NCS000107_2020 DMR_20201110

Attn: Central Files
NCDED — Division of Energy and Land Resources
1617 Mail Service Center
Ralrigh, North Carolina, 27699-1617
Subject: 2020 Stormwater Discharge Outfall (SDO)
LANXESS Corporation
Greensboro, North Carolina
Guilford County
Permit No. NCS00107
Dear Central Files
In accordance with the above referenced permit, enclosed is the Stormwater
Discharge Outfall (SDO) Monitoring Report.
If you have any questions or require additional information, please contact me at
labarron.mcmillian®lanxess.com or [phone]. extension 115.
Sincerely,
} LaBarron O. McMillian
Plant Manager
LANXESS Corporation, Greensboro Plant
Enclosures
LANXESS
i
November 10, 2020
t-ANXESS Corporation
LaBarron 0 McMillian
520 Broome Road
Greensboro_ NC 27406
Phone [phone] x. 115
Fax [phone]
iabarron.mcmiilran Q lanxess.com
www.us.lanxess.com

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November 09, 2020
Labarron McMillian
LANXESS Corporation
520 Broome Rd
Greensboro, NC 27406
RE, Project. STORMWATER
Pace Project No.. 92502939
Dear Labarron McMillian
Pace Analytical Services, LLC
9800 Kincey Ave Suite too
Huntersville, NC 28078
(704}875-9092
Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report
The test results provided in this final report were generated by each of the following laboratories within the Pace Network-
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Amanda Payne
[e-mail]
[phone]
Project Manager
Enclosures
cc: Franchellie Brewer, LANXESS Corporation
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full
without the written consent of Pace Ana'ytical Services LLC
Page 1 of 14

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Project: STORMWATER
Pace Proecl No.: 92502939
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 25078
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification * 12
Pace Analytical Services Asheville
2225 Riverside Drive. Ashevil;e, NC 28804
Frorda/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification # 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification M 84
vrginWIVELAP Certification # 460221
North Carolina Wastewater Certification # 40
South Carolina Certification # 99030001
Virgin iaNELAP Certification #. 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in fu! i
withect tre written consent of Pace Analytical Services LLC Page 2 of 14

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SAMPLE ANALYTB COUNT
Pace Analytical Services, LLC
9900 Kinsey Ave. Suite 100
Huntersville. NC 2a079
[phone]
Project
Pace Project No
STORMWATER
- 92502939
Analytes
Lab ID
Sample 10
Method
Analysts
Reported
Laboratory
92502939001
OUT FLOW 1
SM 6200B
SAS
4
PASI -C
EPA 9040C
SMK
1
PASI-A
SM 522013-2011
NA!_
1
PASI-A
92502939002
OUT FLOW 2 E FARM
SM 6200B
SAS
4
PASI-C
EPA 9040C
SMK
1
PASI-A
SM 5220D-2011
NAL
1
PASI -A
92502939003
TRAVEL BLANK
SM 5200B
SAS
4
PASI C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except n full
without the written consent of Pace Analytical Services L LC Page 3 of 14

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville NC 28078
[phone]
Project STORMWATER
Pace Project No. 92502939
Sample: OUTFLOW 1 Lab ID: 92SO2939001 Coltected- 10/28/20 14 30 Received. 10/29/20 16 03 Matrix Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV
Analytical Method- SM 6200B
Pace Analytical Services - Charlotte
o-Xylene
6.3 ug1L
0.50
1
11/05/2015.24
95.47-6
Surrogates
1,2-Dichloroethane-d4 (S)
102 %
70-130
1
11/05/20 15.24
17060-07-0
4-BromoOuombenzene (S)
97 %
70-130
1
11/05/20 15:24
460-00-4
Toluene-d8 (S)
100 %
70-130
1
1110512015:24
2037-26-5
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.3 Sid Units
0.10
1
11108/20 18:59
H3
5220D COD
Analytical Method- SM 5220D-2011 Preparation Method- SM 5220D-2011
Pace Analytical Services - Asheville
Chemical Oxygen Demand
58.5 mg1L
250
1
11101/20 21.14 11/02/20 12.27
Sample: OUT FLOW 2 E FARM Lab ID: 92502939002 Collected- 10/28120 14 30 Received. 10/29/20 16 03 Matrix- Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No Qual
6200B MSV
Analytical Method. SM 6200B
Pace Analytical Services - Charlotte
o-Xylene
1.9 ug1L
0.50
1
11/05/2015 42
95-47-6
Surrogates
1,2-Dichloroelhane-d4 (S)
101 %
70-130
1
11/05/20 15 42
17060-07-0
4•BromoOuorobenzene (S)
98 %
70-130
1
11/05/20 15.42
460-00-4
Toluene -dB (S)
100 %
70-130
1
111051201542
2037-26-5
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.4 Sid Units
0.10
1
11/08/20 19 05
H3
5220D COD
Analytical Method. SM 5220D-2011 Preparation Method. SM 5220D-2011
Pace Analytical Services -Asheville
Chemical Oxygen Demand
201 mg1L
25.0
1
11/01/20 21.14 111021201227
Sample: TRAVEL BLANK Lab ID: 92502939003 Collected: 10128/20 00.00 Received: IM9120 15 03 Matrix. Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No Qual
6200B MSV Analytical Method SM 6200B
Pace Analytical Services - Charlotte
o-Xylene ND ug1L 0.50 1 11/06120 13 23 95-47-6
Surrogates
1,2-Dich:oroethane-d4(S) 101 % 70-130 1 111061201323 17060.07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full
Date 41/09/2020 03.53 PM withaut the written consent of Pace Analytical Services. LLC Page 4 of 14

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ANALYTICAL RESULTS
Project STORMWATER
Pace Project No 92502939
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
HuntersviGe. NC 28078
[phone]
Sample: TRAVEL BLANK Lab 10: 92502939003 Collected: 10/28/20 00 00 Received 10/29/20 16 03 Matrix- Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No Qual
6200E MSV Analytical Method SM 6200B
Pace Analytical Services - Charlotte
Surrogates
4-Bromofluorobenzene (S) 97 % 70-130 1 11/06/20 13:23 460-00-4
Toluene-d8 (S) 100 % 70-130 1 11/06/2013 23 2037-26-5
Date: 11/09/2020 03 53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
without the written consent of Pace Analytical Services LLC
Page 5 of 14

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Project: STORMWATER
Pace Project No.: 92502939
QC Batch: 578212
OC Balch Method SM 6200B
Associated Lab Samples: 92502939001. 92502939002
METHOD BLANK: 3058988
Associated Lab Samples. 92502939001. 92502939002
Parameter Units
o-Xylene ug1L
1.2-Dichloroelhane-d4 (S) %
4-Bromofiuorobenzene (S) %
Toluene-d8 (S) %
QUALITY CONTROL DATA
Analysis Method SM 6200B
Analysis Description: 6200E MSV
Laboratory: Pace Analytica I Services - Charlotte
Matrix. Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
0.50
1110512012.08
97
70-130
11/05/20 12 08
96
70-130
11/05/20 12 08
100
70-130
11/05/20 12 08
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville. NC 28078
[phone]
LABORATORY CONTROL_ SAMPLE,
3058989
Spike LCS t.CS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
o-Xylene
uglL
50 52.4 105
60-140
1.2-Dichloroelhane-d4 (S)
%
98
70-130
4-Bromofiuorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3060483
3060494
MS
M9D
92502947005 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
o-Xylene
uglL 490 100
100
630
623 140
133
60-140 1
1.2-Dichloraethane-d4 (S)
%
101
104
70-130
4-Bromofluorobenzene(S)
%
99
100
70-130
Toluene-d8 (S)
%
99
98
70-130
Results presented on this page are In the units indicated by the "UnW column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in run
Daie: 11/09/2020 03 53 PM without the written consent of Pace Analytical Services LLC Page 6 of 14

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville. NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 92502939
QC Batch: 578537
Analysis Method: SM 6200B
OC Batch Method. SM 6200B
Analysis Description 6200B MSV
Laboratory- Dace Analytical Services - Charlotte
Associated Lab Samples. 92502939003
METHOD BLANK 3060816
Matrix: Water
Associated Lab Samples 92502939003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
o-Xylene
ug1L
ND 0 50
11/06/20 12 11
1,2-Dichloroethane-d4 (S)
%
99 70-130
11/06/20 12.11
4-Bromofluorobenzene (S)
%
96 70-130
11/06120 12.11
Toluene -dB (S)
%
100 70-130
11/06/20 12 11
LABORATORY CONTROL SAMPLE:
3060817
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
o-Xylene
ug1L
50 500
100 60-140
1,2-Dichioroethane-d4 (S)
%
99 70-130
4-Bromolluorobenzene (S)
%
102 70-130
Toluene -dB (S)
%
98 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3060818 3060819
MS MSD
92502947003
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
o-Xylene
ug1L
856
400 400 532
535 112 112
60.140 1
1,2-Dichloraethane-d4 (S)
%
102 102
70-130
4•Bromofluorobenzene (S)
%
99 98
70-130
Toluene -dB (S)
%
98 98
70-130
Results presented an this page are In the units Indicated by the 'Units" column except where an altemate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full
Date 11/09/2020 03.53 PM without the written consent of Pace Analytical Services LLC
Page 7 of 14

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QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No - 92502939
QC Batch: 578768 Analysis Method: EPA9040C
QC Batch Method EPA 9040C Analysis Description: 9040 pH
LaboTatory: Pace Analytical Services - Asheville
Associated Lab Samples: 92502939001, 92502939002
SAMPLE DUPLICATE. 3062328
92502167002 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Sid. Units 6.5 6.2 4 D6,1-13
SAMPLE DUPLICATE: 3062329
92502727003 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std Units 6.3 6 0 4 D6.H3
Pace Analytical Services, LLC
9800 Kincey Ave Su.te 100
Huntersville NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Unas" column except where so alternate unit Is presented to the rigid of the result
REPORT OF LABORATORY ANALYSIS
This report shal not be reproduced except in full.
Date; 11/09/2020 03-53 PM without Lhe written consent of Pace Ana ytical Services, LS_C
Page 8 of 14

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QUALITY CONTROL DATA
Project STORMWATER
Pace Project No., 92502939
OC Batch- 577203 Analysis Method SM 52200-2011
OC Batch Method- SM 5220D-2011 Analysis Description 5220D COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92502939001. 92502939002
METHOD BLANK. 3054274 Matrix: Water
Associated Lab Samples. 92502939001. 92502939002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg1L ND 25.0 11/02/20 12:21
LABORATORY CONTROL SAMPLE. 3054275
Spike
Parameter Units Conc
Chemical Oxygen Demand mg1L 750
Pace Analytical Services, LLC
9800 Kincey Ave Suite 100
Huntersville NC 28078
[phone]
LCS LCS % Rec
Result % Rec Limits Qualifiers
765 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE 3054276 3054277
MS MSD
92502926001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 147 100 100 254 257 107 110 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE 3054278 3054279
MS MSD
92502926002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cane. Cane. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 236 100 100 343 343 107 107 90-110 0
Results presented an this page are in the units indicated by the "units" column except whom an alternate unit In presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report she not be reproduced except in full
Date: 11/09/2020 03 53 PM without the written consent of Pace Analytical Services LLC
Page 9 of 14

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QUALIFIERS
Project STORMWATER
Pace Project No 92502939
DEFINITIONS
DF - Dilution Factor, if reported. represents the factor applied to the reported data due to dilution of the sample aliquot
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitalion Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1.2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for. but not detected.
Acid preservation may not be appropriate for 2 Chloroelhylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonrtrile by EPA
Method 8260
N-Nitrosofthenylamine decomposes and cannot be separated from Diphenylamme using Method 8270 The result reported for
each aiialyte is a combined concentration
Pace Ana-tytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Dale- 1110912020 03 63 PM without the written consent of Pace Analytical Services, LLC Page 10 of 14

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincay Ave Suite 100
kuntersville. NC 25078
[phone]
Project STORMWATER
Pace Project No 92502939
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92SO2939001
OUT FLOW 1
SM 6200B
578212
92502939002
OUT FLOW 2 E FARM
SM 6200B
578212
92502939003
TRAVEL BLANK
SM 6200E
57853E
92SO2939001
OUT FLOW 1
EPA 9040C
578768
92502939002
OUT FLOW 2 E FARM
EPA 9040C
578768
92SO2939001
OUT FLOW 1
SM 5220D.2011
577203 SM 5220D-2011
92502939002
OUT FLOW 2 E FARM
SM 5220D.2011
577243 SM 52200-2011
Date: 11/09/2020 03 53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except n fuli
without the written consent of Pace Analytical Services LLG
577261
577261
Page 11 of 14

! ;,71ceAna1pical
Document Name -
Condition Upon Receil
Document No :
F•CAR-CS-033-Rev.07
Document Revised: Uctaoer Cd, ZULU
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh
Mechanicsville[]Atlanta❑ Kernersville❑
ConditionSample Client Name:
Upon Receipt I Project q;
Courier: Fed Ex ❑UPS LISPS ❑Client
Cl commercial )3Pate ❑Other
Custody Seal Present? ❑Yes PTNo Seals Intact? ❑Yes IffNa
Packing Material: ❑Bubble Wrap Bubble flags ❑None ❑ Other
WO## : 92 42939
1111111111111111111111
92502939
Date/Initials Person Exam.ning Contents.
Biological Tissue Frozen?
❑Yes ❑No ON/A �al���
Thermometer: wet ❑blue ❑None
EfIR Gun ID: 92TO61 Type of ice.
Correction Factor:
Cooler Temp: Add/Subtract IT) 0.0 Temp should be above freez'ng to 6•C
❑Samples out of temp criteria. Samples an ice, cooling process
Cooler Temp Corrected ('C): �' has begun
USDA Regulated Soil I /`N/A, water sample)
Did samples originate innaa quarant.ne zone within the United States CA, NY, or SC (check maps)? Did samples originate from a foreign source linlernationally,
COMMENTS/SAMPLE DISCREPANCY 4 Field Data Required? ❑Yes ❑Na
CLIENT NOTIFICATION/RESOLUTION
Person ca itacted'
Project Manager SCURF Review:
Project Manager 5RF Rev;ew:
Date/Time
Lot ID of split containers.
Date!
Date:
Page 12 of 14

,' ,•2aceAnaiytical
uocument Name
Condition Upon Rei
Document No.
F-CAR-CS-033-Rev.07
IJULUMCIiL IMMICV ULWUC1 LO, 4VZU
Page 2 of 2
Issuing Authority'
Pace Carolinas Quality Office
'Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions. VOA, CDliform, TOC. Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project N -WO# : 92502939
PM: AP Due Datet 11/12/20
CLIENT: 92—Lanxess
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pH Adjustment Log for Preserved Samples
Sample to
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
lot p
Nate- Whenever there 15 a discrepancy affecting North Carolina compliance same es. a copy of this form w it be ient to the North Carolina DEHNR Certification Office (i e
Out of hold, incorrect preservative, out of temp, incorrect containers
Page 13 of 14

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