NC0005487_Regional Office Historical File Pre 2018

aceAnalytical:N
WI'Ay. pacelabs.com
December 12, 2006
Pace Analytical Services, Inc. f
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax.. [phone]:
Me. Ellen Huffman
NC Div. of Water Resources
610 East Center Ave
Suite 301
Mooresville, NC 28115
RE:. Lab Project Number: 9213332E
Client Project ID: Color -Tex WWP Sludge Spill
Dear Me. Huffman:
Enclosed are the analytical results for sample(s) received by the laboratory on December 5, 2006. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory' unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager `
Enclosures
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater 40
This report shall not 6e reproduced, except in full,
NG Wastewater
12
NC Drinking Water 37712
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water
37706
SC Environmental 99030
'
SC
99006
FL NELAP E87648
FL NELAP
E87627
A

aceAnalytical"
wi hv. pacelabs.com
Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Lab Sample No: 927752667 Project Sample Number: 92133328-001 Date Collected: 12/01/06 13:25
Client Sample ID: BANKS OF ANUT TO YADKIN RIVER Matrix: Soil Date Received: 12/05/06 08:05
Parameters Results Units Report Limit DF Analyzed By CAS No. Oual RecrLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 12/06/06 14:00 12/06/06 14:00
Trace ICP Metals, TCLP Leach
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date Digested
Prep/Method: EPA 3010 / EPA 6010
ND
mg/l
0.025
0.20
mg/l
0.025
ND
mg/l
0.0050
ND
mg/l
0.025
0.072
mg/l
0.025
ND
mg/l
0.050
ND
mg/1
0.025
12/07/06 11:20
Mercury, CVAAS, TCLP Leachate Method: EPA 7470
Mercury ND mg/l
Date: 12/12/06
1.0 12/10/06 14:45 JDA1 7440-38-2
1.0 12/10/06 14:45 JDA1 7440-39-3
1.0 12/10/06 14:45 JDA1 7440-43-9
1.0 12/10/06 14:45 JDA1 7440-47-3
1.0 12/10/06 14:45 JDA1 7439-92-1
1.0 12/10/06 14:45 JDA1 7782-49-2
1.0 12/10/06 14:45 JDA1 7440-22-4
12/07/06 11:20
0.00020 1.0 12/11/06 15:11 ALV 7439-97-6
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs
NC Wastewater 40 This report shall not he reproduced, except in full, NC Wastewater 12
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706
SC Environmental 99030 Sc 99006
P E87648 7 FL NELAP E87627
FL NELA
�bebc`�,
Page: 1 of 6
f

aceAnalytical:w
wv v. pacelabs.com
PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract, or moisture content
Method 9071B modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
Date: 12/12/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs
NO Wastewater 40 This report shall not he reproduced, except in full, NO Wastewater 12
NO Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. NO Drinking Water 37706
SC Environmental 99030 SC 99006
FL NELAP E87648 FL NELAP E87627
s(11G1C1,�.'
Page: 2 of 6
f

aceAnalytical"
wtA%. pacelabs.com
QC Batch: 174942
QC Batch Method: EPA 7470
Associated Lab Samples:
927752667
METHOD BLANK: 927767921
Associated Lab Samples: 927752667
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
QUALITY CONTROL DATA
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Analysis Method: EPA 7470
Analysis Description: Mercury, CVAAS, TCLP Leachate
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/1 ND 0.0002
LABORATORY CONTROL SAMPLE: 927767939
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Mercury mg/l 0.0025 6.0027 107
MATRIX SPIKE: 927767947
927757112 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Mercury mg/l 0.00001 0.0025 0.0027 109
SAMPLE DUPLICATE: 927767954
Parameter Units
Mercury mg/l
Date: 12/12/06
927762351 DUP
Result Result RPD Footnotes
0.00500 ND NC
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs
NC Wastewater 40 This report shall not be reproduced, except In full, NC Wastewater 12
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706
SC Environmental 99030 SC 99006
FL NELAP E87648 5 o FL NELAP E87627
��'elac
Page: 3 of 6
F

aceAnalytical"
wi nv. pacelabs.com
QC Batch: 174842
QC Batch Method: EPA 3010
Associated Lab Samples:
METHOD BLANK: 927761619
Associated Lab Samples:
927752667
927752667
Parameter
Units
Arsenic
mg/l
Barium
mg/l
Cadmium
mg/l
Chromium
mg/l
Lead
mg/l
Selenium
mg/l
Silver
mg/l
LABORATORY CONTROL SAMPLE: 927761627
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Analysis Method: EPA 6010
Analysis Description: Trace ICP Metals, TCLP Leach.
Blank
Reporting
Result
Limit Footnotes
ND
0.025
ND
0.025
ND
0.0050
ND
0.025
ND
0.025
ND
0.050
ND
0.025
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Arsenic
mg/l
2.500
2.460
98
Barium
mg/l
2.500
2.390
96
Cadmium
mg/1
2.500
2.290
92
Chromium
mg/l
2.500
2.205
88
Lead
mg/l
2.500
2.130
85
Selenium
mg/1
2.500
2.485
99
Silver
mg/l
1.250
1.110
89
MATRIX SPIKE: 927761635
927752873
Spike
MS
MS
Parameter
Units
Result
Conc.
Result
% Rec Footnotes
Arsenic
mg/l
0.00980
2.500
2.435
97
Barium
mg/l
0.6800
2.500
2.490
72 1
Cadmium
mg/1
0.01065
2.500
2.115
84
Chromium
mg/1
0
2.500
2.070
83
Lead
mg/1
2.230
2.500
4.265
81
Date: 12/12/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs
NC Wastewater 40 This report shall not be reproduced, except in full, NC Wastewater 12
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706
SC Environmental 99030 _ Sc 99006
FL NELAP E87648 FL NELAP E87627
It C`=
Page: 4 of 6

aceAnalytical'"
wiA%:pacelabs.com
MATRIX SPIKE: 927761635
Parameter
Selenium
Silver
SAMPLE DUPLICATE: 927761643
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 92133328
.Client Project ID: Color -Tex WWP Sludge Spill
927752873
Spike
MS
MS
Units
Result
Conc.
Result
% Rec Footnotes
mg/1
0.00545
2.500
2.425
97
mg/1
0.00860
1.250
1.100
87
927752865
DUP
Parameter
Units
Result
Result
RPD Footnotes
Arsenic
mg/l
ND
ND
NC
Barium
mg/l
0.4700
0.4900
5
Cadmium
mg/l
0.1900
0.2000
4
Chromium
mg/l
ND
ND
NC
Lead
mg/l
0.2500
0.2600
6
Selenium
mg/l
ND
ND
NC
Silver
mg/l
ND
ND
NC
Date: 12/12/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs
NC Wastewater 40 This report shall not be reproduced, except in full, NC Wastewater 12
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706
SC Environmental 99030 SC 99006
FL NELAP E87648 «o FL NELAP E87627
Page: 5 of 6
F

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
a78
ce Analytical " HPhone: 70 NC 28092
Phone: [phone]
w: nu pacelabs.com Fax: [phone]
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
[1] The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
Date: 12/12/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs
NC Wastewater 40 This report shall not he reproduced, except in full, NC Wastewater 12
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37706
SC Environmental 99030 SC 99006
FL NELAP E87648 " L FL NELAP E87627
11C?
Page: 6 of 6
F

INVOICE
9800 Kincey Avenue, Suite 100
'�Urnie
j'�i]' /�ryl7Tf
Huntersville, NC- 28078 92156382
�/1®�
(yy�j 0 /(�,I �(
Phone: [phone]/2006 "
-www.pacelabs.com
Fax: [phone]
:ease •;,_, :emit ®
_
' Ms. _Ellen Huffman Pace_ Analytical S@rvices Inca
NC`Div.. of water Resources . , ,
BOX `684056
610 East Center Ave ;:
Milwaukee WI - 53268-4056
Suite' 301 .
Mooresville, NC 28115'
S°v
C(�ertt No
,a 1�ti 'w .,Si'::'i=� V" : 4Y5!•i�r.:'.
Purchase �r�er o�� hPro
fiS Y -'r. r',..;,,, �z -
ect Marta �Y
h �' '�i r' ,Z2,��1`
Terms
5�n.`f Y.,'< .'s'_ •.,' a k
Pa
. ,
2 fl ."[
.....£...•,a.....::
*. •Sr. ,„ .�" 3 'Ct-
-6..Aeb..w.53...,.,5:.u�.fd.'2,..u^4`35,....x.,..w�e
.n..L"• f�U.�" �wwv�
616566/92-NCDENR _
-Kevin Herring
Due Upon Receipt
1
.. ,;
Client -Reference:
Colon -Tex WWP,-Sludge Spill"
Pace Project -No:'
92133328
-. •
Quantity .•
U/M
Description
Method Matrix : '
Pride :..
Total
ANALYTICAL Charges:
`
1.00
ea;,
Environmental Sample
Disposal•,'
Soil
5 0.0:'
$ 5.00
`
1:00
e "
a
Trace ICP Metals, TCLP Leach.:: ';
EPA 6010 Soil
50.00".
$ 50.00
1.60
-: ea
Mercury, CVAAS,';TCLP
Leachate
EPA 7470 Soil
25.00
$ 25.00 .
1.00
=, ea
Charge for-TCLP Extraction
Soil
40.00 _.
$ 40,00 ...
AN ALYTICAL SUBTOTAL:
120:00 ;
' TOTAL INVOICE AMOUNT. -
$ 120.00
W IE .
JE [E­
DECi 5
OS ;
PLEASE PRINT
INVOICE
# AND CLIENT # is
_
ON YOUR CHECK
NC ©ENR
RO
DWQ - Aquifer
rateetion
J.
1.5%'MONTHLY
FINANCE
.CHARGE ASSESSED AFTER,30 DAYS.
=
LEASE REFER TO
INVOICE
_NUMBER-92156382 WHEN REMITTIN
.
.'..'
A T E
AN EQU L OPPOR UNITY EMPLOYER

acenalytical °
www.pacelabs.com
December 12, 2006
Ms. Ellen Huffman
NC Div. of Water Resources
610 East Center Ave
Suite 301
Mooresville, NC 28115
RE: Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Dear Ms. Huffman:
r
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254,7176
Fax., 828.252.4618
Enclosed are the analytical results for sample(s) received by the laboratory on December 5, 2006. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
Asheville Certification IN REPORT OF LABORATORY AI4LYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 " p"
,
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Solid results are reported on a dry weight basis
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254, 7176
Fax., 828.252.4618
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Lab Sample No: 927752667 Project Sample Number: 92133328-001 Date Collected: 12/01/06 13:25
Client Sample ID: BANKS OF ANUT TO YADKIN RIVER Matrix: Soil Date Received: 12/05/06 08:05
Parameters Results Units Report Limit OF Analyzed By CAS No. Qual RegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 12/06/06 14:00 12/06/06 14:00
Trace ICP Metals, TCLP Leach
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date Digested
Prep/Method: EPA 3010 / EPA 6010
ND
mg/l
0.025
0.20
mg/l
0.025
ND
mg/l
0.0050
ND
mg/l
0.025
0.072
mg/l
0.025
ND
mg/l
0.050
NO
mg/l
0.025
12/07/06 11:20
Mercury, CVAAS, TCLP Leachate Method: EPA 7470
'Mercury NO mg/l
Date: 12/12/06
1.0 12/10/06 14:45 JDA1 7440-38-2
1.0 12/10/06 14:45 JDA1 7440-39-3
1.0 12/10/06 14:45 JDA1 7440-43-9
1.0 12/10/06 14:45 JDA1 7440-47-3
1.0 12/10/06 14:45 JDA1 7439-92-1
1.0 12/10/06 14:45 JDA1 7782-49-2
1.0 12/10/06 14:45 JDA1 7440-22-4
12/07/06 11:20
0.00020 1.0 12/11/06 15:11 ALV 7439-97-6
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
N ACCOA
FL NELAP E87648
Page: 1 of 6
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

9800 Kincey Avenue, Suite 100
2225 Riverside- Drive
Huntersville, NC 28078
Asheville, NC 28804
Phone: [phone]
Phone: 828.254,7176
Fax., 704.875.9091
Fax: [phone]
Lab Project Number:
92133328
Client Project ID:
Color -Tex WWP Sludge Spill
PARAMETER FOOTNOTES
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract, or moisture content
Method 9071E modified to use ASE.
All -pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted'reporting limit
MDL Adjusted Method Detection Limit
Date: 12/12/06
Asheville Certification IN REPORT OF LA ORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
N FCCOH
FL.NELAP E87648
nea
Page: 2 of 6
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006.
FL NELAP E87627

9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
ace AnalyticalO Phone: [phone] Phone: [phone]
Fax., 704.875.9091 Fax [phone]
www.pacelabs.com , QUALITY CONTROL DATA
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
QC Batch: 174942 Analysis Method: EPA 7470
QC Batch Method: EPA 7470: Analysis Description: Mercury, CVAAS, TCLP Leachate
Associated Lab Samples 927752667
METHOD BLANK: .927767921
Associated LabSamples: 927752667
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/l ND 0.0002
LABORATORY CONTROL SAMPLE: 927767939
Parameter Units
Mercury mg/l
MATRIX SPIKE: 927767947
Parameter
Mercury
SAMPLE DUPLICATE: 927767954
Spike LCS LCS
Conc. Result X Rec Footnotes
0.0025 0.0027 107
927757112 ' Spike MS MS
Units Result Conc. Result X Rec Footnotes
mg/l 0.00001 0.0025 0.0027 109
Parameter Units
Mercury mg/l
Date: 12/12/06
927762351 DUP
Result Result RPD Footnotes
0.00500 ND NC
Asheville Certification IN REPORT OF LABORATORY 'ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc..
ry AC`C Oq .,
FL NELAP E87648 °
Page: 3 of 6
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
aceAnalytical o Phone: [phone] Phone-828.254.7176
Fax: [phone] Fax. [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92133328
Client Project ID:.Color-Tex WWP Sludge Spill
QC Batch: 174842 Analysis Method: EPA 6010_
QC Batch Method: EPA 3010 - Analysis Description: Trace ICP Metals, TCLP Leach.
Associated Lab Samples 927752667
METHOD BLANK: 927761619
Associated Lab Samples:
927752667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
-Arsenic
mg/l
NO
0.025
Barium
mg/l
ND
0,025
Cadmium
mg/l
ND
0.0050
Chromium
mg/l
NO
0.025
Lead
mg/l
ND
0.025
Selenium
mg/l
ND
0.050
Silver
mg/l
ND
0.025
LABORATORY CONTROL SAMPLE: 927761627
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
Arsenic
mg/l
2.500
2.460
98
Barium
mg/l
2.500
2.390
96
Cadmium
mg/l
2.500,
2.290
92
Chromium
mg/l
2.500
2.205
88
Lead
mg/1
2.500
2.130
85
Selenium
mg/l
2.500
2.485
99
Silver
mg/l
1.250
1.110
89
MATRIX SPIKE: 927761635
927752873
Parameter
Units
Result
Arsenic
mg/l
0.00980
Barium
mg/l
0.6800
Cadmium
mg/l
0.01065
Chromium
mg/l
0
Lead
mg/l
2.230
Date: 12/12/06
Spike
MS
MS
Conc.
Result
% Rec Footnotes
2.500
2.435
97
2.500
2.490
72 1
2.500
2.115
84
2.500
2.070
83
2.500
4.265
81
Page: 4 of 6
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IN
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc
99030
without the written consent of Pace Analytical Services, Inc.
SC
99006
FL NELAP
E87648
N_ A�'oR°4
FL NELAP
E87627

9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
aceAnaly ical o Phone: 704.875.909
Fax [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number;
Client Project ID;
MATRIX SPIKE: 927761635
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax [phone]
92133328
Color -Tex WWP Sludge Spill
927752873
Spike
MS
MS
Parameter
Units
Result
Conc.
Result
Rec Footnotes
Selenium
mg/l
0.00545
2.500
2.425
97
Silver
mg/l
0.00860
1.250,
1.100
87
SAMPLE.DUPLICATE: 927761643
927752865
DUP
Parameter
Units
Result
Result
RPD
Footnotes
Arsenic
mg/l
ND
ND
NC
Barium
mg/l
0.4700
0.4900
5
Cadmium
mg/l
0.1900
0.2000
4
Chromium
mg/1
ND
ND
NC
Lead
mg/l
0.2500
0.2600
6
Selenium
mg/l
ND.
ND
NC
Silver
mg/l
ND
ND
NC
Date: 12/12/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NO Wastewater 40
NO Drinking Water 37712 This report shall not be reproduced, except in full,
SC 37712 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 N co'?
�,
Page: 5 of 6
Charlotte Certification IDs
NO Wastewater 12
NO Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
QUALITY CONTROL DATA PARAMETER FOOTNOTES
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
�2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Consistent with EPA guidelines,' unrounded concentrations are displayed and have been used to calculate X Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D), Matrix Spike (Duplicate).
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
[1] The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
Date: 12/12/06
Asheville Certification IDs REPORT OF LABORATORY
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 N AccoR
l4'O'•_'09 O
hc
,-_
Page: 6 of 6
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Report tu:
WATER QUALITY SECTION
CHAIN OF CUSTODY (C 05Q_RLC,0R__D.
ff
Pagc� . f �
INC I)ENR/DWQ LABORATORY (check one): 11 CENTRAL I JARO I J WBRO
For Invesbgation of: d�
6d
Sample collector (print name)
and DM-1 forms completed by: r, L+,11
4 Sample collecor's signature: 4
Field storage conditions and location
(when applicable):
is
Lab Uc Onty
LAB NO.
STATION NO.
V
STATION LOCATION
DATE
SAMPLED
TIME
SAMPLED
NUMBER
OF
NTALNER-9
4-
Relinquished by (sigpature�):..?
Date-
Time
RcceM by, (4ignatinc):
Date-
Time
Relinquished by (sipatute.) T
Date
Time
Received by (signature):
Date'
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment (circle one):
State Courier Hand --delivered Federal Ex ress UPS
Other --
Security Typb and Conditions:
Sealed by:
t
Go I
Broken by:
LNTRAL.kBORA.TORY CHAIN OF CUSTODY - Lab Use Only
LAB NUMBERS
FROM THROUGH
NUMBER
BOTTLES
ANALYSES
REQUESTED
RELINQUISHED
BY:
RECEIVED
BY:
DATE
TLIVIE
QA\Fomis\Samplc Recciving\COC form WQ
4!J010ldbs
IQ_

DIVISION OF WATER QUALITY
Chemistry Laboratory Report/ Water Quality
W❑ SAMPLE TYPE
COUNTY ROWAN
PRIORITY
RIVER BASIN:
AMBIENT QA
X❑ STREAM
0 EFFLUENT
REPORT TO MROSP Regional Office
COMPLIANCE X❑ CHAIN OF CUSTODY
❑ LAKE
❑ INFLUENT
Other :
X❑ EMERGENCY VISIT ID
❑ ESTUARY
COLLECTOR(S) : W BELL
❑1
Estimated BOD Range: Station Location: UPSTREAM AT UTTO YADKING ROVER
Seed: Chlorinated: Remarks:
Station # Date Begin (yy/mm/dd) Date End (yy/mm/dd) Time Begin ITimeEnd I Depth- DM, DB, DBM Value Type -A, H, L I Composite-T, S, Sample Type
1 20061201 1233 1
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L
Coliform: MF Fecal31616 /100ml
Coliform: MF Total 31504 /100m1
Coliform: tube Fecal31615 /100ml
Coliform: Fecal Strep 31673 /100ml
Residue: Total500 mg/L
Volatile 505 mg/L
Fixed 510 mg/L
Residue: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 mg/L
pH 403 units
Acidity to pH 4.5 436 mg/L
Acidity to pH 8.3 435 mg/L
Alkalinity to pH 8.3 415 mg/L
Alkalinity to pH 4.5 410 mg/L
TOC 680 mg/L
Turbidity 76 NTU
Coliform Total Tube "/100 mis
COMMENTS
Chloride 940 mg/L
Chl a: Tri 32217 ug/L
Chl a: Corr 32209 uWL
Pheophytin a 32213 ug/L
Color: True 80 C.U.
Color: (pH ) 83 pH= C.U.
Color: pH 7.6 82 C.U.
Cyanide 720 mg/L
Fluoride 951 mg/L
Formaldehyde 71880 mg/L
Grease and Oils 556 mg/L
Hardness Total900 mg/L
Specific Cond. 95 umhos/cm
MBAS 38260 mg/L
Phenols 32730 ug/L
Sulfate 945 mg/L
Sulfide 745 mg/L
Boron
Tannin & Lignin mg/L
Hexavalent Chromium ug/L
Bicarbonate mg/L
Carbonate mg/L
Total Dissolved Solids mg/L
NH3 as N 610
mg/L
TKN an N 625
mg/L
NO2 plus NO3 as N 630
mg/L
P: Total as P 665
mg/L
PO4 as P 70507
mg/L
P: Dissolved as P 666
mg/L
K-Potassium
mg/L
X
Cd- Cadmium 1027
2.OU ug/L
X
Cr-Chromium:Tota11034
25U ug/L
X
Cu-Copper 1042
2.OU ug/L
X
Ni-Nickel1067
1OU ug/L
X
Pb-Lead 1051
1OU ug/L
X
Zn- Zinc 1092
1OU ug/L
V-Vanadium
ug/L
Ag-Silver 1077
5.OU ug/L
X
AI -Aluminum 1105
160 ug/L
Be- Beryllium 1012
ug/L
Ca- Calcium 916
mg/L
Co -Cobalt 1037
ug/L
X
Fe -Iron 1045
900 ug/L
Mo-Molybdenum
ug/L
Sb-Antimony
ug/L
Sn-Tin
ug/L
Tl-Thallium
ug/L
Ti-Titanium
ug/L
Hg-1631
ng/L

DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Water Quality
0 SAMPLETYPE
COUNTY ROWAN
PRIORITY
RIVERBASIN:
AMBIENT QA
X❑ STREAM
EFFLUENT
REPORTTO MROSP Regional Office
COMPLIANCE 0 CHAIN OF CUSTODY
LAKE
INFLUENT
Other
X❑ EMERGENCY VISITID
ESTUARY
COLLECTOR(S) : W BELL
2❑
Estimated BOD Range: Station Location: DOWNSTREAM PUT TO YADKIN RIVER
Seed: Chlorinated: Remarks:
Station# Date Begin (yy/mm/dd) Date End (yy/mm/dd) Time Begin Time End I Depth- DM, DB, DBM Value Type -A, H, L Composite-T, S, Sample Type
2 20061201 1435 1
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L
Coliform MF Fecal31616 1100m1
Coliform: MFTotal31504 /100m1
Coliform: tube Fecal31615 /IOOmI
Coliform: Fecal Strep 31673 /100m1
Residue: Total 500 mg/L
Volatile 505 mg/L
Fixed 510 mg/L
Residue: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 mg/L
pH 403 units
Acidity to pH 4.5 436 mg/L
Acidityto pH 8.3 435 mg/L
Alkalinity to pH 8.3 415 mg/L
Alkalinity to pH 4.5 410 mg/L
TOC 680 mg/L
Turbidity 76 NTU
Coliform Total Tube "/100 mis
COMMENTS
Chloride 940 mg/L
Cal s Tri 32217 ug/L
Cal s Corr 32209 ug/L
Pheophytin a 32213 ug/L
Color: True 80 C.U.
Color: (pH) 83 pH= C.U.
Color: pH 7.6 82 C.U.
Cyanide 720 mg/L
Fluoride 951 mg/L
Formaldehyde 71880 mg/L
Grease and Oils 556 mg/L
Hardness Total900 mg/L
Specific Cond. 95 umhos/cm
MBAS 38260 mg/L
Phenols 32730 ug/L
Sulfate 945 mg/L
Sulfide 745 mg/L
Boron
Tannin & Lignin mg/L
Hexavalent Chromium ug/L
Bicarbonate mg/L
Carbonate mg/L
Total Dissolved Solids mg/L
NH3 as N 610
mg/L
TKN an N 625
mg/L
NO2 plus NO3 as N 630
mg/L
P: Total as P 665
mg/L
PO4 as P 70507
mg/L
P: Dissolved as P 666
mg/L
K-Potassium
mg/L
X
Cd- Cadmium 1027
2.OU ug/L
X
Cr-Chromium:Tota11034
25U ug/L
X
Cu-Copper 1042
43 ug/L
X
Ni-Nickel1067
10U ug/L
X
Pb-Lead 1051
10U ug/L
X
Zn- Zinc 1092
12 ug/L
V-Vanadium
ug/L
Ag-Silver 1077
5.OU ug/L
X
Al -Aluminum 1105
1400 ug/L
Be- Beryllium 1012
ug/L
Ca- Calcium 916
mg/L
Co- Cobalt 1037
ug/L
X
Fe- Iron 1045
5000 ug/L
Mo-Molybdenum
ug/L
Sb-Antimony
ug/L
Sn-Tin
ug/L
Tl-Thallium
ug/L
Ti-Titanium
ug/L
Hg-1631
ng/L

f DIVISION OF WATER QUALITY
Chemistry Laboratory Report/ Water Quality
W❑ SAMPLE TYPE
COUNTY ROWAN
PRIORITY
RIVER BASIN:
AMBIENT QA
X� STREAM
EFFLUENT
REPORTTO :. MROSP Regional Office
COMPLIANCE 0 CHAIN OF CUSTODY
LAKE
INFLUENT
Other : -
0 EMERGENCY VISITID
ESTUARY
COLLECTOR(S) : W BELL
Estimated BOD Range: Station Location: DOWNSTREAM @ UTTO YADKIN RIVER
Seed: Chlorinated: Remarks:
Station# Date Begin (yyhnm/dd) Date End (yy/mm/dd) Time Begin ITimeEnd I Depth- DM, DB, DBM Value Type -A, H, L I Composite-T, S, Sample Type
3 20061201 1350 1
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L
Coliform: MF Fecal31616 /100ml
Coliform: MFTotal 31504 /100ml
Coliform: tube Fecal 31615 /100ml
Coliform: Fecal Strep 31673 /100ml
Residue: Total 500 mg/L
Volatile 505 mg/L
Fixed 510 mg/L
Residue: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 mg/L
pH 403 units
Acidity to pH 4.5 436 mg/L
Acidity to pH 8.3 435 mg/L
Alkalinity to pH 8.3 415 mg/L
Alkalinity to PH 4.5 410 mg/L
TOC 680 mg/L
Turbidity 76 NTU
Coliform Total Tube "/100 mis
COMMENTS
Chloride 940 mg/L
Chl a: Tri 32217 ug/L
Chl a Corr 32209 ug/L
Pheophytin a32213 ug/L
Color: True 80 C.U.
Color: (pH ) 63 pH= C.U.
Color: pH 7.6 82 C.U.
Cyanide 720 mg/L
Fluoride 951 mg/L
Formaldehyde 71680 mg/L
Grease and Oils 556 mg/L
Hardness Total900 ' mg/L
Specific Cond. 95 umhos/cm
MBAS 38260 mg/L
Phenols 32730 ug/L
Sulfate 945 mg/L
Sulfide 745 mg/L
Boron
Tannin & Lignin mg/L
Hexavalent Chromium ug/L
Bicarb onate mg/L
Carbonate mg(L
Total Dissolved Solids mg/L
NH3 as N 610
mg/L
TKN an N 625
mg/L
NO2 plus NO3 as N 630
mg/L
P: Total as P 665
mg/L
PO4 as P 70507
mg/L
P: Dissolved as P 666
mg/L
K-Potassium
mg/L
X
Cd- Cadmium 1027
2.0U ug/L
X
Cr-Chromium:Total1034
25U ug/L
X
Cu-Copper 1042
2.7 ug/L
X
Ni-Nickel1067
IOU ug/L
X
Pb-Lead 1051
1OU ug/L
X
Zn- Zinc 1092
1 OU ug/L
V-Vanadium
ug/L
Ag-Silver 1077
5.OU ug/L
X
Al -Aluminum 1105
590 ug/L
Be- Beryllium 1012
ug/L
Ca- Calcium 916
mg/L
Co- Cobalt 1037
ug/L
X
Fe -Iron 1045
4600 ug/L
Mo-Molybdenum
ug/L
Sb-Antimony
ug/L
Sn-Tin
ug/L
Tl-Thallium
ug/L
Ti-Titanium
ug/L
Hg-1631
ng/L

Mo
ug/L
Sb
ug/L
Sn
ug/L
TI
ug/L
Ti
ug/L
Hg-1631
ng/L

' Report to: WATER QUALITY SECTION
CHAIN OF CUSTODY (COC) RECORD
NC DENR/DWQ LABORATORY (check one): CENTRAL ARO [ ] WaRO
Page i of_J_
For Investigation of: �a
Sample collector (print name)
and DM -I forms completed by: hT 4 _
�— I o ld Co l0 i ' /r1 X fir` r'
UC � �L� �l � r ? �t'
Sample collector's signature: -
Field storage conditions and location (when applicable):
rs fri � ! t'' C '�" ;
Lab Use Only
LAB NO. STATION NO. STATION LOCATION
—7 e lovr ,
`i f' i�t i7 1 � e T./r` i� ci c• t' i'' —NUMBER
DATE TIME OF
SAMPLED SAMPLED CONTAINERS
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4-e r. ,1 %`f/ • L'.F'
4/ Y-' �7C
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61
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Relinquished by (signatur ):
Relinquished by (signature):
Date
Date
Time
Time
ive y si ntar)
Receive by (signature):
Date
Date
�n�
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment (circle one):
State Courier 1 Hand -delivered Federal Express UPS Other:
•L17
Security Type and Conditions:
Se�by,
)
y:
INTRALABORAI'URY CHAINN
LAB NUMBERS
FROM THROUGH
VI' l;u�iUlil
NUMBER
BOTTLES
- i.au u ll
ANALYSES
REQUESTED
RELINQUISHED
BY:
RECEIVED
BY:
DATE
TIME
n
4 7i4''i: 'iJ '4 �'K •.r 4 tl `o'i ] P$
� 2d`�' ev:
4/10/Oldbs
QA\Forms\Sample Receiving\COC form WQ

i-oc. Descr.:
OLD COLOR - TEX WWTP LAGQ0o m ,� wvIko6ai;
AND NATO PAL I�EMURCES
Location ID:
NC0005487
N.
��RlmSifaa OFFICE
1PlA1
County:
River Basin
ROWAN
--- _ _
G:`. - ^�
�0 E,QQ
G
Report To
MROSP
.tea
r
Region:
MRO
LIAR 2 C Z00%
� -'I
Collector:
W BELL
\
Sample Matrix:
WASTEWATER
Loc. Type:
TRIP BLANK
Sample Depth
t V )
Sample ID:
AB14387
PO Number #
7W1764
VisitlD
`'Collect Date:
03/09/2007
Collect Time::
10:05
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/16/2007
Sample Comment EATER
R� Emergency Yes/No
COC Yes/No YES
CAS Analyte Name PQL - Result Qualifier Units Approved By
LAB
Sample temperature at receipt by lab 2.6 °C MMATHIS
MIST
75-78-1
Dichlorodifluoromethane
1.0
Not detected
ug/L
RKELLING
7.4-87-3
Chloromethane
0.50
Not detected
ug/L
RKELLING
75-01-4
Vinyl Chloride
0.50
Not detected
ug/L
RKELLING
74-83-9
Bromomethane
0.50
Not detected
ug/L
RKELLING
75-00-3
Chloroethane
0.50
Not detected
ug/L
RKELLING
75-69-4
Trichlorofluoromethane
0.50
Not detected
ug/L
RKELLING
75-35-4
1,1-Dichloroethene
0.25
Not detected
ug/L
RKELLING
75-09-2
Methylene Chloride
10
Not detected
ug/L
RKELLING
156-60-5
trans-1,2-Dichloroethene
0.25
Not detected
ug/L
RKELLING
163404-4
Methyl Tert-Butyl Ether
0.25
Not detected
ug/L
RKELLING
75-3473
1,1-Dichloroethane
0.25
Not detected
ug/L
RKELLING
156-59-4
cis-1,2-Dichloroethene
0.25
Not detected
ug/L
RKELLING
74-97-5
Bromochloromethane
0.25
Not detected
ug/L
RKELLING
67-66-3
Chloroform
0.25
5.0
ug/L
RKELLING
590-20-7
2,2-Dichloropropane
5.0
Not detected
ug/L
RKELLING
107-06-2
1,2-Dichloroethane
0.25
Not detected
ug/L
RKELLING
71-55-6
1, 1,1 -Trichloroethane
0.25
Not detected
ug/L
RKELLING
563-58-6
1,1-Dichloropropene
0.25
Not detected
ug/L
RKELLING
56-23-5
Carbon Tetrachloride
0.25
Not detected
ug/L
RKELLING
7143-2
Benzene
0.25
Not detected
ug/L
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 3

Loc. Descr.: OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
WASTEWATER
Loc. Type:
TRIP BLANK
Sample Depth
Sample Comment
Sample ID:
AB14387
PO Number#
7W1764
VisitlD
WA7icRQ
�0F
Collect Date:
03/09/2007
Collect Time::
10:05
--1
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/16/2007
Emergency Yes/No
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result Qualifier
Units
Approved By
74-95-3
Dibromomethane
1.0
Not detected
ug/L
RKELLING
78-87-5
1,2-Dichloropropane
0.25
Not detected
ug/L
RKELLING
79-01-6
Trichloroethene
0.25
Not detected
ug/L
RKELLING
75-27-4
Bromodichloromethane
0.25
0.58
ug/L
RKELLING
10061-01-5
cis-1,3-Dichloropropene
0.25
Not detected
ug/L
RKELLING
10061-02-6
trans-1,3-Dichloropropene
0.25
Not detected
ug/L
RKELLING
79-00-5.
1,1,2-Tdchloroethane
0.25
Not detected
ug/L
RKELLING
108-88-3
Toluene
0.25
Not detected
ug/L
RKELLING
14248-9
1,3-Dichloropropane
0.25
Not detected
ug/L
RKELLING
124-48-1
Dibromochloromethane
0.25
Not detected
ug/L
RKELLING
106-93-4
(EDB)1,2-Dibromoethane
0.25
Not detected
ug/L
RKELLING
127-18-4
Tetrachloroethene .
0.25
Not detected
ug/L
RKELLING
108-90-7
Chlorobenzene
0.25
Not detected
ug/L
RKELLING
100-41-4
Ethylbenzene
0.25
Not detected
ug/L
RKELLING
75-25-2
Bromoform
1.0
Not detected
ug/L
RKELLING
108-38-3
m,p-Xylene
0.50
Not detected
ug/L
RKELLING
100-42-5
Styrene
0.25
Not detected
ug/L
RKELLING
79-34-5
1,1,2,2-Tetrachloroethane
0.25
Not detected
ug/L
RKELLING
630-20-6
1,1,1,2-Tetrachloroethane
0.25
Not detected
ug/L
RKELLING
95-47-6
o-Xylene
0.25
Not detected
ug/L
RKELLING
96-18-4
1,2,3-Tdchloropropane
0.25
Not detected
ug/L
RKELLING
98-82-8
Isopropylbenzene
0.25
Not detected
ug/L
RKELLING
108-86-1
Bromobenzene
0.25
Not detected
ug/L
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 3

Loc. Descr.: OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
WASTEWATER
Loc. Type:
TRIP BLANK
Sample Depth
Sample Comment
Sample ID:
AB14387
PO Number #
7W1764
VisitlD
Collect Date:
03/09/2007
Collect Time::
10:05
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/16/2007
Emergency Yes/No
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result Qualifier
Units
Approved By
103-65-1
n-Propylbenzene
0.25
Not detected
ug/L
RKELLING
95-49-8
2-Chlorotoluene
0.25
Not detected
ug/L
RKELLING
106-43-4
4-Chlorotoluene
0.25
Not detected
ug/L
RKELLING
108-67-8
1,3,5-Trimethylbenzene
0.25
Not detected
ug/L
RKELLING
98-06-6
tert-Butylbenzene
0.25
Not detected
ug/L
RKELLING
95-63-6
1,2,4-Trimethylbenzene
0.25
Not detected
ug/L
RKELLING
135-98-8
sec-Butylbenzene
0.25
Not detected
ug/L
RKELLING
543-73-1
m-Dichlorobenzene (1,3)
0.25
Not detected
ug/L
RKELLING
/ 106-46-7
p-Dichlorobenzene (1,4)
0.25
Not detected
ug/L
RKELLING
95-50-1
o-Dichlorobenzene (1,2)
0.25
Not detected
ug/L
RKELLING
99-87-6
p-Isopropyltoluene
0.25
Not detected
ug/L
RKELLING
104-51-8
n-Butylbenzene
0.25
Not detected
ug/L
RKELLING
96-12-8
1,2-Dibromo-3-Chloropropane
2.0
Not detected
ug/L
RKELLING
120-82-1
1,2,4-Trichlorobenzene
0.50
- Not detected
ug/L
RKELLING
91-20-3
Naphthalene
0.50
Not detected
ug/L
RKELLING
87-68-3
Hexachlorobutadiene
0.50
Not detected
ug/L
RKELLING
87-61-6
1,2,3-Trichlorobenzene
1.0
Not detected
ug/L
RKELLING
2-Chloroethyl vinyl ether
- X
ug/L
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 3 of 3

PPV
COUNTY
RIVER BASIN:
REPORT TO M j Regional Office
Other
COLLECTORS): Gi1J a .? u
Estimated BOD Range:
coo'.,
DIVISION OF WATER QUALITY 1�r�//��
Chemistry Laboratory Report / Water Quality Lab Number
El SAMPLE TYPE Date Received
PRIORITY Time Received Q
AMBIENT � A E] STREAM � EFFLUENT Received B
COMPLIANCE © CHAIN OF CUSTODY ❑ LAKE INFLUENT
EMERGENCY a VISIT ID ESTUARY ❑ Data Released
' Date Reported
t / C
Station Location: ) _
Seed:
Chlorinated:
Remarks:
Station #/Location Code
Det Begin (yy/mm/dd)
I Date End (yy/mm/dd)
Time Begin
Time End
Depth - DM, DB, BMF---]
Value Type - A, H, L
Composite-T, S, B
Sample Type
I
BOD 310 mg/L
COD High 340 mgtL
COD Low 335 mg/L
Coliform: MF Fecal 31616 /100ml
Coliform: MF Total 31504 /100ml
Coliform: tube Fecal 31615 /100ml
Coliform: Fecal Strep 31673 /loom]
Residue: Total 500 mg/L
Volatile 505 mg/L
Fixed 510 mgtL
Residue: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 m9tL.
pH 403 units
Acidity to pH 4.5 436 mStL
Acidity to pH 8.3 435 me/I.
Alkalinity to pH 83 415 mg/L
Alkalinity to pH 4.5 410 mg/L
TOC 680 mg/L
Turbidity 76 NTU
Coliform Total Tube /100 ml
COMMENTS: ! 5 t' V �C� Ll! / 1 1 C
Chloride 940 mg(L
Chlorophyll a EPA 445.0 modified option ug(L
Color: True 80 C.U.
.Color:
(pH) 83 pH= C.U.
Color: pH7.6 82 C.U.
Cyanide 720 mg(L
Fluoride 951 mg/L
Formaldehyde 71880 mg1L
Grease and Oils 556 mgtL
Hardness Total900 mgtL
Specific Cond. 95 umhos/cm
MBAS 38260 msfL
Phenols 32730 ug(L
Sulfate 945 M91L
Sulfide 745 mg/L
Boron
Tannin & Ligtin ug/L
Hexavalent Chromium ug/L
Bicarbonate mg/L
Carbonate mg/L
Total Dissolved Solids mg/L
NH3 as N 610 rng/L
TKN an N 625 mg/L
NO2 plus NO3 as N 630 mg/L
P: Total as P 665 mg/L
PO4 as P 70507 mg/L
P: Dissolved as P 666 mg/L
K-Potassium mg/L
Cd- Cadmium 1027 ug/L
Cr-Chromium:Total 1034 ug/L
Cu- Copper 1042 ug/L
Ni-Nickel 1067 ug1L
Pb- Lead 1051 ug/L
Zn- Zinc 1092 up
V-Vanadium ug(L
Ag- Silver 1077 ug/L
Al- Aluminum 1105 ug/L
Be -Beryllium 1012 ug/L
Ca- Calcium 916 mg/L
Co- Cobalt 1037 ug/L
Fe -Iron 1045 ug/L
Mo-Molybdenum —/L
Sb-Antimony ug/L
Sn-Tin ug/L
TI-Thallium ug/L
Ti-Titanium ug/L
Hg-1631 V ng/L
Li -Lithium 1132 ug/L
Mg. Magnesium 927 mg/L
Mn-Manganese 1055 ug/L
Na- Sodium 929 mg/L
Arsenic:Total1002 ug/L
Se- Selenium 1 147 ug/L
Hg- Mercury 71900 ug(L
Ba-Barium ug/L
Organochlorine Pesticides
Organophosphorus Pesticides
Organonitrogen Pesticides
Acid Herbicides
Base(Neutral&Acid Extractable Organics
TPH Diesel Range
Purgeable Organics (VOA bottle req'd)
TPH Gasoline Range
TPH/BTEX Gasoline Range
hytoplankton
Temperature on arrival (°C):.

ENRIDWQ LABORATORY
LAB NO. AB14387
REPORTED BY
AA
VAVn
VOLATILE ANALYTICAL REPORTP
SUPERVISOR K
CHECKED BY
'T
DATE
REVIEWED BY
r
ENTERED BY
SAMPLE TYPE:
WATER
ANALYTICAL RESULTS
DATE
::��YrSlahlA
Os Ariic
. i?gL.....:F�ESIli.T ..-........- :�::VolatileOY sine :::::::::::::::::::::
..•.•!� .•.•...•.•.•.•...... �.-.-.-.-
••••Slr�=��'F'�'•'
'���''�'`:`��� G�, .......atgek�otaRaitnd
...•.•.�
................0 L......:ag/i;.....�........•........ CA .... s etGccn ..und ::........•.......
9
75-71-8
Dichlorodifluoromethane
1.0
U
630-20-6
1,1,1,2-Tetrachloroethane
0.25 U
74-87-3
Chloromethane
0.50
U
75-25-2
Bromoform
1.0 U
75-01-4
Vinyl Chloride
0.50
U
79-34-5
1,1,2,2-Tetrachloroethane
0.25 U
74-83-9
Bromomethane
0.50
U
96-18-4
1,2,3-Trichooropropane
0.25 U
75-00-3
Chloroethane
0.50
U
108-86-1
Bromobenzene
0.25 U
76-69-4
Trichlorofluoromethane
0.50
U
95-49-8
2-Chlorotoluene
0.25 U
75-35-4
1,1-Dichloroethene
0.25
U
106-43-4
4-Chlorotoluene
0.25 U
75-09-2
Methylene Chloride
10
U
541-73-1
1,3-Dichlorobenzene
0.25 U
156-60-5
trans-1,2-Dichloroethene
0.25
U
106-46-7
1,4-Dichlorobenzene
0.25 U
75-34-3
1,1-Dichloroethane
0.25
U
95-50-1
1,2-Dichlorobenzene
0.25 U
594-20-7
2,2-Dichloropropane
5.0
U
96-12-8
1,2-Dibromo-3-Chloropropane
2.0 U
156-59-4
cis-1,2-Dichloroethene
0.25
U
120-82-1
1,2,4-Trichlorobenzene
0.50 U
67-66-3
Chloroform
0.25
5.0
87-68-3
Hexachlorobutadiene
0.50 U
74-97-5
Bromochloromethane
0.25
U
87-61-6
1,2,3-Trichlorobenzene
1.0 U
71-55-6
1, 1, 1 -Trichloroethane
0.25
U
-1634-04-4
Methyl-tert-butyl ether
0.25 U
563-58-6
1,1-Dichloropropene
0.25
U
71-43-2
Benzene
0.25 U
56-23-5
Carbon Tetrachloride
0.25
U
108-88-3
Toluene
0.25 U
107-06-2
1,2-Dichloroethane
0.25
U
100-41-4
Ethyl benzene
0.25 U
79-01-6
Trichloroethene
0.25
U
108-38-3
m,p-Xylenes
0.50 U
78-87-5
1,2-Dichloropropane
0.25
U
95-47-6
o-Xylene
0.25 U
75-27-4
Bromodichloromethane
0.25
0.58
100-42-5
Styrene
0.25 U
74-95-3
Dibromomethane
1.0
U
98-82-8
Isopropylbenzene
0.25 U
10061-01-5
cis-1,3-Dichloropropene
0.25
U
103-65-1
n-Propylbenzene
0.25 U
10061-02-6
trans-1,3-Dichloropropene
0.25
U
108-67-8
1,3,5-Tdmethylbenzene
0.25 U
79-00-5
1,1,2-Trichloroethane
0.25
U
98-06-6
tent-Butylbenzene
0.25 U
127-18-4
Tetrachloroethene
0.25
U
95-63-6
1,2,4-Tdmethylbenzene
0.25 U
142-28-9
1,3-Dichloropropane
0.25
U
135-98-8
sec-Butylbenzene
0.25 U
124-48-1
Dibromochloromethane
0.25
U
99-87-6
p-isopropyltoluene
0.25 U
106-93-4
1,2-Dibromoethane
0.25
U
104-51-8
n-Butylbenzene
0.25 U
108-90-7
Chlorobenzene
0.25
U
91-20-3
Naphthalene
0.50 U
POL Practical Quantitation Limit- Subject to
change due to instrument sensitivity
N- Tentatively Identified, not confirmed
J- Estimated Value
U- Samples analyzed for this compound but not detected
X- Sample not analyzed for this compound
N3- Estimated concentration is <PQL and >MDL
P Elevated PQL due to matrix interference and/or'sample dilution
COMMENTS: NOT ANALYZED FOR 2-CHLOROETHYL VINYL ETHER
mg/L mg/L
GasDliireAarigeE§timafeii:Tdtal:Petroleuiri:Hydiocori.::: 0.20 X
.............................................
Other Volatile Organics Detected Result
(up to 10 highest peaks) ug/L

Descr.: OLD COLOR - TEX WWTP LAGOON, 0) -I- tit t—
AND wun k L RESOURCES
Location ID: NC0005487 r ."ONALCIFFICE
County: ROWAN �fr \NAT +�?
River Basin
Report To MROSP r
Region: MRO >
Collector: W BELL MAR 2 82007 o c
Sample Matrix: GROUNDWATER
Loc. Type: TRIP BLANK I
Sample Depth
Sample ID: AB14388
PO Number# 7W1765
VisitlD
Collect Date: 03/09/2007 i
Collect Time:: 10:00
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/26/2007
I Sample Comment I'tC (. ��� �'1� a
Emergency Yes/No
COC Yes/No YES
CAS # Analyte Name PQL Result Qualifier Units Approved By
LAB
Sample temperature at receipt by lab I I 1.9 °C MMATHIS
vni I
75-78-1
Dichlorodifluoromethane
1.0
Not detected
ug/L
RKELLING
74-87-3
Chloromethane
0.50
Not detected
ug/L
RKELLING
75-01-4
Vinyl Chloride
0.50
Not detected
ug/L
RKELLING
74-83-9
Bromomethane
0.50
Not detected
ug/L
RKELLING
75-00-3
Chloroethane
0.50
Not detected
ug/L
RKELLING
75-69-4
Trichlorofluoromethane
0.50
Not detected
ug/L
RKELLING
75-35-4
1,1-Dichloroethene
0.25
Not detected
ug/L
RKELLING
75-09-2
Methylene Chloride
10
Not detected
ug/L
RKELLING
156-60-5
trans-1,2-Dichloroethene
0.25
Not detected
ug/L
RKELLING
1634-04-4
Methyl Tert-Butyl Ether
0.25
Not detected
ug/L
RKELLING
75-34-3
1,1-Dichloroethane
0.25
Not detected
ug/L
RKELLING
156-59-4
cis-1,2-Dichloroethene
0.25
Not detected
ug/L
RKELLING
74-97-5
Bromochloromethane
0.25
Not detected
ug/L
RKELLING
67-66-3
Chloroform
0.25
5.4
ug/L
RKELLING
590-20-7
2,2-Dichloropropane
0.25
Not detected
ug/L
RKELLING
107-06-2
1,2-Dichloroethane
0.25
Not detected
ug/L
RKELLING
71-55-6
1,1,1-Trichloroethane
0.25
Not detected
ug/L
RKELLING
563-58-6
1,1-Dichloropropene
0.25
Not detected
ug/L
RKELLING
56-23-5
Carbon Tetrachloride
0.25
Not detected
ug/L
RKELLING
71-43-2
Benzene
0.25
Not detected
ug/L
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 3

re cr.:
OLD COLOR - TEX WWTP LAGOON
ocation ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
GROUNDWATER
Loc. Type:
TRIP BLANK
Sample Depth
Sample Comment
_Q�pF wA�F�Q�
o -<
Sample ID:
AB14388
PO Number#
7W1765
VisitlD
Collect Date:
03/09/2007
Collect Time::
10:00
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/26/2007
Emergency Yes/No
COC Yes/No
YES
AS
Analyte Name
PQL
Result Qualifier
Units
Approved By
74-95-3
Dibromomethane
1.0
Not detected
ug/L
RKELLING
78787-5
1,2-Dichloropropane
0.25
Not detected
ug/L
RKELLING
79-01-6
Trichloroethene
0.25
Not detected
ug/L
RKELLING
75-27-4
Bromodichloromethane
0.25
0.56 J2
ug/L
RKELLING
10061-01-5
cis-1,3-Dichloropropene
0.25
Not detected
ug/L
RKELLING
10061-02-6
trans-1,3-Dichloropropene
0.25
Not detected
ug/L
RKELLING
79-00-5
1,1,2-Trichloroethane
0.25
Not detected
ug/L
RKELLING
108-88-3
Toluene
0.25
Not detected
ug/L
RKELLING
14228-9
1,3-Dichloropropane
0.25
Not detected
ug/L
RKELLING
124-48-1
Dibromochloromethane
0.25
Not detected
ug/L
RKELLING
106-93-4
(EDB)1,2-Dibromoethane
0.25
Not detected
ug/L
RKELLING
127-18-4
Tetrachloroethene
0.25
Not detected
ug/L
RKELLING
108-90-7
Chlorobenzene
0.25
Not detected
ug/L
RKELLING
100-41-4
Ethylbenzene
0.25
Not detected
ug/L
RKELLING
75-25-2
Bromoform
1.0
Not detected
ug/L .
RKELLING
108-38-3
m,p-Xylene
0.50
Not detected
ug/L
RKELLING
100-42-5
Styrene
0.25
Not detected
ug/L
RKELLING
79-34-5
1,1,2,2-Tetrachloroethane
0.25
Not detected
ug/L
RKELLING
630-20-6
1, 1, 1,2-Tetrachloroethane
0.25
Not detected
ug/L
RKELLING
95-47-6
o-Xylene
0.25
Not detected
ug/L
RKELLING
96-18-4
1,2,3-Trichloropropane
0.25
Not detected
ug/L
RKELLING
98-82-8
Isopropylbenzene
0.25
Not detected
ug/L
RKELLING
108-86-1
Bromobenzene
0.25
Not detected
ug/L
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 3

'ection
scr.:
OLD COLOR - TEX WWTP LAGOON
rocationID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
GROUNDWATER
Loc. Type:
TRIP BLANK
Sample Depth
Sample Comment
Sample ID:
AB14388
PO Number#
7W1765
VisitlD
Collect Date:
03/09/2007
Collect Time::.
10:00
Date Received:
03/1312007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/26/2007
Emergency Yes/No
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result Qualifier
Units
Approved By
103-65-1
n-Propylbenzene
0.25
Not detected
ug/L
RKELLING
95-49-8
2-Chlorotoluene
0.25
Not detected
ug/L
RKELLING
106-43-4
4-Chlorotoluene
0.25
Not detected
ug/L
RKELLING
108-67-8
1,35-Trimethylbenzene
0.25
Not detected
ug/L
RKELLING
98-06-6
tert-Butylbenzene
0.25
Not detected
ug/L
RKELLING
95-63-6
1,2,4-Trimethylbenzene
0.25
Not detected
ug/L
RKELLING
135-98-8
sec-Butylbenzene
0.25
Not detected
ug/L
RKELLING
543-73-1
m-Dichlorobenzene(1,3)
0.25
Not detected
ug/L
RKELLING
106-46-7
p-Dichlorobenzene(1,4)
0.25
Not'detected
ug/L
RKELLING
95-50-1
o-Dichlorobenzene (1,2)
0.25
Not detected
ug/L
RKELLING
99-87-6
p-Isopropyltoluene
0.25
Not detected
ug/L
RKELLING
104-51-8
n-Butylbenzene
0.25
Not detected
ug/L
RKELLING
96-12-8
1,2-Dibromo-3-Chloropropane
2.0
Not detected
ug/L
RKELLING
120-82-1
1,2,4-Trichlorobenzene
0.50
Not detected
ug/L
RKELLING
91-20-3
Naphthalene
0.50
Not detected
ug/L
RKELLING
87-68-3
Hexachlorobutadiene
0.50
Not detected
ug/L
RKELLING
87-61-6
1,2,3-Trichlorobenzene
1.0
Not detected
ug/L
RKELLING
2-Chloroethyl vinyl ether
- X
ug/L
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 3 of 3

I
AT BM
SHIPPED BY: Bus Courier to7P Other
COLLECTOR(S): I;LI / %/ ! I
LOCATION CODE: 14y1C. o ;
LATITUDE: LONGITUDE:
WATER QUALITY SEDMENT/TISSUE FORM
5�u�gf
Sedgy Soil(,,Tissue
STATION LOCATION:
REMARKS: V I T lr� S
For Lab Use ONLY 0 ("
Lab Number'
Date Received' ime' d
Redd by:
From: Bus ourler- and
DATA ENTRY BY: K:
DATE REPORTED:
Station #
Date Begin (yy/mm/dd)
Time Begin
Date End (yy/mm/dd)
Time End
Depth DM DB DBM
Value Type
Composite
Sampe
�L ? f �j
I l �j
/(I ; q(I
-
A H L
T S B
IC G GNXX
*For parameters not listed on this fieldsheet, verify capability with the laboratory then write the requested analyses in the appropriate column.
Tissue'
Sediment/Soil•
Units
Tissue'
Units
Sediment/Soil`
Units
Tissue*
Units
Sediment/Soil•
Units
1
As — Arsenic
A — Silver
m /k
Chlorinated Pest
Oil and Grease
2
AI -Aluminum
EUnits
AI -Aluminum
m /k
PCBs
TOC
3
Cd—Cadmium
As —Arsenic
mg/kg
PBBs
J!4
Cr — Chromium
Cd — Cadmium
mg/kg
5
Cu— Copper
mg/kg
Cr—Chromium
mg/kg
6
Fe — Iron
mg/kg
Cu — Copper
m /k
7
Hg — Mercury
mg/kg
Fe — Iron
mg/kg
8
Mn — Manganese
mg/kg
Hg — Mercury
m /k
9
Ni — Nickel
m /k
Mn — Manganese
mg/kg
10
Pb - Lead
mg/kg
Ni — Nickel
mg/kg
11
Se —Selenium
mg/kg
Pb - Lead
mg/kg
12
Zn — Zinc
mg/kg
Se — Selenium
mg/k
13
Zn — Zinc
mg/kg
14
Ca - Calcium
m /k
15
K- Potassium
mg/kg
16
M — Magnesium
m /k
17
Na— Sodium
mg/kg
Fish species(p84005)
18
Fish species— Numeric (p74990)
19
20
Temperature777�In7al
('C)_
Sample Wt. (g)
Length (cm) Sample Wt. (g)
Length (cm) Sam le Wt. ()
Length (cm)
O
WHOLE FISH
1
5 -
9
O
FILLET
2
6
10
112
O
VISCERA
3
7
11
O
SHELLFISH
4
$
O
OTHER

LAB NO.AE14388
Pr
AT
REPORTED BY
AT
CHECKED BY
REVIEWED BY
L'
SAMPLE TYPE: WATER
ENR/DWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYTICAL RESULTS
SUPERVISOR
DATE � 'y
ENTERED BY
DATE
�.:...................................
V ladle:i7 aiila:'
:::::::::::::.:::::::.::::::::::....... P. RESl1L
.:.:!'9...............................:.:.:.:.:.:.:.:.:.:.:.:.:.:.: Q........................,.T.......,...:.:.:.:.:.:.:.:.:.;.:.:.:.:.:.:.:...:.............Vo1a#ile:0 nle..:.:.:.:.;.:.;.:..........................�.PQL.:.:.:.:.:.:.:.:RESULT:.�.:•:�
C .5#.....ac et.Com ound............•........................0 L..............0 /L..•. :.:.:::.:.:.CAS#:.:.:.:.7ar et:Gom ::::::::::u.L::::::::::::=::::-tip
:::::::::::
75-71-8
Dichlorodifluoromethane
1.0
U
630-20-6
1,1,1,2-Tetrachloroethane
0.25
74-87-3
Chloromethane
0.50
U
75-25-2
Bromoform
1.0
75-01-4
Vinyl Chloride
0.50
U
79-34-5
1,1,2,2-Tetrachloroethane
0.25
74-83-9
Bromomethane
0.50
U
96-18A
1,2,3-Trichloropropane
0.25
75-00-3
Chloroethane
0.50
U
108-86-1
Bromobenzene
0.25
75-69-4
Trichlorofluoromethane
0.50
U
95-49-8
2-Chlorotoluene
0.25
75-35A
1,1-Dichloroethene
0.25
U
106-43-4
4-Chlorotoluene
0.25
75-09-2
Methylene Chloride
10
U
541-73-1
1,3-Dichlorobenzene
0.25
156-60-5
trans-1,2-Dichloroethene
0.25
U
106-46-7
1,4-Dichlorobenzene
0.25
75-34-3
1,1-Dichloroethane
0.25
U
95-50-1
1,2-Dichlorobenzene
0.25
594-20-7
2,2-Dichloropropane
0.50
U
96-12-8
1,2-Dibromo-3-Chloropropane
2.0
156-59-4
cis-1,2-Dichloroethene
0.25
U
120-82-1
1,2,4-Trichlorobenzene
0.50
67-66-3
Chloroform
0.25
5.4
87-68-3
Hexachlorobutadiene
0.50
74-97-5
Bromochloromethane
0.25
U
87-61-6
1,2,3-Trichlorobenzene
1.0
71-55-6
1,1,1-Trichloroethane
0.25
U
1634-04A
Methyl-tert-butyl ether
0.25
563-58-6
1,1-Dichloropropene
0.25
U
71-43-2
Benzene
0.25
56-23-5
Carbon Tetrachloride
0.25
U
108-88-3
Toluene
0.25
107-06-2
1,2-Dichloroethane
0.25
U
100-41-4
Ethyl benzene
0.25
79-01-6
Trichloroethene
0.25
U
108-38-3
m,p-Xylenes
0.50
78-87-5
1,2-Dichloropropane
0.25
U
95-47-6
o-Xylene
0.25
75-27-4
Bromodichloromethane
0.25
0.56 J2
100-42-5
Styrene
0.25
74-95-3
Dibromomethane
1.0
U
98-82-8
Isopropylbenzene
0.25
10061-01-5
cis-1,3-Dichloropropene
0.25
U
103-65-1
n-Propylbenzene
0.25
10061-02-6
trans-1,3-Dichloropropene
0.25
U
108-67-8
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0.25
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0.25
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NCDENR MRO
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Mooresville, North Carolina 28115
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REVISED SLUDGE SPILL CLEANUP PLAN
FORMER NC FINISHING / COLOR-TEX FACILITY
2555 NC HIGHWAY 29
SPENCER, ROWAN COUNTY, NORTH CAROLINA
NCDENR INCIDENT #NOV-2006-DV-0071
I
Developer:
1
High Rock Properties, LLC
8734 Brentfield Road
Huntersville, North Carolina 28078��
Property Owner: I S
North Carolina Warehouse LLC
c/o Consilium Partners
399 Boylston Street, Lbby 3
Boston, Massachusetts 02116-3319
Primary Consultant:
Triad Environmental
2321 Walker Avenue
Winston-Salem, North Carolina 27103
Prepared By:
Blue Ridge Geological Services, Inc.
306 Eden Terrace, Suite C
Archdale, North Carolina 27263
336-431-5454 phone/fax
March 2007 (Revised April 2007)

March 29, 2007 (Revised April 12, 2007)
Mr. Mike Francis
Triad Environmental
2321 Walker Avenue
Winston-Salem, North Carolina 27103
Subject: Revised Sludge Spill Cleanup Plan
Former NC Finishing / Color -Tex Facility
2555 NC Highway 29
Spencer, Rowan County, North Carolina
Blue Ridge Project #200725
Dear Mike:
As authorized by your acceptance of our proposal dated March 9, 2007, Blue Ridge Geological Services,
Inc. (Blue Ridge) prepared the attached plan describing the cleanup activities performed to date as well as
the remaining proposed cleanup activities at the subject site. After our conversation with Mr. John Lesley
of the NCDENR on April 12, 2007, we have made several revisions to the plan. We appreciate the
opportunity to assist you on this project. Please contact the undersigned at 336-431-5454 if you have any
questions concerning this plan.
Sincerely,
Jeffrey L. Gerlock, L.G.
NC Licensed Geologist #1141
Attachment
Blue Ridge Geological Services, Inc. * 306 Eden Terrace, Suite C, Archdale, NC 27263 * Phone/Fax: [phone]

March 29, 2007 (Revised April 12, 2007)
Mr. John Lesley, Acting Regional Supervisor
North Carolina Department of Environment and Natural Resources
Division of Water Quality
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Subject: Revised Sludge Spill Cleanup Plan
Former NC Finishing / Color -Tex Facility
2555 NC Highway 29
Spencer, Rowan County, North Carolina
Incident #NOV-2006-DV-0071
Dear Mr. Lesley:
On behalf of High Rock Properties, LLC and Triad Environmental, Blue Ridge Geological Services, Inc.
(Blue Ridge) prepared the attached plan summarizing the activities completed to date and outlining the
proposed cleanup activities at the subject site. The plan was requested during our telephone conversation
on March 2, 2007 and was revised per the items requested in our telephone conversation on April 12,
2007. Please contact the undersigned if you have any questions concerning this plan or this project.
Sincerely,
6 t f
Jeff Gerlock, L.G.
NC Licensed Geologist #1141
Attachment
Cc: Mr. Mike Francis, Triad Environmental
Blue Ridge Geological Services, Inc. * 306 Eden Terrace, Suite C, Archdale, NC 27263 * Phone/Fax: [phone]

Revised Sludge Spill Cleanup Plan Revised April 2007
Former NC Finishing / Color -Tex Facility Blue Ridge Geological Services
Spencer, North Carolina
I. INTRODUCTION
The subject property is the former NC Finishing / Color -Tex Facility at 2555 NC Highway 29 in
Spencer, Rowan County, North Carolina (Figures 1 and 2). On November 27, 2006 an estimated two
to three million gallons of wastewater sludge discharged from an inactive aeration basin at the former
NC Finishing / Color -Tex facility to an unnamed tributary of the Yadkin River (Item 1 on Figure 2).
The release was caused when FC Development LLC of Statesville, North Carolina (FCD), a
contractor for High Rock Properties, LLC (site developer), dislodged a valve connected to a plug in
the bottom of the aeration basin while removing scrap metal around the edge of the basin.
Within two days following the release, FCD personnel installed a silt fence and an earthen dam at the
bottom of the slope of the tributary to contain the wastewater sludge and prevent the sludge from
migrating into the Yadkin River. On November 30, 2006 personnel from the Division of Water
Quality of the Mooresville Regional Office of the North Carolina Department of Environment and
Natural Resources (NCDENR) inspected the subject site and determined that approximately 300 to
500 feet of the tributary was impacted by sludge accumulations from the release. NCDENR
personnel tested the wastewater sludge and determined that the material was non -hazardous and did
not pose an immediate threat to the environment. On December 8, 2006 the NCDENR issued a
Notice of Violation (NOV) letter to High Rock Properties, LLC requesting cleanup of the sludge from
the area. On December 28, 2006 High Rock Properties, LLC submitted a letter to the NCDENR
stating that the cleanup was in progress and they intended to comply with the NCDENR requirements.
Copies of these two letters are attached.
In December 2006 and January 2007 FCD performed cleanup activities at the site. FCD and its
subcontractors used a vacuum truck and hoses and a backhoe and dump trucks to remove the
wastewater sludge from the spill area (Item 2 on Figure 2). The cleanup focused on removal of the
black thick sludge material in the spill area. FCD personnel transported the sludge to an on -site
abandoned digester for storage (Item 4 on Figure 2). According to Mr. Tom Gamelin of FCD,
approximately 50 to 60 loads of material were removed from the spill area and transported to the
digester.
On March 2, 2007 Blue Ridge personnel contacted Mr. John Lesley and Mr. Wes Bell of the
NCDENR. During the telephone conversation, the NCDENR requested a written plan describing the

Revised Sludge Spill Cleanup Plan Revised April 2007
Former NC Finishing/Color-Tex Facility Blue Ridge Geological Services
Spencer, North Carolina
methods and schedule of the remaining cleanup activities for the site. On March 6, 2007 Blue Ridge
personnel visited the site with Mr. Mike Francis of Triad Environmental and Mr. Tom Gamelin of
FCD to familiarize ourselves with the site layout and activities completed. This plan provides the
information requested by the NCDENR.
H. SITE DESCRIPTION
The subject site is the former NC Finishing / Color -Tex facility. According to the Rowan County tax
records, the property is currently owned by North Carolina Warehouse LLC c/o Consilium Partners of
Boston, Massachusetts. The property is currently being developed by High Rock Properties LLC of
Huntersville, North Carolina. The NC Finishing / Color -Tex facility buildings and structures are
currently being demolished and removed. A race track complex with condominiums is to be
constructed in the general vicinity of the area of the spill.
The subject site is located in the Charlotte Geologic Belt. Based on a review of the Geologic Map of
North Carolina, the site is underlain by igneous rock (granite) of the Salisbury Plutonic Suite. The
soils encountered in this area are the residual product of chemical weathering of rock presently
underlying the site. The soil weathering is more advanced near the surface grading with depth to less
weathered rock and finally bedrock. The Rowan County Soil Survey indicates that soils in the
unnamed tributary where the spill occurred are classified as the Chewacla loam. Chewacla soils are
poorly drained with moderate permeability and consist of loam and sandy clay loam. Chewacla soils
are frequently flooded with a seasonal high water table from November to April of 0.5 to 1.5 feet
below ground surface. According to the soil survey, the depth to the bedrock in this soil type is
greater than five feet.
The site is located in the Piedmont Physiographic Province of North Carolina (Piedmont). According
to the topographic map of the site vicinity, the site is located along the eastern flank of a northeast -
southwest trending topographic ridge along NC Highway 29/70 (Figure 1). Elevations in the spill
area range from approximately 620 to 650 feet above mean sea level (MSL). Surface drainage
patterns within the Piedmont typically indicate the direction contaminants would be transported by
surface water or groundwater. Based on our interpretation of the topographic map and on -site
observations, surface water at the site is expected to flow to the east and northeast into an unnamed
tributary of the Yadkin (Figure 1). The surface drainage from the site and adjacent properties could
2

Revised Sludge Spill Cleanup Plan Revised April 2007
Former NC Finishing / Color -Tex Facility Blue Ridge Geological Services
Spencer, North Carolina
be influenced by cultural features, such as buildings, paved areas, curbs, gutters, and storm drain
systems.
III. RECEPTOR INFORMATION
The site is located in an undeveloped and industrial area east of the Town of Spencer. Undeveloped
wooded property, the Yadkin River, and the former NC Finishing / Color -Tex facility are located in
the immediate vicinity. The drainage feature / unnamed tributary and the Yadkin River are the only
receptors in the immediate area of the release of sludge material. No underground utilities, basements,
or water supply wells were observed in the immediate vicinity of the spill. The nearest surface water
feature is the unnamed tributary and overflow areas of the Yadkin River. The main channel of the
Yadkin River is located approximately 700 feet northeast of the limits of the spill (Figures 1 and 2).
IV. INITIAL INVESTIGATION RESULTS
On November 30, 2006 personnel from the NCDENR Division of Water Quality inspected the subject
site and determined that approximately 300 to 500 feet of the unnamed tributary to the Yadkin River
was impacted by wastewater sludge from the release. On December 1, 2006 NCDENR personnel
collected a sample of the wastewater sludge from the banks of the unnamed tributary and transported
the sample to Pace Analytical Services, Inc. in Huntersville, North Carolina for analysis. The sample
was analyzed for eight RCRA metals using the Toxic Characteristic Leaching Procedure (TCLP).
Barium (0.2 milligrams per liter — mg/L) and lead (0.072 mg/L) were the only metals detected in the
sample collected. These two metals were detected at concentrations below the TCLP regulatory limits
for barium (100 mg/L) and lead (5.0 mg/L) established by the EPA, therefore, the NCDENR
determined that the sludge was a non -hazardous material. NCDENR personnel also checked the
water quality parameters (ph, conductivity, dissolved oxygen) of the surface water in the unnamed
tributary and determined that the water quality had not been affected by the release. A copy of the
laboratory report is attached.
3

Revised Sludge Spill Cleanup Plan
Former NC Finishing / Color -Tex Facility
Spencer, North Carolina
Revised April 2007
Blue Ridge Geological Services
V. PROPOSED ADDITONAL CLEANUP / REMEDIATION PLAN
Based on the results of the initial investigation and cleanup, the area of the spill appears to be limited
to the area at the base of the hill below the former aeration basin in the unnamed tributary to the
Yadkin River. The majority of the dark sludge material was removed from the spill area in December
2006 and January 2007 and transported to the on -site digester. Blue Ridge personnel did not observe
any dark sludge on the surface in the spill area on March 6, 2007. Minor amounts of sludge appeared
to be located in the bottom of several pools of water in the drainage ditch / disturbed area in the base
of the slope. The following additional actions will be performed at the site:
FCD personnel will mobilize a backhoe / trackhoe to the site and scoop out the dark sludge material
remaining in the spill area. The removal will be based on identifying and removing any dark sludge
material encountered. We estimate the five to ten loads of material will be removed. FCD will place
the sludge into dump trucks and transport the material to the on -site digester for storage (Item 4 on
Figure 2). FCD personnel will then regrade the site to pre -spill and cleanup conditions. FCD will
plant grass and vegetation as needed in the disturbed areas similar to the surrounding vegetation.
Triad Environmental and/or Blue Ridge personnel will observe and document the activities with field
notes and photographs. Blue Ridge will prepare and submit a cleanup report to the NCDENR
summarizing the additional actions performed at the property.
VI. SCHEDULE
The proposed schedule for the remaining activities is as follows:
e Sludge Removal and Regrading / Landscaping — to be completed on or before May 25, 2007.
• Reporting — to be submitted to the NCDENR within one week following the completion of
the field activities.
4

APPENDIX
FIGURES
NCDENR CORRESPONDENCE
LAB DATA

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Site Location Map
Former NC Finishing / Color -Tex Facility
REF.: Salisbury, North Carolina USGS Quadrangle Map revised 1987 2555 NC Highway 29
from Microsoft Terraserver Spencer, North Carolina
Date: March 2007 1 Figure 1

Pace Analytical Servtass, 1e7e.
98m3,Kncey=Avenue, Suite 100
ac�[ Huntersville,.rVz 28079
ie ` nalX cal/ ." Phone 704 8E5.9092
s,snti;pacelabs.ccarra Fax: 794,875,9091
t
D ce3eber 12, .2006
a,C Div. of Water Re4aurces-
610East- Center Ave
Suite 3 l
.ccres.iiie, NC 2.3115
EE: Lah P-anent h nber: 9213332e
Client Project M Color -Tex WWP Sludge Spill l a
Lea_ Vs. Huffman .
fi:closed are the: analytical results for sanale(s} received by the laboratory on December.5, 2G053. .Re.sulte
reperted herein conioxx to tho „ost current NELAC standards, -,;hero applicable, unless otherwise narrated in th=_
hody-cf the report
I cr_anit Piet Che =Sstzy and Xetais Analyses were perfo=ed at our Pace Aahev l•le laboratory and Organic tes
;ae serforsed at. ns- Yace:.Clarlotte laboratory unle:ca othervise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
D
kerin.herring�'pacelabs.coz2
project. manager
Enclosures -
REPORT OF LABORATORY ANALYSIS
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High Rock Properties LLC
c/o David L. Risdon
8734: Srentfield Road
Huntersville, NC 28078
December 28, 2006
Mr. Wes Bell
Environmental Technician IV
Surface °Water Protection Section
Division of Water Quality
North Carolina Department of Environment and Natural Resources
SENT VIA E-MAIL.
To wes.bell@ ncmail.net
Dear Mr. Bell;
As requested in Mr. Lesley's letter to me dated December 8, 2006, this is a
response indicating the actions to contain, collect, and properly dispose of the
sludge from all affected areas.
Doug Thomas and his crew have erected berms and have trucked out large
quantities of sludge and, working under the direction of Triad Environmental, has
contracted to have the remaining sludge pumped from the affected area. The
sludge is being trucked and/or pumped to a secure empty holding. pond on our
property. We believe. that within two to three weeks the potential for sludge to
spread from the affected area will be completely contained. We will continue to
work under the direction of Triad Environmental to ensure that we meet the
State's cleanup requirements.
Please do not hesitate to contact me should you have any questions or concerns.
Thank. you.
Sincerely,
David L. Risdon
Chief Executive Officer

,ylichaelF,Easley,Governor
William G, Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources.
Alan W. Klimek, P.E. Director
Division of Water Quality'
December 8, 2006
!CERTIFIED HAIL
RETURN Rj� 'CCIPT R QELiSTED
Mr. Dave Risdon, Owner
High, Rock Properties, LLC
8734 I3rentfield Road
lluntersville, North Carolina 28078
Subject: Notice of Violation/Not ice of
Recommendation for Enforcement
Violatibns of G.S. 143-2.15A and G.S. 143-
21.5.C(c)
Non -permitted Discharge/Failure to Report
Old Color -Tex WWTP
Incidenttf: NOV-2006-DV-0071
Rowan County, N.C.
Dear Mr. Risdon.,.
Chapter 143, Article 21 of the North Carolina General Statutes (G.S.) authorizes and directs the
Environmental Management Commission of the Department of Env iroament. &Natural Resources to
protect and preserve the water resources of the State. Tile Division- of Water Quatity (DWQ) has the
delegated authority to enforce adopted water pollution control rules and regulations,
As a result of the initial investigation conducted by DWQ staff on November 30, 2006, the
following conditions were .found to be it) violation of G.S. 143-21.5.land G.S. 143-215.C(c),:
On November27, 2006 (early afternoon), an estimated 2 to 3 million
gallons of: wastewater/sludge was discharged to an unnamed. -tributary to
Yadkin River from an inactive aeration basin. at'the old Color -Tex
Wastewater Treatment Plant. (W WTP). The valve was
removed/dislodged during the on -site, removal of scrap metal.
Approximately 300 - 500 feet of stream was impacted with sludge
accumulations. The unpermitted discharge was never reported to DWQ:
Be advised that G.S. I43-215.6A, provides for a:civil penalty assessment. of not more, that twenty-
five thousand dollars ($25,000.00), or twenty-five thousand dollars ($25,000.00) per day when tine
violation is or continuing nature, against any person who is required but fails. to apply for or to secure a
perni t required by G.S. 143-215.1. Penalties may also be assessed for any damage to the surface waters of
ATA the State that may result from. the unpermitted discl.arge. NorihCirolin
DlENR

I.4
Mr. Dave Risdon
Page Two
December S, 2006
It is requested. that you. respond, in writing, to this Notice, indicating the actions taken to contain,
collect, and properly dispose of the sludge from all affected areas. In addition, your response shall include
the actions taken to restore all affected areas. Please address your response to Mr. Bell by no later than
3cember 29, 2006.
This letter is also to.advise you that this Office is considering sending a recommendation for
enforcement: action to the Director of' the Division of Water Quality for the violations of G.S. 1 43-215.1
(unperinitted discharge) and G.S. 14372I 5.C(c) (failure to. report the discharge)..If you have an
explanation for the violations that you wish to present, please include same in the requested response:
'Your explanation will be reviewed and if an enforcement action is still deernedappropriate, your
explanation will be forwarded to the Director along with the enforcement package for his consideration.
To comply with the regulations, it will be necessary to contain, collect, and properly dispose of the
sludge from all affected areas, in addition, all affected areas must be restored to the conditions existing
prior to the discharge.
Should you have questions, please do not hesitate to contact Mr. Bell or me :at (704) �63-1699.
Sincerely,
ohn Lesley
Acting Regional Supervisor."
Surface Water Protection
Attachments
cc: Rowan County Health Department
Rick Shiver, Assistant Director of Regional Operations, DWQ
Andrew Pitner, Regional Supervisor, DWQ/APS
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INVOICE
rM
aceAnalytical
www.pacelabs.com
Ms. Ellen Huffman
NC Div. of Water Resources
610 East Center Ave
Suite 301
Mooresville, NC 28115
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Number: 92156382
Di
" 12/12/2006
e
Please Remit To:
Pace Analytical Services, Inc.
Box 684056
Milwaukee, WI 53268-4056 -
Client No
r Purchase Ostler No y
Proecf Manager 5' q a
Terms'
3.PageNo �3
616566/92-NCDENR-
Kevin Herring
Due Upon Receipt
1
Client Reference:
Color -Tex WWP Sludge Spill
Pace Project No:
92133328
Quantity U/M
Description Method- Matrix
Price
Total
ANALYTICAL Charges:
'
1.00 ea
Environmental Sample Disposal Soil
5.00
$ 5.00
1.00 ea
Trace ICP Metals, TCLP Leach. EPA 6010 Soil
50.00
$ 50.00
1.00 ea
Mercury, CVAAS, TCLP Leachate EPA 7470 Soil
25.00
$ 25.00
1.00 ea
Charge for TCLP Extraction Soil
40.00
$ 40.00
ANALYTICAL SUBTOTAL:
$ 120.00
TOTAL INVOICE AMOUNT:
--------------
$ 120.00
WIE
DEC 1 5
M06
PLEASE PRINT
INVOICE # AND CLIENT #
NC DENR PARO
ON YOUR CHECK
DWQ _ Aquifer
rotection
1.5% MONTHLY FINANCE CHARGE ASSESSED AFTER 30 DAYS.
LEASE REFER TO INVOICE NUMBER 92156382 WHEN REMITTING.
AN EQUAL OPPORTUNITY EMPLOYER

Un
ceAnalyticl °
www.pacelabs.com
December 12, 2006
Ms. Ellen Huffman
NC Div. of Water Resources
610 East Center Ave
Suite 301
Mooresville, NC 28115
RE: Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Dear Ms. Huffman:
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
2225 Riverside' Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 5, 2006. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail].
Project Manager
Enclosures
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 37712 without the written consent of Pace Analytical Services, Inc.
99030
FL NELAP E87648 N p
W F
P-la=
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Parameters
Metals
Trace ICP Metals;-.TCLP'Leach
Date Digested-;"
Trace ICP.Metals, TCLP Leach
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date Digested
Mercury, CVAAS, TCLP Leachate
Mercury
Date: 12/12/06
Results
Method: EPA 6010
12/06/06 14:00
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
Project Sample Number: 92133328-001 Date Collected: 12/01/06 13:25
Matrix: Soil Date Received: 12/05/06 08:05
Units Report Limit DF Analyzed By CAS No
Prep/Method: EPA 3010 / EPA 6010
ND
mg/l
0.025
0.20
mg/l
0.025
ND
mg/l
0.0050
ND
mg/l
0.025
0.072
mg/l
0.025
ND
mg/l
0.050
ND
mg/l
0.025
12/07/06 11:20
Method: EPA 7470
ND mg/l
12/06/06 14:00
1.0 12/1Q/06 14:45 JDA1 7440-38-2
1.0 12/10/06 14:45 JDA1 7440-39-3
1.0 12/10/06 14:45 JDA1 7440-43-9
1.0 12/10/06 14:45 JDA1 7440-47-3
1.0 12/10/06'14:45 JDA1 7439-92-1
1.0 12/10/06 14:45 JDA1 7782-49-2
1.0 12/10/06 14:45 JDA1 7440-22-4
12/07/06 11:20
0.00020 1.0 12/11/06 15,:11 ALV 7439-97-6
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
SC 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 " ACCRR
¢feel
Qual RegLmt
Page: 1 of 6
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

aceAlnalicl °
www.pacelabs.com
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
PARAMETER FOOTNOTES
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract, or moisture content
Method 9071B modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
Date: 12/12/06
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
37712 This report shall not be reproduced, except in full,
NC Drinking Water
SC 37712 without the written consent of Pace Analytical Services, Inc.
99030
FL NELAP E87648 �° N FCCQR09
We
Page: 2 of 6
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
ceniical ° Phone: [phone] Phone: [phone]
Fax: [phone] Fax. [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
QC Batch: 174942 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: Mercury, CVAAS, TCLP Leachate
Associated Lab Samples: 927752667
METHOD BLANK: 927767921
Associated Lab Samples: 927752667
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/l NO 0.0002
LABORATORY CONTROL SAMPLE: 927767939 ,
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Mercury mg/l 0.0025 0.0027 107
MATRIX SPIKE: 927767947
Parameter Units
Mercury mg/l
SAMPLE DUPLICATE: 927767954
927757112 Spike MS MS
Result Conc. Result % Rec Footnotes
0.00001 0.0025 0.0027 109
927762351 DUP
Parameter Units Result Result RPD Footnotes
Mercury mg/l 0.00500 NO NC
Date: 12/12/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written. consent of Pace Analytical Services, Inc.
E� p AC COg09
'hlc_
Page: 3 of 6
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
aceAnalytical o Phone. 704.875.909
Fax: [phone]
www.pacelabs.com , QUALITY CONTROL DATA
Lab Project Number:
Client Project ID:
2225 Riverside- Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
92133328
Color -Tex WWP Sludge Spill
QC Batch: 174842
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis
Description: Trace ICP Metals, TCLP Leach.
Associated Lab Samples
927752667
METHOD BLANK: 927761619
Associated Lab Samples:
927752667
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Arsenic
mg/l
ND
0.025
Barium
mg/l
ND
0.025
Cadmium
mg/l
ND
0.0050
Chromium
mg/l
ND
0.025
Lead
mg/l
ND
0.025
Selenium
mg/l
NO
0.050
Silver
mg/l
ND
0.025
LABORATORY CONTROL SAMPLE: 927761627
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
MATRIX SPIKE: 927761635
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Date: 12/12/06
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Spike
LCS
LCS
Units
Conc.
Result
Rec Footnotes
mg/l
2.500
2.460
98
mg/l
2.500
2.390
96
mg/l
2.500
2.290
92
mg/l
2.500
2.205
88
mg/l
2.500
2.130
85
mg/l
2.500
2.485
99
mg/l
1.250
1.110
89
927752873
Units
Result
mg/l
0.00980
mg/l
0.6800
mg/l
0.01065
mg/l
0
mg/l
2.230
Spike
MS
MS
Conc.
Result
% Rec Footnotes
2.500
2.435
97
2.560
2.490
72 1
2.500
2.115
84
2.500
2.070
83
2.500
4.265
81
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
p N ACiOgO
CAW
l
Page: 4 of 6
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

9800 Kincey Avenue, Suite 100
2225 Riverside Drive
Huntersville, NC 28078
Asheville, NC 28804
°
' ace
Phone: [phone]
Phone: [phone]
�nal�tical
Fax [phone]
Fax [phone]
www.pacelabs.com
QUALITY
CONTROL DATA
Lab Project Number:
92133328
Client Project ID:
Color -Tex WWP Sludge Spill
MATRIX SPIKE: 927761635
927752873
Spike MS MS
Parameter Units
Result
Conc. Result X Rec Footnotes
Selenium mg/l
0.00545
2.500 2.425 97
Silver mg/l
0.00860
1.250 1.100 87
SAMPLE DUPLICATE: 927761643
Parameter
Units
Arsenic
mg/l
Barium
mg/l
Cadmium
mg/l
Chromium
mg/l
Lead
mg/l
Selenium
mg/l
Silver
mg/l
Date: 12/12/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
927752865 DUP
sult Result RPD Footnotes
ND ND NC
0.4700 0.4900 5
0.1900 0.2000 4
ND ND NC
0.2500 0.2600 6
ND ND NC
ND ND NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\�O= N_-A CCOA09
elacllt.
Page: 5 of 6
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

9800 Kincey Avenue, Suite 100 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
ace Aria/ytical Phone: [phone] Phone: [phone]
Fax: [phone] Fax- 828.252.4618
www. pacelabs. com
Lab Project Number: 92133328
Client Project ID: Color -Tex WWP Sludge Spill
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines,:uInrounded concentrations are displayed and have been used to calculate X Rec and RPD values.
LCS(D) Laboratory .,Control Sample (Duplicate)
MS(D) Matrix.Spike`(Duplicate).
DUP Sample,Duplicate
ND Notdetected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
Ell The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
Date: 12/12/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
y AC��q
v�
Page: 6 of 6
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

'Ti ti
f; i )
WATER QUALITY" SECTION
Papc � aC�
CHAIN OF CUSTODY (COC C.0_RD
�• i
INC DENRJDIVQ LABORATORY (check one): I J CENTRAL I J ARO I J WaRO C d.
J
For Investigation of: 5fill C, I
c) /Tex
ir
Sample collector (printname JJ {{ {{
and DM -I forms completed by: i iJ' 1`'1 Ti l i'7-3 3�L'i P Sample collector's signature:
1 y T
Field storage conditions and location (when applicable): t �ti) •C��
1 L,;.
r.' , r,s � :3 .� �,`.�-*'rat r�1- ) t's3' i;'G i L',✓ C �i r'� '� ;<�� i _ tr.z'!!; r.
Lab Use Onty
LAB NO.
STATION NO.
V
STATION LOCATION ,
DATE
SAMPLED
TIME
SAMPLED
NUMBER
OF
CONTAIINERS
� J rf ' `3 %^ t 0+
11 J
cQ ill
1 � yIR
Relinquished by (sigpature) I
Date! �,
Time
Receik
• by (i�nature):
W,t
Date-
Time „
[� .
Relinquished by (signature)!;
ar
Date
Time
Received by (signature):
Date
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment circle one)- State Courier Hand�eliver a ' Federal Ex r-ss . UPS Other.
5'e c ; t r, ,+ -} ,.
SecurityTyp� e
and C.nditions:
d b
Sealed �-1
C �s��
Bken b
ro
1 y:
R
INTRALABORATORY CHAIN OF CUSTODY - Lab Use Only
LAB NUMBERS
.FROM. THROUGH
NUMBER
BOTTLES
ANALYSES
REQUESTED
RELINQUISHED
BY:
RECEIVED
BY:
DATE
TIME
QA\Fomis\Sample Receiving\COC form WQ
4f] 0101 &s
r
C

XC DWO Laboratory
Section
Wesults
PrICD-
��.•., �,�, I_e,s �
UPSTREAM @ UT TO YADKIN RIDER " "� ?.
„ ,
Sample ID:
PO Number #
AB11245
6W8227
Location:
MROSPNLC
�- OFFICE
VisitlD
County:
River Basin
ROWAN
_ �dF wp`rFRQ
`Q G`tX
Collect Date:
Collect Time::
12/01/2006
12:33
Report To
MROSP
j
r
Region:
MRO
DEC 2 1 200t O
Y
Date Received:
12I05/2006
Collector:
W BELL
Time Received:
10:05
Sample Matrix:
SURFACEWATER
Labworks LoginlD
MMA
Loc. Type:
RIVER/STREAM
i.
Date Reported:
12/18/2006
Sample Depth
1
.n
U TER
Emergency Yes/No
YES
Sample Comment
i b kny
COC Yes/No
YES
CAS#
Analyte Name PQL Result Qualifier
Units
Approved By
LAB
Sample temperature at receipt by lab ' I
1.2
°C
MMATHIS
MET-
-
--- -----
25 U
7440-02-0 Ni by ICPMS
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 1
ESTAFFORD

PV
COUNTY ILL,)C1yl
RIVER BASIN : . j . r. 6,61 -- f"•? IV •� �
REPORT TO /b !� Regional Office
Other :
COLLECTOR(S) [d (
Estimated BOD Range:
Seed:
k/Location Code
601
Chlorinated: ..C:
Date Begin (yy/mm/dd) Date End (yy/mm/dd)
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg(L
Coliform: MF Fecal 31616 /100m1
Coliform: MF Total 31504 /100ml
Coliform: tube Fecal 31615 /100ml
Coliform: Fecal Strap 31673 /100ml
Residue: Total 500 mg/L
Volatile 505 mg/L
Fixed 510 mg1L
Residue: Suspended 530 mg/L
Volatile 535 mg1L
Fixed 540 mg/L
pH 403 units
Acidity to pH 4.5 436 mg/L
Acidity to pH 8.3 435 mg/L
Alkalinity to pH 8.3 415 mg/L
Alkalinity to pH 4.5 410 mg/L
TOC 680 mg/L
Turbidity 76 NfU
Coliform Total Tube "/100 mis
DIVISION OF WATER QUALITY //,
Chemistry Laboratory Report / Water Quality Lab Number (9 ! V
SAMPLE TYPE Date Received •,iL Fj 'A
PRIORITY Time Received
AMBIENT QA 4TREAM EFFLUENT Received By
COMPLIANCE CHAIN OF CUSTODY ❑ LAKE 0 INFLUENT
�MERGENCY VISIT ID ESTUARY Data Released
® Date Reported
Station Location: ®� 1
j%�Remarks: � � �/' �"�-p7Ci 1')) � �1,`I' 44t ��Ls �7 1 it Y) / j/ "iia cf
Time Begin Time End Depth - DM, DB, DBM Value Type- A, H, L Composite-T, S, Sample Type
.r /✓'r4--i ^' CY
Chloride 940 mg/L
Chi a: Tri 32217 ug/L
Chi a: Corr 32209 ug/L
Pheophytin a 32213 ug/L
Color: True 80 C.U.
Color: (pH) 83 pH= C.U.
Color:pH7.6 82 C.U.
Cyanide 720 mg/L
Fluoride 951 mg(L
Formaldehyde 71380 mg/L
Grease and Oils 556 mg/L
Hardness Total 900 mg/L
Specific Cond. 95 umhos(cm
MBAS 38260 mg/L
Phenols 32730 ug(L
Sulfate 945 mg/L
Sulfide 745 mg(L
Boron
Tannin & Lignin ug/L
Hexavalent Chromium ug(L
Bicarbonate mg/L
Carbonate mg/L
Total Dissolved Solids mg/L
NH3 as N 610 mg/L
TKN an N 625 mg/L
NO2 plus NO3 as N 630 mg/L
P: Total as P 665 mg/L
PO4 as P 70507 mg/L
P: Dissolved as P 666 mg/L
K-Potassium mg/L,
Cd- Cadmium 1027 ug/L
Cr-Chromium:Total 1034 ug/L
Cu- Copper 1042 ug(L
Ni-Nickel 1067 ug/L
l
Pb- Lead 1051 u_elL
Zn- Zinc 1092 ug/L
V-Vanadium ug/L
Ag- Silver 1077 uv/L
At- Aluminum 1105 ug/L
Be- Beryllium 1012 ug/L
Ca- Calcium 916 mg/L
Co- Cobalt 1037 ug/L
Fe -Iron 1045 ug/L
Mo-Molybdenum ug/L
Sb-Antimony ug/L
Sn-Tin ug/L
TI-Thallium ug/L
Ti-Titanium ug/L
llg-1631 ng/L
Li -Lithium 1132 ug/L
Mg- Magnesium 927 mg/L
Mn-Manganese 1055 ug/L
Na- Sodium 929 mg(L
Arsenic:Total 1002 uYL
e- Selenium 1147 ug(L
Hg- Mercury 71900 ug/L,
Ba-Barium ug/L
Organochlorine Pesticides
Organophosphorus Pesticides
Acid Herbicides
Base/Neutral&Acid Extractable Organic
TPH Diesel Range
Purgeable Organics (VOA bottle req'd)
TPH Gasoline Range
TPH/BTEX Gasoline Range
Phytoplankton
Temnerature on arrival PC):
1.
COMMENTS:
!1 f! I P t c

Descr.:
Location ID:
County:
River Basin
Report To
Region:
Collector:
Sample Matrix:
Loc. Type:
Sample Depth
DOWNSTREAM @ UT TO YADKIN RIVEftcll r �' "
121
MROSPNLC '�� �� 1v3' E '6'alONAL OFFICE
ROWAN r 4 NN A
MROSP r
MRO DEC 2 1 2001 a ,c
W BELL
SURFACEWATER
RIVER/STREAM
1
Sample Comment
`VI T E L' '� ! � ITS ECTIO e
Sample ID: AB11246
PO Number # 6W8228
VisitlD
Collect Date: 12/0112006
Collect Time:: 14:35
f� Date Received: 12/05/2006
U Time Received: 10:05
Labworks LoginlD MMA
Date Reported: 12/18/2006
Emergency Yes/No YES
COC Yes/No YES
CAS # Analyte Name PQL Result Qualifier Units Approved By
LAB
Sample temperature at receipt by lab I I 1.2 °C MMATHIS
RA CT
7440-22-4
Ag by ICPMS
5.0
5.0
U
ug/L
ESTAFFORD
7429-90-5
AI by ICP
50
1400
ug/L
ESTAFFORD
7440-38-2
As by ICPMS
5.0
5.0
U
ug/L
ESTAFFORD
7440-43-9
7440-47-3
Cd by ICPMS
Cr by ICPMS
2.0
25
2.0
25
U
U
ug/L
ug/L
ESTAFFORD
ESTAFFORD
7440-50-8
Cu by ICPMS
2.0
43
ug/L
ESTAFFORD
7440-48-4
Fe by ICP
50
5000
ug/L
ESTAFFORD
7439-97-6
Hg 245.1
0.2
0.20
U
ug/L
ESTAFFORD
7439-93-2
Li ICP
25
25
U
ug/L
ESTAFFORD
7439-95-4
Mg by ICP
0.10
6.7
mg/L
ESTAFFORD
7439-96-5
Mn by ICPMS
10
1500
ug/L
ESTAFFORD
7440-02-0
Ni by ICPMS
10
10
U
ug/L
ESTAFFORD
7439-92-1
Pb by ICPMS
10
10
U
ug/L
ESTAFFORD
7440-66-6
Zn by ICP
10
12
ug/L
ESTAFFORD
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 1

COUNTY K
RIVER BASIN: G, t
REPORT TO { gL Regional Office
Other :
COLLECTOR(S)
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Water Quality
SAMPLE TYPE
PRIORITY
AMBIENT QA EZ/S�EAM EFFLUENT
C MPLIANCE CHAIN OF CUSTODY LAKE INFLUENT
EMERGENCY VISIT ID ESTUARY
0 '
Lab Number wwewcg
Date Received : t�96'/A,p
Time Received
Received
Data Released :
Date Reported
lJ
Estimated BOD Range: Station Location: 0yl..�
Seed: Chlorinated: AI Remarks: f4 C�nm i ! re q -" t L14— 4
Y ,'
Station N/Location Code Date Begin (yy/mm/dd) 71Date End (yy/mm/dd) Time Begin Time End Depth - DM, DB, DBM Value Type- A, H, L1 - &14 1
Composite-T, S, Sample Type
BOD 310 mE/L
COD High 340 mg(L
COD Low 335 mE/L
Coliform: MF Fecal 31616 /100MI
Colifomt: MF Total 31504 /100m1
Colifomt tube Fecal 31615 /100ml
Colifonn: Fecal Strep 31673 /100MI
Residue: Total 500 mg/L
Volatile 505 mg/L
Fixed 510 mg/L
Residue: Suspended 530 me,JL
Volatile 535 mg/L
Fixed 540 mg/L
pH 403 units
Acidity to pH 4.5 436 mg(L
Acidity to pH 8.3 435 mg/L
Alkalinity to pH 8.3-415 mg/L
Alkalinity to pH 4.5 410 mg/L
TOC 680 mg/L
Turbidity 76 NTU
ColiformTotal Tube "/I00 mis
Chloride 940 mg/L,
Chl a: Tri 32217 ur,./L
Chl a: Corr 32209 u9rL
Pheophytin a 32213 ug/L
Color: True 80 C.U.
Color: (pH) 83 pH= C.U.
Color: pH 7.6 82 C.U.
Cyanide 720 mgJL
Fluoride 951 mg/L
Formaldehyde 71880 mg/L "
Grease and Oils 556 mE/L
Hardness Total900 mSIL
Specific Cond. 95 umhos/cm
MBAS 38260 mg/L
Phenols32730 ug(L
Sulfate 945 mg/L
Sulfide 745 mg/L
Boron
Tannin & Lignin ugtL,
Hexavalent Chromium ug/L
Bicarbonate mg(L
Carbonate mg(L
Total Dissolved Solids mg/L
NH3 as N 610 mg/L
TKN an N 625 mg/L
NO2 plus NO3 as N 630 mg/L
P: Total as P 665 mg/L
PO4 as P 70507 mg/L
P: Dissolved as P 666 mg/L
K-Potassium M9/L
Cd- Cadmium 1027 ug/L
•%/.Cr-Chromium:Total
1034 ug/L
Cu-Copper 1042 ugIL
Ni-Nickel 1067 ug/L
Pb-Lead 1051 ue/L
Zn- Zinc 1092 ug/L
V-Vanadium ug1L
Ag- Silver 1077 ug/L
AI -Aluminum 1105 ug/L
Be- Beryllium 1012 ug/L
Ca- Calcium 916 mg/L
Co- Cobalt 1037 ug/L
Fe -Iron 1045 uWL
Mo-Molybdenum ug(L
Sb-Antimony ug/L
Sn-Tin uE/L
TI-Thallium ug/L
Ti-Titanium ug(L
14g.163 I nE/L
Li -Lithium 1132 ug/L
Mg- Magnesium 927
mg/L
Mn-Manganese 1055
ug/L
Na- Sodium 929
mg/L
Arsenic :Total1002
ug/L
Se -Selenium 1147
ug/L
Hq- Mercury 71900
ug/L
COMMENTS: U Tf > fJl �% �� % C='1
Organochlorine Pesticides
Organophosphoms Pesticides
Acid Herbicides
Base(Neutral&Acid Extractable Organic
TPH Diesel Range
Purgeable Organics (VOA bottle req'd)
TPH Gasoline Range
TPH/BTEX Gasoline Range
Phytoplankton
Temperature on arrival M): �Iq

XC DWO Laboratory Section Results
oc. Descr.: DOWNSTREAM @ UT TO YADKIN RLVBRr i . OV LNI 9"rCUKIIdra Sample ID: AB11247
Location ID: MROSPNLC AND NATURAL RESOURCES
PO Number # 6W8229
County: ROWAN
plOORESViLLE R- REGIONAL OFFICE VisitlD
F \NA)E
River Basin r� Collect Date: 12/01/2006
�� QG /—
Report To MROSP y Collect Time:: 13:50
r
Region: MRO >Date Received: 12/0512006
Collector: W BELL DEC 2 200t 0 Time Received: 10:05
Sample Matrix: SURFACEWATER
Loc. Type: RIVER/STREAM Labworks LoginlD MMA
Sample Depth 1 C Date Reported: 12/18/2006
Sample Comment €'' I a r, Emergency Yes/No YES
AT o e ®IY SIEITI ' R COC Yes/No YES
CAS# Analyte Name PQL Result Qualifier Units Approved By
LAB
Sample temperature at receipt by lab I I 1.2 °C MMATHIS
Uy 1%.rrvio 1U 10 U ug/L ESTAFFORD —
7440-66-6 Zn by ICP 110 10 U uq/L ESTAFFORD
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 1

COUNTY
RIVER BASIN:t`A
REPORT TO Nl �V Regional Office
Other :
COLLECTOR(S) &
14"�ktvnst kl
Estimated BOD Range:
Seed: Chlorinated: IV
A—
COMMENTS:
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Water Quality
PRIORITY SAMPLE TYPE
AMBIENT QA STREAM EFFLUENT
COMPLIANCE dCIN OF CUSTODY 0 LAKE INFLUENT
�MERGENCY VISIT ID ESTUAR
L31IStation Location:
—s
Remarks: 4- `IeiC(T ns
ide 940
Tri 32217
Corr 32209
hytin a 32213
True 80 C.U.
(pH) 83 pH= C.U.
C556
p.,L
pH 82 C.U.
e 720
e 951
ldehyde 71880
and Oils 556
Hardness Total 900 mg/L ,
Specific Cond. 95 umhos/cm
MBAS 38260 mg/L
Phenols 32730 ug/L
Sulfate 945 mWL
Sulfide 745 mg/L
Boron
Tannin & Lignin ug/L
Hexavalent Chromium uWL ,
Bicarbonate mg/L
Carbonate mg/L
Total Dissolved Solids mg/L
610
625
NO3 as N 630s
EEEmgIlL
P 665
70507
P: Dissolved as P 666 mg(L
K-Potassium mg/L
Cd- Cadmium 1027 ug/L
Cr-Chromium:Total 1034 ug/L
Cu- Copper 1042 ug/L
{/
Ni-Nickel 1067 ug/L
51 ug/L
92 up
ug/L
EAlumi.,Inum
077 ug/L
1105 uofL
Be- Berylium 1012 ug/L
Ca- Calcium 916 mg/L
Co- Cobalt 1037 up/L
Fe- Iron 1045 ug/L
Mo-Molybdenum ug/L
Sb-Antimony ug/L
Sn-Tin ug/L
TI-Thallium ug/L
Ti-Titanium ug/L
Hg-1631 ng/L
Lab Number�71
Date ReceiveTime ReceiveReceivedBy
Data Released :
Date Reported

5VC DWO Laboratory Section
L-k.:4)escr.: OLD COLOR - TEX WWTP LAGOON f C tApS,t�
'e
t su tiro Location ID: NC0005487r-
County: ROWAN lts+�mi r 0�aF w,gjF�QG
River Basin
Qy
Report To MROSP
Region: MRO
Collector: W BELL APR 00 o Y�
Sample Matrix: SOIL/SEDIMENT l .
Loc. Type: SOIL/SEDIMENT
Sample Depth 3 y A
Sample Comment�ii�p,�
Sample ID:
AB14383
PO Number#
7W1760
VisitlD
Collect Date:
03/0912007
Collect Time::
12:05
Date Received:
03/1312007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
YES
COC Yes/No
YES
CAS # Analyte Name PQL Result Qualifier Units Approved By
LAB
Sample temperature at receipt by lab I 2.6 °C MMATHIS
MET F
7440-22-4
Ag in solid samples by ICPMS
0.20
0.38
mg/Kg
ESTAFFORD
7429-90-5
AI in solid samples by ICP
5.0
12000
J2
mg/Kg
ESTAFFORD
7440-38-2
Arsenic solid samples by ICPMS
0.20 _
4.4
mg/Kg
ESTAFFORD
7440-43-9
Cadmium in solids samples by ICPMS
0.20
1.6
J2
mg/kg
ESTAFFORD
7440-70-2
Calcium in solid samples by ICP
10
4400
J2
mg/Kg
ESTAFFORD
7440-47-3
Cr in solids samples by ICPMS
0".20
290
J2
mg/kg
ESTAFFORD
7440-50-8
Cu solid samples by ICPMS
0.20
200
J2
mg/kg
ESTAFFORD
7439-97-6
Hg 245.5 solid
0.02
1.0
mg/Kg
ESTAFFORD
7439-89-6
Iron in solids samples by ICPMS
0.25
15000
J2
mg/kg
ESTAFFORD
7439-92-1
Lead in solids samples by ICPMS
0.20
93
J2
mg/kg
ESTAFFORD
7439-95-4
Mg in solid samples by ICP
10
8000
J2
mg/Kg
ESTAFFORD
7439-96-5
Mn solid samples by ICPMS
0.20
130
J2
mg/kg
ESTAFFORD
7440-02-0
Nickel in solids samples by ICPMS
0.20
64
mg/kg
ESTAFFORD
Peer Review % DrySolids
ES
%
ESTAFFORD
Percent Dry Solids
44.4
%
ESTAFFORD
7440-09-7
Potasium in solid samples by ICP
10
1200
J2
mg/Kg
ESTAFFORD
7782-49-2
Selenium in solids samples by ICPMS
0.20
0.66
mg/kg
ESTAFFORD
7440-09-7
Sodium in solid samples by ICP
10
750
J2
mg/Kg
ESTAFFORD
7440-66-6
Zinc in solids samples by ICPMS
0.20
400
J2
mg/kg
ESTAFFORD
VOL
75-78-1 Dichlorodifluoromethane 178 I Not detected ug/Kg RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 4

Lnc. Descr.:
OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
SOIL/SEDIMENT
Loc. Type:
SOIL/SEDIMENT
Sample Depth
3
Sample Comment
\N ATERQG
� r
J
Q � Y
Sample ID:
AB14383
PO Number #
7W1760
VisitiD
Collect Date:
03/09/2007
Collect Time::
12:05
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
YES
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result Qualifier
Units
Approved By
74-87-3
Chloromethane
39
Not detected
ug/Kg
RKELLING
75-01-4
Vinyl Chloride
139
39
Not detected
ug/Kg
RKELLING
74-83-9
Bromomethane
39
Not detected
ug/Kg
RKELLING
75-00-3
Chloroethane
Not detected
ug/Kg
RKELLING
75-69-4
Trichlorofluoromethane
39
Not detected
ug/Kg
RKELLING
75-35-4
1,1-Dichloroethene
19
Not detected
ug/Kg
RKELLING
75-09-2
Methylene Chloride
780
Not detected
ug/Kg
RKELLING
156-60-5
trans-1,2-Dichloroethene
19
Not detected
ug/Kg
RKELLING
1634-04-4
Methyl Tert-Butyl Ether
19
Not detected
ug/Kg
RKELLING
75-34-3
1,1-Dichloroethane
19
Not detected
ug/Kg
RKELLING
156-59-4
cis-1,2-Dichloroethene
19
Not detected
ug/Kg
RKELLING
74-97-5
Bromochloromethane
19
Not detected
ug/Kg
RKELLING
67-66-3
Chloroform
19
Not detected
ug/Kg
RKELLING
590-20-7
2,2-Dichloropropane
39
Not detected
ug/Kg
RKELLING
107-06-2
1,2-Dichloroethane
19
Not detected
ug/Kg
RKELLING
71-55-6
1,1,1-Trichloroethane
19
Not detected
ug/Kg
RKELLING
. 563-58-6
1,1-Dichloropropene
19
Not detected
ug/Kg
RKELLING
56-23-5
Carbon Tetrachloride
19
Not detected
ug/Kg
RKELLING
71-43-2
Benzene
19
Not detected
ug/Kg
RKELLING
74-95-3
Dibromomethane
78
Not detected
ug/Kg
RKELLING
78-87-5
1,2-Dichloropropane
19
Not detected
ug/Kg
RKELLING
79-01-6
Trichloroethene
19
Not detected
ug/Kg
RKELLING
75-27-4
Bromodichloromethane
19
Not detected
ug/Kg
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 4

Loc. Descr.:
OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
SOIL/SEDIMENT
Loc. Type:
SOIL/SEDIMENT
Sample Depth
3
Sample Comment
'Q Laboratory Section W esurts
Sample ID:
AB14383
PO Number #
7W1760
VisitlD
Collect Date:
03/09/2007
Collect Time::
12:05
r
j
Date Received:
03/13/2007
a -r
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
YES
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result
Qualifier
Units
Approved By
10061-01-5
cis- 1,3-Dichloropropene
19
Not detected
ug/Kg
RKELLING
10061-02-6
trans-1,3-Dichloroprope ne
19
Not detected
ug/Kg
RKELLING
79-00-5
1,1,2-Trichloroethane
19
Not detected
ug/Kg
RKELLING
108-88-3
Toluene
19
10
N3,P
ug/Kg
RKELLING
142-28-9
1,3-Dichloropropane
19
Not detected
ug/Kg
RKELLING
124-48-1
Dibromochloromethane
19
Not detected
ug/Kg
RKELLING
106-93-4
(EDB)1,2-Dibromoethane
19
Not detected
ug/Kg
RKELLING
127-18-4
Tetrachloroethene
19
Not detected
ug/Kg
RKELLING
108-90-7
Chlorobenzer)e
19
68
P
ug/Kg
RKELLING
100-41-4
Ethylbenzene
19
12
N3,P
ug/Kg
RKELLING
75-25-2
Bromoform
78
Not detected
ug/Kg
RKELLING
108-38-3
m,p-Xylene
39
20
N3,P
ug/Kg
RKELLING
100-42-5
Styrene
19
Not detected
ug/Kg
RKELLING
79-34-5
1,1,2,2-Tetrachloroethane
19
Not detected
ug/Kg
RKELLING
630-20-6
1,1,1,2-Tetrachloroethane
19
Not detected
ug/Kg
RKELLING
95-47-6
o-Xylene
19
16
N3,P
ug/Kg
RKELLING
96-18-4
1,2,3-Trichloropropane
19
Not detected
ug/Kg
RKELLING
98-82-8
Isopropylbenzene
19
Not detected
ug/Kg
RKELLING
108-86-1
Bromobenzene
19
Not detected
ug/Kg
RKELLING
103-65-1
n-Propylbenzene
19
Not detected
ug/Kg
RKELLING
95-49-8
2-Chlorotoluene
19
Not detected
ug/Kg
RKELLING
106-43-4
4-Chlorotoluene
19
Not detected
ug/Kg
RKELLING
108-67-8
1,3,5-Trimethylbenzene
19
Not detected
ug/Kg
RKELLING
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 3 of 4

ection
Lc,p. Pescr.:
OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
SOIL/SEDIMENT
Loc. Type:
SOIL/SEDIMENT
Sample Depth
3
Sample Comment
4 `C
Sample ID:
AB14383
PO Number#
7W1760
VisitlD
Collect Date:
03/09/2007
Collect Time::
12:05
Date Received:
03/1312007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
YES
COG Yes/No
YES
CAS #
Analyte Name
PQL
Result
Qualifier
Units
Approved By
98-06-6
tert-Butylbenzene
19
Not detected
ug/Kg
RKELLING
95-63-6
1,2,4-Trimethylbenzene
19
120
P
ug/Kg
RKELLING
135-98-8
sec-Butylbenzene
19
Not detected
ug/Kg
RKELLING
543-73-1
m-Dichlorobenzene (1,3)
19
Not detected
ug/Kg
RKELLING
106-46-7
p-Dichlorobenzene (1,4)
19
Not detected
ug/Kg
RKELLING
95-50-1
o-Dichlorobenzene (1,2)
19
Not detected
ug/Kg
RKELLING
99-87-6
p-Isopropyltoluene
19
Not detected
ug/Kg
RKELLING
104-51-8
n-Butylbenzene
19
Not detected
ug/Kg
RKELLING
96-12-8
1,2-Dibromo-3-Chloropropane
160
Not detected
ug/Kg
RKELLING
120-82-1
1,2,4-Trichlorobenzene
39
40
P
ug/Kg
. RKELLING
91-20-3
Naphthalene
39
110
P
ug/Kg
RKELLING
87-68-3
Hexachlorobutadiene
39
Not detected
ug/Kg
RKELLING
87-61-6
1,2,3-Trichlorobenzene
78
Not detected
ug/Kg
RKELLING
2-Chloroethyl vinyl ether
-
X
ug/Kg
RKELLING
ALKANES
4600
N1,P
ug/Kg
RKELLING
ALKENES
4100
N1,P
ug/Kg
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 4 of 4 ,

Report to: _MRO
NC DENR/DWQ Laboratory
Sample Anomaly Report (SAR)
Lab Number: AB14383
Station Location: NC0005487
County: Rowan
Sample ID:
Region: MRO
Sample Type: Sludge Priority: emergency Collector:
')ate collected: 03/09/07 Date received: 03/13/07 Date anal,
effected Parameter(s): Metals quality control sample j p— (�1 . P�
Analytical Area (check one):
❑ W CH ®METALS
❑NUT ❑MICRO
The following anomalies occurred (check all that apply):
®Samples
❑Improper container used
❑VOA vials with headspace
❑Sulfide samples with headspace
❑Samples not received, but listed on fieldsheet
❑Samples received, but not listed on fieldsheet
❑Mislabeled as to tests, preservatives, etc.
❑Holding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
❑Sample exhibits gross non -homogeneity
❑Sample not chemically preserved properly
❑pH out of range (record pH):
❑Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑Heavy emulsion formed during. extraction
❑Sample bottle broken in lab - no reportable results
❑Other (specify):
Comments: Q t f r-wk e
Corrective Action: W 1, 4
W Bell .
03/21/07
❑VOA ❑SVOA
❑PEST
Quality Control
❑Instrument failure — no reportable results
❑Analyst error — no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
®Spike recovery
❑None added
®Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑Internal standards
❑Blank contamination
❑QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
approval
❑Invalid instrument calibration
❑Elevated detection limits due to:
❑Insufficient sample volume
Qb r' - 20 S� Sa" PCB e e kr l�
Pit
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used:J2
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date:
Form completed by: . Jurgevic Date: 3/26/2007
Lead Chemist Review (initial):
❑BIOCHEM
®METALS
❑PEST
❑VOA
Branch Head Review (initial): 3 -2.7'.2,0®7
QA/QC Review (initi
❑SVGA
Logged into database by (initial):
QA\Forms\Laboratory\SAR 10/23/01 dbs

DIVISION OF Fro
TER QUALITY
COUNTY: LUc1 )I
WATER Z!Sy00S1i6PM&6F0e
RIVER BASIN: - — E' e
REPORT TO: ARO FR MRO RRO WaRO WiRO WSRO TS 4, y e . ��)
AT BM Seditnei* QSOII QTISSue
Other
SHIPPED BY: Bus, Courier St a Other
For Lab Use ONLY
Lab Number -
Date Received:0 ime:d
Rec'd by: From:; Bus- urger and
DATA ENTRY BY:. K:
DATE REPORTED:
COLLECTOR(S): 1( .%e/� �j /- % /,J� / J J
LOCATION CODE: Ac- _ 6 STATION LOCATION: / IC Do�1�' )AI/ q /( — �O(C►' r6 & — tl T` , b� /�Li C�/�
LATITUDE: LONGITUDE: REMARKS: t I%t
Station #
Date Begin (yy/mm/dd)
Time Begin
Date End (yy/mm/dd)
Time End
Depth DM DB DBM
Value Type
Composite
Sample pe
G 9
?j
NO y1
r/
A H L
T S B
C I G GNXX
Tissue•
Units
Sediment/Soil•
Units
Tissue'
Units
Sediment/Soil•
Units
Tissue`
Units
Sediment/Soil•
Units
1
As —Arsenic
mg/k
A — Silver
mg/k
Chlorinated Pest
Oil and Grease
2
Al - Aluminum
mg/kg
Al - Aluminum
mg/kgmg/kg
PCBs
TOC
3
Cd—Cadmium
mg/kg
As —Arsenic
mg/kg
PBBs
4
Cr—Chromium
mg/kg
Cd—Cadmium
mg/kg
5
Cu— Copper
mg/kg
Cr=Chromium
mg/kg
6
Fe — Iron
mg/kg
Cu— Copper
mg/kg
7
Hg — Mercury
mg/kg
V
Fe — Iron
mg/kg
8
Mn — Manganese
mg/kg
Hg — Mercury
mg/k
9
Ni — Nickel
mg/kg
Mn — Manganese
m /k
10
Pb - Lead
mg/kg
Ni— Nickel
mg/kg
11
Se —Selenium
mg/kg
Pb - Lead
mg/kg
12
Zn —Zinc
mg/kg
Se — Selenium
mg/kg
13
Zn—Zinc
mg/k
14
Ca -Calcium
m /kg
15
- Potassium
mg/kg
16
M — Magnesium
m /k
17
Na—Sodium
mg/kg
Fish species (p84 5)
Fish species— Nu do 4990)
18
19
Temperature on ayFival , -
20
w
Sample Wt. (g)
Length (cm) Sample Wt. (g)
Length (cm) Sample Wt. (g)
Length (cm) O
WHOLE FISH
1
5
9
O
FILLET
2
6
10
112
Q
VISCERA
3
7
11
O
SHELLFISH
4
$
0
OTHER

ENR/DWQ LABORATORY
LAB NO. AB14383
VOLATILE ANALYTICAL REPORT
REPORTED BY
A,'T^
SUPERVISOR
CHECKED BY
VA
DATE
REVIEWED BYft
ENTERED BY
SAMPLE TYPE:
SOIL
ANALYTICAL RESULTS
DATE
:�::::::::::::::::Volfitlle:Osgahtc.......�........�.......
P;f£JL....:R�SULT .:.......:.....::::;;;:;:::::Uolatil'e.Q.9ahlc;����.......:.......:�:�.•:�.�.�:�:�:�:•:•:�:�.
crnP�4nd :::::::::::::
`E`C.S# :Tao
::ug/K :•:•:•: :.•::: ug44 :::::::::... A ......... rseiCom ..und .:.•...•...•.•.•.•.•.•.........
:: :7 : '' ' 1fE '
I g ':::::`: q .
75-71-8
Dichlorodifluoromethane
78
U
630-20-6
1,1,1,2-Tetrachloroethane
19
U
74-87-3
Chloromethane
39
U
75-25-2
Bromoform
78
U
75-01-4
Vinyl Chloride
39
U
79-34-5
1,1,2,2-Tetrachloroethane
19
U
74-83-9
Bromomethane
39
U
96-18-4
1,2,3-Tdchloropropane
19
U
75-00-3
Chloroethane
39
U
108-86-1
Bromobenzene
19
U
75-69-4
Trichlorofluoromethane
39
U
95-49-8
2-Chlorotoluene
19
U
75-35-4
1,1-Dichloroethene
19
U
106-434
4-Chlorotoluene
19
U
75-09-2
Methylene Chloride
780
U
541-73-1
1,3-Dichlorobenzene
19
U
156-60-5
trans-1,2-Dichloroethene
19
U
106-46-7
1,4-Dichlorobenzene
19
U
75-34-3
1,1-Dichloroethane
19
U
95-50-1
1,2-Dichlorobenzene
19
U
594-20-7
2,2-Dichloropropane
39
U
96-12-8
1,2-Dibromo-3-Chloropropane
160
U
156-59A
cis-1,2-Dichloroethene
19
U
120-82-1
1,2,4-Trichlorobenzene
39
40 P
67-66-3
Chloroform
19
U
87-68-3
Hexachlorobutadiene
39
U
74-97-5
Bromochloromethane
19
U
87-61-6
1,2,3-Trichlorobenzene
78
U
71-55-6
1,1,1-Trichloroethane
19
U
1634-04A
Methyl-tert-butyl ether
19
U
563-58-6
1,1-Dichloropropene
19
U
71-43-2
Benzene
19
U
56-23-5
Carbon Tetrachloride
19
U
108-88-3
Toluene
19
10 N3, P
107-06-2
1,2-Dichloroethane
19
U
10OA14
Ethyl benzene
19
12 N3, P
79-01-6
Trichloroethene
19
U
108-38-3
m,p-Xylenes
39
20 N3, P
78-87-5
1,2-Dichloropropane
19
U
9547-6
o-Xylene
19
16 N3, P
75-27-4
Bromodichloromethane
19
U
100-42-5
Styrene
19
U
74-95-3
Dibromomethane
78
U
98-82-8
Isopropylbenzene
19
U
10061-01-5
cis-1,3-Dichloropropene
19
U
103-65-1
n-Propylbenzene
19
U
10061-02-6
trans-1,3-Dichloropropene
19
U
108-67-8
1,3,5-Trimethylbenzene
19
U
79-00-5
1,1,2-Trichloroethane
19
U
98-06-6
tert-Butylbenzene
19
U
127-18A
Tetrachloroethene
19
U
95-63-6
1,2,4-Trimethylbenzene
19
120 P
142-28-9
1,3-Dichloropropane
19
U
135-98-8
sec-Butylbenzene
19
U
124A8-1
Dibromochloromethane
19
U
99-87-6
p-isopropyltoluene
19
U
106-93A
1,2-Dibromoethane
19
U
104-51-8
n-Butylbenzene
19
U
108-90-7
Chlorobenzene
19 68 P
91-20-3
Naphthalene
39
110 P
mg/Kg
mg/Kg
PQL
PracticalQuantitationLimit- Subject to
Gasdline:Range:Estimated:TbtaFFelfolerirh:Hydrocarbbh::::::
0.20
X
change due to instrument sensitivity
.........................................
..
N-
Tentatively Identified, not confirmed
Other Volatile Organics Detected
Result
J-
Estimated Value
(up to 10 highest peaks)
ug/Kg
U-
Samples analyzed for this compound but not detected
X-
Sample not analyzed for this compound
ALKANES
4600 N1, P
N3-
Estimated concentration is <PQL and >MDL
ALKENES
4100 N1, P
P
Elevated PQL due to matrix interference and/or sample dilution
COMMENTS: NOT ANALYZED FOR 2-CHLOROETHYL VINYL ETHER

ffC DM Laboratory Section Wesults
Sample ID: AB14386
Loc. Descr.: OLD COLOR - TEX WWTP LAGOON;
PO Number # 7W1763
Location ID: NC0005487 ~ �'' "°� `�'� VisitlD
County: ROWAN wArFR
River Basin (*} Collect Date: 03/09/2007
Report To MROSP Collect Time:: 11:45
r
Region: MRO �d®7 � Date Received: 03/13/2007
Collector: 1Na&EIIII a \ Time Received: 08:00
Sample Matrix: WASTEWATER \
Labworks LoginlD MMA
Loc. Type: EFFLUENT
Sample Depth 1 Date Reported: 04/11/2007
�11
a � Emergency Yes/No YES
Sample Comment i4 s'
mate. COC Yes/No YES
VMIt
A
Analyte Name
PQL
Result Qualifier
Units
Analyst
Approved By
LAB
Sample temperature at receipt by lab
1.9
°C
MMATHIS
MMATHIS
Method Reference
Analysis Date
3/13/07
WET
Chemical Oxygen Demand in liquid
20
48
mg/L
JSTALEY
MOVERMAN
Method Reference Hach 8000
Analysis Date
3/16/07
NUT
NH3 as N in liquid
0.02
3.0
mg/L as N
MAJAYI
CGREEN
Method Reference LaclO-107-06-1-J
Analysis Date
3/16/07
Total Kjeldahl N as N in liquid
0.2
5.1
mg/L as N
MOVERMAN
CGREEN
Method Reference Lachat107-06-2-H
Analysis Date
3/15/07
NO2+NO3 as N in liquid
0.02
0.51
mg/L as N
MAJAYI
CGREEN
Method Reference Lac10-107-04-1-c
Analysis Date
3/16/07
Phosphorus total as P in liquid
0.02.
0.14
mg/L as P
GBELK
CGREEN
Method Reference Lac10-115-01-lEF
Analysis Date
3/14/07
MET
4r
7440-22-4
Ag by ICPMS
5.0
5.0 U
ug/L
PGAUTHIER
ESTAFFORD
Method Reference EPA 200.8
Analysis Date
3/29/07
7429-90-5
Al by ICP
50
900 /
ug/L
JJURGEVICH
ESTAFFORD
Method Reference EPA 200.7
Analysis Date
3/27/07
7440-38-2
As by ICPMS
5.0
5.2 `
ug/L
DSTANLEY1
ESTAFFORD
Method Reference EPA 200.8
!ir
Analysis Date
3/30/07
7440-38-3
Ba by ICP
10
46
ug/L
JJURGEVICH
ESTAFFORD
Method Reference EPA 200.7
Analysis Date
3/27/07
7440-43-9
Cd by ICPMS
1.0
1.0 U
ug/L
PGAUTHIER
ESTAFFORD
Method Reference EPA 200.8
Analysis Date
3/29/07
Laboratory.Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone]
Pagel of 6

NC (DWQQ Laboratory Section Results Sample D AB14386
Location ID: NC0005487 Collect Date: 03/09/2007
Lod. Descr.: bLD COLOR - TEX WTP LAGOON Collect Time:: 11:45
W
7440-47-3
Cr by ICPMS
10
10
U
ug/L
PGAUTHIER
ESTAFFORD
Method Reference EPA 200.8
Analysis Date
3/29/07
7440-50-8
Cu by ICPMS
2.0
6.6
ug/L
DSTANLEY1
ESTAFFORD
Method Reference EPA 200.8
Analysis Date
4/2/07
7440-48-4
Fe by ICP
50
1200
ug/L
JJURGEVICH
ESTAFFORD
Method Reference EPA 200.7
Analysis Date
3/27/07
7439-97-6
Hg 245.1
0.2
0.20
U
ug/L
DSTANLEYI
ESTAFFORD
Method Reference EPA 245.1
Analysis Date
3/16/07
7439-95-4
Mg by ICP
0.10
7.5
mg/L
JJURGEVICH
ESTAFFORD
Method Reference EPA 200.7
Analysis Date
3/27/07
7439-96-5
Mn by ICPMS
10
200
ug/L
JJURGEVICH
ESTAFFORD
Method Reference EPA 200.8
Analysis Date
3/27/07
7440-23-4
Na by ICP
0.10
38
mg/L
JJURGEVICH
ESTAFFORD
Method Reference EPA 200.7
Analysis Date
3/27/07
7440-02-0
Ni by ICPMS
10
10
U
ug/L
PGAUTHIER
ESTAFFORD
Method Reference EPA 200.8
Analysis Date
3/29/07
- 7439-92-1
Pb by ICPMS
10
10
U
ug/L
PGAUTHIER
ESTAFFORD
Method Reference EPA 200.8
Analysis Date
3/29/07
7782-49-2
Se by ICPMS
5.0
5.0
U
ug/L
PGAUTHIER
ESTAFFORD
Method Reference EPA 200.8
Analysis Date
3/29/07
7440-66-6
Zn by ICP
10
86
ug/L
JJURGEVICH
ESTAFFORD
Method Reference EPA 200.7
Analysis Date
3/27/07
VOL
75-78-1
Dichlorodifluoromethane
1.0
Not detected
ug/L
VANDREWS
WELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
74-87-3
Chloromethane
0.50
Not detected
ug/L
VANDREWS
WELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
75-01-4
Vinyl Chloride
0.50
Not detected
ug/L
VANDREWS
WELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
74-83-9
Bromomethane
0.50
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA50301624/8260
Analysis Date
3/14/07
_75-00-3
Chloroethane
0.50
Not detected
ug/L
VANDREWS
WELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone] Page 2 of 6

NC DWQ .Laboratory Section Results Sample ID AB14386
l ocation ID: . NC0005487 Collect Date: 03/09/2007
Collect Time:: 11:45
Loc. Descr.: OLD COLOR - TEX WWTP LAGOON
75-69-4 Trichlorofluoromethane 0.50 Not detected
ug/L
VANDREWS RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14107
75-35-4 1,1-Dichloroethene 0.25 Not detected
ug/L
VANDREWS RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
75-09-2 Methylene Chloride 10 Not detected
ug/L
VANDREWS RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
156-60-5
trans-1,2-Dichloroethene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
1634-04-4
Methyl Tert-Butyl Ether
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
75-34-3
1,1-Dichloroethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
156-59-4
cis-1,2-Dichloroethene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA50301624/8260
Analysis Date
3/14/07
74-97-5
Bromochloromethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
67-66-3
Chloroform
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
590-20-7
2,2-Dichloropropane
5.0
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/62418260
Analysis Date
3/14/07
107-06-2
1,2-Dichloroethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
71-55-6
1,1,1-Trichloroethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
563-58-6
1,1-Dichloropropene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
56-23-5
Carbon Tetrachloride
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
71-43-2
Benzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3114/07
74-95-3
Dibromomethane
1.0
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
78-87-5
1,2-Dichloropropane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/62418260
Analysis Date
3/14/07
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 3 of 6

XC DWQ Laboratory Section q(esufts ample ID AB14386
Location lb:� NC0005487 Collect Date: 03/09/2007
Collect Time:: 11:45
Loc. Descr.: OLD COLOR - TEX WWTP LAGOON
79-01-6
Trichloroethene
0.25
Not detected
ug/L
VANDKLWS
KKLLLINU
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
75-27-4
Bromodichloromethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
10061-01-5
CIS-1,3-Dichloropropene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14107
10061-02-6
trans-1,3-Dichloropropene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
79-00-5
1,1,2-Trichloroethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
108-88-3
Toluene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/62418260
Analysis Date
3114/07
142-28-9
1,3-Dichloropropane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
124-48-1
Dibromochloromethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
106-93-4
(EDB)1,2-Dibromoethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
127-18-4
Tetrachloroethene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
108-90-7
Chlorobenzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
100-41-4
Ethylbenzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
75-25-2
Bromoform
1.0
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
108-38-3
map-Xylene
0.50
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA50301624/8260
Analysis Date
3/14/07
100-42-5
Styrene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
79-34-5
1,1,2,2-Tetrachloroethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
630-20-6
1,1,1,2-Tetrachloroethane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 4 of 6

NC (DWQQ Laboratory Section Results Sample ID AB14386
Location'ID: . NC0005487 Collect Date: 03/09/2007
Collect Time:: 11:45
Loc. Descr.: OLD COLOR - TEX WWTP LAGOON
95-47-6
o-Xylene
0.25
Not detected
ug/L
VANDREWS
KKtLUNIi
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
96-18-4
1,2,3-Trichloropropane
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
98-82-8
Isopropyl benzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
108-86-1
Bromobenzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
103-65-1
n-Propylbenzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
95-49-8
2-Chlorotoluene
0.25
0.18 N3
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3114/07
106-43-4
4-Chlorotoluene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
108-67-8
1,3,5-Trimethyl benzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/62418260 -
Analysis Date
3/14/07
98-06-6
tert-Butyl benzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
95-63-6
1,2,4-Tri methyl benzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
135-98-8
sec -Butyl benzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
543-73-1
m-Dichlorobenzene (1,3)
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
106-46-7
p-Dichlorobenzene (1,4)
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
95-50-1
o-Dichlorobenzene (1,2)
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
99-87-6
p-isopropyltoluene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
104-51-8
n-Butylbenzene
0.25
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/62418260
Analysis Date
3/14/07
96-12-8
1,2-Dibromo-3-Chloropropane
2.0
Not detected
ug/L
VANDREWS
RKELLING
Method Reference EPA5030/624/8260
Analysis Date
3/14/07
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 5 of 6

XC )WQ Laboratory Section results Sample ID AB14386
Lbcation ID: . NC0005487 Collect Date: 03/09/2007
Loc. Descr.: OLD COLOR - TEX WWTp LAGOON Collect Time:: 11:45
120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected
Method Reference EPA5030/624/8260
ug/L VANDR
Analysis Date 3/14/07
91-20-3 Naphthalene 0.50 Not detected ug/L VANDREWS WELLING
Method Reference EPA5030/624/8260 Analysis Date 3/14/07
87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L VANDREWS WELLING
Method Reference EPA5030/624/8260 Analysis Date 3/14/07
87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L VANDREWS WELLING
Method Reference EPA5030/624/8260 Analysis Date 3/14/07
2-Chloroethyl vinyl ether - X ug/L VANDREWS WELLING
Method Reference EPA5030/624/8260 Analysis Date 3/14/07
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 6 of 6

C000aw C) C=000*
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Water Quality
❑ SAMPLE TYPE
Lab Numbej/_
Date Receieed,40'2��© 313
COUNTY (A}
PRIORTI Y
"
Time Received': � '
RIVER BASIN : 1 — DYE �
�, AMBIENT
� QA
� STREAM
EFFLUENT
Received By
('`('
REPORT TO {C 11 f 10 (� Regional Office
COMPLIANCE CHAIN OF CUSTODY
El LAKE ❑ INFLUENT
Other
EMERGENCY
VISITS)
ESTUARY
Data Released
COLLECTOR(S) : (, ,/� ��_ � �
�
❑
Date Reported
Estimated BOD Range: 41A
Station Location:
Seed: Chlorinated:
/��/
Remarks: /�'t{S,-I
AI LZ
Station H/Location Code
Date Begin (yy/mm/dd)
Date End (yy/mm/dd) �/�
Time Begin
Time End
Depth - DM, DB, DBM
Value Type- A, H, L
Composite-T, S, B
Sam tLle Type
A/c0o0 5
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L
Coliform: MF Fecal 31616 /100ml
Coliform: MF Total 31504 /100m1
Coliform: tube Fecal 31615 /100MI
Coliform: Fecal Strep 31673 /100ml
Residue: Total 500 mg/L
Volatile 505 mg/L
Fixed 510 mg/L
Residue: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 mg/L
pH 403 units
Acidity to pH 4.5 436 mg/L
Acidity to pH 8.3 435 mg/L
Alkalinity to pH 8.3 415 mg/L
Alkalinity to pH 4.5 410 mg/L
TOC 680 _91L
Turbidity 76 NTU
Coliform Total Tube / l00 ml
COMMENTS:
Chloride 940 mg/L
Chlorophyll a EPA 445.0 modified option ug/L
Color: True 80 c.u.
Color: (pH) 83 pH- C.U.
Color: pH 7.6 82 C.U.
Cyanide 720 mg/L
Fluoride 951 mg(L
Formaldehyde 71880 mg1L
Grease and Oils 556 mg/L
Hardness Total900 mg/L
Specific Cond. 95 umhos/cm
MBAS 38260 mg(L
Phenols32730 ug/L
Sulfate 945 mg(L
Sulfide 745 mg(L
Boron
Tannin & Lignin ug/L
Hexavalent Chromium ugIL
Bicarbonate mg/L
Carbonate mg(L
Total Dissolved Solids mg/L,
as N 610 mg/L
T an N 625 mg/L
N 2 plus NO3 asN 630 mg/L
P: Total as P 665 mg(L
PO4 as P 70507 mg/L
P: Dissolved as P 666 mg/L
K-Potassium mg/L
d- Cadmium 1027 ug/L
2r-ChromiumTotal1034 ug/L
- Copper 1042 ug(L
Ni-Nickel 1067 ug/L
Pb- Lead 1051 ug/L
Zn- Zinc 1092 ug/L
-Vanadium ug/L
Ag- Silver 1071 ug/L
Al -Aluminum "05 ug(L
Be- Beryllium 1012 ug/L
Ca- Calcium 916 mg/L
o- Cobalt 1037 ug/L
Fe -Iron 1045 ug/L
Mo-Molybdenum ug/L
Sb-Antimony ug/L
Sn-Tin ug/L
TI-Thallium ug/L
Ti-Titanium ug/L
111g.1631 ng/L
Li -Lithium 1132 ug/L
Mg- Magnesium 927 mg/L
Mn-Manganese 1055 ug/L
✓
Na- Sodium 929 mg/L
Arsenic:Total1002 ug/L
Se- Selenium 1147 ug/L
Hg. Mercury 71900 ug/L
Ba-Barium ug/L
Organochlorine Pesticides
Organophosphorus Pesticides
Orgartonitrogen Pesticides
Acid Herbicides
BasetNeutral&Acid Extractable Organics
TPH Diesel Range
Purgeable Organics (VOA bottle req'd)
TPH Gasoline Range
TPHBTEX Gasoline Range
Phytoplankton
Temperature on arrival (aC):

LAB No. AB14386
REPORTED BY VA•A
CHECKED BY
REVIEWED BY ��(G
SAMPLE TYPE: WATER
ENRIDWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYTICAL RESULTS
SUPERVISOR
DATE % D
ENTERED BY
DATE
�
T .. Ud, aql�,(?rg8nic.......................................... �(iL........- RE....1�-.-.-.-.-. •... •................. •.,.. �....-. �.-. �$.-..-... _.,.:.,.;..-. �.. �. �.-.-.-.-.-.-.-.-.-.-: q..-:-...-.-.-.-..-. �.. •. �. �. •. •. •.
T. ei .::;�u�::�::���=��������'•�
75-71-8
Dichlorodifluaromethane
1.0
U
630-20-6
1,1,1,2-Tetrachloroethane
0.25
74-87-3
Chloromethane
0.50
U
75-25-2
Bromoform
1.0
75-01-4
Vinyl Chloride
0.50
U
79-34-5
1,1,2,2-Tetrachloroethane
0.25
74-83-9
Bromomethane
0.50
U
96-18-4
1,2,3-Trichloropropane
0.25
75-00-3
Chloroethane
0.50
U
108-86-1
Bromobenzene
0.25
75-69-4
Trichlorofluoromethane
0.50
U
95-49-8
2-Chlorotoluene
0.25
75-35-4
1,1-Dichloroethene
0.25.
U
106-434
4-Chlorotoluene
0.25
75-09-2
Methylene Chloride
10
U
541-73-1
1,3-Dichlorobenzene
0.25
156-60-5
trans-1,2-Dichloroethene
0.25
U
10646-7
1,4-Dichlorobenzene
0.25
75-34-3
1,1-Dichloroethane
0.25
U
95-50-1
1,2-Dichlorobenzene
0.25
594-20-7
2,2-Dichloropropane
5.0
U
96-12-8
1,2-Dibromo-3-Chloropropane
2.0
156-594
cis-1,2-Dichloroethene
0.25
U
120-82-1
1,2,4-Trichlorobenzene
0.50
67-66-3
Chloroform
0.25
U
87-68-3
Hexachlorobutadiene
0.50
74-97-5
Bromochloromethane
0.25
U
87-61-6
1,2,3-Trichlorobenzene
1.0
71-55-6
1,1,1-Trichloroethane
0.25
U
1634-044
Methyl-tert-butyl ether
0.25
563-58-6
1,1-Dichloropropene
0.25
U
7143-2
Benzene
0.25
56-23-5
Carbon Tetrachloride
0.25
U
108-88-3
Toluene
0.25
107-06-2
1,2-Dichloroethane
0.25
U
100-414
Ethyl benzene
0.25
79-01-6
Trichloroethene
0.25
U
108-38-3
m,p-Xylenes
0.50
78-87-5
1,2-Dichloropropane
0.25
U
95-47-6
o-Xylene
0.25
75-274
Bromodichloromethane
0.25
U
10042-5
Styrene
0.25
74-95-3
Dibromomethane
1.0
U
98-82-8
Isopropylbenzene
0.25
10061-01-5
cis-1,3-Dichloropropene
0.25
U
103-65-1
n-Propylbenzene
0.25
10061-02-6
trans-1,3-Dichloropropene
0.25
U
108-67-8
1,3,5-Trimethylbenzene
0.25
79-00-5
1,1,2-Trichloroethane
0.25
U
98-06-6
tert-Butylbenzene
0.25
127-184
Tetrachloroethene
0.25
U
95-63-6
1,2,4-Trimethylbenzene
0.25
142-28-9
1,3-Dichloropropane
0.25
U
135-98-8
sec-Butylbenzene
0.25
124-48-1
Dibromochloromethane
0.25
U
99-87-6
p-isopropyltoluene
0.25
106-934
1,2-Dibromoethane
0.25
U
104-51-8
n-Butylbenzene
0.25
108-90-7
Chlorobenzene
0.25
U
91-20-3
Naphthalene
0.50
PQL Practical Quantitation Limit- Subject to
change due to instrument sensitivity
N- Tentatively Identified, not confirmed
J- Estimated Value
U- Samples analyzed for this compound but not detected
X- Sample not analyzed for this compound
N3- Estimated concentration is <PQL and >MDL
P Elevated PQL due to matrix interference and/or sample dilution
COMMENTS: NOT ANALYZED FOR 2-CHLOROETHYL VINYL
U
U
U
U
U
0.18 N3
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
mg/L mg/L
GasolineRarige E§timafeil:Tdtal Petro[euiri:F{ydiocaitinri_:::: 0.20 X
..............................................
Other Volatile Organics Detected Result
(up to 10 highest peaks) ug/L

L8c;0escr.: OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
-Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
SOIL/SEDIMENT
Loc. Type:
SOIL/SEDIMENT
Sample Depth
3
Sample Comment
XC DWO Laboratory Section Results
i".. r Sample ID: AB14384
PO Number # 7W1761
OFFICE VisitlD
WA7FRQ Collect Date: 03/09/2007
�fl Collect Time:: 12:15
r l
APR 0 2 200- d Date Received: 03/13/2007
4e�' -< 0 —0 . Time Received: 08:00
TLabworks LoginlD MMA
Date Reported: 03/28/2007
WATE LITY SOT I �'j Emergency Yes/No YES
COG Yes/No YES
CAS # Analyte Name PQL Result Qualifier Units Approved By
LAB
Sample temperature at receipt by lab I I 2.6 °C MMATHIS
MFT
7440-22-4
Ag in solid samples by ICPMS
0.20
0.82
mg/Kg
ESTAFFORD
7429-90-5
AI in solid samples by ICP
5.0
9200
mg/Kg
ESTAFFORD
7440-38-2
Arsenic solid samples by ICPMS
0.20
5.1
mg/Kg
ESTAFFORD
7440-43-9
Cadmium in solids samples by ICPMS
0.20
2.1
mg/kg
ESTAFFORD
7440-70-2
Calcium in solid samples by ICP
10
5600
mg/Kg
ESTAFFORD
7440-47-3
Cr in solids samples by ICPMS
0.20
220
mg/kg
ESTAFFORD
7440-50-8
Cu solid samples by ICPMS
0.20
530
mg/kg
ESTAFFORD
7439-97-6
Hg 245.5 solid
0.02
1.0 J2
° mg/Kg
ESTAFFORD
7439-89-6
Iron in solids samples by ICPMS
0.25
1100
mg/kg
ESTAFFORD
7439-92-1
Lead in solids samples by ICPMS
0.20
60
mg/kg
ESTAFFORD
7439-95-4
Mg in solid samples by ICP
10
4900
mg/Kg
ESTAFFORD
7439-96-5
Mn solid samples by ICPMS.
0.20
150
mg/kg
ESTAFFORD
7440-02-0
Nickel in solids samples by ICPMS
0.20
37
mg/kg
ESTAFFORD
Peer Review % Dry Solids
ES
%
ESTAFFORD
Percent Dry Solids
25.4
%
ESTAFFORD
7440-09-7
Potasium in solid samples by ICP
10
710
mg/Kg
ESTAFFORD
7782-49-2
Selenium in solids samples by ICPMS
0.20
0.79
mg/kg
ESTAFFORD
7440-09-7
Sodium in solid samples by ICP
10
430
mg/Kg
ESTAFFORD
7440-66-6
Zinc in solids samples by ICPMS
0.20
580
mg/kg
ESTAFFORD
VOL
75-78-1 Dichlorodifluoromethane 139 Not detected ug/Kg RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone] Page 1 of 4

'ection
Loc. Descr.: OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
SOIL/SEDIMENT
Loc. Type:
SOIL/SEDIMENT
Sample Depth
3
Sample Comment
Sample ID:
AB14384
PO Number#
7W1761
VisitlD
Collect Date:
03/09/2007
Collect Time::
12:15
Date Received:
03/1312007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
YES
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result Qualifier
Units
Approved By
74-87-3
Chloromethane
20
Not detected
ug/Kg
RKELLING
75-01-4
Vinyl Chloride
20
Not detected
ug/Kg
RKELLING
74-83-9
Bromomethane
20
Not detected
ug/Kg
RKELLING
75-00-3
Chloroethane
20
Not detected
ug/Kg
RKELLING
75-69-4
Trichlorofluoromethane
20
Not detected
ug/Kg
RKELLING
75-35-4
1,1-Dichloroethene
9.8
Not detected
ug/Kg
RKELLING
75-09-2
Methylene Chloride
390
Not detected
ug/Kg
RKELLING
156-60-5
trans-1,2-Dichloroethene
9.8
Not detected
ug/Kg
RKELLING
1634-04-4
Methyl Tert-Butyl Ether
9.8
Not detected
ug/Kg
RKELLING
75-34-3
1,1-Dichloroethane
9.8
Not detected
ug/Kg
RKELLING
156-59-4
cis-1,2-Dichloroethene
9.8
Not detected
ug/Kg
RKELLING
74-97-5
Bromochloromethane
9.8
Not detected
ug/Kg
RKELLING
67-66-3
Chloroform
9.8
Not detected
ug/Kg
RKELLING
590-20-7
2,2-Dichloropropane
20
Not detected
ug/Kg
RKELLING
107-06-2
1,2-Dichloroethane
9.8
Not detected
ug/Kg
RKELLING
71-55-6
1, 1,1 -Trichloroethane
9.8
Not detected
ug/Kg
RKELLING
563-58-6
1,1-Dichloropropene
9.8
Not detected
ug/Kg
RKELLING
56-23-5
Carbon Tetrachloride
9.8
Not detected
ug/Kg
RKELLING
71-43-2
Benzene
9.8
Not detected
ug/Kg
RKELLING
74-95-3
Dibromomethane
39
Not detected
ug/Kg
RKELLING
78-87-5
1,2-Dichloropropane
9.8
Not detected
ug/Kg
RKELLING
79-01-6
Trchloroethene
9.8
Not detected
ug/Kg
RKELLING
75-27-4
Bromodichioromethane
9.8
Not detected
ug/Kg
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 4

ection
Loc. Vescc: OLD COLOR - TEX WWTP LAGOON
Location ID: NC0005487
County: ROWAN
River Basin
Report To MROSP
Region: MRO
Collector: W BELL
Sample Matrix: SOIL/SEDIMENT
Loc. Type: SOIL/SEDIMENT
Sample Depth 3
Sample Comment
Sample ID:
AB14384
PO Number#
7W1761
VisitlD
Collect Date:
03/09/2007
Collect Time::
12:15
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
YES
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result Qualifier
Units
Approved By
10061-01-5
cis- 1,3-Dichloropropene
9.8
Not detected
ug/Kg
RKELLING
10061-02-6
trans-1,3-Dichloropropene
9.8
Not detected
ug/Kg
RKELLING
79-00-5
1,1,2-Trichloroethane
9.8
Not detected
ug/Kg
RKELLING
108-88-3
Toluene
9.8
6.8 N3
ug/Kg
RKELLING
142-28-9
1,3-Dichloropropane
9.8
Not detected
ug/Kg
RKELLING
124-48-1
Dibromochloromethane
9.8
Not detected
ug/Kg
RKELLING
106-93-4
(EDB)1,2-Dibromoethane
9.8
Not detected
ug/Kg
RKELLING
127-18-4
Tetrachloroethene
9.8
Not detected
ug/Kg
RKELLING
108-90-7
Chlorobenzene
9.8
Not detected
ug/Kg
RKELLING
100-41-4
Ethylbenzene
9.8
Not detected
ug/Kg
RKELLING
75-25-2
Bromoform
39
Not detected
ug/Kg
RKELLING
108-38-3
m,p-Xylene
20
10 N3
ug/Kg
RKELLING
100-42-5
Styrene
9.8
Not detected
ug/Kg
RKELLING
79-34-5
1,1,2,2-Tetrachloroethane
9.8
Not detected
ug/Kg
RKELLING
630-20-6
1,1,1,2-Tetrachloroethane
9.8
Not detected
ug/Kg
RKELLING
95-47-6
o-Xylene
9.8
Not detected
ug/Kg
RKELLING
96-18-4
1,2,3-Tiichooropropane
9.8
Not detected
ug/Kg
RKELLING
98-82-8
Isopropylbenzene
9.8
Not detected
ug/Kg
RKELLING
108-86-1
Bromobenzene
9.8
Not detected
ug/Kg
RKELLING
103-65-1
n-Propylbenzene
9.8
Not detected
ug/Kg
RKELLING
95-49-8
2-Chlorotoluene
9.8
Not detected
ug/Kg
RKELLING
106-43-4
4-Chlorotoluene
9.8
Not detected
ug/Kg
RKELLING
108-67-8
1,35-Trimethylbenzene
9.8
22
ug/Kg
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone] Page 3 of 4

Lab
'ection
I,'oc, Descr.: OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
SOIL/SEDIMENT
Loc. Type:
SOIL/SEDIMENT
Sample Depth
3
Sample Comment
`o�pF W ArERQG
=� r
y
a ,c
Sample ID:
AB14384
PO Number #
7W1761
VisitlD
Collect Date:
03/09/2007
Collect Time::
12:15
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
YES
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result Qualifier
Units
Approved By
98-06-6
tert-Butylbenzene
9.8
Not detected
ug/Kg
RKELLING
95-63-6
1,2,4-Trimethylbenzene
9.8
34
ug/Kg
RKELLING
135-98-8
sec-Butylbenzene
9.8
Not detected '
ug/Kg
RKELLING
543-73-1
m-Dichlorobenzene(1,3)
9.8
Not detected
ug/Kg
RKELLING
106-46-7
p-Dichlorobenzene (1,4)
9.8
Not detected
ug/Kg
RKELLING
95-50-1
o-Dichlorobenzene (1,2)
9.8
Not detected
ug/Kg
RKELLING
99-87-6
p-Isopropyltoluene
9.8
Not detected
ug/Kg
RKELLING
104-51-8
n-Butylbenzene
9.8
Not detected
ug/Kg
RKELLING
96-12-8
1,2-Dibromo-3-Chloropropane
78
Not detected
ug/Kg
RKELLING
120-82-1
1,2,4-Trichlorobenzene
20
Not detected
ug/Kg
RKELLING
91-20-3
Naphthalene
20
Not detected
ug/Kg
RKELLING
87-68-3
Hexachlorobutadiene
20
Not detected
ug/Kg
RKELLING
87-61-6
1,2,3-Trchlorobenzene
39
Not detected .
ug/Kg
RKELLING
2-Chloroethyl vinyl ether
- X
ug/Kg
RKELLING
ALKENES
1800 N1
ug/Kg
RKELLING
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone] Page 4 of 4

Report to: _MRO
NC DENR/DWQ Laboratory
Sample Anomaly Report (SAR)
Lab Number:
Station Location:
AB14384 Sample ID
NC0005487
Sample Type: SEDIMENT
')ate collected: 3/9/07
effected Parameter(s):
County: ROWAN
Priority: ER
Date received: 3/13/07
Analytical Area (check one):
❑ WCH ®METALS
❑NUT ❑MICRO
The following anomalies occurred (check all that apply):
❑Samples
❑Improper container used
❑VOA vials with headspace
❑Sulfide samples with headspace
❑Samples not received, but listed on fieldsheet
❑Samples received, but not listed on fieldsheet
❑Mislabeled as to tests, preservatives, etc.
❑Holding time expired
❑Prior to receipt in lab
❑After receipt in lab
❑Insufficient quantity for analysis
❑Sample exhibits gross non -homogeneity
❑Sample not chemically preserved properly
❑pH out of range (record pH):
❑Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑Heavy emulsion formed during extraction
❑Sample bottle broken in lab - no reportable results
❑Other (specify):
Comments: Possible matrix interference
Corrective Action:Report with J2 qualifer
4
Region: MRO
Collector: W. BELL
Date analyzed: 3/20/07
❑VOA ❑SVOA
❑PEST
®Quality Control
❑Instrument failure — no reportable results
[]Analyst error — no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
®Spike recovery
❑None added
®Recovery outside acceptance limits
❑Failed to meet criteria for precision
❑Internal standards
❑Blank contamination
❑QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
approval
❑Invalid instrument calibration
❑Elevated detection limits due to:
❑Insufficient sample volume
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until:
®Sample reported with qualification. Data qualification code used J2
❑Other (explain):
Notification Required? ❑ Yes ❑ No
Person Contacted: Date:
Form completed by: Oebra Stanle Date: 3/20/07
Lead Chemist Review (initial):
❑BIOCHEM ❑PEST ❑SVOA
[METALS ❑VOA
Branch Head Review (initial):
QA/QC Review (initial): Logged into database by (initial): fk7_—�
QA\Forms\Laboratory\SAR 10/23/Oldbs

DIVISION OF WATER QUALITY WATER ALITY SED T/ S FORM
COUNTY: Q© CO
RIVER BASIN: e -e vee
REPORT TO: ARO FRO RO RO WaRO WiRO WSRO TS �Sleeftnitnt
5l tt,1V e
AT BM 0Soil QTissue
SHIPPED BY: Bus Courier Staff, Other
COLLECTOR(S): (il hP_ 11
LOCATION CODE: /VL ono J 1)
LATITUDE: LONGITUDE:
Fnr I ah 11.P nhli V A 1 6_)
Lab Number:
Date Recei ed:D irrl 60
Rec'd by: .. From: Bus urier- and
DATA ENTRY BY: K:
DATE REPORTED:. \�
STATION LOCATION: jj 0[(;( �(��/ ��x � (/yt�%
REMARKS: L- CI G 6 1� 1 •F��i 1,11�l -l�"
Station #
Date Begin (yy/mm/dd)
Time Begin
Date End (yy/mm/dd)
Time End
Depth DM DB DBM
Value Type
Composite
Sample Type
COD C 1-
L7
I �� 1
f 1
A H L
I T S B
IS G GNXX
Tissue
Units
Sedlment/Soil'
Units
Tissue
Units
Sediment/Soit*
Units
Tissue•
Units
SedimentlSoil'
Units
1
As — Arsenic
mg/kg
A --Silver
m /k
Chlorinated Pest
Oil and Grease
2
AI - Aluminum
mg/kg
AI -Aluminum
m /k
PCBs
TOC
3
Cd—Cadmium
mg/kg
V
As — Arsenic
mg/kg
PBBs
4
Cr—Chromium
m /k
Cd—Cadmium
mg/kg
5
Cu—Copper
mg/kg
L.,
16r — Chromium
mg/kg
6
Fe — Iran
mg/kg
Cu — Copper
m /k
7
Hg — Mercury
mg/kg
Fe — Iron
mg/kg
S
Mn — Manganese
m /k
Hg — Mercury
m /k
9
Ni — Nickel
m /k
Mn — Manganese
mg/kg
10
Pb - Lead
mg/kg
Ni —Nickel
mg/kg
11
Se — Selenium
mg/kg
Pb -Lead
mg/kg
12
Zn—Zinc
mg/kg
Se — Selenium
mg/kg
13
Zn — Zinc
mg/kg
14
Ca - Calcium
mg/kg
15
K-Potassium
mg/kg
16
M —Magnesium
mg/kg
17
Na— Sodium
mg/kg
Fish species ( 005)
16
Fish species — meri p74990)
19
Temperature or9,arriva
20
('9 J , . ,.
�,
Sample Wt. g)
Length (cm) Sample Wt. (g)
Length (cm) Sample Wt. g)
Length (cm)
O
WHOLE FISH
1
5
9
O
FILLET
2
6
10
O
VISCERA
3
7
11
O
SHELLFISH
4
$
12
O
OTHER

LAB No. AB14384
REPORTED BY AT A i
CHECKED BY
REVIEWED BY
SAMPLE TYPE: SOIL
ENR/DWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYTICAL RESULTS
SUPERVISOR
DATE
ENTERED BY
DATE
::: VO at le Or '0iii'': :: :::i :::::::: ...:::::: :.....::.:::::::.: :::::::::::
..9..5......•...................•.................Pql..:.......RESULT.....•.•.;...,._..._.,.,.,.,.•.•...,.•.;.,...:.•.11�3ah10.Q.s3..lc,.,.,.,.;.•.•.:.....•.•......._...,.,.•.•.•FQL::::::::RESUI
'''
.
A ..... Tar9eko[ispirund.. u' IK . ::...... ti9l►c9...........:..............cAs#...,.,:TargetCcm .ound.. ::::::::::...ri /14 ......::. ng/keg:
75-71-8
Dichlorodifluoromethane
39
U
630-20-6
1,1,1,2-Tetrachloroethane
9.8
74-87-3
Chloromethane
20
U
75-25-2
Bromoform
39
75-014
Vinyl Chloride
20
U
79-34-5
1,1,2,2-Tetrachloroethane
9.8
74-83-9
Bromomethane
20
U
96-18-4
1,2,3-Trichloropropane
9.8
75-00-3
Chloroethane
20
U
108-86-1
Bromobenzene
9.8
75-69-4
Trichlorofluoromethane
20
U
95-49-8
2-Chlorotoluene
9.8
75-35-4
1,1-Dichloroethene
9.8
U
106-434
4-Chlorotoluene
9.8
75-09-2
Methylene Chloride
390
U
541-73-1
1,3-Dichlorobenzene
9.8
156-60-5
trans-1,2-Dichloroethene
9.8
U
106-46-7
1,4-Dichlorobenzene
9.8
75-34-3
1,1-Dichloroethane
9.8
U
95-50-1
1,2-Dichlorobenzene
9.8
594-20-7
2,2-Dichloropropane
20
U
96-12-8
1,2-Dibromo-3-Chloropropane
78
156-594
cis-1,2-Dichloroethene
9.8
U
120-82-1
1,2,4-Trichlorobenzene
20
67-66-3
Chloroform
9.8
U
87-68-3
Hexachlorobutadiene
20
74-97-5
Bromochloromethane
9.8
U
87-61-6
1,2,3-Trichlorobenzene
39
71-55-6
1,1,1-Trichloroethane
9.8
U
1634-044
Methyl-tert-butyl ether
9.8
563-58-6
1,1-Dichloropropene
9.8
U
7143-2
Benzene
9.8
56-23-5
Carbon Tetrachloride
9.8
U
108-88-3
Toluene
9.8
107-06-2
1,2-Dichloroethane
9.8
U
100A14
Ethyl benzene
9.8
79-01-6
Trichloroethene
9.8
U
108-38-3
m,p-Xylenes
20
78-87-5
1,2-Dichloropropane
9.8
U
95-47-6
o-Xylene
9.8
75-27-4
Bromodichloromethane
9.8
U
100-42-5
Styrene
9.8
74-95-3
Dibromomethane
39
U
98-82-8
Isopropylbenzene
9.8
10061-01-5
cis-1,3-Dichloropropene
9.8
U
103-65-1
n-Propylbenzene
9.8
10061-02-6
trans-1,3-Dichloropropene
9.8
U
108-67-8
1,3,5-Trimethylbenzene
9.8
79-00-5
1,1,2-Trichloroethane
9.8
U
98-06-6
tert-Butylbenzene
9.8
127-18-4
Tetrachloroethene
9.8
U
95-63-6
1,2,4-Trimethylbenzene
9.8
142-28-9
1,3-Dichloropropane
9.8
U
135-98-8
sec-Butylbenzene
9.8
124A8-1
Dibromochloromethane
9.8
U
99-87-6
p-isopropyltoluene
9.8
106-93-4
1,2-Dibromoethane
9.8
U
104-51-8
n-Butylbenzene
9.8
108-90-7
Chlorobenzene
9.8
U
91-20-3
Naphthalene
20
PQL Practical Quantitation Limit- Subject to
change due to instrument sensitivity
N- Tentatively Identified, not confirmed
J- Estimated Value
U- Samples analyzed for this compound but not detected
X- Sample not analyzed for this compound
N3- Estimated concentration is <PQL and >MDL
P Elevated PQL due to matrix interference and/or sample dilution
COMMENTS: NOT ANALYZED FOR 2-CHLOROETHYL VINYL ETHER
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
6.8 N3
U
10 N3
U
U
U
U
22
U
34
U
U
U
U
mg/Kg mg/Kg
Gasdline:Range:E'stirimated Total F�2raleum:Hydrbcarbbh:::::: 0.20 X
.......................... ..
Other Volatile Organics Detected Result
(up to 10 highest peaks) ug/Kg
ALKENES 1800 N1

X (D Laboratory Section We
hoc. Descr.: OLD COLOR - TEX WWTP LAGOON
location ID: NC0005487
County: ROWAN pT a� zn �¢ V`1+47ER
River Basin Q
Report To MROSP vJ r
Region: MRO
Collector: W BELL APR 0 r 2IN7 a -
Sample Matrix: SOIL/SEDIMENT
Loc. Type: SOIL/SEDIMENT
Sample Depth 1 r `�
Sample Comment TV
Sample ID:
AB14385
PO Number #
7W1762
VisitlD
Collect Date:
03/09/2007
Collect Time::
12:30
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
COC Yes/No
YES
LAB
Sample temperature at receipt by lab ' I 2.6 °C MMATHIS
MET
7440-22-4
Ag in solid samples by ICPMS
0.20
0.38
mg/Kg
ESTAFFORD
7429-90-5
AI in solid samples by ICP
5.0
23000
mg/Kg
ESTAFFORD
7440-38-2
Arsenic solid samples by ICPMS
0.20
1.3
mg/Kg
ESTAFFORD
7440-43-9
Cadmium in solids samples by ICPMS
0.20
0.60
mg/kg
ESTAFFORD
7440-70-2
Calcium in solid samples by ICP
10
5800
mg/Kg
ESTAFFORD
7440-47-3
Cr in solids samples by ICPMS
0.20
100
mg/kg
ESTAFFORD
7440-50-8
Cu solid samples by ICPMS
0.20
870
mg/kg
ESTAFFORD
7439-97-6
Hg 245.5 solid
0.02
0.70
mg/Kg
ESTAFFORD
7439-89-6
Iron in solids samples by ICPMS
0.25
16000
mg/kg
ESTAFFORD
7439-92-1
Lead in solids samples by ICPMS
0.20
27
mg/kg
ESTAFFORD
7439-95-4
Mg in solid samples by ICP
10
5400
mg/Kg
ESTAFFORD
7439-96-5
Mn solid samples by ICPMS
0.20
330
mg/kg
ESTAFFORD
7440-02-0
Nickel in solids samples by ICPMS
0.20
47
mg/kg
ESTAFFORD
Peer Review % Dry Solids
ES
%
ESTAFFORD
Percent Dry Solids
13.3
%
ESTAFFORD
7440-09-7
Potasium in solid samples by ICP
10
1300
mg/Kg
ESTAFFORD
7782-49-2
Selenium in solids samples by ICPMS
0.20
0.84
mg/kg
ESTAFFORD
7440-09-7
Sodium in solid samples by ICP
10
860
mg/Kg
ESTAFFORD
- 7440-66-6
Zinc in solids samples by ICPMS
0.20
220
mg/kg
ESTAFFORD
VOL
75-78-1 Dichlorodifluoromethane 100 I Not detected ug/Kg RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 4

,
J
JLZt. Descr.: OLD COLOR - TEX WWTP LAGOON
Location ID: NC0005487
County: ROWAN
River Basin
Report To MROSP
Region: MRO
Collector: W BELL
Sample Matrix: SOIL/SEDIMENT
Loc. Type: SOIL/SEDIMENT
Sample Depth 1
Sample Comment
Sample ID:
AB14385
PO Number #
7W1762
VisitlD
Collect Date:
03/09/2007
Collect Time::
12:30
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result Qualifier
Units
Approved By
74-87-3
Chloromethane
50
Not detected
ug/Kg
RKELLING
75-01-4
Vinyl Chloride
50
Not detected
ug/Kg
RKELLING
74-83-9
Bromomethane
50
Not detected
ug/Kg
RKELLING
75-00-3
Chloroethane
50
Not detected
ug/Kg
RKELLING
75-69-4
Trichlorofluoromethane
50
Not detected
ug/Kg
RKELLING
75-35-4
1,1-Dichloroethene
25
Not detected
ug/Kg
RKELLING
75-09-2
Methylene Chloride
1000
Not detected
ug/Kg
RKELLING
156-60-5
trans-1,2-Dichloroethene
25
Not detected
ug/Kg
RKELLING
1634-04-4
Methyl Tert-Butyl Ether
25
Not detected
ug/Kg
RKELLING
75-34-3
1,1-Dichloroethane
25
Not detected
ug/Kg
RKELLING
156-59-4
cis-1,2-Dichloroethene
25
Not detected
ug/Kg
RKELLING
74-97-5
Bromochloromethane
25
Not detected
ug/Kg
RKELLING
67-66-3
Chloroform
25
Not detected
ug/Kg
RKELLING
590-20-7
2,2-Dichloropropane
50
Not detected
ug/Kg
RKELLING
107-06-2
1,2-Dichloroethane
25
Not detected
ug/Kg
RKELLING
71-55-6
1,1,1-Trichloroethane
25
Not detected
ug/Kg
RKELLING
563-58-6
1,1-Dichloropropene
25
Not detected
ug/Kg
RKELLING
56-23-5
Carbon Tetrachloride
25
Not detected
ug/Kg
RKELLING
71-43-2
Benzene
25
Not detected
ug/Kg
RKELLING
74-95-3
Dibromomethane
100
Not detected
ug/Kg
RKELLING
78-87-5
1,2-Dichloropropane
25
Not detected
ug/Kg
RKELLING
79-01-6
Tiichooroethene
25
Not detected
ug/Kg
RKELLING
75-27-4
Bromodichloromethane
25
Not detected
ug/Kg
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 2 of 4

JLDop Descr.:
OLD COLOR - TEX WWTP LAGOON
Location ID:
NC0005487
County:
ROWAN
River Basin
Report To
MROSP
Region:
MRO
Collector:
W BELL
Sample Matrix:
SOIL/SEDIMENT
Loc. Type:
SOIL/SEDIMENT
Sample Depth
1
Sample Comment
Sample ID:
AB14385
PO Number#
7W1762
VIsitI D
Collect Date:
03/09/2007
Collect Time::
12:30
Date Received:
03/13/2007
Time Received:
08:00
Labworks LoginlD
MMA
Date Reported:
03/28/2007
Emergency Yes/No
COC Yes/No
YES
CAS
Analyte Name
PQL
Result Qualifier
Units
Approved By
10061-01-5
cis-1,3-Dichloropropene
25
Not detected
ug/Kg
RKELLING
10061-02-6
trans-1,3-Dichloroprope ne
25
Not detected
ug/Kg
RKELLING
79-00-5
1,1,2-Trichloroethane
25
Not detected
ug/Kg
RKELLING
108-88-3
Toluene
25
12 N3
ug/Kg
RKELLING
142-28-9
1,3-Dichloropropane
25
Not detected
ug/Kg
RKELLING
124-48-1
Dibromochloromethane
25
Not detected
ug/Kg
RKELLING
106-93-4
(EDB)1,2-Dibromoethane
25
Not detected
ug/Kg
RKELLING
127-18-4
Tetrachloroethene
25
Not detected
ug/Kg
RKELLING
108-90-7
Chlorobenzene
25
Not detected
ug/Kg
RKELLING
100-41-4
Ethylbenzene
25
Not detected
ug/Kg
RKELLING
75-25-2
Bromoform
100
Not detected
ug/Kg
RKELLING
108-38-3
m,p-Xylene
50
Not detected
ug/Kg
RKELLING
100-42-5
Styrene
25
Not detected
ug/Kg
RKELLING
79-34-5
1,1,2,2-Tetrachloroethane
25
Not detected
ug/Kg
RKELLING
630-20-6
1, 1, 1,2-Tetrachloroethane
25
Not detected
ug/Kg
RKELLING
95-47-6
o-Xylene
25
Not detected
ug/Kg
RKELLING
96-18-4
1,2,3-Tdchloropropane
25
Not detected
ug/Kg
RKELLING
98-82-8
Isopropylbenzene
25
Not detected
ug/Kg
RKELLING
108-86-1
Bromobenzene
25
Not detected
ug/Kg
RKELLING
103-65-1
n-Propylbenzene
25
Not detected
ug/Kg
RKELLING
95-49-8
2-Chlorotoluene
25
300
ug/Kg
RKELLING
106-43-4
4-Chlorotoluene
25
Not detected
ug/Kg
RKELLING
108-67-8
1,3,5-Trimethylbenzene
25
35
ug/Kg
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 3 of 4

9V-C OM Laboratory Section Wesults
11oz. Descr.:
OLD COLOR - TEX WWTP LAGOON
Sample ID:
AB14385
PO Number #
7W1762
Location ID:
NC0005487
VisitlD
County:
ROWAN
OF \NA
River Basin
P
Collect Date:
03/09/2007
Report To
MROSP
�a G
� �
Collect Time::
12:30
Region:
MRO
0 Y
Date Received:
03/13/2007
Collector:
W BELL
Time Received:
08:00
Sample Matrix:
SOIL/SEDIMENT
Loc. Type:
SOIL/SEDIMENT
Labworks LoginlD
MMA
Sample Depth
1
Date Reported:
03/28/2007
Sample Comment
Emergency Yes/No
COC Yes/No
YES
CAS #
Analyte Name
PQL
Result
Qualifier
Units
Approved By
98-06-6
tert-Butylbenzene
25
Not detected
ug/Kg
RKELLING
95-63-6
1,2,4-Trimethylbenzene
25
53
ug/Kg
RKELLING
135-98-8
sec-Butylbenzene
25
Not detected
ug/Kg
RKELLING
543-73-1
m-Dichlorobenzene (1,3)
25
Not detected
ug/Kg
RKELLING
106-46-7
p-Dichlorobenzene (1,4)
25
Not detected
ug/Kg
RKELLING
95-50-1
o-Dichlorobenzene(1,2)'
25
Not detected
ug/Kg
RKELLING
99-87-6
p-Isopropyltoluene
25
Not detected
ug/Kg
RKELLING
104-51-8
n-Butylbenzene
25
Not detected
ug/Kg
RKELLING
96-12-8
1,2-Dibromo-3-Chloropropane
200
Not detected
ug/Kg
RKELLING
120-82-1
1,2,4-Trichlorobenzene
50
Not detected
ug/Kg
RKELLING
91-20-3
Naphthalene '
50
Not detected
ug/Kg
RKELLING
87-68-3
Hexachlorobutadiene
50
Not detected
ug/Kg
RKELLING
87-61-6
1,2,3-Trichlorobenzene
100
Not detected
ug/Kg
RKELLING
2-Chloroethyl vinyl ether
-
X
ug/Kg
RKELLING
ALKANES
860
N1
ug/Kg
RKELLING
ALKENES
940
N1
ug/Kg
RKELLING
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 4 of 4

f '. ISION OF WATER QUALITY WAT QUALITY DME T SSUE ORM For Lab Use ONLY
COUNTY: U U"u I' I Lab Number
-71
RIVER BASIN: T Date Recei ed / ime
REPORT TO: ARO FR MRO)RRO WaRO WiRO WSRO TS i /U(�p, C Rec'd by: - -H=221 From: Bus- rle Hand
AT BM - SEf�1 7ltrtettt Soil QTissue DATA -ENTRY BY: K:
DATE REPORTED:,.,
Other
SHIPPED BY: Bus CourierlStaff, Ot er
COLLECTOR(S): r�I, {
LOCATION CODE:
LATITUDE: LONGITUDE
Station #
Date Be/gin (yy/mm/dd)
Time Begin
Date End (yy/mm/dd)
Time End
Depth DM DB DBM
Value Type
Composite
Sample T pe
%�?o i •� �l i7 /
DY7! ' , 7 lr�
I� �� . 1►J
j ��
A H L
T S B
C G GNXX
Tissue*
Units
Sediment/Soil*
Units
Tissue
Units
SedimentlSoil*
Units
Tissue*
Units
SedimenUSoil*
Units
1
As —Arsenic
mg/kg
A — Silver
m /k
Chlorinated Pest
Oil and Grease
2
AI -Aluminum
mg/kg
AI -Aluminum
mg/k
PCBs
TOC
3
Cd—Cadmium
mg/kg
As —Arsenic
mg/kg
PBBs
4
Cr—Chromium
m /k
Cd—Cadmium
mg/kg
5
Cu—Copper
mg/kg
Cr—Chromium
mg/kg
6
Fe — Iron
m /k9
Cu — Copper
m /kg
7
Hg — Mercury
mg/kg
F e — Iron
mg/kg
8
Mn — Manganese
mg/kg
g — Mercury
mg/k
9
Ni — Nickel
m /k
Mn — Manganese
m /k
101
Pb - Lead
mg/kg
Ljf4i
— Nickel
mg/kg
11
Se — Selenium
m /k
Pb- Lead
m /k
12
Zn — Zinc
mg/kg
Se — Selenium
mg/kg
13
Zn — Zinc
m /k
14
Ca - Calcium
m /k
15
K-Potassium
mg/kg
16
x,
Mg — Magnesium
mg/k
17
Na — Sodium
mg/kg
Fish speci (p840
18
Fish speci — N ehc (p74990)
19
Temperatu on arri
20
`l
Sample Wt. (g)
Length (cm) Sample Wt. (g)
Length (cm) Sample Wt. (g)
Length (cm)
0
WHOLE FISH
1
5
9
O
FILLET
2
6
10
112
0
VISCERA
3
7
11
0
SHELLFISH
4
$
O
OTHER

LAB No. AB14385
REPORTED BY AAT
CHECKED BY
REVIEWED BY
SAMPLE TYPE: SOIL
ENR/DWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYTICAL RESULTS
SUPERVISOR -Ner %[G
r
DATE a4PPRGkTs8
ENTERED BY
DATE
75-71-8
Dichlorodifluoromethane
100
U
630-20-6
1,1,1,2-Tetrachloroethane
25
74-87-3
Chloromethane
50
U
75-25-2
Bromoform
100
75-01-4
Vinyl Chloride
50
U
79-34-5
1,1,2,2-Tetrachloroethane
25
74-83-9
Bromomethane
50
U
96-18-4
1,2,3-Tdchloropropane
25
75-00-3
Chloroethane
50
U
108-86-1
Bromobenzene
25
75-69-4
Trichlorofluoromethane
50
U
95-49-8
2-Chlorotoluene
25
75-354
1,1-Dichloroethene
25
U
106-43-4
4-Chlorotoluene
25
75-09-2
Methylene Chloride
1000
U
541-73-1
1,3-Dichlorobenzene
25
156-60-5
trans-1,2-Dichloroethene
25
U
106-46-7
1,4-Dichlorobenzene
25
75-34-3
1,1-Dichloroethane
25
U
95-50-1
1,2-Dichlorobenzene
25
594-20-7
2,2-Dichloropropane
50
U
96-12-8
1,2-Dibromo-3-Chloropropane
200
156-594
cis-1,2-Dichloroethene
25
U
120-82-1
1,2,4-Trichlorobenzene
50
67-66-3
Chloroform
25
U
87-68-3
Hexachlorobutadiene
50
74-97-5
Bromochloromethane
25
U
87-61-6
1,2,3-Trichlorobenzene
100
71-55-6
1,1,1-Trichloroethane
25
U
1634-04-4 _
Methyl-tert-butyl ether
25
563-58-6
1,1-Dichloropropene
25
U
7143-2
Benzene
25
56-23-5
Carbon Tetrachloride
25
U
108-88-3
Toluene
25
107-06-2
1,2-Dichloroethane
25
U
100-41-4
Ethyl benzene
25
79-01-6
Trchloroethene
25
U
108-38-3
m,p-Xylenes
50
78-87-5
1,2-Dichloropropane
25
U
95-47-6
o-Xylene
25
75-274
Bromodichloromethane
25
U
10042-5
Styrene
25
74-95-3
Dibromomethane
100
U
98-82-8
Isopropylbenzene
25
10061-01-5
cis-1,3-Dichloropropene
25
U
103-65-1
n-Propylbenzene
25
10061-02-6
trans-1,3-Dichloropropene
25
U
108-67-8
1,3,5-Trimethylbenzene
25
79-00-5
1,1,2-Trichloroethane
25
U
98-06-6
tert-Butylbenzene
25
127-18-4
Tetrachloroethene
25
U
95-63-6
1,2,4-Trimethylbenzene
25
142-28-9
1,3-Dichloropropane
25
U
135-98-8
sec-Butylbenzene
25
124-48-1
Dibromochloromethane
25
U
99-87-6
p-isopropyltoluene
25
106-93-4
1,2-Dibromoethane
25
U
104-51-8
n-Butyibenzene
25
108-90-7
Chlorobenzene
25
U
91-20-3
Naphthalene
50
PQL Practical Quantitation Limit- Subject to
change due to instrument sensitivity
N- Tentatively Identified, not confirmed
J- Estimated Value
U- Samples analyzed for this compound but not detected
X- Sample not analyzed for this compound
N3- Estimated concentration is <PQL and >MDL
P Elevated PQL due to matrix interference and/or sample dilution
COMMENTS: NOT ANALYZED FOR 2-CHLOROETHYL VINYL ETHER
300
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
12 N3
U
U
U
U
U
U
35
U
53
U
U
U
U
..............................................
mg/Kg mg/Kg
asolineRariggEstimafedTotal•Petroteaiti:Hydiocarbbri:::: 0.20 X
.................................... ... ...
Other Volatile Organics Detected Result
(up to 10 highest peaks) sE4gl'.
ALKANES 860 N1
ALKENES 940 N1

Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Kerr T. Stevens, Director
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
. r
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RF50URCES
6/19/2000
JAMES W. OGLE
COLOR-TEX FINISHING CORP.
P.O. BOX 45
SPENCER NC 28159
SUBJECT: NOTICE OF VIOLATION AND REVOCATION FOR NON PAYMENT
PERMIT NUMBER NC0005487
COLOR-TEX FINISHING CORP. —
ROWAN COUNTY
Dear Permittee:
Payment of the required annual administering and compliance monitoring fee of $2865.00 for this year has not
been received for the subject permit. This fee is required by Title 15 North Carolina Administrative Code 2H.0105, under
the authority of North Carolina General Statutes 143-215.3(a)(1), (ia) and (1b). Because this fee was not fully paid within
30 days after being billed, this letter initiates action to revoke the subject permit, pursuant to 15 ncac 2H.0105(b) (2) (k)
(4), and G.S. 143-215.1 (b) (3).
Effective 60 days from receipt of this notice, subject permit is hereby revoked unless the required Annual
Administering and Compliance Monitoring Fee is received within that time. Discharges without a permit are subject to the
enforcement authority of the Division of Water Quality. Your payment should be sent to:
N.C. Department of Environment and Natural Resources
Division of Water Quality
Budget Office
1617 Mail Service Center
Raleigh, NC 27699-1617
If you are dissatisfied with this decision, you have the right to request an administrative hearing within Thirty (30)
days following recipt of this notice, identifying the specific issues to be contended. This request must be in the form of a
written petition conforming to Chapter 150E of the North Carolina General Statutes, and filed with the Office of Administrative
Hearings, Post Office Drawer 27447, Raleigh, North Carolina, 27611-7447. Unless such request for hearing is made or
payments received, revocation shall be final and binding. If you have any questions, please contact:
Mr. Rex Gleason, Mooresville Water Quality Regional Supervisor, [phone].
Sincerely,
Kerr T. Stevens
cc: Supevisor, Water Quality Permits and Engineering Unit
Mooresville Regional Office
County Health Department
P.O. Box 29535,: Raleigh, North Garolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled / 10% post -consumer paper

[Fwd: Requests]
Subject: [Fwd: Requests]
Date: Fri, 26 Jan 2001 11:56:46 -0500
From: Rex Gleason <[e-mail]>
Organization: NC DENR - Mooresville Regional Office
To: [e-mail]
John,
Please handle Tony's request. Also answer his question re. ORC for Star
Enterprises.
Thanks,
Rex
Rex Gleason - [e-mail]
%TITLE%
North Carolina Dept. of Environment & Natural Resources
Div. of Water Quality
919 N. Main St.
Mooresville, NC 28115
Ph: [phone] Fax: [phone]
Subject: Requests
Date: Fri, 26 Jan 2001 10:53:20 -0500
From: Tony Arnold <[e-mail]>
Organization: N.C. Dept. of Environment and Natural Resources
To: Rex Gleason <[e-mail]>
Good Morning Rex,
A couple of items have come along and I was wondering if you could
provide me with some information.
First, I have sent two letters to ColorTex - NC Finishing (NC0005487)
to get an updated ORC Designation form for our records (the ORC has
resigned) both times the letter were returned with "wrong address".
Could you let whoever has this facility in your office fax or send them
a blank ORC designation form and have the facility return it to us. I
have attached the new designation form.
Second, Star Enterprises (NC0022187) has lost their ORC (they were
classificated years ago as a class 1 biological system). After
reviewing the permit I found that the system is a oil/water separator.
Oil/water separators will fall within the new physical/chemical
certification program once it is in place. I hate to make this facility
get a certified grade one biological'operator and turn around in 6
months and require a P/C operator when they are reclassified. Just
wanted to know if you have a problem with this, if there had been past
problems at the facility, and your thoughts on this matter.
Thanks for the help. Tony A
p.s. I will miss Don, he has been very helpful to me, I believe you
will be pleased with your selection.. TA
1 of2 1/26/2001 12:15 PM

NC Finishing-LColor Tex, WWTP Sampling
9/7/05 -.1koni-the :bank using asampling, cup
LL. I -Large Lagoon influent side
U2 - Large Lagoon effluent side
CTI - Clarifier 91
CTI - darifiler #2
9/l/3'05 - sampling from a boat usingatel 2 feet from surface
a sludge judge, approxI.In y
and offthe bottorn for sludge layer.
CTI - Clarifier ftl Top Layer.
CBI - Clarifier #'I Bottom- Layer(sludge)
CT2 -, Clarifier w2 Top.: Layer
CB2 - Clarifier 42 Bottom Layer (sludge,)
UMT -Large: Lagoon atinidp in n 0 tofifluentsid6-top layer
LIMB -Large Lagoon at rnidpoint of � fluent side,- bottom layer (slud 16)
in
BWS - Midpoint. of Large Lagoon Raffle Wall - Smooth sludge :layer
BWC - Midpoint of Large, Lagoon Baffle Wall - Ch
unky sludge layer
WW - Wet Well, Vault and Building composite
Clarifiers were 12.fect deep -with between. I fbot acid :2.5- feet, ofslud e on bottom.
Large Lagoon was 1.1 feet' deep in the midpointlof tile influent side. Cron.
foot to 10.5 feet Sludge ranged froI
near the wall, Sludge ranged from a smooth consistency I to a.
chunky consistency similar to peanut butter.. Color was black.
No samples were taken from the effluent side.
I a
Sludge,inthe Wet Well, Vault Punip Building f! -oni.210 feet.
To estimate tbe, amount. of sludge it will be necessary to use a-slud'gojud e-at various
g,
intervals onboth sides of the lagoon. Time did not permit this on 9/1310
Paramders thait Will be tested initially areas follows:
Total Solids
Total, Vo latile, Solids
Metals
Mercury
Ole'-flical Oxygen demand
Cyanide
PheapIs
Chloride
Sulfate.

Metals
0 r- (A i�k c
lAnalyst: UVVLA—' I I r-F-15
1-- -3. 1
Date an4l`zed
q-15
R"?, --
q-.,)
^%
-ky
--I - k;t-
it-
Metal
'Conc. Units
Zn
mg/L
Cu
mg/L
Pb
mg/L
mg/L
Ag
021L
Cd
mg/L
'cr
fri /L
As
mg/L
Se
m - g/L
3b
mg/L
15ftf
Curve
05-3.00
.005-.025
.005-.050
.005-.050
.001-.010
.001,010
.002-.020
.010-.050
.010-.050
.0'10-.050
Max. Conc.
5.00
5.00
5.00
:5.00
5.00
5.00
5.00
0.050
0.050
0.050
Sample
Date
c- c
05*
­d.0b5-
-0005
S'
4.001-
4.005-
'.Oo
<.0 0:5
4.00
c-
Cr
I
0.5
< .00
0 01
-4 '00�L
-,bib
4.010
.01D
OC; Cr
1 57
5
<,q
<'.
cc
0 O'�-
0: 1
<.CIO
.-POT'
ooTs'
<�.Oag
<'-cz)
.4.001
0 p
<
J3, L,)S
Lf73
7
I �kxll
44- Ft'-) 5
D3+3
1, 556 0 S-
.ac014
5,3 i 5�
<.bfo
.53 7cl
4-o
4_ c
<
'e. 0
<.CIO
Lr,rA
ffpC71
cj"Iso
8 "T
1,1870,
B -5 * 7
001
<Cot
0 1
7 6'
ti. Z
169
5,
C. ci d
4.010
010,

Anajy�tjj
Total % 'Solids Sid
Date -

CHLORIDE by Mercuric Nitrate A.nalrroqi-° k;
Adapted from 18tb Edition of Standard Methods 4500CI=C

1 , c 5F.� 1- -5 /t "/A
-- P-Z�i4 j,3A)al-
Mercury /Yl 0911-1* -Ijr
lAnal yst*l
Icon c. UnitsJL
Sam
-Sample Date
Hg
Date Run
AS
L L7,
q -7
LEM T
Ll- m; 6
"7.11,7
wo
7. (,- 15;
c I
i1,650-
—

Subject: NC Finishing Report.xls
From: "Carol Hamilton" <[e-mail]>
Date: Wed, 5 Oct 2005 16:44:47 -0400
To: "Al Quarles" <[e-mail]>
CC: "Matt Bernhardt" <[e-mail]>, "Randy Cauble" <[e-mail]>, "Mike
Frick" <[e-mail]>
This report includes analytical and sampling fees. To what address and who's attention should the bill be
sent?
Thanks, Carol Hamilotn
Content -Description: NC Finishing Report.xls
j NC Finishing Report.xls Content -Type: application/vnd.ms-excel
Content -Encoding: base64
1 of 1 11/18/2005 2:58 PM

NC Finishing / Colortex WWTP Evaluation * results are in mg/I unless otherwise indicated
Code
Date
Hg
Zn
Cu
Pb
Ni
Ag
Cd
Cr
As
Se
Sb
CT1
9/13/2005
<.2 u /I
<.05
<.005
<.005
<.005
<.001
<.001
<.002
<.010
<.010
<.010
CB1
9/13/2005
11.69
3.758
17.299
0.3978
0.7751
<.001
0.026
1.6946
0.5505
<.010
<.010
CT2
9/13/2005
<.2 ug/I
<.05
<.005
0.0055
<.005
<.001
<.001
<.002
<.010
<.010
<.010
CB2
9/13/2005
11.717
2.161
11.337
0.3331
0.3653
<.001
0.0183
0.9663
0.4811
<.010
<.010
LIMT
9/13/2005
<.2 ug/I
<.05
<.005
0.0054
<.005
<.001
<.001
<.002
<.010
<.010
<.010
LIMB
9/13/2005
7.117
6.171
9.758
0.4152
0.3375
<.001
0.0182
6.7711
0.2675
<.010
<.010
BWS
9/13/2005
0.59
0.473
1.223
0.1129
0.0341
<.001
0.0047
0.1203
<.010
<.010
<.010
BWC
9/13/2005
13.973
7.74
44.975
1.0343
1.5605
<.001
0.0262
5.3155
0.5379
<.010
<.010
WW
9/13/20051
7.6591
29.8751
9.8851
1.7871
0.382
<.001
1 0.27691
0.97961
0.3237
<.010
<.010
Code
Date
Chloride
Sulfate
T. Phos
%TS
%TVs
COD
Phenol
CT1
9/13/2005
14.6
31.6
0.086
0.017
30
45
ND
CB1
9/13/2005
243
330
1
1.9
51.64
828
ND -
CT2
9/13/2005
17.5
29.3
0.1625
0.025
100
54
ND
CB2
9/13/2005
48.5
0.1
8.55
1.07
56.73
408
ND
LIMT
9/13/2005
8.7
23.9
0.125
0.015
100
63
ND
LIMB
9/13/2005
146
12.5
6
1.02
48.53
419
ND
BWS
9/13/2005
NR
NR
NR
0.17
80.3
385
ND
BWC
9/13/2005
146
78.5
NR
4.17
49.4
462
ND
WW
9/13/2005
146
76
9.05
0.92
5
2297
ND
Analytical Fees:
Mercury
$30
Metals
$30
Chloride
$10
Sulfate
$27
T. Phos
$20
%TS
$10
%TVs
$15
COD
$30.50
Phenol
no charge
test kit
Total
$270
Sampling Fee + Equipment (Boat & sampling equipment) _ $135
$2,700
2 hour @$25 per hour times 5 people = $250
$80
$80
$3,750
$120
$135
$90
$250
$135
$4,135 Grand Total
$274.50
0
$3,750 -

<s'
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
DIVISION OF WATER QUALITY
August 24, 1998
Mr. J. Michael Boykin
DuCharme, McMillen & Associates, Inc.
6610 Mutual Drive
Fort Wayne, In 46825
Subject: Tax Certification
NC Finishing Company.
Rowan County, NC
Dear Mr. Boykin:
In response to your letter dated August'14, 1998,
the subject facility has already been issued a Tax
Certification by this Office, therefore, there is no need
for another certification.
Please note that maintenance items such as
repairs and replacement equipment are covered under the
original certification.'
If you have any questions concerning this matter,
please do not hesitate to contact Mr. Samar Bou-Ghazale or
me.
SBG
Sincerely,
D. Rex Gleason, P. E.
Water Quality Regional Supervisor
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 261 15
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/1 O% POST -CONSUMER PAPER

DuCharme, McMillen & Associates, Inc.
August 14, 1998
Mr. Rex Gleason
Regional Supervisor
Water Quality Division
NCDENR
919 North Main Street
Mooresville, NC 28115
RE: Personal Property Tax Exemption
NC Finishing Company, Spenser, Rowan County, NC
Dear Mr. Gleason:
Tax Consultants
6610 Mutual Drive
Fort Wayne, IN 46825
Phone: [phone]
Fax: [phone]
;ra 1 7 i993
Enclosed please find a letter we received from Mr. Michael S. Landis of the Air Quality
division. We have also enclosed information regarding assets that were added to our
clients facility in Spenser, North Carolina during tax year 1997. These assets are strictly
for water quality control and pollution abatement.
We would like a certificate for tax exemption for these assets, please call me if you have
any questions or need additional information.
Sincerely,
Michael Boykin
Senior Consultant
Atlanta Bostd_.— - Cincinnati Cleveland Columbus
Dallas/Fort Worth Denver Detroit Fort Wayne Hartford Houston Indianapolis Kansas City
Los Angeles New York City Philadelphia Phoenix San Antonio San Francisco

' NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF AIR QUALITY
MOORESVILLE REGIONAL OFFICE
August 11, 1998
Mr. J. Michael Boykin
Tax Consultant
DuCharme, McMillan & Associates, Inc.
6610 Mutual Drive
Fort Wayne, Indiana 46825
Subject: Tax Certification
North Carolina Finishing Company
Color -Tex Finishing Corporation
Spencer, North Carolina
Rowan County
Site Number: 03/80/00081
Dear Mr. Boykin:
This Office received your letter dated May 22, 1998, in which you requested a tax
certification for air pollution control equipment at the NC Finishing Company,
Fieldcrest Cannon, Inc., Rowan County, North Carolina. As of January 23, 1998, NC
Finishing Company was sold by Fieldcrest Cannon, Inc. to Color -Tex, Finishing
Corporation.
This office is only authorized to issue tax certifications for air cleaning devices
and appurtenances listed on a valid NC Air Quality Permit. Since there are no air
cleaning devices or appurtenances listed on Air Permit No. 03161R07 issued to ,NC
Finishing Company, Color -Tex Finishing Corporation, this Office is not authorized to
issue a tax certification. If you have any questions with reference to this matter, please
do not hesitate to contact Brendan Davey or me at [phone].
Sincerely,
Michael S. Landis
Regional Supervisor
BGD:sl
G:\DEM\AQ\WPDATA\COUNTIES\ROWAN\00081\98081 LLET
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 28115
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

0 YEAR 1998
APPL1GATtON 51NE55S PROPERTY TAX EXEMPT
County Rowan City or Town 5a ; Gb.,�..
Fieldcrest Cannon, Inc ( North Caro
sh
Trade Name of Business Carolina Fin"
Fieldcrest Cannon, Inc. ag a artment
Name of Owner � g E. S ..a ium Dr.
Mailing Address Eden
Location of Property .
tNSTRUCT14f'f� -
�.---- destx� below claiming exemption
Under the provisions d Ca.S.105-282.1: everyowner d the types of Pets ertythe is for exemption
or exclusion from property taxes thereon must demonstrate that it meets twith the he statutory requir of th minty in which
or classification. claims for exemption or exclusion must ReverselSide) �.
the property is located during the statutory listing period -
The undersigned owner or authorized representative hereby petitions for exemptions or exclusion of the following
described property. Tlmp�Cost
Imported property held at seaport terminal
( ) 2. Special nuclear materials
• (g) 3. Property used for pollution abasement and recycling
() 4. Motor vehicle chassis temPoran7y entering the State
for having a body mounted thereon.
( ) 5. Property held in a foreign trade zone
( ) 6. Cargo containers and chassis used in ocean commerce
105-275(2)
105-275(6)
371,478-
105-275(8)
105-275(14)
105-275(23)
105-275(24)
( ) T. Tangible Personal Property shipped into this State for repair 105-275(25)
- or service and reshipment to the owner outside this State 105-277 01
( ) 8. Advances on farm products by U.S. Govt. Agency or
371,478
cooperative marketing association
TOTAL
• Application only required one time unless there are additions to the property or a change in ownership.
The above statutory citations are for identification purposes only.
Full texts of all exemption and classification statutes are available at the office of the county Assessor.
AFFIRMATION
Under penalties prescribed by law. I hereby affirm that to the best of my knowledge
hereincdescribed from taxation. lief, the statements in i I
application arc true and correct and are made for the purpose of exempting the property
further affirm that the amounts claimed on this form are taken from the records of the taxpayer and may be verified from
said re ords.
19
!if
�% Si na(ure of owner or authors ed representative
�/ � � � g
Title Telephone No.
APPROVED ED YES [�—] NO

Fieldcrest Cannon, Inc.
Rowan County
1998 - Pollution Control Equipment
Account # 211304
Year
Original
Acquired
Description
Cost
1973
200,000 gal Tank
42,717
1973
#6 Fuel Oil Pump
5,672
1973
#6 Fuel Oil Pump
5,673
1973
Oil Gun Assemblies
4,051
1976
NO.2600 Hot Plate
115
1976
Tlrn Burner
485
1976
Electric Oven
285
1976
Spectronic 88 Unit
230
1976
Electric Furnace
575
1976
Two Switchgear
15,145
1976
Switch Control Panel
10,630
1976
Analyzer, Probe, Agitator
1,943
1976
Turbmeter
1,426
1992
Paco Sludge Pump
6,920
1992
Paco Sludge Pump
6,920
1992
Paco Sludge Pump
6,920
1993
Pump Repairs and Parts
61,818
1995
Reinsulate Caustic Storage Tank
20,438
1995
PH Control System
34,768
1995
Reinsulate Steam Line - Bleach
6,876
1995
Reinsulate Steam Line - Bleach
8,843
1997
75 HP Floating Aereators
40,990
1997
Piping for 200,000 gal Oil Tank
29,607
Total Water Pollution
313,037
1978
Model LTC 2-12 Oven
2,465
1978
Model WC-24 Crusher
11,027
1978
Model WC-24 Crusher
11,027
1978
Model WC-24 Crusher
11,027
1978
Detroit Elec Host
. 7,803
1978
Detroit Elec Host
7,803
1978
John Deere 950 Tractor
7,289
Total Electrostatic Precipitator
58,441
Total 1997 Pollution Control
3719,478
J10
0GL,���j�
1
7

DIVISION OF ENVIRONMENTAL MANAGEMENT
May 12, 1997
MEMORANDUM TO: D. Rex Gleason
FROM: Samar Bou-Ghazale 158&
SUBJECT: Tax Certification
Wastewater Pretreatment Facilities
Fieldcrest Cannon, Inc., Plant No.1
417 Glen Avenue
Rowan County, North Carolina
This Office has conducted an on -site investigation confirming
the construction and operation of wastewater pretreatment
facilities at the Fieldcrest Cannon, Inc., facility in Kannapolis,
North Carolina. The wastewater treatment facilities are operating
under a valid permit (No. 1001) from the Cabarrus County Water and
Sewer Authority. The attached Tax Certification has been prepared
for your signature.
If you have any questions or require additional information,
please advise.
Attachment
SBG

State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Mr. Jerry Rowland
Tax Administrator
402 North Main Street
Salisbury, NC 28144
Dear Mr. Rowland:
E:3EHNR
DIVISION OF WATER QUALITY
May 12, 1997
Subject: Tax Certification
Wastewater Treatment/Pollution
Abatement Facilities
Fieldcrest Cannon, Inc.
Plant No.l
417 Glen Avenue
Rowan County, NC
Transmitted -herewith is Tax Certification No. TCS-542 covering
wastewater treatment/pollution abatement facilities at the
Fieldcrest Cannon, Inc., plant located at 417 Glen Avenue,
Kannapolis, Rowan County, North Carolina. The facilities are
described in plans on file with the Division of Water Quality and
the Water and Sewer Authority of Cabarrus County and operated under
Permit Number 1001 issued by the Water and Sewer Authority of
Cabarrus County.
By letter dated May 7, 1997 (copy attached), Ms. Elizabeth
Hawkins, with Fieldcrest Cannon Inc., requested tax certification
for the items as listed in her letter (attached). An inspection
conducted by Division of Water Quality staff on May 7, 1997
indicated that the constructed facilities (except item No.8) are
used exclusively to abate, reduce or prevent the pollution of
waters in accordance with North Carolina General Statute 105-
275.(8)(a).
919 North Main Street, 7W 4FAX [phone]
Mooresville, North Carolina 28115 NvAWfC An Equal Opportunity/Affirmative Action Employer
Voice 704-663-1699 _ __ 50% recycled/10% post -consumer paper

Mr. Jerry Rowland
Page 2
May 12, 1997
The Company may use this Certification to obtain tax benefits
in keeping with the appropriate Statutes.
Attachment
SBG
J
Sincerely
��/� ��
D. Rex Gleason, P. E.
Acting Regional Supervisor

'State of North Carolina
Department of Environment,
Health and Natural Resources 1 •
Mooresville Regional Office
James B. Hunt, Jr., Governor 1D� H N R
Jonathan B. Howes, Secretary
DIVISION OF WATER QUALITY
May 12, 1997
Ms. Elizabeth Hawkins, State and Local Taxes
Fieldcrest Cannon, Inc.
326 East Stadium Drive
Eden, North Carolina 27288
Dear Ms. Hawkins:
Attached are two
cov_ering the operation
subject facility.
Subject: Tax Certification
Wastewater. Treatment/Pollution
Abatement Facilities
Fieldcrest Cannon, Inc.
417 Glen Avenue
Plant No.l
Permit No.1001
Rowan County, NC
(2) copies of Tax Certification No. TCS-542
of wastewater treatment facilities at the
In a letter from you dated May 7, 1997, tax certification was
requested for certain wastewater treatment/pollution abatement
facilities (letter attached). An inspection of the plant indicated
that the following wastewater treatment facilities are used
exclusively for waste disposal or to abate, reduce or prevent the
pollution of waters in accordance with North Carolina General
Statute 105-275.(8)(a):
1. Flow splitter mechanism
2. Comminutors/Screens
3. Flow equalization
4. Fly ash settling lagoons
5. Biological treatment via
6. Secondary clarifiers
7. Solids equalization
trickling filters
919 North Main Street, W FAX [phone]
Mooresville, North Carolina 28115 An Equal Opportunity/Affirmative Action Employer
Voice 704-663-1699 50% recycled/ 10% post -consumer paper

Elizabeth Hawkins
2
May 12, 1997
The above wastewater treatment components represent the items
included in the Water and Sewer Authority of Cabarrus County's
pretreatment permit issued to Fieldcrest Cannon, Inc. on May 31,
1995, (copy attached) with the exception of the following:
Spill protection area
Please note that the spill protection area is not a wastewater
treatment device and, therefore, does not qualify for tax
certification.
The Company may use this Certification to obtain tax benefits
in keeping with the appropriate Statutes.
Sincerely
/0,
R,
D. Rex Gleason, P. E.
Acting Regional Supervisor
Attachment
SBG

State of North Carolina ,
Department of Environment, r
Health and Natural Resources a . 1 • •
Mooresville Regional Office
James B. Hunt, Jr., Governor p E H N
Jonathan B. Howes, Secretary
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
RALEIGH
TAX CERTIFICATION
(Franchise/privilege; Amortization; Property)
In accordance with the provisions of the General Statutes of North
Carolina (G. S. 105-122(d), 105-130.10, 105-147(13), 105-275(8)),
this is to certify that:
Fieldcrest Cannon, Inc.
Plant No.1
Rowan County
HAS BEEN ISSUED
Permit No. 1001 by the Water and Sewer Authority of Cabarrus County
for the operation of wastewater treatment/pollution abatement
facilities consisting of the following:
1. Flow splitter mechanism
2. Comminutors/Screens
----3---Flow--equalization - ---
4. Fly ash settling lagoons
5. Biological treatment via trickling filters
6. Secondary clarifiers
7. Solids equalization with aeration
The Environmental Management Commission and the Department of
Environment, Health, and Natural Resources have found that the
treatment facilities:
a. Have been constructed or installed;
b. Comply with the requirements of the Commission;
c. Are being effectively operated in accordance with the
terms and conditions of the Permit, Certificate of
Approval, or other document or approval issued by the
Commission;.and
d. Have as their primary rather than incidental purpose the
919 North Main Street, 4. FAX [phone]
Mooresville, North Carolina 28115 fC An Equal Opportunity/Affirmative Action Employer
Voice 704-663-1699 _ 500/o recycled/10% post -consumer paper

reduction of water pollution resulting from the discharge
of wastewater.
Issued at Raleigh, North Carolina this the 12th day of May, 1997 by
the directive of the North Carolina Environmental Management
Commission and the North Carolina Department of Environment, Health
and Natural Resources.
D. Rex Gleason, P.E.
Acting Regional Supervisor
Mooresville Regional Office
TCS-542

N.C.ENVIROP
FIELDCREST CANNON, INC. & NATUr _ , ,•;;•, ;, _S
326 East Stadium Drive
Eden, North Carolina 27288 ;Y 97
May 7, 1997
North Carolina Department of Environment,
Health & Natural Resources
Attn: Samar Bou-Ghazale
919 North Main Street
Mooresville, North Carolina 28115
Dear Mr. Bou-Ghazale:
The purpose of this letter is to request that your department consider the following list of
equipment at out Kannapolis Plant 1 manufacturing facility for tax certification as tax
exempt pollution control equipment for North Carolina property tax purposes:
• blenders;
• comminutors/screens;
• flow equalization;
• fly ash settlers;
• biological treatment via trickling filters;
• secondary clarifiers;
• solids equalization with aeration; and
• spill protection
The above equipment is authorized for pollution abatement purposes under Permit #1001
issued by the Water and Sewer Authority of Cabarrus County. If you require further
information about the equipment, please contact me at [phone]. I will obtain any
additional information you may need from our engineers or make arrangements for you to
see the equipment, if necessary.
Thank you in advance for your attention to this matter.
Very truly yours,
Elizabeth Hawkins
Senior Tax Accountant

Z�19-' 96 FR I 1 i : 32M I M SHEET TOWEL MF0 FAX NO: ?04-939-2922
I
l
WATER AND SEWER AUTHORITY
I OF CABARRUS COUNTY
Coneord, North Carolina
Tn
the
is he]
into t
listed
Industrial User Pretreatment PermitUUP)
To Discharge Wastewater Under the
IndustrW Pretreatment Program
Permit No. loos 40 CFR 410
#458 P02
we with the Water & Sewer Authority of Cabarrus County CMA ) Sewer Use
North Carolina General Statute 143-215.1, other lawful standards an regulations
1 and adopted by the'North Carolina Environmental lmagement Com 'ssion, and
FiF:T.I()CREST CANNON, INC. PLANT 1 U' t' l Q
1 LAKE CIRCLE DRIVE
KANNAPOLIS, N.C. 28082
r authorized to discharge wastewater from a facility located at the above listed address
sanitary sewer collection system and the wastewater treatment facility of the WSACC
Rocky River Regional Wastewater Treatment Plant
NPDES No. NCO036269
6400 Breezy Lane
Concord, N.C. 28025
in acc ordanoe with effluent limitations, monitoring rcquirements, and other conditions sct forth
in Pat ts I, II, and M of this industrial user pretreatment permit MP). All such discharges shall
be nude at discharge locations approved in advance by the WSACC.
This Oermit' shall become effective July 1, 1995.
This I ermit and the authorixatiori to discharge shall expire at midnight on rune 30, 2000..
Signe I this1_ day of -5,JA -
r
4Brxecutive
hn C: rdock, M r

A.
9-196 FRI 1i:32M ID:SHEET TOWEL MFG FAX NO:704-939-2922 #45B 003
Pcrmit No. 1001
Part I
pART I_ INDUSTRIAL USER SPECIFIC CONDITIONS
rip,Basic. information:
ReMiving'FOIV: '
Rocky River Regional wastewater ireauTwnt rlwlt
POTW NPDES#:
NCO036269
IUP Name:
Fieldcrest Cannon, Inc. Plant 1
IUP Number:
1001
WP Effective Date:
July 1, 1995
IUP Expiration Date:
June 30, 2000
Regulated Pipes:
pipe 01, 02, 03 and 04
Np 40 CFR#:
40 CFR 410
Authorization Statement:
1) The permittee is hereby authorized to discharge wastewater in accordance with
the effluent limitations, monitoring requirements, and all other conditions set forth
in this industrW User Pretrcatmcnt Permit (nm) into the sewer collection system
and wastewater treatment facility of the WSACC. This discharge is comprised of
two wastestrcams: the effluent from the pretreatment facility and the effluent from
the fly ash settling system. During dredgings, there am two discharges from the
fly ash settling system: one frorn the fly ash settling basin and one from the fly
ash settling ponds.
1I
The permittee is hereby authorized to continue operation of and discharge
wastewater from the following treatment or pretreatment facilities, consisting of:
• J blenders; —
• J comminutors/screens;
• flow equalization;
• ® fly ash settlers; s
• biological treatment via UickBg filU:rs; \ L
• secon arifiers
• .( solids equalizAtion with aeration; and
.spill protection.
3) After receiving authorization to construct from the WSACC, construct and
operate additidnal pretreatment units as needed to meet final effluent limitations.
K

14
19-196 FRI 1i:32M ID:SHEET TOWEL MFG
FAX NO:704-939-2922
#458 PO
Permit No. 1001
Part I
Description of Discharge
Pipe 01 Total discharge f om. the pretreatment facility, including
process and fly ash effluent wastewater.
Pipe 02 Discharge of wastewater from the fly ash settling basin during
non -dredging schedule.
Pipe 03 Discharge of wastewater from the fly ash storage lagoon during
dredging schedule.
Pipe 04 Discharge of wastewater from the fly ash settling basin during
dredging schedule.
3

Prate of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Ms. Elizabeth Hawkins
Senior Tax Accountant
Fieldcrest Cannon, Inc.
326 East Stadium Drive
Eden, North Carolina 27288
Dear Ms. Hawkins:
DEHNR
DIVISION OF WATER QUALITY
February 17, 1997
Subject: Tax Certification
Fieldcrest Cannon, Inc.
Kannapolis & Spencer Plants
Cabarrus &. Rowan Counties, NC
In response to your letter dated February 6, 1996, this
Office was not able to locate a Tax Certification for the subject
facilities. Therefore,it is suggested that a Tax Certification
request be submitted for all WWT facilities and appurtenance at the
respective plants.
Tax Certification requests should indicate the
appropriate permit number and include a list/description of items
related to wastewater treatment only. The list should also include
appropriate appurtenances such as pumps, piping, etc. associated
with the wastewater treatment facilities.
Maintenance items such as repairs and replacement
equipment are also covered under the Tax certification.
If you have any questions concerning this matter, please
do not hesitate to contact Mr. Samar Bou-Ghazale or me.
Sincerely,
D. Rex Gle son, P. E.
Water Quality -Regional Supervisor
SBG
919 North Main Street, �1�a� FAX [phone]
Mooresville, North Carolina 28115 An Equal Opportunity/Affirmative Action Employer
Voice 704-663-1699 - 50% recycled/10% post -consumer paper

FIELOCREST CANNON, INC.
326 EAST STADIUM DRIVE
EDEN, NORTH CAROLINA 27288
N.C. U8PT. of
FNVjreOj,,'�AF-NT, HEALTH
dx NATURAL RESOURCE, S
February 6, 1997}F r, ; :, eP+�IPr-
E�Y1iiEVih :uif�c�. Y. E1141� �itiGlff
v fit? �,� ` Gi'uh� OFEif;E
D. Rex Gleason, P.E.
State of North Carolina Department of
Environment, Health and Natural Resources
919 North Main Street
Mooresville, North Carolina 28115
Re: Tax Certification
Fieldcrest Cannon, Inc.
Kannapolis and Spencer Plants
Dear Mr. Gleason:
I recently contacted Mr. Samar Bou-Ghazale to clarify the procedure regarding tax
certification of pollution control equipment at the,above plants. Mr. Bou-Ghazale indicated to
me that because we have previously obtained tax certification for pollution control equipment
at these facilities, it may be unnecessary to obtain tax certification for the additional equipment
purchased at the facilities each year. It was his opinion that the original tax certification letter
would have been broadly defined in order to include future purchases of repair and
replacement equipment.
I also consulted with a representative at the Cabarrus County Tax Assessor's Office. She
advised me that the county requires a letter of tax certification from the appropriate
department for each additional asset placed in service at a permitted pollution control facility.
This includes all replacement equipment. I have enclosed a copy of North Carolina General
Statute 105-275(8)a which appears to support the position of the County Tax Assessor.
I received a letter from M. Steven Mauney indicating that my request of January 30, 1997 for
tax certification of pollution control equipment at our Kannapolis Waste Water Treatment
Plant has been referred to your office. Please advise me as to how you will proceed with the
tax certification of this property.
Also, I located a letter to Jimmie Rice, Fieldcrest Cannon, Inc., from you dated July 23, 1996
regarding our request for tax certification of pollution control equipment purchased in 1995 at
the same facilities. Ms. Rice has since left the company, and I am unsure whether we obtained
the proper certification for this equipment. Please let me know whether this situation was

red appropriately. If you have any questions or require additional information, please call
me at [phone]. Thank you for your assistance in this matter.
Very truly yours,
Elizabeth Hawkins
Senior Tax Accountant
Enclosure

Law § 105-275 Property classified and excluded from the tax base.
§ 105-275. Property classified and excluded from the tax base. The following classes
of property are hereby designated special classes under authority of Article V, Sec. 2(2),
of the North Carolina Constitution and shall not be listed, appraised, assessed, or taxed:
Law § 105-275(8)a
a. Real and personal property that is used or, if under construction, is to be used
exclusively for air cleaning or waste disposal or to abate, reduce, or prevent the pollution
of air or water (including, but not limited to, waste lagoons and facilities owned by public
or private utilities built and installed primarily for the purpose of providing sewer service
to areas that are predominantly residential in character or areas that lie outside territory
already having sewer service), if the Department of Natural Resources and Community
Development or a local air pollution control program for air -cleaning devices located in an
area where the Environmental Management Commission has certified a local air pollution
control program pursuant to G.S. 143-215.112 furnishes a certificate to the tax
supervisor of the county in which the property is situated or to be situated stating that the
Environmental Management Commission or local air pollution control program has found
that the described property:
1. Has been or will be constructed or installed;
2. Complies with or that plans therefor which have been submitted to the Environmental
Management Commission or local air pollution control program indicate that it will
comply with the requirements of the Environmental Management Commission or local air
pollution control program;
3. Is being effectively operated or will, when completed, be required to operate in
accordance with the terms and conditions of the permit, certificate of approval, or other
document of approval issued by the Environmental Management Commission or local air
pollution control program; and
North Carolina State & Local Taxes: Copyright 1997, Research Institute of America Inc. 2/06/97 Page 1

4. Has or, when completed, will have as its primary rather than incidental purpose the
reduction of water pollution resulting from the discharge of sewage and waste or the
reduction of air pollution resulting from the emission of air contaminants.
North Carolina State & Local Taxes: Copyright 1997, Research Institute of America Inc. 2/06/97 Page 2

hl��J �w�w�✓�r.J l/1'�/O/V
2