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Home My WebLink AboutWI0400074_Monitoring (Report)_20140708RECEIVED/GENF -,�. I J !-"- 0 S ". o " water Quali• r►. M ,:. ANNUAL GROUNDWATER MONITORING REPORT BE AEROSPACE FACILITY 1455 FAIRCHILD ROAD WINSTON-SALEM, NORTH CAROLINA NCD060302577 PREPARED FOR: BE AEROSPACE, INC. 1400 CORPORATE CENTER WAY WELLINGTON, FLORIDA PREPARED BY: CRB GEOLOGICAL & ENVIRONMENTAL SERVICES, INC. 8744 S.W. 133RD STREET MIAMI, FLORIDA 33176 JUNE 30, 2014 TABLE OF CONTENTS Page(s) 1.0 INTRODUCTION.............................................................................................................. 1 2.0 GROUNDWATER MONITORING.................................................................................. 3 2.1 GROUNDWATER ELEVATION MONITORING....................................................... 3 2.2 GROUNDWATER MONITORING.............................................................................. 3 2.3 GROUNDWATER ANALYTICAL RESULTS............................................................. 3 2.3.1 Courtyard Area Groundwater Results............................................................. 4 2.3.2 Former Fairchild Storage Shed Area............................................................... 4 2.3.3 Northwest Area............................................................................................... 5 2.3.4 Hazardous Waste Storage Area....................................................................... 5 3.0 REMEDIAL ACTION....................................................................................................... 7 3.1 AERATION WELLS..................................................................................................... 7 3.2 BIOREMEDIATION BY REDUCTIVE DECHLORINATION.................................... 7 3.3 SOIL VAPOR EXTRACTION...................................................................................... 7 4.0 CONCLUSIONS & RECOMMENDATIONS.................................................................. 9 Figures Figure 1 — Site Location Map Figure 2 — Site Map Figure 3 — Shallow Groundwater Potentiometric Surface — May 2014 Figure 4 — PCE in Groundwater — May 2014 Tables Table 1 — Groundwater Elevation Measurements Table 2 — Historic Groundwater Analytical Results Table 3 — Groundwater Physical Parameters Appendix Appendix I — Laboratory Reports and Chain of Custody Records BEA 414-02 11 CRB Geological & Environmental Services, Inc. 1.0 INTRODUCTION This Conceptual Site Model (CSM) update was prepared by B/E Aerospace, Inc. (BE) and CRB Geological & Environmental Services, Inc. (CRB), in partial satisfaction of the requirements of the September 2012 Administrative Order On Consent (AOC) to prepare a Conceptual Site Model (CSM) for the BE facility located at 1455 Fairchild Road, Winston-Salem, North Carolina (the Site). The first site assessment was completed in 1997 in response to the December 20, 1996 Notice of Violation (NOV) for groundwater quality standard exceedances issued by the North Carolina Department of Environmental and Natural Resources (NCDENR). Additional assessment of the site since 1997 has included quarterly groundwater monitoring through 2014. The Site is registered as a Large Quantity Generator of Hazardous Waste, and is a Part A Permitted Treatment, Storage or Disposal Facility (TSDF) as a result of soil contamination contained in the former Solid Waste Management Unit (SWMU)-5 (aka, Closed RCRA Hazardous Waste Management Unit). A Remedial Action Plan (RAP) was submitted to the North Carolina Department of Waste Management (NCDWM) in October 2003, which proposed a comprehensive remedial strategy for the site. Voluntary implementation of the 2003 RAP was initiated in May 2004 with soil excavation followed by installation of soil vapor extraction systems in December 2004 and May 2005. Voluntary implementation of groundwater remediation proposed in the 2003 RAP was initiated in March 2006 and July 2006 with the construction of groundwater aeration wells and bioremediation injection wells, respectively. A revised Closure Plan for the site was submitted to the NCDWM in June 2005, and was approved in a letter from NCDWM dated June 29, 2007. A Post -Closure Plan was submitted to NCDWM in December 2008 for the former Hazardous Waste Storage Area (HWSA) located at the site. Approval of the Post -Closure Plan was given by NCDWM on October 15, 2009. Groundwater monitoring included in this report for the former HWSA is performed in accordance with the approved Post -Closure Plan. A deed notice and site plat was recorded with the Forsyth County Register of Deeds during July 2009, in accordance with the Closure Plan and Post -Closure Plan requirements. In April 2011, the North Carolina Department of Water Quality QN'CDWQ) issued a renewal of Underground Injection (UIC) Permit Number W 10400074 for the site. The UIC Permit was obtained in order to perform additional injections of bioremediation substrate at the site. A Conceptual Site Model was originally presented as the report titled Comprehensive Site Assessment Addendum, July 2000. Updates to the CSM have been submitted semi- annually and quarterly as Groundwater Monitoring Reports from 2001 through 2012. This report updates the CSM with the most recent groundwater monitoring results and remedial system evaluation. In a letter dated July 19, 2013, NCDENR approved the Site CSM based on the February 2013 groundwater analytical data. CRB Geological & Environmental Services, Inc. BEA 414-02 CSR Update This report is organized into four (4) sections. Referenced tables, figures, and appendices are included following the text. Section 1.0 presents introductory information regarding the purpose and format of the report. The results of the groundwater and surface water monitoring are discussed in Section 2.0. A discussion of remedial action performed during the monitoring period is presented in Section 3.0. Conclusions and recommendations are presented in Section 4.0. BEA 414-02 CSR Update 2 CRB Geological & Environmental Services, Inc. 2.0 GROUNDWATER MONITORING This section summarizes field measurements and groundwater data collected from the annual sampling of monitoring wells on March 2014 and May 2014. The groundwater analytical results from this event are discussed relative to historical groundwater concentrations observed at the Site. 2.1 GROUNDWATER ELEVATION MONITORING Depth -to -water measurements were collected from on -site monitoring wells on May 12, 2014, pursuant to the methodology specified in the Groundwater Sampling and Analysis Plan (GWSAP). Depth -to -water measurements were used to determine the elevation of the groundwater at the site relative to a public NAD 27 benchmark located on the Smith - Reynolds Airport property. The groundwater elevation data and top of casing elevation measurements are summarized in Table 1. The locations of the monitoring wells are shown in Figure 2. Across the site, measured groundwater elevations decreased between 0.76 and 3.4 feet between December 2013 and May 2014, with the exception of MW-1 which increased 1.28 feet. A groundwater elevation map is provided as Figure 3. Groundwater flowed from upgradient recharge to the south and towards the Bowen Branch Creek, located south of Fairchild Road. Shallow groundwater flow diverged slightly east and west of a bedrock ridge located beneath Building 1. Based on historic observations, vertical groundwater flow is upward from the underlying bedrock into the sapro lite. 2.2 GROUNDWATER MONITORING CRB personnel collected groundwater samples from select on -site monitoring wells. Monitoring wells were purged using pre -packaged polyethylene bailers or a submersible pump. The wells were purged until pH, temperature, ORP, dissolved oxygen, and conductivity stabilized, or until the wells were purged to near dryness. Final groundwater monitoring readings from sampling are summarized in Table 3. Groundwater samples were collected using pre -packaged polyethylene bailers or through disposable polyethylene pump tubing. Groundwater sampling was performed in accordance with CRB's Comprehensive Quality Assurance Plan (ComQAP) and pursuant to methodologies specified in the GWSAP. Groundwater samples and a trip blank were preserved on ice and submitted via in person to Pace Analytical located in Huntersville, North Carolina, for analysis by EPA Method 8260. Laboratory analytical reports and chain of custody records are included in Appendix I. 2.3 GROUNDWATER ANALYTICAL RESULTS Based on laboratory analytical results, groundwater concentrations remained stable across the majority of the site, with some exceptions. The primary compound above North Carolina 2L Groundwater Standards (NC 2L) at the site was tetrachloroethylene (PCE). The overall magnitude of the PCE concentrations decreased significantly across the site during BEA 414-02 CSR Update 3 CRB Geological & Environmental Services, Inc the past annual monitoring period and continued a long term reduction trend. Concentrations of trichloroethylene (TCE) and 1,1-dichloroethene (1,1-DCE), and cis-1,2- dichloroethene (cis-1,2-DCE) were also reported above NC 2L in a limited number of wells. Historic groundwater analytical results are summarized in Table 2, respectively. The distribution of PCE concentrations in groundwater is shown in Figure 4. 2.3.1 Courtyard Area Groundwater Results The Courtyard Area (CYA) refers to the area located between Buildings 1 and 2 in the northern part of the site. Two (2) vapor degreasers were formerly located in the CYA. The CYA has been identified as the source area for groundwater contamination at the site and has exhibited the largest concentration reductions as source material has been eliminated through soil vapor extraction and bioremediation. Between 1997 and 2009, concentrations of PCE in the CYA were generally reduced from over 10 mg/L to less than 10 µg/L. Concentrations in the CYA continued to decrease through the monitoring period and concentrations of PCE slightly above the NC 2L standard of 0.7 µg/L were detected in groundwater samples collected from CYA. The concentration of PCE was reported as BDL (less than 1 µg/L) in MW-6, MW-11, MW-13, MW-26D, MW-27D, MW-27DD in May 2014. At MW-6, PCE decreased from 13.6 µg/L in December 2013 to 1.8 µg/L in March 2014 to BDL in May 2014. At MW- 29, PCE decreased from 30 µg/L in May 2013 to 1.9 in May 2014. In MW-30 PCE decreased from 31 µg/L in May 2013 to 7.4 in May 2014. Historically, the levels have remained near or below detection limits since May 2011 in the CYA. Downgradient of the CYA at MW-33, the concentrations of PCE decreased to 4.1 µg/L in May 2014 from 5.5 µg/L in December 2013. PCE was defined vertically in bedrock wells MW-27D, MW-27DD, and MW-12D at 1.1 µg/L, which decreased from 3.1 µg/L in December 2013. 2.3.2 Former Fairchild Storage Shed Area The Former Fairchild Storage Shed Area (FSS) is located in the northeast corner of the Site where unknown releases of PCE were identified. Concentrations of PCE in the FSS have been reduced from over 1 mg/L in 2002 to less than 10 µg/L since 2006. Concentrations of PCE in MW-1 increased to 81 µg/L in December 2013 and then decreased to 12.2 µg/L in March 2014 and further decreased to 6.3 µg/L in May 2014. Monitoring wells MW-lOD and MW-9 continued to be reported as BDL for all target VOCs in May 2014. The concentration of PCE declined in MW-8 from 10 µg /L in April of 2006 to 4 µg/L in May 2014. PCE increased slightly in MW-28, from 6.5 µg/L in April of 2013 to 8.5 µg/L in May 2014. In downgradient well MW-7, PCE remained stable since the April 2013 sampling event with PCE measured at 4.1 µg/L and TCE at 7.6 µg/L in May 2014. BEA 414-02 CSR Update 4 CRB Geological & Environmental Services, Inc. 2.3.3 Northwest Area The Northwest Area (NWA) refers to the northwestern portion of the site and includes the former Air Compressor Area and the Storm Water Outfall. The primary contaminant reported in the NWA is PCE with concentrations of TCE, and 1,1-DCE historically reported above NC 2L standards. In MW-18, the concentration of PCE decreased to 66.6 µg/L in March 2014 and then increased to 197 µg/L in May 2014. The concentration of TCE reported in MW-18 increased in May 2014 to 10.2 µg/L, slightly greater than the 6.4 µg/L from the previous sampling. In the intermediate depth well MW-19, PCE concentration decreased from 65.4 µg/L in December 2013 to 35.9 µg/L in March 2014 and further to 31.7 µg/L in May 2014. 1,1-DCE also decreased from 30 µg/L, to 8.4 µg/L between the December 2013 and May 2014 sampling events. In MW-20, concentrations of PCE decreased to 55.7 µg/L, while 1,1-DCE decreased to 15.1 µg/L in May 2014. Target VOC concentrations in MW-20 decreased since May 2013 to May 2014. In MW-5 and MW-17D, PCE and target VOC concentrations were reported to be BDL in May 2014. MW-4 was inaccessible due to several loaded shipping containers located above the monitoring well. 2.3.4 Hazardous Waste Storage Area The Hazardous Waste Storage Area (HWSA) is in the southwestern part of the site and was formerly an open storage shed area. Between 2006 and 1011 the concentration of PCE was generally reduced in the HWSA from over 5 mg/L to 1 mg/L as a result of bioremediation and SVE. Since August 2013, the concentration of PCE has been further reduced from above 1 mg/L to near 0.5 mg/L across the HWSA. As shown in Figure 4, the axis of elevated groundwater concentrations observed in the HWSA extended southward near the western edge of Building 3 towards MW-14D and downgradient monitoring well MW-15R and in the path of a bedrock contour towards the creek. Concentrations of PCE, TCE, l,l-DCE, and cis-1,2-DCE exceeded NC 2L groundwater standards in HWS monitoring wells, but decreased in all wells in April. In deep saprolite well MW-14D, the concentration of PCE decreased to 624 µg/L and TCE increased to 28 µg/L through May 2014. The concentration of cis-1,2 DCE rose above 2L standards to 98 µg/L. In the deep saprolite well MW-21D, the PCE concentration decreased significantly to 531 µg/L while TCE concentrations increased slightly at 20.4 µg/L. The concentrations of cis-1,2-DCE level remained relatively stable at 73.4. In MW-24, the PCE concentration decreased significantly to 111 µg/L and TCE concentrations decreased to 19.2 µg/L. MW-3, the PCE concentration decreased significantly to 397 µg/L and TCE remained stable at 41.8 µg/L. Concentrations of PCE decreased to BDL in bedrock well MW-22D in May 2014. BEA 414-02 CSR Update 5 CRB Geological & Environmental Services, Inc. Concentrations of PCE decreased in upgradient shallow well MW-23 to 8 µg/L. In MW- 16, PCE concentration decreased to 83.4 µg/L, and TCE decreased to 3.6 µg/L in May 2014. MW-32 concentrations of PCE remained stable at 12.3 µg/L. Concentrations were defined to the west by the absence of shallow groundwater as a result of high bedrock elevations approximately 50-feet west of the Site boundary. The concentrations of VOCs historically reported in downgradient aeration wells AW-1 through AW-5, recovery well RW-3, and monitoring well MW-15R further delineated the main axis of the plume as shown in Figure 4. At the downgradient boundary, PCE decreased in well RW-3 to 19.5 µg/L in May 2014. In downgradient well MW-15R through March 2014, PCE decreased from 735 µg/L to 285 µg/L; TCE decreased to 7.3 µg/L; and 1,1-DCE decreased to below the 2L standard to 7.3 µg/L. MW-15R was not accessible during the May 2014 sampling event, due to dense poison ivy patch which will be removed prior to the next sampling event. BEA 414-02 CSR Update 6 CRB Geological & Enviromnental Services, Inc. 3.0 REMEDIAL ACTION Remediation performed at the site through May 2014 included soil vapor extraction, groundwater aeration, and ongoing groundwater bioremediation. Summaries of remedial action performed at the site are presented below. 3.1 AERATION WELLS In March 2006, five (5) aeration wells AW-1 through AW-5, were installed along the southern property boundary in order to mitigate off -site migration of groundwater contaminants. The aeration wells were installed with dual screened zones above bedrock contact at approximately forty to sixty (40-60) feet below land surface (bls) and to ten (10) feet above the water table. Based on down -hole flow measurements, the aeration wells recover, strip, and recharge groundwater at a rate of 2-4 gallons per minute. The aeration wells were designed as air-lift circulation wells to withdraw migrating groundwater in the lower screen section followed by in -situ stripping and venting of VOCs from the withdrawn groundwater, and then recharging the treated groundwater through an upper screen installed in the vadose zone. The aeration wells did not function during June 2013 while repairs were performed on the blower coupling. The aeration wells will continue to operate as a boundary control remediation technology. The effect of boundary remediation is considered to be significant as measured in the continued reduction trend of PCE in boundary groundwater and downgradient surface water. 3.2 BIOREMEDIATION BY REDUCTIVE DECHLORINATION A total of thirty-nine (39) injection wells and nine (9) temporary injection points were installed at the site during ,June 2006 and injection of a lactate/soybean oil bioremediation substrate was performed to stimulate anaerobic degradation of the chlorinated ethenes. The continued reductive dechlorination of PCE and generation of breakdown products 1,1-DCE, cis-DCE, and vinyl chloride confirm bioremediation is occurring. No bioremediation injections "ere performed during the period from April 2013 to May 2014. Additional bioremediation injectiot s are planned in 2014 16 maintain favorable geochemical conditions for reductive dechlorination. 3.3 SOIL VAPOR EXTRACTION Soil vapor extraction (SVE) was performed at the site during the monitoring period in order to remove residual source material from inaccessible soils in the CYA and the HWS. SVE was initiated in the CYA in August 2005 and operated through July 2012 with vapor extraction from three (3) vent wells, CYA SVE-1, CYA SVE-2, and CYA SVE-3. BEA 414-02 CSR Update 7 CRB Geological & Environmental Services, Inc. SVE was initiated in the HWS in July 2005 and continued through July 2012 with vapor extraction from one vent well HWS SVE-1 installed to a depth of 55-feet and two soil vapor inlet wells installed to depths of 25-feet. The SVE units in the CYA and HWSA were turned off during August 2012 after exhaust measurements were analyzed for VOCs using an organic vapor analyzer (OVA) and no VOC vapors were measured. The SVE units were restarted during October 2013 in order to evaluate any rebound in soil vapors in these areas and remained operational from December 2013 through May 2014. BEA 414-02 CSR Update 8 CRB Geological & Environmental Services, Inc. 4.0 CONCLUSIONS & RECOMMENDATIONS Based on laboratory analytical results, concentrations of target groundwater compounds decreased significantly in key monitoring wells in each area of the Site during the monitoring period. Concentrations of PCE, TCE, 1,1-DCE, and cis-1,2-DCE above NC 2L standards were detected in groundwater samples from monitoring wells across the site through May 2014. The greatest reductions were observed in the HWSA and southern Site boundary area, which were attributed to reductive dechlorination and bioremediation injections. Historically, the primary contaminant identified at the site was PCE. Since the initiation of in -situ bioremediation, the magnitude and area of elevated PCE concentrations have been significantly reduced and continue to decrease. Reduced surface water concentrations measured during 2011 are consistent with an overall reduction of the plume. Performance of reductive dechlorination at the site has been shown to reduce PCE and TCE concentrations with little to no accumulation of degradation compounds, including vinyl chloride. Total VOH concentrations have been reduced by 99% in several CYA monitoring wells, and the highest concentrations are now present in the HWSA well below 1 mg/L and continue to decrease in downgradient wells RW-3, MW-15R and MW-7. Concentrations of PCE were below the USEPA Drinking Water standard of 5 µg/L, but remained slightly above NC 2L standard of 0.7 µg/L in the CYA during the monitoring period. Based on favorable bioremediation indictors, these concentrations are expected to continue to decline. The upgradient extent of PCE concentrations at the site remained defined along the northern edge of the property by monitoring wells MW-1 MW-9, MW-5, MW-11 and MW-17. The western extent of the groundwater contamination was defined by a bedrock ridge and the absence of significant shallow groundwater flow beyond the western site boundary. The eastern extent of groundwater contamination was defined by the FSS monitoring wells and along a topographic low that extended from the northern boundary of the site south towards Fairchild Road. Annual monitoring of surface water will continue to be performed during the low -flow period of autumn and early winter. Operation of the boundary aeration wells will continue until boundary groundwater concentrations are reduced to NC 2L Standards. A schedule for additional bioremediation injections will be submitted to NCDENR during the upcoming quarterly monitoring period. Operation of the SVE units installed in the HWS and CYA will continue in order to reduce residual source material. The next quarterly groundwater sampling will be performed during July 2014. BEA 414-02 CSR Update 9 CRB Geological & Environmental Services, Inc. FIGURES Figure 1 — Site Location Map Figure 2 — Site Map Figure 3 — Shallow Groundwater Potentiometric Surface — May 2014 Figure 4 — PCE in Groundwater — May 2014 Source: USGS 7.5-Minute'` ' �tf •F (� �' t,tif �, . �' %;'�� r `�' i.� IBM Walkertown, NC Quadrangle J'S' S a `= T�''` r e? 1 ✓J� r( l' j �.Rti ••sl(y �0 .� ..•tt t7 �'r�{. �.L • p' ..r< �'• Nor-� � _ • r I � t 1•%. (i1 � r> ja`r'�+` � {�`�` ` ��, �` �'�'Wi`..4 mot") :� ��.v. 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GRAPHIC SCALE. 60 FEET TM Mt-kA contokwd hwWn Iscor&ldentlW -4 no port of N con b< reproduced eldm the e+Mreswd Witten pertisdvf of CRB GeoloycoU t EnrYwpewngl Servkee, Inc 0 MONITORING WELL MONITORING WELL/SOL PUMPING TEST WELL M FIRE HYDRANT • LIGHT POLE * ELECTRIC TRANSFONER • DRADVAGE e CATCH BASIN TRENCH DRAIN • SS MANHOLE ----M"ERTY BOUNDARY ------' -FIXE -SEVER LINE FORSYTH COUNTY GARAGE K.Jc� TEST i FACD mAIRPORT \ SMITH REYNOLDS i N 1 i ` UNDEVELOPED ! LAID i } f f i f I I � l f f SMI AIRWf I f --"2DING I! i i SMITH REYINILDS AFIPORT My-T SOURCE) SITE DESIGN. INC. 2/2001 .,r LEGEND: GRAPHIC SCALE ® MONITORING WELL — PROPERTY BOUNDARY 100-FEE7 ® RECOVERY WELL -------FptCIE n' —CROUNOWATER ELEVATION IN FEET ABOVE MSL \ FORSYTH COUNTY GARAGE ER EILVAnb1 T ;Iw ee7.N The moterlW contolnad heroin is kkntid and no port of it con be r w"thwt the e.preued Witten p—issian of Ged.*,d & E.4--td Srkm In. 865 870 SHALLOW GROUNDWATER SURFACE 5/12/2014 B/E AFROTACE FACILITY 1455 FApORD ROAD, 104STDN-SALEM, NC s/Is/EOI4 M0. ^E"41-� FIGURE er: u ecnE: As wI� 1 - 4 1- Tetrachloroethylene (PCE) contours shown as ug/L Figure PCE in Groundwater— May 2014 BE Aerospace Facility 4 1455 Fairchild Road, Winston-Salem, North Carolina 08 TABLES Table 1 — Groundwater Elevation Measurements Table 2 — Historic Groundwater Analytical Results Table 3 — Groundwater Physical Parameters Table 1 - Groundwater Elevation Measurements B/E Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina TIC Screened Casing Screened Depth To Water Well ID Total 1 Interval Depth Elevation (ft bls) (ft bls) Formation 5/12/2014 GW Elev. MW-1 48.00 949.71 33-48 - Saprolite 34.29 915.42 MW-3 58.33 938.89 43-58 - Saprolite 54.47 884.42 MW-4 39.48 950.92 25-50 - Saprolite - - MW-5 48.25 951.24 33-48 - Saprolite 30.49 920.75 MW-6 40.00 950.93 25-40 - Saprolite 31.58 919.35 MW-7 47.40 916.00 33-48 - Saprolite 36.03 879.97 MW-8 37.55 945.49 23-38 - Saprolite 37.01 908.48 MW-9 39.18 951.79 25-40 - Saprolite 26.38 925.41 MW-lOD 68.05 949.32 58-68 55 Bedrock 33.87 915.45 MW-11 37.97 952.39 23-38 - Saprolite 29.81 922.58 MW-12D 65.00 950.90 55-65 52 Bedrock 31.65 919.25 MW-13 37.15 950.47 22-37 - Saprolite 36.62 913.85 MW-14D 94.75 938.52 90-95 81 Saprolite 53.79 884.73 MW-15 60.00 937.03 45-60 - Saprolite 56.14 880.89 MW-15R 45.00 895.17 25-45 - Saprolite - - MW-16 59.30 941.40 45-60 - Saprolite 53.90 887.50 MW-17D 63.20 954.70 53-63 55 Saprolite 33.10 921.60 MW-18 42.85 952.47 28-43 - Saprolite 33.82 918.65 MW-19 82.45 949.29 73-83 - Saprolite 34.41 914.88 MW-20 46.57 949.24 32-47 - Saprolite 35.41 913.83 MW-21D 88.88 940.17 79-89 80 Saprolite 53.59 886.58 MW-22D 154.00 937.10 open borehole 128 Bedrock 53.10 884.00 MW-23 62.05 943.70 47-62 - Saprolite 53.78 889.92 MW-24 61.75 939.11 47-62 - Saprolite 53.54 885.57 MW-26D 81.61 950.91 75-85 50 Bedrock 30.98 919.93 MW-27D 68.61 950.36 58-68 45 Bedrock 35.85 914.51 MW-27DD 90.60 950.35 80-90 45 Bedrock 37.66 912.69 MW-28 48.83 944.13 34-49 - Saprolite 35.95 908.18 MW-29 47.70 950.99 33-48 - Saprolite 30.80 920.19 MW-30 37.05 951.02 27-37 - Saprolite 32.65 918.37 MW-32 57.00 942.36 42-57 - Saprolite 51.75 890.61 MW-33 52.00 948.62 37-52 - Saprolite 45.36 903.26 RW-3 36.00 904.11 21-36 - Saprolite 24.18 879.93 - 1UP tit nute► % asu►g elevations surveyed to 1Vlivu kNAD-2 i) by Site Design, mc., January LVV i " - " Not measured MW-1 OD - Monitoring wells constructed using surface casing are designated with "D" Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina cis 1,2 Vinyl PCE TCE 1,1-DCE 1,1,1-TCA Sample ID Sample Date DCE Chloride L NC 2L GR' Standard' 0.7 3 7 70 200 0.03 MW-1 02 09,96 280 7.6 < < < < 0516.,97 280 6.4 < 68 < < 04 1001 53 < < < < < 04;23/02 3900 180 < 1700 < < 04;09,03 1030 46.4 < 347 < < 04/ 19/04 96.5 1.5 < 12.4 < < 04 27.05 20 < < < < < 04 05 06 8.4 < < < < < 03 19,07 3.3 < < < < < 0429 08 3.7 < < < < < 04 21..09 3.4 < < < < 04'05/ 10 2 < < < < < 10/28/10 2.5 < < < < 01/24,11 2.6 < < < < 0426,1 I 1.4 < < < < < 07/22/11 3.6 < < < < < 10/06.11 3.4 < < < < < 04 03112 3.5 < < < < < 07'25 12 3.4 < < < < < 11 /08/12 5.9 < < < < < 02/07/13 5 < < 1.1 < < 04/30/13 6.2 < < < < < 08M 13 5.3 < < < < < 12 03/13 81.3 12.5 < 184 < < 03/07/14 12.2 < < 1.2 < < 0512114 6.3 < < < < < MW-3 02/06/96 1400 320 < < < < 05/19 97 940 130 < < < < 07i28,,99 864 92.4 4.46 11.9 6.4 < 010500 450 110 6 17 < < 07.110 01 2100 160 52 < 23.0 < 06/24 03 901 64.1 78.9 12.7 32.0 < 04/20/04 985 61.6 108 14.1 37.4 < 04r28/05 900 57 76 < 24 < 04/06,106 2600 < < < < < 03/20/07 1000 85 100 20 19 < 04/30/08 890 56 85 17 11 < 04/06%10 900 36 43 11 < < 0503/11 370 38 19 30 1.5 < 04/02/12 640 42 26 25 1.6 < 05/01/13 550 41 18 31 < < 05,12: 14 397 41.8 16.7 29 < < MW4 02/06/96 75 < 6.9 < 8.6 < 05/16/97 76 3.4 9.8 < 10 < 07/29,99 87.7 3.1 2.5 < 11.5 < 07AW01 84 < 33 < 12 < 06/24,,03 130 5.6 47.2 < 27.4 < 04/ 19/04 66.2 4.2 30.2 < 6.4 < 04/27/05 22 3.2 7.4 < 1.8 < 04/05/06 28 3.1 5 < < < 04,22,,09 26 2.2 5.3 < < 04/06°10 24 1.9 < < < < 05/0311 18 1.5 2.1 < < < 04,0312 16 1.4 1.7 < < < 1 of 12 CRB Geological Environmental Services. Inc. Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCDO60302577 1455 Fairchild Road, Winston-Salem, North Carolina VWYI Sample ID Sample Date PCE TCE 1,1-DCE DCE 1,1,1-TCA Chloride L NC 2L GW Standard' 0.7 3 7 70 200 0.03 MW-5 02 06 96 < < < < < < 05/16/97 < < < < < < 0729 99 < 2.3 < < < 07/09/01 < < < < < 08/07/02 < < < < < < 06/24/03 < < < < < < 04/19/04 1.5 < < < < < 04,2705 < < < < < < 04/05/06 1.2 < < < < < 03/19,07 < < < < < < 04 29/08 1.9 < < < < < 04/22/09 < < < < _ < 04/05/10 < < < < < < 04/27/11 < < < < < < 04/03/12 < < < < < < 04/30/13 < < < < < < 05/12/14 < < < < < < 1h1W-6 02-06-96 2000 < < < 160 < 05/17/97 14000 < < < < < 04/23/02 720 < < < < < 0420/04 6760 18.3 3.1 3.6 10 < 04/27i05 1900 < < < < < 04/05/06 950 < < < < < 03/20/07 250 < < < < < 09/12/07 12 < < < < < 04/30/08 14 < < 45 < < 04/22/09 3.2 < < 36 < 04/06/10 2.2 < < 26 < < 10/28/10 190 2.6 1 18 - < 01/24/11 22 < < 9.2 - < 05/02/11 < < < 5.9 < < 07/22/11 < < < 10 < < 10/06/11 2.2 < < 7.1 < < 01/24/12 < < < 3.1 < < 04-'02/12 1 < < 1.9 < < 07/25/12 < < < 1.3 < < 11/08/12 < < < < < < 02/07/13 < < < 1.6 < < 05/01/13 1.1 < < 1.8 < < 08/05/13 3.5 < < 1.9 < < 12/03/13 13.6 < < < < < 03/07/14 1.8 < < < < < 05/12/14 < < < < < < MW-7 02/13/96 < 16 < < < < 07/08/96 29 5.8 < < LO < 05/16/97 3.4 12 < 6.8 < < 07/29/99 13.3 19.2 < 10.5 < < 02/11/00 11 17 < < 1.0 < 07/09/01 < 2.3 < 2.3 < < 08/07/02 7.9 19.1 1.6 11.3 < < 06/24/03 6.9 9.9 1.4 5.2 < < 04/21 /04 6.0 12.4 1.1 7.0 < < 0428/05 5.6 16 13 < < < 04/04/06 11 23 1.4 14 < < 03/19,07 13 35 2.7 19 < < 04'29/08 9 22 1.8 12 < < 04/23/09 5.5 14 1.6 7.7 - < 04/05/10 4.1 83 < 4.3 < < 05/02/11 3.6 10 < 5.9 < < 04/03/12 3.6 7.2 < 4.3 < < 04/3013 49 9.5 < 4.3 < < 0512/14 4.1 7.6 < 3.2 < < 2 of 12 CRa CkokWcal En voomemr savK*s, Inc. Table 2 - Historic dronndwatef Analytical Remits B/E Aerospace Facility, NCDO60302577 1455 Fairchild Road, Winston-Salem, North Carolina `ICE Vmyl Sample ID Sample Date PCE TCE 1,1-DCE 1,1,1-TCA Chloride pg L NC 2L GW Standard' 0.7 3 7 70 200 0.03 MW-8 05 1997 99 45 < 21 < 04/21/04 33.2 7.2 2.8 04 28 05 t8 4.6 < 04/04/06 10 3 05/12/14 4 Mw_9 05 1997 13 < < < 07/2919 < < < < 07/09/01 < < < < < 08 07 02 < < < < < 06/24/03 < < < < < 04/19/04 < < < < < 04/27/05 < < < < < 04/05/06 < < < < < < 03/1%07 < < < < < < 04/22/09 < < < < < 04/29 10 < < < < < < 0426111 < < < < < < 04/03/12 < < < < < < 04/30/13 < < < < < < 05/12/14 < < < < < < MWAOD 05 1997 4.7 < < < < < 07/29/99 < < < < < < 10/12/00 < < < < < < 04/10/01 < < < < < 04/23/02 < < < < < 04/09/03 < < < < < < 04/19/04 < < < < < < 04/27/05 < < < < < < 04 05/06 < < < < < < 03/19,07 < < < < < 04/29/08 < < < < < 04/21/09 < < < < 04/0510 < < < < 04 26/11 < < < < 04/03/12 < < < < 04/30/13 < < < < 05/12/14 < < < < < MW-11 05,19 97 2.1 < < 15 120 < 07,28,99 1.7 < < < 20 < 07/09/01 < < 1.1 < 5 < 08/07/02 < < < < 2.2 < 06/24/03 < < < < 3.3 < 04/19/04 1.0 < < < 4.4 < 04/27/05 < < < < < < 04/05/06 < < < < < < 0319/07 < < < < 1.1 < 04/05/10 7.4 < < < < < 01/24/11 13 < < < _ < 04/27/11 7.9 < < < < < 07/22/11 8.7 < < < < < 10/06/11 2.2 < < < < < Ol /24 12 1.9 < < < < < 04,03/12 1.2 < < < < 0413013 < < < < 0512/14 < < < < 3 of 12 CRB Geok%ical Environmental Servitea, Inc- Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina cis 1,2 Vinyl Sample ID Sample Date PCE TCE 1,1-DCE DCE 1,1,1-TCA Chloride pg,L NC 2L GVR' Standard` 0.7 3 7 70 200 0.03 MW421) 0519:97 4.9 < 1.3 < 6.0 < 07;28;99 109 < < < 9.7 < 101200 17 < < < < < 04/ 10/01 7.6 < < < < 041*23/02 11 < < < < < 04/09/03 8.4 < _ < < < 04.2004 3.8 < < < < < 04 27 05 15 < < < < < 04,105/06 6.4 < < < < < 03i20.07 5 < < < 04 30/08 3.9 < < < 07/23/08 5.8 < < < < < 11/18/08 8.8 < < < < 04/22/09 2.8 < < < < 04, 06,10 3.3 < < < < < 05/02/11 1.7 < < < < < 07122.11 1.8 < < < < 04 02/12 1.6 < < < < 07/25'12 1 < < < < 11/09/12 < < < < < < 02i07/13 < < < 05/0113 < < < 08105.13 < < < 12 03/13 < 03/07,14 < < < < 05.12/14 1.1 < < < < MW-13 05/19/97 7.4 < < < < < 04/04:06 1.3 < < < < < 03/20/07 1.7 < < < < < 04/2611 < < < < < < 05, 12.14 < < < < < MW-14D 05/l9/97 1200 170 < < < 10:1'13i'00 2000 120 61 < 58 04/10/01 770 67 75 < 55 < 04,123/02 1600 71 100 < 69 < 04 09'03 1050 46.2 109 1.4 569 < 04 20:04 1270 38.8 117 1.16 649 < 04/27/05 2000 39 100 < 46 04/06/06 1700 24 56 < 23 03/20/07 2400 30 91 4.5 25 04/30108 1500 29 61 30 l5 < 04.'23109 2000 24 57 110 - < 04/06/10 900 31 25 220 5.5 < 10/28/10 1300 27 22 190 - < OVUM 1300 23 17 170 < 04/25 11 650 < < 190 < < 0802111 1000 19 11 120 < < 10/06/11 1200 17 12 67 1.8 < 01.24/12 900 14 < 50 < < 04'04/12 1000 < < 60 < < 07/26/12 1000 17 10 46 < < 11/08/12 1000 20 8.9 45.6 < < 02,0713 1200 15 6 36 < 05i01113 1100 19 < 53 < 08!05 13 1100 17 5 56 < 1103113 848 21.1 3.9 68.5 < < 03/07/14 853 20.5 < 60.4 < < 0512/14 624 28 3.9 98 < < 4 of 12 CRB Geological Environmental Services. Inc. Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCDO60302577 1455 Fairchild Road, Winston-Salem, North Carolina Vinyl Sample ID Sample Date1'CE TCE 1,1-DCE DC1E 1,1,1-TCA Chloride pg,L NC 2L GR' Standard 0.7 3 7 70 200 0.03 MW-15R 092606 1200 40 70 2 23 03/20/07 1200 42 81 2 22 < 05101 "08 1300 39 83 2.1 17 < 04'23/09 1800 38 86 < - < 03/10/10 1400 26 64 9.8 < < 10/28/10 1600 27 51 44 - < 01/24/11 1100 20 34 44 - < 05/03/11 940 19 38 50 < < 10/05/11 990 19 32 57 3.4 < 01/2412 990 19 26 66 < < 04;03/12 890 19 25 69 < < 07/26/12 890 16 18 63 2.2 < 11/08/12 817 24 25 79 < < 02/07/13 780 19 19 68 < < 05/01/13 830 20 23 66 < < 08/05/13 820 17 17 60 1.5 < 12/03"13 735 15.8 13.1 56.7 < < 03/07/14 285 7.3 4.9 19.1 < < 05/19/97 1800 70 120 < 270 < 07/28/99 773 94.1 < 98 < 07/11/01 930 26 54 2.2 62 < 06/24/03 1490 25.2 62.6 1.66 49 04/20/04 1040 16.9 44.4 1.22 27.8 04/28/05 320 6.9 18 < I < 04/06/06 440 5.8 9 < 7.1 < 03/20/07 560 11 20 < 10 < 04/30/08 920 10 16 < 6.7 < 04/22/09 680 < < < - < 04/06/10 720 < < 22 < < 01/24/11 410 3.9 3.4 4.1 - < 05/03"11 310 < < < < 08/02/11 420 < 6.7 < < 04/03/12 290 < 8 < < 05/01 / 13 380 5.6 < 15 < < 05/12/14 83.4 3.6 < 13.1 < < MR--17D 12/15,99 < < < < < 01/05/00 < < < < < 07/09i01 < < < < 08/07/02 < < < < 06/24.03 < < < < 04/19/04 < < < < < 04/27/05 < < < < < 04/05/06 < < < < < 03/19/07 < < < < < 04/29t08 < < < < < 04/2309 < < < < - < 0405/10 < < < < < < 01/24/11 < < < _ < 04/27/11 < < < < < 04/03/12 < < < < < 04/30/13 < < < < < 05/12/14 < < < < < < 5 of 12 CRs Cxolupcal EnvironwmW Services. Inc. Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina G1s 1,2 Vinyl PCE TCE 1,1-DCE 1,1,1-TCA Sample ID Sample Date DCE Chloride L NC 2L GW Standard' 0.7 3 7 70 200 0.03 MW-18 1215 99 171 13.9 3.6 22.1 22 < 07/10/01 71 21 4 33 3.1 < 08 07 02 50.9 7.71 2.57 15.6 2.0 < 06 24 03 549 28.3 3.9 26.7 2.5 < 04119'04 227 45.3 5.6 54.8 2.6 < 0427;05 190 43 6.3 < 3.1 < 04/05/06 210 36 6 82 < < 03,20/07 98 20 4.6 53 1.3 < 09/12/07 93 33 2.3 30 1.3 < 0430/08 160 11 1.6 24 < < 04/23, 09 160 11 2.1 23 < 09,0209 210 25 < 27 < 04 061,10 180 15 2 26 < < 1028/10 80 22 1.6 25 < 01124, 11 85 13 1.5 25 < 0503/11 86 10 1.7 25 < < 08.102/11 190 19 1.8 41 < < 10/0611 78 9.8 < 25 < < 012412 91 10 1.2 25 < < 04 03/12 150 16 1.7 34 < < 0726i12 64 12 1.6 43 < < 11108/12 131 9.4 < 22,8 < < 02/07/13 36 4.5 < 12 < < 05101' 13 97 9.2 < 16 < < W05 13 110 11 < 23 < < 12/03'13 105 6.4 9.2 40.1 < < 03.07,14 66.6 7 9.1 15.8 < < 0512/14 197 10.2 < 12.9 < < MW-19 01/06/00 150 8 48 < < < 04/10/01 64 < 55 < 23 < 04 23 02 220 < 49 < 12 < 04 09 03 70 1.33 36.1 < 12.8 < 04 19/04 74.5 1.9 36.8 < 10.5 < 04,27,05 220 6.5 100 < 16 < 04 05 06 180 4.8 100 < 14 < 03/20 07 180 3.8 140 1 15 < 04/30`08 130 3 130 < 9.3 < 04/22/09 120 2.2 110 < - < 04 06/10 100 1.7 33 < 3.6 < 10128/10 110 2.2 82 < - < 01/24/11 100 1.6 68 < - < 05/03/11 65 1.1 49 < 2.2 < 08/0211 85 1.5 64 < 2.7 < 10 06111 83 1.3 53 < 2.1 < 01,24/12 37 < 19 < < < 04//04/12 53 1 30 < 1.4 < 07/2612 56 1.2 42 < 1.6 < 11/08.12 29.9 < 29.4 < < < 02/0713 45 < 25 < < < 05/01,13 42 < 16 < < < 08 051'13 44 < 20 < < < 12/03/ 13 65.4 1.1 30 < < < 03/07/14 35.9 < 12.1 < < < 05/12/14 31.7 < 8.4 < < < 6 of 12 CRB Geological Enciromental Services, Inc. Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCD060302577 1455 FAirrhild Road, Winston-Salem, North Carolina cis 1.2 Vinyl Sample ID Sample Date PCE TCE 11-DCE DCE 1,1,1-TCA Chloride µ ;L NC 2L GIA' Standard[ 0.7 3 7 70 200 0.03 MW-20 0106/00 44 6 11 < 5 < 07.10 01 72 7.6 16 < 8.9 < 08 07 02 84.1 5.6 35.8 < 8.0 < 06/24,03 274 7.5 109 1.1 31.2 < 0419,'04 267 5.2 188 1.0 24.3 < 04/27/05 250 6.4 220 < 31 < 04 05 06 150 < 120 < < < 0320 07 230 5.8 220 1.2 22 < 04 W08 210 5.8 270 1.2 15 < 04 22 09 140 4.4 130 < - < 04 06110 35 2.6 8.4 < < < 05,03/11 49 3 36 < 1.7 < 04/03/12 64 3.2 31 < 1.4 < 05/01/13 78 2.9 23 < < < 0512,14 55.7 2.9 15.1 < < < MW-21D 01 0500 1200 68 170 < 180 < 07`10/01 2200 70 190 1.9 150 < 08/07/02 1480 39.2 140 11.9 96 < 06/24/03 1090 26.5 121 < 89 < 04/20/04 1580 34.9 139 1.3 67.3 < 04 27/05 1700 26 91 < 49 < 04/05/06 5600 < < < < < 03.20/07 2200 18 50 7.4 16 < 04,/30/08 1200 12 21 8 6.6 < 04/22/09 880 < < < - < 04i06/10 1400 < < < < < 10/28AO 1600 9.9 6.8 21 < 01r24/11 1500 13 6.6 26 < 05/0311 970 < < 26 < < 08; 02 11 1300 12 < 37 < < 1006,1111 1300 13 3.8 37 < < 01,24/12 1300 18 < 62 < < 04/04/12 800 15 < 68 < < 0726./12 1100 13 3.7 69 < < 11/OS/12 1060 24.4 < 76.9 < < 02/07/13 740 19 2.5 73 < < 05/01/13 1000 21 < 68 < < 08;0513 1100 18 2.4 72 < < 12/03/13 920 15.5 < 77.1 < < 03 0714 629 15.1 < 62.2 < < 05! 12 14 531 20.4 1.5 73.4 < < MW-22D 011,05,00 570 55 20 < 50 < 07/ 11 /01 200 8.1 3.5 1.3 2.5 < 08/07/02 941 26.3 42.3 11.9 28.7 < 06.24103 < < < < < < 04 20 04 < < < < < < 04/2705 < < < < < < 04;06/06 < < < 2.6 < < 04 30 08 38 2.9 11 87 < < 04/221!09 31 < < 6.2 < 04/04/12 190 17 2.3 130 < < 07/26, 12 38 11 < 58 < < 05 01 13 18 4.8 < 8.2 < < 05/12,14 < < < < < < 7 of 12 CRB Geological Environmental Services. Inc. Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina cis 1,2 Vinyl PCE TCE 11-DCE 1,1,1-TCA Sample ID Sample Date DCE Chloride Pg L NC 2L GW Standard' 0.7 3 7 70 200 0.03 MW-23 010600 1200 29 130 < 150 < 02:11 00 1200 < 130 < 110 < 07 1001 1000 22 62 < 63 < 06.2403 465 9 43.8 < 33 < 0420 04 440 6.73 30.9 < 19.7 < 04/28/05 770 8 16 < 11 < 04 05�06 680 < < < < < 03:20 07 920 7.1 9.8 < 5.7 < 0430,08 1000 6.2 7 < 2.6 < 04 22 09 320 < 12 680 - 0.019 04 06,110 93 < < 400 < < 05/03/11 18 1.4 2.4 450 < 6.4 04.04/12 7.7 < < 200 < < 05/0113 16 < < 120 < < 0542,14 14 8 < < 66.9 < < MW-24 01 06 00 1100 67 66 < 52 < 0426100 1500 87 68 < 57 < 07/10,01 930 55 61 3.4 39 < 08/07/02 620 38 49 6.3 25 < 06/24/03 802 55 57 16 24 < 04;20r04 1040 85 48 13 13 < 04 28 05 530 66 38 < 9.9 < 04'06106 510 44 29 20 < < 03'.20 07 610 56 46 21 11 < 04 30.`08 570 42 22 13 5.2 < 04/22/09 520 21 12 11 - < 04:'06/10 560 26 12 12 < < 05/03/11 460 13 8.1 9.7 1.7 < 04/04/12 490 23 < 15 < < 05/01/13 280 47 < 30 < < 05/ 12 14 111 19.2 < 15.4 < < MW-261) 01/05,'00 10 < < < < < 071001 1.8 < < < < < 08%07/02 < < < < < < 06i24iO3 < < < < < < 04119./04 < < < < < < 04,27/05 < < < < < < 04,05/06 < < < < < < 03120/07 < < < < < < 04/30/08 < < < < < < 04/22/09 < < < < < W106'10 < < < < < < 05 02/11 35 3.1 < 5 < < 07/22r11 < < < < < < 04'02/12 < < < < < < 05/01/13 < < < < < < 051,1214 < < < < < < MW-27D 01.06'00 8 < < < < < 07,109:01 4.5 1.5 < < < < 08/07/02 3.9 1.0 < < < < 06/24/03 2.1 < < < < < 04/20/04 3.4 < < < < < 04/28/05 1.5 < < < < < 04 04 06 2.2 < < < < < 03 '20 07 2.9 < < < < 1.7 05 01108 2.7 < < < < < 04: 23, 09 2.6 < < < < 04.07/ 10 2.2 < < < < < 04 26/ I 1 < < < < < < 04/03/12 < < < < < < 043013 < < < < < < 0512114 < < < < < < 8 of 12 CRB Geological Environmental Semces, Inc. Table 2 - Historic Groundwater Analytical Results B/F Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina cis 1,2 Vinyl PCE TCE 1,1-DCE 1,1,1-TCA Sample ID Sample Date DCE Chloride L NC 2L GW Standard 07 3 7 70 200 0.03 MW-27DD 07 09 01 < 1.4 < < < < 0807,02 < < < 1.08 < < 06 24 03 < < < < < < 04.20;04 < < < < < 0428,05 < < < < < 04/04/06 1 < < < < < 03/2007 1.2 1.1 < < < < 04 22 09 1.3 < < < 040710 < < < < < < 04 26 11 < < < < < 04 0312 < < < < < 041,30/13 < < < < < < 05/12/14 < < < < < < MW-28 01,06,00 13 < < < < 070901 16 5.2 1.6 < 2.0 < 04 23 02 18 6.6 < 12 1.7 06/24�03 48.2 11.4 9.5 < 7.1 04 21,04 24.1 5.3 2.4 < 2.5 04/28/05 5 12 < < < < 04/04/06 6.1 1.3 < < < < 03/1907 5.5 1.3 < < < < 04'29 08 6.1 1.2 < < < < 0422,09 3.8 < < < < 04105;10 9.1 1.8 < < < <. 04.26/ I 1 5.8 1.5 < < < 04/03/12 4.5 < < < < 04 30/13 6.5 12 < < < < 05112/14 8.5 2.1 < < < < MTV-29 01 0500 350 6 7 < 16 < 02./1100 280 7.4 8.9 < 19 < 0740i01 360 7.7 4.6 3.2 9.1 08/07/02 250 5.9 < 1.7 10.4 06.'24.03 1410 11.7 7.9 1.9 13.8 < 04,19,04 1410 7.4 3.5 1.8 5.58 < 04,27/05 1200 < < < < < 0405.06 620 < < < < < 03/20/07 550 3.9 < 2.1 < < 04t30/08 58 < < < < < 04i22/09 180 < < 100 04/06;10 120 < < 62 < 05*0211 13 < < 54 < < 04 02112 13 < < 20 < < 05.01;'13 30 12 < 21 < < 05,12/14 1.9 < < 24.4 < < MNV-30 01/05r00 3400 39 38 < 120 04;26,00 8100 < < < 04/10/01 2900 25 21 < - 04/09;03 7450 48.9 10.2 4.0 36.5 < 04/20/04 14200 55.6 9.5 7.5 29.9 < 04:27 05 3900 < < < < < 04 05:06 5500 15 < < < < 03/2007 1500 4.7 < 1.5 1.4 09.12r07 170 < 16 < < 04,3008 40 < < < < 04 22'09 21 < < 3.0 - 04 0610 24 < < 82 < < 05 02il1 53 1.1 < 16 < < 01/2412 48 1,1 < 46 < < 04/02'l2 22 1 < 19 < < 050113 31 < < 21 < < 05121:14 7.4 < < 52.5 < 9 of 12 CRB Geological Emvonmenial Sery e- tnc. Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem. North Carolina cu1,2 Vinyl Sample ID Sample Date PCE TCE 1,1-DCE DCE 1,1,1-TCA Chloride q'L NC 2L GW Standard 0.7 3 7 70 200 0.03 MW-32 03 3100 48 21 < < < < 07.10 01 27 13 < < < < 04 28 05 23 5.8 < < < < 040406 41 5.8 < 1.3 < < 03 2007 32 6.5 < 1.9 < < 04 29108 20 4.2 < 1.3 < < 0423 09 14 2.5 < < < 0406 10 18 3.1 < < < < 0502 11 17 1.6 < < < < 0404 12 9.9 1.1 < < < < 0501'13 13 1.2 < < < < 05'12'14 12.3 l < < < < MW-33 03 31;00 55 < < < < < 04,10,01 17 < < < < 04 2302 15 1.2 < < < < 04 09 03 7.2 < < < < < 0420,04 24 < < < < < 04, 28, 05 43 < < < < < 04/04/06 46 l < < < < 03'20/07 36 < < < < < 04/30 08 10 < < < < < 04 23 09 10 < < < < 04 0710 6.9 < < < < < OL24i11 14 < < < < < 0427/11 5 < < < < < 07/22/11 7.8 < < < < < 10-06/11 6 < < < < < 01/24,12 6.3 < < < < < 04 03/ l 2 5.2 < < < < < 07/25r12 5.1 < < < < < 1140812 5.7 < < < < < 02 07 13 4.7 < < < < < 04 30 13 5.3 < < < < < 12,03 13 5.5 < < < < < 03,071i14 3.3 < < < < < 0512/14 4.1 < < < < < 10 of 12 CRB Geoloaical Eu irot=enial Services. Inc. Table 2 - Historic Groundwater Analytical Results B/E Aerospace Facility, NCDO60302577 1455 Fairchild Road, Winston-Salem, North Carolina cis 1,2 vinyl Sample ID Sample Date PCE TCE 1,1-DCE DCE 1,1,1-TCA Chlo de ,L NC 2L GVL' Standard 0.7 3 7 70 200 0.03 RW-1 03 31 00 2500 27 19 < 64 10/12/00 5500 < < < < < 07/ 11/01 1500 < < < < < 10/18/02 1030 7.21 4.9 < 10.6 < 06/24/03 4150 17.8 8.3 2.0 18 < 04/20/04 6740 30 4.6 3.7 15.5 < RR =2 03 31 00 1700 89 120 < 89 < 10/12/00 2200 < 160 < 120 < 07/ 11 /01 2000 < I80 < < < 08/07702 1710 56.7 136 1.6 99 < 06/24/03 1250 43.9 45.3 < 72.8 < RW-3 03 31,00 140 22 < 16 < < 10/12/00 280 27 1.1 16 1.2 < 07/11/01 160 25 < 20 < < 08/06/02 171 19.9 < 19.4 < < 06/24/03 190 22.4 24 22.3 < 04/ 21 /04 164 18 1.1 19.4 04/28/05 100 12 < < < 04/06/06 75 7.9 < 14 < < 03/20/07 140 13 < 20 < < 05101, 08 91 8.6 < 1.5 < 041.23/09 89 6.8 < I - 04/06/10 46 4.6 < 6.8 < < 08./02/11 34 3 < 3.7 < < 04/03/12 28 2.7 < 3.4 < < 05/01/13 24 2.2 < 1.9 < < 05/12/14 19.5 1.9 < 1.8 < < 11 of 12 CRB Geolopcal Environmental services, Ine. Table 2 - Historic Groundwater Analytical Results BiE Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina cis 1.2 Vinyl Sample ID Sample Date PCE TCE 1,1-DCE DCE 1,1,1-TCA Chloride L NC'-),' GR' Standard' 0.7 3 7 70 200 0.03 B-2 03,20/07 3 < 1 < < C-3 0406 10 4 < < < < < 04- 04-1_ 43 1.0 20 20 < < C-3 04/30/08 68 4.5 18 2.8 < < C-5 12 1206 59 < < < < < 0406 10 1000 < < < < < 0404 12 47 < < < < C-8 04, 06,10 24 < < 15 < C-9 0406,10 990 < < 75 < < 04, 04,12 1100 < < 270 < < C-11 07 25 06 290 22 < 1.1 13 < 12/1206 5 < < < < 03 20 07 69 < < < < 04 30/08 14 1 < 1.7 < < D-2 1006,11 360 < 84 19 < < D-3 10 06./11 5 < < 5.8 < D-5 07/25/06 380 2.4 2 < 2.4 < 03120707 190 < < 6.7 < 0430/08 6 < < 35 < < D-7 07 25:06 3700 13 5 2.6 6.6 < 12 1206 1700 11 4.9 1.6 2.9 < 03 20 07 2400 10 < < < < 04 30:08 1200 46 4 750 < 7.2 0422,09 110 < < 2000 28 0406 10 65 < < 580 < < 10 06/ I 1 82 < < 87 < 1.9 04 04112 18 < < 110 < < D-11 0407 10 13 < < < < < F-2 12/13/06 21 3.9 21 1.2 2.2 1 03/20'07 21 6.2 18 1.7 < 1.6 F-3 12/ 13'06 7.2 < < < < < F-1 44/05/12 15 1.8 < 3.7 < < <-Below Detection Limits 1-CE-Trichloroethene TCA-Trichloroethane (D)-Duplicate Sample DCE-Dichloroethene PCE-Tetrachloroethene NC 2L-North Carolina Title 15 A Subchapter 2L Groundwater Quality Standards. 12 of 12 C'RB Geolowcal Enciroumenul Services. Inc. Table 3 - Groundwater Physical Parameters B/E Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina hI%V ID Sample PH DO ORP Conductnin• Date PPm UIV us NRVI 4,52006 7.3 2.2 60 31 9:25:2006 5.6 3 5 301 - 3 202007 7.6 - 40 34 4292M 7.3 -170 5 4# 212009 6.2 7.5 125 41 4'5i2010 7,6 2.8 76 35 124i2011 5.9 1.7 250 75 7%22i2011 6.6 0.0 28 53 1016.2011 5.6 - 184 28 4'3'2012 6.6 6.8 60 32 7'25/2012 6.5 6.8 121 28 11:8i2012 5.9 6.3 86 27 2/7,2013 5.9 4.9 83 - 4; 30.2013 6.1 6.1 195 27 8'52013 6.l 6.7 211 28 113/2013 - - 55 286 5/12: 2014 6.7 6.5 149 - I.1W3 4i62006 5.5 - 381 69 9252006 4.9 2.1 419 - 3,20/2007 5.9 - 350 66 4/30R008 5.3 - 249 73 4'5,2010 5.6 0.6 238 96 5/3/2011 45 - - 84 4i2/2012 4.3 2.3 160 103 5/1i2013 5.7 1.5 374 82 5,13i2014 4.7 0.7 - - AIW4 4/5/2006 6.2 5.9 101 140 9.25/2006 5.3 4.8 280 - 4 21,2009 7.3 4.6 215 154 4 `5.'2010 6.6 1.6 117 150 43/2012 6.6 3.2 96 164 MW5 4 52006 6.3 5.3 64 103 3.12012007 6.2 - 151 99 4i29/2008 4.6 - 89 85 4:21,2009 6.8 0.1 -57 437 45/2010 6.2 0.5 -55 300 4/32012 6.6 0.4 -4 176 4/30/2013 65 0.1 -12 177 5/12/2014 5.8 4.5 - - MW6 4,52006 5.0 9.1 160 277 9252006 5.0 4.2 190 - 9'122007 5.1 0.5 -170 195 4/30/2008 6.8 - -80 195 4/22,2009 6.6 1.1 -111 950 4'5/2010 6.7 2.2 -93 1325 1/24/2011 5.7 0.3 -70 509 7/22,2011 3.8 0.0 -122 628 I062011 5.9 - -33 360 l:'24;2012 5.9 1.1 -69 400 4,i2/2012 6.0 2.4 205 242 7/25/2012 6.5 2.0 -25 272 11/8/2012 6.4 2.1 -50 200 217'2013 5.9 2.4 -51 - 5 1/2013 6.4 1.1 -69 230 8/5/2013 6.3 0.3 -82 315 12/3/2013 - - 16 230 3/7/2014 10.9 96 165 5/12/2014 6.0 0.6 - - Page 1 of 7 Table 3 - Groundwater Physical Parameters WE Aerospace Facility, NCDO60302577 1455 Fairchild Road, Winston-Salem, North Carolina MW ID Sample pH DO ORP Couductiv'in• Date p at uIv us MW7 4,4,2006 6.7 8.8 51 77 3:20:2007 6.3 - 123 78 4292008 7.9 - 175 123 4: 212W 5.4 7.7 176 94 4 52010 6.8 9.4 124 88 5'2011 4.2 - - ill 4311412 6.6 7.8 89 136 VW2013 5.7 7.8 272 117 5.132014 5.0 7.9 - - MW8 4'4/zo011 - - - - 5/13T_014 NOT ENOUGH WATER AfW9 452006 6.8 - 108 19 3202007 6.3 - 188 20 4.21;2009 6.0 7.7 172 32 4.52010 5.7 9.0 106 39 42620i1 - - - - 4!3/2012 6.9 9.0 155 53 4130,2013 5.5 7.4 131 66 5112R014 5.3 6.0 20 - MW10D 4OP-006 7.2 - -26 143 3/202007 11.4 - -170 327 429 2008 9.5 - -310 218 4217009 10.3 3.5 67 202 415/20W 7.7 1.2 -7 353 4,12012 7.0 6.4 -18 206 430,2013 7.1 2.2 73 141 5-122014 6.6.3 1.4 130 - MWI1 4`5/2" 5.4 - 189 46 3/20'2007 5.7 - 115 56 92'2009 52 5.7 13 763 4'5/2010 5.8 0.5 -50 1296 1/24/2011 5.0 13 49 554 7,22/2011 5.6 - -51 750 10/6,2011 5.0 - 33 635 1'24_'2012 8.1 2.1 10 499 4/3i2012 5.8 1.7 60 560 4/30/2013 6.2 6.1 178 285 5.'12,'2014 dry - - - bfW12D 4;5/2006 73 5.8 82 46 9.25.2006 5.5 3.2 308 - 3'20'2007 Z5 - 28 41 4/30/2003 6.0 - 103 37 4/21/2009 6.5 7.0 200 49 4'15/2010 6.7 83 125 58 7/22/2011 5.3 1.5 134 67 4/2:1)12 6.6 9.2 54 74 725'2012 6.3 9.0 110 79 11!8.2012 6.3 8.1 125 85 2!7/2013 5.9 72 47 - 5/ 1!2013 6.5 7.7 105 81 8/5/2013 5.6 6.6 107 77 1213.2013 - - 59 79 37/2014 - 6.8 18 14 5/12i2014 5.7 0.9 - - bSW13 414/2006 8.8 8.6 2 173 3/20/2007 10.3 - 101 221 5,13/2014 dry - - - Pace 2 of 7 Table 3 - Groundwater Physical Parameters WE Aerospace Facility, NCDO60302577 1455 Fairchild Road, Winston-Salem. North Carolina VA' ID SanTle pH DO ORP Conductivity Date m at"' its %IW 14D 4:62006 5 5 - 127 101 9 23:2006 5.2 49 291 - 9122007 7.3 6.5 123 108 4 292008 5.7 - 107 176 4.222009 5.5 2.8 150 129 4'Si2010 5.9 0.8 227 160 11242011 4.7 0.1 94 136 4,Z/2011 4.9 - - 150 8, 2 2011 50 0.0 140 I l2 1062011 5.3 129 130 1'24"2012 6.1 2.8 192 135 4;42012 6 1 3.0 77 127 T262012 6.8 5.5 133 107 1 1'820l_' &0 43 159 126 272013 5.5 3.4 147 5• U2013 6.0 0.9 290 126 12/32013 - 167 124 3'72014 - 11.8 103 130 5132014 5 9 0.3 - NM"15R 320/2007 6.7 - 105 104 4'92007 - - 77 17 11152008 5.8 5.1 63 111 5,T2008 6.9 -60 101 7 23,2008 6.2 7.3 185 120 1l'182008 6.2 5.5 200 223 4222,2009 6.7 5.8 132 117 1242011 51 3.7 201 137 1015:2011 5.7 - 198 142 1 24 2012 7.3 2.9 198 128 4'3/2012 6.1 2.9 100 125 7/2&2012 72 3.0 94 116 11182012 6.1 2.6 144 D4 2/70-013 6.7 2.9 133 - 5/1!2013 6.2 0.7 284 129 12/32013 - - 182 130 372014 - - - - NM'16 4i62006 5.9 - 118 120 9i 252006 5.0 - 330 12'132006 4.8 4.0 267 87 320,12007 6.2 - 220 108 912'2007 6.2 5.0 50 70 41302008 5.8 - 218 107 4121,2009 5.5 4.6 246 145 4/52010 6.3 4.7 162 136 1£242011 4.7 4.2 138 128 51.2011 5.1 - 122 Si2.2011 5.5 0.0 109 115 4'32012 9.9 4.2 60 113 5/12013 5.9 4.1 300 114 5/112014 5.5 2.5 - MW17D 4-52006 6.3 4.5 60 101 3202M7 6.4 - 59 90 429,7W8 4.6 - 86 79 4M/12009 5.1 0.4 174 85 415,2010 5.2 0.8 97 131 1:242011 4.8 1.5 150 218 4'32012 6.4 0.7 146 85 4302013 5.8 0.3 108 83 51•122014 5.3 0.4 - - Page 3 of 7 Table 3 - Groundwater Physical Parameters B-'E Aerospace Facility, NCDO60302577 1455 Fairchild Road, Winston-Salem, North Carolina TOWID �k PH DO ORP ConductlNit)' m mV us NA'18 4'52006 6.1 4.6 74 75 9 25.2006 4.9 3 2 314 - 12 122006 &9 - 255 - 3202007 6.4 - 17 63 9 122007 5_2 19 -115 44 4130008 5.5 106 61 4/21,2009 4.6 1.3 247 77 4,'5:2010 5.8 0.9 216 97 24:2011 4.0 1.5 115 180 5 3.2011 4.1 - - 100 8T2011 5.2 0.0 133 123 10,62011 5.1 - 167 105 I12.42012 74 0.6 -21 106 4.32012 7.0 0.9 175 87 7262012 6.1 3.6 163 95 11,&2012 5.9 1.8 116 130 Z72013 5.9 2.4 110 - 512013 6.0 0.3 245 118 8.'5/2013 5.5 0.7 200 111 12/3/2013 - - 88 127 N12014 - 0.9 107 100 5112014 5.8 0.1 - - MW19 4/5,2p06 6.6 6.1 109 208 9 25,2006 5.9 3.2 224 12 12 2006 6.3 - -50 182 3'202007 6.9 - -62 160 9/122007 5.9 3.2 -110 115 1.15.2008 6.1 2.4 35 175 4302008 6.2 - 190 183 7,23.2008 6.2 4.9 93 218 11/1&2008 6.1 3.2 220 220 4/212009 63 4.1 161 203 4.'5/2010 6.7 3.4 130 129 11 ,7011 5.6 2.9 30 199 5/32011 6.3 - - 190 8112011 6.3 0.0 77 191 10.'62011 5.8 - 147 196 V2412012 5.7 3.5 190 202 4.42012 9.0 4.3 -15 184 7262012 6.5 46 150 188 I18.2012 6.5 3.5 40 197 21,1013 6.1 3.7 121 5112013 6.3 3.7 196 164 8!5/2013 6.1 2.5 239 I60 12/32013 - - 122 184 3.'72014 - 10.8 88 156 5'12,2014 6.0 5.6 - - MW20 45/2006 6.4 8.8 107 74 9.'25/2006 5.1 5.1 313 - 3120,2007 6.1 - 72 lot 4'302008 5.2 - 205 107 4�21.2009 5.4 1.7 213 122 4 51-010 6.4 1.5 63 85 513/-1011 5.6 - - 120 4/3 2012 7.2 1.0 158 139 5/L2013 6.1 2.8 231 156 5;112014 6.0 0.4 - Page 4 of 7 Table 3 - Groundwater Physical Parameters BB Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina MW ID Semple Date PH DO ORP Cond--ity w mC us NfW21 D 4 5.2006 62 8.0 125 116 9252006 53 4.8 291 - 9I22007 7.2 5.3 110 120 4/302008 6.0 - 228 123 4222009 6.5 6.3 201 145 4152010 6.3 5.0 186 139 1/24/2011 4.9 41 70 146 5132011 52 - - ISO 9/2,2011 5.1 00 105 158 lO 2011 5.6 - 127 149 1242012 8.1 3.9 62 159 447012 5.7 4.9 91 145 7262012 7A 5.2 193 133 11/82012 5.6 3.8 188 143 Y12013 5.5 2.7 153 - 5/12013 6.1 19 238 143 8.'52013 40 3.5 220 147 12/32013 - - 142 147 3/72014 - 11.3 84 146 5/132014 5.8 1.6 - - Mnl'22D 4&2006 - - - - 4/302008 7.6 - -106 33 4/22/2009 9.0 0.1 -67 58 4/3,2012 82 0.7 -2 37 7:'262012 7.6 0.7 -53 78 511,2013 83 0.1 -308 40 5/ 132014 8.6 1.0 - - bfW23 4'5,2006 6.1 - 127 90 3202007 6.4 - 112 109 4/302008 6.0 - 106 118 9/12009 5.4 - 186 691 4152010 5.8 003 65 550 4/42012 8.4 1.6 40 457 5/12013 5.3 3.2 113 230 5/132014 4.3 0.8 - - MW24 4/6,2006 5.6 23 124 55 M52006 - 0.9 297 - 3'202007 59 - 71 83 4/302008 5.4 - 249 83 4'222009 5.0 0.8 228 109 4/52010 5.8 0.7 235 101 5/32011 4.3 - - 88 4/4/2012 7.0 1.0 40 91 5112013 5.7 23 275 113 3/131014 5.3 0.6 - - ' 4'6.2006 63 - 108 77 3202007 6.4 - 72 55 S/ll2014 5.8 L2 - - S1W26D 452006 6.1 6.7 138 85 YM2007 7.7 - 100 55 4/30/7009 6.5 - 50 53 412l2009 7A 3.6 165 65 4/5,2010 7.0 3.4 107 68 5/22011 53 - - 59 7/222011 5.2 0.0 -22 70 4/12012 6.6 53 32 75 5/1,2013 6.9 3.4 253 61 5/122014 6.6 2.8 - - Page 5 of 7 Table 3 - Groundwater Physical Parameters B/E Aerospace Facility, NCD060302577 1455 Fairchild Road, Winston-Salem, North Carolina NMAD &vWk PH DO ORP C011dUCt-IN Date m My NiW27D 4/4-2006 12.5 4.8 -55 33l 3202007 14.0 - -92 1290 4 23 2009 7.8 3.8 73 24 415,2010 11.5 4.8 13 919 4'3'2012 11.6 6.8 -107 494 4 304013 10.7 6.9 94 113 5,132014 10.8 43.6 - - MW271313 4�42006 8.9 1.7 -30 231 3202007 8.6 - 62 220 4.123.'2009 7.4 3.9 75 212 4i5r'_OIO 6.7 4.4 154 251 4/3.2012 10.0 0.7 -300 275 A 30 2013 7.5 0.3 48 263 5 132014 7.4 5.4 - - N1W28 4i42006 5.5 4.8 119 135 3 *202007 5.8 - 235 101 4'29,2008 4.6 - 118 107 4/212009 5.0 3.6 161 1464 45C(110 5.1 4.1 225 163 492012 6.3 5.8 165 150 4,102013 5.4 3.7 256 157 5/12/2014 4.6 16.3 711 - N1W29 4 52006 5.7 - 145 103 9/25:2006 4.7 6.3 315 - 3/202007 6.2 - 14 86 4302008 6-9 - 40 405 4222009 4.7 0.4 -6 3015 415201C 56 - 13 1680 5/1/2013 5.8 1.4 37 1099 5/122014 63 0.2 - - NAV30 4;52006 5.9 6.2 139 79 9425,2006 5.0 6.5 366 - 3/202007 6.3 - 139 74 9/132007 3.8 0.1 160 390 41212009 4.3 0.8 28 1300 4i5iWI0 5.4 2.5 51 1094 U24=2012 6.8 2.5 40 371 42/2012 4.2 5.3 14 372 S'WO 3 5.7 3.2 122 551 5/112014 5.7 0.9 - - NR'32 4142006 62 - 99 42 3r202007 6.3 40 47 4'29 ZOOS 4.3 83 46 4,23/2009 5.8 - 179 51 4'5)2010 5.7 5.0 216 57 5/21?011 4.2 - 164 4/42012 8.6 0.7 -184 4s 511.:2013 5-8 0.8 258 48 5 13.2014 5.0 1.2 - - - NI 33 4i42006 6.8 - 105 59 3/20/2007 9.0 -23 263 4/292008 7.1 - -31 71 4/232009 63 5.6 142 64 4'5/2010 10.5 6.7 49 106 1/24,2011 5.1 4.0 210 80 7.22:2011 5.4 0.0 174 74 10!62011 6.9 - 150 76 1'24,12012 7.1 5.2 124 82 4/3 2012 10.3 4.0 -110 106 7/252012 6.4 5.2 150 84 11!8Will 6.2 4.3 163 82 2/72013 5.9 4.3 105 - 4,302013 63 4.2 222 93 12/3,2013 - - 110 86 3 V2014 - 6.4 111 27 5/13/2014 7.8 3.8 - Page 6 of 7 Table 3 - Groundwater Physical Parameters B,'E Aerospace Facility, NCDO60302577 1455 Fairchild Road, Winston-Salem. North Carolina Ply!' [D Sample PH DO ORP Conductivity Date m my us RR"-3 4`6;2006 6.5 5.9 174 62 3 20,2007 6A - 142 56 5'I'200S 6.2 4.5 -53 57 4232009 6.2 3.0 127 660 452010 6A 4S 225 66 8'2i2011 4.7 0.0 152 64 4i12012 7.1 4.9 102 61 5/1;2013 5.9 4.9 214 61 5;13,1014 5.6 2.5 - - .A-t 12112,2006 &0 - -120 - B-2 3,20r2007 6.3 - -t08 401 C-2 9252006 5.4 13 111 - C-3 4`52010 6.2 0.0 -81 108 M62011 5.9 - -30 2282 412012 6.6 1.5 -293 777 C-4 4/30/2008 5.9 - -178 292 C'-5 4/4r2012 6.0 1.3 -40 500 C-8 462010 5.7 1.1 35 243 C-9 4.1412012 5.2 0.4 -317 3660 C-11 725.2006 6.8 - 111 82 12.I22006 4.9 - 39 27_ V20i2007 5.6 - -7 484 D-1 3120/2007 6.5 -150 210 D-2 10/6,2011 5.9 - -99 2470 D-3 10`6r2011 5.9 - 113 206 D-5 7,152006 6.5 - 34 177 3.20.2007 5.9 - -3 850 4302008 5.7 -35 731 D-7 7`252006 7.3 - 106 83 12'122006 6.1 - -125 - 3/202007 6.7 - -183 253 4/302045 5.7 0.2 -153 1027 1 V 18.2008 5.9 0.2 -108 1978 IOi6201I 5.7 - 16 - 4142012 6.2 0.9 -85 992 D-11 4/5/2010 6.9 161 121 F-2 12/13/2006 4.6 - 145 360 3 202W 5.7 - 120 379 F-3 12/132006 4.3 - 219 237 F4 4•512012 8.1 2.3 -120 270 AC-2 30-0OM 6.7 - -15 130 AC-3 3:'202007 5.7 - 95 54 Page 7 of 7 APPENDIX I LABORATORY REPORTS AND CHAIN OF CUSTODY RECORDS ��keAnalyficale www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 May 21, 2014 Rob Workman CRB 5000 Old Buncombe Road Suite 2 Greenville, SC 29617 RE: Project: 414-02 Pace Project No.: 92201204 Dear Rob Workman: Enclosed are the analytical results for sample(s) received by the laboratory on May 14, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, ly, ow" " q"l - k-e,� Angela Baioni angela.baioni@pacelabs.com Project Manager Enclosures cc: Braden Rambo, CRB REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 84 -��6kwcal 0 m*w pacefaDs.com Pace Analytical Services, Inc. 9800 Kinoey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: 414-02 Pace Project No.: 92201204 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certircation #: 37706 Kentucky UST Certification M 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 84 liceAnalyticale ~pacelabs.cw Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: 414-02 92201204 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92201204001 MW-1 EPA 8260 MCK 63 PASI-C 92201204002 MW-10D EPA 8260 MCK 63 PASI-C 92201204003 MW-28 EPA 8260 MCK 63 PASI-C 92201204004 MW-9 EPA 8260 MCK 63 PASI-C 92201204006 MW-11 EPA 8260 MCK 63 PASI-C 92201204006 MW-5 EPA 8260 MCK 63 PASI-C 92201204007 MW-17D EPA 8260 MCK 63 PASI-C 92201204008 MWA8 EPA 8260 MCK 63 PASI-C 92201204009 MW-20 EPA 8260 MCK 63 PASI-C 92201204010 MW-19 EPA 8260 MCK 63 PASI-C 92201204011 MW-6 EPA 8260 MCK 63 PASI-C 92201204012 MW-30 EPA 8260 MCK 63 PASI-C 92201204013 MW-12D EPA 8260 MCK 63 PASI-C 92201204014 MW-26D EPA 8260 MCK 63 PASI-C 92201204015 MW-29 EPA 8260 MCK 63 PASI-C 92201204016 MW-13 EPA 8260 MCK 63 PASI-C 92201204017 MW-27D EPA 8260 MCK 63 PASI-C 92201204018 MW-27DD EPA 8260 MCK 63 PASI-C 92201204019 MW-33 EPA 8260 MCK 63 PASI-C 92201204020 MW-32 EPA 8260 MCK 63 PASI-C 92201204021 MW-23 EPA 8260 MCK 63 PASI-C 92201204022 MWA6 EPA 8260 MCK 63 PASI-C 92201204023 MW-21D EPA 8260 MCK 63 PASI-C 92201204024 MW-24 EPA 8260 MCK 63 PASI-C 92201204026 MW-14D EPA 8260 MCK 63 PASI-C 92201204026 MW-3 EPA 8260 MCK 63 PASI-C 92201204027 MW-25 EPA 8260 MCK 63 PASI-C 92201204028 MW-15 EPA 8260 MCK 63 PASI-C 92201204029 MW-8 EPA 8260 MCK 63 PASI-C 92201204030 MW-7 EPA 8260 MCK 63 PASI-C 92201204031 RW-3 EPA 8260 MCK 63 PASI-C 92201204032 MW-22D EPA 8260 MCK 63 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 84 Ike Analical ~pacelebxcom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-1 Lab ID: 92201204001 Collected: 05/12/14 11:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA8260 Acetone ND ug/L 25.0 1 05/17/14 04:57 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 04:57 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 04:57 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 04:57 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 04:57 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 04:57 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 04:57 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 04:57 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 04:57 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 04:57 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 04:57 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 04:57 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 04:57 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 04:57 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 04:57 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 04:57 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 04:57 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 04:57 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 04:57 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 04:57 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 04:57 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 04:57 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 04:57 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 04:57 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 04:57 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 04:57 75-35-4 cis- 1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 04:57 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 04:57 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 04:57 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 04:57 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 04:57 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 04:57 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 04:57 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 04:57 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 04:57 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 04:57 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 04:57 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 04:57 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 04:57 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 04:57 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 04:57 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 04:57 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 04:57 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 04:57 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 04:57 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 04:57 79-34-5 Tetrachloroethene 6.3 ug/L 1.0 1 05/17/14 04:57 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 84 lice Analical www.pacelabs.cw Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-1 Lab ID: 92201204001 Collected: 05/12/14 11:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/17/14 04:57 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/1711404:57 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 04:57 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 04:57 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 04:57 79-00-5 Trichloroethene ND ug/L 1.0 1 05/17/14 04:57 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/17/14 04:57 75-69-4 1,2,3-Tdchloropropane ND ug/L 1.0 1 05/1711404:57 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 04:57 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/17/14 04:57 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/17/14 04:57 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 04:57 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 04:57 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/17/14 04:57 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 05/17/14 04:57 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 05/17/14 04:57 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 84 Ike Analical i W*w.pacelabs.m" Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 414-02 Pace Project No.: 92201204 Sample: MW-10D ANALYTICAL RESULTS Lab ID: 92201204002 Collected: 05/12/14 11:10 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 05:13 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 05:13 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 05:13 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 05:13 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 05:13 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 05:13 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 05:13 74-83-9 2-Butanone (MEK) ND ugfL 5.0 1 05/17/14 05:13 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 05:13 56-23-5 Chlorobenzene ND ug1L 1.0 1 05/17/14 05:13 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 05:13 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 05:13 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 05:13 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 05:13 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 05:13 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 05:13 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 05:13 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 05:13 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 05:13 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 05:13 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 05:13 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/1405-13 106-46-7 D ichlorodifluorc methane ND ug1L 1.0 1 05/17/1405-13 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 05:13 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 05:13 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 05:13 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 05:13 156-59-2 trans- 1,2-Dich lo roethene ND ug/L 1.0 1 05/17/14 05:13 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 05:13 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/1405-13 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 05:13 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 05:13 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 05:13 10061-01-5 trans- 1,3-Dichloroprope ne ND ug/L 1.0 1 05/17/14 05:13 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 05:13 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 05:13 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 05:13 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 05:13 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 05:13 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 05:13 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 05:13 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 05:13 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 05:13 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 05:13 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 05:13 630-20-6 1,12,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 05:13 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/17/14 05:13 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 84 lkeAnalyfical* www.pace4abs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-10D Lab ID: 92201204002 Collected: 05/12/14 11:10 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene NO ug/L 1.0 1 05/17/14 05:13 108-88-3 1,2,3-Trichlorobenzene NO ug/L 1.0 1 05/17/14 05:13 87-61-6 1,2,4-Trichlorobenzene NO ug/L 1.0 1 05/17/14 05:13 120-82-1 1,1,1-Trichloroethane NO ug/L 1.0 1 05/17/14 05:13 71-55-6 1,1,2-Trichloroethane NO ug/L 1.0 1 05/17/14 05:13 79-00-5 Trichloroethene NO ug/L 1.0 1 05/17/14 05:13 79-01-6 Trichlorofluoromethane NO ug/L 1.0 1 05/17/14 05:13 75-69-4 1,2,3-Trichloropropane NO ug/L 1.0 1 05/17/14 05:13 96-18-4 Vinyl acetate NO ug/L 2.0 1 05/17/14 05:13 108-05-4 Vinyl chloride NO ug/L 1.0 1 05/17/14 05:13 75-01-4 Xylene (Total) NO ug/L 2.0 1 05/17/14 05:13 1330-20-7 m&p-Xylene NO ug/L 2.0 1 05/17/14 05:13 179601-23-1 o-Xylene NO ug/L 1.0 1 05/17/14 05:13 95-47-6 Surrogates 4-Bromofluorobenzene (S) 30 % 70-130 1 05/17/14 05:13 460-00-4 1,2-Dichloroethane-d4 (S) 29 % 70-130 1 05/17/14 05:13 17060-07-0 Toluene-d8 (S) 88 % 70-130 1 05/17/14 05:13 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 84 Ike Analical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-28 Lab ID: 92201204003 Collected: 05/12/14 11:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 05:29 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 05:29 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 05:29 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 05:29 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 05:29 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 05:29 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 05:29 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 05:29 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 05:29 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 05:29 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 05:29 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 05:29 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 05:29 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 05:29 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 05:29 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 05:29 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 05:29 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 05:29 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 05:29 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 05:29 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 05:29 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 05:29 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 05:29 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 05:29 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 05:29 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 05:29 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 05:29 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 05:29 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 05:29 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 05:29 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 05:29 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 05:29 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 05:29 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 05:29 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 05:29 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 05:29 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 05:29 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 05:29 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 05:29 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 05:29 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 05:29 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 05:29 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 05:29 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 05:29 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 05:29 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 05:29 79-34-5 Tetrachloroethene 8.5 ug/L 1.0 1 05/17/14 05:29 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 84 ?1�tlWnalyfical-' www.pece/abs.uom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-28 Lab ID: 92201204003 Collected: 05/12/14 11:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/17/14 05:29 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/17/14 05:29 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 05:29 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 05:29 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 05:29 79-00-5 Trichloroethene 2.1 ug/L 1.0 1 05/17/14 05:29 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/17/14 05:29 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/17/14 05:29 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 05:29 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/17/14 05:29 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/17/14 05:29 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 05:29 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 05:29 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/17/14 05:29 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 05/17/14 05:29 17060-07-0 Toluene-d8 (S) 95 % 70-130 1 05/17/14 05:29 2037-26-5 Date: 05/21/2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 84 aceAnalytical wwwpacelebs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-9 Lab ID: 92201204004 Collected: 05/12/14 11:40 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 05:46 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 05:46 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 05:46 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 05:46 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 05:46 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 05:46 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 05:46 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 05:46 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 05:46 56-23-5 Chiorobenzene ND ug/L 1.0 1 05/17/14 05:46 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 05:46 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 05:46 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 05:46 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 05:46 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 05:46 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 05:46 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 05:46 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 05:46 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 05:46 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 05:46 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 05:46 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 05:46 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 05:46 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 05:46 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 05:46 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 05:46 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 05:46 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 05:46 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 05:46 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 05:46 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 05:46 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 05:46 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 05:46 10061-01-5 trans- 1,3-Dichloroprope ne ND ug/L 1.0 1 05/17/14 05:46 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 05:46 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 05:46 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 05:46 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 05:46 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 05:46 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 05:46 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 05:46 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 05:46 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 05:46 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 05:46 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 05:46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 05:46 79-34-5 Tetra chloroethene ND ug/L 1.0 1 05/17/14 05:46 127-18-4 REPORT OF LABORATORY ANALYSIS TN5 report shall not be reproduced, except in full, Date: 05/21/2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 84 aceAnalytical www. pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-9 Lab ID: 92201204004 Collected: 05/12/14 11:40 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/17/14 05:46 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/17/14 05:46 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 05:46 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 05:46 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 05:46 79-00-5 Trichloroethene ND ug/L 1.0 1 05/17/14 05:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/17/14 05:46 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/17/14 05:46 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 05:46 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/17/14 05:46 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/17/14 05:46 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 05:46 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 05:46 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/17/14 05:46 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 05/17/14 05:46 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 05/17/14 05:46 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 84 lkeAnalyfical" Nww.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-11 Lab ID: 92201204005 Collected: 05/12/14 11:50 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 79.0 ug/L 25.0 1 05/17/14 06:02 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 06:02 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 06:02 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 06:02 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 06:02 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 06:02 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 06:02 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 06:02 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 06:02 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 06:02 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 06:02 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 06:02 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 06:02 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 06:02 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 06:02 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 06:02 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 06:02 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/17/14 06:02 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 06:02 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:02 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:02 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:02 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 06:02 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 06:02 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 06:02 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 06:02 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 06:02 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 06:02 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 06:02 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 06:02 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 06:02 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 06:02 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 06:02 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 06:02 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 06:02 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 06:02 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 06:02 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 06:02 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 06:02 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 06:02 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 06:02 108-10-1 Methyl-tert-butyl ether ND uglL 1.0 1 05/17/14 06:02 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 06:02 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 06:02 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 06:02 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 06:02 79-34-5 Tetra ch loroethene ND ug/L 1.0 1 05/17/14 06:02 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 84 ��acbeAnalXicale www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-11 Lab ID: 92201244.005 Collected: 05/12/14 11:50 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21/201402:51 PM Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 100 % 91 % 96 % 1.0 1 05/17/14 06:02 108-88-3 1.0 1 05/17/14 06:02 87-61-6 1.0 1 05/17/14 06:02 120-82-1 1.0 1 05/17/14 06:02 71-55-6 1.0 1 05/17/14 06:02 79-00-5 1.0 1 05/17/14 06:02 79-01-6 1.0 1 05/17/14 06:02 75-69-4 1.0 1 05/17/14 06:02 96-18-4 2.0 1 05/17/14 06:02 108-05-4 1.0 1 05/17/14 06:02 75-01-4 2.0 1 05/17/14 06:02 1330-20-7 2.0 1 05/17/14 06:02 179601-23-1 1.0 1 05/17/14 06:02 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 05/17/14 06:02 460-00-4 05/17/14 06:02 17060-07-0 05/17/14 06:02 2037-26-5 Page 13 of 84 ��keAnalXicals www.pacelabs.mm Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-5 Lab ID: 92201204006 Collected: 05/12/14 12:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 06:18 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 06:18 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 06:18 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 06:18 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 06:18 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 06:18 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 06:18 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 06:18 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 06:18 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 06:18 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 06:18 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 06:18 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 06:18 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 06:18 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 06:18 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 06:18 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 06:18 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/17/14 06:18 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 06:18 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:18 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:18 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:18 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 06:18 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 06:18 75-34-3 12-Dichloroethane ND ug/L 1.0 1 05/17/14 06:18 107-06-2 1, 1 -Dichloroethene ND ug/L 1.0 1 05/17/14 06:18 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 06:18 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 06:18 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 06:18 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 06:18 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 06:18 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/1711406:18 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 06:18 10061-01-5 trans-1,3-Dichloroprope ne ND ug/L 1.0 1 05/17/14 06:18 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 06:18 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 06:18 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 06:18 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 06:18 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 06:18 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 06:18 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 06:18 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 06:18 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 06:18 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 06:18 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/1711406:18 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05117/1406:18 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/17/14 06:18 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 84 4ce Anal ical wwwpacelabacom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-5 Lab ID: 92201204006 Collected: 05/12/14 12:00 Received: 05/14/14 09:45 Matrix: Water Parameters 8260 MSV Low Level Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluorometha ne 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-c14 (S) Toluene-d8 (S) Date: 05/21 /2014 02:51 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ug/L 1.0 1 05/17/14 06:18 108-88-3 ND ug/L 1.0 1 05/17/14 06:18 87-61-6 ND ug/L 1.0 1 05/17/14 06:18 120-82-1 ND ug/L 1.0 1 05/17/14 06:18 71-55-6 ND ug/L 1.0 1 05/17/14 06:18 79-00-5 ND ug/L 1.0 1 05/17/14 06:18 79-01-6 ND ug/L 1.0 1 05/17/14 06:18 75-69-4 ND ug/L 1.0 1 05/17/14 06:18 96-18-4 ND ug/L 2.0 1 05/17/14 06:18 108-05-4 ND ug/L 1.0 1 05/17/14 06:18 75-01-4 ND ug/L 2.0 1 05/17/14 06:18 1330-20-7 ND ug/L 2.0 1 05/17/14 06:18 179601-23-1 ND ug/L 1.0 1 05/17/14 06:18 95-47-6 101 % 70-130 1 05/17/14 06:18 460-00-4 89 % 70-130 1 05/17/14 06:18 17060-07-0 96 % 70-130 1 05/17/14 06:18 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 15 of 84 4eAnalyfical www.pacslabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-17D Lab ID: 92201204007 Collected: 05/12/14 13:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 06:34 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 06:34 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 06:34 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 06:34 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 06:34 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 06:34 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 06:34 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 06:34 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 06:34 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 06:34 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 06:34 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 06:34 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 06:34 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 06:34 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 06:34 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 06:34 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 06:34 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 06:34 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 06:34 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:34 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:34 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:34 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 06:34 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 06:34 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 06:34 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 06:34 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 06:34 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 06:34 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 06:34 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 06:34 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 06:34 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 06:34 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 06:34 10061-01-5 trans- 1,3-Dichloroprope ne ND ug/L 1.0 1 05/17/14 06:34 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 06:34 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 06:34 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 06:34 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 06:34 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 06:34 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 06:34 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 06:34 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 06:34 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 06:34 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 06:34 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 06:34 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 06:34 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/17/14 06:34 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 84 aceAnal ical www.pacefabs com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-17D Lab ID: 92201204007 Collected: 05/12/14 13:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/17/14 06:34 108-88-3 1,2,3-Tdchlorobenzene ND ug/L 1.0 1 05/17/14 06:34 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 06:34 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 06:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 06:34 79-00-5 Trichloroethene ND ug/L 1.0 1 05/17/14 06:34 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/17/14 06:34 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/17/14 06:34 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 06:34 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/17/14 06:34 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/17/14 06:34 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 06:34 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 06:34 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/17/14 06:34 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 05/17/14 06:34 17060-07-0 Toluene-d8 (S) 95 % 70-130 1 05/17/14 06:34 2037-26-5 Date: 05/21/2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 17 of 84 labeAnalytical wwwpacelabscom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-18 Lab ID: 92201204008 Collected: 05/12/14 13:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 06:51 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 06:51 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 06:51 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 06:51 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 06:51 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 06:51 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 06:51 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 06:51 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 06:51 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 06:51 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 06:51 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 06:51 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 06:51 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 06:51 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 06:51 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 06:51 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 06:51 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 06:51 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 06:51 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:51 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:51 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 06:51 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 06:51 75-71-8 1,1-Dichloroethane 10.3 ug/L 1.0 1 05/17/14 06:51 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 06:51 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 06:51 75-35-4 cis-1,2-Dichloroethene 12.9 ug/L 1.0 1 05/17/14 06:51 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 06:51 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 06:51 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 06:51 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 06:51 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 06:51 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 06:51 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 06:51 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 06:51 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 06:51 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 06:51 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 06:51 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 06:51 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 06:51 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 06:51 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 06:51 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 06:51 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 06:51 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 06:51 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 06:51 79-34-5 Tetrachloroethene 197 ug/L 1.0 1 05/17/14 06:51 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 84 ��keAnalyfical wwwpacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-18 Lab ID: 92201 204008 Collected: 05/12/14 13:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/17/14 06:51 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/17/14 06:51 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 06:51 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 06:51 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 06:51 79-00-5 Trichloroethene 10.2 ug/L 1.0 1 05/17/14 06:51 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/17/14 06:51 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/17/14 06:51 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 06:51 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/17/14 06:51 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/17/14 06:51 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 06:51 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 06:51 95-47-6 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 05/17/14 06:51 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 05/17/14 06:51 17060-07-0 Toluene-d8(S) 94 % 70-130 1 05/17/14 06:51 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 84 acekial ical wwx pacNabs.=n Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-20 Lab ID: 92201204009 Collected: 05/12/14 14:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 07:07 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 07:07 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 07:07 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 07:07 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 07:07 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 07:07 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 07:07 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 07:07 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 07:07 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 07:07 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 07:07 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 07:07 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 07:07 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 07:07 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 07:07 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 07:07 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 07:07 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 07:07 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 07:07 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:07 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:07 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:07 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 07:07 75-71-8 1,1-Dichloroethane 1.2 ug/L 1.0 1 05/17/14 07:07 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 07:07 107-06-2 1,1-Dichloroethene 15.1 ug/L 1.0 1 05/17/14 07:07 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 07:07 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 07:07 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 07:07 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 07:07 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 07:07 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 07:07 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 07:07 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 07:07 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 07:07 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 07:07 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 07:07 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 07:07 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 07:07 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 07:07 75-09-2 4-Methyl-2-pentanone (MIRK) ND ug/L 5.0 1 05/17/14 07:07 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 07:07 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 07:07 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 07:07 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 07:07 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 07:07 79-34-5 Tetrachloroethene 55.7 ug/L 1.0 1 05/17/14 07:07 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 84 IkMnalyfical' www.pacelabs.cam Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-20 Lab ID: 92201204009 Collected: 05/12/14 14:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA8260 Toluene ND ug/L 1.0 1 05/17/14 07:07 108-88-3 1,2,3-Tdchlorobenzene ND ug/L 1.0 1 05/17/14 07:07 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 07:07 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 07:07 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 07:07 79-00-5 Trichloroethene 2.9 ug/L 1.0 1 05/17/14 07:07 79-01-6 Trichlorofluoromethane 2.1 ug/L 1.0 1 05/17/14 07:07 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/17/14 07:07 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 07:07 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/17/14 07:07 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/17/14 07:07 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 07:07 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 07:07 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/17/14 07:07 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 05/17/14 07:07 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 05/17/14 07:07 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 84 aceAnal ical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-19 Lab ID: 92201204010 Collected: 05/12/14 14:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 07:23 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 07:23 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 07:23 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 07:23 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 07:23 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 07:23 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 07:23 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 07:23 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 07:23 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 07:23 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 07:23 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 07:23 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 07:23 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 07:23 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 07:23 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 07:23 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 07:23 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 07:23 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 07:23 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:23 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:23 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:23 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 07:23 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 07:23 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 07:23 107-06-2 1,1-Dichloroethene 8.4 ug/L 1.0 1 05/17/14 07:23 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 07:23 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 07:23 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 07:23 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 07:23 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 07:23 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 07:23 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 07:23 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 07:23 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 07:23 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 07:23 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 07:23 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 07:23 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 07:23 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 07:23 75-09-2 4-Methyl-2-pentanone (MIRK) ND ug/L 5.0 1 05/17/14 07:23 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 07:23 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 07:23 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 07:23 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05117/1407:23 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 07:23 79-34-5 Tetrachloroethene 31.7 ug/L 1.0 1 05/17/14 07:23 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 84 _ Ike Analical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-19 Lab ID: 92201204010 Collected: 05/12/14 14:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA8260 Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluorometha ne 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21/2014 02:51 PM ND ug/L 1.0 1 05/17/14 07:23 108-88-3 ND ug/L 1.0 1 05/17/14 07:23 87-61-6 ND ug/L 1.0 1 05/17/14 07:23 120-82-1 ND ug/L 1.0 1 05/17/14 07:23 71-55-6 ND ug/L 1.0 1 05/17/14 07:23 79-00-5 ND ug/L 1.0 1 05/17/14 07:23 79-01-6 ND ug/L 1.0 1 05/17/14 07:23 75-69-4 ND ug/L 1.0 1 05/17/14 07:23 96-18-4 ND ug/L 2.0 1 05/17/14 07:23 108-05-4 ND ug/L 1.0 1 05/17/14 07:23 75-01-4 ND ug/L 2.0 1 05/17/14 07:23 1330-20-7 ND ug/L 2.0 1 05/17/14 07:23 179601-23-1 ND ug/L 1.0 1 05/17/14 07:23 95-47-6 100 % 70-130 1 05/17/14 07:23 460-00-4 94 % 70-130 1 05/17/14 07:23 17060-07-0 95 % 70-130 1 05/17/14 07:23 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 23 of 84 Ike Analical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-6 Lab ID: 92201204011 Collected: 05/12/14 15:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 07:39 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 07:39 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 07:39 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 07:39 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 07:39 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 07:39 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 07:39 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 07:39 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 07:39 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 07:39 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 07:39 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 07:39 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 07:39 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 07:39 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 07:39 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 07:39 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 07:39 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/17/14 07:39 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 07:39 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:39 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:39 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:39 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 07:39 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 07:39 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 07:39 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 07:39 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 07:39 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 07:39 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 07:39 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 07:39 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 07:39 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 07:39 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 07:39 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 07:39 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 07:39 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 07:39 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 07:39 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 07:39 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 07:39 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 07:39 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 07:39 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 07:39 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 07:39 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 07:39 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 07:39 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 07:39 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/17/14 07:39 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 84 labeAnalytical www.pacews.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-6 Lab ID: 92201204011 Collected: 05/12/14 15:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/17/14 07:39 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/17/14 07:39 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 07:39 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 07:39 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 07:39 79-00-5 Trichloroethene ND ug/L 1.0 1 05/17/14 07:39 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/17/14 07:39 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/17/14 07:39 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 07:39 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/17/14 07:39 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/17/14 07:39 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 07:39 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 07:39 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/17/14 07:39 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 05/17/14 07:39 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 05/17/14 07:39 2037-26-5 Date: 05/21/201402:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 25 of 84 lkeAnalytical' *"..pacblabs.mn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW30 Lab ID: 92201204012 Collected: 05/12/14 15:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 187 ug/L 25.0 1 05/17/14 07:56 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 07:56 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 07:56 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 07:56 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 07:56 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 07:56 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 07:56 74-83-9 2-Butanone (MEK) 11.8 ug/L 5.0 1 05/17/14 07:56 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 07:56 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 07:56 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 07:56 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 07:56 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 07:56 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 07:56 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 07:56 106-43-4 1,2-Dibromo-3-ch[oropropane ND ug/L 5.0 1 05/17/14 07:56 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 07:56 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/17/14 07:56 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 07:56 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:56 95-50-1 15-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:56 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 07:56 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 07:56 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 07:56 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 07:56 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 07:56 75-35-4 cis-1,2-Dichloroethene 52.5 ug/L 1.0 1 05/17/14 07:56 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 07:56 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 07:56 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 07:56 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 07:56 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 07:56 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 07:56 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 07:56 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 07:56 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 07:56 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 07:56 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 07:56 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 07:56 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 07:56 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 07:56 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 07:56 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 07:56 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 07:56 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 07:56 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 07:56 79-34-5 Tetrachloroethene 7.4 ug/L 1.0 1 05/17/14 07:56 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 26 of 84 Ike Analical www.pacWabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-30 Lab ID: 92201204012 Collected: 05/12/14 15:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA8260 Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofl uorometha ne 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21 /2014 02:51 PM ND ug/L 1.0 1 05/17/14 07:56 108-88-3 ND ug/L 1.0 1 05/17/14 07:56 87-61-6 ND ug/L 1.0 1 05/17/14 07:56 120-82-1 ND ug/L 1.0 1 05/17/14 07:56 71-55-6 ND ug/L 1.0 1 05/17/14 07:56 79-00-5 ND ug/L 1.0 1 05/17/14 07:56 79-01-6 ND ug/L 1.0 1 05/17/14 07:56 75-69-4 ND ug/L 1.0 1 05/17/14 07:56 96-18-4 ND ug/L 2.0 1 05/17/14 07:56 108-05-4 ND ug/L 1.0 1 05/17/14 07:56 75-01-4 ND ug/L 2.0 1 05/17/14 07:56 1330-20-7 ND ug/L 2.0 1 05/17/14 07:56 179601-23-1 ND ug/L 1.0 1 05/17/14 07:56 95-47-6 98 % 70-130 1 05/17/14 07:56 460-00-4 91 % 70-130 1 05/17/14 07:56 17060-07-0 96 % 70-130 1 05/17/14 07:56 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 27 of 84 Ike Analytical www.pacelabs.wm Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-12D Lab ID: 92201204013 Collected: 05/12/14 16:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 08:12 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 08:12 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 08:12 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 08:12 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 08:12 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 08:12 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 08:12 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 08:12 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 08:12 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 08:12 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 08:12 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 08:12 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 08:12 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 08:12 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 08:12 10643-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 08:12 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 08:12 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/17/14 08:12 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 08:12 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:12 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:12 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:12 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 08:12 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/1711408:12 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 08:12 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 08:12 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 08:12 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 08:12 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 08:12 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 08:12 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 08:12 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 08:12 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 08:12 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 08:12 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 08:12 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 08:12 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 08:12 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 08:12 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 08:12 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 08:12 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 08:12 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 08:12 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 08:12 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 08:12 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 08:12 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 08:12 79-34-5 Tetrachloroethene 1.1 ug/L 1.0 1 05/17/14 08:12 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 28 of 64 lkeAnalyficalo www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 414-02 Pace Project No.: 92201204 Sample: MW-12D Parameters 8260 MSV Low Level Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluorometha ne 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21/201402:51 PM ANALYTICAL RESULTS Lab ID: 92201204013 Collected: 05/12/14 16:30 Received: 05/14/14 09:45 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Analytical Method: EPA 8260 ND ug/L 1.0 1 05/17/14 08:12 108-88-3 ND ug/L 1.0 1 05/17/14 08:12 87-61-6 ND ug/L 1.0 1 05/17/14 08:12 120-82-1 ND ug/L 1.0 1 05/17/14 08:12 71-55-6 ND ug/L 1.0 1 05/17/14 08:12 79-00-5 ND ug/L 1.0 1 05/17/14 08:12 79-01-6 ND ug/L 1.0 1 05/17/14 08:12 75-69-4 ND ug/L 1.0 1 05/17/14 08:12 96-18-4 . ND ug/L 2.0 1 05/17/14 08:12 108-05-4 ND ug/L 1.0 1 05/17/14 08:12 75-01-4 ND ug/L 2.0 1 05/17/14 08:12 1330-20-7 ND ug/L 2.0 1 05/17/14 08:12 179601-23-1 ND ug/L 1.0 1 05/17/14 08:12 95-47-6 99 % 70-130 1 05/17/14 08:12 460-00-4 94 % 70-130 1 05/17/14 08:12 17060-07-0 96 % 70-130 1 05/17/14 08:12 2037-26-5 Qual REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 29 of 84 Ike Analical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvdle, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-26D Parameters Lab ID: 92201204014 Collected: 05/12/14 16:30 Results Units Report Limit DF Received: 05/14/14 09:45 Matrix: Water Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/17/14 08:28 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 08:28 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 08:28 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 08:28 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 08:28 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 08:28 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 08:28 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/17/14 08:28 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 08:28 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 08:28 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 08:28 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 08:28 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 08:28 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 08:28 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 08:28 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 08:28 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/17/14 08:28 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/17/14 08:28 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 08:28 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:28 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:28 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:28 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/17/14 08:28 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 08:28 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 08:28 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 08:28 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 08:28 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 08:28 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 08:28 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 08:28 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 08:28 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 08:28 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/17/14 08:28 10061-01-5 trans- 1,3-Dichloroprope ne ND ug/L 1.0 1 05/17/14 08:28 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 08:28 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 08:28 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 08:28 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 08:28 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/17/14 08:28 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 08:28 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/17/14 08:28 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 08:28 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 08:28 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 08:28 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 08:28 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 08:28 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/17/14 08:28 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 30 of 84 Ike Analical ~pacelabs.wn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-26D Lab ID: 92201204014 Collected: 05/12/14 16:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/17/14 08:28 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/17/14 08:28 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 08:28 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 08:28 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 08:28 79-00-5 Trichloroethene ND ug/L 1.0 1 05/17/14 08:28 79-01-6 TrichIorofluoromethane ND ug/L 1.0 1 05/17/14 08:28 75-694 1,2,3-Trichloropropane ND ug/L 1.0 1 05117/1408:28 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 08:28 108-054 Vinyl chloride ND ug/L 1.0 1 05/17/14 08:28 75-014 Xylene (Total) ND ug/L 2.0 1 05/17/14 08:28 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 08:28 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 08:28 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 05/17/14 08:28 460-004 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 05/17/14 08:28 17060-07-0 Toluene-d8 (S) 95 % 70-130 1 05/17/14 08:28 2037-26-5 Date: 05/21/2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without tha written consent of Pace Analytical Services, Inc.. Page 31 of 84 lkeAnalytical" wwwpacetabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-29 Lab ID: 92201204015 Collected: 05/12/14 17:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 103 ug/L 25.0 1 05/17/14 08:44 67-64-1 Benzene ND ug/L 1.0 1 05/17/14 08:44 71-43-2 Bromobenzene ND ug/L 1.0 1 05/17/14 08:44 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/17/14 08:44 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/17/14 08:44 75-27-4 Bromoform ND ug/L 1.0 1 05/17/14 08:44 75-25-2 Bromomethane ND ug/L 2.0 1 05/17/14 08:44 74-83-9 2-Butanone (MEK) 8.5 ug/L 5.0 1 05/17/14 08:44 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/17/14 08:44 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/17/14 08:44 108-90-7 Chloroethane ND ug/L 1.0 1 05/17/14 08:44 75-00-3 Chloroform ND ug/L 1.0 1 05/17/14 08:44 67-66-3 Chloromethane ND ug/L 1.0 1 05/17/14 08:44 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/17/14 08:44 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/17/14 08:44 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/17/14 08:44 96-12-8 Dibromochlorom ethane ND ug/L 1.0 1 05/17/14 08:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/17/14 08:44 106-93-4 Dibromomethane ND ug/L 1.0 1 05/17/14 08:44 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:44 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:44 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/17/14 08:44 106-46-7 Dichlorodifluorom ethane ND ug/L 1.0 1 05/17/14 08:44 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/17/14 08:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/17/14 08:44 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/17/14 08:44 75-35-4 cis-1,2-Dichloroethene 24.4 ug/L 1.0 1 05/17/14 08:44 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/17/14 08:44 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/17/14 08:44 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/17/14 08:44 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/17/14 08:44 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/17/14 08:44 563-58-6 cis- 1,3-Dichloroprop ene ND ug/L 1.0 1 05/17/14 08:44 10061-01-5 trans-1,3-Dichloroprope ne ND ug/L 1.0 1 05/17/14 08:44 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/17/14 08:44 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/17/14 08:44 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/17/14 08:44 87-68-3 2-Hexanone ND ug/L 5.0 1 05/17/14 08:44 591-78-6 p4sopropyltoluene ND ug/L 1.0 1 05/17/14 08:44 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/17/14 08:44 75-09-2 4-Methyl-2-pentanone (MIBK) 13.2 ug/L 5.0 1 05/17/14 08:44 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/17/14 08:44 1634-04-4 Naphthalene ND ug/L 1.0 1 05/17/14 08:44 91-20-3 Styrene ND ug/L 1.0 1 05/17/14 08:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 08:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/17/14 08:44 79-34-5 Tetrachloroethene 1.9 ug/L 1.0 1 05/17/14 08:44 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 32 of 84 lkeAnalyfical' wwwpacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-29 Lab ID: 92201204015 Collected: 05/12/14 17:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/17/14 08:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/17/14 08:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/17/14 08:44 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/17/14 08:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/17/14 08:44 79-00-5 Trichloroethene ND ug/L 1.0 1 05/17/14 08:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/17/14 08:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/17/14 08:44 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/17/14 08:44 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/17/14 08:44 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/17/14 08:44 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/17/14 08:44 179601-23-1 o-Xylene ND ug/L 1.0 1 05/17/14 08:44 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/17/14 08:44 460-00-4 1,2-Dichloroethane-d4(S) 92 % 70-130 1 05/17/14 08:44 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 05/17/14 08:44 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 33 of 84 la6eAnalyfical' www pacela mwm Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-13 Lab ID: 92201204016 Collected: 05/13/14 08:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 18:03 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 18:03 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 18:03 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 18:03 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 18:03 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 18:03 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 18:03 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 18:03 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 18:03 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 18:03 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 18:03 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 18:03 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 18:03 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 18:03 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 18:03 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 18:03 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 18:03 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 18:03 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 18:03 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:03 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:03 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/1811418:03 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 18:03 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 18:03 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 18:03 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 18:03 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 18:03 156-59-2 trans- 1,2-Dich loroethene ND ug/L 1.0 1 05/18/14 18:03 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 18:03 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 18:03 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 18:03 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 18:03 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 18:03 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 18:03 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 18:03 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 18:03 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 18:03 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 18:03 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 18:03 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 18:03 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 18:03 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 18:03 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 18:03 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 18:03 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 18:03 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 18:03 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/18/14 18:03 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 34 of 84 ��keAnalyficale www.paceiabs.corn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-13 Lab ID: 92201204016 Collected: 05/13/14 08:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 18:03 108-88-3 1,2,3-Tdchlorobenzene ND ug/L 1.0 1 05/1811418:03 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 18:03 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 18:03 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 18:03 79-00-5 Trichloroethene ND ug/L 1.0 1 05/18/14 18:03 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 18:03 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/1811418:03 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 18:03 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/18/14 18:03 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 18:03 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 18:03 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 18:03 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 05/18/14 18:03 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 05/18/14 18:03 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 05/18/14 18:03 2037-26-5 Date: 05/21/2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 35 of 84 ��keAnalyfical www,pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-27D Lab ID: 92201204017 Collected: 05/13/14 09:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 18:19 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 18:19 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 18:19 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 18:19 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 18:19 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 18:19 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 18:19 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 18:19 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 18:19 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 18:19 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 18:19 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 18:19 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 18:19 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 18:19 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 18:19 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 18:19 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 18:19 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 18:19 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 18:19 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:19 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:19 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:19 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 18:19 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 18:19 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 18:19 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 18:19 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 18:19 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 18:19 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 18:19 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 18:19 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 18:19 594-20-7 1, 1 -Dichloropropene ND ug/L 1.0 1 05/1811418:19 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 18:19 10061-01-5 trans- l,3-Dichloropropene ND ug/L 1.0 1 05/18/14 18:19 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 18:19 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 18:19 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/1811418:19 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 18:19 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 18:19 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 18:19 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 18:19 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 18:19 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 18:19 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 18:19 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 18:19 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 18:19 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/18/14 18:19 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 36 of 84 �keAnalytical www.pacelaftmn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-27D Lab ID: 92201204017 Collected: 05/13/14 09:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 18:19 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/18/14 18:19 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 18:19 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 18:19 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 18:19 79-00-5 Trichloroethene ND ug/L 1.0 1 05/18/14 18:19 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 18:19 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 18:19 96-184 Vinyl acetate ND ug/L 2.0 1 05/18/14 18:19 108-054 Vinyl chloride ND ug/L 1.0 1 05/18/14 18:19 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 18:19 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 18:19 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 18:19 95-47-6 Surrogates 4-B romofluo robe nzene (S) 97 % 70-130 1 05/18/14 18:19 460-004 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 05/18/14 18:19 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 05/18/14 18:19 2037-26-5 Date: 05/21/2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 37 of 84 lkeAnalyfical' www pacelabsx= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-270D Lab ID: 92201204018 Collected: 05/13/14 08:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO ug/L 25.0 1 05/18/14 18:36 67-64-1 Benzene NO ug/L 1.0 1 05/1811418:36 71-43-2 Bromobenzene NO ug/L 1.0 1 05/1811418:36 108-86-1 Bromochloromethane NO ug/L 1.0 1 05/1811418:36 74-97-5 Bromodichloromethane NO ug/L 1.0 1 05/18/14 18:36 75-27-4 Bromoform NO ug/L 1.0 1 05/18/14 18:36 75-25-2 Bromomethane NO ug/L 2.0 1 05/18/14 18:36 74-83-9 2-Butanone (MEK) NO ug/L 5.0 1 05/18/14 18:36 78-93-3 Carbon tetrachloride NO ug/L 1.0 1 05/18/14 18:36 56-23-5 Chlorobenzene NO ug/L 1.0 1 05/1811418:36 108-90-7 Chloroethane NO ug/L 1.0 1 05/18/14 18:36 75-00-3 Chloroform NO ug/L 1.0 1 05/18/14 18:36 67-66-3 Chloromethane NO ug/L 1.0 1 05/18/14 18:36 74-87-3 2-Chlorotoluene NO ug/L 1.0 1 05/18/14 18:36 95-49-8 4-Chlorotoluene NO ug/L 1.0 1 05/18/14 18:36 106-43-4 1,2-Dibromo-3-chloropropane NO ug/L 5.0 1 05/18/14 18:36 96-12-8 Dibromochloromethane NO ug/L 1.0 1 05/18/14 18:36 124-48-1 1,2-Dibromoethane (EDB) NO ug/L 1.0 1 05/18/14 18:36 106-934 Dibromomethane NO ug/L 1.0 1 05/18/14 18:36 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:36 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 05/18/14 18:36 541-73-1 1,4-Dichlorobenzene NO ug/L 1.0 1 05/18/14 18:36 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 05/18/14 18:36 75-71-8 1,1-Dichloroethane NO ug/L 1.0 1 05/18/14 18:36 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 18:36 107-06-2 1,1-Dichloroethene NO ug/L 1.0 1 05/18/14 18:36 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 18:36 156-59-2 trans- 1,2-Dichloroethene NO ug/L 1.0 1 05/18/14 18:36 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 05/18/14 18:36 78-87-5 1,3-Dichloropropane NO ug/L 1.0 1 05/1811418:36 142-28-9 2,2-Dichloropropane NO ug/L 1.0 1 05/18/14 18:36 594-20-7 1, 1 -Dichloropropene ND ug/L 1.0 1 05/18/14 18:36 563-58-6 cis- 1,3-Dichloropropene NO ug/L 1.0 1 05/18/14 18:36 10061-01-5 trans-1,3-Dichloropropene NO ug/L 1.0 1 05/18/14 18:36 10061-02-6 Diisopropyl ether NO ug/L 1.0 1 05/18/14 18:36 108-20-3 Ethylbenzene NO ug/L 1.0 1 05/18/14 18:36 100-414 Hexachloro-1,3-butadiene NO ug/L 1.0 1 05/18/14 18:36 87-68-3 2-Hexanone NO ug/L 5.0 1 05/18/14 18:36 591-78-6 p-Isopropyltoluene NO ug/L 1.0 1 05/18/14 18:36 99-87-6 Methylene Chloride NO ug/L 2.0 1 05/18/14 18:36 75-09-2 4-Methyl-2-pentanone (MIBK) NO ug/L 5.0 1 05/18/14 18:36 108-10-1 Methyl-tert-butyl ether NO ug/L 1.0 1 05/18/14 18:36 1634-04-4 Naphthalene NO ug/L 1.0 1 05/18/14 18:36 91-20-3 Styrene NO ug/L 1.0 1 05/18/14 18:36 10042-5 1,1,1,2-Tetrachloroethane NO ug/L 1.0 1 05/18/14 18:36 630-20-6 1,1,2,2-Tetrachloroethane NO ug/L 1.0 1 05/18/14 18:36 79-34-5 Tetrachloroethene NO ug/L 1.0 1 05/18/14 18:36 127-184 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 38 of 84 ��keAnalyfical" www.pacelabs.cw Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-27DD Lab ID: 92201204018 Collected: 05/13/14 08:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 18:36 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05118/1418:36 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 18:36 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05118/1418:36 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05118/1418:36 79-00-5 Trichloroethene ND ug/L 1.0 1 05/18/14 18:36 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 18:36 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 18:36 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 18:36 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/18/14 18:36 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 18:36 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05118/1418:36 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 18:36 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 05/18/14 18:36 460-00-4 1,2-Dichloroethane-d4(S) 91 % 70-130 1 05/18/14 18:36 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 05/18/14 18:36 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 39 of 84 aceAnal�/tical J www.pacelabs.cmrr Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-33 Lab ID: 92201204019 Collected: 05/13/14 09:15 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 18:52 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 18:52 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 18:52 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 18:52 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 18:52 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 18:52 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 18:52 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 18:52 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 18:52 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 18:52 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 18:52 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 18:52 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 18:52 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 18:52 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 18:52 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 18:52 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 18:52 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 18:52 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 18:52 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:52 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:52 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 18:52 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 18:52 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 18:52 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 18:52 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 18:52 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 18:52 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 18:52 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 18:52 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 18:52 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 18:52 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 18:52 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 18:52 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 18:52 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 18:52 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 18:52 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 18:52 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 18:52 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 18:52 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 18:52 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 18:52 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 18:52 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 18:52 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 18:52 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 18:52 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 18:52 79-34-5 Tetra chlo roethene 4.1 ug/L 1.0 1 05/18/14 18:52 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 40 of 84 ��keAnalytical' www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-33 Lab ID: 92201204019 Collected: 05/13/14 09:15 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluorometha ne 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xyfene (Total) m&p-Xyfene o-Xyfene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21/2014 02:51 PM Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 97 % 92 % 97 % 1.0 1 05/18/14 18:52 108-88-3 1.0 1 05/1811418:52 87-61-6 1.0 1 05/18/14 18:52 120-82-1 1.0 1 05/18/14 18:52 71-55-6 1.0 1 05/18/14 18:52 79-00-5 1.0 1 05/18/14 18:52 79-01-6 1.0 1 05/18/14 18:52 75-69-4 1.0 1 05/1811418:52 96-18-4 2.0 1 05/18/14 18:52 108-05-4 1.0 1 05/1811418:52 75-01-4 2.0 1 05/18/14 18:52 1330-20-7 2.0 1 05/18/14 18:52 179601-23-1 1.0 1 05/18/14 18:52 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 05/18/14 18:52 460-00-4 05/18/14 18:52 17060-07-0 05/1811418:52 2037-26-5 Page 41 of 84 ��keAnalyfical www pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-32 Lab ID: 92201204020 Collected: 05/13/14 10:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 19:08 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 19:08 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 19:08 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 19:08 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 19:08 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 19:08 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 19:08 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 19:08 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 19:08 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 19:08 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 19:08 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 19:08 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 19:08 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 19:08 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 19:08 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 19:08 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 19:08 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 19:08 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 19:08 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:08 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:08 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:08 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 19:08 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 19:08 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 19:08 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 19:08 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 19:08 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 19:08 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 19:08 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 19:08 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 19:08 594-20-7 1, 1 -Dichloropropene ND ug/L 1.0 1 05/18/14 19:08 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 19:08 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 19:08 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 19:08 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 19:08 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 19:08 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 19:08 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 19:08 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 19:08 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 19:08 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 19:08 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 19:08 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 19:08 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 19:08 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 19:08 79-34-5 Tetrachloroethene 12.3 ug/L 1.0 1 05/18/14 19:08 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 42 of 84 aceAnalyfical www.pacelabs.rom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-32 Lab ID: 92201204020 Collected: 05/13/14 10:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05116/1419:08 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/1811419:08 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/1811419:08 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 19:08 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 19:08 79-00-5 Trichloroethene 1.0 ug/L 1.0 1 05/18/14 19:08 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 19:08 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 19:08 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 19:08 108-054 Vinyl chloride ND ug/L 1.0 1 05/18/14 19:08 75-014 Xylene (Total) ND ug/L 2.0 1 05/18/14 19:08 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 19:08 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 19:08 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/18/14 19:08 460-00-4 1,2-Dichloroethane-d4(S) 92 % 70-130 1 05/18/14 19:08 17060-07-0 Toluene-d8(S) 99 % 70-130 1 05/18/14 19:08 2037-26-5 Date: 05/21/201402:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 43 of 84 ��keAnalyfical' *".pacelabs.wm Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-23 Lab ID: 92201204021 Collected: 05/13/14 10:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 409 ug/L 62.5 2.5 05/20/14 10:41 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 19:25 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 19:25 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 19:25 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 19:25 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 19:25 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 19:25 74-83-9 2-Butanone (MEK) 281 ug/L 5.0 1 05/18/14 19:25 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 19:25 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 19:25 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 19:25 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 19:25 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 19:25 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 19:25 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 19:25 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 19:25 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 19:25 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 19:25 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 19:25 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:25 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:25 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:25 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 19:25 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 19:25 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 19:25 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 19:25 75-35-4 cis-1,2-Dichloroethene 66.9 ug/L 1.0 1 05/18/14 19:25 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 19:25 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 19:25 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 19:25 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 19:25 594-20-7 1, 1 -Dichloropropene ND ug/L 1.0 1 05/18/14 19:25 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 19:25 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 19:25 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 19:25 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 19:25 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 19:25 87-68-3 2-Hexanone 252 ug/L 5.0 1 05/18/14 19:25 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 19:25 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 19:25 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 19:25 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 19:25 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 19:25 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 19:25 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 19:25 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 19:25 79-34-5 Tetrachloroethene 8.0 ug/L 1.0 1 05/18/14 19:25 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without ;he written consent of Pace Analytical Services, Inc.. Page 44 of 84 ;1!�46ftlyfical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-23 Lab ID: 92201204021 Collected: 05/13/14 10:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluorometha ne 1,2,3-Trich loropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21/201402:51 PM Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 94 % 91 % 95 % 1.0 1 05/18/14 19:25 108-88-3 1.0 1 05/18/14 19:25 87-61-6 1.0 1 05/18/14 19:25 120-82-1 1.0 1 05/18/14 19:25 71-55-6 1.0 1 05/18/14 19:25 79-00-5 1.0 1 05/18/14 19:25 79-01-6 1.0 1 05/18/14 19:25 75-69-4 1.0 1 05/18/14 19:25 96-18-4 2.0 1 05/18/14 19:25 108-05-4 1.0 1 05/18/14 19:25 75-01-4 2.0 1 05/18/14 19:25 1330-20-7 2.0 1 05/18/14 19:25 179601-23-1 1.0 1 05/18/14 19:25 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 05/18/14 19:25 460-004 05/18/14 19:25 17060-07-0 05/18/14 19:25 2037-26-5 Page 45 of 84 Ike Analical *"..pacelabs.mn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-16 Lab ID: 92201204022 Collected: 05/13/14 10:40 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 42.5 ug/L 25.0 1 05/18/14 19:41 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 19:41 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 19:41 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 19:41 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 19:41 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 19:41 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 19:41 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 19:41 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 19:41 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 19:41 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 19:41 75-00-3 Chloroform 1.4 ug/L 1.0 1 05/18/14 19:41 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 19:41 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 19:41 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 19:41 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 19:41 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 19:41 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 19:41 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 19:41 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:41 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:41 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:41 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 19:41 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 19:41 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 19:41 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 19:41 75-35-4 cis-1,2-Dichloroethene 13.1 ug/L 1.0 1 05/18/14 19:41 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 19:41 156 60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 19:41 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 19:41 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 19:41 594-20-7 1, 1 -Dichloropropene ND ug/L 1.0 1 05/18/14 19:41 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 19:41 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 19:41 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 19:41 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 19:41 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 19:41 87-68-3 2-Hexanone 19.0 ug/L 5.0 1 05/18/14 19:41 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 19:41 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 19:41 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 19:41 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 19:41 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 19:41 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 19:41 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 19:41 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 19:41 79-34-5 Tetrachlorcethene 83.4 ug/L 1.0 1 05/18/14 19:41 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 46 of 84 aceAnalytical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-16 Lab ID: 92201204022 Collected: 05/13/14 10:40 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Toluene 1,2,3-Tdchlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichlorcethane 1,1,2-Trichlorcethane Trichloroethene Trichlorofluorometha ne 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21/201402:51 PM Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 3.6 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 96 % 91 % 98 % 1.0 1 05/18/14 19:41 108-88-3 1.0 1 05/18/14 19:41 87-61-6 1.0 1 05/18/14 19:41 120-82-1 1.0 1 05/18/14 19:41 71-55-6 1.0 1 05/18/14 19:41 79-00-5 1.0 1 05/18/14 19:41 79-01-6 1.0 1 05/18/14 19:41 75-69-4 1.0 1 05/18/14 19:41 96-18-4 2.0 1 05/18/14 19:41 108-05-4 1.0 1 05/18/14 19:41 75-01-4 2.0 1 05/18/14 19:41 1330-20-7 2.0 1 05/18/14 19:41 179601-23-1 1.0 1 05/18/14 19:41 95-47-6 70-130 1 05/18/14 19:41 460-00-4 70-130 1 05/18/14 19:41 17060-07-0 70-130 1 05/18/14 19:41 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 47 of 84 ��a�eAnalyfical" ~..pacNabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-21D Lab ID: 92201204023 Collected: 05/13/14 11:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 19:58 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 19:58 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 19:58 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 19:58 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 19:58 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 19:58 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 19:58 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 19:58 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 19:58 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 19:58 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 19:58 75-00-3 Chloroform 4.5 ug/L 1.0 1 05/18/14 19:58 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 19:58 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 19:58 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 19:58 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 19:58 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 19:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 19:58 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 19:58 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:58 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:58 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 19:58 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 19:58 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 19:58 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 19:58 107-06-2 1,1-Dichloroethene 1.5 ug/L 1.0 1 05/18/14 19:58 75-35-4 cis- 1,2-Dichloroethene 73.4 ug/L 1.0 1 05/18/14 19:58 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 19:58 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 19:58 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 19:58 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 19:58 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 19:58 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 19:58 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 19:58 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 19:58 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 19:58 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 19:58 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 19:58 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 19:58 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 19:58 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 19:58 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 19:58 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 19:58 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 19:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 19:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 19:58 79-34-5 Tetrachloroethene 631 ug/L 10.0 10 05/19/1412:39 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 48 of 84 ��a6eAnalyfical' www.pacelabs corn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-21D Lab ID: 92201204023 Collected: 05/13/1411:00 Received: 05/14/1409:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 19:58 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/18/14 19:58 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/1811419:58 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 19:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 19:58 79-00-5 Trichloroethene 20.4 ug/L 1.0 1 05/18/14 19:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 19:58 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 19:58 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 19:58 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/18/14 19:58 75-014 Xylene (Total) ND ug/L 2.0 1 05/18/14 19:58 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 19:58 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 19:58 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/18/14 19:58 460-004 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 05/18/14 19:58 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 05/18/14 19:58 2037-26-5 Date: 05/21/2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 49 of 84 lkeAnalytical* www.paceiabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-24 Lab ID: 92201204024 Collected: 05/13/14 11:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 20:14 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 20:14 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 20:14 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 20:14 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 20:14 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 20:14 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 20:14 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 20:14 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 20:14 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 20:14 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 20:14 75-00-3 Chloroform 1.0 ug/L 1.0 1 05/18/14 20:14 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 20:14 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 20:14 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 20:14 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 20:14 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 20:14 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/18/14 20:14 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 20:14 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:14 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:14 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:14 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 20:14 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 20:14 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 20:14 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 20:14 75-35-4 cis-1,2-Dichloroethene 15.4 ug/L 1.0 1 05/18/14 20:14 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 20:14 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 20:14 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 20:14 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 20:14 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 20:14 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 20:14 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 20:14 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 20:14 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 20:14 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 20:14 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 20:14 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 20:14 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 20:14 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 20:14 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 20:14 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 20:14 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 20:14 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 20:14 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 20:14 79-34-5 Tetrachloroethene 111 ug/L 1.0 1 05/18/14 20:14 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 50 of 84 �ke Affll kal www.paL*abs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-24 Lab ID: 92201204024 Collected: 05/13/14 11:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 20:14 108-88-3 1,2,3-Tdchlorobenzene ND ug/L 1.0 1 05/18/14 20:14 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 20:14 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 20:14 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 20:14 79-00-5 Trichloroethene 19.2 ug/L 1.0 1 05/18/14 20:14 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 20:14 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 20:14 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 20:14 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/18/14 20:14 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 20:14 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 20:14 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 20:14 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 05/18/14 20:14 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 05/18/14 20:14 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 05/18/14 20:14 2037-26-5 Date: 05/21 /2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 51 of 84 I&Analyfical' ' www.paoelabscrom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-14D Lab ID: 92201204025 Collected: 05/13/14 11:45 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 20:31 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 20:31 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 20:31 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 20:31 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 20:31 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 20:31 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 20:31 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 20:31 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 20:31 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 20:31 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 20:31 75-00-3 Chloroform 4.7 ug/L 1.0 1 05/18/14 20:31 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 20:31 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 20:31 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 20:31 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 20:31 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 20:31 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 20:31 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 20:31 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:31 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:31 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:31 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 20:31 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 20:31 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 20:31 107-06-2 1,1-Dichloroethene 3.9 ug/L 1.0 1 05/18/14 20:31 75-35-4 cis-1,2-Dichloroethene 98.0 ug/L 1.0 1 05/18/14 20:31 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 20:31 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 20:31 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 20:31 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 20:31 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 20:31 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 20:31 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 20:31 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 20:31 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 20:31 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 20:31 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 20:31 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 20:31 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 20:31 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 20:31 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 20:31 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 20:31 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 20:31 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 20:31 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 20:31 79-34-5 Tetrachloroethene 624 ug/L 10.0 10 05/19/14 12:55 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 52 of 84 1�xa4eAnalyticale wwwpacelabxcw Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-14D lab ID: 92201204025 Collected: 05/13/14 11:45 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 20:31 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/18/14 20:31 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 20:31 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 20:31 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 20:31 79-00-5 Trichloroethene 28.0 ug/L 1.0 1 05/18/14 20:31 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 20:31 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 20:31 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 20:31 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/18/14 20:31 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 20:31 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 20:31 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 20:31 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 05/18/14 20:31 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 05/18/14 20:31 17060-07-0 Toluene -dB (S) 96 % 70-130 1 05/18/14 20:31 2037-26-5 Date: 05/21 /2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 53 of 84 keAnal kal www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-3 Lab ID: 92201204026 Collected: 05/13/14 12:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 20:47 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 20:47 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 20:47 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 20:47 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 20:47 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 20:47 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 20:47 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 20:47 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 20:47 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 20:47 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 20:47 75-00-3 Chloroform 2.0 ug/L 1.0 1 05/18/14 20:47 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 20:47 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 20:47 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 20:47 106-434 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 20:47 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 20:47 12448-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 05/18/14 20:47 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 20:47 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:47 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:47 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 20:47 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 20:47 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 20:47 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 20:47 107-06-2 1,1-Dichloroethene 16.7 ug/L 1.0 1 05/18/14 20:47 75-354 cis-1,2-Dichloroethene 29.0 ug/L 1.0 1 05/18/14 20:47 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 20:47 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 20:47 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 20:47 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 20:47 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 20:47 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 20:47 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 20:47 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 20:47 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 20:47 100-414 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 20:47 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 20:47 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 20:47 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 20:47 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 20:47 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 20:47 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 20:47 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 20:47 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 20:47 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 20:47 79-34-5 Tetrachloroethene 397 ug/L 10.0 10 05/19/14 13:12 127-184 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 54 of 84 Ike Analical wwwpacelebs.aom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-3 Lab ID: 92201204026 Collected: 05/13/14 12:00 Received: 05/14/14 09:45 Matrix: Water Parameters 8260 MSV Low Level Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trich loroethane 1,1,2-Trichloroethane Trichloroethene T ri ch lorofluo rometh a ne 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21/201402:51 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ug/L 1.0 1 05/18/14 20:47 108-88-3 ND ug/L 1.0 1 05/18/14 20:47 87-61-6 ND ug/L 1.0 1 05/18/14 20:47 120-82-1 ND ug/L 1.0 1 05/18/14 20:47 71-55-6 ND ug/L 1.0 1 05/18/14 20:47 79-00-5 41.8 ug/L 1.0 1 05/18/14 20:47 79-01-6 ND ug/L 1.0 1 05/18/14 20:47 75-69-4 ND ug/L 1.0 1 05/18/14 20:47 96-18-4 ND ug/L 2.0 1 05/18/14 20:47 108-05-4 ND ug/L 1.0 1 05/18/14 20:47 75-01-4 ND ug/L 2.0 1 05/18/14 20:47 1330-20-7 ND ug/L 2.0 1 05/18/14 20:47 179601-23-1 ND ug/L 1.0 1 05/18/14 20:47 95-47-6 98 % 70-130 1 05/18/14 20:47 460-00-4 91 % 70-130 1 05/18/14 20:47 17060-07-0 96 % 70-130 1 05/18/14 20:47 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 55 of 84 Ike Analical wwwpacelabscom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-25 Lab ID: 92201204027 Collected: 05/13/14 12:15 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 21:04 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 21:04 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 21:04 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 21:04 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 21:04 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 21:04 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 21:04 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 21:04 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 21:04 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 21:04 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 21:04 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 21:04 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 21:04 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 21:04 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 21:04 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 21:04 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 21:04 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 21:04 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 21:04 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:04 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:04 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:04 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 21:04 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 21:04 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 21:04 107-06-2 1,1-Dichloroethene 7.4 ug/L 1.0 1 05/18/14 21:04 75-35-4 cis-1,2-Dichloroethene 332 ug/L 5.0 5 05/19/1413:28 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 21:04 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 21:04 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 21:04 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 21:04 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 21:04 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 21:04 10061-01-5 trans-1,3-Dichloroprope ne ND ug/L 1.0 1 05/18/14 21:04 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 21:04 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 21:04 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 21:04 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 21:04 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 21:04 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 21:04 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 21:04 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 21:04 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 21:04 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 21:04 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 21:04 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 21:04 79-34-5 Tetrachloroethene 25.9 ug/L 1.0 1 05/18/14 21:04 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 56 of 84 Ike Analical www.paceiabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-25 Lab ID: 92201204027 Collected: 05/13/14 12:15 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 21:04 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/18/14 21:04 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 21:04 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 21:04 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 21:04 79-00-5 Trichloroethene 17.8 ug/L 1.0 1 05/18/14 21:04 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 21:04 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 21:04 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 21:04 108-05-4 Vinyl chloride 1.8 ug/L 1.0 1 05/18/14 21:04 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 21:04 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 21:04 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 21:04 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/18/14 21:04 460-00-4 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 05/18/14 21:04 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 05/18/14 21:04 2037-26-5 Date: 05/21/2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 57 of 84 Ike Analical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-15 Lab ID: 92201204028 Collected: 05/13/14 13:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 21:20 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 21:20 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 21:20 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 21:20 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 21:20 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 21:20 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 21:20 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 21:20 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 21:20 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 21:20 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 21:20 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 21:20 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 21:20 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 21:20 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 21:20 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 21:20 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 21:20 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 21:20 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 21:20 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:20 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:20 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:20 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 21:20 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 21:20 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/1811421:20 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 21:20 75-35-4 cis-1,2-Dichloroethene 2.7 ug/L 1.0 1 05/18/14 21:20 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 21:20 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 21:20 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 21:20 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 21:20 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 21:20 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 21:20 10061-01-5 trans- l,3-Dichloropropene ND ug/L 1.0 1 05/18/14 21:20 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 21:20 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 21:20 100-41-4 Hexachloro-1 ,3-butadiene ND ug/L 1.0 1 05/18/14 21:20 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 21:20 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 21:20 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 21:20 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 21:20 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 21:20 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 21:20 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 21:20 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 21:20 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 21:20 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/18/14 21:20 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 58 of 84 Ike Analical www pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-15 Lab ID: 92201204028 Collected: 05/13/14 13:00 Received: 05/14/14 09:45 Matrix: Water Parameters 8260 MSV Low Level Toluene 1,2,3-Tdchlorobenzene 1,2,4-Tdchlorobenzene 1,1,1-Trichloroetha ne 1,1,2-Trichloroethane Trichloroethene Trichlorofl uorometha ne 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4 -Bromof luoro benzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 05/21/201402:51 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ Analytical Method: EPA 8260 ND ug/L 1.0 1 05/18/14 21:20 108-88-3 ND ug/L 1.0 1 05/18/14 21:20 87-61-6 ND ug/L 1.0 1 05/18/14 21:20 120-82-1 ND ug/L 1.0 1 05/18/14 21:20 71-55-6 ND ug/L 1.0 1 05/18/14 21:20 79-00-5 ND ug/L 1.0 1 05/18/14 21:20 79-01-6 ND ug/L 1.0 1 05/18/14 21:20 75-69-4 ND ug/L 1.0 1 05/18/14 21:20 96-18-4 ND ug/L 2.0 1 05/18/14 21:20 108-05-4 ND ug/L 1.0 1 05/18/14 21:20 75-01-4 ND ug/L 2.0 1 05/18/14 21:20 1330-20-7 ND ug/L 2.0 1 05/18/14 21:20 179601-23-1 ND ug/L 1.0 1 05/18/14 21:20 95-47-6 98 % 70-130 1 05/18/14 21:20 460-00-4 92 % 70-130 1 05/18/14 21:20 17060-07-0 98 % 70-130 1 05/18/14 21:20 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 59 of 84 Ike Analical wwwpacelabs.00m Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-8 Lab ID: 92201204029 Collected: 05/13/14 14:15 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 21:37 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 21:37 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 21:37 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 21:37 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 21:37 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 21:37 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 21:37 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 21:37 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 21:37 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 21:37 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 21:37 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 21:37 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 21:37 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 21:37 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 21:37 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 21:37 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 21:37 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 21:37 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 21:37 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:37 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:37 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:37 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 21:37 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 21:37 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 21:37 107-06-2 1, 1 -Dichloroethene ND ug/L 1.0 1 05/18/14 21:37 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 21:37 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 21:37 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 21:37 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/1811421:37 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 21:37 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 21:37 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 21:37 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 21:37 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 21:37 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 21:37 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 21:37 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 21:37 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 21:37 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 21:37 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 21:37 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 21:37 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 21:37 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 21:37 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 21:37 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 21:37 79-34-5 Tetra ch loroethene 4.0 ug/L 1.0 1 05/18/14 21:37 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 60 of 84 aceAnal ical WW%pacelabscom ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 r704)875-9092 RECEIVED/DENR/Ok , All Water Quality R,- rin%.Y`-1}fin Sample: MW-8 Lab ID: 92201204029 Collected: 05/13/14 14:15 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 21:37 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/18/14 21:37 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 21:37 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 21:37 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 21:37 79-00-5 Trichloroethene ND ug/L 1.0 1 05/18/14 21:37 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 21:37 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 21:37 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 21:37 108-05-4 Vinyl chloride ND ug/L 1.0 1 05118J14 21:37 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 21:37 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 21:37 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 21:37 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/18/14 21:37 460-00-4 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 05/18/14 21:37 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 05/18/14 21:37 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 61 of 84 Ike Analical www.pacelabscw Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-7 Lab ID: 92201204030 Collected: 05/13/14 14:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 21:53 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 21:53 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 21:53 108-86-1 Bromoch lorom ethane ND ug/L 1.0 1 05/18/14 21:53 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 21:53 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 21:53 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 21:53 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 21:53 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 21:53 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 21:53 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 21:53 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 21:53 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 21:53 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 21:53 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 21:53 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/1811421:53 96-12-8 Dibromoch lorom ethane ND ug/L 1.0 1 05/18/14 21:53 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 21:53 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 21:53 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:53 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:53 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 21:53 106-46-7 Dichlorodifluoro methane ND ug/L 1.0 1 05/18/14 21:53 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 21:53 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 21:53 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 21:53 75-35-4 cis-1,2-Dichloroethene 3.2 ug/L 1.0 1 05/18/14 21:53 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 21:53 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 21:53 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 21:53 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 21:53 594-20-7 1, 1 -D ich lorop ropen e ND ug/L 1.0 1 05/18/14 21:53 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 21:53 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 21:53 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 21:53 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 21:53 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 21:53 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 21:53 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 21:53 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 21:53 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 05/18/14 21:53 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 21:53 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 21:53 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 21:53 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 21:53 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 21:53 79-34-5 Tetrachloroethene 4.1 ug/L 1.0 1 05/18/14 21:53 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 62 of 84 lkeAnalytical" www.pacNabscom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-7 Lab ID: 92201204030 Collected: 05/13/14 14:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 21:53 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/18/14 21:53 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 21:53 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 21:53 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 21:53 79-00-5 Trichloroethene 7.6 ug/L 1.0 1 05/18/14 21:53 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 21:53 75-694 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 21:53 96-184 Vinyl acetate ND ug/L 2.0 1 05/18/14 21:53 108-054 Vinyl chloride ND ug/L 1.0 1 05/18/14 21:53 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 21:53 1330-20-7 map-Xylene ND ug/L 2.0 1 05/18/14 21:53 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 21:53 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 05/18/14 21:53 460-004 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 05/18/14 21:53 17060-07-0 Toluene-d8(S) 98 % 70-130 1 05/18/14 21:53 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 63 of 84 lkeAnalyfical' www.pacelabs.corn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: RW-3 Lab ID: 92201204031 Collected: 05/13/14 15:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 05/18/14 22:10 67-64-1 Benzene ND ug/L 1.0 1 05/18/14 22:10 71-43-2 Bromobenzene ND ug/L 1.0 1 05/18/14 22:10 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 22:10 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 22:10 75-27-4 Bromoform ND ug/L 1.0 1 05/18/14 22:10 75-25-2 Bromomethane ND ug/L 2.0 1 05/18/14 22:10 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 22:10 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 05/18/14 22:10 56-23-5 Chlorobenzene ND ug/L 1.0 1 05/18/14 22:10 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 22:10 75-00-3 Chloroform ND ug/L 1.0 1 05/18/14 22:10 67-66-3 Chloromethane ND ug/L 1.0 1 05/18/14 22:10 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 05/18/14 22:10 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 05/18/14 22:10 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 05/18/14 22:10 96-12-8 Dibromochloromethane ND ug/L 1.0 1 05/18/14 22:10 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 05/18/14 22:10 106-93-4 Dibromomethane ND ug/L 1.0 1 05/18/14 22:10 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 05/18/14 22:10 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 05/18/14 22:10 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 22:10 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 05/18/14 22:10 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 22:10 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 22:10 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 22:10 75-35-4 cis- 1,2-Dichloroethene 1.8 ug/L 1.0 1 05/18/14 22:10 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 1 05/18/14 22:10 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 05/18/14 22:10 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 05/18/14 22:10 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 05/18/14 22:10 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 22:10 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 22:10 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 22:10 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 22:10 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 22:10 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 05/18/14 22:10 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 22:10 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 22:10 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 22:10 75-09-2 4-Methyl-2-pentanone (MIRK) ND ug/L 5.0 1 05/18/14 22:10 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 05/18/14 22:10 1634-04-4 Naphthalene ND ug/L 1.0 1 05/18/14 22:10 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 22:10 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 22:10 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 22:10 79-34-5 Tetrachloroethene 19.6 ug/L 1.0 1 05/18/14 22:10 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 64 of 84 lkeAnalytical' wwwpacela6scom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: RW-3 Lab ID: 92201204031 Collected: 05/13/14 15:00 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene NO ug/L 1.0 1 05/18/14 22:10 108-88-3 1,2,3-Tdchlorobenzene NO ug/L 1.0 1 05/18/14 22:10 87-61-6 1,2,4-Trichlorobenzene NO ug/L 1.0 1 05/18/14 22:10 120-82-1 1,1,1-Trichloroethane NO ug/L 1.0 1 05/18/14 22:10 71-55-6 1,1,2-Trichloroethane NO ug/L 1.0 1 05/18/14 22:10 79-00-5 Trichloroethene 1.9 ug/L 1.0 1 05/18/14 22:10 79-01-6 Trichlorofluoromethane NO ug/L 1.0 1 05/18/14 22:10 75-69-4 1,2,3-Trichloropropane NO ug/L 1.0 1 05/18/14 22:10 96-18-4 Vinyl acetate NO ug/L 2.0 1 05/18/14 22:10 108-05-4 Vinyl chloride NO ug/L 1.0 1 05/18/14 22:10 75-01-4 Xylene (Total) NO ug/L 2.0 1 05/18/14 22:10 1330-20-7 m&p-Xylene NO ug/L 2.0 1 05/18/14 22:10 179601-23-1 o-Xylene NO ug/L 1.0 1 05/18/14 22:10 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 05/18/14 22:10 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 05/18/14 22:10 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 05/18/14 22:10 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 65 of 84 lkeAnalyticalo www.pacelabs.mm Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-22D Lab ID: 92201204032 Collected: 05/13/14 16:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO ug/L 25.0 1 05/18/14 22:26 67-64-1 Benzene NO ug/L 1.0 1 05/18/14 22:26 71-43-2 Bromobenzene NO ug/L 1.0 1 05/18/14 22:26 108-86-1 Bromochloromethane ND ug/L 1.0 1 05/18/14 22:26 74-97-5 Bromodichloromethane ND ug/L 1.0 1 05/18/14 22:26 75-27-4 Bromoform NO ug/L 1.0 1 05/18/14 22:26 75-25-2 Bromomethane NO ug/L 2.0 1 05/18/14 22:26 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 05/18/14 22:26 78-93-3 Carbon tetrachloride NO ug/L 1.0 1 05/18/14 22:26 56-23-5 Chlorobenzene NO ug/L 1.0 1 05/18/14 22:26 108-90-7 Chloroethane ND ug/L 1.0 1 05/18/14 22:26 75-00-3 Chloroform NO ug/L 1.0 1 05/18/14 22:26 67-66-3 Chloromethane NO ug/L 1.0 1 05/18/14 22:26 74-87-3 2-Chlorotoluene NO ug/L 1.0 1 05/18/14 22:26 95-49-8 4-Chlorotoluene NO ug/L 1.0 1 05/18/14 22:26 106-43-4 1,2-Dibromo-3-chloropropane NO ug/L 5.0 1 05/18/14 22:26 96-12-8 Dibromochloromethane NO ug/L 1.0 1 05/18/14 22:26 124-48-1 1,2-Dibromoethane(EDB) NO ug/L 1.0 1 05/18/14 22:26 106-93-4 Dibromomethane NO ug/L 1.0 1 05/18/14 22:26 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 05/18/14 22:26 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 05118/1422:26 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 05/18/14 22:26 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 05/18/14 22:26 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 05/18/14 22:26 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 05/18/14 22:26 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 05/18/14 22:26 75-35-4 cis-1,2-Dichloroethene NO ug/L 1.0 1 05118/1422:26 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 05/18/14 22:26 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 05/18/14 22:26 78-87-5 1,3-Dichloropropane NO ug/L 1.0 1 05/18/14 22:26 142-28-9 2,2-Dichloropropane NO ug/L 1.0 1 05/18/14 22:26 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 05/18/14 22:26 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 05118/1422:26 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 05/18/14 22:26 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 05/18/14 22:26 108-20-3 Ethylbenzene ND ug/L 1.0 1 05/18/14 22:26 100-41-4 Hexachloro-1,3-butadiene NO ug/L 1.0 1 05/18/14 22:26 87-68-3 2-Hexanone ND ug/L 5.0 1 05/18/14 22:26 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 05/18/14 22:26 99-87-6 Methylene Chloride ND ug/L 2.0 1 05/18/14 22:26 75-09-2 4-Methyl-2-pentanone (MIBK) NO ug/L 5.0 1 05/18/14 22:26 108-10-1 Methyl-tert-butyl ether NO ug/L 1.0 1 05/18/14 22:26 1634-04-4 Naphthalene NO ug/L 1.0 1 05/18/14 22:26 91-20-3 Styrene ND ug/L 1.0 1 05/18/14 22:26 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 22:26 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 05/18/14 22:26 79-34-5 Tetrachloroethene ND ug/L 1.0 1 05/18/14 22:26 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 66 of 84 ,l�laeeAnalytical® wwwpacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 414-02 Pace Project No.: 92201204 Sample: MW-22D Lab ID: 92201204032 Collected: 05/13/14 16:30 Received: 05/14/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 05/18/14 22:26 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 05/18/14 22:26 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 05/18/14 22:26 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 05/18/14 22:26 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 05/18/14 22:26 79-00-5 Trichloroethene ND ug/L 1.0 1 05/18/14 22:26 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 05/18/14 22:26 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 05/18/14 22:26 96-18-4 Vinyl acetate ND ug/L 2.0 1 05/18/14 22:26 108-05-4 Vinyl chloride ND ug/L 1.0 1 05/18/14 22:26 75-01-4 Xylene (Total) ND ug/L 2.0 1 05/18/14 22:26 1330-20-7 m&p-Xylene ND ug/L 2.0 1 05/18/14 22:26 179601-23-1 o-Xylene ND ug/L 1.0 1 05/18/14 22:26 95.47-6 Surrogates 4-Bromofiuorobenzene (S) 98 % 70-130 1 05/18/14 22:26 460-00-4 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 05/18/14 22:26 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 05/18/14 22:26 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Qual Page 67 of 84 156eAnalytical www.pacelabs.c= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 QC Batch: MSV/26840 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92201204001, 92201204002, 92201204003, 92201204004, 92201204005, 92201204006, 92201204007, 92201204008,92201204009,92201204010,92201204011,92201204012,92201204013,92201204014, 92201204015 METHOD BLANK: 1200900 Matrix: Water Associated Lab Samples: 92201204001, 92201204002, 92201204003, 92201204004, 92201204005, 92201204006, 92201204007, 92201204008,92201204009,92201204010,92201204011,92201204012,92201204013,92201204014, 92201204015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1, 1, 1,2-Tetrachloroethane ug/L ND 1.0 05/17/14 03:20 1,1,1-Trichloroethane ug/L ND 1.0 05/17/14 03:20 1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/17/14 03:20 1,1,2-Trichooroethane ug/L ND 1.0 05/17/14 03:20 1,1-Dichloroethane ug/L ND 1.0 05/17/14 03:20 1,1-Dichloroethene ug/L ND 1.0 05/17/14 03:20 1,1-Dichloropropene ug/L ND 1.0 05/17/14 03:20 1,2,3-Tdchlorobenzene ug/L ND 1.0 05/17/14 03:20 1,2,3-Tdchloropropane ug/L ND 1.0 05/17/14 03:20 1,2,4-Trichoorobenzene ug/L ND 1.0 05/17/14 03:20 1,2-Dibromo-3-chloropropane ug/L ND 5.0 05/17/14 03:20 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/17/14 03:20 1,2-Dichlorobenzene ug/L ND 1.0 05/17/14 03:20 1,2-Dichloroethane ug/L ND 1.0 05/17/14 03:20 1,2-Dichloropropane ug/L ND 1.0 05/17/14 03:20 1,3-Dichlorobenzene ug/L ND 1.0 05/17/14 03:20 1,3-Dichloropropane ug/L ND 1.0 05/17/14 03:20 1,4-Dichlorobenzene ug/L ND 1.0 05/17/14 03:20 2,2-Dichloropropane ug/L ND 1.0 05/17/14 03:20 2-Butanone (MEK) ug/L ND 5.0 05/17/14 03:20 2-Chlorotoluene ug/L ND 1.0 05/17/14 03:20 2-Hexanone ug/L ND 5.0 05/17/14 03:20 4-Chlorotoluene ug/L ND 1.0 05/17/14 03:20 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 05/17/14 03:20 Acetone ug/L ND 25.0 05/17/14 03:20 Benzene ug/L ND 1.0 05/17/14 03:20 Bromobenzene ug/L ND 1.0 05/17/14 03:20 B romoch lo rom ethane ug/L ND 1.0 05/17/14 03:20 Bromodichloromethane ug/L ND 1.0 05/17/14 03:20 Bromoform ug/L ND 1.0 05/17/14 03:20 Bromomethane ug/L ND 2.0 05/17/14 03:20 Carbon tetrachloride ug/L ND 1.0 05/17/14 03:20 Chlorobenzene ug/L ND 1.0 05/17/14 03:20 Chloroethane ug/L ND 1.0 05/17/14 03:20 Chloroform ug/L ND 1.0 05/17/14 03:20 Chloromethane ug/L ND 1.0 05/17/14 03:20 cis-1,2-Dichloroethene ug/L ND 1.0 05/17/14 03:20 cis-1,3-Dichloropropene ug/L ND 1.0 05/17/14 03:20 Dibromochloromethane ug/L ND 1.0 05/17/14 03:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 68 of 84 ,�aceAnal ical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 METHOD BLANK: 1200900 Matrix: Water Associated Lab Samples: 92201204001, 92201204002, 92201204003, 92201204004, 92201204005, 92201204006, 92201204007, 92201204008,92201204009,92201204010,92201204011,92201204012,92201204013,92201204014, 92201204015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dibromomethane ug/L ND 1.0 05/17/14 03:20 Dichlorodifluoromethane ug/L ND 1.0 05/17/14 03:20 Diisopropyl ether ug/L ND 1.0 05/17/14 03:20 Ethylbenzene ug/L ND 1.0 05/17/14 03:20 Hexachloro-1,3-butadiene ug/L ND 1.0 05/17/14 03:20 m&p-Xylene ug/L ND 2.0 05/17/14 03:20 Methyl-tert-butyl ether ug/L ND 1.0 05/17/14 03:20 Methylene Chloride ug/L ND 2.0 05/17/14 03:20 Naphthalene ug/L ND 1.0 05/17/14 03:20 o-Xylene ug/L ND 1.0 05/17/14 03:20 p-Isopropyltoluene ug/L ND 1.0 05/17/14 03:20 Styrene ug/L ND 1.0 05/17/14 03:20 Tetra chloroethene ug/L ND 1.0 05/17/14 03:20 Toluene ug/L ND 1.0 05/17/14 03:20 trans-1,2-Dichloroethene ug/L ND 1.0 05/17/14 03:20 trans-1,3-Dichloropropene ug/L ND 1.0 05/17/14 03:20 Trichloroethene ug/L ND 1.0 05/17/14 03:20 Trichlorofluoromethane ug/L ND 1.0 05/17/14 03:20 Vinyl acetate ug/L ND 2.0 05/17/14 03:20 Vinyl chloride ug/L ND 1.0 05/17/14 03:20 Xylene (Total) ug/L ND 2.0 05/17/14 03:20 1,2-Dichloroethane-d4 (S) % 94 70-130 05/17/14 03:20 4-Bromofluorobenzene (S) % 101 70-130 05/17/14 03:20 Toluene-d8 (S) % 96 70-130 05/17/14 03:20 LABORATORY CONTROL SAMPLE: Parameter 1200901 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 47.0 94 70-130 1,1,1-Trichloroethane ug/L 50 44.1 88 70-130 1,1,2,2-Tetrachloroethane ug/L 50 49.1 98 70-130 1,1,2-Trichloroethane ug/L 50 52.4 105 70-130 1,1-Dichloroethane ug/L 50 44.7 89 70-130 1,1-Dichloroethene ug/L 50 41.6 83 70-132 1,1-Dichloropropene ug/L 50 49.6 99 70-130 1,2,3-Trichlorobenzene ug/L 50 53.9 108 70-135 1,2,3-Trichloropropane ug/L 50 48.8 98 70-130 1,2,4-Trichlorobenzene ug/L 50 55.1 110 70-134 1,2-Dibromo-3-chloropropane ug/L 50 41.6 83 70-130 1,2-Dibromoethane (EDB) ug/L 50 50.4 101 70-130 1,2-Dichlorobenzene ug/L 50 53.5 107 70-130 1,2-Dichloroethane ug/L 50 45.3 91 70-130 1,2-Dichloropropane ug/L 50 48.8 98 70-130 1,3-Dichlorobenzene ug/L 50 51.4 103 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 69 of 84 ,�aceAnal�/�'ical I J` www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 LABORATORY CONTROL SAMPLE: Parameter 1200901 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,3-Dichloropropane ug/L 50 50.6 101 70-130 1,4-Dichlorobenzene ug/L 50 50.8 102 70-130 2,2-Dichloropropane ug/L 50 38.8 78 58-145 2-Butanone (MEK) ug/L 100 73.9 74 70-145 2-Chlorotoluene ug/L 50 48.9 98 70-130 2-Hexanone ug/L 100 70.4 70 70-144 4-Chlorotoluene ug/L 50 46.8 94 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 71.2 71 70-140 Acetone ug/L 100 72.2 72 50-175 Benzene ug/L 50 54.8 110 70-130 Bromobenzene ug/L 50 47.8 96 70-130 Bromochloromethane ug/L 50 51.0 102 70-130 Bromodichloromethane ug/L 50 41.7 83 70-130 Bromoform ug/L 50 41.5 83 70-130 Bromomethane ug/L 50 28.4 57 54-130 Carbon tetrachloride ug/L 50 42.6 85 70-132 Chlorobenzene ug/L 50 50.4 101 70-130 Chloroethane ug/L 50 30.1 60 64-134 LO Chloroform ug/L 50 44.6 89 70-130 Chloromethane ug/L 50 32.2 64 64-130 cis-1,2-Dichloroethene ug/L 50 45.2 90 70-131 cis-1,3-Dichloropropene ug/L 50 47.3 95 70-130 Dibromochloromethane ug/L 50 42.3 85 70-130 Dibromomethane ug/L 50 53.6 107 70-131 Dichlorodifluoromethane ug/L 50 56.9 114 56-130 Diisopropyl ether ug/L 50 36.3 73 70-130 Ethylbenzene ug/L 50 48.3 97 70-130 Hexachloro-1,3-butadiene ug/L 50 50.8 102 70-130 m&p-Xylene ug/L 100 95.0 95 70-130 M ethyl -tert-butyl ether ug/L 50 38.0 76 70-130 Methylene Chloride ug/L 50 43.0 86 63-130 Naphthalene ug/L 50 52.9 106 70-138 o-Xylene ug/L 50 48.7 97 70-130 p-Isopropyltoluene ug/L 50 49.9 100 70-130 Styrene ug/L 50 51.6 103 70-130 Tetra ch loroethene ug/L 50 56.5 113 70-130 Toluene ug/L 50 52.4 105 70-130 trans-1,2-Dichloroethene ug/L 50 43.4 87 70-130 trans-1,3-Dichloropropene ug/L 50 44.1 88 70-132 Trichloroethene ug/L 50 55.6 111 70-130 Trichlorofluoromethane ug/L 50 43.9 88 62-133 Vinyl acetate ug/L 100 86.5 86 66-157 Vinyl chloride ug/L 50 51.2 102 69-130 Xylene (Total) ug/L 150 144 96 70-130 1,2-Dichloroethane-d4(S) % 92 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 98 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 70 of 84 Zee Analical www.pKWabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1201750 1201751 MS MSD 92201204004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1-Dichloroethene ug/L ND 50 50 51.3 49.6 103 99 70-166 3 Benzene ug/L ND 50 50 59.8 58.8 120 118 70-148 2 Chlorobenzene ug/L ND 50 50 53.6 53.7 107 107 70-146 0 Toluene ug/L ND 50 50 52.4 52.0 105 104 70-155 1 Trichloroethene ug/L ND 50 50 60.5 59.4 121 119 69-151 2 1,2-Dichloroethane-d4 (S) % 91 91 70-130 4-Bromofluorobenzene (S) % 98 97 70-130 Toluene-d8(S) % 97 98 70-130 Date: 05/21/2014 02:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 71 of 84 1� aeeAnal kal www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 QC Batch: MSV/26856 Analysis Method: EPA 8260 QC Batch Method: EPA8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92201204016, 92201204017, 92201204018, 92201204019, 92201204020, 92201204021, 92201204022, 92201204023,92201204024,92201204025,92201204026,92201204027,92201204028 METHOD BLANK: 1201768 Matrix: Water Associated Lab Samples: 92201204016, 92201204017, 92201204018, 92201204019, 92201204020, 92201204021, 92201204022, 92201204023,92201204024,92201204025,92201204026,92201204027,92201204028 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/18/14 15:34 1,1,1-Trichloroethane ug/L ND 1.0 05/18/14 15:34 1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/18/14 15:34 1,1,2-Trichloroethane ug/L ND 1.0 05/18/14 15:34 1,1-Dichloroethane ug/L ND 1.0 05/18/14 15:34 1,1-Dichloroethene ug/L ND 1.0 05/18/14 15:34 1,1-Dichloropropene ug/L ND 1.0 05/18/14 15:34 1,2,3-Trichlorobenzene ug/L ND 1.0 05/18/14 15:34 1,2,3-Tiichloropropane ug/L ND 1.0 05/18/14 15:34 1,2,4-Trichlorobenzene ug/L ND 1.0 05/18/14 15:34 1,2-Dibromo-3-chloropropane ug/L ND 5.0 05/18/14 15:34 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/18/14 15:34 1,2-Dichlorobenzene ug/L ND 1.0 05/18/14 15:34 1,2-Dichloroethane ug/L ND 1.0 05/18/14 15:34 1,2-Dichloropropane ug/L ND 1.0 05/18/14 15:34 15-Dichlorobenzene ug/L ND 1.0 05/18/14 15:34 1,3-Dichloropropane ug/L ND 1.0 05/18/14 15:34 1,4-Dichlorobenzene ug/L ND 1.0 05/18/14 15:34 2,2-Dichloropropane ug/L ND 1.0 05/18/14 15:34 2-Butanone (MEK) ug/L ND 5.0 05/18/14 15:34 2-Chlorotoluene ug/L ND 1.0 05/18/14 15:34 2-Hexanone ug/L ND 5.0 05/18/14 15:34 4-Chlorotoluene ug/L ND 1.0 05/18/14 15:34 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 05/18/14 15:34 Acetone ug/L ND 25.0 05/18/14 15:34 Benzene ug/L ND 1.0 05/18/14 15:34 Bromobenzene ug/L ND 1.0 05/18/14 15:34 Bromochloromethane ug/L ND 1.0 05/18/14 15:34 Bromodichloromethane ug/L ND 1.0 05/18/14 15:34 Bromoform ug/L ND 1.0 05/18/14 15:34 Bromomethane ug/L ND 2.0 05/18/14 15:34 Carbon tetrachloride ug/L ND 1.0 05/18/14 15:34 Chlorobenzene ug/L ND 1.0 05/18/14 15:34 Chloroethane ug/L ND 1.0 05/18/14 15:34 Chloroform ug/L ND 1.0 05/18/14 15:34 Chloromethane ug/L ND 1.0 05/18/14 15:34 cis-1,2-Dichloroethene ug/L ND 1.0 05/18/14 15:34 cis-1,3-Dichloropropene ug/L ND 1.0 05/18/14 15:34 Dibromochloromethane ug/L ND 1.0 05/18/14 15:34 Dibromomethane ug/L ND 1.0 05/18/14 15:34 Dichlorodifluoromethane ug/L ND 1.0 05/18/14 15:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 72 of 84 aceAnal ical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 METHOD BLANK: 1201768 Matrix: Water Associated Lab Samples: 92201204016, 92201204017, 92201204018, 92201204019, 92201204020, 92201204021, 92201204022, 92201204023,92201204024,92201204025,92201204026,92201204027,92201204028 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diisopropyl ether ug/L ND 1.0 05/18/14 15:34 Ethylbenzene ug/L ND 1.0 05/18/14 15:34 Hexachloro-1,3-butadiene ug/L ND 1.0 05/18/14 15:34 m&p-Xylene ug/L ND 2.0 05/18/14 15:34 Methyl-tert-butyl ether ug/L ND 1.0 05/18/14 15:34 Methylene Chloride ug/L ND 2.0 05/18/14 15:34 Naphthalene ug/L ND 1.0 05/18/14 15:34 o-Xylene ug/L ND 1.0 05/18/14 15:34 p-Isopropyltoluene ug/L ND 1.0 05/18/14 15:34 Styrene ug/L ND 1.0 05/18/14 15:34 Tetrachloroethene ug/L ND 1.0 05/18/14 15:34 Toluene ug/L ND 1.0 05/18/14 15:34 trans-1,2-Dichloroethene ug/L ND 1.0 05/18/14 15:34 trans-1,3-Dichloropropene ug/L ND 1.0 05/18/14 15:34 Trichloroethene ug/L ND 1.0 05/18/14 15:34 Trichlorofluoromethane ug/L ND 1.0 05/18/14 15:34 Vinyl acetate ug/L ND 2.0 05/18/14 15:34 Vinyl chloride ug/L ND 1.0 05/18/14 15:34 Xylene (Total) ug/L ND 2.0 05/18/14 15:34 1,2-Dichloroethane-d4 (S) % 90 70-130 05/18/14 15:34 4-Bromofluorobenzene (S) % 98 70-130 05/18/14 15:34 Toluene-d8 (S) % 99 70-130 05/18/14 15:34 LABORATORY CONTROL SAMPLE: Parameter 1201769 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 53.6 107 70-130 1,1,1-Trichloroethane ug/L 50 51.7 103 70-130 1,1,2,2-Tetrachloroethane ug/L 50 54.8 110 70-130 1,1,2-Trichloroethane ug/L 50 54.0 108 70-130 1,1-Dichloroethane ug/L 50 50.2 100 70-130 1,1-Dichloroethene ug/L 50 51.3 103 70-132 1,1-Dichloropropene ug/L 50 55.4 111 70-130 1,2,3-Trichlorobenzene ug/L 50 54.3 109 70-135 1,2,3-Trichloropropane ug/L 50 52.8 106 70-130 1,2,4-Trichlorobenzene ug/L 50 54.4 109 70-134 1,2-Dibromo-3-chloropropane ug/L 50 51.9 104 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.8 106 70-130 1,2-Dichlorobenzene ug/L 50 53.1 106 70-130 1,2-Dichloroethane ug/L 50 50.8 102 70-130 1,2-Dichloropropane ug/L 50 52.8 106 70-130 1,3-Dichlorobenzene ug/L 50 51.7 103 70-130 1,3-Dichloropropane ug/L 50 53.9 108 70-130 1,4-Dichlorobenzene ug/L 50 52.4 105 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 73 of 84 ladeAnalytical' www.pacelabs.mn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 LABORATORY CONTROL SAMPLE: Parameter 1201769 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2,2-Dichloropropane ug/L 50 52.3 105 58-145 2-Butanone (MEK) ug/L 100 76.6 77 70-145 2-Chlorotoluene ug/L 50 51.6 103 70-130 2-Hexanone ug/L 100 79.9 80 70-144 4-Chlorotoluene ug/L 50 51.6 103 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 80.5 81 70-140 Acetone ug/L 100 75.3 75 50-175 Benzene ug/L 50 58.3 117 70-130 Bromobenzene ug/L 50 52.3 105 70-130 Bromochloromethane ug/L 50 53.8 108 70-130 Bromodichloromethane ug/L 50 51.6 103 70-130 Bromoform ug/L 50 54.8 110 70-130 Bromomethane ug/L 50 50.8 102 54-130 Carbon tetrachloride ug/L 50 50.4 101 70-132 Chlorobenzene ug/L 50 50.6 101 70-130 Chloroethane ug/L 50 49.8 100 64-134 Chloroform ug/L 50 51.3 103 70-130 Chloromethane ug/L 50 44.2 88 64-130 cis-1,2-Dichloroethene ug/L 50 50.4 101 70-131 cis-1,3-Dichloropropene ug/L 50 54.7 109 70-130 Dibromochloromethane ug/L 50 50.8 102 70-130 Dibromomethane ug/L 50 52.3 105 70-131 Dichlorodifluoromethane ug/L 50 55.3 111 56-130 Diisopropyl ether ug/L 50 39.9 80 70-130 Ethylbenzene ug/L 50 51.1 102 70-130 Hexachloro-1,3-butadiene ug/L 50 52.6 105 70-130 m&p-Xylene ug/L 100 104 104 70-130 Methyl-tert-butyl ether ug/L 50 44.8 90 70-130 Methylene Chloride ug/L 50 50.3 101 63-130 Naphthalene ug/L 50 54.4 109 70-138 o-Xylene ug/L 50 52.6 105 70-130 p-Isopropyltoluene ug/L 50 52.6 105 70-130 Styrene ug/L 50 55.5 111 70-130 Tetrachloroethene ug/L 50 53.5 107 70-130 Toluene ug/L 50 53.3 107 70-130 trans-1,2-Dichloroethene ug/L 50 51.0 102 70-130 trans-1,3-Dichloropropene ug/L 50 52.7 105 70-132 Trichloroethene ug/L 50 57.1 114 70-130 Trichlorofluoromethane ug/L 50 48.3 97 62-133 Vinyl acetate ug/L 100 104 104 66-157 Vinyl chloride ug/L 50 60.6 121 69-130 Xylene (Total) ug/L 150 157 104 70-130 1,2-Dichloroethane-d4 (S) % 96 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8(S) % 100 70-130 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 74 of 84 laeeAnalyfical' www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1201934 1201935 MS MSD 92201204016 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD 1,1-Dichloroethene ug/L ND 50 50 49.7 45.7 99 91 70-166 8 Benzene ug/L ND 50 50 54.3 50.0 109 100 70-148 8 Chlorobenzene ug/L ND 50 50 49.4 45.6 99 91 70-146 8 Toluene ug/L ND 50 50 48.1 44.4 96 89 70-155 8 Trichloroethene ug/L ND 50 50 55.1 50.9 110 102 69-151 8 1,2-Dichloroethane-d4 (S) % 96 94 70-130 4-Bromofluorobenzene (S) % 98 98 70-130 Toluene-d8(S) % 97 97 70-130 Date: 05/21/201402:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual Page 75 of 84 Pace Analytical Services, Inc. ll �aaleemalyticale 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 QC Batch: MSV/26857 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92201204029, 92201204030, 92201204031, 92201204032 METHOD BLANK: 1201770 Matrix: Water Associated Lab Samples: 92201204029, 92201204030, 92201204031, 92201204032 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/18/14 15:51 1,1,1-Trichloroethane ug/L ND 1.0 05/18/14 15:51 1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/18/14 15:51 1,1,2-Trichloroethane ug/L ND 1.0 05/18/14 15:51 1,1-Dichloroethane ug/L ND 1.0 05/18/14 15:51 1,1-Dichloroethene ug/L ND 1.0 05/18/14 15:51 1,1-Dichloropropene ug/L ND 1.0 05/18/14 15:51 1,2,3-Thchlorobenzene ug/L ND 1.0 05/18/14 15:51 1,2,3-Tiichloropropane ug/L ND 1.0 05/18/14 15:51 1,2,4-Thchlorobenzene ug/L ND 1.0 05/18/14 15:51 1,2-Dibromo-3-chloropropane ug/L ND 5.0 05/18/14 15:51 1,2-Dibromoethane (EDB) ug/L ND 1.0 05/18/14 15:51 1,2-Dichlorobenzene ug/L ND 1.0 05/18/14 15:51 1,2-Dichloroethane ug/L ND 1.0 05/18/14 15:51 1,2-Dichloropropane ug/L ND 1.0 05/18/14 15:51 1,3-Dichlorobenzene ug/L ND 1.0 05/18/14 15:51 1,3-Dichloropropane ug/L ND 1.0 05/18/14 15:51 1,4-Dichlorobenzene ug/L ND 1.0 05/18/14 15:51 2,2-Dichloropropane ug/L ND 1.0 05/18/14 15:51 2-Butanone (MEK) ug/L ND 5.0 05/18/14 15:51 2-Chlorotoluene ug/L ND 1.0 05/18/14 15:51 2-Hexanone ug/L ND 5.0 05/18/14 15:51 4-Chlorotoluene ug/L ND 1.0 05/18/14 15:51 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 05/18/14 15:51 Acetone ug/L ND 25.0 05/18/14 15:51 Benzene ug/L ND 1.0 05/18/14 15:51 Bromobenzene ug/L ND 1.0 05/18/14 15:51 Bromochloromethan e ug/L ND 1.0 05/18/14 15:51 Bromodichloromethane ug/L ND 1.0 05/18/14 15:51 Bromoform ug/L ND 1.0 05/18/14 15:51 Bromomethane ug/L ND 2.0 05/18/14 15:51 Carbon tetrachloride ug/L ND 1.0 05/18/14 15:51 Chlorobenzene ug/L ND 1.0 05/18/14 15:51 Chloroethane ug/L ND 1.0 05/18/14 15:51 Chloroform ug/L ND 1.0 05/18/14 15:51 Chloromethane ug/L ND 1.0 05/18/14 15:51 cis- 1,2-Dichloroethene ug/L ND 1.0 05/18/14 15:51 cis- 1,3-Dichloropropene ug/L ND 1.0 05/18/14 15:51 Dibromochloromethane ug/L ND 1.0 05/18/14 15:51 Dibromomethane ug/L ND 1.0 05/18/14 15:51 Dichlorodifluoromethane ug/L ND 1.0 05/18/14 15:51 Diisopropyl ether ug/L ND 1.0 05/18/14 15:51 Ethylbenzene ug/L ND 1.0 05/18/14 15:51 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 76 of 84 46Anal ical www.pacelabs.corn Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 METHOD BLANK: 1201770 Matrix: Water Associated Lab Samples: 92201204029, 92201204030, 92201204031, 92201204032 Blank Reporting Parameter Units Result Limit Analyzed Hexachloro-1,3-butadiene ug/L ND 1.0 05118/1415:51 m&p-Xylene ug/L ND 2.0 05/18/14 15:51 Methyl-tert-butyl ether ug/L ND 1.0 05/18/14 15:51 Methylene Chloride ug/L ND 2.0 05/18/14 15:51 Naphthalene ug/L ND 1.0 05/18/14 15:51 o-Xylene ug/L ND 1.0 05/18/14 15:51 p-Isopropyltoluene ug/L ND 1.0 05/18/14 15:51 Styrene ug/L ND 1.0 05/18/14 15:51 Tetrachloroethene ug/L ND 1.0 05/18/14 15:51 Toluene ug/L ND 1.0 05/18/14 15:51 trans-1,2-Dichloroethene ug/L ND 1.0 05/18/14 15:51 trans-1,3-Dichloropropene ug/L ND 1.0 05118/1415:51 Trichloroethene ug/L ND 1.0 05118/1415:51 Trichlorofluoromethane ug/L ND 1.0 05118/1415:51 Vinyl acetate ug/L ND 2.0 05/18/14 15:51 Vinyl chloride ug/L ND 1.0 05/18/14 15:51 Xylene (Total) ug/L ND 2.0 05/18/14 15:51 1,2-Dichloroethane-d4 (S) % 92 70-130 05/18/14 15:51 4-Bromofluorobenzene (S) % 97 70-130 05/18/14 15:51 Toluene-d8 (S) % 99 70-130 05/18/14 15:51 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1201771 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 54.4 109 70-130 1,1,1-Trichloroethane ug/L 50 50.8 102 70-130 1,1,2,2-Tetrachloroethane ug/L 50 55.8 112 70-130 1,1,2-Trchloroethane ug/L 50 54.7 109 70-130 1,1-Dichloroethane ug/L 50 49.8 100 70-130 1,1-Dichloroethene ug/L 50 51.0 102 70-132 1,1-Dichloropropene ug/L 50 55.4 111 70-130 1,2,3-Trichlorobenzene ug/L 50 57.8 116 70-135 1,2,3-Trichloropropane ug/L 50 53.5 107 70-130 1,2,4-Trichlorobenzene ug/L 50 56.2 112 70-134 1,2-Dibromo-3-chloropropane ug/L 50 55.2 110 70-130 1,2-Dibromoethane (EDB) ug/L 50 53.1 106 70-130 1,2-Dichlorobenzene ug/L 50 54.4 109 70-130 1,2-Dichloroethane ug/L 50 50.2 100 70-130 1,2-Dichloropropane ug/L 50 53.0 106 70-130 1,3-Dichlorobenzene ug/L 50 51.9 104 70-130 1,3-Dichloropropane ug/L 50 53.3 107 70-130 1,4-Dichlorobenzene ug/L 50 53.5 107 70-130 2,2-Dichloropropane ug/L 50 51.9 104 58-145 2-Butanone (MEK) ug/L 100 81.6 82 70-145 2-Chlorotoluene ug/L 50 52.3 105 70-130 REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 77 of 84 la6eAnalyfical' www.paceiabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: 414-02 Pace Project No.: 92201204 LABORATORY CONTROL SAMPLE: Parameter 1201771 Units Spike Conc. LCS Result 2-Hexanone ug/L 100 83.9 4-Chlorotoluene ug/L 50 51.9 4-Methyl-2-pentanone (MIBK) ug/L 100 81.6 Acetone ug/L 100 78.6 Benzene ug/L 50 57.9 Bromobenzene ug/L 50 52.8 Bromochloromethane ug/L 50 52.6 Bromodichloromethane ug/L 50 51.4 Bromoform ug/L 50 55.2 Bromomethane ug/L 50 51.4 Carbon tetrachloride ug/L 50 50.2 Chlorobenzene ug/L 50 51.0 Chloroethane ug/L 50 46.2 Chloroform ug/L 50 51.1 Chloromethane ug/L 50 42.2 cis-1,2-Dichloroethene ug/L 50 51.0 cis-1,3-Dichloropropene ug/L 50 54.5 Dibromochloromethane ug/L 50 51.1 Dibromomethane ug/L 50 52.7 Dichlorodifluoromethane ug/L 50 54.2 Diisopropyl ether ug/L 50 39.9 Ethylbenzene ug/L 50 50.9 Hexachloro-1,3-butadiene ug/L 50 53.8 m&p-Xylene ug/L 100 104 Methyl-tert-butyl ether ug/L 50 45.3 Methylene Chloride ug/L 50 53.1 Naphthalene ug/L 50 58.6 o-Xylene ug/L 50 52.6 p-Isopropyltoluene ug/L 50 53.5 Styrene ug/L 50 55.5 Tetrachloroethene ug/L 50 53.9 Toluene ug/L 50 52.8 trans-1,2-Dichloroethene ug/L 50 50.0 trans-1,3-Dichloropropene ug/L 50 52.4 Trichloroethene ug/L 50 56.9 Trichlorofluoromethane ug/L 50 47.3 Vinyl acetate ug/L 100 104 Vinyl chloride ug/L 50 57.4 Xylene (Total) ug/L 150 157 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Date: 05/21/2014 02:51 PM LCS % Rec % Rec Limits 84 70-144 104 70-130 82 70-140 79 50-175 116 70-130 106 70-130 105 70-130 103 70-130 110 70-130 103 54-130 100 70-132 102 70-130 92 64-134 102 70-130 84 64-130 102 70-131 109 70-130 102 70-130 105 70-131 108 56-130 80 70-130 102 70-130 108 70-130 104 70-130 91 70-130 106 63-130 117 70-138 105 70-130 107 70-130 111 70-130 108 70-130 106 70-130 100 70-130 105 70-132 114 70-130 95 62-133 104 66-157 115 69-130 105 70-130 95 70-130 99 70-130 100 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Page 78 of 84 aceAnal ical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: 414-02 Pace Project No.: 92201204 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21 /2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 79 of 84 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite100 aceAnalytical Huntersville, NC 28078078 www.paceWs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: 414-02 Pace Project No.: 92201204 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92201204001 MWA EPA 8260 MSV/26840 92201204002 MW-10D EPA 8260 MSV/26840 92201204003 MW-28 EPA 8260 MSV/26840 92201204004 MW-9 EPA 8260 MSV/26840 92201204005 MWA1 EPA 8260 MSV/26840 92201204006 MW-5 EPA 8260 MSV/26840 92201204007 MW-17D EPA 8260 MSV/26840 92201204008 MWA8 EPA 8260 MSV/26840 92201204009 MW-20 EPA 8260 MSV/26840 92201204010 MW-19 EPA 8260 MSV/26840 92201204011 MW-6 EPA 8260 MSV/26840 92201204012 MW-30 EPA 8260 MSV/26840 92201204013 MW-12D EPA 8260 MSV/26840 92201204014 MW-26D EPA 8260 MSV/26840 92201204015 MW-29 EPA 8260 MSV/26840 92201204016 MW-13 EPA 8260 MSV/26856 92201204017 MW-27D EPA 8260 MSV/26856 92201204018 MW-27DD EPA 8260 MSV/26856 92201204019 MW-33 EPA 8260 MSV/26856 92201204020 MW-32 EPA 8260 MSV/26856 92201204021 MW-23 EPA 8260 MSV/26856 92201204022 MW-16 EPA 8260 MSV/26856 92201204023 MW-21D EPA 8260 MSV/26856 92201204024 MW-24 EPA 8260 MSV/26856 92201204025 MW-14D EPA 8260 MSV/26856 92201204026 MW-3 EPA 8260 MSV/26856 92201204027 MW-25 EPA 8260 MSV/26856 92201204028 MW-15 EPA 8260 MSV/26856 92201204029 MW-8 EPA 8260 MSV/26857 92201204030 MW-7 EPA 8260 MSV/26857 92201204031 RW-3 EPA 8260 MSV/26857 92201204032 MW-22D EPA 8260 MSV/26857 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/21/2014 02:51 PM without the written consent of Pace Analytical Services, Inc.. Page 80 of 84 -P,iceAfUlytical Sample Condition Upon Receil Document Number: F-CHR-CS-003-rev.14 Hage "I Or Z Issuing Authority: Pace Huntersville Quality Office Client Name: CRQ, �tP( ',rc 1 '�'T Courier: ❑ Fed Ex ❑ UPS❑ USPClient❑ Commercial[] Pace Other Custody Seal on Cooler/Box Present: yes yes /////�no Seals intact: Elyes ❑ no Packing Material: ❑ Bubble Wrap [,Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T11024 1 Type of Ice: a Blue None Samples on ice, cooling process has begun Temp Correction Factor T1102: No Correction T13�No Correction Corrected Cooler Temp.:.•C Biological Tissue is Frozen: Yes No r/A Date and Initi t of erson a amining contents:,fi�� Temp should be above freezing to 6°C Comments: Chain of Custody Present: es ONO ❑N/A 1. Chain of Custody Filled Out: PYep ONO ❑NIA 2. Chain of Custody Relinquished: Y s ONO ❑N/A 3. Sampler Name & Signature on COC: Yes ONO ❑N/A 4. Samples Arrived within Hold Time: 12Yes ONO ❑N/A 5. Short Hold Time Analysis (<72hr): El Yes No ❑N/A 6. Rush Turn Around Time Requested: ❑Yes PNIO ❑N/A 7. Sufficient Volume: Yes ❑No ❑N/A 8. Correct Containers Used: [ (Yes ONO ❑N/A g. -Pace Containers Used: es ONO ❑N/A Containers Intact: VYes ❑No ❑N/A 10, Filtered volume received for Dissolved tests ❑Yes ONO R N/A 11, Sample Labels match COC: es No ❑N/A 12. ( i� -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. ❑Yes ❑No ,idN/A 13. All containers needing preservation are found to be in ❑Yes ❑No 1/A compliance with EPA recommendation. exceptions: VOA, coliform, TOC, O&G, WI -SRO (water) PYes ❑No Samples checked for dechlorination: ❑Yes ❑No /A 14. Headspace in VOA Vials (>6mm): ❑Yes No ❑N/A 15. Trip Blank Present: ❑Yes ONO V(N/A 16. Trip Blank Custody Seals Present ❑Yes ONO C/N/A Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: Comments/ Resolution: Date/Time: SCURF Review: f f late: ate: lq q SRF Review: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) woa:e2201204 11111111111d1111111 92201204 Page 81 of 84 PaceAnalytical www.pacelabs.com Section A Required Client Information* R.0-0 cw {r 2 t Email To: 2� c-�N�wccc) M y , —a 4,_, Fax Yi CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Section C Page: 1 of 3 Required Project Information: Invoice Information: Report To: �,x. 9~1 Attention: 1792985 wC.- Ct Copy To. JCompany Name: Purchase Order No.: Project Name. ), I 1-1 Section D Matrix Codes Required Client Information MATRIX ! CODE °' s COLLECTED Drinking Water DW UUO Water WT Waste Water WW U m COMPOSITE COMPOSITE U Product P < START END'GRA3 J SodtSolld SL U p SAMPLE ID Oil OIL w Wipe (A-Z, 0-9 l-) Air AR p w Q a Z Sample IDS MUST BE UNIQUE Tissue TS O a `w < Other OT O ~ O X E w a LU U F a `a a a LL O — g DATE TIME DATE TIME # 2 !1/tU1- i O 17 1 It to REGULATORY AGENCY ass: NPDES GROUND WATER DRINKING WATER Quote UST RCRA OTHER ence Protect Site Location ger: Proffle # q STATE: Requested Analysis Filtered (YIN) T- z Preservatives i 0 a IY Pace Project No./ Lab I.D. a 6 e �■t■■■■i■■�■�■■■■i�■■■■ ©■■■■■■■■■■■■ VP SAMPLE CONDITIONS ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION ACCEPTED BY I AFFILIATION SAMPLER NAME AND SIGNATURE Its-s ;i PRINT Name of SAMPLER: Gft✓ 6-faiiwic-0 SIGNATURE of SAMPLER: f DATE Signed ) i . ��' (MM/DD/YY): S l F J c Irnponarl Nut, Gv vg'arg!ha form you are acc pting Pace's NET 30 day payment terms and agreeing to late charges of 1.5°k per month any Invoices not paid y4tV.30 days F-ALL-0-020rev.07, 15-May-2007 I PaceAnalyt Y/ww.pacelaos.com Section A Section B Section C Required Client Information: Required Project Information: Invoice Information, Company r t Report To. Attention, v Page: � of 17 2 9 86 Address. OU`, ` Copy To: Company Name. REGULATORY AGENCY L. "1 S L Address. NPDES GROUND WATER DRINKING WATER UST RCRA OTHER Email To,r, N, Purchase (; c,e-L� � c•n ct•' *l Order No.: Pace Quote Reference. o L, Fax: Project Name y �� J W (%��! 041 Pae.e Prolell Manager Site Location STA TE: j "C aquested Due DateiTAT: Project Number. C n h Pace Profile a Requested Analysis Filtered (Y/N) i - Section D Matrix Codes Required Chen; lnforr•tat— MATRIX r CODE Drinking Water DW Water WT Waste Water WW Product P Soil/Solid SL SAMPLE ID oII OL Wipe WP (A-Z. 0-9 I ,-) R Air A Sample IDS MUST BE UNIQUE Tissue TS Other OT $ - p O U X_ r S U U m a ae (D w ya ~ w a s COLLECTED zO — J p n- s w w a Q rn w Z t— Z O O w O # Preservatives i COMPOSITE START COf.iPOSiTE EwD'GRne Z m df a c Z) _ p Z _ U = _ Otn"t cU Z O (M Z C m d) 2 u L O y F— rA to ?` l6 c Q. y '� Z Y U m m Q) Pace Project No./ Lab I.D. DATE TIME DATE TIME 2�6a(J 3� l 3 I� 7 Sell; 4 — 'IS( ()e y s 7 AA. W 8 g L ao ,o Ail ` tolle „ •- �. Q ice 4-41 X I 12 MW- 't lt3v 1 1 1 Pq ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY / AFFILIATION DATE TIME SAMPLE CONDITIONS 0-- IVACE Cl '- t9 - _ SAMPLER NAME AND SIGNATURE - - - PRINT Name of SAMPLER: �'v �.,� •lWCCI SIGNATURE of SAMPLER: DATE Signed (MMIDDYY): 'Impunanl N nr r., y;rraa 1— m Vaicepong Pace's NL 130 d.ty paVment leans and agreeing to late ChalgeS of 1 5% per month n7"r any —o,A, R4Z: aid wnhm ;tp dayy I -ALL-0-020rev 07. 15-May-2007 CHAIN -OF -CUSTODY / Analytical Request Document Pace The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Clio, Required Client Information- Required Project Information: Invoice Information: Company: n Repon To , - umµ^ Attention. 179298 7 —1 (� T r( ClC `C_ ` Address: 01jCopy To: Company Name: REGULATORY AGENCY t t� Address: NPDES X GROUND WATER DRINKING WATER UST RCRA OTHER Email To L n cr '1` Purchase Order No . Pace Quote Reference. P o Fax Project Name: Pace Project Slte Location Manager STATE: / V - equested Due DaterTAT: Project Number: Q Pace Prohlc- # Requested Analysis Filtered (Y/N) Section D Matrix Codes — z Required Client Information MATRIX / CODE _ COLLECTED Preservatives Y Drinking Water DW U p Water WT Waste Water WW Product P $ U m COMPOSITE START COMPOSITE END �.RAff w Z . \ L� Soil/Solid SL Cr (7 p fn y `�`�V SAMPLE ID W WE, `" �? w in e (A-Z. 0-9 / ,-i Airp AR 0 w a -o H o •�� Sample IDS MUST BE UNIQUE Tissue TS O a w ~ a, H U Other OT U x_ w w Z O � w O co?` # w ¢ a a E O a p cn 2 O ca L T cc O u F rn DATE TIME DATE TIME N 00 _ _ = Z Z 2 O y D_ Pace Project No./ Lab I.D. 1 ANUJ ], (� � l 5 2 1 CAL 2 3 t— 2 4 Nl W - S dv 5 MJ." - 1 S s JAill 8 e f!l IJ :' 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS <<c- 3' 4,bL, /9gc 'SI1 1 Litt SAMPLER NAME AND SIGNATURE y PRINT Name of SAMPLER: c � tiwc ~ =• — x ` c_ SIGNATURE of SAMPLER: - DATE Signed �� — (MM/DD/YY): unp,,1,W No�,r By thc:you arr. A cepung Pace's Nf i 30 day payment teens and a<lreeu+.g to late charge, of 1 5% per monthVany invoices nM p30 days F-ALL-0-020rev 07. 15-May-2007