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HomeMy WebLinkAboutNCG120064_DMR_20201109October 27, 2020 Chambers Development of NC, Inc. and Waste Connections of the Carolinas, Inc. Anson Waste Management Facility 375 Dozer Road Polkton, NC 28135 Attention: Mr. Tyler Fitzgerald Reference: Monthly Stormwater Monitoring Anson Waste Management Facility NCG120064 Polkton, North Carolina S&ME Project No. 4140-15-007 Dear Mr. Fitzgerald: tlb\ d F ()ONA6L(;4:1. , I(, S&ME, Inc. (S&ME) is pleased to submit this report detailing the results of the October 2020 stormwater monitoring activities conducted at the Anson Waste Management Facility (AWMF) in Polkton, North Carolina. This work was completed in accordance with our Master Services Agreement dated January 2, 2017, and in accordance with Task 2 in S&ME Proposal No. 41-1600394 (Rev. 1) dated August 8, 2016. This letter summarizes results of sampling efforts conducted by facility personnel. Background Stormwater sampling is required on a semi-annual basis, as defined by the National Pollutant Discharge Elimination System (NPDES) General Permit for Landfills (Permit No. NCG120000) for the facility outfalls. The following outfalls are identified at the facility: Outfall 1, Outfall 2, Outfall 3, Outfall 4, Borrow Area North Outfall, and Borrow Area West Outfall. Outfall 2 was eliminated in August 2018 by the expansion of Sediment Basin 3 and, therefore, is no longer sampled. Outfall 1, Outfall 2, Outfall 3, Outfall 4, Borrow Area North Outfall, and Borrow Area West Outfall continue to be monitored on a semi-annual basis. Monthly sampling was also initiated following December 2019 results at Outfall 3 and Outfall 4, in response to Tier 2 and Tier 3 response actions at the facility. Monthly sampling ceased at Outfall 3 following three consecutive sample results below the benchmark values for the months June through September and only Outfall 4 continues to be monitored on a monthly basis. Parameters for quantitative analysis include chemical oxygen demand (COD) per Standard Method (SM) 2540D, fecal coliform per SM 9222D, and total suspended solids (TSS) utilizing SM 2540D. In addition to the previously listed parameters, Outfall 1 and Outfall 3 are also sampled for chemical parameters associated with vehicle maintenance which include total petroleum hydrocarbons (TPH) per Environmental Protection Agency (EPA) Method 1664B and pH utilizing SM 4500. S&ME, Inc. 1 644 Eastern Star Road I Kingsport, TN 37663 1 p 423.349.2800 1 www.smeinc.com Monthly Stormwater Monitoring Anson Waste Management Facility S&ME Project No.4140-15-007 0 Stormwater Sampling and Quantitative Analyses AWMF personnel collected the monthly stormwater samples at one designated outfall location on October 20, 2020. The total rainfall for the October 20, 2020 storm event was reported as approximately 0.11 inch in 24 hours. Sampling was performed during that storm event. Quantitative chemical laboratory results for the monitoring event are compared to benchmark values established by the facility NPDES permit on the attached Discharge Monitoring Report (DMR). Parameter exceedances of benchmark values, if any were documented through field and laboratory analyses, are summarized in bold type below. ANR = Analyte not requested and not required by the NPDES Permit mg/l= milligrams per liter CFU/ml= colony -forming units per milliliter The DMR is included with this letter as Attachment I for signature and submittal to the North Carolina Department of Environmental Quality (NCDEQ), Division of Water Quality. The Laboratory Data Report for this sampling event is included as Attachment IL Closure S&ME appreciates this opportunity to be of service to Waste Connections and trust this information is responsive to your current needs. If you have any questions, please contact us at your convenience. Sincerely, S&ME, Inc. rdAOrris James R. Bruce Project Manager Senior Reviewer Attachments: Discharge Monitoring Report Laboratory Data Report Site SWPPP Map cc: Mike Lawyer, Fayetteville Regional Office Lana Brown, Waste Connections Nelson Breeden, Waste Connections of the Carolinas, Inc. Page 2 Attachments Attachment I — Discharge Monitoring Report Q c 0 t F L m E L. 0 m c m w N Z ❑LU j a ❑ W C. 7 C- LA W El " Z 0 O m 3 z i v 4 w L = El 0 p O ❑03Os W 0 cz N 0 C ❑❑❑ W W h OC aL+ c 5. cm 2 Ih °C t O Z El —� O❑❑■u Q a O V �ui p� O Z 0 a a a a x Q Q t N c 0 W C N t`u7 U o W Q Oa Zv u Gcu w C -j w a zQ 00 LL Z wZ 0 W Q 0 W m U U. U C. H m _ m O c O d 0 v G1 c. E v, O IA O u r c C _ 'a m !g O a m c 0 (6 c 'O al 'O v CL 'Da -� Ln M M - � 0 E o LM o L6 o r � H ..r E o v a c tD O cM U m N u ar e. 1L O u c o°1n x 0 O _ m. In E p E c V al t u w c c 0 t N L r r = E O v r m N O CL v 0 N t N ' r 0 ° N O z o0 u — O 8 a, � O C m 4 c v E o 4 c L o L% Vf C :3 E cu Ln > . v 7 a a) X to � c n ++ c L O a1 m L E w, E 0 m .L 'rLo m 4� cuM 41 c Z E E O +. v v Ln v L v r v o C. fa i_+ fa LO Z i L "0 3 0 t v 0. o ° -0 E V tg L cu J E a, 4L X C. C aJ N m X C N L .0 a..i V v ° �s E o ai u o E 3 aXi E o c c E= `o Ln E m-0 u r s cu y= a) a c 'n Ln Ln U v o v m 3 :a X -0 Ln u o ai v a1 :.c L a) t+ v, 4� c a) co i u E v 3 O i v c LA i E Ou = cu > O w a N .0 O 0 " o E OV 7 E N +-+ QJ _ u o c O aci m L v 3 E ro c a, 3 c C O 'U LL .0 tw a) Q an+' v m a y (A•c -0 a) L. C. > Vf c0 c E c .5 `~ v u M j r V J o a �r, ' y o c v a� c aoa c E w E co m O c E u aui c a - v aJ 'O N N O c0 N �= m H o v. cu+= E a.; c W n 3 c v .. v c C „n 0 +, y L o bD .° mo E ° C w Q L = 4- LI 0. C d— f 0 E E tines+= CL v O E � aci (Du o 41 c O G1 U O L cu a1 aJ � V) O � v ry m v Z c a 00 0 r-I N N I- I- ar O ai �o aa) a O aJ 4 ice.. N C ,H OCL = ❑ c O bA Ln Ln n dA C .m m ai ho IA O u •7 M p I 5 E VO Z t 0 0 O w z M . O � o c LO M o\A e Ln o V W o LM 10 O H w coo L 0 LA Ln O Z L . O 9- c O Z C 7 O E f0 f0 w N f N r r ` e O 7 O r N -a t O T O U M N w -0 r E O E N f0 O w � m al U Z _ t O co p = o m t m a JA i0•, M a m O N f6 a f0 a O N O c O O LL Z z O� b O Z W NV N �. W a � a ~ J C J WLlaL � a � W O W UJ N z H 0 Z >- W z 2 a W Q cr w � w cr m N a 0L uui a V ~WW W ``^^ N V — W Q J ~ H O O Z z w LU a O Z® WCWC G W W In Q 0 >. VI W 2 X w Z h W U Q w W W Q O W U z Lu z O ca l7 a w LU °c W CW CO c�c N C C G a w W W'^ Oo W ccao O 2 v"-�� ZQ O J o W a z u Z � o W se cc U OT O} 2 LU 0 M: z ULU M m W W i Q N 1- LL L aj N � w C 1 ° o Y CL vo bA T s f0 N � O � � Y � fO T C u O U 7 f0 E M to s O 3 3 I o U Y C O •- L L O a c aci O '° E c C O "a O O w w L CL a w o E O O T m �+ E LO :3 o c C O 4� 4- ° E w o n v E41 O O +.iCA 0 N L Q 'O CO w w C 4-1 N v v E c co E ,n N -a C u L :3 O .c {L H , d p E O 41 E c E c O w O 4, .0 U w c _vwi 1 4� O (a a + 4- N 1 M w O+ c v c E 4 1 � C Y N w w L E v c o U Y w w T m r0 OA C � Y a L Q O 4- 4-1� � w c Y a 'N N iH C C C p0 Q 'r w O_ T m c, v w w w w Q ?� s f0 Y a 7 � m C r C s 7 r O 4-11Y Ln w � w � U t O E w 41 .1 a O 00 0 Attachment II - Laboratory Data Report aceAnalXical www.pacelabs.com October 26, 2020 Lindsey Harris SWE, Inc. 644 Eastern Star Road Kingsport, TN 37663, RE: Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 bear Lindsey Harris: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 20, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures A? , REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 Iacl Analytical (� www.pacelabs.com CERTIFICATIONS Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalj cal www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92501260001 Outfall 4 SM 9222D-2006 KDF 1 PASI-C SM 2540D-2011 RED 1 PASI-A SM 5220D-2011 NAL 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalytical www.pacolabs.com SUMMARY OF DETECTION Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92501260001 Outfall 4 SM 9222D-2006 Fecal Coliforms 230 CFU/100 mL 1.0 10/21/20 13:55 SM 254OD-2011 Total Suspended Solids 5.3 mg/L 3.7 10/22/20 19:02 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Outfall 4 Lab ID: 92501260001 Collected: 10/20/20 08:29 Received: 10/20/20 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 230 CFU/100 mL 1.0 1 10/20/20 15:46 10/21/20 13:55 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids 5.3 mg/L 3.7 1 10/22/20 19:02 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand ND mg/ L 25.0 1 10/25/20 18:24 10/26/20 10:48 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2020 02:27 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 Pace Analytical Services, LLC aceAnalytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 QC Batch: 574488 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92501260001 METHOD BLANK: 3041373 Matrix: Water Associated Lab Samples: 92501260001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 10/21/20 13:55 SAMPLE DUPLICATE: 3041374 92501290003 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL ND ND Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2020 02:27 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 amAnalytical www.pacilabs.com QUALITY CONTROL DATA Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 QC Batch: 575126 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92501260001 METHOD BLANK: 3044675 Matrix: Water Associated Lab Samples: 92501260001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/22/20 18:47 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 3044676 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 3044677 92501390001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 230 234 2 SAMPLE DUPLICATE: 3044678 92501623001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 214 210 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2020 02:27 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnaijdical www.pecolobs.com QUALITY CONTROL DATA Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 575573 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92501260001 METHOD BLANK: 3046933 Matrix: Water Associated Lab Samples: 92501260001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 10/26/20 10:47 LABORATORY CONTROL SAMPLE: 3046934 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 762 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3046935 3046936 MS MSD 92501260001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 116 121 104 108 90-110 4 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3046937 3046938 MS MSD 92501266001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits. RPD Qual Chemical Oxygen Demand mg/L 1330 100 100 1400 1400 71 71 90-110 0 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2020 02:27 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 Pace Analytical Services, LLC acte 100 eAnalytical® 9800Huntersvlle, CKincey Ave. 128078 www.pacefabs.com (704)875-9092 QUALIFIERS Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 DEFINITIONS DF Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/2020 02:27 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 Pace Analytical Services, LLC aceAnalytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Anson LF Stormwater - Monthly Pace Project No.: 92501260 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92601260001 Outfall 4 SM 9222D-2006 574488 SM 9222D-2006 574489 92601260001 Outfall 4 SM 2540D-2011 575126 92601260001 Outfall 4 SM 5220D-2011 575573 SM 5220D-2011 575665 Date: 10/26/2020 02:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recei t(SCUR) Page 1 of 1 ace Analytical Document No.: issuing Authority: F-CAR•CS•033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ EdenEden[]Greenwood ❑ Huntersville ff Raleigh Mechanicsville ❑ ConditionSample Client Name: Project WO# : 92501260 Upon Receipt Courier: ❑Fed Ex OUPS ❑USPS ❑Cllent I IN 11111111111111 ❑ Commercial OPace ❑Other: 92501260 Date/InitlatsPerson ExaminingContents: l U•-c U ' C AMP IY/ Packing Material: ❑Bubble Wrap ❑Bubble Bags [3None [IOther Biological Tissue Frozen? ❑Yes -[]No (31V/A Thermometer: 92TO61 Type of Ice: [3wet [:]Blue[:]None ❑IR Gun ID: Cooler Temp (°C): ) - (6 ' Correction Factor: Add/Subtract (°C) 0.0 Temp should be above freezing to VC Cooler Temp Corrected (°C): U „ _ ❑Samples out of temp chterla. samples on Ice, cooling process has begun USDA Regulated Soil ([rN/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did s�mapluawaes 'ulandePuerto R coifrom a l? ❑Yes source (internationally, and Yes No ..,.,.......,..-�-- - — comments/Discrepancy: Chain of Custody Present? IJres QNo N/A 1. Samples Arrived within Hold Time? [a] es No N/A 1, Short Hold Time Analysis (02 hr.)? yes N/A 3. Rush Turn Around Time Requested? Yes QNo EJNJA 4. Sufficient Volume? Qfes []No ❑N/A 5. Correct Containers Used? @] es (-]NO []NIA 6. -Pace Containers Used? 9es QNo N/A Containers Intact? Yes ❑No ❑N A 7, Dissolved analysis: Samples Field Filtered? ❑yes ❑No ti n B. Sample Labels Match COC? ['Yes ❑No ❑N/A 9. -Includes Date/Time/ID/Analysis Matrix: `% Heads ace In VOA Vials (>5.6mm)? []Yes ONO 01 /A 10. Trip Blank Present? []Yes [_-]No ©N/A 11. Trip Blank Custody Seals Present? Dyes QNo N/A COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Y Y lliD Field Date Required? UYes "NO Date: -Z'0 , -m &O Date: 'U'"-Z'0- 7,0-1,0 Page 11 of 13 o - ciCEARaI}/�ICciI Document Name: Sample Condition .Upon Recelpt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: F•CAR-05-033-Rev,06 Issuing Authority: Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination Is verified and within the acceptance range for preservation samples. Exceptions; VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Project f WO# 92501260 pM; AMB Due Date: 10/27/20 CLIENT: 92-SBME TN _ W a c u a E nil ne. m GI n c u 6 E qq iJ a m •� a c u d E 6N. m ? w a M w ` V a U 6. E � N O Z U 6 6 to c� r73 }� iad E a _ O. U a E 7 tQ a E 9 U1-un 'zp c E ¢ iu _ n u s E ¢ G t OJ m 4 J e o 'r.�i V _ yq� N x E Q `v V z EE d J a d Z a .� E %. rgr Z u x '! E ? Z O E Z o •� E g a ? x E °q ? Y o .I'1 ' =° O > Y A s y 3 ` I Z F E Q .Zy C. J to n i Z J E c� N Z '•A E p z N 3 J. E 9y5 L 0. J E l7 1 � 1 ' z 3 4 S \\\J \\N I N 6A -1 \�\N 8 9 10 11 \NN 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # f th' far—111 M ra,o rj—th rarnlina oEHNR Certification Office (i.e. Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy o Out of hold, Incorrect preservative, out of temp, Incorrect containers, Page •12 of 13 V F (NIA) r- loelul seldweS w NIA �e1003 pelees A olsno �— (NIA) 00l aJj a .aC Z �; 1 :: UO peAID78a .� 1 (NIA) eWP0140 lenp!se d 0 4! dV431 A a 61 } rn J E vi SS1 x (PIoH JH S) !IoO 1eoe3 x � c . F'' 003 x iv Je410 loueylew cd CD ? q £OZSZeN HOeN _ 3 IOH c N . eoNH � # a VO9ZH 0 '� tl E °o m z o a v a a 1'• Poweseldun 'o m E v Sil3NIV1NO3 d0 A in ° Qz cg Q a C S d', w- w N0110311001tldW313ldWVS �,_iLj ry O w W 4 � J Wa. ) in- 'CO' N co i" (MO1.0 SVNJ=O) UA131dVIVS i• Q Q ;E 2 j (yal of aepop pI1eA oes) 3000 XIHIVW a O E 1 n 9 o p m p~ �S3'3s�o3abr$ o• Q 0 is .. i i U. W o w E CL A �s m j � N Q= a m � e of All Q a ° a M fa' � " , IPage 13 # W311 of 13 Attachment III - Site SWPPP Map