WQ0016247_Regional Office Historical File Pre 2018 (10)

RECEIVEO/NCQENRIDWR
435 Williams Court, Suite 100
Baltimore, MD 21220
Nvwwsynagro.coin
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center .
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0016247
Dear NCDEQ:
WQROS
S
YNAG Ro REGIONAL OFFICE
Synagro is submitting one copy and one electronic copy of the above referenced report as
required by Synagro Central, LLC's land application of Class B residuals permit. Residuals
from the City of Statesville, Town of Columbus, Town of Granite Falls, Norwood and Stanly
County Utilities were applied in 2019.
If you have any questions or need additional information, please do not hesitate to contact Nate
Roth at336-403-4324.
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Nate Roth - Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00016247 County Alexander Year 201'9
Facility Name (as shown on permit) West Stanly WWTP City of Statesville. Third Creek WWTP, Fourth Creek WWTP, Columbus
WWTP Granite Falls WWTP, Granite Falls WTP & Norwood WWTP NPDES No. NC0043532, NC0020591, NC0031836,
NC0021369, NC0021890, NCO082546 & NCO021628
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 54
Total number of fields utilized for land application during the year: 22
Total amount of dry tons applied during the year for all application sites: 1035.01
Total number of acres utilized for land application during the year: 347.3
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations." �
Robert Roth, Technical Services Mana er%4/%
Permittee Name and Title (type or print) Signature of PerAitA e
Signature of Preparer* Date Signatu o` !7and Appli&J . + D
(if different from Permittee) (if different from ermittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

CITY OF STATESVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0016247
2019 ANNUAL REPORT

City of Statesville, NC
Residuals Land Application Program
2019 Annual -Report
TABLE OF CONTENTS
1. Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR
Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
STATESVILLE, NG
STATESVILLE, NC FOURTH CREEK CAKE
1TiCi1 I
February 2019
April 2019
May 2019
June 2019
July 2019
September 2019
October 2019
YEARLY TOTAL
DRY METRIC
AMOUNT
UNIT
DRY TONS
UNIT
TONS
1,470.00
Y
154.78
D
140.36
1,072.00
Y
109.25
D
99.09
180.00
Y
18.35
D
16.64
860.00
Y
87.65
D
79.48
525.00
Y
53.50
D
48.53
1,300.00
Y
132.48
D
120.17
75.00
Y
7.83
D
7.10
5,482.00
Y
563.84
D
511.37
STATESVILLE, NC THIRD CREEK CAKE
DRY METRIC
MONTH/YEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
May 2019
30.00
Y
3.89
D
3.53
June 2019
1,325.00
Y
171.86
D
155.87
July 2019
530.00
Y
68.74
D
62.35
September 2019
225.00
Y
29.19
D
26.46
October 2019
410.00
Y
45.93
D
41.66
YEARLY TOTAL
2,520.00
Y
319.61
D
289.87
2/4/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO031836
or WQ# (residual only)
WWTP Name: FOURTH CREEK
Residuals Analysis Data
Product Type CAK CAK
Date Sampled (grab) or 01/07/19 04/03/19
Date Composited
Percent Solids 12.50 12.10
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
Laboratory
PACE ANALYTICAL SERVICE INC.
Waypoint Analytical Virginia Inc.
CAK CAK
08/28/19 10/29/19
12.40 17.30
<6.3
<5
<5
6.42
3.2
1.59
3.27
9.6
0.5
0.329
0.472
0.601
NR
37.3
56.1
113
366
203
268
355
25.3
18.3
34.4
94.2
12.7
6.6
10.9
21.8
32
28.6
33
51
<6.3
5.91
<5
5.73
772
579
624
1100
27200
23500
24300
21600
47500
64900
52300
53100
10200
4960
15300
1090
<15.2
42.9
<4.63
78.6
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significar perplties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X LK !A� V V Ww � Date M4 IU ( a'(J VK1/
(SIGNATURP OF PREPARER)
DENR FORM RSSF (5/2003) Printed: Tuesday - February 4, 2020 at 18:17:02 for: 2084 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number
WQ0016247 Laboratory
Facility Name
STATESVILLE, NC PACE ANALYTICAL SERVICE INC.
NPDES#
NCO031836 Waypoint Analytical Virginia Inc.
or WQ# (residual only)
WWTP Name
FOURTH CREEK
Residual Analysis Data
Product Type
CAK
CAK
CAK
CAK
Date Sampled
01/07/19
04/03/19
08/28/19
10/29/19
Date Composited
Percent Soilds
12.50
12.10
12.40
17.30
PARAMETERS (mg/kg dry weight)'
Aluminium
30800
29100
24700
17100
Calcium
11000
8570
61800
12400
Magnesium
4560
3170
2940
2550
pH
8.00
7.40
7.80
5.90
Potasium
5580
4940
3070
2710
Sodium
<3160
749
571
780
PAN
16305
20505
18755
16224
SAR
2.2526
0.6087
0.2141
0.6914
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitti fal information, inclu ing the possibility of fines and imprisonment for knowing violations."
X Date p2 ,,7
(SIGNATUR y
OF PREPARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/5/2020 10:44:31 AM

aceAnalytical
wmpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 18, 2019
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
RE: Project: Statesville (4th Creek)
Pace Project No.: 92413565
Dear Erik Bruce:
Enclosed are the analytical results for sample(s) received by the laboratory on January 10, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
c: � ea L, v, - 1
Lord Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
NCCRFO,
NI
l,9BORA'�D�J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 18

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Statesville (4th Creek)
Pace Project No.: 92413565
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville,_NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Statesville (4th Creek)
92413565
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92413565001
4th Creek WWTP
EPA 601OD
DS
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 254OG-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA9045D
SMK
1
PASI-A
SM 271OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA365.1 Rev 2.01993
MFO
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 18

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Statesville (4th Creek)
Pace Project No.: 92413565
Sample: 4th Creek WWTP Lab ID: 92413565001 Collected: 01/07/19 09:00 Received: 01/10/19 09:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7471 Mercury
Mercury
i40G Total Percent Solids
)tal Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Date: 01/18/2019 03:00 PM
Analytical Method: EPA 601OD Preparation Method: EPA 3050E
30800
mg/kg
63.3
1
01/14/1910:15
01/15/1915:01
7429-90-5
ND
mg/kg
6.3
1
01/14/1910:15
01/15/1915:01
7440-38-2
3.2
mg/kg
0.63
1
01/14/1910:15
01/15/1915:01
7440-43-9
11000
mg/kg
63.3
1
01/14/1910:15
01/15/1915:01
7440-70-2
366
mg/kg
3.2
1
01/14/1910:15
01115/1915:01
7440-50-8
25.3
mg/kg
3.2
1
01/14/1910:15
01/15/1915:01
7439-92-1
4560
mg/kg
63.3
1
01/14/1910:15
01/15/1915:01
7439-95-4
12.7
mg/kg
3.2
1
01/14/1910:15
01/15/1915:01
7439-98-7
32.0
mg/kg
3.2
1
01/1411910:15
01/15/1915:01
7440-02-0
5580
mg/kg
3160
1
01/14/1910:15
01/15/1915:01
7440-09-7
ND
mg/kg
6.3
1
01/14/1910:15
01/15/1915:01
7782-49-2
ND
mg/kg
3160
1
01/14/1910:15
01/15/1915:01
7440-23-5
772
mg/kg
6.3
1
01/14/1910:15
01/15/1915:01
7440-66-6
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
0.50 mg/kg 0.036 1 01/17/1916:00 01/18/1910:47 7439-97-6
Analytical Method: SM 2540G-2011
12.5 % 0.000010 1 01/10/1917:24
Analytical Method: ASTM D2974-87
87.5 % 0.10 1 01/10/1917:18
Analytical Method: EPA 9045D
8.0 Std. Units 0.10 1 01/15/19 10:44 H3
Analytical Method: SM 271OB-2011
16300 mg/kg 0.12 1 01/15/1917:46 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
10200 mg/kg 486 10 01/12/1910:40 01/12/1916:30 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
47500 mg/kg 3320 10 01/14/19 11:34 01/15/19 06:00 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 15.2 1 01/11/19 22:50 01/12/19 03:29
ND mg/kg 15.2 1 01/11/19 22:50 01/12/19 03:29 14797-55-8
15.9 mg/kg 7.6 1 01/11/19 22:50 01/12/19 03:29 14797-65-0
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
27200 mg/kg 399 50 01/14/19 19:23 01/14/19 23:23 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (4th Creek)
Pace Project No.: 92413565
QC Batch: 452998 Analysis Method: EPA 7471B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Associated Lab Samples: 92413565001
METHOD BLANK: 2475568 Matrix: Solid
Associated Lab Samples: 92413565001
Blank Reporting
Parameter Units Result Limit Analyzed
Mercury mg/kg ND 0.0060 01118/1910:36
Qualifiers
LABORATORY CONTROL SAMPLE: 2475569
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.068 81 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2475570 2475571
MS MSD
92414199001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
ercury mg/kg ND 0.071 0.071 0.036 0.037 50 50 75-125 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 18

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (4th Creek)
Pace Project No.: 92413565
QC Batch: 452237 Analysis Method: EPA 6010D
QC Batch Method: EPA3050B Analysis Description: 6010 MET
Associated Lab Samples: 92413565001
METHOD BLANK: 2472599 Matrix: Solid
Associated Lab Samples: 92413565001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Aluminum
mg/kg
ND
10.0
01/15/1913:19
Arsenic
mg/kg
ND
1.0
01/15/1913:19
Cadmium
mg/kg
ND
0.10
01/15/1913:19
Calcium
mg/kg
ND
10.0
01/15/1913:19
Copper
mg/kg
ND
0.50
01/15/1913:19
Lead
mg/kg
ND
0.50
01/15/1913:19
Magnesium
mg/kg
ND
10.0
01115/1913:19
Molybdenum
mg/kg
ND
0.50
01/15/1913:19
Nickel
mg/kg
ND
0.50
01/15/1913:19
Potassium
mg/kg
ND
500
01/15/1913:19
Selenium
mg/kg
ND
1.0
01/15/1913:19
Sodium
mg/kg
ND
500
01/15/1913:19
Zinc
mg/kg
ND
1.0
61/15/1913:19
_ABORATORY CONTROL SAMPLE:
2472600
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
Aluminum
mg/kg
500
524
105
80-120
Arsenic
mg/kg
50
49.2
98
80-120
Cadmium
mg/kg
50
51.9
104
80-120
Calcium
mg/kg
500
537
107
80-120
Copper
mg/kg
50.
53.5
107
80-120
Lead
mg/kg
50
51.9
104
80-120
Magnesium
mg/kg
500
517
103
80-120
Molybdenum
mg/kg
50
55.1
110
80-120
Nickel
mg/kg
50
52.9
106
80-120
Potassium
mg/kg
500
527
105
80-120
Selenium
mg/kg
50
47.8
96
80-120
Sodium
mg/kg
500
550
110
80-120
Zinc
mg/kg
50
50.9
102
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472601
2472602
MS
MSD
92413393001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits RPD Qua]
Aluminum
mg/kg 3270
363
368
7520
7880 1170 1250
75-125 5 M1
Arsenic
mg/kg ND
36.3
36.8
32.0
33.2
84 86
75-125 4
Cadmium
mg/kg ND
36.3
36.8
32.1
32.7
88 89
75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (4th Creek)
Pace Project No.: 92413565
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472601
MS
92413393001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2472602
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qua[
Calcium
mg/kg
396
363
368
642
665
68
73
75-125
4 M1
Copper
mg/kg
6.9
36.3
36.8
33.6
34.1
74
74
75-125
1 M1
Lead
mg/kg
5.8
36.3
36.8
39.4
39.0
92
90
75-125
1
Magnesium
mg/kg
1030
363
368
1470
1580
122
149
75-125
7 M1
Molybdenum
mg/kg
ND
36.3
36.8
31.6
32.3
87
87
75-125
2
Nickel
mg/kg
8.4
36.3
36.8
44.5
45.4
99
100
75-125
2
Potassium
mg/kg
1170
363
368
2540
2720
379
422
75-125
7 M1
Selenium
mg/kg
ND
36.3
36.8
28.6
28.3
79
77
75-125
1
Sodium
mg/kg
ND
363
368
ND
ND
90
90
75-125
Zinc
mg/kg
23.3
36.3
36.8
64.7
66.6
114
118
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Statesville (4th Creek)
Pace Project No.: 92413565
QC Batch: 451857
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92413565001
SAMPLE DUPLICATE: 2470825
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2470826
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92413658013 Dup
Units Result Result
% 9.9 9.5
92413607001 Dup
Units Result Result
% 36.2 40.1
RPD Qualifiers
4
RPD Qualifiers
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18

acmnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (4th Creek)
Pace Project No.: 92413565
QC Batch: 452172 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92413565001
SAMPLE DUPLICATE: 2472426
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2472427
Parameter
pH at 25 Degrees C
92413563001 Dup
Units Result Result
Std. Units 5.2 5.3
92413312001 Dup
Units Result Result
Std. Units 6.8 6.8
RPD Qualifiers
0 H3
RPD Qualifiers
0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (4th Creek)
Pace Project No.: 92413565
QC Batch: 452023 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92413565001
METHOD BLANK: 2471582
Matrix: Solid
Associated Lab Samples: 92413565001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Nitrogen, Ammonia
mg/kg
ND
8.9
01/12/19 15:09
LABORATORY CONTROL SAMPLE:
2471583
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
Nitrogen, Ammonia
mg/kg
472
464
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471584
2471585
MS
MSD
92413357001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD Qual
itrogen, Ammonia
mg/kg 13200
10300
10500
21800
22500 83
89
90-110
3 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471586
2471587
MS
MSD
92413358001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD Qua]
Nitrogen, Ammonia
mg/kg ND
2320
2320
2210
2210 93
93
90-110
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (4th Creek)
Pace Project No.: 92413565
QC Batch: 452219 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Associated Lab Samples: 92413565001
METHOD BLANK: 2472536
Matrix: Solid
Associated Lab Samples: 92413565001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed
Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
ND
50.0
01/15/19 04:45
LABORATORY CONTROL SAMPLE: 2472537
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits
Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000
967
97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472538
2472539
MS
MSD
92413357001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD Qua[
itrogen, Kjeldahl, Total mg/kg 62000
21200
19000
74700
74800 60
67
90-110
0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472540
2472541
MS
MSD
92413358001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 5230
5170
5170
8110
9500 56
83
90-110
16 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (4th Creek)
Pace Project No.: 92413565
QC Batch: 452122 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92413565001
METHOD BLANK: 2472244
Associated Lab Samples: 92413565001
Parameter
Units
Nitrogen, Nitrate
mg/kg
Nitrogen, Nitrite
mg/kg
Nitrogen, NO2 plus NO3
mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 2.0 01/12/19 03:27
ND 0.99 01/12/19 03:27
ND 2.0 01/12/19 03:27
Qualifiers
LABORATORY CONTROL SAMPLE:
2472245
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.3
15.2 106 90-110
Nitrogen, Nitrite
mg/kg
9.6
10.2 107 90-110
Nitrogen, NO2 plus NO3
mg/kg
23.9
25.4 106 90-110
IATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2472246
2472247
MS
MSD
92413583001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua]
Nitrogen, Nitrate
mg/kg
ND
522
529
374
401
72
76
90-110
7
Nitrogen, Nitrite
mg/kg
212
348
351
525
545
90
94
90-110
4
Nitrogen, NO2 plus NO3
mg/kg
ND
870
880
899
946
99
103
90-110
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (4th Creek)
Pace Project No.: 92413565
QC Batch: 452341 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92413565001
METHOD BLANK: 2473119
Associated Lab Samples: 92413565001
Parameter Units
Phosphorus mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 01/14/19 23:27
LABORATORY CONTROL SAMPLE: 2473120
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 48.1 51.4 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2473121 2473122
MS MSD
92413583001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
hosphorus mg/kg 2300 1580 1680 3650 3550 85 74 90-110 3 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 18

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Statesville (4th Creek)
Pace Project No.: 92413565
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Statesville (4th Creek)
92413565
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92413565001
4th Creek WWTP
EPA 3050B
452237
EPA 6010D
452330
92413565001
4th Creek WWTP
EPA 7471 B
452998
EPA 7471 B
453128
92413565001
4th Creek WWTP
SM 2540G-2011
452044
92413565001
4th Creek WWTP
ASTM D2974-87
451857
92413565001
4th Creek WWTP
EPA 9045D
452172
92413565001
4th Creek WWTP
SM 2710B-2011
452617
92413565001
4th Creek WWTP
EPA 350.1 Rev 2.0 1993
452023
EPA 350.1 Rev 2.0 1993
452144
Mod.
Mod.
92413565001
4th Creek WWTP
EPA 351.2 Rev 2.0 1993
452219
EPA 351.2 Rev 2.0 1993
452403
92413565001
4th Creek WWTP
EPA 353.2 Rev 2.0 1993
452122
EPA 353.2 Rev 2.0 1993
452124
92413565001
4th Creek WWTP
EPA 365.1 Rev 2.0 1993
452341
EPA 365.1 Rev 2.0 1993
452369
Date: 01/18/2019 03:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 18

t• Sample Condition Upon Recelp SOUR Fage 10s L
h'i%(l" n„�.,�,e�* nr� . Issufn$ Authority:
Laboratory receiving samples:
Asheviffe ❑. Eden[] Greenwood ❑ Huntersitille Q� . Raleigh❑ Mechanicsville❑
Client Name: W®# : 92413565
Upon •M. Project #:
� !; v n agklto
Courier: []Fed Ex ❑UPS []LISPS [] II I II' (I II I (III I I (I III
❑ Commercial []Pace ❑other: � 92413565
Custody Seal Present? []Yes Ja- Sealslntact? []Yes r o
palrllnitiils Fuson Exam(ning Contents
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g . []Bubble Wrap ❑Bubble Bags one ❑ Other }
Therritometer � Dyes []NO rg1G/A
Lg Gun ID: 92T04ti Typle of Ice: M et , ❑Blue ❑Neva=
Coole'rTemp ('C): Correction Factor: Add/Subtract CC) 0.0 Tempsheuld be above freezingto 6°C
Cooler Temp. Corrected ('C): [Jtamples out of temp criteria. Samples an Ice, cooling process
hasbMm
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States; CA, NY, or SC (check maps)? ' Did sasrphs odghate from a foreign source (Internal nally,
Flyes i-INn inciudt ilawail and Puerto Rico)? []Yes 19IV0
Camments/Discrepancy;
Chain of CtutodyPresent?
Yes
No
j]N/A
1.
Samples Arrived within Hold time?
Imes
[]No
t]N A
2.
Short Hold VmeArialysfs (42 hr.),?
0Yes
[O1Qo
EINIA
3.
Rush tun Around Time Requested?
M.
[PNo
❑N/A
4.
SuftidentVolorm?
[Ili
[]No
El NIA
5.
Correct Containers Used?
f
j]No
(]N/A
6•
-Pace Containers Used?
©©Y
[]No
❑N A
Containers ►ntact?
Elf/es
No
NIA.-
7.
Dissolved arralysts:Samples FleldFiltered?
[1$es,
[]NO
R6A
B.
Sample Labels Match COC? �c1
es
[jNo
❑N/A
9•
i 1
l
-IncludesDatefrrne/ID/Analysis Matril
Heads are in V0A Vials (>5-6mm)?
[]Yes
No
,_
LR N/A
10•
Trip Blank Present?
[]Yes
❑No
N/A
L1
Trip BlankQstod Seals Present?
[]yes
MN,
/A
COMMENTSIMUPIE DISCREPANCY Field DataRequlred7 1]Yes �t o
Lot ID ofs sprit containers:
CLIENT NOTIFI(XION/RESOLUTION
Person contacted: Date/Time:
Project Manger SCURF Review: Date:
Protect Manager SRF Review: Date:
(D
Page 16 of 18

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AG3S-2SO mL Amber HZSO4 (pH < 2)
AG3A(DG3A)-25o mL Amber NH4Cl•(N/A)(CI-)
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Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 1/7/2019 1/1/2019-3/31/2019 2.2526
Na mg/I = (Na mg/kg x % Solids) -= 100 = (3160 x 12.5000) -= 100 = 395
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (11000 x 12.5000) = 100 = 1375
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (4560 x 12.5000) _ 100 = 570
Na meq = Na mg/I = Molec.Wgt.Na = 395 = 23 = 17.1739
Ca meq = Ca mg/I = Molec.Wgt.Ca = 1375 = 20 = 68.75
Mg meq = Mg mg/I = Molec.Wgt.Mg = 570 _ 12 = 47.5
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 17.1739 _ SgrRoot[0.5(68.75+47.5)] = 2.25262
Printed: 2/5/2020
Page 1 09:37

Wayp®int_(2)
ANALYTICAL
4/15/2019
Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-095-0203
Project Description: Statesville 4th Creek
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/5/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable,
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
FW;' P 61_r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
L1EA .-y
tt

(D
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-095-0203
Client Project Description: Statesville 4th Creek
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65764
Statesville 4th Creek
Solids
04/03/2019 09:00
04/05/2019
65764
Statesville 4th Creek
Solids
04/03/2019 09:00
04/05/2019
SM-4500-NH3C
WTN
65764
Statesville 4th Creek
Solids
04/03/2019 09:00
04/05/20i9
9045D
WTN
65764
Statesville 4th Creek
Solids
04/03/2019 09:00
04/05/2019
4500NO3F-2011
WTN
65764
Statesville 4th Creek
Solids
04/03/2019 09:00
04/05/2019
6010D
WTN
65764
Statesville 4th Creek
Solids
04/03/2019 09:00
04/05/2019
SW-7471B
WTN
65764
Statesville 4th Creek
Solids
04/03/2019 09:00
04/05/2019
SM-4500-NH3C-TKN
WTN
65764
Statesville 4th Creek
Solids
04/03/2019 09:00
04/05/2019
SM-254OG
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 19-095-0203
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 65764
Sample Id : Statesville 4th Creek
Waypo0 (D
int
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 4th Creek
REPORT OF ANALYSIS
Date Sampled: 4/3/2019 09:00:00
Date Received: 04/05/2019 00:00
Date Reported: 04/15/2019
Total Solids
12.10
121000
100.0
CJR
04/09/2019 15:20
SM-2540G
Moisture'`
87.90
100.0
CJR
04/09/2019 15 :20
SM-2540G
Total Kjeldahl Nitrogen
6.49
64900
250
CLP
04/11/2019 13:30
SM-4500-NH3C-TKN
Phosphorus
2.35
23500
50.0
BKN
04/10/2019 23:42
601 OD
Potassium
0.49
4940
50.0
BKN
04/11/201919:21
6010D
Sulfur
0.67
6730
50.0
BKN
04/11/201919:21
601 OD
Calcium
0.86
8570
250
BKN
04/10/2019 23:42
601 OD
Magnesium
0.32
3170
50.0
BKN
04/10/2019 23:42
601 OD
Sodium
0.07
749
250
BKN
04/10/2019 23:42
601 OD
Iron
20500
50.0
KKM
04/10/2019 23:42
601 OD
Aluminum
29100
50.0
BKN
04/10/2019 23:42
601 OD
Manganese
833
5.00
BKN
04/10/2019 23:42
6010D
Copper
203
2.50
BKN
04/10/2019 23:42
6010D
Zinc
579
12.5
BKN
04/10/2019 23:42
6010D
Ammonia Nitrogen
0.50
4960
100
JPJ
04/12/2019 12:00
SM-4500-NI3C
Organic N
5.99
59940
250
04/11/2019 13:30
CALCULATION
Nitrate+Nitrite-N
42.9
4.60
ZBD
04/08/201915:52
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding
Time
pwir-
#1C 6ewr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior- written authorization.
Agronomist

Report Number: 19-095-0203
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 65764
Sample Id : Statesville 4th Creek
s
•
Waypoi ■ ■t.0 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Project : Statesville 4th Creek
REPORT OF ANALYSIS
Date Sampled: 4/3/2019 09:00:00
Date Received: 04/05/2019 00:00
Date Reported: 04/15/2019
Cadmium
1.59
1.00
BKN
04/10/2019 23:42
601 OD
Chromium
37.3
2.50
BKN
04/10/2019 23:42
601 OD
Nickel
28.6
2.50
BKN
04/10/2019 23:42
601 OD
Lead
18.3
3.00
BKN
04/10/2019 23:42
601 OD
Arsenic
<5.00
5.00
BKN
04/10/2019 23:42
6010D
Mercury
0.329
0.0152
TJS
04/10/2019 14:36
SW-7471 B
Selenium
5.91
5.00
BKN
04/10/2019 23:42
601 OD
pH *
7.4
JSL
04/11/2019 07:09
9045D
Molybdenum
6.60
2.50
BKN
04/10/2019 23:42
601 OD
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Powfic. XC Gar
Pauric McGroary
Agronomist

(D
WayPAoint-
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46493
Customer Name: Synagro Central LLC/ Statesville .
Report -Number: 19-095-0203
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
_
Shipping container/cooler uncompromised?
0 Yes
.0 No
Number of coolers received
1;
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F- High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F- High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: IBrandi Watson Date & Time: 4/05/2019,13:18:47

SAMPLING LOG # ��
IIIIIIIIIIIIIIillllllllllllllllllilllilllllllllllllllllllllllllll
06493
4--0520193 INC.
CHARM OF CUSTODY
Svnagro Central LLCI Statesville
13:18:05
RF-CORD & ANALYSESStatesville
CUSTOMER: SiYI�BAGRO
41h Creek
���®�®
;7
PROJECT MANAGER: �t ���
l attest that the proper field sampling procedures
were used during the collection of these samples.
Phone: (336
SAMPL
A & L CUSTOMER SAMPLING
SAMPLE
# OF
SAMPLING
METHOD METHOD
LAS # SAMPLE I.D. LOCATION
TYPE
CONTAINERS
BATE TIME
PRESERVED SHIPPED
L(+, r reek. S oL
G.— P
y /3 1 c
j E C-
Relinquished by Sampler:
k
Date Time
Recieved by:
REMARKS:
C`• i
H rz .; & o
Relinquished by:
t Time
Rec
Relinquished by:
ff&te I Time
Recieved by:
SPECIAL INSTRUCTIONS:
For �— monitoring purposes.
pO#:
SAMPLE
ANALYSIS REQUEST
1.0.
SL9
SL2
NI f$-N
NO3-N
Organic
Cd
of
Ni
Pb
As
H
Se
P H
CaCO3
equiv.
Volatile
Solids
Mo
Cl
NO
s-�-cr�sbl(i�
ULI.- total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
Sl!2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 4/3/2019 4/112019-9111/2019 0.6087
Na mg/I = (Na mg/kg x % Solids) + 100 = (749 x 12.1000) = 100 = 90.629
Ca mg/1 = (Ca mg/kg x % Solids) = 100 = (8570 x 12.1000) = 100 = 1036.97
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3170 x 12.1000) _ 100 = 383.57
Na meq = Na mg/I + Molec.Wgt.Na = 90.629 = 23 = 3.94039
Ca meq = Ca mg/1 + Molec.Wgt.Ca = 1036.97 = 20 = 51.8485
Mg meq = Mg mg/1= Molec.Wgt.Mg = 383.57 _ 12 = 31.9642
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.94039 = SgrRoot[0.5(51.8485+31.9642)] = 0.608695
Printed: 2/5/2020
Page 1 09:37

Way/topoin
ANALYTICAL
9/9/2019
Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
Ref: Analytical Testing
Report Number: 19-241-0007
Project Description: STATESVILLE WWTP 4TH CREEK
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/29/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P";. P 0-1-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014

O
C
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-241-0007
Client Project Description: STATESVILLE WWTP 4TH CREEK
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
67997
67997
67997
67997
67997
67997
67997
67997
STATESVILLE WWTP 4TH CREEK
Solids
STATESVILLE WWTP 4TH CREEK
Solids
STATESVILLE WWTP 4TH CREEK
Solids
STATESVILLE WWTP 4TH CREEK
Solids
STATESVILLE WWTP 4TH CREEK
Solids
STATESVILLE WWTP 4TH CREEK
Solids
STATESVILLE WWTP 4TH CREEK
Solids
STATESVILLE WWTP 4TH CREEK
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
08/28/2019
09:10
08/29/2019
08/28/2019
09:10
08/29/2019
08/28/2019
09:10
08/29/2019
08/28/2019
09:10
08/29/2019
08/28/2019
09:10
08/29/2019
08/28/2019
09:10
08/29/2019
08/28/2019
09:10
08/29/2019
08/28/2019
09:10
08/29/2019
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-254OG
WTN

Report Number: 19-241-0007
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 67997
Sample Id : STATESVILLE WWTP 4TH CREEK
s
Waypoi t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: STATESVILLE WWTP 4TH CREEK
REPORT OF ANALYSIS
Date Sampled: 8/28/2019 09:10:00
Date Received: 08/29/2019 00:00
Date Reported: 09/09/2019
Total Solids *
12.40
ADM
08/30/2019 15:57
SM-2540G
Moisture *
87.60
ADM
08/30/2019 15:57
SM-2540G
Total Kjeldahl Nitrogen
5.23
52300
250
JPJ
09/06/2019 09:00
SM-4500-NH3C-TKN
Phosphorus
2.43
24300
50.0
JTR
09/05/2019 21:38
6010D
Potassium
0.31
3070
50.0
JTR
09/05/2019 21:38
601 OD
Sulfur
0.79
7870
50.0
JTR
09/05/2019 21:38
601 OD
Calcium
6.18
61800
250
JTR
09/05/2019 21:38
601 OD
Magnesium
0.29
2940
50.0
JTR
09/05/2019 21:38
601 OD
Sodium
0.06
571
250
BKN
09/06/201913:27
601 OD
Iron
22700
50.0
JTR
09/05/2019 21:38
601 OD
Aluminum
24700
50.0
JTR
09/05/2019 21:38
601 OD
Manganese
667
5.00
JTR
09/05/2019 21:38
6010D
Copper
268
2.50
JTR
09/05/2019 21:38
6010D
Zinc
624
12.5
JTR
09/05/2019 21:38
6010D
Ammonia Nitrogen
1.53
15300
100
JPJ
09/06/2019 14:30
SM-4500-NI3C
Organic N
3.70
37000
250
09/06/2019 09:00
CALCULATION
Nitrate+Nitrite-N
<4.63
4.63
ZBD
09/04/201915:24
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
B-Analyte detected in blank
H - Beyond holding time
pot�&
Inc 6-0wr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist

Report Number: 19-241-0007
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 67997
Sample Id : STATESVILLE WWTP 4TH CREEK
Wav Hintz,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: STATESVILLE WWTP 4TH CREEK
REPORT OFAINALYSIS
Date Sampled: 8/28/2019 09:10:00
Date Received: 08/29/2019 00:00
Date Reported: 09/09/2019
Cadmium
3.27
1.00
JTR
09/05/2019 21:38
6010D
Chromium
56.1
2.50
JTR
09/05/2019 21:38
601 OD
Nickel
33.0
2.50
JTR
09/05/2019 21:38
6010D
Lead
34.4
3.00
JTR
09/05/2019 21:38
6010D
Arsenic
<5.00
5.00
JTR
09/05/2019 21:38
6010D
Mercury
0.472
0.0133
TJS
09/04/2019 13:56
SW-7471 B
Selenium
<5.00
5.00
JTR
09/05/2019 21:38
6010D
pH *
7.8
JSL
09/04/2019 06:13
9045D
Molybdenum
10.9
2.50
JTR
09/05/2019 21:38
601 OD
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
?WC1C. 1% C 106~r
Pauric McGroary
Agronomist

I
0 (D
ANALYTICAL
Waypoint,
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46493
Customer Name: Synagro Central LLC/ Statesville
Report Number: 19-241-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
® Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample Iabel(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
41 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
• N/A
F High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: jBrandi Watson Date & Time: 08/29/2019 14:15:38

SAMPL_.a LOG #
�g 11111111111111111111IIIIIIN1111IIIIIIIIIII11111I1111 IllIIII oa29019'
CUSTOMER: S u NAG O Svnaaro Central LLC! Statesville 14:14:31
STATESVILLE WWTP 4TH CREEK
r
PROJECT MANAGER:
Phone:_ 70 j FS(9 S'
A car L CUSTOMER SAMPLING SAMPLE
LAB #} SAMPLE I.D. (LOCATION TYPE
Relinquished by Sampler: 11-
rleiinqulsneo by:
Relinquished by:
SPECIAL INSTRUCTIONS:
U-� 1 1-A For
monitoring purposes.
# OF
CONTAINERS
I
IRALLASS, INC.
CPrri1QOR!1 OF 6US7®UD 17
IRIECI®RD 0. ANAL VS118
6446 RECORD
I attest that the proper field sampling procedures
were used during the collection of these samples.
SAMPLER•
SAMPLING METHOD METHOD
DATE TIME PRESERVED SHIPPED
i/—Z®ra; 5 :10 T-C'r-_ - m-
Date
Time
Recieved by:
'Zg11y
.0
(V .S
Date
Time
Recieved by:
Date
Time
Recieved by:
PO#:
REMARKS:
0
SAMPLE ANALYSIS BEQUEST
I.D' SL'I SL2 NH4 N NO3 N OrNnic Cd Cr Ni Pb As Hg Se ply CaCO3 Volatile
CC II jj equiv. Solids Mo Cf NO N
�Y+,7a5 rr���.L
y � C, �
Sr_J: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL 1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-01-CAK-NC STATESVILLE, NC FOURTH CREEK CAKE 8/28/2019 9/12/2019-10/3112019 0.2141
Na mg/1 = (Na mg/kg x % Solids) = 100 = (571 x 12.4000) = 100 = 70.804
Ca mg/I = (Ca mg/kg x % Solids) - 100 = (61800 x 12.4000) _ 100 = 7663.2
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2940 x 12.4000) + 100 = 364.56
Na meq = Na mg/I _ Molec.Wgt.Na = 70.804 _ 23 = 3.07843
Ca meq = Ca mg/I + Molec.Wgt.Ca = 7663.2 _ 20 = 383.16
Mg meq = Mg mg/1 + Molec.Wgt.Mg = 364.56 = 12 = 30.38
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.07843 + SgrRoot[0.5(383.16+30.38)] = 0.214085
Printed: 2/5/2020
Page 1 09:37

Waypoln(2)t.0
ANALYTICAL
11 /8/2019
Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-303-0005
Project Description: Statesville-4th creek
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/30/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P":. X. car
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

0
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
' Sample Summary Table
Report Number: 19-303-0005
Client Project Description: Statesville-4th creek
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
69300
Statesville-4th creek
Solids
10/29/2019 09:00
10/30/2019
69300
Statesville-4th creek
Solids
10/29/2019 09:00
10/30/2019
SM-4500-NH3C
WTN
69300
Statesville-4th creek
Solids
10/29/2019 09:00
10/30/2019
9045D
WTN
69300
Statesville-4th creek
Solids
10/29/2019 09:00
10/30/2019
4500NO3F-2011
WTN
69300
Statesville-4th creek
Solids
10/29/2019 09:00
10/30/2019
6010D
WTN
69300
Statesville-4th creek
Solids
10/29/2019 09:00
10/30/2019
SW-7471B
WTN
69300
Statesville-4th creek
Solids
10/29/2019 09:00
10/30/2019
SM-4500-NH3C-TKN
WTN
69300
Statesville-4th creek
Solids
10/29/2019 09:00
10/30/2019
SM-254OG
WTN
WTN: Waypoint Analytical - TN, Memphis, TN

Waypoi to
ANALYTICAL
46493
Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Submitted By: Alex Fox
Report Number : 19-303-0005
Lab No : 69300
Sample ID : Statesville-4th creek
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Alex Fox
Project Statesville-4th creek
Information :
REPORT OFANALYSIS
Report Date : 11/08/2019
Received : 10/30/2019
powiz. XF 6aWr
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 10/29/2019 9:00
Moisture
82.7
%
0.010
1 11/04/1917:15
ADM
SM-2540G
Selenium
5.73
mg/Kg - dry
2.89
1 11/04/19 23:57
JTR
6010D
Total Solids
17.3
%
0.010
1 11/04/19 17:15
ADM
SM-2540G
Total Kjeldahl Nitrogen
53100
mg/Kg - dry
1450
1 11/06/19 10:00
JPJ >M-4500-NH3C-TKP
Phosphorus
21600
mg/Kg - dry
28.9
1 11/04/19 23:57
JTR
6010D
Potassium
2710
mg/Kg - dry
28.9
1 11/04/19 23:57
JTR
6010D
Sulfur
9130
mg/Kg - dry
28.9
1 11/04/19 23:57
JTR
6010D
Calcium
12400
mg/Kg - dry
145
1 11/04/19 23:57
JTR
6010D
Magnesium
2550
mg/Kg - dry
28.9
1 11/04/19 23:57
JTR
6010D
Iron
33200
mg/Kg - dry
28.9
1 11/04/19 23:57
JTR
6010D
Manganese
682
mg/Kg - dry
2.89
1 11/04/19 23:57
JTR
6010D
Copper
355
mg/Kg - dry
1.45
1 11/04/19 23:57
JTR
6010D
Organic N
52000
mg/Kg - dry
1450
1 11/06/19 10:00
CALCULATION
Nitrate+ N itrite-N
78.6
mg/Kg - dry
28.4
1 11/06/19 14:17
ZBD
4500NO3F-2011
Nickel
51.0
mg/Kg - dry
1.45
1 11/04/19 23:57
JTR
6010D
Mercury
0.601
mg/Kg - dry
0.0849
1 11/01/19 14:46
TJS
SW-7471B
pH
5.9
S.U.
1 11/05/19 06:18
JSL
9045D
Qualifiers/
*
Outside QC Limit
B
Analyte detected in blank
-- Definitions
C
GCMS Confirmation Analysis
E
Result above cal range
9
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
N
Refer to cover letter.

WavDointo
ANALYTICAL
I46493
Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Submitted By: Alex Fox
Report Number : 19-303-0005
Lab No : 69300
Sample ID : Statesville-4th creek
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Alex Fox
Project Statesville-4th creek
Information :
REPORT OFAINAL YSIS
Report Date : 11/08/2019
Received : 10/30/2019
?WZ'. XF 64wr
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 10/29/2019 9:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
1090
mg/Kg - dry
578
1
11/06/19 14:00
JPJ
SM-4500-NH3C
Aluminum
17100
mg/Kg - dry
28.9
1
11/04/19 23:57
JTR
6010D
Arsenic
6.42
mg/Kg - dry
2.89
1
11/04/19 23:57
JTR
6010D
Cadmium
9.60
mg/Kg - dry
0.578
1
11/04/19 23:57
JTR
6010D
Chromium
113
mg/Kg - dry
1.45
1
11/04/19 23:57
JTR
6010D
41 Lead
94.2
mg/Kg - dry
1.73
1
11/04/19 23:57
JTR
6010D
Molybdenum
21.8
mg/Kg - dry
1.45
1
11/04/19 23:57
JTR
6010D
Sodium
780
mg/Kg - dry
145
1
11/04/19 23:57
JTR
6010D
Zinc
1100
mg/Kg - dry
7.23
1
11/04/19 23:57
JTR
6010D
Qualifiers/ B Analyte detected in blank H Beyond holding time
Definitions

t
Waypoint.(Z)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointa nalytical.coni
Cooler Receipt Form
Customer Number: 46493
Customer Name: Synagro Central LLC/ Statesville
Report Number: 19-303-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
19 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
I, Yes
0 No
Sufficient sample volume for indicated test(s)?
ID Yes
0 No
All samples received within holding time?
40 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: jBrandi Watson I Date & Time: 10/30/2019 14:50:34

Y
I SAW a LOG #
Time Recieved by:
Z_ov
Time Recieved_hw
Recieved by:
CUSTOMER: 'SYf INAGRO
PROJECT MANAGER:
Phone:_( 33& ) 7y �
A &- L CUSTOMER SAMPLING
LAB # 1 SAMPLE I.D. LOCATION
.t�
Relinquished by Sampler: i (�
v
Heiinqulsned by:
Relinquished by:
SPECIAL INSTRUCTIONS:
1IffibR For
IIIIIIIIIIIIIINIIIIIIIIIIIIIIUIIII 1111111111111111111111111111119-303-0005 JAW ©56" CUS400V
1' Svnaaro Central Statesville 10-30-2019 ®(r ®�St
xa c 8 Statesville-41hcreek 14:49:57 RECORD
dd sampling procedures
ever ed aura cullection of these samples.
SAMPLER
SAMPLE »�` OF SAMPLING METHOD METHOD
TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
Date
10 /7
u30
D to
monitoring purposes.
uJ� IcJL oL-1 Pius �uttur, L:alcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
REMARKS:

Sodium Absorption Ratio Calculation (SAR)
F
Product Code
Product Name
Sample Date
Report Range
Ratio
2084-01-CAK-NC
STATESVILLE, NC FOURTH CREEK CAKE
10/29/2019
11/1/2019-12/31/2019
0.6914
Na mg/1 = (Na mg/kg x % Solids) = 100 = (780 x 17.3000) = 100 = 134.94
Ca mg/1 = (Ca mg/kg x % Solids) _ 100 = (12400 x 17.3000) = 100 = 2145.2
Mg mg/1 = (mg mg/kg x % Solids) = 100 = (2550 x 17.3000) + 100 = 441.15
Na meq = Na mg/I _ Molec.Wgt.Na = 134.94 + 23 = 5.86696
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 2145.2 = 20 = 107.26
Mg meq = Mg mg/1 t- Molec.Wgt.Mg = 441.15 = 12 = 36.7625
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.86696 _ SgrRoot[0.5(107.26+36.7625)] = 0.691373
Printed: 2/5/2020
Page 1 09:37

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0016247
Facility Name: STATESVILLE, NC
NPDES# : NCO020591
or WQ# (residual only)
WWTP Name: THIRD CREEK
Residuals Analysis Data
Product Type CAK CAK CAK
Date Sampled (grab) or 01/07/19 04/03/19 08/28/19
Date Composited
Percent Solids 15.20 15.40 13.30
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
Laboratory
PACE ANALYTICAL SERVICE INC.
Waypoint Analytical Virginia Inc.
CAK
10/29/19
24.00
<3.5
<5
6.03
5.13
10.7
8.3
1.48
36.6
0.3
0.173
0.461
0.733
NR
102
42.6
164
397
302
252
458
83.6
60.6
23.2
115
24
18
8
23.3
45.3
44.9
27.6
75.4
<3.5
<5
6.08
3.7
1020
933
480
1350
12300
19000
27700
16700
40500
56100
64100
40800
<48.3
2010
11100
767
128
68.2
<4.78
292
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significantpenaltiesfor submitting false information, including the possibility of fines and imprisonment for knowing violations."
/I A I A
Ii
(SIGNATURP O
Date D a&
DENR FORM RSSF (5/2003) Printed: Tuesday - February 4, 2020 at 18:17:09 for: 2084 02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number WQ0016247 Laboratory
Facility Name STATESVILLE, NC PACE ANALYTICAL SERVICE INC.
NPDES# NCO020591 Waypoint Analytical Virginia Inc.
or WQ# (residual only)
WWTP Name THIRD CREEK
Residual Analysis Data
Product Type
CAK
CAK
CAK
CAK
Date Sampled
01/07/19
04/03/19
08/28/19
10/29/19
Date Composited
Percent Soilds
15.20
15.40
13.30
24.00
PARAMETERS (mg/kg dry weight)'
Aluminium
14200
13600
34400
14900
Calcium
10800
15100
5410
11500
Magnesium
2310
3250
1530
3170
pH
5.20
6.00
6.10
5.50
Potasium
2180
4110
2170
2160
Sodium
<1750
893
435
625
PAN
12288
17300
21455
12676
SAR
1.55
0.6728
0.4889
0.6499
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitti false 'nformation, including th possibility of fines and imprisonment for knowing violations."
XPA SDate �� 171�0
(SIGNATURE O 1
PREPARE
NR - Data Not Reported or Data Not Required Report Run Date:- 2/5/2020 10:55:38 AM

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 18, 2019
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
RE: Project: Statesville (3rd Creek)
Pace Project No.: 92413563
Dear Erik Bruce:
Enclosed are the analytical results for sample(s) received by the laboratory on January 10, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
fIf you have any questions concerning this report, please feel free to contact me.
Sincerely,
7
Lord Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
Q pCCRFO�
i
��eORA'�O�J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 18

aceAnaIXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Statesville (3rd Creek)
92413563
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92413563001
3rd Creek WWTP
EPA 6010D
IDS
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271 OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
MFO
1
PASI-A
b
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
Sample: 3rd Creek WWTP Lab ID: 92413563001 Collected: 01/07/19 09:00 Received: 01/10/19 09:38 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Aluminum
14200 mg/kg 34.9 1 01/14/1910:15
01/15/1914:58
7429-90-5
Arsenic
ND mg/kg 3.5 1 01/14/1910:15
01/15/1914:58
7440-38-2
Cadmium
10.7 mg/kg 0.35 1 01/14/1910:15
01/15/1914:58
7440-43-9
Calcium
10800 mg/kg 34.9 1 01/14/1910:15
01/1511914:58
7440-70-2
Copper
397 mg/kg 1.7 1 01/14/1910:15
01/15/1914:58
7440-50-8
Lead
83.6 mg/kg 1.7 1 01/14/1910:15
01/15/1914:58
7439-92-1
Magnesium
2310 mg/kg 34.9 1 01/14/1910:15
01/15/1914:58
7439-95-4
Molybdenum
24.0 mg/kg 1.7 1 01/14/1910:15
01/15/1914:58
7439-98-7
Nickel
45.3 mg/kg 1.7 1 01/14/1910:15
01/15/1914:58
7440-02-0
Potassium
2180 mg/kg 1750 1 01/14/1910:15
01/1511914:58
7440-09-7
Selenium
ND mg/kg 3.5 1 01114/1910:15
01/15/1914:58
7782-49-2
Sodium
ND mg/kg 1750 1 01/1411910:15
01/15/1914:58
7440-23-5
Zinc
1020 mg/kg 3.5 1 01/14/1910:15
01/15/1914:58
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
0.30 mg/kg 0.039 1 01/17/1916:00
01/18/1910:45
7439-97-6
W540G Total Percent Solids
Analytical Method: SM 2540G-2011
otal Solids
15.2 % 0.000010 1
01/10/19 17:24
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
84.8 % 0.10 1
01/10/19 17:18
9045 pH Soil
Analytical Method: EPA9045D
pH at25 Degrees C
5.2 Std. Units 0.10 1
01/15/19 10:41
H3
Plant Available Nitrogen
Analytical Method: SM 271 OB-2011
Plant Available Nitrogen
12300 mg/kg 0.12 1
01/15/19 17:46
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method:
EPA 350.1 Rev 2.0
1993 Mod.
Nitrogen, Ammonia
ND mg/kg 48.3 1 01/12/19 10:40
01/12/19 15:37
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
40500 mg/kg 1560 5 01/14/19 11:34
01/15/19 05:59
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
128 mg/kg 12.9 1 01/11/19 22:50
01/12/19 03:28
Nitrogen, Nitrate
128 mg/kg 12.9 1 01/11/19 22:50
01/12/19 03:28
14797-55-8
Nitrogen, Nitrite
ND mg/kg 6.5 1 01/11/19 22:50
01/12/19 03:28
14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus
12300 mg/kg 310, 50 01/14/19 19:23
01/14/19 23:22
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/18/2019 03:00 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 18

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
QC Batch: 452998 Analysis Method: EPA 7471B
QC Batch Method: EPA 7471B Analysis Description: 7471 Mercury
Associated Lab Samples: 92413563001
METHOD BLANK: 2475568 Matrix: Solid
Associated Lab Samples: 92413563001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 01/18/1910:36
LABORATORY CONTROL SAMPLE: 2475569
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.068 81 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2475570 2475571
MS MSD
92414199001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
rercury mg/kg ND 0.071 0.071 0.036 0.037 50 50 75-125 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 18

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
I
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
QUALITY CONTROL DATA
QC Batch: 452237 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050E Analysis Description: 6010 MET
Associated Lab Samples: 92413563001
METHOD BLANK: 2472599 Matrix: Solid
Associated Lab Samples: 92413563001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aluminum
mg/kg
ND
10.0
01/15/1913:19
Arsenic
mg/kg
ND
1.0
01/1511913:19
Cadmium
mg/kg
ND
0.10
01/15/1913:19
Calcium
mg/kg
ND
10.0
01/15/1913:19
Copper
mg/kg
ND
0.50
01/15/1913:19
Lead
mg/kg
ND
0.50
01/15/1913:19
Magnesium
mg/kg
ND
10.0
01/1511913:19
Molybdenum
mg/kg
ND
0.50
01/15/1913:19
Nickel
mg/kg
ND
0.50
01/15/1913:19
Potassium
mg/kg
ND
500
01/15/1913:19
Selenium
mg/kg
ND
1.0
01/15/1913:19
Sodium
mg/kg
ND
500
01115/1913:19
Zinc
mg/kg
ND
1.0
01/1511913:19
ABORATORY CONTROL SAMPLE: 2472600
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/kg
500
524
105
80-120
Arsenic
mg/kg
50
49.2
98
80-120
Cadmium
mg/kg
50
51.9
104
80-120
Calcium
mg/kg
500
537
107
80-120
Copper
mg/kg
50
53.5
107
80-120
Lead
mg/kg
50
51.9
104
80-120
Magnesium
mg/kg
500
517
103
80-120
Molybdenum
mg/kg
50
55.1
110
80-120
Nickel
mg/kg
50
52.9
106
80-120
Potassium
mg/kg
500
527
105
80-120
Selenium
mg/kg
50
47.8
96
80-120
Sodium
mg/kg
500
550
110
80-120
Zinc
mg/kg
50
50.9
102
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2472601
2472602
MS
MSD
92413393001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum mg/kg
3270
363
368
7520
7880
1170
1250
75-125
5 M1
Arsenic mg/kg
ND
36.3
36.8
32.0
33.2
84
86
75-125
4
Cadmium mg/kg
ND
36.3
36.8
32.1
32.7
88
89
75-125
2
' Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 18

Pace Analytical Services, LLC
QQn qlJ l qI®
�CGf1�UIICaI
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2472601
2472602
MS
MSD
92413393001
Spike
Spike
MS
MSb
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Calcium
mg/kg
396
363
368
642
665
68
73
75-125
4 M1
Copper
mg/kg
6.9
36.3
36.8
33.6
34.1
74
74
75-125
1 M1
Lead
mg/kg
5.8
36.3
36.8
39.4
39.0
92
90
75-125
1
Magnesium
mg/kg
1030
363
368
1470
1580
122
149
75-125
7 M1
Molybdenum
mg/kg
ND
36.3
36.8
31.6
32.3
87
87
75-125
2
Nickel
mglkg
8.4
36.3
36.8
44.5
45.4
99
100
75-125
2
Potassium
mg/kg
1170
363
368
2540
2720
379
422
75-125
7 M1
Selenium
mg/kg
ND
36.3
36.8
28.6
28.3
79
77
75-125
1
Sodium
mg/kg
ND
363
368
ND
ND
90
90
75-125
Zinc
mg/kg
23.3
36.3
36.8
64.7
66.6
114
118
75-125
3
' Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 01/18/2019 03:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
QC Batch: 451857 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92413563001
SAMPLE DUPLICATE: 2470825
92413658013 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 9.9 9.5 4
SAMPLE DUPLICATE: 2470826
92413607001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 36.2 40.1 10
I
' Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
I QUALITY CONTROL DATA
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
QC Batch: 452172 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92413563001
SAMPLE DUPLICATE: 2472426
92413563001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.2 5.3 0 H3
SAMPLE DUPLICATE: 2472427
92413312001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.8 6.8 0 H3
1
' Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 18

Pace Analytical Services, LLC
aceAnaiytical ® � 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacefabs.com [phone]
QUALITY CONTROL DATA
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
QC Batch:. 452023 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92413563001
METHOD BLANK: 2471582 Matrix: Solid
Associated Lab Samples: 92413563001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 8.9 01/12/19 15:09
LABORATORY CONTROL SAMPLE: 2471583
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 472 464 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2471584
MS
92413357001
Spike
Parameter
Units
Result
Cone.
�itrogen, Ammonia
mg/kg
13200
10300
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2471586
MS
92413358001
Spike
Parameter
Units
Result
Cone.
Nitrogen, Ammonia
mg/kg
ND
2320
2471585
MSD
Spike MS MSD MS MSD % Rec
Cone. Result Result % Rec % Rec Limits RPD Qual
10500 21800 22500 83 89 90-110 3 M6
2471587
MSD
Spike MS MSD MS MSD % Rec
Cone. Result Result % Rec % Rec Limits RPD Qual
2320 2210 2210 93 93 90-110 0
' Resultspresentedon this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
QC Batch: 452219 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Associated Lab Samples: 92413563001
METHOD BLANK: 2472536
Associated Lab Samples: 92413563001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
LABORATORY CONTROL SAMPLE: 2472537
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 01/15/19 04:45
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1000 967 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472538 2472539
MS MSD
92413357001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
�itrogen, Kjeldahl, Total mg/kg 62000 21200 19000 74700 74800 60 67 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472540 2472541
MS MSD
92413358001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Nitrogen, Kjeldahl, Total mg/kg 5230 5170 5170 8110 9500 56 83 90-110 16 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 01/18/2019 03:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 18

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
I
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
QUALITY CONTROL DATA
QC Batch: 452122 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92413563001
METHOD BLANK: 2472244
Matrix: Solid
Associated Lab Samples: 92413563001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND 2.0
01/12/19 03:27
Nitrogen, Nitrite
mg/kg
ND 0.99
01/12/19 03:27
Nitrogen, NO2 plus NO3
mg/kg
ND 2.0
01/12/19 03:27
LABORATORY CONTROL SAMPLE:
2472245
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
14.3
15.2 106 90-110
Nitrogen, Nitrite
mg/kg
9.6
10.2 107 90-110
Nitrogen, NO2 plus NO3
mg/kg
23.9
25.4 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2472246
2472247
/
MS
MSD
92413583001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
ND
522
529
374
401
72
76
90-110
7
Nitrogen, Nitrite
mg/kg
212
348
351
525
545
90
94
90-110
4
Nitrogen, NO2 plus NO3
mg/kg
ND
870
880
899
946
99
103
90-110
5
0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 01/18/2019 03:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 18

Pace Analytical Services, LLC
g ®
acm In alyfic l
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
QC Batch: 452341
Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92413563001
METHOD BLANK: 2473119
Matrix: Solid
Associated Lab Samples: 92413563001
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Phosphorus mg/kg
ND 1.0 01/14/19 23:27
LABORATORY CONTROL SAMPLE: 2473120
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg
48.1 51.4 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2473121 2473122
MS MSD
92413583001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
phosphorus mg/kg 2300
1580 1680 3650 3550 85 74
90-110 3 M6
' Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 01/18/2019 03:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Statesville (3rd Creek)
Pace Project No.: 92413563
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELACITNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Statesville (3rd Creek)
92413563
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92413563001
3rd CreekWWfP
EPA3050B
452237
EPA 601OD
452330
92413563001
3rd Creek WWTP
EPA 7471 B
452998
EPA 7471 B
453128
92413563001
3rd Creek WWTP
SM 2540G-2011
452044
92413563001
3rd Creek WWTP
ASTM D2974-87
451857
92413563001
3rd Creek WWTP
EPA 9045D
452172
92413563001
3rd Creek WWTP
SM 271OB-2011
452617
92413563001
3rd Creek WWTP
EPA 350.1 Rev 2.0 1993
452023
EPA 350.1 Rev 2.0 1993
452144
Mod.
Mod.
92413563001
3rd Creek WWTP
EPA 351.2 Rev 2.0 1993
452219
EPA 351.2 Rev 2.0 1993
452403
92413563001
3rd Creek WWTP
EPA 353.2 Rev 2.0 1993
452122
EPA 353.2 Rev 2.0 1993
452124
92413563001
3rd Creek WWTP
EPA 365.1 Rev 2.0 1993
452341
EPA 365.1 Rev 2.0 1993
452369
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /18/2019 03:00 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 18

Nq.: -
Lebomtoiy receiving samples:
As.hevilie 0. Eden[] Greenwood [] Huntersville U.
RalelghQ Medtanicsvilfe0
Client Name., WO# : 92413563
Prajectl
Courier: ❑FedB( LI ©g.11
ent 11111111111111111111111
❑ Commercial []Pace 0Other.' 82413353
Custody lea[ Present? DYES [9No • Seals Intact? Dyes- iaK • 1 �1 0- 69
'. - Gate%(nKlalsPenon,fxemininaContents: 7
Paddngmaterial.- []Bubble Wrap []Bubble Sags Qt0;W/et1__1[3B1ue
Other Bloloec-al TissueFrozeit?.
[]yes- []No OVA
Thermometer. Type of ICE: ❑Note
R 6un ID: 92TO146
Coolet•TeMpJ'(]: CorrectldnFactor:Add/SukactCC). Q,p Tempshduldbeabove freezingto6'C
DORIES out of temp alfalfa. Samples an ke, cooling process
CoclerTemp-Carrected eq. harbe3un
USDARegulatedSoll Q N/A,watersample)
Did samples or9 lsate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did same °dginatefrom aforeign source Nu ovally,
nYes nao inrlaft Hawaii and FuertoRrCor-aes
Chain of W tod •Present?
. 2
S.
4.
Samples Wved within Hold Time? M1°es r]koo r]N A
Short HoH T€mekArialysts (41 hr.).? Cly, lyno .: ❑NIA
Rush Turn AraundT'Ime Requested?
SuMdahtVafume?
K.
No iJN/A
5.
Correct Containers Used?
,L
17res
[ZNo
QN/A
6.
-Pace foatalners Used?
Elm
DN A
Contains bt'taet?
[IN��/
7•
8.
Dissalvedaa� sls:Sa- ' lesField Fikered? �`! No 98
Sample Labeishfiateh COC?
es
oria
LIN/A
9.
}
3
-includ'sDate/Ttme1f0/Anal sts Matrb
Headspaca N YOAVials(>S-6mm)?
OvesONO
LAN
10•
1t
Trip BlankRerent? (]Yes [jNo /A
Trip BlankQstodySeals Present? Lives No lsry/A
geld Data Required? -[]Yes No
OOMMENTS(S�MPLE DISCREPANCY /—
lot iD of. It containers:
CLIENT NOTIFICAMMIRESOWTION
Person contacted: Date/lime:
I O .
Project Nhrugar SCURF Review: Date: ( r
' Date:
Project Manager SttF Review:
I I
Page 16 of 18,

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-
isiIIATE
!
tlhi :
S"PIFCONOlno"
%•
Z•.3o..
`•._q:
Zia
i
9
SAf1�+LEiL1W4�jEANDS1fvNfA7U1�• _ - :•';= •-+-�- _"�'`- :;i• ;+;�
+.PRWrNamecf8AIYIPLEFt0AlE �En' .-
-•.�. -"'-
c7
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o
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Y d \ !�'
FI-
'"
[MNID�D
1
'Ir>.n...N...:Br-..u....,...•.......->...P.._. aET�..>.>......_...•......-... u......... w1.63.w...,.... >......•...... ..,..3o..>.. F-ALL-Q-020>..09. 12-dcrZO07

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 1/7/2019 1/1/2019-3/31/2019 1.5500
Na mg/I = (Na mg/kg x % Solids) = 100 = (1750 x 15.2000) = 100 = 266
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (10800 x 15.2000) + 100 = 1641.6
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2310 x 15.2000) _ 100 = 351.12
Na meq = Na mg/I _ Molec.Wgt.Na = 266 _ 23 = 11.5652
Ca meq = Ca mg/I = Molec.Wgt.Ca = 1641.6 = 20 = 82.08
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 351.12 _ 12 = 29.26
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 11.5652 _ SgrRoot[0.5(82.08+29.26)] = 1.55004
Printed: 2/5/2020
Page 1 09:37

Waypoint.(D
ANALYTICAL
4/15/2019
Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-095-0202
Project Description: Statesville 3rd Creek
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/5/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P�•r�° cad'
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014

Waypoint.(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-095-0202
Client Project Description: Statesville 3rd Creek
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
65763
Statesville 3rd Creek
Solids
04/03/2019 09:10
04/05/2019
65763
Statesville 3rd Creek
Solids
04/03/2019 09:10
04/05/2019
SM-4500-NH3C
WTN
65763
Statesville 3rd Creek
Solids
04/03/2019 09:10
04/05/2019
9045D -
WTN
65763
Statesville 3rd Creek
Solids
04/03/2019 09:10
04/05/2019
4500NO3F-2011
WTN
65763
Statesville 3rd Creek
Solids
04/03/2019 09:10
04/05/2019
6010D
WTN
65763
Statesville 3rd Creek
Solids
04/03/2019 09:10
04/05/2019
SW-7471B
WTN
65763
Statesville 3rd Creek
Solids
04/03/2019 09:10
04/05/2019
SM-4500-NH3C-TKN
WTN
65763
Statesville 3rd Creek
Solids
04/03/2019 09:10
04/05/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 19-095-0202
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 3rd Creek
REPORT OFANALYSIS Date Sampled: 4/3/2019 09:10:00
Lab Number: 65763 Date Received: 04/05/2019 00:00
Sample Id : Statesville 3rd Creek Date Reported: 04/15/2019
Iota] Solids
15.40
154000
100.0
CJR
04/09/2019 15:20
SM-2540G
Moisture *
84.60
100.0
CJR
04/09/2019 15:20
SM-2540G
Total Kjeldahl Nitrogen
5.61
56100
250
CLP
04/11/2019 13':30
SM-4500-NH3C-TKN
Phosphorus
1.90
19000
50.0
BKN
04/10/2019 23:37
601 OD
Potassium
0.41
4110
50.0
BKN
04/10/2019 23:37
601 OD
Sulfur
0.81
8060
50.0
BKN
04/11/201919:15
6010D
Calcium
1.51
15100
250
BKN
04/10/2019 23:37
601 OD
Magnesium
0.33
3250
50.0
BKN
04/10/2019 23:37
601 OD
Sodium
0.09
893
250
BKN
04/10/2019 23:37
601 OD
Iron
22900
50.0
KKM
04/10/2019 23:37
601 OD
Aluminum
13600
50.0
BKN
04/10/2019 23:37
601 OD
Manganese
865
5.00
BKN
04/10/2019 23:37
6010D
Copper
302
2.50
BKN
04/10/2019 23:37
6010D
Zinc
933
12.5
BKN
04/10/2019 23:37
6010D
Ammonia Nitrogen
0.20
2010
100
JPJ
04/12/2019 12:00
SM-4500-NH3C
Organic N
5.41
54090
250
04/11/2019 13:30
CALCULATION
Nitrate+Nitrite-N
68.2
4.61
ZBD
04/081201915:52
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series
is on a wet basis.
B-Analyte detected in blank
H - Beyond Holding
Time
Pofi4
X 60wr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist

Report Number: 19-095-0202
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 65763
Sample Id : Statesville 3rd Creek
s
Waypoi t
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Statesville 3rd Creek
REPORT OF ANALYSIS
Date Sampled: 4/3/2019 09:10:00
Date Received: 04/05/2019 00:00
Date Reported: 04/15/2019
Cadmium
8.30
1.00
BKN
04/10/2019 23:37
601 OD
Chromium
102
2.50
BKN
04/10/2019 23:37
601 OD
Nickel
44.9
2.50
BKN
04/10/2019 23:37
601 OD
Lead
60.6
3.00
BKN
04/10/2019 23:37
601 OD
Arsenic
<5.00
5.00
BKN
04/10/2019 23:37
6010D
Mercury
0.173
0.0150
TJS
04/10/201914:34
SW-7471B
Selenium
<5.00
5.00
BKN
04/10/2019 23:37
6010D
pH *
6.0
JSL
04/11/2019 07:09
9045D
Molybdenum
18.0
2.50
BKN
04/10/2019 23:37
601 OD
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
pof�4 AIC 60wr
Pauric McGroary
Agronomist

Waypoint-
Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46493
Customer Name: Synagro Central LLC/ Statesville
Report Number: 19-095-0202
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
is UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
® Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
49 Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
• Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
10 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
9 N/A
F_ High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
• No
Comments:
Signature: lBrandi Watson Date & Time: 04/05/2019 13:17:07

SAMPLING LOG %L�
e II�II�IIIII�IIIIII�III��IIII�IIIIIIIII��IIIIII�IIIII��II�IIIIIIII
464
OF CUSTODY
J�
20192
BARK
i Svnaoro Central LLCI Statesville
13:14:59
:d:�l�i� �t �►���,��q�
@�p��
CUSTOMER: S ll UY1AGRO
E Statesville 3rd Creek
RECORD
PROJECT MANAGER: S���
M k
� (-0—
I accesr mar the proper field sampling procedures
_
were used during the collection of these samples.
Phone: (33tp ) `Ta3 _ �(��k
-
SAMPLER
A & L CUSTOMER
SAMPLING.~
SAMPLE
# OF
SAMPLING
METHOD METHOD
LAB # SAMPLE I.D.
LOCATION
TYPE
CONTAINERS
DATE TIME
PRESERVED SHIPPED
Sh v\tlY .
.SA"-
a
? �
Relinquished by Sampler:
Date Time
Recieved by:
REMARKS:
�(.f 1Z% ar.,
Relinquished by:
Da Time
Recieved by:
Relinquished by:
Dat Time
Recieved by:
SPECIAL INSTRUCTIONS:
For
monitoring purposes,
PO#:
SAMPLE
ANALYSIS REQUEST
I.D.
SLI SL2
NH44N
NO3 N
Organic
N
Cd
CV
Ni
Pb
As
H
$e
P H
CaCo3
equiv.
Volatile
Solids
Mo.
CI
NO2-N
3( r� Ci
P
POO
fYPO
R-u: IULUI aouas �ivioisrure), imai Kyeiaa171 Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 4/3/2019 41112019-911112019 0.6728
Na mg/I = (Na mg/kg x % Solids) = 100 = (893 x 15.4000) = 100 = 137.522
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (15100 x 15.4000) = 100 = 2325.4
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3250 x 15.4000) = 100 = 500.5
Na meq = Na mg/I + Molec.Wgt.Na = 137.522 _ 23 = 5.97922
Ca meq = Ca mg/I = Molec.Wgt.Ca = 2325.4 = 20 = 116.27
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 500.5 = 12 = 41.7083
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.97922 _ SgrRoot[0.5(116.27+41.7083)] = 0.672761
Printed: 2/5/2020
Page 1 09:37

Waypoint
ANALYTICAL
9/9/2019
Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.wa,yppini6nalytical.com
Ref: Analytical Testing
Report Number: 19-241-0006
Project Description: STATESVILLE WWTP 3RD CREEK
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/29/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40.CFR 136 Method Update Rule May2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside, of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014

Wayo11p
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-241-0006
Client Project Description: STATESVILLE WWTP 3RD CREEK
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
67996
STATESVILLE WWTP 3RD CREEK
Solids
08/28/2019 13:00
08/29/2019
67996
STATESVILLE WWTP 3RD CREEK
Solids
08/28/2019 13:00
08/29/2019
SM-4500-NH3C
WTN
67996
STATESVILLE WWTP 3RD. CREEK
Solids
08/28/2019 13:00
08/29/2019
9045D
WTN
67996
STATESVILLE WWTP 3RD CREEK
Solids
08/28/2019 13:00
08/29/2019
4500NO3F-2011
WTN
67996
STATESVILLE WWTP 3RD CREEK
Solids
08/28/2019 13:00
08/29/2019
6010D
WTN
67996
STATESVILLE WWTP 3RD CREEK
Solids
08/28/2019 13:00
08/29/2019
SW-7471B
WTN
67996
STATESVILLE WWTP 3RD CREEK
Solids
08/28/2019 13:00
08/29/2019
SM-4500-NH3C-TKN
WTN
67996
STATESVILLE WWTP 3RD CREEK
Solids
08/28/2019 13:00
08/29/2019
SM-254OG
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

Report Number: 19-241-0006
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
o
Waypoi nt
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: STATESVILLE WWTP 3RD CREEK
REPORT OF ANALYSIS Date Sampled: 8/28/2019 13:00:00
Lab Number: 67996 Date Received: 08/29/2019 00:00
Sample Id : STATESVILLE WWTP 3RD CREEK Date Reported: 09/09/2019
lota15011CIS
13.30
ADM
08/30/201915:57
SM-2540G
Moisture *
86.70
ADM
08/30/2019 15:57
SM-2540G
Total Kjeldahl Nitrogen
6.41
64100
250
JPJ
09/06/2019 09:00
SM-4500-NH3C-TKN
Phosphorus
2.77
27700
50.0
JTR
09/05/2019 21:33
6010D
Potassium
0.22
2170
50.0
JTR
09/05/2019 21:33
601 OD
Sulfur
0.67
6720
50.0
JTR
09/05/2019 21:33
601 OD
Calcium
0.54
5410
250
JTR
09/05/2019 21:33
6010D
Magnesium
0.15
1530
50.0
JTR
09/05/2019 21:33
6010D
Sodium
0.04
435
250
BKN
09/06/201913:22
6010D
Iron
24400
50.0
JTR
09/05/2019 21:33
601 OD
Aluminum
34400
50.0
JTR
09/05/2019 21:33
601 OD
Manganese
360
5.00
JTR
09/05/2019 21:33
6010D
Copper
252
2.50
JTR
09/05/2019 21:33
6010D
Zinc
480
12.5
JTR
09/05/2019 21:33
6010D
Ammonia Nitrogen
1.11
11100
100
JPJ
09/06/2019 14:30
SM-4500-NI3C
Organic N
5.30
53000
250
09/06/2019 09:00
CALCULATION
Nitrate+Nitrite-N
<4.78
4.78
ZBD
09/04/201915:22
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist

Report Number: 19-241-0006
Account Number: 46493
Send To: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 67996
Sample Id : STATESVILLE WWTP 3RD CREEK
0 0
Waypoint,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: STATESVILLE WWTP 3RD CREEK
REPORT OF ANALYSIS
Date Sampled: 8/28/2019 13:00:00
Date Received: 08/29/2019 00:00
Date Reported: 09/09/2019
Cadmium
1.48
1.00
JTR
09/05/2019 21:33
601 OD
Chromium
42.6
2.50
JTR
09/05/2019 21:33
601 OD
Nickel
27.6
2.50
JTR
09/05/2019 21:33
6010D
Lead
23.2
3.00
JTR
09/05/2019 21:33
601 OD
Arsenic
6.03
5.00
JTR
09/05/2019 21:33
6010D
Mercury
0.461
0.0134
TJS
09/04/2019 13:54
SW-7471 B
Selenium
6.08
5.00
BKN
09/06/201913:22
6010D
pH *
6.1
JSL
09/04/2019 06:13
9045D
Molybdenum
8.00
2.50
JTR
09/05/2019 21:33
601 OD
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
pcw�e. it C 10JIr"
Pauric McGroary
Agronomist

•
WayP
®' ��,- 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46493
Customer Name: Synagro Central LLC/ Statesville
Report Number: 19-241-0006
Shipping Method
0 Fed Ex 0 US Postal 0 Lab _ - 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1;
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035.— compliance criteria met
0 Yes
0 No
N/A
F— High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F— High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: lBrandi Watson = Date & Time: 8/29/2019 14:11:05

SAMP�._._j LOG #
-ABS, INC. 6HAUN OF
CUSTOMER: SYNAGRO II�II�IIIII�IIIIIIIII�IIII��II�IIIII�II�III�IIIIIIIIIIIIIIIIIIIII o46493
s i9 Doss RECORD
Svnagro Central LLCf Statesville 14:09:26
STATESVILLE 1N4NTP 3RD CREEK
PROJECT MANAGER: �eX on sf that the proper field sampling procedures
used during the collection of these samples.
Phone: 3 _i) 70 3 - ifh tr ( C---'
li
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD
LAB # % SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
JT�.tr5vtl( L✓i,J f� ��Sr w� �� C9xsr /
�I 2$ f ti
Relinquished by mpler: Date Time Recieved by- REMARKS:
Relinquished by: Date Time Recieved by:
Relinquished by: Date Time Recieved by:
SPECIAL INSTRUCTIONS:
For 41 tsrA-rt� monitoring purposes. PO#:
�
SAMPLE ANALYSIS REQUEST
I.D. SLI SL2 NH _N NO _N Organic CaCO Volatile
a a N Cd Cr Ni Pb As Hg Se pH s
equiv Solids MO. Cl NOZ N
5-�.�r��l/r✓ I 94� P1010,
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL i plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 8/28/2019 9/12/2019-10/31/2019 0.4889
Na mg/I = (Na mg/kg x % Solids) _ 100 = (435 x 13.3000) _ 100 = 57.855
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (5410 x 13.3000) _ 100 = 719.53
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1530 x 13.3000) = 100 = 203.49
Na meq = Na mg/I _ Molec.Wgt.Na = 57.855 _ 23 = 2.51543
Ca meq = Ca mg/I + Molec.Wgt.Ca = 719.53 _ 20 = 35.9765
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 203.49 + 12 = 16.9575
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.51543 = SgrRoot[0.5(35.9765+16.9575)] = 0.488946
Printed: 2/5/2020
Page 1 09:37

Waypdlont.(2)
ANALYTICAL
11 /8/2019
Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-303-0004
Project Description: Statesville-3rd Creek
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/30/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P ry prat
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

s
•
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-303-0004
Client Project Description: Statesville-3rd Creek
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
69299
Statesville-3rd creek
Solids
10/29/2019 09:00
10/30/2019
69299
Statesville-3rd creek
Solids
10/29/2019 09:00
10/30/2019
69299
Statesville-3rd creek
Solids
10/29/2019 09:00
10/30/2019
69299
Statesville-3rd creek
Solids
10/29/2019 09:00
10/30/2019
69299
Statesville-3rd creek
Solids
10/29/2019 09:00
10/30/2019
69299
Statesville-3rd creek
Solids
10/29/2019 09:00
10/30/2019
69299
Statesville-3rd creek
Solids
10/29/2019 09:00
10/30/2019
69299
Statesville-3rd creek
Solids
10/29/2019 09:00
10/30/2019
WTN: Waypoint Analytical - TN, Memphis, TN
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-254OG
WTN

e
Waypoint, 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46493
Synagro Central LLC/ Statesville
Mary Brewer Project Statesville-3rd Creek Report Date : 11/08/2019
284 Boger Road Information : Received : 10/30/2019
Macksville , NC 27028
Report Number :19-303-0004
REPORT OFANAIYSIS
Pauric McGroary
Agronomist
Lab No : 69299 Matrix: Solids
Sample ID : Statesville-3rd creek Sampled: 10/29/2019 9:00
Moisture 76.0 % 0.010 1 11/04/1917:15 ADM SM-254OG
Selenium 3.70 mg/Kg - dry 2.08 1 11/04/19 23:53 JTR 6010D
Total Solids
24.0
%
0.010
1 11/04/19 17:15
ADM
SM-254OG
Total Kjeldahl Nitrogen
40800
mg/Kg - dry
1040
1 11/06/19 10:00
JPJ
>M-4500-NH3C-TKP
Phosphorus
16700
mg/Kg - dry
20.8
1 11/04/19 23:53
JTR
6010D
Potassium
2160
mg/Kg - dry
20.8
1 11/04/19 23:53
JTR
6010D
Sulfur
9630
mg/Kg - dry
20.8
1 11/04/19 23:53
JTR
6010D
Calcium
11500
mg/Kg - dry
104
1 11/04/19 23:53
JTR
6010D
Magnesium
3170
mg/Kg - dry
20.8
1 11/04/19 23:53
JTR
6010D
Iron
29000
mg/Kg - dry
20.8
1 11/04/19 23:53
JTR
6010D
Manganese
717
mg/Kg - dry
2.08
1 11/04/19 23:53
JTR
6010D
Copper
458
mg/Kg - dry
1.04
1 11/04/19 23:53
JTR
6010D
Organic N
40000
mg/Kg - dry
1040
1 11/06/19 10:00
CALCULATION
Nitrate+Nitrite-N
292
mg/Kg - dry
19.9
1 11/06/19 14:16
ZBD
4500NO3F-2011
Nickel
75.4
mg/Kg - dry
1.04
1 11/04/19 23:53
JTR
6010D
Mercury
0.733
mg/Kg - dry
0.0637
1 11/01/19 14:42
TJS
SW-7471B
pH
5.5
S.U.
1 11/05/19 06:18
JSL
9045D
Qualifiers/
*
Outside QC Limit
B
Analyte detected in blank
Definitions
C
GCMS Confirmation Analysis
E
Result above cal range
9
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter.

•
Waypol
7621 Whitepine Road, Richmond, VA 23237
■ ■�z
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46493
Synagro Central LLC/ Statesville
Mary Brewer
Project
Statesville-3rd Creek
Report Date : 11/08/2019
284 Boger Road
Information :
Received : 10/30/2019
Mocksville , NC 27028
Pauric McGroary
Report Number :19-303-0004
REPORT OFANALYSIS
Agronomist
Lab No : 69299
Matrix: Solids
Sample ID : Statesville-3rd creek
Sampled: 10/29/2019 9:00
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
767
mg/Kg - dry
417
1 11/06/19 14:00 JPJ SM-4500-NH3C
Aluminum
14900
mg/Kg - dry
20.8
1 11/04/19 23:53 JTR 6010D
Arsenic
5.13
mg/Kg - dry
2.08
1 11/04/19 23:53 JTR 6010D
Cadmium
36.6
mg/Kg - dry
0.417
1 11/04/19 23:53 JTR 6010D
Chromium
164
mg/Kg - dry
1.04
1 11/04/19 23:53 JTR 6010D
Lead
115
mg/Kg - dry
1.25
1 11/04/19 23:53 JTR 6010D
Molybdenum
23.3
mg/Kg - dry
1.04
1 11/04/19 23:53 JTR 6010D
Sodium 625 mg/Kg - dry 104 1 11/04/19 23:53 JTR 6010D
Zinc 1350 mg/Kg - dry 5.21 1 11/04/19 23:53 JTR 6010D
Qualifiers/ B Analyte detected in blank H Beyond holding time
Definitions

•
P
�' �� - 7621 (2) Whitepine Road, Richmond, VA 23237
Way Main 804-743-9401 ° Fax [phone]
A N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46493
Customer Name: Synagro Central LLC/ Statesville
Report Number: 19-303-0004
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
is Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
40 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: lBrandi Watson Date & Time: 10/30/2019 14:35:51

SAMPL ____ LOG #
CUSTOMER: SY INAG rRi O
PROJECT MANAGER:
Phone:( 33%) Zy
I llllll lllll lfl Illlll l 111 lllii llll llllll lllll lllll lllll llll llil 10 0-20194
Svnaaro Central LLC/ Statesville 14:16:55
Statesville-3rd Creek
A Cox L CUSTOMER
LAB # SAMPLE I.D.
SAMPLING
LOCATION
SAMPLE
TYPE
4 OF
CONTAINERS
j
.()G'JI ©F C�MSTI OOV
DR© az AMALV393
RECORD
sampling procedures
-_ - ----c6 L.urrct;tlon of These samples.
SAMPLER
SAMPLING METHOD METHOD
DATE TIME PRESERVED �SgHIPPED
-' �t �o ri q = ol) -T6r vt P
u
%o-1y-3t icu uy Dampier: Date Time Recieved by:
I 24A q. 0 d REMARKS:
Relinquished by: u to Time Reciev
Relinquished by: D to Time Recieved by:
SPECIAL INSTRUCTIONS:
For monitoring purposes.
(STATE) PO#t:
SAMPLE ANALYSIS REQUEST
I.D. SLR SL2 NH4N NO3 N Organic Gd Cr Ni Pb qS Hg Se PH CaCO3 Volatile Mo CI NO -N
equiv. Solids z
3` I I �
lam` rc h
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL i plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
MM �

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2084-02-CAK-NC STATESVILLE, NC THIRD CREEK CAKE 10/29/2019 11/1/2019-12/31/2019 0.6499
Na mg/I = (Na mg/kg x % Solids) = 100 = (625 x 24.0000) _ 100 = 150
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (11500 x 24.0000) _ 100 = 2760
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3170 x 24.0000) _ 100 = 760.8
Na meq = Na mg/I _ Molec.Wgt.Na = 150 + 23 = 6.52174
Ca meq = Ca mg/I + Molec.Wgt.Ca = 2760 _ 20 = 138
Mg meq = Mg mg/I = Molec.Wgt.Mg = 760.8 _ 12 = 63.4
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.52174 = SgrRoot[0.5(138+63.4)] = 0.649903
Printed: 2/5/2020
Page 1 09:37

SECTION 3

FACILITY NAME: STATESVILLE, NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: APPLING
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 37.06
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.10 ACRES PERMITTED: 11.10
Page
Lune Applied ***
Date
Lbs Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
ova
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/6/19
300.00 (CY)
27.0271
12.10
2.754
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
Sep-19
300.00 (CY)
27.027
I
9/6/19
50.00 (CY)
4.5051
15.40
0.584
STTCC
I DRY
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
Sep-19
50.00 (CY)
4.505
1
1
1
r orai varronsivc:
Total Wet Tons/Ac:
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
133
0.033
0.018
0.325
1.471
0.172
0.002
0.057
0.210
0.038
4.280
151.65
Cumulative lbs/acre
0.198
0.437
5.095
16.021
2.107
0.057
0.612
2.581
0.202
34.698
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
!
137
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Statesville, NC Total Dry Tons Applied (Annual): 37.06
Permit #: WQ0016247 Cation Exchange Capacity (non 503 only):
erator: Dennis Phillips Owner: Dennis Phillips Predominant Soil Series: Appling
Acres Used: 11.1 Acres Permitted: 11.1 Site #: NC IR 00020 Field #: IR 00020 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
4/3/19
2
4/3/19
3
4
5
6
7
8
9
10
11
12
% Solids
12.1
15.4
Arsenic
5
5
Cadmium
1.59
8.3
Copper
203
302
Chromium
37.3
102
Lead
18.3
60.6
Mercury
0.329
0.173
Molyb-
denum
6.6
18
Nickel
28.6
44.9
Selenium
5.91
5
Zinc
579
933
Total
Phos-
torus
23500
19000
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
in
a
Im
M
93
MEMO'
on
! !
1 11 •
1 111
1 111
1 111
1 111
! ! ! !
! 111
ME 1
1 111
! 111
1 111
! 1
1 11•
1 1 1
1 111
1 111
! 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1!
...-
;
�
1 111
1 111
! 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
��
•
1 1
1 •
1 111
1 111
1 111
1 111
ME 1
1 111
1 111
Mir, 1
1 111
1 111
�I
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Im
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
ffITITIT11
r1r,11
1 111
we
�
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
••
1
1 1
Mir, 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 1!•
1 111
1 111
1 111
1 111
1 111
1 111
WIT, 11
1 111
1 111
1 111
1 1
®
:•
1.1
1 111
1 11!
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
Total
•
M
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
. 1
• .
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisopgient for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS PHILLIPS PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 30.57
SITE #: NC IR 00020 FIELD# : IR 00020 0002 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 11.50 ACRES PERMITTED: 11.50
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or
or Wet Tons (WT) (specify)
Solids
Dry
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/6/19
200.00 (CY)
17.3911
12.10
1.772
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
9/9/19
100.00 (CY)
8.696
12.10
0.886
STFCC
DRY .
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
Sep-19
300.00 (CY)
26.087
total Nation$/Ac:
Total Wet Tons/Ac:
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
109
0.027
0.008
0.198
1.079
0.097
0.002
0.035
0.152
0.031
3.079
124.95
Cumulative Ibs/acre
0.156
0.229
2.702
12.512
1.452
0.054
0.460
1.571
0.159
25.452
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
._--
126
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
erator:
Acres Used:
Statesville, NC Total Dry Tons Applied (Annual): 30.57
WQ0016247
Dennis Phillips Owner:
11.5 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Dermis Phillips Predominant Soil Series: Cecil
11.5 Site #: NC IR 00020 Field #: IR 00020 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
4/3/19
2
4/3/19
3
4
5
6
7
8
9
10
11
12
% Solids
12.1
15.4
Arsenic
5
1 5
Cadmium
1.59
8.3
Copper
203
302
Chromium
37.3
102
Lead
18.3
60.6
Mercury
0.329
0.173
Molyb-
denum
6.6
18
Nickel
28.6
44.9
Selenium
5.91
5
Zinc
579
933
Total
Phos-
'torus
23500
19000
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
'Non
on
MEMO
1 111
1 111
1 111
1 111
1 11100008
..
1 11:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11:
...
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
ME 11
1 111
1•
1 •:
1 111
1 Ili
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •:
•�
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 lil
1 111
1 111
1 1•
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
�-�
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1
1 111
1 111
1 111
l i 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
E 1:
Total
' •
.
1 111
1 111
1 111
1 111
1 111
i 111
i 111
1 111
1 111
1 111
1 111
•
.•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisonment for knowing violations".
MY �__ & 2 llaz7j
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS PHILLIPS PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 31.96
SITE #: NC IR 00020 FIELD# : IR 00020 0003 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 10.40 ACRES PERMITTED: 10.40
Page
Lime Applied ***
Date
Lbs Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or%
Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I
DATE or
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/9/19
250.00 (CY)
24.0381
12.10
2.450
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
Sep-19
250.00 (CY)
24.038
9/6/19
50.00 (CY)
4.808I
15.40
0.624
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
Sep-19
50.00 (C
4.808
1
Total Gallon/Ac:
Total Wet Tons/Ac:
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs/acre
122
0.031
0.018
0.310
1.371
0.165
0.002
0.055
0.196
0.035
4.000
138.83
Cumulative lbs/acre
0.231
0.516
5.427
17.976
3.168
0.070
0.700
2.666
0.247
39.567
_ I
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
128
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 9
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
erator:
Acres Used:
Statesville, NC Total Dry Tons Applied (Annual):
WQ0016247 Cation Exchange Capacity (non 503 only):
Dennis Phillips Owner: Dennis Phillips Predominant Soil Series:
31.96
Cecil
10.4 Acres Permitted: 10.4 Site #: NC IR 00020 Field #: IR 00020 0003
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or[!]
Com-
posite
Date
4/3/19
2
4/3/19
3
4
5
6
7
8
9
10
11
12
% Solids
12.1
15.4
Arsenic
5
5
Cadmium
1.59
8.3
Copper
203
302
Chromium
37.3
102
Lead
18.3
60.6
Mercury
0.329
0.173
Molyb-
denum
6.6
18
Nickel
28.6
44.9
Selenium
5.91
5
Zinc
579
933
Total
Phos-
' torus
23500
19000
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 1
1 11 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11:
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
fff 1 :
•.•-
1 ••
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®''
1 1.1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
MY, 11
1 111MT,
M,
�
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
�_�
1 �1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 '•
1 1 •
1 11.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
•�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� 11
Total
' •
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:: •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisopTent for knowing violations".
r
allo go
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: STATESVILLE,NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0004 A
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 176.94
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 34.90 ACRES PERMITTED: 34.90
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
2/1/19
240.00 (CY)
6.877
12.50
0.724
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
47,500. p
10,200.00 p
15.20 p
16305
FESCUE HAY
2/2/19
60.00 (CY)
1.719
12.50
0.181
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
47,500. p
10,200.00 p
15.20 p
16305
FESCUE HAY
2/4/19
225.00 (CY)
6.447
12.50
0.679
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
47,500. p
10,200.00 p
15.20 p
16305
FESCUE HAY
2/5/19
135.00 (CY)
3.868
12.50
0.407
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
47,500. p
10,200.00 p
15.20 p
16305
FESCUE HAY
2/6/19
255.00 (CY)
7.307
12.50
0.769
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
47,500. p
10,200.00 p
15.20 p
16305
FESCUE HAY
2/7/19
255.00 (CY)
7.307
12.50
0.769
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
47,500. p
10,200.00 p
15.20 p
16305
FESCUE HAY
Feb-19
1,170.00 (CY)l
33.525
10/10/19
75.00 (CY)
2.1491
12.40
0.224
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
52,300. p
15,300.00 p
4.63 p
18755
FESCUE HAY
Oct-19
75.00 (1
2.149
I
1
10/10/19
410.00 (CY)
11.7481
13.30
1.316
STTCC
DRY
:=UR
0.5
0.30
64,100. p
11,100.00 p
4.78 p
21455
FESCUE HAY
Oct-19
410.00 (CY)
11.748
1

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS PHILLIPS PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 176.94
SITE #: NC IR 00020 FIELD# : IR 00020 0004A OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 34.90 ACRES PERMITTED: 34.90
Page : 2
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
180
0.063
0.028
0.137
3.367
0.255
0.005
0.116
0.313
0.063
6.993
275.81
Cumulative Ibs/acre
0.211
0.238
2.053
15.530
2.084
0.046
0.568
1.534
0.193
31.418
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
202
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
Lim
1339.0
267.9
15.0 —
375.0
89.0
2500.0 C
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X� 2/ro/z,
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Statesville, NC Total Dry Tons Applied (Annual): 176.94
Permit #:
orator:
Acres Used:
WQ0016247
Dennis Phillips
Cation Exchange Capacity (non 503 only):
Owner: Dennis Phillips Predominant Soil Series
34.9 Acres Permitted:
Cecil
34.9 Site #: NC IR 00020 Field #: 111100020 0004A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 11
4/3/19
1,213
4/3/19
1/7/19
4
8/28/19
5
8/28/19
6
7
8
9
10
11
12
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
5
5
6.3
5
6.03
Cadmium
1.59
8.3
3.2
3.27
1.48
Copper
203
302
366
268
252
Chromium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
27.6
Selenium
5.91
5
6.3
5
1 6.08
Zinc
579
933
772
624
480
Total
Phos-
Torus
23500
19000
27200
24300
27700
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
off,
App .
Event
0.00
0.00
3.53
0.22
1.32
Arsenic
0.000
0.000
0.044
0.002
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Cadmium
0.000
0.000
0.023 1
0.001
0.004
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.028
Copper
0.000
0.000
2.583
0.120
0.663
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.367
Chromium
0.000
0.000
0.000
0.025
0.112
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.137
Lead
0.000
0.000
0.179
0.015
0.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.255
Mercury
0.000
0.000
0.004
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.000
0.000
0.090
0.005
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.116
denum
Nickel
0.000
0.000
0.226
0.015
0.073
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.313
Selenium
0.000
0.000
0.044
0.002
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Zinc
0.000
0.000
5.449 1
0.280
1.263
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
6.992
Total
Phos-
0.000
0.000
191.978
10.886
72.906
0.000
0.000
0.000
0.000
0.000
0.000
0.000
275.770
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
pris nment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

r
FACILITY NAME: STATESVILLE,NC
OWNER: DENNIS PHILLIPS
SITE #: NC IR 00020 FIELD# : IR 00020 0004 B
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 66.74
OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 14.10 ACRES PERMITTED: 14.10
Page
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm )
Cro p
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
2/8/19
225.00 (CY)
15.957
12.50
1.680
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
47,500. p
10,200.00 p
15.20 p
16305
FESCUE HAY
2/9/19
75.00 (CY)
5.319
12.50
0.560
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
47,500. p
10,200.00 p
15.20 p
16305
FESCUE HAY
Feb-19
300.00 (CY)
21.276
4/2/19
120.00 (CY)
8.511
12.10
0.867
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
I FESCUE HAY
4/3/19
105.00 (CY)
7.447
12.10
0.759
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
I FESCUE HAY
4/11/19
30.00 (CY)
2.128
12.10
0.217
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
I FESCUE HAY
4/18/19
90.00 (CY)
6.383
12.10
0.650
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20501
FESCUE HAY
Apr-19
345.00 (CY)
24.469
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual lbs/acre
175
0.053
0.022
0.186
2.652
0.205
0.004
0.090
0.286
0.058
6.346 239.05
Cumulative Ibs/acre
0.183
0.197
1.897
13.972
1.961
0.051
0.463
1.338
0.157
28.303
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
202
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 p
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
x L
77� zs lv Zv
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM`
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
erator:
Acres Used:
Statesville, NC Total Dry Tons Applied (Annual): 66.74
WQ0016247 Cation Exchange Capacity (non 503 only):
Dennis Phillips Owner: Dennis Phillips Predominant Soil Series:
14.1 Acres Permitted: 14.1 Site #: NC IR 00020 Field #: IR 00020 0004B
Cecil
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or9
Com-
posite
Date
1
4/3/19
2
4/3/19
3
1/7/19
4
8/28/19
5
8/28/19
6
7
al -
10
11 J
1121
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
5
5
6.3
5
6.03
Cadmium
1.59
8.3
3.2
3.27
1.48
Copper
203
302
366
268
252
Chromium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
1 27.6
Selenium
5.91
5
6.3
5
6.08
Zinc
579
933
772
624
480
Total
Phos-
--'torus
23500
19000
27200
24300
27700
nual Heavy Metal Field Loadings (Calculated in llbs/acre):
• •.
Event
•
1 11
"IMITM
WITIT,1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11:
1 111
1 1
1 111
1 111
1 111
1 111
1 111
IT, 11
1 111
1 lil
1 111
1 1
••.
1 111
•� 1
KIT, 11
1 111
1 111
1 111
1 111
1 111
1 111
ff1 111
M111
1:•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
ffor, 1
1 :.
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 ill
1 111
1 1
ramm
1 11
1 111
will 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111�
1 1
1111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1111
1 111
1111
1 1.1
•-��
WIT,1
1111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :•
1 1'
1 111
1 1 :
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
::
1111
•
1111
1111
1111
1111
1111
1111
1111
1111
1111
•
Total
' •
1 111
: •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• 1
.•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
?ris n ent for knowing violations".
?k �73
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITYNAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: APPLING
OWNER: DENNIS PHILLIPS PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 33.35
SITE #: NC IR 00020 FIELD# : IR 00020 0008 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 10.30 ACRES PERMITTED: 10.30
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/6/19
200.00 (CY)
19.417
12.10
1.979
STFCC
DRY
0-<I/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
Sep-19
200.00 (cry
19.417
9/6/19
1 100.00 (CY)
9.7091
15.40
1.259
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
Sep-19
100.00 (Cl)
9.709
1
1
Total Gallons/Ac:
Total Wet Tons/Ac:
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
125
0.032
0.027
0.405
1.564
0.225
0.002
0.071
0.226
0.036
4.641
140.86
Cumulative lbs/acre
0.192
0.230
2.381
15.315
1.874
0.055
0.570
1.441
0.270
28.406_.-_
i
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
6
139
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
L_
1339.0
267.9
15.0 ;
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
erator:
Acres Used:
Statesville, NC Total Dry Tons Applied (Annual): 33.35
WQ0016247 Cation Exchange Capacity (non 503 only):
Dennis Phillips Owner: Dennis Phillips Predominant Soil Series:
10.3 Acres Permitted: 10.3 Site #: NC IR 00020
Appling
Field #: IR 00020 0008
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
Lif
4/3/19
1 2
4/3/19
3
1/7/19
4 j5
8/28/19
8/28/19
6
7
8
9
10
11
12
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
5
5
6.3
5
6.03
Cadmium
1.59
8.3
3.2
3.27
1.48
Copper
203
302
366
268
252
Chromium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
27.6
Selenium
5.91
5
6.3
5
6.08
Zinc
579
933
772
624
480
Total
Phos-
iorus
23500
19000
27200
24300
27700
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
..
00,060,0
NONE
1 1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
.••
WIT, 1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
•..-
1 :1
1 .1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•�
1 �:
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 �1�
1 1
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�.
1 11
WIT, 11
1 111
1 111
1 111
1 11 i
1 111
1 111
1 111
MIT, 11
1 111
WIT, 11
ffIT,1
•
1 1 •
1 1�
1 111
1 111
1 111
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
•-�
���
1 111
1 111
1 111
1 111
1 111
1 111
1 111
l i 11
1 111
1 111
1 •
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
®�
' •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�,
Total
' •
• 1
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�1
••
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisonnjent for knowing violations".
J
Q v `Z/wzj
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITYNAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS PHILLIPS PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 28.72
SITE #: NC IR 00020 FIELD# : IR 00020 0009 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 11.40 ACRES PERMITTED: 11.40
Page : 1
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm )
Crop
p
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/6/19
225.00 (CY)
19.737
12.10
2.011
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
9/9/19
25.00 (CY)
2.193
12.10
0.223
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
Sep-19
250.00 (CY)
21.930
9/6/19
25.00 (CY)
2.1931
15.40
0.284
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
Sep-19
25.00 (1
2.193
I
1
1
1
lbtal Gallons/Ac:
Total Wet Tons/Ac:
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual Ibs/acre
101
0.025
0.012
0.225
1.079
0.116
0.002
0.040
0.153
0.029
3.119 115.85
Cumulative lbs/acre
0.182
0.240
2.333
15.045
1.999
0.057
0.562
1.426
0.251
28.588-�
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
4
136
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X 1 `�" z/10, /Z, >
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Statesville, NC Total Dry Tons Applied (Annual): 28.72
Permit #: WQ0016247 Cation Exchange Capacity (non 503 only):
erator: Dennis Phillips Owner: Dennis Phillips Predominant Soil Series:
Acres Used: 11.4 Acres Permitted: 11.4 Site #: NC IR 00020 Field #:
Cecil
IR 00020 0009
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
4/3/19
2
4/3/19
3
1/7/19
4
8/28/19
5
8/28/19
6
7
8
9
10
11
12
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
5
5
6.3
5
6.03
Cadmium
1.59
8.3
3.2
3.27
1.48
Copper
203
302
366
268
252
Chromium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
27.6
Selenium
5.91
5
6.3
5
6.08
Zinc
579
933
772
624
480
Total
Phos-
torus
23500
19000
27200
24300
27700
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 ;
M1 In
NOT,1
111
1 111
1 M,
.•� �
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
••.-
1 '1
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 ' .
�•
1•
1 1
1 111
1 111
1 111
1 111
1 Ili
1 111
1 111
1 111
1 111
1 111
1 1;
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 1 •
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1� 1
•-•
WIMM
1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
MITI=
Total
•
1� ••;
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•1
••
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
pris nment for knowing violations".
L2ho/?,Q
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: DENNIS PHILLIPS PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 92.43
SITE #: NC IR 00020 FIELD# : IR 00020 0011 OPERATOR: DENNIS PHILLIPS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 32.90 ACRES PERMITTED: 32.90
Page
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
4/11/19
112.00 (CY)
3.404
12.10
0.347
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
4/18/19
135.00 (CY)
4.103
12.10
0.418
STFCC
DRY
0-<I/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
4/29/19
255.00 (CY)
7.751
12.10
0.790
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
4/30/19
225.00 (CY)
6.839
12.10
0.697
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
Apr-19
1 727.00 (CY)
22.097
5/1/19
135.00 (CY)
4.103I
12.10
0.418
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
I FESCUE PASTURE
5/2/19
45.00 (CY)
1.368
12.10
0.139
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
May-19
180.00 (CY)
5.471
1
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
115
0.028
0.009
0.210
1.141
0.103
0.002
0.037
0.161
0.033
3.253 132.05
Cumulative Ibs/acre
0.133
0.117
1.482
9.860
0.953
0.047
0.371
1.050
0.144
18.029
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
151
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 z
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X�(1
a
� L)7�6
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to 'be submitted in Annual Report
Facility Name:
Permit #:
,rator:
Acres Used:
Statesville, NC
WQ0016247
Dennis Phillips Owner
32.9 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Dennis Phillips Predominant Soil Series:
32.9 Site #: NC IR 00020 Field #:
92.43
Cecil
lR 00020 0011
Residual Analysis Data (Leavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
4/3/19
2
4/3/19
3
1/7/19
4
8/28/19
5
8/28/19
6
7
8
9
10
11
12
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
5
1 5
6.3
5
6.03
Cadmium
1.59
8.3
3.2
3.27
1 1.48
Copper
203
302
366
268
252
Chromium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
27.6
Selenium
5.91
1 5
6.3
5
6.08
Zinc
579
933
772
624
480
Total
Phos-
-',orus
23500
19000
27200
24300
27700
nual Heavy Metal Field Loadings (Calculated in Ibs/acre):
•.too
1 1
or, 11
ff, 111
1 111
1 111
1 lil
1 111
IT, 11
1 111
1 111
1 111
1 111
1 1
1 11'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11'
•..-
� 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
MIT, 11
1 111
1 111
1 111
1 11
�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
�-�
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
MWITIM,
1 111
1 111
1•
1 1
1 ill
1 111
1 111
1 111
1 111
WIT,
1 111
1 111
1 111
1 111
1 Ili
1 1
®®
1 111
1 111
1 11 i
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
'•M
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
•'
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
iris nment for knowing violations".
Signature of Land Applier ' Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 100.29
SITE #: NC IR 00023 FIELD# : IR 00023 0003 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 27.40 ACRES PERMITTED: 27.40
Page
Lime Applied * * *
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/26/19
125.00 (CY)
4.562
12.10
0.465
STFCC
MOIST
0-<I/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE PASTURE
Jun-19
125.00 (1 Y)
1 4.562
6/26/19
350.00 (CY)
12.774
15.40
1.657
STTCC
MOIST
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
I FESCUE PASTURE
6/27/19
325.00 (CY)
11.861
15.40
1.538
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
Jun-19
675.00 (CY)
24.635
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual lbs/acre
130
0.037
0.055
0.687
2.119
0.404
0.001
0.121
0.314
0.037
6.501 143.27
Cumulative lbs/acre
0.103
0.117
1.531
7.877
0.890
0.033
0.326
0.841
0.125
17.394 S
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
162
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
LX
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
,rator:
Acres Used:
Statesville, NC Total Dry Tons Applied (Annual): 100.29
WQ0016247 Cation Exchange Capacity (non 503 only):
Eddie Porter Owner: Lorane Page Predominant Soil Series:
27.4 Acres Permitted: 27.4 Site #: NC IR 00023 Field #:
Cecil
IR 00023 0003
Residual Analysis Data (Heavy Metals and 'Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
4/3/19
2
4/3/19
3
1/7/19
4
8/28/19
5
8/28/19
6
7
8
9
10
11 I
12
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
5
1 5
6.3
5
1 6.03
Cadmium
1.59
8.3
3.2
3.27
1.48
Copper
203
302
366
268
252
Chromium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
27.6
Selenium
5.91
1 5
6.3
5
1 6.08
Zinc
579
933
772
624
480
Total
Phos-
torus
23500
19000
27200
24300
27700
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
0
In
B
M
]onrm
.
1
1
Wfflfflm1
11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
MT, MI",
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
•..•
1 :•
• 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�
NITM
1.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
MT, 11
1 111
1 111
1 .: •
1 1
MMfflffi11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1'1'
Ron
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
�
1 11•
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1111
1 111
1 111
�••
1 1
1
1 111
1 111
1 111
1 lil
1 111
1 111
1 111
1 111
1 111
1 111
1
MT, 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1
•.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
. 11
Total
•
M
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
. •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prispnknent for knowing violations".
�c 1_� .6 V z,
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITYNAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: W00016247 ANNUAL DRY TONS APPLIED: 68.09
SITE #: NC IR 00023 FIELD# : IR 00023 0004 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 14.80 ACRES PERMITTED: 14.80
Page
Lime Applied ***
Date
Lb,/A.
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm )
Crop
p
Total
Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/24/19
450.00 (CY)
30.405
15.40
3.944
STTCC
MOIST
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
6/25/19
25.00 (CY)
1.689
15.40
0.219
STTCC
MOIST
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
6/26/19
50.00 (CY)
3.378
15.40
0.438
STTCC
MOIST
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
Jun-19
1 525.00 (CY)
35.472
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
159
0.046
0.076
0.939
2.779
0.558
0.002
0.166
0.413
0.046
8.585 174.84
Cumulative Ibs/acre
0.169
0.289
3.272
13.998
2.127
0.043
0.644
1.637
0.230
33.735
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
162
FD Cumulative Pollutant LoadingRate Limit Ibs(acre
( )
36.6
34.8
— —
1339.0
267.9
15.0
_ �
375.0
89.0
2500.0 ( -
s
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X K/_/�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, InjectionfIncorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Statesville, NC Total Dry Tons Applied (Annual): 68.09
Permit #:
zrator:
Acres Used:
WQ0016247 Cation Exchange Capacity (non 503 only):
Eddie Porter Owner: Lorane Page Predominant Soil Series:
14.8 Acres Permitted:
Cecil
14.8 Site #: NC IR 00023 Field #: IR 00023 0004
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
1
4/3/19
2
4/3/19
31
1/7/19
8/28/19
1=5
8/28/19
6
1 81
10
11
12
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
1 5
5
6.3
5
6.03
Cadmium
1.59
8.3
3.2
3.27
1.48
Copper
203
302
366
268
252
Chromium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
27.6
Selenium
5.91
5
6.3
5
6.08
Zinc
579
933
772
624
480
Total
Phos-
' torus
23500
19000
27200
24300
27700
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
D
non
p
MI.,
Event
IT, "I,
0 000
KITIT,0
Nor,
0 000
0 000
0 0�.
..�
o, Me
0 000
0 000
0 000
0,
0, M110
000
0 000
0 0.
...
o 000
o 000
0 000
0 000
0 000
0 000
0 000
0,"11
o oeo
Mr,"11
i 000
o 000
0•
o 000
0 000
0 000
0 000
KITIT,0
KITIT,0
ff, e
0,
0,
0 000
0..
1 000
0
o 000
0 000
0 000
0 goo
0 000
0 0�0
0 000
0 goo
0 000
� o00
0
o 000
0 00
0 000
0 000
0 000
0 000
0 000
0 000
0 000
o 000
0 000
o00
o 00
o 000
0 ..
o 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 ..
.-�
�
o 000
0�
o 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0
I
o 000�
®
o 000
o 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
Total
Phos-
o 000
:
o 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
0 000
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
priso en'
for knowing violations
2
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: LORANE PAGE PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 95.01
SITE #: NC IR 00023 FIELD# : IR 00023 0005 OPERATOR: EDDIE PORTER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 19.60 ACRES PERMITTED: 19.60
Page
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm )
Cro p
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
5/8/19
30.00 (CY)
1.531
15.40
0.199
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68. 00 PT
11311
FESCUE HAY
May-19
30.00 (Cl)
1.531
I
6/17/19
350.00 (CY)
17.857
12.10
1.820
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
I FESCUE HAY
6/21/19
335.00 (CY)
17.092
12.10
1.742
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
I FESCUE HAY
6/26/19
50.00 (CY)
2.551
12.10
0.260
STFCC
MOIST
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
21515
FESCUE HAY
Jun-19
735.00 (CY)
37.500
6/26/19
125.00 (CY)
6.378
15.40
0.827
STTCC
MOIST
0-<1/2"
SUR
0.5
0.3q
56,100. p
2,010.00 p
68.20 p
17300
FESCUE HAY
Jun-19
125.00 (CY)
6.378
I
1
1
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual lbs/acre
192
0.048
0.029
0.494
2.171
0.264
0.003
0.087
0.311
0.055
6.339 218.59
Cumulative lbs/acre
0.218
0.296
3.505
17.759
2.458
0.060
0.742
1.925
0.282
FI-
38.875
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
15.0 1
375.0
89.0
2500.0
STTCC = STATESVILLE, NC THIRD CREEK CAKE
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
X-L
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mgjkg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Statesville, NC Total Dry Tons Applied (Annual): 95.01
permit #: WQ0016247 Cation Exchange Capacity (non 503 only):
erator: Eddie Porter Owner: Lorane Page Predominant Soil Series:
Acres Used: 19.6 Acres Permitted: 19.6 Site #: NC IR 00023 Field #:
Cecil
IR 00023 0005
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
4/3/19
2
4/3/19
3
1/7/19
4
8/28/19
5
8/28/19
6
7
8
9
10
11
12
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
5
5
6.3
5
6.03
Cadmium
1.59
8.3
3.2
3.27
1.48
Copper
203
302
366
268
252
Chromium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
27.6
Selenium
5.91
5
6.3
5
6.08
Zinc
579
933
772
624
480
Total
Phos-
torus
23500
19000
27200
24300
27700
mual Leavy Metal Field Loadings (Calculated in lbs/acre):
0
on
-
1NONE
1 1 :
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�: i
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
NOT, 11
1 111
1 111
1 1 •
••.
®
1• 1
1 111
1 111
1 lil
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 1`
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1� �
1 1
1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 .�
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
••
1 `
1 1`
1 111
1 111
1 111
1 111
1 111
1 111
i ill
1 111
1 111
1 111
1 1�
1 1 1
1 111
1 111
1 111
1 111
1 111
i 111
1 111
1 111
1 111
1 111
1 M,
®
" •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• �1
Total
'•
`.�
`::
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
:•
.•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
pris ent for knowing violations".
7A01n)
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: BADIN
OWNER: ROBERT RIDENHOUR PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 40.21
SITE #: NC ST 00003 FIELD# : ST 00003 0001 OPERATOR: ROBERT RIDENHOUR CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 19.10 ACRES PERMITTED: 19.10
Page: 1
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past24
Method
zation
zation
TKN
Nitrogen
and
(pprn)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
7/15/19
310.00 (CY)
16.2301
15.40
2.105
STTCC
DRY
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE PASTURE
Jul-19
310.00 (CY)l
16.230
I
1
1
1
1 V 141 1J411V11J/tW.
Total Wet Tons/Ac:
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annual Ibs/acre
73
0.021
0.035
0.429
1.272
0.255
<.001
0.076
0.189
0.021
3.928 80.00
Cumulative lbs/acre
0.082
0.056
0.967
5.056
0.523
0.011
0.240
0.437
0.085
14.050
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
102
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8-�
_
1339.0
267.9
15.0
375.0
89.0
2500.0
STTCC = STATESVILLE, NC THIRD CREEK CAKE
V
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Statesville, NC Total Dry Tons Applied (Annual): 40.21
permit #: WQ0016247
erator:
Acres Used:
Robert Ridenhour
Cation Exchange Capacity (non 503 only):
Owner: Robert Ridenhour Predominant Soil Series:
Badin
19.1 Acres Permitted: 19.1 Site #: NC ST 00003 Field #: ST 00003 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
I 1
4/3/19
2
4/3/19
3
1/7/19
4
8/28/19
5
8/28/19
6
7
8
9
10
11
12
% Solids
12.1
15.4
12.5
12.4
13.3
Arsenic
5
5
6.3
5
6.03
Cadmium
1.59
8.3
3.2
3.27
1.48
Copper
203
302
366
268
252
Clu-omium
37.3
102
0
56.1
42.6
Lead
18.3
60.6
25.3
34.4
23.2
Mercury
0.329
0.173
0.5
0.472
0.461
Molyb-
denum
6.6
18
12.7
10.9
8
Nickel
28.6
44.9
32
33
27.6
Selenium
5.91
5
6.3
5
6.08
Zinc
579
933
772
624
480
Total
Phos-
torus
23500
19000
27200
24300
27700
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
.• •
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
•..-
1 111
®
1 111
1 111
1 111
1 111
1111
1 111
1111
1 111
1111
1111
••
1 111
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
KIT, 11
1 111
KIT, 11
ff, I •
1 111
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 111
1 1 .
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
�•
1 111
1 :•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :•
KIT, 11
1 1
1 111
1 111
1 111
1111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 111
•
1 111
1 111
1 111
MITI 11
KITITI1
1 111
1 111
1 111
1 111
1 111
• .
Total
•
1 111
• ••1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •'1
..
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
pris K
t for knowing violations".
2
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITYNAME: STATESVILLE, NC PREDOMINANT SOIL SERIES: BADIN
OWNER: ROBERT RIDENHOUR PERMIT #: WQ0016247 ANNUAL DRY TONS APPLIED: 82.04
SITE #: NC ST 00003 FIELD# : ST 00003 0003 OPERATOR: ROBERT RIDENHOUR CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 24.60 ACRES PERMITTED: 24.60
Page
Lime Applied ***
Date
i_Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm )
Crop
p
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
7/11/19
525.00 (CY)
21.341
12.10
2.175
STFCC
DRY
0-<1/2"
SUR
0.5
0.30
64,900. p
4,960.00 p
42.90 p
20505
FESCUE HAY
Jul-19
525.00 (CY)
21.341
I
7/15/19
220.00 (CY)
8.943I
15.40
L 160
STTCC
I DRY
0-<1/2"
SUR
0.5
0.30
56,100. p
2,010.00 p
68.20 p
17300
FESCUE HAY
Jul-19
220.00 (CY)l
8.943
1
1
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
129
0.033
0.026
0.399
1.584
0.220
0.002
0.070
0.229
0.037
4.683
146.30
Cumulative lbs/acre
0.095
0.053
0.946
6.891
0.637
0.017
0.268
0.569
0.118
17.631
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
163
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0 1 4
STFCC = STATESVILLE, NC FOURTH CREEK CAKE
STTCC = STATESVILLE, NC THIRD CREEK CAKE
X L C�
- &,, Z/� I df
G v
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Statesville, NC Total Dry Tons Applied (Annual): 82.04
Permit #:
erator:
Acres Used:
WQ0016247
Robert Ridenhour
Cation Exchange Capacity (non 503 only):
Owner: Robert Ridenhour Predominant Soil Series:
Badin
24.6 Acres Permitted: 24.6 Site #: NC ST 00003 Field #: ST 00003 0003
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
4/3/19
4/3/19
L 3
4
5
6
7
8
9
10 I
Ill
12
% Solids
12.1
15.4
Arsenic
5
1 5
Cadmium
1.59
8.3
Copper
203
302
Chromium
37.3
102
Lead
18.3
60.6
Mercury
0.329
0.173
Molyb-
denum
6.6
18
Nickel
28.6
44.9
Selenium
5.91
5
Zinc
579
933
Total
Phos-
-'-torus
23500
19000
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
My, 11
ME 11
1 1
1 11
1 1 •
1 111
1 111
1 111
MITI 11
1 111
1 111
1 111
1 111
1 111
1 111
1 1
•••KIT.,
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:�
• .
1 •
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 ..
1 1:1
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 lil
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 1 •
1 1�
1 111
1 111
1 111
1 111
1 lil
1 111
1 111
1 111
1 111
1 111
1 1 1
�•
1
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
��
1 1 .
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� .:
Total
'.•
1
�� 1:1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�• 1
.•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
prisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

SECTION 4

m9symmq
Atr�ria+tlrad i�!`�r�radorJes
January 24, 2019
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Statesville
Dear Erik Bruce:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: httzp:llwww.settek.com
Order No.: 19010535
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/10/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
tl-)�
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 27

Summit Environmental Technologies, Inc. Case Narrative
SUMMIT 3310 Win St.
�IY1�l ?�tJIa1=Y•1TttLicC}iPTOI {;.}, INC, Cuyahoga Falls, Ohio 44223 WO#: 19010535
Ar?Mytieal ia0oralorFss TEL: [phone] FiLY.• [phone]
Website: htto.Ilwww.setfek.com Date: 1/24/2019
CLIENT: Synagro
Project: Statesville
WorkOrder Narrative:
19010535: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Prep Sample Comments:
19010535-001A 424938: Prep Comments for MtlPrep_TCLP(3010A), Sample 19010535-OOIA: TCLP
was filtered after digestion.
Analytical Sequence Sample Notes:
19010535-001a TCLP-SVOC-CPest(8081B): The CCV (Batch R93761) exhibits high recovery for
Methoxychlor. All samples are ND
19010535-001a TCLP-SVOC-CPest(8081B): The ICV (Batch R93761) exhibited high recovery for
Methoxychlor. The associated samples are ND for Methoxychlor.
Original
Page 2 of 27

Summit Environmental Technologies, In Qualifiers and Acronyms
sufAmlat 3310 Win 5
EI�t4�l?�FJh9� ITAL 6�c?�€�ot_clt ���s, t,t,; Cuyahoga Falls, Ohio 4421 WO#: 19010535
Analy fleal t_lborwortes TEL: [phone] FAX.- (330) 253-446
Website: httD:11www.settek.co. Date: 1/24/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
A The hold time for sample preparation and/or analysis was exceeded. Not Clean Water Act compliant.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
W Samples were received outside temperature limits (00 — 6° C). Not Clean Water Act compliant.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLv1
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MiuCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 27

Summit Environmental Technologies, Inc.
!BSUMMIrt 3310 Win St.
�h'C+Nth+PJh9b1TAL.a�C!4Sti9f}1.43f;1=�,9Pde. Cuyahoga Falls, Ohio44223
AwlfyU al iaboralortec TEL: [phone] FAX.- [phone]
Website: http://Www.settek.com
CLIENT: Synagro
Project: Statesville
Workorder
Sample Summary
WO#: 19010535
24-Jan-19
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
19010535-001 4th Creek WWTP 1/7/2019 9:00:00 AM 1/10/2019 10:15:00 AM Solid
Page 4 of 27

ff]SUIOMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
Et VIi2CtitdtArnaTaL'rc ttav©t �Gi�s, VC.
Cuyahoga Falls, Ohio 44223
r1 n.7lyt1i`ai Lafaaratordog TEL: [phone] FfIX.• [phone]
WO#: 19010535
Website: http://www.settek-.com
24-Jan-19
Client:
Synagro
Project:
Statesville
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
19010535-OOIA 4th Creek WWTP 1/7/2019 9:00:00 AM Solid Ignitability of Solids (SW-846: 1030)
1/11/2019 11:00:00 AM
pH (SW9045D)
1/17/2019 3:09:04 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
1/14/2019 11:38:00 AM
Reactive Sulfide (9034)/7.3.4.2
1/14/2019 11:08:00 AM
TCLP Herbicides Analysis (SW1311/81/10/2019 5:44:59 PM
1/11/2019 5:00:00 PM 1/18/2019 8:44:00 PM
TCLP Mercury Analysis (SW1311/74-/1/10/2019 5:44:59 PM
1/16/2019 11:30:00 A 1/16/2019 4:48:00 PM
TCLP Metals Analysis (SW1311/6010' 1/10/2019 5:44:59 PM
1/14/2019 8:25:00 AM 1/14/2019 4:40:31 PM
TCLP Pesticides Analysis (SW1311/8(1/10/2019 5:44:59 PM
1/15/2019 2:45:00 PM 1/23/2019 3:48:00 AM
TCLP Semi-Volatiles Analysis 1/10/2019 5:44:59 PM
1/14/2019 10:45:00 A 1/16/2019 4:17:00 PM
(SW1311/8270)
—
TCLP Volatiles Analysis
1/10/2019 5:46:19 PM 1/14/2019 5:10:00 PM
Original
Page 5 of 27

Summit Environmental Technologies, Inc. Analytical Report
S tj Wr 3310 Win St.
ENVIRt4NMENTALTr-GWJ01-QC :3, 9ptL, Cuyahoga Falls, Ohio44223 (base report)
Anr+lyNcal Laboratordi}e. TEL: [phone] FAX.- [phone] WO#: 19010535
Website: htto://www.settek.com Date Reported: 1/24/2019
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/7/2019 9:00:00 AM
Lab ED: 19010535-001A
Project: Statesville
Client Sample ED 4th Creek WWTP
Analyses Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
0.00500
mg/L
1
1/16/2019 4:48:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW3010A
Analyst: KMO
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND
0.500
mg/L
1
1/14/2019 4:40:31 PM
TCLP Barium(Ba) ND
5.00
mg/L
1
1/14/2019 4:40:31 PM
TCLP Cadmium(Cd) ND
0.100
mg/L
1
1/14/2019 4:40:31 PM
TCLP Chromium(Cr) ND
0.200
mg/L
1
1/14/2019 4:40:31 PM
TCLP Lead(Pb) ND
0.500
mg/L
1
1/14/2019 4:40:31 PM
TCLP Selenium(Se) ND
0.0500
mg/L
1
1/14/2019 4:40:31 PM
TCLP Silver(Ag) ND
0.500
mg/L
1
1/14/2019 4:40:31 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND
0.0800
mg/L
2
1/16/2019 4:17:00 PM
2,4,5-Trichlorophenol ND
0.200
mg/L
2
1/16/2019 4:17:00 PM
2,4,6-Trichlorophenol ND
0.200
mg/L
2
1/16/2019 4:17:00 PM
2,4-Dinitrotoluene ND
0.0400
mg/L
2
1/16/2019 4:17:00 PM
o-Cresol ND
0.200
mg/L
2
1/16/2019 4:17:00 PM
m/p-Cresol(s) ND
0.200
mg/L
2
1/16/2019 4:17:00 PM
Cresols, Total ND
4.00
mg/L
2
1/16/2019 4:17:00 PM
Hexachloro-1,3-butadiene ND
0.0160
mg/L
2
1/16/2019 4:17:00 PM
Hexachlorobenzene ND
0.0400
mg/L
2
1/16/2019 4:17:00 PM
Hexachloroethane ND
0.0800
mg/L
2
1/16/2019 4:17:00 PM
Nitrobenzene ND
0.0800
mg/L
2
1/16/2019 4:17:00 PM
Pentachlorophenol ND
0.200
mg/L
2
1/16/2019 4:17:00 PM
Pyridine ND
0.200
mg/L
2
1/16/2019 4:17:00 PM
Surr: 2-Fluorophenol 30.6
10 - 109
%Rec
2
1/16/2019 4:17:00 PM
Surr: Phenol-d6 36.0
10 - 109
%Rec
2
1/16/2019 4:17:00 PM
Surr: Nitrobenzene-d5 41.1
19 - 120
%Rec
2
1/16/2019 4:17:00 PM
Surr: 2,4,6-Tribromophenol 58.8
10 - 120
%Rec
2
1/16/2019 4:17:00 PM
Surr: 2-Fluorobiphenyl 42.6
22 - 117
%Rec
2
1/16/2019 4:17:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 6 of 27

S Ir
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
FIc1'I.?nNP.rePdTauTactiltiC]u7Ge�S,INC
k7<:rfy6aW Laboratorloe
Cuyahoga Falls, Ohio44223
TEL: [phone] FAX.• [phone]
(base report)
WO#: 19010535
Website: http://www.settek.com
Date Reported: 1/24/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SOLID
Collection Date:
1/7/2019 9:00:00 AM
Lab ID:
19010535-OOIA
Project:
Statesville
Client Sample ID 4th Creek WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14
95.8 34 - 116
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
SW8270D SW351OC Analyst: BJH
%Rec 2 1/16/2019 4:17:00 PM
SW8081 SW351OC Analyst: MES
Chlordane, total
ND
0.0250 mg/L
10
1/23/2019 3:48:00 AM
Toxaphene
ND
0.0500 mg/L
10
1/23/2019 3:48:00 AM
Endrin
ND
0.00500 mg/L
10
1/23/2019 3:48:00 AM
gamma-BHC
ND
0.00500 mg/L
10
1/23/2019 3:48:00 AM
Heptachlor
ND
0.00500 d mg/L
10
1/23/2019 3:48:00 AM
Heptachlor epoxide
ND
0.00500 d mg/L
10
1/23/2019 3:48:00 AM
Methoxychlor
ND
0.00500QV+QC+mg/L
10
1/23/2019 3:48:00 AM
Surr: TCMX
15.0
10 - 119 %Rec
10
1/23/2019 3:48:00 AM
Surr: DCB
23.0
10 - 119 %Rec
10
1/23/2019 3:48:00 AM
NOTES:
The CCV (Batch R93761) exhibits high recovery for Methoxychlor. All samples are ND
The ICV (Batch R93761) exhibited
high recovery for Methoxychlor. The associated samples are ND for Methoxychlor.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)
2,4-D
2,4,5-TP
Surr: DCAA
SW8151A SW8151A Analyst: MES
ND 1.00 mg/L 1 1/18/2019 8:44:00 PM
ND 0.500 d mg/L 1 1/18/2019 8:44:00 PM
68.3 20 - 140 %Rec 1 1/18/2019 8:44:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND
0.125
mg/L 25 1/14/2019 5:10:00 PM
1,2-Dichloroethane ND
0.125
mg/L 25 1/14/2019 5:10:00 PM
MEK ND
0.625
mg/L 25 1/14/2019 5:10:00 PM
Benzene ND
0.125
mg/L 25 1/14/2019 5:10:00 PM
Carbon tetrachloride ND
0.125
mg/L 25 1/14/2019 5:10:00 PM
Chlorobenzene ND
0.125
mg/L 25 1/14/2019 5:10:00 PM
Chloroform 1.22
0.125
mg/L 25 1/14/2019 5:10:00 PM
Qualifiers: Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 7 of 27

SIM UU ot
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
EWIfIONNENTALTFC!%NOI_QGt 3,INo
Cuyahoga Falls, Ohio44223
(base report)
Anjo cal Laborarortee TEL:
[phone] FAX.- [phone]
WO#: 19010535
Website: http:/lwww.settelccom
Date Reported: 1/24/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SOLID
Collection Date:
1/7/2019 9:00:00 AM
Lab ID:
19010535-OOIA
Project:
Statesville
Client Sample ID 4th Creek WWTP
Analyses
Result RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
96.9
Surr: Dibromofluoromethane
118
Surr: Toluene-d8
102
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
RCI-SOLID-W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
RCI-SOLID-W/ IGNITABILITY1030
PH (SW9045D)
pH 7.5
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
SW8260B SW1311M Analyst: CTB
0.125
mg/L
25
1/14/2019 5:10:00 PM
0.125
mg/L
25
1/14/2019 5:10:00 PM
0.0500
mg/L
25
1/14/2019 5:10:00 PM
70 - 130
%Rec
25
1/14/2019 5:10:00 PM
70 - 130
%Rec
25
1/14/2019 5:10:00 PM
70 - 130
%Rec
25
1/14/2019 5:10:00 PM
SW9014
Analyst: MS
0.490
mg/Kg
1
1/14/2019 11:38:00 AM
SW1030
Analyst: AJT
1
1 /11 /2019 11:00:00 AM
SW9045D
Analyst: VVK
s.u.@20.2C
1
1/17/2019 3:09:04 PM
SW9034
Analyst: MS
25.0
mg/Kg
1
1/14/2019 11:08:00 AM
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 27

Summit Environmental Technologies, Inc. Accreditation Program
sufAmlir 3310 Win St. Anal teS Report
ph;lrli?0Wt fi)ENTAL FEC?tc�2O IwS, INN Cuyahoga Falls, Ohio 44223 y p
AjiatyUcal LaborworloG TEL: [phone] FAX.- [phone] WO#: 19010535
Website: http://www.settek.com 24-Jan-19
Client: Synagro State: NW
Project: Statesville Program Name: NC WW_SCM
Sample ID Matrix Test Name Analyte Status
19010535-OOIA
Solid
Ignitability of Solids (SW-846: 1030)
Ignitability A
Solid
pH (SW9045D)
Hydrogen Ion (pH) A
Solid
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive U
Solid
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive U
Solid
TCLP Herbicides Analysis (SWI311/8151)
2,4,5-TP A
Solid
TCLP Herbicides Analysis (SWI311/8151)
2,4-D A
Solid
TCLP Herbicides Analysis (SWI311/8151)
DCAA A
Solid
TCLP Mercury Analysis (SW1311/7470)
Mercury A
Solid
TCLP Metals Analysis (SW1311/6010)
Arsenic A
Solid
TCLP Metals Analysis (SW1311/6010)
Barium A
Solid
TCLP Metals Analysis (SW1311/6010)
Cadmium A
Solid
TCLP Metals Analysis (SW1311/6010)
Chromium A
Solid
TCLP Metals Analysis (SW1311/6010)
Lead A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium A
Solid
TCLP Metals Analysis (SW1311/6010)
Silver A
Solid
TCLP Pesticides Analysis (SWI311/8081)
2,2',3,3'54,4',5,5',6,6'- A
Decachlorobiplienyl
Solid
TCLP Pesticides Analysis (SWI311/8081)
Chlordane, total A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Endrin A
Solid
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor A
Solid
TCLP Pesticides Analysis (SW 1311/8081)
Heptachlor epoxide A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Tetrachloro-m-xylene A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene A
Solid
TCLP Sena-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Tribromophenol A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorophenol A
Original #1
Page 9 of 27

Summit Environmental Technologies, Inc. Accreditation Program
summ, Iwt 3310 Will St. AnalteS Report
Eh',dll?C7h1te1�t•11J�.L GZC4:L�1cJLC} FwS, tht;, Cuyahoga Falls, Ohio 44223 Y p
�,tycde! Lor�1�r1E TEL: [phone] FAX.- [phone] WO#: 19010535
Website: http.*11w nv.settek.com 24-Jan-19
Client: Synagro
State: NW
Project: Statesville
Program Name: NC_WW_SCM
Sample ID
Matrix
Test Name
Analyte
Status
19010535-001A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
3,4-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW131118270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Solid
TCLP Senu-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene-d5
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Phenol-d6
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
p-Terphenyl-d14
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Solid
TCLP Volatiles Analysis
I,1-Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-Butanone
A
Solid
TCLP Volatiles Analysis
4-Bromofluorobenzene
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbon tetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chlorofonn
A
Solid
TCLP Volatiles Analysis
Dibromofluoromethane
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Toluene-d8
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl chloride
A
Original #1
Page 10 of 27

ism
Summit Environmental Technologies, Inc. 3310 Wig: St. QC SUMMARY REPORT
ED;4'In�N61K;dTAL`rE Ti ![SLAG{gig, JhG Cuyahoga Falls, Ohio 44223
.ljvf Ova/ Lat�earatonos WO#: 19010535
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: 35472
Sample ID MB-35472
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 1/1012019
RunNo: 93332
Dlient ID: PBS
Batch ID: 35472
TestNo: SW8260B SW1311M
Analysis Date: 1/11/2019
SegNo: 1903835
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowL]mit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
464
Surr: Dibromofl uorom ethane
602
Surr: Toluene-d8
496
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
500.0 92.8 70
500.0 120 70
500.0 99.2 70
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
130
130
130
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 11 of 27

Summit Environmental Technologies, Inc.ffJ S ir 3310 Win St. QC SUMMARY REPORT
cENA'lrL0tJh1EaJTAL rccma )CwGIEa,1Kc, Cuyahoga Falls, Ohio 44223
WO#: 19010535
A3Wriy�Ucu/ Labnrjrordo!; TEL: [phone] FAX.- [phone]
Website: http://www.settek-.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: 35523
mple ID Ics-35523
SampType: LCS
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
ent ID: LCSS
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914631
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 78.4
43.8
130
2,4,5-TP
ND
0.500 0.500
0 62.9
51.5
111
Surr: DCAA
357
500.0
71.4
34.2
150
Sample ID mb-35523
SampType: MBLK
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
Client ID: PBS
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914632
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D ND 1.00 0 0 d
2,4,5-TP ND 0.500 0 0
Surr: DCAA 320 500.0 64.0 20 140
Sample ID 19010307-001ams
SampType: MS
TestCode: tclp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
Client ID: BatchQC
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914634
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 100
37
105
W
2,4,5-TP
ND
0.500 0.500
0 89.8
38
106
W
Surr: DCAA
567
500.0
113
20
140
W
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 12 of 27

Mm
S Mt
Summit Environmental Technologies,
331 10 D Win St. St.
QC SUMMARY REPORT
EP•�4I16UtJM�P•]TaL'a �ttt�oL��siq,, JNr.
ArnaPyNoa/ Laborasono_ TEL:
Cuyahoga Falls, Ohio 44223
[phone] FAX.- [phone]
WO#: 19010535
Wehsite: http://www.settek.com
24-Jan-19
Client:
Synagro
Project:
Statesville
BatchID• 35523
Sample ID 19010307-001amsd
SampType: MSD
TestCode: telp-svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
client ID: BatchQC
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914646
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 83.7 37 105 0 0 30 W
2,4,5-TP ND 0.500 0.500 0 71.5 38 106 0 0 30 W
Surr: DCAA 453 500.0 90.6 20 140 0 W
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 13 of 27

MSUPArdill
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY "PORT
=P,.0110ANIrilTAL TEs nNOLL)GII:5, jPdf
?kt�lrticai' L�.f�oratoras TEL:
Cuyahoga Falls, Ohio 44223
[phone] FAX.• [phone]
WO#: 19010535
Website: http://www.settek.com
24-Jan-19
Client:
Synagro
Project:
Statesville
BatchID: 35549
Sample ID MB-35549
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: PBS
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909423
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
ample ID MB2-35549
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
lent ID: PBS
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909424
ialyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00500
Sample ID LCS-35549
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: LCSS
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909425
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00401 0.00200 0.00400 0 100 80 120
Sample ID 19010659-002AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: Batch=
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909440
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury 0.00468 0.00200 0.00400 0.000380 108 75 125
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 14 of 27
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
sumfolst 3310 Win St.
€�at�113�ryiJ�.ttt•.TAL fcC?td3�7LC?G��a,INC Cuyahoga Falls, Ohio44223
WO#: 19010535
�tf'tit;�i iaborarr�ric�� TEL: [phone] FAX.• [phone]
t;n
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: 35549
Sample ID 19010659-002AMS
SampType: MS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: Batch=
Batch ID: 35549
TestNo:
SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909440
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 19010659-002AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: BatchQC
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909441
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
0.00462 0.00200 0.00400 0.000380 106 75 125 0.00468 1.29 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 15 of 27

fn
S it
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
��.t�l{it71Jr9T t�rnL cttitaoL��G�� , INC,
Cuyahoga Falls, Ohio 44223
Arra4100W L;Iboforon,, , TEL: [phone] FAX.- [phone]
WO#: 19010535
Website: http://www.settek.com
24-Jan-19
Client:
Synagro
Project:
Statesville
BatchID: R93297
Ignitability 8.08 7.240 0 112 70 130
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is Original
p greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 16 of 27

summutSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENNIIIOAPA1 MTAL �_L:'ChNOLC G1!::S, I.NC Cuyahoga Falls, Ohio 44223
WO#: 19010535
A RutyUcUf LaOorarrvk-�5 TEL: [phone] FAX:[phone]
Website: http://www.settelc.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93297
Sample ID 19010440-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902697
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 19010531-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: Batch=
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902699
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
ample ID 19010532-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
lient ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902701
nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
ample ID 19010533-001ADUP
SampType: DUP
TestCode:
Ignitability_S Units:
Prep Date:
RunNo: 93297
lient ID: BatchQC
Batch ID: R93297
TestNo:
SW1030
Analysis Date: 1/11/2019
SegNo: 1902703
nalyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 17 of 27
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

P,
Summit Environmental Technologies, Inc.summlot QC SUMMARY REPORT
3310 Win St.
t�ti°li4�ti1JP.11 t•:rttL7 Crt�woLr7Gly , WC Cuyahoga Falls, Ohio 44223
AJ7,--i}�tacaf L2borarc�roo� TEL: [phone] FAX.- [phone] WO#: 19010535
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93297
Sample ID 19010534-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
;lient ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902705
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability non-flammable 0 0 20
'ample ID 19010535-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
;lient ID: 4th Creek WWTP
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902707
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability
non-flammable
0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 18 of 27

sumfortSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
E 1�1.4+ISiUtJblLtdTt�L `a c�t6NOt tz 1�S, ltiC Cuyahoga Falls, Ohio 44223
WO#: 19010535
}zJ7iri;,Uhoul L<?br3PotoYlUL' TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93390
mple ID 19010535-01AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
gnt ID: BatchQC
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906045
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 8.98 0.490 10.00 0 89.8 81.6 122
Sample ID 19010535-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
Client ID: 4th Creek WWTP
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906046
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive
9.09 0.495 10.00 0 90.9 81.6 122
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 19 of 27

summint Summit Environmental Technologies, Inc. 3310 Win St.QC SUMMARY REPORT
INC, Cuyahoga Falls, Ohio44223
Ar:u,rlcul i.b.]aal,stetcs WO#: 19010535
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: R93390
Sample ID LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 93390
,lient ID: LCSW
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906029
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
cyanide, Reactive
9.57 0.490 10.00 0 95.7 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 20 of 27

S ummilu Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ED
EM'111C)WtJCNTA.LTE.CiItVOWGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 19010535
rkj7aty0v.,J Laborolonog TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: R93465
Sample ID 19010535-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
Client ID: 4th Creek WWTP
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908916
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4210 25.0 4800 0 87.7 80 120
mple ID 19010535-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
ent ID: 4th Creek WWTP
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908917
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
(fide, Reactive 4320 25.0 4800 0 90.0 80 120 4210 2.58 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 21 of 27
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

MM
sumalklir3310
Summit Environmental Technologies, Inc.
Win St.
QC SUMMARY REPORT
ENW1 10UN1�NTALT-tzUhNQLr3G1Z5, 41C
Cuyahoga Falls, Ohio 44223
.insf�ytirdl' Lalrorwrartes TEL: [phone] FAX.- [phone]
WO#: 19010535
Website: http://Www.settek.com
24-Jan-19
Client:
Synagro
Project:
Statesville
BatchID: R93465
Sample ID MB-R93465
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 93465
Client ID: PBW
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908902
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive ND 25.0
Sample ID LCS-R93465
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 93465
Client ID: LCSW
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908903
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive 4620 25.0 4800 0 96.2 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is Original
p greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 22 of 27

Summit Environmental Technologies, Inc. sumbAlffir 3310 Win St. QC
SUMMARY
REPORT
EPh1l11t0tJh1EMTAL$ECHNGLOGICS, liar Cuyahoga Falls, Ohio 44223
llrrat�cic�^P L�ttant'�7fr3Pin_ s: TEL: [phone] FAX.- [phone]
WO#: 19010535
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: R93510
Sample ID CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@21.6C
Prep Date:
RunNo: 93510
Client ID: LCSS
Batch ID: R93510
TestNo: SW9045D
Analysis Date: 1/17/2019
SegNo: 1911700
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighL]mit RPD Ref Val
%RPD RPDLim]t Qua]
pH 7.0 7.0 0 101 90 110
mple ID CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u. _21.00
Prep Date:
RunNo: 93510
ent ID: LCSS
Batch ID: R93510
TestNo: SW9045D
Analysis Date: 1/17/2019
SegNo: 1911706
alyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 90 110
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 23 of 27
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Sumiant Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
EP;t+I 2i7►Jrd�r•.TAL `i �CT6t�OLi�GI�a, INC. Cuyahoga Falls, Ohio 44223
WO#: 19010535
Af''WytlCaP LauOfellUYlo!3TEL:[phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93510
Sample ID LCS-R93510
SampType: LCS
TestCode: pH_0i1(9045 Units: s.u. o(21.6C
Prep Date:
RunNo: 93510
'lient ID: LCSW
Batch ID: R93510
TestNo: SW9045D
Analysis Date: 1/17/2019
SegNo: 1911010
5,nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0 0 101 90 110
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 24 of 27

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
M9 SUMMIT 3310 Win St.
1 C,t'Iili)fJPalEtTrAt--T—rCM0LC}GIZ--r, INC. Cuyahoga Falls, Ohio 44223 WO#: 19010535
AnafyUcLf La.borat000s TEL: [phone] FAX- [phone]
Website: htto://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93510
Sample ID 19010626-004ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@20.1C
Prep Date:
RunNo: 93510
client ID: Batch=
Batch ID: R93510
TestNo: SW9045D
Analysis Date: 1/17/2019
SegNo: 1911018
analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH
7.5
7.6 1.1 5 W
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 25 of 27

Sumlmit Environmental Technologies, Inc. Analysis Request/Chain of Custody
3310 Win Street For Summit Environmental Technologies, Inc. use only
M9 Cuyahoga Falls, Ohio 44223 Tel: [phone] Fax: [phone] Page of- SET' No.
116(
Company Name (Please Print) Project Name Ct� PdE'8fl1ewlCS.Sni� Methods;
�y j.
S A r V 5+R SV\`1q— I I --
Company dd - Project Address
2$�1 is.sitr K4
oC=SWle-WL Z G
Client Phone Na Report to
Client Fax Na. PleaselFaxlResultiZ
PO#
d
a 11
Client Email Please Email Resit 1 /
Quote No.
Contact Person
LA
Sampled by
Check if Ohio V.AP samples ✓ ❑
E
l
date_
Time' •
E
I Sample Identification
I
r
z
""
Collected
Collected
0
C.0
:5 n
m•... rat
l
Aoslvtiral
Rnx
NNE
ME
:
ONE
MENOMINEE
MENEMEN
IN
IMMEMINIMMINEM
MENNEN
IN
10�w
M
MEN
IN ROMEO MM.
White and yellow pires shoulet accompany samples - uu iaooratory, 1 nc cnem rcunm — p,ae party.
t,n r A�.1. r n l d
Page 26 of 27
121450
age of 1

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
c^h',�I{?OtJte7��lT,4L`s c!thOtn.;ha;lr�4 . Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Amai! lt'lcal L-abonsf rfee TEL: [phone] FAX' [phone]
Website: http://www.settek.com
Client Name: SYN-NC-27028 Work Order Number: 19010535 RcptNo: 1
Logged by: Rachel Thomas 1/10/2019 10:15:00 AM
Completed By: Christopher Livengood 1/10/2019 3:02:10 PM 44
Reviewed By: Jennifer Woolf - 2 1/10/2019 3:09:39 PM
Chain of Custody
1. Is Chain of Custody complete?
2. How was the sample delivered?
Log In
3. Coolers are present?
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >0° C to 6.0°C
7, Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
g. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 114 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Hand/in_g (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
d❑
No ❑
Not Present ❑
UPS
Yes
d❑
No ❑
NA ❑
Yes
0
No ❑
Yes
❑
No ❑
Not Present 0
Signed By:
Yes
0
No ❑
NA ❑
Yes
W
No ❑
NA ❑
Yes
0
No ❑
Yes
W
No ❑
Yes
W
No ❑
Yes
❑
No Se
NA ❑
Yes
❑
No ❑
No VOA Vials 0
Yes
❑
No 0
Yes
W
No ❑
Yes
W
No ❑
Yes
W
No ❑
Yes
R]
No ❑
Yes ❑ No ❑ NA W
Person Notified: Date
By Whom: f Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
I Seal No
Seal Date
Signed By
1 13.1
Goodl
Not Present
Page 27 of 27

RDsummiat
cF;�'Ii?QNIrI=FJTAL `S�t:Ft6rti7l.13{;ir$, 9{�tC.
i�n6ftytical tetioraiorl€r.
January 24, 2019
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Statesville
Dear Erik Bruce:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: htto://Www.settek.com
Order No.: 19010534
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/10/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
r
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 28

Summit Environmental Technologies, Inc. Case Narrative
SUMAMIT 3310 Win St.
EN V1RON1.15MTALTEC}tNO (}C,i S, INC Cuyahoga Falls, Ohio 44223 WO#: 19010534
M9 A."?aI rtical L aboraforfas TEL: [phone] FAX.- [phone]
Website: htto:Ilwww.settek.com Date: 1/24/2019
CLIENT: Synagro
Project: Statesville
WorkOrder Narrative:
19010534: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19010534-001a TCLP-SVOC-CPest(8081B): The CCV (Batch R93761) exhibits high recovery for
Methoxychlor. All samples are ND
19010534-001a TCLP-SVOC-CPest(8081B): The ICV (Batch R93761) exhibited high recovery for
Methoxychlor. The associated samples are ND for Methoxychlor.
Analytical Sequence QC Notes:
MB-35513 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
LCS-35513 SVOC-BNA_TCLP(8270): LCS-35513 exhibited low recovery of Surrogate: 2-
Original
Page 2 of 28

Summit Environmental Technologies, Inc. Case Narrative
SUMMAIT 3310 Win St.
Et VIROt, Wb WTALTECHNO[-[} ;l S, INC. Cuyahoga Falls, Ohio 44223 wo#: 19010534
r1nafirGleal Laboralarlde TEL: [phone] FAX.- [phone]
Website: hitn:llwww.settek.com Date: 1/24/2019
CLIENT: Synagro
Project: Statesville
Fluorophenol.
LCS-35513 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
Original
Page 3 of 28

Summit Environmental Technologies, In. Qualifiers and Acronyms
Mfl sumfort 3310 Win S
€f4lrlf?t]ldP+1 lTAL FCrihtiSl t).e ar5,'hdC. Cuyahoga Falls, Ohio 442� WO#: 19010534
AiTtrrvUcal Laboraloyfe TEL: [phone] FAX.- (330) 253-446
Website: httD:11www.settek.co. Date: 1/24/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded. Not Clean Water Act compliant.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
In Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
W Samples were received outside temperature limits (0' — 6° C). Not Clean Water Act compliant.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximurn Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 28

Summit Environmental Technologies, Inc.
S, rom I T 3310 Win St.
^clflrl;rriNht�P1iAL SGC?iN01.(}�i«S, 9Ptti, Cuyahoga Falls, Ohio 44223
An rfyticfll tabnralorfeE TEL: [phone] FAX.• [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: Statesville
Lab SampleID Client Sample ID
19010534-001 3rd Creek WWTP
Tag No Date Collected
1/7/2019 9:05:00 AM
Workorder
Sample Summary
WO#: 19010534
24-Jan-19
Date Received Matrix
1/10/2019 10:15:00 AM Solid
Page 5 of 28

Summit Environmental Technologies, Inc. DATES REPORT
R9 SUMMIT3310 Win St.
ENVIIIOWAI�IATuL'7EC16?40U5m1 s, 1t.C,. Cuyahoga Falls, Ohio44223
a WO#: 19010534
uh�tlt<�1' irrt�at'�toYtca� TEL: [phone] FAX.- [phone]
�?
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date
Analysis Date
19010534-OOIA 3rd Creek WWTP 1/7/2019 9:05:00 AM Solid Ignitability of Solids (SW-846: 1030)
1/11/2019 11:00:00 AM
pH (SW9045D)
1/17/2019 3:09:04 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
1/14/2019 11:38:00 AM
Reactive Sulfide (9034)/7.3.4.2
1/14/2019 11:08:00 AM
TCLP Herbicides Analysis (SW1311/81/10/2019 5:44:59 PM
1/11/2019 5:00:00 PM
1/18/2019 7:24:00 PM
TCLP Mercury Analysis (SWI311/7471/10/2019 5:44:59 PM
1/16/2019 11:30:00 A
1/16/2019 4:46:00 PM
TCLP Metals Analysis (SW1311/6010.1/10/2019 5:44:59 PM
1/14/2019 8:25:00 AM
1/14/2019 4:36:23 PM
TCLP Pesticides Analysis (SW1311/8(1/10/2019 5:44:59 PM
1/15/2019 2:45:00 PM
1/23/2019 3:21:00 AM
TCLP Semi-Volatiles Analysis 1/10/2019 5:44:59 PM
1/14/2019 10:45:00 A
1/16/2019 3:42:00 PM
(S W 1311 /8270)
—
TCLP Semi-Volatiles Analysis 1/10/2019 5:44:59 PM
1/14/2019 10:45:00 A
1/16/2019 4:59:00 AM
(S W 13 I 1 /8270)
AA
TCLP Volatiles Analysis
1/10/2019 5:46:19 PM
1/14/2019 4:39:00 PM
Original
Page 6 of 28

Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
MSUM101ir
Ehtt1110NM--- •JTAL'rzCitN0LONG] Z-S, 1NC.
Cuyahoga Falls, Ohio 44223
(base report)
Anj: vt,'cal L aboratortes TEL: (330)
253-8211 FAX.- [phone]
WO#: 19010534
Website: htta://www.settek.com
Date Reported: 1/24/2019
CLIENT: Synagro
Tag Number:
Matrix: SOLID
Collection Date:
1/7/2019 9:05:00 AM
Lab ID: 19010534-OOIA
Project: Statesville
Client Sample ED 3rd Creek WWTP
Analyses Result
RL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
0.00200
mg/L
1 1/16/2019 4:46:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW601OD
SW3010A Analyst: KMO
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND
0.500
mg/L
1 1/14/2019 4:36:23 PM
TCLP Barium(Ba) ND
5.00
mg/L
1 1/14/2019 4:36:23 PM
TCLP Cadmium(Cd) ND
0.100
mg/L
1 1/14/2019 4:36:23 PM
TCLP Chromium(Cr) ND
0.200
mg/L
1 1/14/2019 4:36:23 PM
TCLP Lead(Pb) ND
0.500
mg/L
1 1/14/2019 4:36:23 PM
TCLP Selenium(Se) ND
0.0500
mg/L
1 1/14/2019 4:36:23 PM
TCLP Silver(Ag) ND
0.500
mg/L
1 1/14/2019 4:36:23 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND
0.0800
mg/L
2 1/16/2019 3:42:00 PM
2,4,5-Trichlorophenol ND
0.200
mg/L
2 1/16/2019 3:42:00 PM
2,4,6-Trichlorophenol ND
0.200
mg/L
2 1/16/2019 3:42:00 PM
2,4-Dinitrotoluene ND
0.0400
mg/L
2 1/16/2019 3:42:00 PM
o-Cresol ND
0.200
mg/L
2 1/16/2019 3:42:00 PM
m/p-Cresol(s) ND
0.200
mg/L
2 1/16/2019 3:42:00 PM
Cresols, Total ND
4.00
mg/L
2 1/16/2019 3:42:00 PM
Hexachloro-1,3-butadiene ND
0.0160
mg/L
2 1/16/2019 3:42:00 PM
Hexachlorobenzene ND
0.0400
mg/L
2 1/16/2019 3:42:00 PM
Hexachloroethane ND
0.0800
mg/L
2 1/16/2019 3:42:00 PM
Nitrobenzene ND
0.0800
mg/L
2 1/16/2019 3:42:00 PM
Pentachlorophenol ND
0.200
mg/L
2 1/16/2019 3:42:00 PM
Pyridine ND
0.200
mg/L
2 1/16/2019 3:42:00 PM
Surr: 2-Fluorophenol 40.9
10 - 109
%Rec
2 1/16/2019 3:42:00 PM
Surr: Phenol-d6 47.2
10 - 109
%Rec
2 1/16/2019 3:42:00 PM
Surr: Nitrobenzene-d5 57.6
19 - 120
%Rec
2 1/16/2019 3:42:00 PM
Surr: 2,4,6-Tribromophenol 65.1
10 - 120
%Rec
2 1/16/2019 3:42:00 PM
Sun-: 2-Fluorobiphenyl 58.2
22 - 117
%Rec
2 1/16/2019 3:42:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
O RSD is greater than
RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 7 of 28

Summit Environmental Technologies, Inc. Analytical Report
sumfolpt 3310 Wirt St.
e14;rI tON1.1EYil"AL fiEC}t11C11- S I S,1NO Cuyahoga Falls, Ohio 44223 (base report)
,drraFytdcal Laboratcrtes- TEL: [phone] FAX.- [phone] WOM 19010534
Website: http://Www.settek.com Date Reported: 1/24/2019
CLIENT:
Synagro Tag Number:
Matrix:
SOLID Collection Date: 1/7/2019 9:05:00 AM
Lab ID:
19010534-OOIA
Project:
Statesville
Client Sample ID 3rd Creek WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14
101 34 - 116
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
SW8270D SW351OC Analyst: BJH
%Rec 2 1/16/2019 3:42:00 PM
SW8081 SW351OC Analyst: MES
Chlordane, total
ND
0.0250 mg/L
10
1/23/2019 3:21:00 AM
Toxaphene
ND
0.0500 mg/L
10
1/23/2019 3:21:00 AM
Endrin
ND
0.00500 mg/L
10
1/23/2019 3:21:00 AM
gamma-BHC
ND
0.00500 mg/L
10
1/23/2019 3:21:00 AM
Heptachlor
ND
0.00500 d mg/L
10
1/23/2019 3:21:00 AM
Heptachlor epoxide
ND
0.00500 d mg/L
10
1/23/2019 3:21:00 AM
Methoxychlor
ND
0.00500QV+QC+mg/L
10
1/23/2019 3:21:00 AM
Surr: TCMX
19.9
10 - 119 %Rec
10
1/23/2019 3:21:00 AM
Surr: DCB
32.9
10 - 119 %Rec
10
1/23/2019 3:21:00 AM
NOTES:
The CCV (Batch R93761) exhibits high recovery for Methoxychlor. All samples are ND
The ICV (Batch R93761) exhibited
high recovery for Methoxychlor. The associated samples are ND for Methoxychlor.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW131118151)
2,4-D
2,4,5-TP
Surr: DCAA
SW8151A SW8151A Analyst: MES
ND 1.00 mg/L 1 1/18/2019 7:24:00 PM
ND 0.500 mg/L 1 1/18/2019 7:24:00 PM
70.7 20 - 140 %Rec 1 1/18/2019 7:24:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B SW1311M Analyst: CTB
TCLP VOLATILES
ANALYSIS
1,1-Dichloroethene
ND
0.125
mg/L 25 1/14/2019 4:39:00 PM
1,2-Dichloroethane
ND
0.125
mg/L 25 1/14/2019 4:39:00 PM
MEK
ND
0.625
mg/L 25 1/14/2019 4:39:00 PM
Benzene
ND
0.125
mg/L 25 1/14/2019 4:39:00 PM
Carbon tetrachloride ND
0.125
mg/L 25 1/14/2019 4:39:00 PM
Chlorobenzene
ND
0.125
mg/L 25 1/14/2019 4:39:00 PM
Chloroform
ND
0.125
mg/L 25 1/14/2019 4:39:00 PM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
M Manual Integration used to deterrrunc area response
MC
Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND
Not Detected
O RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL Permit Limit Original
R
RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 8 of 28

Summit Environmental Technologies, Inc. Analytical Report
fn sumfolir3310 Win St.
t h{Vlf?QNhl=ta7 L a C!tNpt_[) ,a4_S, INC Cuyahoga Falls, Ohio 44223 (base report)
Analy0cal Laboratorl&e TEL: [phone] FAX: [phone] WO#: 19010534
Website: http://Www.settekeom Date Reported: 1/24/2019
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/7/2019 9:05:00 AM
Lab ID: 19010534-001A
Project: Statesville
Client Sample ID 3rd Creek WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Tetrachloroethene
NC
Trichloroethene
N❑
Vinyl chloride
NC
Surr: 4-Bromofluorobenzene
97.5
Surr: Dibromofluoromethane
104
Surr: Toluene-d8
102
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
RCI-SOLID-W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
RCI-SOLID-W/ IGNITABILITY1030
PH (SW9045D)
pH
5.4
RCI-SOLID-W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
SW8260B SW1311 M Analyst: CTB
0.125
mg/L
25
0.125
mg/L
25
0.0500
mg/L
25
70 - 130
%Rec
25
70 - 130
%Rec
25
70 - 130
%Rec
25
SW9014
0.485
mg/Kg
1
SW1030
1
SW9045D
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
s.u.@21.00 1
SW9034
25.0 mg/Kg 1
1/14/2019 4:39:00 PM
1114/2019 4:39:00 PM
1/14/2019 4:39:00 PM
1/14/2019 4:39:00 PM
1/14/2019 4:39:00 PM
1/14/2019 4:39:00 PM
Analyst: MS
1/14/2019 11:38:00 AM
Analyst: AJT
1 /11 /2019 11:00:00 AM
Analyst: VVK
1/17/2019 3:09:04 PM
Analyst: MS
1/14/2019 11:08:00 AM
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 28

Summit Environmental Technologies, Inc.
Accreditation
Program
ffl sus"Milt 3310 Win St.
Anal tes Report
y
PA(l110tJ�e ENTALTrEC}i(Vt71.QG]>$,INC.-
Cuyahoga Falls, Ohio 44223
JInaty0cal L3borworw
TEL: [phone] FAX.- [phone]
WO#:
19010534
Wehsite: htto://Www.settekcom
24-Jan-19
Client: Synagro
State: NW
Project: Statesville
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19010534-OOIA Solid
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Solid
TCLP Herbicides Analysis (SW1311/8151)
2,4,5-TP
A
Solid
TCLP Herbicides Analysis (SW1311/8151)
2,4-D
A
Solid
TCLP Herbicides Analysis (SW1311/8151)
DCAA
A
Solid
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Solid
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Solid
TCLP Metals Analysis (SW1311/6010)
Barium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Lead
A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Solid
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
ganuna-BHC
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Tetrachloro-m-xylene
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Tribromophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl
A
Solid
TCLP Senu-Volatiles Analysis (SW1311/8270)
2-Fluorophenol
A
Original #1
Page 10 of 28

-
Summit Environmental Technologies, Inc.
Accreditation
Program
3310 Win St.
Anal te5 Report
y p
EPAIKIONh1Eri1Tt1LTiC1t6VOLij4;i
$,frtc, Cuyahoga Falls, Ohio44223
AJ7,Ff rttcarl Laboralort&e
TEL: [phone] FAX.- [phone]
WOM
19010534
Website: http://Www.settek-.com
24-Jan-19
Client: Synagro
State: NW
Project: Statesville
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19010534-001A Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1-311/8270)
3,4-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW131-1/8270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Solid
TCLP Senii-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene-d5
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Phenol-d6
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
p-Terphenyl-d14
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Solid
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-Butanone
A
Solid
TCLP Volatiles Analysis
4-Bromofluorobenzene
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbon tetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chloroform
A
Solid
TCLP Volatiles Analysis
Dibromofluoromethane
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Toluene-d8
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl chloride
A
Original #1
Page 11 of 28

summuirSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENWIiLOWtit Et-irAL1—L:Gttt190L1G1ZS,WC Cuyahoga Falls, Ohio44223
an.sfyNrf1' Lal14YvtorJos TEL: [phone] FAX.- [phone]
Wok 19010534
Website: htto://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: 35472
Sample ID MB-35472
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date: 1/10/2019
RunNo: 93332
Client ID: PBS
Batch ID: 35472
TestNo: SW8260B SW1311M
Analysis Date: 1/11/2019
SegNo: 1903835
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
464
Surr: Dibromofluorom ethane
602
Surr: Toluene-d8
496
500.0 92.8 70 130
500.0 120 70 130
500.0 99.2 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 12 of 28

suftualirSummit
Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
EM'lI1L01V,1Em':T&u'i i_�rv�dot.x�Ga�S, tr�G Cuyahoga Falls, Ohio 44223
Anaty[ic:,P Ler.baratnroo,� TEL: [phone] FAX.- [phone]
WO#: 19010534
Website: httn://H ww.settek.com
24-Jan-19
Client:
Synagro
Project:
Statesville
BatchID: 35523
2,4-D
ND 1.00
0.500
0 78.4
43.8
130
2,4,5-TP
ND 0.500
0.500
0 62.9
51.5
ill
Surr: DCAA
357
500.0
71.4
34.2
150
2,4-D ND 1.00 0 0 d
2,4,5-TP ND 0.500 0 0
Surr: DCAA 320 500.0 64.0 20 140
2,4-D
ND
1.00 0.500
0 100
37
105
W
2,4,5-TP
ND
0.500 0.500
0 89.8
38
106
W
Surr: DCAA
567
500.0
113
20
140
W
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 13 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc.M9 QC SUMMARY REPORTsumm-13310 Win St.
ElM+t'IitOWAM rlTAL TECHNOL3Gtrs, JNC Cuyahoga Falls, Ohio 44223
WO#: 19010534
TEL [lc•�i L�.t�orasnrle+% : [phone] FAX.- [phone]
Website: http://Www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: 35523
Sample ID 19010307-001amsd
SampType: MSD
TestCode: tclp�svoc-her Units: mg/L
Prep Date: 1/11/2019
RunNo: 93601
Client ID: BatchQC
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914646
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD.Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0.500 0 83.7 37 105 0 0 30 W
2,4,5-TP ND 0.500 0.500 0 71.5 38 106 0 0 30 W
Surr: DCAA 453 500.0 90.6 20 140 0 W
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is Original
p greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 14 of 28

sutomiluSummit
Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
EN4rIliCAMEr•:TaiL.6ECIMOLLIGH2_S,INC Cuyahoga Falls, Ohio44223
ft-ui(yOcal L2abarjtonos TEL: [phone] FAX.- [phone]
WO#: 19010534
Website: http://www.settek.com
24-Jan-19
Client:
Synagro
Project:
Statesville
BatchID: 35549
TCLP Mercury ND 0.00200
TCLP Mercury ND 0.00500
TCLP Mercury 0.00401 0.00200 0.00400 0 100 80 120
Sample ID 19010659-002AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: BatchQC
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909440
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00468 0.00200
0.00400 0.000380 108 75
125
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected
O
RSD is.greater than RSDlimit Original
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 15 of 28

Summit Environmental Technologies, Inc.Rn summlir 3310 Win St. QC SUMMARY REPORT
c �SrltiblJPi1! laT1xL'P�Gr1A10L�3 lti.i, j.c Cuyahoga Falls, Ohio44223
WO#: 19010534
Azrt�tiauP Labor�tnri�,� TEL: [phone] FAX.- [phone]
r+
Website: http:/1www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: 35549
Sample ID 19010659-002AMS
SampType: MS
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: BatchQC
Batch ID: 35549
TestNo:
SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909440
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sample ID 19010659-002AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/16/2019
RunNo: 93469
Client ID: Batch=
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909441
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
T'CLP Mercury 0.00462 0.00200 0.00400 0.000380 106 75 125 0.00468 1.29 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PI, Permit Limit R RPD outside accepted recovery limits
Page 16 of 28

Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
eC?4'Iiit�tJhiCA:Tl�L'a cGasetiJOl i7G1�S, if-zc Cuyahoga Falls, Ohio 44223
Apef��Ovff Lal�crwormm WO#: 19010534
y TEL: [phone] FAX.• [phone]
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: R93297
mple ID LCS-R93297
SampType: LCS
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
ent ID: LCSS
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902691
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability 8.08 7.240 0 112 70 130
Sample ID 19010438-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: Batch=
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902693
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability non-flammable 0 0 20.
mple ID 19010439-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
ant ID: Batch=
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902695
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19010440-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: Batch=
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902697
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 17 of 28

sumfArrSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
E�W[110fltIEHTALTctrM0t_0GjE5,dNC, Cuyahoga Falls, Ohio44223
WO#: 19010534
11.rP.riftlCJ1' LexbnratoYoo-ei TEL: [phone] FAX.• [phone]
Website: http://www.settek-.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: R93297
Sample ID 19010440-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902697
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sample ID 19010531-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902699
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID 19010532-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902701
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
gnitability non-flammable 0 0 20
Sample ID 19010533-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902703
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability
non-flammable
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not -Detected
PL Permit Limit
Page 18 of 28
0 0 20
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc.ffl SUMMIT 3310 Win St. QC SUMMARY REPORT
''ENW11'i0mtort-iTAL ECrirdOWGIC--5,Jflr, Cuyahoga Falls, Ohio44223
ArpiN Ocu/ Laboraron0!] WO#: 19010534
TEL: [phone] FAX.- [phone]
Website: http://xww.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: R93297
Sample ID 19010534-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
:lient ID: 3rd Creek WWTP
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902705
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Ignitability non-flammable 0 0 20
Sample ID 19010535-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
client ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1/11/2019
SegNo: 1902707
kna[yte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability
non-flammable
0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 19 of 28

Sir Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENWIrL01040-ITAL TccraNOLOGiZz5, JFtG. Cuyahoga Falls, Ohio 44223
Aj7aiytical Ladorwordo!3 TEL: [phone] FAX.- [phone] WO#: 19010534
Website: http://www.settek-com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93390
Sample ID 19010535-01AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
Client ID: BatchQC
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906045
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 8.98 0.490 10.00 0 89.8 81.6 122
Sample ID 19010535-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
Client ID: BatchQC
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906046
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.09 0.495 10.00 0 90.9 81.6 122
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to detemune
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 20 of 28

sum"wr
Summit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
Et%kV]110tJh1r-MTAL7cc1INOLOGIES,J.NG
Cuyahoga Falls, Ohio44223
arrMyticaP Laborwnrio!� TEL:
[phone] FAX.- [phone]
WO#: 19010534
Website: http://www.settek.com
24-Jan-19
Client:
Synagro
Project:
Statesville
BatchED: R93390
Sample ID LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 93390
client ID: LCSW
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906029
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.57 0.490 10.00 0 95.7 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 21 of 28

Summit Environmental Technologies, Inc.RD SUMMINt 3310 Win St. QC SUMMARY REPORT
chhl�lY�i?hltArAlT4L'FEG}y,p��3Glr, INC, Cuyahoga Falls, Ohio 44223
WO#: 19010534
:knr�yticai L:aG4ratorlcj!; TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93465
Sample ID 19010535-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
Client ID: BatchQC
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908916
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 4210 25.0 4800 0 87.7 80 120
Sample ID 19010535-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
Client ID: BatchQC
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908917
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4320 25.0 4800 0 90.0 80 120 4210 2.58 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 22 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc.fn sulftimlir 3310 Win St. QC SUMMARY REPORT
�C•t4'IFL tJh1�t•:T L`�crtNo��� f>.,, INC Cuyahoga Falls, Ohio 44223
dnafr,t,oLf Laborxorlos' TEL: [phone] FAX.- [phone] WO#: 19010534
Website: http://www.settek.com 24-Jaya-19
Client: Synagro
Project: Statesville BatchED: R93465
ample ID MB-R93465
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 93465
lient ID: PBW
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908902
nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
;ulfide, Reactive ND 25.0
Sample ID LCS-R93465
SampType: LCS
TestCode:
Sulfide,React Units: mg/L
Prep Date:
RunNo: 93465
Client ID: LCSW
Batch ID: R93465
TestNo:
SW9034
Analysis Date: 1/14/2019
SegNo: 1908903
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
ulfide, Reactive 4620 25.0 4800 0 96.2 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 23 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
fn sulardist 3310 Win St.
Es, 4�Itt�5NwlKrarxL"caetiol i3G1�3, 3h:c Cuyahoga Falls, Ohio 44223
A MFlyfloaf L.aboreirnn5g TEL: [phone] FAX.- [phone] WO#: 19010534
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93510
mple ID CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@21.6C
Prep Date:
RunNo: 93510
ent ID: LCSS
Batch ID: R93510
TestNo: SW9045D
Analysis Date: 1/17/2019
SegNo: 1911700
alyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 90 110
Sample ID CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@21.00
Prep Date:
RunNo: 93510
Client ID: LCSS
Batch ID: R93510
TestNo: SW9045D
Analysis Date: 1/1712019
SegNo: 1911706
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
pH 7.0 7.0 0 101 90 110
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 24 of 28
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
P71�1 2iaNhtLtal'eiL %�r6&It7L�31 $, INC. Cuyahoga Falls, Ohio 44223
ff1summilt
3310 Win St.
['�
WO#: 19010534
.%infrif�tic�1� L?,7jC�.YvrUt'i�aS TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchED: R93510
sample ID LCS-R93510
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@21.6C
Prep Date:
RunNo: 93510
;lient ID: LCSW
Batch ID: R93510
TestNo: SW9045D
Analysis Date: 1/17/2019
SegNo: 1911010
knalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
pH
7.0
7.0 0 101 90 110
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is Original
p greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 25 of 28

Summit Environmental Technologies, Inc.!BSUNOMIT 3310 Win St. QC SUMMARY REPORT
�DP'Ii4�tiA1PdCldTtiL'TC�t6wlt�LrsGIS, �h�> Cuyahoga Falls, Ohio 44223
WO#: 19010534
.ln4�ty[icaP Layoratorloi TEL: [phone] FAX.- [phone]
Website: http•//www.settek.com 24-Jan-19
Client: Synagro
Project: Statesville BatchID: R93510
Sample ID 19010626-004ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@20.1C
Prep Date:
RunNo: 93510
Client ID: BatchQC
Batch ID: R93510
TestNo: SW9045D
Analysis Date: 1/17/2019
SegNo: 1911018
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
7.5
7.6 1.1 5 W
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected O RSD is Original
P greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits
Page 26 of 28

Summit Environmental Technologies, Inc.
3310 Win Street Analysis Request/Chain of Custody
Cuyahoga Falls, Ohio 44223 Tel: 330.253.821 I Fax: [phone] For Summit Environmental Technologies, Inc. use only,
Page of Company Name (please Print) No. m) Project Name
Analytical Parameters and Methods;
Comps y g ss Project Address
-TT
a 11-
..�
Client Phone No_ Report to 0
33 (- -1a3 SI 9) ;4.
impled by
0
Sample Identification
i� ass
a
w
�
' Samples ✓
❑
rn on
�
c
Date
Collected
'lime
-
E:`�
°J
,
d
Colfe "
C7
Cg
m.
L'
(�,
1.0
Received in tab by: bate Time Must he Bush Requested By: approved
Date' by rub manager
White and yellow pages should accompany samples to the laboratory.
Page 27 of 28
Notes/Commtnts:
nAM^ f r Smte ofmpl: Ori��ti
XJ/!*ems I a rOIiCOhfiIJANC@ Y
Clin'I R iC'.1'I ION itrj i) ES NO
h101/l0l9 REPOI:T'r0ST:�T (nWGNL YES
�J If YES
I,riivide pws' s,ru, .c Nipt�C)
"li non ann<tlic. , hic. aewnz.. ala„r k inappCcaM¢ uml •.ill o.n:.:, n, ow,,:wu.,r.,m,.
Thclainspnkp121451 9 j
Pae101

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
crti��Ii?L+tJFatchlrAL`iac!�cJols;� .,, �ft4.. Cuyahoga Falls, Ohio 44223 Sample Log -In Check List
A17jfyUcal Laboralorfos TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Client Name: SYN-NC-27028 Work Order Number: 19010534 RcptNo: 1
Logged by: Rachel Thomas 1/10/2019 10:15:00 AM + J'��—�
Completed By: Christopher Livengood 1/10/2019 2:58:17 PM
Reviewed By: Jennifer Woolf 1/11/2019 9:52:54 AM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lo_q /n
3,
Coolers are present?
Yes
d❑
No ❑
NA ❑
4.
Shipping container/cooler in good condition?
Yes
d❑
No ❑
Custody seals intact on shipping container/cooler?
Yes
❑
No ❑
Not Present ❑�/
No. Seal Date:
Signed By:
5.
Was an attempt made to cool the samples?
Yes
❑v/
No ❑
NA ❑
6,
Were all samples received at a temperature of >0° C to 6.0°C
Yes
W
No ❑
NA ❑
7,
Sample(s) in proper container(s)?
Yes
No ❑
8,
Sufficient sample volume for indicated test(s)?
Yes
No ❑
9,
Are samples (except VOA and ONG) properly preserved?
Yes
Se
No ❑
10.
Was preservative added to bottles?
Yes
❑
No 0
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No 0
13. Does paperwork match bottle labels?
Yes
se
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
No ❑
15. Is it clear what analyses were requested?
Yes
0
No ❑
16. Were all holding times able to be met?
Yes
0
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA ❑d
Person Notified: Date
By Whom: l�— Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions: -
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
13.1
Goodl
Not Present
Page 28 of 28

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP WQ Permit Number: WQ 0016247
WWTP Name: Statesville Fourth Creek WWTP NPDES Number: NC 0031836
Monitoring Period: From 01/01/19 To 03/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (tune/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt 4/1) (No Prior Test) Alt 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirnhle to niternntive norfarmod Whi— A nr C7nss R) emmnlete the fnllnwina mnnitnrina Ilata-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10tothe 6"
MPN
17,778
18955
19835
MPN/g
0
Quarterly
Grab
Sm9221ce
Colifor i
power per gram
- 2006
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0pdon/Ah. 1
Option/Alt 2
Option/Alt. 3 Option/Alt 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying —Unstable)
Option/Alt 9
Option/Alt 10
(Infection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that fire pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inc d g fine and' rent"
Andy Smith O s Manager l ��
Pr are ame and Title (y e or print) Land Applie Name and Title (if applicable) (type or print)
Signature of Preparer* Da a Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results STATESVILLE
ANALYTICAL
)ynagro
284 Boger Rd. -
Mocksville, NC 27028
Receive Date:
01/14/2019
Reported:
01/15/2019
For:
4th Creek
Comments:
Geometric Mean 18,955 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190114-18-01
Fecal Coliforms
1
19672
MPN/g
SM92210E-2006
01/14/2019
WC
190114-18-01
Percent Solids
1
12.2
%
SM254OB-2011
01/14/2019
WC
190114-18-02
Fecal Coliforms
2
19835
MPN/g
SM92210E-20W
01/14/2019
WC
190114-18-02
Percent Solids
2
12.1
%
SM254OB-2011
01/14/2019
WC
190114-18-03
Fecal Coliforms
3
18898
MPN/g
SM92210E-2006
01/14/2019
WC
190114-18-03
Percent Solids
3
12.7
%
SM254OB-2011
01/14/2019
WC
190114-18-04
Fecal Coliforms
4
19355
MPN/g
SM92210E-2006
01/14/2019
WC
190114-18-04
Percent Solids
4
12.4
%
SM254OB-2011
01/14/2019
WC
10114-18-05
Fecal Coliforms
5
19200
MPN/g
SM92210E-2006
01/14/2019
WC
190114-18-05
Percent Solids
5
12.5
%
SM254OB-2011
01/14/2019
WC
190114-18-06
Fecal Coliforms
6
17778
MPN/g
SM92210E-2006
01/14/2019
WC
190114-18-06
Percent Solids
6
13.5
%
SM254OB-2011
01/14/2019
WC
190114-18-07
Fecal Coliforms
7
18045
MPN/g
SMMICE-2606
01/14/2019
WC
190114-18-07
Percent. Solids
7 .
13.3
%
SM25409-2011
01/14/2019
WC
Respectfully submitted,
�O.e"-W�ft' J")')')t )
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190114-18-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-18-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-18-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thlosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-18-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-18-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 o Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
ampie Number 190114-18-06 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate. Received on Ice
Chemicals in containers, lab
Sample Number 190114-18-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Client:
.._JC ri&CLD
STATESVFLLEAPTALY7'ICAX.
/�
Address: ; ? q 60G e /Z �Q
d 7
122 Court St=t • P.O. Box 228
Statesville. NC 2M7
{ t 1
aC tC .S V: t E e f �f C— p� � D a �
[phone]
Chain of
Contact Person: /LAG So Phone # 9d y�- FAX# 336
Po # r� -t� G Requisitioned by: � �rs+g �)
Custody Record
Customer
SampleID#
Lab-0D#
Time Sampled
{crap Only)
Dale Sampled
(Grab Only)
12
a
Matrix
ParamMrs eraquestedforanffiysis
J �
lmla
Relinquished by:
Received by: ��
Relinquished by:
Received by:
GOitlt !2 ite J�gmplinq
Time begin am, pm Date _ J /—
Time and am, pm Date _/ /_
Composite Sampling #2:
Time begin am, pm Date /
Time end am, pm Date! l_
Time l m, pm Date! l,(lj8 Sampled by: % } W t /f-,dL
Time �epm Date 1� Transported by:
Time am, pm Date _!_/^ Holding times met:
Time am, pm Date _l_/ Compliance work:
Mon -compliance work:
Lab Comments: Samples Transported On Ice:
fnittels:
00
N
N
O
C3
0
a

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
1 1/23/19 10:52 AM 1
300 Imilliliters
Beginning Temperature:
11.4
End Temperaturel
11.7
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
9.57
1
9.68
2
9.75
3
9.67
4
9.75
5
9.79
6
9.74
7
9.8
8
9.75
9
9.68
10
9.67
11
9.64
12
9.61
13
9.51
14
9.5
15
9.57
Slope: 0.0
Intercept: 9.7
Correlation Coefficient: 0.5
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Celsius
Celsius
0.63 mg Oxygen/hr
0.14 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1 0.24 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

9.75
9.7
a�
E
9c65
m
a�
O
v
m
2.6
0
N
N
9.55
9.5
9.45
9.4
y =-0.0105x + 9.7565
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Fourth Creek WW7
Biosolids Permit Number:
Date:
1 /24/2019
Digester Temperature:
12.8
Sampling Date/Time:
1/24/19 1:12 PM
Sampled By:
LC
Analysis Date/Time:
1/24/19 1:17 PM
Analyzed By:
BJ
Sample Volume:
300
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9.28
9.32
9.37
9.25
9.11
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
.2
0.0
9.3
0.8
liliters
rees Celsius
rees Celsius
1.39 mg Oxygen/hr
0.34 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate:1 0.54 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

9.4
9.3
9.2
a�
E
8.1
d
a
x
C�
m
>9
0
w
in
0
: •
8.7
8.5
y =-0.0232x + 9.3608
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.47
9.48
9.48
9.4
73
9.32
9.23
9.1
9.07
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1 /25/2019
10.7
5/19 1:01 PM
LC
5/19 1:08 PM
BJ
300 milliliters
11.1 Idegrees Celsius
11.9 Idearees Celsius
0.0
9.5
0.9
1.56 mg Oxygen/hr
0.37 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1 0.614 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

• e
9.5
9.3
c
m
x
Al
m
2.2
0
U)
cn
0
9.1
�o
y =-0.026x + 9.5633
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek \N
Biosolids Permit Number:
Date: 1 /28/2019
Digester Temperature: 15.7
Sampling Date/Time: 1/28/19 1:58
Sampled By:
Analysis Date/Time: 1j
Analyzed By:
Sample Volume:
9 2:02 PM
BJ
Beginning Temperaturel
16
End Temperaturel
15.5
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.77
1
7.66
2
7.61
3
7.58
4
7.54
5
7.43
6
7.72
7
7.79
8
7.81
9
7.79
10
7.76
11
7.69
12
7.55
13
7.59
14
7.61
15
7.61
Slope: 0.0
Intercept: 7.7
Correlation Coefficient: 0.0
iliters
rees Celsius
rees Celsius
Oxygen Uptake Rate: 0.05 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.01 mg Oxygen/g/hr
Average Temperature: 16 degrees Celsius
Temperature Correction Factor: 1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:1 0.02 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.9
7.8
7.7
7.5
7.4
7.3
7.2
y =-0.0009x + 7.6645
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
1 /29/2019
20.2
1 /29/19 1:00 PM
KG
1/29/19 1:13 PM
BJ
300 milliliters
Beginning Temperature:1 20.2
End Temperaturel 20.1
Dissolved Oxygen Level
(mg/1)
6.59
6.51
6.43
6.3
6.28
6.24
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
rees Celsius
rees Celsius
0.1
6.6
1.0
4.54 mg Oxygen/hr
0.97 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:1 0.97 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7
5
a�
E
m
tM4
x
O
m
0
0
w
0
3
2
1
0
y =-0.0757x + 6.6408
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
1 /30/2019
17.7
1/30/19 1:01 PM
LC
1/30/19 1:12 PM
BJ
300 milliliters
Beginning Temperature:1
17.3
End Temperature:1
16.9
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.12
1
7.04
2
6.99
3
6.98
4
7.01
5
6.95
6
6.94
7
6.93
8
6.87
9
6.8
10
6.74
11
6.73
12
6.7
13
6.66
14
6.63
15
6.58
Slope: 0.0
Intercept: 7.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
egrees Celsius
egrees Celsius
2.04 mg Oxygen/hr
0.48 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.59 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.2
7.1
7
6.9
a�
E
c
m
11
m
0
C4.7
6.5
6.4
6.3
y =-0.0339x + 7.1427
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
9.79
1
9.9
2
9.91
3
9.88
4
9.82
5
9.77
6
9.689
7
9.66
8
9.65
9
9.6
10
9.54
11
9.47
12
9.38
13
9.37
14
9.37
15
9.32
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
urth Creek WWTP
milliliters
degrees Celsius
deorees Celsius
1 /31 /2019
11.9
1/31/19 1:00 PM
RG
1/31/19 1:09 PM
BJ
300
12.3
12.4
0.0
9.9
1.0
2.49 mg Oxygen/hr
0.61 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1 1.05 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

10
9.7
E
8.6
a)
rn
iz
O
a
a)
2.5
0
0
L'x!
9.3
9.2
An
9
y =-0.0416x + 9.9856
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP WQ Permit Number: WQ 0016247
WWTP Name: Statesville Fourth Creek WWTP NPDES Number: NC 0031836
Monitoring Period: From 04/01/19 To 06/30/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class B complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61h
MPN
2917
9374
25,000
MPN/g
0
Quarterly
Grab
Sm9221ce
Coliform
power per gram
- 2006
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certificatiorrding fine and imprisonment."`
And Smith O s Manager b AllTSS
Pr are Name and Title type or print) Q-0—
Land App ier Name and Title (if applicable) (type or print)
/J& rj�jjj mi-- 9 11x 1 < w 7
ignature of Preparer* ate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
:ity of Statesville WWTP
PO Box 1111
Statesville, NC 28687
Receive Date:
05/16/2019
Reported:
11 /20/2019
For:
4th Creek
Comments:
Geometric Mean: 9374 MPN/g
STATESVILLE
ANALYTICAL
t-�
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190516-09-01
Fecal Coliforms
1
2917
MPN/g
SM92210E-2006
05/16/2019
CL
190516-09-01
Percent Solids
1
12.0
%
SM2540B-2011
05/16/2019
CL
190516-09-02
Fecal Coliforms
2
25000
MPN/g
SM92210E-2006
05/16/2019
CL
190516-09-02
Percent Solids
2
12.0
aka
SM254OB-2011
05/16/2019
CL
190516-09-03
Fecal Coliforms
3
18333
MPN/g
SM92210E-2006
05/16/2019
CL
190516-09-03
Percent Solids
3
12.0
%
SM2540B-2011
05/16/2019
CL
190516-09-04
Fecal Coliforms
4
14050
MPN/g
SM92210E-2006
05/16/2019
CL
190516-09-04
Percent Solids
4
12.1
%
SM254OB-2011
05/16/2019
CL
a0516-09-05
Fecal Coliforms
5
5674
MPN/g
SM92210E-2006
05/16/2019
CL
190516-09-05
Percent Solids
5
14.1
%
SM254OB-2011
05/16/2019
CL
190516-09-06
Fecal Coliforms
6
10484
MPN/g
SM92210E-2006
05/16/2019
CL
190516-09-06
Percent Solids
6
12.4
%
SM2540B-2011
05/16/2019
CL
190516-09-07
Fecal Coliforms
7
5691
MPN/g
SM92210E-2006
05/16/2019
CL
190516-09-07
Percent Solids
7
12.3
%
SM254OB-2011
05/16/2019
CL
Respectfully submitted,
�JRXWO(-,apt')
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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STATESVILLEANALYTICAL
122 Courtstreet • P.O. Box 228
Stawsville, NC 28687
[phone]
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Address: q XW C�
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Contact Person: L�� Phone # Q y - 'P0, us•4 FAX#
PO # Requisitioned by: i^Snme Date)
Custody Record
Customer
Sample IN(Grab
Lab -ID R
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Only)
Date Sampled
(Grab Only)
elan
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parameters requested for anarysis
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Received by:
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date ^l�l
Time end am, pm Date _/�
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date —/_/
Time
Time Q._•
Time
Time
Lab Comments:
am, pm Date
am, pm Date �/ ! LV_!LIV
am, pm Date _1_/
am, pm Date _/
Sampled by:
Transported by:
Holding times met:
Compliance work:
Non-compliance work:

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
3.71
3.55
3.46
3.35
3.28
2.95
2.86
2.78
2.63
2.56
2.49
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
milliliters
degrees Celsius
degrees Celsius
5/20/2019
22.3
5/20/19 8:06 AM
BD
5/20/19 8:09 AM
BD
300
22.3
22.7
0.1
3.6
1.0
5.01 mg Oxygen/hr
1.32 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 1.14 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4
3.5
3
9.5
c
m
x
a
1.5
1
0.5
0
y =-0.0834x + 3.7143
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Fou
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: &
Sampled By:
Analysis Date/Time: &
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
2.53
2.38
2.62
2.77
2.67
2.43
2.27
2_2
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
19 2:53 PM
KG
300 Imilliliters
rees Celsius
rees Celsius
0.0
2.8
0.7
1.95 mg Oxygen/hr
0.53 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:1 0.48 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

3.5
3
2.5
1.5
1
0.5
0
y =-0.0325x + 2.8378
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By.
Sample Volume
Beginning Temperature
End Temperature;
Dissolved Oxygen Level
3.41
3.25
3.09
2.57
2.37
2.56
2.52
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
5/23/2019
23.3
5/23/19 2:22 PM
KG
5/23/19 2:24 PM
KG
300
23.3
24.1
0.1
3.5
0.9
milliliters
Jegrees Celsius
Jegrees Celsius
6.40 mg Oxygen/hr
1.78 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 1.46 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4.5
4
3.5
3
E
c
m
5
O
a�
0
1.5
1
0.5
0
y =-0.1067x + 3.6533
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature
End Temperature
Dissolved Oxygen Level
3.6
3.49
1•
2.96
2.83
2.32
2.13
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
5/24/2019
21.9
5/24/19 7:20 AM
BD
5/24/19 7:27 AM
BD
300
21.9
22.3
0.1
3.8
1.0
milliliters
Jegrees Celsius
legrees Celsius
6.30 mg Oxygen/hr
1.63 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:1 1.48 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4.5
4
3.5
3
E
c
m
'5
O
��
1.5
1
0.5
a
y =-0.105x + 3.9323
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Fourth Creek WWTP
Biosolids Permit Number:
Date: 5/28/2019
Digester Temperature: 26.3
Sampling Date/Time: 5/28/19 10:50AM
Sampled By: BD
Analysis Date/Time: 5/28/19 12:00 AM
Analyzed By: BD
Sample Volume:1 300 milliliters
Beginning Temperature:1 26.3 Idegrees Celsius
End Temperaturel 25.8 Idegrees Celsius
Dissolved Oxygen Level
5.47
5.38
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
5.5
0.3
3.23 mg Oxygen/hr
1.06 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate:1 0.79 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

IIIIIIIIA:
.7
M
C�
m
>4
0
w
U)
3
2
1
0
y =-0.0539x + 5.5247
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By:
Analysis Date/Tim&
Analyzed By
Sample Volume
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)(mg/1)
0
5.98
1
5.88
2
5.77
3
5.65
4
5.55
5
6.45
6
5.35
7
5.24
8
5.15
9
5.02
10
4.87
11
4.9
12
4.85
13
4.81
14
4.77
15
4.72
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
5/29/2019
22.7
5/29/19 7:38 AM
BD
5/29/19 7:43 AM
BD
300
7222.7
3.1
0.1
6.0
0.9
milliliters
legrees Celsius
Jegrees Celsius
5.70 mg Oxygen/hr
1.44 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 1.24 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7
6
�6i
E
tM4
X
0
6
3
2
1
0
Y = -0.095x + 6.1178
Oxygen Uptake Rate Chart
A
J,
4�
L
1:
2 3 4 5 6 7 8 9 10 11 12 13 14 15
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
i
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
5/30/2019
22.2
5/30/19 7:34 AM
BD
5/30/19 7:39 AM
BD
300 milliliters
22.2 degrees Celsius
22.6 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/1)
0 5.61
1 5.45
2 5.32
3 5.22
4 5.13
5 5.04
6 4.95
7 4.88
8 4.8
9 4.74
10 4.68.
11 4.58
12 4.49
13 4.43
14 4.38
15 4.35
Slope: 0.1
Intercept: 5.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 4.90 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.36 mg Oxygen/g/hr
Average Temperature: 22 degrees Celsius
Temperature Correction Factor: 0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:1 1.23 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes The Calculation and the Spreadsheet execute automatically.

6
5
4
E
0
3
0
5
2
I
0
Y = -0.0817x + 5.5723
Oxygen Uptake Rate Chart
tz-
yf.
ee
,ea
2 3 4 5 6 7 8 9 10 11 12 13 14 15 1
Time (minutes)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP WQ Permit Number: WQ 0016247
WWTP Name: Statesville Fourth Creek WWTP NPDES Number: NC 0031836
Monitoring Period: From 07/01/19 To 09/30/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6`
MPN
17857
25339
28735
MPN/g
0
Quarterly
Grab
Sm9221ce
Coliform
power per gram
- 2006
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inchd/ing fine //a Ld imprisonment."
Andy Smith O s Manager Kk 0 je / J�
Pr aver me and Title (fvd& or print) Land Ap i Name and Title (if applicable) (type or print)
j &� —a - �0 C�;R6L
Signature of reparer* *ate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
'ynagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 08/13/2019
Reported: 08/15/2019
For: 4th Creek
Comments: GM 25339 MPN/g
Sample Number Parameter Sample ID Result
STATESVILLE
ANALYTICAL
Unit Method Analyzed Analyst
190813-35-01
Fecal Coliforms
1-4
26316
MPN/g
SM92210E2006
08/14/2019
WC
190813-35-01
Percent Solids
1-4
19
%
SM254OB-2011
08/14/2019
WC
190813-35-02
Fecal Coliforms
2-4
21778
MPN/g
SM92210E-2006
08/14/2019
WC
190813-35-02
Percent Solids
2-4
18
%
SM254OB-2011
08/14/2019
WC
190813-35-03
Fecal Coliforms
3-4
27174
MPN/g
SM92210E-2006
08/14/2019
WC
190813-35-03
Percent Solids
3-4
18.4
%
SM254OB-2011
08/14/2019
WC
190813-35-04
Fecal Coliforms
4-4
17857
MPN/g
SM92210E-2006
08/14/2019
WC
190813-35-04
Percent Solids
4-4
28
%
SM254OB-2011
08/14/2019
WC
0813-35-05
Fecal Coliforms
5-4
25000
MPN/g
SM92210E-2DW
08/14/2019
WC
190813-35-05
Percent Solids
5-4
20
%
SM254OB-2011
08/14/2019
WC
190813-35-06
Fecal Coliforms
6-4
26318
MPN/g
SM92210E-20DS
08/14/2019
WC
190813-35-06
Percent Solids
6-4
19
%
SM2540B-2011
08/14/2019
WC
190813-35-07
Fecal Coliforms
7-4
28735
MPN/g
SM92210E-2006
08/14/2019
WC
190813-35-07
Percent Solids
7-4
17.4
%
SM25408-2011
08/14/2019
WC
Respectfully submitted,
0
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190813-35-01 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-35-02 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-35-03 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-35-04 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-35-05 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-35-06 Temp on Arrival:
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-36-07 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate . Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature
End Temperature
Dissolved Oxygen Level
mgn)
5.9
5.73
5.78
5.77
5.72
5.58
5.5
5.42
5.32
5.26
5.17
5.01
4.96
Fourth Creek WWTP
7/12/2019
24
7/12/19 8:57 AM
BD
7/12/19 9:01 AM
BD
300
24
24
milliliters
,y
iegrees Celsius
iegrees Celsius
Slope: 0.1
Intercept: 5.9
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 4.13 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.06 mg Oxygen/g/hr
Average Temperature: 24 degrees. Celsius
Temperature Correction Factor: 0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.87 m�lmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7
6
5
aM
E
c
d
M
K 4
O
m
0
w
A
C
3
2
1
0
y =-0.0688x + 5.9723
Oxygen Uptake Rate Chart
t�
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Fourth Creek WWTP
Biosolids Permit Number:
Date:
7/15/2019
Digester Temperature:
23.7
Sampling Date/Time:
7/15/19 7:30 AM
Sampled By:
BD
Analysis Date/Time:
7/15/19 7:35 AM
Analyzed By:
BD
Sample Volume:
300
milliliters
Beginning Temperature:
23.7
degrees Celsius
End Temperature:
24
degrees Celsius
Dissolved Oxygen Level
6.35
6.34
5.96
5.92
5.87
5.86
5.84
Slope: 0.0
Intercept: 6.4
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.37 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Average Temperature: 24 degrees Celsius
Temperature Correction Factor: 0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.46 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Oxygen Uptake Rate Chart
6.5
6.4
6.3
6.2
m
0
w
A.9
5.8
5.7
5.6
5.5
y =-0.0394x + 6.4258
�-���■sue®� �®® ����®�
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourt
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time: 7/1
Sampled By:
Analysis Date/Time: 7/1
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
5.52
1
5.42
2
5.38
3
5.34
4
5.31
5
5.28
6
5.24
7
5.23
8
5.22
9
5.21
10
5.2
11
5.19
12
5.19
13
5.15
14
5.1
15
5.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
7/16/2019
25.4
6/19 1:15 PM
KG
6/19 1:20PM
BD
300 milliliters
25.4 degrees Celsius
25.2 Idegrees Celsius
0.0
5.4
1.0
1.44 mg Oxygen/hr
0.37 mg Oxygen/g/hr
25 degrees. Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:1 0.29 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

5.6
5.5
5.4
93
c
m
oM
K
C�
m
0
w
w
5.1
5
4.9
y =-0.0239x + 5.456
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWTP
Biosolids Permit Number:
Date:
7/17/2019
Digester Temperature:
23
Sampling Date/Time:
7/17/19 7:28 AM
Sampled By:
BD
Analysis Date/Time:
7/17/19 7:32 AM
Analyzed By:
BD
Sample Volume:1
300
milliliters
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
(mg/1)
7.02
6.78
6.6
6.43
6.39
6.28
6.25
6.16
6.03
5.96
5.88
5.83
5.8
5.73
5.7
5.67
23 Idegrees Celsius
23.4 Idearees Celsius
Slope: 0.1
Intercept: 6.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 4.98 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.26 mg Oxygen/g/hr.
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 1.09 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

MM
7
E5
c
m
a�
x
C�
m
>4
0
0
3
2
1
0
y =-0.083x + 6.8625
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWT
Biosolids Permit Number:
Date:
7/18/2019
Digester Temperature:
23.8
Sampling Date/Time:
7/18/19 7:31 AM
Sampled By:
BD
Analysis Date/Time:
7/18/19 7:36 AM
Analyzed By:
BD
Sample Volume:1
300
Beginning Temperature:1
23.8
End Temperaturel
23.7
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.65
1
6.58
2
6.39
3
6.32
4
6.3
5
6.24
6
6.17
7
6.09
8
6.04
9
6.02
10
6
11
5.95
12
5.9
13
5.86
14
5.81
15
5.92
Slope: 0.1
Intercept: 6.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
iliters
egrees Celsius
egrees Celsius
3.06 mg Oxygen/hr
0.79 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.65 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

.:
6.4
5.8
5.6
5.4
5.2
y =-0.0511 x + 6.574
Oxygen Uptake Rate Chart
Tl�
4
1 2 3 4 5 6 7 8 9' 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By:
Analysis Date/Tim&
Analyzed By
Sample Volume:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)(mg/1)
0
7.48
1
7.2
2
7.11
3
7.03
4
6.96
5
6.92
6
6.89
7
6.87
8
6.85
9
6.86
10
6.92
11
6.83
12
6.76
13
6.71
14
6.69
15
6.64
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
7/19/2019
23.7
7/19/19 7:36 AM
BD
7/19/19 7:40 AM
BD
300
23.7
23.5
0.0
7.2
0.9
milliliters
jegrees Celsius
jegrees Celsius
2.39 mg Oxygen/hr
0.61 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.50 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.6
7.4
7.2
I
w
on •
6.4
6.2
6
y =-0.0398x + 7.2585
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8; 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.54
1
7.39
2
7.25
3
7.23
4
7.27
5
7.27
6
7.22
7
7.11
8
7.06
9
7.02
10
6.97
11
6.96
12
6.87
13
6.82
14
6.79
15
6.75
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:,
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
7/20/2019
24.1
7/20/19 7:37 AM
BD
7/20/19 7:42 AM
BD
300
24.1
24.1
0.0
7.4
1.0
milliliters
legrees Celsius
degrees Celsius
2.82 mg Oxygen/hr
0.78 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.64 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.6
7.4
7.2
6.8
6.4
6.2
Oxygen Uptake Rate Chart y - -0.047x + 7.4942
2 3 4 5 6 7 8 9 10 11 12 13 14 15
Time (minutes)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville Fourth Creek WWTP WQ Permit Number: WQ 0016247
WWTP Name: Statesville Fourth Creek WWTP NPDES Number: NC 0031836
Monitoring Period: From 10/01/19 To 12/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class B complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
<105
<127
<143
MPN/g
0
Quarterly
Grab
Sm9221ce
Coliform
power per gram
- 2006
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Mt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification in /ding fine and imprisonment."
Andy Smith O s Manager
Pr aver ame �Title e or print) Land plier Name and Title (if applicable) (type or print)
�
Signature of Preparer*Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results � SV LL
AL
5ynagr®
z84 Boger Rd.
Mocksville, NC 27028
Receive Date:
10/09/2019
Reported:
10/11/2019
For:
4th Creek
Comments:
GM <127 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
191009-24-01
Fecal Coliforms
4-1
<125
MPN/g
SM92210E-2006
10/09/2019
WC
191009-24-01
Percent Solids
4-1
16
%
SM254OB-2011
10/09/2019
WC
191009-24-02
Fecal Coliforms
4-2
<105
MPN/g
SM92210E-2006
10/09/2019
WC
191009-24-02
Percent Solids
4-2
19
%
SM254OB-2011
10/09/2019
WC
191009-24-03
Fecal Coliforms
4-3
<133
MPN/g
SM92210E-2006
10/09/2019
WC
191009-24-03
Percent Solids
4-3
15
%
SM254OB-2011
10/09/2019
WC
191009-24-04
Fecal Coliforms
4-4
<118
MPN/g
SM92210E-2oo6
10/09/2019
WC
191009-24-04
Percent Solids
4-4
17
%
SM254OB-2011
10/09/2019
WC
1009-24-05
Fecal Coliforms
4-5
<140
MPN/g
SM92210E-2006
10/09/2019
WC
191009-24-05
Percent Solids
4-5
14.3
%
SM254OB-2011
10/09/2019
WC
191009-24-06
Fecal Coliforms
4-6
<143
MPN/g
SM92210E-2006
10/09/2019
WC
191009-24-06
Percent Solids
4-6
14
ova
SM254OB-2011
10/09/2019
WC
191009-24-07
Fecal Coliforms
4-7
<131
MPN/g
SM92210E-2006
10/09/2019
WC
191009-24-07
Percent Solids
4-7
15.3
%
sM254013-2011
10/09/2019
WC
Respectfully submitted,
'Op 'v4/ ' J%1)
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 Statesville, NC 28687 e 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 191009-24-01 Temp on Arrival: 3.2
pH on Arrival: <2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 191009-24-02 Temp on Arrival: 3.2
pH on Arrival: <2
Chemicals in containers, lab
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-24-03 Temp on Arrival: 3.2
pH on Arrival: <2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-24-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
pH on Arrival: <2 Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-24-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 2 of 4

pH'on Arrival: <2
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
'ample Number 191009-24-06 Temp on Arrival: 3.2
PH on Arrival: <2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-24-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PH on Arrival: <2 Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687.704/872/4697
Page 3 of 4

Client: fk r—o
S'I'A'IESVIiLEANAI,YTICAL
t22 Coca Smet • P.O. Bar 228
5�(704) 8724697687
Address s2? 7 O g et � /} �
�1
!�.
�y
OGK 5 } e G f 4 O
Contact Person; mac^ 1 1 �, Phone # r7,,q - 0 - ,7 ) I,
�} T
FAX#
Chain of
Custody Record
PO # _ _ crr r" i I 1 D W� {r'ma Daley
Requisitioned by: if ('
I
Customer
Sample ID#
lab -ID ►
17me Sampled
(Grab Only)
Date Sampled
(Grab Orly)
Io-9—1
„
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X
a
MarriX
yy vrH
➢arametasrequestrd {prartaly3is
f ec� ae� 6`
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W .T tiQ
Relinquished by:
Time lQ 00
am, pm Date LL � !
Sampled by:
Received by:
Time to
am, pm Datelo R ! {
Transported by:
Relinquished by:
Time
am, pm Date ._ _/ /_-_
Holding times met:
Received by:
Time
am, pm Date I
�/
Compliance work -
Composite Samg_#l:
Time begin am, pm Date �1 �I
Non-compliance work:
Time and am, pm Date _/
Cpmraosite Samaltna #2:
l ab Comments:
Samples Transported On ice;
Time begin am, pm Date _!
Time end am, pm Date _!�
Initials;
N
00
u3
00
N
C.3
Z
0
y
4+
00
N
N
X
Q
0
IL

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWTP
Biosolids Permit Number:
-
-
Date:
10/1 /2019
Digester Temperature:
23
Sampling Date/Time:
10/1/19 9:32 AM
Sampled By:
BD
Analysis Date/Time:
10/1/19 9:36 AM
Analyzed By:
BD
Sample Volume:
300
milliliters
Beginning Temperature:
F23
degrees Celsius
End Temperature:1
23.4
degrees Celsius
Time Dissolved Oxygen Level
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Slope: 0.0
Intercept: 8.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.84 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.68 mg Oxygen/g/hr
.Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.863837599
Temperature Corrected Specific Oxygen Uptake Rate: 0.58 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

8.2
in
FAM
7.4
7.2
7
y =-0.0473x + 8.1905
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.14
1
8.1
2
8.06
3
8.02
4
7.97
5
7.93
6
7.88
7
7.84
8
7.81
9
7.77
10
7.73
11
7.69
12
7.65
13
7.61
14
7.57
15
7.53
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/2/2019
22.7
10/2/19 7:39 AM
BD
10/2/19 7:44 AM
BD
300
22.7
22.7
0.0
8.1
1.0
milliliters
Jegrees Celsius
Jegrees Celsius
2.44 mg Oxygen/hr
0.58 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 0.50 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

M
8.1
8
7.9
E
E.8
a�
a�
O
-a
m
2.7
0
w
w
0
7.6
7.5
7.4
7.3
7.2
y =-0.0406x + 8.1768
Oxygen Uptake Rate Chart
Shl
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1 E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.07
8.03
7.92
7.89
7.76
7.71
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/3/2019
22.2
10/3/19 7:28 AM
BD
10/3/19 7:31 AM
BD
300
22.2
22.3
0.0
8.3
1.0
milliliters
legrees Celsius
legrees Celsius
2.51 mg Oxygen/hr
0.56 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:j 0.51 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

8.4
8.2
7.8
7.6
7.4
7.2
y =-0.0418x + 8.3775
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Fourth Creek
Biosolids Permit Number:
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
8.65
8.6
8.56
8.52
8.48
8.32
8.28
8.24
8.17
8.12
8.07
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
10/4/19 7:24 AM
BD
10/4/19 7:28 AM
BD
300 milliliters
21.5 degrees Celsius
21.7 degrees Celsius
0.0
8.6
1.0
2.43 mg Oxygen/hr
0.54 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:1 0.49 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

E
M
8.4
E
8.3
0
x
Cam:
.a
m
Z.2
0
w
0
0
GRE
8
7.9
7.8
7.7
y =-0.0405x + 8.6843
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.54
8.49
8.36
8.31
8.21
8.17
8.13
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
1 /5/2019
21
10/5/19 8:25 AM
BD
10/5/19 8:29 AM
BD
300
--.
21
21
0.0
8.7
0.8
milliliters
legrees Celsius
legrees Celsius
2.22 mg Oxygen/hr
0.50 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:1 0.48 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

M
::
8.6
E
8.2
8
y =-0.037x + 8.7505
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
9.25
1
9.24
2
9.23
3
9.19
4
9.18
5
9.17
6
9.16
7
9.14
8
9.12
9
9.1
10
9.08
11
9.06
12
9.04
13
9
14
8.96
15
8.93
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
iurth Creek WWTP
10/7/2019
18.8
10/7/19 7:34 AM
BD
10/7/19 7:38 AM
BD
300 milliliters
18.8 degrees Celsius
19 degrees Celsius
0.0
9.3
1.0
1.22 mg Oxygen/hr
0.24 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.26 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

M
9.2
M
O
M
m
>9
0
W
Al
8.7
y =-0.0203x + 9.2883
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9.04
9.03
•
.*
8.85
8.83
8.81
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/8/2019
19.8
10/8/19 7:31 AM
BD
10/8119 7:34 AM
BD
300
19.8
19.8
0.0
9.1
1.0
milliliters
iegrees Celsius
iegrees Celsius
1.01 mg Oxygen/hr
0.24 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:1 0.24 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

WIN
9.05
8.95
ll—tl
8.75
8.7
y =-0.0168x + 9.089
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville WQ Permit Number: WQ 0016247
WWTP Name: Statesville Third Creek WWTP NPDES Number: NC 0020591
Monitoring Period: From 01/01/19 To 3/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61h
MPN
<96
<120
<127
MPN/g
0
Quarterly
Grab
SM9221C
Coliform
power per gram
E-2006
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification i ding fin`` d imprisonment."
And Smith O s Manager I� S5
Pr ar Name d Title ype or print) Land lier Name and Title (if applicable) (type or print)
QG i L < l02-�
SignaturIof Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
'ynagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
01/14/2019
Reported:
01/15/2019
For:
3rd Creek
Comments:
Geometric Mean <120 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190114-17-01 Fecal Coliforms
1
<127
MPN/g
SM92210E-2006
01/14/2019
WC
190114-17-01 Percent Solids
1
15.8
%
SM25468-2011
01/14/2019
WC
190114-17-02 Fecal Coliforms
2
<125
MPN/g
SM92210E-2006
01/14/2019
WC
190114-17-02 Percent Solids
2
16
ova
SM2540B-2011
01/14/2019
WC
190114-17-03 Fecal Coliforms
3
<127
MPN/g
SM9221cE-2006
01/14/2019
WC
190114-17-03 Percent Solids
3
15.7
%
SM254OB-2011
01/14/2019
WC
190114-17-04 Fecal Coliforms
4
<127
MPN/g
sM92210E-2006
01/14/2019
WC
190114-17-04 Percent Solids
4
15.8
%
SM254OB-2011
01/14/2019
WC
10114-17-05 Fecal Coliforms
5
<118
MPN/g
SM92210E-2006
01/14/2019
WC
190114-17-05 Percent Solids
5
17
%
SM2540B-2011
01/14/2019
WC
190114-17-06 Fecal Coliforms
6
<96
MPN/g
SM92210E-2006
01/14/2019
WC
190114-17-06 Percent Solids
6
20.8
%
SM2540B-2011
01/14/2019
WC
190114-17-07 Fecal Coliforms
7
<125
MPN/g
SM92210E-2006
01/14/2019
WC
190114-17-07 Percent Solids
7
16
%
SM2540B 2011
01/14/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190114-17-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-17-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-17-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-17-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-17-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
ample Number 190114-17-06 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190114-17-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Client:
f�,(a fl,�
STATC5VILLEANAL'L'TICAL
t22 Covet sueat Po. Box 228
Statcsvillc, NC 28687
[phone]
Chain a�
Address: a'y q dD &' 2 PQ
D{{ �7 �+
Djes v C tic- � 1 O a G
Contact Aerson:G So Phone # •33� Mrar�!- 9'PYS, FAX# 33�'
PC # r- O ^l� Q
�7 d 0
Requisitioned by: �`� �;5�»,g rr� f �: Oa f +. j Date)
Custody
Custody Record
CLPAarrmer
Sample IDik
Lab -ID 0
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
Mabix
Pwamaas reqwstLd for wWysis
w
I ww
N. 11.01
TOOPO�
C
.-vr C..-ee�k_
t rc
1 •�2
Relinquished by: -
Received by: {��-
Relinquished by:
Received by:
Composite Sampling #1I:
Time begin am, pm Date _ j /
Time end am, pm Date / /__
Composite Sampling #2:
Time begin am, pm Date /
Time end am, pm Date 1 /
Time Opm Date L 1171_fi Sampled by: rjC
rime pm Date �Y-1 � f Transported by:
Time am, pm Date _/�/_ Holding times met:
Time am, pm Date _/� Compliance work: ✓
Hon -compliance work.
Lab Comments: Samples Transported On Ice:
In�Hals:
00
LO
00
N
U
z
tv
h
W
t!1
r.4
N
X
O
ca
O

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
1 /2/2019
Digester Temperature:
12
Sampling Date/Time:
1/2/19 8:41
Sampled By:
SA
Analysis Date/Time:
1/2/18 8:54
Analyzed By:
SA
Sample Volume:
300
milliliters
Beginning Temperature:
13.1
degrees Celsius
End Temperature:
14.4
degrees Celsius
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
10.37
1
10.33
2
10.28
3
10.27
4
10.23
5
10.22
6
10.18
7
10.16
8
10.15
9
10.11
10
10.08
11
10.02
12
9.99
13
9.95
14
9.92
15
9.89
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
10.4
1.0
1.86 mg Oxygen/hr
0.39 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:1 0.58 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

10.5
10.4
10.3
10.2
aM
is
d
O
m
0
N
! l
9.7
y = -0.031 x + 10.398
Oxygen Uptake Rate Chart
lIzz
z
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample VolumeT
Third Creek WWTP
milliliters
WQ0016247
1 /3/2019
11.9
1/3/19 8:58
SA
1/3/18 9:04
SA
300
Beginning Temperature:1 12.1 Idegrees Celsius
End Temperature: 14.2 degrees Celsius
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
11.11
1
11.07
2
11.05
3
11.01
4
10.98
5
10.95
6
10.91
7
10.87
8
10.83
9
10.8
10
10.75
11
10.71
12
10.68
13
10.65
14
10.61
15
10.59
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
11.1
1.0
2.15 mg Oxygen/hr
0.45 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate:1 0.72 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

11.2
11
10.9
as
E
m
a)
1IT 8
O
rM-
10.6
10.5
10.4
10.3
y =-0.0359x + 11.153
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
9.19
1
9.17
2
9.15
3
9.13
4
9.1
5
9.06
6
9.02
7
8.98
8
8.96
9
8.96
10
8.94
11
8.93
12
8.9
13
8.88
14
8.86
15
8.85
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
degrees Celsius
degrees Celsius
WQ0016247
1 /4/2019
15.5
1/4/19 10:14
SA
1/4/18 10:19
SA
300 ,milliliters
15.4
15
0.0
9.2
1.0
1.43 mg Oxygen/hr
0.30 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 0.42 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

9.3
9.2
9.1
M.
M. .
•
y =-0.0238x + 9.207
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
1/7/2019
Digester Temperature:
15.7
Sampling Date/Time:
1/7/19 13:03
Sampled By:
SA
Analysis Date/Time:
1/7/18 13:09
Analyzed By:
SA
Sample Volume:
300
milliliters
Beginning Temperature:
16
degrees Celsius
End Temperature:1
14.9
degrees Celsius
Dissolved Oxygen Level
8.76
8.74
8.66
8.62
8.57
8.56
8.49
8.46
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.8
1.0
1.35 mg Oxygen/hr
0.28 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 0.39 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

M
8.4
8.3
8.2
y =-0.0225x + 8.7973
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
VQ0016247
1/8/2019
10.4
1/8/19 8:23
SA
1/8/18 8:31
SA
300 milliliters
Beginning Temperature:1
10.9
End Temperaturel
12.6
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
11.65
1
11.64
2
11.61
3
11.59
4
11.55
5
11.53
6
11.5
7
11.48
8
11.43
9
11.4
10
11.38
11
11.36
12
11.32
13
11.3
14
11.25
15
11.22
Slope: 0.0
Intercept: 11.7
Correlation Coefficient: 1.0
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
egrees Celsius
earees Celsius
1.75 mg Oxygen/hr
0.36 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:1 0.63 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

11.8
11.7
11.6
11.5
E
m
a�
1t4
O
m
0
am
11.2
10.9
y =-0.0291 x + 11.698
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:1
Third Creek M
WQ001624'
1 /9/2019
14.8
1/9/19 7:33
SA
1/9/18 7:41
SA
300
Beginning Temperature:1 14.9
End Temperature:1 15.1
Dissolved Oxygen Level
8.63
8.6
8.54
8.1
48 8
8.44
8.42
8.35
8.33
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Ililiters
0.0
8.6
0.7
Celsius
Celsius
1.32 mg Oxygen/hr
0.28 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:1 0.39 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

8.7
AM
E
8.4
m
x
0
V
m
,$.3
0
U)
w
W
8.2
8.1
E�
7.9
y =-0.0221 x + 8.6613
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Third Creek WWTP
WQ0016247
1/10/2019
10.8
1/10/19 8:44
SA
1 /10/18 8:50
SA
300 milliliters
Beginning Temperature:1 10.9
End Temperaturel 11.3
Dissolved Oxygen Level
(mg/I)
9.83
9.08
9.78
9.75
9.73
9.72
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
egrees Celsius
egrees Celsius
0.0
9.7
0.3
0.75 mg Oxygen/hr
0.16 mg Oxygen/g/hr
11 degrees Celsius
1.838459212
Temperature Corrected Specific Oxygen Uptake Rate:1 0.29 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

10
9
y =-0.0124x + 9.7012
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville WQ Permit Number: WQ 0016247
WWTP Name: Statesville Thud Creek WWTP
NPDES Number: NC 0020591
Monitoring Period: From 04/01/19 To 6/30/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Au Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the followine monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maxirnum Units
dences
Analysis
Fecal
2x10 to the 6 h
MPN
256
589
2809
MPN/g
0
Quarterly
Grab
SM9221C
Coliform
power per gram
E-2006
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying —Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
0 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification uding fine an i nprisonment."
An S 'dn 0 s Mana er �71 Al X
P ar Nam nd Titl ( type or print) Land lier Name and Title (if applicable) (type or print)
Signature of Preparer* e Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results STATESVILLE
ANALYTICAL
.ity of Statesville WWTP
PO Box 1111-
Statesville, NC 28687
Receive Date: 05/16/2019
Reported: 11 /20/2019
For: 3rd Creek
Comments: Geometric Mean: 589 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190516-08-01
Fecal Coliforms
1
267
MPN/g
SM92210E-2006
05/16/2019
CL
190516-08-01
Percent Solids
1
15.0
%
SM2540B-2011
05/16/2019
CL
190516-08-02
Fecal Coliforms
2
2809
MPN/g
SM92210E-2006
05/16/2019
CL
190516-08-02
Percent Solids
2
17.8
%
SM2540B-2011
05/16/2019
CL
190516-08-03
Fecal Coliforms
3
1523
MPN/g
SM92210E-2006
05/16/2019
CL
190516-08-03
Percent Solids
3
15.1
%
SM25408-2011
05/16/2019
CL
190516-08-04
Fecal Coliforms
4
296
MPN/g
SM92210E-2006
05/16/2019
CL
190516-08-04
Percent Solids
4
13.5
%
SM254OB-2011
05/16/2019
CL
30516-08-05
Fecal Coliforms
5
526
MPN/g
SM92210E-2006
05/16/2019
CL
190516-08-05
Percent Solids
5
15.2
%
SM254OB-2011
05/16/2019
CL
190516-08-06
Fecal Coliforms
6
256
MPN/g
SM92210E-2006
05/16/2019
CL
190516-08-06
Percent Solids
6
15.6
%
SM2540B-2011
05/16/2019
CL
190516-08-07
Fecal Coliforms
7
541
MPN/g
SM92210E-2006
05/16/2019
CL
190516-08-07
Percent Solids
7
14.8
%
SM2540B-2011
05/16/2019
CL
Respectfully submitted,
C'r,-O-jTbl,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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Client:
S•fATESVILLEANAINTICAL
122 CourtStreet • P.O. Box 228
Statesville, NC 28687
(7e4) 872-4697
Address:
in �d �r
/ �s
7 �1/
M CI ! i/f //G /L Z �V�
Contact Person: # Phone
Z1ts'G
FAX#
Chain of
Custody Record
PO # Requisitioned by: (Time Date)
Customer
Sample IDl3
Lab -ID fr
Time Sampled
(Grab On
Gran Off) d
s Matrix
h4" w
ww
Parameters requested for analysis
v7�
So l�
-
y 6A 4,1;eG4
-
- 7
Relinquished by..t�fl ,
Received by:
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date ^/T/
Time end am, pm Date _/�
Composite Sampling Vo
Time begin am, pm Date
Time end am, pm Date _/_/
Time (�g D
Time &i&o
Time
Time
Lab Comments:
am, pm Date L 1P
am, pm Date �l iGy�
am, pm Date _/_I
am, pm Date _/
Sampled by:
Transported by:
Holding times met:
Compliance work:
Non-compliance work:

Specific Oxygen Uptake Rate
SOUR
Facility Name:1 Third Creek WWTP
Biosolids Permit Number:1 WQ0016247
Date:
4/1/2019
Digester Temperature:
16.1
Sampling Date/Time:
4/1/19 10:28
Sampled By:
SA
Analysis Date/Time:
4/1/19 10.34
Analyzed By:
SA
Sample Volume:
300
milliliters
;.^.!fir.
Beginning Temperature:
16.1
degrees Celsius
End Temperature:1
15.8
degrees Celsius
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.91
1
6.88
2
6.85
3
6.84
4
6.82
5
6.79
6
6.77
7
6.74
8
6.71
9
6.7
10
6.68
11
6.67
12
6.65
13
6.63
14
6.61
15
6.6
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake 'Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.9
1.0
1.25 mg Oxygen/hr
0.21 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:1 0.27 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

. 7
6.9
6.8
E
c
m
aM
O
m
.B.7
0
w
0
6.6
6.5
6.4
y =-0.0208x + 6.9173
Oxygen Uptake Rate Chart
2 3 4 5 6 7 8 9 10 11 12 13 14 15
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
4/2/2019
Digester Temperature:
15.3
Sampling Date/Time:
4/2/19 8:26
Sampled By:
SA
Analysis Date/Time:
4/2/19 8:33
Analyzed By:
SA
Sample Volume:
300
milliliters
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.19
7.18
7.17
7.15
7.13
7.1
7.06
7.05
7.03
6.97
s
6.95
5.5 Idegrees Celsius
5.7 Idegrees Celsius
Slope: 0.0
Intercept: 7.2
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 1.25 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.22 mg Oxygen/g/hr
Average Temperature: 16 degrees Celsius
Temperature Correction Factor: 1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:1 0.29 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

f
E
Oxygen Uptake Rate Chart
y =-0.0209x + 7.247
2 3 4 5 6 7 8 9 10 11 12 13 14 15
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Third Creek W\A
W00016247
4/3/2019
17.1
4/3/19 13:04
SA
4/3/19 13:13
SA
300
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7.1
7.06
704
7.01
6.98
6.96
6.94
.::
6.8
6.78
s
Ililiters
rees Celsius
rees Celsius
Slope: 0.0
Intercept: 7.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 1.25 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.22 mg Oxygen/g/hr
Average Temperature: 17 degrees Celsius
Temperature Correction Factor: 1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.27 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically

7.2
7.1
II
C�
.a
m
A.9
0
U)
w
.:
6.7
y =-0.0209x + 7.1205
Oxygen Uptake Rate Chart
Y
-r
a
g
b
r
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:1
Third Creek M
WQ001624;
4/4/2019
15.3
4/4/19 8:33
SA
4/4/19 8:41
SA
300
Beginning Temperature:1 14.4
End Temperature:1 14.8
Dissolved Oxygen Level
6.56
6.54
6.53
6.49
6.48
6.4
6.39
6.37
6.28
6.27
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
rees Celsius
rees Celsius
0.0
6.6
1.0
1.25 mg Oxygen/hr
0.22 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.31 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

6.55
6.5
6.45
E
6.4
m
a
x
0
a
m
W5
0
w
N
0
6.3
6.25
6.2
6.15
y =-0.0208x + 6.593
Oxygen Uptake Rate Chart
"N4
a
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:1
Beginning Temperature:1
End Temperature:1
Third Creek WWTP
milliliters
degrees Celsius
degrees Celsius
WQ0017247
4/5/2019
17.4
4/5/19 8:32
SA
4/5/19 8:40
SA
300
17.2
17.1
Dissolved Oxygen Level
6.32
6.31
6.26
6.26
6.18
6.16
6.1
6.08
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.4 .
1.0
1.09 mg Oxygen/hr
0.19 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.23 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

6.4
6.35
6.3
6.25
a�
E
6.2
m
a�
K
O
V
0
05
0
w
N
in
6.1
6.05
6
5.95
5.9
y =-0.0182x + 6.3835
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:1
Third Creek WV�
WQ0016247
4/8/2019
18.8
4/8/19 9:12
SA
4/8/19 9:20
SA
300
Beginning Temperature:1 18.6
End Temperature:1 18.8
Dissolved Oxygen Level
5.09
5.06
5.04
4.94
4.91
4.84
4.81
4.69
4.66
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Ililiters
0.0
5.1
1.0
Celsius
Celsius
1.84 mg Oxygen/hr
0.32 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.34 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

5.2
5.1
5
4.7
4.6
4.5
4.4
y =-0.0306x + 5.1565
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:1
Third Creek W%
WQ001624'.
4/9/2019
18.6
4/9/19 8:32
SA
4/9/19 8:39
SA
300
Beginning Temperature:1
18.9
End Temperature:
19'.3
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.754
1
6.73
2
6.7
3
6.68
4
6.65
5
6.64
6
6.61
7
6.59
8
6.56
9
6.54
10
6.52
11
6.49
12
6.45
13
6.43
14
6.4
15
6.38
Slope: 0.0
Intercept: 6.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Ililiters
rees Celsius
rees Celsius
1.49 mg Oxygen/hr
0.26 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.28 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

6.7
0
E
c
d
5
O
v
m
0
N
0
6.4
6.3
6.2
6.1
y =-0.0249x + 6.7815
Oxygen Uptake Rate Chart
i
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville
WWTP Name: Statesville Third Creek WWTP
WQ Permit Number: WQ 0016247
NPDES Number: NC 0020591
Monitoring Period: From 07/01/19 To 9/30/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lune Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirnhle to niternntiva nerfnrmed (..Iris A nr Class R) rmmnlete thr fnllnwina mnnitnrina dntn-
n
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maxhnum Units
dences
Analysis
Fecal
2x10to the 601
MPN
3125
3388
3571
MPN/g
0
Quarterly
Grab
SM9221C
Coliform
power per gram
E-2006
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
colifonn)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inAg-k
fine and�risomnent."
And Smith O s Manager
Pre rer a and Title (tyt or print) Land plier Name and Trtle if applicable) (type or print)
o
Signature o Preparer* ate Signature. of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
lynagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date:
08/13/2019
Reported:
08/15/2019
For:
3rd Creek
Comments:
GM 3388 MPN/g
�. STATE VILLE
ANALYTICAL
Sample Number parameter Sample ID Result Unit Method Analyzed Analyst
190813-34-01
Fecal Coliforms
1-3
3472
MPN/g
SM92210E-2006
08/14/2019
WC
190813-34-01
Percent Solids
1-3
14.4
%
SM254OB-2011
08/14/2019
WC
190813-34-02
Fecal Coliforms
2-3
3125
MPN/g
SM92210E-2006
08/14/2019
WC
190813-34-02
Percent Solids
2-3
16
%
SM25408-2011
08/14/2019
WC
190813-34-03
Fecal Coliforms
3-3
3571
MPN/g
SM92210E-2006
08/14/2019
WC
190813-34-03
Percent Solids
3-3
14
%
SM254OB-2011
08/14/2019
WC
190813-34-04
Fecal Coliforms
4-3
3333
MPN/g
SM92210E-2006
08/14/2019
WC
190813-34-04
Percent Solids
4-3
15
%
SM25408-2011
08/14/2019
WC
0813-34-05
Fecal Coliforms
5-3
3571
MPN/g
SM92210E-2006
08/14/2019
WC
190813-34-05
Percent Solids
5-3
14
%
SM2540B-2011
08/14/2019
WC
190813-34-06
Fecal Coliforms
6-3
3333
MPN/g
SM92210E-2005
08/14/2019
WC
190813-34-06
Percent Solids
6-3
15
%
SM25409-2011
08/14/2019
WC
190813-34-07
Fecal Coliforms
7-3
3333
MPN/g
SM9221GE-2W6
08/14/2019
WC
190813-34-07
Percent Solids
7-3
15
%
SM2540B-2011
08/14/2019
WC
Respectfully submitted,
'0P - -vvl.Z. JI)1p ,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 0 704/872/4697
Page 1 of 3

Condition of Receipt
Sample Number 190813-34-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-34-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-34-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-34-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-34-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-34-06 Temp on Arrival: 3.2
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 3

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190813-34-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 3 of 3

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0016247
Date:
7/2/2019
Digester Temperature:
21.3
Sampling Date/Time:
7/2/19 10:26
Sampled By:
SA
Analysis Date/Time:
7/2/19 10:31
Analyzed By:
SA
Sample Volume:
milliliters
Beginning Temperature:
"20.8degrees
Celsius
End Temperature:
degrees Celsius
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
7.58
7.51
7.43
7.41
Slope: 0.0
Intercept: 7.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 1.61 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.28 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:1 0.27 m7mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7fti]
7.8
7.7
W
7.4
7.3
7.2
y =-0.0269x + 7.8342
Oxygen Uptake Rate Chart
,
1 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
W00016247
7/3/2019
21.6
7/3/19 7:38
SA
7/3/19 7:45
SA
300
21.4 Idegrees Celsius
21.5 Idearees Celsius
0.0
7.3
1.0
1.66 mg Oxygen/hr
0.29 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:1 0.28 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.4
7.3
7.2
FA
ME
y =-0.0276x + 7.377
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1F
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
WQ0019247
Date:
7/5/2019
Digester Temperature:
23.2
Sampling Date/Time:
7/5/19 7:34
Sampled By:
SA
Analysis Date/Time:
7/5119 7:41
Analyzed By:
SA
Sample Volume:
300 milliliters
Beginning Temperature:
MVww
22.9 degrees Celsius
End Temperature:
22.5
degrees Celsius
Dissolved Oxygen Level
L
6.34
6.33
6.31
6 28
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
6.6
1.0
1.41 mg Oxygen/hr
0.25 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 0.21 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

6.7
6.5
0
E
c
d
R4
x
O
m
0
N
_N
0
6.3
6.2
6.1
y =-0.0235x + 6.6508
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 . 14 15 16
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample. Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
5.46
5.41
35 85.33
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
reek WWTP
milliliters
degrees Celsius
degrees Celsius
0016247
B/2019
23.7
(19 9:58
SA
19 10:07
SA
300 _
24.4
23.7
0.0
5.9
1.0
2.24 mg Oxygen/hr
0.39 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate:1 0.32 jmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

6
5.9
5.8
5.7
E
8.6
0
rn
iz
O
m
.b.5
0
NN
N_
0
5.4
5.3
MA
5.1
y =-0.0373x + 5.9423
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility N
Biosolids Permit Nur
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature
End Temperature
Dissolved Oxygen Level
6.31
6.28
6.26
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W 00016247
Ililiters
23.4 'degrees Celsius
22.5 decrees Celsius
0.0
6.3
1.0
1.78 mg Oxygen/hr
0.31 mg Oxygen/g/hr
23 degrees Celsius
0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 0.27 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

6.4
I
6.2
�1
a
5.9
61M
5.7
y =-0.0296x + 6.3548
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
6.52
6.35
6.31
6.27
6.15
6.1
06 8
6.02
95 8
7/10/19 8:03
SA
7/10/19 8:10
22.8
Ililiters
egrees Celsius
egrees Celsius
Slope: 0.0
Intercept: 6.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.31 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.41 mg Oxygen/g/hr
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 0.35 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

M.
6.5
6.4
6.3
!1.
m
0
06
5.9
5.8
5.7
5.6
5.5
y =-0.0385x + 6.5115
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
6.76
v
6.71
6.67
6.55
6.52
6.44
6.42
6.27
6.23
WQ0016247
7/11/2019
23.3
7/11 /19 7:03
SA
7/11/19 7:09
SA
300 milliliters
23degrees Celsius
22.6 Idegrees Celsius
Slope: 0.0
Intercept: 6.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.36 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.41 mg Oxygen/g/hr
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.863837599
Temperature Corrected Specific Oxygen Uptake Rate:1 0.36 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

• •
•
6.7
�5
c
m
a
6.4
m
0
U)
rM
6.2
6.1
6
5,9
5.8
y =-0.0393x + 6.83
Oxygen Uptake Rate Chart
4
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Statesville WQ Permit Number: WQ 0016247
WWTP Name: Statesville Third Creek WWI? NPDES Number: NC 0020591
Monitoring Period: From 10/01/19 To 12/31/2019
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf annlirahip to alternative narfnrmnrl (('lace A nr ('lace R) ramnlPtP the fall—ina mnnitnrina data-
9
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10tothe 6°i
MPN
<25
<44
<77
MPN/g
0
Quarterly
Grab
SM9221C
Coliform
power per gram
E-2006
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
Ation/Alt.
reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake) X
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed _
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the ppathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inc lu ' g fine and inyrisonment." _
And SmWi 0 s Manager /� Ay
Pr a am d Titl ( type or print) Lanacne and Title (if applicable) (type or print)
Z�C� Z;Signature of Preparer* 40aSignature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part503.9(r) and 15A NCAC 2T.1102 (26)

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 10/09/2019
Reported: 10/11/2019
For: 3rd Creek
Comments: GM <44 MPN/g
Sample Number Parameter Sample ID Result
Unit Method Analyzed Analyst
191009-23-01 Fecal Coliforms
3-1
<77
MPN/g
SM92210E-20o6
10/09/2019
WC
191009-23-01 Percent Solids
3-1
26
%
SM254OB-2011
10/09/2019
WC
191009-23-02 Fecal Coliforms
3-2
<30
MPN/g
SM92210E-2006
10/09/2019
WC
191009-23-02 Percent Solids
3-2
67
%
SM254OB-2011
10/09/2019
WC
191009-23-03 Fecal Coliforms
3-3
<42
MPN/g
SM92210E-2oo6
10/09/2019
WC
191009-23-03 Percent Solids
3-3
48
%
SM254OB-2011
10/09/2019
WC
191009-23-04 Fecal Coliforms
3-4
<26
MPN/g
SM92210E-2006
10/09/2019
WC
191009-23-04 Percent Solids
3-4
78
%
SM2540B-2011
10/09/2019
WC
11009-23-05 Fecal Coliforms
3-5
<67
MPN/g
SM92210E-2006
10/09/2019
WC
191009-23-05 Percent Solids
3-5
30
%
SM254OB-2011
10/09/2019
WC
191009-23-06 Fecal Coliforms
3-6
<77
MPN/g
SM92210E-2006
10/09/2019
WC
191009-23-06 Percent Solids
3-6
26
%
SM254OB-2011
10/09/2019
WC
191009-23-07 Fecal Coliforms
3-7
<25
MPN/g
SM92210E-2006
10/09/2019
WC
191009-23-07 Percent Solids
3-7
80
%
SM254OB-2011
10/09/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 o Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 191009-23-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-23-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-23-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-23-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-23-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 . 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Conforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
ample Number 191009-23-06 Temp on Arrival: 3.0
-Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 191009-23-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

client: r�
sraxustShW ,xPO.SocnlL
I22 Curt Shut � PO. Box 2..8
Address Q?9 B o3e(L (,4
Staiuville,NC 28687
(704) 8724697
Chan of
m o+:k 5 v. 1} e- :2 7 a
Contact Person: 5.� I }, Phone# � E% d -*1 t �b FAX#
T
PO* Requisitioned b3r 't►, �)oW'A (r(me Da1a7
�
Custody Record
_
Customer
Sample Sample IDlr
LatrlD•
Time Sampled
(Orao Onty)
Date Sampted
(Grab Ontir)
Matrix
w WW
Parrmetasxe v ab-s"
� f
► t 3
10 - 9-1
X
e�,� YKRV
u
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Relinquished by.
Time � QQ
q
am, pm Date /
Lo L �
Sampled by: gQjg,J 015-
Received by:
Time LOW
am, pm Date 101,51 / (q
Transported by:
Relinquished by:
Time
am, pm Date _f
Holding times met:
Received by.
Time
am, pm Date _/ J
Compliance work:
Composite Sam i�S #1:
Time begin am, pm Date _l /
Non-compliance work:
Time end am, pm Date I._ _f
composite Sampling #2:
LabComments:
samples Transported On Ice:
Time begin am, pm Date _/ 1
Time end am, pm Date
tnmats:
MA
00
N
N
x
O
M P

Specific Oxygen Uptake Rate
SOUR
I Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Beginning Temperatu
End Temperatu
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
E
0.0
7.5
1.0
Celsius
Celsius
1.93 mg Oxygen/hr
0.36 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:1 0.32 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.6
7.5
7.4
7.3
rn
E
c
m
rn
0'.2
O
m
0
w
U)
4.1
7
6.7
y=-0.0321x+7.5518
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
I Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Beginning Temperatu
End Temperatu
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
22 ,degrees Celsius
11.6 Idearees Celsius
0.0
7.8
1.0
1.55 mg Oxygen/hr
0.35 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:1 0.31 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.9
7.8
F
M
F.6
c
m
x
O
-a
m
2.5
0
U)
(A
ail
7.4
7.3
7.2
7.1
y =-0.0259x + 7.855
Oxygen Uptake Rate Chart
2 3 4 5 6 7 8 9 10 11 12 13 14 15
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
W00017247
Date:
10/3/2019
Digester Temperature:
21.7
Sampling Date/Time:
10/3/19 8:39
Sampled By:
SA
Analysis Date/Time:
10/3/19 8:47
Analyzed.By:
SA
Sample Volume:
300
milliliters
) � *W
tw w ,"' is i :)r
Beginning Temperature:
21.6
degrees Celsius
End Temperature:
21.2
degrees Celsius
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
.12
13
14
15
Dissolved Oxygen Level
7.4
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.4
1.0
1.29 mg Oxygen/hr
0.29 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:1 0.27 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.5
II!
7.3
7
y=-0.0214x+7.4185
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 1E
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
35
6.87
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W00016247
Ililiters
0.0
7.4
1.0
Celsius
Celsius
2.16 mg Oxygen/hr
0.48 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:1 0.46 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.5
7.4
VACM
IW:
rn
E
M. "
6.7
'Alto
y=-0.0361x+7.4615
Oxygen Uptake Rate Chart
2 3 4 5 6 7 8 9 10 11 12 13 14 15 1
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10 _
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility N
Biosolids Permit Nur
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.67
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1 10/7/19 7:34 1
19.4
19.7
illiliters
rees Celsius
rees Celsius
0.0
8.1
1.0
1.82 mg Oxygen/hr
0.40 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.40 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

8.2
8.1
8
0
7.7
7.6
7.5
7.4
y =-0.0303x + 8.138
Oxygen Uptake Rate Chart
2 3 4 5 6 7 8 9 10 11 12 13 14 15
Time (minutes)

Specific Oxygen Uptake Rate
SOUR
Facility Name:1 Third Creek WU1
Biosolids Permit Number: WQ0016247
Date:
10/8/2019
Digester Temperature:
19.5
Sampling Date/Time:
10/8/19 7:24
Sampled By:
SA
Analysis Date/Time:
10/8/19 7:33
Analyzed By:
SA
Sample Volume:
300
milliliters
Beginning Temperature:
19.6
degrees Celsius
End Temperature:
19.8
degrees Celsius
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
8.21
8.17
8.16
8.1
8.06
8.04
8.02
7.97
7.94
7.9
7.87
7.82
7.79
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.2
1.0
1.57 mg Oxygen/hr
0.35 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:1 0.35 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

8.3
8.2
8.1
E�
7.7
VADI
7.5
y =-0.0262x + 8.2385
Oxygen Uptake Rate Chart
..1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
7
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W 00016247
liliters
egrees Celsius
egrees Celsius
0.0
7.6
1.0
1.87 mg Oxygen/hr
0.42 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.45 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

7.7
F"S
7.5
7.4
7.1
7
y =-0.0312x + 7.6205
Oxygen Uptake Rate Chart
2 3 4 5 6 7 8 9 10 11 12 13 14 15 1
Time (minutes)

SECTION 6

I Agricultural Lime Application Log
Year: 2019
Project:
Statesville
Field
FSoil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -Feld)
pH
(from soil analysis)
Applied(CCE Eq.)
I I R-23-03 1 6.7 1 O.OT/Ac. I I
IR-20-01
5.9
O.OT/Ac.
IR-20-02
6.2
O.OT/Ac.
IR-20-03
6.2
O.OT/Ac
IR-20-04A
6.7
O.OT/Ac
IR-20-04B
6.9
O.OT/Ac
IR-20-08
6.2
O.OT/Ac
IR-20-09
6.9
O.OT/Ac
IR-20-11
6.8
O.OT/Ac
St-3-1
St-3-3
6.3 0.0
6.2 0.0

SECTION 7

NCDA$CS A omic Division Phone: [phone]
Website: wwu
gr.gov/agronomi/
Report No.
;!0-SL004622
Predictive
Client:
Dennis Phillips
201 Barry Oak Rd
Advisor:
Alex Fox
synagro
Soil Report
Mehlich-3
Extraction
Statesville, NC 28625
284 Boger Rd
Mocksviille, NC 27028
Sampled County: Iredell
Links to Helaful Information
--
Client ID: 259693
Advisor
ID: 501947
Sampled: 09/09/2019 Received: 09/12/2019 Completed: 09/21/2019
Farm: NC-IR-20
Sample ID: 01
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M
0.0
120-200 0
0
0 0 0
0
0
0
Note: 12
2 -
0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100
cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1
K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1
Na ESP
SS-1 NO3-N
0.41 1.03 9.9 87 1.3 5.9 174
103
59 23
73
344
223 317
317
189
0.1 1
Sample ID: 02
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M
0.0
120-200 0
0
0 0 0
0
0
0
Note: 12
2 -
0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100
cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1
K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1
Na ESP
SS-1 NO3-N
0.32 1.12 8.2 89 0.9 6.2 141
108
62 20
84
274
179 221
221
175
0.1 1
Sample ID: 03
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M
0.0
120-200 0
100
0 0 0
0
0
0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100
cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1
K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
0.36 1.05 8.1 88 1.0 6.2 108
21
68 18
30
213
141 327
327
221
0.1 1
North Carolina
Tobago 3rust f uiul t oa lmisslon
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler. Commissioner ofAariculture

NCDA&CS
omic Division Phone: [phone]
Website: wwv
gr.gov/agronomi/
Report No.
!0-SL004622
Dennis Phillips
Page 2 of 4
Sample ID: 4A
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
100
0
0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.32 1.09
10.1 93 0.7 6.7 219 19
79 14
37
1242
752
475
475
370 0.1
1
Sample ID: 4B
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
100
0
0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.27 1.10
10.6 97 0.4 6.9 114 21
81 15
32
478
290
242
242
237 0.1
1
Sample ID: 8
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
10
0
0
0
.0
0 0
Note: 12
2 - 0.0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.46 1.04
12.2 90 1.2 6.2 205 72
73 14
45
428
270
547
547
392 0.1
1
Sample ID: 9
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
40
0
0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.41 1.02
15.4 97 0.5 6.9 314 49
81 14
42
444
270
710
710
591 0.1
1

NCDA&CS.4
omic Division Phone: [phone]
Website: wwu
gr.gov/agronomi/
Report No. ?0-SL004622
Dennis Phillips
Page 3 of 4
Sample ID: 11
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg
S
Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
0 0
0
pH$ 0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units -W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All
Mn-AI2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.51 1.13
11.0 96 0.4 6.8 180 127
79 11
40 305 188
217 217
160 0.1 1

NCDA&CS A omic Division Phone: [phone] Website: ww% gr.gov/agronomi/
Report No. M-SL004622
Dennis Phillips
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat(
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer.
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmfsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilize/
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cud, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrsthtm
Page 4 of 4
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-1
manganese index
M-0
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

NCDA&C:,..y.onomic Division Phone: [phone]
Website: wwv....--,jr.gov/agronomi/
Report No. F', ", jL004620
Client:
Shane Porter
Advisor:
Alex Fox
_'4s 8 fir.
Predictive
106 Page Road
Synagro
#F
Soil Report Mehlich-3
Extraction
Cleveland, NC 27013
284 Boger Rd
Mocksville, NC27028
Sampled County : Iredell
Links to Helpful Information
Client ID: 502300
Advisor
ID: 501947
Sampled: 09/09/2019 Received: 09/12/2019 Completed: 09/21/2019
Farm: NC-IR-23
Sample ID: 03
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
20
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 1.15
9.4 94 0.6 6.7 211 62
78 12
44
198
125
221
221
169
0.1 1
Sample ID: 04
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
10
0 0
pH$
0
0
0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.46 1.16
13.6 98 0.3 7.0 261 73
85 10
71
287
174
310
310
267
0.1 1
Sample ID: 05
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
10
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units
- WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.51 1.14
11.6 93 0.8 6.4 207 74
77 12
64
198
129
221
221
170
0.1 1
North Carolina
libido 1 i u.t F Ulkl t uJl1l11b>unp
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDABCL _ ___onomic Division Phone: [phone] Website: wwv....__gr.gov/agronomi/
Report No. F. _---;L004620
Shane Porter
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
M-0
N
mineral -organic soil class
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncapr.crov/agronomi/oboart4.htmt fsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-1
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.goy/ac7ronomi/uyrst.htm

Page 1 of 1
Report No: 20-022-0618
Account No: 46493
Advisor: Synagro Central LLC/ Statesville
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoeinte'r ANALYTICAL
Client: Robert Ridenhour
Statesville
Synagro
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: NC-ST-03
Date Received: 01/22/202D
Date of Report: 01/23/2020
Lab No Field ID
Sample ID
Soil Class
HM% W/V
pH
Ac
P-1
K-1
S-1
Mn-1
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO3 N
04064
03-01
MIN
1.0
6.2
0.4
22
8
35
81
68
68
100
3.5
89
58
29
1.1
0
04065
03-03
MIN
1.2
6.8
0.1
11
9
33
81
68
68
155
4.3
98
62
34
1.2
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mgldm3; WN in g1cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.