Loading...
HomeMy WebLinkAboutNC0021211_Renewal Modification_20201125 Titg of 6raiyult P. 0. Drawer 357 201 South Main Street Graham, North Carolina 27253 Tel: (336) 570-6700/Fax: (336) 570-6703 November 13, 2020 Mr. Michael Montebello RECEIVED N.C. Department of Environmental Quality Division of Water Resources NOV 2 5 2020 Water Quality Permitting - NPDES �1PDES 1617 Mail Service Center N �� �DW Raleigh, North Carolina 27699-1617 Re: City of Graham Graham WWTP NPDES Permit Renewal Permit No. N0021211 Dear Mr. Montebello: Enclosed is the permit renewal package for the NPDES Permit for the Graham Wastewater Treatment Plant (WWTP) for the City of Graham, North Carolina. The permit renewal package includes the completed NPDES Permit Application (Form 2A), with all required supplements provided as attachments as well as the major modification application fee of $1,030. Please let us know if you have any questions or comments on this renewal package. Respectfully, Ton[a A. Mann Utilities Director 1 CITY OF -F� RAH A NORTH CAROLINA Graham WWTP Major Modification NPDES Permit Application- EPA Form 2A City of G NC Graham WWTP Improvement November, 2020 City of Graham, North Carolina EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 Form U.S.Environmental Protection Agency 2A ` EPA Application for NPDES Permit to Discharge Wastewater NPDES NEW AND EXISTING PUBLICLY OWNED TREATMENT WORKS SECTION 1.BASIC APPLICATION INFORMATION FOR ALL APPLICANTS(40 CFR 122.21(j)(1)and (9)) 1.1 Facility name City of Graham Mailing address(street or P.O.box) P.O.Drawer 357 City or town State ZIP code 0 Graham NC 27253 Contact name(first and last) Title Phone number Email address c Tonya A.Mann Utilities Director (336)570-6721 tmann@cityofgraham.com Location address(street,route number,or other specific identifier) ❑ Same as mailing address ro 1204 East Gilbreath Street u City or town State ZIP code Graham NC 27253 1.2 Is this application for a facility that has yet to commence discharge? RECEIVED ElYes 4 See instructions on data submission ❑✓ No requirements for new dischargers. NOV 2 5 2020 1.3 Is applicant different from entity listed under Item 1.1 above? NCDEQIDWRINPDES El Yes ❑ No 4 SKIP to Item 1.4. Applicant name Applicant address(street or P.O. box) 0 City or town State ZIP code Contact name(first and last) Title Phone number Email address • 1.4 Is the applicant the facility's owner,operator,or both?(Check only one response.) El Owner ❑ Operator 0 Both 1.5 To which entity should the NPDES permitting authority send correspondence?(Check only one response.) El Facility ❑ Applicant 0 Facility and applicant (they are one and the same) 1.6 Indicate below any existing environmental permits.(Check all that apply and print or type the corresponding permit number for each.) Existing Environmental Permits ✓❑ NPDES(discharges to surface 0 RCRA(hazardous waste) ❑ UIC(underground injection water) control) ;= NC0021211 WQCS00065 NA 0 0 PSD(air emissions) ❑ Nonattainment program(CM) ❑ NESHAPs(CM) w Stormwater,NCS000408 NA NA a) ❑ Ocean dumping(MPRSA) ❑ Dredge or fill(CWA Section ❑ Other(specify) w 404) NA NA Non Discharge WQ0003824 EPA Form 3510-2A(Revised 3-19) Page 1 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 1.7 Provide the collection system information requested below for the treatment works. Municipality Population Collection System Type Ownership Status Served Served (indicate percentage) a City of Graham 15,969 no %separate sanitary sewer El Own ❑ Maintain a) 0 %combined storm and sanitary sewer ❑ Own ❑ Maintain d _ ❑ Unknown El Own ❑ Maintain co NA %separate sanitary sewer 0 Own El Maintain o NA NA NA %combined storm and sanitary sewer 0 Own ❑ Maintain 0 ❑ Unknown 0 Own ❑ Maintain 0- O NA NA NA %separate sanitary sewer 0 Own ❑ Maintain c NA %combined storm and sanitary sewer 0 Own ❑ Maintain `o ❑ Unknown ❑ Own ❑ Maintain E NA %separate sanitary sewer ❑ Own ❑ Maintain co NA NA NA %combined storm and sanitary sewer 0 Own ❑ Maintain c ❑ Unknown ❑ Own ❑ Maintain 0 Total 15,969 a' Population o Served Separate Sanitary Sewer System Combined Storm and Sanitary Sewer Total percentage of each type of o 0 sewer line(in miles) 100 /o NA /o C 1.8 Is the treatment works located in Indian Country? o ❑ Yes 0 No U v 1.9 Does the facility discharge to a receiving water that flows through Indian Country? ❑ Yes 0 No 1.10 Provide design and actual flow rates in the designated spaces. Design Flow Rate 3.5 mgd To y Annual Avera a Flow Rates Actual a2 Two Years Ago Last Year This Year a = 0 2018,2.13 mgd 2019,2.10 mgd Up to July,1.95 mgd L a: Maximum Daily Flow Rates(Actual) o Two Years Ago Last Year This Year 2018,8.54 mgd 2019,6.11 mgd Up to July,6.32 mgd N 1.11 Provide the total number of effluent discharge points to waters of the United States by type. o Total Number of Effluent Discharge Points by Type a a Combined Sewer Constructed P. Treated Effluent Untreated Effluent Bypasses Emergency - ver Oflows Overflows V -- N 0 1 0 0 0 0 EPA Form 3510-2A(Revised 3-19) Page 2 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 Outfalls Other Than to Waters of the United States 1.12 Does the POTW discharge wastewater to basins,ponds,or other surface impoundments that do not have outlets for discharge to waters of the United States? ❑ Yes 0 No 4 SKIP to Item 1.14. 1.13 Provide the location of each surface impoundment and associated discharge information in the table below. Surface Impoundment Location and Discharge Data Average Daily Volume Continuous or Intermittent Location Discharged to Surface Impoundment (check one) ❑ Continuous gpd ❑ Intermittent ❑ Continuous gpd 0 Intermittent ❑ Continuous gpd 0 Intermittent 1.14 Is wastewater applied to land? ❑ Yes ❑r No4SKIPtoItem1.16. 0 1.15 Provide the land application site and discharge data requested below. y Land Application Site and Discharge Data Continuous or 8 Location Size Average Daily Volume Intermittent Applied (check one) N acresgpd 0 Continuous o 0 Intermittent acres d 0 Continuous o gp ❑ Intermittent acres d ❑ Continuous gp 0 Intermittent 1.16 Is effluent transported to another facility for treatment prior to discharge? o ❑ Yes ❑✓ No 4 SKIP to Item 1.21. 1.17 Describe the means by which the effluent is transported(e.g.,tank truck,pipe). 1.18 Is the effluent transported by a party other than the applicant? ❑ Yes E No SKIP to Item 1.20. 1.19 Provide information on the transporter below. Transporter Data Entity name Mailing address(street or P.O.box) City or town State ZIP code Contact name(first and last) Title Phone number Email address EPA Form 3510-2A(Revised 3-19) Page 3 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 1.20 In the table below, indicate the name,address,contact information, NPDES number,and average daily flow rate of the receiving facility. Receiving Facility Data Facility name Mailing address(street or P.O.box) City or town State ZIP code 0 Contact name(first and last) Title 0 Phone number Email address NPDES number of receiving facility(if any) 0 None Average daily flow rate mgd 0_ 1.21 Is the wastewater disposed of in a manner other than those already mentioned in Items 1.14 through 1.21 that do not have outlets to waters of the United States(e.g., underground percolation,underground injection)? ❑ Yes ❑ No 4 SKIP to Item 1.23. 0 1.22 Provide information in the table below on these other disposal methods. Information on Other Disposal Methods o Disposal Location of Size of Annual Average Continuous or Intermittent Method Disposal Site Disposal Site Daily Discharge (check one) Description Volume cn ° acresgpd 0 Continuous 0 Intermittent 0 Continuous acres gpd ❑ Intermittent acresgpd ❑ Continuous ❑ Intermittent 1.23 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(n)?(Check all that apply. Consult with your NPDES permitting authority to determine what information needs to be submitted and when.) a a ❑ Discharges into marine waters(CWA ❑ Water quality related effluent limitation(CWA Section j Section 301(h)) 302(b)(2)) ❑✓ Not applicable 1.24 Are any operational or maintenance aspects(related to wastewater treatment and effluent quality)of the treatment works the responsibility of a contractor? ❑ Yes E No+SKIP to Section 2. 1.25 Provide location and contact information for each contractor in addition to a description of the contractor's operational and maintenance responsibilities. Contractor Information Contractor 1 Contractor 2 Contractor 3 Contractor name (company name) `0 Mailing address (street or P.O.box) o City,state,and ZIP code Contact name(first and c.) last) Phone number Email address Operational and maintenance responsibilities of contractor EPA Form 3510-2A(Revised 3-19) Page 4 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 SECTION 2.ADDITIONAL INFORMATION(40 CFR 122.21(j)(1)and(2)) c Outfalls to Waters of the United States = 2.1 Does the treatment works have a design flow greater than or equal to 0.1 mgd? El Yes ❑ No 4 SKIP to Section 3. 0 2.2 Provide the treatment works'current average daily volume of inflow Average Daily Volume of Inflow and Infiltration '� and infiltration. 388,000 gpd = Indicate the steps the facility is taking to minimize inflow and infiltration. The City of Graham follows the provisions of its Collection System Permit to minimize inflow and infiltration. 0 0 4- 2.3 Have you attached a topographic map to this application that contains all the required information?(See instructions for v specific requirements.) 01 Lr 0 0 ElYes ❑ No E 2.4 Have you attached a process flow diagram or schematic to this application that contains all the required information? o2 (See instructions for specific requirements.) 0, FL co ElYes El No 2.5 Are improvements to the facility scheduled? El Yes El No 4 SKIP to Section 3. Briefly list and describe the scheduled improvements. 0 1 Expansion of the WWTP from a capacity of 3.5 mgd to 5.0 mgd. Refer to figure 4 for more details. E c 2. E "E) 3. d co 4. -0 2.6 Provide scheduled or actual dates of completion for improvements. Scheduled or Actual Dates of Completion for Improvements Affected Attainment of Scheduled Begin End Begin Outfalls Operational 0 Improvement Construction Construction Discharge p (from above) (list outfall (MM/DDIYYYY) (MM/DDIYYYY) (MM/DD/YYYY) (MM/DD/LevYYYY) number ) a 1• 1 08/01/2022 02/01/2025 02/01/2025 02/01/2025 0 2. co 3. 4. 2.7 Have appropriate permits/clearances concerning other federal/state requirements been obtained?Briefly explain your response. El Yes El No El None required or applicable Explanation: Environmental document currently under review,submitted November 2020.Finding of no significant impacts anticipated spring 2021. EPA Form 3510-2A(Revised 3-19) Page 5 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 SECTION 3.INFORMATION ON EFFLUENT DISCHARGES(40 CFR 122.21(j)(3)to(5)) 3.1 Provide the following information for each outfall.(Attach additional sheets if you have more than three outfalls.) Outfall Number o01 Outfall Number Outfall Number State NC County Alamance o City or town Graham 0 ° Distance from shore NA ft• ft. ft. a. Depth below surface NA ft. ft. ft. Average daily flow rate mgd mgd mgd Latitude 36° 02' 44" Longitude 79° 22' 06" 3.2 Do any of the outfalls described under Item 3.1 have seasonal or periodic discharges? o ❑ Yes r❑ No 4 SKIP to Item 3.4. r, 3.3 If so,provide the following information for each applicable outfall. y Outfall Number Outfall Number Outfall Number 0 Number of times per year discharge occurs a Average duration of each discharge(specify units) To Average flow of each discharge mgtl mgd mgd Months in which discharge occurs 3.4 Are any of the outfalls listed under Item 3.1 equipped with a diffuser? ❑ Yes ❑r No 4 SKIP to Item 3.6. C.) 3.5 Briefly describe the diffuser type at each applicable outfall. c Outfall Number Outfall Number Outfall Number — d ui 3.6 Does the treatment works discharge or plan to discharge wastewater to waters of the United States from one or more discharge points? E Yes ❑ No -SKIP to Section 6. EPA Form 3510-2A(Revised 3-19) Page 6 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 3.7 Provide the receiving water and related information(if known)for each outfall. Outfall Number °o1 Outfall Number Outfall Number Receiving water name Haw River Name of watershed,river, =o or stream system Cape Fear Q U.S.Soil Conservation N Service 14-digit watershed NA o code L R Name of state g management/river basin Cape Fear a) U.S.Geological Survey U 8-digit hydrologic 03030002 cc cataloging unit code Critical low flow(acute) 34 cfs cfs cfs Critical low flow(chronic) 85 cfs cfs cfs Total hardness at critical mg/L of mg/L of mg/L of low flow NA CaCO3 CaCO3 CaCO3 3.8 Provide the following information describing the treatment provided for discharges from each outfall. Outfall Number 001 Outfall Number Outfall Number Highest Level of 0 Primary 0 Primary 0 Primary Treatment(check all that 0 Equivalent to 0 Equivalent to 0 Equivalent to apply per outfall) secondary secondary secondary O Secondary 0 Secondary 0 Secondary O Advanced 0 Advanced ❑ Advanced 0 Other(specify) 0 Other(specify) ❑ Other(specify) 0 a Design Removal Rates by NA 0 Outfall N w o BOD5 or CBOD5 96 d g CID TSS 95 % % % H 0 Not applicable 0 Not applicable 0 Not applicable Phosphorus 98.5 % oh oh 0 Not applicable 0 Not applicable 0 Not applicable Nitrogen 97 % % % Other(specify) ® Not applicable 0 Not applicable 0 Not applicable % EPA Form 3510-2A(RevisedPage 7 3-19) 9 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 3.9 Describe the type of disinfection used for the effluent from each outfall in the table below. If disinfection varies by season,describe below. Chlorination utilizing liquid bleach(12%sodium hypochlorite). o Outfall Number 001 Outfall Number Outfall Number .2- Disinfection type Chlorination 43 d 0 Seasons used All a Dechlorination used? ❑ Not applicable ❑ Not applicable pp ❑ Not applicable 0 Yes ❑ Yes ❑ Yes ❑ No ❑ No ❑ No 3.10 Have you completed monitoring for all Table A parameters and attached the results to the application package? 0 Yes El No 3.11 Have you conducted any WET tests during the 4.5 years prior to the date of the application on any of the facility's discharges or on any receiving water near the discharge points? O Yes ❑ No 4 SKIP to Item 3.13. 3.12 Indicate the number of acute and chronic WET tests conducted since the last permit reissuance of the facility's discharges by outfall number or of the receiving water near the discharge points. Outfall Number 001 Outfall Number Outfall Number Acute Chronic Acute Chronic Acute Chronic Number of tests of discharge 18 water Number of tests of receiving water 3.13 Does the treatment works have a design flow greater than or equal to 0.1 mgd? co ❑✓ Yes ❑ No 4 SKIP to Item 3.16. 0 3.14 Does the POTW use chlorine for disinfection,use chlorine elsewhere in the treatment process,or otherwise have reasonable potential to discharge chlorine in its effluent? ❑� Yes 4 Complete Table B, including chlorine. ❑ No 4 Complete Table B,omitting chlorine. 3.15 Have you completed monitoring for all applicable Table B pollutants and attached the results to this application CO package? ❑✓ Yes El No 3.16 Does one or more of the following conditions apply? • The facility has a design flow greater than or equal to 1 mgd. • The POTW has an approved pretreatment program or is required to develop such a program. • The NPDES permitting authority has informed the POTW that it must sample for the parameters in Table C, must sample other additional parameters(Table D),or submit the results of WET tests for acute or chronic toxicity for each of its discharge outfalls(Table E). Yes 4 Complete Tables C,D,and E as ❑ applicable. ❑ No 4 SKIP to Section 4. 3.17 Have you completed monitoring for all applicable Table C pollutants and attached the results to this application package? ❑✓ Yes ❑ No 3.18 Have you completed monitoring for all applicable Table D pollutants required by your NPDES permitting authority and attached the results to this application package? ❑✓ Yes ❑ No additional sampling required by NPDES permitting authority. EPA Form 3510-2A(Revised 3-19) Page 8 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 3.19 Has the POTW conducted either(1)minimum of four quarterly WET tests for one year preceding this permit application or(2)at least four annual WET tests in the past 4.5 years? E Yes ❑ No 4 Complete tests and Table E and SKIP to Item 3.26. 3.20 Have you previously submitted the results of the above tests to your NPDES permitting authority? 0 Yes ❑ No 4 Provide results in Table E and SKIP to Item 3.26. 3.21 Indicate the dates the data were submitted to your NPDES permitting authority and provide a summary of the results. Date(s)Submitted Summary of Results (MM/DD/YYYY) Second Species: 12/16/2016, All passing results.Primary species ceriodaphnia.Second species fathead cu 03/23/2017, 06/28/2018, minnow. cu 09/19/2019 "2 Primary Species Quarterly as 3.22 Regardless of how you provided your WET testing data to the NPDES permitting authority,did any of the tests result in toxicity? �' ❑ Yes ❑✓ No-9 SKIP to Item 3.26. w 3.23 Describe the cause(s)of the toxicity: d w 3.24 Has the treatment works conducted a toxicity reduction evaluation? ❑ Yes ❑✓ No 4 SKIP to Item 3.26. 3.25 Provide details of any toxicity reduction evaluations conducted. 3.26 Have you completed Table E for all applicable outfalls and attached the results to the application package? ❑ Yes ❑ Not applicable because previously submitted information to the NPDES permittin• authorit . SECTION 4.INDUSTRIAL DISCHARGES AND HAZARDOUS WASTES(40 CFR 122.21(j)(6)and(7)) 4.1 Does the POTW receive discharges from Sills or NSCIUs? ❑✓ Yes ❑ No 4 SKIP to Item 4.7. 4.2 Indicate the number of SIUs and NSCIUs that discharge to the POTW. Number of Sills Number of NSCIUs 5 3 4.3 Does the POTW have an approved pretreatment program? N ❑� Yes ❑ No g 4.4 Have you submitted either of the following to the NPDES permitting authority that contains information substantially cp identical to that required in Table F:(1)a pretreatment program annual report submitted within one year of the application or(2)a pretreatment program? 0 Yes ❑ No-4 SKIP to Item 4.6. 0 Tts 4.5 Identify the title and date of the annual report or pretreatment program referenced in Item 4.4.SKIP to Item 4.7. City of Graham Pretreatment Annual Report for 2019 02/27/2020 c — 4.6 Have you completed and attached Table F to this application package? ❑✓ Yes ❑ No EPA Form 3510-2A(Revised 3-19) Page 9 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 4.7 Does the POTW receive,or has it been notified that it will receive, by truck, rail,or dedicated pipe,any wastes that are regulated as RCRA hazardous wastes pursuant to 40 CFR 261? ❑ Yes 0 No 4 SKIP to Item 4.9. 4.8 If yes, provide the following information: Annual Hazardous Waste Waste Transport Method Amount of Units Number (check all that apply) Waste Received ❑ Truck ❑ Rail ❑ Dedicated pipe ❑ Other(specify) 0 d ❑ Truck ❑ Rail ❑ Dedicated pipe ❑ Other(specify) 0 N ❑ Truck ❑ Rail ❑ Dedicated pipe ❑ Other(specify) ti 4.9 Does the POTW receive,or has it been notified that it will receive,wastewaters that originate from remedial activities, including those undertaken pursuant to CERCLA and Sections 3004(7)or 3008(h)of RCRA? ❑ Yes El No 4 SKIP to Section 5. 17) 4.10 Does the POTW receive(or expect to receive)less than 15 kilograms per month of non-acute hazardous wastes as specified in 40 CFR 261.30(d)and 261.33(e)? ❑ Yes 4 SKIP to Section 5. El No 4.11 Have you reported the following information in an attachment to this application:identification and description of the site(s)or facility(ies)at which the wastewater originates;the identities of the wastewater's hazardous constituents;and the extent of treatment,if any,the wastewater receives or will receive before entering the POTW? ❑ Yes El No SECTION 5.COMBINED SEWER OVERFLOWS(40 CFR 122.21(j)(8)) 5.1 Does the treatment works have a combined sewer system? ❑ Yes 0 No 4SKIP to Section 6. 13 5.2 Have you attached a CSO system map to this application?(See instructions for map requirements.) a ElYes ElNo cc 5.3 Have you attached a CSO system diagram to this application?(See instructions for diagram requirements.) U ❑ Yes El No EPA Form 3510-2A(Revised 3-19) Page 10 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 5.4 For each CSO outfall,provide the following information.(Attach additional sheets as necessary.) CSO Outfall Number CSO Outfall Number CSO Outfall Number = City or town 0 Q- State and ZIP code 0 co o County al o Latitude 11 0 co Longitude " U Distance from shore ft. ft. ft. Depth below surface ft. ft. ft. 5.5 Did the POTW monitor any of the following items in the past year for its CSO outfalls? CSO Outfall Number CSO Outfall Number CSO Outfall Number Rainfall 0 Yes ❑ No 0 Yes ❑ No 0 Yes 0 No a, c 7i) CSO flow volume El Yes 0 No ❑ Yes 0 No 0 Yes El No o CSO pollutant 0 concentrations 0 Yes El No 0 Yes 0 No El Yes 0 No co c.' Receiving water quality ❑ Yes 0 No 0 Yes El No ❑ Yes 0 No CSO frequency ❑ Yes El No 0 Yes ❑ No 0 Yes 0 No Number of storm events 0 Yes ❑ No ❑ Yes ❑No El Yes 0 No 5.6 Provide the following information for each of your CSO outfalls. CSO Outfall Number CSO Outfall Number CSO Outfall Number L co N>- umber of CSO events in N the past year events events events co a Average duration per hours hours hours d event 0 Actual or❑ Estimated 0 Actual or❑ Estimated 0 Actual or 0 Estimated > cu o Average volume per event million gallons million gallons million gallons oo 0 Actual or 0 Estimated 0 Actual or❑ Estimated 0 Actual or 0 Estimated Minimum rainfall causing inches of rainfall inches of rainfall inches of rainfall a CSO event in last year 0 Actual or 0 Estimated 0 Actual or 0 Estimated 0 Actual or 0 Estimated EPA Form 3510-2A(Revised 3-19) Page 11 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 5.7 Provide the information in the table below for each of your CSO outfalls. CSO Outfall Number CSO Outfall Number CSO Outfall Number Receiving water name Name of watershed/ stream system U.S. Soil Conservation ❑ Unknown 0 Unknown ❑Unknown Service 14-digit watershed code '5 (if known) Name of state management/river basin U.S.Geological Survey ❑Unknown ❑Unknown 0 Unknown 8-Digit Hydrologic Unit Code(if known) Description of known water quality impacts on receiving stream by CSO (see instructions for exam files SECTION 6.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d)) 6.1 In Column 1 below,mark the sections of Form 2A that you have completed and are submitting with your application.For each section, specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note that not all applicants are required to provide attachments. Column 1 .` Column 2 ❑ Section 1: Basic Application ❑✓ w/variance request(s) ❑✓ w/additional attachments Information for All Applicants ❑ Section 2:Additional ✓❑ w/topographic map ✓❑ wl process flow diagram Information w/additional attachments ✓❑ wl Table A ✓❑ w/Table D ❑ Section 3: Information on ✓❑ wl Table B ❑✓ w/Table E Effluent Discharges ✓❑ wl Table C ❑✓ w/additional attachments Section 4: Industrial ❑✓ w/SIU and NSCIU attachments ❑ wl Table F 0 Discharges and Hazardous o Wastes ✓❑ wl additional attachments zcs ' Section 5: Combined Sewer ❑ wl CSO map ❑ wl additional attachments ❑ Overflows a ❑ wl CSO system diagram ID Section 6: Checklist and ❑ w/attachments Certification Statement :re 6.2 Certification Statement /certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information,the information submitted is, to the best of my knowledge and belief, true,accurate,and complete.I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name(print or type first and last name) Official title Tonya Mann Utilities Director Signature Date signed EPA Form 3510-2A(Revised 3-19) Page 12 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham 001 0MB No.2040-0004 TABLE A. EFFLUENT PARAMETERS FOR ALL POTWS Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL Pollutant Number of Value Units Value Units Methods (include units) Samples Biochemical oxygen demand o ML o BOD5 or❑CBOD5 17.9 Mg/I 6.9 Mg/I 104 5210 B-2011 2 o MDL resort one o ML Fecal coliform 2419.6 #/100m1 30.8 #/100m1 106 IDEXX Colilert 18(MPN) 1 o MDL Design flow rate 6.3 MGD 1.9 MGD 366 pH(minimum) 6.9 SU pH (maximum) 7.4 SU Temperature(winter) 21 Celsius 13.8 Celsius 101 Temperature(summer) 26 Celsius 22 Celsius 150 El ML Total suspended solids(TSS) 20.8 Mg/I 6.7 Mg/I 102 2540 D-2011 2.5 o MDL 1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2A(Revised 3-19) Page 13 This page intentionally left blank. EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham 001 OMB No.2040-0004 TABLE B. EFFLUENT PARAMETERS FOR ALL POTWS WITH A FLOW EQUAL TO OR GREATER THAN 0.1 MGD Maximum Daily Discharge Average Daily Discharge Pollutant Analytical ML or MDL Value Units Value Units Number of Method' (include units) Samples o ML Ammonia(as N) 14.8 Mg/I 2.9 Mg/I 106 4500 NH3 D-2011 0.10 0 MDL Chlorine ❑ML (total residual,TRC)2 <20 ug/I <20 ug/I 263 4500 CI G-2011 20 p MDL 0 ML Dissolved oxygen 4.8 Mg/I 1.0 Mg/I 361 4500 0 G-2011 0.10 2 MDL 0 ML Nitrate/nitrite 17.7 Mg/I 1.4 Mg/I 51 EPA 353.2 0.10 ID MDL 0 ML Kjeldahl nitrogen 12.5 Mg/I 3.9 Mg/I 52 EPA 351.1 0.20 I]MDL • 0 ML Oil and grease <5 Mg/I <5 Mg/I 3 EPA 1664A 5.00 E3 MDL 0 ML Phosphorus 3.3 Mg/I 0.4 Mg/I 105 4500 P E-2011 0.10 0 MDL 0 ML Total dissolved solids 1320 Mg/I 898.4 Mg/I 5 SM 2540 10.0 E MDL ' Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). 2 Facilities that do not use chlorine for disinfection,do not use chlorine elsewhere in the treatment process,and have no reasonable potential to discharge chlorine in their effluent are not required to report data for chlorine. EPA Form 3510-2A(Revised 3-19) Page 15 This page intentionally left blank. EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham 001 OMB No.2040-0004 TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL Pollutant Number of Method1 (include units) Value Units Value Units Samples Metals,Cyanide,and Total Phenols o ML Hardness(as CaCO3) 68.0 Mg/I 62.7 Mg/I 3 SM 234C 0.662 E MDL Antimony,total recoverable <0.025 Mg/I <0.025 Mg/I 3 EPA 200.8 0.025 E MDL 0 ML Arsenic,total recoverable <0.01 Mg/I <0.01 Mg/I 3 EPA 200.8 0.010 E MDL 0 ML Beryllium,total recoverable <0.005 Mg/I <0.005 Mg/I 3 EPA 200.8 0.005 E MDL 0 ML Cadmium,total recoverable <0.002 Mg/I <0.002 Mg/I 3 EPA 200.8 0.002 MDL 0 ML Chromium,total recoverable <0.005 Mg/I <0.005 Mg/I 3 EPA 200.8 0.005 E MDL ML Copper,total recoverable 0.018 Mg/I 0.010 Mg/I 3 EPA 200.8 0.002 2 MDL 0 ML Lead,total recoverable <0.01 Mg/I <0.01 Mg/I 3 EPA 200.8 0.010LI MDL 0 ML Mercury,total recoverable 7.51 ng/I 3.47 ng/I 5 EPA 1631 1.000 E MDL 0 ML Nickel,total recoverable <0.01 Mg/I <0.01 Mg/I 3 EPA 200.8 0.010 0 MDL Selenium,total recoverable <0.01 Mg/I <0.01 Mg/I 3 EPA 200.8 0.010 E MDL 0 ML Silver,total recoverable <0.005 Mg/I <0.005 Mg/I 3 EPA 200.8 0.005 E MDL 0 ML Thallium,total recoverable <0.02 Mg/I <0.02 Mg/I 3 EPA 200.8 0.020 E MDL 0 ML Zinc,total recoverable 0.079 Mg/I 0.072 Mg/I 3 EPA 2008 0.010 MDL 0 ML Cyanide <0.005 Mg/I <0.005 Mg/I 3 EPA 335.4 0.005 E MDL 0 ML Total phenolic compounds 0.047 Mg/I .0.26 Mg/I 3 EPA 420.1 0.010 E MDL Volatile Organic Compounds o ML Acrolein <50 µg/I <50 µg/I 3 EPA 624.1 0.050 E MDL 0 ML Acrylonitrile <10 µg/I <10 µg/I 3 EPA 624.1 0.010 E MDL Benzene <1.0 µg/I <1.0 µg/1 3 EPA 624.1 0.001 ❑ML E MDL 0 ML Bromoform <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 E MDL EPA Form 3510-2A(Revised 3-19) Page 17 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham 001 OMB No.2040-0004 TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS __ Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL Pollutant Value Units Value Units Number of Method' (include units) Samples Carbon tetrachloride <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML O MDL Chlorobenzene <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML MDL Chlorodibromomethane 4.83 µg/I 3.54 µg/I 3 EPA 624.1 0.001 ❑ML ®MDL Chloroethane <5.0 µg/I <5.0 µg/I 3 EPA 624.1 0.005 0 ML O MDL 2-chloroethylvinyl ether <5.0 µg/I <5.0 µg/I 3 EPA 624.1 0.005 0 ML O MDL Chloroform 7.23 µg/I 4.46 µg/I 3 EPA 624.1 0.001 0 ML O MDL O Dichlorobromomethane 7.99 µg/I 4.81 µg/I 3 EPA 624.1 0.001 ML O MDL 1,1-dichloroethane <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 0 ML O MDL _ 1,2-dichloroethane <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML O MDL trans-1,2-dichloroethylene <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML O MDL 0 ML 1,1-dichloroethylene <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 MDL 1,2-dichloropropane <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 O MDL 1,3-dichloropropylene <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 EI ML O MDL Ethylbenzene <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML 2 MDL 0 ML Methyl bromide <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.005 O MDL Methyl chloride <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.005 ❑ML 2 MDL 0 ML Methylene chloride <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 O MDL 1,1,2,2-tetrachloroethane <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML O MDL Tetrachloroethylene <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML 0 MDL Toluene <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 0 ML O MDL 1,1,1-trichloroethane <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML O MDL 1,1,2-trichloroethane <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML O MDL EPA Form 3510-2A(Revised 3-19) Page 18 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham 001 0MB No.2040-0004 TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL Pollutant Number of Method1 (include units) Value Units Value Units Samples Trichloroethylene <1.0 µg/I <1.0 µg/I 3 EPA 624.1 0.001 ❑ML 0 MDL ML Vinyl chloride <5.0 µg/I <5.0 µg/I 3 EPA 624.1 0.005 0 MDL Acid-Extractable Compounds 0 ML p-chloro-m-cresol <10 µg/I <10 µg/I 3 EPA 625.1 0.010 E MDL 2-chlorophenol <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML 0 MDL 2,4-dichlorophenol <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ML E MDL El 2,4-dimethylphenol <10 µg/I <10 µg/I 3 EPA 625.1 0.050 ML E MDL 4,6-dinitro-o-cresol <50 µg/I <50 µg/I 3 EPA 625.1 0.050 0 ML E MDL 2,4-dinitrophenol <50 µg/I <50 µg/I 3 EPA 625.1 0.050 ❑ML 0 MDL 2-nitrophenol <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML E MDL 4-nitrophenol <50 µg/I <50 µg/I 3 EPA 625.1 0.050 ❑ML E MDL Pentachlorophenol <50 µg/I <50 µg/I 3 EPA 625.1 0.050 0 ML E MDL Phenol <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML 0 MDL 2,4,6-trichlorophenol <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL Base-Neutral Compounds Acenaphthene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 E MDL • Acenaphthylene <i0 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL Anthracene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL Benzidine <50 µg/I <50 µg/I 3 EPA 625.1 0.050 ❑ML E MDL Benzo(a)anthracene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL 0 ML Benzo(a)pyrene <io µg/I <10 µg/I 3 EPA 625.1 0.010 E MDL 3,4-benzofluoranthene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ML 0 MDL EPA Form 3510-2A(Revised 3-19) Page 19 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham 001 OMB No.2040-0004 TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL Pollutant Value Units Value Units Number of Methods (include units) Samples Benzo(ghi)perylene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML 0 MDL Benzo(k)fluoranthene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML 0 MDL Bis(2-chloroethoxy)methane <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML 0 MDL Bis(2-chloroethyl)ether <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML MDL Bis(2-chloroisopropyl)ether <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML O MDL Bis(2-ethylhexyl)phthalate <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML CI MDL 0 ML 4-bromophenyi phenyl ether <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 MDL Butyl benzyl phthalate <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML 0 MDL 2-chloronaphthalene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML 0 MDL 4-chlorophenyl phenyl ether <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML 0 MDL Chrysene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML O MDL di-n-butyl phthalate <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML O MDL di-n-octyl phthalate <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML O MDL Dibenzo(a,h)anthracene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML 0 MDL 1,2-dichlorobenzene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML O MDL 1,3-dichlorobenzene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML 0 MDL 1,4-dichlorobenzene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML 0 MDL 3,3-dichlorobenzidine <10 µg/I <10 µg/I 3 EPA 625.1 0.010 O ML O MDL Diethyl phthalate <10 µg/I <10 µg/I 3 EPA 625.1 0.050 ❑ML O MDL Dimethyl phthalate <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML O MDL 2,4-dinitrotoluene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML O MDL 2,6-dinitrotoluene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML 0 MDL EPA Form 3510-2A(Revised 3-19) Page 20 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham 001 OMB No.2040-0004 TABLE C.EFFLUENT PARAMETERS FOR SELECTED POTWS Maximum Daily Discharge Average Daily Discharge Analytical ML or MDL Pollutant Number of Method1 (include units) Value Units Value Units Samples 1,2-diphenylhydrazine <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL Fluoranthene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL Fluorene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML E MDL Hexachlorobenzene <10 µg/I <10 mil 3 EPA 625.1 0.010 0 ML CI MDL Hexachlorobutadiene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML ❑MDL Hexachlorocyclo-pentadiene <50 µg/I <50 µg/I 3 EPA 625.1 0.050 0 ML E MDL Hexachloroethane <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML 0 MDL Indeno(1,2,3-cd)pyrene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL Isophorone <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL Naphthalene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL Nitrobenzene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 E ML E MDL N-nitrosodi-n-propylamine <10 µg/I <10 µg/I 3 EPA 625.1 0.010 0 ML ®MDL N-nitrosodimethylamine <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL 0 ML N-nitrosodiphenylamine <10 µg/I <10 µg/I 3 EPA 625.1 0.010 E MDL Phenanthrene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL 0 ML Pyrene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 E MDL 1,2,4-trichlorobenzene <10 µg/I <10 µg/I 3 EPA 625.1 0.010 ❑ML E MDL 1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR Chapter I,Subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2A(Revised 3-19) Page 21 This page intentionally left blank. EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 TABLE D.ADDITIONAL POLLUTANTS AS REQUIRED BY NPDES PERMITTING AUTHORITY Maximum Daily Discharge Average Daily Dischar e Pollutant Analytical ML or MDL (list) Value Units Value Units Number of Method1 (include units) Samples ElNo additional sampling is required by NPDES permitting authority. ❑ML ❑MDL ❑ML ❑MDL ❑ML 0 MDL ❑ML 0 MDL 0 ML 0 MDL 0 ML ❑MDL ❑ML ❑MDL ❑ML 0 MDL ❑ML 0 MDL ❑ML 0 MDL ❑ML ❑MDL ❑ML ❑MDL ❑ML ❑MDL 0 ML 0 MDL ❑ML ❑MDL ❑ML ❑MDL ❑ML ❑MDL 1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2A(Revised 3-19) Page 23 This page intentionally left blank. EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 TABLE E. EFFLUENT MONITORING FOR WHOLE EFFLUENT TOXICITY The table provides response space for one whole effluent toxicity sample.Copy the table to report additional test results. Test Information Test Number Test Number Test Number Test species Age at initiation of test Outfall number Date sample collected Date test started Duration Toxicity Test Methods Test method number Manual title Edition number and year of publication Page number(s) Sample Type Check one: E Grab ❑ Grab ❑ Grab ❑ 24-hour composite ❑ 24-hour composite ❑ 24-hour composite Sample Location Check one: ❑ Before Disinfection ❑ Before Disinfection ❑ Before disinfection ❑ After Disinfection ❑ After Disinfection ❑ After disinfection ❑ After Dechlorination ❑ After Dechlorination ❑ After dechlorination Point in Treatment Process Describe the point in the treatment process at which the sample was collected for each test. Toxicity Type Indicate for each test whether the test was ❑ Acute ❑ Acute ❑ Acute performed to asses acute or chronic toxicity, or both.(Check one response.) ❑ Chronic ❑ Chronic ❑ Chronic ❑ Both ❑ Both ❑ Both EPA Form 3510-2A(Revised 3-19) Page 25 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 Cityof Graham OMB No.2040-0004 TABLE E.EFFLUENT MONITORING FOR WHOLE EFFLUENT TOXICITY The table provides response space for one whole effluent toxicity sample.Copy the table to report additional test results. 11111111111111.1 Test Number Test Number Test Number Test Type Indicate the type of test performed.(Check one ❑ Static ❑ Static ❑ Static response.) ❑ Static-renewal ❑ Static-renewal ❑ Static-renewal ❑ Flow-through ❑ Flow-through ❑ Flow-through Source of Dilution Water Indicate the source of dilution water.(Check ❑ Laboratory water ❑ Laboratory water ❑ Laboratory water one response.) ❑ Receiving water 0 Receiving water 0 Receiving water If laboratory water,specify type. If receiving water,specify source. Type of Dilution Water Indicate the type of dilution water. If salt ❑ Fresh water 0 Fresh water 0 Fresh water water,specify"natural"or type of artificial sea salts or brine used. ElSalt water(specify) 0 Salt water(specify) ElSalt water(specify) Percentage Effluent Used Specify the percentage effluent used for all concentrations in the test series. Parameters Tested Check the parameters tested. ❑ pH 0 Ammonia ❑ pH 0 Ammonia ❑ pH ❑ Ammonia ❑ Salinity ❑ Dissolved oxygen 0 Salinity ❑ Dissolved oxygen 0 Salinity 0 Dissolved oxygen ❑ Temperature ❑ Temperature ❑ Temperature Acute Test Results Percent survival in 100%effluent % LCso 95%confidence interval Control percent survival % % % EPA Form 3510-2A(Revised 3-19) Page 26 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 TABLE E.EFFLUENT MONITORING FOR WHOLE EFFLUENT TOXICITY The table provides response space for one whole effluent toxicity sample. Copy the table to report additional test results. Test Number Test Number Test Number Acute Test Results Continued Other(describe) Chronic Test Results NOEC I C25 Control percent survival % Other(describe) Quality Control/Quality Assurance Is reference toxicant data available? ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No Was reference toxicant test within acceptable bounds? ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes El No What date was reference toxicant test run (MM/DDIYYYY)? Other(describe) EPA Form 3510-2A(Revised 3-19) Page 27 This page intentionally left blank. EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 TABLE F.INDUSTRIAL DISCHARGE INFORMATION Response space is provided for three SIUs.Copy the table to report information for additional Sills. SIU 1 SIU 2 SIU 3 Name of SIU Cintas Corporation Luxfer Gas Cylinders Novaflex Hose Corp. Mailing address(street or P.O.box) 610 Woody Drive 235 Riverbend Rd. 449 Trollingwood Road City,state,and ZIP code Graham, NC 27253 Graham,NC 27253 Haw River,NC 27258 Description of all industrial processes that affect Industrial Laundry Gas Cylinders,Aluminum Forming Rubber Manufacturing or contribute to the discharge. List the principal products and raw materials that Product: Cleaning Uniforms Product: Gas Cylinders Product: Rubber and Plastic affect or contribute to the SIU's discharge. Raw Material: Bleach,Sulfuric Acid, Raw Material: Metals,Caustic,Lubricants Hose/Assembled and Coupled Hose Detergent,Clay Solution,Ferric,Caustic, and Powder Paint Raw Material: Natural and Synthetic Surfactants Rubber and Additives,Thermoplastic Resins Indicate the average daily volume of wastewater discharged by the SIU.* 57,000 gpd 43,300 gpd 9,820 gpd How much of the average daily volume is attributable to process flow?+ 52,000 gpd 36,000 gpd 6,000 gpd How much of the average daily volume is attributable to non-process flow?+ 2,500 gpd 2,10o gpd 3,400 gpd Is the SIU subject to local limits? 1 ElYes El No El Yes El No El Yes El No Is the SIU subject to categorical standards? El Yes El No El Yes El No El Yes ❑ No * Source of data from The City of Graham's Pretreatment Annual Report for January 1, 2019 (Appendix D). + Source of data from the most recent pretreatment application (2016). EPA Form 3510-2A(Revised 3-19) Page 29 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 TABLE F.INDUSTRIAL DISCHARGE INFORMATION Response space is provided for three Sills.Copy the table to report information for additional Sills. SIU 1 SIU 2 SIU 3 Under what categories and subcategories is the NA 40 CFR Part 467.36-Subpart C 40 CFR 428-Subpart F SIU subject? Rubber Manufacturing Has the POTW experienced problems(e.g., upsets, pass-through interferences)in the past 4.5 ❑ Yes 0 No ❑ Yes 0 No ❑ Yes E No years that are attributable to the SIU? If yes,describe. NA NA NA EPA Form 3510-2A(Revised 3-19) Page 30 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 Cityof Graham OMB No.2040-0004 TABLE F.INDUSTRIAL DISCHARGE INFORMATION Response space is provided for three Sills.Copy the table to report information for additional SIUs. SIU 4 SIU 5 SIU Name of SIU Prescient Company Inc. Stericycle Inc. Mailing address(street or P.O.box) 2125 Senator Ralph Scott Parkway 1168 Porter Ave. City,state,and ZIP code Mebane,NC 27302 Haw River,NC 27258 Description of all industrial processes that affect Metal Finisher Medical Waste or contribute to the discharge. List the principal products and raw materials that Product: Light Gauge Steel Frames,Trusses, Product: Ash From Medical Waste affect or contribute to the SIU's discharge. Building Columns and Beams Incineration Raw Material: Dubois GF Phos.427, Dubois Raw Material: Muriatic Acid,Ferric Depress-Max, Dubois Secure Seal,Powder Chloride,Caustic Soda,Ammonia,Nitric Paint Acid Indicate the average daily volume of wastewater discharged by the SIU.* 1,10o gpd 14,600 gpd gpd How much of the average daily volume is attributable to process flow?+ 1,soo gpd 23,000 gpd gpd How much of the average daily volume is attributable to non-process flow?+ 1,050 gpd 1,615 gpd gpd Is the SIU subject to local limits? ❑r Yes ❑ No CI Yes ❑ No ❑ Yes ❑ No Is the SIU subject to categorical standards? CI Yes El No ❑ Yes CI No ❑ Yes ❑ No * Source of data from The City of Graham's Pretreatment Annual Report for January 1, 2019 (Appendix D). + Source of data from the most recent pretreatment application (2016). EPA Form 3510-2A(Revised 3-19) Page 29 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000761890 NC0021211 City of Graham OMB No.2040-0004 TABLE F.INDUSTRIAL DISCHARGE INFORMATION Response space is provided for three Sills.Copy the table to report information for additional Sills. SIU 4 SIU 5 SIU Under what categories and subcategories is the 40 CFR 433.17- Metal Finishing NA SIU subject? Has the POTW experienced problems(e.g., upsets, pass-through interferences)in the past 4.5 ❑ Yes 0 No ❑ Yes 0 No ❑ Yes ❑ No years that are attributable to the SIU? If yes,describe. NA NA EPA Form 3510-2A(Revised 3-19) Page 30 Appendix A: Figures � At lk _i t • io I- I 1- 41 , * li. 11 . *41* ' -" It 'I..--46. - \ ft..4 tr * • • % 0 .40, '7;4' t lw I \ 'ff * , b. lip i . ♦ 1 • k \ , 2 I 1 * : , *"%41' ' , ,. ao. • RINit , ..- 4 zSPe6a,1%.,, , ._ - Ri • ' *C St 144111S10 .".• -<:.),(1.... sue.- \ b, .00" • sh. ,/,,,._ .,..-1,,, s 1' j. -.. 4` ' ?i b ,a. 36°02'44" 79° 22'06" g �µ sr It* to * Jr , F 4 Legend # i • NPDES Discharge Location Influent Gravity Main 1 oi� nght 2013 National Geographic Society,i-cubed .,.._.".,,� Effluent Pipeline I GWVI/TP Boundary Area SCALE I-, I Figure 1 0 250 500 GRAHAM GWWTP Boundary Area with Feet L Influent Effluent Graham Pipeline 1 inch = 500 feet Wastewater e City of GrahamTreatm, NorthntPlant CarolinaExpansion Screen and Grit Removal Aeration Basins Final Settling Tanks Sand Filtration Disinfection Facility IChloriratian/Dec lorin=1or; 1.95MGD ' 2.4 39MGD q/ il, 11.95MGD 1 9:\ GDr 0 =4 °'' 0 0 2.15 MGD 1_o5NSGD 1.95MGD I.9:MGD r isi Influent Pump Station Primary Settling Tanks RAS/WAS Pump Station Post-Aeration —, —\ lOriginal Secondary Clarifiers; � 11 `� 1 9:MGD 1.95 MGD ,W rnmio t. 0 MGD 1.95 MGD Land Application Sludge Truck Loading Station Sludge Storage Aerobic Digesters Haw River 111,6, . °6 *. * >,,,,„ A , :.: :,,.,, Blue =Liquid Train Red=Solid Train Figure 2: GWWTP Process Flow Diagram Aeration Basins Maintenance . ,, Building ' a ,, ci Primary Settling Tanks FST 1 and 2 Return Activated Sludge - 7 Pump Station „ „` ," --'=- - ..'> .-,..- ,s. ina ett ing an s , die { w 1 & �7. • i - Digester#3 FST 3 and4 Return v ,,�, F--- _ ' , - ! Activated Sludge e-` • , Main Office&lab Pump Station w 4 i -- _ II .,- — Chlorination& Influent Pump Station and Sludge Sludge Thickening HoldingTank De-chlorination Screening/Grit Facility Storage Basin Sand Filter rt -lYV_ e t* f F. : t _ „, ._ ' 1 / . :: f Final Ma Aerator Truck Filling Lime Digester High Rate Filter ,__, _ „, Station Stabilization 1&2 (Out of Service) ; ', , Tank , , Figure 3: Existing GWWTP Facility Layout 5-Stage BNR Prop.. Modifications/Upgrades Process Liquid Train InPuent pumping and No upgrades necessary _ - prefiminarr treatment '" ,^ • Equalization maybe implemented based on the Ci s " ^- E4uatization ,vet weather operational strategy ry •]'•' _ jt• . ,t AB irk Carbon "r Sputter Box Primary Settling Tanks v Out of sere Facility ' • Add 1 25 MG of volume �i • Convert to four(4)5-stage BNR tanks Blower '� Aeration Basins • Remove surface aerators-Install blowers and fine Facility Eiectrtcal bubble diffusers Mp, s B s • RAS piping modifications l r Chemical Facifities • New supplemental carbon facility ,,,•,y• • No modifications to existing PACI facility • New MISS distribution box for SC 3 and 4 1.5 MG Sludge - •- 12111211 Re-aeration Final Settling Tanks • Install smallRAS pumps 1 Storage • Parallel effluent tine Parsttal Flume • New Parshal florae Parallel 24 " Eflbenl Filers •• New effluent raters FST Line till Chlorine Contact • NrN chlorine contact tanks • Modify existing chlorine and sodium bisufite storage AE Digester ®,,Y ACT Tanks facility for additional capacity e dtr f Blowers -et• ` e ,, • Instal now re-aeration faulty(cascade aeration or . '- ^ 1 .1 Re-Aeration fine bubble diffusers) 2.5 MG AE ✓ • New effluent One from re-aeration to effluent manhole v x� S" I Digestion ea �+i i / Solid.Train 1 Y e W Fad tY .3CJ Effluent / - Aerobic Digestion • Add 2.6 MG of aerobic.digestion volume wdh fine Line bubble diffusers and blowers • Convert existing aerobic<F aster to sludge storage for jil Rehab/Modify Facility . Sludge Storage a sludge storage vobmeoflSMG • Install new moans system in Platte'No 3 Figure 4: GWWTP Proposed Expansion to 5 MGD. Appendix B: Second Species/WET Test Reports for 2016-2019 Effluent Toxicity Report Form-Chronic Fathead Minnow Multi-Concentration Test Date:12/16/2016 1 Facility: City of Graham NPDES:NC0021211 Pipe#_ 001 County: Alamance Labors ory: Meritech,Inc. / Comments x ( / / Signature of Operator in Resp)onsib e�Charge x fe /v% ?; �._� �f . Signature of Laboratory Supervisor MAIL ORIGINAL TO: Water Sciences Section Aquatic Toxicology Branch Division of Water Quality 1623 Mail Service Center Raleigh,NC 27699-1623 Test Initiation Date/Time 12/6/2016 2.40 PM Avg WVSurv.Control 0.780 Test Organisms Eff. Repl. 1 2 3 4 1 Cultured In-House Control Surviving# 10 9 10 10 %Survival 97.5 1% Outside Supplier Original# 10 10 10 10 WVoriginal(mg) 0.864 0.732 0.791 0.653 Avg Wt(mg) 0.760 Hatch Date: 12/5/16 3.5 Surviving# 10 10 10 10 %Survival 100.0 Hatch Time' 3 00PM CT Original# 10 10 10 10 Wt/original(mg) 0.684 0.796 0.757 0.723 Avg Wt(mg) 0.740 7 Surviving# 9 9 10 10 %Survival 95.0 Original# 10 10 10 10 WVoriginal(mg) 0.719 0.780 0.784 0.793 Avg Wt(mg) 0.769 14 Surviving# 10 8 10 10 %Survival 95.0 Original# 10 10 10 10 Wt/original(mg) 0.711 0.705 0.761 0.882 Avg Wt(mg) 0.765 21 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 Wt/original(mg) 0.837 0.772 0.875 0.829 Avg Wt(mg) 0.828 28 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 Wt/original(mg) 0.802 0.885 0.821 0.809 Avg Wt(mg) 0.829 Water Quality Data Day Control 0 1 2 3 4 5 6 pH(SU)Init/Fin 8.07 / 7.79 8.15 / 7.60 8.13 / 8.08 8.21 / 8.04 8 16 / 8.08 8 14 / 7.85 8.13 / 7.75 DO(mg/L) InitFin 7.66 / 6.75 7.91 7 5.90 7.92 / 7.49 7.92 / 7.89 8.06 / 7.75 8.02 / 7.08 7.86 / 6.22 Temp(C)Init/Fin 24.5 / 25.2 25.5 / 24.9 24.9 I 25.3 25.4 / 25.9 25.7 / 24.8 25.3 / 25.5 24.9 / 25.1 High Concentration 0 1 2 3 4 5 6 pH(SU)Ina/Fin 7.80 I 7.77 7.82 I 7.45 7.83 / 8.00 7.95 / 8 16 8.09 / 8.15 8.05 / 7.81 7.90 / 7.63 DO(mg/L) Init/Fin 7.94 I 6.83 7.91 / 5.17 7.83 / 7.57 8.07 I 7.95 8.11 / 7.55 7.98 / 7.10 7.92 / 5.93 Temp(C)InitFin 24.8 / 25.3 25 9 / 25.5 25.7 I 24.9 25.1 / 25.4 25.5 / 24.3 25.2 / 25.7 24.6 / 25.0 Sample 1 2 3 Survival Growth Overall Result Collection Start Date 12/5/2016 12/7/2016 12/8/2016 Normal 1'I Fl ChV >28 Grab Horn.Var. f F) Composite(Duration) 24.00 24.00 24.00 NOEC 28 28 Hardness(mg/L) 56.00 56.00 64.00 LOEC >28 >28 Alkalinity(mg/L) 63.00 62.00 59.50 ChV >28 >28 Conductivity(umhos/cm) 2220 1781 1839 Method Steel's Dunnett's Chlorine(mg/L) <0.1 <0.1 <0.1 Temp.at Receipt(°C) 2.2 1.8 0.6 Stats Survival Growth Conc. Critical Calculated Critical Calculated Dilution H2O Batch# 1098 1099 1100 1101 1102 3.5 10 20 2.41 0,4734 ' Hardness(mg/L) 44 48 46 42 44 7 10 16 2.41 -0.2130 Alkalinity(mg/L) 51 59 59 50 58 14 10 17.5 2.41 -0.1124 Conductivity(umhos/cm) 192 207 200 189 _ 211 21 10 20 2.41 -1.6154 28 10 20 2.41 -1.6391 DWQ Form AT-5(1/04) Effluent Toxicity Report Form-Chronic Fathead Minnow Multi-Concentration Test Date:3/23/2017 Facility: Graham WWTP NPDES#NC00 21211 Pipe#: 001 County: Alamance Laboratory: Meritech, Inc. Comments' x c.... ate,. .'i, iC Signature of Operator in Responsible Charge x - Signature of Laboratory Supervisor �--- MAIL ORIGINAL TO: Water Sciences Section Aquatic Toxicology Branch Division of Water Resources 1621 Mail Service Center Raleigh,N.C.27699-1621 Test Initiation Date/Time 3/14/2017 4:31 PM Avg Wt/Surv.Control 0.693 Test Organisms % Eff. Repl. 1 2 3 4 f- Cultured In-House Control Surviving# 10 9 9 9 %Survival 92.5 F Outside Supplier Original# 10 10 10 10 Wt/original(mg) 0.797 0.540 0.626 0.611 Avg Wt(mg)[ 0.644 Hatch Date: 3/13/17 3.5 Surviving# 10 10 10 9 %Survival 97.5 Hatch Time: 3:00 pm CT Original# 10 10 10 10 WUoriginal(mg) 0.604 0.625 0.657 0.623 Avg Wt(mg) 0.627 7 Surviving# 10 9 10 10 %Survival 97.5 Original# 10 10 10 10 WUoriginal(mg) 0.657 0.669 0.672 0.691 Avg Wt(mg) 0.672 14 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 Wt/original(mg) 0.983 0.731 0.959 0.663 Avg Wt(mg) 0.834 21 Surviving# 9 10 9 10 %Survival 95.0 Original# 10 10 10 10 ^ WUoriginal(mg) 0.652 0.660 0.684 0.757 Avg Wt(mg) 0.688 28 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 WUoriginal(mg) 0.712 0.790 0.759 0.802 Avg Wt(mg) 0.766 Water Quality Data Day Control 0 1 2 3 4 5 6 pH(SU)IniUFin 8.13 / 8.00 8.17 / 7.85 8.17 / 7.98 8.22 / 8.12 8.23 / 7.93 8.18 / 7.96 8.17 / 7.57 DO(mg/L) Init/Fin 8.00 / 7.33 7.83 / 6.95 7.87 / 7.23 7.66 / 7.57 7.77 / 7.25 8.03 / 7.30 7.78 / 6.46 Temp(C)Init/Fin 24.4 / 25.1 24.0 / 24.8 25.1 / 25.6 24.6 / 25.9 24.6 / 24.6 24.7 / 24.2 25.8 / 25.4 High Concentration 0 1 2 3 4 5 6 pH(SU)IniUFin 7.81 / 7.95 7.99 / 7.84 7.79 / 7.88 7.96 / 7.91 8.00 / 7.77 7.88 / 7.92 7.95 / 7.53 DO(mg/L) IniUFin 8.13 ; 7.40 7.86 / 6.98 7.97 / 7.22 7.74 / 7.51 7.78 / 7.07 7.76 / 7.32 7.73 / 6.03 Temp(C)Init/Fin 24.9 / 25.1 24.6 / 24.6 25.2 / 24.7 25.0 / 25.9 25.0 / 24.7 24.9 / 25.3 25.5 / 25.8 Sample 1 2 3 Survival Growth Overall Result Collection Start Date 3/13.'2017 3/15/2017 3/16/2017 Normal YES irI ChV >28 Grab Horn.Var. IC"] NO Composite(Duration) 24.2 23.9 25.1 NOEC 28 28 Hardness(mg/L) 60 60 62 LOEC >28 >28 Alkalinity(mg/L) 48 37 38 ChV >28 >28 Conductivity(umhos/cm) 1549 1592 1647 Method Steel's Steers Chlorine(mg/L) <0.1 <0.1 <0.1 . Temp.at Receipt(°C) 1.8 0.7 0.9 Stats Survival Growth Conc. Critical Calculated Critical Calculated Dilution H2O Batch# 1135 1136 1137 1138 3.5 10 22 10 18.0 Hardness(mg/L) 42 44 42 46 7 10 22 10 22.0 Alkalinity(mg/L) 60 54 53 511 14 10 24 10 24.0 Conductivity(umhos/cm) 217 213 220 211 21 10 20 10 22.0 28 10 24 10 23.0 DWQ Form AT-5(1/04) Effluent Toxicity Report Form-Chronic Fathead Minnow Multi-Concentration Test Date:6/28/2018 Facility: Graham WWTP NPDES#NC00 21211 Pipe#: 001 County: Alamance Laboratory: Meritech, Inc.. Comments! x Z? 7 /� Signature-of4Respansible Charge Signature of Laboratory Supervisor MAIL ORIGINAL TO: Water Sciences Section Aquatic"hoxicology Branch Division of Water Resources 1621 Mail Service Center Raleigh,N.C.27699-1621 Test Initiation Date/Time 6/19/2018 2:30 PM Avg Wt/Surv. Control 0.769 Test Organisms Eff. Repl. 1 2 3 4 Cultured In-House Control Surviving# 10 10 10 10 %Survival 100.0 Outside Supplier Original# 10 10 10 10 Wt/original(mg) 0.840 0.782 0.762 0.690 Avg Wt(mg) 0.769 Hatch Date: 6/18/18 3.5 Surviving# 10 10 10 10 %Survival 100.0 Hatch Time: 3:00 pm CT Original# 10 10 10 10 WUoriginal(mg) 0.754 0.789 0.618 0.726 Avg Wt(mg) 0.722 7 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 Wt/original(mg) 0.822 0.800 0.843 0.754 Avg Wt(mg) 0.805 14 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 Wt/original(mg) 0.843 0.766 0.702 0.795 Avg Wt(mg) 0.777 21 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 Wt/original(mg) 0.879 0.881 0.816 0.920 Avg Wt(mg) 0.874 28 Surviving# 10 9 10 10 %Survival 97.5 Original# 10 10 10 10 Wt/original(mg) 0.851 0.784 0.905 0.893 Avg Wt(mg) 0.858 Water Quality Data Day Control 0 1 2 3 4 5 6 pH(SU)Init/Fin 8.19 / 7.94 8.19 / 7.94 8.18 / 7.85 8.17 / 8.24 8.25 / 8.19 8.28 / 7.87 8.23 / 7.82 DO(mg/L) Init/Fin 7.66 / 7.37 7.87 / 7.27 7.89 / 6.87 7.74 / 7.87 8.02 / 8.04 8.11 / 6.92 7.74 / 7.10 Temp(C)Init/Fin 25.7 / 24.4 24.8 / 25.6 24.7 / 25.3 24.7 / 25.9 24.9 / 24.1 24.1 / 25.5 24.3 / 25.0 High Concentration 0 1 2 3 4 5 6 pH(SU)Init/Fin 7.84 / 7.85 7.91 / 7.83 7.92 / 7.81 7.91 / 8.04 8.20 / 8.15 8.14 / 7.84 8.00 / 7.96 DO(mg/L) !nit/Fin 7.73 / 7.40 7.81 / 7.16 8.00 / 6.78 7.74 / 7.75 7.79 / 8.00 8.15 / 7.05 7.87 / 7.47 Temp(C)IniUFin 25.3 / 24.9 24.9 / 25.0 24.9 / 25.5 24.9 / 25.3 24.7 / 25.0 24.9 / 24.5 24.7 / 25.0 Sample 1 2 3 Survival Growth Overall Result Collection Start Date 6/18/2018 6/20/2018 6/21/2018 Normal rI FI ChV >28 Grab Hom.Var. ri F Composite(Duration) 24.3 24.1 23.9 NOEC 28 28 Hardness(mg/L) 64 62 70 LOEC >28 >28 Alkalinity(mg/L) 44 52 51 ChV >28 >28 Conductivity(umhos/cm) 1791 1803 1822 Method Steel's Dunnett's Chlorine(mg/L) <0.1 <0.1 <0.1 Temp. at Receipt(°C) 1.6 1.6 1.4 Stats Survival Growth Conc. Critical Calculated Critical Calculated Dilution H2O Batch# 1281 1282 1283 1284 3.5 10 18 2.41 _ 1.1734 Hardness(mg/L) 42 42 46 42 7 10 18 2.41 -0.9099 Alkalinity(mg/L) 50 52 53 53 14 10 18 2.41 -0.2008 Conductivity(umhos/cm) 196 194 200 206 21 10 18 2.41 -2.6481 28 10 16 2.41 -2.2528 Effluent Toxicity Report Form-Chronic Fathead Minnow Multi-Concentration Test Date:9/19/2019 Facility. Graham WWTP NPDES#NCO() 21211 Pipe#: 001 County: Alamance Laboratory: Meritech, lnc. { Comments' x: ,_-/ILC'C4',. / /li,/' Signature of Operator in Responsible Charge Signature of Laboratory Supervisor MAIL ORIGIN.A1.TO: Water Sciences Section Aquatic'Toxicology Branch Division of Water Resources 1621 Mail Service Center Raleigh,N.C.27699-1621 Test Initiation Date/Time 9/10/2019 4:49 PM Avg WUSurv.Control 0.539 Test Organisms %Eff. Rep!. 1 2 3 4 C" Cultured In-House Control Surviving# 10 10 10 10 %Survival 100.0 17 Outside Supplier Original# 10 10 10 10 WUoriginal(mg) 0.491 0.462 0.610 0.591 Avg Wt(mg) 0.539 Hatch Date: 9/9/19 3.5 Surviving# 10 10 10 10 %Survival 100.0 Hatch Time: 3:00 pm CT Original# 10 10 10 10 Wt/original(mg) 0.571 0.588 0.543 0.574 Avg Wt(mg) 0.569 7 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 Wt/original(mg) 0.494 0.528 0.569 0.665 Avg Wt(mg) 0.564 14 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 WUoriginal(mg) 0.646 0.500 0.515 0.633 Avg Wt(mg) 0.574 21 Surviving# 9 10 10 10 %Survival 97.5 Original# 10 10 10 10 Wt/original(mg) 0.518 0.548 0.527 0.597 Avg Wt(mg) 0.548 28 Surviving# 10 10 10 10 %Survival 100.0 Original# 10 10 10 10 Wt/original(mg) 0.504 0.594 0.443 0.572 Avg Wt(mg) 0.528 Water Quality Data Day Control 0 1 2 3 4 5 6 pH(SU)Init/Fin 7.74 / 7.65 7.89 / 7.60 7.72 I 7.67 7.89 / 7.85 7.95 i 7.94 7.91 / 7.65 7.93 / 7.64 DO(mg/L) Init/Fin 7.86 / 7.75 7.80 / 6.89 7.53 / 7.25 7.72 / 7.88 7.97 / 7.83 7.83 / 7.36 7.75 / 6.96 Temp(C)!nit/Fin 24.7 / 24.5 24.6 / 24.5 24.5 I 24.5 24.1 / 24.3 24.1 / 24.4 24.8 / 24.3 24.5 / 24.4 High Concentration 0 1 2 3 4 5 6 pH(SU)Init./Fin 7.84 / 7.93 7.94 / 7.72 7.80 17.85 7.95 / 8.05 8.14 / 8.08 8.11 / 7.86 7.96 / 7.76 DO(mg/L) Init/Fin 7.94 / 7.69 7.87 / 6.76 7.67 17.16 7.74 / 7.85 8.05 / 7.67 7.93 / 7.37 7.74 / 6.80 . Temp(C)InitFin 24.8 / 24.3 24.3 / 24.3 24.8 / 24.9 24.2 / 24.8 24.8 / 24.1 24.3 / 24.4 25.0 / 24.3 Sample 1 2 3 Survival Growth Overall Result Collection Start Date 9/9/2019 9/11/2019 9/12/2019 Normal ri Ft ChV >28 Grab Hom.Var. 1-1 Fi Composite(Duration) 24.1 23.8 24.1 NOEC 28 28 Hardness(mg/L) 68 76 80 LOEC >28 >28 Alkalinity(mg/L) 122 135 133 ChV >28 >28 Conductivity(umhoslcm) 2300 2940 2670 Method Steel's Dunnet's Chlorine(mg/L) <0.1 <0.1 <0.1 Temp.at Receipt(`C) 2.5 2.0 1.2 Stats Survival Growth Conc. Critical Calculated Critical Calculated Dilution H2O Batch# 1436 1437 1438 3.5 10 18 2.41 -0.6971 Hardness(mglL) 50 48 46 7 10 18 2.41 -0.5828 Alkalinity(mglL) 34 32 30 14 10 18 2.41 -0.7999 Conductivity(umhos/cm) 171 164 170 21 10 16 2.41 -0.2057 28 10 18 2.41 0.2343 Appendix C: Effluent Toxicity Reports from 2019-2020 Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/12/19 Facility: CITY OF GRAHAM WWTP NPDES#: NC0021211 Pipe#: 001 County: ALAMANCE Laboratory r�rmiGt: MERITECH LABS, INC. .__/_ //�1//// Comments: x Signature� oft Oper for in Responsible Charge X " .r77 6-a ._..._ Signature of Laboratory Supervisor * PASSED: -15.58% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -2.908 Tabular t = 2 .508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -15.58 % Mortality Avg.Reprod. # Young Produced 20 24 15 15 22 18 22 18 18 17 23 19 0. 00 19.25 Control Control Adult (L) ive (D) ead L L L L L L L L L L L L 0.00 22.25 Treatment 2 Treatment 2 Effluent %: 14% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 15.525% PASS FAIL # Young Produced 21 21 24 21 19 21 22 26 21 24 23 24 % control orgs X producing 3rd brood Check One Adult (L) ive (D) ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 12/04/19 Control 8.12 8.03 7.95 7.92 8.02 7.93 Collection (Start) Date Sample 1: 12/02/19 Sample 2: 12/04/19 Treatment 2 8.01 8.02 7.86 8 .07 7. 98 8.04 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24.4 hrs L A A r d r d r d U M M 1 t t t Sample 2 X 23 . 1 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness (mg/1) 45 Control 7.86 7.59 7.60 7.42 7.65 7.48 Spec. Cond. (pmhos) 160 1130 1642 Treatment 2 7.87 7.56 7.64 7.47 7.66 7.52 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt (°C) 2.4 2 .8 (Mortality expressed as %, combining replicates) Note: Please % % % % % % % % % % Concentration Complete This Section Also % % % % % % % % % Mortality a % start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit % -- % Spearman Karber _ Other - High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/12/20 Facility: CITY OF GRAHAM WWTP NPDES#: NC0021211 Pipe#: 001 County: ALAMANCE Laboratory Performing T t: MERITECH LABS, INC. X IW �v, . ����ii�� Comments - Si(/Ignat6"ar_e of Operat in Rponsible Charge _ Signature of Laboratory Supervisor * PASSED: -3 .14% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -0.949 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -3 .14 % Mortality Avg.Reprod. # Young Produced 22 20 18 24 20 22 24 23 23 20 21 18 0.00 21.25 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 21.92 Treatment 2 Treatment 2 Effluent %: 14% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 9.856% PASS FAIL # Young Produced 23 23 22 22 21 23 22 21 20 22 24 20 % control orgs X producing 3rd brood Check One Adult (L) ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 03/04/20 Control 8.15 7.66 7.85 7.59 7.67 7.80 Collection (Start) Date Sample 1: 03/02/20 Sample 2: 03/04/20 Treatment 2 7.84 7.90 7.88 7.92 7.84 8.02 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24.0 hrs L A A r d r d r d U M M t t t Sample 2 X 23 .6 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness (mg/1) 42 Control 7.87 7.51 7.80 7.58 7.98 7.42 Spec. Cond. (pmhos) 134 1314 1331 Treatment 2 7.98 7.53 7.75 7.88 8 .02 7.37 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 3 .0 2.7 (Mortality expressed as %, combining replicates) I Note: Please % % % % % % % % % % Concentration Complete This Section Also % % % % % % % % % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit _ % -- % Spearman Karber - Other High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4 .41) /,/ Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 06/16/20 Facility: CITY OF GRAHAM WWTP NPDES#: NC0021211 Pipe#: 001 County: ALAMANCE Laboratory Performin Testf MERITECH LABS, INC. j` r,c� Comments: X _! eY- / (n"�'6 Signa�/o��f /O�per }or in Responsible Charge X �0�/ r4:c� Signature of Laboratory Supervisor * PASSED: 0.83% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = 0.202 Tabular t = 2 .508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = 0.83 % Mortality Avg.Reprod. # Young Produced 21 16 20 20 21 24 21 20 18 22 21 18 0. 00 20. 17 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 20.00 Treatment 2 Treatment 2 Effluent %: 14% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 10.322% PASS FAIL # Young Produced 20 21 18 22 19 22 19 19 19 20 24 17 % control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 06/10/20 Control 7.76 8 .12 8.10 8.21 8. 07 8.22 Collection (Start) Date Sample 1: 06/08/20 Sample 2: 06/10/20 Treatment 2 8.08 8.13 8.10 8.16 7.99 8.22 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 23 .6 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24.3 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 44 Control 8.08 7.69 8 .01 7.77 8 .12 7.45 Spec. Cond. (pmhos) 149 1311 1605 Treatment 2 8.04 7.77 7.93 7.64 7.91 7.63 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt (°C) 2.0 1.7 (Mortality expressed as %, combining replicates) 1 Note: Please % % % % % % % % % % Concentration Complete This Section Also % % % % % % % % % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit _ % -- % Spearman Karber _ Other High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/23/20 Facility: CITY OF GRAHAM WWTP NPDES#: NC0021211 Pipe#: 001 County: ALAMANCE Laboratory Performing Test: MERITECH LABS, INC. �1 /<� Comments: X L 12t% .� t • /' \ . Signatu e of�per or �� Responsible Charge Signature of Laboratory Supervisor * PASSED: -3 .28% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -1.263 Tabular t = 2 .508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -3 .28 % Mortality Avg.Reprod. # Young Produced 22 23 23 22 20 22 23 25 23 26 22 23 - 0.00 22 .83 Control Control Adult (L) ive (D) ead LLLLLLLLLLLL 0.00 23 .58 Treatment 2 Treatment 2 Effluent %: 14% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 6.690% PASS FAIL # Young Produced 22 22 23 26 25 23 23 25 22 24 23 25 % control orgs X producing 3rd brood Check One Adult (L) ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test 1 pH Test Start Date: 09/16/20 Control 7.99 8 .06 7.95 8 .20 8.14 8.01 Collection (Start) Date Sample 1: 09/14/20 Sample 2: 09/16/20 Treatment 2 8 .00 8 .15 8 .09 8 .04 8 . 02 8 .14 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24.1 hrs L A A r d r d r d - U M M t t t Sample 2 X 23 .8 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness (mg/1) 44 Control 8.07 7.88 8.21 7.68 7. 92 7.38 Spec. Cond. (pmhos) 144 1921 1790 Treatment 2 7.97 7.90 8.21 7.66 7. 90 7.24 Chlorine(mg/1) <0 .1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt (°C) 1.8 1.0 (Mortality expressed as %, combining replicates) 1 Note: Please % % % % % % % % % Concentration Complete This Section Also % % % % % % % % % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average _ Probit % -- % Spearman Karber Other _ High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4 .41) Appendix D: Pretreatment Annual Report 2019 with S I U Information CZitg ti ObraIamt P. 0, Drawer 357 201 South Main Street Graham, North Carolina 27253 Tel: (336) 570-6700/Fax: (336) 570-6703 February 27, 2020 Ms. Vivien Zhong NC Division of Water Resources PERCS Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE: 2019 PAR for City of Graham Dear Ms. Zhong, Please find attached the City of Graham's Pretreatment Annual Report for the January 1, 2019 through December 31, 2019 reporting period. Should you need further information or if you have any questions regarding the report, please contact me at 336-570-6721 or ssmith@citvofgraham.com. Sincerely, 14.1414. Shelby S. Smith Pretreatment Coordinator City of Graham Narrative - 2019 City of Graham General Information General Program Information: • Allocation Table, Long Term Monitoring Plan, Sewer Use Ordinance, Headworks Analysis,Enforcement Response Plan, Industrial Waste Survey and Permits are up to date. As required by the last approved HWA on 10/3/18, City of Graham will submit an updated allocation table with updated POTW average flow to reflect new TP loading by September 1, 2020. City of Graham has also made some detection level updates and added detection level language to our LIMP and it was approved on February 13, 2020. As discussed with the PERCS office and mentioned in our PAR Narrative for 2018,we began monitoring total nitrogen in 2019 as specified in our LIMP for all sites specified with the exception of plant effluent which has already been being monitored per the NPDES permit. • The detection level language change to our LTMP that was mentioned above, was to address some issues already mentioned in the 2018 PAR Narrative with the commercial lab which analyzes our metals and the problems they are having getting the lower detection limits due to the nature of the samples and interferences which cause major, expensive issues with the equipment resulting in malfunctioning of that equipment and need to revert different methods (200.7)with higher detection levels. Our approach to handle this situation at this time is to always request the lowest detection limits but with the understanding that the nature/matrix of the samples, specifically industrial samples, may be unobtainable and other methods with higher detection limits may be necessary. Documentation, which will remain with the sampling results, will always be required explaining these situations • The ERP for City of Graham was updated to reflect the Dental Amalgam Rule. This background work for the change was in process in 2019,but the actual updated ERP was submitted to DWR on February 7,2020 and approved on February 14, 2020. • No SIUs were in Significant Noncompliance in 2019. • Data on the Division's Pretreatment Program Information Database has two corrections that need to be made. These corrections are date updates that did occur until after we received the Program Info. sheet, but I just wanted to mention. First,the Date Received by DWR for the LTMP is January 3, 2020 and Date Approved is February 13, 2020. Secondly,the ERP Date Received by DWR is February 7, 2020 and Date Approved is February 14, 2020. General Permit Information: • SIU Permits for Cintas Corporation, Luxfer Gas Cylinders,Novaflex Hose, Inc. and Stericycle, Inc. are now in their fourth year of the five year permit cycle. There were no permit modifications for these industries during 2019. • SIU Permit for Prescient Company,Inc. is in their third year of the five year permit cycle. Prescient Company did not have any permit modifications during 2019. SIU Information 1. Cintas Corporation - Permit No. 0007 (Industrial Laundry) 610 Woody Drive, Graham, N.C. 27253 Cintas Corporation had the following activities during the Jan.1- Jun. 30, 2019 reporting period: • Cintas Corporation had no violations this reporting period to report. • Cintas Corporation was monitored for 624 compounds, not listed on the IDSF forms. We found no problems with the results which are on file and available if needed. • Cintas Corporation was inspected on June 19, 2019 • Orders and Schedule Information: None • A to C and Construction Information: None Cintas Corporation had the following activities during the Jul.1- Dec.31, 2019 reporting period: • Cintas Corporation had one TSS violation this reporting period for which a Notice of Non-Compliance was issued. The Notice of Non-Compliance required 2 additional resamples. These resamples were taken by Cintas Corporation for the parameter and the resamples were both within their permit limits. They were not in SNC for TSS. • Cintas Corporation was monitored for 624 compounds, not listed on the IDSF forms. We found no problems with the results which are on file and available if needed. • Orders and Schedule: None • A to C and Construction Information: None. 2. Luxfer Gas Cylinders Permit No. 2001 (Gas Cylinders) 40CFR 467.36 (Aluminum Forming) 235 Riverbend Rd., Graham, N.C. 27253 Luxfer had the following activities during the Jan.1-Jun. 30, 2019 reporting period: • Luxfer had no violations this reporting period to report. • Luxfer was monitored for TTO compounds under 40 CFR 467. 36. The results were all less than detect, therefore, well under the 0.424 mg/L permit limit. • Orders and Schedule Information: None • A to C and Construction Information: None Luxfer had the following activities during the Jul. 1- Dec. 31, 2019 reporting period: • Luxfer had no violations this reporting period to report. 2 • Luxfer was monitored for TTO compounds under 40 CFR 467. 36. Due to a high level or organic acids, esters and other non-target compounds present in the sample the laboratory was unable to achieve lower detection limits for semi-volatile organic analysis. This sample required a x10 dilution. All values were not detected. • Luxfer was inspected on October 3, 2019. • Orders and Schedule Information: None • A to C and Construction Information: None 3. Novaflex Hose Corp. Permit No. 1001 40 CFR 428 (Rubber Manufacturing) 449 Trollingwood Road, Haw River, N.C. 27258 Novaflex had the following activities during the Jan. 1- Jun. 30, 2019 reporting period: • Novaflex had had one pH violation this reporting period for which a Notice of Non-Compliance was issued. A resample was taken by Novaflex for the parameter and the resample was within their permit limits. They were not in SNC for pH. • Orders and Schedule Information: None • A to C and Construction Information:None NovaFlex had the following activities during the July 1- Dec. 31, 2019 reporting period: • NovaFlex had no violations this reporting period to report. • Novaflex was inspected on October 31, 2019. • Orders and Schedule Information: None • A to C and Construction Information: None 4. Prescient Company, inc. Permit No. 3001 40 CFR 433.17 (Metal Finisher) 2125 Senator Ralph Scott Parkway, Mebane, NC 27302 Prescient Company, Inc. had the following activities during the Jan. 1- Jun. 30, 2019 reporting period: • Prescient Company, Inc. had one BOD violation this reporting period for which a Notice of Non-Compliance was issued. The Notice of Non-Compliance required 2 additional resamples. Two resamples was taken by Prescient for the parameter and the resamples were both within their permit limits. They were not in SNC for BOD. • Orders and Schedule Information: None • A to C and Construction Information: None • Total Toxic Organics Certification Statement received 6/10/19. Prescient Company, Inc. had the following activities during the July 1-Dec. 31, 2019 reporting period: 3 • Prescient Company, Inc. had no violations this reporting period to report. • Prescient Company, Inc. was inspected on October 9, 2019. • Orders and Schedule Information: None • A to C and Construction Information: None • Total Toxic Organics Certification Statement received 12/2/19. 5. Stericycle, Inc. Permit No. 0030 (Medical Waste) 1168 Porter Ave., Haw River,N.C.27258 Due to the extremely high levels of matrix interferences present in the Stericycle samples during samplings events during 2019,the commercial lab which was used for metals was unable to reach the lower detection limits that are stated in the City of Graham LTMP. The commercial lab did provide documentation as to the cause of this. This documentation is kept with the sample results and is available for review if needed. Stericycle had the following activities during the Jan. 1- Jun. 30,2019 reporting period: • Stericycle, Inc. had no violations this reporting period to report. • Orders and Schedules Information:None • A to C and Construction Information: None Stericycle had the following activities during the July 1-Dec. 31, 2019 reporting period: • Stericycle had no violations this reporting period to report. • Stericycle was inspected on September 12, 2019. • Orders and Schedule Information: None • A to C Information:None 4 Pretreatment Program Info Database printed on: 12/20/2019 for Program Name Graham I irmit.'41' % WWTP Name City of Graham Stream Information IWC at 7010 13.74 Program Approval Date 08/05/1983 7010 Flow cfs/mgd 34 / 21.96 1010 Flow cfs/mgd 27.96 / 18.07 Pretreatment Status Full WS-V/NSW Stream Classification Region WSRO Basin Number CPF02 I County Alamance Receiving Stream Name HAW RIVER NPDES Number NC0021211 NPDES Effective Date Last PAR Rec 02/18/2019 PAR Due Date 03/01/2020 mercury 07/01/2013 Current Fiscal 1631 NPDES Expire Date 05/31/2016 09/06/2018 required Year PCI Done POTW is Primary WTP TRUE Last Audit on 09/12/2019 Audit Year Next23/24 yes W Design Flow mgd 3.5000 %Design mgd is SIU permitted 7.57 Permitted SIU flow(mgd)[Pt_SIU) .265 WWTP SIU's 5 Program Sills I5 WWTP CIU's 3 Program CIUs 3 HWA LTMP IWS SUO ERP date Inactive Date Next Due 09/01/2023 04/02/2023 02 jo 7) ..o2O Date Received by DWR 08/30/2018 05/27/2018 03/29/2018 09/07/2011 12/15/2011 Date Approved 10/03/2018 10/04/2018 04/04/2018 09/14/2011 01/23/2012- Adopt Date Required 61,Jf3J2o20 ();/... J )) Zo 2.4.) Date Adopted 11/01/2011 Info in this Box from Pt_Contacts i Date Date Date PT_Pro Attended Attended Attended Formal Name g.prime Phonel ext Fax HWA Wksp IUP Wksp PAR Wksp Ms.Shelby Smith IPrirn II336-570-6721 I 1336-513-5502 II 1123/2018 ' 5/24/2016 101/29/20191 ssmith@cityofgraham.com Pretreatment Coordinator PO Box 357 27253 Tonya Mann I 11(336)570-6721 J I 11/23/2018 I I 1/29/2019 I tmann@cityofgraham.com Utilities Director PO Box 357 27253 J Pretreatment Related NOVs from DWQ DWR Central Office Contact Vivien Zhong DWR Regional Contact Jim Gonsiewski s A\:,c- Al'°i\- - Chapter 9, PAR Guidance Pretreatment Performance Summary (PPS) 1. Pretreatment Town Name: City of Graham 2. "Primary"NPDES Number NCO() 21211 or Non_Discharge Permit# if applicable=> 3. PAR Begin Date, please enter 01/01/yyyy 3.=> 1/1/2019 4. PAR End Date, please enter 12/3 1/yyyy 4.=> 12/31/2019 5. Total number of SIUs, includes CIUs 5.=> 5 6. Number of CIUs 6._> 3 7. Number of SIUs with no IUP, or with an expired IUP 7.=> 0 8. Number of SIUs not inspected by POTW 8._> 0 9. Number of SIUs not sampled by POTW 9.=> 0 10. Number of SIUs in SNC due to IUP Limit violations 10.=> 0 11. Number of SIUs in SNC due to Reporting violations 11._> 0 12. Number of Ms in SNC due to violation of a Compliance Schedule,CO,AO or similar 12._> 0 13. Number of CIUs in SNC 13.=> 0 14. Number of SIUs included in Public Notice 14.=> 0 15 Total number of SIUs on a compliance schedule, CO,AO or similar 15.=> 0 16. Number of NOVs,NNCs or similar assesed to SIUs 16.=> 3 17. Number of Civil Penalties assessed to SIUs 17.=> 0 18. Number of Criminal Penalties assessed to SIUs 18.=> 0 19. Total Amount of Civil Penalties Collected 19._> $ 0 20. Number of IUs from which penalties collected 20.=> 0 Foot Notes: AO Administrative Order IUP Industrial User Pretreatment Permit POTW Publicly Owned Treatment Works CIU Categorical Industrial User NNC Notice of Non-Compliance SIU Significant Industrial User CO Consent Order NOV Notice of Violation SNC Significant Non-Compliance IU Industrial User PAR Pretreatment Annual Report revised 1/2018: PAR PPS 2018 Pretreatment Annual Report (PAR) PAR covers this calendar year=> 2019 Significant Non-Compliance Report (SNCR) Control Authority=Program=Town Name => City of Graham WWTP = Wastewater Treatment Plant,use separate form for each WWTP. WWTP Name => Graham WWTP SIU= Significant Industrial User NPDES # => NC0021211 SNC = Significant Non-Compliance A SNCR Form must be submitted with every PAR, please write "None" if you had No SIUs in SNC during calendar year SNC ? (Yes /No ) IUP Pipe Industry Name Parameter for each 6-month period. # # or "Reporting" Jan. - June July-Dec. "NONE" Attach a copy of the Division's "SIUs in SNC Historical Report" for your POTW's SIUs behind this page . Is the database correct ? Notify the Division of any errors ! Database indicates SNC history for previous years. EVERY SNC MUST be explained in the Narrative, How was, is, or will it be resolved? REPEAT SNCs are serious matters that MUST be explained in the Narrative. Form name: PAR,SNCR,200I Date Revised: 1/4/2001 Pretreatment Annual Report (PAR) Control Authority, Industry Industrial Data Summary Form (IDSF) Town Name=> City of Graham Name Cintas Corporation WWTP Name=> Graham WWTP IUP# 0007 Use separate forms for each industry/pipe NPDES#=> NC002121 1 Pipe# 01 Enter BDL values as < (value) Ist 6 months,dates=> 1/1/2019 to 6/30/19 2nd 6 months, dates=> 7/1/2019 to 12/31/19 Flow. m6d BOD TSS Ammonia 1st 6 months lnd 6 months 1st 6 months 2nd 6 months 1st 6 months Jlnd 6 months 1st 6 months lnd 6 months Total #of samples=> 3 6 2 2 2 4 1 1 * Maximum (mg/I)_> 0.0713 0.0779 540 258 65 375 1.2 5.9 * or Maximum (lb/d)_> 'or 6 mos.Using V2 BDL Average(mg/I)_> 0.057 0.072 354 240 65 173 I.? 5.9 * or Average Loading(lb/d)=> % violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 NA NA %TRC violations, (SNC is>=33 %)_> 0 0 0 0 0 0 NA NA 'Arsenic Cadmium Chromium COD 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months I st 6 months 2nd 6 months I st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 I 1 1 I * Maximum (mg/I)_> 0.003 0.002 0.0039 0.00066 0.007 0.005 826 1510 * or Maximum (lb/d)_> 'or 6 may.Using l„BDL Average(mg/1)_> 0.003 0.002 0.0039 0.00066 0.007 0.005 826 1510 * or Average Loading(lb/d)_> violations, (chronic SNC is>=66%)_> NA NA 0 0 0 0 NA NA %TRC violations, (SNC is>=33 %)_> NA NA 0 0 0 0 NA NA Comer Cyanide LeadMercury 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months I st 6 months 2nd 6 months I st 6 months 2nd 6 months Total#of samples=> I 1 1 1 1 1 3 3 * Maximum (mg/1)_> 0.129 0.047 0.014 <0.005 0.021 0.016 <0.0002 <0.0002 * or Maximum (1b/d)_> 'or 6 mos.Using V2 BDL Average(mg/1)_> 0.129 0.047 0.014 0.0025 0.021 0.016 0.0001 0.0001. * or Average Loading(lb/d)=> %violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 0 0 %TRC violations,(SNC is>=33 %)_> 0 0 0 0 0 0 0 0 BDL=>Below Detection Limit mg/I=>milligrams per liter * POTW must enter at least one of these 1UP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month.Qtr.or 6-month&if BDL, 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: PACRotif}9fslhi Rediaiidedy'iftaQtertatsi,ctRArlB,pages 12, 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page of -- Pretreatment Annual Report (PAR) Industry Name Cintas Corporation Industrial Data Summary Form (IDSF) IUP# 0007 Use separate forms for each industry/pipe Pipe# 01 Nickel Selenium 'Silver Zinc 1st 6 months 2nd 6 months 1st 6 months lnd 6 months 1st 6 months lnd 6 months 1st 6 months 1nd 6 months Total#of samples=> I 1 I 1 1 1 1 1 * Maximum (mg/1)_> 0.013 0.021 0.002 <0.002 <0.0005 <0.0005 0.392 0.491 * or Maximum (lb/d)_> •or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.013 0.021 0.002 0.0010 0.00025 0.00025 0.392 0.491 * or Average Loading(lb/d)=> %violations, (chronic SNC is>= 66%)_> 0 0 NA NA NA NA 0 0 %TRC violations,(SNC is>=33 %)=> 0 0 NA NA NA NA 0 0 pH Temperature NO2 +NO3 Total Nitrogen 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months l st 6 months 2nd 6 months Total#of samples=> 2 2 2 2 1 1 1 I * Maximum=> 9.33 7.4 30.6 30.8 0.2 <0.10 17.7 9.67 * or Minimum=> 'orb mos Using 1,2 BDL Average (mg/I)_> 30 28 0.2 0.05 17.7 10 * %violations, (chronic SNC is>=66%)=> 0 0 0 0 NA NA NA NA %TRC violations,(SNC is>=33 %)=> N/A 0 0 NA NA NA NA IT. Phosphorus Total Molybdenum TKN FOG 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/1)_> 0.477 1.18 0.044 0.019 I7.5 9.67 18 8 * or Maximum (lb/d)=> `or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.477 1.18 0.044 0.019 17.5 9.7 18 8 * or Average Loading(lb/d)=> % violations, (chronic SNC is>=66%)_> 0 0 NA NA 0 0 0 0 TRC violations, (SNC is>=33 %)=> 0 0 NA NA 0 0 0 0 BDL=>Below Detection Limit mg/I=>milligrams per liter * POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Ave period could be month.Qtr,or 6-month&if BDL. I/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: PFTorlfpf ha Redisiatedgiha¢ten is ciRAl3B,pages 12. 13. 14 Blank 1DSF Form,Copy and use in your PAR Number each set for each 1UP pipe-Page — of -- Pretreatment Annual Report (PAR) Control Authority, Industry Industrial Data Summary Form (IDSF) Town Name=> City of Graham Name Luxfer Gas Cylinders Use separate forms for each industry/pipe WWTP Name=> Graham WWTP IUP# 2001 Enter BDL values as < (value) NPDES#=> NC0021211 Pipe# 01 1st 6 months, dates=> 1/1/2019 to 6/30/2019 2nd 6 months, dates=> 7/1/2019 to 12/31/2019 Flow, med BOD jTSS Ammonia 1st 6 months 2nd 6 months 1st 6 months 2nd b months 1st 6 months 2nd 6 months 1st 6 months 2nd b months ' Total#of samples=> 2 2 2 2 2 2 1 1 * Maximum (mg/1)=> 0.0615 0.0386 10.5 16.7 3 17.8 0.4 0.4 * or Maximum (Ib/d)=> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.0443 0.0382 5.44 11.3 2.8 10.9 0.4 0.4 * or Average Loading(lb/d)_> %violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 NA NA %TRC violations,(SNC is>=33 %)_> Q 0 0 0 0 0 0 NA NA %violations,(chronic SNC is>=66%)_> T %TRC violations, (SNC is>=33 %)_> Arsenic 'Cadmium Chromium COD 1st 6 months '2nd 6 months 1st 6 months 2nd 6 months 1st 6 months nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/1)=> <0.002 <0.002 <0.00015 <0.00015 <0.002 <0.002 19 34 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/1)=> 0.001 0.001 0.000075 0.000075 0.001 0.001 19 34 * or Average Loading(lb/d)—> %violations, (chronic SNC is>=66%)_> ,, NA NA 0 0 0 0 NA NA %TRC violations, (SNC is>=33 %)_> .o NA NA 0 0 0 0 NA NA %violations,(chronic SNC is>=66%)_> 0 0 %TRC violations, (SNC is>=33 %)_> i 0 0 Copper Cyanide Lead Mercury 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 Maximum (mg/1)=> 0.007 0.006 <0.005 <0.005 <0.0005 <0.0005 <0.0002 <0.0002 * or Maximum (1b/d)_> *or 6 mos.Using 1/2 BDL Average(mg/I)_> 0.007 0.006 0.0025 0.0025 0.00025 0.00025 0.0001 0.0001 * or Average Loading(lb/d)_> %violations, (chronic SNC is>=66%)_> 0 0 0 0 0 0 NA NA %TRC violations, (SNC is>=33 %)_> c 0 0 0 0 0 0 NA NA %violations,(chronic SNC is>=66%)_> 0 0 %TRC violations, (SNC is>=33 %)_> 0 0 BDL=>Below Detection Limit mg/1=>milligrams per liter * POTW must enter at least one of these IUP=>Industrial User Permit lb/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month,Qtr.or 6-month&if BDL, 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant / Chapter: PAR Guidance File name: PPRorIipS etiisiteCisiittedfriha¢ si tag> qct B,pages 12, 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page 1 of `d Pretreatment Annual Report (PAR) Industry Name Luxfer Gas Cylinders Industrial Data Summary Form (IDSF) lup# 2001 Use separate forms for each industry/pipe pipe# 01 Nickel - `Selenium Silver Zinc 1st b months 2nd 6 months Ist 6 months 2nd b months )1st b months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/1)_> 0.0015 0.0011 <0.001 <0.002 <0.0005 <0.0005 0.016 0.02 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/I)_> 0.0015 0.0011 0.0005 0.001 0.00025 0.00025 0.016 0.02 * or Average Loading(lb/d)=> %violations,(chronic SNC is>=66%)_> ,, 0 0 NA NA NA _ NA 0 0 %TRC violations,(SNC is>=33 %)_> 0 0 0 NA NA NA NA 0 0 %violations, (chronic SNC is>=66%)_> T 0 0 TRC violations,(SNC is>=33 %)_> i 0 0 pH Temperature°C NO2 & NO3 'Total Nitrogen 1st 6 months -2nd b months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months -2nd 6 months Total#of samples=> 2 2 2 2 1 1 1 1 * Maximum => 8.19 8.77 20.2 26 0.45 1.89 1.98 2.31 * or Minimum=> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 17.8 24.4 0.45 1.89 1.98 2.31 * %violations, (chronic SNC is>=66%)_> 0 0 0 0 NA NA NA NA %TRC violations,(SNC is>=33 %)_> o N/A 0 0 NA NA NA NA %violations, (chronic SNC is>=66%)_> N/A %TRC violations, (SNC is>=33 %)=> N/A T.Phosphorus Total Molybdenum TKN FOG 1st 6 months 2nd 6 months 1st 6 months -2nd 6 months 161st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/1)=> 0.538 3.39 <0.002 <0.002 1.53 1.89 <5 <5 * or Maximum (lb/d)=> *or 6 mos.Using 1/2 BDL Average(mg/1)=> 0.538 3.39 0.001 0.001 1.53 1.89 2.5 2.5 * or Average Loading(lb/d)_> %violations, (chronic SNC is>=66%)_> ,, NA NA NA NA 0 0 0 0 %TRC violations, (SNC is>=33 %)_> n NA NA NA NA 0 0 0 0 %violations, (chronic SNC is>=66%)_> %TRC violations, (SNC is>=33 %)_> i BDL=>Below Detection Limit mg/l=>milligrams per liter * POTW must enter at least one of these CUP=>Industrial User Permit lb/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Ave period could be month.4tr,or 6-month&if BDL, 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant / Chapter: PAR Guidance File name: P. PorlIpSdhmsi3e�ialeclett#tafttartatsl�eti64B,pages 12, 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each 1UP pipe-Page "" of �'-' Pretreatment Annual Report (PAR) Industry Name Litxfer Gas Cylinders Industrial Data Summary Form (IDSF) IUP# 2001 Use separate forms for each industry/pipe Pipe# of Enter BDL values as < (value) Ip-Chloro-m cresol ' 2-chlorophenol 2,4 dinitrotoluene 1,2 Diphenylhdrazine 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 12nd 6 months Total #of samples=> 1 1 1 1 I 1 1 1 * Maximum (mail)_> <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.005 0.05 0.005 0.05 0.005 0.05 0.005 0.05 * or Average Loading(lb/d)_> %violations,(chronic SNC is>= 66%)_> 0 0 0 0 0 0 0 0 %TRC violations.(SNC is>=33 %)_> 0 0 0 0 I 0 0 0 0 I ethyblenzene fluoranthene isophorone napthalene 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total #of samples=> 1 I 1 1 1 1 1 1 Maximum (mg/l)_> <0.001 <0.001 <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 or Maximum (lb/d)=> _ *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.0005 0.0005 0.005 0.05 0.005 0.05 0.005 0.05 * or Average Loading(lb/d)=> %violations, (chronic SNC is>=66%)_> 0 0 0 0 0 0 0 0 %TRC violations.(SNC is>_33 %)_> 0 0 0 0 0 0 0 0 N-nitrosodi phenyl amine phenol benzo(a)pyrene Benzo(g,h,i)perylene 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> I 1 l 1 I 1 1 1 * Maximum (mg/I)_> <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.005 0.05 0.005 0.05 0.005 0.05 0.005 0.05 * or Average Loading(lb/d)=> %violations, (chronic SNC is>=66%)_> 0 0 0 0 0 0 0 0 %TRC violations.(SNC is>=33 %)_> 0 0 0 0 0 0 0 0 BDL=>Below Detection Limit mail=>milligrams per liter • POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance and=>million gallons per day Avg period could be month.Qtr.or 6-month&if BDL, 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: PARotirpSifiezirsileGnidedEhafttratiktstc1WB,pages 12. 13. 14 Blank 1DSF Form.Copy and use in your PAR Number each set for each IUP pipe-Page - of `- Pretreatment Annual Report (PAR) Form (IDSF) Industry Name Luxfer Gas Cylinders Industrial Data Summary IUP# 2001 Use separate forms for each industry/pipe Pipe# 01 Enter BDL values as < (value) fluorene phenanthrene dibenzo(a,h)anthracene indeno(1,2,3-c,d)pyrene I 1st 6 months I2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mgil)_> <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/1)=> 0.005 0.05 0.005 0.05 0.005 0.05 0.005 0.05 * or Average Loading(lb/d)_> 1 %violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 0 0 %TRC violations,(SNC is>=33 %)_> 0 0 0 0 0 0 0 0 pyrene tetrachlorocthylene I toulene trichloroethylene 1,1,1 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months "2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/1)_> <0.01 <0.10 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 * or Maximum (lb/d)=> *or 6 mos.Using 1/2 BDL Average (mg/1)_> 0.005 0.05 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005 ,. Average Loading(lb/d)_> %violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 0 0 %TRC violations, (SNC is>=33 %)_> 0 0 0 0 .1 0 0 0 0 endosulfansulfate 1,1,2 bis(2ethyl hexyl)phthalate diethylphthalate 3.4 benzofluouranthene 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months I2nd 6 months 1st 6 months -2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/1)_> <0.001 <0.001 <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/I)=> 0.0005 0.0005 0.005 0.05 0.005 0.05 0.005 0.05 * or Average Loading(lb/d)_> %violations, (chronic SNC is>=66%)_> 0 0 0 0 0 0 0 0 %TRC violations,(SNC is>=33 %)_> 0 0 0 0 0 0 0 0 BDL=>Below Detection Limit mgll=>milligrams per liter • POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows. Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month,Qtr,or 6-month&if BDL.1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant t Chapter: PAR Guidance File name: PF¢'ort(l3&ffiels deNCiiiiidedatiha¢tent tshelli IB,pages 12. 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page I of ' Pretreatment Annual Report (PAR) Industry Name 'Alder Gas Cylinders Industrial Data Summary Form (IDSF) JUP# 2001 Use separate forms for each industry/pipe Pipe# 01 Enter BDL values as < (value) 1 benzo(k)fluoranthene chrysene acenaphthylene anthrancene I st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 Maximum (mg/1)_> <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 <0.01 <0.10 or Maximum (lb/d)_> *or 6 mos. Using 1/2 BDL Average(mg/1)_> 0.005 0.05 0.005 0.05 0.005 0.05 0.005 0.05 * or Average Loading(lb/d)=> — %violations, (chronic SNC is>=66%)_> 0 0 0 0 0 0 0 0 %TRC violations.(SNC is>=33 %)_> 0 0 0 0 0 0 0 0 di-n-butyl phthalate edrin ' endrin aldehyde PCB1242 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> l 1 1 I 1 1 I l * Maximum (mg/1)_> <0.01 <0.10 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 * or Maximum OM)=> *or 6 mos.Using 1/2 BDL Average(mg/1)=> 0.005 0.05 0.0005 0.0005 0.0005 0.0005 0.0025 0.0025 * or Average Loading(Ib/d)=> %violations, (chronic SNCis>=66%)_> 0 0 0 0 0 0 0 0 TRC violations,(SNC is>=33 %)_> 0 0 0 0 0 0 0 0 IPCB 1254 PCB 1221 PCB 1232 PCB 1248 ' 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months l2nd 6 months Total#of samples=> 1 I I 1 1 I 1 1 ,r Maximum (mg/I)=> <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 l <0.005 * or Maximum (lb/d)_> 'tor 6 mos.Using 1/2 BDL Average(mg/1)_> 0.0025 0.0025 0.0025 ( 0.0025 0.0025 0.0025 0.0025 0.0025 * or Average Loading(lb!d)_> %violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 0 0 %TRC violations.(SNC is>=33 %)_> 0 0 0 0 0 0 0 0 BDL=>Below Detection Limit mg/1=>milligrams per liter * POTW must enter at least one of these [UP=>industrial User Permit lb/d=>pounds per day four rows. Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month.Qtr.or 6-month&if BDL. 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: Pr Porlfgdhrssi!Ze�Ciaiaded:ffehaAtert9,2s'ectRAt1B,pages 12, 13. 14 Blank IDSF Form,Copy and use in your PAR Number each set for each 1UP pipe-Page J of CT. Pretreatment Annual Report (PAR) Industry Name Luxfer Gas Cylinders Industrial Data Summary Form (IDSF) IUP# 2001 Use separate forms for each industry/pipe Pipe# 01 Enter F3DL values as < (value) PCB 1260 PCB 1016 acenaphthene 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total #of samples=> 1 1 1 1 1 Maximum (mg/I)_> <0.005 <0.005 <0.005 <0.005 <0.01 <0.10 k or Maximum (lb,/d)=> *or 6 mos.Using 1/2 BDL Average(mg/I)_> 0.0025 0.0025 0.0025 0.0025 0.005 0.05 or Average Loading(lb/d)=> %violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 %TRC violations, (SNC is>=33 %)_> 0 0 0 0 0 0 1st 6 months 2nd 6 months I st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total #of samples=> * Maximum (mg/I)_> 1 * or Maximum (1b/d)_> *or 6 mos. Using 1/2 BD1 Average(mg/I)=> Average Loading(lb/d)_> %violations,(chronic SNC is>=66%)_> %TRC violations, (SNC is>=33 %)_> 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months -2nd 6 months 1 st 6 months 2nd 6 months Total#of samples=> Maximum (mg/1)=> or Maximum (lb/d)_> *or 6 mos. Using 1/2 BDI Average(mg/I)_> * or Average Loading(lb/d)_> %violations, (chronic SNC is>=66%)_> %TRC violations,(SNC is>=33%)_> BDL=>Below Detection Limit mg/1=>milligrams per liter " POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month,Qtr,or 6-month&if BDL. 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: Pt rTTfiMeciFiZeNegiiniedLha{tterd t cil B.pages 12, 13. 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page L^ of IC Pretreatment Annual Report (PAR) Control Authority Industry Industrial Data Summary Form (IDSF) Town Name=> City of Graham Name Novaflex Hose, Inc. WWTP Name=> Graham WWTP IUP# 1001 Use separate forms for each industry/pipe NPDES#_> NC002121 I Pipe# 02 Enter BDL values as < (value) 1st 6 months, dates=> 1/1/2019 to 6/30/2019 2nd 6 months, dates=> 7/1/2019 to 12/31/2019 Flow, mgd JBOD TSS Ammonia I st 6 months 2nd 6 months 1st 6 months 2nd b months 1st b months -2nd 6 months 1st 6 months Lnd 6 months Total#of samples=> 2 2 2 2 2 2 1 1 * Maximum (mg/1)_> 0.01483 0.01477 111 102 26 31 1.1 1.4 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.00982 0.00957 82.8 61 21.5 20 1.1 1.4 * or Average Loading(lb/d)_> %violations,(chronic SNC is>=66%)—> 0 0 0 0 0 0 NA NA %TRC violations,(SNC is>=33 %)_> 0 0 0 0 0 0 NA NA Arsenic Cadmium _ChromiumL COD 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months '2na 6 months_ Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/1)_> 0.010 <0.002 <0.00015 <0.00015 0.003 <0.002 220 85 * or Maximum (lb/d)=> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.010 0.001 0.000075 0.000075 0.003 0.001 220 85 * or Average Loading(lb/d)_> I %violations, (chronic SNC is>=66%)_> NA NA 0 0 0 _ 0 NA NA %TRC violations,(SNC is>=33 %)_> NA NA 0 0 0 0 NA NA Copper Cyanide Lead Mercury 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 I 1 1 1 1 * Maximum (mg/1)_> 0.130 0.101 <0.005 <0.005 0.0024 0.0010 <0.0002 <0.0002 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.130 0.101 0.0025 0.0025 0.0024 0.0010 0.0001 0.0001 * or Average Loading(Ib/d)=> %violations, (chronic SNC is>=66%)_> 0 0 0 0 0 0 NA NA %TRC violations,(SNC is>=33 %)_> 0 0 0 0 0 0 NA NA BDL=>Below Detection Limit mg//1=>milligrams per liter * POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month,Qtr,or 6-month&if BDL, 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter. PAR Guidance File name: PfBortEpSi tmiisReN ieirdEtl talittgtajshct& B,pages 12, 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page of 2. Pretreatment Annual Report (PAR) Industry Name Novaflex Hose, Inc. Industrial Data Summary Form (IDSF) IUP# 1001 Use separate forms for each industry/pipe Pipe# 02 Nickel Selenium Silver Zinc 1st 6 months 2nd 6 months l st 6 months Ind 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/l)_> 0.0055 0.0019 0.015 <0.002 <0.0005 <0.0005 0.291 0.125 * or Maximum (Ib/d)_> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.0055 0.0019 0.015 0.001 0.00025 0.00025 0.291 0.125 * or Average Loading(lb/d)_> %violations,(chronic SNC is>=66%)_> 0 0 NA NA NA NA 0 0 %TRC violations,(SNC is>=33 %)=> 0 0 NA NA NA NA 0 0 pH 'Temperature'C NO2 & NO3 Total Nitrogen 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months -2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 3 2 2 2 1 1 1 1 * Maximum=> 10.98 7.32 18.1 29.1 <0.10 <0.10 9.69 4.43 * or Minimum=> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 16.7 29 0.05 0.05 9.69 4.43 * %violations,(chronic SNC is>=66%)_> 0 0 0 0 NA NA NA NA %TRC violations, (SNC is>=33 %)_> N/A 0 0 NA NA NA NA T. Phosphorus Total Movbdenum TKN FOG 1st 6 months 2nd 6 months 1st 6 months nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 I 1 1 1 1 1 1 * Maximum (mg/I)=> 36.2 0.234 0.004 <0.002 9.69 4.43 67 <5 * or Maximum (lb/d)_> *or 6 mos.Using 12 BDL Average(mg/1)_> 36.2 0.234 0.004 0.0010 9.69 4.43 67 2.5 * or Average Loading(lb/d)=> %violations,(chronic SNC is>=66%)_> NA NA NA NA 0 0 0 0 %TRC violations, (SNC is>=33 %)=> NA NA NA NA 0 0 0 0 BDL=>Below Detection Limit mg/I=>milligrams per liter • * POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mod=>million gallons per day Avg period could be month,Qtr,or 6-month&if BDL, l2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: PAPortfkilhecisReCtaidrddlhafttcgtit AzetRih413,pages 12, 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page of Pretreatment Annual Report (PAR) Control Authority, Industry Industrial Data Summary Form (IDSF) Town Name=> City of Graham Name Prescient Company, Inc. WWTP Name=> Graham WWTP IUP# 3001 Use separate forms for each industry/pipe NPDES#=> NC002121 1 Pipe# 01 Enter BDL values as < (value) 1st 6 months,dates=> 1/1/2019 to 6/30/2019 2nd 6 months, dates=> 7/1/2019 to 12/31/2019 I Flow, mad BOD TSS Ammonia 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 4 2 4 2 2 2 1 1 * Maximum (mg/1)_> 0.0015 0.0044 729 40.8 28 19.0 <0.1 0.5 * or Maximum (lb/d)_> *or 6 mos.Using 1/2 BDL Average(mg/1)_> 0.0011 0.0030 252 32.5 24.5 15.5 0.05 0.5 * or Average Loading(lb/d)_> %violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 NA NA %TRC violations,(SNC is>=33 %)_> 0 0 0 0 0 0 NA NA 'Arsenic Cadmium Chromium -CUU I st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months '2nd 6 months Total#of samples=> 1 I 1 I 1 1 I 1 * Maximum (mg/1)_> <0.002 <0.002 <0.00015 <0.00015 <0.002 <0.002 250 117 * or Maximum (Ib/d)_> *or 6 mos.Using 1/2 BDL Average(mg/I)=> 0.001 0.001 0.000075 0.000075 0.001 0.001 250 117 or Average Loading(lb/d)=> %violations, (chronic SNC is>=66%)_> NA NA 0 0 0 0 NA NA %TRC violations,(SNC is>=33 %)_> NA NA 0 0 0 0 NA NA Conner Cyanide Lead Mercury 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months "2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/1)_> 0.091 0.154 <0.005 <0.005 <0.0005 <0.0005 <0.0002 <0.0002 * or Maximum (Ib/d)_> *or 6 mos.Using 1/2 BDL Average(mg/I)_> 0.091 0.154 0.0025 0.0025 0.00025 0.00025 0.0001 0.0001 * or Average Loading(Ib/d)_> violations, (chronic SNC is>=66%)_> 0 0 0 0 0 0 NA NA TRC violations, (SNC is>=33 %)_> 0 0 0 0 0 0 NA NA BDL=>Below Detection Limit mg/I=>milligrams per liter * POTW must enter at least one of these [UP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month,Qtr,or 6-month&if BDL, I/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant J Chapter: PAR Guidance File name: PARodtPfhsdazdeNGaiided&thaQtmat e,ctRAr1B,pages 12, 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page 1 of —f Pretreatment Annual Report (PAR) Industry Name Prescient Company, Inc. Industrial Data Summary Form (IDSF) IUP# 3001 Use separate forms for each industry/pipe Pipe# 01 Nickel !Selenium Silver Zinc 1st b months 2nd 6 months 1st 6 months 2nd 6 months 1st b months 12nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg/I)=> 0.012 0.0068 <0.001 <0.002 <0.0005 <0.0005 0.292 0.I24 * or Maximum (lb/d)=> *or 6 mos.Using 1/2 BDL Average(mg/1)=> 0.012 0.0068 0.0005 0.001 0.00025 0.00025 0.292 0.124 * or Average Loading(lb/d)_> %violations,(chronic SNC is>=66%)_> 0 0 NA NA 0 0 0 0 TRC violations, (SNC is>=33 %)_> 0 0 NA NA 0 0 0 0 pH Temperature° C 'Fluoride NO2&NO3 1st b months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 134 127 2 2 1 1 1 1 * Maximum=> 7.6 7.8 22.2 29.8 3.4 1.50 <0.10 0.11 * or Minimum=> *or 6 mos.Using 1/2 BDL Average(mg/I)_> 21.6 29.4 3.4 1.50 0.05 0.11 * %violations, (chronic SNC is>=66%)_> 0 0 NA NA NA NA %TRC violations, (SNC is>=33 %)=> N/A 0 0 NA NA NA NA T. Phosphorus Total Molybdenum TKN FOG 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> I I 1 1 1 1 1 1 * Maximum (mg/I)_> 28.3 9.85 0.006 0.003 4.86 5.89 <5 <5 * or Maximum (Ib/d)=> *or 6 mos.Using 1/2 BDL Average(mg/I)=> 28.3 9.85 0.006 0.003 4.86 5.89 2.5 2.5 * or Average Loading(lb/d)=> %violations, (chronic SNC is>=66%)_> NA NA NA NA 0 0 0 0 %TRC violations,(SNC is>=33 %)_> NA NA NA NA 0 0 0 0 BDL=>Below Detection Limit mg/I=>millierams per liter * POTW must enter at least one of these 1UP=>Industrial User Permit lb/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month.Qtr,or 6-month&if BDL, 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: P, TI1giihedsReCtaiided afitcgat lecIRIMB,pages 12. 13. 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page of -v' Pretreatment Annual Report (PAR) Industry Name Prescient Company, Inc. Industrial Data Summary Form (IDSF) IUP# 3001 Use separate forms for each industry/pipe Pipe# 0I Enter BDL values as < (value) Total Nitrogen 1st 6 months 2nd 6 months /1st 6 months 2nd 6 months 1st 6 months 2nd 6 months l st 6 months -2nd 6 months Total#of samples=> 1 1 * Maximum (mg/1)_> 4.86 6.00 * or Maximum (Ib/d)=> *or 6 mos. Using 1/2 BDL Average(mg/1)_> 4.86 6.00 * or Average Loading(Ib/d)=> %violations, (chronic SNC is>=66%)_> NA NA %TRC violations,(SNC is>=33 %)_> NA NA 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months '1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> * Maximum (mg/1)_> * or Maximum (lb/d)_> * or Average(mg/1)=> * or Average Loading(lb/d)=> %violations, (chronic SNC is>=66%)_> %TRC violations,(SNC is>=33 %)_> I I 1st 6 months [2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> * Maximum (mg/I)_> * or Maximum (Ib/d)=> * or Average(mg/I)_> * or Average Loading(lb./d)_> violations,(chronic SNC is>=66%)_> %TRC violations,(SNC is>=33 %)_> BDL=>Below Detection Limit mg/I=>milligrams per liter * POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month.Qtr.or 6-month&if BDL, 1/2BDL.or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: PARorffpfdhairFweNatiided atttez(3tsigclidl#B,pages 12,13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page 3 of Pretreatment Annual Report (PAR) Control Authority, Industry Industrial Data Summary Form (IDSF) Town Name=> City of Graham Name Stericycle, Inc. Use separate forms for each industry/pipe WWTP Name=> Graham WWTP IUP# 0030 Enter BDL values as < (value) NPDES #=> NC002121 1 Pipe# 01 1st 6 months, dates=> 1/1/2019 to 6/30/2019 2nd 6 months, dates=> 7/1/2019 to 12/31/2019 Flow. mad BOD TSS Ammonia 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months Ind 6 months 1st 6 months 2nd 6 months Total#of samples=> 7 7 2 2 2 2 1 1 * Maximum (mg/1)_> 0.0190 0.0218 6.6 10.5 38 16 88.4 67.8 * or Maximum (Ib/d)=> *or 6 mos.Using 1/2 BDL Average(mg/I)=> 0.0146 0.0153 3.3 9.9 22.8 14.9 88.4 67.8 * or Average Loading(lb/d)=> violations,(chronic SNC is>=66%)_> 0 0 0 0 0 0 NA NA %TRC violations, (SNC is>=33 %)_> 0 0 0 0 0 0 NA NA 'Arsenic Cadmium l Chromium COD 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total #of samples=> I 1 1 1 1 1 1 1 * Maximum (mg/1)=> <0.100 <0.004 <0.020 0.00095 <0.050 <0.004 379 724 * or Maximum (lb/d)=> *or 6 mos.Using l/2 BDL Average(mg/1)=> 0.05 0.002 0.010 0.00095 0.025 0.002 379 724 * or Average Loading(lb/d)_> %violations,(chronic SNC is>=66%)=> NA NA 0 0 0 0 NA NA %TRC violations, (SNC is>=33 %)=> NA NA 0 0 0 0 NA NA Copper Cyanide LeadMercury 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total # of samples=> 1 I 1 1 1 1 6 6 * Maximum (mg/1)_> 0.052 0.040 <0.005 <0.005 <0.100 0.0035 0.0023 <0.0002 * or Maximum (lb/d)_> *or6 mos.Using 1/2 BDL Average(mg/1)=> 0.052 0.040 0.0025 0.0025 0.05 0.0035 0.0003 0.0001 * or Average Loading(lb/d)=> %violations, (chronic SNC is>= 66%)_> 0 0 0 0 0 0 NA NA %TRC violations,(SNC is>=33 %)=> 0 0 0 0 0 0 NA NA BDL=>Below Detection Limit mg/1=>milligrams per liter * POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month.Qtr.or 6-month&if BDL. l/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: PFQtodig3hatsiteCtaiidediGhaptc tatskct8Rr1B,pages 12, 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page 1 of - Pretreatment Annual Report (PAR) Industry Name Stericycle, Inc. Industrial Data Summary Form (IDSF) IUP# 0030 Use separate forms for each industry/pipe Pipe# 01 Nickel Selenium 'Silver > "Zinc 1st 6 months 'Lnd 6 months ' 1st 6 months 2nd 6 months 1st 6 months Lnd b months 1st 6 months Lnd 6 months Total#of samples=> 1 1 1 1 1 1 1 1 * Maximum (mg./1)=> <0.100 0.015 <0.100 0.006 <0.050 <0.0025 0.62 0.065 * or Maximum (Ib/d)=> *or 6 mos.Using 1/2 BDL Average(mg/1)=> 0.05 0.015 0.05 0.006 0.025 0.00125 0.62 0.065 * or Average Loading(lb/d)=> %violations, (chronic SNC is>=66%)_> 0 0 NA NA NA NA 0 0 %TRC violations, (SNC is>=33 %)_> 0 0 NA NA NA NA 0 0 pH Temperature°C NO2&NO3 Total Nitrogen 1st 6 months 2nd 6 months I st 6 months 2nd 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total#of samples=> 2 2 2 2 1 1 1 I * Maximum=> 9.08 5.3 21.6 39.1 1.27 1.13 102 82.4 * or Minimum=> *or 6 mos.Using 1/2 BDL Average(mg/1)=> 20.1 35.1 1.27 1.13 102 82.4 * %violations,(chronic SNC is>=66%)_> 0 0 0 0 NA NA NA NA %TRC violations,(SNC is>=33 %)_> N/A 0 0 NA NA NA NA T. Phosphorus Total Molybdenum TKN FOG 1st 6 months 2nd 6 months 1st 6 months Ind 6 months 1st 6 months 2nd 6 months 1st 6 months 2nd 6 months Total #of samples=> 1 1 1 I 1 I 1 1 * Maximum (mg/1)_> 0.418 0.381 0.063 0.054 101 81.3 <5 <5 * or Maximum (1b/d)=> *or 6 mos.Using 1/2 BDL Average(mg/1)=> 0.418 0.381 0.063 0.054 101 81.3 2.5 2.5 * or Average Loading(lb/d)=> %violations,(chronic SNC is>=66%)_> NA NA NA NA 0 0 0 0 %TRC violations, (SNC is>=33 %)_> NA NA NA NA 0 0 0 0 BDL=>Below Detection Limit mg/I=>milligrams per liter * POTW must enter at least one of these IUP=>Industrial User Permit Ib/d=>pounds per day four rows, Please indicate how averages were calculated SNC=>Significant Non-Compliance mgd=>million gallons per day Avg period could be month,Qtr,or 6-month&if BDL, 1/2BDL,or zero values used. TRC=>Technical Review Criteria WWTP=>wastewater treatment plant Chapter: PAR Guidance File name: P1Vudfl3Slhm4sidediaicdcdEihalrtettBds etBA1413,pages 12, 13, 14 Blank IDSF Form,Copy and use in your PAR Number each set for each IUP pipe-Page of Workbook Name : HWAATDesign (February 2008) (4)- revised with TP update for July 1 2018 - June 3CP2OsP8Maiiiilsiiiitilm Page 1 of 5 Name: AT Allocation Table Spreadsheet Instructions: Headworks last approved: 10/03/18 1)Applicable Values should be entered in the Heavy Bordered cells. Rest of worksheet is protected,password is Allocation Table updated: 10/24/18 2)Formulas are discussed in the Comprehensive Guidance,Chapter 6,Section C. Permits last modified: 10/24/18 3)HWA and AT worksheets in this workbook are linked. Pollutant Names,MAHI.s,Basis,and Uncontrollable load in this AT worksheet are automatically entered from the HWA spreadsheet. This includes pollutant names in columns AT through BK. POTw=> Graham NPDES , NC0021211 FLOW BOD TSS Industry Type Renewal Modification Date Permit Limits Permit Limits Permit Limits IUP INDUSTRY NAMES Permit Pipe of Effective Effective Permit Conc. Load Conc. Load Count (please listulphubdicly) number number Industry Date Date Expires MGD gal/day mg/1 lbs/day mg/1 lbs/day 1 Cintas Corp. 0007 0001 >25,000 06/13/17 06/30/21 0.1100 110,000 1000.00 917.40 250.00 229.35 2 LuxferGas Cylinders 2001 0001 467 07/01/16 06/30/21 0.0800 80,000 400.00 266.88 250.00 166.80 3 Novaflex I001 0002 428 07/01/16 06/30/21 0.0350 35,000'. 400.00 116.76 250.00 72.98 4 Prescient 3001 0001 433 10/24/18 05/01/22 0.0100 10,000 300.00 25.02 250.00 20.85 w 5 Stericycle 0030 0001 >25,000 07/01/16 06/30/21 0.0300 30,000` 400.00 100.08 250.00 62.55 6 7 8 I 9 10 Column Totals=> 0.2650 265,000 1426 553 Basis=> NPDES NPDES Design MAHL from HWA(lbs/day)=> NPDES Permitted Flow=> 3.5000 10� 4343 10946 Uncontrollable Loading(lbs/day)_> 1.5999 4123 4617 Total Allowable for Industry(MAIL)(lbs/day)-> 1.9001 6211 6330 Total Permitted to Industry(lbs/day)_> 0.2650 1426 553 MAIL left abs/day)_> 1.6351 4784 5777 Percent Allow.Ind.(MAIL)still available(%)=> _ 86.1% 77.0% 91.3% Percent MAHL still available(%)_> 46.7% 46.3% 52.8% 5 Percent MAHL(lbs/day)=> 0.1750 517 547 HWA.AT Revised:November 2005 Workbook Name : HWAATDesign (February 2008) (4)- revised with TP update for July 1 2018 - June 3( Oe1 W sh Name: AT Page 2 of 5 Allocation Table Headworks last approved: 10/03/18 Allocation Table updated: 10/24/18 Permits last modified: 10/24/18 Pony,-, Graham NPDEs > NC0021211 TKN for Ammonia Arsenic Cadmium Chromium Copper Cyanide Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Cone. Load Conc. Load Conc. Load Conc. Load Count (pleur last alphaattid}9 number number mg/I Ibs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/I lbs/day 1 Cintas Corp. 0007 0001 100.00 91.74 0.0500 0.0459 0.7500 0.6881 0.5000 0.45871 0.1500 0.1376 2 LuxferGas Cylinders 2001 0001 100.00` 66.72 i 0.0500 0.0334 0.0920 0.0614 0.5000 0.3336 0.0490 0.0327 3 Novaflex 100I 0002 100.00 29.19 0.0500 0.0146 0.7500 0.2189 0.5000 0.1460 0.1500 0.0438 4 Prescient 3001 0001 100.00 8.34 0.0700 0.0058 0.7500 0.0626 0.5000 0.0417 0.3000 0.0250 5 Stericycle 0030 0001 200.00, 50.04 0.0500 0.0125 0.7500 0.1877 0.5000 0.1251 0.1500 0.0375 6 7 8 9 .� 10 Column Totals-> 246 0.0000 0.1122 1.2186 1.1051 0.2766 Sludge AS/Nit/TF Ceiling AS/NitfTF Sludge AS/Nit/TF Basis=> Design inhibition HASL inhibition Ceiling inhibition MAHL from HWA(Ibs/day)_> 875.70r 1.4984 0.2976 6.9284 4.3775 2.0526 Uncontrollable Loading(lbs/day)_> 394.96 0.1668 0.0147 0.0974 0.6031 0.0334 Total Allowable for Industry(MAIL)(lbs/day)=> 480.74 1.3316 0.2829 6.8310 3.7744 2.0192 Total Permitted to Industry(lbs/day)_> 246.03 0.0000 0.1122 1.2186 1.1051 0.2766 MAIL left(lbs/day)_> 234.71 1.3316 0.1707 5.6125 2.6694 1.7426 Percent Allow.Ind.(MAIL)still available(%)=> 48.8% 100.0% 60.3% 82.2% 70.7% 86.3% Percent MAHL still available(%)=> 26.8% 88.9% 57.4% 81.0% 61.0% 84.9% 5 Percent MAHL(lbs/day)=> 43.79. 0.0749 0.0149 0.3464' 0.2189 0.1026 HWA.AT Revised:November 2005 i 2 Workbook Name : HWAATDesign (February 2008) (4)- revised with TP update for July 1 2018 - June 30°2,9,W Fsii Page 3 of 5 Name: AT Allocation Table Headworks last approved: 10/03/18 Allocation Table updated: 10/24/18 Permits last modified: 10/24/18• POTW=> Graham NPDES ' NC0021211 Lead Mercury Molybdenum Nickel Selenium Silver Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc_ Load Conc. Load Conc. Load Count , (pl¢sc list alpbabeuay) number number mg/l lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day I Cintas Corp. 0007 0001 0.2000 0.I835 0.00020 0.00018 0.2000 0.1835 2 LuxferGas Cylinders 2001 0001 , 0.1500 0.1001 0.2000 0.1334 3 Novaflex 1001 0002 0.2000 0.0584 0.2000 0.0584 4 Prescient 3001 0001 0.2000 0.0167 0.2000i 0.0167 0.0500 0.0042 5 Stericycle 0030 0001 0.1500 0.0375 0.4000 0.1001 i- 6 r 7 9 10 ► r Column Totals=> 0.3962, 0.000183, 0.0000 0.4921 0.0000 0.0042 Cumul. Sludge Sludge Sludge Sludge Sludge Stream Basis=> Ceiling Loading Ceiling Ceiling Ceiling Std MAHL from HWA(lbs/day)_> 1.0689 0.043643 0.1764 0.7762 0.1552 0.0476 Uncontrollable Loading(lbs/day)=> 0.2135 0.001601 0.0734 0.0907 0.1388 0.0334 Total Allowable for Industry(MAIL)(lbs/day)_> 0.8554 0.042042 0.1030 0.6855 0.0165 0.0142 Total Permitted to Industry(lbs/day)_> 0.3962 0.000183 0.0000 0.4921 0.0000 0.0042 MAIL left(lbs/day)=> 0.4593 0.041858 0.1030 0.1935 0.0165 0.0100 Percent Allow.Ind.(MAIL)still available(%)=> 53.7% 99.6% 100.0% 28.2% 100.0% 70.6% Percent MAHL still available(%)=> 43.0% 95.9% 58.4% 24.9% 10.6% 21.1% 5 Percent MAHL(lbs/day)_> 0.0534 0.002182 0.0088 0.0388 0.0078 0.0024 HWA.AT Revised:November 2005 Workbook Name : HWAATDesign (February 2008) (4)- revised with TP update for July 1 2018 - June 361949FiN Psi Name: AT Page 4 of 5 Allocation Table Headworks last approved: 10/03/18 Allocation Table updated: 10/24/18 Permits last modified: 10/24/18 POTw=> Graham NPnesS> NC0021211 Zinc Total Nitrogen Total Phos. 0 d e Industry Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits Permit Limits IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load Conc. Load Count 1 (picue list yphabeticly) number number mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day I Cintas Corp. 0007 0001 1.5000 1.3761 10.00 9.17 2 LuxferGas Cylinders 2001 0001 0.2610 0 741 3 Novaflex 1001 0002 1.5000 0.4379 4 Prescient 3001 0001 0.7500 0.0626 5 Stericycle 0030 0001 1.5000 0.3753 • 6 R , , 7 8 9 Column Totals=> 2.4259 f 0.00 9.17 0.0000 0.0000 0.0000 Sludge Basis=> Ceiling NPDES MARL from HWA(lbs/day)_> 9.8342 208.41 Uncontrollable Loading(lbs/day)=> 2.7260 92.26 Total Allowable for Industry(MAIL)(lbs/day)=> 7.1082 116.15 Total Permitted to Industry(lbs/day)=> 2.4259 0.00 9.17 0.0000 0.0000 0.0000 MAIL left(lbs/day)=> 4.6822 106.97 Percent Allow.Ind.(MAIL)still available(%)=> 65.9% ####### 92.1 % ####### ####### ##�##### Percent MAHL still available(%)=> 47.6% ####### 51.3% ####### ####### ####### 5 Percent MAHL(lbs/day)=> 0.4917 10.4203 HWA.AT Revised:November 2005 Workbook Name : HWAATDesign (February 2008) (4)- revised with TP update for July 1 2018 - June 3o20 9 Psii m Page 5 of 5 Name: AT Allocation Table Headworks last approved: 10/03/18 Allocation Table updated: 10/24/18 Permits last modified:, 10/24/18 Porw=> Graham NPDESt�> NC0021211 f g h [ Industry Permit Limits Permit Limits Permit Limits Permit Limits IUP INDUSTRY NAMES Permit Pipe Conc. Load Conc. Load Conc. Load Conc. Load Count (plc i nalphab„a,) number number mg/1 lbs/day mg/1 lbs/day mg/1 lbs/day mg I lbs/day 1 Cintas Corp. 0007 0001 2 LuxferGas Cylinders 2001 0001 3 Novaflex 1001 0002 4 Prescient 3001 0001 5 Stericycle 0030 0001 6 7 3 9 to —� Column Totals=> 0.0000 0.0000 0.0000 0.0000 Basis=> MAHL from HWA(lbs/day)=> Uncontrollable Loading(lbs/day)_> Total Allowable for Industry(MAIL)(lbs/day)=> Total Permitted to Industry(lbs/day)=> 0.0000 0.0000 0.0000 0.0000 MAIL left(lbs/day)_> Percent Allow.Ind.(MAIL)still available(%)_> ####### ####### ####### ####### Percent MAUL still available(%)_> ####### ####### ####### ####### 5 Percent MAHL(lbs/day)_> HWA.AT Revised:November 2005 Titg of ( rallant P. 0 Drawer 357 201 South Main Street Graham, North Carolina 27253 Tel: (336) 570-6700/Fax: (336) 570-6703 February 27, 2020 PUBLIC NOTICE OF INDUSTRIES IN NON-COMPLIANCE WITH PRETREATMENT STANDARDS FOR JANUARY 1, 2019—DECEMBER 31, 2019: THERE ARE NO PUBLIC NOTICES FOR THIS TIME PERIOD DUE TO THE FACT THAT THERE WERE NO INDUSTRIES IN SIGNIFICANT NON-COMPLIANCE FOR THE JANUARY 1, 2019 THROUGH DECEMBER 31, 2019 REPORTING PERIOD. Respectfully Submitted, 1 ' Shelby S. Smith City of Graham Appendix E: Effluent Parameter Data for Table C from 2017-2019. Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 i Revised Date: 3/30/2017 Contact: Cris Routh Report Date: 3/28/2017 Client: Graham,City of NPDES #: NC0021211 P.O.Drawer 357 P.O.#: Credit Card Graham, NC 27253 Date Sample Rcvd: 3/16/2017 Meritech Work Order# 03161724 Sample: Plant Effluent Composite 3/15-16/17 Parameters Result Analysis Date Reporting Limit Method Total Dissolved Solids 956 mg/L 3/16/17 10.0 mg/L SM 2540C Ammonia,Nitrogen <0.1 mg/L 3/20/17 0.1 mg/L EPA 350.1 TKN 1.63 tng/L 3/22/17 0.20 mg/L EPA 351.1 Nitrate/Nitrite,Nitrogen 13.60 mg/L 3/17/17 0.10 mg/L EPA 353.2 Nitrogen,total 15.23 mg/L 3/22/17 0.20 mg/L EPA 353.2 Antimony,total <0.025 mg/L 3/21/17 0.025 mg/L EPA 200.7 Arsenic,total <0.010 mg/L 3/21/17 0.010 mg/L EPA 200.7 Beryllium,total <0.005 mg/L 3/21/17 0.005 mg/L EPA 200.7 Cadmium,total <0.002 mg/L 3/21/17 0.002 mg/L EPA 200.7 Chromium,total <0.005 mg/L 3/21/17 0.010 mg/L EPA 200.7 Copper,total 0.018 mg/L 3/21/17 0.002 mg/L EPA 200.7 Lead,total <0.010 mg/L 3/21/17 0.010 mg/L EPA 200.7 Nickel,total <0.010 mg/L 3/21/17 0.010 mg/L EPA 200.7 Phosphorus,total 0.738 mg/L 3/21/17 0.020 mg/L EPA 200.7 Selenium,total <0.010 mg/L 3/21/17 0.010 mg/L EPA 200.7 Silver,total <0.005 mg/L 3/21/17 0.005 mg/L EPA 200.7 Thallium,total <0.020 mg/L 3/21/17 0.020 mg/L EPA 200.7 Zinc,total 0.079 mg/L 3/21/17 0.010 mg/L EPA 200.7 Hardness (titration) 64 mg/L 3/23/17 1 mg/L SM 2340C Meritech Work Order# 03161725 Sample: Plant Effluent Grab 3/16/17 Parameters Result Analysis Date Reporting Limit Method Cyanide,total <0.005 mg/L 3/22/17 0.005 mg/L EPA 335.4 Oil&Grease (HEM) <5 mg/L 3/20/17 5 mg/L EPA 1664A Phenols,total 0.021 mg/L 3/17/17 0.010 mg/L EPA 420.1 EPA 624 - Attached 3/27/17 - 624 EPA 625 Attached 3/25/17 - 625 I hereby certify that I have reviewed and approve these data. G. lint-- Laboratory Representative 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, INC. Environmental Laboratories Laboratory Certification#165 Client: City of Graham WWTP Meritech ID#: 03161725 Project: 624 Analysis: 03/27/17 Client Sample ID: Plt.Effluent Analyst: VWV Sample Collection: 03/16/17 Dilution Factor: 1 Report Date: 03/28/17 EPA 624 VOLATILE ORGANICS Parameter Result Benzene < 1.00 ug/L Dichlorobromomethane 5.44 ug/L Bromoform < 1.00 ug/L Methyl Bromide <5.00 ug/L Carbon Tetrachloride < 1.00 ug/L Chlorobenzene < 1.00 ug/L Chloroethane <5.00 ug/L 2-Chloroethyl vinyl ether <5.00 ug/L Chloroform 5.14 uglL Methyl Chloride <5.00 ug/L Chlorodibromomethane 4.78 ug/L 1,2-Dibromoethane <1.00 ug/L 1,1-Dichloroethane <1.00 ug/L 1,2-Dichloroethane < 1.00 ug/L 1,4-Dichlorobenzene < 1.00 ug/L 1,2-Dichlorobenzene < 1.00 ug/L 1,3-Dichlorobenzene < 1.00 ug/L 1,I-Dichloroethyiene < 1,00 ug/L trans-1,2-Dichloroethylene < 1.00 ug/L 1,2-Dichloropropane < 1.00 ug/L cis-1,3-Dichloropropylene < 1.00 ug/L trans-1,3-Dichloropropylene < 1.00 ug/L Ethyl benzene < 1.00 uglL Methylene chloride < 1.00 ug/L 1,1,2,2-Tetrachloroethane <1.00 ug/L Tetrachloroethylene <1.00 ug/L Toluene < 1.00 ug/L 1,I,1-Trichloroethane < 1.00 ug/L 1,1,2-Trichloroethane < 1.00 ug/L Trichloroethylene < 1.00 ug/L Trichlorofluoromethane <5.00 ug/L Vinyl chloride <5.00 ug/L Additional Compounds Acrolein <50.0 ug/L Acrylonitrile <10.0 ug/L I hereby certify that I have reviewed and approve these data. 4 . ear..4 Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax . . , MERITECH, INC. a Environmental Laboratories ' • Laboratory Certificate#165 Client: City of Graham WWTP Meritech ID#: 03161725 Project: 625 Analysis: 03/25/17 Client Sample ID: Plt.Effluent Extraction: 03/20/17 Sample Collection: 03/16/17 Analyst: PM Dilution Factor: 1 EPA 625 SEMIVOLATILE ORGANICS Parameter Result Parameter Result Acenaphthene <10 ug/L Fluoranthene <10 ug/L Acenaphthylene <10 ug/L Fluorene <10 ug/L Anthracene <10 ug/L Hexachlorobenzene <10 ug/L Benzidine <50 ug/L Hexachlorobutadiene <10 ug/L Benzo(a)anthracene <10 ug/L Hexachlorocyclopentadiene <50 ug/L Benzo(a)pyrene <10 ug/L Hexachloroethane <10 ug/L Benzo(b)fluoranthene <10 ug/L Indeno(1,2,3-cd)pyrene <10 ug/L Benzo(k)fluoranthene <10 ug/L Isophorone <10 ug/L Benzo(g,h,i)peiylene <10 ug/L 2-Methylnaphthalene <10 ug/L Benzyl butyl phthalate <10 ug/L Naphthalene <10 ug/L Bis(2-chloroethoxy)methane <10 ug/L Nitrobenzene <10 ug/L Bis(2-chloroethyl)ether <10 ug/L N-Nitrosodimethylamine <10 ug/L Bis(2-chloroisopropyl)ether <10 ug/L N-Nitrosodi-n-propylamine <10 ug/L Bis(2-ethyIhexyl)phthalate <10 ug/L N-Nitrosodiphenylamine <10 ug/L 4-Bromophenyl phenyl ether <10 ug/L Phenanthrene <10 ug/L 2-Chloronaphthalene <10 ug/L Pyrene <10 ug/L 4-Chlorophenyl phenyl ether <10 ug/L 1,2,4-Trichlorobenzene <10 ug/L Chrysene <10 ug/L Dibenzo(a,h)anthracene <10 ug/L 4-Chloro-3-methylphenol <10 ug/L 1,2-Dichlorobenzene <10 ug/L 2-Chlorophenol <10 ug/L 1,3-Dichlorobenzene <10 ug/L 2,4-Dichlorophenol <10 ug/L 1,4-Dichlorobenzene <10 ug/L 2,4-Dimethylphenol <10 ug/L 3,3'-Dichlorobenzidine <50 ug/L 2,4-Dinitrophenol <50 ug/L Diethyl phthalate <10 ug/L 4,6-Dinitro-2-methylphenol <50 ug/L Dimethyl phthalate <10 ug/L 2-Nitrophenol <10 ug/L Di-n-butyl phthalate <10 ug/L 4-Nitrophenol <50 ug/L 2,4-Dinitrotoluene <10 ug/L Pentachlorophenol <50 ug/L 2,6-Dinitrotoluene <10 ug/L Phenol <10 uglL Di-n-octyl phthalate <10 ug/L 2,4,6-Trichlorophenol <10 ug/L 1,2-Diphenylhydrazine <10 ug/L I hereby certify that I have reviewed and approve these data. b_ &,..77 Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax 5-9-2016 Chain of Custody Record (COC) NPDES#: JUCoo'3-I Z.1 I Client: C.A.-11 Of G( J\O' w iittriP Phone: 336 -570 - ld -721 M E RITECH, INC. Address: ?• O . £ra e. - 357 Fax: g -5f3-s5o 2 ors ENVIRONMENTAL LABORATORIES 6-ecxi1Go-\) N" C., aj.as3 Email: G`dLL4-,6 C.:4).cir a...�^^ r;~. 642 Tamco Rd. Phone: 336-342-4748 Project: nn__,n, � 0 ,w� •' Reidsville NC 27320 Fax 336-342-1522 P.O.#: QPtCt: e-(41-4 4,` Email: info@meritechlabs.com Cr)5 4orc*'., Turn Around Time* @ Attention: How would you like your report sent? *RUSH work needs prior approval. WWW.111eCl$I?ChiabS.cc�rn t ` sd{10 Ys) - s 24-48Hrs Circle all that apply:( Email (preferred) Fax, Mail i -;; Person T ki g Sam le(Sign/Print): )e) Sampling Dates &Times , : rcf- AAd Gk^,s Sl,el1xi Lab Use Only Sample Location and/or ID # Start End Comp? #of On Ice' e pH OK? Date Time Date Time Grab? Cont. Test(s) Required / N7 CI OK? V. E L - 3/I.sll- o 9 oo 3/,e Jo as- C H T. P6.55. )~-b s -ro N: .(NQzt ) 1 N o 31 TKN' N H3iq , Havd n4 , ---•-- re.- 4Q(5 . ) Rs. )ge,. Cd. ,Cf, C.,, : , N 't , ,e , N. )71e , 2n .) ���catl,e�'� n -5 e 1pC R��, f tee, -�1&� , g 9 C �? C.n o 0 I 1 4-G ) T- o4s, -- 6a s- 6 a5(+ ;k_ ccy,�. . �, Pad ��c4� ,c �,�.aa , � ) Temperature Upon Receipt: `��IC Method of ***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done in the field prior to preservation.*** I, Comments: Compositor# Shipment: UPS Jug# L Fed Ex Are these results for regulatory purposes? Yes No • Report results in: mg/L mg/kg ug/L I.,., R i cashed D te: Tire• Rec by D e: Ti and Delivery -1 i io�J� ri3 z p (Q/I✓1't,L._. v r //z7t "7 " Z_d Other Relinq h d bye ��_ j ((iDI�: Time: Received by: t Date: Time: _ • -4 Relinquis ed by: Date: Time: R wed Lit 3 J lc !at, Tpn1 I Meritech, Inc. , Environmental Laboratory Laboratory Certification No. 165 4 s Contact: Cris Routh Report Date: 7/9/2018 Client: Graham,City of NPDES#: NC0021211 P.O. Drawer 357 P.O. #: Credit Card Graham,NC 27253 Date Sample Rcvd: 6/19/2018 Meritech Work Order# 06191828 Sample: Plant Effluent Composite 6/18-19/18 Parameters Result Analysis Date Reporting Limit Method Total Dissolved Solids 1040 mg/L 6/19/18 10.0 mg/L SM 2540C Ammonia, Nitrogen <0.1 mg/L 6/25/18 0.1 mg/L EPA 350.1 TKN 0.20 mg/L 6/26/18 0.20 mg/L EPA 351.1 Nitrate/Nitrite,Nitrogen 20.3 mg/L 6/20/18 0.10 mg/L EPA 353.2 Nitrogen,total 20.50 mg/L 6/26/18 0.20 mg/L EPA 353.2 Antimony,total <0.025 mg/L 6/25/18 0.025 mg/L EPA 200.7 Arsenic,total <0.010 mg/L 6/25/18 0.010 mg/L EPA 200.7 Beryllium,total <0.005 mg/L 6/25/18 0.005 mg/L EPA 200.7 Cadmium,total <0.002 mg/L 6/25/18 0.002 mg/L EPA 200.7 Chromium,total <0.005 mg/L 6/25/18 0.010 mg/L EPA 200.7 Copper,total 0.011 mg/L 6/25/18 0.002 mg/L EPA 200.7 Lead,total <0.010 mg/L 6/25/18 0.010 mg/L EPA 200.7 Nickel,total <0.010 mg/L 6/25/18 0.010 mg/L EPA 200.7 Phosphorus, total 0.337 mg/L 6/25/18 0.020 mg/L EPA 200.7 Selenium,total <0.010 mg/L 6/25/18 0.010 mg/L EPA 200.7 Silver,total <0.005 mg/L 6/25/18 0.005 mg/L EPA 200.7 Thallium,total <0.020 mg/L 6/25/18 0.005 mg/L EPA 200.7 Zinc,total 0.060 mg/L 6/25/18 0.010 mg/L EPA 200.7 Hardness (titration) 56 mg/L 6/21/18 1 mg/L SM 2340C Meritech Work Order# 06191829 Sample: Plant Effluent Grab 6/19/18 Parameters Result Analysis Date Reporting Limit Method Cyanide,total <0.005 mg/L 6/20/18 0.005 mg/L EPA 335.4 Oil&Grease (HEM) <5 mg/L 6/25/18 5 mg/L EPA 1664B Phenols,total 0.047 mg/L 6/25/18 0.010 mg/L EPA 420.1 EPA 624+Acrolein+Acrylinitrile Attached 7/2/18 - - 624 EPA 625 BNA Attached 7/5/18 - - 625 I hereby certify that I have reviewed and approve these data. aboratory Representative 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 • MERITECH INC. _ = Environmental Laboratories Laboratory Certification#165 • Client: City of Graham WWTP Meritech ID#: 06191829 Project: Plant Effluent Analysis: 07/02/18 Client Sample ID: Plt.Effluent Analyst: VWV Sample Collection: 06/19/18 Dilution Factor: 1 Report Date: 07/05/18 EPA 624.1 VOLATILE ORGANICS Parameter Result Benzene < 1.00 ug/L Dichlorobromomethane 7.99 ug/L Bromoform < 1.00 ug/L Methyl Bromide <5.00 ug/L Carbon Tetrachloride < 1.00 ug/L Chlorobenzene < 1.00 ug/L Chloroethane <5.00 ug/L 2-Chloroethyl vinyl ether <5.00 ug/L Chloroform 7.23 ug/L Methyl Chloride <5.00 ug/L Chlorodibromomethane 4.83 ug/L 1,2-Dibromoethane < 1.00 ug/L 1,1-Dichloroethane < 1.00 ug/L 1,2-Dichloroethane < 1.00 ug/L I,4-Dichlorobenzene < 1.00 ug/L 1,2-Dichlorobenzene < 1.00 ug/L 1,3-Dichlorobenzene < 1.00 ug/L 1,1-Dichloroethylene < 1.00 ug/L trans-1,2-Dichloroethylene < 1.00 ug/L 1,2-Dichloropropane < 1.00 ug/L cis-1,3-Dichloropropylene < 1.00 ug/L trans-1,3-Dichloropropylene <1.00 ug/L Ethyl benzene < 1.00 ug/L Methylene chloride < 1.00 ug/L 1,1,2,2-Tetrachloroethane < 1.00 ug/L Tetrachloroethylene < 1.00 ug/L Toluene < 1.00 ug/L 1,1,1-Trichloroethane < 1.00 ug/L 1,1,2-Trichloroethane <1.00 ug/L Trichloroethylene < 1.00 ug/L Trichlorofluoromethane <5.00 ug/L Vinyl chloride <5.00 ug/L Additional Compounds Acrolein <50.0 ug/L Aciylonitrile <10.0 ug/L I hereby certify that I have reviewed and approve these data. Labor}atoryy Rep sentative 642 Talmo Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax MERITECH, INC. -= Environmental Laboratories Laboratory Certificate#165 Client: City of Graham WWTP Merited)ID#: 06191829 Project: 625 Analysis: 07/05/18 Client Sample ID: Plt. Effluent Extraction: 06/25/18 Sample Collection: 06/19/18 Analyst: PM Dilution Factor: 1 EPA 625.1 SEMIVOLATILE ORGANICS Parameter Result Parameter Result Acenaphthene <10 ug/L Fluoranthene <10 ug/L Acenaphthylene <10 ug/L Fluorene <10 ug/L Anthracene <10 ug/L Hexachlorobenzene <10 ug/L Benzidine <50 ug/L Hexachlorobutadiene <10 ug/L Benzo(a)anthracene <10 ug/L Hexachlorocyclopentadiene <50 ug/L Benzo(a)pyrene <10 ug/L Hexachloroethane <10 ug/L Benzo(b)fluoranthene <10 ug/L Indeno(1,2,3-cd)pyrene <10 ug/L Benzo(h)fluoranthene <10 ug/L Isophorone <10 ug/L Benzo(g,h,i)perylene <10 ug/L 2-Methylnaphthalene <10 ug/L Benzyi butyl phthalate <10 ug/L Naphthalene <10 ug/L Bis(2-chloroethoxy)methane <10 ug/L Nitrobenzene <10 ug/L Bis(2-chloroethyl)ether <10 ug/L N-Nitrosodimethylamine <10 ug/L Bis(2-chloroisopropyl)ether <10 ug/L N-Nitrosodi-n-propylamine <10 ug/L Bis(2-ethylhexyl)phthalate <10 ug/L N-Nitrosodiphenylamine <10 ug/L 4-Bromophenyl phenyl ether <10 ug/L Phenanthrene <10 ug/L 2-Chloronaphthalene <10 ug/L Pyrene <10 ug/L 4-Chlorophenyl phenyl ether <10 ug/L 1,2,4-Trichlorobenzene <10 ug/L Chrysene <10 ug/L Dibenzo(a,h)anthracene <10 ug/L 4-Chloro-3-methylphenol <10 ug/L 1,2-Dichlorobenzene <10 ug/L 2-Chlorophenol <10 ug/L 1,3-Dichlorobenzene <10 ug/L 2,4-Dichlorophenol <10 ug/L 1,4-Dichlorobenzene <10 ug/L 2,4-Dimethylphenol <10 ug/L 3,3'-Dichlorobenzidine <50 ug/L 2,4-Dinitrophenol <50 ug/L Diethyl phthalate <10 ug/L 4,6-Dinitro-2-methylphenol <50 ug/L Dimethyl phthalate <10 ug/L 2-Nitrophenol <10 ug/L Di-n-butyl phthalate <10 ug/L 4-Nitrophenol <50 ug/L 2,4-Dinitrotoluene <10 ug/L Pentachlorophenol <50 ug/L 2,6-Dinitrotoluene <10 ug/L Phenol <10 ug/L Di-n-octyl phthalate <10 ug/L 2,4,6-Trichlorophenol <10 ug/L 1,2-Diphenylhydrazine <10 ug/L I hereby certify that I have reviewed and approve these data. (/, ,-- w (/,,,.1- Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax .-9.2016 Chain of Custody Record (COC) NPDES#: ki C0021 L l I Client: �a 0 f i G "\c VJ-1.S►-,p Phone: ,-- i, -J� 90 - 4,7 2 I E ITCM Address: P. . A 1` 367 Fax: 33 C:s -J). —530 2— v,,,, ;, ENVIRONMENTAL LABORATORIES G kci ,.j N'G a-7 )1/453 Email: OC:4rP art.e.,2", 642 Tamco Rd. Phone: 336-342-4748 Project: K>> '"' Reidsville NC 27320 Fax: 336-342-1522 P.O.#: ..Mct Caid Email:info@meritechlabs.com Attention: Cr o� P Turn Around Time* *RUSH work needs prior approval. How would you like your report sent? V1!\NW.merltechlabs.C®rl std(10 .. s 24-48Hrs Circle all that apply: Emai (preferred), Fax Mail Sampling Dates &Times Persq�n Taking Sa ple(Si �/ rint): lv1t �` r. -1 ' , 1.i 1�.hS Ste` Lab Use Only Sample Location and/or ID# Start End Comp? #of On Ice? Yes pH OK? Date Time Date Time Grab? Cont. Test(s) Required 4 / No Cl OK? Fi4, -f-Fcve - 6/ia1,a !° 50 'j9)18 IIoS Cr 3 -T P .. , 'TD5 ;To 10,4 ,„Lu02+ - No5 ,TKN) } NH3N ) Hcif-d ., ( 1, LS6d , A ..j Be_, CJ a Cr. )CA .d j Pt., r- . N ; , Sc. , Al . T LL 12n ) l'Q, A _ c�l q.3 C, CAIIS 1110 G Ci,. CI- 1 ,i- Gfe.pr,._ -1-04-A 1.1\401\01.s ---- 7 0,4 4 (O 15 ( u,cc `}2 0{)ov.;c C. r"Po clo j f cad 2.,a-rttir460..e.-Co^-,.?oc.n$Q 4 Sc== c„ .L.L _, _ ` `-r".4.---p p Temperature Upon Receipt: c�i ' 0.Ju5a }�1 cam'Cf1U+e4�C: G Method of ***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done in the field prior to preservation.*** 3' Comments: Compositor# Shipment: UPS Jug# Fed Ex Are these results for regulatory purposes? Yes No Report results in: mg/L 4�Fmg/k g ug/L Re' q ish y: te: Tien Received b ate: Time: zHii ndDelivery - l—j F ',©� j�( \ ��" 6// /i / €9.5- Relinquished at / Time: i eceiv by: Date: Time: Other / --- 67t JI 8 /31 s v Relinquished by: / Date: Time: Receiv by Lab: Date: Time: , Permit No. NC002.121 i ,A (9.) EFFLUENT POLLUTANT SCAN The Permittee shall perform a total of three (3) Effluent Pollutant Scans for all parameters listed below. One scan must be performed in each of the following years: 2012, 2013, and 2014. Analytical methods shall be in accordance with 40 CFR Part 136 and shall be sufficiently sensitive to determine whether parameters are present in concentrations greater than applicable standards and criteria. Samples should be collected with one quarterly toxicity test each year, and must represent seasonal variation [i.e., do not sample in the same quarter every year]. Unless otherwise indicated, metals shall be analyzed as "total recoverable." Ammonia(as N) Trans-1,2-d ichloroethylene Bis(2-chloroethyl)ether Chlorine(total residual,TRC) 1,1-dichloroethylene 13is(2-chioroisopropyl)ether Dissolved oxygen 1,2-dichloropropane Bis(2-ethylhexyl)phthalate Nitrate/Nitrite 1,3-dichloropropylene 4-bromophenyl phenyl ether Kjeldahl nitrogen Ethylbenzene Butyl benzyl phthalate Oil and grease Methyl bromide 2-chloronaphthalene Phosphorus Methyl chloride 4-chlorophenyl phenyl ether Total dissolved solids Methylene chloride Chrysene Hardness 1,1,2,2-tetrachloroethane Di-n-butyl phthalate Antimony Tetraachloroethylene Di-n-octyl phthalate Arsenic Toluene Dibenzo(a,h)anthracene Beryllium 1,1,1-trichloroethane 1,2-dichlorobenzene Cadmium 1,1,2-trichloroethane 1,3-dichlorobenzene Chromium Trichloroethylene I,4-dichlorobenzene Copper Vinyl chloride 3,3-dichlorobenzidine Lead Acid-extractable compounds: Diethyl phthalate Mercury(EPA Method 1631 E) P-chloro-m-cresol Dimethyl phthalate Nickel 2-chlorophenol 2,4-dinitrotoluene Selenium 2,4-dichlorophenol 2,6-dinitrotoluene Silver 2,4-dimethylphenol 1,2-diphenylhydrazine Thallium 4,6-dinitro-o-cresol Fluoranthene Zinc 2,4-dinitroplienol Fluorene • Cyanide 2-nitrophenol Hexachlorobenzene Total phenolic compounds 4-nitrophenol Hexachlorobutadiene Volatile organic compounds: Pentachlorophenol Hexachlorocyclo-pentadiene Acrolein Phenol liexachloroethane Acrylonitrile 2,4,6-trichlorophenol Indeno(1,2,3-cd)pyrene Benzene Base-neutral compounds: Isophorone Bromofonn Acenaphthene Naphthalene Carbon tetrachloride Acenaphthytene Nitrobenzene Chlorobenzene - Anthracene s N-nitrosodi-n-propylamine Chlorodibromomethane Benzidine N-nitrosodimethylamine Chloroethane 13enzo(a)anthracene N-nitrosodiphenylamine - 2-chloroethylvinyl ether Benzo(a)pyrene Phenanthrene Chloroform 3,4 benzofluoranthene Pyrene Dich lorobromomethane Benzo(ghi)perylene I,2,4-trichlorobenzene 1,1-dichloroethane Benzo(k)fluoranthene 1,2-d ichloroethane Bis(2-chloroethoxy)methane Reporting. Test results shall be reported on DWQ Form-A MR-PPA1 (or in a form approved by the Director)by December 31st of each designated sampling year. The report shall be submitted to the following address:NC DENR/DWQ/Central Files,1617 Mail Service Center,Raleigh,North Carolina 27699-1617. Page 110 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Cris Routh Report Date: 9/25/2019 Client: Graham,City of NPDES#: NC0021211 P.O.Drawer 357 P.O.#: Credit Card Graham,NC 27253 Date Sample Rcvd: 9/10/2019 Meritech Work Order# 091019119 Sample: Effluent Composite 9/9-10/19 Parameters Result Analysis Date Reporting Limit Method rotal Dissolved Solids 1320 mg/L 9/11/19 10.0 mg/L SM 2540C 9mmonia,Nitrogen 0.7 mg/L 9/16/19 0.1 mg/L EPA 350.1 TKN 1.97 mg/L 9/17/19 0.20 mg/L EPA 351.1 Nitrate/Nitrite,Nitrogen 0.22 mg/L 9/13/19 0.10 mg/L EPA 353.2 Nitrogen,total 2.19 mg/L 9/17/19 0.20 mg/L EPA 353.2 4ntimony,total 0.0043 mg/L 9/12/19 0.0005 mg/L EPA 200.8 4rsenic,total <0.002 mg/L 9/12/19 0.002 mg/L EPA 200.8 3eryllium,total <0.0005 mg/L 9/12/19 0.0005 mg/L EPA 200.8 ;admium,total <0.00015 mg/L 9/12/19 0.00015 mg/L EPA 200.8 ;hromium,total <0.002 mg/L 9/12/19 0.002 mg/L EPA 200.8 topper,total <0.002 mg/L 9/12/19 0.002 mg/L EPA 200.8 „ead,total 0.0019 mg/L 9/12/19 0.0005 mg/L EPA 200.8 Molybdenum,total 0.009 mg/L 9/12/19 0.002 mg/L EPA 200.8 Nickel, total 0.0039 mg/L 9/12/19 0.0005 mg/L EPA 200.8 ?hosphorus,total 0.270 mg/L 9/13/19 0.020 mg/L EPA 200.7 selenium,total <0.001 mg/L 9/12/19 0.001 mg/L EPA 200.8 ;liver,total <0.0005 mg/L 9/12/19 0.0005 mg/L EPA 200.8 Challium,total <0.0005 mg/L 9/12/19 0.0005 mg/L EPA 200.8 !inc,total 0.078 mg/L 9/12/19 0.005 mg/L EPA 200.8 lardness (titration) 68 mg/L 9/12/19 1 mg/L SM 2340C Meritech Work Order# 091019120 Sample: Effluent Grab 9/10/19 'arameters Result Analysis Date Reporting Limit Method :yanide,total <0.005 mg/L 9/17/19 0.005 mg/L EPA 335.4 )il&Grease (HEM) <5 mg/L 9/16/19 5 mg/L EPA 1664B 'henols,total <0.010 mg/L 9/20/19 0.010 mg/L EPA 420.1 sPA 624.1 Attached 9/12/19 - - 624.1 PA 625,1 Attached 9/19/19 - - 625.1 hereby certify that I have reviewed and approve these data. AQ iV ,bk.irWri 1 Laboratory Representative 642 Talmo Road,Reidsville,North Carolina 27320 te1 (336)342-4748 fax.(336)342-1522 MERI TECH INC. Environmental Laboratories Laboratory Certification#165 Client: City of Graham WWTP Meritech ID#: 091019120 Project: 624.1 Analysis: 09/12/19 Client Sample ID: Plt.Effluent Analyst: VWV Sample Collection: 09/10/19 Dilution Factor: 1 Report Date: 09/16/19 EPA 624.1 VOLATILE ORGANICS Parameter Result Benzene < 1.00 ug/L Dichlorobromomethane < 1.00 ug/L Bromoform < 1.00 ug/L Methyl Bromide <5.00 ug/L Carbon Tetrachloride < 1.00 ug/L Chlorobenzene < 1.00 ug/L Chloroethane <5.00 ug/L 2-Chloroethyl vinyl ether <5.00 ug/L Chloroform < 1,00 ug/L Methyl Chloride <5.00 ug/L Chlorodibromomethane < 1.00 ug/L 1,2-Dibromoethane < 1.00 ug/L 1,1-Dichloroethane < 1.00 ug/L 1,2-Dichloroethane < 1.00 ug/L 1,4-Dichlorobenzene < 1.00 ug/L 1,2-Dichlorobenzene < 1.00 ug/L 1,3-Dichlorobenzene < 1.00 ug/L 1,1-Dichloroethylene < 1.00 ug/L trans-1,2-Dichloroethylene < 1.00 ug/L 1,2-Dichloropropane < 1.00 ug/L cis-1,3-Dichloropropylene < 1.00 ug/L trans-1,3-Dichloropropylene < 1.00 ug/L Ethyl benzene < 1.00 ug/L Methylene chloride < 1.00 ug/L 1,1,2,2-Tetrachloroethane < 1.00 ug/L Tetrachloroethylene < 1.00 ug/L Toluene < 1.00 ug/L 1,1,1-Trichloroethane < 1.00 ug/L 1,1,2-Trichloroethane < 1.00 ug/L Trichloroethylene < 1.00 ug/L Trichlorofluoromethane <5.00 ug/L Vinyl chloride <5.00 ug/L Additional Compounds Acrolein <50.0 ug/L Acrylonitrile <10.0 ug/L I hereby certify that I have reviewed and approve these data. Lab ratory Repre tative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 * info@meritechlabs.com MERITECH, INC. ,„: - .. ,.. Environmental Laboratories Laboratory Certificate#165 Client: City of Graham Meritech ID#: 091019120 Project: 625.1 Analysis: 09/19/19 Client Sample ID: Pit.Effluent Extraction: 09/16/19 Sample Collection: 09/10/19 Analyst: PM Report Date: 09/23/19 Dilution Factor: 1 EPA 625.1 SEMIVOLATILE ORGANICS Parameter Result Parameter Result , Acenaphthene <10 ug/L Fluoranthene <10 ug/L Acenaphthylene <10 ug/L Fluorene <10 ug/L Anthracene <10 ug/L Hexachlorobenzene <10 ug/L Benzidine <50 ug/L Hexachlorobutadiene <10 ug/L Benzo(a)anthracene <10 ug/L Hexachlorocyclopentadiene <50 ug/L Benzo(a)pyrene <10 ug/L Hexachloroethane <10 ug/L Benzo(b)fluoranthene <10 ug/L Indeno(1,2,3-cd)pyrene <10 ug/L Benzo(k)fluoranthene <10 ug/L Isophorone <10 ug/L Benzo(g,h,i)perylene <10 ug/L 2-Methylnaphthalene <10 ug/L Benzyl butyl phthalate <10 ug/L Naphthalene <10 ug/L Bis(2-chloroethoxy)methane <10 ug/L Nitrobenzene <10 ug/L Bis(2-chloroethyl)ether <10 ug/L N-Nitrosodimethylamine <10 ug/L Bis(2-chloroisopropyl)ether <10 ug/L N-Nitrosodi-n-propylamine <10 ug/L Bis(2-ethylhexyl)phthalate <10 ug/L N-Nitrosodiphenylamine <10 ug/L 4-Bromophenyl phenyl ether <10 ug/L Phenanthrene <10 ug/L 2-Chloronaphthalene <10 ug/L Pyrene <10 ug/L 4-Chiorophenyl phenyl ether <10 ug/L 1,2,4-Trichlorobenzene <10 ug/L Chrysene <10 ug/L Dibenzo(a,h)anthracene <10 ug/L 4-Chloro-3-methylphenol <10 ug/L 1,2-Dichlorobenzene <10 ug/L 2-Chlorophenol <10 ug/L 1,3-Dichlorobenzene <10 ug/L 2,4-Dichlorophenol <10 ug/L 1,4-Dichlorobenzene <10 ug/L 2,4-Dimethylphenol <10 ug/L 3,3'-Dichlorobenzidine <50 ug/L 2,4-Dinitrophenol <50 ug/L Diethyl phthalate <10 ug/L 4,6-Dinitro-2-methylphenol <50 ug/L Dimethyl phthalate <10 ug/L 2-Nitrophenol <10 ug/L Di-n-butyl phthalate <10 ug/L 4-Nitrophenol <50 ug/L 2,4-Dinitrotoluene <10 ug/L Pentachlorophenol <50 ug/L 2,6-Dinitrotoluene <10 ug/L Phenol <10 ug/L Di-n-octyl phthalate <10 ug/L 2,4,6-Trichlorophenol <10 ug/L 1,2-Diphenylhydrazine <10 ug/L , I hereby certify that I have reviewed and approve these data. /4,,._iv,(4, Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 * info@meritechlabs.com 819;,6 Chain of Custody Record (COC) NPDES#: 0-,002.12.J 1 C. Client: C74f &o to , I1, Phone:33C "5-70 -�6,72 I r::: M BIOTECH IN 1 Address: . ; 1- 337 Fax: �.- 3 t�30 L ENVIRONMENTAL LABORATORIES (-11-t-cjoG NC a72.33 Email: CPO\ ('"cl c¢C7' pf c> aA &:AA E; 642 Tamco Rd. Phone: 336-342-4748 Project: rr }} _ ` � rP ' Reidsville NC 27320 Fax 336-342-1522 P.0.#: ae -. C'�S' , q, !�- Turn Around Time* Email: info@meritechlabs.com Attention: Cr:5 ,.h� ._. *RUSH work needs prior approval, How would you like your report sent? Charges Aooly www.meritechlabs.com Circle all that a PP y•I �tmail (preferred), Fax, Mail S ld(10 d 3-5 Da s 24-48 Hrs ti Person Taking Sample(Si n/Print): Sampling Dates &Times 61-,,, 5 5 ,1 . Lab Use Only Sample Location and/or ID# Start End com #of On ice? pH OK? Date Time Date Time Grab I Cont. Yes Required Yes / No CI OK? -, E. i 91 o )9 O90'2) 9 icA99 No-4 C. I T. PINos ,lei - " \I P -. vr,vkex' 1116-_�1039 )011 �:014C I _opt. c4c-t 7-jc V \ -, u,, 9 3 c# , i, , 9 l°))9 Gl`iot:4 _ - i 1,4-,1 N) : .(Nei 110-7(N 1 W3 _ V. -PF`,,+P 111 '1 .0903 9 foie r.1ge cyf C 1 i- 1 P)A. E-F-R.LA&(\-t 119119 O90 9kM oci k 0- I ► e- ( t s_ a (A @ . a.. 71. -in. 9 No .) 4 M' 900. Ae * } P I � ueAt 9 J 10 19 173s .---- G #7 C4.4.0i,f id , O 4-C . T - U4 s i ca-Ue 4 pr2cio Temperature Upon �r r i Receipt: '"\ Method of *** Dechlorination(<0.5 ppm)of Ammonia, Cyanide,Phenol and TKN samples must be done in the field prior to preservation.*** ° Shipment: fl Comments: t c`Civri C C \ a 1 Compositor# UPS Jug# Fed Ex Are these results for regulatory purposes? Yes No ❑: _ Report results in: mg/L I mg/kg d [ ug/L Relinggi e -y: 9_iDetf 11 Time)J bRecel b Y fQ0 -Q,yland Delivery 9/irate-if, TIn 0 Other Relinquishe y pi C tit I Time: f7Q� Rec ived by: Date: Time: Relinquished - 'Date' Time:( Received by Lab: iF- i�,, ( -- 4 Y : '4Ver ty, Time Permit No. NC002 LI1 ,A (9.) EFFLUENT POLLUTANT SCAN The Permittee shall perform a total of three (3) Effluent Pollutant Scans for aD parameters listed below. One scan must be performed in eadi of the following years: 2012, 2013, and 2014. Analytical methods shall be in accordance with 40 CFR Part and thanshall be Iicablehstandards sensitive and erifieriaetermine whether 5�Samples should parameters are present in concentrations greaterapplicable be collected with one quarterly toxicity test each otherwise u�dicated,si petals shall be analyzed asent seasonal variation [i.e., L�total sample in the same quarter every year]. Un � recoverable." Ammonia(as N) + Trans-I,2-dichloroethylene Bis(2-chloroethyl)ether Chlorine(total residual,TRC) 1,1-di chloroethylene 13is(2-chlorolsopropyl)ether I Ihex Dissolved oxygen 1,2-dicltloropropane 13is(2-eth Y Y)phthalate l,3-dichloropropylene 4-bromophenyl phenyl ether Nitr:tteMitr•ita I KJoldahl nitrogen Ethylbenzene Butyl bent I Y phthalate Oil and grease Methyl bromide 2-chloronaphthalene Methyl chloride 4-chlorophenyl phenyl ether Phosphorus setle Total dissolved solids Methylene chloride Chr ys liminess 1,1,2,2-tetrachloroethane Di-n-butyl phthalate Tetrachloroethylene Di-n-octyl phthalate Antimony Di benzo(a,h)anthr1tcene Arsenic Toluene Beryllium I,1,1-trichloroethane 1,2-dichlorobenzene f,1,2-trichloroethane 1,3-dichlorobenzene Cadmium oct C hronuum Tricltloroethylene I,4-dichlorobenzene Vinyl chloride 3,3-dichlorobenzidine Loppet phthalate I Lead Acid-extractable compounds: Dieth Y p (EPAP-chloro-m-cresol Dinlethyl phthalate Mercury Method 1631B) Nickel 2-chlorophenol 2,4-d initrotoluene Selenium 2,4-dichlorophenol 2,6-dinitrotoluene Silver 2,4-dimethylphenol 1,2-diphenylhydrazine 'lltallium 4,6-dinitro-o-cresol P luoranthene • 2,4-dinitrol�llenol l?luorene CyanideZinc 2-nitrophenol llexachlorobenzene Total phenolic compounds 4-nitrophenol Hexachlorobutadiene Pentachioro henol Hexachlorocyclo-pentadiene Volatile manic�ontpncmrls: I llexaehloroetbane Acrolein Phenol Acrylonitrile 2,4,6-trichlorophenol l ndeno(I,2,3-cd)pyrene Benzene Base-,neutral compouI ids: I sophorone 13ro111ofonu Acenaphthene Naphthalene Carbon tetrachloride Acenaphihylene Nitrobenzene Chlorobenzene • Antlu•acene s N-nitrosodi-n-propylanline Chlorodibromomethane Benzidine N-nitrosodimethylamine Chlo•oethane l3enzo(a)anthnlcene N-nitrosodiphenylamine 2-chloroethyl vinyl ether I3enzo(a)pyrene Phenanthrene Chloroform 3,4 benzofluoranthene Pyrene Dichlorobromomethane Benzo(ghi)pe►ylene 1,2,4-trichlorobenzene 1,1-c1 ichloroethane Benzo(k)fluoranthene 12-dichloroethane Bis(2-chloroethoxy)methane Reporting. Test results shall be reported on DWQ Form-A MR-PPA1. (or in a form approved by the Director)by December 315t of each designated sampling year. The report shall be submitted to the following address:NC DENR/DWQ/Central Files,1617 Mail Service Center,Raleigh,North Carolina 27699-1617. 1 Page I 10