
3
Molyb-
denum
27.6
42
Nickel
31.2
91
Selenium
16.7
22
Zinc
888
1900
Total
Phos-
-horus
12500
22000
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
-
1
.
1 1.
1 11.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
W. M11
My, 1
1 111
1 111
1 111
1 111
1 111
1 111
1111
1 111
1 111
1 111
1 11•
•.•
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1111
1 111
1 111
. •
1 Ili
1 1�
1 111
1 111
1 111
1 111
1 lil
IT, 11
1 111
i 111
1 111
1 111
1 1�
®''
1 1••
1 1•:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 �
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
1 111
1 111
1 111
1 111
1 111
1 111
MEMEMEEMMMEEM
1 111
1 111
1 111
1 111
1 111
1 111
1
WIT, •
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
KIT, 11
MIT, 11
ff1 111
1 1
®�M
1 :•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:�
Total
Phos-
�.:
•::
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
\I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisonment for knowing violations".
` 2 /Z 12o2d
Signature of L nd pplier Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: NORWOOD, NC
OWNER: ANDERSON LIVING TRUST
SITE #: NC ST 00004 FIELD# : ST 00004 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM�]
PREDOMINANT SOIL SERIES: BADIN
PERNUT #: WQ0016247 ANNUAL DRY TONS APPLIED: 8.49
OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.70 ACRES PERMITTED: 6.70
Page
Lime Applied ***
Date
Lb,/A.
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/11/19
49,600.00 (G)
7402.985
0.61
0.187
NOABL
MOIST
0-<1/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
Sep-19
49,600.00 (G)
7,402.985
9/5/19
1 86,800.00 (G)
12955.2241
2.00
1.080
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
Sep-19
86,800.00 (G)
12,955.224
1
I otal Gallons/Ac: 20,358.21
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
40
0.041
0.006
0.034
0.891
0.094
0.003
0.075
0.101
0.044
2.630 35.24
Cumulative lbs/acre
0.055
0.009
0.128
1.332
0.134
0.005
0.099
0.153
0.059
4.120
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
------------ -
--_ —
— - — -
144
-
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
L -^R `y'
1339.0
267.9
15.0 6
375.0
89.0
2500.0
NOABL = NORWOOD, NC WWTP AERATION BASIN LIQUID
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
XJ0 212Z 219Z�
(SIGN OF L D APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there'are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
gyrator:
Acres Used:
Stanly County Utilities/ Norwood, NC Total Dry Tons Applied (Annual): 8.49
WQ0016247
Henry Anderson
Cation Exchange Capacity (non 503 only):
Owner: Anderson Living Trust Predominant Soil Series: Badin
6.7 Acres Permitted:
6.7 Site #: NC ST 00004 Field #: ST 00004 0005
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
1/8/19
2
8/20/19
3
4
[5T
L 1
7
8
9
10
11
12
% Solids
2
0.606
Arsenic
16.7
14
Cadmiuml
1.7
6.2
Copper
300
650
Chromium
0
92
Lead
17.7
150
Mercury
0.83
3
Molyb-
denum
27.6
42
Nickel
31.2
91
Selenium
16.7
22
Zinc
888
1900
Total
Phos-
-' orus
12500
22000
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
-
1:
1 •
'�
1 1 •
1 11
1 111
1 111MENOMONEE
1 1�
o
111�
1 11
1 111
1 111
1 111
1 111
1 111
1110
1 111
IT, 11
1 111
1 lol
KIT, 1•
•.•
1 �:
1
1 111
1 111
1 111
1 111
IT, 11
1 111
1 111
IT, 11
0 111
1 111
1 :•
•
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
0 111
1 111
1 111
1 111
1 1
1 1MITI".1
111
1 111
1 111
1 111
1 111
i 111
1 111
1 111
1 111
1 111
1 1••
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 1.1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
••
1 1.
1 1 �
1 111
1 111
1 111
i 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 1 •
1 11:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1..
®
1 111
1 111
1 111
1 111
1 111
loll
1 111
1 111
1 111
1 Ili
• •
Total
' •
111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
.•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
AI am aware that there are significant penalties for submitting false information, including the possibility of fines and
)risonment for knowing violations".
2 f2 tC2(7
Signatur o and plier Date
DENR FORM MFLSF (12/2006)

SECTION 4

ff1summmor
r�,��fyticaf L�t�crrarvrJz�s
January 21, 2019
Adam Brigman
Synagro, NC 28134
12701 Lancaster Hwy
Pineville, NC 28134
TEL: [phone]
FAX: [phone]
RE: West Stanley
Dear Adam Brigman:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://wwiv.settek.com
Order No.: 19010440
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/9/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho 01-100923, Illinois
200061, Indiana C-011-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey 01-1006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-I1-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 32

Summit Environmental Technologies, Inc. Case Narrative
In SUMMIT 3310 Win St.
ENVIRONMENTAL r cSi�oLCtctzG, INC.. Cuyahoga Falls, Ohio 44223 WO#: 19010440
AsTittlyfIc t L_sboraforly= TEL: [phone] FAY: [phone]
Website: h�://wwiv.settek.com Date: 1/21/2019
CLIENT: Synagro, NC 28134
Project: West Stanley
WorkOrder Narrative:
19010440: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Enviromnental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19010440-001A SVOC-BNA_TCLP(8270d): Possible low bias for Pyridine due to low recovery in
CCV; Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
19010440-OOIA SVOC-BNA_TCLP(8270d): Sample exhibited low recovery of Surrogates: 2-
Fluorophenol, Phenol-d6 possibly due to matrix effect.
Analytical Sequence QC Notes:
ccv 250 18712 re svoc-cPEST_npw(8081): CCV exhibits high recovery for endrin. All samples are ND
CCV 40ng 14287 SVOC-MSTR_S(8270): The CCV (Batch R93442) exhibited high recovery for
Hexachlorobutadiene and Pentachlorophenol. The associated samples are ND for the analytes with high
Revision v1
Page 2 of 32

Summit Environmental Technologies, Inc. A7
M9SUMMIT 3310 Win St. Case Narrative
hFV14iOtdP.trRlrbL eGCtin�o��7otz5, INC. Cuyahoga Falls, Ohio 44223 WO#: 19010440
fdma(v0dal TEL: [phone] FAX: [phone]
Website: http:lAviviv.settek.corn Date: 1/21/2019
CLIENT: Synagro, NC 28134
Project: West Stanley
recoveries.
CCV 40ng 14287 SVOC-MSTR_S(8270): The CCV (Batch R93442) exhibited low recovery for
Pyridine. Possible low bias for Pyridine due to low recovery in CCV; Reporting Limit Check shows
adequate instrument sensitivity for reporting purposes.
MB-35513 SVOC-BNA_TCLP(8270): MB-35513 exhibited low recovery of Surrogate: 2-Fluorophenol.
MB-35513 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
LCS-35513 SVOC-BNA_TCLP(8270): LCS-35513 exhibited low recovery of Surrogate: 2-
Fluorophenol.
LCS-35513 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
REVISED REPORT: 1/21/19 Includes Case Narrative
Revision vl
Page 3 of 32

Summit Em,ironmental Technologies, In Qualifiers and Acronyms
MM S"tomint 3310 Win 5
EPA'I?C�#JtdKhrrALiEC!iNOLC1Gi�S,WC CzryahogaFalls, Ohio 442� WO#: 19010440
AmTfyfhd ai L-n6orafories TEL: [phone] FAX: [phone]
Website: httD:/Avwiv.settek.co Date: 1/21/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded. Not Clean Water Act compliant.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+),
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
W Samples were received outside temperature limits (0' — 6° C). Not Clean Water Act compliant.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLv1
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 4 of 32

Summit Environmental Technologies, Inc.
Workorder
summlir
3310 Win St.
Sample Summary
E('dVlfiClldfrteNTkL-3cCN.7QLt}C1S.an,C
Cuyahoga Falls, Ohio 44223
Anafytici�J La.brr2inria!�
TEL: [phone] FAX.- [phone]
WO#: 19010440
Website: htro:/hviviv.seliek.com
21-Jan-19
CLIENT:
Synagro, NC 28134
Project:
West Stanley
Lab SampleID Client Sample ID Tag No Date Collected
Date Received Matrix
19010440-001
West Stanley 2019 TCLP
1/8/2019 10:45:00 AM
1/9/2019 10:20:00 AM Sludge
Page 5 of 32

Summit Environmental Technologies, Inc. DATES REPORT
frSUMSWIT 3310 Win St.
ENV1110f-d-AEb1TAL �8C]%11t7LCEGlES, INC. Cuyahoga Falls, Ohio 44223 WO#: 19010440
�3tr rfb t1C�f LbQret�rJe� TEL: [phone] FAX.- [phone]
Website: http:1APvw.se1tek.com 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
19010440-OOIA West Stanley 2019 TCLP 1/8/2019 10:45:00 AM Sludge
Ignitability of Solids (SW-846: 1030)
1/11/2019 11:00:00 AM
Paint Filter Free Liquids Test (SW-846
1/9/2019 3:15:00 PM
9095)
pH (SW9045D)
1/10/2019 3:52:16 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
1/14/2019 11:38:00 AM
Reactive Sulfide (9034)/7.3.4.2
1/14/2019 11:08:00 AM
SVOC PCB (8082) 7-Arochlors
1/10/2019 9:30:00 AM
1/14/2019 1:56:00 PM
TCLP Herbicides Analysis (SW1311/81/9/2019 6:00:00 PM
1/11/2019 5:00:00 PM
1/18/2019 5:11:00 PM
TCLP Mercury Analysis (SW1311/74 i 1/9/2019 6:00:00 PM
1/10/2019 12:45:00 PM
1/10/2019 5:51:00 PM
TCLP Metals Analysis (SW1311/60101/9/2019 6:00:00 PM
1/10/2019 11:45:00 A
1/11/2019 3:13:34 PM
TCLP Pesticides Analysis (SW1311/8(1/9/2019 6:00:00 PM
1;11/2019 11:45:00 A
1/16/2019 12:23:00 PM
TCLP Semi-Volatiles Analysis 1/9/2019 6:00:00 PM
1/14/2019 10:45:00 A
1/16/2019 12:14:00 AM
(S W 1311 /8270)
—
TCLP Volatiles Analysis
1/9/2019 6:00:00 PM
1/10/2019 3:49:00 PM
Revision v1
Page 6 of 32

Summit Environmental Technologies, Inc. Analytical Report
SUM10101- 3310 Win St.
EMVWONfdcutAL FE-14NOLOGI-$,INC. Cuyahoga Falls, Ohio44223 (base report)
llnalvadaf E aboraicanLtfi TEL: [phone] FAX: [phone] WO#: 19010440
Website: http://wivw.settek eom Date Reported: 1/21/2019
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 1/8/2019 10:45:00 AM
Lab ID: 19010440-OOIA
Project: West Stanley
Client Sample ID West Stanley 2019 TCLP
Analyses Result
RL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
0.00500
mg/L
1 1/10/2019 5:51:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW301OA Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND
0.500
mg/L
1 1/11/2019 3:13:34 PM
TCLP Barium(Ba) ND
5.00
mg/L
1 1/11/2019 3:13:34 PM
TCLP Cadmium(Cd) ND
0.100
mg/L
1 1/11/2019 3:13:34 PM
TCLP Chromium(Cr) ND
0.200
mg/L
1 Ill1/2019 3:13:34 PM
TCLP Lead(Pb) ND
0.500
mg/L
1 1/11/2019 3:13:34 PM
TCLP Selenium(Se) ND
0.0500
mg/L
1 1/11/2019 3:13:34 PM
TCLP Silver(Ag) ND
0.500
mg/L
1 1/11/2019 3:13:34 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND
0.0800
mg/L
2
1/16/2019 12:14:00 AM
2,4,5-Trichlorophenol ND
0.200
mg/L
2
1/16/2019 12:14:00 AM
2,4,6-Trichlorophenol ND
0.200
mg/L
2
1/16/2019 12:14:00 AM
2,4-Dinitrotoluene ND
0.0400
mg/L
2
1/16/2019 12:14:00 AM
o-Cresol ND
0.200
mg/L
2
1/16/2019 12:14:00 AM
m/p-Cresol(s) ND
0.200
mg/L
2
1/16/2019 12:14:00 AM
Cresols, Total ND
4.00
mg/L
2
1/16/2019 12:14:00 AM
Hexachloro-1,3-butadiene ND
0.0160
QC+
mg/L
2
1/16/2019 12:14: 00 AM
Hexachlorobenzene ND
0.0400
mg/L
2
1/16/2019 12:14:00 AM
Hexachloroethane ND
0.0800
mg/L
2
1/16/2019 12:14:00 AM
Nitrobenzene ND
0.0800
mg/L
2
1/16/2019 12:14:00 AM
Pentachlorophenol ND
0.200
QC+
mg/L
2
1/16/2019 12:14:00 AM
Pyridine ND
0.200
QC-
mg/L
2
1/16/2019 12:14:00 AM
Surr: 2-Fluorophenol 8.32
10 - 109
S
%Rec
2
1/16/2019 12:14:00 AM
Surr: Phenol-d6 9.24
10 - 109
S
%Rec
2
1/16/2019 12:14:00 AM
Surr: Nitrobenzene-d5 66.4
19 - 120
%Rec
2
1/16/2019 12:14:00 AM
Surr: 2,4,6-Tribromophenol 15.8
10 - 120
%Rec
2
1/16/2019 12:14:00 AM
Surr: 2-Fluorobiphenyl 69.2
22 - 117
%Rec
2
1/16/2019 12:14:00 AM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
0 RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Revision v1
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 7 of 32

Summit Environmental Technologies, Inc. Analytical Report
M9 S at 3310 Win St.
Eh�VI{101JP.11=N1'6tL"4iCN�7i]l.r?Gl<$, INC Cuyahoga Falls, Ohio 44223 (base report)
ilnalytical /ral4orararl'ag TEL: [phone] FAX: [phone] WO#: 19010440
Wehsite: hup.-Mvwiv.settek.com Date Reported: 1/21/2019
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 1/8/2019 10:45:00 AM
Lab ID: 19010440-OOIA
Project: West Stanley
Client Sample ID West Stanley 2019 TCLP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14 100 34 - 116 %Rec 2 1/16/2019 12:14:00 AM
NOTES:
Possible low bias for Pyridine due to low recovery in CCV; Reporting Limit Check shows adequate instrument sensitivity for reporting
purposes.
Sample exhibited low recovery of Surrogates: 2-Fluorophenol, Phenol-d6 possibly due to matrix effect.
SVOC PCB (8082) 7-AROCHLORS
SW8082
SW3550C Analyst: PGP
Aroclor 1016
ND
0.00598
mg/Kg
1
1/14/2019 1:56:00
PM
Aroclor 1260
ND
0.00598
mg/Kg
1
1/14/2019 1:56:00
PM
Aroclor 1221
ND
0.00598
mg/Kg
1
1/14/2019 1:56:00
PM
Aroclor 1232
ND
0.00598
mg/Kg
1
1/14/2019 1:56:00
PM
Aroclor 1242
ND
0.00598
mg/Kg
1
1/14/2019 1:56:00
PM
Aroclor 1248
ND
0.00598
mg/Kg
1
1/14/2019 1:56:00
PM
Aroclor 1254
ND
0.00598
mg/Kg
1
1/14/2019 1:56:00
PM
Total PCBs
ND
0.00598
mg/Kg
1
1/14/2019 1:56:00
PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
24.7
Surr: DCB
35.3
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW131118151)
2,4-D ND
SW8081 SW351OC Analyst: MES
0.0250
mg/L
10
1/16/2019 12:23:00 PM
0.0500
mg/L
10
1/16/2019 12:23:00 PM
0.00500 QC+
mg/L
10
1/16/2019 12:23:00 PM
0.00500
mg/L
10
1/16/2019 12:23:00 PM
0.00500
mg/L
10
1/16/2019 12:23:00 PM
0.00500
mg/L
10
1/16/2019 12:23:00 PM
0.00500
mg/L
10
1/16/2019 12:23:00 PM
10 - 119
%Rec
10
1/16/2019 12:23:00 PM
10 - 119
%Rec
10
1/16/2019 12:23:00 PM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
SW8151A SW8151A Analyst: MES
1.00 mg/L 1 1/18/2019 5:11:00 PM
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Revision v1
RL Reporting Detection Limit
Page 8 of 32

Summit Environmental Technologies, Inc. Analytical Report
fn SUARMIT 3310 Win St.
FJiUlfi�i•!M_NTdL riECHNOWGIZ,, INC Cuyahoga Falls, Ohio 44223 (base report)
/lrrafvrlt;af La.bnranl ar/e TEL: [phone] FAX: [phone] WO#: 19010440
Website: httP:1Avww.settek.com Date Reported: 1/21/2019
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 1/8/2019 10:45:00 AM
Lab ID: 19010440-001A
Project: West Stanley
Client Sample ID West Stanley 2019 TCLP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)
2,4,5-TP ND 0.500
Surr: DCAA 70.1 20 - 140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
96.9
Surr: Dibromofluoromethane
95.0
Surr: Toluene-d8
97.7
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
PAINT FILTER FREE LIQUIDS TEST (SW-846: 9095)
Free Liquid fail
RCI-SOLID-W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
SW8151A SW8151A Analyst: MES
mg/L 1 1/18/2019 5:11:00 PM
%Rec 1 1/18/2019 5:11:00 PM
SW8260B SW1311 M Analyst: RMT
0.0500
mg/L
10
1/10/2019 3:49:00 PM
0.0500
mg/L
10
1/10/2019 3:49:00 PM
0.250
mg/L
10
1/10/2019 3:49:00 PM
0.0500
mg/L
10
1/10/2019 3:49:00 PM
0.0500
mg/L
10
1/10/2019 3:49:00 PM
0.0500
mg/L
10
1/10/2019 3:49:00 PM
0.0500
mg/L
10
1/10/2019 3:49:00 PM
0.0500
mg/L
10
1/10/2019 3:49:00 PM
0.0500
mg/L
10
1/10/2019 3:49:00 PM
0.0200
mg/L
10
1/10/2019 3:49:00 PM
70 - 130
%Rec
10
1/10/2019 3:49:00 PM
70 - 130
%Rec
10
1/10/2019 3:49:00 PM
70 - 130
%Rec
10
1/10/2019 3:49:00 PM
SW9014
Analyst: MS
0.495
mg/Kg
1
1/14/2019 11:38:00 AM
SW9095
Analyst: DHC
1
1/9/2019 3:15:00 PM
SW1030
Analyst: AJT
1
1/11/2019 11:00:00 AM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Revision v1
RL Reporting Detection Limit
Page 9 of 32

Summit Environmental Technologies, Inc. Analytical Report
prs"Mmur 3310 Win St.
€J`WIROHFol =NTAL TIC VIOLt1GIES, INC Cuyahoga Falls, Ohio 44223 (base report)
rIffafyilcal F.abow0ria-e TEL: [phone] FAX.- [phone] WO#: 19010440
Website: htto:/hvivw.settek.com Date Reported: 1/21/2019
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 1/8/2019 10:45:00 AM
Lab ID: 19010440-OOIA
Project: West Stanley
Client Sample ID West Stanley 2019 TCLP
Analyses Result RL Qual Units DF Date Analyzed
RCI-SOLID-WI IGNITABILITY1030 SW9045D Analyst: VVK
PH (SW9045D)
pH 6.2 s.u.@20.4C 1 1/10/2019 3:52:16 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 1/14/2019 11:08:00 AM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Revision v1
RL Reporting Detection Limit
Page 10 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
RMSUMM.1y3310 Win St.
Anal tes Report
y 1�
ENVli'OtdtalcNTALTECtiNOLOC,ir-S,SNC
Cuyahoga Falls,Ohio44223
Amalyacai L-2borarones
TEL: [phone] FAX.- [phone]
WO#:
19010440
Website: htto://iviviv.settek.coni
21-Tan-19
Client: Synagro, NC 28134
State: NW
Project: West Stanley
Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19010440-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Paint Filter Free Liquids Test (SW-846: 9095)
Free Liquid
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1016
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1221
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1232
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1242
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1248
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1254
A
Sludge
SVOC PCB (8082) 7-Arochlors
Aroclor 1260
A
Sludge
SVOC PCB (8082) 7-Arochlors
Total PCBs
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4,5-TP
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4-D
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
DCAA
A
Sludge
TCLP Mercury Analysis (SW131 in470)
Mercury
A
Sludge
TCLP Metals Analysis (SW131 I/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW 1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW 1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW 1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW 13 11/60 10)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SWI311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Version #2
Page 11 of 32

Summit Environmental Technologies, Inc.
Accreditation
Program
InSUMMIEF 3310 Win St.
Anal tes Report
Y P
€N.VlrtOt.lr4lPNlTAL'FrClino
LICGi=S, INC Cuyahoga Falls, Ohio 44223
A-m7lytic7l L2boretorleg
TEL: [phone] FAX.- [phone]
WO#:
19010440
Website: htto://lpwii,.settek.com
21-Jan-19
Client: Synagro, NC 28134
State: NW
Project: West Stanley
Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19010440-OOIA Sludge
TCLP Pesticides Analysis (SW1311/8081)
Tetrachloro-m-xylene
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Tribromophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
3,4-Methylphenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene-d5
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Phenol-d6
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
p-Terphenyl-d14
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
4-Bromofluorobenzene
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chlorofonn
A
Sludge
TCLP Volatiles Analysis
Dibromofluoromethane
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Toluene-d8
A
Version #2
Page 12 of 32

Summit Environmental Technologies, Inc.
surArAly 3310 Win St.
ERUIRONMEMTAL Tf:C]1N0LlAC1A$, INC Cuyahoga Falls, Ohio 44223
Anafytical LaboratorJag TEL: [phone] FAX: [phone]
Website: hito:/hviviv.settek.com
Client: Synagro, NC 28134
Accreditation Program
Analytes Report
WO#: 19010440
21-Jan-19
State: NW
Project: West Stanley Program Name: NC WW_SCM
Sample ID Matrix Test Name Analyte Status
19010440-OOIA Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis
Vinyl chloride A
Version #2
Page 13 of 32

Sunnnit Environmental Technologies, Inc. QC SUMMARY REPORT
'91 summ-1 1 3310 Win St. l� SUMMARY REPORT
1�, j
ENVIr20#JP.12T.TALTECHNOL-QCIbS;INC Cuyahoga Falls, Ohio44223 WO#: 19010440
ArrrdyrFcal L-riSoratorfin TEL: [phone] FAX.- [phone]
Website: http:/hviviv.settek.cont 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: 35455
Sample ID MB-35455
SampType: MBLK
TestCode: TCLP-voc-ms Units: mg/L
Prep Date: 1/9/2019
RunNo: 93248
client ID: PBS
Batch ID: 35455
TestNo: SW8260B SW1311M
Analysis Date: 1/1012019
SegNo: 1902259
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
ND
0.00500
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200
Surr: 4-Bromofluorobenzene
48.0
Surr: Dibromofluoromethane
48.0
Surr: Toluene-d8
48.0
50.00 95.9 70 130
50.00 95.9 70 130
50.00 95.9 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit ReVISIOri V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 14 of 32

Summit Environmental Technologies, Inc.
S umfoill 3310 Win St.
Ph;l�li±C�tJtllthlTPYL'TE�fihtOl ()Gig, fPiG Cuyahoga Falls, Ohio 44223
z<<Iytical,L atiartaSrtrles TEL: [phone] FAX. [phone]
Website: hito://ivivx,.settek.coni
QC SUMMARY REPORT
WO#: 19010440
21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: 35458
Sample ID MB-35458
SampType: MBLK
TestCode:
SVOC-PCB_ Units: %Rec
Prep Date: 1/10/2019
RunNo: 93274
Client ID: PBS
Batch ID: 35458
TestNo:
E608 SW3550C
Analysis Date: 1/10/2019
SegNo: 1902113
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr: DCB
35.2
33.40
105
10
165 m
Surr: TCMX
24.1
33.40
72.1
10
139
Sample ID LCS-35458
SampType: LCS
TestCode: SVOC-PCB_ Units: %Rec
Prep Date: 1/10/2019
RunNo: 93274
Client ID: LCSS
Batch ID: 35458
TestNo: E608 SW3550C
Analysis Date: 1/10/2019
SegNo: 1902114
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr: DCB
34.9
33.40
104
40.6
130 m
Surr: TCMX
23.9
33.40
71.5
28.2
130
Sample ID 19010442-001AMS
SampType: MS
TestCode: SVOC-PCB_ Units: %Rec
Prep Date: 1/10/2019
RunNo: 93274
Client ID: BatchQC
Batch ID: 35458
TestNo: E608 SW3550C
Analysis Date: 1/10/2019
SegNo: 1903336
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Surr: DCB 120 200.0
Surr: TCMX 59.9 200.0
59.9 11.9 124
29.9 32.6 105 S
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision V 1
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 15 of 32

sumforrSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
£h;4�Ii?�+tJM1 'hiT�L TL3;6It� CS Lf}1T S,, arac. Cuyahoga Falls, Ohio 44223 WO#: 19010440
rti7aiytical LatiarntonoSc TEL: [phone] FAX.- [phone]
Website: http:/hnviv.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: 35458
Sample ID 19010442-001AMSD
SampType: MSD
TestCode:
SVOC-PCB_ Units: %Rec
Prep Date: 1/10/2019
RunNo: 93274
Client ID: BatchQC
Batch ID: 35458
TestNo:
E608 SW3550C
Analysis Date: 111012019
SegNo: 1903336
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Surr: DCB 120 200.0 59.9 11.9 124 0 0
Surr: TCMX 79.8 200.0 39.9 32.6 105 0 0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Revision V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 16 of 32

ly Stuttttrit Environmental Technologies, Inc. QC SUMMARY' REPORT
3310 Win St.
OP;till?C7tJtrJ�P•1TALiEri!i64C1tLFtFS.1jrt Cuyahoga Falls, Ohio44223
.4ttzti}Fticaf Labcirattrrlc�e WO#: 19010440
TEL: [phone] FAX.- [phone]
Website: hap.-Ilwiviv.settekcom 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: 35459
Sample ID MB-35459
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID: PBS
Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 111012019
SegNo: 1903301
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-35459
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID: LCSS
Batch ]D: 35459
TestNo: SW7470A SW7470A
Analysis Date: 111012019
SegNo: 1903302
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Mercury 0.00439 0.00200 0.00400 0 110 80 120
Sample ID 19010394-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID: BatchQC
Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 1/10/2019
SegNo: 1903306
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury 0.00445 0.00200 0.00400 0.0000500 110 75 125
Sample ID 19010394-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
Client ID: BatchQC
Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 1/10/2019
SegNo: 1903306
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00441 0.00200 0.00400 0.0000500 109 75 125 0.00445 0.903 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit ReV1S10ri V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 17 of 32

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
S u MM I v 3310 Win St.
P:S�Ii fJgdfEAtT�.L rtc9i67p1 C3 at1S. 9hdC Cuyahoga Falls, Ohio 44223 WO#: 19010440
A17afytfcad—abr�radoneg,. TEL: [phone] FAX: [phone]
Website: htta://iviviv.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: 35459
Sample ID 19010394-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/10/2019
RunNo: 93323
client ID: BatchQC
Batch ID: 35459
TestNo: SW7470A SW7470A
Analysis Date: 1/10/2019
SegNo: 1903306
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Revision Vl
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 18 of 32

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Sum, f"Ict 3310 Win St.
Eh4rIROIJ?AEtJTAL TLC!iNOLja'g]ZS, pzC� CztyahogaFalls, Ohio 44223 WO#: 19010440
rartdsfytical Labcr,31aries. TEL: [phone] FAX.- [phone]
Website: http.•Ilwwiv.settek.cont 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: 35480
Surr: TCMX
12.0
50.00
24.0
10
119
Surr: DCB
18.2
50.00
36.5
10
119
Surr: TCMX
12.6
50.00
25.1
10
119
Surr: DCB
19.6
50.00
39.2
10
119
Surr: TCMX 24.5
50.00 49.1 10
119
Surr: DCB 41.1
50.00 82.2 10
119
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit ReViS10ri V 1
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 19 of 32

S mfd ill
Summit Environmental Technologies, Inc.
3310 Win St.
Tr M ,� 7� Y REPORT
� E PO T
1. t7 LJ j!1 Limit P.r i\ 1
QC SUMMARY
PF;4�IR+3#Jtdl�tdTAL,�c;i� t#tt}.G��S, tPiC
Cuyahoga Falls, Ohio 44223
WO#: 19010440
Arralytical L3boraxodoe TEL: [phone] FAX.- [phone]
Website: http://iviviv.settek.com
21-Jan-19
Client:
Synagro, NC 28134
Project:
West Stanley
BatchID: 35480
Sample ID 19010257-001amsd
SampType: MSD
TestCode: tclp-svoc-CP Units: %Rec
Prep Date: 1/11/2019
RunNo: 93408
client ID: BatchQC
Batch ID: 35480
TestNo: E608 SW3510C
Analysis Date: 1/15/2019
SegNo: 1906922
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Surr: TCMX 25.9 50.00 51.7 10 119 0
Surr: DCB 39.7 50.00 79.5 10 119 0
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit ReV1SI0ri V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 20 of 32

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
M9 SUMMINt 3310 Win St.
Ft,Wlr?Ofdfilrb T'AL`Fr-CH aOLQGIr-3, IpTC Cuyahoga Falls, Ohio 44223 WO#: 19010440
Ai7c,(yrIcal Laboratories TEL: [phone] FAX.- [phone]
Website: hap.-Mvivw.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchIID: 35513
Sample ID MB-35513
SampType: MBLK
TestCode:
SVOC-BNA T Units: %Rec
Prep Date: 1/14/2019
RunNo: 93442
client ID: PBS
Batch ID: 35513
TestNo:
E625 SW3510C
Analysis Date: 1/15/2019
SegNo: 1908302
knalyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Surr: 2-Fluorophenol
0.0980
1.000
9.80
10
109 S
Surr: Phenol-d6
0.100
1.000
10.0
10
109
Surr: Nitrobenzene-d5
0.665
1.000
66.5
19
120
Surr: 2,4,6-Tribromophenol
0.146
1.000
14.6
10
120
Surr:2-Fluorobiphenyl
0.654
1.000
65.4
22
117
Surr: p-Terphenyl-d14
0.893
1.000
89.3
34
116
Sample ID LCS-35513
SampType: LCS
TestCode: SVOC-BNA_T Units: %Rec
Prep Date: 1/14/2019
RunNo: 93442
client ID: LCSS
Batch ID: 35513
TestNo: E625 SW3510C
Analysis Date: 1/16/2019
SegNo: 1908303
knalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr: 2-Fluorophenol
0.110
1.000
11.0
17.1
130 S
Surr: Phenol-d6
0.108
1.000
10.8
10
130
Surr: Nitrobenzene-d5
0.721
1.000
72.1
32.6
130
Surr: 2,4,6-Tribromophenol
0.179
1.000
17.9
4.43
130
Surr:2-Fluorobiphenyl
0.734
1.000
73.4
41.8
130
Surr: p-Terphenyl-d14
1.05
1.000
105
36.4
130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
Revision V l
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 2.1 of 32

summlir
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
E ,'' ld?CtifJPal-tRAL'TtCtrl�acilAC;I�S, JrZG
Cuyahoga Falls, Ohio 44223
WO#: 19010440
ArtatlrtdcaP L-I>;s?ratorloc TEL: [phone] FAX.- [phone]
Website: httD•/hviviv.settek.com
21-Jan-19
Client:
Synagro, NC 28134
Project:
West Stanley
BatchID: 35513
Sample ID 19010307-001AMS
SampType: MS
TestCode:
SVOC-BNA_T Units: %Rec
Prep Date: 1/1412019
RunNo: 93442
client ID: BatchQC
Batch ID: 35513
TestNo:
E625 SW3510C
Analysis Date: 1/15/2019
SegNo: 1908304
analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr:2-Fluorophenol
0.107
1.000
10.7
3.39
89.9
W
Surr: Phenol-d6
0.107
1.000
10.7
-2.08
55
W
Surr: Nitrobenzene-d5
0.683
1.000
68.3
14.5
154
W
Surr:2,4,6-Tribromophenol
0.175
1.000
- 17.5
19.5
93.2
SW
Surr:2-Fluorobiphenyl
0.753
1.000
75.3
34.4
121
W
Surr: p-Terphenyl-d14
1.01
1.000
101
8.86
156
W
Sample ID 19010307-001AMSD
SampType: MSD
TestCode:
SVOC-BNA T Units: %Rec
Prep Date: 1/14/2019
RunNo: 93442
client ID: BatchQC
Batch ID: 35513
TestNo:
E625 SW3510C
Analysis Date: 1/15/2019
SegNo: 1908305
analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr:2-Fluorophenol 0.0844
1.000 8.44
3.39
89.9
0
W
Surr: Phenol-d6 0.0900
1.000 9.00
-2.08
55
0
W
Surr: Nitrobenzene-d5 0.586
1.000 58.6
14.5
154
0
W
Surr:2,4,6-Tribromophenol 0.152
1.000 15.2
19.5
93.2
0
SW
Surr:2-Fluorobiphenyl 0.677
1.000 67.7
34.4
121
0
W
Surr: p-Terphenyl-d14 0.965
1.000 96.5
8.86
156
0
W
Qualifiers: * Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Revision Vl
MC Value is below Minimum Compound Limit.
ND
Not Detected
0
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 22 of 32

Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENI '' rOfJF1EINT11L EC11hoLOGI1:5, IrZC
Cuyahoga Falls, Ohio 44223
WO#: 19010440
�liT^riyttl al t�iioralrtrlc�s TEL: [phone] FAX. [phone]
Website: hup.-Mviviv.seae%com
21-Jan-19
Client:
Synagro, NC 28134
Project:
West Stanley
BatchID: 35523
Sample ID Ics-35523
SampType: LCS
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
Client ID: LCSS
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914631
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 78.4
43.8
130
2,4,5-TP
ND
0.500 0.500
0 62.9
51.5
ill
Surr: DCAA
357
500.0
71.4
34.2
150
Sample ID mb-35523
SampType: MBLK
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
Client ID: PBS
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914632
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0 0 d
2,4,5-TP ND 0.500 0 0
Surr: DCAA 320 500.0 64.0 20 140
Sample ID 19010307-001ams
SampType: MS
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
Client ID: BatchQC
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914634
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND 1.00
0.500 0 100 37
105
W
2,4,5-TP
ND 0.500
0.500 0 89.8 38
106
W
Surr: DCAA
567
500.0 113 20
140
W
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Revision Vl
MC
Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 23 of 32

Sununit Environmental Technologies, Inc. QC
SUMMARY
REPORT
InSummior 3310 Win St.
%l�lf2t]fJrnEtrrtiL3E4;d91tSllti�ws, irtc Cuyahoga Falls, Ohio 44223 WO#: 19010440
Anadylfcal Lafior�lorlo€ TEL: [phone] FAX.- [phone]
Website: htt,2.-1Avivw.set1ek.corn 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: 35523
Sample ID 19010307-001amsd
SampType: MSD
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
Client ID: Batch=
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914646
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D ND 1.00 0.500 0 83.7 37 105 0 0 30 W
2,4,5-TP ND 0.500 0.500 0 71.5 38 106 0 0 30 W
Surr: DCAA 453 500.0 90.6 20 140 0 W
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Revision V l
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 24 of 32

M9
S U mhu ir
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
El'Arl[TONMEMAL TECIMOLoCi:E5, INC
Cuyahoga Falls, Ohio 44223
WO#: 19010440
Anjlfr[Icat Labo' ratdr/QLe TEL: [phone] FAX.- [phone]
Website: htto:/fiviviv.seliek.com
21-Tan-19
Client:
Synagro, NC 28134
Project:
West Stanley
BatchID: R93258
Sample ID LCS-R93258
SampType: LCS
TestCode: pH_011(9045 Units: s.u.@21.9C -
Prep Date:
RunNo: 93258
Client ID: LCSW
Batch ID: R93258
TestNo: SW9045D
Analysis Date: 1/1012019
SegNo: 1901827
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.7 90 110
Sample ID CHECK 7
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@21.9C
Prep Date:
RunNo: 93258
Client ID: LCSW
Batch ID: R93258
TestNo: SW9045D
Analysis Date: 111012019
SegNo: 1901844
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.0 7.0 0 100 90 110
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Revision V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 25 of 32

summlirSunrrnft Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
L:4rI1ZLj#Jtq�tWTitL$'Le9ii+znlc3Gltig;9PdC. Cuyahoga Falls, Ohio44223
•Af7arfjltfCaPTEL: [phone] FAX.- [phone]
WO#: 19010440
Website: htto://wivtiv.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: R93297
Sample ID LCS-R93297
SampType: LCS
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
client ID: LCSS
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902691
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDUrnit Qual
Ignitability
8.08
7.240 0 112 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit ReViSlOri Vl
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 26 of 32

SUMMITSumuzit Em�ironn:ental Technologies, 1ne. 3310 Win St. QC SUMMARY REPORT
EftVIfloOU142t,1TA. LTt1;BAN0Latal�S,'onc. Cuyahoga Falls, Ohio44223
Anattlitfcal L3Loraxor1eG TEL: [phone] FAX.- [phone] WO#: 19010440
Website: http://iviviv.settek.com 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: R93390
Sample ID 19010535-01AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
Client ID: Batch=
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906045
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 8.98 0.490 10.00 0 89.8 81.6 122
Sample ID 19010535-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
Client ID: BatchQC
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906046
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.09 0.495 10.00 0 90.9 81.6 122
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit Revision v1
P Second column confirmation exceeds PL Pen -nit Limit R RPD outside accepted recovery limits
Page 27 of 32

SU JM'M.1 ,
Summit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
�F#L�If;�tJ1dIE7JrAL SEfi!%dU©LtTG19S, ihtl.
Cuyahoga Falls, Ohio 44223
ArrvtyUcal L ri5c�raiort s TEL: [phone] FAX.- [phone]
WO#: 19010440
Website: http:/hviviv.settek.com
21-Jan-19
Client:
Synagro, NC 28134
Project:
West Stanley
BatchID: R93390
Sample ID LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mg1L
Prep Date:
RunNo: 93390
client ID:' LCSW
Batch ID: R93390
TestNo: SW9014
Analysis Date: 111412019
SegNo: 1906029
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.57 0.490 10.00 0 95.7 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected 0 RSD is greater than RSDlimit Revision v1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 28 of 32

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
PM summlir 3310 Win St.
Er Vlltel+JY4r:t•tTtit 1 �olhpl ctpa S, trtG Cuyahoga Falls, Ohio 44223 WO#: 19010440
Arraf. rGlcaf Lattaratorin?s TEL: [phone] FAX. [phone]
Website: hap.-Ilivrviv.settek.conz 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: R93465
Sample ID 19010535-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
Client ID: BatchQC
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908916
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4210 25.0 4800 0 87.7 80 120
Sample ID 19010535-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
Client ID: BatchQC
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/1412019
SegNo: 1908917
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 4320 25.0 4800 0 90.0 80 120 4210 2.58 30
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit ReV1S10n V 1
P Second column confirmation exceeds PL Penn it Limit R RPD outside accepted recovery limits
Page 29 of 32

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
M9 SUMMINt 3310 Win St. \C 1. SUMMARY i REPORT
�ht�lrtC�tlfdl tJTAL:LC!iNCj1 C}GiSa, 1PtG Cuyahoga Falls, Ohio 44223
A,nptyt/cat LabcYratorle� TEL: [phone] FAX.- [phone] WO#: 19010440
Website: hup:/hviviv.settekcom 21-Jan-19
Client: Synagro, NC 28134
Project: West Stanley BatchID: R93465
Sample ID MB-R93465
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 93465
Client ID: PBW
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908902
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID LCS-R93465
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 93465
Client ID: LCSW
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/1412019
SegNo: 1908903
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4620 25.0 4800 0 96.2 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit ReV1S10n V 1
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 30 of 32

DC-QACOC338 RevA.l
Efrecuve Dom: 1111212ais
SUM,M�T
ENYIRONh1ENTAL TEci OL�OGII INC.
3310 Wm Sn.et
Cuyotrpo rung Onto "223
IIu0.270-OS40
($ 7Q 1 I-Lt ncq aer- f-bw
'den('�l Nc Z113`'
6 Sr0 - Li 3 Lf
oatjj��ct eRon �jj�
1T�4h? j,�C"t,gi'ti4h
Ment Email Addeen
ab - c, Sy���;ro
sampled (PrintNameand vide na/un
� n �
'or DW aNY. results have cd to
rthel.6?Ifyp,lab.Teemeyapply Y�
I
Analysis Request / Chain of Custody
For Summit Environmental Technologies, Inc. use only SET WO No.:
Flud us at. www.settekcom
ll% 4il I e AnalyticmlParsmetot
s
SO't �-rcoq ,
rtTo
dCfm 8
d IAAA
;FA
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Quato Number
fit
Fadt[tylD
0-21 i0
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rnaWAeereditatfon Requirements
Ohio VAP OEPA Pb, Cu
Dtink[neWater Compltance
Other Compltaace
,
x.(ListStaidProgram): t�
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Collated
ZGIq
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It
Was suflic em volume Pmvldtd to run QC: YES I NO Cooler. YES I No Other
Received In I.sb by: DAt* Tine Carrkr
Rush Requested: Z L�DaY(s)
Must be approved by Lmb Maaager Rec. Tam J Ice ES NO /melted
Legend: Ptcser atives: INO , 2=H2SO4, 3-HCI, 4-Zinc Acetate, 5-NaOH, 6-EDA, 7=none, &other s
Page I of] i pecified in comments) Refer to lab's terms and conditions at vrwwe c .settcom
9
A
Page 1 of 1
Page 31 of 32

Slim Suntn:it Em ironmental Technologies, Inc.
3310 Win St.
EPIVIROW,.IENTALTECNNOL[JG1ES,INC. Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Amalyticaf Laiieratar/eg TEL: [phone] FAX: [phone]
Website: http://tiviviv.settek.coni
Client Name: SYN-NC-28134 Work Order Number: 19010440 RcptNo: 1
Logged by: Rachel Thomas 1/9/2019 10:20:00 AM f f>
Completed By: Christopher Livengood 1/9/2019 2:17:52 PM
Reviewed By: Jennifer Woolf - 2 1/10/2019 3:31:44 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? UPS
Log In
3. Coolers are present? Yes S6 No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes W No ❑ NA ❑
7. Sample(s) in proper container(s)?
Yes
Se
No ❑
8. Sufficient sample volume for indicated test(s)?
Yes
d❑
No ❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
k
No ❑
10. Was preservative added to bottles?
Yes
❑
No ❑
NA ❑d
NA
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑
No VOA Vials
12. Were any sample containers received broken?
Yes
❑
No W
13. Does paperwork match bottle labels?
Yes
❑
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
d❑
No ❑
15. Is it clear what analyses were requested?
Yes
❑d
No ❑
16. Were all holding times able to be met?
Yes
❑d
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
W
No ❑
NA ❑
Person Notified: I Adam Brigman Date 8/15/2018
By Whom: f Jennifer Woolf Via: ❑./ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding: �sa mple date
Client Instructions: 1 coc is inccorect - date is 8/13/18 -
18. Additional remarks:
Cooler Information
•I Cooler No Temp °C Condition I Seal Intact I Seal No I Seal Date I Signed By
1 15.5 Goodl Not Present
Page 32 of 32

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: West Stanly WWTP WQ Permit Number: WQ0016247
WWTP Name: West Stanly WWTP NPDES Number: NCO043532
Monitoring Period: From 01/01/2019 To 12/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahle to alternative nerformed (C'.lac.c A nr C'lacc R) rmmnlete the fnllnwino mnnitnrino rlatav
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6th
MPN
Coliform
power per gram
MPN/g
of total solids
CFU
174,435
286,476
660,720
CFU/g
1
Annually
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and, evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Tommy Gibbons Plant ORC
Preparer Name and Title (type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: West Stanley Biosolids
Project Number: 50-2170
Lot Number:UA09021
Date Completed:01/14/2019
01/17/2019 1:34 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
P«R�
it
2� G
ACLREOITEO
`9BORASO�`
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UA09021
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Geometric Mean
286,476
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

Client:Synagro Laboratory ID: UA09021 -001
Description: West Stanley 2019 Fecal Matrix: Solid
Date Sampled:01/09/2019 0615 % Solids: 2.87 01/10/2019 0111
)ate Received:01/0912019
Inorganic non-metals
.tun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/10/2019 1955 AMR 01/09/2019 2030
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 174435 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
6 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

Client: Synagro Laboratory ID: UA09021-002
Description: West Stanley 2019 Fecal Matrix: Solid
Date Sampled:01/09/2019 0615 % Solids: 2.54 01/10/2019 0111
Date Received:01/09/2019
Inorganic non-metals
Aun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/10/2019 1955 AMR 01/09/2019 2030
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 276058 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
No = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
6 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Synagro Laboratory ID:UA09021-003
Description: West Stanley 2019 Fecal Matrix: Solid
Date Sampled:01/09/2019 0615 % Solids: 2.55 01/10/2019 0111
Date Received: 01/0912019
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/10/2019 1955 AMR 01/09/2019 2030
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 215602 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
iealy Environmental Services, Inc.
6 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Synagro Laboratory ID:UA09021-004
Description: West Stanley 2019 Fecal Matrix: Solid
Date Sampled:01/09/2019 0615 % Solids: 2.84 01/10/2019 0111
Date Received: 01109/2019
Inorganic non-metals
.tun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/10/2019 1955 AMR 01/09/2019 2030
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 423087 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
iealy Environmental Services, Inc.
6 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Synagro Laboratory ID: UA09021-005
Description: West Stanley 2019 Fecal Matrix: Solid
Date Sampled:01/09/2019 0615 % Solids: 2.48 01/10/2019 0111
Date Received:01109/2019
Inorganic non-metals
stun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/10/2019 1955 AMR 01/09/2019 2030
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D- 201800 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
iealy Environmental Services, Inc.
6 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 12

Client:Synagro Laboratory ID:UA09021-006
Description: West Stanley 2019 Fecal Matrix: Solid
Date Sampled:01/09/2019 0615 % Solids: 2.96 01/10/2019 0111
Date Received:01/09/2019
Inorganic non-metals
.tun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/10/2019 1955 AMR 01/09/2019 2030
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 270371 20 col/g 1
LOQ = Limit of Quantitaton B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
6 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 12

Client:Synagro Laboratory ID: UA09021-007
Description: West Stanley 2019 Fecal Matrix: Solid
Date Sampled:01/09/2019 0615 % Solids: 2.12 01/10/2019 0111
Date Received:01/0912019
Inorganic non-metals
Aun Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 01/10/2019 1955 AMR 01/09/2019 2030
CAS Analytical
Parameter Number Method Result Q LOQ' DL Units Run
Fecal Coliform-MF SM 9222 D- 660720 20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
ealy Environmental Services, Inc.
6 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

8o)
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Timm 13.1tecr Zd by, Ta-,
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s are mado is civet' en !ca R-Wolpt 7,P--np. Tuin ?lank(Cilank.l I Y N e' N
FT-`9Cd12! Date

SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy r4Lvhw11r=UI SUMS.*, I¢,; I lid I : I
Pxumofit NvrnUx. rdnCU13C-14 L•ficc6i�e Daly, $r2ZU1S
Sample Receipt C;heeid9s>t (SC'j
Client; -5vt..�Ul 0 f Coulur Inspected b}+!date_ I
Meads ofrcm*t: EPSESI .-j Client I,_I UPS E] Fedkx Cl Other
Yes _ No 1. Were cnsrody seals present on Iftc cxtleri
Yes Q No _ N ?. If austady seals were prc3..nt, were then intact and era mkcn'
pH Strip 1t): _ Chlorine Strip ID; -- Tested by; ` - _
Qrigirwt tccrrnperature upim receipt? Derived (Corccled) temperature llpon receiut: %Solid Snap -Cup 11); _f
Method.- WT-arnperau;-i�mr Blank ❑Against B�attics IR Gun It): � IR Cst n Correction Factor. C} 'C
Method o[cuvlant= I Wet lee El [cc Packs El Dry Ice CI Norte
�,
❑ NuNA
3_ I(icrnperatum as any cpo[cr ccee,]ad b.Cl°C', v,ps I'n��ecL
Manager Notif
P1w� waq Noritied by: phone ? ernatl ? CaLU4,arfstcc (eiry�le
one).
L 1 Yes
❑ No
I NA
�4. Is the CarmmCTG aI courier's flocking slip attached to t[
is forau?
Yes
❑ No
d. Vl'ere proper custody procedurt-s (relinquish+ d!rct civ
to[iowecl?
Yes
❑ No
fr. Were sample [Las listed (in thi COC?
I Yes
Ej No
1
7. Wcno sample IDs listed on all .cu qik roniaiuers?
Yes
❑ N':0
S. IV-Iq collodion date & time listed on the CO(7?
Yes
E No
9. %Vr a collection date & time listed on all sumpfv coma
eIV
1'cs
`= !tiro
10. Did all container lalicl information (ID; date, time) w
r ee with the COC?
T Yes
❑ Nol,
11. Were test: w bo performed listed on the COC?
f
— 1— au Imries arsine in the proper coauainem for ea
(unbroken; Iids on, etc,)?
It teSL and?or in good condition
—
Yus
❑ No
11 Wasadrquate sample volinno avaitab[O
YeS
Tfu
1'1. Won all santplc5 rcceived willtin ;fz the holdian tir[re
jr 48 hours, ,xhlche`'el' Ct nw!i [Irst?
='es
No
15. Were any stmplc.'5 oolltafila1'S rnissing/m\CAS& (cfrckG
e) samples Not listed on COC?
Yes
❑ NoN�
16, For VOA and RSK-175 sast7[�Ics, were bubble~ f�resc
t>`=p a-si>' (!'�"or 6rtlrn in diamcttr) is
Any of the VOA vials?
If Yes
Nio
NA
I o- IV= all DROrl11041sfnutrieat sarnplcs rceeivad at a p
Hl of <2?
❑ Ye
❑ No
NA
18. AVere all cyanide samples received at a pH -• 12 and s
[tide samples rexxivv�tl at a lal r s 9?
Dyes
?7' Tdo
NA
19. NVare all apu Ica le NH;+`iltiNfcyanir�elphenel.+ti2� (`
0.5rn�+'L}samples free ol-residual
El Yes ❑ Nol " Nr4ieorre<;-Jly
26. Wvrc client remarhti'rvqucses (i.e. requested dilutions NlS/MSD desiglll dons, eta...)
f' I trrnscribed frOM the COC. into the colmment cep ion in Lf'vlS7
❑ Yes No1 121, Was the quate. number listed un the coutainor label? [ yes, Qteote 1
iarnple 1'reservattion (ivltrsl be cumpieted for any smaipic.(s) incorrectly preserved or with headspa ce.)
arrtplc{s}i _ Wcm r"elved incon%=tl}: Pj tsenlod and w -adjusted acculjirtg[y
n sarllp[c rcccivin with - utL of circle one: 1-l2SQ-% HNO3, I ICI, ldrrClli usingq SR +?
ime of prescrvattaea . If rnure than one IN -awn utivc is needed, please 11 w in the comments below.
vrere reet.ive with blrbblcs -G turn in diameter,
ls) were r:ceivctl tieith 7'RC : 0.5 m&'L (If It rt is no) i7rlcl vrcrc
accordingly in sanxple reepiving with sodium thiasllitale (N.a_S,,Cs) with Sh aly ID.
narcode labels applied by:
Hate: , j_Cf _
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

AM
PA
PROMPT -ACCURATE- RELIABLE
LABORATORIBS, INC
AV%VNN.PARLABS.0011
REPORT OF ANALYSES
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: JAN 19
DATE: 02/13/19
SAMPLE NUMBER- 134568 SAMPLE ID- WEST STANLEY SAMPLE MATRIX- SO
DATE SAMPLED- 01/08/19 TIME SAMPLED- 1030
DATE RECEIVED- 01/09/19 SAMPLER- AB RECEIVED BY- DJ
TIME RECEIVED- 0800 DELIVERED BY- AB TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 01/09/19 1010 RE 0.73 I
LABORATORY DIRECTOR L% `^ .; iL=':s fZi'✓ G
f
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fat: [phone]

PA&F;Z
PROM PT -ACCURATE- RELIABLE
I ABORAX01E IES, IWC
WWW. PARLABS. COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
• WEST STANLEY
134668
r 01/09/19
02/07/19
Start: End:
TS
0.1616
0.1663
TS%
1.63%
1.64%
VS )
0.1133
0.1150
VS%
70.11 %
69.15%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0114266
0.0113418
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0048712
0.0050594
FSVR Mass Balance)
0.73%
FSVR Van Kleeck
0.73%
FSVR Mass Balance <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] Fax: [phone]

PAR
PROMPT'
ACCURATE- RELIABLE
R LABOATORIES, INC
W W W. PARLABS.COM
Collected
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge Wt
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample Wt
+ Tare Wt (g)
Dried Sludge Wt (g)
Fixed Solids Wt (g)
Furnace Temp °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
30 Day Bench Scale Extended Aeration Test
VAR Ootion 3. Percent Volatile Solids Reduction
SYNAGRO
® WEST STANLEY
134568
■ 01/09/19
■ ■ 02/07/19
As Received Day 0 Day 7 Day 14 Day 21 Day 28
nlfno/icil n111nr19 n1117/19 01/2A/19 01/31/19 02/07/19
4.90
5.38
5.88
6.70
6.91
X33
X9
X34
X3
X9
X15
28.4889
21.5192
21.5470
21.5815
21.5190
23.1823
38.5148
31.4347
31.4753
31.7505
31.6322
33.3218
10.0259
9.9155
9.9283
10.1690
10.1132
10.1395
106
106
105
106
106
105
01/09/19 10:10
01/10/19 09:30
01/17/19 08:50
01/24/19 10:00
01/31/19 11:20
02/07/19 09:20
01/10/19 11-10
01/11/19 10:00
01/18/19 09:10
01/25/19 10:00
02/01/19 11:00
02/08/19 09:30
28.6982
21.6808
21.7108
21.7503
21.6838
23.3486
0.2093
0.1616
0.1638
0.1688
0.1648
0.1653
0.0483
0.0495
0.0514
0.0504
0.0513
550
550
550
550
550
01/11/19 13:40
01/18/19 12:30
01/25/19 12:15
02/01/19 14:00
02/08/19 15:30
4
01/11/19 17:20
01/18/19 14:45
01/25/19 13:50
02/01/19 13:10
02/08/19 16:35
21.5675
21.5965
21.6329
21.5694
23.2336
0.1133
0.1143
0.1174
0.1144
0.1150
1.63%
1.65%
1.66%
1.63%
1.64%
[E2.09%
70.11 %
69.78%
69.55%
69.42%
69.15%
yf Mass Fraction of Volatile Solids In Liquid (Feed)
yb Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at Start of Test
0.0114266
Sludge at End o1 Test
0.0113418
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
Xb Mass Fraction of Fixed Solids in Liquid (Bottom)
at Start of Test
0.0048712
Sludge at End of Test
0.0050594
TS (9)1
0.1616
TS (9)
0.1663
VS ()
1 0.1133
VS ()
0.115
Volatile Fraction In: 1 0.43012
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]
Volatile Fraction Out: 1 0.42165

AR
CHAIN OF CUSTODY
BORATORIES. INC.
E
PAR Laboratories, Inc
Phone [phone]
www.parlabs.com
Fax (704)•588.8335
Shipping:
Mailing:
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28273
Charlotte, NC 28241-1483
It is essential that all information be reco ded on this Chain
of Custody document for acceptance by PAR Laboratories. Inc. and the North
Carolina Department of Environmental and Natural Resources.
Company Name (billing)
Comments/ Special Instructions
SYNAGRO CENTRAL
Clarifier Effluent provided in the event that
Address
the sample needs to be reduced to below
12701 LANCASTER HWY
2% solids.
City, State & zip code
PINEVILLE NC 28134
Point of Contact 8 Telephone Number
ADAM BRIGMAN 704-650-4341
Sample n
Taken By: SIGNATURE � it PRINTED NAME /qJ2/,,7 hr �P"a'7
ARE SAMPLES FOR STATE or EPA REPORTING? YES NO
"Sample Type: DW VWV r/ GWMW HW Soil other
Sample Temp at time of sampling: a C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
Bent Sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
DateMme
Collection
Datemme
Analyses
Requested
&A siaf? le �0-b� er/
✓
i��/9 /0.�0
3� �� �e«c1? S��/e
q
01.9UPS Irali:,
' C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste
fw-

SECTION 6

Agricultural Lime Application Log
Year: 2018
Project: West Stanley 50-2170
Fiel
I Grower =SoilJ
Lime Requirement
Tons/Acre
Date
Total
(state-county-site-field)I
�H
from soil analysis)A
lied
A lied
Acres
NC-ST-02-01 11
Sylvester Little
6.8
0.0
0.0
0
13
NC-ST-02-02 11
Sylvester Little
—6.9-11
0.0
NC-ST-04-01 11
HenryAnderson
6.5
0.0
0.0
0
26.8
NC-ST-04-02 11
HenryAnderson
6.6___I
0.0
0.0
0
12.8
NC-ST-04-03 11
HenryAnderson
6.5
0.0 10.0
0
6.9
NC-ST-04-05 11
HenryAnderson IF
0.0
# lime has been ordered but not spread

SECTION 7

Page 1 of 1
Report No: 20-021-1022
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypoint0 er
ANALYTICAL
Client: Sylvester Little
West Stanley
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-ST-02
Date Received: 01/21/2020
Date of Report: 01/22/2020
ab No Field /D
Sample ID
Soil Class
HM% W/V
pH
Ac
P-I
K-I
S-I
Mn-I
Zn-/
Zn-Al
Cu4
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO N
)3189
02-01
MIN
1.4
6.8
0.2
5
20
96
44
43
43
105
5.4
96
71
21
2.7
0.1
)3190
02-02
MIN
1.2
6.9
0.1
2
17
104
13
20
20
60
4.5
97
71
21
3.2
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; 1\103 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No: 20-021-1021
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypoint.er
ANALYTICAL
Client: Henry Anderson
West Stanley
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-ST-04
Date Received:01/21/2020
Date of Report: 01/22/2020
Lab No Field ID
Sample ID
Soil Class
HM%
WN pH
Ac
P-1
K-I
S-1
Mn-/
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO N
03185
04-01
MIN
2.0
6.5
0.3
1
9
212
38
18
18
15
4.6
92
60
30
1.7
0.1
03186
04-02
MIN
2.0
6.6
0.3
2
10
154
50
20
20
25
4.7
94
62
30
1.8
0.1
03187
04-03
MIN
2.0
6.5
0.4
2
16
64
75
40
40
50
5.2
93
61
29
1.8
0.1
03188
04-05
MIN
2.0
6.5
0.4
2
16
60
81
43
43
50
5.5
92
61
29
1.7
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

TOWN OF COLUMBUS, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ00016247
2019 ANNUAL REPORT

TOWN OF COLUMBUS, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Page
3. Annual Land Application Field Summary Form
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analysis

SECTION 1

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
COLUMBUS, NC
COLUMBUS, NC WWTF LIME STABILIZED LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
May 2019 2357600.00 G 36.85 D 33.41
YEARLY TOTAL 235,600.00 G 36.85 D 33.41
1 /30/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FARM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
Facility Name: COLUMBUS, NC
NPDES#:
or WQ# (residual only)
WWTP Name: COLUMBUS WWTF
Residuals Analysis Data
Product Type
LSLIQ
Date Sampled (grab) or 05/21/19
Date Composited
Percent Solids
3.75
PARAMETERS (mg/kg dry weight)
Arsenic
<5
Cadmium
1.36
Mercury
0.474
Chromium
49.1
Copper
505
Lead
27.7
Molybdenum
5.38
Nickel
21.1
Selenium
<5
Zinc
880
Total Phosphorus
13500
TKN
46800
Ammonia -Nitrogen
2 630
Nitrate and Nitrite
2680
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF. PIVEPARER
Date Qk, /„io,-)c)
DENR FORM RSSF (5/2003) Printed: Thursday - February 6, 2020 at 10:58:39 for: 2143 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
Facility Name
NPDES#
or WQ# (residual only)
WWTP Name
Residual Analysis Data
Product Type
Date Sampled
Date Composited
Percent Soilds
COLUMBUS, NC
COLUMBUS WWTF
LSLIQ
05/21 /19
3.75
PARAMETERS (mg/kg dry weight)'
Aluminium
21000
Calcium
127000
Magnesium
3120
pH
12.20
Potasium
1810
Sodium
987
PAN
17246
SAR
0.1446
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, in uding the possibili of fines and imprisonment for knowing violations."
X Date �/ �pJ� 0,2n
(SIGNATUR P EPARE
NR - Data Not Reported or Data Not Required Report Run Date:- 2/6/2020 11:00:07 AM

•
Wayp®intN
ANALYTICAL
6/5/2019
Synagro SW LLC/ Columbus MS
C Simmons- 56-2994
501 Woodall Road
Decatur, AL, 35601
Ref: Analytical Testing
Report Number: 19-143-0209
Project Description: Columbus WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear C Simmons- 56-2994:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/23/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

•
Waynoint
ANALYTICAL
eport Number: 19-143-0209
Client Project Description: Columbus WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
SM-2540G
WTN
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
SW-7471B
WTN
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
SM-4500-NH3C-TKN
WTN
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
4500NO3F-2011
WTN
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
6010D
WTN
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
SM-4500-NH3C
WTN
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
9045D
WTN
66543
Columbus WWTP
Solids
05/21/2019 12:00
05/23/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Re Number: 19-143-0209
Account Number: 90024
Send To: Synagro SW LLC/ Columbus MS
C Simmons- 56-2994
501 Woodall Road
Decatur, AL 35601
Wav � �to
�
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Columbus WWTP
REPORT OF ANALYSIS Date Sampled: 5/21/2019 12:00:00
Lab Number: 66543 Date Received: 05/23/2019 00:00
Sample Id: Columbus WWTP Date Reported: 06/05/2019
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
3.75
96.20
4.68
1.35
0.18
0.72
12.70
0.31
0.10
0.26
4.42
46800
13500
1810
7180
127000
3120
987
12000
21000
250
505
880
2630
44170
2680
250
50.0
50.0
50.0
2500
50.0
250
50.0
50.0
5.00
2.50
12.5
100
250
4.83
ADM
ADM
JPJ
KKM
KKM
KKM
KKM
KKM
KKM
KKM
KKM
KKM
KKM
KKM
JPJ
ZBD
05/28/2019 16:26
05/28/2019 16:26
05/31 /2019 10:30
05/30/2019 18:17
06/04/2019 17:56
05/30/2019 18:17
05/31 /2019 13:50
05/30/2019 18:17
05/30/2019 18:17
05/30/2019 18:17
05/30/2019 18:17
05/30/2019 18:17
05/30/2019 18:17
05/30/2019 18:17
05/29/2019 14:00
05/29/2019 14:00
05/31 /2019 13:51
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
601 OD
601 OD
601 OD
6010D
601 OD
601 OD
601 OD
601 OD
6010D
601 OD
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
pofir' mC G01
Pauric McGroary
Agronomist
Page 3 of 6

Re Number: 19-143-0209
Account Number: 90024
Send To: Synagro SW LLC/ Columbus MS
C Simmons- 56-2994
501 Woodall Road
Decatur, AL 35601
Waypoi t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Columbus WWTP
REPORT OF ANALYSIS Date Sampled: 5/21/2019 12:00:00
Lab Number: 66543 Date Received: 05/23/2019 00:00
Sample Id : Columbus WWTP Date Reported: 06/0512019
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Calcium Carbonate Equivalent
Molybdenum
Comments:
1.36
1.00
KKM
05/30/201918:17
601OD
49.1
2.50
KKM
05/30/201918:17
601OD
21.1
2.50
KKM
05/30/201918:17
601OD
27.7
3.00
KKM
05/30/201918:17
601OD
<5.00
5.00
KKM
05/30/201918:17
601OD
0.474
0.0149
TJS
05/29/2019 14:02
SW-7471 B
<5.00
5.00
KKM
05/30/201918:17
6010D
12.2
JSL
05/28/2019 06:49
9045D
25.70 257000
1000
DXT
06/03/2019 09:30
AOAC 955.01
5.38
2.50
KKM
05/30/201918:17
601OD
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
pofie. m` G0O''�
Pauric McGroary
Agronomist
Page 4 of 6

0
Wa�/PA®int..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 90024
Customer Name: Synagro SW LLC/ Columbus MS
Report Number: 19-143-0209
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
I. UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F77
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
IS Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
I, Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
40 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
• Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
• N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 41 No
Comments:
Signature: lBrandi Watson Date & Time: 05/23/2019 11:27:48
Page 5 of 6

SAMPLING LOG #
@DoRichmc
7621 11�1
IIIIIIIIIIIIII�IIIIIIIII�IIII�I�IIIIII�IIIIIIIII�IIlllllllflllll
9024 0199 OF CUSTODY
Swaaro SW LLC/ Columbus MS 11:27:16 D & ANALYSES
LYSES
CUSTOMER:
�,g �p
S ll NAGR®
804/74:
ColumbusWWTP IECOR+D
PROJECT MANAGER: enL
ducsr rnarme proper veld sampling procedures
ere used during the collection of these samples.
�33
Vo
Phone:
ki'
sA
A & L
CUSTOMER
SAMPLING SAMPLE
# OF SAMPLING METHOD METHOD
LAS #
SAMPLE I.D.
LOCATION TYPE
CONTAINERS DATE TIME PRESERVED SHIPPED
�n , U, t') ,
D'W-I'r C ;" ,
t
22- (0 A v,,
Relinquished by Sampler: Dat Time Recleved by: REMARKS:
Relinquished by: PS t�3 Time Reciev by:
Relinquished by: r Date Time Recle ed by:
SPECIAL INSTRUCTIONS:
For monitoring purposes. POD.
(STATE)
SAMPLE ANALYSIS REQUEST
SLI SL2 NH4-N NO3 N Organic Cd Ct Ni Pb P.s H Se CSCO3 VolStite
N 9 pH lequiv. Solids I Mo. C( NOZ-N I
1 -M, !E
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL 2 Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
Page 6 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2143-01-LSLIQ-NC COLUMBUS, NC WWTF LIME STABILIZED 5/21/2019 111/2019-12/31/2019 0.1446
LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (987 x 3.7500) + 100 = 37.0125
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (127000 x 3.7500) _ 100 = 4762.5
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3120 x 3.7500) _ 100 = 117
Na meq = Na mg/1 _ Molec.Wgt.Na = 37.0125 _ 23 = 1.60924
Ca meq = Ca mg/I = Molec.Wgt.Ca = 4762.5 + 20 = 238.125
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 117 = 12 = 9.75
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.60924 _ SgrRoot[0.5(238.125+9.75)] = 0.14455
Printed: 2/5/2020
Page 1 18:14

SECTION 3

FACILITY NAME: COLUMBUS, NC
OWNER: DANNY & ETHAN EDWARDS
SITE #: NC PO 00007 FIELD# : PO 00007 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CEB2
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 23.27
OPERATOR: DANNY & ETHAN EDWARDS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 10.60 ACRES PERMITTED: 10.60
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
5/24/19
62,000.00 (G)
5849.057
3.75
0.915
COLLSL
DRY
0-<1/2"
SUR
0.5
0.30
46,800. p
2,630.00 p
2,680.00 p
17246
FESCUE HAY
5/28/19
37,200.00 (G)
3509.434
3.75
0.549
COLLSL
DRY
0-<1/2"
SUR
0.5
0.30
46,800. p
2,630.00 p
2,680.00 p
17246
FESCUE HAY
5/29/19
49,600.00 (G)
4679.245
3.75
0.732
COLLSL
DRY
0-<1/2"
SUR
0.5
0.30
46,800. p
2,630.00 p
2,680.00 p
17246
FESCUE HAY
May-19
1 148,800.00 (G)
14,037.736
ioun vauons/Hc:
Total Wet Tons/Ac:
14,UJ-/: /4
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual Ibs/acre
76
0.022
0.006
0.216
2.217
0.122
0.002
0.024
0.093
0.022
3.863 59.27
Cumulative lbs/acre
0.040
0.011
0.383
4.297
0.240
0.004
0.045
0.166
0.040
7.313
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
209
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0J
375.0
89.0
2500.0 ( - J
COLLSL = COLUMBUS, NC WWTF LIME STABILIZED LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Columbus, NC
Permit #: WQ0016247
erator: Danny & Ethan Edwards Owner:
Acres Used: 10.6 Acres Permitted:
Total Dry Tons Applied (Annual): 23.27
Cation Exchange Capacity (non 503 only):
Danny & Ethan Edwards Predominant Soil Series:
1 -1
CEB2
Site #: NC PO 00007 Field #: PO 00007 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
5/21/19
L2J_3
J
L4]5
6
7
8
9
'10
11
12
% Solids
3.75
Arsenic
5
Cadmium
1.36
Copper
505
Chromium
49.1
Lead
27.7
Mercury
0.474
Molyb-
denum
5.38
Nickel
21.1
Selenium
5
Zinc
880
Total
Phos-
_' orus
13500
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
• •.
Event
1
1 1
Nor, 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1T, 11
1 111
1 1
1 11.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 !1!
1 111
1 111
1 111
1 11•
•..•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
'
• •
1 •
1 111
1 111
1 111
1 111
NOT, 11
MIT, 11
1 111
1 !11
1 1!!
1 111
1 111
1 •
®''
�,
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
IMM111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
KITIM,
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1•
1 111
1 111
1 1!1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1
1 111
! 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
: •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
: •
Total
' •
• •
1111
1 111
1 111
1 111
1 1!1
1 111
1 111
1 111
1 111
1 111
1 111
• •
.•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
risohni.ent for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: COLUMBUS,NC
OWNER: DANNY & ETHAN EDWARDS
SITE #: NC PO 00007 FIELD# : PO 00007 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: PACOLET
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 13.57
OPERATOR: DANNY & ETHAN EDWARDS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.70 ACRES PERMITTED: 7.70
Page
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
5/29/19
86,800.00 (G)
11272.727
3.75
1.763
COLLSL
DRY
0-<1/2"
SUR
0.5
0.30
46,800. p
2,630.00 p
2,680.00 p
17246
FESCUE HAY
May-19
86,800.00 (G)
11,272.727
I
1
1
1 Mal Ua11QRS/EiC:
Total Wet Tons/Ac:
-„ 1 _.. 1 -
11,L/Z./3
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
61
0.018
0.005
0.173
1.780
0.098
0.002
0.019
0.074
0.018
3.102
47.59
Cumulative Ibs/acre
0.025
0.007
0.244
2.661
0.148
0.003
0.028
0.105
0.025
4.564
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
--
—
—
158
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8E_
1339.0
267.9
15.0 i 1
375.0
89.0
2500.0
COLLSL = COLUMBUS, NC WWTF LIME STABILIZED LIQUID
v
xL '-- � 2a
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
erator:
Acres Used:
Columbus, NC
WQ0016247
Danny & Ethan Edwards Owner:
7.7 Acres Permitted:
Total Dry Tons Applied (Annual): 13.57
Cation Exchange Capacity (non 503 only):
Danny & Ethan Edwards Predominant Soil Series:
7.7 Site #: NC PO 00007
Pacolet
Field #: PO 00007 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
1 1
5/21/19
2
3
4
5
6
7
8
9
10
11 j
1121
% Solids
3.75
Arsenic
5
Cadmium
1.36
Copper
505
Chromium
49.1
Lead
27.7
Mercury
0.474
Molyb-
denum
5.38
Nickel
21.1
Selenium
5
Zinc
880
Total
Phos-
~ orus
13500
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 1 :
1 111
1 111
1 111
1 111
1 111
1 111
KIT, 11
1 111
1 111
1 I l i
1 111
1 1
.••• .
1 11
1 111
1 111
1 111
1 111
1 111
1 Ili
1 111
1 111
1 111
1 111
1 111
ffITIM,
...
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
off-M,
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1`:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111MIT,11
1 1`:
1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1 `
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 `
��
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 �
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
i 111
1 111
1 111
1 1
®�
1 111
1 11 i
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
•M
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•1
• •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
rispnAnent for knowing violations".
2 0
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

SECTION 4

Aumai'Grtlr_,71 Laborasoraaig
April 12, 2019
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Columbus NC
Dear Erik Bruce:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Order No.: 19031712
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/28/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH009232011-1, Virginia VELAP 9456, Washington C891
Page 1 of 34

Summit Environmental Technologies, Inc. Case Narrative
MS-U-M-MIT 3310 Win St.
ERVI1'?C7WNFEtdTA.L .:ci 7oi_gC;i�S, INC. Cuyahoga Falls, Ohio 44223 WO#: 19031712
Ln.riSltrt! itioralori:�, TEL: [phone] FAX [phone]
Website: httn://www.settek.com Date: 4/12/2019
'LIENT: Synagro
Project: Columbus NC
WorkOrder Narrative:
19031712: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Forin, and other applicable forins as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
'-)r use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19031712-OOIA TCLP-SVOC-CPest(8081B): The LCS (Batch 36694/R96658) exhibtied high recovery
for gamma-BHC and Heptachlor. Associated samples were ND
19031712-00IA TCLP-SVOC-Herb NPW(8151): LCS exhibited high recovery for 2,4,5-TP.
Associated samples were ND
Original
Page 2 of 34

MSUMMSummit Environmental Technologies, In Qualifiers and Acronyms
IT 3310 Win S
hi4rlf� tlFalt hlT�L3 �+t�lntr� � "eras. Cuyahoga Falls, Ohio442� WO#: 19031712
AjTri�ytical Latioraforfos TEL: [phone] FAX.- (330) 253-446
Website: httnJ/www.settek.co Date: 4/12/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 34

MSUMMIffit
- -
AjTriifyU ai Laborarorlge
CLIENT: Synagro
Project: Columbus NC
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://wwiv.settek.com
Workorder
Sample Summary
WO#: 19031712
12 Apr-19
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
19031712-001 Columbus WWTP 3/27/2019 11:00:00 AM 3/28/2019 10:15:00 AM Sludge
Page 4 of 34

MS
SUMMIT
Summit Environmental Technologies, Ins 3310 Win S DATES I PORT
Er Vl,T0tJPelEtaTAL D rcai t-aGizs, ar-tc, Cuyahoga Falls, Ohio 44223 WO#: 19031712
A.nam ytical .Ltpbororr nos TEL: [phone] FAX.- [phone]
Website: htW.-Ilwww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
19031712-001A Columbus WWTP 3/27/2019 11:00:00 AM Sludge Ignitability of Solids (SW-846: 1030) 4/11/2019 3:00:00 PM
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
4/11/2019 2:44:00 PM
4/2/2019 11:11:00 AM
Reactive Sulfide (9034)/7.3.4.2 4/2/2019 11:11:00 AM
SVOC SW-846: 8151 Herbicides-TCL4/2/2019 6:00:00 PM 4/3/2019 3:30:00 PM 4/5/2019 11:38:00 PM
TCLP Mercury Analysis (SW1311/74-/4/2/2019 6:00:00 PM 4/5/2019 12:10:00. PM 4/5/2019 3:26:00 PM
TCLP Metals Analysis (SW1311/6010 4/2/2019 6:00:00 PM 4/4/2019 6:38:38 PM
TCLP Pesticides Analysis (SW1311/8(4/2/2019 6:00:00 PM 4/2/2019 6:45:00 PM 4/5/2019 7:24:00 AM
TCLP Semi-Volatiles Analysis 4/2/2019 6:00:00 PM 4/8/2019 2:00:00 PM 4/10/2019 8:30:00 PM
(SW1311/8270)
TCLP Volatiles Analysis 4/2/2019 6:00:00 PM 4/3/2019 12:46:00 PM
Original
Page 5 of 34

Sunsnsit Environmental Technologies, Inc. Analytical Report
m9summlv . 3310 Win St.
ERVIIrONfx ENTAL` E-C1tW0LGC,1Z z.IN . Cuyahoga Falls, Ohio 44223 (base report)
AnniPy0cal Laborarortas TEL: [phone] FAX.- [phone] WO#: 19031712
Website: hitp://ivivw.settek.coni Date Reported: 4/12/2019
'LIENT: Synagro
Matrix: SLUDGE
Lab ID: 19031712-001 A
Project: Columbus NC
Client Sample ID Columbus WWTP
Tag Number:
Collection Date:
3/27/2019 11:00:00 AM
Analyses Result
RL
Qua] Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND
0.00200
mg/L
1
4/5/2019 3:26:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
Analyst: KMO
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
4/4/2019 6:38:38 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
4/4/2019 6:38:38 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
4/4/2019 6:38:38 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
4/4/2019 6:38:38 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
4/4/2019 6:38:38 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
4/4/2019 6:38:38 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
4/4/2019 6:38:38 PM
CLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW3510C Analyst: BJH
CLP SEMI-VOLATILES ANALYSIS (SW131118270)
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
4/10/2019 8:30:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
4/10/2019 8:30:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
4/10/2019 8:30:00 PM
2,4-Dinitrotoluene
ND
.0.0400
mg/L
2
4/10/2019 8:30:00 PM
Cresols, Total
ND
4.00
mg/L
2
4/10/2019 8:30:00 PM
Hexachloro-1,3-butadiene
ND
0.0160
mg/L
2
4/10/2019 8:30:00 PM
Hexachlorobenzene
ND
0.0400
mg/L
2
4/10/2019 8:30:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
4/10/2019 8:30:00 PM
Nitrobenzene
ND
0.0800
mg/L
2
4/10/2019 8:30:00 PM
Pentachlorophenol
ND
0.200
mg/L
2
4/10/2019 8:30:00 PM
Pyridine
ND
0.200
mg/L
2
4/10/2019 8:30:00 PM
Surr: 2-Fluorophenol
36.2
10 - 109
m %Rec
2
4/10/2019 8:30:00 PM
Surr: Phenol-d6
41.0
10 - 109
%Rec
2
4/10/2019 8:30:00 PM
Surr: Nitrobenzene-d5
40.5
19 - 120
%Rec
2
4/10/2019 8:30:00 PM
Surr: 2,4,6-Tribromophenol
79.9
10 - 120
%Rec
2
4/10/2019 8:30:00 PM
Surr: 2-Fluorobiphenyl
43.1
22 - 117
%Rec
2
4/10/2019 8:30:00 PM
Surr: p-Terphenyl-d14
103
34 - 116
%Rec
2
4/10/2019 8:30:00 PM
Qualifiers: E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine
area response
MC Value is below Minimum
Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column
confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal
< MDL
Page 6 of 34

Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
FEhtirll?0Whl�t•1TAL'Tr-04E�0WC,4z,,1PaC. Cuyahoga Falls, Ohio44223 (base report)
m9summilt
Amrttytleaaf Lalinratorw TEL: [phone] FAX.- [phone] WO#: 19031712
Website: http://wwiv.settek.com Date Reported: 4/12/2019
'LIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 3/27/2019 11:00:00 AM
Lab ID:
19031712-001 A
Project:
Columbus NC
Client Sample ID Columbus WWTP
Analyses
Result
RI,
Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C Analyst: SFG
TCLP PESTICIDES ANALYSIS
(SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
10
4/5/2019 7:24:00 AM
Toxaphene
ND
0.0500
mg/L
10
4/5/2019 7:24:00 AM
Endrin
ND
0.00500
mg/L
10
4/5/2019 7:24:00 AM
gamma-BHC
ND
0.00500
QL+
mg/L
10
4/5/2019 7:24:00 AM
Heptachlor
ND
0.00500
QL+
mg/L
10
4/5/2019 7:24:00 AM
Heptachlor epoxide
ND
0.00500
mg/L
10
4/5/2019 7:24:00 AM
Methoxychlor
ND
0.00500
d
mg/L
10
4/5/2019 7:24:00 AM
Surr: TCMX
62.9
10 - 119
%Rec
10
4/5/2019 7:24:00 AM
Surr: DCB
80.5
10 - 119
%Rec
10
4/5/2019 7:24:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SVOC SW-846: 8151 HERBICIDES-TCLP
SW8151A SW8151A Analyst: SFG
2,4-D
ND
0.0100
d mg/L
1 4/5/2019 11:38:00 PM
2,4,5-TP
ND
0.00500
QL+ mg/L
1 4/5/2019 11:38:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50 4/3/2019 12:46:00 PM
1,2-Dichloroethane
ND
0.250
mg/L
50 4/3/2019 12:46:00 PM
MEK
ND
5.00
mg/L
50 4/3/2019 12:46:00 PM
Benzene
ND
0.250
mg/L
50 4/3/2019 12:46:00 PM
Carbon tetrachloride
ND
0.250
mg/L
50 4/3/2019 12:46:00 PM
Chlorobenzene
ND
2.50
mg/L
50 4/3/2019 12:46:00 PM
Chloroform
ND
0.250
mg/L
50 4/3/2019 12:46:00 PM
Tetrachloroethene
ND
0.250
mg/L
50 4/3/2019 12:46:00 PM
Trichloroethene
ND
0.250
mg/L
50 4/3/2019 12:46:00 PM
Vinyl chloride
ND
0.100
mg/L
50 4/3/2019 12:46:00 PM
Surr: 4-Bromofluorobenzene
93.2
70 - 130
%Rec
50 4/3/2019 12:46:00 PM
Surr: Dibrom ofluorom ethane
103
70 - 130
%Rec
50 4/3/2019 12:46:00 PM
Surr: Toluene-d8
97.9
70 - 130
%Rec
50 4/3/2019 12:46:00 PM
Qualifiers: E Value above quantitation range
H Holding times for preparation. or analysis exceeded
M Manual Integration used to determine
area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column
confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal < MDL
Page 7 of 34

Summit Environmental Technologies, Inc. 3310 Win St.
=Wq'jFMM1T
Analytical Report
a'If?C�h1P9cE3T 1.L ri�±Et�Ql,t'r ;i $, me
Cuyahoga Falls, Ohio 44223
(base report)
Anailyficai Lgboraicrio TEL: (330)
253-8211 FAX: [phone]
WO#: 19031712
Website: htty:llivww.settek.com
Date Reported: 4/12/2019
'LIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
3/27/2019 11:00:00 AM
Lab ID: 19031712-OOIA
Project: Columbus NC
Client Sample ID Columbus WWTP
Analyses Result
RL Qual Units
DF Date Analyzed
RCI-SOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.490 mg/Kg
1 4/2/2019 11:11:00 AM
RCI-SOLID-W/ IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1 4/11/2019 3:00:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH 7.7
s.u.@21.1C
1 4/11/2019 2:44:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1 4/2/2019 11 -.11:00 AM
Qualifiers: E
Value above quantitation range
M
Manual Integration used to determine area response
N
Tentatively identified compounds
O
RSD is greater than RSDlimit
PL
Permit Limit
RL
Reporting Detection Limit
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CalcVa1 < MDL
Page 8 of 34

Summit Environmental Technologies, Inc. Accreditation Program
msummlir 3310 Win St. Anal tes Report
1 '4+Id?L1hlP�1"c➢lTkL �a ttd�lCS��i '1 5, INC Cuyahoga Falls, Ohio 44223 Y P
.�F�t�tyrlcal Za t+raz rt s TEL: [phone] FAX: [phone] WO#: 19031712
Website: h9p://www.settek.cona 12 Apr-19
Client: Synagro
State: NW
Project: Columbus NC
Program Name: NC_WW
SCM
Sample ID
Matrix
Test Name
Analyte
Status
19031712-001A
Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
SVOC SW-846: 8151 Herbicides-TCLP
2,4,5-TP
A
Sludge
SVOC SW-846: 8151 Herbicides-TCLP
2,4-D
A
Sludge
TCLP Mercury Analysis (SW13I in470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis.(SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
Key
NC WW SCM A
Accredited
NC WW SCM U Unavailable
Original # 1
Page 9 of 34

Summit Environmental Technologies, Inc. Accreditation Program
SUMM.1y 3310 Win St.
Anal tes Report
�i4'e�li�L}tJA+1�7JTAL'�cn�[]L4ct��,1�tC: Cuyahoga Falls, Ohio 44223 y p
AnalyOcal L-,algaratort6s TEL: [phone] FAX.- [phone] WO#: 19031712
Website: hQ.-Ilwww.settek.com 12 Apr-19
Client: Synagro State: NW
Project: Columbus NC Program Name: NC_WW SCM
Sample ID Matrix
Test Name
Analyte
Status
19031712-001A Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original # 1
Page 10 of 34

Summit Environmental Technologies, Inc. QC SUMMARY l PORT
3310 Win St.
C°4�I�«}r1b1Et•7T�.Lre��+ot [���g �t� Cuyahoga Falls, Ohio 44223 WO#: 19031712
:rr f,tlG�'t LcY.t7CrY�dr�t1! 5' TEL: [phone] FAX: [phone]
Website: http://www.settelc.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: 36680
Sample ID MB-36680
SampType: MBLK
TestCode:
tclp-voc-mstr Units: mg/L
Prep Date: 4/2/2019
RunNo: 96569
'lient ID: PBS
Batch ID: 36680
TestNo:
SW8260 SW1311M
Analysis Date: 4/3/2019
SegNo: 2036152
\nalyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
1.00
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
455
Surr: Dibromofluorom ethane
528
Surr: Toluene-d8
482
500.0 91.0 70 130
500.0 106 70 130
500.0 96.5 70 130
Sample ID LCS-96569
SampType: LCS
TestCode:
tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 96569
Client ID: LCSS
Batch ID: 36680
TestNo:
SW8260 SW1311M
Analysis Date: 4/3/2019
SegNo: 2036165
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.0185
0.00500
0.0200
0
92.5
70
131
1,2-Dichloroethane
0.0205
0.00500
0.0200
0
103
70
137
MEK
0.101
0.100
0.100
0
101
55.1
163
Benzene
0.0194
0.00500
0.0200
0
97.2
70
132
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 11 of 34

Summit Environmental Technologies, Inc.
3310 Win St. QC SUMMARY liuPORT
11MUNkMIT
ENWI, C1tJlA9 NTr4L 1I4C, Cuyahoga Falls, Ohio 44223 WO#: 19031712
Q..I�ittl[l4'c�/ L�r. ar�Jcst'ao� TEL: [phone] FAX- [phone]
Website: hQ:Ilwww.settelc.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: 36680
Sample ID LCS-96569
SampType: LCS
TestCode:
tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 96569
Client ID: LCSS
Batch ID: 36680
TestNo:
SW8260 SW1311M
Analysis Date: 4/3/2019
SegNo: 2036165
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Carbon tetrachloride
0.0195
0.00500
0.0200
0
97.3
63.7
139
Chlorobenzene
ND
0.0500
0.0200
0
98.8
70
139
Chloroform
0.0184
0.00500
0.0200
0
91.8
70
130
Tetrachloroethene
0.0181
0.00500
0.0200
0
90.6
56.2
187
Trichloroethene
0.0171
0.00500
0.0200
0
85.6
64.1
138
Vinyl chloride
0.0165
0.00200
0.0200
0
82.4
22.1
147
Surr:4-Bromofluorobenzene
49.0
50.00
98.0
70
130
Surr: Dibromofluoromethane
53.5
50.00
107
70
130
Surr: Toluene-d8
50.6
50.00
101
70
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 12 of 34

[ Summit Environmental Technologies, Inc. QC SUMMARY l PORT
10 UMMIT3310 Win St.
ENWITION1Ar:NTAL'I-EC9MO[,oGirc$, IgC Cuyahoga Falls, Ohio 44223 WO#: 19031712
Anan'y,trozI i.abari7tr. r;o!g TEL: [phone] FAX.- [phone]
Website: htti2:llwww.settelc.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID• 36680
Sample ID LCS-96567
SampType: LCS
TestCode: TCLP-voc-ms Units: mg/L
Prep Date:
RunNo: 96567
Client ID: LCSS
Batch ID: 36680
TestNo: SW8260 SW1311M
Analysis Date: 4/3/2019
SegNo: 2036129
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.0185
0.00500
0.0200
0
92.4
70
131
1,2-Dichloroethane
0.0179
0.00500
0.0200
0
89.5
70
137
MEK
0.102
0.100
0.100
0
102
55.1
163
Benzene
0.0203
0.00500
0.0200
0
101
70
132
Carbon tetrachloride
0.0170
0.00500
0.0200
0
84.9
63.7
139
Chlorobenzene
ND
0.0500
0.0200
0
108
70
139
Chloroform
0.0180
0.00500
0.0200
0
90.0
70
130
Tetrachloroethene
0.0184
0.00500
0.0200
0
92.1
56.2
187
Trichloroethene
0.0192
0.00500
0.0200
0
96.0
64.1
138
Vinyl chloride
0.0165
0.00200
0.0200
0
82.4
22.1
147
Surr:4-Bromofluorobenzene
50.0
50.00
100
70
130
Sum Di brom of] uorom ethane
47.6
50.00
95.1
70
130
Sum Toluene-d8
49.4
50.00
98.7
70
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 13 of 34

I � SumnsitEnvii•onmental Technologies, Inc.me k 3310 Win St. Nt �C QC SUMMARY I PORT
EtW111014MEh]TAL' _rC NOLOGJZ.S, 31KC' Cuyahoga Falls, Ohio 44223
�Anzf. y /caf Labarodoaos TEL: [phone] FAX: [phone] WO#: 19031712
Website: hQ.'11www.settek.com 12-Apr-19
Client: Synagro
Project: Columbus NC BatchIll: 36694
Sample ID MB-36694
SampType: MBLK
TestCode: TCLPSVOC- Units: mg/L
Prep Date: 4/2/2019
RunNo: 96658
;lient ID: PBS
Batch ID: 36694
TestNo: SW8081 SW3510C
Analysis Date: 4/4/2019
SegNo: 2038925
knalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.0250
Toxaphene
ND
0.0500
Endrin
ND
0.00250
gamma-BHC
ND
0.00250
Heptachlor
ND
0.00250 d
Heptachlor epoxide
ND
0.00250 d
Methoxychlor
ND
0.00250 d
Surr: TCMX
14.1
20.00 70.7 10 119
Surr: DCB
19.6
20.00 97.8 10 119
Sample ID LCS-36694
SampType: LCS
TestCode:
TCLPSVOC- Units: mg/L
Prep Date: 4/2/2019
RunNo: 96658
Client ID: LCSS
Batch ID: 36694
TestNo:
SW8081 SW3510C
Analysis Date: 4/4/2019
SegNo: 2038926
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.0152
0.00250
0.0100
0
152
20
157
gamma-BHC
0.0139
0.00250
0.0100
0
139
22
137
Heptachlor
0.0126
0.00250
0.0100
0
126
24
121
Heptachlor epoxide
0.0136
0.00250
0.0100
0
136
27
152
Methoxychlor
0.0158
0.00250
0.0100
0
158
10
199
Surr: TCMX
15.6
20.00
77.9
10
119
Surr: DCB
21.5
20.00
107
10
119
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
S
S
Original
Page 14 of 34

Summit Environmental Technologies, Inc. QC SUMMARY I PORT
w 3310 Win St. �c
R^4�1i C]RJta1EAlT#�L "76tdO[ t'r�,^:�gG J��, Cuyahoga Falls, Ohio 44223
Anzf,P,ietlrra1 TEL: [phone] FAX.- [phone]
WO#: 19031712
Website: hW.-Ilivivw.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: 36720
2,4-D ND 0.0100 0 0 d
2,4,5-TP ND 0.00500 0 0
Surr: DCAA 486 500.0 97.3 20 140 m
2,4-D
0.560 0.0100
0.500
0 112
43.8
130
m
2,4,5-TP
0.579 0.00500
0.500
0 116
51.5
111
S
Surr: DCAA
529
500.0
106
34.2
150
m
2,4-D
0.497 0.0100
0.500
0 99.3
37
130 m
2,4,5-TP
0.541 0.00500
0.500
0 108
38
130
Surr: DCAA
492
500.0
98.3
20
140
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
0 RSD is greater than RSDlimit P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 15 of 34

Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY Ix-L:.P®RT
€iWIrLCti 4rir: TrAL "d`L-mmow'ic Cuyahoga Falls, Ohio 44223 WO#: 19031712
�+t?"ee,/J.�t oaf C sat tt t'lc��; TEL: [phone] FAX.- [phone]
Website: hhQ:Ilwww.settelc.com 12 Apt'-19
Client: Synagro
Project: Columbus NC BatchlD: 36720
Sample ID
19031528-001AMSD SampType: MSD
TestCode:
TCLP-SVOC- Units: mg/L
Prep Date: 4/3/2019
RunNo: 96718
client ID:
BatchQC Batch ID: 36720
TestNo:
SW8151A SW8151A
Analysis Date: 4/5/2019
SegNo: 2040615
4nalyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.534 0.0100
0.500
0 107
37
130 0.497
7.33 30 m
2,4,5-TP
0.568 0.00500
0.500
0 114
38
130 0.541
4.93 30 m
Surr: DCAA
513
500.0
103
20
140
0 m
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 16 of 34

IU-MIMM"IT
Summit Environmental Technologies, Inc. QC SUMMARY 1W�'ORT
n -OWN 3310 Win St.
ENWl'1L4NMt!MTAL Lmd , JAr Cuyahoga Falls, Ohio 44223
.4nalyrtica/ Labataw"''es: TEL: [phone] FAX.- [phone] WO#: 19031712
Website: htti2:llwww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchED: 36739
Sample ID MB-36739
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/5/2019
RunNo: 96686
Client ID: PBS
Batch ID: 36739
TestNo: SW7470A SW7470A
Analysis Date: 4/5/2019
SegNo: 2039667
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
rCLP Mercury ND 0.00200
Sample ID LCS-36739
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/5/2019
RunNo: 96686
Client ID: LCSS
Batch ID: 36739
TestNo: SW7470A SW7470A
Analysis Date: 4/5/2019
SegNo: 2039668
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
rCLP Mercury 0.00414 0.00200 0.00400 0 104 80 120
Sample ID MB2-36739
SampType: MBLK
TestCode: HG_TCLP(74, Units: PPM
Prep Date: 4/5/2019
RunNo: 96686
Client ID: PBS
Batch ID: 36739
TestNo: SW7470A SW7470A
Analysis Date: 4/5/2019
SegNo: 2039669
Analyte
Result
PQL SPK value. SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
rCLP Mercury ND 0.00200
Sample ID 19031871-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/5/2019
RunNo: 96686
Client ID: BatchQC
Batch ID: 36739
TestNo: SW7470A SW7470A
Analysis Date: 4/5/2019
SegNo: 2039682
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.0104 0.00500 0.0100 0 104 75 125
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 17 of 34

I Summit Environmental Technologies, Inc. QC SUMMARY
A RY J PORT
U M_ M_ I it 3310 Win St. ��..[[ �7 V lrllar�i` i TORT
1
�ll�ll�'hIMiT]T�L 8 r�F€C[SGJt A& Cuyahoga Falls, Ohio 44223 WO#: 19031712
Aaaire"Llcaftallaralort es TEL: [phone] FAX.- (330).253-4489
Website: htW:Ilwww.settelc.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: 36739
Sample ID 19031871-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/5/2019
RunNo: 96686
Client ID: Batch=
Batch ID: 36739
TestNo: SW7470A SW7470A
Analysis Date: 4/5/2019
SegNo: 2039682
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sample ID 19031871-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/5/2019
RunNo: 96686
Client ID: BatchQC
Batch ID: 36739
TestNo: SW7470A SW7470A
Analysis Date: 4/5/2019
SegNo: 2039683
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Mercury
0.0102 0.00500
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
0.0100 0 103 75
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
125 0.0104 0.971 20
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 18 of 34

i Summit Environmental Technologies, Inc. 3310 Win St. SUMMARY �l 1 QC 1, , T POR
��^4rlii[�tdMe9C 1T�L'u rti�8 5LC',�I� , INC.; Cuyahoga Falls, Ohio 44223
Antriytlt<nt t.abaradarlrs TEL: [phone] FAX.• [phone]
WO#: 19031712
Website: http:lAvww.settelc.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: 36771
Sample ID MB-36771
SampType: MBLK
TestCode:
TCLP-SVOC_ Units: mg/L
Prep Date: 4/8/2019
RunNo:
96825
Client ID: PBS
Batch ID: 36771
TestNo:
SW8270 SW3510C
Analysis Date: 4/9/2019
SegNo:
2045610
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD
RPDLimit Qua]
1,4-Dichlorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Trichlorophenol
ND
0.100
2,4-Dinitrotoluene
ND
0.0200
o-Cresol
ND
0.100
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
Pentachlorophenol
ND
0.100
Pyridine
ND
0.100
Surr: 2-Fluorophenol
0.650
Surr: Phenol-d6
0.695
Surr: Nitrobenzene-d5
0.711
Surr: 2,4,6-Tribromophenol
0.879
Surr: 2-Fluorobiphenyl
0.674
Surr: p-Terphenyl-d14
0.959
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
1.000
65.0
10
109
1.000
69.5
10
109
1.000
71.1
19
120
1.000
87.9
10
120
1.000
67.4
22
117
1.000
95.9
34
116 .
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 19 of 34

I Summit Environmental Technologies, Inc. QC SUMMARY l�P®RT
NO UU, 3310 Win St.
EKWIRO. MENTAL T-ECTM ]L0s,3ls5, lNC Cuyahoga Falls, Ohio 44223 WO#: 19031712
iA, tr.�'r/oa, .tal�rase�tae�� TEL: [phone] FAX.- [phone]
Website: http:1Avww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC
PatchID: 36771
Sample ID LCS-36771
SampType: LCS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 4/8/2019
RunNo: 96825
Client ID: LCSS
Batch ID: 36771
TestNo: SW8270 SW3510C
Analysis Date: 4/9/2019
SegNo: 2045611
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
0.476
0.0400
0.8000
0
59.5
19.1
126
2,4,5-Trichlorophenol
0.783
0.100
0.8000
0
97.9
11.7
151
2,4,6-Trichlorophenol
0.777
0.100
0.8000
0
97.1
12.4
150
2,4-Dinitrotoluene
0.748
0.0200
0.8000
0
93.5
20.6
140
o-Cresol
0.709
0.100
0.8000
0
88.6
13.8
137
Cresols, Total
ND
2.00
1.600
0
87.5
10
129
Hexachloro-1,3-butadiene
0.376
0.00800
0.8000
0
47.0
14.7
137
Hexachlorobenzene
0.677
0.0200
0.8000
0
84.6
12
139
Hexachloroethane
0.358
0.0400
0.8000
0
44.8
14.8
132
Nitrobenzene
0.950
0.0400
0.8000
0
119
15.6
138
Pentachlorophenol
0.593
0.100
0.8000
0
74.2
10
156
Pyridine
0.398
0.100
0.8000
0
49.7
1
130
Surr: 2-Fluorophenol
0.741
1.000
74.1
10
147
Surr: Phenol-d6
0.844
1.000
84.4
10
140
Surr: Nitrobenzene-d5
0.794
1.000
79.4
10
169
Surr: 2,4,6-Tribromophenol
0.996
1.000
99.6
10
185
Surr: 2-Fluorobiphenyl
0.761
1.000
76.1
10
169
Surr: p-Terphenyl-d14
1.09
1.000
109
10
179
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 20 of 34

Summit Environmental Technologies, Inc. QC SUMMARY A 7�ZT 1`x POR '
3310 Win St. ll.. �7 V 1V11V11 fit 1
e Ff4�IiiU?JFe1E raTm.L`e-'ectb�•tor c�,i�, JPtC Cuyahoga Falls, Ohio 44223
WO#: 19031712
Arv.iyt/ca1 Laborv1r.)4G8 TEL: [phone] FAX.- [phone]
Website: http:1Avww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchlD: 36771
Sample ID 19040244-002AMS
SampType: MS
TestCode:
TCLP-SVOC_ Units: mg/L
Prep Date: 4/8/2019
RunNo: 96825
Client ID: BatchQC
Batch ID: 36771
TestNo:
SW8270 SW3510C
Analysis Date: 4/9/2019
SegNo: 2045615
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
0.445
0.0800
0.8000 0
55.6
15.2
124
2,4,5-Trichlorophenol
0.705
0.200
0.8000 0
88.2
30.6
152
2,4,6-Trichlorophenol
0.709
0.200
0.8000 0
88.6
27.6
150
2,4-Dinitrotoluene
0.641
0.0400
0.8000 0
80.2
58
141
o-Cresol
0.699
0.200
0.8000 0
87.4
26.9
132
Cresols, Total
ND
4.00
1.600 0
82.7
27.6
132
Hexachloro-1,3-butadiene
0.328
0.0160
0.8000 0
41.1
-5.3
156
Hexachlorobenzene
0.586
0.0400
0.8000 0
73.2
54.3
142
Hexachloroethane
0.339
0.0800
0.8000 0
42.4
1.92
131
Nitrobenzene
0.965
0.0800
0.8000 0
121
21
135
Pentachlorophenol
0.480
0.200
0.8000 0
60.0
47.4
134
Pyridine
0.249
0.200
0.8000 0
31.2
-10.3
64.2 QMR
Surr:2-Fluorophenol
0.682
1.000
68.2
9.77
146
Surr: Phenol-d6
0.781
1.000
78.1
20.7
130
Surr: Nitrobenzene-d5
0.728
1.000
72.8
13.9
156
Surr 2,4,6-Tribromophenol
0.810
1.000
81.0
27.3
183
Surr:2-Fluorobiphenyl
0.723
1.000
72.3
21.4
153
Surr: p-Terphenyl-d14
0.912
1.000
91.2
54.8
154
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area
response
MC Value is below Minimum Compound
ND Not Detected
0 RSD is greater than RSDlimit
P Second column confirmation exceeds Original
PL Permit Limit
R RPD outside accepted recovery
limits
RL Reporting Detection Limit
Page 21 of 34

I SummitEnvironmental Technologies, Inc. QC SUMMARY 1�PORT
N&'0%ffl'2Nk,MJT3310 Win St.
EftVIIILC5WOEE ITAL t-rChH0LGG1!:q, 1ptc Cuyahoga Falls, Ohio 44223 WO#: 19031712
- Anz-?yrloaf L:Tbcrr 1or;ot; TEL: [phone] FAX: [phone]
Website: htto:11www.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: 36771
Sample ID 19040244-002AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 4/8/2019
RunNo: 96825
Client ID: BatchQC
Batch ID: 36771
TestNo: SW8270 SW3510C
Analysis Date: 4/10/2019
SegNo: 2045616
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene
0.442
0.0800
0.8000
0
55.2
15.2
124
0.4448
0.722
30
2,4,5-Trichlorophenol
0.696
0.200
0.8000
0
87.0
30.6
152
0.7052
1.37
30
2,4,6-Trichlorophenol
0.704
0.200
0.8000
0
88.0
27.6
150
0.7092
0.793
30
2,4-Dinitrotoluene
0.646
0.0400
0.8000
0
80.8
58
141
0.6412
0.808
30
o-Cresol
0.698
0.200
0.8000
0
87.2
26.9
132
0.6988
0.115
30
Cresols, Total
ND
4.00
1.600
0
82.6
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.379
0.0160
0.8000
0
47.4
-5.3
156
0.3284
14.3
30
Hexachlorobenzene
0.548
0.0400
0.8000
0
68.5
54.3
142
0.5860
6.77
30
Hexachloroethane
0.357
0.0800
0.8000
0
44.6
1.92
131
0.3388
5.18
30
Nitrobenzene
0.929
0.0800
0.8000
0
116
21
135
0.9652
3.84
30
Pentachlorophenol
0.459
0.200
0.8000
0
57.4
47.4
134
0.4800
4.43
30
Pyridine
0.403
0.200
0.8000
0
50.4
-10.3
64.2
0.2492
47.1
30
Surr:2-Fluorophenol
0.665
1.000
66.5
9.77
146
0
Surr: Phenol-d6
0.790
1.000
79.0
20.7
130
0
Sum Nitrobenzene-d5
0.736
1.000
73.6
13.9
156
0
Surr:2,4,6-Tribromophenol
0.810
1.000
81.0
27.3
183
0
Surr:2-Fluorobiphenyl
0.699
1.000
69.9
21.4
153
0
Surr: p-Terphenyl-d14
0.885
1.000
88.5
54.8
154
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analA
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
R
Original
Page 22 of 34

Summit Environmental Technologies, Inc. ^C SUMMARY
UMM ,� R T K.PORT
!!�* 3310 Win St. ll �.7 �J 1-lil Y i it 1
�I trli�4tdP,9 t,1T�L .uae Q4� ��.��5, INC, Cuyahoga Falls, Ohio 44223 WO#: 19031712
A nzaty0cal Lalevaralorjo!g TEL: [phone] FAX.- [phone]
Website: hgp:/hvww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: R96476
Sample ID 19031815-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 96476
Client ID: Batch=
Batch ID: R96476
TestNo: SW9034
Analysis Date: 4/2/2019
SegNo: 2031885
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4530 25.0 4800 0 94.4 80 120
Sample ID 19031815-001AMSD
SampType: MSD
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 96476
Client ID: BatchQC
Batch ID: R96476
TestNo:
SW9034
Analysis Date: 4/2/2019
SegNo: 2031886
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive
4430 25.0 4800 0 92.3 80 120 4530 2.23 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
0 RSD is greater than RSDlimit P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 23 of 34

Summit Environmental Technologies, Inc. QC SUMMARY
RY hiL.TORT
l M- 11 3310 Win St. 1. �7 V lrll�ll�it 1 i i�
EK', e I rL 0 tJ P.1 r:.M TA L 'I—t: C16P4b LaC,I S, is C, Cuyahoga Falls, Ohio 44223
WO#: 19031712
Ar,j?,Xtical tab�r�darP,:-)s TEL: [phone] FAX.- [phone]
Website: ham://Www.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: R96476
Sample ID MB-R96476
SampType: MBLK
TestCode:
Sulfide,React Units: mg/L
Prep Date.-
RunNo: 96476
Client ID.- PBW
Batch ID: R96476
TestNo:
SW9034
Analysis Date: 4/2/2019
SegNo: 2031869
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
ND 25.0
Sample ID LCS-R96476
SampType: LCS
TestCode:
Sulfide,React Units: mg/L
Prep Date:
RunNo: 96476
,lient ID: LCSW
Batch ID: R96476
TestNo:
SW9034
Analysis Date: 4/2/2019
SegNo: 2031870
analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4730 25.0 4800 0 98.5 85 115
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 24 of 34

1 ­1 a 0 im am AL . Summit Environmental Technologies, Inc. QC SUMMARY 1xL1 0RT
Ing 3310 Win St.
hatirliiC}.hJNa9E7T,uLC}N@dt7t [SG�rr �(r`� Cuyahoga Falls, Ohio 44223
- �k1�Py^#Ir1 t.acrr�scsre TEL: [phone] FAX.• [phone] WO#: 19031712
Website: httl2:llwww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID• R96493
Sample ID 19031815-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 96493
Client ID: BatchQC
Batch ID: R96493
TestNo: SW9014
Analysis Date: 4/2/2019
SegNo: 2032363
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.50 0.500 10.00 0 95.0 81.6 122
Sample ID
19031815-001AMSD SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 96493
Client ID:
BatchQC Batch ID: R96493
TestNo: SW9014
Analysis Date: 4/2/2019
SegNo: 2032364
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
:yanide, Reactive 9.18 0.490 10.00 0 91.8 81.6 122 9.504 3.47 5
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 25 of 34

Summit Environmental Technologies, Inc. i QC SUMMARY 7LDO�RT
3310 Win St. 1 i 1
ENV[iOANI; .mTAL'�ti�����il �s�l��, ts� Cuyahoga Falls, Ohio 44223
- WO#: 19031712
Ano./y(J'Ord LaboreforJos TEL: [phone] FAX.- [phone]
Website: hQ.-11www.settek.com 12-Apr 19
Client: Synagro
Project: Columbus NC BatchID: R96493
Sample ID Blank
SampType: MBLK
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 96493
Client ID: PBW
Batch ID: R96493
TestNo:
SW9014
Analysis Date: 4/2/2019
SegNo: 2032344
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
ND 0.495
Sample ID LCS
SampType: LCS
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 96493
Client ID: LCSW
Batch ID: R96493
TestNo:
SW9014
Analysis Date: 4/2/2019
SegNo:.2032346
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.39 0.495 10.00 0 93.9 85 115
Sample ID RLCheck
SampType: RLC
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 96493
Client ID: BatchQC
Batch ID: R96493
TestNo:
SW9014
Analysis Date: 4/2/2019
SegNo: 2032347
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
ND 0.485 0.5000 0 94.2 50 150
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 26 of 34

Summit Environmental Technologies, Inc. QC SUMMARY 1xx�,PORT
is"Aam-lit
3310 Win St.
k`'��lithlP�ih]T�L �ttmaC[�a{,.it Cuyahoga Falls, Ohio 44223
$ ffj�kr��lgPtl��l' isharaloa1'os TEL: [phone] FAX- [phone]
WO#: 19031712
Wehsite: hgp:Ilwww.settelc.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: R96918
Sample ID 19031687-012ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: [e-mail]
Prep Date:
RunNo: 96918
Client ID: Batch=
Batch ID: R96918
TestNo: SW9045D
Analysis Date: 4/11/2019
SegNo: 2048621
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH
8.5
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
0 0 0 0 8.4 0.5 10
E Value above quantitation range
M Manual Integration used to determine area response
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 27 of 34

{ I OW-0
_ Summit Environmental Technologies, Inc. QC SUMMARY l�PORT
3310 Win St.
ENNVIriONP4r: MTj.LTE-MiN C � S, a Cuyahoga Falls, Ohio 44223 WO#: 19031712
Ana.tydca' LabaradDAm TEL: [phone] FAX.- [phone]
Website: hC://www.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: R96918
Sample ID 19040743-001ADUP
SampType: DUP
TestCode: pH_0il(9045 Units: s.u.@22.8C
Prep Date:
RunNo: 96918
Client ID: Batch=
Batch ID: R96918
TestNo: SW9045D
Analysis Date: 411112019
SegNo: 2048681
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 6.8 0 0
6.8 0.6 10
'Sample ID CHECK 7
SampType: LCS
TestCode:
PH_0IL(9045 Units: s.u.@21.6C
Prep Date:
RunNo: 96918
Client ID: LCSW
Batch ID: R96918
TestNo:
SW9045D
Analysis Date: 4/11/2019
SegNo: 2048775
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.6 90 110
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 28 of 34

( i Summit Environmental Technologies, Inc. QC SUMMARY 1`.,PORT
3310 Win St. �C
rENVInONtd211TAL1fc. ��t][ct l ..ING Cuyahoga Falls, Ohio44223
WO#: 19031712
Ar+a:W/ea9 Lahara;tra,ri, ' TEL: [phone] FAX.- [phone]
Website: hQ:Ilwww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: R96918
Sample ID LCS-R96918
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@21.4C
Prep Date:
RunNo: 96918
Client ID: LCSW
Batch ID: R96918
TestNo: SW9045D
Analysis Date: 4/11/2019
SegNo: 2048600
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.0 7.0 0 99.3 98.6 101.4
Sample ID CHECK 7
SampType: LCS
TestCode: PH_NPW(450 Units: s.u.@21.5C
Prep Date:
RunNo: 96918
Client ID: LCSW
Batch ID: R96918
TestNo: SW9045D
Analysis Date: 4/11/2019
SegNo: 2048634
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit_ Qua[
pH 7.0 7.0 0 99.6 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 29 of 34

I Summit Environmental Technologies, Inc. QC SUMMARY hx2ORT
3310 Win St.
ENti+In0AJPM5WALTECIINOt,[ CjCCfi, g,4 Cuyahoga Falls, Ohio 44223 WO#: 19031712
,4jrttlyfl aY Laborats�t"We'� TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID• R96943
Sample ID LCS-R96943
SampType: LCS
TestCode: Ignitability_S ,Units:
Prep Date:
RunNo: 96943
Client ID: LCSS
Batch ID: R96943
TestNo: SW1030
Analysis Date: 4/11/2019
SegNo: 2049251
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability 8.22 7.240 0 114 70 130
Sample ID 19031712-001ADUP
SampType: DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 96943
Client ID: Columbus WWTP
Batch ID: R96943
TestNo:
SW1030
Analysis Date: 4/11/2019
SegNo: 2049253
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability non-flammable 0 0 20
Sample ID 19031815-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 96943
Client ID: BatchQC
Batch ID: R96943
TestNo: SW1030
Analysis Date: 4/11/2019
SegNo: 2049265
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
non-flammable
0 0 20
Sample ID 19040180-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 96943
Client ID: BatchQC
Batch ID: R96943
TestNo: SW1030
Analysis Date: 4/11/2019
SegNo: 2049257
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 30 of 34

I Summit Environmental Technologies, Inc. QC SUMMARY IxL.PORT
3310 Win St.
6Wlldt}�Jli1J hJTL (rr,Ct�t4@�,J,; Cuyahoga Falls, Ohio 44223
AnotyUcal LabaralIDrdas TEL: [phone] P4X.• [phone] WO#: 19031712
Website: hQ:Ilwww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchID: R96943
Sample ID 19040180-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 96943
Client ID: BatchQC
Batch ID: R96943
TestNo: SW1030
Analysis Date: 4/11/2019
SegNo: 2049267
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sample ID 19040180-003ADUP
SampType: DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 96943
client ID: BatchQC
Batch ID: R96943
TestNo:
SW1030 .
Analysis Date: 4/11/2019
SegNo: 2049259
4nalyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit . HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19040721-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 96943
Client ID: Batch=
Batch ID: R96943
TestNo: SW1030
Analysis Date: 4/11/2019
SegNo: 2049261
Ahalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability non-flammable 0 0 20
Sample ID 19040721-003ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 96943
Client ID: Batch=
Batch ID: R96943
TestNo: SW1030
Analysis Date: 4/11/2019
SegNo: 2049263
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 31 of 34

1 Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY l.LPORT
E14V1n0iJh1tm-rAL'MC* 1QLpd,IZ. ,'I G CuyahogaFalls,'Ohio44223
r P; tical l Catrra c� c�a TEL: [phone] FAX.- [phone] WO#: 19031712
Website: hM.-Ilwww.settek.com 12 Apr-19
Client: Synagro
Project: Columbus NC BatchED: R96943
Sample ID 19040722-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 96943
Client ID: Batch=
Batch ID: R96943
TestNo: SW1030
Analysis Date: 4/11/2019
SegNo: 2049265
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
gnitability
; not propagate
0 0 20
Sample ID 19040722-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 96943
Client ID: BatdhQC
Batch ID: R96943
TestNo: SW1030
Analysis Date: 4/11/2019
SegNo: 204§266
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
; not propagate
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
0 0 20
H Holding times for preparation or anal,
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 32 of 34

SummiltEnvironmental Technologies, Inc.
33,10 Win stl;pet analysis Roqu-esWhalin of Custody
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qVVI
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Page 33 of 34

Summit Environmental Technologies, Inc.
ffj SUMMIT 3310 Win St.
.Pltulhal�t��ALt�3�calns'r,,IP€^ Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Ar(ally0cat Laboralomes TEL: [phone] FAX: [phone]
Website: hQ.*11vww.settek.com
Client Name: SYN-NC-27028 Work Order Number: 19031712 RcptNo: 1
Logged by: Kayla L. Oulton 3/28/2019 10:15:00 AM
Completed By: Jacqueline Rasile 3/28/2019 5:28:48 PM
Reviewed By: Jennifer Woolf - 2 3/29/2019 10:05:27 AM
Chain of Custody
1. Is Chain of Custody complete?
2. How was the sample delivered?
Log In
3, Coolers are present?
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6, Were all samples received at a temperature of >0° C to 6.0°C
7. Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
9. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
d❑
No ❑
Not Present ❑
UPS
Yes
v/❑
No
❑
NA ❑
Yes
0
No
❑
Yes
❑
No
❑
Not Present �/❑
Signed By:
Yes
W
No
❑
NA ❑
Yes
d❑
No
❑
NA ❑
Yes
0
No
❑
Yes
No
❑
Yes
W
No
❑
Yes
❑
No
V
NA ❑
Yes
❑
No
❑
No VOA Vials❑
Yes
❑
No
d❑
Yes
No
❑
Yes
91
No
❑
Yes
0
No
❑
Yes
0
No
❑
Yes ❑ No ❑ NA V
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed B
1
5.0
Good
Not Present
Page 34 of 34

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
Columbus NC
WWTP Name: Columbus WWTP
WQ Permit Number: WQ 0016247
NPDES Number: NC 0021369
Monitoring Period: From 01/01/19 To 12/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) .Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Beta Ray
Class B:
Alt. (1) Fecal Density
Heat Drying
Gamma Ray
Heat Treatment
Pasteurization
Thermophilic
Alt. (2) Process to Significantly Reduce Pathogens x
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying
Anaerobic Digestion
Composting Aerobic Digestion
If applicable to alternative performed Class A or Class 13com lete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6tn
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Alt. 6
(Alk Stabilization) x
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the thogen and vector attraction rejWction requirements have
been met. I am aware that there are signif cant penalties for false certification inc ng fine an prisonment." ST
Todd Larson, Regional Director l
Preparer Nam it y e r' Land Applllrtame and Tit e (if applicable) (type or print)
I' �k
Signature of Pre er* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Alex Fox
From: [e-mail]
Sent: Thursday, December 5, 2019 1:28 PM
To: Alex Fox
Subject: Lime Sheet
Town of Columbus NC
5-21-19
2:00 pm PH 12.42 21 deg. C
5-21-19
4:00 pm PH 12.37 22 deg. C
5-22-19
2:00 pm PH 12.32 23 deg. C
•
11
i

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project: Columbus
Field
SCM-11
Lime Requirement
Tons/Acr7Eq)
Date Applied
(state -county -site -field)
pH
(from soil analysis)
Applied(CCE

SECTION 7

NCDA&CS Al
;mic Division Phone: [phone]
Website: wwi
igr.gov/agronomi/
Report No. 120-SL004619
0�'
Predictive
Client:
Ethan / Danny Edwards
160 Floyd Blackwell Rd
Advisor: Alex Fox
Synagro
ut11)-.I1
Tryon, NC 28782
284 Boger Rd
SoRe p Mehlich-3
Extraction
Mocksville, NC 27028
Sampled County: Polk
Links to Helpful Information
Client ID: 474750
Advisor ID: 501947
Sampled: 09/06/2019 Received: 09/12/2019 Completed: 09/21/2019
Farm: NC-PO-07
Sample ID: 01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 100
110
0 0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC , BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 1.08
7.4 95 0.4 6.7 17 17
72 22
27 176
112
95
95
ill 0.1 1
Sample ID: 02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0
120-200 20
120
0 20
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 1.26
6.9 94 0.4 6.8 55 12
70 23
23 373
229
138
138
68 0.1 1
North Carolina
7 7k�
3*I+�ct'n truss 1=iairii`r:��iia�a5si«ts
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Trox/er. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report -No. FY20-SL004619
Ethan / Danny Edwards
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You. can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-AI2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients- In general, homeowners do not
M-O
N
mineral -organic soil class
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ricagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
'
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report,'visit www.ncagr.gov/a-gronomi/obpart4.htirn ;fs#ind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-1, S-1, SS-1, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncaar.gov/agronomi/uvrst.htm

TOWN OF GRANITE FALLS, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0016247
2019 ANNUAL REPORT

Town of Granite Falls, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Page
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
GRANITE FALLS, NC
GRANITE FALLS, NC WWTP LIME STABILIZED LIQUID
DRY METRIC
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
October 2019
68,200.00 G
7.91
D
7.17
YEARLY TOTAL
68,200.00 G
7.91
D
7.17
GRANITE FALLS, NC WTP LIQUID
DRY METRIC
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
October 2019
204,600.00 G
25.67
D
23.29
YEARLY TOTAL
204,600.00 G
25.67
D
23.29
1 /22/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
Facility Name: GRANITE FALLS, NC
NPDES#:
or WQ# (residual only)
WWTP Name: GRANITE FALLS WTP
Residuals Analysis Data
Product Type
WPL
Date Sampled (grab) or
09/23/19
Date Composited
Percent Solids
3.01
PARAMETERS (mg/kg
dry weight)
Arsenic
12
Cadmium
<1
Mercury
0.234
Chromium
43.8
Copper
38.8
Lead
24.6
Molybdenum
<2.5
Nickel
18
Selenium
<5
Zinc
78.2
Total Phosphorus
1730
TKN
30300
Ammonia -Nitrogen
<100
Nitrate and Nitrite
<4.8
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties or submitting f formation, including the possibility of fines and imprisonment for knowing violations."
X Date 7
(SIGN TURF O PR ARER)
DENR FORM RSSF (5/2003) Printed: Wednesday - January 22, 2020 at 16:48:52 for: 2209 02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
Facility Name
NPDES#
or WQ# (residual only)
WWTP Name
Residual Analysis Data
Product Type
Date Sampled
Date Composited
Percent Soilds
GRANITE FALLS, NC
GRANITE FALLS WTP
WPL
09/23/19
3.01
PARAMETERS (mg/kg dry weight)'
Aluminium
125000
Calcium
2350
Magnesium
1740
pH
6.30
Potasium
1190
Sodium
<250
PAN
12175
SAR
0.1646
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the pos ' ity of fines and imprisonment for knowing violations."
X Date
(SIGNATURE OFf PR A R)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/5/2020 11:02:16 AM

Waypdlont(2)
ANALYTICAL
10/2/2019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-267-0008
Project Description: Granite Falls WTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/24/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam« p 6,-r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

(2)
Wavpoint
�7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-267-0008
Client Project Description: Granite Falls WTP
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
68325
Granite Falls WTP
Solids
09/23/2019 10:30
09/24/2019
68325
Granite Falls WTP
Solids
09/23/2019 10:30
09/24/2019
SM-4500-NH3C
WTN
68325
Granite Falls WTP
Solids
09/23/2019 10:30
09/24/2019
9045D
WTN
68325
Granite Falls WTP
Solids
09/23/2019 10:30
09/24/2019
4500NO3F-2011
WTN
68325
Granite Falls WTP
Solids
09/23/2019 10:30
09/24/2019
6010D
WTN
68325
Granite Falls WTP
Solids
09/23/2019 10:30
09/24/2019
SW-7471B
WTN
68325
Granite Falls WTP
Solids
09/23/2019 10:30
09/24/2019
SM-4500-NH3C-TKN
WTN
68325
Granite Falls WTP
Solids
09/23/2019 10:30
09/24/2019
SM-254OG
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia

Report Number: 19-267-0008
Account Number: 46622
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number-: 68325
Sample Id : Granite Falls WTP
C
Waypoi t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.wayoointanalytical.com
Project: Granite Falls WTP
REPORT OF ANALYSIS Date Sampled: 9/23/2019 10:30:00
Date Received: 09/24/2019 00:00
Date Reported: 10/02/2019
Total Solids *
3.01
ADM
09/25/2019 16:40
SM-2540G
Moisture *
97.00
ADM
09/25/2019 16:40
SM-2540G
Total Kjeldahl Nitrogen
3.03
30300
250
JPJ
10/01/2019 08:30
SM-4500-NH3C-TKN
Phosphorus
0.17
1730
50.0
JTR
09/27/201918:11
601OD
Potassium
0.12
1190
50.0
JTR
09/27/201918:11
601OD
Sulfur
0.30
3010
50.0
JTR
09/27/201918:11
601OD
Calcium
0.24
2350
250
JTR
09/27/201918:11
601OD
Magnesium
0.17
1740
50.0
JTR
09/27/201918:11
601OD
Sodium
<0.03
<250
250
JTR
09/27/201918:11
601OD
Iron
41400
50.0
JTR
09127/201918:11
601OD
Aluminum
125000
500
KKM
10/01/201913:03
601OD
Manganese
1650
5.00
JTR
09/27/201918:11
6010D
Copper
38.8
2.50
JTR
09/27/201918:11
6010D
Zinc
78.2
12.5
JTR
09/27/201918:11
6010D
Ammonia Nitrogen
<0.01
<100
100
JPJ
10/01/2019 12:00
SM-4500-NH3C
Organic N
3.03
30300
250
10/01/2019 08:30
CALCULATION
Nitrate+Nitrite-N
<4.80
4.80
ZBD
09/27/201915:47
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series is on a wet basis.
B - Analyte detected in blank
H - Beyond holding time
a
M.0 GQAN
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau rlc MCGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist

Report Number: 19-267-0008
Account Number: 46622
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68325
Sample Id : Granite Falls WTP
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyiical.com
Project Granite Falls WTP
REPORT OF ANALYSIS
Date Sampled: 9/23/2019 10:30:00
Date Received: 09/24/2019 00:00
Date Reported: 10/02/2019
Cadmium
<1.00
1.00
JTR
09/27/201918:11
6010D
Chromium
43.8
2.50
JTR
09/27/201018:11
6010D
Nickel
18.0
2.50
JTR
09127/201918:11
6010D
Lead
24.6
3.00
JTR
09/27/201918:11
6010D
Arsenic
12.0
5.00
KKM
10/01/201913:18
6010D
Mercury
0.234
0.0139
TJS
09/27/2019 13:50
SW-7471 B
Selenium
<5.00
5.00
JTR
09/27/201918:11
6010D
pH *
6.3
JSL
09/30/2019 06:58
9045D
Molybdenum
<2.50
2.50
JTR
09/27/201918:11
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist

0 0
Waypoint"
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt.Form
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number: 19-267-0008
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F- High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F- High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: 113randi Watson Date & Time: 9/24/2019 13:29.06

SAIVIPL LOG #
CUST01VIER: SYNAGRO
PROJECT MAINAGER:_ —Eli Ie
19-26
46622Zp°°8
Synaqro Central LLC; Technical
09-2419
Granite Falls VVTP 3:28:01
A,!' � it L 1l)MER SAMPLING SAMPLE
LAS 1; SAMPLE I.D. LOCATION
TYPE
Relinquished by Sampler:
q 00 5- t LO 5-71'0 El �� V
H R __7 r, (D IMP LED
:per , proceoures
thO Collection of those- spmples.
S MPLE
`� OF SAMPLING
METHOD M E' H 0 ED
CONTAINERS DA-iE TIME
PRESERVED S H IPP Ill
me Recieved by:
<
Relinquished by:
Q-ite Time Recieved by:,,�-
L
Relinquished by: Ll
Efate. If Tit ITI e Recieved by:
SPECIAL INSTRUCTIONS:
0 3-LS
monitoring purposes.
SAM, PLE ANAU-ISIS REQUEST
I.D. � I ill; 1:'l 11, 'Organic
S Ll SL2 j Cd I Cr I Ni I Pb j. As i gig
So
PO,l
SLI: 101al Solids (Moisture), Total Kieldaf-1 Nitr000n, Phosphorus, and P' tassiurn
S! ?., Basic Test SLI Plus Sulfur, Calcium, Magnesium, Sodium, iron, Aluminum, Manganese, Copper and Zinc
REMARKS:
calco,
eq t I i V.* o
Solider

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2209-02-WPL-NC GRANITE FALLS, NC WTP LIQUID 9/23/2019 9/112019-12/31/2019 0.1646
Na mg/I = (Na mg/kg x % Solids) _ 100 = (250 x 3.0100) _ 100 = 7.525
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (2350 x 3.0100) _ 100 = 70.735
Mg mg/I = (mg mg/kg x % Solids) + 100 = (1740 x 3.0100) _ 100 = 52.374
Na meq = Na mg/I _ Molec.Wgt.Na = 7.525 + 23 = 0.327174
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 70.735 = 20 = 3.53675
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 52.374 _ 12 = 4.3645
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.327174 _ SgrRoot[0.5(3.53675+4.3645)] = 0.164606
Printed: 1 /22/2020
Page 1 16:57

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
Facility Name: GRANITE FALLS, NC
NPDES# : NCO021890
or WQ# (residual only)
WWTP Name: GRANITE FALLS WWTP
Residuals Analysis Data
Product Type
LSLIQ
Date Sampled (grab) or 09/23/19
Date Composited
Percent Solids
2.78
PARAMETERS (mg/kg dry weight)
Arsenic
<5
Cadmium
1.77
Mercury
2.63
Chromium
57.2
Copper
197
Lead
46.8
Molybdenum
4.43
Nickel
24.8
Selenium
6.02
Zinc
532
Total Phosphorus
22100
TKN
40400
Ammonia -Nitrogen
<100
Nitrate and Nitrite
12600
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
Date 9 //
DENR FORM RSSF (5/2003) Printed: Monday - February 17, 2020 at 10:07:29 for: 2209 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
Facility Name GRANITE FALLS, NC
NPDES# NCO021890
or WQ# (residual only)
WWTP Name GRANITE FALLS WWTP
Residual Analysis Data
Product Type
LSLIQ
Date Sampled
09/23/19
Date Composited
Percent Soilds
2.78
PARAMETERS (mg/kg dry weight)'
Aluminium
23200
Calcium
64400
Magnesium
2470
pH
6.40
Potasium
2340
Sodium
1150
PAN
24770
SAR
0.2014
Laboratory
Waypoint Analytical Virginia Inc.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, incl 'ng a possibility of fines and imprisonment for knowing violations."
X Date 0 b 4j.1jQ, ")
(SIGNATURE OF P PARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/17/2020 10:07:26 AM

0
W-a 0 nt ypol
ANALYTICAL
10/2/2019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-267-0007
Project Description: Granite Falls WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/24/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

Waypointe)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-267-0007
Client Project Description: Granite Falls WWTP
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
SM-254OG
WTN
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
SW-7471B
WTN
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
SM-4500-NH3C-TKN
WTN
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
4500NO3F-2011
WTN
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
6010D
WTN
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
SM-4500-NH3C
WTN
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
9045D
WTN
68324
Granite Falls WWTP
Solids
09/23/2019 10:00
09/24/2019
AOAC 955.01
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia

Report Number: 19-267-0007
Account Number: 46622
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68324
Sample Id : Granite Falls WWTP
e
Waypoi t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Granite Falls WWTP
REPORT OF ANALYSIS
Date Sampled: 9/23/2019 10:00:00
Date Received: 09/24/2019 00:00
Date Reported: 10/02/2019
Total Solids *
2.78
ADM
09/25/2019 16:40
SM-2540G
Moisture *
97.20
ADM
09/25/2019 16:40
SM-2540G
Total Kjeldahl Nitrogen
4.04
40400
250
JPJ
10/01/2019 08:30
SM-4500-NH3C-TKN
Phosphorus
2.21
22100
50.0
JTR
09/27/201918:06
601OD
Potassium
0.23
2340
50.0
JTR
09/27/201918:06
601OD
Sulfur
0.90
8980
50.0
JTR
09/27/201918:06
6010D
Calcium
6.44
64400
250
JTR
09/27/201918:06
6010D
Magnesium
0.25
2470
50.0
JTR
09/27/201918:06
6010D
Sodium
0.12
1150
250
JTR
09/27/201918:06
6010D
Iron
28500
50.0
JTR
09/27/201918:06
6010D
Aluminum
23200
50.0
JTR
09/27/201918:06
6010D
Manganese
355
5.00
JTR
09/27/201918:06
6010D
Copper
197
2.50
JTR
09/27/201918:06
6010D
Zinc
532
12.5
JTR
09/27/201918:06
6010D
Ammonia Nitrogen
<0.01
<100
100
JPJ
10/01/2019 12:00
SM-4500-NH3C
Organic N
4.04
40400
250
10/01/2019 08:30
CALCULATION
Nitrate+Nitrite-N
12600
4.75
ZBD
09/27/201915:46
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank
H - Beyond holding
time
pwie.
1%C 1011 %
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist

Report Number: 19-267-0007
Account Number: 46622
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 68324
Sample ld : Granite Falls WWTP
s
Waypoi t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Granite Falls WWTP
REPORT OFANALYSIS
Date Sampled: 9/23/2019 10:00:00
Date Received: 09/24/2019 00:00
Date Reported: 10/02/2019
Cadmium
1.77
1.00
JTR
09/27/201918:06
601OD
Chromium
57.2
2.50
JTR
09/27/201918:06
601OD
Nickel
24.8
2.50
JTR
09/27/201918:06
601OD
Lead
46.8
3.00
JTR
09127/201918:06
601OD
Arsenic
<5.00
5.00
KKM
10/01/201912:58
6010D
Mercury
2.63
0.0141
TJS
09/27/2019 13:49
SW-7471 B
Selenium
6.02
5.00
JTR
09/27/2019 18:06
6010D
pH *
6.4
JSL
09/30/2019 06:58
9045D
Calcium Carbonate Equivalent
10.80 108000
1000
DXT
09/27/2019 13:00
AOAC 955.01
Molybdenum
4.43
2.50
JTR
09/27/201918:06
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
pw4 X Gawr
Pauric McGroary
Agronomist

Waypoi.nto
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number: 19-267-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
_
Shipping container/cooler uncompromised?
• Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
• Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
• Yes
0 No
COC properly completed
• Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
40 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
® N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
• N/A
F_ High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: jBrandi Watson Date & Time: ,09/24/2019 13:27:18

SAMPI LOG
CUSTOMER: SYNAG RO
PROJECT MANAGER:
Phone: ( � L,, ) 7D3-- _ v`S 1
A&L
LAB #
CUSTOMER
SAMPLE I.D.
vtv
T'0
Helinquished by Sampler:
Helinquished by:
Relinquished by:
SPECIAL INSTRUCTIONS:
M,
S
LL EASTERN AGRICULTURAL -LASS, INC.
7621 Whitepine Road
Richmond, VA 23237
A— n n A ln, 1-6446
IIIIIIIIIiIIIIIIII�IIIiIIIllillllllllllllllllllllllllllllllllllll 4562 Z0007 l LLC/ Technical 019
Granite Falls WWTP 73:26:32
SAMPLING
LOCATION
SAMPLE
TYPE
7
U15L�i
g,
Time
1/11"
Time
Time
C(nl UM (OF C USIT(Dov
RIECORD ez ARi ILVIS53
RECORD
1 attest that the proper field sampling procedures
were used during the collection of these samples.
SAMPLER
# OF SAMPLING METHOD METHOD
CONTAINERS DATE TIME PRESERVED SHIPPED
Pj
Recieved b REMARKS:
Recieved by:
Recieved by:
For monitoring purposes. PO#:
(STATE)
SAMPLE
I.D. SL1 SL2
ANALYSIS
REQUEST
NH4 N
I NO:, N
Q� anic
Cd
Cr
Ni
Pb
As
HgTeH
CaCO 3
Volatile
Solids
Mo.
ClE-N
IN
�`equiv.
V-rcn� 1L
W I✓7-P
1lG'
l
V
',!'`
SI_b • Tntni gr'lirlc
- - -, I 1 1 iuoI,n Iul UJ, an❑ t-oiassium
SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
Pacre 6 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2209-01-LSLIQ-NC GRANITE FALLS, NC WWTP LIME 9/23/2019 91112019-12/3112019 0.2014
STABILIZED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (1150 x 2.7800) = 100 = 31.97
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (64400 x 2.7800) = 100 = 1790.32
Mg mg/1 = (mg mg/kg x % Solids) _ 100 = (2470 x 2.7800) _ 100 = 68.666
Na.meq = Na mg/I _ Molec.Wgt.Na = 31.97 = 23 = 1.39
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 1790.32 _ 20 = 89.516
Mg meq = Mg mg/1 _ Molec.Wgt.Mg = 68.666 = 12 = 5.72217
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.39 + SgrRoot[0.5(89.516+5.72217)] = 0.20143
Printed: 1/22/2020
Page 1 16:56

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: GRANITE FALLS, NC PREDOMINANT SOIL SERIES: PACOLET
OWNER: ARLENE MILLSAPS PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 33.59
SITE #: NC AL 00013 FIELD# : AL 00013 0001 A OPERATOR: DANNY MILLSAPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 15.10 ACRES PERMITTED: 15.10
Page: 1
Lune Applied a..
Date
LbdAc
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
10/10/19
55,800.00 (G)
3695.364
2.78
0.428
GFLSLIQ
DRY
0-<I/2"
SUR
0.5
0.30
40,400. p
100.00 p
12,600.01 p
24770
FESCUE PASTURE
10/11/19
12,400.00 (G)
821.192
2.78
0.095
GFLSLIQ
DRY
0-<I/2"
SUR
0.5
0.30
40,400. p
100.00 p
12,600.01 p
24770
FESCUE PASTURE
Oct-19
68,200.00 (G)
4,516.556
10/9/19
93,000.00 (G)
6158.940
3.01
0.773
GFWPL
DRY
0-<1/2"
SUR
0.5
0.40
30,300. p
100.00 p
4.80 p
12175
FESCUE PASTURE
10/10/19
24,800.00 (G)
1642.384
3.01
0.206
GFWPL
DRY
0-<1/2"
, SUR
0.5
0.40
30,300. p
100.00 p
4.80 p
12175
FESCUE PASTURE
10/11/19
86,800.00 (G)
5748.344
3.01
0.722
GFWPL
DRY
0-<1/2"
SUR
0.5
0.40
30,300. p
100.00 p
4.80 p
12175
FESCUE PASTURE
Oct-19
204,600.00 (G)
13,549.668
1 ULdl Ua11UnSIAG: 1b,000.GJ
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual lbs/acre
67
0.046
0.005
0.209
0.338
0.133
0.004
0.013
0.087
0.023
0.823 29.03
Cumulative lbs/acre
0.065
0.080
1.009
2.194
0.613
0.006
0.123
0.390
0.062
6.611
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
l _
194
FD Cumulative Pollutant Loading'
Rate Limit (lbs/acre )
36.6
34.8
_
1339.0
267.9
1
15.0 1i i
375.0
89.0
2500.0
GFLSLIQ = GRANITE FALLS, NC WWTP LIME STABILIZED LIQUID
GFWPL = GRANITE FALLS, NC WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
,rator:
Acres Used:
Granite Falls, NC
WQ0016247
Total Dry Tons Applied (Annual): 33.59
Cation Exchange Capacity (non 503 only):
Danny Millsaps Owner: . Arlene Millsaps Predominant Soil Series:
15.1 Acres Permitted: 15.1 Site #: NC AL 00013
Pacolet
Field #: AL 00013 0001A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Ph.
.0rus
M
ENEEMENEEN
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 11
1 1�
1 111
1 lel
1 111
1 ellon
111
1 111
1 111
1 111
1 Ile
1 110MITI1•
1 11
1 11
1 111
IT, 11
1 111
IT, le
1 111
1 111
1 ell
1 111
1 111
! lel
1 11
.••
1 1•
1
1 111
1 111
1 III
1 III
1 111
1 III
1 111
1 111
1 111
1 111
1 Ile
1 111
1 111
1 lol
1 111
1 111
1 III
1 111
1 1'
1 1� •
1 1:�
1 111
1 111
1 111
1 111lz
111
1 111
1 111
0 111
1 III
1 111
1 11
1 11
1 111
1 111
l ell
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11�
1 11
1 11•
1 111
1 Ill
1 111
1 111
1 Ill
1 111
1 111
1 lee
1 l01
1 111
1 1
•-• ,
EMM
1 1 .
1 1.
1 lol
1 111
1 Ill
1 111
1 Ill
1 111
1 111
1 III
1 111
1 Ill
1 1:
111.
11
feel
1111
llll
elll
llll
1111
ffITIT,1
1111
0lll
11
1 .
1 ..
1 Ile
1 111
1 111
1 Ill
1 111
1 111
1 Ill
1 Ill
1 111
1 111
1
Total
•
;;
1 111
1 111
1 111
1 Ile
1 Ill
1 111
1 111
1 111
1 ell
1 111
• 11
_Rhorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
3riso meat for knowi g violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

SECTION 4

TCLP data is not included in the 2019 Annual Report for Granite Falls WTP. A TCLP sample was taken in
2016 and is only required to be taken once per permit cycle.

�t{lrl!?OtJPetPF•iTfiL'F��7th+t711?: zS.INC
Analytical Laboratvrw,
June 05, 2019
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Granite Falls
Dear Erik Biuce:
Summit Environmental Technologies, Inc.
3310 Wig: St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http:IAvww.settek.com
Order No.: 19051263
Summit Environmental Technologies, Inc. received 1 sample(s) on 5/16/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH00923201 1 -1, Virginia VELAP 9456, Washington C891
Page 1 of 34

Summit Environmental Technologies, zne. Case Narrative
SUMMIT 3310 Win St.
L=NVU10MPd_tdTAL TE-MHNOLO i45, IpI . Cuyahoga Falls, Ohio 44223 WO#: 19051263
Anaiyticsl ia6nratorlas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com Date: 6/5/2019
CLIENT: Synagro
Project: Granite Falls
WorkOrder Narrative:
19051263: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19051263-OOIA TCLP-SVOC-CPest(8081B): CCV exhibited high recoveries for Endrin. Associated
samples were ND
Revision v1
Page 2 of 34

Summit Environmental Technologies, In,Summit 3310 Win S Qualifiers and Acronyms
hVli?Cr1d61chdTE1L T C94E1d1.C¢Ga�S, INC Cuyahoga Falls, Ohio 442� WO#: 19051263
Ae7tcly0abl Lafjoxaior'les TEL: [phone] FAX.- (330) 253-446
Website: httD:11Www.settek.co. Date: 6/5/2019
These commmonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
In Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confinned by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision v1
Page 3 of 34

Summit Environmental Technologies, Inc. Workorder
Ins"Mmilu
3310 Win St.
L�S,1I4 Cuyahoga Falls, Ohio44223 Sample Summary
AlTalyucal Laboralarias TEL: [phone] FAX.- [phone] WO#: 19051263
Website: htto:llwww.settek.com 05-Jun-19
CLIENT: Synagro
Project: Granite Falls
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
19051263-001 Granite Falls WWTP 5/15/2019 8:00:00 AM 5/16/2019 10:20:00 AM Sludge
Page 4 of 34

Summit Environmental Technologies, Inc. DATES REPORT
ffJ SUMMIT3310 Win St.
ph,Vl11Wr ,1E+fTAL HGHNOLCDI�H-:S, 1F:C. Cuyahoga Falls, Ohio 44223
WO#: 19051263
4,rt;rlytlryt! LgbOxJlotdc7E TEL: [phone] FAX.- [phone]
Website: htta://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
19051263-OOIA Granite Falls WWTP 5/15/2019 8:00:00 AM Sludge Ignitability of Solids (SW-846: 1030)
6/3/2019 5:55:23 PM
pH (SW9045D)
5/31/2019 3:40:31 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
5/17/2019 8:10:00 PM
Reactive Sulfide (9034)/7.3.4.2
5/17/2019 8:10:00 PM
TCLP Herbicides Analysis (SW1311/85/20/2019 6:00:00 PM
5/24/2019 2:15:00 PM
6/1/2019 8:05:00 AM
solid
TCLP Mercury Analysis (SW1311/7475/20/2019 6:00:00 PM
5/22/2019 2:10:00 PM
5/22/2019 5:03:00 PM
TCLP Metals Analysis (SW1311/6010 5/20/2019 6:00:00 PM
5/21/2019 5:30:00 PM
5/23/2019 2:53:42 PM
TCLP Metals Analysis (SW1311/6010 5/20/2019 6:00:00 PM
5/21/2019 5:30:00 PM
5/22/2019 11:07:21 PM
TCLP Pesticides Analysis (SW1311/8(5/20/2019 6:00:00 PM
5/24/2019 1:00:06 PM
5/31/2019 10:50:00 PM
TCLP Semi-Volatiles Analysis 5/20/2019 6:00:00 PM
5/23/2019 10:42:41 PM
5/28/2019 4:31:00 PM
(SW 1311/8270)
TCLP Volatiles Analysis by SW8260B
5/20/2019 6:00:00 PM
5/21/2019 6:55:00 PM
Revision vl
Page 5 of 34

Summit Environmental Technologies, Inc. Analytical Report
ms"Mmist 3310 Win St.
=A,ti�l#?OtJf9_7IT2L GEC34P olrl 1h40 Cuyahoga Falls, Ohio 44223 (base report)
A:r.,httieal Lahoralorlee TEL: [phone] FAX.- [phone] WO#: 19051263
Website: http://www.settek.com Date Reported: 6/5/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 5/15/2019 8:00:00 AM
Lab ID: 19051263-OOIA
Project: Granite Falls
Client Sample ED Granite Falls WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00500 mg/L 1 5/22/2019 5:03:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW601OD
SW3010A Analyst: KMO
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
5/22/2019 11:07:21 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
5/22/2019 11:07:21 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
5/23/2019 2:53:42 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
5/22/2019 11:07:21 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
5/22/2019 11:07:21 PM
TCLP Selenium(Se) 0.0591
0.0500
mg/L
1
5/22/2019 11:07:21 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
5/22/2019 11:07:21 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
5/28/2019 4:31:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
5/28/2019 4:31:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
5/28/2019 4:31:00 PM
2,4-Dinitrotoluene
ND
0.0400
mg/L
2
5/28/2019 4:31:00 PM
o-Cresol
ND
0.200
mg/L
2
5/28/2019 4:31:00 PM
m/p-Cresol(s)
ND
0.200
mg/L
2
5/28/2019 4:31:00 PM
Cresols, Total
ND
4.00
mg/L
2
5/28/2019 4:31:00 PM
Hexachloro-1,3-butadiene
ND
0.0160
mg/L
2
5/28/2019 4:31:00 PM
Hexachlorobenzene
ND
0.0400
mg/L
2
5/28/2019 4:31:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
5/28/2019 4:31:00 PM
Nitrobenzene
ND
0.0800
mg/L
2
5/28/2019 4:31:00 PM
Pentachlorophenol
ND
0.200
mglL
2
5/28/2019 4:31:00 PM
Pyridine
ND
0.200
mg/L
2
5/28/2019 4:31:00 PM
Surr: 2-Fluorophenol
26.5
10 - 109
%Rec
2
5/28/2019 4:31:00 PM
Surr: Phenol-d6
31.8
10 - 109
%Rec
2
5/28/2019 4:31:00 PM
Surr: Nitrobenzene-d5
31.4
19 - 120
%Rec
2
5/28/2019 4:31:00 PM
Surr: 2,4,6-Tribromophenol
31.8
10 -120
%Rec
2
5/28/2019 4:31:00 PM
Surr: 2-Fluorobiphenyl
32.2
22 - 117
%Rec
2
5/28/2019 4:31:00 PM
Qualifiers: E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine
area response
MC Value is below Minimum
Compound Limit,
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Revision v1
RL Reporting Detection Limit
U Samples with CalcVal < MDL
Page 6 of 34

Summit Environmental Technologies, Inc. Analytical Report
MZurAmist 3310 Win St.
ch#t�IS?4NPe=tdTtYL','l ! F!pl_r}Ci $, 9htG Cuyahoga Falls, Ohio 44223 (base report)
AiTalytica/ L-aboratorles TEL: [phone] FAX: [phone] WOM 19051263
Website: httD:1Avww.settekcom Date Reported: 6/5/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 5/15/2019 8:00:00 AM
Lab ID: 19051263-OOIA
Project: Granite Falls
Client Sample ID Granite Falls WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14 53.8
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma-BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Surr: TCMX
57.9
Surr: DCB
73.9
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)-SOLID
2,4-D ND
2,4,5-TP ND
Surr: DCAA 60.6
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS BY SW8260B
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
SW8270D SW351OC Analyst: BJH
34 - 116 %Rec 2 5/28/2019 4:31:00 PM
SW8081 SW351OC Analyst: SFG
0.0250
mg/L
10
5/31/2019 10:50:00 PM
0.0500
mg/L
10
5/31/2019 10:50:00 PM
0.00500
mg/L
10
5/31/2019 10:50:00 PM
0.00500
d mg/L
10
5/31/2019 10:50:00 PM
0.00500
mg/L
10
5/31/2019 10:50:00 PM
0.00500
mg/L
10
5/31/2019 10:50:00 PM
0.00500
d mg/L
10
5/31/2019 10:50:00 PM
10 - 119
%Rec
10
5/31/2019 10:50:00 PM
10 - 119
%Rec
10
5/31/2019 10:50:00 PM
SW8151A SW8151A Analyst: MES
0.0100 mg/L 1 6/1/2019 8:05:00 AM
0.00500 mg/L 1 6/1/2019 8:05:00 AM
20 - 140 %Rec 1 6/1/2019 8:05:00 AM
SW8260 SW1311M Analyst: CTB
0.250
mg/L
50
5/21/2019 6:55:00 PM
0.250
mg/L
50
5/21/2019 6:55:00 PM
5.00
mg/L
50
5/21/2019 6:55:00 PM
0.250
mg/L
50
5/21/2019 6:55:00 PM
0.250
mg/L
50
5/21/2019 6:55:00 PM
2.50
mg/L
50
5/21/2019 6:55:00 PM
0.250
mg/L
50
5/21/2019 6:55:00 PM
0.250
mg/L
50
5/21/2019 6:55:00 PM
0.250
mg/L
50
5/21/2019 6:55:00 PM
0.100
mg/L
50
5/21/2019 6:55:00 PM
Qualifiers: E
Value above quantitation range
M
Manual Integration used to determine area response
N
Tentatively identified compounds
O
RSD is greater than RSDlimit
PL
Permit Limit
RL
Reporting Detection Limit
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits Revision V 1
U Samples with CalcVal < MDL
Page 7 of 34

Summit Environmental Technologies, Inc. Analytical Report
Sum MIT 3310 Win St.
—W,(M0tJr.1KtdT L SEC*iN01_Cf{al $,1hjc Cuyahoga Falls, Ohio 44223 (base report)
Rrrallrtical i°aboraiorhee TEL: [phone] FAX- [phone] WOM 19051263
Website: http://vww.settek.com Date Reported: 6/5/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 5/15/2019 8:00:00 AM
Lab ID: 19051263-OOIA
Project: Granite Falls
Client Sample ID Granite Falls WWTP
Analyses Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M
Analyst: CTB
TCLP VOLATILES ANALYSIS BY SW8260B
Surr: 4-Bromofluorobenzene 88.9
70 - 130
%Rec
50
5/21/2019 6:55:00 PM
Sum Dibromofluoromethane 87.2
70 - 130
%Rec
50
5/21/2019 6:55:00 PM
Sum Toluene-d8 99.8
70 - 130
%Rec
50
5/21/2019 6:55:00 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.490 mg/Kg 1 5/17/2019 8:10:00 PM
RCI-SOLID-W/ IGNITABILITY1030 SW1030 Analyst: CXS
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability nonflammable 1 6/3/2019 5:55:23 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9045D Analyst: VVK
PH (SW9045D)
pH 6.6 s.u.@21.1C 1 5/31/2019 3:40:31 PM
RCI-SOLID-W/ IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 5/17/2019 8:10:00 PM
Qualifiers: E
Value above quantitation range
M
Manual Integration used to determine area response
N
Tentatively identified compounds
O
RSD is greater than RSDlimit
PL
Permit Limit
RL
Reporting Detection Limit
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits Revision vl
U Samples with CalcVal < MDL
Page 8 of 34

Summit Environmental Technologies, Inc.
Mt
Accreditation
Program
3310 Win St.
M9 S ki #wm I
Anal teS Report
PI%(II?CtJrdIE dTAL :F-0hWra4J7GdzS,
WC Cuyahoga Falls, Ohio 44223
�IJ?JfyUcal Lab craIcr(&B
TEL: [phone] FAX.- [phone]
WOM
19051263
Website: http://www.settek.com
05-Jun-19
Client: Synagro
State: NW
Project: Granite Falls
Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19051263-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides Analysis (SW1311/8151)-solid
2,4,5-TP
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)-solid
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW 1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachloroplienol
N
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
N
Key
Key
Key
NC_WW SCM A Accredited
NC_WW SCM N Not Accredited
NC WW SCM U
Unavailabl
Version #2
Page 9 of 34

Summit Environmental Technologies, Inc. Accreditation Program
S Ir 3310 Win St. Anal�7teS Report
EPAIIf�OWMENT'AL is C3%QJt)Lt). i> $, INC Cuyahoga Falls, Ohio 44223 J Y
AJ7,uiytUCaJ Laboralorloc TEL: [phone] FAX: [phone] Wo#: 19051263
Website: http://www.settek.com 05-Jun-19
Client: Synagro State: NW
Project: Granite Falls Program Name: NC WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19051263-001A Sludge
TCLP Volatiles Analysis by SW8260B
1,1-Dichloroethene
N
Sludge
TCLP Volatiles Analysis by SW8260B
1,2-Dichloroethane
N
Sludge
TCLP Volatiles Analysis by SW8260B
2-Butanone
N
Sludge
TCLP Volatiles Analysis by SW8260B
Benzene
N
Sludge
TCLP Volatiles Analysis by SW8260B
Carbon tetrachloride
N
Sludge
TCLP Volatiles Analysis by SW8260B
Chlorobenzene
N
Sludge
TCLP Volatiles Analysis by SW8260B
Chloroform
N
Sludge
TCLP Volatiles Analysis by SW8260B
Tetrachloroethene
N
Sludge
TCLP Volatiles Analysis by SW8260B
Trichloroethene
N
Sludge
TCLP Volatiles Analysis by SW8260B
Vinyl chloride
N
NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailab)
Version #2
Page 10 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
S to. M 111 3310 Win St.
ELh4111i%?hlh9'Cr7T�L7z ?flWt]L�361� , li'IC Cuyahoga Falls, Ohio44223 WO#: 19051263
An,-r ytic,2f Laboratarles TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 05-Jun-19
Client: Synab o
Project: Granite Falls BatchID: 37530
Sample ID MB-37530
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 5/20/2019
RunNo: 98618
client ID: PBS
Batch ID: 37530
TestNo: SW8260 SW1311M
Analysis Date: 5/22/2019
SegNo: 2122158
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
1.00
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
504
Surr: Dibromofluoromethane
456
Surr: Toluene-d8
546
500.0 101 70 130
500.0 91.2 70 130
500.0 109 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 11 of 34

SUMMITSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
p�74rlr�LryNrdCi3l't.L Sca retioty3�IS, :hC Cuyahoga Falls, Ohio 44223
WO#: 19051263
4 a'+ui!,�itcai' Laboratat7e+s TEL: [phone] FAX.- [phone]
Website: http.•Ilwww.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: 37530
Sample ID LCS-98614
SampType: LCS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 98614
client ID: LCSS
Batch ID: 37530
TestNo: SW8260 SW1311M
Analysis Date: 512112019
SegNo: 2121431
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDL[mit Qua]
1,1-Dichloroethene
0.0229
0.00500
0.0200
0
115
70
131
1,2-Dichloroethane
0.0204
0.00500
0.0200
0
102
70
137
MEK
ND
0.100
0.100
0
99.3
55.1
163
Benzene
0.0201
0.00500
0.0200
0
100
70
132
Carbon tetrachloride
0.0194
0.00500
0.0200
0
97.0
63.7
139
Chlorobenzene
ND
0.0500
0.0200
0
103
70
139
Chloroform
0.0204
0.00500
0.0200
0
102
70
130
Tetrachloroethene
0.0233
0.00500
0.0200
0
117
56.2
187
Trichloroethene
0.0208
0.00500
0.0200
0
104
64.1
138
Vinyl chloride
0.0210
0.00200
0.0200
0
105
22.1
147
Surr:4-Bromofluorobenzene
48.7
50.00
97.4
70
130
Surr: Dibromofluoromethane
45.5
50.00
90.9
70
130
Surr: Toluene-d8
50.9
50.00
102
70
130
Sample ID LCS-98614
SampType: LCS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 98614
client ID: LCSS
Batch ID: 37530
TestNo: SW8260 SW1311M
Analysis Date: 5/21/2019
SegNo: 2122204
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,1-Dichloroethene
0.0229
0.00500
0.0200
0
115
70
131
1,2-Dichloroethane
0.0204
0.00500
0.0200
0
102
70
137
MEK
ND
0.100
0.100
0
99.3
55.1
163
Benzene
0.0201
0.00500
0.0200
0
100
70
132
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision v1
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 12 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
S"tamlir 3310 Win St.
E04 110tdhlrt-ITAL`rccrdt ot,�lGu�:5, it,tC Cuyahoga Falls, Ohio44223
A naty [�riWO#: 19051263
f La.boraron �G TEL: [phone] FAX.• [phone]
Website: http://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: 37530
Sample ID LCS-98614
SampType: LCS
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 98614
Zlient ID: LCSS
Batch ID: 37530
TestNo: SW8260 SW1311M
Analysis Date: 5/21/2019
SegNo: 2122204
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.0194
0.00500
0.0200
0
97.0
63.7
139
Chlorobenzene
ND
0.0500
0.0200
0
103
70
139
Chloroform
0.0204
0.00500
0.0200
0
102
70
130
Tetrachloroethene
0.0233
0.00500
0.0200
0
117
56.2
187
Trichloroethene
0.0208
0.00500
0.0200
0
104
64.1
138
Vinyl chloride
0.0210
0.00200
0.0200
0
105
22.1
147
Surr:4-Bromofluorobenzene
48.7
50.00
97.4
70
130
Surr: Dibromofluoromethane
45.5
50.00
90.9
70
130
Surr: Toluene-d8
50.9
50.00
102
70
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 13 of 34

sul"SAIT
Summit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
�c,.t�lf?� tltalCtaT.ttL'��ts�lot �3G� .;, INC
Cuyahoga Falls, Ohio 44223
FlntrtytlC�P L�.L%�rvtti,rin_ TEL: [phone] FAX.- [phone]
WO#: 19051263
Website: http://www.settek.cont
05-Jun-19
Client:
Synagro
Project:
Granite Falls
BatchID: 37542
TCLP Cadmium(Cd) ND 0.100
TCLP Cadmium(Cd) 1.91 0.100 2.000 0 95.5 80 120
TCLP Cadmium(Cd) 1.93 0.100 2.000 0 96.3 70 130
TCLP Cadmium(Cd) 1.94 0.100 2.000 0 96.9 70 130 1.926 0.600 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 14 of 34

Summit Environmental Technologies, Inc.ff1summly 3310 Win St. QC SUMMARY REPORT
EP,sVll'LO t,l Et-7TAL 3 Ito JOl oGl , ih Cuyahoga Falls, Ohio 44223
WO#: 19051263
:t.naiyricat L.abcrrJrtarios TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchID: 37542
Sample ID 19051435-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 5/21/2019
RunNo: 98696
-lient ID: Batch=
Batch ID: 37542
TestNo: SW6010D SW3010A
Analysis Date: 5/23/2019
SegNo: 2126739
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 34

Summit Environmental Technologies, Inc. QC SUIO� MARY REPORT
SUMMIT3310 Win St.
P;i4�lle�+tllal�t•�TnL`aLcr� ttau3e��4s, JING Cuyahoga Falls, Ohio44223 WO#: 19051263
A.pjhy(t Vnf L.aboratc0ig TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: 37542
Sample ID MB-37542
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 5/21/2019
RunNo: 98666
Client ID: PBS
Batch ID: 37542
TestNo: SW6010D SW3010A
Analysis Date: 5/22/2019
SegNo: 2124713
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
'ample ID LCS-37542
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 5/21/2019
RunNo: 98666
;lient ID: LCSS
Batch ID: 37542
TestNo: SW6010D SW3010A
Analysis Date: 5/22/2019
SegNo: 2124714
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.12
0.500
2.000
0
106
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
ill
80
120
TCLP Chromium(Cr)
2.24
0.200
2.000
0
112
80
120
TCLP Lead(Pb)
2.24
0.500
2.000
0
112
80
120
TCLP Selenium(Se)
2.20
0.0500
2.000
0
110
80
120
TCLP Silver(Ag)
2.32
0.500
2.000
0
116
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision Vl
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 16 of 34

SUMMITSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENWIiiOWAI =NTAL Ycct�tWoui� 1� , INC, Cuyahoga Falls, Ohio 44223
do,7iytlt~,rl LabofatonoEs TEL: [phone] FAX.- [phone] WO#: 19051263
Website: http://www.settek.com 05-Jun-19
Client: Synab o
Project: Granite Falls BatchED: 37542
Sample ID 19051435-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 5/21/2019
RunNo: 98666
Client ID: Batch=
Batch ID: 37542
TestNo: SW6010D SW3010A
Analysis Date: 5/22/2019
SegNo: 2124726
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.26
0.500
2.000
0.01452
112
70
130
TCLP Barium(Ba)
ND
5.00
2.000
2.329
101
70
130
TCLP Chromium(Cr)
2.17
0.200
2.000
0.01447
108
70
130
TCLP Lead(Pb)
2.11
0.500
2.000
0
105
70
130
TCLP Selenium(Se)
2.35
0.0500
2.000
0
118
70
130
TCLP Silver(Ag)
1.87
0.500
2.000
0
93.5
70
130
'ample ID 19051435-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 5/21/2019
RunNo: 98666
;lient ID: BatchQC
Batch ID: 37542
TestNo: SW6010D SW3010A
Analysis Date: 5/22/2019
SegNo: 2124728
knalyte
Result
PQL SPK value SPK Ref Val
%REC LowL]mit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Arsenic(As)
2.34
0.500
2.000
0.01452
116
70
130
2.256
3.58
20
TCLP Barium(Ba)
ND
5.00
2.000
2.329
109
70
130
0
0
20
TCLP Chromium(Cr)
2.24
0.200
2.000
0.01447
111
70
130
2.172
2.88
20
TCLP Lead(Pb)
2.17
0.500
2.000
0
109
70
130
2.108
3.11
20
TCLP Selenium(Se)
2.45
0.0500
2.000
0
123
70
130
2.352
4.18
20
TCLP Silver(Ag)
2.10
0.500
2.000
0
105
70
130
1.870
11.5
20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 17 of 34

Summit Environmental Technologies, Inc.fffl SUMMIT 3310 Win St. QC SUMMARY REPORT
r-PWJn0W,1L-mT,i.L 1.U21N0L0G1ZS,. INC Cuyahoga Falls, Ohio 44223
4r;�t, tic�1 L;a.f�or�taracf- TEL: [phone] FAX.- [phone]
WO#: 19051263
Website: http://www.settek.conz 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: 37553
mple ID MB-37553
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/22/2019
RunNo: 98627
ant ID: PBS
Batch ID: 37553
TestNo: SW7470A SW7470A
Analysis Date: 5/22/2019
SegNo: 2123466
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-37553
SampType: LCS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 5/22/2019
RunNo: 98627
Client ID: LCSS
Batch ID: 37553
TestNo:
SW7470A SW7470A
Analysis Date: 5/22/2019
SegNo: 2123467
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Mercury 0.00406 0.00200 0.00400 0 102 80 120
Sample ID 19051422-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/22/2019
RunNo: 98627
Client ID: BatchQC
Batch ID: 37553
TestNo: SW7470A SW7470A
Analysis Date: 5/22/2019
SegNo: 2123474
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
-P Mercury
0.00527 0.00200 0.00400 0 132 75 125
S
mple ID 19051422-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/22/2019
RunNo: 98627
ant ID: BatchQC
Batch ID: 37553
TestNo: SW7470A SW7470A
Analysis Date: 5/22/2019
SegNo: 2123475
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00501 0.00200 0.00400 0 125 75 125 0.00527 5.06 20 S
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 18 of 34

suskmilSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
EmvlrLO lJtirmTAL`i—rG N0 LOGICS, NG. Cuyahoga Falls, Ohio44223
WO#: 19051263
AnufyUvaP Lat:Graron5 �TEL: [phone] FAX.- [phone]
Website: htto://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: 37553
Sample ID 19051422-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 5/22/2019
RunNo: 98627
client ID: BatchQC
Batch ID: 37553
TestNo: SW7470A SW7470A
Analysis Date: 5/22/2019
SegNo: 2123475
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 19 of 34

IT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
Gt+SrI,�C�1Jr1�r3T,�L'rc7aad 9t�LtSCI juc. Cuyahoga Falls, Ohio44223
WO#: 19051263
A?at;,tical LaGoratot7os TEL: [phone] FAX- [phone]
Website: http://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: 37570
Sample ID 19051375-001AMS
SampType: MS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 5/23/2019
RunNo: 98947
Client ID: BatchQC
Batch ID: 37570
TestNo: SW8270D SW3510C
Analysis Date: 5/29/2019
SegNo: 2137533
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
ND
2.00
0.8000 0
51.3
33.8
126
m
2,4,5-Trichlorophenol
ND
5.00
0.8000 0
46.2
28.7
144
2,4,6-Trichlorophenol
ND
5.00
0.8000 0
48.8
12.8
153
2,4-Dinitrotoluene
ND
1.00
0.8000 0
43.8
20.4
155
QMR
o-Cresol
ND
5.00
0.8000 0
26.3
10
148
QMR
m/p-Cresol(s)
ND
5.00
0.8000 0
68.8
10
148
Cresols, Total
ND
100
1.600 0
47.5
10
148
Hexachloro-1,3-butadiene
ND
0.400
0.8000 0
45.0
29
126
Hexachlorobenzene
ND
1.00
0.8000 0
56.2
33.7
134
Hexachloroethane
ND
2.00
0.8000 0
47.5
32.8
132
Nitrobenzene
ND
2.00
0.8000 0
77.5
20
158
QMR
Pentachlorophenol
ND
5.00
0.8000 0
0
10
176
S
Pyridine
ND
5.00
0.8000 0
0
10
130
S
Surr:2-Fluorophenol
0.460
1.000
46.0
3.39
130
Surr: Phenol-d6
0.600
1.000
60.0
5
130
Surr: Nitrobenzene-d5
0.660
1.000
66.0
14.5
154
Surr: 2,4,6-Tribromophenol
0.390
1.000
39.0
19.5
130
Surr:2-Fluorobiphenyl
0.770
1.000
77.0
34.4
130
Surr: p-Terphenyl-d14
0.710
1.000
71.0
8.86
156
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area
response
MC Value is below Minimum Compound
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
Revision V 1
PL Permit Limit
R RPD outside accepted recovery
limits
RL Reporting Detection Limit
Page 20 of 34

Summit Environmental Technologies, Inc.ffJ sumfArr 3310 Win St. QC SUMMARY REPORT
1 C,4rIi2�1JP8Kh1rkL`➢cCtlhfOLiC,1�_;, INC Cuyahoga Falls, Ohio 44223
Anent} 0ont L boratorlo5 TEL: [phone] FAX.- [phone] WO#: 19051263
Website: http://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls
BatchID: 37570
Sample ID 19051375-001AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 5/2312019
RunNo: 98947
Client ID: BatchQC
Batch ID: 37570
TestNo: SW8270D SW3510C
Analysis Date: 5/29/2019
SegNo: 2137534
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
2.00
0.8000 0
45.0
33.8
126
0
0
30
m
2,4,5-Trichlorophenol
ND
5.00
0.8000 0
40.0
28.7
144
0
0
30
2,4,6-Trichlorophenol
ND
5.00
0.8000 0
48.8
12.8
153
0
0
30
2,4-Dinitrotoluene
ND
1.00
0.8000 0
26.3
20.4
155
0
0
30
R
o-Cresol
ND
5.00
0.8000 0
15.0
10
148
0
0
30
R
m/p-Cresol(s)
ND
5.00
0.8000 0
57.5
10
148
0
0
30
Cresols, Total
ND
100
1.600 0
36.3
10
148
0
0
30
Hexachloro-1,3-butadiene
ND
0.400
0.8000 0
35.0
29
126
0
0
30
Hexachlorobenzene
ND
1.00
0.8000 0
50.0
33.7
134
0
0
30
Hexachloroethane
ND
2.00
0.8000 0
45.0
32.8
132
0
0
30
Nitrobenzene
ND
2.00
0.8000 0
56.2
20
158
0
0
30
R
Pentachlorophenol
ND
5.00
0.8000 0
0
10
176
0
0
30
S
Pyridine
ND
5.00
0.8000 0
0
10
130
0
0
30
S
Surr:2-Fluorophenol
0.330
1.000
33.0
3.39
130
0
Surr: Phenol-d6
0.510
1.000
51.0
10
130
0
Surr: Nitrobenzene-d5
0.470
1.000
47.0
14.5
154
0
Surr: 2,4,6-Tribromophenol
0.230
1.000
23.0
19.5
130
0
Surr:2-Fluorobiphenyl
0.620
1.000
62.0
34.4
130
0
Surr: p-Terphenyl-d14
0.630
1.000
63.0
8.86
156
0
Qualifiers: B Analyte detected in the
associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area
response
MC
Value is below Minimum Compound
ND Not Detected
O RSD is greater than RSDlimit
P
Second column confirmation
exceeds
Revision V 1
PL Permit Limit
R RPD outside accepted recovery
limits
RL
Reporting Detection Limit
Page 21 of 34

Summit Environmental Technologies, Inc.Mfl sum-141ir 3310 Win St. QC SUMMARY REPORT
eP.0110flbl'[!NTAL`ecIcrrnoLOGi!:S, ire Cuyahoga Falls, Ohio44223 WO#: 19051263
Anot',v onf Lat orat.3rkl:3 TEL: [phone] FAX.- [phone]
Website: http://www.settek.coni 05-Jun-19
Client: Synagro
Project: Granite Falls BatchID• 37570
Sample ID MB-37570
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 5/23/2019
RunNo: 98694
Client ID: PBS
Batch ID: 37570
TestNo: SW8270D SW3510C
Analysis Date: 5/23/2019
SegNo: 2129150
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
ND
0.0400
2,4,5-Trichlorophenol
ND
0.100
2,4,6-Trichlorophenol
ND
0.100
2,4-Dinitrotoluene
ND
0.0200
o-Cresol
ND
0.100
m/p-Cresol(s)
ND
0.100
Cresols, Total
ND
2.00
Hexachloro-1,3-butadiene
ND
0.00800
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.0400
Nitrobenzene
ND
0.0400
PentachIorophenol
ND
0.100
Pyridine
ND
0.100
Surr: 2-Fluorophenol
0.403
1.000
40.3
10
109
Surr: Phenol-d6
0.439
1.000
43.9
10
109
Surr: Nitrobenzene-d5
0.445
1.000
44.5
19
120
Surr: 2,4,6-Tribromophenol
0.518
1.000
51.8
10
120
Surr:2-Fluorobiphenyl
0.436
1.000
43.6
22
117
Surr: p-Terphenyl-d14
0.684
1.000
68.4
34
116
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND Not Detected
O RSD is greater than RSDlimit
P
Second column confirmation exceeds Revision V 1
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 22 of 34

Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
fr' sundiAlir
LEP-7t(I110W,ILn:n4L 1-cc lHOLOG11:5, INC Cuyahoga Falls, Ohio 44223 WO#: 19051263
Anc'PtyNcnl Lzabofziror1o!= TEL: [phone] FAX.- [phone]
Website: htto://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: 37570
Sample ID LCS-37570
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 5/23/2019
RunNo: 98694
Client ID: LCSS
Batch ID: 37570
TestNo: SW8270D SW3510C
Analysis Date: 5/23/2019
SegNo: 2129151
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
0.467
0.0400
0.8000
0
58.4
36.4
130
2,4,5-Trichlorophenol
0.675
0.100
0.8000
0
84.4
31.7
132
2,4,6-Trichlorophenol
0.676
0.100
0.8000
0
84.5
31.1
133
2,4-Dinitrotoluene
0.672
0.0200
0.8000
0
84.0
43.3
130
o-Cresol
0.650
0.100
0.8000
0
81.3
32.9
130
m/p-Cresol(s)
0.648
0.100
0.8000
0
81.0
30.4
130
Cresols, Total
ND
2.00
1.600
0
81.2
31.7
130
Hexachloro-1,3-butadiene
0.455
0.00800
0.8000
0
56.9
31.4
130
Hexachlorobenzene
0.643
0.0200
0.8000
0
80.4
43.1
130
Hexachloroethane
0.436
0.0400
0.8000
0
54.6
36.5
130
Nitrobenzene
0.609
0.0400
0.8000
0
76.1
39.5
130
Pentachlorophenol
0.761
0.100
0.8000
0
95.1
34
130
Pyridine
0.401
0.100
0.8000
0
50.1
10
130
Surr: 2-Fluorophenol
0.743
1.000
74.3
17.1
130
Surr: Phenol-d6
0.809
1.000
80.9
10
130
Surr: Nitrobenzene-d5
0.763
1.000
76.3
32.6
130
Surr:2,4,6-Tribromophenol
0.895
1.000
89.5
4.43
130
Surr:2-Fluorobiphenyl
0.706
1.000
70.6
41.8
130
Surr: p-Terphenyl-d14
1.03
1.000
103
36.4
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 23 of 34

sutom-lot Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
EP,Wln0t4Po1Et•,TAL u rc: moLoGii:S, iNc Cuyahoga Falls, Ohio 44223
WO#: 19051263
Anaiyt/rv1' Labnrvfet'!'c�� TEL: [phone] FAX.- [phone]
Website: http://`ww.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchID• 37600
Sample ID MB-37600
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 5/24/2019
RunNo: 98799
Client ID: PBS
Batch ID: 37600
TestNo: SW8081 SW3510C
Analysis Date: 5/24/2019
SegNo: 2142057
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
d
Heptachlor
ND
0.000500
d
Heptachlor epoxide
ND
0.000500
d
Methoxychlor
ND
0.000500
d
Surr: TCMX
9.56
20.00 47.8 10 119
Surr: DCB
16.6
20.00 82.9 10 119
Sample ID LCS-37600
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 5/24/2019
RunNo: 98799
Client ID: LCSS
Batch ID: 37600
TestNo: SW8081 SW3510C
Analysis Date: 5/24/2019
SegNo: 2142058
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.0101
0.000500
0.0100
0
101
20
216
gamma-BHC
0.00768
0.000500
0.0100
0
76.8
20
197
Heptachlor
0.00679
0.000500
0.0100
0
67.9
20
200
Heptachlor epoxide
0.00803
0.000500
0.0100
0
80.3
20
200
Methoxychlor
0.00978
0.000500
0.0100
0
97.8
20
227
Surr: TCMX
11.5
20.00
57.5
20
143
Surr: DCB
18.7
20.00
93.5
20
151
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision v1
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 24 of 34

summlor
3310 Win St.
Summit Environmental Technologies, Inc.fffl
QC SUMMARY REPORT
ENK11111' f-AIL7.7TAL TECTINOLOGIC-S, INC,
Cuyahoga Falls, Ohio 44223
.k�7;•�fyticuP Lavn.r�tc5rlas TEL: [phone] FAX.- [phone]
WO#: 19051263
Website: htta://www.settek.com
05-Jun-19
Client:
Synagro
Project:
Granite Falls
BatchID: 37650
2,4-D ND 0.0100 0 0 d
2,4,5-TP ND 0.00500 0 0 d
Surr: DCAA 253 500.0 50.6 20 140
2,4-D
0.406 0.0100
0.500
0 81.2
43.8
130
2,4,5-TP
0.413 0.00500
0.500
0 82.6
51.5
ill
Surr: DCAA
597
500.0
119
34.2
150
2,4-D
0.408 0.0100
0.500
0 81.6
43.8
130
0.406 0.589 30
2,4,5-TP
0.428 0.00500
0.500
0 85.5
51.5
130
0.413 3.54 30
Surr: DCAA
292
500.0
58.3
34.2
150
0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 25 of 34

sulamrr3310
Summit Environmental Technologies, Inc.
Win St.
QC SUMMARY REPORT
C,+Ulii%titJrdt A]TitL'9 cars?dOLi3G�L y, INC,,
Cuyahoga Falls, Ohio 44223
Anui;.,ricaf LaGoratortcs TEL: [phone] FAX.- [phone]
WO#: 19051263
Website: http://www.settek.com
05-Jun-19
Client:
Synagro
Project:
Granite Falls
BatchED: R98750
Sample ID Blank
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 98750
Client ID: PBW
Batch ID: R98750
TestNo: SW9014
Analysis Date: 5/17/2019
SegNo: 2129296
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLim[t Qua[
Cyanide, Reactive ND 0.485
Sample ID LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 98750
Client ID: LCSW
Batch ID: R98750
TestNo: SW9014
Analysis Date: 5/17/2019
SegNo: 2129297
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive 9.43 0.490 10.00 0 94.3 85 115
Sample ID RLCheck
SampType: RLC
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 98750
Client ID: BatchQC
Batch ID: R98750
TestNo: SW9014
Analysis Date: 5/17/2019
SegNo: 2129299
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive 0.524 0.490 0.5000 0 105 50 150
Sample ID 19051158-011AMS
SampType: MS
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 98750
Client ID: BatchQC
Batch ID: R98750
TestNo:
SW9014
Analysis Date: 5/17/2019
SegNo: 2129319
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive
10.0 0.500
10.00 0.3081 97.3 81.3
118
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal,
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
O RSD is greater than RSDlimit
P
Second column confirmation exceeds Revision vl
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 26 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Mfl SUMMIT3310 Win St.
EPAIIT'%0tJhlLt-JIAL` -.1t 1J0LCSGH:5, INC Cuyahoga Falls, Ohio44223 WO#: 19051263
Anaf,vtivgf Laisaralorie:; TEL: [phone] FAX.- [phone]
Wehsite: htto://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchID: R98750
Sample ID 19051158-011AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 98750
Client ID: BatchQC
Batch ID: R98750
TestNo: SW9014
Analysis Date: 5/17/2019
SegNo: 2129319
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 19051158-011AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 98750
Client ID: BatchQC
Batch ID: R98750
TestNo: SW9014
Analysis Date: 5/17/2019
SegNo: 2129320
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive 10.2 0.500 10.00 0.3081 98.7 81.3 118 10.04 1.39 5
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 27 of 34

Summit Environmental Technologies, Inc.summm QC SUMMARY REPORT
3310 Win St.
C;4rIiiUPIPdE:JT1tL'3c�?iP9dLO{I^,lht% Cuyahoga Falls, Ohio44223 WO#: 19051263
Anzai}�Uoal' Laboratono:� TEL: [phone] FAX.- [phone]
Website: htto://www.settek.cont 05-Jun-19
Client: Synagro
Project: Granite Falls BatchID: R98776
Sample ID MB-R98776
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 98776
Client ID: PBW
Batch ID: R98776
TestNo: SW9034
Analysis Date: 5/17/2019
SegNo: 2130197
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID LCS-R98776
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 98776
Client ID: LCSW
Batch ID: R98776
TestNo: SW9034
Analysis Date: 5/17/2019
SegNo: 2130198
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 4560 25.0 4800 0 95.0 85 115
Sample ID 19051158-011AMS
SampType: MS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 98776
Client ID: Batch=
Batch ID: R98776
TestNo: SW9034
Analysis Date: 5/17/2019
SegNo: 2130209
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4720 25.0 4800 0 98.3 75 125
Sample ID 19051158-011AMSD
SampType: MSD
TestCode:
Sulfide,React Units: mg/L
Prep Date:
RunNo: 98776
Client ID: BatchQC
Batch ID: R98776
TestNo:
SW9034
Analysis Date: 5/17/2019
SegNo: 2130210
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 4680 25.0 4800 0 97.5 75 125 4720 0.851 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 28 of 34

Summit Environmental Technologies, Inc.ffJ sufamlot QC SUMMARY REPORT
3310 Win St.
P:4+I'I3%)t1M�1CA]TitL"tc�?sidt7ti3Gl�a,7fvf, Cuyahoga Falls, Ohio44223
AnMytictzl LaboPeldr no! TEL: [phone] FAX.- [phone] WOM 19051263
Website: htto://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchID: R98776
Sample ID 19051158-011AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 98776
[lent ID: BatchQC
Batch ID: R98776
TestNo: SW9034
Analysis Date: 5/17/2019
SegNo: 2130210
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 29 of 34

SUMMITSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
4°IrtCalJtel�t7T4tiL'�i�rt;�ir]uZ{,Ir�,1�G Cuyahoga Falls, Ohio44223 WO#: 19051263
An.r{fyNonf isabcatwon,,!; TEL: [phone] FAX.• [phone]
Website: htto://www.settek.cont 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: R98995
mple ID LCS-R98995
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@22.00
Prep Date:
RunNo: 98995
ent ID: LCSS
Batch ID: R98995
TestNo: SW9045D
Analysis Date: 5/31/2019
SegNo: 2139142
alyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.0 7.0 0 100 90 110
Sample ID CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@22.3C
Prep Date:
RunNo: 98995
Client ID: LCSS
Batch ID: R98995
TestNo: SW9045D
Analysis Date: 5/31/2019
SegNo: 2140377
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 90 110
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
O RSD is greater than RSDlimit P Second column confirmation exceeds Revision V 1
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 30 of 34

_ summint
Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
��4+ISi�+1Vh1CA37 L"accrYe�e�Lt3Gi ,WC Cuyahoga Falls, Ohio44223 WO#: 19051263
A noty0o,of La_faorwaxi« TEL: [phone] FAX.- [phone]
Website:-http://www.settek-.coni 05-Jun-19
Client: Synagro
Project: Granite Falls BatchED: R98995
Sample ID 19052000-001BDUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@20.3C
Prep Date:
RunNo: 98995
'lient ID: Batch=
Batch ID: R98995
TestNo: SW9045D
Analysis Date: 5/31/2019
SegNo: 2140375
\nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
pH
6.9
6.9 0.6 5
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 31 of 34

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMIT3310 Win St.
P,h4�lii�ry.f•Jtdr't,TnL'Yz�o-tAlot s3Gl�, iNtr, Cuyahoga Falls, Ohio 44223
Ant tytical Laboratorre�! TEL: [phone] FAX.- [phone] WO#: 19051263
Website: htto://www.settek.com 05-Jun-19
Client: Synagro
Project: Granite Falls BatchID: R99073
'ample ID LCS-R99073
SampType: LCS
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 99073
;lient ID: LCSS
Batch ID: R99073
TestNo: SW1030
Analysis Date: 6/3/2019
SegNo: 2142958
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability
7.94
7.240 0 110 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds Revision vl
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 32 of 34

Nuinni!tL,iii,iroiiiiienta]TeviiiAnl,rt ; Inc.
3310 Win Street Analysis Request/Chain
Cuyahoga Rills, Ohio 14223 Tel: [phone] Fay: 330.253.4489 For Summit I'llivironmenizil
Whirr and Nullov., pages Should samples w Ifi,
Of Custody
I - In , -in
Ok L . 0
()N'4J-QLI
- 0-1 (ZT3�
Fl� (DWONIA)
11 YES
Nr[,
Page 33 of 34

Summit Environmental Technologies, Inc.
PT M 3310 Win St.
NIS'li?0Nhi_idl'ALT C!tU1Ol,iiCiTS, gttn Cuyahoga Falls, Ohio 44223 Sample Log -in Check List
Anct fyUcal L-aboratorles TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Client Name: SYN-NC-27028 Work Order Number: 19051263 RcptNo: 1
Logged by: Kayla L. Oulton 5/16/2019 10:20:00 AM
Completed By: Jesseca E. Westfall 5/16/2019 5:29:46 PM
Reviewed By: Jennifer Woolf 5/17/2019 3:17:55 PM � %►
Chain of Custody
1, Is Chain of Custody complete? Yes W No ❑ Not Present ❑
2. How was the sample delivered? UPS
Log In
3,
Coolers are present?
Yes
0
No ❑
NA ❑
4.
Shipping container/cooler in good condition?
Yes
W
No ❑
Custody seals intact on shipping container/cooler?
Yes
❑
No ❑
Not Present ❑d
No. Seal Date:
Signed By:
5.
Was an attempt made to cool the samples?
Yes
R]
No ❑
NA ❑
6,
Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No ❑
NA ❑
7.
Sample(s) in proper container(s)?
Yes
0
No ❑
8,
Sufficient sample volume for indicated test(s)?
Yes
❑d
No ❑
g,
Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No ❑
10.
Was preservative added to bottles?
Yes
❑
No ❑d
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
�/❑
13. Does paperwork match bottle labels?
Yes
d❑
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No
❑
15. Is it clear what analyses were requested?
Yes
❑d
No
❑
16. Were all holding times able to be met?
Yes
d❑
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA ❑d
Person Notified: rDate i
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding: - — - — -- -..
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
I Temp °C
I Condition
Seal Intact
I Seal ko=
Seal Date
Signed By
1
14.6
1 Goodl
Not Present
Page 34 of 34

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period
Town of Granite Falls
Granite Falls WWTP
From 01/01/19 To
WQ Permit Number
NPDES Number:
12/31/2019
WQ 0016247
NC 0021890
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1 /A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens X
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirnhle to nitrrnnfive nerfnrmed (f ln.cc A nr C1ncc R) rmmnlete fhe fnllnwina mnnitnrinu data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6`"
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Optiion/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization) X
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification incltj lipg fine and imprisonment."
Todd Larson, Operations Director
PreparerNam eandTitle( pe rprint) Land
J
Name and Title (if applicable) (type or print) /7/p
Signature of Pr Date Signature of Land App ier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Lime Stabilization Of Aerobic Digested Sludge
To Meet Vector And Pathogen Reduction Requirements
Town Of Granite Falls Lime Stabilization For Land Application Of Class "B" Sludge
Date 10:1—lg
Analyst-1- CO 6Air r
Pounds of Lime Slurry Added q(eO 40
Start Lime Addition Date tQ-q-l!j "rime: 10.00
End Lime Addition Date: 10-q-11 Time: l 0 : 30
PH Before Lime 63
Corrected pH Ig.I
Temp. la.q e-
Time :O0 Date
PH After Lime 12.5
Corrected pH 12,3
Temp. I!J.!(or-
Time 0 Date t -• -07
PH After Lime l2.
Corrected pH 12.�
Temp. 14).q
Time 2: 30 Date t 0
PH After Lime 12. (0
Corrected pH 12.5
Temp. 20 •a c Time �4 : 30 Date 0 - —l9
PH After Lime 12•(o
Corrected pH l Z.
Temp. 19.4 G
Time (p:50 Date l O- 49
H 24 Hours After Lime l °
p 2-� Corrected pH (2.5 Temp I i• I, TimeJ0L-3pDate l p-t0-(?

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project: Granite falls
�IField ::IlSoil
Lime Requirement
Tons/Acre
Date Applied
(state-county-site-field)
pH
(from soil analysis)
Applied(CCE Eq.)

SECTION 7

NCDA&CS AS imic Division Phone: [phone] Website: www
jr.gov/agronomi/
ReportNo. )-SL012708
Client: Alex Fox Advisor:
4 V4. Predictive Synagro
��� ��Id�s-ti� 284 Boger Rd
Soil Report Mehlich-3 Extraction Mocksvil►e, NC27028
.�:. • -:ice .
r'
Links to Helful Information Sampled County: Alexander
Client ID: 501947 Advisor ID:
Sampled: 10126/2019 Received: 10/30/2019 completed: 11/08/2019 Farm: NC-Al-13 Danny Mallisaps
Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1- Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 pH$ 0 0 0 Note: 12 Note:
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.81 0.99 14.6 94 0.9 6.7 379 147 69 20 49 215 135 706 706 663 0.1 1
North Carolina
j
g4�-i a
�c?l?ac�ie irir.;R FUfbII'Clta111fi16SbIP1�
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS AI imic Division Phone: [phone] Website: www Ir.gov/agronomi/
Report No. )-SL012708
Alex Fox
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at o
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full ra
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 Ib per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Page 2 of 2
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
Na
NO3-N
ORG
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find I pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmV sFind information that P-1
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205
S-1
Test Results SS-1
W/V
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine] Zn-I
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrst.htm
nitrogen
sodium
nitrate nitrogen
organic soil class
current soil pH
phosphorus index
phosphate
sulfur index
soluble salt index
weight per volume
zinc availability index
zinc index

NORWOOD, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0016247
2019 ANNUAL REPORT

SECTION 1

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
NORWOOD, NC
NORWOOD, NC WWTP AERATION BASIN LIQUID
DRY METRIC
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
August 2019
316,200.00 G
8.00
D
7.25
September 2019
49,600.00 G
1.25
D
1.14
YEARLY TOTAL
365,800.00 G
9.25
D
8.39
1 /30/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
Facility Name: NORWOOD, NC
NPDES#:
or WQ# (residual only)
WWTP Name: NORWOOD WWTP
Residuals Analysis Data
Product Type
ABLIQ
Date Sampled (grab) or 08/20/19
Date Composited
Percent Solids
0.606
PARAMETERS (mg/kg dry weight)
Arsenic
<14
Cadmium
6.2
Mercury
<3
Chromium
92
Copper
650
Lead
150
Molybdenum
42
Nickel
91
Selenium
<22
Zinc
1900
Total Phosphorus
22000
TKN
44000
Ammonia -Nitrogen
12000
Nitrate and Nitrite
80
Laboratory
SHEALY ENVIRONMENTAL SERVICES INC.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
R)
Date
DENR FORM RSSF (5/2003) Printed: Thursday - February 6, 2020 at 13:57:32 for: 2106 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
Facility Name
NPDES#
or WQ# (residual only)
WWTP Name
Residual Analysis Data
Product Type
Date Sampled
Date Composited
Percent Soilds
NORWOOD, NC
NORWOOD WWTP
ABLIQ
08/20/19
0.606
PARAMETERS (mg/kg dry weight)'
Aluminium
45000
Calcium
14000
Magnesium
3800
pH
7.00
Potasium
4800
Sodium
5000
PAN
15680
SAR
0.7506
Laboratory
SHEALY ENVIRONMENTAL SERVICES INC.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
X Date
(SIGNATURE OF PREPARE )
NR - Data Not Reported or Data Not Required Report Run Date:- 2/6/2020 1:56:51 PM

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Norwood WWTP
Lot Number:UH21082
Date Completed:09/11/2019
09/11/2019 10:50 AM
Approved and released by:
Lab Director - Greenville: Lucas Odom
P'CC
AM2 O
ACCREDIT ED
eORA(O DODEUP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UH21082
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, sample -001 has been analyzed with 3X the normal amount of sample
mass. The LOQs have been adjusted accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2of7

Client:Synagro Laboratory ID:UH21082-001
Description: 2019 N+M Norwood Matrix: Solid
Date Sampled:08/20/2019 1000 % Solids: 0.606 08/23/2019 0046
Date Received:08/21/2019
Inorganic
non-metals
un Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
2
(% Solids) SM 2540G
1
08/23/2019 0046 MOM
26831
2 350.1
(Ammonia - N ) 350.1
5
09/06/2019 1617 DFR
27821
1
(Nitrate - N ) 9056A
1
09/04/2019 2016 GMH
28021
1
(Nitrite - N ) 9056A
1
09/04/2019 2016 GMH
28023
1
(pH) 9045D
1
09/04/2019 1905 HET
27939
1
(Phosphorus) 365.1
5
08/29/2019 0951 DMA
08/28/2019 1536 27283
1 351.4
(TKN) 351.2
1
08/29/2019 1241 DMA
08/28/2019 1822 27335
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 2540G
0.606
%
2
Ammonia - N (gas diffusion)
350.1
12000
830
430
mg/kg
2
Nitrate - N (soluble)
9056A
80
33
4.0
mg/kg
1
Nitrite - N (soluble)
9056A
41
33
3.2
mg/kg
1
pH @ 22.6 ° C
9045D
7.0
su
1
Phosphorus
7723-14-0 365.1
22000
4100
830
mg/kg
1
TKN
351.2
44000
4100
4100
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 08/27/2019 1452 KSH2
08/26/2019 1340 26962
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
-ercury
7439-97-6 7471B
ND
13
3.0
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601 OD
1 08/27/2019 0228 LLL
08/26/2019 1026 26956
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 601OD
45000
1100
410
mg/kg
1
Arsenic
7440-38-2 6010D
ND
41
14
mg/kg
1
Cadmium
7440-43-9 6010D
6.2 J
14
3.4
mg/kg
1
Calcium
7440-70-2 6010D
14000
14000
1700
mg/kg
1
Chromium
7440-47-3 6010D
92
27
6.8
mg/kg
1
Copper
7440-50-8 6010D
650
27
12
mg/kg
1
Iron
7439-89-6 601OD
41000
270
120
mg/kg
1
Lead
7439-92-1 601OD
150
27
12
mg/kg
1
Magnesium
7439-95-4 6010D
3800 J
14000
1700
mg/kg
1
Manganese
7439-96-5 6010D
990
41
16
mg/kg
1
Molybdenum
7439-98-7 6010D
42 J
110
27
mg/kg
1
Nickel
7440-02-0 6010D
91 J
110
28
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
Out of holding time
W = Reported on wet weight basis
_.._aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 7

Client:Synagro Laboratory ID:UH21082-001
Description: 2019 N+M Norwood Matrix: Solid
Date Sampled:08/20/2019 1000 % Solids: 0.606 08/23/2019 0046
Date Received:08/21/2019
ICP-AES
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601 OD 1 08/27/2019 0228 LLL 08/26/2019 1026 26956
Parameter
CAS
Number
Analytical
Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7
6010D
4800 J
14000
1700
mg/kg
1
Selenium
7782-49-2
601OD
ND
54
22
mg/kg
1
Sodium
7440-23-5
6010D
5000 J
14000
1700
nrl
1
Zinc
7440-66-6
601OD
1900
140
34
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
_aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 7

Chain(,' Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 7

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um �h71r1:1 T;nG !sdalri: C yfl�J{ir lay —�_.I I � 4_LJ
�Fr�'rxltequsedrGr�r413R�T�'ly Sa�tlFiaGi�po53:
j,� Retum
rnqureta'3 hy! SonTl
to Cils:nr
[� L11a_�t��l 3r' Lala
r 't, !;'
Dnt'^
Oak-
Holimuz 9.1ad by
U
Kc—ILD:All s-,MTJSs for
I41C:a Nc.
+il l9ri'�&�
N'r:lAor -1 D—m nom
5arle
UH21082
�i'"�r• a
ua
t'•r rluiremonta (Irl::eae 4r, ifu}
j_tjNon-Maiz�ard I�hla�m�.;e l�Sr~irr;ant
OI:.Q1S0.i jfL-l''.j?irll;rJr1
I A
by
frarr M.ccrPtknJe,~s atF1ar L A S I!sf:rvLY
d D 14er ^rvodn iaE fCl'I ult} ��'r FI ❑ Re
Ice F'.rck
P. To;np, plank
t1 _
Erti=MwA r:.r., na.� .m:•q

SHEALY ENVIRONMENTAL SERVICES, INC.
5'rcaly ls:i tc7n:n�7lla[ Stc.iccs, tnc.
hmuma-nt Numbor; rt aju E HC-1 d
Chou: Synugro
PAIVa. 1 nl'l
k MCCtc•�e Cntc: S�2 �?,o �
Sample Receipt Checkiisi (SRC'
!'—L". tnonw. f—I r,..i,7..a,.- Rffi<!: ttS1:? r:r0 art aa, noz
FRcats of receipe c SESF ❑ Glicnt ❑ 'S : ❑ FcdFat El Oil]cr:
0 Yes 0 No 1. Wcfe cu.,tnrly seals Present un the conler
Yes h[q 1iA 2_ FPcus;od seals vrrn; P--t, tf-cs the -A intact And unubrukt:n?
pH Strife II): s%, Cftlat9ne Strap ID: NA Tested by: �'A
Oit^ginal tMIPCE Lure UP033 RXript, DC6 e3 (Cnr'-acted) [ermperA(uro u'c0n iaceilit u/.Solid Snap-Cnp ID: 19-1020
"C'
NA ,`TEA 'tr NA !NA tC: .NA 1NA -�
M rF]r_:r-1: g]'1; amperatnr, BLtttk ®Psgainst Bo[tles IR 0311ID: 5 IR Gun Correction Factor: 0 'C
W--tliod of urulanr 0 wet ice © Ice Packs ❑. 1)a Ice ❑ None
�Y- El No
lets] t 1f uratum of any conkr cxcee
� - I7
ZINA de�i c6-M.«ss I'sojec14i [ anagcr h7otiFiael?
P r1'.4its lwutifcd by: phone I rmni1,' faze-tu-face. (circle <rte).
Yes G] No
® NFL 4- is tite c, mrncrdal eouritir'a pnckirtg slily attachcd to tWs firm?
ycs ONO
S. Were Prop=cusrody prouedarce (rdi quislled-rronbmd) fulluwed?
V. Yus ® No
fi. sample ID.y )istcd on the C(DC? -
0 Yee Vo
—No
?. Wliru sample IDS listrd on all sarnple annrainers?
Yes ❑
8. Vlrafi vc€lccuan da[e Sc tim4 listed on the COCCI
L1E Ycs t iy 0
4_ G4'ag co11eC[i0rt clal+; s tEE]le liStt <l Qi] al) xina;alU t U9f83:1Cr51
—all
Yes
�] NE'
10. Did Cnnfait]cr label ittiutmtEtEon (1IJ, date„ tiu]e) agrr ru:th tltc C'C�G?
0 IGS
❑ Nrr,
11. Ivem tests ttr be performed liz;(txl on the C0+^?
Yes'
❑ pjo
12. Did a[l samples arriv'C fu the prr�Ptrr containers far inch test anNor in n<- ennrfitic�tt
(unbroke-n khi On. CCC.y?
® Yes
❑ No
13. Was udNuate sample vnirtma available?
Yes
❑ No
19_ WE- all saluples rtx:eavcd wiin holdh g IittEt or 48 hours, whichcver conics 517s0
❑ Ycs
Ns]
15. Weze any :samples contaircrs u]issinL-�'exctn•81' (circle aae) sprttplLs Neil li srai ou C"a
El Yes
❑ No
0 NM
Ri- For krC}, anr3 RSY-1?5 Samples, we a bubules arv�seut'�"pea-riac'' ;'o'or 6sraru in tEiaute[er)
,n any cff tl:e VOA vials-1
17_ Wvro all 1)R0,'rrtet91s,'hutde 1 samp[cs rcceived at a pH of <??
] Y&q
No
NA
( yGti
%1
NA
18, %gemall cyr-nido samples recc j'vrd Na P11 > 12 and sull'ide sumplz i,eceivetl ut a Iyg1 g?
® �'es
lVo
®N4
19' LVerle 4l1 apples cb?c NA7r"[ KN:cyanidelplter]ol+'fi2.5 {'= _SmgrL) samples frcc of residual
!
chlorin,^.'r'
2st- Wirrc client re:r:arkVr ucsts i.e- r nested dil�
�. 1. c+l 4i+:ns, ls'1SriciSD �r4E;natiorts, e[c.,.]
i
© Yes
No
®�1:1
coy ds' transcribed from the COC into the roa1L•ltent section in LITYIS?
Yes
_ No
21.1�as tl]e .?uolt nunnher (isred on the coma -user la1x:1? )Y -as, Quote # NA
Sample k'resei'vati0t] (ivlust L+e Cclmptt twd fair ;jjy' sanmlc(3) iflCi2tT;G l4 preservad ur vdth hea&Vacr,)
SaijJple(s) NA
wcrereaeiyetlirtcnrrcE-r1}ps�er4eclandxet� acljnste�itccorlin�tly
in slIample receiving •pith 1NA mi. of rircIa One: H2SO4} L'+''_ 03, N(J, Nat3H using; Sit # N?
afareservtt(ion 'NA
TirrLadjj,Uted'
lr"ttta a thm ons presetwative is needal p[eascnotL in the commet]ts below.
i
ti rc:ra feceived with bubbles, tfi nuts in diameter,
A ware received v�ilh TRC > {I.5 u WL. (If 919 i3 no) and iv:ere
diugfy in Hample eeiving •hi8tsodium #biasuBate
fNa2_AQ3) ;yids Shealy FD: l'Abels
applied by. BN108SH ]�atc: [tt§;`�l,'f9
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2106-01-ABLIQ-NC NORWOOD, NC WWTP AERATION BASIN 8/20/2019 8/1/2019-12/31/2019 0.7506
LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (5000 x 0.6060) + 100 = 30.3
Ca mg/1 = (Ca mg/kg x % Solids) _ 100 = (14000 x 0.6060) = 100 = 84.84
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3800 x 0.6060) + 100 = 23.028
Na meq = Na mg/I _ Molec.Wgt.Na = 30.3 = 23 = 1.31739
Ca meq = Ca mg/I + Molec.Wgt.Ca = 84.84 _ 20 = 4.242
Mg meq = Mg mg/I = Molec.Wgt.Mg = 23.028 _ 12 = 1.919
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.31739 = SgrRoot[0.5(4.242+1.919)] = 0.750592
Printed: 2/6/2020
Page 1 13:48

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: NORWOOD, NC PREDOMINANT SOIL SERIES: BADIN
OWNER: ANDERSON LIVING TRUST PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 10.22
SITE #: NC ST 00004 FIELD# : ST 00004 0001 OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 26.80 ACRES PERMITTED: 26.80
Page
Lime Applied ***
Date
Lbs/A.
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/20/19
117,800.00 (G)
4395.522
0.61
0.111
NOABL
MOIST
0-<1/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
Aug-19
117,800.00 (G)
4,395.522
1
9/3/19
31,000.00 (G)
1156.716
2.00
0.096
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
I FESCUE HAY
9/4/19
55,800.00 (G)
1 2082.0901
2.00
0.174
SCUWSA
MOIST
0-<1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
Sep-19
86,800.00 (G)
1 3,238.806
Total Gallons/Ac: 7,634.33
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
12
0.012
0.002
0.020
0.306
0.043
0.001
0.024
0.037
0.014
0.902
11.64
Cumulative lbs/acre
0.085
0.048
0.778
8.585
0.605
0.022
0.298
0.450
0.109
17.705
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
160
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
NOABL = NORWOOD, NC WWTP AERATION BASIN LIQUID
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X //0'I 2 l2/2,!�zp
(SIGNATU L LIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations:"
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
--mit #:
erator:
Acres Used:
Stanly County Utilities/ Norwood, NC Total Dry Tons Applied (Annual)
WQ0016247 Cation Exchange Capacity (non 503 only):
Henry Anderson
Owner: Anderson Living Trust Predominant Soil Series:
26.8 Acres Permitted:
10.22
Badin
26.8 Site #: NC ST 00004 Field #: ST 00004 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
1/8/19
2
8/20/19
3
4
5
6
7
8 1
9
10
11
12
% Solids
2
0.606
Arsenic
16.7
1 14
Cadmium
1.7
6.2
Copper
300
650
Chromium
0
92
Lead
17.7
150
Mercury
0.83
3
Molyb-
denum
27.6
42
Nickel
31.2
91
Selenium
16.7
22
Zinc
888
1900
Total
Phos-
torus
12500
22000
_ __nual Heavy Metal Field Loadings (Calculated in lbs/acre):
M3
in
o oo•
o f
0 000
0 000
l 011
0,
i t
0 00,
o,
0 000
0 000
0 000
0 0
,.MIT,0
i t
0 000
WIT, MI
0,
0 000
0,
0 00
M$Io
o00
WIT, M,
0 T, Me0
000
KIT, eo
0 000
we M.
....
o oo�
o 0 0
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 00�
o 000
� o 0
o 0 0
0 0
0 000
0 000
0 000
0 oie
o 000
0 000
0 000
0 000
0 000
0 000
0,
zuqm
o 000
l l MIKIrl
MINITIT,0
0 I
�
0 000
0 000
m o11
0 000
0 000fflylmll
EITIMI,
o 0
0 00•
o 000
0 000
0 000
0 000
0 000
0 000
0 ooe
o 000
0 000
0 ��0
0 0
.-• ��
o 0
0 0 0
0 000
l 011
�
0 lyl
�
l 0001�
0 I,
KIT,00
0 000
0 0
o oo•
I Io
0 000
0 00I
o 000
l fog
o 000
0 000
0 000
0 Ioo
i t
0 0,
0 0
o �:o
o
o00
0 000
0 000
0 000
0 000
0 000
0 000
0 0I,
0 000
0 000
0 •o
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
Y am aware that there are significant penalties for submitting false information, including the possibility of fines and
►risonment for knowing violations".
1 l I -
Signature & Lan Applier
2 /2 2 o
Date
nFNR PnRRA RAFI .qF tl?/?MFI

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: NORWOOD, NC PREDOMINANT SOIL SERIES: BADIN
OWNER: ANDERSON LIVING TRUST PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 3.45
SITE #: NC ST 00004 FIELD# : ST 00004 0002 OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 12.80 ACRES PERMITTED: 12.80
Page
Lune Applied ***
Date
iLba/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/22/19
74,400.00 (G)
5812.500
0.61
0.147
NOABL
MOIST
0-<1/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
8/23/19
43,400.00 (G)
3390.625
0.61
0.086
NOABL
MOIST
0-<I/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
8/27/19
18,600.00 (G)
1453.125
0.61
0.037
NOABL
MOIST
0-<1/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
Aug-19
1 136,400.00 (G)
10,656.250
Total Gallons/Ac: 10,656.25
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
8
0.008
0.003
0.050
0.350
0.081
0.002
0.023
0.049
0.012
1.023
11.85
Cumulative lbs/acre
0.102
0.065
1.170
10.448
1.029
0.034
0.418
0.641
0.122
24.296
k
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
ir
._. _
152
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 k
375.0
89.0
2500.0
NOABL = NORWOOD, NC WWTP AERATION BASIN LIQUID
X
(SIGNAfURE,OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Norwood, NC Total Dry Tons Applied (Annual):
Permit #: WQ0016247 Cation Exchange Capacity (non 503 only):
erator: Henry Anderson Owner: Anderson Living Trust Predominant Soil Series:
Acres Used: 12.8 Acres Permitted: 12.8 Site #: NC ST 00004 Field #:
3.45--7
Badin
ST 00004 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
2
8/20/19
3
4
5
6
7
8
9
10
11
12
% Solids
0.606
Arsenic
14
Cadmium
6.2
Copper
1
650
Chromium
92
Lead
150
Mercury
3
Molyb-
denum
42
Nickel 1
91
Selenium
22
Zinc
1900
Total
Phos-
—'torus
22000
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
'Non
...
1 111
ff, 1 1
MIT, 11
MIT, 11
ff#TITI1
1 111
Key, 11
MIT, 11
KIT, 11
E e
��
1 111���
111
1 111
1 111
ffIT, 11
1 111
i 111�
9
I #
i 111
�
KIT,me
KIT, 1i
,11
I Ii�
TotalPhos-
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
3risonme t for knowing violations".
/�/ - "---7 1 2 1z Z026
Signatur of an pplier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: NORWOOD, NC PREDOMINANT SOIL SERIES: BADIN
OWNER: ANDERSON LIVING TRUST PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 14.49
SITE #: NC ST 00004 FIELD# : ST 00004 0003 OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 6.90 ACRES PERMITTED: 6.90
Page
Line Applied ***
Date
Lbs/Ac
allons (G). or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
8/27/19
62,000.00 (G)
8985.5071
0.61
0.227
NOABL
MOIST
0-<1/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
Aug-19
62,000.00 (G)
8,985.507
I
8/30/19
68,200.00 (G)
1 9884.0581
2.00
0.824
SCUWSA
MOIST
0- 1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
Aug-19
68,200.00 (G)
9,884.058
I
9/3/19
86,800.00 (G)
12579.7101
2.00
1.049
SCUWSA
MOIST
0- 1/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
Sep-19
86,800.00 (G)
12,579.710
Total Gallons/Ac: 31,449.28
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS
Annual Ibs/acre
67
0.069
0.009
0.042
1.419
0.134
0.004
0.122
0.158
0.073
4.190 56.83
Cumulative lbs/acre
0.069
0.009
0.042
1.419
1 0.134
0.004
0.122
0.158
0.073
4.190
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
m
_.
163
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
�Aw
1339.0
267.9
15.0
375.0
89.0
2500.0
NOABL = NORWOOD, NC WWTP AERATION BASIN LIQUID
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
x 2 /2 2Q2p
(SIGN OF APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Stanly County Utilities/ Norwood, NC Total Dry Tons Applied (Annual): 14.49
mit #: WQ0016247 Cation Exchange Capacity (non 503 only):
_ erator: Henry Anderson Owner: Anderson Living Trust Predominant Soil Series: Badin
Acres Used: 6.9 Acres Permitted: 6.9 Site #: NC ST 00004 Field #: ST 00004 0003
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or1
Com-
posite
Date
1/8/19
2
8/20/19
3
4
5
6
7
8
9
10
11
12
% Solids
2 .
0.606
Arsenic
16.7
1 14
Cadmium
1.7
6.2
Copper
300
650
Chromium
0
92
Lead
17.7
150
Mercury
0.83
3
Molyb-
denum
27.6
42
Nickel
31.2
91
Selenium
16.7
22
Zinc
888
1900
Total
Phos-
torus
12500
22000
«.Inual Heavy Metal Field Loadings (Calculated in lbs/acre):
•..�.--
_
App.
Event
i I.
o ,e.
, e,
No I,�
I ���
o00
l f1
��
lmI,
�
fmo�
NOT, nw,
.on",",
oISKITIT,o
o ,I
�
l goo
o �o�
�e�
o oo�
���
��• ;
..
l
I Iii
I I
o 000
l fI
o poi
i o00
I ,o,
mm11
�
o loo�,
o 000
l oo�
o o� ,
NOT, ..
I I,
i o00
0 000
0 0��
o 000
0 000
0 goo
0 000
�
l ,�
a ,I
a ,Il�
m mm
lm10
�
I I
�
l ll
Nor, l�
l �e
� �
� �
� ��o
� ���
� ���
� goo
� iio
i ���
� ���
o ���
� ��o
o i�o
.-•� �
I III�
i IMF
o III�
o l
�
I III
III
I
- 1
I I.
I I
l l=1�
1 11�
1 11i
��
I I1�
I Iit
o ono
I III
ff, M,
��N
:.
goo
KITITIo
I III
WITITII
III#
;.
Total
Ph.
�.:
• •::
o o��
i o00
0 000
�o�
o 000
0 000
goo
0 000
0 000
goo
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
T -m aware that there are significant penalties for submitting false information, including the possibility of fines and
prisonment for knowing violations".
`L �120zo
Signature of Land A pli Date
nrKin re­innn nnm c+r /Aninnnn_\

FACILITY NAME: NORWOOD, NC
OWNER: ANDERSON LIVING TRUST
SITE #: NC ST 00004 FIELD# : ST 00004 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: BADIN
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 8.49
OPERATOR: HENRY ANDERSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.70 ACRES PERMITTED: 6.70
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/11/19
49,600.00 (G)
7402.9851
0.61
0.187
NOABL
MOIST
0-<1/2"
SUR
0.5
0.30
44,000. p
12,000.00 p
80.00 p
15680
FESCUE HAY
Sep-19
49,600.00 (G)
7,402.985
1
9/5/19
86,800.00 (G)
12955.2241
2.00
1.080
SCUWSA
I MOIST
0-<I/2"
SUR
0.5
0.30
52,200. p
1,320.00 p
95.90 p
16020
FESCUE HAY
Sep-19
86,800.00 (G)
12,955.224
1
1
1
1
Total Gallons/Ac: 20,358.21
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual lbs/acre
40
0.041
0.006
0.034
0.891
0.094
0.003
0.075
0.101
0.044
2.630 35.24
Cumulative lbs/acre
0.055
0.009
0.128
1.332
0.134
0.005
0.099
0.153
0.059
4.120
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
144
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
x
375.0
89.0
-
2500.0
r
NOABL = NORWOOD, NC WWTP AERATION BASIN LIQUID
SCUWSAEDL = STANLY COUNTY UTIL., NC WEST STANLY WWTP AEROB DIG LIQUID
X 2 12 2,0 20
(SIGNAT O D APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
K Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Stanly County Utilities/ Norwood, NC Total Dry Tons Applied (Annual): 8.49
mit #: WQ0016247 Cation Exchange Capacity (non 503 only):
erator: Henry Anderson Owner: Anderson Living Trust Predominant Soil Series: Badin
Acres Used: 6.7 Acres Permitted: 6.7 Site #: NC ST 00004 Field #: ST 00004 0005
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
1/8/19
2
8/20/19
3
4
5
6
7
8
9
10
11
�12
% Solids
2
0.606
Arsenic
16.7
14
Cadmium
1.7
6.2
Copper
300
650
Chromium
0
92
Lead
17.7
150
Mercury
0.83
3
Molyb-
denum
27.6
42
Nickel
31.2
91
Selenium
16.7
22
Zinc
888 1
1900
Total
Phos-
torus
12500
22000
_unual Heavy Metal Field Loadings (Calculated in lbs/acre):
..
-
D
-
• .
n
1:
1 •
Nor,
1 111
1 111
Willy,1
1 111
1 111
1 111
1 111
more 1
1 111
Min
1 1�
.Nll
1 11�
or,
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1111
•..-
1 .�:
1 �
1111
1111
1 111
1 111
1 111
1 111
1111
1 111
1 111
1111
1 :'
•� .
1 111
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 �
1 1 :
1 1 .
1 111
1 111
1 ill
1 111
1 111
1 111
1 111
1 111
ME1
1 111�
Mir,
1 11
or, 1
more 1
1 111
nor, 1
1 111
1 111
more 1
1 111
1 111
Mir, 1
Mir,
�
1 1.1
1 1 .
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
•-�
1 1.
1 1
1 111
Mr, 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1 .
1 11:
1 111
1 111
1 111
1 111
o.00vEMMI1
1 111
1 111
1 111
1 111�
.®
•
1 111
1 111
1 111
1 111
0.000
1 111
1 111
1 111
1 111
1 111
. •
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
g am aware that there are significant penalties for submitting false information, including the possibility of tines and
prisonment fo knowing violations".
Z[22ozo
Signature L App ' Date
nFniR FnRnn nnFi .qF (19i?nnn)

SECTION 4

PAR
PROMPT -ACCURATE- RELIABLE
LABORATORIES, INC
N%VNV PARLABS.CO111
REPORT OF ANALYSES
Attn: RONNIE OAKS
L&L ENVIRONMENTAL SERVICES LLC PROJECT NAME: APR 18
PO BOX 19491 DATE: 05/21/18
CHARLOTTE, NC 28219-9491
SAMPLE NUMBER- 131346 SAMPLE ID- TOWN OF NORWOOD WWTP SAMPLE MATRIX- SO
DATE SAMPLED- 04/17/18 TIME SAMPLED- 1500
DATE RECEIVED- 04/18/18 SAMPLER- DO RECEIVED BY- DJ
TIME RECEIVED- 1137 DELIVERED BY- DO TYPE SAMPLE- Grab
Page 1 of 3
ANALYSIS
ANALYSIS
METHOD
DATE
TIME
BY
RESULT
UNITS
AMMONIA NITROGEN
EPA
350.1
04/23/18
1036
CT
221
ppm
KJELDAHL NITROGEN
EPA
351.2
04/24/18
0907
CT
555
ppm
NITRATE/NITRITE
EPA
353.2
04/26/18
1243
CT
0.11
ppm
TOTAL PHOSPHOROUS
EPA
365.4
04/25/18
0959
CT
298
ppm
ALUMINUM, TOTAL
EPA
200.7.
05/21/18
1007
CT
279
ppm
ARSENIC, TOTAL
EPA
200.7
04/26/18
1405
DM
< 7.4
ppm
CALCIUM, TOTAL
EPA
200.7
05/21/18
1007
CT
146
ppm
CADMIUM, TOTAL
EPA
200.7
04/25/18
1141
CT
0.015
ppm
CHROMIUM, TOTAL
EPA
200.7
04/25/18
1331
CT
0.593
ppm
COPPER, TOTAL
EPA
200.7
04/24/18
1428
CT
5.52
ppm
MERCURY, TOTAL
EPA
245.2
04/23/18
1535
LM
1.5
ppm
POTASSIUM, TOTAL
EPA
200.7
05/21/18
1007
CT
65.7
ppm
MAGNESIUM, TOTAL
EPA
200.7
05/21/18
1007
CT
48.7
ppm
MOLYBDENUM, TOTAL
EPA
200.7
05/-17/18
0923
CT
0.142
ppm
SODIUM, TOTAL
EPA
200.7
05/18/18
1308
CT
29.4
ppm
NICKEL, TOTAL
EPA
200.7
04/26/18
0944
CT
1.10
ppm
LEAD, TOTAL
EPA
200.7
04/26/18
1143
CT
0.176
ppm
SELENIUM, TOTAL
EPA
200.7
04/26/18
1440
DM
< 8.9
ppm
ZINC, TOTAL
EPA
200.7
04/24/18
1139
CT
18.1
ppm
P.O. Box 411483 • Charlotte, NC 28241-1483
Plione: [phone] • Fax: [phone]

AIL
PA
PROMPT -ACCURATE- RELIABLE
1,ABOI2AT0IZIES, INC
WNV%V PARLABS.CODI
Page 2 of 3
CONTINUATION OF DATA FOR SAMPLE NUMBER 131346
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
TCLP CHARACTERISTICS
TCLL'
U4/27/18
1802
JK
pH VALUE
TCLP
04/27/18
1802
JK
7.1
S.U.
CORROSIVITY
TCLP
04/27/18
1802
JK
NON
REACTIVITY
TCLP
04/27/18
1802
JK
REACTIVE CYANIDE
TCLP
04/27/18
1802
JK
< 0.78
ppm
REACTIVE SULFIDE
TCLP
04/27/18
1802
JK
55.0
ppm
FLASH POINT
TCLP
04/27/18
1802
JK
> 200
degrees F
IGNITABILITY
TCLP
04/27/18
1802
JK
NON
PAINT FILTER TEST
TCLP
04/27/18
1802
JK
FL
TCLP METALS
TCLP
04/26/18
1610
DM
ARSENIC
TCLP
04/26/18
1610
DM
< 0.5
ppm
BARIUM
TCLP
04/26/18
1610
DM
< 10
ppm
CADMIUM
TCLP
04/26/18
1610
DM
< 0.1
ppm
CHROMIUM
TCLP
04/26/18
1610
DM
< 0.5
ppm
LEAD
TCLP
04/26/18
1610
DM
< 0.5
ppm
MERCURY
TCLP
04/26/18
1610
DM
< 0.02
ppm
SELENIUM
TCLP
04/26/18
1610
DM
< 0.1
ppm
SILVER
TCLP
04/26/18
1610
DM
< 0.5
ppm
TCLP PESTICIDES
TCLP
05/01/18
1256
KL
ENDRIN
TCLP
05/01/18
1256
KL
< 0.002
ppm
LINDANE
TCLP
05/01/18
1256
KL
< 0.04
ppm
METHOXYCHLOR
TCLP
05/01/18
1256
KL
< 1
ppm
TOXAPHENE
TCLP
05/01/18
1256
KL
< 0.05
ppm
CHLORDANE
TCLP
05/01/18
1256
KL
< 0.003
ppm
HEPTACHLOR (AND ITS EPDXIDE)
TCLP
05/01/18
1256
KL
< 0.0008
ppm
TCLP HERBICIDES
TCLP
05/03/18
1337
EM
2,4-D
TCLP
05/03/18
1337
EM
< 1
ppm
2,4,5-TP(SILVEX)
TCLP
05/03/18
1337.EM
< 0.1
ppm
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]
:# r

P AM
PROMPT' ACLU RATE- RELIABLE
1,ASC)RA.,r0pl ESy INC
AV1V'XV.PARLABS.00Ai
Page 3 of 3
CONTINUATION OF DATA FOR SAMPLE NUMBER 131346
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
TC . P ORGANICS
TC7
i �.��i
1141i;V
BENZENE
TCLP
05/04/18
1141
MV
< 0.05
ppm
CARBON TETRACHLORIDE
TCLP
05,./04/18
1141
MV
< 0.05
ppm
CHLOROBENZENE
TCLP
05/04/18
1141
MV
< 10
ppm
CHLOROFORM
TCLP
05/04/18
1141
MV
< 0.6
ppm
o—CRESOL
TCLP
05/04/18
1141
MV
< 20
ppm
p—CRESOL
TCLP
05/04/18
1141
MV
< 20
ppm
m—CRESOL
TCLP
05/04/18
1141
MV
< 20
ppm
1,4—DICHLOROBEIA]ZENE
TCLP
05/04/18
1141
MV
< 0.75
ppm
1,2—DICHLOROETHANE
TCLP
05/04/18
1141
MV
< 0.05
ppm
1,1.—DICHLOROETHYLENE
TCLP
05/04/18
1141
MV
< 0.07
ppm
2,4—DINITROTLUENE
TCLP
05/04/18
1141
MV
< 0.013
ppm
HEXACHLOROBENZENE
TCLP
05/04/18
1141
MV
< 0.013
ppm
HEXACHLOROBUTDIENE
TCLP
05/04/18
1141
MV
< 0.05
ppm
HEXACHLOROETHANE
TCLP
05/04/18
1141
MV
< 0.3
ppm
METHYL ETHYL KETONE
TCLP
05/04/18
1141
MV
< 20
ppm
NITROBENZENE
TCLP
05/04/18
1141
MV
< 0.2
ppm
PENTACHLOROPHENOL
TCLP
05/04/18
1141
MV
< 10
ppm
PYRIDINE
TCLP
05/04/18
1141
MV
< 0.5
ppm
TETRACHLORETHYLENE
TCLP
05/04/18
1141
MV
0.0926
ppm
TRICHLOROETHYLENE
TCLP
05/04/18
1141
MV
< 0.05
ppm
2,4,5-TRICHLOROPHENOL
TCLP
05/04/18
1141
MV
< 40
ppm
2,4,6-TRICHLORPHENOL
TCLP
05/04/18
1141
MV
< 0.2
ppm
VINYL CHLORIDE
TrLF
05/04/18
1141
MV
<. 0.02
ppm
LABORATORY DIRECTOR 4' •� ,-.._.� �l —
P.O. Boa 411483 > Charlotte. NC 29241-1483
Phone: [phone] ^ Fax: [phone]
mmmmwmu0

PAFZ
PROMPT -ACCURATE- RELIABLE
J�tLB®P,A-rC)R)'ES, IWC
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN OF CUSTODY
Phone [phone]
Fax [phone]
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Carolina Department of Environmental and Natural Resources,
Company Name (billing) Comments/ Special Instructions
LItL ENVIRONMENTAL SERVICES LLC
Address
PO BOX 19491
City, State Et zip code
CHARLOTTE, NC 28219-9491
Point of Contact Et Telephone Number
RONNIE OAKS 704-332-0911
Sample
Taken By: SIGNATURE _
PRINTED NAME /,)&, ¢:-,- 0, jCJ
ARE SAMPLES FOR STATE or EPA REPORTING? YES NO
'Sample Type: DW WW GWMW HW Soil Other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN):
Bent Sample I:D,
(Sample.Location / Number)
Comp
Grab
Preserv.
Set Up
Dater Pme
Collection
Datelrime
nalyse's
Requested
ro"'t 0c Yo". �t
L/ f l7//
FULL TCLP
NH3, TKN, NO2+NO3, TP04,
s, Cd, Cr, Cu, Hg, Ni, Pb,
Se, Zn A i- e CA , /lAo
KNA
nu
snetl by: Date/Time Received by: Date/Time
Relinquished by: Datelrime Received by: Daterrime
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

Lysa Finnerty
From: Adam Brigman
Sent: Friday, February 7, 2020 9:11 AM
To: Lysa Finnerty, Derrick Shivar; Nate Roth
Subject: Fwd: [External] Norwood WWTP Land Application
Sent from my iPhone
Begin forwarded message:
From: "Schutte, Maria" <[e-mail]>
Date: May 20, 2019 at 4:46:53 PM EDT
To: Nate Roth <[e-mail]>
Cc: Adam Brigman <[e-mail]>, "Pitner, Andrew" <[e-mail]>, "Doby,
Troy" <[e-mail]>
Subject: RE: [External] Norwood WWTP Land Application
Nate,
Per our conversation and your confirmation in this email that "new" material was NOT introduced,
sampling results are representative and additional application activity from the Norwood WWTP is not
anticipated this year. Yes, I am okay with proceeding with the data you have submitted and confirmed
with Troy Doby (Central Office). However, should excessive odors or vectors be detected upon
application additional "PVAR" testing may be warranted.
Please include a copy of this email in the 2019 Annual Report with the 2018 data for this facility.
And finally, have Adam send me an update when he knows the specific field and date of application.
Thank you,
Maria
From: Nate Roth [mailto:[e-mail]]
Sent: Monday, May 20, 2019 1:28 PM
To: Schutte, Maria <[e-mail]>
Cc: Adam Brigman <[e-mail]>
Subject: [External] Norwood WWTP Land Application
Maria,
As a follow up to our conversation Friday, I would like to confirm that the samples used to add Norwood
WWTP as a source to the Synagro Western Piedmont permit can be used for this upcoming application
event?

The material that was analyzed to verify permit requirements has not been altered or added to since
testing and is representative of the material currently.
Please reply with approval.
Nate
Nate Roth
Technical Services Manager
284 Boger Road, Mocksville, NC, 27028
0: 1-336-790-1610 1 M: 1-336-403-4324
rroth(a-)-SYNAGRO.com I synagro.com
Facebook I Twitter I Linkedin
4
gff A:
�i
FA
Adam Brigman
Technical Services Specialist
1005 Goodman Circle I, Gastonia, NC, 28134
0: 1-828-447-4753 1 M: 1-704-650-4341
[e-mail] I synagro.com
Facebook I Twitter I Linkedin

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Monitoring Period
Norwood WWTP
Norwood WWTP
From 01/01/2019
WQ Permit Number:
NPDES Number:
To 12/31/2019
WQ0016247
NCO021628
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annUrnhle to nitern ntive nerfnrmad (Glace A nr Clace M rmmnlntP tha fnllnwina mnnifnr:na data•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 h
MPN
Coliform
power per gram
MPN/g
Grab
SM9221 C
of total solids
CFU
60,000
83,432
197,451
CFU/g
0
Annually
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying —Unstable)
Option/Alt. 9
Option/Alt: 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. aware that there are significant penalties for false certification including fine and imprisonment."
Scb w0v& ( d� X%A ' _►ti1%nk �z I1a(()�-
Preparer Name and Title Or r��
or print) Land Applier Name and Title (if applicable) (type or print)
v i`a0
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Norwood
Lot Number:T105074
Date Completed:09/12/2018
09/12/2018 3:43 PM
Approved and released by:
Project Manager: Lucas Odom
PUR��
-
`geORASO
ACCREDITED
op---A—
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: T105074
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Geometric Mean
83,432
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

Client:Synagro Laboratory ID:TI05074-001
Description: NORWOOD 2018 FECAL #1 Matrix: Solid
Date Sampled:09/05/2018 0800 % Solids: 1.51 09/06/2018 0123
Date Received:09/05/2018
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 3000 09/06/2018 2045 SA1 09/05/2018 1553
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 66260 60000 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
Daly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

Client:Synagro Laboratory I D: T105074-002
Description: NORWOOD 2018 FECAL #2 Matrix: Solid
Date Sampled:09/05/2018 0800 % Solids: 2.54 09/06/2018 0123
Date Received:09105/2018
Inorganic non-metals
Lin Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 3000 09/06/2018 2045 SA1 09/05/2018 1553
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D-200 ND 60000 col/g 1
Footnote(s): '<39327 CFU/g
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Synagro Laboratory ID:T105074-003
Description: NORWOOD 2018 FECAL #3 Matrix: Solid
Date Sampled:09/05/2018 0800 % Solids: 2.91 09/06/2018 0123
Date Received:09105/2018
Inorganic non-metals
'un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 3000 09/06/2018 2045 SA1 09/05/2018 1553
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D-200 ND 60000 col/g 1
Footnote(s): "<34319 CFU/g
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
. -aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Synagro Laboratory ID:TI05074-004
Description: NORWOOD 2018 FECAL #4 Matrix: Solid
Date Sampled:09/05/2018 0800 % Solids: 2.47 09/06/2018 0123
Date Received:09/0512018
Inorganic non-metals
Lin Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 3000 09/06/2018 2045 SA1 09/05/2018 1553
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D-200 ND 60000 col/g 1
Footnote(s): *<40466 CFU/g
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Synagro Laboratory ID:TI05074-005
Description: NORWOOD 2018 FECAL #5 Matrix: Solid
Date Sampled:09/05/2018 0800 % Solids: 3.31 09/06/2018 0123
Date Received:09105/2018
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 3000 09/06/2018 2045 SA1 09/05/2018 1553
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 165968 60000 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 12

Client:Synagro Laboratory ID:TI05074-006
Description: NORWOOD 2018 FECAL #6 Matrix: Solid
Date Sampled:09/05/2018 0800 % Solids: 2.79 09/06/2018 0123
Date Received:09/05/2018
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 3000 09/06/2018 2045 SA1 09/05/2018 1553
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D- 197451 60000 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8of12

Client:Synagro Laboratory ID:TI05074-007
Description: NORWOOD 2018 FECAL #7 Matrix: Solid
Date Sampled:09/05/2018 0800 % Solids: 1.72 09/06/2018 0123
Date Received:09/0512018
Inorganic non-metals
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 3000 09/06/2018 2045 SA1 09/05/2018 1553
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF SM 9222 D-200 ND 60000 col/g 1
Footnote(s): "<58278 CFU/g
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
Out of holding time W = Reported on wet weight basis
aly Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

Chain i Custody
and '
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

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Slairaly Environmental Services, Inc.
14G Vantage Point Drive
West Columbia, South Caraiina 20172
Telephcre ,1o. {603) 7E,1-97CD Fax ND. (803)791-Q1 11
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SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Hnriranmrcint G miP, s. ine.
rhxu1nmi Atimher mimi-:I119C-14
Sample Receipt Check-li ti )
Client: i t Cooler Inspected by date_ �`'! +� T r,l �i-
P.�r;e
6afrcdw talc: $r; 3G1S
ivleus of l'eccipt: ErrSSEST e Li C:lieni EI UPS IJ i edEx LJ C11her. ---
LI Yes
I . '.lien: custody sca13 present ott rise ceder?
El YeS
l_J Nrl
l_ N:i 2. If L`t8Stg&y seals were I}reseur Veere ilrey intact and unbroken'
pH Strip ID: _ (.:hlorine Strip 1D: 'rested by: '
Origiul ten dd eralmit uprin rrc ,1�4 i Derived (C'or-we; :J) tcmpurawre upon receipt: %Solid Snap-C'up ley: /I `,F
Aietliod: Terripvraturr Blank ° ±Against bottles IR Gun It)- IR Chun Corwrtion Factor: T
r
11[ethad irI 4r�u"stint; i�'et Ice p Ice Vicky. d Dry Ice None
Yes
0 Nol
1� �;rl
3. If (L pCraturc of my cooler rxrc;ded 6.0' , %vas Pi0ject i briagur Mitified?
PM was Notified by: phone r email i fhrr.-to-face (circle ot:e).
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A
4. It the urmmrrclial vourlel's paclklnr slip a.ttr']chGd to this for'ril"
❑ Nu
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S. Crum pr,.par custody procedure (r-clinquisl,rd+rcceived) fullc%ved?
'es
6. l ere sa.nple IDs li;+tril un the COC?
`
IJ No
?. Were sample IL,s fisted on all sample contairiars?
Yes
f _ 9 N11
8. 'VV4s coller:tion date � time listed o,i llte COC?
1. ''r'es
_' No
q_ Was cokctian dore & time lixlcci on all sample containers?
ff 't'cs
01 No
10_ Did all Wnlainer Int;al urfainna.ton (1D. date, time) a_uw with idle COC?
D'Yes
Ll No
11. Wem tests to b-_ perforomd liswd cm the COC.?
���CS
El NO
—
12. Dirl all Samples arrive in the prap�-.r containei; for ear;lt test andrirr in good condition
(wlbrr}ken, lids un,
El Yes
D N-n
12. IV-11 A&quatc sample volowe avaiiublc?
No
_12'
_
id. Were all srtnples reccivcd within r_ the 1101ding time or 4K Irolrrs, whichever conies First?
` YD
15, wcra anl: samples containers InissinVexce$!� (ciri lc uric) sumplcs Not listed on CO
Cl ies
N°
'�'
16. Far VOA and RSK- l r5 samplcs,. veci•e bubbleprascnt }"pea size" ('4a'oc Groin in diarrtrtcr) in
anty of the VOA vials?
ED Yes
L1 No
N,�
17. 1k ere aJl ©1�Cz+etal5?nutrient samples received at a pH of -: 7.9
rn
'D lies
D No
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19. V-Ve all iyanidc sainple_s received at a pH > 1? and sulfide sumplus mccived at a pll > g?
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U Yes
No
[ILIA
20, Were client remark rre!quus.F3 (i.c, rcquesred dilutions, A�€.&M.SD desigiatiens, etc.._)
concfrosts d aly transer Ibed he (OU into thr Co711111eAll SeeLiou to LEMS?
7 �Y
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ku
ail. V4-M the qljole number listed on thi- container label? If yes, ouote 4,
Sample P1-eserv2tE0n {Nh]RI. 115 uorupk.ted f,%r arty "szntlyle(s) incorrectly preserved Dr with bcadsp ice.)
Sample(s) _._ w6re rtc;cive,d into reztly preserved rind vrerr arljrrsird accordingly
its Saniplt:r.'..ccivilrg with MI. cifeirrlr-onr: llLtiCt; IEN03, NCI, NaOR using SR 4
I-ime ofprCsuvaticn 11more'than one preservauve is n.Cdad, please-,icrle in the c nninclits lx.lo,v,
Sanlple(s} werr. ruck-ed WiTh b1lbbles = 6 mm in diameter.
S;,rrrplcs(s} _ 'Were receive] Willi T RC -- 0..i myL (lf'�19 is eta) and werc
adjrlsted accordin gly in mmpkt. receiving with .sodium thiosulFate I?]a,S,C7,) wish Shealy W:
SR harzodf. hibcls applied by. --�- Date:-- -
comments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

Pbk
PROMPT- A CCU RATE -RELIABLE
LABORATORIES, INC
WWW.PARLABS.00IN1
REPORT OF ANALYSES
Attn: ADAM BRIGMAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: SEP 18
DATE: 10/15/18
SAMPLE NUMBER-
133183
SAMPLE ID- NORWOOD
SAMPLE MATRIX- SO
DATE SAMPLED-
09/05/18
TIME SAMPLED- 0815
DATE RECEIVED-
09/05/18
SAMPLER- AB
RECEIVED BY- DJ
TIME RECEIVED-
1020
DELIVERED BY- AB
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD DATE TIME BY
RESULT UNITS
30 DAY BENCH SCALE
TEST
VAR 09/05/18 1320 RE
6.92 %
LABORATORY DIRECTOR
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]

p A�R
PROM PT•AC CU RATE- RELIABLE
LABORATORIES INC
WWW.PAP,LASS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
CLIENT NAME: f
-SAMPLE ID:. I
' •
• ' • • •
SAMPLE #: I
;START DATE:
.
,END DATE:
Start: End:
TS ()
0.2078
0.1997
TS%
2.00%
1.95%
VS ()
0.1007
0.0926
VS%
48.46%
46.37%
y Mass Fraction of Volatile Solids in Liquid Sludge
0.0097140
0.0090412
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0103314
0.0104569
FSVR (Mass Balance)
6.98%
FSVR (Van Kleeck)
6.92%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: [phone] Fax: [phone]

PbLR
PRCMP- AC CURATE• RELIABLE
LABORATORIES, INC
W W W.PARLASS.COM
30 ®ay Bench Scale Extended Aeration Test
vHK Vptlorl 3, t'erceni Volatile JOIIas t(eouctlon
SYNAGRO
NORWOOD
133183
09/05/18
10/03/18
As Received Day 0 Day 7 Day 14 Day 21 Day 28
Collected 09/05/18 09/05/18 09/12/18 09/19/18 09/26/18 10/03/18
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge W
(g)
Oven Temp °C
Date/Time In
Date/Time Out
Dried Sample W
+ Tare Wt (g)
Dried Sludge Wt (g;
Fixed Solids Wt (g;
Furnace Temp °C
Date/Time In
Date/Time Out
Burned Sample
Wt + Tare Wt (g)
Volatile Solids Wt (g)
TS%
VS%
X12
X12
X10
X13
X11
X15
19.3049
19.3049
22.7067
21.8725
22.6246
1 23.1817
29.6714
29.6714
31.5349
31.0344
32.0454
33.4237
10.3665
10.3665
8.8282
9.1619
9.4208
10.2420
106
106
107
106
106
106
09/05/18 13:20
09/05/18 13:20
09/12/18 08:40
09/19/18 09:00
09/26/18 10:00
10/03/18 09:20
09/06/18 12:30
09/06/18 12:30
09/13/18 09:00
09/20/18 09:15
09/27/18 10:00
10/04/18 09:30
19.5127
19.5127
22.8797
22.0530
22.8074
23.3814
0.2078
0.2078
0.1730
0.1805
0.1828
0.1997
0.1071
0.0906
0.0953
0.0972
0.1071
550
550
550
550
550
09/06/18 14:50
09/13/18 13:30
09/20/18 14:20
09/27/18 14:30
10/04/18 13:30
09/06/18 16:00
09/13/18 14:30
09/20/18 15:15
09/27/18 15:30
10/04/18 14:50
19.4120
22.7973
21.9678
22.7218
23.2888
0.1007
0.0824
0.0852
0.0856
0.0926
2.00%
2.00%
1.96%
1.97%
1.94%
1.95%
48.46%
47.63%
47.20%
46.83%
46.37%
yf Mass Fraction of volatile Solids in Liquid (Feed)
Sludge at Start of Test
0.0097140
yb Mass Fraction of Volatile Solids in Liquid (Bottom)
Sludge at End of Test
0.0090412
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
at Stan of Test
0.0103314
Xb Mass Fraction of Fixed Solids in Liquid (Bottom)
Sludge at End of Test
0.0104569
TS ()
0.2078
TS (g)
0.1997
VS (g)
1 0.1007
VS g) 1
0.0926
Volatile Fraction In: I 0.24230
P.O. Box 4114S3 • Charlotte, NC 28241.1483
Phone: [phone] s Fax: [phone]
Volatile Fraction Out: 1 0.23779

L
AA' CHAIN OF CUSTODY
BORATORIES.WC.
PAR Laboratories, Inc
Phone [phone]
www.pariabs.com Fax [phone]
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain or Custody document for acceptance by PAR Laboratories. Inc. and the North
rar.,rna rl—rf—t and Nat,,-f Rncnurrwe
Company Name (billing)
Commentsf Special Instructions
Clarifier Effluent provided in the event that
SYNAGRO CENTRAL
Address
the sample needs to be reduced to below
12701 LANCASTER HWY
2% solids.
City, State It zip code
PINEVILLE NC 28134
Point of Contact fs Telephone Number
ADAM BRIGMAN 704-650-4341
Sample
Taken By:
SIGNATURE
PRINTED NAME��� �i�y
ARE SAMPLES FOR STATE or EPA REPORTING? YES -- NO
'Sample Type: DW VWtf GWMW HW Soil other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN):
Client Sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Daterrime
Collection
DateMme
Analyses
Requested
04 6el1f h
Relinquis ed Date/T me Keceivea b uarel I Ime
9 3 ix - to :zD 0 OS o ao
Resin a by: Daterrime Received by: Datemme
' C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project: Norwood
Field Grower Soil
Lime Re uirement Tons/AcreI Dat7el Total::]
(state -county -site -field)
from soil anal sis A lied Appli-e—d1l Acres
NC-ST-04-01 !FH—eneryAnderson 6.5
0.0 0.0 26.8
NC-ST-04-02 Henery Anderson 6.6
0.0 0.0 12.8
NC-ST-04-03 H—en er Anderson 6.5
0.0 r 0.0 6.9
NC-ST-04-05 IFH—enery Anderson]=1
0.0 1 0.0 11 ir 6.7
# lime has been ordered but not spread

SECTION 7

Page 1 of 1
Report No: 20-021-1021
Account No: 46441
Advisor: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
Waypoint
ANALYTICAL
Client: Henry Anderson
West Stanley
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-ST-04
Date Received: 01/21/2020
Date of Report: 01/22/2020
Lab No Field'ID
Sample ID
Soil Class
HM% W/V
pH
A"c
P-1
K /
S-1
Mn.'-1
Zn-1
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO N
03185
04-01
MIN
2.0
6.5
0.3
1
9
212,
38
18
18
18
4.6
- 92
60
30
1.7
0.1
03186
04-02
MIN
2.0
6.6
0.3
2
10
154
50
20
20
25
4.7
94
62
30
1.8
0.1
03187
04-03
MIN
2.0
6.5
0.4
2
16
64
75
40
40
50
5.2
93
61
29
1.8
0.1
03188
04-05
MIN
2.0
6.5
0.4
2
16
60
81
43
43
50
5.5
92
61
29
1.7
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.