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HomeMy WebLinkAboutWQ0034468_Renewal Application_20201109Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0034468 Applicant/Permittee Brunswick County Applicant/Permittee Address Post Office Box 249; Bolivia, N.C. 28422 Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type County Facility Name Brunswick County DCAR County Brunswick Fee Category Major Fee Amount $0 Is this a complete application?* r Yes r No Complete App Date 11/09/2020 Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other .......................................................... electronic surece, aner correspondence. _ - Name * Rob Willcox Email Address* rob@willcoxmabesoil.com Project Information ........ ..................................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3363399128 O Modification - Minor G Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WQ0034468 Fbs Current Existing pernit number Applicant/Permittee* Brunswick County Applicant/Permittee Address* Post Office Box249; Bolivia, N.C. 28422 Facility Name * Brunswick County DCAR Please provide comments/notes on your current submittal below. Permit Renewal - WQ0034468 - Renewal Only (No fee) At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Spec'rfications, Calculations, Rc.) Renewal of Distribution of Class A Residuals WQ0034468 42.68MB (November 2020).pdf upload only 1 RCFdocurrent (less than 250 M3). Multiple docurrents rrust be combined into one R7Ffile unless file is larger than upload linit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature * � k�w Submission Date 11-9-20 Is filled in autorratically once subrritted. APPLICATION FOR PERMIT RENEWAL DISTRIBUTION OF CLASS A RESIDUALS BRUNSWICK COUNTY NON -DISCHARGE PERMIT NO. W00034468 WMSS Project No. 15-04, Phase: 11 Prepared for: Brunswick County — Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 Prepared by: Willcox & Mabe Soil Solutions, PLLC 7231B Summerfield Road Summerfield, North Carolina 27358 willcox&mabe SOIL SOLUTIONS November 2020 November 5, 2020 NCDEQ/DWR Water Quality Permitting Section Non -Discharge Branch 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Non -Discharge Branch Reference: Application for Permit Renewal Distribution of Class A Residuals — Permit No. WQO034468 • Northeast Brunswick Regional WWTP • West Brunswick Regional WWTP • Beaver Dam Creek WTP WMSS Project No. 15-04, Phase: 11 Non -Discharge Branch: Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting the enclosed Distribution of Class A Residuals permit renewal application for Brunswick County on behalf of Brunswick County. The application package includes information for renewal of the following sources: Northeast Brunswick Regional WWTP — 1,000 dry tons, West Brunswick Regional WWTP — 1,000 dry tons, Beaver Dam Creek WTP — 3,500 dry tons. If there is any further information required or questions regarding this application please do not hesitate to contact Brunswick County, Mr. Tim Webb at (910) 253-2479 or WMSS at 336-339-9128 for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabe Partner / Agronomist cc: Brunswick County Rob Willcox, L.S.S. Partner / Soil Scientist Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 11 - 2020 Class A Permit Renewal\Renewal of Distribution of Class A Residuals Application Package (October 2020).doc TABLE OF CONTENTS APPENDIX TITLE I DISTRIBUTION OF CLASS A RESIDUALS APPLICATION FORM (FORM: DCAR 06-16) OPERATION AND MAINTENANCE PLAN (RENEWAL) II FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION) • NORTHEAST BRUNSWICK REGIONAL WWTP • WEST BRUNSWICK REGIONAL WWTP • BEAVER DAM CREEK WTP III RESIDUALS SOURCE CERTIFICATION APPLICATION FORM • NORTHEAST BRUNSWICK REGIONAL WWTP (FORM: RSC 06-16) IV RESIDUALS SOURCE CERTIFICATION APPLICATION FORM • WEST BRUNSWICK REGIONAL WWTP (FORM: RSC 06-16) V RESIDUALS SOURCE CERTIFICATION APPLICATION FORM • BEAVER DAM CREEK WTP (FORM: RSC 06-16) APPENDIX I DISTRIBUTION OF CLASS A RESIDUALS APPLICATION FORM (FORM: DCAR 06-16) OPERATION AND MAINTENANCE PLAN (RENEWAL) DISTRIBUTION OF CLASS A RESIDUALS APPLICATION FORM (FORM: DCAR 06-16) State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): ® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The project name should be consistent on the plans, specifications, etc. ® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) RENEWAL — N/A ❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit I Major Modification' Major (residuals permitted for distribution > 3,000 dry tons/year) F $1,310 $395 Minor (residuals permitted for distribution < 3,000 dry tons/year) 1 $810 $245 ' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 1 of 3 D. Program Information (All Application Packages) (APPENDIX II) ❑ Provide a narrative explaining the following: ❑ How the materials will be handled and transported from where the residuals were produced to where it will be treated. ❑ How the residuals will be processed/treated (attach process flow diagram). ❑ How leachate collection will be handled. ❑ Where the residuals will be stored until processed. ❑ How the final product will be distributed (packaging, bulk, etc.) ❑ What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. ❑ Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ❑ Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: ❑ Name and address of the person who prepared the residual that is sold or given away. ❑ A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. ❑ A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ❑ A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ❑ Information on all applicable setbacks in accordance with 15A NCAC 02T . 1108(b). ❑ A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) (N/A) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T .I 108(a) on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T .1104(a)(2)(B), including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) (N/A) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). G. Environmental Assessments (May be Required — See 15A NCAC 1C .0300) (N/A) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Operation and Maintenance Plan (New and Renewal Application Packages) (APPENDIX I) ❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ❑ Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: ❑ Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ❑ Maintenance schedules; may include equipments calibration, maintenance of signs, etc. ❑ Safety measures; may include safety training program, manuals, signs, etc. ❑ Spill response plan; including control, containment, remediation, emergency contact information, etc. ❑ Inspection plan including the following information; ❑ Names and titles of personnel responsible for conducting the inspections. ❑ Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ❑ Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ❑ Sampling and monitoring plan including the following information; ❑ Names and titles of personnel responsible for conducting the sampling and monitoring. ❑ Detailed description of monitoring procedures including parameters to be monitored. ❑ Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: By Courier/Special Delivery: 1617 MAIL SERVICE CENTER 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27699-1617 RALEIGH, NORTH CAROLINA 27604 TELEPHONE NUMBER: (919) 807-6464 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 L APPLICANT INFORMATION: 1. Applicant's name: Brunswick County Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility Federal ❑ State ❑ Municipal ® County Signature authority's name per 15A NCAC 02T .0106: Donald B. Dixon Title: Deputy Director Applicant's mailing address: Post Office Box 249 City: Bolivia State: N.C. Zip: 28422 Telephone number: (910) 253-2485 Email Address: donald.dixongbrunswickcolMnc.gov 2. Consultant's name: Rob Willcox, LSS License Number (for P.E.): N/A Affiliation: ❑ On Staff E Retained (Firm: Willcox & Mahe Soil Solutions, PLLC) Consultant's mailing address: 7231B Summerfield Road City: Suminerfield State: N.C. Zip: 27358 Telephone number: (336) 339-9128 Email Address: rob&willcoxmabesoil.com 3. Fee submitted: $0.00 (See Instruction B) IL PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00034468 Date of most -recently issued permit: May 6, 2016 Date of most -recently certified Attachment A (if different than the permit): December 23, 2019 III. FACILITY INFORMATION: 1. Name of residuals processing facility: Northeast Brunswick WWTP, West Brunswick Regional WWTP, Beaver Dam WTP City: NE —Leland, West —Supply, Beaver Dam -Supply State: N.C. Zip: - Coordinates: NE Latitude: 34' 16' 17" Longitude: 78° 00' 20" Coordinates: West Latitude: 34° 01' 39" Longitude: 78' 16' 22" Coordinates: Beaver Dam Latitude: 33' 57' 35" Longitude: 78° 04' 56" Datum: NAD 83 Level of accuracy: nearest second Method of measurement: MAP County where facility is located: Brunswick 2. Facility contact (person familiar with residuals preparation): Name: Tim Webb Title: Wastewater Superintendent Mailing address: Post Office Box 249 City: Bolivia State: N.C. Zip: 28422 Telephone number. (910) 253-2479 E-mail address: tim.webbnae brmswickcountync.gov FORM: DCAR 06-16 Page 1 of 3 3. Is the residual process facility also the generator? ® Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: > 30 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: 1. Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); Land applied as a liquid or cake residual Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added Der 1.0 dry ton of residuals (dry ton) N/A 3. Approximate amounts of the residuals received and processed at the facility: NE-1.000: West 1.000. Beaver Dam-3.500 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: NE-1.000: West 1.000. Beaver Dam-3.500 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): NE-(2) Post-ATAD Tanks, 375,000 Total, West-(2) 238,000 WAS Tanks, (4) ATAD Tanks-24,000 each. (1) ATAD Storage Tank-450.000: Beaver Dam -Drying Beds & Lagoon, all sources >30 days 6. Does the facility have a stormwater management plan? ❑ Yes; ® No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: N/A V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. En RSC 06-16.doc (APPENDIX III) FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) I, A , attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ® Yes ❑ No, Explain; I, Donald B. Dixon Deputy Director (Signature Authority's Name PLEASE PRINT) (Title) attest that this application for Renewal of Brunswick County Distribution of Class A Residuals Permit No. WO0034468 (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: �--1-�` �S . Date: ti s Zv FORM: DCAR 06- l6 Page 3 of 3 OPERATION AND MAINTENANCE PLAN (RENEWAL) OPERATION AND MAINTENANCE PLAN Brunswick County Public Utilities Non -Discharge Permit No. WQ0034468 DISTRIBUTION OF CLASS A BIOSOLIDS / RESIDUALS Northeast Brunswick Regional WWTP West Brunswick Regional WWTP Beaver Dam Creek WTP Class A Biosolids / Residuals Description and Overview The purpose of the Brunswick County Public Utilities Operation and Maintenance Plan is to put into place a plan that implements the requirements of North Carolina Department of Environmental Quality (NCDEQ) — Division of Water Resources (DWR) Distribution of Class A Residuals Permit (WQ0034468). I. Operational Functions The operational functions of this program involve hauling biosolids / residuals from the respective WWTP's and WTP's and land applying in accordance with regulatory requirements. Biosolids / residuals will be land applied at or below agronomic rates that are determined using the Realistic Yield Expectations (RYE) as outlined in the permit. The current land application contractor will also account for any nutrient sources the landowner/lessee has applied. Source(s) may be land applied as either a liquid or cake material utilizing either pumper trucks, vacuum trucks, tractor trailer, tractor and cake spreader and/or tractor and pull tank. Whichever method is utilized to land apply the biosolids / residuals, the current land application contractor will spread evenly and at consistent rates. Biosolids / residuals will be land applied on fields that are used for hay production, grazing, or row crop production harvested for animal feed. In the case where biosolids / residuals are land applied on fields utilized for grazing, applications rates will be reduced by 25% in accordance with USDA-NRCS 590 Nutrient Management Standards. Grazed fields will be determined by the current land application contractors manager on site. II. Maintenance Schedules The Brunswick County Public Utilities staff is responsible for maintenance of the facilities and equipment at the respective WWTP's. The current land application contractor is responsible for maintenance of the equipment associated with the land application program. Maintenance schedules are as follows: • Preventive maintenance is performed throughout the plant site. 9 Oiling/greasing gear boxes on moving parts. Operation and Maintenance Plan Brunswick County Public Utilities - Class A Biosolids / Residuals Permit No. W00034468 • Check belts for tightness. III. Safety Measures Safety plans and training are the responsibility of the personnel associated with the land application program. All employees involved with the land application program will be required to comply with safety plans and training as applicable to the Class A Distribution Permit. Land application program employees shall be trained, as appropriate, in general awareness for the protection of water and pollution prevention general practices. This training will be provided as part of a new employee orientation program or as part of ongoing environmental awareness training. General refresher training for those employees involved will be provided in accordance with applicable regulatory or permit requirements. IV. Spill Response Plan Includes the following: • Spill Control Plan (Attached), • Spill Prevention Plan (Attached), • Spill Control, Containment and Cleanup Plan (Attached). V. Inspection Plan Names and/or titles of personnel responsible for conducting the inspections: Michael Garrity - West Brunswick Regional WWTP - ORC Matt Henry - Northeast Brunswick WWTP — ORC Jeremy Sexton - Beaver Dam Creek WTP— ORC The Operator in Responsible Charge (ORC) of the WWTP and WTP facilities are responsible for the daily operations at the designated facilities. The land application ORC or personnel under the direct supervision of the ORC has responsibilities to include inspections land application sites / activities (when land application is scheduled). The land application ORC will maintain daily record keeping logs of land application activities, inspections of field applications equipment and maintenance, loading operation, roads, crops, crop maintenance and harvesting practices. All daily record keeping logs will be coordinated with the ORC at the end of each day. In the event that a noncompliance event is observed during any inspection, the ORC of the WWTP will be immediately notified. The ORC will determine the course of action to be taken in order to rectify the noncompliance issue. NCDEQ will be notified as soon as Operation and Maintenance Plan Brunswick County Public Utilities - Class A Biosolids / Residuals Permit No. W00034468 possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence. At a minimum, these inspections will consist of the following • Verify that a biosolids / residuals analysis has been collected prior to land application activities being performed and that it meets the criteria for land application. • Verify that pathogen and vector attraction reduction data (if applicable) has been collected for the source to be land applied and that it meets the criteria for land application. • Verify the crop that is planted or is to be planted on the respective field(s). • Confirm that the correct amount of biosolids / residuals are being land applied. • Confirm that manned equipment has a copy of the permit and the operations and maintenance plan. • Check that the field has been properly flagged and that buffers are adhered to. • Check that proper signage is posted. • Confirm that records are turned in at the end of each business day. Inspections will also be conducted by the respective employees of the biosolids / residuals generating facilities (at the source generating facility). The land application contractor will not be responsible for inspections at the source generating facilities. These inspections should be conducted by the respective ORC of each facility and should fall under their own Operations and Maintenance Plans. VI. Sampling and Monitoring Plan The respective WWTP's / WTP's Class A Biosolids / Residuals will be monitored to confirm compliance with conditions in Non -Discharge Permit No. WQ0034468 to include: • Toxicity Characteristics Leaching Procedure (TCLP), • Reactivity, Ignitability and Corrosivity, • 15A NCAC 02T .1105 Pollutant Limits and nutrient analysis, • Pathogen and Vector Attraction Reduction requirements (if applicable), • Annual Representative Soil Analysis of each field which receives land application during each respective year. • Any other applicable Permit conditions. All sampling and monitoring shall be performed in accordance with the current Permit. Operation and Maintenance Plan Brunswick County Public Utilities - Class A Biosolids / Residuals Permit No. WO0034468 Pollutant concentrations in the Brunswick County Public Utilities WWTP / WTP Class A Biosolids / Residuals shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs): Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 The Brunswick County Public Utilities WWTP Class A Biosolids / Residuals shall be analyzed to demonstrate it is non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed based on conditions (monitoring frequencies) set forth in Permit No. WQ0034468. TCLP shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dic loro pyridine (5.0) )ethylene Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride Endrin (0.02) Silver (5.0) (0.5) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachlor -1,3-butadiene Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) 4 Operation and Maintenance Plan Brunswick County Public Utilities - Class A Biosolids / Residuals Permit No. W00034468 An analysis shall be conducted on the Brunswick County Public Utilities WWTP / WTP Class A Biosolids / Residuals based on conditions (monitoring frequencies) set forth in Permit No. WQ0034468. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) The Brunswick County Public Utilities WWTP / WTP Class A Biosolids / Residuals shall be analyzed to demonstrate compliance with Pathogen Reduction and Vector Attraction Reduction requirements based on conditions (monitoring frequencies) set forth in Permit No. WQ0034468. The current Pathogen Reduction Alternatives and Vector Attraction Reduction Options utilized are as follows: Pathogen Reduction: Per 15A NCAC 02T.1106 For Land Application of Class A: ® [15A NCAC 02T.1106(a)(2)(A)] - Fecal Coliform Density Demonstration And (for Biological Residuals) Alternative 5 [15A NCAC 02T.1106(a)(3)(E)] - Process to Further Reduce Pathogens (PFRP) Specify one: composting, heat drying, ® heat treatment, thermophilic aerobic digestion, ❑ beta ray irradiation, gamma ray irradiation, or ❑ pasteurization. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107 For Land Application of Class A WWTP Biosolids: ® Alternative 1 [15A NCAC 02T.1107(a)(1)] — 38-Percent Volatile Solids Reduction Or Alternative 3 [15A NCAC 02T.1107(a)(3)] — 30-Day Bench Scale Test (Aerobic Digestion) 5 Operation and Maintenance Plan Brunswick County Public Utilities - Class A Biosolids / Residuals Permit No. W00034468 For Land Application of Class A WTP Biosolirls: ® Not Applicable — Non -Biological Residuals with NO Domestic Wastewater Contribution. Attachments: Spill Control Plan Spill Prevention Plan Spill Control, Containment and Cleanup Plan Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 11 - 2020 Class A Permit Renewal\O&M Plan -Brunswick County- WQ0034468-October 2020.doc BRUNSWICK COUNTYPUBLIC UTILITIES SPILL CONTROL PLAN NON -DISCHARGE PERMIT NO. WQ0034468 THE FOLLOWING ACTIONS MUST BE TAKEN IN THE EVENT OF A SPILL: 1. Halt the source of the spill: Ruptured line, valve, or container / damaged tank or transport unit. 2. Contain spill: Use straw bales to form a barrier. Straw or hay bales can be obtained from several sources for this purpose. Soil near the site can also be used to form a barrier for containment. 3. Clean up: Use land application equipment to recover as much of the material as possible. After the application equipment has recovered as much of the material as possible, it will be land applied as per the management plan. A temporary sump pit may be dug in the containment area to enhance recovery, if necessary. 4. Notification: As soon as possible after a spill occurs notify: • NC Department of Environmental Quality Division of Water Resources Regional Office Wilmington Regional Office (910) 796-7215 • Fire Department if assistance is required for wash down 5. Management of clean up efforts: The responsible parry for land application shall take immediate charge of the clean up activities. Additional labor will be requested as needed. 6. Reporting: Within 24 hours of a spill the responsible party for land application shall present a written report detailing the cause of the spill and all action taken in response to the spill. The Wilmington Regional Office shall be notified in no case more than 24 hours or on the next working day following the occurrence. SPILL PREVENTION PLAN The spill prevention plan requires that all equipment used to transport biosolids / residuals be subject to periodic safety inspections. Tires, brakes, lights, and turn signals will be inspected for proper working order. Each truck will be equipped with safety flares and appropriate signs to be used in the event of a breakdown. Any deficiencies observed during the safety inspections will result in the vehicle being removed from service and the responsible party for land application will be notified so that these deficiencies can be corrected and documented. Routes leading from the storage point to the land application sites will be inspected for road hazards. The road hazards will be documented and the drivers will be informed of the hazards. Alternate routes will be investigated and routes which minimize road hazards will be selected. Hazardous situations resulting from rush-hour traffic will be avoided during hauling. Drivers and management personnel associated with the hauling of biosolids / residuals will be instructed in the spill prevention plan and will be required to attend training sessions. Drivers will be trained in defensive driving techniques in order to minimize road hazards. A driver who observes a road hazard will be required to report the hazard to the field superintendent who, in turn, will warn other drivers. As part of the spill prevention plan, drivers will be required to inspect the safety equipment of their vehicles on a daily basis. Any deficiency in safety equipment will be noted for corrective action. Drivers will be trained in the procedures to be taken in the event of a spill that occurs during the hauling of biosolids / residuals. These procedures are discussed in the spill control, containment, and cleanup plan. SPILL CONTROL, CONTAINMENT, AND CLEANUP PLAN Spills that occur during loading or unloading biosolids / residuals will occur at the generation point and the land application sites, respectively. These spills will not involve an environmental hazard or an over the road hazard and, therefore, will be handled using the equipment that will be available at either site. Spills that occur over -the -road will be subject to the contingencies contained in the spill control, containment, and cleanup plan. The equipment used in the spill control, containment, and cleanup consists of the following: 1. Vacuum pump, pump truck or tanker truck. A vacuum truck, vacuum pump or tanker truck will be used to assist with clean-up of biosolids / residuals spills. 2. Outside equipment if required The following personnel will be involved in the spill control, containment, and cleanup. 1. The responsible parry for land application will respond to the spill site and make an assessment of the spill and determine the containment procedures to be initiated and the equipment to be used to clean up the spill. 2. The responsible parry for land application will be responsible for the direction of the cleanup team. In the event of a spill, the driver of the truck or application vehicle, if he has not sustained a debilitating injury, will call the responsible parry for land application and report the spill. The responsible party for land application will notify the appropriate authorities and will also notify the NCDEQ-DWR Regional Office. The driver will set up safety flares and signs to warn motorists of the hazard. The responsible party for land application will mobilize the necessary equipment and personnel to the site, and will initiate the containment procedures. When the cleanup team arrives at the site, the site will be cleaned up according to the contingency plan. Biosolids / residuals cleaned up from the site will be transported to the land application sites where it will be applied in accordance with the permit. In the event that the driver is incapacitated due to personal injury, the responsible party for land application will mobilize the cleanup team as soon as the authority's notification of an incident. APPENDIX II FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION) • NORTHEAST BRUNSWICK REGIONAL WWTP • WEST BRUNSWICK REGIONAL WWTP BEAVER DAM CREEK WTP FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION) • NORTHEAST BRUNSWICK REGIONAL WWTP D. Program Information (NORTHEAST BRUNSWICK REGIONAL WWTP) • How the materials will be handled and transported from where the residuals were produced to where it will be treated. All residuals will remain at the WWTP until ready for land application • How the residuals will be processed/treated (attach process flow diagram). (Attached at the end of this Section) • How leachate collection will be handled. Leachate will not be generated • Where the residuals will be stored until processed. (Same as Above) - All residuals will remain at the WWTP until ready for land application • How the final product will be distributed (packaging, bulk, etc.) The final product will be land applied to private farm land • What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. One of the primary benefits of the WWTP residuals will be its ability to be utilized as a nitrogen source to replace the need for commercial nitrogen. Plant Available Nitrogen (PAN) will be applied at agronomic rates in accordance with existing permit conditions that regulate application rates. • Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. Product Information Sheet and Application Information Sheet attached at the end of this Section • Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: • Name and address of the person who prepared the residual that is sold or given away. D. Program Information (NORTHEAST BRUNSWICK REGIONAL WWTP) Page 2 • A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. • A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. • A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. • Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b). • A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. Product Information Sheet and Application Information Sheet attached at the end of this Section BRUNS WICK COUNTY PUBLIC UTILITIES OPERATIONS CENTER 250 GREY WATER ROAD NE SUPPLY, NORTH CAROLINA 28462 MAILING ADDRESS P. O. Box 249 BOLIVIA, NORTH CAROLINA 28422 TELEPHONE (910)253-2657 FAX (910)253-4305 Operational data for the Northeast Brunswick Regional WRF (WQ0034468) Sludge Treatment for Pathogen and Vector Attraction Reduction The Northeast Brunswick Regional WRF (NC0086819) utilizes the Kruger ATAD process for residuals treatment and stabilization of our biosolids. Over the last year our ATAD tanks 50,000 gallons each run at an average temperature of 68.0 degrees Celsius while batch feeding approximately 6,000 gallons five days/week. In the most extreme "drop" in temperature the ATAD's went as low as 60.0 degrees Celsius for no more than 2 hours. At the average operational temperature, the facility needs approximately 0.4 days to meet the time and temperature portion of the Class "A" requirements. Our process at minimum stays at or above the average temperature on a daily basis. The attached Fecal Density (and sludge analysis) shows the pathogen reduction was met. Also attached is our 30-day Bench Scale analysis for meeting the Vector Attraction Reduction (VAR). Production for calendar year 2019 was 349.38 dry tons with a permitted capacity of 1,000 dry tons per year. Residuals are land applied on Brunswick County permitted sites at 4.5% to 5.5 % solid. The Northeast Brunswick Regional WRF is currently being expanded to 4.975 MGD, this construction will be completed in late 2021. If you would like to contact me for additional information I can be reached at: 910-253-2479 or by email: tim.webb a,brunswickcountync, ov Tim Webb Wastewater Superintendent Brunswick County Public Utilities NORTHEAST BRUNSWICK REGIONAL WWTP PRODUCT INFORMATION SHEET Produced By Preparer Brunswick County Tim Webb Northeast Brunswick Regional WWTP Wastewater Superintendent Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 For information on this product contact Brunswick County Public Utilities Tim Webb, Wastewater Superintendent (910) 253-2479 The Class A Residual (Northeast Brunswick Regional WWTP) is generated by treatment of industrial and domestic wastewater. The generated residuals are stable and contain a high nitrogen value for their application as a nitrogen fertilizer. Northeast Brunswick Regional WWTP is permitted for land application to farmland in accordance with Permit No. WQ0034468. Provisions for Application Application of Northeast Brunswick Regional WWTP is prohibited except in accordance with the provisions specified in the Application Information Sheet. Application must conform to standards identified in Permit WQ0034468 and include but are not limited to: Setback Description Setback (feet) Liquid Cake Private or public water supply sources 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 100 25 Surface water diversions (ephemeral streams, waterways, ditches) 25 0 Groundwater lowering ditches (where the bottom intersects the SHWT) 25 0 Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 Application Information Sheet 1. Northeast Brunswick Regional WWTP is intended for use as a nitrogen fertilizer. Applications of Northeast Brunswick Regional WWTP should be made in accordance with approved application standards and WQ0034468 permit conditions. 2. Northeast Brunswick Regional WWTP shall not be applied to flooded, frozen, or snow covered areas. 3. Application and storage of Northeast Brunswick Regional WWTP must be conducted in such a way as to prevent runoff from the application or storage site to any surface water. 4. Applications and loading rates of Northeast Brunswick Regional WWTP shall be applied at rates that comply with realistic yield expectations based on the soil series and crops found at: http://nutrients.soil.ncsu.edu/yields/. 5. Northeast Brunswick Regional WWTP shall not be applied if the land fails to assimilate the material or the application causes the contravention of surface water or groundwater standards. 6. Northeast Brunswick Regional WWTP shall not be applied within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-hour period following a residuals land application event. 7. Northeast Brunswick Regional WWTP shall not be applied during a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period. 8. Northeast Brunswick Regional WWTP shall not be applied if the slope is greater than 10% for surface applied material, or if the slope is greater than 18% for injected or incorporated material. 9. Northeast Brunswick Regional WWTP shall not be applied if the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24- hour period following a residuals land application event. Any field that is in a USDA no - till program shall be exempted from meeting this vegetative cover requirement. 10. Northeast Brunswick Regional WWTP shall not be applied if the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot. 11. Northeast Brunswick Regional WWTP shall not be applied if the vertical separation of bedrock and the depth of residuals application is less than one foot. Contact Brunswick County for a copy of the most recent residuals analysis and loading rates. NORTHEAST BRUNSWICK REGIONAL WWTP RECEIPT FORM I , (printed name) have received gallons/wet tons of the Northeast Brunswick Regional WWTP Residuals, a copy of the Northeast Brunswick Regional WWTP Residuals Product Information Sheet, and a copy of the most recent analysis of the product. I have read these documents and agree to adhere to the directions specified on the Application Information Sheet and the Product Information Sheet. Signature of Receiver Date of Receipt FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION) • WEST BRUNSWICK REGIONAL WWTP D. Program Information (WEST BRUNSWICK REGIONAL WWTP) • How the materials will be handled and transported from where the residuals were produced to where it will be treated. All residuals will remain at the WWTP until ready for land application • How the residuals will be processed/treated (attach process flow diagram). (Attached at the end of this Section) • How leachate collection will be handled. Leachate will not be generated • Where the residuals will be stored until processed. (Same as Above) - All residuals will remain at the WWTP until ready for land application • How the final product will be distributed (packaging, bulk, etc.) The final product will be land applied to private farm land • What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. One of the primary benefits of the WWTP residuals will be its ability to be utilized as a nitrogen source to replace the need for commercial nitrogen. Plant Available Nitrogen (PAN) will be applied at agronomic rates in accordance with existing permit conditions that regulate application rates. • Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. Product Information Sheet and Application Information Sheet attached at the end of this Section • Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: • Name and address of the person who prepared the residual that is sold or given away. D. Program Information (WEST BRUNSWICK REGIONAL WWTP) Page 2 • A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. • A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. • A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. • Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b). • A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. Product Information Sheet and Application Information Sheet attached at the end of this Section S*11 K 0� COUNTY OF BRUNSWICK sm�J� yr, PUBLIC UTILITIES DEPARTMENT i Wastewater Treatment Division }� hyOpr�a'ds PO BOX 249 BOLIVIA, NC 28422 (910) 755-7921 (910) 755-7927 FAX Operational data for the West Brunswick Regional WWTP (WQ0034468) Sludge Treatment for Pathogen and Vector Attraction Reduction The West Brunswick Regional \\'WTP (W'Q0034468) utilizes the ATAD process for residuals treatment and stabilization of our bio-solids. We have four (4) A`hAD tanks that over the last year have operated at an average of 125.0 to 1 35.0 degrees Fahrenheit while batch feeding approx. 6.000 gallon per tank as needed.. In the most extreme "drop'- in temperature we have went as low as 122.0 degrees Fahrenheit. At the average temperature we are operating we need approximately .43 to 2.63 days to meet the time and temperature portion of the Class --A*' requirements. Our process at the minimum stars at our above that temperature for 48-72 hours (we transfer to the ATAD tanks to our residuals storage tank. Our attached Fecal Density (and sludge analysis) show s the pathogen reduction was met. We have also attached our 30-Day Bench Scale analysis for meeting the Vector Attraction Reduction (VAR). We have all the historical data trends on our SCADA server to show- that time/temp was met although it would take a considerable amount of paper to print. Residuals are land applied on Brunswick County permitted sites at a 3% to 4 % solid. Production for calendar year 2015 was 464 dry tons with a permitted capacity of 500 dry tons per year. disposal capacity will be increased as flow increases to facility. If you would like to contact me for additional info I can be reached ,a. (910) 755-7921 or by email: donald.dixon a: brunswickeountvnc.goe Donald B. Dixon Wastewater Superintendent Brunswick County Public Utilities WEST BRUNSWICK REGIONAL WWTP PRODUCT INFORMATION SHEET Produced By Preparer Brunswick County Tim Webb West Brunswick Regional WWTP Wastewater Superintendent Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 For information on this product contact Brunswick County Public Utilities Tim Webb, Wastewater Superintendent (910) 253-2479 The Class A Residual (West Brunswick Regional WWTP) is generated by treatment of industrial and domestic wastewater. The generated residuals are stable and contain a high nitrogen value for their application as a nitrogen fertilizer. West Brunswick Regional WWTP is permitted for land application to farmland in accordance with Permit No. WQ0034468. Provisions for Application Application of West Brunswick Regional WWTP is prohibited except in accordance with the provisions specified in the Application Information Sheet. Application must conform to standards identified in Permit WQ0034468 and include but are not limited to: Setback Description Setback (feet) Liquid Cake Private or public water supply sources 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 100 25 Surface water diversions (ephemeral streams, waterways, ditches) 25 0 Groundwater lowering ditches (where the bottom intersects the SHWT) 25 0 Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 Application Information Sheet 1. West Brunswick Regional WWTP is intended for use as a nitrogen fertilizer. Applications of West Brunswick Regional WWTP should be made in accordance with approved application standards and WQ0034468 permit conditions. 2. West Brunswick Regional WWTP shall not be applied to flooded, frozen, or snow covered areas. 3. Application and storage of West Brunswick Regional WWTP must be conducted in such a way as to prevent runoff from the application or storage site to any surface water. 4. Applications and loading rates of West Brunswick Regional WWTP shall be applied at rates that comply with realistic yield expectations based on the soil series and crops found at: http://nutrients.soil.ncsu.edg/yields/. 5. West Brunswick Regional WWTP shall not be applied if the land fails to assimilate the material or the application causes the contravention of surface water or groundwater standards. 6. West Brunswick Regional WWTP shall not be applied within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-hour period following a residuals land application event. 7. West Brunswick Regional WWTP shall not be applied during a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period. 8. West Brunswick Regional WWTP shall not be applied if the slope is greater than 10% for surface applied material, or if the slope is greater than 18% for injected or incorporated material. 9. West Brunswick Regional WWTP shall not be applied if the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24- hour period following a residuals land application event. Any field that is in a USDA no - till program shall be exempted from meeting this vegetative cover requirement. 10. West Brunswick Regional WWTP shall not be applied if the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot. 11. West Brunswick Regional WWTP shall not be applied if the vertical separation of bedrock and the depth of residuals application is less than one foot. Contact Brunswick County for a copy of the most recent residuals analysis and loading rates. WEST BRUNSWICK REGIONAL WWTP RECEIPT FORM I , (printed name) have received gallons/wet tons of the West Brunswick Regional WWTP Residuals, a copy of the West Brunswick Regional WWTP Residuals Product Information Sheet, and a copy of the most recent analysis of the product. I have read these documents and agree to adhere to the directions specified on the Application Information Sheet and the Product Information Sheet. Signature of Receiver Date of Receipt FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION) • BEAVER DAM CREEK WTP D. Program Information (BEAVER DAM CREEK -HIGHWAY 211 WTP RESIDUALS) • How the materials will be handled and transported from where the residuals were produced to where it will be treated. All residuals will remain at the WTP until ready for land application • How the residuals will be processed/treated (attach process flow diagram). (Attached at the end of this Section) • How leachate collection will be handled. Leachate will not be generated • Where the residuals will be stored until processed. (Same as Above) - All residuals will remain at the WTP until ready for land application • How the final product will be distributed (packaging, bulk, etc.) The final product will be land applied to private farm land • What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. One of the primary benefits of the WTP residuals, in addition to the hydraulic loading (irrigation capacity), will be its potential to be utilized as a liming amendment to adjust soil pH of receiver soils. The potential exists for the WTP residuals to react with the receiver soils and adjust soil pH's upward. Target pH of mineral soils is typically around 6.0 and most receiver soils will be below that target due to not receiving agricultural lime on an as needed basis. Therefore soil pH adjustment or soil neutralizing capability will be a potential benefit associated with the WTP residuals. • Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. Product Information Sheet and Application Information Sheet attached at the end of this Section • Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the D. Program Information (WTP RESIDUALS) Page 2 processed residual. The label or information sheet shall contain, at a minimum, the following information: • Name and address of the person who prepared the residual that is sold or given away. • A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. • A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. • A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. • Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b). • A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. Product Information Sheet and Application Information Sheet attached at the end of this Section i:•RYING BEu:: 3, HAZEN AND SAWYER CLEARWELL DRYING BED UNDERFLOW EXISTING ^ SLUDGE LAGOON CLEARWELL LAGOON DECANT p BACKWASH BACKWASH 1 FILTERFILTER Q� m p� p FILTER' ,FILTER .FILTER; BACKWASH EO f f UPFLOW AND SETTLING CONTACT BASIN:; .2' CLARIFIER BIN SLUDGE 1 PUMPS BIN RECYCLE MAINTENANCE P PPUMPS BLDG UPFLOW P ( P CONTACT - CLARIFIER T RAW WATER FM RECYCLE BRUNS FLOW METER } NC TO BEAVER DAM CREEK RECARBONATION TANK LAB/OFFICE BLDG FIGURE 1.2 BEAVER DAM CREEK WTP - PRODUCT INFORMATION SHEET Produced By Preparer Brunswick County - Beaver Dam Creek WTP Jeremy Sexton Southport, North Carolina Water Resources Superintendent Brunswick County Public Utilities Post Office Box 249 Bolivia, North Carolina 28422 For information on this product contact Brunswick County Public Utilities Jeremy Sexton, Water Resources Superintendent (910) 477-0918 The Class A Residual (Beaver Dam Creek WTP) is generated by treatment of potable water. The generated residuals are stable and contain a high calcium value for their application as a lime amendment. Beaver Dam Creek WTP is permitted for land application to farmland in accordance with Permit No. WQ0034468. Provisions for Application Application of Beaver Dam Creek WTP is prohibited except in accordance with the provisions specified in the Application Information Sheet. Application must conform to standards identified in Permit WQ0034468 and include but are not limited to: Setback Description Setback (feet) Liquid Cake Private or public water supply sources 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 100 25 Surface water diversions (ephemeral streams, waterways, ditches) 25 0 Groundwater lowering ditches (where the bottom intersects the SHWT) 25 0 Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 Application Information Sheet 1. Beaver Dam Creek WTP is intended for use as a liming amendment. Applications of Beaver Dam Creek WTP should be made in accordance with approved application standards and WQ0034468 permit conditions. 2. Beaver Dam Creek WTP shall not be applied to flooded, frozen, or snow covered areas. 3. Application and storage of Beaver Dam Creek WTP must be conducted in such a way as to prevent runoff from the application or storage site to any surface water. 4. Applications and loading rates of Beaver Dam Creek WTP shall be applied at rates that comply with realistic yield expectations based on the soil series and crops found at: http://nutrients.soil.ncsu.edu/yields . 5. Beaver Dam Creek WTP shall not be applied if the land fails to assimilate the material or the application causes the contravention of surface water or groundwater standards. 6. Beaver Dam Creek WTP shall not be applied within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-hour period following a residuals land application event. 7. Beaver Dam Creek WTP shall not be applied during a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period. 8. Beaver Dam Creek WTP shall not be applied if the slope is greater than 10% for surface applied material, or if the slope is greater than 18% for injected or incorporated material. 9. Beaver Dam Creek WTP shall not be applied if the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement. 10. Beaver Dam Creek WTP shall not be applied if the soil pH is not maintained at 6.0 or greater unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved variations to the acceptable soil pH (6.0) will be noted in the permit. 11. Beaver Dam Creek WTP shall not be applied if the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot. 12. Beaver Dam Creek WTP shall not be applied if the vertical separation of bedrock and the depth of residuals application is less than one foot. Contact Brunswick County for a copy of the most recent residuals analysis and loading rates. BEAVER DAM CREEK WTP RECEIPT FORM I (printed name) have received gallons/wet tons of the Beaver Dam Creek WTP Residuals, a copy of the Beaver Dam Creek WTP Residuals Product Information Sheet, and a copy of the most recent analysis of the product. I have read these documents and agree to adhere to the directions specified on the Application Information Sheet and the Product Information Sheet. Signature of Receiver Date of Receipt APPENDIX III RESIDUALS SOURCE CERTIFICATION APPLICATION FORM • NORTHEAST BRUNSWICK REGIONAL WWTP (FORM: RSC 06-16) State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16, FORM: DCAR 06-16, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 06-16): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Brunswick County Status a Code Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R Brunswick County Northeast Brunswick Regional WWTP Brunswick NCO086819 1,000 1,000 R Brunswick County West Brunswick Regional WWTP Brunswick NCO023693 1,000 11000 R Brunswick County Beaver Dam Creek WTP Brunswick NCO040061 3,500 3,500 'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Brunswick County — Northeast Brunswick Regional WWTP 2. Facility permit holder is: U Federal, 0 State, 0 Local Government, or 0 Private. Facility permit issued by: JE Div. of Water Resources, Div. of Environmental Health, or ❑I Other (explain: _). 3. Facility contact person and title: Tim Webb, Wastewater Superintendent Complete mailing address: Post Office Box 249 City: Bolivia State: N.C. Zip: 28422 Telephone number: (910) 253-2479 E-mail address: tim.webbgbnmswickcotmtync.gov 4. Facility physical address: 10480 Royster Road City: Navassa State: N.C. Zip: 28451 Coordinates: Latitude: 34' 16' 17" Longitude: 78° 00' 20" Datum: NAD 83 Level of accuracy: nearest second Method of measurement: MAP 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: <2 % industrial and >98 % domestic) other (explain: = ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: 2.45 MGD and facility average daily flow: 1.10 MGD 8. Average amount of residuals being generated at this facility 350 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: (2) Auto -Thermal Thermophilic Digestion Units, 50,000 gallons of treatment capacity Type and volume of residuals storage (i.e., outside of residuals treatment units): (2) Post-ATAD storage tanks with jet aeration, 375K gallons of storage II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 021.1102(6) as: Biological ❑ Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes FlI no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: EnviroChem and Date of analysis: 2/24/20 Passed corrosivity test: yes W no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes ❑ no. Flashpoint: >205 OF (> 140°F) Passed reactivity test: Eyes ao. HCN: 0.234 mg/kg (<250) & H2S: 1.75 mg/kg (<500) TCLP Parameter Limit (m917) Result (m91q) TCLP Parameter Limit (m917) Result (m917) Arsenic 5.0 <1.0 Hexachlorobenzene 0.13 <0.050 Barium 100.0 <1.0 Hexachloro-1,3-Butadiene 0.5 <0.050 Benzene 0.5 <0.04 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <1.0 Lead 5.0 <1.0 Carbon Tetrachloride 0.5 <0.04 Lindane 0.4 <0.0005 Chlordane 0.03 <0.02 Mercury 0.2 <0.0002 Chlorobenzene 100.0 <0.04 Methoxychlor 10.0 <0.0005 Chloroform 6.0 <0.04 Methyl Ethyl Ketone 200.0 0.24 Chromium 5.0 <1.0 Nitrobenzene 2.0 <0.050 m-Cresol 200.0 <0.050 Pentachlorophenol 100.0 <0.250 o-Cresol 200.0 <0.050 Pyridine 5.0 <0.050 p-Cresol 200.0 <0.050 Selenium 1.0 <1.0 Cresol 200.0 <0.050 Silver 5.0 <1.0 2,4-D 10.0 <0.0003 Tetrachloroethylene 0.7 <0.04 1,4-Dichlorobenzene 7.5 <0.050 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.04 Trichloroethylene 0.5 <0.04 1, 1 -Dichloroethylene 0.7 <0.04 2,4,5-Trichlorophenol 400.0 <0.050 2,4-Dinitrotoluene 0.13 <0.050 2,4,6-Trichlorophenol 2.0 <0.050 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 <0.0003 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.04 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: EnviroChem and Date of analysis: 2/24/20 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 10.5 Cadmium 85 39 <6.67 Copper 4,300 1,500 358 Lead 840 300 19.9 Mercury 57 17 1.10 Molybdenum 75 n/a 14.7 Nickel 420 420 44.2 Selenium 100 100 8.08 Zinc 7,500 2,800 1,840 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 3.69 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: EnviroChem and Date of analysis: 2/24/20 Parameter Result (mglkg) Aluminum 11,000 Ammonia -Nitrogen 57,900 Calcium 33,900 Magnesium 9,020 Nitrate -Nitrite Nitrogen 18.6 pH (Standard Unit) 7.56 Phosphorus 2,030 Potassium 32,100 Sodium 3,770 Total Kjeldahl Nitrogen 112,000 c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.90 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): JJ default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: _ e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1s) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 45,199 55,753 Inj ection/Incorporation 74,149 84,703 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): 14 Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. Q Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment. Q Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, 0 heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, F1 gamma ray irradiation, or I pasteurization. b. For Land Application of Class B. 71 Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, [� composting, or I lime stabilization. c. For Surface Disposal: TJ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. El Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. El Exempt -If Daily Cover Alternative is chosen in Item II.8. below [ 15A NCAC 02T.1106(a)(2)]. El Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). E] Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Q Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Q Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. E] Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. E] Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Q Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. Q Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. Q Alternative 10 [15A NCAC 02T. 1107(a)(10)] - Incorporation. Q Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. 0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 • NORTHEAST BRUNSWICK REGIONAL WWTP (FORM: RSC 06-16) (ATTACHMENTS) o VICINITY MAP o PROCESS FLOW DIAGRAM AND/OR NARRATIVE o QUANTITATIVE JUSTIFICATION o SAMPLING PLAN o ANALYTICAL AL . . . . . . . . . . . . . . . . . . . . . . . . It COUNTY OF BRUNSWICK PUBLIC UTILITIES DEPARTMENT Wastewater Treatment Division PO BOX 249 BOLIVIA. NC 28422 (910) 755-7921 (910) 755-7927 FAX Operational data for the Northeast Brunswick Regional WWTP (W00034468) Sludge Treatment for Pathogen and Vector Attraction Reduction The Northeast Brunswick Regional WWTP (NC0086819) utilizes the Kruger ATAD process for residuals treatment and stabilization of our bio-solids. Over the last vear our ATAD tanks 50.000 gallon each run at an average of 69.0 degrees Celsius while batch feeding approx. 5,000 gallon 3 times per week. With expansion of our facility we anticipate weekly operation to increase to 5 days a week. Upgrades to our thickened sludge transfer pumps will allow for more efficient operation and less time requirements on operations staff. In the most extreme "drop" in temperature we have went as low as 65.0 degrees Celsius for no more than 2 hours. At the average temperature we are operating we need approximately .43 hours to meet the time and temperature portion of the Class "A" requirements. Our process at the minimum stays at our above that temperature for 48-72 hours (we transfer to the ATAD every 2-3 days according to sludge generation- expansion of facility will decrease the "hold" time but these hours are well in excess of requirements). Our attached Fecal Density (and sludge analysis) show *s the pathogen reduction was met. We have also attached our 30-Day Bench Scale analysis for meeting the Vector Attraction Reduction (VAR). We have all the historical data trends on our SCADA server to show that time/temp was met although it would take a considerable amount of paper to print. The expanded system (2.75 MGD) will provide an additional 375.000 gallons of storage prior to disposal. In addition with existing capacity total storage will be increased to 59 days. With expansion the process will produce 498 dry tons of residuals at 2.75 MGD. Production for calendar year 2015 was 222 dry tons with a permitted capacity of 220 dry tons per year, disposal capacity will be increased as flow increases to facility. Residuals are land applied on Brunswick County permitted sites at a 1.5% to 2 % solid. If you would like to contact me for additional info I can be reached n (910) 755-7921 or by email: donald.dixonu;brunswickcountync. Uov Donald B. Dixon Wastewater Superintendent Brunswick County Public Utilities RESIDUALS SOURCE CERTIFICATION (RSC 06-16) QUANTITATIVE JUSTIFICATION NORTHEAST BRUNSWICK REGIONAL WWTP Annual Dry Tons (DT) Land Applied 2019 - Approximately 350 DT Currently Permitted —1,000 DT Proposed for Renewal —1,000 DT SAMPLING PLAN Northeast Brunswick Regional WWTP Non -Discharge Permit No. WQ0034468 LAND APPLICATION OF WWTP BIOSOLIDS Sampling and Monitoring Plan The Northeast Brunswick Regional WWTP Biosolids will be monitored to confirm compliance with conditions in Non -Discharge Permit No. WQ0034468 to include: • Toxicity Characteristics Leaching Procedure (TCLP), • Reactivity, Ignitability and Corrosivity, • 15A NCAC 02T .1105 Pollutant Limits and nutrient analysis (based on permitted monitoring frequency), • Pathogen Reduction requirements, • Vector Attraction Reduction requirements, • Annual Representative Soil Analysis of each field which receives land application during each respective year. • Any other applicable Permit conditions. Names and/or titles of personnel responsible for conducting the sampling and monitoring: • Brian Blanton All sampling and monitoring shall be performed in accordance with the current Permit. Pollutant concentrations in the Northeast Brunswick Regional Biosolids shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs) Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 Sampling and Monitoring Plan Brunswick County Northeast Brunswick Regional WWTP - Class A Biosolids Permit No. WQ0034468 The Northeast Brunswick Regional WWTP Class A Biosolids shall be analyzed to demonstrate it is non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed annually. TCLP shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dic (Oo r)ethylene pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachlor -1,3-butadiene Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) An analysis shall be conducted on the Northeast Brunswick Regional WWTP Class A Biosolids based on conditions (monitoring frequencies) set forth in Permit No. WQ0034468. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) 2 Sampling and Monitoring Plan Brunswick County Northeast Brunswick Regional WWTP - Class A Biosolids Permit No. WQ0034468 The Northeast Brunswick Regional WWTP Class A Biosolids shall be analyzed to demonstrate Pathogen Reduction requirements based on conditions (monitoring frequencies) set forth in Permit No. WQ0034468: Pathogen Reduction: Per 15A NCAC 02T.1106 For Distribution/Land Application of Class A Equivalent: ED A fecal coliform density that is demonstrated to be less than 1,000 MPN/gram of total dry solids - [15A NCAC 02T.1106(a)(2)(A)] And Alternative 5 [15A NCAC 02T. 1 106(a)(3)(E)] - Process to Further Reduce Pathogens (PFRP). M thermophilic aerobic digestion Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107 For Land Application of Class A WWTP Biosolids: Alternative 1 [15A NCAC 02T.1107(a)(1)] — 38-Percent Volatile Solids Reduction Or Alternative 3 [15A NCAC 02T.1107(a)(3)] — 30-Day Bench Scale Test (Aerobic Digestion) Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 11 - 2020 Class A Permit Renewal\Northeast Brunswick Regional WWTP\Sampling Plan - Northeast WWTP - October 2020.doc 3 BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 8, 2020 NE Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 3.69 % Solids 7.56 pH Parameter F- % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Tod (Mg/Kg x 0.002) Nitrogen (TKN) 11.200 112,000.000 224.000 Phosphorus 0.203 2,030.000 4.060 Potassium 3.210 32,100.000 64.200 PAN (injected)* 7.415 74,148.600 148.297 PAN (surface)* 4.520 45,198.600 90.397 Ammonia Nitrogen 5.790 57,900.000 115.800 Calcium 3.390 33,900.000 67.800 Calcium Carbonate Eq. --- --- Magnesium --- 9,020.000 18.040 Sodium --- 3,770.000 7.540 Sulfur --- ___ Nitrate N / Nitrite N --- 18.600 0.037 Barium --- ___ Chloride --- --- Iron --- -__ Aluminum --- 11,000.00 22.000 Arsenic --- 10.50 0.021 Cadmium --- 6.67 0.013 Chromium --- 70.50 0.141 Copper --- 358.00 0.716 Lead --- 19.90 0.040 Mercury --- 1.100 0.002 Molybdenum --- 14.70 0.029 Nickel --- 44.20 0.088 Selenium --- 8.08 0.016 Zinc --- 1,840.00 3.680 Envirochem: 2020-0043 8 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. SAR 0.90 Ceiling Concen. (Mg/Kg) 75 85 4,300 840 57 75 420 100 7,500 r Environmental Chemists, Inc. ! ! ! 6602 Windmill Way, Wilmington, NC 28405 9 910.392.0223 Lab b 910.392.4424 Fax 71.0 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab; Fax �M. 255-A Wilmington Highway, Jacksonville., NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infi-)ka enviranmentalcliemists.com Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Matthew Henry Report #: 2020-00438 Project ID: NEBR Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-01044 Site: Sludge 1/8/2020 9:00 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 8081B/3510 <0.02 mg/L 01/22/2020 Endrin (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/22/2020 Heptachlor (TCLP) SW 846 Method 80816/3510 <0.0005 mg/L 01/22/2020 Heptachlor epoxide (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/22/2020 Lindane (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/22/2020 Methoxychlor (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/22/2020 Toxaphene (TCLP) SW 846 Method 8081B/3510 <0.05 mg/L 01/22/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22l2020 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 o-Cresol (TCLP) SW 846 method 8270/3610 <0.050 mg/L 01/22/2020 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 01/22/2020 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/22/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0.0003 mg/L 01/23/2020 2,4-D (TCLP) SW846 Method 8151A <0.0003 mg/L 01/23/2020 1, 1 -Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Benzene (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Report #:, 2020-00438 Paae 1 of 4 envirocleM ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Matthew Henry Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ` 910.392.0223 Lab • 910.392.4424 Fax 710 Bo sertown Road, Manteca. NC 27954 ° 252.4735702 Lab/Fax 255 �A Wilmington Highway, Jacksonville, NC 28540 ° 91.0.347,5843 Lab/Fax info(, cnrironmentalchemists.com Date of Report: Feb 24, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-00438 Project ID: NEBR Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Chloroform (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 0.24 mg/L 01/15/2020 Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.04 mg/L 01/15/2020 RCI Cyanide EPA 335.4 0.234 mg/kg 01/13/2020 Sulfide SM 4500 S D 1.75 mg/kg 01/22/2020 Ignitability SW 846 method 1010 >205 °F 01/23/2020 pH SW 846 Method 9045D 7.56 units 01/20/2020 Sludge Residuals Aluminum EPA 200.7 11000 mg/kg 01/13/2020 Arsenic EPA 200.7 10.5 mg/kg 01/13/2020 Cadmium EPA 2007 <6.67 mg/kg 01/13/2020 Calcium EPA 200.7 33900 mg/kg 01/13/2020 Chromium EPA 200.7 70.5mg/kg 01/13/2020 Copper EPA 200.7 358 mg/kg 01/13/2020 Lead EPA 200.7 19.9mg/kg 01/13/2020 Magnesium EPA200.7 9020mg/kg 01/13/2020 Molybdenum EPA 200.7 14.7mg/kg 01/13/2020 Nickel EPA 200.7 44.2 mg/kg 01/13/2020 Potassium EPA 200.7 32100 mg/kg 01/13/2020 Selenium EPA 200.7 8.08 mg/kg 01/13/2020 Sodium EPA 200.7 3770 mg/kg 01/13/2020 Zinc EPA 200.7 1840 mg/kg 01/13/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 18.6 mg/kg 01/16/2020 Total Solids (%) SM 2540 B 3.69 % 01/10/2020 Ammonia Nitrogen SM 4500 NH3 C 57900 mg/kg 01/10/2020 Total Kjeldahl Nitrogen (TKN) SM45000rgB 112000mg/kg 01/10/2020 Report #;. 2020-00438 Page 2 of 4 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ` 910.392.0223 Lab • 910.392.4424 Fax (SM 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 'Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(«environmentalcheniists.com Brunswick County Public Utilities Date of Report: Feb 24, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Matthew Henry Report #: 2020-00438 Project ID: NEBR Total Phosphorus SM 4500 P F 2030 mg/kg 01/23/2020 Mercury SW846 74718 1.10 mg/kg 01/17/2020 TCLP Metals Arsenic EPA 200.7 <1.0mg/L 01/22/2020 Barium EPA 200.7 <1.0 mg/L 01/22/2020 Cadmium EPA 200.7 <1.0 mg/L 01/22/2020 Chromium EPA 200.7 <1.0mg/L 01/22/2020 Lead EPA 200.7 <1.0 mg/L 01/22/2020 Selenium EPA 200.7 <1.0mg/L 01/22/2020 Silver EPA 200.7 <1.0 mg/L 01/22/2020 Mercury EPA245.1 <0.0002 mg/L 01/24/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-01045 Site: #1 1/8/2020 9:01 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.50 % 01/10/2020 Fecal Density SM 9221C E MPN 24 hr 503 <515 MPN/g 01/08/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-01055 Site: #2 1/8/2020 9:02 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (%) SM 2540 B 3.73 % 01/10/2020 Fecal Density SM 9221C E MPN 24 hr 503 <483 MPN/g 01/08/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-01056 Site: #3 1/8/2020 9:03 AM Solid/Sludge Matthew Henry Test Method Results Date Analyzed Total Solids (°/o) SM 2540 B 3.48 % 01/10/2020 Fecal Density SM 9221 C E MPN 24 hr 503 <518 MPN/g 01/08/2020 Report #:. 2020-00438 Paae 3 of 4 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Matthew Henry Lab ID 20-01057 Test Sample ID: Site: #4 Total Solids (%) Fecal Density Lab ID Sample ID: 20-01058 Site: #5 Test Total Solids (%) Fecal Density Lab ID Sample ID: 20-01059 Site: #6 Test Total Solids (%) Fecal Density Lab ID Sample ID: 20-01060 Site: #7 Test Environmental Chemists, Inc. 6602 Windmill VVay, Wilmington, NC 28405 ' 910.392.0223 L.ab s 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Llighway jacksonviiie, NC 28540 ' 910.347.5843 Lab/Fax info.cienvironmentalchemists.ccm Date of Report: Feb 24, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-00438 Project ID: NEBR Collect Date/Time Matrix 1/8/2020 9:04 AM Solid/Sludge Method SM 2540 B SM 9221 C E MPN 24 hr 503 Collect Date/Time 1/8/2020 9:05 AM Method SM 2540 B SM 9221C E MPN 24 hr 503 Collect Date/Time 1/8/2020 9:06 AM Method SM 2540 B SM 9221C E MPN 24 hr 503 Method Collect Date/Time 1/8/2020 9:07 AM Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Comment: Sludge residuals reported on a dry weight basis. Reviewed b T Results Sampled by Matthew Henry Date Analyzed 3.52 % 01/10/2020 <512 MPN/g 01/08/2020 Matrix Sampled by Solid/Sludge Matthew Henry Results Date Analyzed 3.65 % 01/10/2020 <494MPN/g 01/08/2020 Matrix Sampled by Solid/Sludge Matthew Henry Results Date Analyzed 3.65 % 01/10/2020 <494 MPN/g 01/08/2020 Matrix Sampled by Solid/Sludge Matthew Henry Results Date Analyzed 3.61 % 01/10/2020 <499 MPN/g 01/08/2020 Report #:: 2020-00438 Paae 4 of 4 COUNTY OF BRUNSWICK �J�SWICKCpG�J West Brunswick Regional Laboratory Public Utilities Department m 235 Grey Water Road Wastewater Treatment Division Supply, NC 28462 rN��RA���� Phone: 910-755-7921 Fax: 910-755-7927 Sample Collection and Chain of Custody Collected By: Matthew Henry Report No.: A,& Sample Type: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludqe Other: Sample Identification Collection Sample Type Composite or Grab Container (Plastic or Glass) Chlorine mg/L LAB ID NUMBER PRESERVATION ANALYSIS REQUESTED DATE TIME TEMP NONE HCI H2SO4 I HNO3 THIO OTHER NEBR 17.8*C SL G P X TCLP/RCl/nutrientV /metals/residuals 1/8/2020 9:00 NEBR 1T8*C SL G P X fecal density 1/8/2020 9:01 NEBR 17.8*C SL.+ G P X fecal density 1/8/2020 9:02 NEBR 17.8*C SL G P I X fecal density 1/8/2020 9:03 NEBR 17.8*C SL G P X fecal density 1/8/2020 9:04 NEBR 17.8*C SL G P �� X fecal density 1/8/2020 9:05 NEBR 178*C . SL G P ` X fecal density 1/8/2020 9:06 NEBR 17.8*C SL G P X fecal density 1/8/2020 9:07 Transfer Relinquished By: Date/Time % ; feceiVed..�y. Date/Time 1777 -e F r' ." Temperature when Received: , Accepted: y Rejected: Resample Required: _ Delivered By / •*-�.... L Comments: f -L,,.� County of Brunswick Public Utilities West Brunswick Regional Facility Laboratory Norlh Carolina Laborataiv Certrteation Vunaber: NC:00903 Anna leRomx, Lab Supervisor PO Box 249 235 Grey Water Road Telepbone: 910-253-2896 anna.leroux(cDbrunswickcoun_ync qov Bolivia, NC 284?2 Supply, N(' 28462 Fax: 910-755-7927 Report Date: l 1-May-2020 EdUil Sample vn� dam le Da °e is"—Heaw Northeast Brunswick Thirty Day Bench Beginning: 4/8/2020 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 5/8/2020 as Required to Meet Option 3 2.01 % WWTP EPA 1503.33(b)(3)] PASS (End of Report) Certified by: k Anna IeRoux, Laboratory Supervisor Willcox & Mabe Soil Solutions, PLLC RESIDUAL PAN CALCULATION Northeast Brunswick Regional WWTP TKN= 112,000 mg/kg NH3= 57,900 mg/kg NO3-NO2-N= 18.6 mg/kg Min Rate= 0.30 PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO21 0.30 54,100 28,950 PAN= 45198.60 mg/kg 18.60 Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine the amount of PAN/DT remaining. 2ND YEAR RESIDUAL PAN PAN= [min.rate (1st year org. - N 2nd year min. - N] 0.15 54,100 16,230 PAN= 5680.50 mg/kg remaining from 1st year application 3RD YEAR RESIDUAL PAN PAN= [min.rate (2nd year org. - N 3rd year min. - N] 0.08 37,870 5,681 PAN= 2575.16 mg/kg remaining from 1st year application 4TH YEAR RESIDUAL PAN PAN= [min.rate (3rd year org. - N 4th year min. - N] 0.05 32,190 2,575 PAN= 1480.72 mg/kg remaining from 1 st year application 5TH YEAR RESIDUAL PAN PAN= [min.rate (4th year org. - N 5th year min. - N] 0.03 29,614 1,481 PAN= 817.84 mg/kg remaining from 1 st year application Residual PAN from years 2 thru 5 after the initial application = 10554.21 mg/kg Application Five Year Maximum Method First Year PAN Adjusted PAN (mg/kg) (mg/kg) Surface 45,199 55,753 Incorporation 74,149 84,703 NE - SAR SAR Calculation Na mg/I Ca mg/I Mg mg/I 139.113 1250.91 332.838 Na Ca Mg SAR 6.048 62.546 27.737 0.900 Na mil eq Ca mil eq Mg mil eq 6.048 62.546 27.737 Enter Enter .% TS 3.69 Data Na mg/kg 3770 Ca mg/kg 33900 Mg mg/kg 9020 Job Name: Northeast Brunswick Regional WWTP Page 2 APPENDIX IV RESIDUALS SOURCE CERTIFICATION APPLICATION FORM • WEST BRUNSWICK REGIONAL WWTP (FORM: RSC 06-16) State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16, FORM: DCAR 06-16, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 06-16): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Brunswick County Status a Code Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R Brunswick County Northeast Brunswick Regional WWTP Brunswick NCO086819 1,000 1,000 R Brunswick County West Brunswick Regional WWTP Brunswick NCO023693 1,000 11000 R Brunswick County Beaver Dam Creek WTP Brunswick NCO040061 3,500 3,500 'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 DWR State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Brunswick County — West Brunswick Regional WWTP 2. Facility permit holder is: Federal, 0 State, 0 Local Government, or 0 Private. Facility permit issued by: Div. of Water Resources, 17 Div. of Environmental Health, or Other (explain: _). 3. Facility contact person and title: Tim Webb, Wastewater Superintendent Complete mailing address: Post Office Box 249 City: Bolivia State: N.C. Zip: 28422 Telephone number: (910) 253-2479 E-mail address: tim.webbgbnmswickcountync.gov 4. Facility physical address: 250 Gray Water Road City: Supply State: N.C. Zip: 28462 Coordinates: Latitude: 33' 53' 38" Longitude: 78° 35' 25" Datum: NAD83 Level of accuracy: nearest second Method of measurement: MAP 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, rq treatment of potable water, treatment of 100% industrial wastewater, Ej treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: 6.0 MGD and facility average daily flow: 2.3 MGD 8. Average amount of residuals being generated at this facility 500 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: (2 23�gallons WAS storage tanks; (4) ATAD Tanks-274,000 gallons each, 1 ATAD Storage Tank — 450,000 gallons Type and volume of residuals storage (i.e., outside of residuals treatment units): Same as above II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 021.1102(6) as: Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: EnviroChem and Date of analysis: 4/13/20 Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes q no. Flashpoint: >180 °F (> 140°F) Passed reactivity test: Eyes [;Jno. HCN: 0.202 mg/kg (<250) & H2S: 2.50 mg/kg (<500) TCLP Parameter Limit (mgfi) Result (mgfi) TCLP Parameter Limit (mgfi) Result (mgfi) Arsenic 5.0 <1.0 Hexachlorobenzene 0.13 <0.050 Barium 100.0 <1.0 Hexachloro-1,3-Butadiene 0.5 <0.050 Benzene 0.5 <0.01 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <1.0 Lead 5.0 <1.0 Carbon Tetrachloride 0.5 <0.01 Lindane 0.4 <0.0005 Chlordane 0.03 <0.02 Mercury 0.2 <0.0002 Chlorobenzene 100.0 <0.01 Methoxychlor 10.0 <0.0005 Chloroform 6.0 <0.01 Methyl Ethyl Ketone 200.0 <0.05 Chromium 5.0 <1.0 Nitrobenzene 2.0 <0.050 m-Cresol 200.0 <0.050 Pentachlorophenol 100.0 <0.250 o-Cresol 200.0 <0.050 Pyridine 5.0 <0.050 p-Cresol 200.0 <0.050 Selenium 1.0 <1.0 Cresol 200.0 <0.050 Silver 5.0 <1.0 2,4-D 10.0 <0.003 Tetrachloroethylene 0.7 <0.01 1,4-Dichlorobenzene 7.5 <0.050 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.01 Trichloroethylene 0.5 <0.01 1, 1 -Dichloroethylene 0.7 <0.01 2,4,5-Trichlorophenol 400.0 <0.050 2,4-Dinitrotoluene 0.13 <0.050 2,4,6-Trichlorophenol 2.0 <0.050 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 <0.003 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.01 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: EnviroChem and Date of analysis: 4/13/20 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 10.2 Cadmium 85 39 <6.04 Copper 4,300 1,500 544 Lead 840 300 20.2 Mercury 57 17 1.50 Molybdenum 75 n/a 12.9 Nickel 420 420 23.5 Selenium 100 100 <6.04 Zinc 7,500 2,800 1,640 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory:_ and Date of analysis:. Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) T7 > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 4.12 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and nucronutnent parameters: Laboratory: EnviroChem and Date of analysis: 4/13/20 Parameter Result (mglkg) Aluminum 35,200 Alinnonia-Nitrogen 36,700 Calcium 24,300 Magnesium 4,270 Nitrate -Nitrite Nitrogen 108 pH (Standard Unit) 8.00 Phosphorus 72,500 Potassium 4,930 Sodium 2,180 Total Kjeldahl Nitrogen 65,200 c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.69 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): 0 default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: _ e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1s) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 27,008 32,568 Inj ection/Incorporation 45,358 50,918 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. q Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment. Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, 0 heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, ❑ gamma ray irradiation, or I pasteurization. b. For Land Application of Class B. El Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, air drying, 0 anaerobic digestion, composting, i I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt -If Daily Cover Alternative is chosen in Item II.8. below [ 15A NCAC 02T.1106(a)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: q Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). E] Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). a Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Q Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). E] Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. E] Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. E] Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Q Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. Q Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. Q Alternative 10 [15A NCAC 02T. 1107(a)(10)] - Incorporation. Q Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. g Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 • WEST BRUNSWICK REGIONAL WWTP (FORM: RSC 06-16) (ATTACHMENTS) o VICINITY MAP o PROCESS FLOW DIAGRAM AND/OR NARRATIVE o QUANTITATIVE JUSTIFICATION o SAMPLING PLAN o ANALYTICAL BRUNSWICK COUNTY PUBLIC UTILITIES OPERATIONS CENTER 250 GREY WATER ROAD NE SUPPLY, NORTH CAROLINA 28462 MAILING ADDRESS P. O. Box 249 BOLIVIA, NORTH CAROLINA 28422 TELEPHONE (910)253-2657 FAX (910)253-4305 Operational data for the West Brunswick Regional WRF (WQ0034468) Sludge Treatment for Pathogen and Vector Attraction Reduction The West Brunswick Regional WRF (WQ0023693) utilizes the Second Generation ATAD process for residuals treatment and stabilization of our biosolids. The facility has four (4) ATAD tanks and one (1) Storage Nitrification Denitrification Reactor. The ATAD's operated at an average temperature of 56 degrees Celsius while batch feeding approximately 7,000 gallons seven days/week. In the most extreme "drop" in temperature the ATAD's went as low as 53.0 degrees Celsius for no more than 2 hours. At the average operational temperature, the facility needs approximately 0.4 to 1.9 days to meet the time and temperature portion of the Class "A" requirements. Our process at minimum stays at or above the average temperature on a daily basis. The attached Fecal Density (and sludge analysis) shows the pathogen reduction was met. Also attached is our 30-day Bench Scale analysis for meeting the Vector Attraction Reduction (VAR). Production for calendar year 2019 was 581.66 dry tons with a permitted capacity of 1,000 dry tons per year. Residuals are land applied on Brunswick County permitted sites at 2.5% to 3.5 % solid. If you would like to contact me for additional information I can be reached at: 910-253-2479 or by email: tim.web bLc�brunswickcountync.pgov Tim Webb Wastewater Superintendent Brunswick County Public Utilities i RESIDUALS SOURCE CERTIFICATION (RSC 06-16) QUANTITATIVE JUSTIFICATION WEST BRUNSWICK REGIONAL WWTP Annual Dry Tons (DT) Land Applied 2019 - Approximately 582 DT Currently Permitted —1,000 DT Proposed for Renewal —1,000 DT SAMPLING PLAN West Brunswick Regional WWTP Non -Discharge Permit No. WQ0034468 LAND APPLICATION OF WWTP BIOSOLIDS Sampling and Monitoring Plan The West Brunswick Regional WWTP Biosolids will be monitored to confirm compliance with conditions in Non -Discharge Permit No. WQ0034468 to include: • Toxicity Characteristics Leaching Procedure (TCLP), • Reactivity, Ignitability and Corrosivity, • 15A NCAC 02T .1105 Pollutant Limits and nutrient analysis (based on permitted monitoring frequency), • Pathogen Reduction requirements, • Vector Attraction Reduction requirements, • Annual Representative Soil Analysis of each field which receives land application during each respective year. • Any other applicable Permit conditions. Names and/or titles of personnel responsible for conducting the sampling and monitoring: • Michael Garity All sampling and monitoring shall be performed in accordance with the current Permit. Pollutant concentrations in the West Brunswick Regional Biosolids shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs) Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 Sampling and Monitoring Plan Brunswick County West Brunswick Regional WWTP - Class A Biosolids Permit No. WQ0034468 The West Brunswick Regional WWTP Class A Biosolids shall be analyzed to demonstrate it is non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed annually. TCLP shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dichl0 o )ethylene pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro(-15)-butadiene Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) An analysis shall be conducted on the West Brunswick Regional WWTP Class A Biosolids based on conditions (monitoring frequencies) set forth in Permit No. WQ0034468. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) Sampling and Monitoring Plan Brunswick County West Brunswick Regional WWTP - Class A Biosolids Permit No. WQ0034468 The West Brunswick Regional WWTP Class A Biosolids shall be analyzed to demonstrate Pathogen Reduction requirements based on conditions (monitoring frequencies) set forth in Permit No. WQ0034468: Pathogen Reduction: Per 15A NCAC 02T.1106 For Distribution/Land Application of Class A Eguivalent: ®' A fecal coliform density that is demonstrated to be less than 1,000 MPN/gram of total dry solids - [I 5A NCAC 02T. 1 106(a)(2)(A)] And Z Alternative 5 [15A NCAC 02T.1106(a)(3)(E)] - Process to Further Reduce Pathogens (PFRP). 0thermophilic aerobic digestion Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107 For Land Application of Class A WWTP Biosolids: Alternative 1 [15A NCAC 02T.1107(a)(1)] — 38-Percent Volatile Solids Reduction Or ® Alternative 3 [15A NCAC 02T.1107(a)(3)] — 30-Day Bench Scale Test (Aerobic Digestion) Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 11 - 2020 Class A Permit Renewal\West Brunswick Regional WWTP\Sampling Plan - West WWTP - October 2020.doc 9 BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 11, 2020 West Brunswick Regional WWTP Permit No. WQ0034468 Mineralization Rate 0.30 4.12 % Solids 8.00 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 6.520 65,200.000 130.400 Phosphorus 7.250 72,500.000 145.000 Potassium 0.493 4,930.000 9.860 PAN (injected)* 4.536 45,358.000 90.716 PAN (surface)* 2.701 27,008.000 54.016 Ammonia Nitrogen 3.670 36,700.000 73.400 Calcium 2.430 24,300.000 48.600 Calcium Carbonate Eq. --- --- Magnesium --- 4,270.000 8.540 Sodium --- 2,180.000 4.360 Sulfur -__ ___ Nitrate N / Nitrite N --- 108.000 0.216 Barium --- --- SAR Chloride --- --- 0.69 Iron --- --- --- I Ceiling Concen. Aluminum --- 35,200.00 70.400 (Mg/Kg) Arsenic --- 10.20 0.020 75 Cadmium --- 6.04 0.012 85 Chromium --- 38.40 0.077 --- Copper --- 544.00 1.088 4,300 Lead --- 20.20 0.040 840 Mercury --- 1.500 0.003 57 Molybdenum --- 12.90 0.026 75 Nickel --- 23.50 0.047 420 Selenium --- 6.04 0.012 100 Zinc --- 1,640.00 3.280 7,500 Envirochem: 2020-04194 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Eenvirochem ANALYTICAL & CONSULTING CHEMISTS Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Environmental Chemists, Inc. 6602 Windmiil Wad,, Wilmington, NC 28405 * 910.392.0223 Lab - 910.392.4424 Fax 710 Bow•sertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 25.5-A Wilmington Highway, Jacksonville, NC 28540 s 910.347.5843 Lab/Fax info(i environmentalchemists.com Date of Report: Apr 13, 2020 Customer PO #: Customer ID: 08100011 Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: 20-10318 Site: Sludge Test Collect Date/Time 3/11/2020 12:10 PM Method Matrix Sampled by Solid/Sludge Brian Blanton Results Date Analyzed Chlordane (TCLP) SW 846 Method 8081B/3510 <0.02 mg/L 03/19/2020 Endrin (TCLP) SW 846 Method 80816/3510 <0.0005 mg/L 03/19/2020 Heptachlor (TCLP) SW 846 Method 8081 B/3510 <0.0005 mg/L 03/19/2020 Heptachlor epoxide (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 03/19/2020 Lindane (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 03/19/2020 Methoxychlor (TCLP) SW 846 Method 80811313510 <0.0005 mg/L 03/19/2020 Toxaphene (TCLP) SW 846 Method 80818/3510 <0.05 mg/L 03/19/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0,050 mg/L 03/20/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 03/20/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4-Dinitrotoluene (TCLP) SW 846 method 827013510 <0.050 mg/L 03/20/2020 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 03/20/2020 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 03/20/2020 2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 03/20/2020 1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Benzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Report #:. 2020-04194 Page 1 of 4 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 9:1.0.392.0223 Lab & 910,392.4424 Fax 710 Powsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, \C 28540 ® 910,347.5843 Lab; Fax infor"a environmerttalchemists.coni Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 03/25/2020 Tetrachloroethylene (TCLP) SW846 Method 8260/6030 <0.01 mg/L 03/25/2020 Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2020 RCI Cyanide EPA 335.4 0.202 mg/kg 03/18/2020 Sulfide SM 4500 S D 2.50 mg/kg 03/31/2020 Ignitability SW 846 method 1010 >180 OF 03/27/2020 Sludge Residuals Aluminum EPA 200.7 35200 mg/kg 03/16/2020 Arsenic EPA 200.7 10.2 mg/kg 03/12/2020 Cadmium EPA 200.7 <6.04 mg/kg 03/12/2020 Calcium EPA 200.7 24300 mg/kg 03/12/2020 Chromium EPA 200.7 38.4mg/kg 03/12/2020 Copper EPA 2003 544 mg/kg 03/12/2020 Lead EPA 200.7 20.2 mg/kg 03/12/2020 Magnesium EPA 200.7 4270 mg/kg 03/12/2020 Molybdenum EPA 200.7 12.9 mg/kg 03/12/2020 Nickel EPA 200.7 23.5 mg/kg 03/12/2020 Potassium EPA 2003 4930 mg/kg 03/12/2020 Selenium EPA 200.7 <6.04 mg/kg 03/12/2020 Sodium EPA 200.7 2180 mg/kg 03/12/2020 Zinc EPA 200.7 1640 mg/kg 03/12/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 108 mg/kg 03/23/2020 Total Solids (%) SM 2540 B 4.12 % 03/12/2020 pH SM 4500 H B 8.00 units 04/02/2020 Ammonia Nitrogen SM 4500 NH3 C 36700 mg/kg 03/15/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 65200 mg/kg 03/15/2020 Report #:: 2020-04194 Page 2 of 4 Environmental Chemists, Inc. 6602 VVindmilt Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax 710 Powsertown Road, Ma.nteo, NC 27954 * 252.473.5702 Lab/ Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info f�i,>cnvironnYentalclternists.conl Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Total Phosphorus SM 4500 P F 72500 mg/kg 03/27/2020 Mercury SW8467471B 1.50mg/kg 03/13/2020 TCLP Metals Arsenic EPA 2001 <1.0 mg/L 03/19/2020 Barium EPA 2003 <1.0 mg/L 03/19/2020 Cadmium EPA 2003 <1.0 mg/L 03/19/2020 Chromium EPA 200.7 <1.0 mg/L 03/19/2020 Lead EPA 200.7 <1.0 mg/L 03/19/2020 Selenium EPA200.7 <1.0mg/L 03/19/2020 Silver EPA 200.7 <1.0 mg/L 03/19/2020 Mercury EPA 245.1 <0.0002 mg/L 03/19/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10319 Site: 1 3/11/2020 12:01 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.20 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <43 MPN/g 03/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10321 Site: 2 3/11/2020 12:02 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.46 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <41 MPN/g 03/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10322 Site: 3 3/11/2020 12:03 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.52 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <40 MPN/g 03/11/2020 Report #:: 2020-04194 Page 3 of 4 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 91.0.392,0223 Lab • 910,392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 # 910.347.5843 Lab/Fax info(tieiivironnl.entalehemists.com Brunswick County Public Utilities Date of Report: Apr 13, 2020 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2020-04194 Project ID: West Brunswick Regional WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10323 Site: 4 3/11/2020 12:04 PM Solid/Sludge Brian Blanton Test _ Method Results Date Analyzed Total Solids (%) SM 2540 B 4.31 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <42 MPN/g 03/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10324 Site: 5 3/11/2020 12:05 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%} SM 2540 B 4.44 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <41 MPN/g 03/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10325 Site: 6 3/11/2020 12:06 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.49 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <41 MPN/g 03/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-10326 Site: 7 3/111/2020 12:07 PM Solid/Sludge Brian Blanton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 4.53 % 03/12/2020 Fecal Density SM 9221C E MPN 24 hr 503 <40 MPN/g 03/11/2020 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report #:: 2020-04194 Page 4 of 4 Environmental Chemist, Inc., Wilmington, NC Lab q94 602 Windmill Way .vilmington, VC 28405 10.392.0223 5ample Receipt Checklist Client: . + / _Date: 3 0 Report Number: Receipt of sample: Delivered YES '❑ y1 0 UPS ❑ FedEx C] Other ❑ lip YES l0 -I Were 1. Were custody seals present on the cooler? N/A 2. if custody seals were present, were the r Original temperature upon receipt k=,C Y ntact/unbroken? Haw temperature taken: ❑ Temperature i3lank ` orrected temperature upon receipt --_— 'C A Gun 10' Thomas Traceable S/N 192511657 against 8ott}es 0 YES ❑ No 3. If temperature of coolerexceeded 6 C Correction NOwas Project M rr, YES l❑ 4. Were proper custo I H /CL4 notified? YES [� y0 dV Procedures (relinquished/received) followed? 5• Were sample ID's listed on the COC? YES i❑ VO 6. 'Nere samples ID's listed on sample co YES ❑ NO 7. Were collentainers? YES ❑ ction date and time listed on the COC? NO 8. Were tests to be performed listed on the COC? 1 `S ❑ ,40 9. Did samples arrive in proper containers f YES '❑ y110. Did sam O p Of each test? l YES ❑ VO es arrive in good condition for each test? Es i� 11. Was adequate sample volume available?' Yi❑ wo 12. Were samples received within proper holding time for requested tests? (7 YES ❑ VO , 13. Were acid preserved samples received at a pH of <2? i ❑ YES 10 140 14. Were Cl '?ES ❑ Y0 cyanide samples received at a pH >12? 15. were sulfide samples received at a pH >97 ❑ YES ❑ 'VO 16. Were NH3/TKN/Phenol received at a chlorine restd ❑ YES ❑ '�O 17. Were Sulfide/Cyanide received at a chlorine residual of <0_S m/�? •• at of <0.5 m/L? ` TOCNolatifes are pH checked at time of analysis and recorded on the benchsheet. "* °acteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet I Sample Preservation: Must be completed for any samplesO n Sample(s) : correctl y preserved or with headspace) b adding •vere received incorrectly preserved and were adjusted accordingly Y g (circle one): -i,so Time of oreservation: a 1NO3 tCl NaOH f more than one preservative ;s needed, Note Notify customer service ;mmediatel notate in comet Y .or ncorrectly preserved samaies. r,btain a new ; enLS below 'Iotify the state 'ao it directed to analyzed h t ample or v he customer. ,vho was ^cc.�ed, d Volatiles Samole(s) f ate and time: vere received with headspace COMMENTS: ..4ri.uU ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way } Sample Collection and Chain of. Custody Wilmington, NC 28405 Phone; (910) 392-0223 Fax (910) 392.4424 rt No: 2.v, -- L4 C 9- Sample Type: I = Influent, E = Effluent, W =Well, ST =Stream, SO =Soil, SL= Sludge Other: a - PRESERVATION w Collection W „ •y= = c v = Sample Identification > n `o L it `o o -a w .� ^. O ANALYSIS REQUESTED a s o o a s a O O O w Q Z DATE TIME TEMP v x x = c WBR 1011 SL X TCLP, Nutrients, metals, RCI 3-h-1� G. WBR t©3 t SL C X FECAL DENSITY 1 G WBR SL C X FECAL DENSITY G WBR �-n-3 SL C X FECAL DENSITY - G WBR ail"3 SL C (�r-) _ X FECAL DENSITY 3-t�.2� i�,L G WBR SL C FECAL DENSITY WBR Lo -5 SL C P X FECAL DENSITY l- W13R SL C P X FECAL DENSITY G C P G G C P G G TRIANNUALS ----_ _-.— Transfer Relinquished By: Date/Time Received By: Date/Time 2. I emperature when deceived: Lt _ Accepted:. ✓ Rejected: Resample Requested: Delivere B Received By: G,I- - -If Date: i t ,- i ;L— Time: ,'� County of Brunswick Public Utilities West Brunswick Regional Facility Laboratory North Carolina Lzbomtoiy Cei-Iffleation Number: NC00903 Anna IcRoux, Lab SoNxvisor 130 Box 249 235 Grey Water Road Telephone: 910-253-2896 anna.leroux(ftfqn2Loiekcountync. ov Bolivia, NC 28422 Supply. NC2M62 Fax: 910-755-7927 Report Date: 29-Apr-2020 SamplLTU,& West Brunswick Thirty Day Bench Beginning.* 3/11/2020 Reduction of Vector Attraction (<15% is considered passing) Regional Digestor Scale Test Ending: 4/13/2020 as Required to Meet Option 3 4.19% WWTP EPA [503,33(b)(3)] PASS (End of Report) Certified by: r-- Anna IeRoux, Laboratory Supervisor Willcox & Mabe Soil Solutions, PLLC RESIDUAL PAN CALCULATION West Brunswick Regional WWTP TKN= 65,200 mg/kg NH3= 36,700 mg/kg NO3-NO2-N= 108.0 mg/kg Min Rate= 0.30 PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO21 0.30 28,500 18,350 108.00 PAN= 27008.00 mg/kg Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine the amount of PAN/DT remaining. 2ND YEAR RESIDUAL PAN PAN= [min.rate (1st year org. - N 2nd year min. - N] 0.15 28,500 8,550 PAN= 2992.50 mg/kg remaining from 1 st year application 3RD YEAR RESIDUAL PAN PAN= [min.rate (2nd year org. - N 3rd year min. - N] 0.08 19,950 2,993 PAN= 1356.60 mg/kg remaining from 1 st year application 4TH YEAR RESIDUAL PAN PAN= [min.rate (3rd year org. - N 4th year min. - N] 0.05 16,958 1,357 PAN= 780.05 mg/kg remaining from 1st year application 5TH YEAR RESIDUAL PAN PAN= [min.rate (4th year org. - N 5th year min. - N] 0.03 15,601 780 PAN= 430.84 mg/kg remaining from 1 st year application Residual PAN from years 2 thru 5 after the initial application = 5559.98 mg/kg Application Five Year Maximum Method First Year PAN Adjusted PAN (mg/kg) (mg/kg) Surface 27,008 32,568 Incorporation 45,358 50,918 WEST-SAR SAR Calculation Na mg/I Ca mg/I Mg mg/I 89.816 1001.16 175.924 Na Ca Mg SAR 3.905 50.058 14.660 0.686 Na mil eq Ca mil eq Mg mil eq 3.905 50.058 14.660 Enter Enter .% TS 4.12 Data Na mg/kg 2180 Ca mg/kg 24300 Mg mg/kg 4270 Job Name: West Brunswick Regional WWTP Page 4 APPENDIX V RESIDUALS SOURCE CERTIFICATION APPLICATION FORM • BEAVER DAM CREEK WTP (FORM: RSC 06-16) State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Brunswick County Status Code' Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R Brunswick County Northeast Brunswick Regional WWTP Brunswick NCO086819 1,000 1,000 R Brunswick County West Brunswick Regional WWTP Brunswick NCO023693 1,000 1,000 R Brunswick County Beaver Dam Creek WTP Brunswick NCO040061 3,500 3,500 'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Beaver Dam Creek WTP 2. Facility permit holder is: F,1 Federal, 0 State, 0 Local Government, or 0 Private. Facility permit issued by: Q Div. of Water Resources, Div. of Environmental Health, or Other (explain: _). 3. Facility contact person and title: Jeremy Sexton Complete mailing address: Post Office Box 249 City: Bolivia State: N.C. Zip: 28422 Telephone number: (910) 477-0918 E-mail address: jeremy.sextongbrunswickcountync.gov 4. Facility physical address: 4305 Southport -Supply Road City: Southport State: N.C. Zip: 26461 Coordinates: Latitude: 33' 57' 35.47" Longitude: 78, 04' 55.55" Datum: NAD83 Level of accuracy: nearest hundredth of second Method of measurement: ADD 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: = ). 6. Does the facility have an approved pretreatment program: Yes ® No (WTP) 7. Facility permitted/design flow: 6.0 MGD and facility average daily flow: 1.83 MGD 8. Average amount of residuals being generated at this facility 3.500 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: N/A - WTP Type and volume of residuals storage (i.e., outside of residuals treatment units): Drying Beds & Lagoon-Approx. 30 Days II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or ® 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 77 Non -Biological (WTP) Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes FlI no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Environmental Chemists, Inc. and Date of analysis: March 4, 2016 Passed corrosivity test: yes T9 no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes ❑ no. Flashpoint: = OF (> 140°F) Passed reactivity test: Eyes ao. HCN: <0.123 mg/kg (<250) & H2S: <0.247 mg/kg (<500) TCLP Parameter Limit (m917) Result (m917) TCLP Parameter Limit (m917) Result (m917) Arsenic 5.0 <1.0 Hexachlorobenzene 0.13 <0.050 Barium 100.0 <1.0 Hexachloro-1,3-Butadiene 0.5 <0.050 Benzene 0.5 <0.01 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <1.0 Lead 5.0 <1.0 Carbon Tetrachloride 0.5 <0.01 Lindane 0.4 <0.0005 Chlordane 0.03 <0.05 Mercury 0.2 <0.0020 Chlorobenzene 100.0 <0.01 Methoxychlor 10.0 <0.0005 Chloroform 6.0 <0.01 Methyl Ethyl Ketone 200.0 <0.05 Chromium 5.0 <1.0 Nitrobenzene 2.0 <0.050 m-Cresol 200.0 <0.050 Pentachlorophenol 100.0 <0.250 o-Cresol 200.0 <0.050 Pyridine 5.0 <0.050 p-Cresol 200.0 <0.050 Selenium 1.0 <1.0 Cresol 200.0 <0.050 Silver 5.0 <1.0 2,4-D 10.0 <0.050 Tetrachloroethylene 0.7 <0.01 1,4-Dichlorobenzene 7.5 <0.050 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.01 Trichloroethylene 0.5 <0.01 1, 1 -Dichloroethylene 0.7 <0.01 2,4,5-Trichlorophenol 400.0 <0.050 2,4-Dinitrotoluene 0.13 <0.050 2,4,6-Trichlorophenol 2.0 <0.050 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 <0.003 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.01 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Environmental Chemists, Inc. and Date of analysis: 10/8/20 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 3.34 Cadmium 85 39 <3.12 Copper 4,300 1,500 4.66 Lead 840 300 5.58 Mercury 57 17 <0.101 Molybdenum 75 n/a <3.12 Nickel 420 420 <3.12 Selenium 100 100 <3.12 Zinc 7,500 2,800 5.04 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 15.4 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Environmental Chemists. Inc. and Date of analysis: 10/8/20 Parameter Result (mglkg) Aluminum 707 Ammonia -Nitrogen 96.8 Calcium 513,000 Magnesium 1,570 Nitrate -Nitrite Nitrogen 1.16 pH (Standard Unit) 8.27 Phosphorus 593 Potassium <156 Sodium 408 Total Kjeldahl Nitrogen 453 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.06 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This rate is a (check one): JJ default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: _ e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1s) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 121 176 Inj ection/Incorporation 169 224 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: _ FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): 14 Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. Q Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment. Q Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. q Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. El Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, 0 heat drying, heat treatment, thermophilic aerobic digestion, beta ray irradiation, F1 gamma ray irradiation, or I pasteurization. b. For Land Application of Class B. 71 Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, [� composting, or I lime stabilization. c. For Surface Disposal: TJ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. El Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. El Exempt -If Daily Cover Alternative is chosen in Item II.8. below [ 15A NCAC 02T.1106(a)(2)]. El Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). E] Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Q Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Q Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Q Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. E] Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. E] Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Q Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. Q Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. Q Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 • BEAVER DAM CREEK WTP (FORM: RSC 06-16) (ATTACHMENTS) o VICINITY MAP o PROCESS FLOW DIAGRAM AND/OR NARRATIVE o QUANTITATIVE JUSTIFICATION o SAMPLING PLAN o ANALYTICAL c _ � J q ai t 'Yh r ))I IR C7 AM al ksJOS �4 t r t , 4s" #y" F � ,s /• �, Y �j xl l.+n 7 cr yt i -. 711E v- N �..•��f n:di- ry E �}-YC�yE fi 'Pv if � � � / '�£,i' eT I � r�,4 � ,pr, y^ l •'t 1F � S}�S � Y� � P ��p f� �1 .�. -. ._• at• �' t�� � _ �� �����i �r 'J r�,� �'j S•F� {'.�Lw 7 7L1'. � i �' rM Or-t'.... � 1 a �lC'd}•%iS "�3� �1{ X �'YF�lt a[rn"+++'""�il... {+ ,� ��' +� � �`�'.� 'E, b ��?r�"" e:.,.-f ,• r�>i � , ��N'i1�� ' �- �"', mac+ n;°�}!Zr. � J"'Y i 'isr�' §�xx'�. •,•�+iP��. w� t f„�,`'��'�' �,,be '�r'':-c,�r•nnk`.J C �rf�:+`1 �NY{�.,` AW W L U ^L `W w� /W W t CLEARWELL DRYING BED UNDERFLOW EXISTING SLUDGE LAGOON CLEARWELL LAGOON DECANT P BACKWASH BACKWASH j FILTER FILTER Off, a� p FILTER FILTER FILTER )RYING BEo 1 BACKWASH EO } I AND SETTLING BASIN!, i 2' BW SLUDGE PUMPS BW RECYCLE P P ! PUMPS I. P HAZEN AND SAWYER Em.--" 60— i s....me 1 f —FM FLOW METER } TO BEAVER DAM CREEK RECYCLE RECAR13ONATION TANK UPFLOW CONTACT CLARIFIER j LAB/OFFICE BLDG MAINTENANCE BLDG UPFLOW CONTACT CLARIFIER RAW WATER FIGURE 1.2 RESIDUALS SOURCE CERTIFICATION (RSC 06-16) QUANTITATIVE JUSTIFICATION BEAVER DAM CREEK - HIGHWAY 211 WTP Currently Permitted — 3,500 DT Proposed for Renewal — 3,500 DT SAMPLING PLAN Beaver Dam Creek — Highway 211 WTP Non -Discharge Permit No. WQ0034468 LAND APPLICATION OF WTP RESIDUALS Sampling and Monitoring Plan The Beaver Dam Creek — Highway 211 WTP Residuals will be monitored to confirm compliance with conditions in Non -Discharge Permit No. WQ0034468 to include: • Toxicity Characteristics Leaching Procedure (TCLP) (For initial Permit Application), • Reactivity, Ignitability and Corrosivity (For initial Permit Application), • 15A NCAC 02T .l 105 Pollutant Limits and nutrient analysis (based on permitted monitoring frequency), • Pathogen Reduction requirements (For initial Permit Application), • Annual Representative Soil Analysis of each field which receives land application during each respective year. • Any other applicable Permit conditions. Names and/or titles of personnel responsible for conducting the sampling and monitoring: • Jeremy Sexton All sampling and monitoring shall be performed in accordance with the current Permit. Pollutant concentrations in the Beaver Dam Creek WTPA Residuals shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs) Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 Sampling and Monitoring Plan Beaver Dam Creek WTP - Class A Residuals Brunswick County Permit No. WQ0034468 The Beaver Dam Creek WTP Class A Residuals shall be analyzed to demonstrate it is non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed for the initial permit application. TCLP shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-DichlOo pyridine (5.0) )ethylene Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro(-1,3-butadiene Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) An analysis shall be conducted on the Beaver Dam Creek WTP Class A Residuals based on conditions (monitoring frequencies) set forth in Permit No. WQ0034468. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) Sampling and Monitoring Plan Beaver Dam Creek WTP - Class A Residuals Brunswick County Permit No. WQ0034468 The Beaver Dam Creek WTP Class A Residuals shall be analyzed to demonstrate Pathogen Reduction requirements for the initial permit application: Pathogen Reduction: Per 15A NCAC 02T.1106 For Distribution/Land Application of Class A Equivalent: t A fecal coliform density that is demonstrated to be less than 1,000 MPN/gram of total dry solids (Non -Biological Residuals are not required to meet an additional Alternative Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107 For Distribution/Land Application of Class A Equivalent: Not Applicable — Non -Biological Residuals with NO Domestic Wastewater Contribution Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 11 - 2020 Class A Permit Renewal\Beaver Dam Creek WTP\Sampling Plan - Highway 211 WTP - October 2020.doc 3 BRUNSWICK COUNTY LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Water Treatment Plant Date Sampled: September 23, 2020 Beaver Dam Creek WTP Permit No. WQ0034468 Mineralization Rate 0.20 15.40 % Solids 8.27 pH Parameter % Mg/Kg Dry Weight (% x '10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 0.045 453.000 0.906 Phosphorus 0.059 593.000 1.186 Potassium 0.016 156.000 0.312 PAN (injected)* 0.017 169.200 0.338 PAN (surface)* 0.012 120.800 0.242 Ammonia Nitrogen 0.010 96.800 0.194 Calcium 51.300 513,000.000 1,026.000 Calcium Carbonate Eq. --- --_ Magnesium --- 1,570.000 3.140 Sodium --- 408.000 0.816 Sulfur --- --_ Nitrate N / Nitrite N --- 1.160 0.002 Barium --- --- SAR Chloride --- --- 0.06 Iron --- --- --- Ceiling Concen. Aluminum --- 707.00 1.414 (Mg/Kg) Arsenic --- 3.34 0.007 75 Cadmium --- 3.12 0.006 85 Chromium --- 3.12 0.006 --- Copper --- 4.66 0.009 4,300 Lead --- 5.58 0.011 840 Mercury --- 0.101 0.000 57 Molybdenum --- 3.12 0.006 75 Nickel --- 3.12 0.006 420 Selenium --- 3.12 0.006 100 Zinc --- 5.04 0.010 7,500 Envirochem: 2020-16318 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. ren7viirochem 6 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ` 910.347.5843 Lab/Fax info@environmentalchemists.com Brunswick County Public Utilities Date of Report: Oct 08, 2020 Post Office Box 249 Customer PO #: JS092220A Bolivia NC 28422 Customer ID: 08100011 Attention: Jeremy Sexton Report #: 2020-16318 Project ID: 211 WTP Lime Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-41789 Site: Sludge - 001 9/23/2020 10:30 AM Solid/Sludge Client Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 707 mg/kg 09/30/2020 Arsenic EPA 200.7 3.34 mg/kg 09/30/2020 Cadmium EPA 200.7 <3.12 mg/kg 09/30/2020 Calcium EPA 200.7 513000 mg/kg 10/05/2020 Chromium EPA 200.7 <3.12 mg/kg 09/30/2020 Copper EPA 200.7 4.66 mg/kg 09/30/2020 Lead EPA 200.7 5.58 mg/kg 09/30/2020 Magnesium EPA 200.7 1570 mg/kg 09/30/2020 Molybdenum EPA 200.7 <3.12 mg/kg 09/30/2020 Nickel EPA 200.7 <3.12mg/kg 09/30/2020 Potassium EPA 200.7 <156 mg/kg 09/30/2020 Selenium EPA 200.7 <3.12mg/kg 10/05/2020 Sodium EPA 200.7 408mg/kg 09/30/2020 Zinc EPA 200.7 5.04 mg/kg 09/30/2020 Nitrate+ Nitrite-N itrogen EPA 353.2 1.16 mg/kg 09/28/2020 Total Solids (%) SM 2540 B 15.4 % 09/25/2020 pH SM 4500 H B 8.27 units 10/06/2020 Ammonia Nitrogen SM 4500 NH3 C 96.8 mg/kg 09/26/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 org B 453 mg/kg 09/26/2020 Total Phosphorus SM 4500 P F 593 mg/kg 10/01 /2020 Mercury SW846 7471 B <0.101 mg/kg 09/30/2020 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 10/05/2020 Barium EPA 200 7 <1.0 mg/L 10/05/2020 Cadmium EPA 2007 <1.0 mg/L 10/05/2020 Report # 2020-16318 Page 1 of 2 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Brunswick County Public Utilities Date of Report: Oct 08, 2020 Post Office Box 249 Customer PO #: JS092220A Bolivia NC 28422 Customer ID: 08100011 Attention: Jeremy Sexton Report #: 2020-16318 Project ID: 211 WTP Lime Sludge Chromium EPA 200 7 <1.0 mg/L 10/05/2020 Lead EPA 200.7 <1.0 mg/L 10/05/2020 Selenium EPA 200.7 <1.0 mg/L 10/05/2020 Silver EPA 200.7 <1.0 mg/L 10/05/2020 Mercury EPA 245.1 <0.0002 mg/L 10/07/2020 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by:Rkia"ow-OL Report # 2020-16318 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 710.392.0 L.�J Sample Receipt Checklist Client: 60,P Lk. Date: '1 z o0 Report Number:o� ^---:— -r - -'-- -r, — ucuvere❑ UPS U FedEx ❑ Other ❑ ❑ YES EONO N/A 1,Were custody seals present on the cooler? O N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt , °C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES 10 NO 13. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified? IZ YES 10 NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COO YES 10 NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? 1 CA YES 10 NO 9. Did samples arrive in proper containers for each test? 14 YES O NO 10, Did samples arrive in good condition for each test? YES 10 NO 11. Was adequate sample volume available?` IV YES ❑ NO 12. Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES 10 NO 14. Were cyanide samples received at a pH >12? ❑ YES ID NO 15. Were sulfide samples received at a pH >9? ❑ ❑ r-1 YES YES vrc I ❑ ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? evn r— -- ,-- - 1— VVC1C V, L„uN,1LJ,Nndie sdmpres Turereo inthe field within 15 minutes? I * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. * * Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H-SO, HNO, HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: __ DOC. QA.002 WAHMMM Analytical & Consulting Chemists Lv I .rP ADDS: 130,S -S a Sampled By• ENVIRONMENTAL CHEMISTS INC6602Windmill WayWilmington, NC2840 NCDENR: OWQ CERTIFICATION # 94 NCDIiHS: DLS CERTIFICATION # 37729 OFFICE: 910-392-0223 FAX 910-39244246 Info COLLECTION AND CHAIN OF CUSTODY i�environmentalchernista.com PROJECT NAME: .-Z )) ?U t�rr�e St REPORT NO: f� CONTACT NAME: � REPORT TO: i PO NO: �j 07.2.7.2t tv'C vY,� �j� �� COPY TO: P-IONOFAX: Collection .....v.■. �r g SPK i SAMPLE TYPE: I = Influent, E = Eftluen W w`el $ >; Well, ST =< Stream, SO Sample Identification a a '' E _ ceJSp a = Soil, PRESERVATION SL = Slud e, Other: O L E p = n W Date Time Tem p C,n. Z v v` v a i i= J 2 K N z w ANALYSIS REQUESTED v to W t4 19. C P� = z o e G z q17� r�•3plq. __-- G, z y ��90 C P ✓ieo q G G C P G G C P G G C P G G C P G G C P NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol end Ba G G Transfer ctsrta must be dechlorinated m 1 • — �re�vti., Relinquished B : ppm or less) In the fleid at Date/Time the time of collection, See reverse for instructions z• Rec 'ved B �+ DatelTime Temperature when Received 'C: Delivered By: Accepted: Re' ted• Comments: eel Received By: Resa e R quested: Co, Date: w. ,c/G . vj/ Time: TURNAROUND: ANALYTICAL FROM INITIAL PERMITTING OF SOURCE POO'"-* Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910:392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@cnvironmentalchemists.com Brunswick County Public Utilities Date of Report: Mar 04, 2016 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Jeremy Sexton Report #: 2016-01515 Project ID: 211 Water Plant Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-03550 Site: Sludge 2/4/2016 9:45 AM Solid/Sludge Jeremy Sexton Test Method Results Date Analyzed Chlordane SW 646 Method 8081B/3510 <0.05 mg/L 02/16/2016 Endrin SW 846 Method 8081B13510 <0.0005 mg/L 02116/2016 Heptachlor SW 846 Method 8081 B1351 0 <0.0005 mq/L 02/16/2016 Heptachlor epoxide SW 846 Method 8081B13510 <0,0005 mg/L 02/16/2016 Lindane SW 846 Method 8081B13510 <0.0005 mg/L 02/16/2016 Methoxychlor SW 846 Method 8081B/3510 <0,0005 mg/L 02/16/2016 Toxaphene SW B46 Method 8081B/3510 <0.05 mg/L 02/16/2016 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mq/L 02/12/2016 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 02/1212016 2,4,6-Trichlorophenol (TCLP) SW 846 method $270/3510 <0.050 mg/L 02/12/2016 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 02/12/2016 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mq/L 02/12/2016 Hexachloro-1,3-butadiene (TCLP) SW 846 method 827013510 <0,050 mg/L 02/1212016 Hexachlorobenzene (TCLP) SW 846 method 827013510 <0,050 mg/L 02/12/2016 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 02/12/2016 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 02/1212016 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 02/12/2016 o-Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 02/12/2016 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 02/12/2016 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 02/12/2016 2,4,5-TP SW846 Method 8151A <0.003 mq/L 02/15/2016 2,4-D SW846 Method 8151A <0.003 mq/L 02115/2016 1,1-Dichloroethylene SW846 Method 826015030 <0.01 mg/L 02/19/2016 1,2-Dichloroethane SW846 Method 826o15030 <0.01 mg/L 02/19/2016 Benzene SW846 Method8260/5030 <0.01 mg/L 02/19/2016 Carbon Tetrachloride SW846 Method826015030 <0.01mg/L 02/19/2016 Report #:: 2016-01515 Page 1 of 4 enviroChF00,10---71 SM ANALYTICAL& CONSULTING CHEMISTS Brunswick County Public. Utilities Post Office Box 249 Bolivia NC 28422 Attention: Jeremy Sexton Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Mar 04, 2016 Customer PO M Customer ID: 08100011 Report M 2016-01515 Project ID: 211 Water Plant Chlorobenzene SW846 Method 8260/5030 <0.01 mg/L Chloroform SW846 Method B26016030 <0.01 mg/L Methyl ethyl ketone SW846 Method 826015030 <0.05 mg/L Tetrachloroethylene SW845 Method 8260/5030 <0.01 mg/L Trichloroethylene SW846 Method 82601BD30 <0.01 mg/L Vinyl Chloride SW846 Method 820015030 <0.01 mg/L RC I Cyanide EPA335.4 < 0.123 mg/kg pH SM4500 H B 10.6 units Sulfide SM 4500 s o <0.247 mg/kg Ignitability SW 846 method 1010 >212 °F Sludge Residuals inum EPA 200.7 619 mg/kg Arsenic EPA200.7 <29.2 mg/kg Cadmium EPA 200.7 <29.2 m g/kg Calcium EPA 200.7 350000 mg/kg Chromium EPA 200.7 <29.2 Copper PA 200.7 < mg/kg Lead EPA '12tT.2 <29.2 mg/kg Magnesium EPA2D0.7 2970 mg/kg Molybdenum EPA,2o0.7 . ow �,, <29.2 mg/kg �� .:max Nickel EPA 200.7 <29.2 mg/kg Potassium EPA 20D• 7 155 mg/kg Selenium EP o.7 <29.2 mglkg Sodium EPA2Do.7 6 mg/kg Zinc EPA 200.7 <29. /kg Total Kieldahl Nit r n (TKN) EPA351.2 436 mg/ _ Nitrate+Nitri itrogen EPA353.2 7.96 mg/kg Total S s (%) SM 2540 B 1.68 % A nia Nitrogen SM 4500 NH3 c 530 mg/kg 02/19/2016 02/19/2016 02/19/2016 02/19/2016 02/19/2016 02/19/2016 02/11/2016 02/16/2016 02/10/2016 02/11/2016 02/10/2016 02/111 ll 1/2016 02/10/2016 02/11/2016 02/11/2016 02/11/2016 02/10/2016 02/11/2016 0Yf"I'I/GU 10��M► 02/15/2016 02/11/2016 02/10/2016 02/11/2016 02/16/2016 /11/2016 02/0 6 02/05/2016 Report #:: 2016-01515 Page 2 of 4 enviroChem SM ANALYTICAL & CONSULTING CHEMISTS r- 7-7 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentatchemists.com Brunswick County Public Utilities Date of Report: Mar 04, 2016 Post Office Box 249 Customer PO M Bolivia NC 28422 Customer ID: 08100011 Attention: Jeremy Sexton Report #: 2016-01515 Project ID: 211 Water Plant TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 02/16/2016 Barium EPA 200.7 <1.0 mg/L 02/16/2016 Cadmium EPA 200.7 <1.0mg/L 02/16/2016 Chromium EPA 200.7 <1.0mg/L 02/16/2016 Lead EPA 200.7 <1.0 mg/L 02/16/2016 Selenium EPA 200.7 <1.0mg/L 02/16/2016 Silver EPA 200.7 <1.0mg/L 02/16/2016 Mercury EPA245.1 <0.0020mg/L 02/19/2016 Lab ID Sample ID: 16-03551 Site:1 Test Total Solids (%) Fecal Density Collect Date/Time 2/4/2016 9:50 AM Method SM 2540 B SM 9221C E MPN 24 hr 503 Matrix Sampled by Solid/Sludge Jeremy Sexton Results Date Analyzed 3.58 % 02/05/2016 <56 MPN/g 02/05/2016 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-03552 Site: 2 2/4/2016 9:54 AM Solid/Sludge Jeremy Sexton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.46 % 02/05/2016 Fecal Density SM 9221C E MPN 24 hr 503 <82 MPN/g 02/05/2016 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-03553 Site: 3 2/4/2016 9:58 AM Solid/Sludge Jeremy Sexton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.67 % 02/05/2016 Fecal Density SM 9221C E MPN 24 hr 503 <75 MPN/g 02/05/2016 Report #:: 2016-01515 Page 3 of 4 F77 C virochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 , 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@cnvironmentalchemists.com Brunswick County Public Utilities Date of Report: Mar 04, 2016 Post Office Box 249 Customer PO 9: Bolivia NC 28422 Customer ID: 08100011 Attention: Jeremy Sexton Report #• 2016-01515 Project ID: 211 Water Plant Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-03554 Site: 4 2/4/2016 10:06 AM Solid/Sludge Jeremy Sexton Test Method Results Date Analyzed Total Solids SM 2540 B 2.55 % 02/05/2016 Fecal Density SM 9221C E MPN 24 hr 503 <79 MPN/q 02/05/2016 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-03555 Site: 5 2/4/2016 10:21 AM Solid/Sludge Jeremy Sexton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.95 % 02/05/2016 Fecal Density SM 9221C E MPN 24 hr 503 <68 MPN/q 02/05/2016 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-03556 Site: 6 2/4/2016 10:28 AM Solid/Sludge Jeremy Sexton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.36 % 02/05/2016 Fecal Density SM 9221C E MPN 24 hr 503 <85 MPN/q 02/05/2016 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-03557 Site: 7 2/4/2016 10:37 AM Solid/Sludge Jeremy Sexton Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.78 % 02/05/2016 Fecal Density SM 9221C E MPN 24 hr503 <113 MPN/g 02/05/2016 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report #:: 2016.01515 Page 4 of 4 -., ENVIRONMENTAL CHEMISTS, IN C OFFICE: 9101392-D 23l mingtonFAX 910-39244245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: US CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: BCPU- 211 Water Plant PROJECT NAME: WTP Sludge REPORT NO: 1 ADDRESS:CONTACT NAME: Jeremy Sexton, ORC PO NO: f y / REPORT TO: r' PHONEI /�-ys7- 9/B„3 COPY TO: ado✓ email: Sampled By:__,5{ C`Q v+'k rj 5_e ,•�-�-Y1 SAMPLE TYPE: I = Influent. E = Effluent- W = Well_ ST c ; rpnm Srl = Snil GI = Cl1irinn n+r,o�- Sample Identification Collection N m a (D .0 ° 2 E° U U _ U a E E U m J Z PRESERVATION ANALYSIS REQUESTED Date Time Temp z to Z 2 = 0 o T o s 2 F_ w ti o Sludge 01 • y 7. 3 SL C P 3 �5 X Full TCLP, RCI, Nut/metals 1) ' /G 4/ .' 0, SL C P ��5 Fecal Density/% TS 2) 2/ 17: r Y SL C P Fecal Density/% TS a 3) t ? . SL 3 Fecal Density/% TS 4) / ? . SL C P [ J Fecal Density/% TS 5) 6) 7 0. 3 r 2. t 7, SL SL SL z 3 ✓� 1!;� Fecal Density/% TS Fecal Density/% TS Fecal Densit /% TS QP C Q' P 212111k, 14 .' C 1" P a) a C P (Lo I r_G> _L Transfer Relinquished By: Date/Time Received By: Date/Time 2. IwuFNGlawlG wnerr muufaiveu. Accepted: e t Resample Requested: Delivered By: Received By: -Date:-,-', -/ Time: / Comments: TURNAROUND: Willcox & Mabe Soil Solutions, PLLC RESIDUAL PAN CALCULATION Beaver Dam Creek WTP TKN= 453 mg/kg NH3= 97 mg/kg NO3-NO2-N= 1.2 mg/kg Min Rate= 0.20 PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO21 0.20 356 48 1.16 PAN= 120.80 mg/kg Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine the amount of PAN/DT remaining. 2ND YEAR RESIDUAL PAN PAN= [min.rate (1st year org. - N 2nd year min. - N] 0.10 356 71 PAN= 28.50 mg/kg remaining from 1st year application 3RD YEAR RESIDUAL PAN PAN= [min.rate (2nd year org. - N 3rd year min. - N] 0.05 285 28 PAN= 13.68 mg/kg remaining from 1st year application 4TH YEAR RESIDUAL PAN PAN= [min.rate (3rd year org. - N 4th year min. - N] 0.03 256 14 PAN= 8.09 mg/kg remaining from 1 st year application 5TH YEAR RESIDUAL PAN PAN= [min.rate (4th year org. - N 5th year min. - N] 0.02 243 8 PAN= 4.55 mg/kg remaining from 1 st year application Residual PAN from years 2 thru 5 after the initial application = 54.82 Application Five Year Maximum Method First Year PAN Adjusted PAN (mg/kg) (mg/kg) Surface 121 176 Incorporation 169 224 mg/kg WTP - SAR SAR Calculation Na mg/I Ca mg/I Mg mg/I 62.832 79002 241.78 Na Ca Mg SAR 2.732 3950.100 20.148 0.061 Na mil eq Ca mil eq Mg mil eq 2.732 3950.100 20.148 Enter Enter .% TS 15.4 Data Na mg/kg 408 Ca mg/kg 513000 Mg mg/kg 1570 Job Name: Beaver Dam Creek WTP Page 6