NC0004685_Regional Office Historical File Pre 2018 (3)

1E Ni on Electric Glass LaserfichePP
Electric Glass Fiber America, LLC
940 Washburn Switch Road, Shelby, NC 28150 Telephone Number: 704-434-1261
a` ECEIVEDINCDENP/DWR
MAR 18 2019
March 14, 2019
WQROS
MOORESVILLE REGIONAL OFFICE
Ori Tuvia, Environmental Engineer
Division of Water Resources, DEQ
Mooresville Regional Office
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Notice of Change of Signatory Certification
Electric Glass Fiber America LLC
NPDES Number NC0004685
Dear Mr. Tuvia:
Please find in attachment copies of two letters for your records that were submitted to the
Water Quality Permitting Section. The first letter regards the addition of Kenneth Hale as
a delegated signature authority and the second addresses the retirement of our Plant
Manager Todd Douthit and appointment of our new Plant Manager Alan Toney is now
responsible for our Facility Certification Responsibilities.
If you have any questions regarding these letters, please feel free to contact me at
[phone] Ext. 2531.
Sincerely,
Richard Young
Manager of Waste Water Treatment
940 Washburn Switch Road, Shelby NC 28150
Email — [e-mail]
Office - 704-434-2261 Ext. 2531.
cc: File

David Van Buren
2002 Kings Rd.
Shelby, NC 28150
Phone [phone]
March 7, 2017
WPCSOCC
1618 Mail Service Center,
Raleigh, NC 27699-1618
NCDEQ Division of Water Resources
610 East Center Ave., Suite 301
Mooresville, NC 28115
SENT VIA CERTIFIED MAIL
Subject: Vacating Backup ORC Position
NPDES Permit: NC0004685
NC Certifications
WW Grade 3 995193
PC Grade 2 995477
RECEIVEDINCDENRIDWR
MAR 10 2017
WOROS
MOORESVILLE REGIONAL OFFICE
This letter is being sent to the Commission and the Regional Division of Water Resources per 15
NCAC 08G .0205 (3). Due to my tennative retirement I will be vacating my position as ORC for
PPG Industries Fiber Glass Products, Inc. effective 03/1/17. Please contact me if there are any
questions.
Sincerely,
David Van Buren
cc: Richard Young
PPG file

FILE
Page 1
To: Point Source Branch
Surface Water Protection Section
Attention: Charles Weaver
SOC Priority Project: No
Date: July 17, 2013
NPDES STAFF REPORT AND RECOMMENDATION
. County: Cleveland
Permit No. NC0004685
PART I - GENERAL INFORMATION
1. Facility and address: PPG Industries, Inc.
940 Washburn Switch Road
Shelby, North Carolina 28150
2. Date of investigation:. July 2, 2013
3. Report prepared by: Sujatha R. Nagulapally, Environmental Specialist
4. Persons contacted and telephone number: Richard Young, [phone], ext. 359.
5. Directions to site: From the intersection of US Hwy 74 and SR 1313 (Washburn Switch Road)
just west of the City of Shelby, travel north on SR 1313 approximately 3.0 miles. The PPG plant
is located on the left side of the road.
6. Discharge point(s), list for all discharge points:
Outfall 001:
Latitude: 35020' 26" Longitude: 81037' 00"
Outfall 002:
Latitude: 35' 19' 28" Longitude: 81' 37' 51"
Attach a USGS map extract and indicate treatment facility site and discharge point on map.
WWTP:
U.S.G.S. Quad No.: F12SW
U.S.G.S. Quad Name: Boiling Springs North, NC
Discharge point:
U.S.G.S. Quad No.: F12SE U.S.G.S. Quad Name: Shelby, NC

1 �•
Page 2
7. Receiving stream or affected surface waters: Brushy Creek (outfall 001), Overflow Branch
(outfall 002)
a. Classification: C (both receiving streams)
b. River Basin and Subbasin No.: Broad 030804
Describe receiving stream features and pertinent downstream uses: Brushy Creek is of
moderate size (15-25 feet wide) with a sandy bottom. General "C" classification uses
downstream. Overflow Branch is 3 - 4 feet wide, and downstream uses are primarily
agricultural in nature.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
a. Volume of wastewater to be permitted: 1.3 MGD (outfall 001), flow is intermittent at
outfall 002.
b. Current permitted capacity of the wastewater treatment facility: 1.3 MGD
C. Actual treatment capacity of the current facility (current design capacity): 1.3 MGD
d. Please provide a description of existing or substantially constructed wastewater treatment
facilities: Existing treatment facilities consists of an influent overflow/storage basin,
influent screening with grinder, wet well with lime addition, a surge tank, an equalization
tank, a flash mix tank for aluminum chloride, coagulant and polymer addition, two (2)
primary clarifiers, two (2) aeration basins with diffused air and bentonite clay addition, a
floc tank with ferric chloride addition, three (3) secondary clarifiers with ferric chloride
addition, a chlorine contact tank being used as an effluent pump tank (no chlorine is
added at this time), traveling bridge sand filter, defoamer addition, gravity sludge
thickener, belt filter press, and an overflow lagoon. Stand-by power is provided for the
industrial process and the WWTP through on -site generators. The permittee has received
approval from the Division to use of bentonite clay for effluent toxicity reduction and the
addition of aluminum chloride as a reactant for fluoride removal, chemical precipitation,
and floc formation. There is no treatment provided at outfall 002.
f. Please provide a description of proposed wastewater treatment facilities: There are no
proposed WWT facilities at this time.
g. Possible toxic impacts to surface waters:
PART III - OTHER PERTINENT INFORMATION
Special monitoring or limitations (including toxicity) requests: None at this time.

Page 3
PART IV - EVALUATION AND RECOMMENDATIONS
The permittee, PPG Industries, Inc., has applied for permit renewal. The current permit expires on
August 31, 2013. This permit allows PPG to discharge treated wastewater at 1.3 MGD to outfall 001 and
to discharge non -cooling water to outfall 002. In addition to the flow from PPG's operation, a high
performance thermoplastic manufacturing facility (Azdel Inc) located adjacent to the PPG site
discharges approximately 10,000 gallons per day to the PPG Wastewater Treatment Plant (WWTP) for
treatment. Azdel Inc uses the fiberglass produced at PPG in part of their industrial process. Outfall 001
includes discharges from the WWTP that treats industrial, domestic and stormwater from both the sites.
Outfall 002 includes discharges from non -contact cooling wastewater and stormwater. PPG has also
obtained coverage under SW general permit number NCG070015, which contains outfalls, 003, 004,
005, 006, 007, and 008.
Based,on the WWT facilities that are available, PPG should be able to continue to meet the
existing and proposed permit effluent limitations, provided there are no significant changes in the current
waste stream.
At this time, there are no additional changes are requested by PPG, it is recommended that the
permit be renewed as requested.
Signature of 6port preparer Dat
Water Quality Regional Supervisor D to

4 ,
NCDENR .
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
March 05, 2013
PPG Industries Fiber Glass Products
940 Washburn Switch Road
Shelby, NC 28150
Subject: Receipt of permit renewal application-
NPDES Permit NCO083348
Cleveland County
Dear Mr. Greg McInnis
John E. Skvarla, III
Secretary
RECEIVED
DIVISION OF WATT R QUALITY
APR 0 2 2013
moo
QFFICr�
The NPDES Unit received your permit renewal application on March 05, 2013. This permit
renewal has been assigned Charles Weaver (919-807-6391) who will contact you if any
additional information is required to complete your permit renewal. Due to current backlog, you
should continue to operate under terms of your current permit, until a new permit is issued. If
you have any questions, please contact the assigned permit writer.
Sincerely,�GG/�
Jeff Poupart
Point Source Branch Program Supervisor IV
Cc: Central Files
Morrisville Regional Office
NPDES Unit
1601 Mail Service Center, Raleigh, North Carolina 27699-1601 NorthCarolina
Phone: [phone] Internet: www.ncdenr.gov /y+ /i
An Equal Opportunity 1 Affirmative Action Employer- 50% Recycled 110% Post Consumer Paper Nah L all y

PPG Industries Fiber Glass Products, Inc.
Greg McInnis
Manufacturing Manager
Fiber Glass Products
February 26, 2013
NC DENR
Division of Water Quality
Surface Water Protection Section — NPDES
1617 Mail Service Center
Raleigh, NC 27699-1617
940 Washburn Switch Road Shelby, N.C. 28150
SENT VIA CERTIFIED MAIL — RETURN RECEIPT REQUESTED
Re: Renewal of NPDES Permit NC0004685
PPG Industries Fiber Glass Products, Inc., Shelby, N.C. Facility
Dear Sir or Madam:
704-434-2261
Extension 206
[e-mail]
RECEIVED
DIVISION OF W8,TER QUALITY
APR 0 2 2013
MOORESVILLE REGIONAL OFFICE
We are pleased to enclose any i F signed NPDES Permit Renewal Application package along
with the two required photo copies. This is for the PPG Industries Fiber Glass Products, Inc. facility in
Shelby, NC. We are requesting the reissuance of NPDES Permit No. NC0004685. The primary SIC
Code for facility operations is 3229-Pressed and Blown Glass- not elsewhere classified. Approximately
one percent of the waste load is from the Hanwha sheet laminate facility (SIC 3083). The wastewater
outfall, Outfall 001, is located at latitude 35 degrees, 20 minutes, 26 seconds, by longitude 81 degrees,
37 minutes, 0 seconds with the receiving water being Brushy Creek.
There have not been any changes to the facility since the previous permit renewal. We request that all
NPDES Permit issues be directed to Mr. Richard Young, Senior Engineer Associate, Environmental.
The facility Manufacturing Manager, Maintenance Manager, and Enterprise Excellence Manager are
authorized to sign all reports required by the permit.

PPG Industries Fiber Glass Products, Inc.
Shelby, North Carolina
NPDES Wastewater Permit Renewal Application for Permit Number NC0004685
TABLE OF CONTENTS
Introduction......................................................................................................................................1
SludgeManagement Plan................................................................................................................2
EPAForm 1............................................................................................................................ Tab A
EPAForm 2C — pages 1-4.......................................................................................................Tab B
Attachments to Form 2C Sections IIA and IIB........................................................................Tab C
EPA Form 2C — Intake and Effluent Characteristics — Outfall 001........................................ Tab D
EPA Form 2C — Intake and Effluent Characteristics — Outfall 002......................................... Tab E
Figures
TopographicalMaps.................:............................................................................................... Tab F
Laboratory Reports
PaceAnalytical....................................................................................................................... Tab G

INTRODUCTION
PPG Industries Fiber Glass Products, Inc. (PPG) operates a Fiber Glass manufacturing facility in
Shelby, North Carolina. This facility operates under the existing NPDES Wastewater Permit
Number NC0004685 which expires on August 31, 2013. This permit allows the facility to
discharge treated wastewater at 1.3 million gallons/day to outfall 001 and to discharge non -
contact cooling water to outfall 002. In addition to PPG's Fiber Glass Manufacturing operation,
a Hanwha sheet laminate manufacturing facility is located adjacent to the PPG site and
discharges approximately 10,000 gallons per day to the PPG Wastewater treatment plant for
treatment. Wastewater from PPG and Hanwha operations are sent to PPG's wastewater plant for
treatment and both operations are covered under the existing permit. Additional details and
clarification for several items relevant to this permit application are highlighted below.
1. SIC Codes and Outfall 001 Testing
The SIC code for the Hanwha (sheet laminate facility) is 3083. The Hanwha site
discharges 10,000 gallons wastewater per day to the PPG wastewater treatment plant for
treatment. This discharge makes up approximately 1/100t" of PPG's wastewater flow.
Therefore, as required for the 3083 SIC code, PPG performed volatile compound testing
on Outfall 001. Results from this testing are incorporated into Form 2C of this
application.
2. Outfall (002) Testing
Outfall 002, the primary stormwater outfall, is currently permitted for the discharge of
non -contact cooling water. Therefore, PPG conducted the testing as set forth in Form 2C.
This testing also included the required volatile compounds for SIC codes 3083.
3. Wet Weather Only Outfalls
Outfalls 003, 004, 005, 006, 007 and 008 are covered under the General Stormwater
Permit #NCG070000, Certificate of Coverage #NCG070015. These outfalls are wet
weather outfalls only and would contain little, if any, drainage from industrial areas. For
this renewal, testing was not conducted on these wet -weather outfalls.
4. Sample Reporting and Averaging
Sample reporting and averaging was provided in Form 2C as per NCDENR DWQ's
"Directions for Completing Monthly Monitoring Reports" dated March, 2009. These
instructions provide guidelines with respect to rules for reporting and averaging less than
detectable "<" values. (i.g., a sample result with a value of less than.the detectable limit
is considered to equal "zero" when calculating monthly and long-term arithmetic
averages). Also per NC DENR DMR reporting guidelines, fecal coliform monthly and
long-term averages were calculated using a geometric mean.
5. Signature Authority
There will be no change requested in signature authority for monthly monitoring report

requirements. Signature authority for monthly reports as a "Duly Authorized
Representative" per 15A NCAC 2B.0506(b)(2)(D), will remain unchanged and is
delegated to the people holding the titles of Manufacturing Manager, Maintenance
Manager and Enterprise Excellence Manager.

SLUDGE MANAGEMENT PLAN
The wastewater treatment plant (WWTP) sludge generated by the Shelby facility is a mixture of
both primary and secondary sludges. The primary sludge is the result of clarification using lime,
aluminum chloride, polymers and coagulants to achieve floc formation and settling. The
secondary sludge is waste activated sludge from the biological treatment system. The secondary
sludge also contains bentonite clay and a small amount of ferric chloride.
Both sludges are combined in a sludge thickener/storage tank prior to dewatering. Polymer
addition and mechanical mixing, along with dilution water, are required to prepare the sludge for
the belt press. The sludge is then pumped to the belt press for dewatering.
The belt press has both a gravity drain section and a pressure section where the water is removed.
Typically, the solids are increased from 4-5% as it leaves the storage tank, to 25-30% solids as
discharged from the belt press. The dewatered sludge is transported via screw conveyors to a
roll -off box. The water is routed back to the head of the WWTP.
Before the roll -off box is picked up for disposal, a paint filter test is conducted on the sludge to
ensure that free liquids are not present. The dewatered sludge is then taken to a permitted, lined
landfill for disposal.

Please print or type in the unshaded areas only
/fill-in areas are cnarPri-fnrelite tvne_ i_e__ 12 rharactersfinch)
For Approved. OMB No. 2040-0086. Approval expires 5-31-92
FORM
_ U.S. ENVIRONMENTALnPROTECTION AGENCY ''
I EPA LD. NUMBER
,'s,
GENERAL INFORMATION
TiA C
110000349070 "° D
F
Consolidated- Perm its. Program
_
xe _
---,GENERAL `
" Reatl fix. "General lnstt�acoons"`before startin-;)
�
F . _ 16
2 13 14
1 LABEL ITEMS _„
GENERAL INSTRUCTIONS
If a preprint. been provided,
esignllted
-,. EPA I.D. NUMBER
affix It in the d space• the
f it is
"information § 'any
III. FACILITY NAME " ��
carefully o
incorrect cross throu 9h it and enter the
correct data in the appfopriate fill-in area,
below. Also, if an of the reprinted data is
absent !(the 'area to theple of the label
V. FACILITY PLEASE'PLACE'LABE'L IN THIS SPACE
„ .
P proper
appear),Sti ash. rovide ttinthepropetfll
below, if thelabel, is
MAILING LIST e„
min area(s complete,
p
correctneednot
Ildl, and VI(x which must be
Refer
VI. FACILITY,„
If noplabe has beensp)roved P to the
LOCATION °
i t unctits, for detailed Item descriptions
n for gg authorization under which
�.
this data- is, collected.
II. POLLUTANT CHARACTERISTICS'
,INSTRUCTIONS: Complete A through J to determine.whether you, need to submit ;any permit application form,
SAO the,EPA. Ifyou answer "yes", to any
questions, you must submit this form and the supplemental`from listed in the parenthesis following the question.
Mark"X" in the --box in the third column if
Jhe supplemental form- is.attached. • If you answer"no" to each' question, you need not submit any of these forms.
You,rnay answer "no" if your activity is
excluded from permit re uirements,, see Section C of the instructions. See also, Section D of the instructlonsfor
definitions of bold-faced terms.
SPECIFIC 'QUES.TIONS
MARK, "X"
_
"SPECIFIC' QUESTIONS.
MARK „X"
FORM
FORM
YES
NO
ATTACHED
YES
NO ATTACHED.
A. Is this facility°a publicly ownedtreatment works",
B` Does or will this, `facility (either", -existing 'or
which results in a discharge to waters of the
❑
®
❑
proposed) include a, concentrated animal
® ❑
U.S.? (FORM 2A)
feeding,y aquatic animal operation or
which results in a discharge
tproduction o waters of the U.S.? (FORM2B)
16,
17
18 ..,-
19 _
20 21'
C'. Is, this facility, which currently results in
®
❑
®
D. is this proposal facility (other than those described
❑
® 1-1
waters of the U.S. other than
into
in A or 8 above) which will result in a discharge
those described in A omB above? FORM 2C
22,
1 23
24, °°`
to waters, of the U.S.?: FORM 2D ,
25 -
26 27
E. Does or will this facility treat, store, or dispose of
F. Do you or will you inject at this, facility industrial or
hazardous Wastes? (FORM 3)
®
❑
❑
municipal effluent below. the lowermost stratum
❑
® ❑
containing, within ,one quarter mile, of the well
bore, underground sources of drinking , water?
28z „
'29
30
(FORM4)
31
"32•
,: 33'
G. Do you or will you inject at this facility any
H. Do you or will you inject at this facility'fluids'for
produced water other fluids which,are brought to
the in connection with conventional oil or
❑
®
❑
special processes„such as mining of sulfer by.the
Frasch solution mining of minerals', in
❑
®
❑
surface
natural gas production, inject fluids used for
process,
situ combustion of fossil fuel, or recovery of
enhanced recovery of oil or natural gas; .or inject `
geothermal energy? (FORM 4) "
fluids for `storage of liquid. hydrocarbons?
34
35
36,
39 .
FORM4�.
�, .,,
w
1. Is this facility a proposed, stationary source J. Is -this facility, a proposed stationarysource'
which is one of the 28 industrial, categories listed which is NOT one of the 28 industrial categories,
emit` ❑ ® ❑ ❑
® ❑
in the instructions and which will potentially li'sted in the'instructions and which will potentially
100 tons per year of any air pollutant regulated emit 250 tons per year o[ any air pollutant
under the Clean Air Actand may, or. be ": regulated under the Clean Air Act and may affect
1 44 1 45'
-affect
located in an attainment area? FORM 5 40 41 42 nr 6e located in nn attainment are? FORM 5 = .43
•III. NAME OF FACILITY
SKIP PPG Industries Fiber Glass Products
15 1 1629 30
69
'IV. FACILITY CONTACT
A. NAME & TITLE. last, first, & title
_ B. PHONE area code & no.) X359
'Young,
Richard Senior Engineer Associate- Environmental
704 434 2261
'46• 48 49. 51 '52". 55,
2
15.' 16 �5 j. 45,=
V. FACILITY MAILING ADDRESS ,
A. STREET OR P:O.'BOX'
'D. ZIP CODE)" '
28150
940 Washburn Switch Road
3
15
1 16 45
p B. C1TY'OR TOWN ' ;" C. STATE
4 Shelby NC
15 16, 40 41' 42
47 51
VI. FACILITY LOCATION
A. STREET, ROUTE,NO, OR OTHERSPECIFIC.IDENTIFIER
. a.
940 Washburn Switch Road
s
15
16 e 45,
B. COUNTY NAME
Cleveland
is 70�.
C. CITY OR TOWN
D. STATE
E. ZIP CODE
F. COUNTY CODE
Shelby
NC
28150
s
,15
f 16. U, ...„. _ ' a ° 40,,.1
AT ' 51
EPA FORM 3510-1 (8-90) CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
UII., SIC CODES ,(4-digit, in, order of priority)
„ " A. FIRST , - B. SECOND .,
° c
3229
(specify)
Stone, Glass, Clay
7' 3083
s
(specify)
Laminated Plastics (Hanwha, LLC)
s -.
16 17
16 19 .
C -.THIRD "D. FOURTH
c (specify) 7- (specify)
15 a 16 17 1 15- 1,16 19 -
VIII OPERATOR. INFORMATION
•„•.. A,., -'NAME- B. -Is the name•listed in Item"
C
PPG Industries Fiber Glass Products Vul-A also -the owner?
®YES ❑ NO
78
C. STATUS OF OPERATOR: Enter th6'appropfiate, letter nto,-the, answerbox; ,if "Other, "specify.) .:
D: PHONE a area code & no, a
F = FEDERAL '', M = PUBLIC (other than federal or state)
P
(specify)
c
704
434
2261
A
S•= STATE O = OTHER (specify)
k_56
na
16 °` 18
19„ 21
22, 25
P = PRIVATE " '
15
E. STREET OR=PO BOX .
940 Washburn Switch Road
26 55
F. CITY OR.TOWN
G. STATE H. ZIP CODE IX. INDIAN LANQ,
Shelby
NC 28150 'Is the facility locafed•on Indian lands?
42 42 47 51 YES M<NO•
B
15 '16 40
X. EXISTING ENVIRONMENTAL PERMITS „
D. PSD. (Air Emissions. from Proposed Sources)
s - .. p
15 _, , 16 1 17 1 18 =. ' 30
A. NPDES (Discharges to Surface Water)
i _..
NC0004885
s
N
15.
'16,,1
17 ..
18. - 30 •
B. UIC
(Underground Injection of Fluids
E. OTHER (specify)
(Specify)
General Stormwater
Discharge Permit
g
C
T
`, '
NA
c
T
8
NCG070015
s.
n'u `
s
15
16
;17
�18 30
15,
.16
17
18, 30 :
C. RCRA (Haiardous Wastes)`" E. OTHER (specify) (Specify)
NCD980559983 ° T. a 01958T58 Air Permit
-
,
18, " a <. 30 15 16 -17 1830
"MAP
Attach to. this, application, a. topographic, map of the,area extending to at least one mile property Themap°must
take
show the outline of the facility, the location of each of its existing and proposed i a, rgendanes
' intake and discharge stFuctures, each of -its
liazardous waste treatment; storage,'or disposal, facilities; and'each well where it injects fluids underground:'= Include all springs,
rivers and other-surfaceawater bodies,in the no rarea.". See instructions. for precise requirements:,
XII NATURE OF BUSINESS (provide a brief description)
Continuous strand fiber glass manufacturing. For NPDES purposes, the site wastewater treatment plant also
receives and treats sanitary effluent from Hanwha, LLC. Hanwha LLC manufactures sheet laminate, SIC Code
3083 as noted in item VII.B. The flow from Hanwha represents only 1 percent of the total flow to the WWTP.
' Xlll. CERTIFICATION '(see instructions),
l certify underpenalty of`law thatl have personally'examirfed,and am familiar with the information'su6mittetl'in this application and "
all attachments and that, based..on my inquiry of those persons immediately responsible -for obtaining�,the information contained in
the application,'( believethat the infomation is Prue, accurate and complete. ! am aware that there are' significant penalties for
submitting; false information; `including the possibility of fine and im risonme • 3. _
A. NAME & OFF�tAL TITLE `(ty-� pe or print) B. GNATURE
�
C. DAT SIGNED
� -l-�wi s t�c�hv►�cc �
2 t.6 (3
avw Ur
COMM NTS FOR OFFICIAL"USE°ONLY
c
a C
15
_.1655,1
EPA FORM 3510-1 (8-90)

TAB B.
EPA FORM 2C
PAGES 1-4

EPA I.D. NUMBER (copyfromIunt I of Form 1) Form Approved.
110000349070 OMB No. 2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM
2C
NPDES
U.S. ENVIRONMENTAL PROTECTION AGENCY
APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
V0,EPA EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consolidated Permits Program
I. OUTFALL LOCATION
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(list)
B. LATITUDE
C: LONGITUDE
D. RECEIVING WATER (name)
1. DEG.
2. MIN.
3. SEC.
1. DEG.
2. MIN.
3. SEC.
001
35
20
26
81
37
0
Brushy Creek
002
35
19
23
81
38
12
Unnamed Tributary to Beaverdam Creek
003
35
19
36
81
38
7
Unnamed Tributary to Beaverdam Creek
004
35
19
.48
81
37
44
Unnamed Tributary to Beaverdam Creek
005
35
19
42
81
37
38
Unnamed Tributary to Beaverdam Creek
II'. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach aline drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW
3. TREATMENT
FALL
NO. (list)
a. OPERATION (list)
b. AVERAGE FLOW
(include units)
a. DESCRIPTION
b. LIST CODES FROM
TABLE 2C-1
001
See Attachment 2C.II.B. Outfall 001
002
Non -Contact Cooling
115,000 GPD
None
Underground Spring Water
35,000 GPD
None
Stormwater- Peak Flow, 1"/hr
74.9 CPS
None
003
Stormwater- Peak Flow, 1"/hr
12.9 CPS
None
004
Stormwater- Peak Flow, 1"/hr
2.3 CPS
None
005
Stormwater- Peak Flow, 1"/hr
1.3 CPS
None
Continued on next page
OFFICIAL USE ONLY (effluent guidelines sub -categories)
EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE

EPA I.D. NUMBER (copyfromItem I of Form 1) Form Approved.
OMB No. 2040-0086.
Please print or type in the unshaded areas only. 110000349070 Approval expires 3-31-98.
FORM
�
NPDES
- U.S. ENVIRONMENTAL PROTECTION AGENCY
APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
O" EPA EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILV CULTURE OPERATIONS
Consolidated Permits Program
I. OUTFALL LOCATION
For each ouffall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(list)
B. LATITUDE
I
I C. LONGITUDE
D. RECEIVING WATER (name)
1. DEG.
I 2. MIN.
3. SEC.
1. DEG.
2. MIN.
3. SEC.
006
35
19
23
181
37
18
Unnamed Tributary.to Beaverdam Creek
007
35
19
25
81
37
29
Unnamed Tributary to Beaverdam Creek
008
35
19
24
81
37
48
Unnamed Tributary to Beaverdam Creek
II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility. Indicate
labeled to correspond to the more detailed descriptions in Item B. Construct
treatment units, and outfalls. If a water balance cannot be determined
sources of water and any collection or treatment measures.
B. For each outall, provide a description of: (1) All operations contributing
and storm water runoff; (2) The average flow contributed by eacfj
necessary.
sources of intake water, operations contributing wastewater to the effluent, and treatment units
a water balance on the line drawing by showing average flows between intakes, operations,
(e.g., for certain mining activities), provide a pictorial description of the nature and amount of any
wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW
3. TREATMENT
FALL
NO. (list)
a. OPERATION (list)
b. AVERAGE
(include
FLOW
units)
a. DESCRIPTION
b. LIST CODES FROM
TABLE 2C-1
006
Stormwater- Peak flow 1"/hr
2.8 CFS
I
None
007
Stormwater- Peak flow 1"/hr
12.2 CFS
None
008
Stormwater- Peak Flow, 1"/hr
12.9 CFS
None
'
I
OFFICIAL USE ONLY (effuentguidelines sub -categories)
EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items B-A or B intermittent or seasonal?
❑ YES (complete the following table) W1 NO (go to Section III)
3. FREQUENCY
4. FLOW
a. DAYS PER
B. TOTAL VOLUME
2. OPERATION(s)
WEEK
b. MONTHS
a. FLOW RATE (innigd)
(specify with units)
1. LONG TERM
2. MAXIMUM
1. LONG TERM
2. MAXIMUM
1. OUTFALL
CONTRIBUTING FLOW
(speck,
PER YEAR
C. DURATION
NUMBER (list)
(list)
awmge)
(specify average)
AVERAGE
DAILY
AVERAGE
DAILY
(in days)
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
❑ YES (complete Item Ill-B) ® NO (go to Section Il)
B. Are the limitations in the applicable effluent guideline expressed in terms of production (orothermeasure of operation)?
❑ YES (complete Item III-C) W] NO (go to Section IV)
C. If you answered "yes" to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the
applicable effluent guideline, and indicate the affected outfalls.
1. AVERAGE DAILY PRODUCTION
2. AFFECTED OUTFALLS
(list outfall numbers)
a. QUANTITY PER DAY
b. UNITS OF MEASURE
c. OPERATION, PRODUCT, MATERIAL, ETC.
(specify)
IV. IMPROVEMENTS _
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to,
permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
❑ YES (complete the following table) © NO (go to Item IV-B)
1. IDENTIFICATION OF CONDITION,
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL COMPLIANCE DATE
AGREEMENT, ETC.
a. NO.
b. SOURCE OF DISCHARGE
a. REQUIRED
b. PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for
construction.
❑ MARK W IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D. NUMBER (copyfrom Item I of Form 1)
CONTINUED FROM PAGE 110000349070
V. INTAKE AND EFFLUENT CHARACTERISTICS
A. B, & C: See instructions before proceeding — Complete one set of tables for each outfall —Annotate the outfall number in the space provided.
NOTE: Tables V-A, V-B, and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged
from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT
2.SOURCE
1.POLLUTANT
2.SOURCE
Acetaldehyde
The compounds detected in
Crotonaldehyde
V.D.1 have been detected in
Ethylene diamine
trace concentrations in a
Formaldehyde
small fraction of PPG's raw
Styrene
materials (based on
Triethanolamine
'manufacturer's MSDSs).
Vinyl acetate
Therefore, these pollutants
may be present in extremely
trace concentrations in the
influent to the WWTP prior to
treatment and in even lower
concentrations (if at all) in
the effluent to Outfall #001.
,
VI. POTENTIAL DISCHARGES NOT COVERED
BY ANALYSIS
or a component of a substance which you
currently use or manufacture as an intermediate
or final product or byproduct?
Is any pollutant listed in Item V-C a substance
❑ YES (list all such pollutants
below )
NO (go to Item VI-B)
EPA Form 3510-2C (5-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII. BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
❑✓ YES (identify the test(s) and describe their purposes below) ❑ NO (go to Section VIII)
Chronic toxicity testing (Ceriodaphnia) is conducted quarterly as per NPDES permit requirements.
Vill. CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
® YES (list the name, address, and telephone number of, and pollutants analyzed by, ❑ NO (go to Section Dt)
each such laboratory orfirm below)
A. NAME
B. ADDRESS
C. TELEPHONE
(area code & no.)
D. POLLUTANTS ANALYZED
(list)
Pace Analytical Services, Inc.
9800 Kincey Ave., Suite 100
[phone]
All except pH, temperature,
WW Cert. No. 12
Huntersville, NC 28078
conductivity, toxicity, and
surfactants (MBAs and CTAS)
Research and Analytical
106 Short St.
[phone]
Toxicity, surfactants (MBAs
Laboratories, Inc.
PO Box 473
and CTAS)
WW Cert No. 34
Kernersville, NC 27284
Biological Cert. 14
IX. CERTIFICATION
1 certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
A. NAME & OFFICIAL TITLE (type orprint)
B. PHONE NO. (area code & no.)
G� mr w; MGh��"(70-
4-3 226
C.
C. SIGNATUR %�
D. DATE SIGNED
IIln�--UUI,ITt L11�� "✓✓l..cc
Z z7 13
EPA Form 3510-2C (8-90) U PAGE 4 of 4

TAB C
ATTACHMENTS TO FORM 2C
SECTIONS IIA AND IIB

EPA FORM 2C SECTION ILA
OUTFALL 001 SCHEMATIC
PPG INDUSTRIES FIBER GLASS PRODUCTS,INC

EPA FORM 2C SECTION ILA
OUTFALL 002 SCHEMATIC
PPG INDUSTRIES FIBER GLASS PRODUCTS, INC.
Stormwater
98.6 acres
peak flow =
74.9 cfs
Outfall
#002
Up to 150,000 gpd
+ stormwater ,
City Water
Supply
Non -Contact
Cooling up to
115,000 gpd
r
Underground
Spring est.
35,000 gpd
Notes:
Outfall #002 is the primary stormwater outfall for the Industrial portions of the property.
Cooling water discharges from the outfall are permitted under #NC0004685.
Stormwater Discharges are covered under the General Stormwater Discharge Permit #NC070000,
COC #NCG070015 i
Stormwater Peak Flows were calculated using the Rational Method (Q = CIA) where:
Q = peak flow (cfs)
C = Runoff Coefficient (where: 0.9 = Impermeable, 0.8 =Graveled, 0.3 = Grassed, 0.1= Wooded)
I = Intensity
A = Area (acres)
Note: The above peak flow for stormwater was calculated using an intensity of 1"/hr. .
The runoff coefficient (C) used was 0.76 based on the following estimate: 80% Industrial, (0.9).
10% wooded (0.1)

EPA FORM 2C SECTION ILA
OUTFALL 003, 004, 005, 006, 007 & 008 SCHEMATIC
PPG INDUSTRIES FIBER GLASS PRODUCTS, INC.
Stormwater I I Stormwater I I Stormwater I I Stormwater I I Stormwater I I Stormwater
30.8 acres 3.1 acres 2.7 acres 9.0 acres 33.8 acres 2.6 acres
;utfa II (�utfa I1 Outfa I I rutfa
11utfa II OutfaII#003 #004 #005 06 #007 #008
Peak Flow Peak Flow Peak Flow Peak Flow Peak Flow Peak Flow
12.9 cfs 2.3 cfs 1.3 cfs 2.8 cfs 12.2 cfs 0.9 cfs
Discharges from Outfalls #003, #004, #005, #006, #007 & #008 are covered under the General
Stormwater Discharge Permit#NC070000, COC #: NCG070015.
These areas contain limited drainage from industrial areas of the property. Outfall 002 is the primary.
stormwater discharge point of the Industrial portions of the property.
Peak Flows were calculated using the Rational Method (Q = CIA) where:
Q = peak flow (cfs)
C = Runoff Coefficient (where: 0.9 = Impermeable, 0.8 = Graveled, 0.3 = Grassed, 0.1= Wooded)
I = Intensity
A = Area (acres)
Note: The above peak flows were calculated using an intensity of 1"/hr. See below for runoff coefficient
calculations.
RUNOFF COEFFICIENT CALCULATIONS
OUTFALL
C
003
0.42
20% Industrial (.9), 80% grassed (.3)
004.
0.75
90% paved parking lot (.9) and 10% grassed (.3)
005
0.48
30% paved parking lot (.9) and 70% grassed (.3)
006
0.31
95% lawn (.3), 2.5% wooded (.1), 2.5% graveled (.8)
007
0.36
10% Industrial (.9) and 90% grassed (.3)
008
0.36
10% Industrial (.9) and 90% grassed (.3)

EPA FORM 2C SECTION 11.13
WWTP Treatment / OUTFALL 001 SCHEMATIC
PPG INDUSTRIES FIBER GLASS PRODUCTS, INC
NPDES Permit NC0004686 Renewal Application
Process Water —(0.8 MGD)
Sanitary — (0.06 MGD)
Bar
Grinding
Flow
Load
Flash Mix
Primary
Screen
1-L
equalization
Equalization
Tank
Clarifiers
Stormwater— (0.12 MGD)
1-T
1-0
2-1)
1-0, 1-G, 2-C
1-U
HANWA — (0.01 8MGD)
Lime
AICI:3j
Anionic Polymer
Cationic Coagulant
CThkenter
OUTFALL #001
ABW
Secondary
Aeration
4-A
Sand _
Clarifiers (3)
Tanks (2)
Filtration
4
2-C, 1-U 1-V
2-U
Recycle /
Cooling Water
Defoamer
FeC13
Lime
4-C
H�PO4
SLUDGE PROCESS SCHEMATIC Anionic
AHeadSludge
ener Polymer Defoamer
Polymer
RAS to
-C DilutionAeration
WaterSludge to
Thickener
Sludge toI andfill S-n
(0-
Bentonite l
Clay
Treatment Codes Used From
Table 2C-1
1-G
Flocculation
1-L
Grinding (Comminutors)
1-0
Mixing
1-T
Screening
1-U
Sedimentation (Settling)
IN
Sand Filtration
2-C
Chemical Precipitation
2-D
Coagulation
3-A
Activated Sludge
4-A
Discharge to Surface Water
4-C
Re -Use / Recycle of Effluent
5-C
Belt Filtration
5-E
Chemical conditioning
5-L
Gravity Thickening
5-Q
Landfill

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (copvfromliem I of Form 1)
on separate sheets (use the same formaf) Instead of completing these pages. 12.0000349070
SEE INSTRUCTIONS.
OUTFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) col
PART A -You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional deffi1s.
3. UNITS
4. INTAKE
2. EFFLUENT
(specifyffblank)
(optionaO
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a MAXIMUM DAILY VALUE
(ifavarlable)
(ifavailable)
AVERAGE VALUE
d. NO.
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
1. POLLUTANT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
(1) CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Biochemical Oxygen
11 1
71.28
8.4
44. 84
1.64
7.39
52
mg/L
Ibs/d
Demand (BOD)
b. Chemical Oxygen
40.0
256.87
1
mg/L
Ibs/d
Demand (COD)
c. Total Organic Carbon
8.5
54.59
1
mg/L
Ibs/d
(T'0C)
d. Total Suspended
Solids(YM
21.6
138.71
4.90
26.15
0.41
1.85
52
mg/L
Ibs/d
e. Ammonia (as AO
0.34
2.18
0.13
0.69
0.05
0.23
52
mg/L
lbs/d
VALUE
VALUE
VALUE
VALUE
f.Row
0.77
0.64
0.54
365
MGD
g. Temperature
VALUE
VALUE
VALUE
VALUE
(winter)
23.7
23.8
18.54
260
°C
h. Temperature
VALUE
VALUE
VALUE
VALUE
(summer)
28.9
27.3
24.37
260
°C
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
i. pH
6.1
7.1
260
STANDARD UNITS
PART B - Mark "X° in column 2a for each pollutant you know or have reason to believe is present Mark "X" In column 2-b for each pollutant you believe to be absent If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent,limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative date or an explanation of their presence In your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.
2. MARK"X"
3. EFFLUENT
4. UNITS
5. INTAKE(optionao
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c LONG TERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a.
b,
a. MAXIMUM DAILY VALUE
(ffavoilable)
(ifavailable)
- VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Bromide
v
(24959-67-9)
b. Chlorine, Total
�/
X
Residual
c. Color
x
d. Fecal Coliform
X
200
7
2
52
#/100 ml
e. Fluoride
(16984-4M)
X
3.20
20.55
0.80
4.27
0.22
0.99
52
mg/L
lbs/d
f. Nitrate.Nitrite
12.70
81.56
12.70
67.79
8.01
36.07
4
mg/L
Ibs/d
EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM
AND
a,
b,
a. MAXIMUM DAILY VALUE
(if-ailable)
(if-ailable)
AVERAGE VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(1)
(lfavailable)
PRESENT
ABSENT
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS'
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
g, Nitrogen,
Total Organic (as
12.70
81.56
12.70
67.79
8.01
36.07
4
mg/L
1bs/d
I
/x\
h.ONand
Grease
X
8.10
52.02
1.60
8.54
0.13
0.59
52
mg/L
lbs/d
I. Phosphorus
\ ,
(as P),Total
x
0.75
4.82
0.75
4.00
0.29
1.31
4
mg/L
lbs/d
(7723-14-0)
j. Radioactivity
(1)Alpha,Total
(2) Beta, Total
`x,
X
(3) Radium,
Total
x
(4) Radium 226,
x
Total
k. Sulfate
WSW
X
43.6
279.99
1
mg/L
lbs/d
(14808-7--8)Q
1. Sulfide
x
(- S)
m. Sulfite
(-Sol)
x
(14265-45-3)
n.Surfactants
x
1.10
7.06
1
mg/L
lbs/d
o. Aluminum,
Total
x
c0.1
0
1
mg/L
lbs/d
(7429-90-5)
P. Barium, Total
(7440-39-3)
x
q. Boron, Total
(7440.42-6)
x
0.180
1.16
1
mg/L
lbs/d
r. Cobalt, Total
�/
x
(7440.48-4)
s.Iron, Total
(7439-89-6)
<0.05
0
1
m L
g/
lbs d
/
L Magnesium,
Tom
X
s0.05
0
1
mg/L
lbs/d
(7439-95 4)
u, Molybdenum,
Total
x
(7439 98-7)
v. Manganese,
Total
x
(7439-96-6)
w. Tin, Total
v
(7440.31-5)
x. Titanium,
Total
X
(7440-32-6)
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copyfrom Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C 1 110000349070 001
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the Instructions to determine which of the GC/MS fractions you must test for. Mark "X' in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalis, and nonrequired GC/MS
fractions), mark "X" in column 2-15 for each pollutant you know or have reason to believe is present Mark 'X' in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant if you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if.you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrle, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each ouffall. See instructions for
additional details and requirements.
2. MARK "X'
3. EFFLUENT
4. UNITS
5. INTAKE (opitonol)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
c.
a. MAXIMUM DAILY VALUE
(ifavatlable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(t)
(1)
(1)
(1)
(lfmatlable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATIDN
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1 PA. Antimony, Total
(7440-36.0)
2M.Arse2Total
X
<0.01
0
1
mg/L
lbs/d
(7440-36-2)
3M. Beryllium, Total
X
(7440-41-7)
4M. Cadmium, Total
X
(7440-43.9)
5M.Chromium.
<0.05
0
1
m L
g/
lbs/d
Total (7440-47-3)
6M. Copper, Total
(744050-8)
X
0.0160
0.10
0.0150
0.08
0.0058
D.03
24
mg/L
lbs/d
7M.Lead, Total
X
0.0000
0.00
0.0000
0.00
0.0000
0.00
12
mg/L
lbs/d
(7439-92-1)
8M. Mercury, Total
X
(7439-97-6)
9M. Nickel, Total
(7440-02-0)
10M. Selenium,
�/
X
Total (7782-49-2)
11 M. Silver, Total
X
<0.0050
0
1
mg/L
1bs/d
(744D-22-4)
12M. Thallium,
Total (7440-28-0)
(74 0-6n6-5c. } otal
X
0.0210
0.13
0.0160
0.09
0.0099
0.04
24
mg/L
lbs/d
14M. Cyanide,
Total (57-12-5)
X
15M. Phenols,
X
Total
DIOXIN
2,3,7,8-Tetra-
DESCRIBE RESULTS
chlorodibenzc-P-
Dioxin (1764-01-6)
EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

CC)NTINI IFI) FROM THE FRMT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
c.
a. MAXIMUM DAILY VALUE
(ifavailaGle)
VALUE (ifavailaGle)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS
1V. Accrolein
<0. 100
1
mg/L
lbs/d
(107-02-8)
2V. Acrylonitrile
X
<0.05
1
mg/L
lbs/d
(107-13-1)
3V. Benzene
(71-43-2)
�/
/�
c0.005
1
mg%L
lbs/d
4V. Bis (Chloro-
\ /
methyl) Ether
x
<0 . 005
1
mg/L
lbs/d
(542-88-1)
5V. Bromoform
�/
x
<0. 005
1
mg/L
lbs/d
(75-25-2)
6V.Carbon
Tetrachloride
,
X
<0.005
1
mg/L
lbs/d
(56-23-5)
7V: Chlorobenzene
<0.005
1
mg/L
lbs/d
(108-90-7)
8V. Chlorodi-
\ /
bromomethane
x
<0.005
l
mg/L
lbs/d
(124-48-1)
/ `
9V. Chloroethane
<0 01
1
mg/L
lbs/d
(75-00-3)
.
10V. 2-Chloro-
ethylvinyl Ether
X
<0 . 01
1
mg/L
lbs/d
(110-75-8)
11V. Chloroform
(67-66-3)
<0.005
1
mg/L
lbs/d
12V. Dichloro-
bromomethane
X
<0.005
1
mg/L
lbs/d
(75-27-4)
13V. Dichloro-
difluoromethane
X
<0.005
1
mg/L
lbs/d
(75-71-8)
14V.1,1-Dichloro-
<0.005
1
mg/L
lbs/d
ethane (75-34-3)
15V.1,2-Dichloro-
x
<0.005
1
m L
g/
lbs/d
ethane (107-06-2)
16V.'1,1-Dichloro-
<0.005
1
mg/L
lbs/d
ethylene (75-35-4)
17V.1,2-Dichloro-
<0.005
I
1
mg/L
lbs/d
propane (78-87-5)
18V.1,3-Dichloro-
\ /
propylene
X
<0.005
1
mg/L
lbs/d
(542-75-6)
19V. Ethylbenzene
<0.005
1
mg/L
lbs/d
(100-41-4)
20V. Methyl
u
<0 01
1
mg/L
1bs/d
Bromide (74-83-9)
.
21V. Methyl
<0.005
1
mg/L
lbs/d
Chloride (74-87-3)
EPA Form 3510-2C (8-90) , PAGE V-4 CONTINUE ON PAGE V-5

r:(1NTINI IF=n PPONA PA(44F V-d
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS (continued)
22V. Methylene
<0.005
0
1
mg/L
lbs/d
Chloride (75-09-2)
23V. 1,1,2,2-
Tetrachloroethane
x
<0.005
0
1
mg/L
lbs/d
79-34-5
24V.Tetrachloro-
<0.005
0
1
mg/L
lbs/d
ethylene (127-18-4)
25V.Toluene
X
<0.005
0
1
mg/L
lbs/d
(108-88-3)
26V. 1,2-Trans-
Dichloroethylene
X
<0.005
0
1
mg/L
lbs/d
156-60-5
27V.1,1,1-Trichloro-
X
<0. 005
0
1
mg/L
lbs/d
ethane (71-55-6)
28V. 1,1,2-Trichloro-
X
<0.005
0
1-
mg/L
lbs/d
ethane (79-00-5)
29VTrichloro-
�/
x
<0.005
0
1
mg/L
lbs/d
ethylene (79-01-6)
30V. Trichloro-
fluoromethane
\ /
x
<0.005
0
1
mg/L
lbs/d
75-69-4
, `
31V. Vinyl Chloride
<0 . 005
0
1
mg/L
lbs/d
(75-01-4)
/ \
GC/MS FRACTION — ACID COMPOUNDS
IA. 2-Chlorophenol
(95-57-8)
2A. 2,4 -Dichloro-
phenol (120-83-2)
3A. 2,4-Dimethyl-
phenol(105-67-9)
4A. 4,6-Dinitro-0-
Cresol (534-52-1)
5A. 2,4-Dinitro-
X
phenol (51-28-5)
6A. 2-Nitrophenol
(88-75-5)
7A. 4-Nitrophenol
\X,
(100-02-7)
/ \
8A. P-Chloro-M-
Cresol (59-50-7)
9A. Pentachloro-
phenol (87-86-5)
10A. Phenol
X
(108-95-2)
11A. 2,4,6-Trichloro-
phenol (88-05-2)
EPA Form 3510-2C (8-90) PAGE V-5' CONTINUE ON REVERSE

r)r1NTINI IFr) FR(1M TPF FRANT
2. MARKW
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
I.POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b,
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (if available)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavarlable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASB
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASEINEUTRAL COMPOUNDS
1 B. Acensphthene
�/
x
(83-32-9)
2B. Acenaphtylene
�/
x
(206.96.8)
3B. Anthracene
�/
(120-12-7)
x
4B, Benzidine
�/
(92-B7-5)
x
68, Benzo (a)
Anthracene
�/
(5M5-3)
/�
6B. Benzo (a)
�/
x
Pyrene (50-32-8)
7B. 3,4-Benzo-
tiuoranthene
X
(205-99-2)
$ 3. Benzo (ghO
�/
x
Perylene (191-24-2)
9B. Benzo (k)
Fluoranthene
(207-OM)
103. Bis (2-Chlaro-
eikmy) Methane
(111-91-1)
11 B. Bis (2-Chloro-
erhyO Ether
�/
x
(111-44-4)
12B. Bis (1-
,
Chloroisopropyl)
Ether (102-80-1)
13B. Bis (2-Ethyl-
hexyo Phthalate
62.1
0.40
1
ug/L
Ibs/d
(117-81-7)
14B.4-Bromophenyl
Phenyl Ether
�/
X
(101-55-3)
15B. Butyl Benzyl
�/
x
Phthalate (B5-6&7)
16B. 2-Chloro-
naphthalene
(91-58.7)
17B. 4-Chloro-
phenyl Phenyl Ether
�/
x
(7005-723)
188. Chrysene
�/
x
(218.01-9)
19B. Dibenzo (alr)
Anthracene
�/
x
(53-70-3)
208.1,2-Dichloro-
�/
x
benzene (95-50-1)
x
benzene(541-73-1)
I
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

r:r)MTIAII ]Pr) PPMA PAr:F \/-R
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (oprionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
c.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
22B. 1,4-Dichloro-
benzene(106-46-7)
23B. 3,3-Dichloro-
benzidine (91-94-1)
24B. Diethyl
X
<5
0
1
u L
g/
lbs/d
'
Phthalate (84-66-2)
.2
25B. Dimethyl
Phthalate
(131 -11-3)
26B. Di-N-Butyl
Phthalate (84-74-2)
27B. 2,4-Dinitro-
toluene (121-14-2)
28B. 2,6-Dinitro-
toluene (606-20-2)
29B. Di-N-Octyl
Phthalate (117-84-0)
30B. 1,2-Diphenyl-
hydrazin e (as Azo-
benzene)(122-66-7)
31B. Fluoranthene
(206-44-0)
32B. Fluorene
(86-73-7)
33B. Hexachloro-
benzene (118-74-1)
34B. Hexachloro-
butadiene (87-68-3)
Hexachloro-
cycl
cyclopentadiene
(77-47-4)
36B Hexachloro-
ethane (67-72-1)
37B.Indeno
(1,2,3-cd) Pyrene
(193-39-5)
38B.Isophorone
-
(78-59-1)
39B. Naphthalene
(91-20-3)
40B. Nitrobenzene
(98-95-3)
41 B. N-Nitro-
sodimethylamine
(62-75-9)
426. N-Nitrosodi-
N-Propylamine
(621-64-7)
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE

r`nNITir`II IFr) PPORA TPr FR(1AIT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
I.POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
43B. N-Nitro-
sodiphenylamine
(86-30-6)
44B. Phenanthrene'
(85-01-8)
45B. Pyrene
(129-00-0)
46S. 1,2,4-Tri-
chlorobenzene
Ix
(120-82-1)
GC/MS FRACTION — PESTICIDES
1P. Aldrin
(309-00-2)
2P. a-BHC
(319-84-6)
3P. (3-BHC
(319-85-7)
4P. y-BHC
(58-89-9)
5P. 8-BHC
(319-86-8)
6P. Chlordane
(57-74-9)
7P. 4,4'-DDT
(50-29-3)
8P. 4,4'-DDE
(72-55-9)
9P. 4,4'-DDD
(72-54-8)
10P. Dielddn
(60-57-1)
11 P. a-Enosulfan
(115-29-7)
12P. (i-Endosulfan
(115-29-7)
13P. Endosulfan
Sulfate
(1031-07-8)
14P. Endrin
(72-20-8)
15P. Endrin
Aldehyde
u
(7421-93-4)
16P. Heptachlor
X
(76-44-8)
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copyfromItem 1 ofPorm 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-8 110000349070 001
2. MARK "X"
3. EFFLUENT
4: UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifmailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavoilable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — PESTICIDES (continued)
17P. Heptachlor
` ,
Epoxide
X
(1024-57-3)
18P. PCB-1242
(53469-21-9)
19P. PCB-1254
x
(11097-69-1)
�\
20P. PCB-1221
\/
(11104-28-2)
x
21 P. PCB-1232
(11141-16-5)
22P. PCB-1248
(12672-29-6)
23P. PCB-1260
(11096-82-5)
24P. PCB-1016
(12674-11-2)
25P.Toxaphene
(8001-35-2)
EPA Form 3510-2C (8-90) PAGE V-9

TAB E
EPA FORM 2C
INTAKE AND EFFLUENT CHARACTERISTICS
OUTFALL 002

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information I 110000349070 EPA I.D. NUMBER (copyffomItem I ofForm I)
on separate sheets (use the same format) instead of completing these pages.
SEE INSTRUCTIONS.
OUTFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) 002
PART A You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfali. See instructions for additional details.
3. UNITS
4. INTAKE
2. EFFLUENT
(specify ifblank)
(optional)
b. MAXIMUM 30 DAY VALUE
C LONG TERM AVRG. VALUE
a. LONG TERM
a. MAXIMUM DAILY VALUE
(ffavailable)
(if -actable)
AVERAGE VALUE
d. NO.
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
1. POLLUTANT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
(1) CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2)MASS
ANALYSES
a. Biochemical Oxygen
<2
0
1
mg/L
lbs/d
Demand(BOD)
b. Chemical Oxygen
33.0
19.27
1
mg/L
lbs/d
Demand (COD)
lOrganicCarbon
4.1
2.39
1
mg/L
lbs/d
(.Tot
d. Total Suspended
Solids (TSS)
49.8
29.07
1
mg/L
lbs/d
e.Ammonia (asM
0.15
0.09
1
mg/L
lbs/d
VALUE
VALUE
VALUE
VALUE
f. Flow
0.07
0.07
0.04
2
MGD
g. Temperature
VALUE
VALUE
VALUE
VALUE
(winter)
12.8
1
oC
h.Temperature
VALUE
VALUE
VALUE
VALUE
(.rummer)
25.0
1
`C
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
I. pH
2
STANDARD UNITS
PART B — Mark "X' in column 2-a for each pollutant you know or have reason to believe is present Mark'r In column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge. Complete one table for each outfell. See the instructions for additional details and requirements.
2. MARK-R
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONGTERM AVERAGE
AND
a
b.
a. MAXIMUM DAILY VALUE
(if-ailable)
(ff—atlable)
VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifmwilable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Bromide
v
(24959.67-9)
Rb. Chorine, Total
Residual
2.0. 0
5. 84
10 . 0
5. 84
10.0 0
3 . 34
2
m L
g/
lbs d
/
a Color
d. Fecal Coliform
�`X
X
,`
e. Fluoride
(16984 tB-B)
f. Nitrst,,Wte
�/
(as M
X
EPA Form 3510-2C (8-90) PAGE V 1 CONTINUE ON REVERSE

ITC�II \/ Con" CDnKlI
v 2. MARK "X" _
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
AND
a
b•
a. MAXIMUM DAILY VALUE
(ifavailable)
(rfavailable)
AVERAGE VALUE
b. NO. OF
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
CAS NO.
(ifavailable)
BELIEVED
PRESENT
BELIEVED
ABSENT
d. NO. OF
ANALYSES
a. CONCEN-
TRATION
b. MASS
ANALYSES
g. Nitrogen,
\
Total Organic (as
M
/X\
h. Oil and
x
Grease
I. Phosphorus
`
(as P), Total
X
(7723-14-0)
j. Radioactivity
(1) Alpha, Total
X
(2) Beta, Total
X
(3) Radium,
Total
(4) Radium 226,
�/
x
Total
k. Sulfate
(as SOO
u
(14808-79-8)
I. Sulfide
(as S)
m. Sulfite
(as SOi)
u
(14265-45-3)
n. Surfactants
X
o. Aluminum,
Total
(7429-90-5)
p. Barium, Total
(7440-39-3)
q. Boron, Total
(7440-42-8)
X
r. Cobalt, Total
(7440-48-4)
s. Iron, Total
(7439-89-6)
t. Magnesium,
i
Total
u
(7439-95-4)
u. Molybdenum,
Total
u '
(7439-98-7)
v. Manganese,
Total
(7439-96-5)
w. Tin, Total
(7440-31-5)
x. Titanium,
Total
(7440-32-6)
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copyfrom Item I of Form 1) OUTFALL NUMBER
CONTINI IFn FROM PAr F:3 OF FORM 9-r: I 11000034907.0 002
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS
fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for
additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optionai)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (rfavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(favailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1 M. Antimony, Total
(7440-36-0)
2M. Arsenic, Total
�/
X
(7440-38-2)
3M. Beryllium, Total
(7440-41-7)
4M. Cadmium, Total
(7440-43-9)
5M. Chromium,
Total (7440-47-3)
6M. Copper, Total
(7440-50-8)
7M. Lead, Total
(7439-92-1)
8M. Mercury, Total
(7439-97-6)
9M. Nickel, Total
(7440-02-0)
10M. Selenium,
Total (7782-49-2)
11 M. Silver, Total
(7440-22-4)
12M. Thallium,
Total (7440-28-0)
13M. Zinc, Total
(7440-66-6)
14M. Cyanide,
Total (57-12-5)
15M. Phenols,
Total
DIOXIN
2,3,7,8-Tetra-
DESCRIBE RESULTS
chlorodibenzo-P-
Dioxin (1764-01-6)
EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS
IV. Accrolein
(107-02-8)
x<0.100
0
1
mg/L
lbs/d
2V. Acrylonitrile
(107-13-1)
l
%\
<0.005
0
1
mg/L
lbs/d
3V. Benzene
(71-43-2)
<0.005
0
1
mg/L
lbs/d
4V. Bis (Chloro-
\ /
methyl) Ether
x
<0.005
0
1
mg/L
lbs/.d
(542-BB-1)
(75-25-2)oform
X
<0.005
0
1
mg/L
lbs/d
Carbon
Tetrachloride
x
<0.005
0
1
mg/L
lbs/d
(56-23-5)
( 08-90-7)benzene
X
<0.005
0
1
mg/L
lbs/d
bromomethane
<0.005
0
1
mg/L
lbs/d
(124-48-1)
/X\
9V. Chloroethane
(75-00-3)
x
<0.100
0
1
mg/L
lbs/d
10V.2-Chloro-
ethylvinyl Ether
<0. 100
0
1
mg/L
lbs/d
(110-75-8)
11V. Chloroform
(67-66-3)
x
<0.005
0
1
mg/L
lbs/d
12V. Dichloro-
bromomethane
X
<0.005
0
1
mg/L
lbs/d
(75-27-4)
13V. Dichloro-
75-71omethane
<0.005
0
1
mg/L
lbs/d
(5-71-8)
7
14V.1,1-Dichloro-
ethane(75-34-3)
�/
X
<0.005
0
1
mg/L
lbs/d
15V. 1,2-Dichloro-
ethane(107-06-2)
x
<0.005
0
1
mg/L
lbs/d
IBV.1,1-Dichloro-
ethylene (75-35-4)
<0.005
0
1
m L
g/
lbs d
/
17V. 1,2-Dichloro-
propane(78-87-5)
x
<0.005
0
I
1
mg/L
lbs/d
18V.1,3-Dichloro-
`.
propylene
<0.005
0
1
mg/L
lbs/d
(542-75-6)
/X\
19V. Ethylbenzene
(100-41-4)
<0.005
0
1
mg/L
lbs/d
20V. Methyl
Bromide(74-83-9)
X
<0.100
0
1
mg/L
lbs/d
21 V. Methyl
<0.005
0
1
mg/L
lbs/d
Chloride (74-87-3)
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5

r'.r)NTINI IPr1 PROM PAnF=\/-A
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable).
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS (continued)
22V. Methylene
X
<0.005
0
1
mg/L
lbs/d
Chloride (75-09-2)
23V. 1,1,2,2-
Tetrachloroethane
X
<0.005
0
1
mg/L
lbs/d
79-34-5
24V.Tetrachloro-
<0.005
0
1
mg/L
lbs/d
ethylene (127-18-4)
25V.Toluene
X
<0.005
0
1
mg/L
lbs/d
(108-88-3)
26V.1,2-Trans-
Dichloroethylene
X
<0.005
0
1
mg/L
lbs/d
156-60-5
27V.1,1,1-Trichloro-
<0.005
0
1
mg/L
lbs/d
ethane (71-55-6)
28V.1,1,2-Trichloro-
X
<0.005
0
1
mg/L
lbs/d
ethane (79-00-5)
29VTrichloro-
<0.005
0
1
mg/L
lbs/d
ethylene (79-01-6)
30V. Trichloro-
fluoromethane
X
<0.010
0
1
mg/L
lbs/d
5-69-4
31V. Vinyl Chloride
<0.005
0
1
mg/L
lbs/d
(75-01-4)
GC/MS FRACTION — ACID COMPOUNDS
1A. 2-Chlorophenol
(95-57-8)
2A. 2,4-Dichloro-
phenol(120-83-2)
3A. 2,4-Dimethyl-
phenol(105-67-9)
4A. 4,6-Dinitro-0-
Cresol (534-52-1)
5A. 2,4-Dinitro-
phenol(51-28-5)
6A. 2-Nitrophenol
(88-75-5)
7A. 4-Nitrophenol
(100-02-7)
j
BA. P-Chloro-M-
Cresol (59-50-7)
9A. Pentachloro-
phenol (87-86-5)
10A. Phenol
(108 95-2)
11 A. 2,4,6-Trichloro-
phenol (88-05-2)
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE

�•i�ti�mu3a�r-rnrrer��riar�
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS
1 B. Acenaphthene
�/
x
(83-32-9)
2B. Acenaphtylene
(208-96-8)
3B. Anthracene
�/
(120-12-7)
4B. Benzidine
�/
(92-87-5)
x
5B. Benzo (a)
Anthracene
�/
x
(56-55-3)
6B. Benzo (a)
�/
Pyrene (50-32-8)
76.3,4-Benzo-
fluoranthene
u
(205-99-2)
8B. Benzo (ghi)
�/
x
Perylene (191-24-2)
9B. Benzo (k)
Fluoranthene
(207-08-9)
10B. Bis (3-Chloro-
elhoxy) Methane
.
(111-91-1)
11B. Bis (2-Chloro-
ethyq Ether
�/
x
(111-44-4)
Bis (2-
Chlo
Chloroisopropyn
Ether (102-80-1)
13B. Bis (2-Lfhyl-
hexyl) Phthalate
(117-81-7)
14B. 4-Bromophenyl
Phenyl Ether
�/
x
(101-55-3)
15B. Butyl Benzyl
�/
x
Phthalate (85-68-7)
16B. 2-Chloro-
naphthalene
(91-58-7)
178. 4-Chloro-
phenyl Phenyl Ether
(7005-72-3)
18B. Chrysene
V
(218-01-9)
/
19B. Dibenzo (a,h)
Anthracene
(53-70-3)
20B. 1,2-Dichloro- .
benzene (95-50-1)
21 B. 1,3-Di-chloro-
benzene (541-73-1)
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b,
c,
a. MAXIMUM DAILY VALUE
(ifmwilable)
VALUE (ifavailable)
AVERAGE VALUE
b. NO. OF
1
()
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
CAS NUMBER
1 available
(.f )
TESTING
REQUIRED
BELIEVED
PRESENT
BELIEVED.
ABSENT
d. NO. OF
ANALYSES
a. CONCEN-
TRATION
b. MASS
ANALYSES
GC/MS,FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
22B. 1,4-Dichloro-
benzene (106-46-7)
23B. 3,3-Dichloro-
benzidine (91-94-1)
24B. Diethyl
Phthalate (84-66-2)
Phthalate
(131 -11-3)
26B. Di-N-Butyl
Phthalate (84-74-2)
27B. 2,4-Dinitro-
toluene (121-14-2)
28B. 2,6-Dinitro-
toluene (606-20-2)
29B. Di-N-Octyl
Phthalate (117-84-0)
30B. 1,2-Diphenyi-
hydrazine (asAzo-
benzene) (122-66-7)
31B. Fluoranthene
(206-44-0)
32B. Fluorene
(86-73-7)
33B. Hexachloro-
benzene (118-74-1)
34B. Hexachloro-
butadiene (87-68-3)
35B. Hexachloro-
cyclopentadiene
X
(77-47-4)
36B Hexachloro-
ethane (67-72-1)
37B.Indeno
(1,2,3-a/) Pyrene
y
(193-39-5)
3BB. isophorone
u
(78-59-1)
/
39B. Naphthalene
(91-20-3)
40B. Nitrobenzene
(98-95-3)
41 B. N-Nitro-
sodimethylamine
(62-75-9)
42B. N-Nitrosodi-
N-Propylamine
(621-64 7)
EPA Form 3510-2C (B-90) PAGE V-7 CONTINUE ON REVERSE

r`(IAITIAII ICfI PPMA TWP CGf1AIT
__.. ...._—_ ..._...
......._...
2. MARK "X"
3. EFFLUENT .
4. UNITS
5. INTAKE (optional
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG,
a. LONG TERM
AND
a.
b,
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
43B. N-Nitro-
sodiphenylamine
(86-30-6)
44B. Phenanthrene
�/
(85-01-8)
45B. Pyrene
(129-00-0)
46B. 1,2,4-Tri-
chlorobenzene
(120-82-1)
GC/MS FRACTION — PESTICIDES
1 P. Aldrin
(309-00-2)
2P. a-BHC
(319-84-6)
3P. (3-BHC
(319-85-7)
4P. y-BHC
(58-89-9)
5P. S-BHC
�/
(319-86-8)
6P. Chlordane
(57-74-9)
7P. 4,4'-DDT
(50-29-3)
BP. 4,4'-DDE
(72-55-9)
9P. 4,4'-DDD
(72-54-8)
10P. Dieldrin
(60-57-1)
11 P. a-Enosulfan
(115-29-7)
12P. (i-Endosulfan
(115-29-7)
X
13P. Endosulfan
Sulfate
(1031-07-8)
14P. Endrin
(72-20-8)
15P. Endrin
Aldehyde
(7421-93-4)
16P. Heptachlor
(76-44-8)
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copyfivin Item I of Form I) OUTFALL NUMBER
CONTINUED FROM PAGE V-8 110000349070 002
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifmailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — PESTICIDES (continued)
17P. Heptachlor
` ,
Epoxide
X
(1024-57-3)
18P. PCB-1242
\/
x
(53469-21-9)
19P. PCB-1254
(11097-69-1)
20P. PCB-1221
(11104-2B-2)
21 P. PCB-1232
\/
(11141-16-5)
x
22P. PCB-1248
(12672-29-6)
23P. PCB-1260
(11096-82-5)
24P. PCB-1016
(12674-11-2)
25P.Toxaphene
(BOD1-35-2)
EPA Form 3510-2C (8-90) PAGE V-9

TAB F
TOPOGRAPHIC MAP
FORM 1
SECTION XI

a
h
h
N
N
N
REFERENCE SCALE IN FEET
1. U.S.G.S. 7.5' TOPOGRAPHIC MAP, BOILING SPRINGS NORTH
AND SHELBY QUADRANGLE, NORTH CAROLINA DATED: 2002. 0
A '
I/A1'r7
IA Z
Civil & Environmental Consultants, Inc.
333 Baldwin Road - Pittsburgh, PA 15205
412-429-2324.800-365-2324
www.cecinc.com
PPG INDUSTRIES FIBER GLASS PRODUCTS, INC.
940 WASHBURN SWITCH ROAD
SHELBY, NORTH CAROLINA
SITE LOCATION MAP
IDRAWN BY:
DATE:
JKS I CHECKED BY: GPT I APPROVED BY:
FEBRUARY 2013 1 DWG SCALE: 1" = 2000'1 PROJECT NO:
-I FIGURE NO.:
122-243-001

TAB G
LABORATORY REPORTS

aceAnalx cal
www.pacelabs.com
January 28, 2013
Mr. Richard Young
PPG Industries
940 Washburn Switch Road
Shelby, NC 28150
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
RE: Project: Permit Renewal 001
Pace Project No.: 92145110
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Young:
Enclosed are the analytical results for sample(s) received by the laboratory on January 16, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Y
Jon D Bradley for
Erin Waters
[e-mail]
Project Manager
Enclosures
cc: Mr. Guy O'Connor, PPG -Shelby
CRFoREPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
l a�
Page 1 of 16

7;a'neAnalXical
www.pacelabs.com
Project: Permit Renewal 001
Pace Project No.: 92145110
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 16

aceAnalytical "
wtvwpacela¢s:com.
Project: Permit Renewal 001
Pace Project No.: 92145110
Lab ID Sample ID
92145110001 001
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Method
Analysts
Analytes
Reported
Laboratory
EPA200.7
JMW
8
PASI-A
EPA 625
BPJ
6
PASI-C
EPA 624
CAH
36
PASI-C
EPA 300.0
AES
1
PASI-A
SM 5220D
AES
1
PASI-A
SM 5310B
AES
1
PASI-A
REPORT OF LABORATORY ANALYSIS Page 3 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacela6s:com
Project: Permit Renewal 001
Pace Project No.: 92145110
Sample: 001
Parameters
200.7 MET ICP
Aluminum
Arsenic
Boron
Chromium
Cobalt
Iron
Molybdenum
Silver
625 MSSV
bis(2-Chloroethyl) ether
Di-n-butylphthalate
bis (2-Ethyl hexyl)phthalate
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
624 Volatile Organics
Acrolein
Acrylonitrile
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethylvinyl ether
Chloroform
Chloromethane
Dibromochloromethane
DichIorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1, 3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 92145110001 Collected: 01/16/13 08:00 Received: 01/16/13 14:10 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA200.7 Preparation Method: EPA200.7
ND ug/L
100
1
01/18/13 19:20
01/22/13 22:49
7429-90-5
ND ug/L
10.0
1
01/18/13 19:20
01/22/13 22:49
7440-38-2
180 ug/L
50.0
1
01/18/13 19:20
01/22/13 22:49
7440-42-8
ND ug/L
5.0
1
01/18/13 19:20
01/22/13 22:49
7440-47-3
ND ug/L
5.0
1
01/18/13 19:20
01/22/13 22:49
7440-48-4
ND ug/L
50.0
1
01/18/13 19:20
01/22/13 22:49
7439-89-6
ND ug/L
5.0
1
01/18/13 19:20
01/22/13 22:49
7439-98-7
ND ug/L
5.0
1
01/18/13 19:20
01/22/13 22:49
7440-22-4
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L
ND ug/L
62.1 ug/L
38 %
36 %
99 %
Analytical Method: EPA 624
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
5.0
1
01/17/1315:00
01/24/1312:26
111-44-4
5.0
1
01/17/1315:00
01/24/1312:26
84-74-2
5.0
1
01/17/1315:00
01/24/1312:26
117-81-7
10-120
1
01/1711315:00
01/24/1312:26
4165-60-0
15-120
1
01/1711315:00
01/24/1312:26
321-60-8
11-131
1
01/1711315:00
01/24/1312:26
1718-51-0
100
1
01/23/13 22:27
107-02-8
50.0
1
01/23/13 22:27
107-13-1
5.0
1
01/23/13 22:27
71-43-2
5.0
1
01/23/13 22:27
75-27-4
5.0
1
01/23/13 22:27
75-25-2
10.0
1
01/23/13 22:27
74-83-9
5.0
1
01/23/13 22:27
56-23-5
5.0
1
01/23/13 22:27
108-90-7
10.0
1
01/23/13 22:27
75-00-3
10.0
1
01/23/13 22:27
110-75-8
5.0
1
01/23/13 22:27
67-66-3
5.0
1
01/23/13 22:27
74-87-3
5.0
1
01/23/13 22:27
124-48-1
5.0
1
01/23/13 22:27
75-71-8
5.0
1
01/23/13 22:27
75-34-3
5.0
1
01/23/13 22:27
107-06-2
5.0
1
01/23/13 22:27
75-35-4
5.0
1
01/23/13 22:27
156-59-2
5.0
1
01/23/13 22:27
156-60-5
5.0
1
01/23/13 22:27
78-87-5
5.0
1
01/23/13 22:27
10061-01-5
5.0
1
01/23/13 22:27
10061-02-6
5.0
1
01/23/13 22:27
100-41-4
5.0
1
01/23/13 22:27
75-09-2
5.0
1
01/23/13 22:27
79-34-5
5.0
1
01/23/13 22:27
127-18-4
5.0
1
01/23/13 22:27
108-88-3
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 4 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92145110
Sample: 001
Lab ID: 92145110001 Collected: 01/16/13
08:00
Received: 01/16/13 14:10 Matrix:
Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qua]
624 Volatile Organics
Analytical Method: EPA 624
1,1,1-Trich]oroethane
ND ug/L
5.0
1
01/23/13 22:27
71-55-6
1,1,2-Trich]oroethane
ND ug/L
5.0
1
01/23/13 22:27
79-00-5
Trichloroethene
ND ug/L
5.0
1
01/23/13 22:27
79-01-6
Trichlorofluoromethane
ND ug/L
10.0
1
01/23/13 22:27
75-69-4
Vinyl chloride
ND ug/L
5.0
1
01/23/13 22:27
75-01-4
Surrogates
Dibromofluoromethane (S)
108 %
70-130
1
01/23/13 22:27
1868-53-7
4-Bromofluorobenzene (S)
92 %
70-130
1
01/23/13 22:27
460-00-4
Toluene-d8 (S)
99 %
70-130
1
01/23/13 22:27
2037-26-5
1,2-Dichloroethane-d4 (S)
109 %
70-130
1
01/23/13 22:27
17060-07-0
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
43.6 mg/L
4.0
2
01/26/1310:33
14808-79-8
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
40.0 mg/L
25.0
1
01/26/13 17:15
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
8.5 mg/L
1.0
1
01/23/13 21:43
7440-44-0
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 5 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92145110
QC Batch: MPRP/12420
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92145110001
METHOD BLANK: 908221
Matrix: Water
Associated Lab Samples: 92145110001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Aluminum
ug/L
ND 100
01/22/13 21:24
Arsenic
ug/L
ND 10.0
01/22/13 21:24
Boron
ug/L
ND 50.0
01/22/13 21:24
Chromium
ug/L
ND 5.0
01/22/13 21:24
Cobalt
ug/L
ND 5.0
01/22/13 21:24
Iron
ug/L
ND 50.0
01/22/13 21:24
Molybdenum
ug/L
ND 5.0
01/22/13 21:24
Silver
ug/L
ND 5.0
01/22/13 21:24
LABORATORY CONTROL SAMPLE:
908222
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits
Qualifiers
Aluminum
ug/L
5000 4550
91
85-115
Arsenic
ug/L
500 450
90
85-115
Boron
ug/L
500 446
89
85-115
Chromium
ug/L
500 458
92
85-115
Cobalt
ug/L
500 464
93
85-115
Iron
ug/L
5000 4580
92
85-115
Molybdenum
ug/L
500 467
93
85-115
Silver
ug/L
250 233
93
85-115
MATRIX SPIKE SAMPLE:
908223
92145003003 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Aluminum
ug/L
ND 5000
4620
92
70-130
Arsenic
ug/L
23.2 500
473
90
70-130
Boron
ug/L
ND 500
464
92
70-130
Chromium
ug/L
ND 500
458
92
70-130
Cobalt
ug/L
ND 500
466
93
70-130
Iron
ug/L
ND 5000
4620
92
70-130
Molybdenum
ug/L
ND 500
470
94
70-130
Silver
ug/L
ND 250
233
93
70-130
MATRIX SPIKE SAMPLE:
908225
92145107001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Aluminum
ug/L
ND 5000
6180
123
70-130
Arsenic
ug/L
ND 500
564
111
70-130
Date: 01/28/2013 12:56 PM
REPORT OF LABORATORY ANALYSIS
Page 6 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

aceAnalytical
twm.pacelabs.com
Project: Permit Renewal 001
Pace Project No.: 92145110
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
908225
92145107001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Boron
ug/L
202
500
738
107
70-130
Chromium
ug/L
ND
500
471
94
70-130
Cobalt
ug/L
ND
500
417
83
70-130
Iron
ug/L
312
5000
4460
83
70-130
Molybdenum
ug/L
ND
500
466
93
70-130
Silver
ug/L
ND
250
320
128
70-130
SAMPLE DUPLICATE: 908224
92145003004
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Aluminum
ug/L
ND
204
Arsenic
ug/L
11.0
9.3J
Boron
ug/L
ND
44.9J
Chromium
ug/L
ND
ND
Cobalt
ug/L
ND
.84J
Iron
ug/L
ND
33.8J
Molybdenum
ug/L
ND
2.1J
Silver
ug/L
ND
.23J
SAMPLE DUPLICATE: 908226
Parameter
Aluminum
Arsenic
Boron
Chromium
Cobalt
Iron
Molybdenum
Silver
Units
92145110001
Result
Dup
Result
ug/L
ND
32.2J
ug/L
ND
ND
ug/L
180
178
ug/L
ND
ND
ug/L
ND
.75J
ug/L
ND
18.3J
ug/L
ND
2.3J
ug/L
ND
ND
RPD Qualifiers
1
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 7 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacelabs.com
Project: Permit Renewal 001
Pace Project No.: 92145110
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/21796 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92145110001
METHOD BLANK: 910018
Associated Lab Samples:
Parameter
92145110001
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
5.0
01/23/13 21:13
1,1,2,2-Tetrachloroethane
ug/L
ND
5.0
01/23/13 21:13
1,1,2-Trichloroethane
ug/L
ND
5.0
01/23/13 21:13
1,1-Dichloroethane
ug/L
ND
5.0
01/23/13 21:13
1,1-Dichloroethene
ug/L
ND
5.0
01/23/13 21:13
1,2-Dichloroethane
ug/L
ND
5.0
01/23/13 21:13
1,2-Dichloropropane
ug/L
ND
5.0
01/23/13 21:13
2-Chloroethylvinyl ether
ug/L
ND
10.0
01/23/13 21:13
Acrolein
ug/L
ND
100
01/23/13 21:13
Acrylonitrile
ug/L
ND
50.0
01/23/13. 21:13
Benzene
ug/L
ND
5.0
01/23/13 21:13
Bromodichloromethane
ug/L
ND
5.0
01/23/13 21:13
Bromoform
ug/L
ND
5.0
01/23/13 21:13
Bromomethane
ug/L
ND
10.0
01/23/13 21:13
Carbon tetrachloride
ug/L
ND
5.0
01/23/13 21:13
Chlorobenzene
ug/L
ND
5.0
01/23/13 21:13
Chloroethane
ug/L
ND
10.0
01/23/13 21:13
Chloroform
ug/L
ND
5.0
01/23/13 21:13
Chloromethane
ug/L
ND
5.0
01/23/13 21:13
cis-1,2-Dichloroethene
ug/L
ND
5.0
01/23/13 21:13
cis-1,3-Dichloropropene
ug/L
ND
5.0
01/23/13 21:13
Dibromochloromethane
ug/L
ND
5.0
01/23/13 21:13
Dichlorodifluoromethane
ug/L
ND
5.0
01/23/13 21:13
Ethylbenzene
ug/L
ND
5.0
01/23/13 21:13
Methylene Chloride
ug/L
ND
5.0
01/23/13 21:13
Tetrachloroethene
ug/L
ND
5.0
01/23/13 21:13
Toluene
ug/L
ND
5.0
01/23/13 21:13
trans-1,2-Dichloroethene
ug/L
ND
5.0
01/23/13 21:13
trans- 1,3-Dichloropropene
ug/L
ND
5.0
01/23/13 21:13
Trichloroethene
ug/L
ND
5.0
01/23/13 21:13
Trichlorofluoromethane
ug/L
ND
10.0
01/23/13 21:13
Vinyl chloride
ug/L
ND
5.0
01/23/13 21:13
1,2-Dichloroethane-d4 (S)
%
109
70-130
01/23/13 21:13
4-Bromofluorobenzene (S)
%
94
70-130
01/23/13 21:13
Dibromofluoromethane (S)
%
108
70-130
01/23/13 21:13
Toluene-d8 (S)
%
99
70-130
01/23/13 21:13
LABORATORY CONTROL SAMPLE: 910019
Parameter Units
1,1,1-Trichloroethane ug/L
Qualifiers
Spike LCS LCS % Rec
Conc. Result % Rec Limits
20 20.1 101 52-162
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 8 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
7;a'neAnalyfical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwpacefa6s.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92145110
LABORATORY CONTROL SAMPLE: 910019
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,2,2-Tetrachloroethane
ug/L
20
19.1
96
46-157
1,1,2-Trichloroethane
ug/L
20
21.8
109
52-150
1,1-Dichloroethane
ug/L
20
20.4
102
59-155
1,1-Dichloroethene
ug/L
20
19.0
95
1-234
1,2-Dichloroethane
ug/L
20
20.8
104
49-155
1,2-Dichloropropane
ug/L
20
20.3
101
1-210
2-Chloroethylvinyl ether
ug/L
40
42.9
107
1-305
Acrolein
ug/L
100
138
138
15-152
Acrylonitrile
ug/L
100
116
116
75-132
Benzene
ug/L
20
20.9
104
37-151
Bromodichloromethane
ug/L
20
20.4
102
35-155
Bromoform
ug/L
20
18.3
92
45-169
Bromomethane
ug/L
20
15.1
76
1-242
Carbon tetrachloride
ug/L
20
19.0
95
70-140
Chlorobenzene
ug/L
20
21.0
105
37-160
Chloroethane
ug/L
20
21.4
107
14-230
Chloroform
ug/L
20
20.5
102
51-138
Chloromethane
ug/L
20
17.9
90
1-273
cis-1,2-Dichloroethene
ug/L
20
20.1
100
68-146
cis- 1,3-Dichloropropene
ug/L
20
20.3
101
1-227
Dibromochloromethane
ug/L
20
19.9
99
53-149
Dichlorodifluoromethane
ug/L
20
18.5
92
70-130
Ethylbenzene
ug/L
20
20.2
101
37-162
Methylene Chloride
ug/L
20
21.3
107
1-221
Tetrachloroethene
ug/L
20
20.1
101
64-148
Toluene
ug/L
20
21.0
105
47-150
trans-1,2-Dichloroethene
ug/L
20
19.4
97
54-156
trans- 1,3-Dichloropropene
ug/L
20
20.1
100
17-183
Trichloroethene
ug/L
20
19.9
100
71-157
Trichlorofluoromethane
ug/L
20
18.7
94
17-181
Vinyl chloride
ug/L
20
19.9
99
1-251
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
90
70-130
Dibromocuoromethane (S)
%
102
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 910020
910021
MS
MSD
92145401001
Spike
Spike
MS
MSD
MS MSD % Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec Limits RPD Qua]
1,1,1-Trichloroethane
ug/L
ND
20
20
24.0
23.0
120
115 46-171 4
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.9
20.0
99
100 73-159 0
1,1,2-Trichloroethane
ug/L
ND
20
20
22.4
22.8
112
114 64-152 2
1,1-Dichloroethane
ug/L
ND
20
20
22.7
22.2
114
111 43-172 3
1,1-Dichloroethene
ug/L
ND
20
20
23.6
22.3
118
112 48-189 6
1,2-Dichloroethane
ug/L
ND
20
20
22.6
22.9
113
114 42-171 _ 1
1,2-Dichloropropane
ug/L
ND
20
20
21.8
21.6
109
108 55-157 1
Date: 01/28/2013 12:56 PM
REPORT OF LABORATORY ANALYSIS
Page 9 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

(�IacieAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92145110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
910020
910021
MS
MSD
92145401001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
2-Chloroethylvinyl ether
ug/L
ND
40
40
44.0
45.2
110
113
70-130
3
Acrolein
ug/L
ND
100
100
145
143
145
143
70-130
1 MO
Acrylonitrile
ug/L
ND
100
100
121
119
121
119
70-130
2
Benzene
ug/L
ND
20
20
22.4
21.8
112
109
54-163
2
Bromodichloromethane
ug/L
ND
20
20
22.6
22.4
113
112
56-152
1
Bromoform
ug/L
ND
20
20
20.9
20.8
104
104
53-151
0
Bromomethane
ug/L
ND
20
20
21.5
18.8
107
94
10-200
13
Carbon tetrachloride
ug/L
ND
20
20
24.5
23.1
122
116
.41-175
6
Chlorobenzene
ug/L
ND
20
20
22.7
22.5
113
112
67-152
1
Chloroethane
ug/L
ND
20
20
23.1
22.6
115
113
23-200
2
Chloroform
ug/L
ND
20
20
22.8
22.7
114
113
51-166
1
Chloromethane
ug/L
ND
20
20
20.7
21.1
104
106
40-175
2
cis- 1,2-Dichloroethene
ug/L
ND
20
20
21.8
21.4
109
107
45-174
2
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.8
22.1
114
111
38-146
3
Dibromochloromethane
ug/L
ND
20
20
22.5
22.3
113
112
65-144
1
Dichlorodifluoro methane
ug/L
ND
20
20
22.5
21.4
112
107
70-130
5
Ethylbenzene
ug/L
ND
20
20
22.6
21.9
113
109
57-152
3
Methylene Chloride
ug%L
ND
20
20
22.7
22.2
112
109
40-167
2
Tetrachloroethene
ug/L
ND
20
20
23.6
22.6
118
113
59-155
4
Toluene
ug/L
ND
20
20
22.5
22.1
113
111
47-162
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.9
21.2
110
106
47-178
3
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.1
21.9
111
109
39-148
1
Trichloroethene
ug/L
ND
20
20
22.4
22.1
112
110
60-153
2
Trichlorofluoromethane
ug/L
ND
20
20
25.1
23.8
125
119
42-199
5
Vinyl chloride
ug/L
ND
20
20
22.1
21.8
111
109
46-176
2
1,2-Dichloroethane-d4 (S)
%
105
105
70-130
4-Bromofluorobenzene (S)
%
91
91
70-130
Dibromofluoromethane (S)
%
103
104
70-130
Toluene-d8 (S)
%
100
100
70-130
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 10 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

(�IaceAnalydcal'
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92145110
QC Batch: OEXT/20422 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92145110001
METHOD BLANK: 907332
Matrix: Water
Associated Lab Samples:
92145110001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
bis(2-Chloroethyl) ether
ug/L
ND
5.0
01/24/13 05:12
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
01/24/13 05:12
Di-n-butylphthalate
ug/L
ND
5.0
01/24/13 05:12
2,4,6-Tribromophenol (S)
%
88
10-137
01/24/13 05:12
2-Fluorobiphenyl (S)
%
71
15-120
01/24/13 05:12
2-Fluorophenol (S)
%
40
10-120
01/24/13 05:12
Nitrobenzene-d5 (S)
%
70
10-120
01/24/13 05:12
Phenol-d6 (S)
%
27
10-120
01/24/13 05:12
Terphenyl-d14 (S)
%
93
11-131
01/24/13 05:12
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
907333
Units
Spike LCS LCS
Conc. Result % Rec
% Rec
Limits
bis(2-Chloroethyl) ether
ug/L
50 49.1 98
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50 50.6 101
8-158
Di-n-butylphthalate
ug/L
50 45.4 91
1-118
2,4,6-Tribromophenol (S)
%
105
10-137
2-Fluorobiphenyl (S)
%
77
15-120
2-Fluorophenol (S)
%
44
10-120
Nitrobenzene-d5 (S)
%
83
10-120
Phenol-d6 (S)
%
31
10-120
Terphenyl-d14 (S)
%
92
11-131
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 907334
92145230001
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
907335
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qua]
bis(2-Chloroethyl) ether
ug/L
ND
100
100
92.3
51.9
92
52
12-158
56
bis(2-Ethylhexyl)phthalate
ug/L
ND
100
100
97.3
87.3
97
87
8-158
11
Di-n-butylphthalate
ug/L
ND
100
100
89.3
77.4
89
77
1-118
14
2,4,6-Tribromophenol (S)
%
88
76
10-137
2-Fluorobiphenyl (S)
%
72
35
15-120
2-Fluorophenol (S)
%
49
24
10-120
Nitrobenzene-d5 (S)
%
71
40
10-120
Phenol-d6 (S)
%
40
19
10-120
Terphenyl-d14 (S)
%
89
71
11-131
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 11 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pac,elabs.com
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Permit Renewal 001
Pace Project No.:
92145110
QC Batch:
WETA/14339 Analysis Method: EPA 300.0
QC Batch Method:
EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92145110001
METHOD BLANK: 910398
Associated Lab Samples: 92145110001
Parameter Units
mg/L
Sulfate
LABORATORY CONTROL SAMPLE: 910399
Parameter Units
Sulfate mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 01/25/1312:42
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 19.5 97 90-110
MATRIX SPIKE SAMPLE:
910400
92145259001
Spike MS MS % Rec
Parameter
Units
Result
Conc. Result % Rec Limits Qualifiers
Sulfate
mg/L
ND
20 19.9 99 90-110
SAMPLE DUPLICATE: 910401
92145259001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Sulfate
mg/L
ND
ND
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 12 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Q /7 �+
aCeAnalytical
205 East Meadow Road - Suite
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pacela.bs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92145110
QC Batch: WETA/14358
Analysis Method: SM 5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 92145110001
METHOD BLANK: 911650
Matrix: Water
Associated Lab Samples: 92145110001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Chemical Oxygen Demand
mg/L
ND 25.0
- 01/26/13 17:15
LABORATORY CONTROL SAMPLE:
911651
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
750 724
97
90-110
MATRIX SPIKE SAMPLE:
911652
92144938007 Spike
MS
MS -
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
4180 7500
12600
113
75-125
MATRIX SPIKE SAMPLE:
911654
92145009001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
ND 750
802
105
75-125
SAMPLE DUPLICATE: 911653
92144938007 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Chemical Oxygen Demand
mg/L
4180 4940
17
SAMPLE DUPLICATE: 911655
92145009001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Chemical Oxygen Demand
mg/L
ND 35.0
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 13 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Q �7 �+
aC8A17alXical
205 East Meadow Road - Suite
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pacclabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92145110
QC Batch: WETA/14330
Analysis Method: SM
5310B
QC Batch Method: SM 5310B
Analysis Description: 5310B TOC
Associated Lab Samples: 92145110001
METHOD BLANK: 909543
Matrix: Water
Associated Lab Samples: 92145110001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Total Organic Carbon
mg/L
ND 1.0
01/23/13 19:19
LABORATORY CONTROL SAMPLE:
909544
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits
Qualifiers
Total Organic Carbon
mg/L
25 23.8
95
90-110
MATRIX SPIKE SAMPLE:
909545
92144545036 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Organic Carbon
mg/L
19.2 25
57.7
154
75-125 M6
MATRIX SPIKE SAMPLE:
909547
92145316001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Organic Carbon
mg/L
3.9 25
29.0
100
75-125
SAMPLE DUPLICATE: 909546
92144545036 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Total Organic Carbon
mg/L
19.2 16.9
13
SAMPLE DUPLICATE: 909548
92145316002 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Total Organic Carbon
mg/L
4.3 4.1
5
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 14 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
wimpacelabsxom
Project: Permit Renewal 001
Pace Project No.: 92145110
1110IMM111041 b9
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
Date: 01/28/2013 12:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 16

aceAnalyt cal
www.pacelabs;crom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Permit Renewal 001
Pace Project No.: 92145110
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92146110001
001
EPA200.7
MPRP/12420 EPA200.7
ICP/11344
92145110001
001
EPA 625
OEXT/20422 EPA 625
MSSV/7244
92145110001
001
EPA 624
MSV/21796
92145110001
001
EPA 300.0
WETA114339
92145110001
001
SM 5220D
WETN14358
92145110001
001
SM 5310B
WETA114330
Date: 01/28/2013 12:56 PM REPORT OF LABORATORY ANALYSIS Page 16 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

WI'?
PakeAq ytjq
CHAIN-OF-CUST '/Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Page: Of
Required Client Information: Required Project Information: Invoice Information:
Company:
�o,p Report To: Attention:
16.340 00
A4d!pg Copy
To:
Company Name:
RW EGUN '.
2kkro
Address:
7P"NPDES GROUND WATER r DRINKING WATER
F UST RCRA r OTHER
Email To: Purchase
Order No.:
Pace Quote
Reference:
lPhone:
7-
16ir - V-714- Zz I(/
IF Project
j.
.:J
Name:
Pace
PI-Mie" l
:'Site LOC3tl01f
Requested Duo DatelTAr. Prolact
Number.,
Pace Profile
9 q
ue
d
6i6.
Fjo
Section 0 Matrix Codes
4g
Requinic1client Information MkTATX I 09T)E
_
COLLECTED
Preservativesvatives
Drinking Water DW
Water WT
a
8.
0
0
U
z
0
Waste Water WW
Product P
0
§
COMPOSITE
START
composr!"12
END/GRAB
15
w
_1
" ` .
�
_115
SoUlSolid SL
SAMPLE ID oil O
tD
0 0
a)
Wip e WLP
(A-Z, 0-9 AR
Sample IDs. MUST BE UNIQUE Tissue TS
u.'
0
to
(L
Q.
w
z
0
j2
Other OT
L)
w
k
-6c
11
�
`;I�
-6
L<
�J
0
a)
Si
lz
)%
,
a-
2
LL
0
0
0
z
0
I
U)
0
CU
J_
- Z5
CD
E
10
I
1(b
. I
4,
k
U)
Jul
<
10
''DATE.
TIME
DATE
TIME
<
in
41,
a
5
.
X
7
X
Co
z
z
2
0
,,a
%q
Y,
%A
C.)
C;
Pace Project No./ Lab J.D.
V,
6
fZA,
(OCA
c
3
61>1
C
C
4
0,0
✓
:g
.0
121
1
1
LLI
1
1
..ADDITIO OMMENT4-
.,...-..-:R�LlNQUISHEDI�Y1.A 46M
TIME:.*
SAMPLE CONDITIONS
X C
6:
ORIGINAL
Z
Z0 —
Z
�:
PRINT Name of SAMPLER-
E
.,
.2
E
SIGNATURE of SAMPLER-
DATE Signed
(MWDDNY): 'fAell.?
U)
tiorhmt Note: Bysigning this form you are accepting Pace's NET30 day payinentterms, and agreeing to late charges ufl.5% per munch for any invoices not paid witfifin 30 days.
t--ALL-w-uzureV.u1, I--Fviay-zuur

�Ice)lna"Cal'
Document Name:
F-CHR-CS-03-rev.08
Document Revised: October 31, 2012
1R Page 1 of 2
Issuing Authority: - .
Pace
Office
Client Name:'\` Project a
Where Received: ❑ untersville ❑ Asheville ❑ Eden ❑ Raleigh
Courier: ❑ Fed Ex ❑ UPS[] LISPS❑ ClientZno
ommercial Pace Other
❑ Custody Seal on Cooler/Box Present: lyes Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble Wrap ❑Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1101 11 Type of Ice: We Blue None ❑ S les on Ice, cooling process has begun
Tema Correction Factor T1101 Correction T1102: No Correction
Corrected Cooler Temp.: C
Biological Tissue is Frozen: Yes 'No NIA
Date and Initla!p (#
person examining
co
-Temp should be above freezing -to °
Cofrirnents:.
Chain of Custody Present:
Yes ❑No
❑NIA
1.
Chain of Custody Filled Out:
Y_es ❑No
❑NIA
2.
Chain of Custody Relinquished:
es ❑No
❑NIA
3.
Sampler Name & Signature on COC:
es ❑No
❑NIA
4.
Samples Arrived within Hold Time:
Yes ❑No
❑NIA
5.
Short Hold Time Analysis <72hr :
Yes ❑ o
❑NIA
6.
Rush Turn Around Time Requested:
❑Yes No
❑NIA
7.
Sufficient Volume:
CBS ❑No
❑NIA
8.
Correct Containers Used:
Yes ❑No
❑NIA
9.
-Pace Containers Used:
UK. ❑No
❑NIA
Containers Intact:
es ❑No
DMIA,
10,
Mitered volume received for Dissolved tests
❑Yes ❑No
[]MIA
11.
-. Sample Labels match COC:
es ❑No
❑NIA
12.
-includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
Yes ❑No
❑NIA
13.
All containers needing preservation are found to be In
/LJYes ONo
❑NIA
compliance with EPA recommendation.
exceptions: VOA, collform, TOC, O&G, WI-DRO (water)
❑Yes ❑No
Initial when completed
$ampler checked for dechlorination:
24. ❑No
❑NIA
14.
Heads ace in VOA Vials >6mm :
❑Yes 014o
DNA
15.
Trip Blank Present:
Dyes ❑No
❑N
16.
Trip Blank Custody Seals Present
❑Yes ❑No
NIA
Pace Trip Blank Lot # if purchased):
Client Notification/ Resolution: Field Data Required? Y I N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: Date: j j lP 1 J SRF Review: Date: 13
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp, Incorrect containers)

'Chain of Custody
Workorder: 92145110
Workorder Name: Permit Renewal 001
Results Requesteo 1/3012013
019AnalXical
WVAV.paC8?abSx=
i 1-'15
M, M
ON I IH ri,1•111,111.
I-M .110
Erin Waters
Pace Analytical Charlotte P.O. 31
9800 Kincey Ave. Suite 100
Huntersvilfe, NC 28078
Phone [phone]
Email: [e-mail]
r
ji• '7
Jul
1
1?5,�4, jrtt
lkiitt
i-,
j Eyt�
To "R
� m
gja
VY
LAB USE ONLY
:5
1
1001
1116/2013 08:00
92145110001
Water
2
3
4
5
1
.
-145E
�
Mi
*
Ai}lIN M
Transfers
Released By
Date/Time
Received By
Date/Time
Oak m
2
v
3
Cooler Temperature on Receipt Qc
Custody Seal Y or N_
Received on lee Y or N
samples intact Y or N
Wednesday, January 16,2013 3:09:43 PM FMT-ALL-C�002rev.00 24March2009 Page 1 of 1

LZORMOR0ES, hC.
p 3,ry�d
° Analytical/Process Consultations
Pace Analytical-Huntersville
.9800 Kincey Ave -;Suite 100
Huntersville, NC 28078
Attn: Erin Waters
4p�86ROtSooU�DgQgp6
4Cli
b� e �• @:r �hr� o
co,
a ^ a
o
adEII8IIA0D���
Date Sample Collected 01/16/13
Date Sample Received 01/17/13
Date Sample Analyzed .01/17/13
Date of Report 01/28/13
?analyses Performed by DW -YJ
Lab Sample Number
--------------------
749025.
Parameter Storet #( Results
CTAS 1.10 mg/1
MBAS (38260) <0.1 mg/1
--------------------
Clients Sample Source. 001
Number
Time Collected (Hrs) 0800
P.O. Box 473 ° 106 Short Street Kernersville, North Carolina 27284 0 336-996-2841 o Fax [phone]
www.randalabs.com

Chain ®f Custody
Workorder: 92145110 Workorder Name: Permit Renewal 001
Results Requested 1/30/2013
aceAnaljdical
www.pacdIabs:com
"�..,.. f=a �
�. yS.
�.�
�3� .
R i�_
n , , t - ,� „t, t >, tk.. N� .;.•. �. .sx r+ � w�a ... yr. � ..: G z €.
Re . � ..:�.:_.�o.��t,_ .�.. r�.....,.'.�; . ;�ti w.�. vr..
� , < ,
.�r�..,�,�. :�_ �~�,��
.��...a„�
�r�t,
_�..��
�
_�.,>...a•
Erin Waters
nI
Pace Analytical Charlotte K V � P.O. 3
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Phone [phone]
Email: [e-mail]
OkM
'�
< 'axF f4f7r*-,rk ^r 5•r r
F M1"zt C r.v`ji
jr.^ t ft'7"Z� 1``
�J
kH
s #i,
P +`*a`. �.,,�``.
c
�2..,x ,4'�';
u*"'i
.
Item x,
Sample•=tDfr��;�, ��
�
�
LAB USE ONLY
�� �
„ ,<*"
, ;�t xt
1
001
1/16/2013 08:00
92145110001
Water
2
3
4
5
a.. .c Sri.... T ... hre+','" ., . r%t... .�+,,^;a.5n. �2 ,irr.:.n„�w�.,a. ..._
R '...r, ?,�.-S"�h.: is s.v:.
....
-,
•.'.'t
...
[F
ifry
.+�4':-. 4 fi'�
'r
� U f'�`
'I.. f.�
�
Yenfs
Y �
� [..
.� ..r.. $� :4w .,%✓'..., .y .,hf. .. { l , .. 4 t<aA .: J. r5 try
., .._._... f;t :1.....:ry.,'s.-..-s ::b:..:�fw._a,f ln.:e�...-. .>•''...}.s a:..u,i_'..'.�-_1�...-`„A.�Ste�r....;;Er:.n. '. ... .. +'8..,. ... �.__��.k•..
i Yi
r} .
.:
..$!3.+.
.:a:...
c.! S_ ..�.q?n+'."'...
.�`iL_...
f. t»
#.:
_,s..k:.......
L.�
_.�}iil
_,.
m
Transfers
Released By
Date/Time
Received By
Datefrime
1I?
2
v
3
Cooler Terrt erature on Recei t + °C
Custod Seaf Y rr N
Received on Ice Y r N
Samples lnta Y r N
Wednesday, January 16, 2013 3:09:43 PM FMT-ALL-C-002rev.00 24March2009 Page 1 of

aceAnalytical
www.pgcelabs.com
January 28, 2013
Mr. Richard Young
PPG Industries
940 Washburn Switch Road
Shelby, NC 28150
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
RE: Project: Permit Renewal 002
Pace Project No.: 92145123
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Dear Mr. Young:
Enclosed are the analytical results for sample(s) received by the laboratory on January 16, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
qtn M wajz-
Erin Waters
[e-mail]
Project Manager
Enclosures
cc: Mr. Guy O'Connor, PPG -Shelby
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 16

aceAnalXical
Y ui w.pacelabssom
Project: Permit Renewal 002
Pace Project No.: 92145123
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 16

aceAnalytical
wwwpacelabs.com
Project: Permit Renewal 002
Pace Project No.: 92145123
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Lab ID Sample ID Method
92145123001 002 EPA 625
EPA 624
SM 2540D
SM 5210B
EPA 350.1
SM 5220D
SM 5310B
Analysts
BPJ
CAH
LMD
JBH
SAE
AES
AES
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported Laboratory
6
PASI-C
35
PASI-C
1
PASI-A
1
PASI-A
1
PASI-A
1
PASI-A
1
PASI-A
REPORT OF LABORATORY ANALYSIS Page 3 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalX cal
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92145123
Sample: 002 Lab ID: 92145123001 Collected: 01/16/13 07:30 Received: 01/16/13 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
bis(2-Chloroethyl) ether
ND ug/L
5.0
1 01/17/13 15:00
01/24/13 12:54
111-44-4
Di-n-butylphthalate
ND ug/L
5.0
1 01/17/13 15:00
01/24/13 12:54
84-74-2
bis(2-Ethylhexyl)phthalate
ND ug/L
5.0
1 01/17/13 15:00
01/24/13 12:54
117-81-7
Surrogates
Nitrobenzene-d5 (S)
35 %
10-120
1 01/17/13 15:00
01/24/13 12:54
4165-60-0
2-Fluorobiphenyl (S)
43 %
15-120
1 01/17/13 15:00
01/24/13 12:54
321-60-8
Terphenyl-d14 (S)
84 %
11-131
1 01/17/13 15:00
01/24/13 12:54
1718-51-0
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
ND ug/L
100
1
01/23/13 22:45
107-02-8
Acrylonitrile
ND ug/L
50.0
1
01/23/13 22:45
107-13-1
Benzene
ND ug/L
5.0
1
01/23/13 22:45
71-43-2
BromodichIoromethane
ND ug/L
5.0
1
01/23/13 22:45
75-27-4
Bromoform
ND ug/L
5.0
1
01/23/13 22:45
75-25-2
Bromomethane
ND ug/L
10.0
1
01/23/13 22:45
74-83-9
Carbon tetrachloride
ND ug/L
5.0
1
01/23/13 22:45
56-23-5
Chlorobenzene
ND ug/L
5.0
1
01/23/13 22:45
108-90-7
Chloroethane
ND ug/L
10.0
1
01/23/13 22:45
75-00-3
2-Chloroethylvinyl ether
ND ug/L
10.0
1
01/23/13 22:45
110-75-8
Chloroform
ND ug/L
5.0
1
01/23/13 22:45
67-66-3
Chloromethane
ND ug/L
5.0
1
01/23/13 22:45
74-87-3
Dibromochloromethane
ND ug/L
5.0
1
01/23/13 22:45
124-48-1
Dichlorodifluoromethane
ND ug/L
5.0
1
01/23/13 22:45
75-71-8
1,1-Dichloroethane
ND ug/L
5.0
1
01/23/13 22:45
75-34-3
1,2-Dichloroethane
ND ug/L
5.0
1
01/23/13 22:45
107-06-2
1,1-Dichloroethene
ND ug/L
5.0
1
01/23/13 22:45
75-35-4
trans-1,2-Dichloroethene
ND ug/L
5.0
1
01/23/13 22:45
156-60-5
1,2-Dichloropropane
ND ug/L
5.0
1
01/23/13 22:45
78-87-5
cis-1,3-Dichloropropene
ND ug/L
5.0
1
01/23/13 22:45
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
5.0
1
01/23/13 22:45
10061-02-6
Ethylbenzene
ND ug/L
5.0
1
01/23/13 22:45
100-41-4
Methylene Chloride
ND ug/L
5.0
1
01/23/13 22:45
75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L
5.0
1
01/23/13 22:45
79-34-5
Tetrachloroethene
ND ug/L
5.0
1
01/23/13 22:45
127-18-4
Toluene
ND ug/L
5.0
1
01/23/13 22:45
108-88-3
1,1,1-Trichloroethane
ND ug/L
5.0
1
01/2311322:45
71-55-6
1,1,2-Trichloroethane
ND ug/L
5.0
1
01/23/13 22:45
79-00-5
Trichloroethene
ND ug/L
5.0
1
01/23/13 22:45
79-01-6
Trichlorofluoromethane
ND ug/L
10.0
1
01/23/13 22:45
75-69-4
Vinyl chloride
ND ug/L
5.0
1
01/23/13 22:45
75-01-4
Surrogates
Dibromofluoromethane (S)
109 %
70-130
1
01/23/13 22:45
1868-53-7
4-Bromofluorobenzene (S)
91 %
70-130
1
01/23/13 22:45
460-00-4
Toluene-d8 (S)
100 %
70-130
1
01/23/13 22:45
2037-26-5
1,2-Dichloroethane-d4 (S)
110 %
70-130
1
01/23/13 22:45
17060-07-0
Date: 01/28/2013 04:33 PM
REPORT OF LABORATORY
ANALYSIS
Page 4 of 16
This report shall not
be reproduced, except in full,
without the written consent
of Pace Analytical Services, Inc..

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
•
Q �7 �+
aceAnal ical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pacefa6s.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
/_1ki/_1W'111110WAa:7*11111111K
Project: Permit Renewal 002
Pace Project No.: 92145123
Sample: 002
Lab ID: 92145123001 Collected:
01/16/13
07:30
Received: 01/16/13 14:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
49.8 mg/L
6.2
1
01/21/13 21:55
5210E BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
ND mg/L
2.0
1
01/17/13 00:15 01/21/13 19:30
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
0A5 mg/L
0.10
1
01/28/13 10:52 7664-41-7
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
33.0 mg/L
25.0
1
01/26/13 17:15
6310B TOG
Analytical Method: SM 5310B
Total Organic Carbon
4.1 mg/L
1.0
1
01/23/13 21:55 7440-44-0
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 5 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacelabs.com
Project: Permit Renewal 002
Pace Project No.: 92145123
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/21796 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92145123001
METHOD BLANK: 910018
Associated Lab Samples:
Parameter
92145123001
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
5.0
01/23/13 21:13
1,1,2,2-Tetrachloroethane
ug/L
ND
5.0
01/23/13 21:13
1,1,2-Trichloroethane
ug/L
ND
5.0
01/23/13 21:13
1,1-Dichloroethane
ug/L
ND
5.0
01/23/13 21:13
1,1-Dichloroethene
ug/L
ND
5.0
01/23/13 21:13
1,2-Dichloroethane
ug/L
ND
5.0
01/23/13 21:13
1,2-Dichloropropane
ug/L
ND
5.0
01/23/13 21:13
2-Chloroethylvinyl ether
ug/L
ND
10.0
01/23/13 21:13
Acrolein
ug/L
ND
100
01/23/13 21:13
Acrylonitrile
ug/L
ND
50.0
01/23/13 21:13
Benzene
ug/L
ND
5.0
01/23/13 21:13
Bromodichloromethane
ug/L
ND
5.0
01/23/13 21:13
Bromoform
ug/L
ND
5.0
01/23/13 21:13
Bromomethane
ug/L
ND
10.0
01/23/13 21:13
Carbon tetrachloride
ug/L
ND
5.0
01/23/13 21:13
Chlorobenzene
ug/L
ND
5.0
01/23/13 21:13
Chloroethane
ug/L
ND
10.0
01/23/13 21:13
Chloroform
ug/L
ND
5.0
01/23/13 21:13
Chloromethane
ug/L
ND
5.0
01/23/13 21:13
cis-1,3-Dichloropropene
ug/L
ND
5.0
01/23/13 21:13
Dibromochloromethane
ug/L
ND
5.0
01/23/13 21:13
Dichlorod ifluoromethane
ug/L
ND
5.0
01/23/13 21:13
Ethylbenzene
ug/L
ND
5.0
01/23/13 21:13
Methylene Chloride
ug/L
ND
5.0
01/23/13 21:13
Tetrachloroethene
ug/L
ND
5.0
01/23/13 21:13
Toluene
ug/L
ND
5.0
01/23/13 21:13
trans- 1,2-Dichloroethene
ug/L
ND
5.0
01/23/13 21:13
trans- 1,3-Dichloropropene
ug/L
ND
5.0
01/23/13 21:13
Trichloroethene
ug/L
ND
5.0
01/23/13 21:13
Trichlorofluoromethane
ug/L
ND
10.0
01/23/13 21:13
Vinyl chloride
ug/L
ND
5.0
01/23/13 21:13
1,2-Dichloroethane-d4 (S)
%
109
70-130
01/23/13 21:13
4-Bromofluorobenzene (S)
%
94
70-130
01/23/13 21:13
Dibromofluoromethane (S)
%
108
70-130
01/23/13 21:13
Toluene-d8 (S)
%
99
70-130
01/23/13 21:13
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 910019
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 20.1 101 52-162
1,1,2,2-Tetrachloroethane ug/L 20 19.1 96 46-157
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 6 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

p Q�g j /�+�/;QD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aC2A11aiytlGal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wKwpacelatis coot_ Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92145123
LABORATORY CONTROL SAMPLE: 910019
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits
Qualifiers
1,1,2-Trichloroethane
ug/L
20
21.8
109
52-150
1,1-Dichloroethane
ug/L
20
20.4
102
59-155
1,1-Dichloroethene
ug/L
20
19.0
95
1-234
1,2-Dichloroethane
ug/L
20
20.8
104
49-155
1,2-Dichloropropane
ug/L
20
20.3
101
1-210,
2-Chloroethylvinyl ether
ug/L
40
42.9
107
1-305
Acrolein
ug/L
100
138
138
15-152
Acrylonitrile
ug/L
100
116
116
75-132
Benzene
ug/L
20
20.9
104
37-151
Bromodichloromethane
ug/L
20
20.4
102
35-155
Bromoform
ug/L
20
18.3
92
45-169
Bromomethane
ug/L
20
15.1
76
1-242
Carbon tetrachloride
ug/L
20
19.0
95
70-140
Chlorobenzene
ug/L
20
21.0
105
37-160
Chloroethane
ug/L
20
21.4 _
107
14-230
Chloroform
ug/L
20
20.5
102
51-138
Chloromethane
ug/L
20
17.9
90
1-273
cis- 1,3-Dichloropropene
ug/L
20
20.3
101
1-227
Dibromochloromethane
ug/L
20
19.9
99
53-149
Dichlorodifluoromethane
ug/L
20
18.5
92
70-130
Ethylbenzene
ug/L
20
20.2
101
37-162
Methylene Chloride
ug/L
20
21.3
107
1-221
Tetrachloroethene
ug/L
20
20.1
101
64-148
Toluene
ug/L
20
21.0
105
47-150
trans- 1,2-Dichloroethene
ug/L
20
19.4
97
54-156
trans- 1,3-Dichloropropene
ug/L
20
20.1
100
17-183
Trichloroethene
ug/L
20
19.9
100
71-157
Trichlorofluoromethane
ug/L
20
18.7
94
17-181
Vinyl chloride
ug/L
20
19.9
99
1-251
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
90
70-130
Dibromofluoromethane (S)
%
102
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
910020
910021
MS
MSD
92145401001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
24.0
23.0
120
115
46-171
4
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.9
20.0
99
100
73-159
0
1,1,2-Trichloroethane
ug/L
ND
20
20
22.4
22.8
112
114
64-152
2
1,1-Dichloroethane
ug/L
ND
20
20
22.7
22.2
114
111
43-172
3
1,1-Dichloroethene
ug/L
ND
20
20
23.6
22.3
118
112
48-189
6
1,2-Dichloroethane
ug/L
ND
20
20
22.6
22.9
113
114
42-171
1
1,2-Dichloropropane
ug/L
ND
20
20
21.8
21.6
109
108
55-157
1
2-Chloroethylvinyl ether
ug/L
ND
40
40
44.0
45.2
110
113
70-130
3
Acrolein
ug/L
ND
100
100
145
143
145
143
70-130
1 M0
Date: 01/28/2013 04:33 PM
REPORT OF LABORATORY ANALYSIS
Page 7 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

/'+ /I n ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aUe/'V fNwicaf 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wttiwpacefabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92145123
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 910020 910021
Parameter
92145401001
Units Result
MS
Spike
Cone.
MSD
Spike
Cone.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acrylonitrile
ug/L
ND
100
100
121
119
121
119
70-130
2
Benzene
ug/L
ND
20
20
22.4
21.8
112
109
54-163
2
Bromodichloromethane
ug/L
ND
20
20
22.6
22.4
113
112
56-152
1
Bromoform
ug/L
ND
20
20
20.9
20.8
104
104
53-151
0
Bromomethane
ug/L
ND
20
20
21.5
18.8
107
94
10-200
13
Carbon tetrachloride
ug/L
ND
20
20
24.5
23.1
122
116
41-175
6
Chlorobenzene
ug/L
ND
20
20
22.7
22.5
113
112
67-152
1
Chloroethane
ug/L
ND
20
20.
23.1
22.6
115
113
23-200
2
Chloroform
ug/L
ND
20
20
22.8
22.7
114
113
51-166
1
Chloromethane
ug/L
ND
20
20
20.7
21.1
104
106
40-175
2
cis- 1,3-Dichloropropene
ug/L
ND
20
20
22.8
22.1
114
111
38-146
3
Dibromochloromethane
ug/L
ND
20
20
22.5
22.3
113
112
65-144
1
Dichlorodifluoromethane
ug/L
ND
20
20
22.5
21.4
112
107
70-130
5
Ethylbenzene
ug/L
ND
20
20
22.6
21.9
113
109
57-152
3
Methylene Chloride
ug/L
ND
20
20
22.7
22.2
112
109
40-167
2
Tetrachloroethene
ug/L
ND
20
20
23.6
22.6
118
113
59-155
4
Toluene
ug/L
ND
20
20
22.5
22.1
113
111
47-162
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.9
21.2
110
106
47-178
3
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.1
21.9
111
109
39-148
1
Trichloroethene
ug/L
ND
20
20
22.4
22.1
112
110
60-153
2
Trichlorofluoromethane
ug/L
ND
20
20
25.1
23.8
125
119
42-199
5
Vinyl chloride
ug/L
ND
20
20
22.1
21.8
111
109
46-176
2
1,2-Dichloroethane-d4 (S)
%
105
105
70-130
4-Bromofluorobenzene (S)
%
91
91
70-130
Dibromofluoromethane (S)
%
103
104
70-130
Toluene-d8 (S)
%
100
100
70-130
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 8 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalyfical
w5 w.pacela6s.ccm
Project: Permit Renewal 002
Pace Project No.: 92145123
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/20422 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92145123001
METHOD BLANK: 907332
Matrix: Water
Associated Lab Samples:
92145123001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
bis(2-Chloroethyl) ether
ug/L
ND
5.0
01/24/13 05:12
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
01/24/13 05:12
Di-n-butylphthalate
ug/L
ND
5.0
01/24/13 05:12
2,4,6-Tribromophenol (S)
%
88
10-137
01/24/13 05:12
2-Fluorobiphenyl (S)
%
71
15-120
01/24/13 05:12
2-Fluorophenol (S)
%
40
10-120
01/24/13 05:12
Nitrobenzene-d5 (S)
%
70
10-120
01/24/13 05:12
Phenol-d6 (S)
%
27
10-120
01/24/13 05:12
Terphenyl-d14 (S)
%
93
11-131
01/24/13 05:12
LABORATORY CONTROL SAMPLE:
Parameter
907333
Spike LCS
Units Conc. Result
bis(2-Chloroethyl) ether
ug/L 50 49.1
bis(2-Ethylhexyl)phthalate
ug/L 50 50.6
Di-n-butylphthalate
ug/L 50 45.4
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 907334
92145230001
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
907335
MS
Result
bis(2-Chloroethyl) ether
ug/L
ND
100
100
92.3
bis(2-Ethylhexyl)phthalate
ug/L
ND
100
100
97.3
Di-n-butylphthalate
ug/L
ND
100
100
89.3
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Qualifiers
LCS
% Rec
% Rec
Limits
98
12-158
101
8-158
91
1-118
105
10-137
77
15-120
44
10-120
83
10-120
31
10-120
92
11-131
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
51.9
92
52
12-158
56
87.3
97
87
8-158
11
77.4
89
77
1-118
14
88
76
10-137
72
35
15-120
49
24
10-120
71
40
10-120
40
19
10-120
89
71
11-131
Qual
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 9 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

(�IaneAndlKical
www.pacelabs.com
Project: Permit Renewal 002
Pace Project No.: 92145123
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: WET/23893 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92145123001
METHOD BLANK: 908610
Associated Lab Samples: 92145123001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
908611
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 908612
Parameter Units
Total Suspended Solids mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 01/21/13 21:52
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 266 106 80-120
92145028002 Dup
Result Result RPD Qualifiers
ND ND
SAMPLE DUPLICATE: 908613
92145123001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 49.8 51.2 3
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 10 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

�;aceAnalyfical'
www.pacelatrs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Permit Renewal 002
Pace Project No.: 92145123
QC Batch: WET/23853
QC Batch Method: SM 5210B
Associated Lab Samples: 92145123001
METHOD BLANK: 906911
Associated Lab Samples: 92145123001
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 906912
Parameter Units
BOD, 5 day mg/L
SAMPLE DUPLICATE: 906913
Parameter Units
BOD, 5 day mg/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 5210E BOD, 5 day
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 01/21/1319:30
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 173 87 84.5-115.4
92145159004 Dup
Result Result RPD
473 458
Qualifiers
3
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 11 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Q n
A/ I aCGalXi /+ aI
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
"..pacelabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92145123
QC Batch: WETA/14365
Analysis Method:
EPA 350.1
QC Batch Method: EPA 350.1
Analysis Description:
350.1 Ammonia
Associated Lab Samples: 92145123001
METHOD BLANK: 911755
Matrix: Water
Associated Lab Samples: 92145123001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Nitrogen, Ammonia
mg/L
ND 0.10 01/28/13 10:45
LABORATORY CONTROL SAMPLE:
911756
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/L
5 4.9
98
90-110
MATRIX SPIKE SAMPLE:
911757
92145107001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/L
ND
5 5.2
103
90-110
MATRIX SPIKE SAMPLE:
911759
92145181002 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/L
29.6
5 34.7
102
90-110
SAMPLE DUPLICATE: 911758
92145113001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Nitrogen, Ammonia
mg/L
2.6
2.6
2
SAMPLE DUPLICATE: 911760
92145189001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Nitrogen, Ammonia
mg/L
ND
ND
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 12 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pgceiabs.com
Project: Permit Renewal 002
Pace Project No.: 92145123
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: WETA/14358 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92145123001
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 911650
Matrix: Water
Associated Lab Samples: 92145123001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Chemical Oxygen Demand
mg/L
ND
25.0
01/26/13 17:15
LABORATORY CONTROL SAMPLE:
911651
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
750
724
97
90-110
MATRIX SPIKE SAMPLE:
911652
92144938007
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
4180
7500
12600
113
75-125
MATRIX SPIKE SAMPLE:
911654
92145009001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
ND
750
802
105
75-125
SAMPLE DUPLICATE: 911653
92144938007
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Chemical Oxygen Demand
mg/L
4180
4940
17
SAMPLE DUPLICATE: 911655
92145009001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Chemical Oxygen Demand
mg/L
ND
35.0
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 13 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
wwwpacelabscom
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Permit Renewal 002
Pace Project No.:
92145123
QC Batch:
WETA/14330 Analysis Method: SM 5310B
QC Batch Method:
SM 5310B Analysis Description: 5310B TOC
Associated Lab Samples:
92145123001
METHOD BLANK: 909543
Associated Lab Samples: 92145123001
Parameter
Units
Total Organic Carbon
mg/L
LABORATORY CONTROL SAMPLE:
909544
Parameter
Units
Total Organic Carbon
mg/L
MATRIX SPIKE SAMPLE:
909545
Parameter
Units
Total Organic Carbon
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 01/23/1319:19
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
25 23.8 95 90-110
92144545036 Spike MS MS % Rec
Result ' Conc. Result % Rec Limits Qualifiers
19.2 25 57.7 154 75-125 M6
MATRIX SPIKE SAMPLE: 909547
92145316001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 3.9 25 29.0 100 75-125
SAMPLE DUPLICATE: 909546
Parameter Units
Total Organic Carbon mg/L
92144545036 Dup
Result Result RPD Qualifiers
19.2 16.9 13
SAMPLE DUPLICATE: 909548
92145316002 Dup
Parameter Units Result Result RPD Qualifiers
Total Organic Carbon mg/L 4.3 4.1 5
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 14 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

5.5nemalXical'
!!i—_pacelabs.mM
!r
Project: Permit Renewal 002
Pace Project No.: 92145123
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
Date: 01/28/2013 04:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 16

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aneAnalyfical 205 East Meadow Road - Suite A 2225 Riverside Dr.
[e-mail] Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Permit Renewal 002
Pace Project No.: 92145123
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92145123001
002
EPA 625
0EXT/20422 EPA 625
MSSV/7244
92145123001
002
EPA 624
MSV/21796
92145123001
002
SM 2540D
WET/23893
92145123001
002
SM 5210B
WET/23853 SM 5210B
WET/23854
92145123001
002
EPA 350.1
WETA/14365
92145123001
002
SM 5220D
WETA/14358
92145123001
002
SM 5310B
WETA/14330
Date: 01/28/2013 04:33 PM REPORT OF LABORATORY ANALYSIS Page 16 of 16
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

CHAIN -OF -CUSTODY I Analytical Request Document
aceAnalytiaal0 ....
. '
The Chain -of -Custody is a
LEGAL DOCUMENT. All relevant fields must be completed accurately.
.
' ' ` www_pacelahs.cam
Page
of
Section A
Section B
Section C
Required Client Information:
Required Project Information:
Invoice Information:
-
CompanT- flp,
RepartTo:
Attention:
1
5102'
Address: .
C 1 A `
%°:/6 �'✓4J.i �trn� �4. ,�+i ri G
Co To:
Copy
�
1Q•�-s H to .
Company Name:
s�elfy A�i a /,f�
Gey v eaq•.oi
Address:
NPDES'. - r' GROUND WATER ' ''"DRINKING WATER '
Email To:
Purchase Order No.:
Pace Quote
) UST r RCRA '
�' OTHER
Reference:
Phone: Fa:
gg
�pf•' 'may aZ �� 7'. yl !
J ro P act Name:
Pace Project''''"
Manager:
:: Site:Locakioh:
Re Requested Due DateffAT:
q
Project Number.
..
file : _
Pace Pro # }} (
;''` :'STATE:`
L-
_
uesfedAna`sis:Eilteied..1N)".°;'>::
Section D Matrix Codes .
Requireddient Information MATRIX'/CODE
m
�.
:-COLLECTED - -
Preservatives
??w.
�r.'
..
., ...:...
Drinking Water DW '
m
z
O
Water
Waste Water
Product
WT
WW
P :
v
�.
.m
COMPOSITE
S.t. ART
COMPUSrt-E
ENDIGRAB
W
'':'
P� r in.T
/
' Sall/Solid
Sj ..
C7.;
.. ; ....t '.
- ... ...
Q
W
7-.:-
�'t%tCti✓®
SAMPLE ID Oil
Wlpe
OL
WP
�;
�.
_
F
4
W
,.:�
.�
p,
�d
. (A-Z, 0-9 ! :) Al, • :
'
.AR
Lu
0 .
". W
Z
':F,"
.'.
r...
. .
Sample IDS MUST BE UNIQUE Tissue
Other
TS'
OT'
O
o
w.'
w
[a—
O
v
m
A
U
X:
O
c•
CA
C
t0
?0
F
rn
DATE
TIME
DATE
TIME
a
=
T
U
=
n3
Z
m
Z
..
O
:Q:
-y:
.t<
•Pace Project No./ Lab I.D.
�2
! 111�
0730
1
✓
✓
co
-2,
73>
�yl
s
e �Z
4
id/
a73o
9
71
ADDITIQNA4.COMMENTSBY.lAfFILIATION':1)A7E'>
D
ACE FA BY/AFFiLfATI„
"
,
• >: a3M.E'>`
SAMPLE CONDITIONS
C
V'QjC0.l
YY­
i�e1� �oZs. Sae+ Ie.4:sr
`X.
SAfi7P..LER":[fAMt4ND;SIGNAT.URE`:::
ORIGINAL
. .
,
..
PRINT Name of SAMPLER:
`y' • 6 C.'.r,. v +.
n "
i
v
m }
`
SIGNATU.REofSAMPLER:
DATE Signed
(MMIDOMy):
F
E
46mpor By signing this form you are accepting Pace's NET 30 daypayment terms and eigreeing to late charges of 1.5 % per month for: as not paidwithin 30"days,
F-ALL-Q-020rev.07, '15--, "07

Document Name: Document Revised: October 31, 2012
ceArtatyUcalW Sample Condition Upon Receipt ($CUR) Rage 1 of 2
Dodument_Number., Issuing Authority: .
F-CHR-CS-03-rev.08 Pace Huntersville Quality Office
Client Name: ` - Project #
Where Received: EVAuntersville ❑ Asheville %Eden ❑ Raleigh
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial❑ Pace Other
Custody Seal on Cooler/Box Present: ❑ yes 4� no Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble Wrap E2"Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1101 T71 Type of Ice-G Blue None
Temp Correction Factor 11101: No Correction T1102: No Correction
❑ Soepiesonlce, cooling process has begun
Corrected Cooler Temp.: C
Biological Tissue is Frozen: Yes No NIA
g
Date and (► ' is f
�oxaml�lng
contents:
-Temp should be above freezing•to 6°C
Comments:
Chain of Custody Present:
s LINo
❑NIA
1.
Chain of Custody Filled Out:
s ONO
❑N/A
2.
Chain of Custody Relinquished:
Yes ❑No
❑NIA
3.
Sampler Name & Signature on COC:
Yes ❑No
❑NIA
4.
Samples Arrived within Hold Time:
Yes ❑No
CIN/A
5.
Short Hold Time Analysis <72hr :
94, ❑No
❑N/A
6.
Rush Turn Around Time Requested:
Dyes No
❑N!A
7.
Sufficient Volume:
P4, ❑No
❑NIA
S.
Correct Containers Used:
.Qr.. ❑No
❑NIA
J.
-Pace Containers Used:
RIY'es ONO
❑NIA
Containers Intact:
es []No
❑NIA
10.
Filtered volume received for Dissolved tests
❑Yes ❑No
C41A
11.
Sample Labels match COC:
❑Yes o
❑N/A
12.
CA Vki l
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
❑No
❑NIA
13.
All containers needing preservation are found to be In
VfYY
[]No
❑ NIA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
[]Yes []No
Initial when completed
Samples checked for dechlorination:
es ❑No
❑NIA
14.
Headspace In VOA Vials ( >6mm):
❑Yes 13K,
❑NIA
15.
Trip Blank Present:
❑Yes ❑No
N/
16.
Trip Blank Custody Seals Present
❑Yes ❑No
Pace Trip Blank Lot # if purchased):
Client Notification/ Resolution: Feld Data Required? Y / N
Person Contacted: DatelTime:
1 Comments/ Resolution:
SCURF Review: Date: 1 I� SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification office ( Le out of hold, incorrect preservative, out of temp, incorrect containers)

o�o� wAT FqQ�
MIiG
Mr. Timothy G. Mathis
Manufacturing Manager
PPG Industries Fiber Glass Products, Inc.
940 Washburn Road
Shelby, North Carolina 28150
Dear Mr. Mathis:
Michael F. Easley
Governor
William G. Ross, Jr., Secretary
North Carolina Department of Environment and Natural Resources
P 17 Cl�
Ca
October 13, 2008
OCT 2 2 2008
�ti� ��i�v�C• fir;=��t.,
Y02-S'urface Water
Subject: Issuance of NPDES Permit NC0004685
Shelby Facility
Cleveland County
Division personnel have reviewed and approved your application for renewal of the subject permit. -
Accordingly, we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North
Carolina and the U.S. Environmental Protection Agency dated October 15, 2007 (or as subsequently amended).
This final permit includes no major changes from the draft permit sent to you on August 13, 2008.
If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to
you, you have the right to an adjudicatory hearing upon written request within thirty (30) days following receipt'of this
letter. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina
General Statutes, and filed with the Office of Administrative Hearings (6714 Mail Service Center, Raleigh, North
Carolina 27699-6714). Unless such demand is made, this decision shall be final and binding.
Please note that this permit is not transferable except after notice to the Division. The Division may require
modification or revocation and reissuance of the permit. This permit does not affect the legal requirements to obtain
other permits which may be required by the Division of Water Quality or permits required by the Division of Land
Resources, the Coastal Area Management Act or any other Federal or Local governmental permit that may be
required. If you have any questions concerning this permit, please contact Sergei Chernikov at telephone number
[phone].
Sincerely,
s
')� Coleen H. Sullins
cc: Central File r
Mooiee svtil�;Regioial Office, Surface Water Protection
EPA Region IV
NPDES Files
N. C. Division of Water Quality / NPDES Unit Phone: [phone]
1617 Mail Service Center, Raleigh, NC 27699-1617 fax: [phone]
Internet: h2o.enr.state.nc.us DENR Customer Service Center: 1 800 623-7748

Permit NC0004685
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
PPG Industries Fiber Glass Products, Incorporated
is hereby authorized to discharge wastewater and stormwater from a facility located at
Shelby Facility
On NCSR 1313
West of Shelby
Cleveland County
to receiving waters designated as Brushy Creek and Overflow Branch in the Broad River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts
I, II, III, and IV hereof.
The permit shall become effective November 1, -2008.
This permit and the authorization to discharge shall expire at midnight on August 31, 2013.
Signed this day October 13, 2008.
Y/\
'Coleen H. Sullins, Director
Division of Water Quality
By Authority of the Environmental Management Commission

Permit NC0004685
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES .Permits issued to this facility, whether for operation or discharge are hereby
revoked, and as of this issuance, any previously issued permit bearing this number is ,no longer
effective. Therefore, the exclusive authority to operate and discharge from this facility arises under the
permit conditions, requirements, terms, and provisions included herein.
PPG Industries Fiber Glass Products, Incorporated is hereby authorized to:
1. Continue operation of a 1.3 MGD wastewater treatment facility consisting of:
• an overflow/ storage basin;
• bar screen and grinder;
• an influent wet well with lime addition;
• influent pumps;
• a surge tank;
• an equalization tank with aluminum chloride addition;
• a flash mix tank;
• coagulant and polymer addition;
• two primary clarifiers;
• two aeration basins with bentonite clay addition;
• a splitter box and floc tank;
• three secondary clarifiers with ferric chloride addition;
• a sand filter;
• an effluent holding tank;
• a sludge thickener tank; and
• a sludge belt press.
These treatment works are located at PPG's Shelby facility on NCSR 1313, west of Shelby, .
Cleveland County and discharge treated process wastewater, stormwater, sanitary sewage,
cooling water, and landfill leachate, at the location specified on the attached map, through
outfall 001 into Brushy Creek, a class C water in the Broad River Basin; and
2. Discharge non -contact cooling water and stormwater through outfall 002, at the location
specified on the attached map, into Overflow Branch, a class C water in the Broad River Basin.

PPG Industries: NC0004685
"� Faculty :�•
Location
i
USGS Quad` Name: Shelby SE/SW S 1 f
Receiving Stream: See Above
Stream Class: C r
w I
Subbasin., Broad = 030804 I �10kt{�
■
Not to S CALE

Permit NC0004685
A. (1) Effluent Limitations and Monitoring Requirements [001]
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is
authorized to discharge from Outfall 001. Such discharges shall be limited and monitored by the
Permittee as specified below:
EFFLUENT LIMITATIONS
MONITORING
REQUIREMENTS
PARAMETER
Monthly
Daily
Measurement
Sample
Sample
Average
Maximum
Frequency
Tye
Location'
Flow
._.----............... —_._.......
1.3 MGD
..... ........... _........ ............
_..__.... _._.._.._-----......---.._._.__._
Continuous
Recording
.... - --
Influent or
Effluent
—......._._.__.._..__..__.._........._...
BOD, 5-day, 200C (mass)
... _.......----------........__..--...__._..._...-----
__.... ................. _......... _.___.
pounds/day
...- -- ... - —
....
pounds/day
— ...-- ...-- .......................
Weekly
Composite
Effluent
BOD, 5-day, 20oC
(concentration)
20.0 mg/L
30.0 mg/L
Weekly
Composite
Effluent
Total Suspended Solids
---._.......__._..._...-------.— ...... _.....
20.0 mg/L
146.0 mg/L
Weekly
Composite
Effluent
_-----
65.0
97.5
NH3-N (mass)
Weekly
Composite
Effluent
pounds/day
pounds/day
-- ----
---...---- -
Effluent
NH3-N (concentration)
6.0 mg/L 9.0 mg/L
Weekly
Composite
Dissolved Oxygen
...... _........ _ --..._._..._._.........._.......
Daily Average >_ 5.0 mg/L
-- -------------
Daily
Grab
Effluent
—._..__....._.._._...._.._.. __.....__—_........... _....._..---...-
Dissolved Oxygen (instream)
Monitor & Report
See Note 1
Grab
U,D
p _
H
>_ 6.0 and < 9.0 standard units
Daily
Grab
Effluent
Temperature, oC
-- - ._.._.__...._...--......... _—.._._.__...
---.............. _..._..._....—.._—
.._.._—._._._.......--................. _.._.....
Daily
--- ..__...._.. --- ......__.
Grab
_.._..........._...............__....
Effluent
— -- - —
Temperature, OC (instream)
See Note 1
Grab
U,D
Fecal Coliform
Weekly
Grab
Effluent
_...._..
Total Nitrogen
--
Quarterly
Composite
.._...... _._
Effluent
Total Phosphorus
--........_...._._.._.._._..._._.—_...-----.._...._.._......_.._-- ._
...__.....__... - ---..............................
....... _._......_......-----.._..........
Quarterly
............ __....__................. _..._...._...._..........._.........._....
Composite
- - -_ ..
Effluent
-........_..---._....._._._—..
Conductivity
____.... _....
See Note 1
Grab
--
U,D
Oil and Grease
10.0 mg/L
15.0 mg/L
Weekly
Grab
Effluent
Total Lead
Monthly
Composite
Effluent
Fluoride
....... _......._........_...._.._...-- - -----.._..._...
----.......... - - —--......--
5.4 mg/L
..._._....-- - _......._.._._
Weekly
............. -- .._..-- -
Composite
— - —....- -- -
Effluent
--.._—....._-.................__...
Total Zinc
2/Month
Composite
Effluent
Total Copper
2/Month
Composite
—Effluent
_
Chloride
2/Month
Composite
Effluent
Total Residual Chlorine2
---._... _.._........................................... _........ -.._....._.__.................... _._....
... ....... _.......... __... _........... .. .............. _........ --..__._
17 µg/L
..._....... ............-............... .... _...-........ --... _.....
Weekly
....... _..--.---_.............. ... ................ .._...._.._..........__..__._.......
Grab
........_._..._......_.—.
Effluent
....... —_....__.
Chronic Toxicitys
Quarterly
Composite
Effluent
NOTES
1 U: upstream at NCSR 1323. D: downstream at NCSR 1305. Instream samples shall be grab
samples collected three times per week during June, July, August, and September and weekly
during the remainder of the year.
2 The facility shall report all effluent TRC values reported by a NC certified laboratory including field
certified. However, effluent values below 50 µg/ L will be treated as zero for compliance purposes.
Monitoring and effluent limitation for TRC apply only if chlorine is added fro disinfection.
3 Chronic Toxicity (Ceriodaphnia) P/F @ 33%; January, April, July, October [see A. (5)].
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE
AMOUNTS.

Permit NC0004685
A. (2) Effluent Limitations and Monitoring Requirements [002]
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is authorized to
discharge from Outfall 002. Such discharges shall be limited and monitored by the Permittee as specified below:
PARAMETER
EFFLUENT LIMITATIONS
MONITORING REQUIREMENTS
Monthly
Average
Daily
Maximum
Measurement
__Frequency
Sample
Tye
Sample
Location
Flow (MGD)
Semi -Annually
Estimate
Effluent
-......_........ -........ __._.._._.._.._�
Temperature
-- ------------ -
See Note 1
— - ---...._.. ---
Semi -Annually
-
Grab
Effluent
Total Residual Chlorine2
28 µg/L
Semi -Annually
Grab
Effluent
pH
> 6.0 and < 9.0 standard units
Semi -Annually
Grab
Effluent
NOTES:
1 The temperature of the effluent shall be such as not to cause an increase in the temperature of the
receiving stream of more than 2.80C and in no case cause the ambient water temperature to exceed
29oC.
2 The facility shall report all effluent TRC values reported by a NC certified laboratory including field
certified. However, effluent values below 50 µg/L will be treated as zero for compliance purposes.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE
AMOUNTS.
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER.
A. (3) Biocide Condition
The Permittee shall not use any biocides except those approved in conjunction with the
permit application. The Permittee shall notify the Director in writing not later than ninety
(90) days prior to instituting use of any additional biocide used in cooling systems which
may be toxic to aquatic life other than those previously reported to the Division of Water
Quality. Such notification shall include completion of Biocide Worksheet Form 101 and a
map locating the discharge point and receiving stream.
A. (4) Disinfection Condition - Outfall 001
In the event that violations of North Carolina's water quality standards for fecal coliform
occur as a result of this discharge, disinfection will immediately be required and the permit
amended to establish a fecal coliform effluent limitation.

Permit NC0004685
A. (5) Chronic Toxicity Permit Limit (Quarterly) - Outfall 001
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 33%.
The permit holder shall perform at a minimum,guarterlu monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent
versions. The tests will be performed during the months of January, April, July and October. Effluent
sampling for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment
processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the
permit limit, then multiple -concentration testing shall be performed at a minimum, in each of the two
following months as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test
Procedure" (Revised -February 1998) or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed. If reporting pass/fail results using the
parameter code TGP3B, DWQ Form AT-1 (original) is sent to the below address. If reporting Chronic Value
results using the parameter code THP313, DWQ Form AT-3 (original) is to be sent to the following address:
Attention: NC DENR / DWQ / Environmental Sciences Section
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Section no later than 30
days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the
facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No
Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences section at
the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include
alternate monitoring requirements or limits.
If the Permittee monitors any pollutant more frequently then required by this permit, the results of such
monitoring shall be included in the calculation & reporting of the data submitted on the DMR & all AT Forms
submitted.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an
invalid test and will require immediate follow-up testing to be completed no later than the last day of the month
following the month of the initial monitoring.

NPDES Permit Standard Conditions
Page 1 of 16
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
Section A. Definitions
2/Month
Samples are collected twice per month with at least ten calendar days between sampling events.
3/Week
Samples are collected three times per week on three separate calendar days.
Act or "the Act"
The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended, 33 USC 1251, et. seq.
Annual Average
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar year. In the case of fecal
coliform, the geometric mean of such discharges.
Arithmetic Mean
The summation of the individual values divided by the number of individual values.
Bypass
The known diversion of waste streams from any portion of a treatment facility including the collection system, which
is not a designed or established or operating mode for the facility.
Calendar Day
The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any
consecutive 24-hour period that reasonably represents the calendar day may be used for sampling.
Calendar Quarter
One of the following distinct periods: January through March, April through June, July through September, and
October through December.
Composite Sample
A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 nil in
such a manner as to result in a total sample representative of the wastewater discharge during the sample period. The
Director may designate the most appropriate method (specific number and size of aliquots necessary, the time
interval between grab samples, etc.) on a case -by -case basis. Samples may be collected manually or automatically.
Composite samples may be obtained by the following methods:
(1) Continuous: a single, continuous sample collected over a 24-hour period proportional to the rate of flow.
(2) Constant time/variable volume: a series of grab samples collected at equal time intervals over a 24 hour
period of discharge and combined proportional to the rate of flow measured at the time of individual sample
collection, or
(3) Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period
with the time intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow recorder and
totalizer, and the preset gallon interval between sample collection fixed at no greater than 1/24 of the
expected total daily flow at the treatment system, or
(4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period at
a constant time interval. Use of this method requires prior approval by the Director. This method
may only be used in situations where effluent flow rates vary less than 15 percent. The following
restrictions also apply:
➢ Influent and effluent grab samples shall be of equal size and of no less than 100 milliliters
Version 10/10/2007

NPDES Permit Standard Conditions
Page 2of16
➢ Influent samples shall not be collected more than once per hour.
➢ Permittees with wastewater treatment systems whose detention time < 24 hours shall collect effluent
grab samples at intervals of no greater than 20 minutes apart during any 24-hour period.
➢ Permittees with wastewater treatment systems whose detention time exceeds 24 hours shall collect
effluent grab samples at least every X hours [X = days detention time] over a 24-hour period. Effluent
samples shall be collected at least every six hours; there must be a minimum of four samples during a 24-
hour sampling period.
Continuous flow measurement
Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance
activities on the flow device.
Daily Discharge
The discharge of a pollutant measured during a calendar dap or any 24-hour period that reasonably represents the
calendar day for purposes of sampling. For pollutants measured in units of mass, the "daily discharge" is calculated as
the total mass of the pollutant discharged over the day. The "daily discharge" concentration comprises the mean
concentration for a 24-hour sampling period as either a composite sample concentration or the arithmetic mean of all
grab samples collected during that period. (40 CFR 122.2)
Daily Maximum
The highest "daily discharge" for conventional and other non -toxicant parameters. NOTE: Permittees may not
submit a "daily average" calculation [for determining compliance with permit limits] for toxicants. See the relevant
Federal effluent guideline[s] for the appropriate calculation interval.
Daily Sampling
Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the
permit. The Division expects that sampling shall be conducted on weekdays except where holidays or other
disruptions of normal operations prevent weekday sampling. If sampling is required for all seven days of the week
for any permit parameter(s), that requirement will be so noted on the Effluent Limitations and Monitoring Page(s).
DWO or "the Division"
The Division of Water Quality, Department of Environment and Natural Resources.
EMC
The North Carolina Environmental Management Commission.
Facility Closure
The cessation of wastewater treatment at a permitted facility, or the cessation of all activities that require coverage
under the NPDES. Completion of facility closure will allow this permit to be rescinded.
Geometric Mean
The Nth root of the product of the individual values where N = the number of individual values. For purposes of
calculating the geometric mean, values of "0" (or "< [detection level]") shall be considered = 1.
Grab Sample
Individual samples of at least 100 ml collected over a period of time not exceeding 15 minutes. Grab samples can be
collected manually: Grab samples must be representative of the discharge (or the receiving stream, for instream
samples).
Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
Version 10/10/2007

NPDES Permit Standard Conditions
Page 3 of 16
Instantaneous flow measurement
A measure of flow taken at the time of sampling, when both the sample and flow will be representative of the total
discharge.
Monthly Average (concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar month. In the case of fecal
coliform, the geometric mean of such discharges.
Permit Issuing Authority
The Director of the Division of Water Quality.
Quarterly Average concentration limit)
The average of all samples taken over a calendar quarter.
Severe property damage
Substantial physical damage to property, damage to the treatment facilities which causes them to become inoperable,
or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage excludes economic loss caused by delays in production.
Toxic Pollutant:
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
U aset
An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance with
permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance caused by
operational error, improperly designed treatment facilities, inadequate treatment facilities, lack of preventive
maintenance, or careless or improper operation.
Weekly Average (concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar week. In the case of fecal
coliform, the geometric mean of such discharges.
Section B. General Conditions
1. Duty to Comply
The Permittee must comply with all conditions of this permit. Any permit noncompliance constitutes a violation
of the Clean Water Act and is grounds for enforcement action; for permit termination, revocation and reissuance,
or modification; or denial of a permit renewal application [40 CFR 122.41].
a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants and with standards for sewage sludge use or disposal established under
section 405(d) of the Clean Water Act within the time provided in the regulations that establish these
standards or prohibitions or standards for sewage sludge use or disposal, even if the permit has not yet been
modified to incorporate the requirement.
b. The Clean Water Act provides that any person who violates section 301, 302, 306, 307, 308, 318 or 405 of the
Act, or any permit condition or limitation implementing any such sections in a permit issued under section
402, or any requirement imposed in a pretreatment program approved under sections 402(a)(3) or 402(b)(8)
of the Act, is subject to a civil penalty not to exceed $25,000 per day for each violation. [40 CFR 122.41 (a)
(2)]
c. The Clean Water Act provides that any person who negligently violates sections 301, 302, 306, 307, 308, 318, or
405 of the Act, or any condition or limitation implementing any of such sections in a permit issued under
Version 1011012007

NPDES Permit Standard Conditions
Page 4 of 16
section 402 of the Act, or any requirement imposed in a pretreatment program approved under section
402(a)(3) or 402(b)(8) of the Act, is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment of not more than 1 year, or both. In the case of a second or subsequent conviction for a
negligent violation, a person shall be subject to criminal penalties of not more than $50,000 per day of
violation, or by imprisonment of not more than 2 years, or both. [40 CFR 122.41 (a) (2)]
d. Any person who knosvin,gyl violates such sections, or such conditions or limitations is subject to criminal
penalties of $5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. In
the case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal
penalties of not more than $100,000 per day of violation, or imprisonment of not more than 6 years, or both.
[40 CFR 122.41 (a) (2)]
e. Any person who knowingly violates section 301, 302, 303, 306, 307, 308, 318 or 405 of the Act, or any permit
condition or limitation implementing any of such sections in a permit issued under section 402 of the Act,
and who knows at that time that he thereby places another person in imminent danger of death or serious
bodily injury, shall, upon conviction, be subject to a fine of not more than.$250,000 or imprisonment of not
more than 15 years, or both. In the case of a second or subsequent conviction for a knowing endangerment
violation, a person shall be subject to a fine of not more than $500,000 or by imprisonment of not more than
30 years, or both. An organization, as defined in section 309(c)(3)(B)(iii) of the CWA, shall, upon conviction
of violating the imminent danger provision, be subject to a fine of not more than $1,000,000 and can be fined
up to $2,000,000 for second or subsequent convictions. [40 CFR 122.41 (a) (2)]
f. Under state law, a civil penalty of not more than $25,000 per violation may be assessed against any person
who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North
Carolina General Statutes § 143-215.6A]
g. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302,
306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such
sections in a permit issued under section 402 of this Act. Admitistrative penalties for Class I violations are
not to exceed $10,000 per violation, with the maximum amount of any Class I penalty assessed not to exceed
$25,000. Penalties for Class II violations are not to exceed $10,000 per day for each day during which the
violation continues, with the maximum amount of any Class II penalty not to exceed $125,000. [40 CFR
122.41 (a) (3)]
2. Duty to Mitigate
The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in
violation of this permit with a reasonable likelihood of adversely affecting human health or the environment [40
CFR 122.41 (d)].
Civil and Criminal Liability
Except as provided in permit conditions on "Bypassing" (Part II. C. 4), "Upsets" (Part II. C. 5) and "Power
Failures" (Part II. C. 7), nothing in this permit shall be construed to relieve the Permittee from any
responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309
of the Federal Act, 33 USC 1319. Furthermore, the Permittee is responsible for consequential damages, such as
fish kills, even though the responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee
from any responsibilities, liabilities, or penalties to which the Permittee is or may be subject to under NCGS 143-
215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
Version 1011012007

NPDES Permit Standard Conditions
Page 5 of 16
5. Property Rights
The issuance of this permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor
any infringement of Federal, State or local laws or regulations [40 CFR 122.41 (g)].
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical structures or
facilities or the undertaking of any work in any navigable waters.
7. Severability
The provisions of this permit are severable. If any provision of this permit, or the application of any provision of
this permit to any circumstances, is held invalid, the application of such provision to other circumstances, and the
remainder of this permit, shall not be affected thereby [NCGS 150B-23].
8. Duty to Provide Information
The Permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any information which the
Permit Issuing Authority may request to determine whether cause exists for modifying, revoking and reissuing, or
terminating this permit or to determine compliance with this permit. The Permittee shall also furnish to the
Permit Issuing Authority upon request, copies of records required by this permit [40 CFR 122.41 (h)].
9. Duty to Reapply
If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit, the
Permittee must apply for and obtain a new permit [40 CFR 122.41 (b)].
10. Expiration of Permit
The Permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the Permittee shall submit such information, forms, and
fees as are required by the agency authorized to issue permits no later than 180 days prior to the expiration date.
Any Permittee that has not requested renewal at least 180 days prior to expiration, or any Permittee that does not
have a permit after the expiration and has not requested renewal at least 180 days prior to expiration, will subject
the Permittee to enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and certified
[40 CFR 122.41 (k)].
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible
corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in
charge of a principal business function, or any other person who performs similar policy or decision
making functions for the corporation, or (b) the manager of one or more manufacturing, production, or
operating facilities, provided, the manager is authorized to make management decisions which govern the
operation of the regulated facility including having the explicit or implicit duty, of making major capital
investment recommendations, and initiating and directing other comprehensive measures to assure long
term environmental compliance with environmental laws and regulations; the manager can ensure that
the necessary systems are established or actions taken to gather complete and accurate information for
permit application requirements; and where authority to sign documents has been assigned or delegated
to the manager in accordance with corporate procedures .
(2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or
ranking elected official [40 CFR 122.22].
Version 1011012007

NPDES Permit Standard Conditions
Page 6of16
b. All reports required by the permit and other information requested by the Permit Issuing Authority shall be
signed by a person described in paragraph a. above or by a duly authorized representative of that person. A
person is a duly authorized representative only if:
1. The authorization is made in writing by a person described above;
2. The authorization specified either an individual or a position having responsibility for the overall
operation of the regulated facility or activity, such as the position of plant manager, operator of a well or
well field, superintendent, a position of equivalent responsibility, or an individual or position having
overall responsibility for environmental matters for the company. (A duly authorized representative may
thus be either a named individual or any individual occupying a named position.); and
3. The written authorization is submitted to the Permit Issuing Authority [40 CFR 122.22]
c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate
because a different individual or position has responsibility for the overall operation of the facility, a new
authorization satisfying the requirements of paragraph (b) of this section must be submitted to the Director
prior to or together with any reports, information, or applications to be signed by an authorized
representative [40 CFR 122.22]
d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the
following certification [40 CFR 122.22]:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the
Permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned
changes or anticipated noncompliance does not stay any permit condition [40 CFR 122.41 (0].
13. Permit Modification. Revocation and Reissuance. or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the
permit, revoking and reissuing the permit, or terminating the permit as allowed by the laws, rules, and regulations
contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina
Administrative Code, Subchapter 2H .0100; and North Carolina General Statute 143-215.1 et. al.
14. Annual Administering and Compliance Monitoring Fee Requirements
The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being
billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 21-1.0105 (b) (2)
may cause this Division to initiate action to revoke the permit.
Section C. Operation. and Maintenance of Pollution Controls
Certified Operator
Upon classification of the permitted facility by the Certification Commission, the Permittee shall employ a
certified water pollution control treatment system operator in responsible charge (ORC) of the water pollution
control treatment system. Such operator must hold a certification of the grade equivalent to or greater than the
classification assigned to the water pollution control treatment system by the Certification Commission. The
Permittee must also employ one or more certified Back-up ORCs who possess a currently valid certificate of the
type of the system. Back-up ORCs must possess a grade equal to (or no more than one grade less than) the grade
of the system [15A NCAC 8G.0201].
Version 1011012007

NPDES Permit Standard Conditions
Page 7 of 16
The ORC of each Class I facility must:
➢ . Visit the facility at least weekly
➢ Comply with all other conditions of 15A NCAC 8G.0204.
The ORC of each Class II, III and IV facility must:
➢ Visit the facility at least five days per week, excluding holidays
➢ Properly manage and document daily operation and maintenance of the facility
➢ Comply with all other conditions of 15A NCAC 8G.0204.
Once the facility is classified, the Permittee shall submit a letter to the Certification Commission designating the
operator in responsible charge:
a. Within 60 calendar days prior to wastewater being introduced into a new system
b. Within 120 calendar days of:
➢ Receiving notification of a change in the classification of the system requiring the designation of a
new ORC and back-up ORC
➢ A vacancy in the position of ORC or back-up ORC.
2. Proper Operation and Maintenance
The Permittee shall at all times provide the operation and maintenance resources necessary to operate the existing
facilities at optimum efficiency. The Permittee shall at all times properly operate and maintain all facilities and
systems of treatment and control (and related appurtenances) which are installed or used by the Permittee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the Permittee to install
and operate backup or auxiliary facilities only when necessary to achieve compliance with the conditions of the
permit [40 CFR 122.41 (e)].
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a Permittee-in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this permit [40 CFR 122.41
(c)]
4. Bypassing of Treatment Facilities
a. Bypass not exceeding limitations [40 CFR 122.41 (m) (2)]
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but
only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject to the
provisions of Paragraphs b. and c. of this section.
b. Notice [40 CFR 122.41 (m) (3)]
(1) Anticipated bypass. If the Permittee knows in advance of the need for a bypass, it shall submit prior
notice, if possible at least ten days before the date of the bypass; including an evaluation of the
anticipated quality and effect of the bypass.
(2) Unanticipated bypass. The Permittee shall submit notice of an unanticipated bypass as required in Part
II. E. 6. (24-hour notice).
c. Prohibition of Bypass
(1) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for bypass, unless:
(A) Bypass was unavoidable to prevent loss of life, personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment facilities,
retention of untreated wastes or maintenance during normal periods of equipment downtime. This
condition is not satisfied if adequate backup equipment should have been installed in the exercise of
reasonable engineering judgment to prevent a bypass which occurred during normal periods of
equipment downtime or preventive maintenance; and
(C) The Permittee submitted notices as required under Paragraph b. of this section.
Version 1011012007

NPDES Permit Standard Conditions
Page 8 of 16
(2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for a bypass as provided in any current or future system -wide collection system
permit associated with the treatment facility.
(3) The Permit Issuing Authority may approve an anticipated bypass, after considering its adverse effects, if
the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph c.
(1) of this section.
5. U sets
a. Effect of an upset [40 CFR 122.41 (n) (2)]: An upset constitutes an affirmative defense to an action
brought for noncompliance with such technology based permit effluent limitations if the requirements of
Paragraph b. of this condition are met. No determination made during administrative review of claims that
noncompliance was caused by upset, and before an action for noncompliance, is final administrative action
subject to judicial review.
b. Conditions necessary for a demonstration of upset: A Permittee who wishes to establish the
affirmative defense of upset shall demonstrate, through properly signed, contemporaneous operating logs, or
other relevant evidence that:
(1) An upset occurred and that the Permittee can identify the cause(s) of the upset;
(2) The Permittee facility was at the time being properly operated; and
(3) The Permittee submitted notice of the upset as required in Part II. E. 6. (b) of this permit.
(4) The Permittee complied with any remedial measures required under Part II. B. 2. of this permit.
c. Burden of proof [40 CFR 122.41 (n) (4)]: The Permittee seeking to establish the occurrence of an
upset has the burden of proof in any enforcement proceeding.
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters
shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant
from such materials from entering waters of the State or navigable waters of the United States. The Permittee
shall comply with all existing Federal regulations governing the disposal of sewage sludge. Upon promulgation of
40 CFR Part 503, any permit issued by the Permit Issuing Authority for the utilization/disposal of sludge may be
reopened and modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR 503. The
Permittee shall comply with applicable 40 CFR 503 Standards for the Use and Disposal of Sewage Sludge (when
promulgated) within the time provided in the regulation, even if the permit is not modified to incorporate the
requirement. The Permittee shall notify the Permit Issuing Authority of any significant change in its sludge use
or disposal practices.
Power Failures
The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 2H.0124 —
Reliability) to prevent the discharge of untreated or inadequately treated wastes during electrical power failures
either by means of alternate power sources, standby generators or retention of inadequately treated effluent.
Section D. Monitoring and Records
Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and nature of
the permitted discharge.. Samples collected at a frequency less than daily shall be taken on a day and time that is
characteristic of the discharge over the entire period the sample represents. All samples shall be taken at the
monitoring points specified in this permit and, unless otherwise specified, before the effluent joins or is diluted
by any other wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to and the approval of the Permit Issuing Authority [40 CFR 122.41 (j)].
Version 1011012007

NPDES Permit Standard Conditions
Rage 9of16
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each month and reported on a
monthly Discharge Monitoring Report (DMR) Form (MR 1, 1.1, 2, 3) or alternative forms approved by the
Director, postmarked no later than the last calendar day of the month following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of
these, and all other reports required herein, shall be submitted to the following address:
NC DENR / Division of Water Quality / Water Quality Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected
and used to ensure the accuracy and reliability of measurements of the voluine of monitored discharges. The
devices shall be installed, calibrated and maintained to ensure that the accuracy of the measurements is consistent
with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a
maximum deviation of less than 10% from the true discharge rates throughout the range of expected discharge
volumes. Flow measurement devices shall be accurately calibrated at a minimum of once per year and maintained
to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device.
The Director shall approve the flow measurement device and monitoring location prior to installation.
Once -through condenser cooling water flow monitored by pump logs, or pump hour meters as specified in Part I
of this permit and based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations (published pursuant to
NCGS 143-215.63 et. seq.), the Water and Air Quality Reporting Acts, and to regulationspublished pursuant to
Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act (as Amended), and 40 CFR 136; or in
the case of sludge use or disposal, approved under 40 CFR 136, unless otherwise specified in 40 CFR 503, unless
other test procedures have been specified in this permit [40 CFR 122.41].
To meet the intent of the monitoring required by this permit, all test procedures must produce minimum
detection and reporting levels that are below the permit discharge requirements and all data generated must be
reported down to the minimum detection or lower reporting level of the procedure. If no approved methods are
determined capable of achieving minimum detection and reporting levels below permit discharge requirements,
then the most sensitive (method with the lowest possible detection and reporting level) approved method must
be used.
5. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any
monitoring device or method required to be maintained under this permit shall, upon conviction, be punished by
a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or
by both. If a conviction of a person is for a violation committed after a first conviction of such person under this
paragraph, punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not more
than 4 years, or both [40 CFR 122.41].
6. Records Retention
Except for records of monitoring information required by this permit related to the Permittee's sewage sludge
use and disposal activities, which shall be retained for a period of at least five years (or longer as required by 40
CFR 503), the Permittee shall retain records of all monitoring information, including:
➢ all calibration and maintenance records
➢ all original strip chart recordings for continuous monitoring instrumentation
Version 1011012007

NPDES Permit Standard Conditions
Page 10 of 16
➢ copies of all reports required by this permit
➢ copies of all data used to complete the application for this permit
These records or copies shall be maintained for a period of at least 3 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time [40 CFR
122.41].
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the Permittee shallrecord
the following information [40 CFR 122.41]:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
8. Inspection and Entry
The Permittee shall allow the Director, or an authorized representative (including an authorized contractor acting
as a representative of the Director), upon the presentation of credentials and other documents as may be required
by law, to;
a. Enter upon the Permittee's premises where a regulated facility or activity is located or conducted, or where
records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this
Permit;
C. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices,
or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise
authorized by the Clean Water Act, any substances or parameters at any location [40 CFR 122.41 (i)].
Section E Reporting Requirements
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit. The discharge
of any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall
constitute a violation of the permit.
2. Planned Changes
The Permittee shall give notice to the Director as
additions to the permitted facility [40 CFR 122.41 (1)].
soon as possible of any planned physical alterations or
Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR
122.29 (b); or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged. This notification applies to pollutants subject neither to effluent limitations in the permit, nor to
notification requirements under 40 CFR 122.42 (a) (1).
c. The alteration or addition results in a significant change in the Permittee's sludge use or disposal practices,
and such alteration, addition or change may justify the application of permit conditions that are different
from or absent in the existing permit, including notification of additional use or disposal sites not reported
during the permit application process or not reported pursuant to an approved land application plan.
3. Anticipated Noncompliance
The Permittee shall give advance notice to the Director of any planned changes to the permitted facility or other
activities that might result in noncompliance with the permit [40 CFR 122.41 (1) (2)].
Version 1011012007

NPDES Permit Standard Conditions
Page 11 of 16
4. Transfers
This permit is not transferable to any person except after notice to the Director. The Director may require
modification or revocation and reissuance of the permit to document the change of ownership. Any such action
may incorporate other requirements as may be necessary under the Clean Water Act [40 CFR 122.41 (1) (3)].
5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit [40 CFR 122.41 (l) (4)].
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part II. D. 2) or forms
provided by the Director for reporting results of monitoring of sludge use or disposal practices.
b. If the Permittee monitors any pollutant more frequently than required by this permit, the results of such
monitoring shall be included in the calculation and reporting of the data submitted on the DMR.
6. Twenty-four Hour Reporting
a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that
potentially threatens public health or the environment. Any information shall be provided orally within 24
hours from the time the Permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the Permittee becomes aware of the circumstances. The written
submission shall contain a description of the noncompliance, and its cause; the period of noncompliance,
including exact dates and times, and if the noncompliance has not been corrected, the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the
noncompliance [40 CFR 122.41 (1) (6)].
b. The Director may waive the written report on a case -by -case basis for reports under this section if the oral
report has been received within 24 hours.
c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response
personnel at [phone], [phone] or [phone].
7. Other Noncompliance
The Permittee shall report all instances of noncompliance not reported under Part II. E. 5 and 6. of this permit at
the time monitoring reports are submitted. The reports shall contain the information listed in Part II. E. 6. of
this permit [40 CFR 122.41 ,(1) (7)].
S. Other Information
Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or
submitted incorrect information in a permit application or in any report to the Director, it shall promptly submit
such facts or information [40 CFR 122.41 (1) (8)].
9. Noncompliance Notification
The Permittee shall report by telephone to either the central office or the appropriate regional office of the
Division as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following:
a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of
wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge
digester; the known passage of a slug of hazardous substance through the facility; or any other unusual
circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps, aerators, compressors, etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass directly to receiving
waters without treatment of all or any portion of the influent to such station or facility.
Version 1011012007

NPDES Permit Standard Conditions
Page 12 of 16
Persons reporting such occurrences by telephone- shall also file a written report within 5 days following first
knowledge of the occurrence.
10. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act, 33
USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the offices
of the Division. As required by the Act, effluent data shall not be considered confidential. Knowingly making
any false statement on any such report may result in the imposition of criminal penalties as provided for in
NCGS 143-215.1(b) (2) or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this permit, including
monitoring reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of
not more than $25,000 per violation, or by imprisonment for not more than two years per violation, or by both
[40 CFR 122.41].
12. Annual Performance Reports
Permittees who own or operate facilities that collect or treat municipal or domestic waste shall provide an annual
report to the Permit Issuing Authority and to the users/customers served by the Permittee (NCGS 143-215.1C).
The report shall summarize the performance of the collection or treatment system, as well as the extent to which
the facility was compliant with applicable Federal or State laws, regulations and rules pertaining to water quality.
The report shall be provided no later than sixty days after the end of the calendar or fiscal year, depending upon
which annual period is used for evaluation.
PART III
OTHER REQUIREMENTS
Section A. Construction
The Permittee shall not commence construction of wastewater treatment facilities, nor add to the plant's treatment
capacity, nor change the treatment process(es) utilized at the treatment plant unless the Division has issued an
Authorization to Construct (AtC) permit. Issuance of an AtC will not occur until Final Plans and Specifications for
the proposed construction have been submitted by the Permittee and approved by the Division.
Section B. Groundwater Monitoring
The Permittee shall, upon written notice from the Director, conduct groundwater monitoring as may be required to
determine the compliance of this NPDES permitted facility with the current groundwater standards.
Section C. Changes in Discharges of Toxic Substances
The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe (40 CFR 122.42):
a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent
basis, of any toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the
following "notification levels";
(1) One hundred micrograms per liter (100 µg/L);
(2) Two hundred micrograms per liter (200 µg/L) for acrolein and acrylonitrile; five hundred micrograms
per liter (500 µg/L) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol; and one milligram per liter
0 mg/L) for antimony;
(3) Five times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge, on a non -routine or
infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the
highest of the following "notification levels";
Version 1011012007

NPDES Permit Standard Conditions
Page 13 of 16
(1) Five hundred micrograms per liter (500 µg/L);
(2) One milligram per liter (1 mg/L) for antimony;
(3) Ten times the maximum. concentration value reported for that pollutant in the permit application.
Section D. Evaluation of Wastewater Discharge Alternatives
The Permittee shall evaluate all wastewater disposal alternatives and pursue the most environmentally sound
alternative of the reasonably cost effective alternatives. If the facility is in substantial non-compliance with the terms
and conditions of the NPDES permit or governing rules, regulations or laws, the Permittee shall submit a report in
such form and detail as required by the Division evaluating these alternatives and a plan of action within 60 days of
notification by the Division.
Section E. Facility Closure Requirements
The Permittee must notify the Division at least 90 days prior to the closure of any wastewater treatment system
covered by this permit. The Division may require specific measures during deactivation of the system to prevent
adverse impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit
continue at the permitted facility.
PART IV
SPECIAL CONDITIONS FOR MUNICIPAL FACILITIES
Section A. Publicly Owned Treatment Works (POTWs)
All POTWs must provide adequate notice to the Director of the following:
1. Any new introduction of pollutants into the POTW from an indirect discharger which would be subject to
section 301 or 306 of CWA if it were directly discharging those pollutants; and
2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger
as influent to that POTW at the time of issuance of the permit.
3. For purposes of this paragraph, adequate notice shall include information on (1) the quality and quantity of
effluent introduced into the POTW, and (2) any anticipated impact of the change on the quantity or quality
of effluent to be discharged from the POTW.
Section B. Municipal Control of Pollutants from Industrial Users.
Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs from
industries using the municipal system may be present in the Permittee's discharge. At such time as
sufficient information becomes available to establish limitations for such pollutants, this permit may be
revised to specify effluent limitations for any or all of such other pollutants in accordance with best
practicable technology or water quality standards.
2. Under no circumstances shall the Permittee allow introduction of the following wastes in the waste
treatment system:
a. Pollutants which create a fire or explosion hazard in the POTW, including, but not limited to,
wastestreams with a closed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees
Centigrade using the test methods specified in 40 CFR 261.21;
b. Pollutants which will cause corrosive structural damage to the POTW, but in no case Discharges
with pH lower than 5.0, unless the works is specifically designed to accommodate such Discharges;
C. Solid or viscous pollutants in amounts which will cause obstruction to the flow in the POTW
resulting in Interference;
d. Any pollutant, including oxygen demanding pollutants (BOD, etc.) released in a.Discharge at a flow
rate and/or pollutant concentration which will cause Interference with the POTW;
e. Heat in amounts which will inhibit biological activity in the POTW resulting in Interference, but in
no case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C
(104°F) unless the Division, upon request of the POTW, approves alternate temperature limits;
Version 1011012007

NPDES Permit Standard Conditions
Page 14 of 16
f. Petroleum oil, nonbiodegradable cutting oil, or products of mineral oil origin in amounts that will
cause interference or pass through;
g. Pollutants which result in the presence of toxic gases, vapors, or fumes within the POTW in a
quantity that may cause acute worker health and safety problems;
h. Any trucked or hauled pollutants, except at discharge points designated by the POTW.
With regard to the effluent requirements listed in Part I of this permit, it may be necessary for the
Permittee to supplement the requirements of the Federal Pretreatment Standards (40 CFR, Part 403) to
ensure compliance by the Permittee with all applicable effluent limitations. Such actions by the Permittee
may be necessary regarding some or all of the industries discharging to the municipal system.
4. The Permittee shall require any industrial discharges sending influent to the permitted system to meet
Federal Pretreatment Standards promulgated in response to Section 307(b) of the Act. Prior to accepting
wastewater from any significant industrial user, the Permittee shall either develop and submit to the
Division a Pretreatment Program for approval per 15A NCAC 2H .0907(a) or modify an existing
Pretreatment Program per 15A NCAC 2H .0907(b).
5. This permit shall be modified, or alternatively, revoked and reissued, to incorporate or modify an approved
POTW Pretreatment Program or to include a compliance schedule for the development of a POTW
Pretreatment Program as required under Section 402(b)(8) of the Clean Water Act and implementing
regulations or by the requirements of the approved State pretreatment program, as appropriate.
Section C. Pretreatment Pro rams
Under authority of sections 307(b) and (c) and 402(b)(8) of the Clean Water Act and implementing regulations 40
CFR Part 403, North Carolina General Statute 143-215.3 (14) and implementing regulations 15A NCAC 2H
.0900, and in accordance with the approved pretreatment program, all provisions and regulations contained and
referenced in the Pretreatment Program Submittal are an enforceable part of this permit.
The Permittee shall operate its approved pretreatment program in accordance with Section 402(b)(8) of the Clean
Water Act, the Federal Pretreatment Regulations 40 CFR Part 403, the State Pretreatment Regulations 15A
NCAC 2H .0900, and the legal authorities, policies, procedures, and financial provisions contained in its
pretreatment program submission and Division approved modifications there of. Such operation shall include
but is not limited to the implementation of the following conditions and requirements:
1. Sewer Use Ordinance (SUO)
The Permittee shall maintain adequate legal authority to implement its approved pretreatment program.
2. Industrial Waste SurvU aWS)
The Permittee shall update its Industrial Waste Survey (IWS) to include all users of the sewer collection
system at least once every five years.
3. Monitoring Plan
The Permittee shall implement a Division -approved Monitoring Plan for the collection of facility specific
data to be used in a wastewater treatment plant Headworks Analysis (HWA) for the development of
specific pretreatment local limits. Effluent data from the Plan shall be reported on the DMRs (as required
by Part II, Section D, and Section E.5.).
4. Headworks Analysis (HWA) and Local Limits
The Permittee shall obtain Division approval of a Headworks Analysis (HWA) at least once every five
years, and as required by the Division. Within 180 days of the effective date of this permit (or any
subsequent permit modification) the Permittee shall submit to the Division a written technical evaluation
of the need to revise local limits (i.e., an updated HWA or documentation of why one is not needed) [40
CFR 122.44]. The Permittee shall develop, in accordance with 40 CFR 403.5(c) and 15A NCAC 2H .0909,
specific Local Limits to implement the prohibitions listed in 40 CFR 403.5(a) and (b) and 15A NCAC 2H
.0909.
Version 1011012007

NPDES Permit Standard Conditions
Page 15-of 16
5. Industrial User Pretreatment Permits (IUZ & Allocation Tables
In accordance with NCGS 143-215.1, the Permittee shall issue to all significant industrial users, permits for
operation of pretreatment equipment and discharge to the Permittee's treatment works. These permits
shall contain limitations, sampling protocols, reporting requirements, appropriate standard and special
conditions, and compliance schedules as necessary for the installation of treatment and control
technologies to assure that their wastewater discharge will meet all applicable pretreatment standards and
requirements. The Permittee shall maintain a current Allocation Table (AT) which summarizes the results
of the Headworks Analysis (HWA) and the limits from all Industrial User Pretreatment Permits (IUP).
Permitted IUP loadings for each parameter cannot exceed the treatment capacity of the POTW as
determined by the HWA.
6. Authorization to Construct (AtC),
The Permittee shall ensure that an Authorization to Construct permit (AtC) is issued to all applicable
industrial users for the construction or modification of any pretreatment facility. Prior to the issuance of
an AtC, the proposed pretreatment facility and treatment process must be evaluated for its capacity to
comply with all Industrial User Pretreatment Permit (IUP) limitations.
7. POTW Inspection & Monitoring of their SIUs
The Permittee shall conduct inspection, surveillance, and monitoring activities as described, ' in its Division
approved pretreatment program in order to determine, independent of information supplied by industrial.
users, compliance with applicable pretreatment standards. The Permittee must:
a. Inspect all Significant Industrial Users (SIUs) at least once per calendar year; and
b. Sample all Significant Industrial Users (SIUs) at least twice per calendar year for all permit -
limited pollutants, once during the period from January 1 through June 30 and once during the
period from July 1 through December 31, except for organic compounds which shall be sampled
once per calendar year;
S. SIU Self Monitoring and Reporting
The Permittee shall- require all industrial users to comply with the applicable monitoring and reporting
requirements outlined in the Division -approved pretreatment program, the industry's pretreatment permit,
or in 15A NCAC 211.0908.
9. Enforcement Response Plan (ERPI
The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards
promulgated pursuant to section 307(b) and (c) of the Clean Water Act (40 CFR 405 et. seq.), prohibitive
discharge standards as set forth in 40 CFR 403.5 and 15A NCAC 2H .0909, and specific local limitations.
All enforcement actions shall be consistent with the Enforcement Response Plan (ERP) approved by the
Division.
10. Pretreatment Annual Reports (PAR)
The Permittee shall report to the Division in accordance with 15A NCAC 2H .0908. In lieu of submitting
annual reports, Modified Pretreatment Programs developed under 15A NCAC 2H .0904 (b) may be
required to meet with Division personnel periodically to discuss enforcement of pretreatment requirements
and other pretreatment implementation issues.
For all other active pretreatment programs, the Permittee shall submit two copies of a Pretreatment
Annual Report (PAR) describing its pretreatment activities over the previous twelve months to the
Division at the following address:
NC DENR / DWQ / Pretreatment Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Version 1011012007

NPDES Permit Standard Conditions
Page 16 of 16
These reports shall be submitted according to a schedule established by the Director and shall contain the
following:
a.) Narrative
A brief discussion of reasons for, status of, and actions taken for all Significant Industrial
Users (SIUs) in Significant Non -Compliance (SNC);
b.) Pretreatment Program SiunmgQr (PPS).
A pretreatment program summary (PPS) on specific forms approved by the Division;
c.) Significant Non -Compliance Report SNCR�
The nature of the violations and the actions taken or proposed to correct the violations on
specific forms approved by the Division;
d.) Industrial Data Summary Forms (DSF)
Monitoring data from samples collected by both the POTW and the Significant Industrial
User (SIU). These analytical results must be reported on Industrial Data Summary Forms
(IDSF) or other specific format approved by the Division;
e.) Other Information
Copies of the POTW's allocation table, new or modified enforcement compliance schedules,
public notice of SIUs in SNC, and any other information, upon request, which in the
opinion of the Director is needed to determine compliance with the pretreatment
implementation requirements of this permit;
11. Public Notice
The Permittee shall publish annually a list of Significant Industrial Users (SIUs) that were in Significant
Non -Compliance (SNC) as defined in the Permittee's Division -approved Sewer Use Ordinance with
applicable pretreatment requirements and standards during the previous twelve month period. This list
shall be published within four months of the applicable twelve-month period.
12. Record Keeping
The Permittee shall retain for a minimum of three years records of monitoring activities and results, along
with support information including general records, water quality records, and records of industrial impact
on the POTW.
13. Funding and Financial Report
The Permittee shall maintain adequate funding and staffing levels to accomplish the objectives of its
approved pretreatment program.
14. Modification to Pretreatment Programs
Modifications to the approved pretreatment program including but not limited to local limits
modifications, POTW monitoring of their Significant Industrial Users (SIUs), and Monitoring Plan
modifications, shall be considered a permit modification and shall be governed by 15 NCAC 2H .0114 and
15A NCAC 2H .0907.
Version 1011012007

SOC Priority Project: No
VTo: NPDES Unit -
Water Quality Section _ _
Attention: Dina Sprinkle
Date: April 11, 2008
NPDES STAFF REPORT AND RECOMMENDATION
County: Cleveland '
Permit No. NC0004685
PART I - GENERAL INFORMATION
1. Facility and address: PPG Industries, Inc.
940 Washburn Switch Road
Shelby, North Carolina 28150
2. Date of investigation: March 26, 2008
3. Report prepared by: Samar Bou-Ghazale, Environmental Engineer II
4. Persons contacted and telephone number: Tim Mathis, [phone].
5,. Directions to site: From the intersection of US Hwy 74 and SR 1313 (Washburn Switch Road)
just west of the City of Shelby, travel north on SR 1313 approximately 3.0 miles. The PPG plant
is located on the left side of the road.
6. Discharge point(s), list for all discharge points:
Outfall 001:.
Latitude: 35° 20' 26" Longitude: 81° 37' 00"
Outfall 002:
Latitude: 35' 19' 28" Longitude: 8103751"
Attach a USGS map extract and indicate treatment facility site and discharge point on map.
WWTP:
U.S.G.S. Quad No.: F12SW
U.S.G.S. Quad Name: Boiling Springs North, NC
Discharge point:
U.S.G.S. Quad No.: F1,2SE U.S.G.S. Quad Name: Shelby, NC
7. Site size and expansion area are consistent with application? Yes. There is ample area for
additional WWTP construction, if necessary.

Page Two
8. Topography (relationship to flood plain included): Flat to moderate slopes; the WWTP is not
located within a 100-year flood plain.
9. Location of nearest dwelling: None within 500 feet of the plant
10. Receiving stream or affected surface waters: Brushy Creek (outfall 001), Overflow Branch
(outfall 002)
a. Classification: C (both receiving streams)
b. River Basin and Subbasin No.: Broad 030804
C. Describe receiving stream features and pertinent downstream uses: Brushy Creek is of
moderate size (15-25 feet wide) with a sandy bottom. General "C" classification uses
downstream. Overflow Branch is ;z� 3 - 4 feet wide, and downstream uses are primarily
agricultural in nature.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
1. a. Volume of wastewater to be permitted: 1.3 MGD (outfall 001), Flow is intermittent at
outfall 002.
b. Current permitted capacity of the wastewater treatment facility: 1.3 MGD
C. Actual treatment capacity of the current facility (current design capacity): 1.3 MGD
d. Date(s) and construction activities allowed by previous Authorizations to Construct
issued in the previous two years: N/A
e. Please provide a description of existing or substantially constructed wastewater treatment
facilities: Existing treatment facilities consists of an influent overflow/storage basin,
influent screening with grinder, wet well with lime addition, a surge tank, an equalization
tank, a flash mix tank for aluminum chloride, coagulant and polymer addition, two (2)
primary clarifiers, two (2) aeration basins with diffused air and bentonite clay addition, a
floc tank with ferric chloride addition, three (3) secondary clarifiers with ferric chloride
addition, a chlorine contact tank being used as an effluent pump tank (no chlorine is
added at this time), traveling bridge sand filter, defoamer addition, gravity sludge
thickener, belt filter press, and an overflow lagoon. Stand-by power is provided for the
industrial process and the WWTP through on -site generators. The permittee has received
approval from the Division to use of bentonite clay for effluent toxicity reduction and the
addition of aluminum chloride as a reactant for fluoride removal, chemical precipitation,
and floc formation. There is no treatment provided at outfall 002.
f. Please provide a description of proposed wastewater treatment facilities: There are no
proposed WWT facilities at this time. .

Page Three
g. Possible toxic impacts to surface waters: Information contained in the files of this office
indicates that this facility is in compliance with its toxicity testing requirements.
h. Pretreatment Program (POTWs only): N/A
2. Residuals handling and utilization/disposal scheme: Residuals are currently land filled at the
Cleveland County landfill. PPG has a non -discharge permit for the land application of residuals
(WQ0001055), however, no residuals have ever been applied.
3: Treatment plant classification: Class IV (no change from previous rating)
4. SIC Code(s): 3229 (PPG), 3083 (Azdel)
Wastewater Code(s) Primary: 64 Secondary: 02, 73, 15, 14, 36
Main Treatment Unit Code: 01602
PART III - OTHER PERTINENT INFORMATION
Is this facility being constructed with Construction Grant Funds or are any public monies involved
(municipals only)? No public monies were involved in the construction of this facility.
2. Special monitoring or limitations (including toxicity) requests: None at this time.
3. Important SOC, JOC or Compliance Schedule dates: N/A '
4. Alternative Analysis Evaluation:
Spray Irrigation: Insufficient area
Connection to Regional Sewer System: There is none presently available to serve this site.
Subsurface: Insufficient area
5. Air quality and/or groundwater concerns or hazardous materials utilized at this facility that may
impact water quality, air quality, or groundwater: No GW concerns at this time. The facility has
obtained the necessary air quality permits. There are no known hazardous materials concerns.
PART IV - EVALUATION AND RECOMMENDATIONS
The permittee, PPG Industries, Inc., is requesting permit renewal to discharge wastewater from
their WWT facilities. The WWTP serves the industrial and domestic needs for PPG and a nearby
company; Azdel, Inc. Azdel is located on the PPG property and uses the fiberglass produced at PPG in
part of their industrial process. Azdel contributes approximately 10,000 gpd to the PPG WWTP.
Outfall 001 is the outfall from the WWTP that treats the industrial, domestic, some of the
stormwater from the two sites, and at this time all non -contact cooling wastewater. Outfall 002 consists
of non -contact cooling water and stormwater.

Page Four
PPG Industries, Inc., Is requesting that Fluoride monitoring frequency be reduced from weekly to
monthly based on the fact that the effluent fluoride limit from the facility is 10 to 20% of the permit
limit.
PPG has also obtained coverage under SW general permit number NCG070015, which contains
outfalls, 003, 004, 005, 006, 007, and 008. During the previous renewal, this office recommended that
the Stormwater permit be combined with the NPDES permit. However, since the stormwater permit
requirements evolved to new directions from previous years, we recommend that the stormwater permit
be a standalone permit and be distinct from the wastewater permit.
Pending review and approval by the P & E, it is recommended that the permit be renewed with the
above changes..
Signature of report preparer Date
Water Quality Regional Supervisor bate

WAT�c Michael F. Easley, Governor
�QG State of North Carolina
� P'n
fnv ID
ivision of Water Quality
August 13, 2008
Mr. Timothy G. Mathis
Manufacturing Manager
PPG Industries Fiber Glass Products, Inc.
940 Washburn Road
Shelby, North Carolina 28150
Dear Mr. Mathis:
AUG 1 4 2009
N0 DENR BIRO .
M-Surface Water Protection
Subject: Draft NPDES Permit
Permit NC0004685
Shelby Facility
Cleveland County
Enclosed with this letter is a copy of the draft permit for your facility. Please review the draft
carefully to ensure thorough understanding of the conditions and requirements it contains.
The draft permit contains no following significant changes from your current permit.
The Division cannot grant your request to reduce the monitoring frequency for fluoride from
weekly to 1/month. Analysis of fluoride data indicated a reasonable potential to exceed the
instream water quality standard. Because the PPG facility is designated Class III, the Division
of Water Quality's current guidance dictates that weekly monitoring be conducted for fluoride.
Please submit any comments to me- no later than thirty days following your receipt of the draft.
Comments should be sent to my attention at the address listed at the bottom of this page. If you
have any comments, questions, or. concerns regarding this draft permit, contact me at (919)
807-6393, or [e-mail].
Sincerely,
tEn
gei Chernikov, Ph. D.
ironmental Engineer II
DES -West
cc: NPDES Unit
¢lIoores�rille Regiocl fl;1.c'e / Surface Water protection (draft permit, fact sheet)
Aqua is Toxico ogy Unit (draft permit)
EPA Region 4 (draft permit, fact sheet, permit application)
1617 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1617 - TELEPHONE [phone]/FAX [phone]
VISIT US ON THE WEB AT http://h2o.enr.state.nc.us/NPDES

'Y
• .,

Permit NC0004685
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER, QUALITY
Draft PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT, DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
PPG Industries Fiber Glass Products, Incorporated
is hereby authorized to discharge wastewater and stormwater from a -facility located at
Shelby Facility
On NCSR 1313
- West of Shelby
Cleveland County
to receiving waters designated as Brushy Creek and Overflew Branch in the Broad River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set .forth in Parts
I, II, III, and IV hereof.
The permit shall become effective
This permit and the authorization to discharge shall expire at midnight on August 31, 2013.
Signed this day November
- Coleen H. Sullins, Director
Division of Water Quality
By Authority of the Environmental Management Commission

Permit NC0004685
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby
revoked, and as of this issuance, any previously issued permit bearing this number is no longer
effective. Therefore, the exclusive authority to operate and discharge from this facility arises under the
permit conditions, requirements, terms, and provisions included herein.
PPG Industries Fiber Glass Products, Incorporated is hereby authorized to:-
1. Continue operation of aA.3 MGD wastewater treatment facility consisting of:
an overflow/ storage basin;
• bar screen and grinder;
• an influent wet well with lime addition;
• . influent pumps;
• -a surge tank;
• an. equalization tank;
• a flash mix tank with aluminum chloride addition;
• coagulant and polymer addition;
• . two primary clarifiers;
• two aeration basins with bentonite clay addition;
• a splitter box and floc tank;
• three secondary clarifiers with ferric chloride addition;
• a sand filter;
• an effluent holding tank;
• a sludge thickener tank; and
• a sludge belt press.
These treatment works are located at PPG's Shelby facility on NCSR 1313, west of Shelby,
Cleveland County and discharge treated process wastewater, stormwater, sanitary sewage,
cooling water, and landfill leachate, at the location specified on the attached map, through,
outfall 001 into Brushy Creek, a class C water in the Broad River Basin; and
2. Discharge non -contact cooling water and stormwater through outfall 002, at the location
.specified on the attached map, into Overflow Branch, a class C water in the Broad River Basin.

V
r, Nl�
7,
-2!
1-3 C
Outfall 001 to Brushy Creek Latitude: 35020'25"
. . . . . . .
Longitude: 81036'58"
4
Q -7 f�
,
V JIL
nL
t,.K
V1,' , PW
t v
A,
PI
M:
V-1
A
f
V,
Outfall 002 to Overflow Branch
T
)U
JC6L,)
Latitude: 3501912711
Longitude: 81037150" Y.= J
z % L
4M19
Pall
—E:y
33
I rl�
A
?
Ps MU V444t,$ Q:
Industries..-
PPG IndU s NC0004685 `Facility
IY
+;
oca USGS Quad.Name: Shelby SE/SW
Receiving Stream:'See Above
Stream Class: C
Not to SCALE
Subbisin": Broad - 030804
North]

Permit NC0004685
A (1.) EFFLUENT LIMITATIONS AND MONITORING 12EQUIREMENTS
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is authorized to
discharge from Outfall 001. Such discharges shall be limited and monitored by the Permittee as specified below:
t
PARAMETER
EFFLUENT` LIMITATIONS :
MONLTORING
REQUIREMENTS
Maxsmuan
;MFre uencq t
mple
Sa e. ...
Sample
cations `'
Flow (MGD)
1.3
Continuous
Recording
I or E.
BOD, 5-day, 20oC (mass)
217.0 lbs/day
325.5 lbs/day
Weekly
Composite
E
BOD, 5-day, 20oC (conic.)
20.0 mg/L
30.0 mg/L
Weekly
Composite
E
Total Suspended Solids
20.0 mg/L
146.0 mg/L
Weekly
Composite
E
NH3-N. (mass)
65.0 lbs/day
97.5 lbs/day
Weekly
Composite
E
NH3-N (conc.)
6.0 mg/L
9.0 mg/L
Weekly
Composite
E
Dissolved Oxygen
Daily Average z 5.0 mg/L
Daily
Grab
E
Dissolved Oxygen (instream)
Monitor & Report
See Note 1
Grab
U,D
pH
Z 6.0 to s 9.0 Standard Units
Daily
Grab
E
Temperature, OC
Daily
Grab
E
Temperature, oC (instream)
See Note 1
Grab
U,D
Fecal Coliform
Weekly
Grab
E
Total Nitrogen
Quarterly
Composite
E
Total Phosphorus
Quarterly
Composite
E
Conductivity
See Note 1
Grab
U,D
Oil and Grease
10.0 mg/L
15.0 mg/L
Weekly
Grab
E
Total Lead •
Monthly
Composite
E
Fluoride
5.4 mg/L
Weekly
Composite
E
Total.Zinc
2/Month
Composite
E
Total Copper
2/Month
Composite
E
Chloride
2/Month
Composite
E
Total Residual Chlorine2
17 µg/L
Weekly
Grab
E
Chronic Toxicity3
Quarterly
Composite
E
NOTES
1 E - Effluent, I — Influent, U — Upstream at NCSR 1323, D — Downstream at NCSR 1305; upstream
and downstream samples shall be grab samples collected three times per week during June, July,
August, and September and weekly during the remainder of the year.
2 The facility shall report all effluent TRC values reported by a NC certified laboratory including field
certified. However, effluent values below 50 ug/1 will be treated as zero for compliance purposes.
3 Chronic Toxicity (Ceriodaphnia) P/F @ 33%; January,. April, July, October. See Part A (3.) of this
permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE
AMOUNTS.
A

Permit NC0004685
A (2.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is authorized'to
discharge from Outfall 002. Such discharges shall be limited and monitored by the Permittee ds specified below:
p
LIMITATIONS,
MONITORINGr;RE UIREMENTSG,e„
'
PARAMETER �y
J 'Monthly i
Dazly
Inc n easur t
Sample
Sample
Aveage,,�
+Maximum
r Fr
e... `.
_ e u`e
Location
Flow (MGD)
Semi -Annually
Estimate
. Effluent
Temperature
See Note 1
Semi -Annually
Grab
Effluent
Total Residual Chlorine2
28 µg/L -
Semi -Annually
Grab-
Effluent
pH
Between 6.0 and 9.0 Standard Units
Semi -Annually
Grab
. Effluent
NOTES:
1 The temperature of the effluent shall be such as not to cause an increase in the temperature of the
receiving stream of more than 2.86C and in no case cause the ambient water temperature to exceed
- 29oC.
2 The effluent limitation for chlorine shall become effective 18 months after the effective date of this
permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE
AMOUNTS.
THE PERMITTEE SHALL OBTAIN AUTHORIZATION FROM THE DIVISION OF WATER QUALITY PRIOR TO
UTILIZING ANY BIOCIDE IN THE COOLING WATER — SEE PART I, A. 4 OF THIS PERMIT.
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER. -

Permit NC0004685
A (3). CHRONIC -TOXICITY PERMIT LIMIT (QUARTERLY) — OUTFALL 001
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 33%.
The permit holder shall perform at a minimum, auarterlu monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent
versions. The tests will be performed during the months of January, April, July and October. Effluent
sampling for this testing shall be performed .at the NPDES permitted final effluent discharge below all treatment
processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the
permit limit, then multiple -concentration testing shall be performed at a minimum, in each of the two
following months as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test
Procedure" (Revised -February 1998) or subsequent versions.
a
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed. If reporting pass/fail results using the
parameter code TGP3B, DWQ Form AT-1 (original) is sent to the below address. If reporting Chronic Value
results using the parameter code THP3B, DWQ Form AT-3 (original) is to be sent to the following address:
Attention: North Carolina Division of Water Quality
Environmental Sciences Section
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with" the Environmental Sciences Section no later than 30
days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for .
disinfection of the waste stream..
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the
facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No
Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences Section at
the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include
alternate monitoring requirements or limits.
If the Permittee monitors any pollutant more frequently then required by this permit, the results of such
monitoring shall be included in the calculation & reporting of the data submitted on the DMR & all AT Forms
submitted.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an
invalid test and will require immediate follow-up testing to be completed no later than the last day of the month
following the month of the initial monitoring.

Permit NC0004685
A (4.) BIOCIDE CONDITION
The Permittee shallnot use any biocides except those approved in conjunction with the permit application. The
Permittee shall notify the Director in writing not later than ninety (90) days prior to instituting use of any
additional biocide used in cooling systems which may be toxic to aquatic life other than those previously reported
to the Division of Water Quality. Such notification shall include completion of Biocide Worksheet Form 101 and a
map locating.the discharge point and receiving stream.
A (5.) DISINFECTION CONDITION — OUTFALL 001
In the event that violations of North Carolina's water quality standards for fecal coliform occur as a result of this
discharge, -disinfection will immediately be required and the permit amended to establish a fecal coliform effluent
limitation..

DENR/DWQ FACT SHEET FOR NPDES PERMIT DEVELOPMENT
NPDES No. NC0004685
.Facility,Inforinatioii
Applicant/Facility Name:
PPG Industries Fiber Glass Products, Inc.
Applicant Address:
940 Washburn Switch Road, Shelby, NC
Facility Address:
940 Washburn Switch Road, Shelby, NC
Permitted Flow
1.3 MGD
Type of Waste:
95% Industrial, 5% Domestic
Facility/Permit Status:
Existing renewal without expansion
County:
Cleveland
Character pt."
Receiving Stream
Brushy Creek (001) and Overflow Branch (002)
303(d) Listed?_
No
Stream Classification
C
Sub -basin
03-08-04
Drainage Area (mi2):
15.1
Summer 7Q 10 (cfs)
4.0
Winter 7Q 10 (cfs):
7.6
Average Flow (cfs):
21.0
IWC (%) @ 3.0 MGD:
33
fi y.u, 5 ii^ t`-k'�" � d y"x2�w
'. ?. Y" i �,'•' .y d' 7 i "5 'c '� -t a: K � " 1:!d
Regional Office:
Mooresville .
USGS Topo Quad:
F12SE
Permit Writer:
Sergei Chernikov
Date
August 5, 2008
1.0 Proposed Changes
• No changes are proposed.
2.0 Backaround
PPG Industries Fiber Glass Products, Inc. operates a fiberglass fiber manufacturing facility in
Shelby; NC. The Shelby plant currently concentrates the bulk of its fiberglass manufacturing
on the reinforced plastics market. ,
Manufacturing begins with glass raw materials including limestone, silica, boron, clay and
fluorspar. These raw materials are blended in powder form and added to melt furnaces. The
batch melt furnaces, operating at 28000F, transform the batch into molten glass. The- molten
glass is then drawn from the furnaces through electrically heated platinum bushings into
continuous fibers. These fibers are gathered into strands and either spooled or chopped into
specified lengths. -Water sprays cool the glass and keep strand contact points clean during the
winding process.
A "binder", which is water based, is applied to the individual fibers as they. are drawn from the
furnaces before being gathered .into strands. The binder is ' a proprietary mixtureof resins, film
formers, lubricants, surfactants and coupling agents emulsified in a water base. The majority of
the wastewater treated by the treatment plant is spray water, lost binder and cleaning water.
Additional wastewater is received from Azdel, Inc. Azdel is a PPG joint venture with GE and
produces a fiber glass reinforced polypropylene sheet material that is sold to molders. This is
considered a plastics laminating process and is cover under 40 CFR 463. The manufacturing
process is dry, so that the wastewater sent to PPG is either cooling water, cleaning water or
domestic wastewater. Therefore, no allocation based on 463 is proposed.
PPG Industries Fact Sheet
NPDES Renewal
Page 1

3. Wasteload Allocation Summary
This permit was first issued on May 31, 1978. The permit was summarily adjudicated. It is not
entirely evident why the permit was adjudicated, however a review of historical files seems to
indicate that the adjudication was filed because of a disagreement with limit development. At
issuance, final effluent limitations were based on 40 CFR 410.32, Subpart C: Textile Dry
Processing. While the permit was being adjudicated, interim limits were established based on
the results of a field calibrated water quality model. Upon resolution of the' adjudication (it was .
determined that textile guidelines did not apply to PPG's discharge), the permit was reissued in : -
August of 1979 with water -quality limitations based on the results of the model. This .original
series of wasteload allocations was based on a discharge flow of 0.875 MGD.
The permit was renewed in 1985 with a change in allocation, however the reason for the
change is not evidenced in the files. In 1988, Jackie Nowell completed a wasteload allocation
for this facility at an expanded flow of 1.3 MGD. The increase in flow was -based on process -
modifications in the manufacturing facility. Jackie evaluated PPG's discharge with a level B
model and developed appropriate water quality -based limitations for BOD5 and NH3-N..
The current effluent limitations for BOD5 and NH3-N are based on the level B model run in
1988, while the current TSS limits are BPJ, apparently based on the BOD5 limits developed as
resolution to the 1978/79 adjudication. -
Extensive research was conducted during the previous renewal process -to determine if any
federal guidelines exist for such a manufacturing operation. Lacy Ballard of PPG was contacted
for a detailed description of the manufacturing process and associated end products. Don
Anderson and Hugh Wise were contacted at EPA in D.C. regarding the applicability of textile
and glass guidelines. After conversations with both, it was determined that neither set of
guidelines applies to PPG's process. As stated earlier, PPG does accept wastewater from Azdel;
Inc. Azdel's operation falls under the.authority of 40 CFR 463, Plastics Laminating. However,
manufacturing at Azdel is a dry process. Azdel's wastewater is largely cooling -water, cleaning -':
water and domestic wastewater. Therefore, guidelines do not apply to this aspect of PPG's
effluent either. _
PPG operates two outfalls, 001 and 002.
Outfall 001
Outfall 001 is the effluent from the wastewater treatment plant and receives the following kinds
of wastewater:
• Sanitary _.
• Research
• Boilers
• Miscellaneous
• Forming
• Fabrication
• Coating
• Process WW
Storm drains/garage pads .
Azdel, Inca WW
Outfall 002
Outfall 002 is a non -contact cooling water outfall and is permitted in accordance with the
general permit for non -contact cooling water.
4.0 Compliance Summary
A review of DMR data has indicated that the facility has a mixed compliance history. During
the period from 01/2004 through 06/2008 four NOVs for violating O&G standard have been
issued on the following dates: 5/ 17/07, 04/24/06, 10/ 18/04, and 9/ 12/04.
PPG Industries Fact Sheet
NPDES' Renewal
Page 2

5 0 Instream Monitoring Requirements
PPG currently monitors dissolved oxygen, fecal colifdrm, temperature and conductivity
instream. This renewal recommends maintaining instream monitoring for DO, temperature,
and conductivity. Y
6.0 Reasonabple Potential Analysis (RPA)
Reasonable potential analyses were conducted for lead, copper, zinc, and fluoride for outfall
001. While the maximum predicted concentration nd for copper azinc exceeded -the allowable
concentration, no limits are proposed as the facility is.not experiencing whole effluent.. toxicity.
7.0 Whole Effluent Toxicity (WET)
-Type of Toxicity Test:. Chronic P/F
Existing Limit: 001: Chronic P/F @ 33%
Recommended Limit: 001: Chronic P/F @ 33%
Monitoring Schedule: January, April, July, and October
The facility has been consistently passing its WET test.
8.0 Proposed Schedule for Permit Issuance --
Draft Permit to Public Notice: August 13, 2008 (est.)
Permit Scheduled to Issue: October 6, 2008 (est.)
9.0 State Contact
If you have any questions regarding any of the above information or the attached permit, please
contact Sergei Chernikov at [phone].
REGIONAL OFFICE COMMENT:
NAME: DATE:
PPG Industries Fact Sheet
NPDES Renewal
Page 3

REASONABLE POTENTIAL ANALYSIS
PPG Industries -Shelby
Outfall 001
NC0004685 _
Qw = 1.3 MGD
Time Period January 2002 - December 2003
Qw (MGD) 1.3
WWTP Class III
7Q10S.(cfs) 4
IWC (%) @.7Q10S 33.5
7Q10W (cfs) _ ' 7.6
@ 7Q10W 20.957
30Q2 (cfs) 0.
@ 36Q2 NIA -
Avg. Stream Flow, QA (cfs) 21
@ QA 8.7552
Rec'ving Stream Brushy Creek
Stream Class C
STANDARDS &
PARAMETER
TYPE
CRITERIA (2) -
PQL
Units
REASONABLE POTENTIAL RESULTS
RECOMMENDED ACTION
NCWQS[ %FAV/
n #Det MaxPredCw AllowableCw
(1)
Chrome Acute_
Acute: 7
Mamtem:mondonn' at 2lmonth While the max predii ted '
Copper
NC
7 AL 7.3
ug/L
36 36
138.E
is greater than the_allowable no WET is occunng thus no?
i
_ _ _
Chronic: 20.9
6mdsjs,, sed
Acute: NIA
Limdand.morntonng remal0 unchanged a r }
78 73
6,080.0
Fluoride
NC
1,800
ug/L
-
_
Chronic 5,373
Acute: 34
Mamtam mondonng at 1/,montftt4 � ` � }
Lead
NC
25 N 33.8
uglL
32 0
2.5
Chronic_K6
_x
# i<rr °
j
. v�`+* w4.. ,�1•i'Pf f .,tat^:: ,.d .r. .. us',}.a _.:...vi ,.. a
Acute: 67
Maintaur mondonng at 2/montti Wh![ the' max predicted ';
Zinc
NC
50 AL", 67
ug/L
36 36'
115.5
isgreatethantheallowable,;noWET's;occunng thusno
_ _ -_
Chronic_ 149
IPrli proposed k5 's s ;
�u

PPGR-v Pn AnMY
e
7
■
Is
copper
Fh9DTld.
LI•d -
ZAx
OW
1 r;e x,C
Dd• 801a150L R••db --
fT 121"� V. S100•r. 12Dw1
19.BI17
Dd• 0- DOLM12M Raub
1(¢ * 1160E 150A bd DIv. 11172N6
2 S 100. 60.0 Mnn 106A1w
Dd•
1° Y�
2i k} i
Data ML•i71DL R-ft
':.➢ SSW 3ADDO
25
D•t D- 9 uIMDL Raub
=?w r wA IDA Sw 41.U33IM
C.V. 0.8195
] Sf00 - 1D0A C.V. 0.700
3- 5, } 23 1
rap 25 G.V. ODDO6
] N MD GV. 02w1
25A n 'JI
77.
1 f 4 1DO:y, Iw.D n 75
a- Y 1D0. 60A -
1 '�
6,•'Y'
5D 25- n >2
-PA 23
I} N NA n L
6 N a NA
�Ff T
7 fY
29A MW FWa• 18800
4 2f j VA Mnr.Vn IDA
°;»# _'++ 160 ISOA Wk FW - 1bOW
7" ,fa � 1100'j 1/wD M V" ]°ODD
8"" k u3.
7'� L 7„
1
LSD : 25 IMDF•pa• 1AOW
6D 2.8 Mu VAu• 25
50' 25 MUPnd- 2.6
°( JS 39D MiA Fstor• l.6IW
77 Xry-6T} 5g(; 59,0 Mmc Vehr 7°A wM1
6i� �29 $ 39A Mo. PraAW 119.6 uA
5 { ix��^fi'
t-04i}}A'N.0 M PSB 1.19
8.0
8:�3 t 41308�%, 13w.0 M Pn Q MOD
B'� - 13W" 1]00.0
8"
gvFx 1
-,,u,j 25
�
- 9� �: # ]5, ', 35.0 '
y;
f0 ,1F
23_
IDA -
10p t' tw.0
11 Z7ao''^. 2700a
ip t
-11 h f
SD},{ 2°
SD'_ 25 -
1p i..( sSF..� ND
11 §;{i ,✓£ 2H �; 29D -
ti
13 tk�`, f
W � IDA
B t 52
�32
-'1
12 2900: 14WA
1]t 2p0p' ZOOOA -
A
12 i
i] LS iy
f G
6D 2D
.6D 111 23
nl
_
ti h i/ 2 39 ;. JB.D
1/ C fit& 4 87 1 6ia
41 n S
EA
Yw
11 2000 2000a
t6 �' 290b;'ry 2900A
11>
1553 Ei
6.0 3b
5023
:
16
182'A
15 Y{}t 14
.3 1IA
} 23.. 23D
16 t N,.S• 33pp',. 3]OpA
15 y# 7 S3
,. SD;.l 29
3
1B� # 11 ,. MA
}`
22 1 Ma
17 t" ': 3000y ]Dooa
17} ;6D'
23 -
1] ik}r 4 �60 SDA
15 h`j •
Y 19 '. IDA
18 i ]i60t; 31WD
2500-t 3800A
t8;3> {
rSD 25
'6D 25
t5 �{'S y. N'� NA ,
1B 3B 1,: J9D
20Po d } j fi
21 %t i, ;
q 31 21M
25 ;, WA
Y,yGl t
20 �. 32W J A
21 e woe„ 5I06.0
20;
21 yY kYS
'. 90 ' u
6A 25
20
21 �•i 3'"^ 0 52D
221, f^Y er
16a 19.0
�Y
22,q '.� y606 ]3wA
23;c�,{ {
.. BA;�i2.9
22 C+T T1t( T2D
2]t_
_70 { 70D
21 125�06' 2800D
% D kl 2�5
p'Yry 1;t "p
'
2Af i
25 y
151 6IA
15.. 15D
t -
25r 3500D
25°
15D u
35 ZS i:. 26A ,
27 Y h
10)k3 IDA -
36ND
27� f 3706.' ]700D
21k t
2T{
S0 . 2S
'SAG 25
25 ry }' k. 1] y 19A
27 '.. Y 139 .{ 250
20CC,. j+Ya'Y. 2I00., . 2IDOD
�~ I500 5 2MA
29
Sb 26
6D 2.5
25 l)y } It y 110
2B 3
1ITA3A
eA
Sy j
]I,. ,t 1BOp 1BOOD
32 3oaU'a 3000a
]t
ax =' / t
_
25
-_6D hf ib4.,
sad, u
E <{. y 210
]0,{ { _
M .'25 qS ]25A _
32f i
9 t<
o-x as
t8t5A
-
33� itifi i000 2000D
9 1,
it1 .(
3]rV { v J5 WA
w ?
39
8 F2 8D
18D1 15.0
x }'y.A 27W 2700.0
36}' 0100(f J100A
pl
]6, 9
51.E
7 aT •,1
31, y'i� !2511 26D
36}33 'p 2D7 20D
>B N�f3
8i'� 95
3gNF Jk2 S,i f7100"Y 2200.0
375 r Y �.2600{ 26DOIC -
Je- j1
37 "}
]B ij `h pia ^a NA +:
31 lY _
3p{ pb%E'
3H �""
t ry
30 C 2 15001E 1500D ..
]9 ' t 220Du -22DOD
YJ i
39
•�
/O I.,Uw}
S _
N �!i• d 2200a 2200A
11 h t
12�Yt v+.
3
It y 6 1500-.# ISDOA
/2 �1 1; i1560`•` 1500.0
12 y
- Y
NC^rrrosss Jt" IX _
N
N kY /700ia}' 1700D
1D00.; 1800A
N rk 't7
41 '
�k
3 S
-
Ig ryr Yk.
/5 iy� S NOp* 2100A
k
18` } .y
,4 y
/S } 73iry
.
1°j L
�j,tj F3 `xx
h
1°t Y2100'g HOOD
11!! L. t10DF^ IIO610
N
IT �`i
S° f
IT
�!„ ++tt
C 1 •
M Yt j % i } 1200'3 12WA -
15 33,,.. '4..
\
N 1.1.'`•� ?try Y
IBC
0{�
0[ i-9 900E44C 3000A
1?
2=.
OF-
��,
53
7D0 , _700D
59Ky :'770 770D
65;•..
�� _
d`I50: /80.0
600.0
SW{
ND.6
6
60 L 3 l
61 t ,�•.X,.:
i fi`y
t611,K§.'V-S
B0 k f` s00 SDOA
t y I10 NOD
82 X'f; 306 200.0
°1
0}
b f1
Aj Rt
DC3' 3S�m� 800 " 800.0
w4 fii�
wQ#g�. NO I; Non
A
K
11 {'• ,. ._
�'
55 720 72DA
S6O� MA
53
Do
7 t i
3{,y't." 3=10� MA
S
m {t^�
1 7<
ki{ t7
390 =.0
70 °tp:' 00.0
70 k13
71 tt } '�,
-
t�{. 3
4, {
71 5` a DDD
DOA
71 F
i2 J'
71
722y 3
Ff..P
724 630A
800 j 800A
nY y
71
x%T'j
S,
na .Y -
71 -
712f
75
S20D
751'`� �T70 . 770A
7
753 H L4-'
7e
18f
76 1
76 ,{wry "&
77
�Y•,ai _
'i i
75 670 670.0
]7 y i2 180D
}
T7 a1E ,t°}
+i.�
t : ,
T71S,>c
yi
7. trvA J, 'Y.;'
_
tQ180
4'M� 5 DOD
.J{'`T
ESL Cepg!
•}}
71�
hi'
j"y 'S T
at
a >.'`
et
825y+NyiP� i'S"
'i t1k� _
OI i b,t;) '�}�7k
&
ri)
52at
'i # .. -
DS' st33yy�'83
wC n
G}
PY
d3•C
59} ty FY�
88Hy
f 3�1 �-
7
58 i J
d0 ej "C '.
}
es x�,Kt
� �
l
89 ��i}h'F¢ �
j!i
N �u"rp
m7 i }
q P { 4 vg
i!
57
81 €i.3 #
m s
-
,
z.a.
5]
07
Do
'4SL
K
el
BSk.iO'l,
DaY
:.
o-a.X ;�
q b `t Y $ -
"9e i} k
".
k i - ( '
oe;}7.1
B5
�i�Ft -
+. J•
g91
Y,3: _
s..Y� i
yY;
i
100
I D14 d
�
1 D i{tt.t•
4N Yr 4,
100
1N .% F
i h
10
1w eC L•. Z
1D3 aya
1wY wE��sw��x
fL
t 'i
�i"i•.I:1
1025
iwrvsf..k� .%'a 1R. �"S+G
tw �,ns_«.��..
��.T�
IN t
tw 2F.v....... ul ...sill -

Whole Effluent Toxicity Testing Self -Monitoring Summary July 14, 2008
FACILITY REQUIREMENT
YEAR JAN
FEB
MAR APR
MAY
_ _ _
JUN JUL
AUG
SEP OCT
NOV
DEC
W Pittsboro WWTP chr lim: 90%
Ceri7dPF i
2004 — '
—
Pass—
-
Pass —
—
Pass,>100(P) —
—
Pass
NCO020354/001 Begim2/l/2007 , Frequency. Q Mar Jun Sep Dec
+ NonComp:Single
2005 >100(P)
—
Pass,>100(P) —
—
Pass,>100(P) —
—
Pass —
—
Pass
County. Chatham Region: RRO Subbasin: CPF04
2006 —
—
Pass —
—
Pass —,
—
Pass —
—
Pass
PF: 0.75 special
2007 —
—
Pass —
—
Pass —
—
Pass —
—
Pass
7Q10:0.000 IWC(%) 100 Order:
2008 "—
—
Pass —
—
Pass
Plantation Pipeline Co. (001) 24hr LC50 so monit epis fthd •
Fthd24Ac
2004 —
>100
NCO051161/001 Begm:2/l/2007 Frequency. A
NonComp:
2005 — .
NRh100
- —
—
— —
—
— —
—
—
County. Guilford Region: WSRO Subbasin: CPF08
2006 >100
—
— —
—
— —
— —
—
—
PF: Special
2007 —-
7QI0:0.0 IWC(%)NA order
2008 —
—
- —
—
Plantation Pipeline Co. (002) - 24hr LC50 ac monit epic ftbd
Fthd24Ac
2004 —-
NC0051161/002 Begim2/l/2007 Frequency A
NonComp:
2005 —
NR/-100
— —
—
— —
—
— —
—
—
County Guilford Region: WSRO Subbasin: CPF08
2006 >100—
'PF: ' Special
2007 —
—
— —
—
— —
—
— —
—
— -
7Q10:0.00 lWC(%)NA Order
_
2008 —
—
— —
—
PPG Industries Lexington Plant chrlim: 48%
Cc
2004 —
Fall
>72 >72
Pass
— —
Pass
— —
Pass
—
NC0004626/001 Begin:9/l/2004 Frequency Q Feb May Aug Nov
+ NonComp:Single
2005'—
Pass
— —
Pass
— —
Pass
——
Pass
—
County Davidson Region: WSRO Subbasin: YAD04
2006 —
Pass
— —
Pass
— —
Pass
— —
Pass
—
PF: 0.6 Special.
. —
Pass—
—
Pass
— —
Pass
— —
Pass(s)
—
7Q10:1.0 IWC(Vo)48.19 '- Ordn:
2008 —
Pass(s).
— —
Pass
PPG -Shelby -001 - chr lim: 33 %
Ceri7dPF
V 2004 Pass
—
—
,' Pass
—
—
Pass
—
. —
Pass
—
—
NC0004685/001 Begin:12/1/2005 •Frequency.'Q Jan Apr Jul Oct
+ NonComp:Single
2005 Pass.
—.
—
, Pass
—
—
Pass
-
—
Pass
—
—
County. Cleveland Region: MRO Subbasin: BRD04
2006 Pass
—
—
Pass
—
—
Pass
—
—
Pass
—
—
PF: 1.3 Special
2007 Pass
—
—
Pass
—
—
Pass
—.
—
Pass
—
—
7Q10: 4.0 IWC(%) 33 Order.
2008 Pass
—
—
Pass
Primary Energy LLC a/W2 Cogentrlx003 chr Inn: 90%-
Cer7dChV
2004 —
>100
—
—
>100
—
—
>100
—
—
>100
N00065081/003 Beghl:2/l/2008 Frequency Q Feb May Aug Nov
+ NonComp:Smgle
2005 —
>10o
-
.—
>100
—
—
94.87'
—
—
>100
—
County. Person - Region: RRO Subbasin: ROA05.
- 2008 -
94.9
—
—
<22.5
<22.5
58.1
>100
>100
>100
>100
>100
PF: VAR Special
2007 >too
>100
94.9
>100
—
—
>100
—
—
>100
—
' 7Q10: 0.0 IWC(%) 100 Order.,
2008 —
>100
—
—
>100
-
-
Princeton WWTP chr lint: 7%
Ceri7dPF
2004 —
.—
Pass
—
--
Pass
—
—
Pass
—
—
Pass
NCO0266621001 Begin:7/1/2008 Frequency. Q Mar Jan Sep Dec
+ NonComp:Single
2005 — .
—
Pass
—
—
Pass
—
—
Pass .
—
—
Pass
County: Johnston Region: RRO Subbasin: NEU06
2006 —
—
Pass
—
—
Pass
• —
Pass
—
—
Pass
PF: 0.275 Special
2007 —
—
Pass
—
—
Pass
—
—
Pass
—
—
Pass
7QI0:5.50 IWC(%)7.19 Ordw.
2008 —
—
Pass
—
—
Pass
Progress Energy-Roxboro/003 24hr ac p/f limn: 90% fthd
Fthd24PF
2004 —
—
Pass
—
—
Pass
—
—
Pass
—
—
. Pass
NC0003425/003 Begin:5/l/2007 Frequency: QP/F + MarJun Sep Dec
NonComp:Single
2005—
—
Pass
—
—
Pass
—
—
Pass
—
—
Pass
County. Person Region: RRO Subbasin: ROA05
2006 —
—
Pass
—
—
Pass
—
—
Pass
—
—
Pass
PF: NA Special
2007 —
—
Pass
—
—
Pass
—
-
Pass
—
—
Pass
7QIO: lake IWC(a/o)NA Order: _
' 2008 —,
—!
Pass
Progress Energy-Roxboro/006 - 24hr LC50 ac monit epis fthd
Fthd24Ac
2004 —
—
—
—
—
>99—
NC0003425/006' Begin:5/1/2007 Frequency. A
NonComp:
2005 —
—
—
—
H
—
>99
—
—
—
—
County Person Region: RRO Subbasin: ROA05 -
2006 >99
—
—
—
—
—
- —
—
—
—
—
—
PF: NA special
2007 —
>99
7Q 10: Lake IWC(%) NA Order.
2008, >100
—
—
—
—
PYA/Monarch Inc. chr lint 90%
Ceri7dPF
2004 —
—
N
—
—
N
—
—
H
—
—
H
.NC0085561/001 Begin:8/1/1996 •Frequency:QP/F + MarJun Sep Dec
'NonComp:Single
2005 —
—
H
—
—
H
—
—
H
County. Mecklenburg Region: MRO Subbasin: CTB34
2006 —
—
H
—
—
H
—
-
H'
—
—
H
PF: 0.0216 Special
2007 —
—
H
—.
—
H
—
—
H
—
—
H
7Q10: 0.0 tWC(%) 100 Order.
2008 —
—
H
—
—
Raeford WWTP 'chr lim: 9%
Ceri7dPF
2004 —
Pass
—
—
Pass
—
—
Pass
—
—
Pass
—
NC0026514/001 Begm:1/1/2007 Frequency-Q Feb May Aug Nov
+ NonComp:Single'
2005 -
Pass
—
—
Pass
—
—
Pass
—
—
Pass
—
Counly. He Region: FRO Subbasin: CPF15
2006 =
Pass
—
—
Pass
—
>36(P)
Pass,>36(P) >36(P)
>36(P)
Pass
PF: 3.0 Special
2007 —
Paw
—
—
Pass
—
—
Pass
7QIO: 49.0. IWC(%) 8.67 Order. -
_ .
2008 —
Pass
—
—
Pass
Pre 2004 Data
LEGEND: -
PERM - Permit Requirement LET- Administrative Letter - Target Frequency- Monitoring Bequency Q. Quarterly, M- Monthly, BM- Bimonthly; SA- Semiannually A- Annually; OWD- Only when discharging; D- Discontinued monitoring requirement
Begin -First month required 7Q I0 =Receiving stream low Flow criterion (efs) +=quarterly monitoring increases to monthly upon failure or NR Months that testing must occur - ex. Jan, Apr, Jul, Oct NonComp - Current Compliance Requirement
PF - Permitted Bow (MGD) IWCOK a Instre ma waste concentmtiun. PIP - Pass/Fad test AC - Acute CHR - Chronic
Data Notation: f - Fathead Minnow; • - Ceriodaphnia sp.; my - Mysid shrimp; ChV - Chronic value; P - Mortality of stated percentage at highest concentration; at - Performed by DWQ Aquatic Tax Unit; bt - Bad test -
Reporting Notation: -- = Data not required; NR - Not reported Facility Activity Status: I - Inactive, N - Newly Issued(To construct); H - Active but not discharging; t-More data available for month in question; 0 = ORC signature needed
37

I

�0F W ATF9QG Michael F. Easley, Governor
O
1 William G. Ross Jr., Secretary.
North Carolina Department of Environment and Natural Resources
C llinl3tr,
isro Wat r uali
R
}
February 28, 2008
TIMOTHY G MATHIS - NL-. DENR MR0
MANUFACTURING MANAGER
PPG INDUSTRIES FIBER GLASS PRODUCTS INC Q�'SGbtccclat�r Protection
940 WASHBURN SWITCH ROAD
SHELBY NC 28150
Subject Receipt of permit renewal application
NPDES Permit NC0004685
PPG Shelby Facility
Cleveland County
Dear Mr. Mathis:
The NPDES Unit received your permit renewal application on February 27, 2008. A member of the
NPDES Unit will review your application. They will contact you if additional information is required to
complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before
your existing permit expires.
If you have any additional questions concerning renewal of the subject permits, please contact Susan
Wilson at [phone], extension 510.
Sincerely,
Dina Sprinkle
NPDES Unit
cc: CENTRAL FILES
Mgr�re ,vi e RTeggo—n- : e/Surface Water Protection
NPDES Unit
Richard Young, Environmental Engineer, PPG Industries Fiber Glass Products, Inc., 940 Washburn
Switch Road, Shelby, NC 28150
No ` Carolina
Ntura!!y
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone [phone] Customer Service
Internet: www.ncwatercgualitv.orLocation: 512 N. Salisbury St. Raleigh, NC 27604 Fax [phone] I-877-623-6748
An Equal Opportunity/Affirmative Action Employer — 50% Recycled110% Post Consumer Paper

v
PPG Industries Fiber Glass Products, Inc.
Timothy G. Mathis
Manufacturing Manager
Fiber Glass Products
February 25, 2008
Mrs.- Valery Stephens
NC DENR
Water Quality
Point Source Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
940 Washburn Switch Road
SENT VIA CERTIFIED MAIL — RETURN RECEIPT REQ UESTED
Shelby, N.C. 28150
704-434-2261
Extension 206
[e-mail]
Rkr=-CE1VL--'2D
F E B 2 9 2008
NC DENR MR®
DWG -Surface Water Protection
Re: Renewal of NPDES Permit NC0004685
PPG Industries rFiber Glass Products, Inc., Shelby, N.C. Facility
Dear Mrs. Stephens:
We are pleased to enclose an original, signed NPDES Permit Renewal Application package
along with the two required photo copies. This is for the PPG Industries Fiber Glass Products,.
Inc. facility in Shelby, NC. We are requesting the re -issuance of NPDES Permit No.
NC0004685. The primary SIC Code for facility operations is 3229-Pressed and Blown Glass -
not elsewhere classified. Approximately one percent of the waste load is from Azdel, Inc. sheet
laminate facility (SIC 3083). The wastewater oufall, Outfall 001 is located at latitude 35
degrees, 20 minutes, 26 seconds, by longitude 81 degrees, 37 minutes, 0 seconds with the
receiving water being Brushy Creek.
There have not been any changes to the facility since the previous permit renewal. There is a
fluoride limit and weekly fluoride monitoring included in our permit. However, over the last
several years our fluoride has been significantly reduced. Typically the effluent fluoride level is

10`to 20 percent of the limit. We are requesting as part of our renewal that the monitoring.
frequency for fluoride be reduced to monthly monitoring. .
We request that all NPDES Permit questions and issues be directed to. Mr. Richard Young, Sr.
Engineer Associate, Environmental.
As part of this permit renewal package, we have included:
1. Cover letter;
2. Introduction;
3. EPA Form l;
4. EPA Form 2C;
5. Narrative description of the sludge management plan; and
6. Analytical data.
The data presented in Form 2C Section V is based on plant operating data for the period August
2006 to July 2007 and special. analysis conducted by Pace Analytical Services Inc. Copies of the
Pace reports on the special analysis have been provided in the package (Tab G).. The plant
operating data is from monthly DMR submittals.
Please feel free to contact me if you need any additional information or if you have any questions
regarding this submittal.
Sincerely,
Timothy G. Mathis
Manufacturing Manager
Attachment
Cc: Richard Young
File

Certification
I certify that I am familiar with the information contained in this application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
Printed Name of Person Signing: 1 i�y►� t°�l� �* ° 4"���
Title: ce+ ' Gi gr
—�
(Signature of 4Appicant) (Date Signed).
North Carolina General Statute 143-215.6 b (i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan or
other document filed or required to be maintained under Article 21 or regulations of the Environmental Management Commission
implementing that Article, or, who falsifies, tampers with or knowingly renders inaccurate any recording or monitoring device or
method required to be operated or maintained under Article 21 or regulations of the Environmental Management Commission
implementing that Article, shall be guilty, of a misdemeanor punishable by a fine not to exceed $25,000, or by imprisonment not to
exceed six months, or by both. (18 U.S.C. Section 1001 provides a punishment by a fine of not more than $25,000 or imprisonment
not more than 5 years, or both, for a similar offense.)

PPG Industries Fiber Glass Products, Inc.
Shelby, North Carolina
NPDES Wastewater Permit Renewal
Application for Permit Number
NC0004685
February 2008

PPG Industries Fiber Glass Products, Inc.
Shelby, North Carolina
NPDES Wastewater Permit Renewal Application for Permit Number NC0004685
I TABLE OF CONTENTS
Introduction....................................................................................................... ................. 1
SludgeManagement Plant .................................................................................................... *..2
EPAForm 1 ............................................................................................................................ Tab A
EPAForm 2C — pages 1-4 ................................................................................... .................. Tab B
Attachments to Form 2C Sections IIA and IIB ................................................................... I ... Tab C
EPA Form 2C — Intake and Effluent Characteristics — Outfall 001.......................................Tab D
EPA Form 2C — Intake and Effluent Characteristics — Outfall 002 ....................................... Tab E
Figures
TopographicalMaps .............................................................................................................. Tab F
Laboratory Reports
PaceAnalytical .................................................................................... .................................. Tab G

INTRODUCTION
PPG Industries Fiber Glass Products, Inc. (PPG) operates a Fiber Glass manufacturing facility in
Shelby, North Carolina. This facility operates under the existing NPDES Wastewater Permit
Number NC0004685 which expires on August31, 2008. This permit allows the facility to
discharge treated wastewater at 1.3 million gallons/day to outfall 001 and to discharge non -
contact cooling water to outfall 002. In addition to PPG's Fiber Glass Manufacturing operation,
an Azdel, Inc. sheet laminate manufacturing facility is located adjacent to the PPG site and
discharges approximately 10,000 gallons per day to the PPG wastewater treatment plant for
treatment. Wastewater from PPG and Azdel operations are sent to PPG's wastewater plant for
treatment and both operations are covered under the existing permit. Additional details and
clarification for several items relevant to this permit application are highlighted below.
1. , SIC Codes and Outfall 001 Testing
The SIC code for the Azdel, Inc. (sheet laminate facility) is 3083. The Azdel site
discharges 10,000 gallons wastewater per day to the PPG wastewater treatment plant for
treatment. This discharge makes up approximately 1/100th of PPG's wastewater flow.
Therefore, as required for the 3083 SIC code, PPG performed volatile compound testing
on Outfall 001. Results from this testing are incorporated into Form 2C of this
application.
2. Outfall (002) Testing
Outfall 002, the primary. stormwater outfall, is currently permitted for the discharge of
non -contact cooling water. Therefore, PPG conducted the testing as set forth in Form 2C.
This testing also included the required volatile compounds for SIC codes 3083. ,
3. Wet Weather Only Outfalls'
Outfalls 003, 004, 005, 006, 007 and 008 are covered under the General Stormwater
Permit #NCG070000, Certificate of Coverage # NCG070015. These outfalls are wet
weather-outfalls only and would contain little, if any, drainage from industrial areas. For
this renewal, testing was not conducted on these wet -weather outfalls.
4. Sample Reporting and Averaging
Sample reporting and averaging was provided in Form 2C as per NC DENR DWQ's
"Directions for Completing Monthly. Monitoring Reports" dated September 1, 2000..
These instructions provide guidelines with respect to rules for reporting and averaging
less than detectable "<" values. (e.g., a sample result with a value of less than the
detectable limit is considered'to equal "zero" when calculating monthly and long-term
arithmetic averages). Also per NC DENR DMR reporting guidelines, fecal coliform
monthly and long-term averages -were calculated using a geometric mean.
5. Signature Authority
There will be no change requested in signature authority for monthly monitoring report
requirements. Signature authority for monthly monitoring reports as a "Duly Authorized
Representative" per 15A NCAC 2B.0506(b)(2)(D), will remain unchanged and is
delegated to the -person holding the title of Maintenance Manager.

SLUDGE MANAGEMENT PLAN
The wastewater treatment plant (WWTP) sludge generated by the Shelby facility is a mixture of
both primary and secondary sludges. The primary sludge is the result of clarification using lime,
aluminum chloride, polymers and coagulants to achieve floc formation and settling. The
secondary sludge is waste activated sludge from the biological treatment system. The secondary
sludge also contains bentonite clay and a small, amount of ferric chloride.
Both sludges are combined in a sludge thickener/storage tank prior to dewatering. Polymer
addition and mechanical mixing, along with dilution water, are required to prepare the sludge for
the belt press. The sludge is then pumped to the belt press for dewatering.
The belt press has both a gravity drain section and a pressure section where the water is removed.
Typically, the solids are increased from 4-5% as it leaves the storage tank, to 25-30% solids as
discharged from the belt press. The dewatered sludge is transported via screw conveyors to a
roll -off box. The water is routed back to the head of the WWTP.
Before the roll -off box is picked up for disposal, a paint filter test is conducted on the sludge to
ensure that free liquids are not present. The dewatered sludge is then taken to a permitted, lined
landfill for disposal.

TAB A
EPA FORM 1

fill-in areas are s aced for elite type, i.e., 12 charactersfinch . rui mppiuvuu. uivio ivu. I_u,+u-uuuo. Hpprovai expires o-si-az
FORM
U.S. ENVIRONMENTAL PROTECTION AGENCY
I. EPA I.D. NUMBER
1
GENERAL INFORMATION
T/A �
F
��� Consolidated Permits Program
110000349070
GENERAL..
(Read the "General Instructions" before starting)
1
2 13 ,4 15
LABEL ITEMS
GENERAL INSTRUCTIONS .
If a preprinted label has. been provided,
:PA I.D. NUMBER
affix it in the designated s ace. Review the
information if P any of it is
III. FACILITY'NAME
carefully;
incorrect cross through it and enter the
correct data in the appropriate fill-in area
below. Also, if any of the preprinted data is
absent (the area to the left of the label
V. FACILITY PLEASE 'PLACE -LABEL IN THIS SPACE
space lists the information that should
appear) please provide it in the proper fill -
MAILING LIST
in areats) below. If the label is complete
and need not complete Items
.correct you
1,111, V, and VI(except VI-B which must.be
completed regardless). Complete all items
-VI. FACILITY
if no label has been roved. Refer to the .
LOCATION
instructions for detailed item .descriptions
and for the legal authorization under which
this data is collected.
.II. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit 'any permit application forms
to the EPA. If you answer "yes" to any
questions, you must submit this form and the supplemental from listed in the.parenthesis following the question.
Mark "X" in the box in the third column if
the supplemental form is attached. If you answer "no." to each question, you need not submit any of. these forms.
You may answer "no" if your activity is
excluded from permit re uirements; see Section C of the instructions. See also, Section D of the instructions
for definitions of bold-faced terms.
MARK'X"
MARK "X"
SPECIFIC QUESTIONS
SPECIFIC QUESTIONS
FORM
FORM
YES
NO
ATTACHED
YES
NO
ATTACHED
A. Is this facility apublicly owned treatment works
B. Does or will this facility .(either existing or
which results in a discharge to waters .of the
❑
®
❑
proposed) include a concentrated animal
❑
®
❑
U:S.? (FORM.2A)
feeding operation or aquatic animal
production. facility which results in a discharge
to waters of the U.S.? (FORM 2B)
16
17
18
19
20
21
C. Is this facility which currently results in
®
❑
®
D. Is this proposal facility (other than those described
❑
0
❑
discharges waters of the U.S. other than
in A or B above) which will result in a discharge
,to.
those described in A or B"above7 FORM'2C
to waters of the U.S.? FORM 2D
22
23
24
25
26
27
E. Does or will this facility treat, store, or dispose of
F. Do you or will you inject at this facility industrial or '
hazardous wastes? (FORM 3) .
4
❑
❑
municipal effluent below. the lowermost stratum
El
®
❑
containing, within one quarter mile of the well
bore, underground sources of drinking water?
28
'29
30
(FORM 4)
31
32
33
G. Do you or will you' inject at this facility any
H. Do you or will you inject at this facility fluids for
produced water.other fluids which are brought to
the surface in connection -with conventional oil or
❑
®
❑
special processes such as mining of sulfer by the
Frasch process, solution mining of minerals, in
❑
®
❑
.
natural gas. production, inject fluids used for
situ combustion of fossil fuel, or recovery of
enhanced -recovery of oil or natural gas, or inject
geothermal energy? (FORM 4)
fluids. 'for storage `of liquid hydrocarbons?
34
35
36
37
36
39
FORM 4
I. Is this facility a proposed stationary source J. Is this facility a proposed. stationary source
•
which is=one of1he 28 industrial. categories` listed which is NOT one of the 28.industrial categories nn
El ® ❑ ❑
in the instructions and which will potentially' emit t
100 tons .per year of any air pollutant regulated emit 250 , tons per year, of any air pollutant
under the Clean Air Act and may affect or be regulated. under the Clean Air. Act and may affect
located in an attainment areal FORM 5 40 41 J., 42:or-be located in an attainment are? FORM 5 43 1 44 45
III. NAME OF FACILITY
C SKIP
1: PPG Industries Fiber Glass Products Inc.
1516-29 30 69
.IV. FACILITY CONTACT
A. NAME &.TITLE (last, first, &title B..PHONE area code & no.)
.0
.2 Young, Richard — Environmental Engineer 704 434 2261 Ext. 359
15 -1 16 45 46 48 49 51 52 55
'V. FACILITYMAILING ADDRESS
A. STREET OR P.O..BOX
C
3 > 940 Washburn Switch Road
15 1 16 45
B. CITY OR TOWN C. STATE D. ZIP CODE
c
4 Shelby NC 28150
15•. 1 '16 40 41 42 47 .51
VI. FACILITY. LOCATION
A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
C
5 940 Washburn Switch Road
15 16 45
B. COUNTY NAME .
Cleveland
70
C. CITY OR TOWN
D. STATE
E. ZIP CODE
F. COUNTY CODE
NC
28150
F-6—T—shelby
15
16 40
41 42
47 51
52 54
EPA FORM 3510-1 (8-90) CONTINUED ON REVERSE

VII. SIC CODES (4-di it, in order of priority)
A. FIRST B. SECOND
c
3229
(specify)
Stone, Glass, Clay
7
7 3083
(specify)
Laminated Plastics (Azdel, Inc.)
7—
15
16 17
15 16 19
C. THIRD D. FOURTH
c (specify) 7 (specify)
- 7
15, 16 19
II: OPERATOR INFORMATION
A. NAME 'B. Is the. name, listed.in Item
c
VIII-A also the owner?
PPG Industries Fiber Glass Products Inc.
Q YES 0 NO
ff.
18
19 55
C. STATUS OF OPERATOR Enter the appropriate letter into the answer box; if "Other,"specify.)
D: PHONE area code & no.
F '_. FEDERAL.. M = PUBLIC (other than federal or state)
.
P
(specify) NA
c
704
434
2261
A
S. STATE _ 0 = OTHER (specify)'
P =. PRIVATE . .
56
1 16 18
19 21
22 25
15
E. STREET OR PO BOX
940 Washburn Switch -Road
26 55
F. CITY OR TOWN
G. STATE H' ZIP CODE
IX. iNDIAN LAND
C
Shelby
NC 28150 Is the facility, located on lndianaands?..., . '
B..
42 42 47 ... - .5r YES". NO .:
15 -16 - 40
X. EXISTING. ENVIRONMENTAL PERMITS .
A. NPDES' (Discharges to Surface Water
D. PSD Air Emissions'froin`Proosed Sources
44-1 18 30
C
r.A
NC0004685
9 '..
N....
15 .
.16,
.17
18 30-17
B. UIC (Underground Injection of Fluids
E. OTHER (specify)
(Specify)
General Stormwater
Discharge Permit
C
T
I
NA
c
1. r
1 e.
CG070000, NCG070015—COG
9,
U
9
15 .
16.'
.17
18. 30
15
16
1 17
1 18 30.
C. RCRA Hazardous Wastes E..OTHER (specify) (Specify)
c T. -a c: T _e 01958R41 Air Permit
9 R. °- < NCD980559983 g -:
15 1 16' 17 1.18 . 30 s t`15 1 16 1 17 JIB ..: 30
XI:.MAP -
Attach to this' application a't6pographic,rn.6p of the.area extending to at'least one`mile beyond property boundaries; The map must
.;how. the -outline .of the facility, the location -of each';of Its existing:'and .proposed intake and -discharge structures,' each of its
iazardous .waste treatment; storage, or .disposal facilities, and each well. where 'it injects fluids underground. Includeall springs,.
rivers and other surface water bodies in the map area. See instructions for- orecise re uirements
XII .NATURE:OF BUSINESS (provide a brief description)
Continuous strand fiber glass manufacturing for NPDES purposes, the site's wastewater
treatment plant also receives and treats sanitary effluent from Azd'el, Inc. Azdel, Inc.
manufacturers sheet laminate, SIC Code 3083 as noted in Item VII.B. The flow from
Azdel represents only 1 percent of the total flow to the WWTP.
XII1. CERTIFICATION (see instructions) .,
l.certify.underpenalty:oflaw that 1 have personally examined andam familiar with the information submitted -in this application and
all attachments and that, based on my inquiry of:those persons immediately responsible for obtaining the information contained in
the.application,.l believe that the information is true,.accurate and complete. 1 `am aware that there are significant penalties for
submitting -false information, includingthe possibility of fine and imprisonment.
A. NAME & OFFICIAL TITLE (type or print) B. SIGNATU
C. DATE SIGNED
)MMENTS FOR -OFFICIAL USE ONLY '
C
15
16 55
EPA FORM 3510-1 (8-90)

TAB B
EPA FORM 2C
PAGES 1-4

NC0004685 Renewal Applicatio EPA I.D. NUMBER (copyfromlrem I of'rorm 1) Form Approved.
OMB No. 2040-0086.
Please print or type in the unshaded areas only. Annm-1 P H, . 1-14,_oa
FORMU.S.
2 (v
NPDES
I. OUTFALL LOCATION
ENVIRONMENTAL PROTECTION AGENCY
APPLICATIOFOR PERMIT To DISCHARGE WASTEWATER
��/EPA EXISTING MANUFACTURINGNCOMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consolidated Permits Program
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(frsr)
B. LATITUDE
C. LONGITUDE
D. RECEIVING WATER (name)
1. DEG.
2. MIN.
3. SEC.
1. DEG.
2. MIN.
3. SEC.
001.
'35
.20
26
81
37
0
Brushy Creek
002
35
19
23
81
38
12
Unnamed Tributary to Beaverdam Cr
003
35
19
36
81
38
7
Unnamed Tributary to Beaverdam Cr
004
35
19
48
81
37
44
Unnamed Tributary to Brushy Creek
005 35 19 42 81 37 38 Unnamed Tributary to Brushy Creek
Il. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water,_ operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfail, provide,a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1 OUT-
2. OPERATION(S) CONTRIBUTING FLOW
3. TREATMENT
FALL
NO. (!!sr)
a. OPERATION (fist)
)
b. AVERAGE FLOW_
(include anitr)
a. DESCRIPTION
b. LIST CODES FROM
TABLE 2C-1
001
See Attachment 2C.II
B. Clutfall 001
002
Non -Contact Cooling
Underground S rMer
35,000 GPD
None
Stormwater -Peak Flow,
74.9 CFS.
None
llr/hr
003
9tormwater - Peak Fl
w, 12.9 CFS
None
1"/hr
004
Stormwater - Peak Flow,
2.3 CFS
None
1" hr
005
Stormwater - Peak Flow,
1.3 CFS
None
1"/hr
Continued on Next Page
LOFFICIAL USE ONLY (c1fluenrguidelines .pub-coregortes)
EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE
Lek
Lek
Cont.

EPA I.D. NUMBER (copvJrnm Iran / n/7%,rm 1) Form Approved,
NC0004685 Renewal Application OMB No.2040-0086.
Please print or type in the unshaded areas only. I e
FORM`
2 `+
NPDES
I. OUTFALL LOCATION
U.S. ENVIRONMENTAL PROTECTION AGENCY
ew CATION FOR PERMIT TO DISCHARGE WASTEWATER
��/EXISTING MANUFACTURING, COMMERCIAL, MINING AND 'SILVICULTURE OPERATIONS
Consolidated Permits Program
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(l isl)
B. LATITUDE
C. LONGITUDE
D. RECEIVING WATER (nnnre)
1. DEG.
2. MIN.
3. SEC.
1. DEG.
2. MIN.
3. SEC.
006
35
19
23
81
37
18
Unnamed Tributary to Beaverdam C
007
35
19
25
81
37
29
Unnamed Tributary to Beaverdam C
008
35 1
19
24
81
37
48
Unnamed Tributary to Beaverdam C
II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach'a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each oulfall, provide a description of: ,(1). All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW
3. TREATMENT
FALL
NO. (list)
a. OPERATION list ( )
b. AVERAGE FLOW
(include unite)
a. DESCRIPTION
b. LIST CODES FROM
TABLE 2C-1
006
er-Peak Flow
2.8 CFS.
None
1"/hr
007
-
None
1"/hr
008
Stormwater-Peak Flow,
12.9 CFS
None
1 hr
OFFICIAL USE ONLY (ejjlueni guidamesssuh-,rrie,gonc.c)
EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE
aek
aek
aek

NC0004685 Renewal Application
CONTINUED FROM THE FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or 8 intermittent or seasonal?
❑ YES (complete thu fbIlowing table) NO (go to Section 111)
3. FREQUENCY
4. FLOW
a. DAYS PER
B. TOTAL VOLUME
2. OPERATION(s)
WEEK
b. MONTHS
a. FLOW RATE (in mgn
(.specify wiih uniu)
1. OUTFALL
NUMBER (fin)
CONTRIBUTING FLOW
(tiv)
(.rpecffy
nvcr-9c)
PER YEAR.
(."pect# nvernge)
C. DURATION
1. LONGTERM
2: MAXIMUM
t. LONG TERM
2. MAXIMUM
AVERAGE
DAILY
AVERAGE
DAILY
(in deyr)
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?.
YES (complete Item III-B) NO (go io Section 10
B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)?
❑ YES (complele llein X-C) , ❑ NO (go to Section 10
C. If you answered "yes" to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the
applicable effluent guideline, and indicate the affected ouffalls.
1. AVERAGE DAILY PRODUCTION
2. AFFECTED OUTFALLS
(list ou(Jall numbers)
a. QUANTITY PER DAY
b. UNITS OF MEASURE
.
cOPERATION, PRODUCT, MATERIAL, ETC.
(specify)
IV. IMPROVEMENTS
A. Are you now required by any'Federal. State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater'
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to,
permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
❑ YES (complete the fidlmving !able) ® NO (go !011em IV--B)
1. IDENTIFICATION OF CONDITION,
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL COMPLIANCE DATE
AGREEMENT, ETC.
a. NO.
b. SOURCE OF DISCHARGE
a. REQUIRED
b. PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for
construction.
❑ MARK W IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3 .

EPA I.D. NUMBER (copy frnm lrem NC0004685Renewal l nJ'Form 1) , Application
CONTINUED FROM PAGE 2
V. INTAKE AND EFFLUENT CHARACTERISTICS
A, B. & C: See instructions before proceeding — Complete one set of tables for each outfall — Annotate the outfall number in the space provided.
NOTE: Tables V-A, V-B, and V-C are Included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged
from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1. POLLUTANT
2. SOURCE
I.POLLUTANT
2. SOURCE
Acetaldehyde
The pollutants listed
Both were below the
Benzyl Chloride
in V.D.1. have been
method detection lim'
Epichlorohydrin
detected in trace f:
Ethylene Diamine
concentrations in a
-Formaldehyde
small fraction of PPG's
Styrene
raw materials (as per
Triethylamine
manufacturer MOSS).
Vinyl Acetate
Therefore, these pollutants
may be present in extremely
trace concentrations in.
the influent to the WWTP
prior to treatment and in
even lower concentrations
(if present at all) in the
effluent to Outfal #001.
Previous vinyl acetate and
M thod 8260B
VI. POTENTIAL DISCHARGES NOT COVERED
BY ANALYSIS
Is any pollutant listed in Item V-C a substance
or a component of a substance which you currently use or manufacture as an intermediate
or final product or byproduct?
❑ YES (hsf all such panufanrs
below ) ❑X NO (ga
EPA Form 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE

NC0004685.Renewal Application
CONTINUED FROM THE FRONT
VII. BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
® YES Went!& the rest(N) and describe their purposes helms) E] NO (go to Section VIM
Chronic toxicity testing (Ceriodaphnia) is conducted quarterly as per NPDES
permit requirements.
VIII. CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
ERYES (list the name, address, and telephone number nf,' and pollutants analyzed by, NO (go to Section IA)
each such laboratory or,/irm below)
A. NAME B. ADDRESS C. TELEPHONE D. POLLUTANTS ANALYZED
(area code X no.) (list)
Pace Analytical 9800 Kincey Ave., Suite 100
Services, Inc. Huntersville, NC 28078 [phone] All except pH,
(EPA Lab Code: fecal, temperature
NC00014) and conductivity
IX. CERTIFICATION
I 'certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
A. NAME & OFFICIAL TITLE (ty.m. or print) S. PHONE NO. (area code & no.)
C. SIGN E 00, U V D. DATE SIGNED
X-m� � z4 de
A Form 3510- (8-90) PAGE 4 of 4

TAB C
'ATTACHMENTS TO FORM 2C
SECTIONS IIA AND IIB

EPA FORM 2C SECTION II.A.
OUTFALL 003, 004, 005, 006, 007 3 008 SCHEMATIC
PPG INDUSTRIES FIBER GLASS PRODUCTS, INC.
Stormwater Stormwater
30.8 acres 3.1 acres
Outfall
IF
l
#003
!#004
Peak flow
Peak flow.
12.9 cfs
2.3 cfs
Stormwater I I Stormwater I I Stormwater I I Stormwater
2.1 acres 9.0 acres 33.8 acres 2.6 acres
Outfall
#005
Peak flow
1.3 cfs
Outfall Outfall Outfall
#006 #007 #008
Peak flow . Peaowl eak flow
2.8.cfs 12.2 cfs 0.9 cfs
Discharges from Outfalls #003, #004, #005, #006, #007 8 #008 are covered under the General Stormwater Discharge Perm!
#NC070000, COC #:NCG070015.
These areas contain limited drainage from industrial areas of the property. Outfall D02 is the primary stormwater discharge point
of the industrial portions of the property.
Peak flows were calculated using the Rational Method (Q = CiA) where:
Q peak flow (cfs)
C = runoff coefficient (where-..9 = impermeable, .8 = graveled, .3 = grassed, .1 = wooded)
i = intensity
A = area (acres)
note: the above peak flows were calculated using an intensity of 17hr. See table below for runoff coefficient calculations.
RUNOFF COEFFICIENT CALCULATIONS
OUTFALL
C
003
0.42
20% industrial (.9), 80%.grassed (.3)
004
0.75
90% paved parking lot (.9) and 10% grassed (.3)
005
0.48
30% paved parking lot (.9) and 70% grassed (.3)
006
0.31
95% lawn (.3), 2.5% wooded (.1), 2.5% graveled (.8)
007
0.36
10% industrial (.9) and 90% grassed (.3)
008
0.36
10% industrial (.9) and 90% grassed (.3)

EPA FORM 2C SECTION II.A.
OUTFALL 001 SCHEMATIC
PPG INDUSTRIES FIBER GLASS PRODUCTS, INC.
City Water .
Supply
1,500,000 gpd
Research Misc. Sanitary Boilers Misc Process Fabrication Forming
1,000 3,000 60,000 43,00011 Water 15,000 850,000
gpd I gpd gpd, I gpd 75,000 gpd . gpd gpd
Evaporation
335,000
gpd
Stormwater
Product
Garage/Pads
1,300
(185.000 gpd)
gpd
1" rainfall
AZDEL SIC
CODE #3083 WWTP
—10,000 gpd (see WVVTP Schematic)
Sludge
1.4
Dewatering recycle
33,250 gpd
O UTFALL
#001
up to 1.3
MGD

EPA FORM 2C SECTION II.A.
OUTFALL 002 SCHEMATIC
PPG INDUSTRIES FIBER GLASS PRODUCTS, INC.
City
Water
Supply
Stormwater Non -Contact
98.6 acres Cooling
up to 115,000
peak flow = gpd
Underground
Spring
est
35.000 and
OUTFALL
4002
up to 150,000 gpd
+ stormwater
Notes: Outfall 002 is the primary stormwater outfall for the industrial portions of the property.
Cooling water discharges from this outfall are permitted under NPDES permit NC00D4635
Stormwater Discharges are covered under the General Stormwater Discharge Permit #NC07D000, COC #:NCG07D015
Stormwater Peak flow was calculated using the Rational Method (Q = CiA) where:
Q = peak flow (cfs)
C = runoff coefficient (where:.9 = impermeable, .a = graveled, .3 = grassed..1 = wooded)
i = intensity
A = area (acres)
note:. the above peak flow for stormwater was calculated using an intensity of 1'Ihr.
The runoff coefficient (C) used was 0.76 based an the following estimate: 80% industrial (.9), 10% grassed (.3), to%
wooded (A)

EPA FORM 2C SECTION II.B.
WWTPTREATMENT /OUTFALL001 SCHEMATIC
PPG INDUSTRIES FIBER GLASS PRODUCTS, INC.
NPDES PERMIT NC0004686 RENEWAL APPLICATIONC�)
GI
8 Process Water - (0.MGD)
Sani- O.D6 MBAR GRIN G FLOW LOAD FLASH MIX PRIMARY
SCREEN EQUALIZATION EQUALIZATION TANK CLARIFIERS
Stormwater 0.12 MGD 1" 1-T 1-L 1-0 2-D 1-0, 1-G; 2-C 1-1_1
AZDEL. Inc - (0.01 MGDI
OUTFALL
#001
4-A
Lime AIC13 Anionic Polymer
sludge to
Cationic Coagulant thickener
ABW SAND SECONDARY AERATION
FILTRATION CLARIFIERS (3) TANKS (2)
1-V 2-C, 1-U 3-A
RECYCLE / FaCts Litne
COOLING Oeloarnef
WATER Anionic H2Po�
4•C Polymer
SLUDGE PROCESS SCHEMATIC +
sludge to
GRAVITY thickener
THICKENER
5 LBELT PRESS
5-E, 1-0, 5-C Polymar /
Dilution Water
water sludge to
to head of Landfill
WWTP 5-Q
4•C ) (
Defoamer
RAS to
Aeration
J
s
6enlonite Clay
Treatment Codes Used from Table 2C-1
1-G
Flocculation
1-L
Grinding (Comminutors)
1-O
Mixing
1-T
Screening
1-U
Sedimentation (Settling)
1-V
Sand Filtration
2-C
Chemical Precipitation
2-D
Coagulation
3-A
Activated Sludge
4-A
Discharge to Surface Water
4-C
Re -Use / Recycle of Effluent
5-C
Belt Filtration
5-E
Chemical Conditioning
5-L
Gravity Thickening
5-Q
Landfill

TAB D
EPA FORM 2C
INTAKE AND EFFLUENT CHARACTERISTICS
, OUTFALL 001
ME

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (copyjromitem 1 ojForrn 1)
on separate sheets (use the same formal) instead of completing these pages.
SEE INSTRUCTIONS.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) OUTFALL NO. O01
PART A -You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional. details.
3. UNITS
4. INTAKE
2. EFFLUENT
(specify ijblank)
(optional)
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a. MAXIMUM DAILY VALUE
(ijarailable)
(ijarailable)
AVERAGE VALUE
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
1. POLLUTANT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
(1) CONCENTRATION
.(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Biochemical Oxygen
Demand (BOD)
12.0
69.05
7.8 .
43.6
2.28
12.95
52
mg/1
lbs
b. Chemical Oxygen
Demand (COD)
25
0
1
mg/1
lbs
c. Total Organic Carbon
(TOC)
4.9
27.0
1
mg/1
lbs
d. Total Suspended
Solids(TSS)
14.0
71.22
4.1
21.08
1.36
7.38
52
Mg/1
lbs
e.Ammonia (as M
8.40
43.40
5.40
30.30
1.35
8.13
52.
mg/1
lbs
I. Flow
VALUE . .
VALUE
VALUE
VALUE
0.87
0.70
0.66.
365
MGD
g. Temperature
VALUE 19.40
VALUE 17 0
VALUE 19
130
ec
VALUE
(u•fnler]
.
h. Temperature
VALUE
VALUE
VALUE
VALUE
(summer)
28..8 _
26.8
24.7
130
°c
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
' '
'
I. pH
5.9
8.9
s
260
STANDARD UNITS
PART B - Mark "X' in column 2=a for each pollutant you know or have reason to believe is present. Mark 'X" in column 2-1; for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either
directly, or indirectly, but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.
Z. MARK'X"
3. EFFLUENT
4. UNITS
S. INTAKE (oplionaq
1. POLLUTANT
AND
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM AVERAGE
CAS NO.
a
b,
a. MAXIMUM. DAILY VALUE
i arailable (j )
(ijarailable)
VALUE
(1)
(1)
(1)
(1)
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(ijarailable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS .
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Bromide
(24959-67-9)
X.
b. Chlorine, Total
Residual
X
c. Color
X
d. Fecal Coliform
X
49
13
2
52'
#/ 100m1
e. Fluoride
(1698448-8)
X
2.0
11.34
1.4
7.68
0.76
4.23
52
mg/1
lbs
L Nitrate -Nitrite
(asM
X
6.8
34.59
5.17
29.93
3
mg/1
lbs
EPA Form 3510-2C (8-90) PAGE V-1
CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
AND
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
CAS NO.
a
b.
a. MAXIMUM DAILY VALUE
(ifavailable)
(ifavailable)
AVERAGE VALUE
(1)
(1)
(1)
(1)
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(ifavoilable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
g. Nitrogen,
Total Organic (as
N)
X
3.10
15.77
1.97
11.16
3
mg/1
lbs
h. Oil and
Grease
x23
155.37
7.0
31.07
1.40
6.78
52
mg/1
lbs
I. Phosphorus
(7
g
(77z3-1a-3-14-a)
1.07
5.44
0. 27
1. 36
4
mg/1
lbs
J. Radioactivity
(1) Alpha, Total
x
(2) Bela, Total
X
(3) Radium,
X
Total
(4) Radium 226,
X
Total
k. Sulfate
'
(a SOJ
X
8.7.
47.9
1
mg/1
lbs
(14808-79-8)
I. Sulfide
(as 5)
X
m. SuKle
(-SO,)
x
(14265-45-3)
2.0
1
Mg/1
lb s
n. Surfactants
X
0.36
o. Aluminum,
Total
(7a29-so-s)
X
4 0. 1.
0
1
Mg/1
lbs
p. Barium, Total
(7440-39-3)
q. Boron, Total
(7440-42-8)
x
0.3
1.6
1
Mg/1
lbs
r. Cobalt, Total
'
(7440484)
X
s. Iron, Total
(7439-89-6)
X
< 0.05
0
1
Mg/1
lbs
I. Magnesium,
Total
x
(7439-954)
-
u. Molybdenum,
Total
X
2.1
11.6
1.
m 1
g /
lbs
(7439-98-7)
v. Manganese,
Total
X
(7439-96-5)
w. Tin, Total
(7440-31-5)
X
x. Titanium,
Total
X
(7440-32-6)
EPA Form 3510-2G (8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copyfrom Lem I of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark W in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater ouffalls, and nonrequired GC/MS
fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe.is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or -have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for
additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
C. LONG TERM AVRG.
a. LONG TERM
AND
a. MAXIMUM DAILY VALUE
(ifayailable)
VALUE (ifarailoble)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO..OF
(1)
(1)
(1)
(1)
(rjarnilable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1 M. Antimony, Total
(7440-36-0)
X
2M. Arsenic, Total
(7440-38-2)
X
40.0050
0
1
Mg/1
lbs
3M. Beryllium, Total
(7449-41-7)
X
4M. Cadmium, Total
(7440-43-9)
SM. Chromium,
Total(7440-47-3)
X
L0.0050
0
1
mg/1
lbs
SM. Copper, Total
(7440-50-8)
0.036
0.19
0.031
0.17
0.019
0.10 24
mg/1
lbs
7M. Lead, Total
(7439-92-1)
X0.00094
0.06
0.0008
0.005
12
Ug/1
lbs
SM. Mercury, Total
(7439-97-6)
X
-
9M. Nickel, Total
(7440-02-0)
X
10M. Selenium,
Total (7782-49-2)
X
11M. Silver, Total
(7440-22-4)
X40.0050
0
1
mg/1
lbs
12M. Thallium,
Total (7440-28-0)
X
13M. Zinc, Total
(7440-66-6)
X
0,088
0.55
0.06&
0.36
0.03
0.19
24
mg/1
lbs
14M. Cyanide,
Total (57-12-5)
X
15M. Phenols,
Total
X
DIOXIN
2.3.7,8-Tetra-
DESCRIBE RESULTS
chlorodibenzo-P-
Dioxin It764-01-6)
X
EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
1-POLLUTANT
2: MARK "X"
3. EFFLUENT`
4. UNITS
5. INTAKE (oprional)
AND
CAS NUMBER
(ifavailable)
a-
TESTING
REQUIRED
b.
BELIEVED
PRESENT
C.
BELIEVED
ABSENT
a- MAXIMUM DAILY VALUE
(1)
CONCENTRATION (2) MASS
b. MAXIMUM 30 DAY VALUE
(ifavailable)
(1)
CONCENTRATION (2) MASS
c. LONG TERM AVRG.
VALUE (ifavailable)
(1) 1
CONCENTRATION (2) MASS
d. NO. OF
ANALYSES
a. CONCEN-
TRATION
b. MASS
a. LONG TERM
AVERAGE VALUE
b. NO. OF
ANALYSES
(1)
CONCENTRATION
(2) MASS
GC/MS FRACTION —VOLATILE COMPOUNDS,
IV. Accrolein
(107-02-8)
g
40,100
0
1
mg/1
lbs
2V. Ac yfonitrile
(107-13-1)
X
-1- 0. 100
0
1
mg/1
lbs
3V. Benzene
(71-43-2)
X
0
1
mg/1
.lbs
W. Bis (Chlorro-
v/hv!) Ether
_
g
< 0.0052 .
0
1
Mg/1
lbs
SV. Bromoform
(75-25-2)
X
40.005
0
1
mg/1
lbs .
6V. Carbon
Tetrachloride
(56-23-5)
X
< 0.005
0
1
m 1
g /
lbs
7V. Chlorobenzene
(108-90-7)
X
0.005
0
1
mg/1
lbs
BV. Chtorodi-•
bromomethane
(124-48-1)
x
40.005
0
1
mg/1
lbs
9V. Chloroethane
(75-00-3)
< 0.005-
0
1
mg/1
lbs
1 OV. 2-Chloro-
elhylvinyi Ether
(110-75-8)
X
< 0.010-
0
_
1
mg/1
lbs
-
-
I IV. Chloroform
(67-66-3)
12V. Dichloro-
bromomethane
(75-27A)
X
G 0.005
40.005
0
0
1 1
1
mg/1
mg/1
lbs
lbs
13V. Dichloro-
difluoromethane
(7541-8)
X
-
< 0.005
0
1
mg/.1
lbs
14V. 1,1-Dichloro-
elhane(75-34-3)
X
<0.605
0
1
mg/1
lbs
15V. 1,2-Dichloro-
ethane (107-06-2)
C 0.005
0
1.
mg/1
lbs
16V. 1,1-Dichloro-
ethylene (75-35A)
x
0.005 '
0
-
1
mg/1
lbs
1 TV. 1,2-Dichloro-
propane (78-87-5)
18V. 1,3-Dichloro-
propylene
(542-75-6)
X
0-005
< 0.005
0
0
-
1
1
mg/1
mg/1
lbs
lbs
19V. Ethylbenzene
(100-41-4)
X
0.005
0
1
mg/1
lbs
20V. Methyl
Bromide (74-83-9)
<. 0. 010
0
1
Mg/1
lb s
21V. Methyl
Chloride(74-87-3)
PPA Fnn., gSin­r"
iu_o—
< 0.005
0
-
1
mg/1
lbs
NAGS V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
1. POLLUTANT
2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
AND
b. MAXIMUM 30 DAY VALUE
I c. LONG TERM AVRG.
a. LONG TERM
CAS NUMBER
a.
b. '
C.
a. MAXIMUM DAILY VALUE
(ifavailnbleJ
VALUE (if-ailable)
AVERAGE VALUE
(ifavailable)
TESTING
REQUIRED
BELIEVED
PRESENT
BELIEVED
ABSENT
U. NO. OF
ANALYSES
a. CONCEN-
TRATION
b. MASS
b. NO. OF
ANALYSES
(1)
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENITRATION
(2) MASS
(t)
CONCENTRATION
(2) MASS
GCIMS FRACTION —VOLATILE COMPOUNDS (continued)
22V. Methylene
X
Chloride(75-09-2)
40.005
0
1
mg/1
lbs
23V. 1.1,2,2-
Telrachloroethane
X
L • 005
0
1
mg/1
lbs
79-34-5
24V. Tetrachloro-
ethylene (127-18-4)
< 0.005
0
1
mg/1
lbs
25V. Toluene
(108-88-3)
—1
26V. 1,2-Trans-
❑ichloroelhylene
156-60-5
X
1,,,,0.005
0
1
mg/1
lbs
27V. 1,1,1-Trichloro-
ethane(71-55-6)
X
0.005
0
1
mg/1
lbs
28V. 1,1,2-Trichloro-
ethane(79-00-5)
0.005
0
1
MR/1
lbs
29V Trichloro-
ethylene (79-01-6)
140.005
0
1
lbs
30V. Trichloro-
mg/1
8uoromelhane
75-69-4
X
G 0. 010
0
1
m/ 1
lbs
31V. Vinyl Chloride
X
(75-01-4)
GC/MS FRACTION —ACID COMPOUNDS
IA. 2-Chlorophenol
(95-57-8)
X
2A. 2,4-Dichloro-
phenol(120-83-2)
3A. 2,4-Dimethyl-
phenol(105-67-9)
X
4A. 4.6-Dinitro-0-
Cresol(534-52-1)
5A. 2,4-Dinitro-
phenol(51-28-5)
X
6A. 2-Nitrophenol
(88-75-5)
X.
7A. 4-Nitrophenol
(100-02-7)
X
BA. P-Chloro-M-
Cresal(59-50-7)
X
9A. Pentachloro-
phenol(87-86-5)
X
10A. Phenol
(108-95-2)
X
11 A. 2,4,6-Trichloro-
phenol (88-05-2)
X
-m oo 1u-c 10-aul PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (oprional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
o. LONG TERM AVRG.
a. LONG TERM
AND
. a.
b.
C.
a. MAXIMUM DAILY VALUE
(ijavailable)
VALUE (ijmnilable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ijanailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION.
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GCIMS FRACTION — BASEINEUTRAL COMPOUNDS
1 B. Acenaphthene
(83-32-9)
X
2B. Acenaphtylene
(208-96-8)
3B. Anlhracene
X
(120-12-7).
4B. Benzidine
(92-87-5)
X
5B. Benzo (a)
-
Anthracene
X .
(56-55-3)
6B. Benzo (a)
Pyrene (50-32-8)
X
7B.3,4-Benzo-
0uoranthene
�{
(205-99-2)
8B. Benzo (ghi)
Perylene (191-24-2)
X
9B. Benzo (k)
Fluoranthene
(207-08-9)
10B. Bis (2-Chlora-
eihmxv) Methane1(111-91-1)
X
11B. Bis (2-C'hloro-
edry✓ Ether
X
(111-44-4)
12B. Bis (2-
ChloroisaproAvl)
X
Ether(102-80-1)
13B. Bis (2-Ethyl-
he)ryt) Phthalate
(117-81-7)
X
47.5
0.26
1
ug/1
lbs
148. 4-Bromophenyl
Phenyl Ether
X
(101-55-3)
158. Butyl Benzyl
Phthalate (85-68-7)
168. 2-Chloro-
X
naphthalene
(91-58-7)
178. 4-Chloro-
phenyl Phenyl Ether
X
(7005-72-3)
18B. Chrysene
(218-01-9)
X
19B. Dibenzo (a,h)
Anlhracene -
-
-
(53-70-3)
X
20B. 1,2-Dichloro-
benzene (95-50-1)
218.1,3-Di-chloro-
'
benzene(541-73-1)
❑rn roan oo iu-2C; (o-au) PAGE V-6
CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
I.POLLUTANT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. a. LONG TERM
AND
a, b. c, a. MAXIMUM DAILY VALUE (ifavailable) VALUE Qfovailoble) AVERAGE VALUE
CAS NUMBER
TESTING BELIEVED BELIEVED (1) d. NO. OF a. CONCEN-
(favailable) REQUIRED PRESENT ABSENT (1) (t) (1) b. NO. OF
CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES TRATION b. MASS CONCENTRATION (2) MASS ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
22B. 1,4-Dichloro-
benzene(106-46-7)
X
23B. 3,3-Dichloro-
benzidine (91-94-1)
X
..
24B. Dielhyl
-
Phthalate (84-65-2)
_
258. Dimelhyl
Phthalate
X
(131 -11-3)
26B. Di-N-Butyl
Phthalate (84-74-2)
X
t 5.2
_
-
1
u g/ 1
lb S
27B. 2,4-Dinitro-
toluene (121-14-2)
28B. 2,6-Dinitro-
toluene (606-20-2)
X
29B. Di-N-Octyl
X
-
Phlhalale (117-84-0)
308. 1,2-Diphenyl-
hydrazine (as Azo-
X
benzene)(122-66-7)
31B.Fluoranthene
(2D644-0)
32B. Fluarene
(86-73-7)
.
33B. Hexachloro-
benzene(118-74-1)
34B. Hexachloro-
X
butadiene (87-68-3)
358. Hexachloro-
cyclopenladiene
X
(77-47-4)
36B Hexachloro-
ethane (67-72-1)
37B..Indeno
(1,2,3-cd) Pyrene
(193-39-5)
38B.Isophorone
(78-59-1)
$
39B. Naphthalene .
(91-20-3)
X
408. Nitrobenzene
(98-95-3)
x
41 B. N-Nitro-
sodimethylamine
(62-75-9)
X
42B. N-Nilrosodi-
N-Propylamine
X
,
(621-64-7)
PAGE-V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK'X"
3. EFFLUENT
4. UNITS
S. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a
b.
o
a. MAXIMUM DAILY VALUE
(ifarailable)
VALUE (iforadable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
h. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —BASEINEUTRAL COMPOUNDS (continued)
43B. N-Nitro-
sodiphenylamine
X
(86-30-6)
44B. Phenanthrene
(85-01-8)
N
45B.Pyrene
(129-00-0)
X
468. 1,2,4-Td-
-
__7
chlorobenzene
(120-82-1)
X
GCfMS FRACTION —PESTICIDES
1P. Aldrin
(309-00-2)
-
2P. a-BHC
(319-84-6)
X
3P. (1-BHC
(319-85-7)
X
4P. y-BHC
(58-89-9)
X
.
5P. 8-BHC
(319-86-8)
X
6P. Chlordane
(57-74-9)
X
7P. 4,4'-DDT
(50-29-3)
8P. 4,4'-DDE
(72-55-9)
9P. 4,4'-DDD
(72-54-8)
1 OP. Dieldrin
(60-57-1)
X
11P. a-Enosullan
(115-29-7)
X
12P. )3-Endosulfan
(115-29-7)
X
13P. Endosulfan
Sulfate
(1031-07-8)
14P. Endrin
(72-20-8)
15P. Endrin
Aldehyde
(7421-934)
16P. Heptachlor
(76-44-8)
crn rune oa iu-2u (e-au) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copyf -om item I of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-B
1. POLLUTANT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (oplionan
AND
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
CAS NUMBER
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ijarailable)
VALUE (ijarailable)
AVERAGE VALUE
(ijarailable)
TESTING
REQUIRED
BELIEVED
PRESENT
BELIEVED
ABSENT
d. NO, OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION'
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GClMS FRACTION —PESTICIDES (continued)
17P. Heplachlor
Epoxide
X
(1024-57-3)
18P. PCB-1242
(53469-21-9)
X
19P. PCB-1254
(11097-69-1)
.
20P. PCB-1221
(11104-28-2)
X
21P. PCB-1232
(11141-16-5)
X
22P. PCB-1248
(12672-29-6)
X
._
23P. PCB-1260
(11096-82-5)
x
24P. PCB-1016
(12674-11-2)
X
25P.Toxaphene
(8001-35-2)
X
_• % - i PAGE V-9

TAB E
EPA FORM 2C
INTAKE AND EFFLUENT CHARACTERISTICS
OUTFALL 002

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information I EPA I.D. NUMBER (copyfromItem I of Form I)
on separate sheets (use the same format) instead of completing these pages.
SEE INSTRUCTIONS.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 o/Form 2-C) OUTFALL NO. 002
PART A —You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
3. UNITS
4. INTAKE
2. EFFLUENT
(specify l(blank)
(optional)
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a. MAXIMUM DAILY VALUE
Qfavarlable) .
(ifarailable)
AVERAGE VALUE
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
1. POLLUTANT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
(1) CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
(1)
CONCENTRATION
(2) MASS
ANALYSES
a. Biochemical Oxygen
Demand (BOO)
< 2
0
1
mg/1
lbs
b. Chemical Oxygen
Demand. (COD)
Z—' 25.0
0
1
mg/1
lbs
c. Total Organic Carbon
(TOC)
4.1
4.1
1
mg/1
lbs
d. Total Suspended
Solids (TS'S)
7.8
7.8
1
Mg/1
lbs
e. Ammonia (as M
0.13
0.13
1
Mg/1
lbs
f. Flow
VALUE
0.16
VALUE
VALUE
0.12
2
MGD
VALUE
g. Temperature
VALUE
VALUE
VALUE
VALUE
(winter)
13.5
1
°C
h. Temperature
VALUE
VALUE
VALUE
VALUE'
(summer)
23.3
_
1
- °C
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
®= - a
r
^
i. pH
6 7
7.0
2
STANDARD UNITS
PART 8 — Mark 'X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the Instructions for additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a
b
a. MAXIMUM DAILY VALUE
(ifamiluble)
(ifavailable)
VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifarailable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Bromide
(24959-67-9)
X
b. Chlorine, Total
Residual
0.022
0.022
1
mg/1
lbs
c. Color
X
d. Fecal Coliform
X
e. Fluoride
X
(16984.48-8)
f. Nitrate -Nitrite
(as N)
X
EPA Form 3510-2C (8-90) PAGE V-1
CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
I.POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONGTERM
AND
a
b.
a. MAXIMUM DAILY VALUE
(ifmwilable)
(ifavailable)
AVERAGE VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1).
(i�uvuiluble)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
g. Nitrogen,
Total Organic (os
X
N)
h. Oil and
Grease
x
I. Phosphorus
(as P), Total
(7723-14-0)
X
j. Radioactivity
(1) Alpha, Total
X
(2) Beta, Total
X
(3) Radium,
Total
X
(4) Radium 226,
-
Total
X
k. Sulfate
X
(14808-79-8)
I. Sulfide
(OS.S)
X
_
m. SuKle
(as SOS)
X
(14265-45-3)
n. Surfaclanls
X
o. Aluminum,
Total
X
(7429-90-5)
p. Barium, Total
(7440-39-3)
X
q. Boron, Total
-
(7440-42-8)
X
r. Cobalt, Total
(7440-08-4)
X
s. Iron, Total
'
(7439-89-6)
X
I. Magnesium,
Total
X
(7439-95-4)
u. Molybdenum,
Total
X
(7439-98-7)
v. Manganese,
Total
X
(7439-96-5)
w. Tin, Total
(7440-31-5)
X
x. Titanium,
-
Total
(7440-32-6)
X
EPA Form 3510-2C (8-90) PAGE V-2
CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copyfrotn, tem I of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS
fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark 'X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinilrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully.- Complete one table (all 7 pages) for each outfall. See instructions for
additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG,
a. LONG TERM
AND
a:
b.
Q.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifaratlable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
-d. NO. OF
a. CONCEN-
b. NO. OF-
(1)
(1)
(1)
(1j
(ijavailnblc)
REDUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2j MA55
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1 M. Antimony, Total
(7440-36-0)
2M. Arsenic, Total
(7440-38-2)
X
3M. Beryllium, Total
(7440-01-7)
X
W. Cadmium, Total
(7440-43-9)
X
5M. Chromium,
Total (7440-17-3)
6M. Copper, Total
(7440-50-8)
X
7M. Lead, Total
(7439-92-1)
BM. Mercury, Total
(7439-97-6)
X
9M. Nickel, Total
(7440-02-0)
X
10M. Selenium,
Total (7782-49-2)
X
11M. Silver, Total
(7440-224)
X
12M. Thallium,
Total(7440-28-0)
13M. Zinc, Total
(7440-66-6)
X
14M. Cyanide,
Total (57-12-5)
X
15M, Phenols,
Total
X
DIOXIN
2,3,7,8-Tetra-
DESCRIBE RESULTS
chlorodibenzo-p-
X
Dioxin (1764-01-6)
EPA Form 3510-2C (8-90) PAGE V-3
CONTINUE ON REVERSE

CONTINUED FROM THE FRONT'
2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1..POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a
b
C.
a. MAXIMUM DAILY VALUE
(ifavoilable)
VALUE (ifm•ailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(t)
(1)
(1)
(ifavailoble)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS
1V. Accrolein
(107-02-8)
X
< 0. 100
0
1
Mg/1
lbs
2V. Acrylonitrile
(107-13-1)
X
< 0.100
0
1
mg/1
lbs
3V. Benzene
(71-43-2)
X
0.005
0
1
mg/ 1
lbs
4V. Bis (Chlono-
:lhyl)Ether
X
G 0. 005
0
1
mg/1
lbs
5V. Bromoform
(75-25-2)
g
< 0.005
0
1
mg/1
lbs .
6V. Carbon
Tetrachloride
(56-23-5)
X
0.
0
1
/1
Mg/1
lbs
7V. Chlorobenzene
(108-90-7)
g
< 0. 005
0
1
mg/1
lbs
BV. Chlorodi-
bromne
X
0.
0
1
mg /005 1
lbs
48-1)
(124-48-1)
9V. Chloroelhane
(75-00-3)
g
< 0.010
0
1
mg/1
lbs
10V.2-Chlora- .
ethylvinyl Ether
<0.010
0
1
m 1
g /
lbs
(110-75-8)
X
11V. Chloroform
(67-66-3)
. X
e 0.005
0
1
Mg/1.
--
lbs
12V. Dichloro-
bromomethane
(75-274)
X
< 0.005
0
1
m 1
g /
lb S
13V. Dichloro-
diBuoromethane
< 0.005
0
1
Mg/1
lbs
(75-71-8)
X
14V. 1,1-Dichloro-
ethane (75-34-3)
g
< 0.005
0
1
Mg/1
lbs
15V. 1,2-Dichloro-
,
ethane (107-06-2)
g
L.0,005
0
1
Mg/1
lbs
16V. 1,1-6ichlora-
ethylene(75-35A)
g
C 0.005
0
1
mg/1
lbs
17V. 1,2-Dichloro-
propane (78-87-5)
X
< 0.005
0
1
Mg/1
lbs
1 BV. 1,3-Dichloro-
propylene
X
< 0.005
0
1
mg/1
lbs
19V. Ethylbenzene
(100-41-4)
X
0.005
0
1
mg/1
lbs
20V. Methyl
Bromide (74-83-9)
x
40,010
0
1
lbs
21V. Methyl
Chloride (74-87-3)
C0.005
0
1J!Mtg/
lbs
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V4
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b,
C.
a. MAXIMUM DAILY VALUE
(ijavailable)
VALUE (ijavailoble)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
1
(ifarailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS (continued)
22V. Methylene
Chloride (75-09-2)
X
40.005
0
1
mg/1
lbs
23V. 1,1,2,2-
�9r34h5roethane
X
<0.005
0
1
mg/1
lbs
24V. Tetrachloro-
ethylene(127-18A)
X
C 0.005
0
1
mg/1
lbs
25V. Toluene
(108-88-3)
X
L 0.005
0
1
mg/1
lbs
26V. 1,2-Trans-
Dichloroelhylene
156-60-5
1/, 0.005
0
1
mg/1
lbs
2TV. 1,1,1-Trichloro-
elhane(71-55-6)
X
0.005
0
1
mg/1
lbs
28V. 1,1,2-Tdchloro-
ethane(79-00-5)
g
<0.005
0
1
mg/1
lbs
29V Trichloro-
ethylene(79-01-6)
X
0-005
0
1
mg/1
lbs
3OV. Trichloro-
B s-69-alhane
X
[ 0. 010
0
1
mg/1
lbs
31V. Vinyl Chloride
(75-014)
X
< 0.005
0
1
mg/1
lbs
GC/MS FRACTION —ACID COMPOUNDS
1A. 2-Chlorophenol
(95-57-8)
,
2A. 2,4-Dichloro-
phenol(120-83-2)
3A. 2,4-Dimethyl-
phenol(105-67-9)
4A. 4,6-Dinitro-0-
Cresol (534-52-1)
-
5A. 2,4-Dinitro-
phenol (51-28-5)
6A. 2-Nitrophenol
(88-75-5)
7A. 4-Nitrophenol
(100-02-7)
8A. P-Chloro-M-
Cresol (59-50-7)
9A. Penlachloro-
phenol (87-86-5)
'
10A. Phenol
(1 OB-95-2)
11 A. 2,4,6-Trichloro-
phenol (88-05-2)
crn r-orm m lu-lL. (n-8u) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG-
a. LONG TERM
AND
a,
b.
C.
a. MAXIMUM DAILY VALUE
(ijavailable)
VALUE (!jm•ailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
1
(ef'available)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GCIMS FRACTION — BASE/NEUTRAL COMPOUNDS
113. Acenaphthene
(83-32-9)
x
2B. Acenaphtylene
(208-96-8)
3B. Anlhracene
X
(120-12-7)
4B. Benzidine
X
(92-87-5)
5B. Benzo (a)
X
Anlhracene
(56-55-3)
6B. Benzo (a)
X
Pyrene (50-32-8)
7B. 3,4-Benzo-
Buoranlhene
(205-99-2)
X
8B. Benzo (ght)
x
Perylene (191-24-2)
9B. Benzo (k)
Fluoranthene
X
(207-08-9)
-
10B. Bis (2-Chloro-
ethosy) Methane
X
(111-91-1)
11B. Bis (2-C'hloro-
edtvo Ether
X
(111-44-4)
12B. Bis (2-
Chroroisopropyl)
X
Ether (1D2-80-1)
13B. Bis (2-Ethyl-
h-yl) Phthalate
X
(117-81-7)
14B. 4-Bromophenyl
'
Phenyl Ether
(101-55-3)
X
15B. Butyl Benzyl
Phthalate (85-60-7)
X
'
16B. 2-Chloro-
naphlhalene
X
(91-58-7)
17B. 4-Chloro-
phenyl Phenyl Ether
X
(7005-72-3)
18B.Chrysene
(218-01-9)
X
19B. Dibenzo (a.h)
Anlhracene
X
(53-7D-3)
20B. 1,2-Dichluro-
benzene(95-50-1)
X
218. 1,3-Dkchtoro-
benzene(541-73-1)
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2. MARK'X'
3. EFFLUENT
4. UNITS
S. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
b.a.
MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifa adable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavarlable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (eonGnued)
22B. 1,4-Dichloro-
benzene (106-46-7)
x
23B. 3,3-Dichloro-
benzidine (91-94-1)
X
24B. Diethyl
Phthalate (84-66-2)
X
25B. Dimethyl
Phthalate
X
(131 -11-3)
268. DiN-Butyl
Phthalate (84-74-2)
x
27B. 2,4-Dinitro-
toluene (121-14-2)
X
288. 2,6-Dinitro-
toluene (606-20-2)
X
29B. Di-N-Octyl
Phthalate (117-84-0)
X
308. 1,2-Diphenyl-
hydrazine (as Azo-
benzene)(122-66-7)
X
31B. Fluoranlhene
x
(206-44-0)
32B. Fluorene
(86-73-7)
X
3313. Hexachloro-
benzene (118-74-1)
X
34B. Hexachloro-
buladiene (87-60-3)
35B. Hexachloro-
_
cyclopentadiene
X
(77-47-4)
369 Hexachloro-
elhane (67-72-1)
X
37B.Indeno
(1,2,3-cd) Pyrene
(193-39-5)
X
_
38B.Isophorone
(78-59-1)
x
39B. Naphthalene
(91-20-3)
408. Nitrobenzene
(98-95-3)
X
41 B. N-Nilro-
sodimelhylamine
(62-75-9)
X
42B. N-Nitrosodi-
N-Propylamine
(621-64-7)
X
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG.
a. LONGTERM
AND.
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifovadable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —BASE/NEUTRAL COMPOUNDS (conlinued)
438. N-Nitro- '
sodiphenylamine
X
'
(86-30-6)
-
44B.Phenanthrene
(85-01-8)
45B.Pyrene
(129-00-0)
X
46B. 1,2,4-Tri-
-
chlorobenzene
-
(120-82-1)
g
GC/MS FRACTION — PESTICIDES
1 P. Alddn
(309-00-2)
X
2P. a-BHC
X
(319-84-6)
3P. p-BHC
(319-85-7)
X
4P. y-BHC
(58-89-9)
X
5P. b-BHC
(319-86-8)
X
6P. Chlordane
(57-74-9)
7P. 4,4'-DDT
X
(50-29-3)
8P. 4,4'-DDE
(72-55-9)
X
9P.4,4'-DDD
(72-54-8)
X
lop, Dieldrin
(60-57-1)
X
lip. a-Enosulfan
(115-29-7)
X
12P. p-Endosulfan
(115-29-7)
X
13P. Endosulfan
Sulfate
X
-
(1931-07-8)
.
14P.Endrin
(72-20-8)
X
15P. Endrin
Aldehyde
-
(7421-93A)
X
16P. Heptachlor
(76-44-8)
X
PAGE V-8 CONTINUE ON PAGE V-9

—]
CONTINUED FROM PAGE V-8 I
EPA I.D. NUMBER (copy from Item ! ofForm !) OUTFACE NUMBER
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
C. LONG TERM AVRG.
a. LONGTERM
AND
.
rR
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1J
(1)
(1)
(1)
(ifavailable)
IRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —PESTICIDES (continued)
17P. Heptachlor
Epoxide
X
(1024-57-3)
18P. PCB-1242
(53469-21-9)
X
19P. PCB-1254
(11097-69-1)
X
20P. PCB-1221
(11104-28-2)
x
21P. PCB-1232
(11141-16-5)
X
22P. PCB-1248
(12672-29-6)
X
23P. PCB-1260
(11096-82-5)
X
24P. PCB-1016
X
(12674-11-2)
25P.Toxaphene
(8001-35-2)
X
EPA Form 3510-2C (8-90) PAGE V-9

TAB F
TOPOGRAPHIC MAP
FORM I
SECTION XI

~0l { ll
I to Brushy Creek
.�
j . r
SL
• �. �'` _ rye `i-�.� /`�5{' 1 ()!.'-!j L. rst .,';�'`
t/J� s'�i�w I •`` ii • �rr�F '�44 ,�°`•' � � �1' � � � � ; r.= • r, p� r4:
Wash b uy'n i
t -�
' s�J Substation
13
..•�f � �-? ." � ' • G'— -� ,� � f � l,i `K�,,,,a-s 3 Y s Y i-�r Vr'T � t1 � .�'j
u(
z3
least' i (
O
LL 002 to Overflow Branch
k
f
_ Latitude. 35'1 g°27°'
- Longitude: 81 *37° r0B9
i -,� _1 i .t--•" _ e f J BlSttlr', -.'�T•r.��—� `'
SCALE: 1: 24000
1 1 /2 0 1 MILE
1000 0 2000 4000 6000 8000 FEET
PPG INDUSTRIES FIBER PRODUCTS, INC. FIGURE 1
N SHELBY, NORTH CAROLINA OUTFALL LOCATION MAP
ARA
REFERENCE: ENVIRONMENTAL® INC
BASE MAPS TAKEN FROM NATIONAL GEOGRAPHIC AL.
SEAMLESS USGS TOPOGRAPHIC MAPS ON CD-ROM AEI PROJECT No. N259-01
SOFTWARE. TOPO CURRENT AS OF 2001_

TAB G
'Is

�aceAnalXical
/ vmwpacelabs.corn
r
i
October 31, 2007
Mr. Richard Young
PPG Industries
940 Washburn Switch Road
Shelby, NC 28150
RE: Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
Dear Mr. Young:
Enclosed are the analytical results for sample(s) received by the laboratory on October 24, 2007.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report. .
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Annette Scott
annette.scott@ pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
t1CYejact
[phone]
Page 1 of 14

I ,.,�ceAnalytical
�' www.pacelabs.com
.i
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
CERTIFICATIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
Florida/NELAP Certification Number: E87627
North Carolina Field Services Certification Number: 5342
Kansas Certification Number: E-10364
South Carolina Certification Number: 990060001
Louisiana/LELAP Certification Number. 04034
South Carolina Bioassay Certification Number: 990060003
North Carolina Drinking Water Certification Number: 37706
Tennessee Certification Number: 04010
North Carolina Wastewater Certification Number:.12
Virginia Certification Number: 00213
Asheville Certification IDs
Florida/NELAP Certification Number: E87648
Pennsylvania Certification Number: 68-03578
Louisiana/LELAP Certification Number: 03095
South Carolina Certification Number: 99030001
New Jersey Certification Number: NC011
South Carolina Bioassay Certification Number: 99030002
North Carolina Drinking Water Certification Number: 37712•
Tennessee Certification Number: 2980
North Carolina Wastewater Certification Number: 40
Virginia Certification Number: 00072
North Carolina Bioassay Certification Number: 9
Eden Certification IDs
North Carolina Drinking Water Certification Number: 37738
North Carolina Wastewater Certification Number:-633
Virginia Drinking Water Certification Number: 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
nelact
Page 2 of 14

aceAnalXical o
www.pacelebs.com
I
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersvlile, NC 28078
[phone]
Analytes
Lab ID Sample ID Method
Reported
Laboratory
926417001 002 EPA 350.1
1
PASI-A
EPA 624
35
PASI-C
EPA 625
7
PASI-C
SM 2540D
1
PASI-A
SM 5210E
1
PASI-A
SM 5220D
1
PASI-A
SM 5310B
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 14

aceAnalytical
�r mw.pacelabs.com
t
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:. PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
Sample: 002 Lab ID: 926417001 Collected: 10/24/07 08:32 Received: 10/24/07 13:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 NISSV Analytical Method: EPA 625 Preparation Method: EPA 625
bis(2-Chloroethyl) ether
ND ug/L
5.0
1
10/30/07 00:00
10/31/07 13:52 111-44-4
Nitrobenzene-d5 (S)
86 %
10-120
1
10/30/07 00:00
10/31/07 13:52 4165-60-0
2-Fluorobiphenyl (S)
83 %
15-120
1
10/3.0107 00:00
10/31/07 13:52 321-60-8
Terphenyl-d14 (S)
87 %
11-131
1
10/30/07 00:00
10/31/07 13:52 1718-51-0
Phenol-d6 (S)
34 %
10-120
1
10/30/07 00:00
10/31/07 13:52 13127-88-3
2-Fluorophenol (S)
48 % "
10-120
1.
10/30/07 00:00
10/31/07 13:52 367-12-4
2,4,6-Tribromophenol (S)
88. %
10-137
1
10/30/07 00:00
10/31/07 13:52 118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
ND ug/L
100
1
.10131107 09:33 107-02-8
Acrylonitrile
ND ug/L
100
1
10/31/07 09:33 107-13-1
Benzene
ND ug/L
5.0
1
10/31/07 09:33 7143-2
Bromodichloromethane
ND ug/L
15.0
1
10/31/07 09:33 75-27-4
Bromoform .
ND ug/L
5.0
1
10/31/07 09:33 75-25-2
Bromomethane
ND ug/L
10.0
1
10/31/07 09:33 74-83-9
Carbon tetrachloride
ND ug/L
5.0
1
10/31/07 09:33 56-23-5
Chlorobenzene
ND ug/L•
5.0
1
10/31/07 09:33 108-90-7
Chloroethane
ND ug/L
10.0
1
10/31/07 09:33 75-00-3
?-Chioroethylvinyl ether
ND ug/L
10.0
1
10/31/07 09:33 110-75-8
;hloroform
ND ug/L
5.0
1
10/31/07 09:33 67-66-3
Chloromethane
ND ug/L
5.0
1
10/31/07 09:33 74-87-3
Dibromochloromethane
ND ug/L
5.0
1
10/31/07 09:33 12448-1
Dichlorodifluoromethane
ND ug/L
5.0
1
10/31/07 09:33 75-71-8
1, 1 -Dichloro ethane
ND ug/L
5.0
1
10/31/07 09:33 75-34-3
1,2-Dichloroethane
ND ug/L
5.0
1
10/31/07 09:33 107-06-2
1,1-Dichloroethene
ND ug/L
5.0
1
10/31/07 09:33 75-35-4
trans-1,2-Dichloroethene
ND ug/L
5.0
1
10/31/07 09:33 156-60-5
1,2-Dichloropropane
ND ug/L
5.0
1
10/31/07 09:33 78-87-5
cis-1,3-Dichloropropene
ND ug/L
5.0
1
10/31/07 09:33 10061-01-5
trans-1,3-Dichloropropene
ND ug/L
5.0
1
10/31/07 09:33 10061-02-6
Ethylbenzene
ND ug/L
5.0
1
10/31/07 09:33 100-41-4
Methylene Chloride
ND ug/L
5.0
1
10/31/07 09:33 75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L
5.0
1
10/31/07 09:33 79-34-5
.Tetrachloroethene
ND ug/L
5.0
1
10/31/07 09:33 127-18-4
Toluene
ND ug/L
5.0
1
10/31/07 09:33 108-88-3
1,1,1-Trichloroethane
ND ug/L
5.0
1
10/31/07 09:33 71-55-6
1,1,2-Trichloroethane
ND ug/L
5.0
1
10/31/07 09:33 79-00-5
Trichloroethene
ND ug/L
5.0
1
10/31/07 09:33 79-01-6
Trichlorofluoromethane
ND ug/L
10.0
1
10/31/07 09:33 75-69-4
Vinyl chloride
ND ug/L
5.0
1
10/31/07 09:33 75-01-4
Dibromofluoromethane (S)
99 %
88-113.
1
10/31/07 09:33 1868-53-7
4-Bromofluorobenzene (S)
105 %
86-1.11
1
10/31/07 09:33 460-00-4
Toluene -dB (S)
94 %
92-105
1
10/31/07 09:33 2037-26-5
1,2-Dichloroethane-d4(S)
124 %
70-130
1
10/31/07 09:33 17060-07-0
)ate: 10/31/2007 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
a
Page 4 of 14

p n m Pace Analytical Services, Inc. Pace Analytical Services, Inc.
- aceAl lalXicalf 2225 Riverside Dr. 9800 Kincey Ave. Sufle 100
1 mwpacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: PERMIT RENEWAL OUTFALL 002
Pace Project -No.: 926417
Sample: 002
Lab ID: 92641.7001 Collected: 10/24/07 08:32
Received: 10124/07 13:02 Matrix: Water
Parameters
. Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
7.8 mg/L
1.8
1
10/25/07 21:31
5210B BOD, Low Level
Analytical Method: SM 5210B
BOD, 5 day.
ND mg/L
2.0
1
10/25/0716:00 10/30/07 16:45
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
0.13'mg/L
0.10
1
10/26/07 09:46 7764-41-7
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg/L
25.0
1
10/27/07 14:00
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
4.1 mg/L
1.0
1
10/27/07 12:13 7440-44-0
)ate: 10/31/2007 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, .
without the written consent of Pace Analytical Services, Inc..
Page 5 of 14

/..,., aceAnalXical
"W.pacefabs.com
1
t
t
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
QC Batch: WET/1859 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, Low Level
Associated Lab Samples: 926417001
METHOD BLANK: 32596
Associated Lab Samples: 926417001
Blank Reporting
Parameter Units Result Limit
BOD, 5 day mg/L ND 2.0
LABORATORY CONTROL SAMPLE: 32597
Parameter Units
BOD, 5 day mg/L
SAMPLE DUPLICATE: 32598
Parameter Units
BOD, 5 day mg/L
Spike LCS L
Conc. Result . %
198 182
926424001 Dup
Result Result
119 119
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
%. Rec
Limits Qualifiers
92 84-115
RPD Qualifiers
0
)ate: 10/31/2007 03:13 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
neiac.
Page 6 of 14

. aceAnalytica!
vmw.pacelabs.00m
r
i
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
. [phone]
QUALITY CONTROL DATA
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
QC Batch: WET/1868 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 926417001
METHOD BLANK: 32737
Associated Lab Samples: 926417001
Blank Reporting
Parameter Units Result 'Limit Qualifiers
Total Suspended Solids mg/L ND 1.0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 32738
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 254 102 80-120
SAMPLE DUPLICATE: 32739
925839007 Dup
Parameter Units 'Result Result RPD Qualifiers
Total Suspended Solids mg/L 11.0 12.0 9
)ate: 10/31/2007 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, adit
Page 7 of 14 ,

V Pace Analytical Services, Inc. Pace Analytical Services, Inc.
i7 aceAI IalXicaIs 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
� wwtivpacelebs.com
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
r
QUALITY CONTROL DATA
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
QC Batch: WETA/1458
Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1
Analysis Description: 350.1 Ammonia
Associated Lab Samples: 926417001
METHOD BLANK: 32751
Associated Lab Samples: 926417001
Blank Reporting
Parameter
Units
Result Limit Qualifiers
Nitrogen, Ammonia
mg/L
ND 0.10
LABORATORY CONTROL SAMPLE:
32752
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
Qualifiers
Nitrogen, Ammonia
mg/L
5 5.5 110
90-110
MATRIX SPIKE SAMPLE:
32753
926306001 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Nitrogen, Ammonia
mg/L
2.5 5 8.6
123
75-125
SAMPLE DUPLICATE: 32754
926397001 Dup
Parameter
Units
Result Result RPD
Qualifiers
Nitrogen, Ammonia
mg/L
0.39 . 0.38
2
Date: 10/31/2007 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
iw�ICLCl:
Page 8 of 14

aceAnaljtical
f . www.pacelabs.com.
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite100
Huntersville, NC 28078
(704)B75-9092
QC Batch: WETA/1473
Analysis Method:
SM 5220D
QC Batch Method: SM 5220D
Analysis Description:
5220D COD
Associated Lab Samples: 926417001
METHOD BLANK: 33370
Associated.Lab Samples: 926417001
Blank Reporting
Parameter Units
Result Limit
Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
LABORATORY CONTROL SAMPLE: 33371
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750 758
101 90-110
MATRIX SPIKE SAMPLE: 33372
926373001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 1540 1500 3150 107 75-125
SAMPLE DUPLICATE: 33373
926417001 Dup
Parameter Units Result Result RPD Qualifiers
Chemical Oxygen Demand mg/L ND ND 0
)ate: 10/31/2007 03:13 PM REPORT OF LABORATORY ANALYSIS Page 9 of 14
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,4o ,x mc�uge 4 '
1e�$c;

FaceAnalytical
www.pacelabs.com
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
QC Batch: WETA/1474
QC Batch Method: SM 5310B
Associated Lab Samples: 926417001
METHOD BLANK: 33374
Associated Lab Samples: 926417001
Parameter Units
Total Organic Carbon mg/L
LABORATORY CONTROL SAMPLE: 33375
Parameter Units
Total Organic Carbon mg/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5310B
Analysis Description: 5310E TOC
Blank Reporting
Result Limit Qualifiers
ND 1.0 -
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec . Limits Qualifiers
10 9.8 98 90-110
MATRIX SPIKE SAMPLE: 33376
.926406005 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 4.6 10 14.6 100 75-125
SAMPLE DUPLICATE: 33377
Parameter
Total Organic Carbon
Date: 10/3112007 03:13 PM
926406006 Dup
Units Result Result
mg/L 42.5 43.0
RPD Qualifiers
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1�Iac
Page 10 of 14

1-,PjceAna1Xica1
/ w wpacelabs.com
1
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/1666 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 926417001
METHOD BLANK: 34012
Associated Lab Samples:
Parameter
926417001.
Units
Blank
Result
Reporting
Limit Qualifiers
1,1,1-Trichloroethane
ug/L
ND
5.0
1,1,2,2-Tetrachloroethane
ug/L
ND
5.0
1,1,2-Trichloroethane
ug/L
ND
5.0
1,1-Dichloroethane
ug/L
ND
5.0
1,1-Dichloroethene
ug/L
ND
5.0
1,2-Dichloroethane
ug/L
ND
5.0
1,2-Dichloropropane
ug/L
ND
5.0
2-Chloroethylvinyl ether
ug/L
ND
10.0
Acrolein
ug/L
ND
100
Acrylonitrile
ug/L
ND
100
Benzene
ug/L
ND
5.0
Bromodichloromethane
ug/L
ND
5.0
Bromoform
ug/L
ND
5.0
Bromomethane
ug/L
ND
10.0
Carbon tetrachloride
ug/L
ND
5.0
Chlorobenzene
ug/L
ND
5.0
Chloroethane
ug/L
ND
10.0
Chloroform
ug/L
ND
5.0
Chloromethane
ug/L
ND
5.0
cis-1,3-Dichloropropene
ug/L
ND
5.0
Dibromochloromethane
ug/L
ND
5.0
Dichlorodifluoromethane
ug/L
ND
5.0
Ethylbenzene
ug/L
ND
5.0
Methylene Chloride
ug/L
ND
5.0
Tetrachloroethene
ug/L
ND
5.0
Toluene
ug/L
ND
5.0
trans-1,2-Dichloroethene
ug/L
ND
5.0
trans-1,3-Dichloropropene
ug/L
ND
5.0
Trichloroethene
ug/L
ND
5.0
Trichlorofluoromethane
ug/L
ND
10.0
Vinyl chloride
ug/L
ND
5.0
1,2-Dichloroethane-d4 (S)
%
119
70-130
4-Bromofluorobenzene (S)
%
104
86-111
Dibromofluoromethane (S)
%
94
88-113
Toluene-d8 (S)
%
96
92-105
Pace Analytical Services, Inc.
98DO Kincey Ave. Suite 100
Huntersville, NC 2807E
(704)B75-9092
LABORATORY CONTROL SAMPLE: 34013
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L ( 20 23.1 116 52-162
1,1,2,2-Tetrachloroethane ug/L 20 18.5 93 46-157
Date: 10/31/2007 03:13 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc..
Page 11 of 14

j e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aC�AI l/7 alXica' 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
LABORATORY CONTROL SAMPLE: 34013
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,2-Trichloroethane
ug/L
20
20.0
100
52-150
1,1-Dichloroethane
ug/L
20
18.2
91
59-155
1,1-Dichloroethene
ug/L
20
24.4
.122
1-234
1,2-Dichloroethane
ug/L
20
23.0
115
49-155
1,2-Dichloropropane
ug/L
20
20.1
100
1-210
2-Chloroethylvinyl ether
ug/L
40
43.5
109
1-305
Acrolein
ug/L
100
ND .
58
15-152
Acrylonitrile
ug/L
100
ND
62
75-132 L2
Benzene
ug/L
20
19.7
99
37-151
Bromodichloromethane
ug/L -
20
22.9
115
35-155
Bromoform
ug/L
20
21.8
109
45-169
Bromomethane
ug/L
20
18.1
91
1-242
Carbon tetrachloride
ug/L
20
27.7
138
70-140
Chlorobenzene
ug/L
20
22.2
111
37-160
Chloroethane
ug/L
20
16.7
83
14-230
Chloroform
ug/L
20
21.3
107
51-138
Chloromethane
ug/L
20
17.5
87
1-273
cis-1,3-Dichloropropene
ug/L
20
20.2
101
1-227
Dibromochloromethane
ug/L
20
22.6
113
53-149
Dichlorodifluoromethane
ug/L
20
35.4
177
70-130 L3
Ethylbenzene
ug/L
20
22.4
112
37-162
Methylene Chloride
ug/L
20
17.8
89
1-221
Tetrachloroethene
ug/L
20
25.2
126
64-148
Toluene
ug/L
20
20.6
103
47-150
trans-1,2-Dichloroethene
ug/L
20
19.4
97
54-156
trans-1,3-Dichloropropene
ug/L
20
20.2
101
17-183
Trichloroethene
ug/L
20
23.0
115
71-157
Trichlorofluoromethane
ug/L
20
28.5
142
17-181
Vinyl chloride
ug/L
20
22.2
111
1-251
1,2-Dichloroethane-d4 (S)
%
117
70-130
4-Bromofluorobenzene (S)
%
105
86-111
Dibromofluoromethane (S)
%
95
88-113
Toluene-d8 (S)
%
96
92-105
Date: 10/31/2007 03:13 PM REPORT OF LABORATORY ANALYSIS Page 12 of 14
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ela,,��` ,
I...I

Pace Analytical
Services, Inc.
Pace Analytical Services, Inc.
►7nr /
l lRlft✓'a'
2225 Riverside Dr.
9800 KinceyAve. Suite 100
'!zA
www.pacelabs.com
Asheville, NC 28804
Huntersville, NC 2807E
[phone]
[phone]
QUALITY CONTROL DATA
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
QC Batch: OEXT/1608
Analysis Method: EPA 625
QC Batch Method: EPA 625
Analysis Description' 625 MSS
Associated Lab Samples: 926417001
METHOD BLANK: 34057
Associated Lab Samples: 926417001
Blank Reporting
Parameter
Units
Result Limit Qualifiers
bis(2-Chloroethyl) ether
ug(L
ND 5.0
2;4,6-Tribromophenol (S)
%
47 10-137
2-Fluorobiphenyl (S)
%
44 15-120
2-Fluorophenol (S)
%
26 10-120
Nitrobenzene-d5 (S)
% -..
46 10-120
Phenol-d6 (S) "
%
17 10-120
Terpheny1-d14 (S)
%
48 11-131
LABORATORY CONTROL SAMPLE:
34058
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
Qualifiers
bis(2-Chloroethyl) ether
ug/L
50 26.0
52 12-158
2,4,6-Tribromophenol (S)
%
63 10-137
2-Fluorobiphenyl (S)
%
62 .. 15-120
2-Fluorophenol (S)
%
36 10-120
Nitrobenzene-d5 (S)
%
60 10-120 ,
Phenol-d6 (S)
%
26 10-120
TerphenyIA14 (S)
%.
65 11-131
Date: 10/31/2007 03:13 PM REPORT OF LABORATORY ANALYSIS Page 13 of 14
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

)n �7 / Pace Analytical Services, Inc. Pace Analytical Services, Inc.
A(lalXic'aI 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwavpacetabs.ccm Asheville, NC 26804 Huntersville, NC 28078
�
[phone] (704)B75-9092
I
QUALIFIERS
Project: PERMIT RENEWAL OUTFALL 002
Pace Project No.: 926417
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. .
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
Date: 10/31/2007 03:13 PM REPORT OF LABORATORY ANALYSIS Page 14 of 14
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
h6h,

Analytical Results
Pace Analytical For: 926418
9800 Kincey Suite 1.00
Huntersville NC 28078
Entered 10/25/2007
Reported: 10/29/2007
Sample Remark
Sample ID
Parameter
Cust ID
Result
Units
Method
Date Analyzed
Analyst
071025-3
MBAS
Eff 001
0.36
mg/L
SM5540C
10/25/07
MD .
Respectfully submitted,
Dena Myers
:ert #440,
--W Cert #37755,
EPA NCO0909
P.O. Box 228 a Statesville, North Carolina 28687. 704/872/4697

e• g Jv - Pace Analytical Services, Ind. Pace Analytical Services, Inc.
AG AnaIXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wawpacelahs.wm Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
October 31, 2007
Mr. Richard Young
PPG Industries
940 Washburn Switch Road
Shelby, NC 28150
RE: Project: PERMIT RENEWAL OUTFALL 001
Pace. Project No.: 926418
Dear Mr. Young:
Enclosed are the analytical results for sample(s) received by the laboratory on October 24, 2007.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Annette Scott
[e-mail]
Project Manager
Enclosures
° REPORT OF LABORATORY ANALYSIS Page 1 of 13
This report shall not be -reproduced, except in full,
wlihout the written consent of Pace Analytical Services, Inc..
,nel

F Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalj4ical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
WwMrpacela6s.com
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
f
CERTIFICATIONS
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418 .
Charlotte Certification IDs
Florida/NELAP Certification Number: E87627
North Carolina Field Services Certification Number: 5342
Kansas Certification Number: E-10364
South Carolina Certification Number: 99006000/
Louisiana/LELAP Certification Number: 04034
South Carolina. Bioassay Certification Number: 990060003
North Carolina. Drinking Water Certification Number: 37706
Tennessee Certification Number: 04010.
North Carolina Wastewater Certification Number: 12
Virginia Certification Number: 00213
Asheville Certification IDs
Florida/NELAP Certification Number: E87648
Pennsylvania Certification Number: 68-03578 -
Louisiana/LELAP Certification Number., 03095
South Carolina Certification Number: 99030001
New Jersey Certification Number: NC011
South Carolina Bioassay Certification Number: 99030002
North Carolina Drinking Water Certification Number: 37712
Tennessee Certification Number: 2980
North Carolina Wastewater Certification Number: 40
Virginia Certification Number: 00072
North Carolina Bioassay Certification Number: 9
Eden Certification IDs
North Carolina Drinking Water Certification Number: 37738
North Carolina Wastewater Certification Number: 633
Virginia Drinking Water Certification Number: 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
i !, . el1C
Page 2 of 13

Z!zAnalXica1c.
www.paceobs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
Pace Analytical Services, Inc.
9800 Kin cey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method Reported Laboratory
926418001 EFFLUENT 001 ASTM D516-90,02 1 PASI-A
EPA 200.7 7 PASI-A
EPA 624 36 PASI-C
EPA 625 9 PASI-C
SM 5220D 1 PASI-A
SM 5310B 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ac
Page 3 of 13

J% a Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/ , aceAnalytkal 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
ftwpacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
I
ANALYTICAL RESULTS
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
Sample: EFFLUENT 001
Lab- ID: 926418001
Collected: 10/24/07 08:00
Received: 10/24/07 13:02 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
Aluminum
ND ug/L
100
1
10/26/07 10:00
10/29/07 02:15 7429-90-5
Arsenic
ND ug/L
5.0
1
10/26/07 10:00
10/29/07 02:15 7440-38-2
Boron
308 -ug/L
10.0
1
10/26/07 10:00
10/29/07 02:15 7440-42-8
Chromium
ND ug/L
5.0
1
10/26/07 10:00
10/29/07 02:15 7440-47-3
Iron
ND ug/L
50.0
1
10/26/07 10:00
10/29/07 02:15 7439-89-6
Magnesium
2100 ug/L
100
1
10/26/07 10:00
10/29/07 02:15 7439-95-4
Silver
ND ug/L
5.0
1
10/26/07 10:00
10/29/07 02:15 7440-22-4
625 MSSV
Analytical Method: EPA 625
Preparation Method: EPA 625
bis(2-Chloroethyl) ether
ND ug/L
5.2
1
10/29/07 00:00
10/30/07 23:35 111744-4
Di-n-butylphthalate
ND ug/L
5.2
1
10/29/07 00:00
10/30/07 23:35 84-74-2
bis(2-Ethylhexyl)phthaIate
47.5 ug/L
5.2
1
10/29/07 00:00
10/30/07 23:35 117-81-7
Nitrobenzene-d5 (S)
65 %
10-120
1
10/29/07 00:00
10/30/07 23:35 4165-60-0
2-Fluorobiphenyl (S)
69 %
15-120
1
10/29/07 00:00
10/30/07 23:35 321-60-8
Terphenyl-d14 (S)
97 %
11-131
1
10/29/07 moo
10/30/07 23:35 1718-51-0
Phenol-d6. (S)
31 %
10-120
1
10/29/07 00:00
10/30/07 23:35 13127-88-3
2-Fluorophenol (S)
36 %
10-120
1
10/29/07 00:00
10/30/07 23:35 367-12-4
2,4,6-Tribromophenol (S)
88 %
10-137
1
10/29/07 00:00
10/30/07 23:35 118-79-6
524 Volatile Organics
Analytical Method: EPA 624
Acrolein
ND ug/L
100
1
10/31/07 09:50 107-02-8
Acrylonitrile
ND ug/L
100
1
10/31/07 09:50 107-13-1
Benzene
ND ug/L
5.0
1
10/31/07 09:50 71-43-2
Bromodichloromethane
ND ug/L
5.0
1
10/31/07 09:50 75-27-4
Bromoform
ND ug/L
5.0
1
10/31/07 09:50 75-25-2
Bromomethane
ND ug/L
10.0
1
10/31/07 09:50 74-83-9
Carbon tetrachloride
ND ug/L
5.0
1
10/31/07 09:50 56-23-5
Chlorobenzene
ND ug/L
5.0
1
10/31/07 09:50 108-90-7
Chloroethane
ND ug/L
10.0
1
10/31/07 09:50 75-00-3
2-Chloroethylvinyl ether
ND ug/L
10.0
1
10/31/07 09:50 110-75-8
Chloroform
ND ug/L
5.0
1
10/31/07 09:50 67-66-3
Chloromethane
ND ug/L
5.0
1
10/31/07 09:50 74-87-3
Dibromochloromethane
ND ug/L
5.0
1
10/31/07 09:50 124-48-1
Dichlorodifluoromethane
ND ug/L
5.0
1
10/31/07 09:50 75-71-8
1,1-Dichloroethane
ND ug/L
5.0
1
10/31/07 09:50 75-34-3
1,2-Dichloroethane
ND ug/L
5.0
1
10131/0709:50 107-06-2
1,1-Dichloroethene
ND ug/L
5.0
1
10/31/07 09:50 75-35-4
cis-1,2-Dichloroethene
ND ug/L
5.0
1
10/31/07 09:50 156-59-2
trans-1,2-Dichloroethene
ND ug/L
5.0
1
10/31/07 09:50 156-60-5
1,2-Dichloropropane
ND ug/L
5.0
1
10/31/07 09:50 78-87-5
cis- 1,3-Dichloropropene
ND ug/L
5.0
1
10/31/07 09:50 10061-01-5
trans- l,3-Dichloropropene
ND ug/L
5.0
1
10/31/07 09:50 10061-02-6
Ethylbenzene
ND ug/L
5.0
1
10/31/07 09:50 100-41-4
Methylene Chloride
ND ug/L
5.0
1
10/31/07 09:50 75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L
5.0
1
10/31/07 09:50 79-34-5
Tetrachloroethene
ND ug/L
5.0
1
10/31/07 09:50 127-18-4
date: 10/31/2007 03:17 PM REPORT OF LABORATORY ANALYSIS Page 4 of 13
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
bela.C,

�1
,,�p J�j� g. Pace Analytical Services, Inc.
G A►t al ICarJ2225 Riverside Dr.
tmtit!paC `alabs.com Asheville, NC 28804
i [phone]
ANALYTICAL RESULTS
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: EFFLUENT 001
Parameters
Lab ID: 926418001 Collected: 10/24/07 08:00
Results Units Report Limit DF
Received: 10/24/07 13:02 Matrix: Water
Prepared Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624
Toluene
ND ug/L
5.0
1
10/31/07 09:50 108-88-3
1,1,1-Trichloroethane
ND ug/L
5.0
1
10/31/07 09:50 71-55-6
1,1,2-Trichloroethane
ND ug/L
5.0
1
10/31/07 09:50 79-00-5
Trichloroethene.
ND ug/L
5.0
1 .
- 10/31/07 09:50 79-01-6
Trichlorofluoromethane
ND ug/L
10.0
1
10/31/07 09:50 75-69-4
Vinyl chloride
ND. ug/L
5.0
1
10/31/07 09:50 75-01-4
Dibromofluoromethane (S)
97 %
88-113
1
10/31/07 09:50 1868-53-7
4-BrOMDflUorobenzene (S).
105 %
86-111
1
10/31107 09:50 460-00-4
Toluene-d8 (S)
97 %
92-105
1
10/31/07 09:50 2037-26-5
1,2-Dichloroethane-d4(S)
123 %•
70-130
1
10131/0709:50 17060-07-0
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg/L
25.0
1
10/27/07 14:00
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
4.9 mg/L
1.0
1
10/27/07 12:13 1440-44-0
ASTM D516-9002 Sulfate Water
Analytical Method: ASTM D516-90,02
Sulfate
8.7 mg/L
5.0
1
10/27/0713:00 14808-79-8
')ate: 10/31/2007 03:17 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical, Services, Inc..
.,1elac
Page 5 of 13

/ s
al✓eAnalXical
Pace Analytical Services, Inc.
2225 Riverside Dr.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
/ wnwpacela6s.com
Asheville. NC 28804
Huntersviile, NC 28078
1
[phone]
[phone]
QUALITY CONTROL DATA
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
QC Batch: MPRP/1354
Analysis Method:
EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 926418001
METHOD BLANK: 32208
Associated Lab Samples: 926418001
Blank Reporting
Parameter
Units
Result
Limit Qualifiers
Aluminum
ug/L
ND
100
Arsenic
ug/L
ND
5.0
Chromium
ug/L
ND
5.0
Iron
ug/L
ND
50.0
Magnesium
ug/L
ND
100
Silver
ug/L
ND
5.0
LABORATORY CONTROL SAMPLE:
32209
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result % Rec Limits
Qualifiers
'Aluminum
ug/L
5000
5340 107 85-115
Arsenic
ug/L
500
563 113 85-115
Chromium
ug/L
500
567 113 85-115
Iron
ug/L
5000
5570 111 85-115
Magnesium
ug/L
5000
5740 115 85-115
Silver
ug/L
250
281 112 85-115
MATRIX SPIKE SAMPLE:
32210
926073001
Spike MS MS
% Rec
Parameter
Units
Result
Conc. Result % Rec
Limits Qualifiers
Aluminum
ug/L
ND
5000 4450'
89
70-130
Arsenic
ug/L
ND
500 .478
95
70-130
Chromium.
ug/L
ND
500 468
93
70-130
Iron
ug/L
ND
5000 4660
93
70-130
Magnesium
ug/L
1870
5000 6610
95
70-130
Silver
ug/L
ND
250 249 100
70-130
SAMPLE DUPLICATE: 32211
926073002
Dup'
Parameter
Units
Result
Result RPD Qualifiers
Aluminum
ug/L
ND
67.6J 6
Arsenic
ug/L
8.2
6.5 23 R2
Chromium
ug/L
ND
1.3J 2
Iron
ug/L
107
113 5
Magnesium
ug/L
1980
2060 4
Silver
ug/L
ND
.15J 35
Date: 10/81/2007 03:17 PM REPORT OF LABORATORY ANALYSIS Page 6 of 13
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,

�5aceAnalXicalo
/ www.pacelabs.com
i
f
Project: . PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/1470 Analysis Method: ASTM D516-90,02
QC Batch Method: ASTM D516-90,02 Analysis Description: ASTM D516-9002 Sulfate Water
Associated Lab Samples: 926418001
METHOD BLANK: 33238
Associated Lab Samples: 926418001
Blank Reporting
Parameter Units Result Limit Qualifiers
Sulfate mg/L ND 5.0
LABORATORY CONTROL SAMPLE: 33239
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS
LCS
% Rec .
Parameter Units
Conc. Result
% Rec
Limits .
Qualifiers
Sulfate mg/L
20 19.1
96
90-110
MATRIX SPIKE SAMPLE: 33240
926418001 Spike
MS
MS
% Rec
Parameter Units
Result Conc.
Result
% Rec
Limits Qualifiers
Sulfate mg/L
8.7 20
31.0
112
75-125
SAMPLE DUPLICATE: 33241
Parameter Units -
Sulfate mg/L
-)ate: 10/31/2007 03:17 PM -
926024001 Dup
Result Result RPD Qualifiers
101 107 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 13

�aceAnalgicqlo
wwwpace1a6s.com
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/1473 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 926418001
METHOD BLANK: 33370
Associated Lab Samples: 926418001
Blank Reporting
Parameter Units Result Limit Qualifiers
Chemical Oxygen Demand mg/L ND 25.0
Pace Analytical Services, Inc.
9800KinceyAve. Suite too
Huntersvllle, NC 2B07B
[phone]
LABORATORY CONTROL SAMPLE:
33371
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Chemical Oxygen Demand
mg/L
750
758
101
90-110
MATRIX SPIKE SAMPLE:
33372
926373001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
1540 1500
3150
107
75-125
SAMPLE DUPLICATE: 33373
926417001
Dup
Parameter
Units
Result
Result
RPD '
Qualifiers
Chemical Oxygen Demand
mg/L
ND
ND
0
Date: 10/31/2007 03:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
`c ,N cctl gp'ry'
Page 8 of 13

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2aceAnalXical' 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
mvw.pacelabs.cam Asheville, NC 28804 Huntersville, NC 28078
[phone] (704)B75-9092
QUALITY CONTROL DATA
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
QC Batch: WETA/1474
Analysis Method:
SM 5310B
QC Batch Method: SM 5310B
Analysis Description:
5310B TOC
Associated Lab Samples: 926418001
METHOD BLANK: 33374
Associated Lab Samples: 926418001
Blank Reporting
Parameter
Units
Result Limit
Qualifiers
Total Organic Carbon
mg/L
ND 1.0
LABORATORY CONTROL SAMPLE:
33375
Spike LCS .
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Organic Carbon
mg/L
10 9.8
98
90-110
MATRIX SPIKE SAMPLE:
33376
926406005 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Organic Carbon
mg/L
4.6 10
14.6
100
75-125
SAMPLE DUPLICATE: 33377
926406006 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Total Organic Carbon
mg/L
42.5 410
1
-)ate: 10/31/2007 03:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,,hehct
Page 9 of 13

!- ,� T. Pace Analytical Services, Inc.
// ,.,RaceAna1Xica1 v 2225 Riverside Dr.
/ www.pacelabs.com Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: OEXT/1592
Analysis Method: EPA 625
QC Batch Method: EPA 625
Analysis Description: 625 MSS
Associated Lab Samples: 926418001
METHOD BLANK: 33729
Associated Lab Samples: 926418001
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
bis(2-Chloroethyl) ether
ug/L
ND
5.0
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
Di-n-butylphthalate
ug/L
ND
5.0
2,4,6-Tribromophenol (S)
%
97
.10-137
2-Fluorobiphenyl (S)
%
74
15-120
2-Fluorophenol (S)
%
47
10-120
Nitrobenzene-d5 (S)
%
87
10-120
Phenol-d6 (S)
%
32
10-120
Terphenyl-d14 ($)
%
105
11-131
LABORATORY CONTROL SAMPLE:
33730 .
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
bis(2-Chloroethyl) ether
ug/L
50
ND
0
12-158 1g
bis(2-Ethylhexyl)phthalate
ug/L
50
ND
0
8-1581g
Di-n-butylphthalate
ug/L
50
ND
0
1-1181g
2,4,6-Tribromophenol (S)
%
80
10-137
2-Fluorobiphenyl (S)
%
'63
15-120
2-Fluorophenol (S)
%
45
10-120
Nitrobenzene-d5 (S)
%
76
10-120
Phenol-d6 (S)
%
28
10-120
Terphenyl-d14 (S)
%
99
11-131
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 33731
926418001
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
33732
MS
Result
bis(2-Chloroethyl) ether
ug/L
ND
100
100
65.1
bis(2-Ethylhexyl)phthalate
ug/L .
47.5
100
100
116
Di-n-butylphthalate
ug/L
ND
100
100
86.8
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-dl4 (S)
%
)ate: 10/31/2007 03:17 PM
MSD
MS
MSD
% Rec
Result
% Rec
% Rec
Limits
RPD Qual
62.4
65
62
12-158'
4
83.8
69
36
8-158
32 R1
84.4
87
84
1-118
3
97
79
10-137
84
83
15-120
40
39
10-120
64
51
10-120
33
30
10-120
79
59
11-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent.of Pace Analytical Services, Inc..
Page 10 of 13

aceAnalXical
r/ wwtivpscelabs.com
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/1666 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 926418001
METHOD BLANK: 34012
Associated Lab Samples:
Parameter
926418001
Units
Blank
Result
Reporting
Limit Qualifiers
1,1,1-Trichloroethane
ug/L
ND
5.0
1,1,2,2-Tetrachloroethane
ug/L
ND
5.0
1,1,2-Trichloroethane
ug/L
ND
5.0
1,1-Dichloroethane
ug/L
ND
5.0
1,1-Dichloroethene
ug/L
ND
5.0
1,2-Dichloroethane
ug/L
ND
5.0
1,2-Dichloropropane
ug/L
ND
5.0
2-Chloroethylvinyl ether
ug/L
ND
10.0.
Acrolein
ug/L
ND
100
Acrylonitrile
ug/L
ND
100
Benzene
ug/L
Nb
5.0
Bromodichloromethane
ug/L
ND
5.0
Bromoform
ug/L
ND
5.0
Bromomethane
ug/L
ND
10.0
Carbon tetrachloride
ug/L
ND
5.0
Chlorobenzene
ug/L
ND
5.0
Chloroethane
ug/L
ND
10.0
Chloroform
ug/L
ND
5.0
Chloromethane
ug/L
ND
5.0
cis-1,2-Dichloroethene
ug/L
ND
5.0
cis-1,3-Dichloropropene
ug/L
ND
5.0
Dibromochloromethane
ug/L
ND
5.0
Dichlorodifluoromethane
ug/L
ND
5.0
Ethylbenzene
ug/L
ND
5.0
Methylene Chloride
ug/L
ND
5.0
Tetrachloroethene
ug/L
ND
5.0
Toluene
ug/L
ND
5.0
trans-1,2-Dichloroethene
ug/L
ND
5.0
trans-1,3-Dichloropropene
ug/L
ND
5.0
Trichloroethene
ug/L
ND
5.0
.Trichlorofluoromethane
ug/L
ND
10.0
Vinyl chloride
ug/L
ND
5.0
1,2-Dichloroethane-d4 (S)
%
119
70-130
4-Bromofluorobenzene (S)
%
104
86-111
Dibromocuoromethane (S)
%
94
88-113
Toluene-d8 (S)
%
96
92-105
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 34013
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 23.1 116 52-162
-)ate: 10/31/2007 03:17 PM REPORT OF LABORATORY ANALYSIS Page 11 of 13
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
o ,._.cci go,M1

/ laceAnafXicale-
mwpacelebs.ccm
1
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
LABORATORY CONTROL SAMPLE: 34013
Parameter
1,1,2,2-Tetrachloroethane
ug/L
1,1,2-Trichloroethane
ug/L
1,1-Dichloroethane
ug/L
1,1-Dichloroethene
ug/L
1,2-Dichloroethane
ug/L
1,2-Dichloropropane
ug/L
2-Chloroethylvinyl ether
ug/L
Acrolein
ug/L
Acrylonitrile
ug/L
Benzene
ug/L
Bromodichloromethane
ug/L
Bromoform
ug/L
Bromomethane
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroethane
ug/L
Chloroform
ug/L
Chloromethane
ug/L
cis-1,2-Dichloroethene
ug/L
cis-1,3-Dichloropropene
ug/L
Dibromochloromethane
ug/L
Dichlorodifluoromethane
ug/L
Ethylbenzene
ug/L
Methylene Chloride
ug/L
Tetrachloroethene
ug/L
Toluene
ug/L
trans-1,2-Dichloroethene
ug/L
trans-1,3-Didhloropropene
ug/L
Trichloroethene
ug/L.
Trichlorofluoromethane
ug/L
Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
2010
4-Bromofluorobenzene (S)
%
Dibromocuoromethane (S)
%
Toluene-d8 (S)
%
)ate: 10/31/2007 03:17 PM
Units
Pace Analytical Services, Inc,
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
20
18.5
93
46-157
20
20.0
100
52-150
20
18.2
91
59-155
20
24.4
122
1-234
20
23.0
115
49-155
20
20.1
100
1-210
40
43.5
109
1-305
100
ND
58
15-152
100
ND
62
75-132 L2
20
19.7
99
37-151
20
22.9
115
35-155
20
21.8
109
45-169
20
18.1
.91
1-242
20
27.7
138
70-140
20
22.2
111
37-160
20
16.7
83
14-230
20 _
21.3
107
51-138
20
17.5
87,
1-273
20
19.5
97
68-146
20
20.2
101
1-227
20
22.6
113
53-149
20
35.4
177
.7D-130 L3
20
22.4
112
37-162
20
17.8
89
1-221
20
25.2
126
64-148,
20
20.6
103
47-150
20
19.4
97
54-156
20
20.2
101
17-183
20
23.0
115
71-157
20
28.5
142
17-181
20
22.2
111
1-251
117
70-130
105
86-111
95
88-113
96
92-105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. .
mP a
Page 12 of 13

j r+ I &. Pace Analytical Services, Inc.
I a"cp AnalX cal 2.225 Riverside Dr.
wwwpacelabs.eam Asheville, NC 28804
r [phone]
QUALIFIERS
Project: PERMIT RENEWAL OUTFALL 001
Pace Project No.: 926418
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS)-was below QC limits. Results for this analyte in associated
samples may be biased low.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
R1 RPD value wasoutside control limits.
R2 RPD value was outside control limits due to matrix interference
1 g Due to a lab error, the spike mix was not added to the LCS. Data was accepted based on acceptable recoveries of the
target compounds in the associated 'MS/MSD and acceptable surrogate recoveries in the associated samples.
)ate: 1,0131/2007 03:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
«oaa
riA act.
Page 13 of 13

Analytical Results
Pace Analytical For: 926418
9800 Kincey Suite 100
Huntersville NC 28078
Entered 10/25/2007
Reported: 10/29/2007
Sample Remark
Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst
071025-3 MBAS Eff-001 0.36 mg/L SM5540C 10/25/07 MD
Respectfully submitted,
Dena Myers
Cert #440,
.DW Cert #37755,
EPA NC00909
P.O. Box 228 9 Statesville, North C&olina 28687 • 704/872/4697

Michael F. Easley, Govemo
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P. E. Director
Division of Water Quality
DIVISION OF WATER QUALITY
November 23, 2005
Mr. Tim Mathis, Manufacturing Manager
PPG Industries Fiber Glass Products, Inc.
940 Washburn Road
Shelby, North Carolina 28150
Subject: NPDES Permit NC0004685
Shelby Facility
Cleveland County
Dear Mr. Mathis:
Our records indicate that NPDES Permit No. NC0004685 was issued on November 4,
2005 for the discharge of wastewater to the surface waters of the State from your facility_. The
purpose of this letter is to advise you of the importance of the Permit and the liabilities in the
event of failure to comply with the terms and conditions of the Permit. If you have not already
done so, it is suggested that you thoroughly read the Permit. Of particular importance are Pages
4and 5.
Pages 4 and 5 set forth the effluent limitations and monitoring requirements for your
discharge. Your discharge must not exceed any of the limitations set forth. The section headed
"Monitoring Requirements" describes the measurement frequencies, sample types and sampling
locations. Uponcommencement of your discharge (or operation), you must initiate the required
monitoring. The monitoring results must be entered on reporting forms furnished or approved by
this Agency. For new permits/facilities, the Division may supply an initial small stock of these
forms; however, if you fail to receive the forms, please contact this Office as quickly as possible.
The forms, including directions for their completion, and other important information are also
available at http://h2o.eiir.state.nc.us/NPDES/documents.html. It is imperative that all applicable
parts be completed, and the original and one copy be submitted as required.
Please be advised that an annual fee may be required for your facility; if so, you will
receive a statement from our Raleigh Office. It is imperative that the fee be paid in a timely
manner so as to prevent enforcement action or possible revocation of your permit.
Nofe Carolina
�turallry
N. C. Division of Water Quality, Mooresville Regional Office, 610 E. Center Ave. Suite 301, Mooresville NC 28115 [phone] Customer Service
1-877-623-6748

8
The remaining parts of the Permit set forth definitions, general conditions and special
conditions applicable to the operation of wastewater treatment facilities and/or discharge(s). The
conditions include special reporting requirements in the event of noncompliance, bypasses,
treatment unit/process failures, etc. Also addressed are requirements for a certified wastewater
treatment plant operator if you are operating wastewater treatment facilities. Any changes in
operation of wastewater treatment facilities, quantity and type of wastewater being treated or
discharged, expansions and/or upgrading of wastewater treatment facilities must be permitted or
approved by this Agency.
To maintain compliance with discharge limitations, proper operation and maintenance of
a wastewater treatment facility and the development of a process control program are essential.
For those facilities having chlorine tablet disinfection, please be advised that chlorine tablets
approved for wastewater treatment use must be used; swimming pool tablets are not approved.
Also, be advised that DWQ staff need to have access to the facility's discharge point into the
receiving stream; please maintain a path along the outfall line to facilitate that access.
Failure to comply with the terms and conditions of an NPDES Permit subjects the
Permittee to enforcement action pursuant to Section 143-215.6 of the North Carolina General
Statutes. A civil penalty of up to $25,000 per violation (and/or criminal penalties) may be
assessed for such violations. If you find at any time that you are unable to comply with the terms
and conditions of the Permit, you should contact this Office immediately. A Special Order by
Consent (SOC) may be necessary while pursuing action to obtain compliance.
As a final note, an NPDES Permit is normally issued for a five-year period. Permits are
not automatically renewed. Renewal requests must be submitted to this Agency no later than 180
days prior to expiration. Please make note of the expiration date of your Permit. This date is set
forth on Page 1 of the Permit. Also note that NPDES Permits are not automatically transferable.
If you, as the Permittee, cease to need this Permit, then you should request that the Division of
Water Quality rescind the Permit or request that DWQ reissue the Permit to another party, if
necessary.
As mentioned previously, the purpose of this letter is to advise you of the importance of
your NPDES Permit. Please read the Permit and contact this Office at 704/663-1699 in
Mooresville if you have any questions or need clarification. We look forward to providing any
assistance.
Sincerely,
J D. Rex Gleason, P.E. Surface Water Protection Regional Supervisor

Michael F. Easley
�0� W ATERQ . pa►�� Governor
O William G. Ross, Jr., Secretary
1 r NCDENR North Carolina Department of Environment and Natural Resources
�? Alan W,.--Kli'rhek; P.E.; Director
l3 _... ,
` Division':of.Water Quality
November 4, 2005
NOV 2 " 200:a
Mr. Tim Mathis, Manufacturing Manager
PPG Industries Fiber Glass Products, Inc. M
940 Washburn Road
Shelby, North Carolina 28150
Subject: Issuance of NPDES Permit
NC0004685
Shelby Facility
Cleveland County
Dear Mr. Mathis:
Division personnel have reviewed and approved your application for renewal of the subject permit.
Accordingly, we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to
the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between North Carolina and the U.S. Environmental Protection Agency dated May 9,1994 (or as
subsequently amended).
This final peanut includes following changes from the draft permit sent to you on June 1, 2004:
• In the supplement to the permit cover sheet "a chlorine contact tank' was replaced with "an
effluent holding tank Change was done because chlorine is no longer used as a disinfecting agent.
• The total lead measurement frequency was changed from 2/month to 1/month to correct an error.
• The daily maximum TSS limit was changed from 30 mg/L to 146 mg/L to correct an error.
• The pH effluent limitations language was changed to ">6.0 to 4" to be consistent with the
previous permit.
The Division has reviewed your request for a revision of the OR and Grease limit. The
request cannot be granted. Review of the OR and Grease effluent data indicates that since February
2001 when the new analytical procedure became effective only 2 violations of the Oil and Grease
limit have occurred. The vast majority of the measurements were below detection levels. In order to
change the limit, you will need to conduct a side -by -side method comparison in accordance with the
procedure described in the Section 2 of the document "Analytical Method Guidance for EPA
Method 1664A Implementation and Use (40 CFR Part 136), February 2000" and submit results to
the Division.
The Division cannot grant your request to reduce the monitoring frequency for BOD and NH, from
weeklyto 2/month. Your facility is classified as a Class III facility and the current monitoring frequency for
oxygen consuming substances for your facility reflects a reduction in the standard monitoring frequency of
3/week for Class III facilities. In addition, both BOD and NH, are major operational parameters that
N. C. Division of Water Quality 1 NPDES Unit Phone: [phone]
1617 Mail Service Center, Raleigh, NC 27699-1617 fax: [phone]
Internet: h2o.enr.state.nc.us DEN Customer Service Center 1800 623-7748 .

indicate effectiveness of treatment system. operation and should be monitored frequently to prevent
deficiencies and limit violations and assure protection of the water quality in the receiving stream
The Division is also unable to grant your request for adding the following statement to the effluent
page for Outfall 002: "Monitoring is required only when non -contact cooling water is discharged to outfall
002". The Outfall 002 is a non -contact cooling water outfall and is permitted in accordance with the general
permit for non -contact cooling water. Provisions in the General Permit for non -contact cooling water do
not allow the modification you have requested.
If anyparts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30)
days following receipt of this letter. This request must be in the form of a written petition, conforming to
Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings
(6714 Mail Service Center, Raleigh, North Carolina 27699-6714). Unless such demand is made, this
decision shall be final and binding.
Please note that this permit is not transferable except after notice to the Division. The Division
may require modification or revocation and reissuance of the permit. This permit does not affect the legal
requirements to obtain other permits which may be required by the Division of Water Quality or permits
required by the Division of Land Resources, the Coastal Area Management Act or any other Federal or
Local governmental permit that may be required. If you have any questions concerning this permit, please
contact Sergei Chernikov at telephone number [phone], extension 594.
Sincerely,
c�Rp- Alan C--,
. KlKlimekJP.E. Gt��J
cc: :.NPDES file's'
Central Files
1VlooresvMe Regional` Office-/ Surface: Water Protection
Aquatic ToxicologyUriit---- ___
Roosevelt Childress, EPA Region 4

Permit NC0004685
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
PPG Industries Fiber Glass Products, Incorporated
is hereby authorized to discharge wastewater and stormwater from a facility located at
Shelby Facility
On NCSR 1313
West of Shelby
Cleveland County
to receiving waters designated as Brushy Creek and Overflow Branch in the Broad River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts
I, II, III, and IV hereof.
The permit shall become effective December 1, 2005.
This permit and the authorization to discharge shall expire at midnight on August 31, 2008.
Signed this day November 4, 2005.
Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

Permit NC0004685
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby
revoked, and as of this issuance, any previously issued permit bearing. this number is no longer
effective. Therefore, the exclusive authority to operate and discharge from this facility arises under the
permit conditions, requirements, terms, and provisions included herein.
PPG Industries Fiber Glass Products, Incorporated is hereby authorized to:
Continue operation of a 1.3 MGD wastewater treatment facility consisting of:
• an overflow/storage basin;
• bar screen and grinder;
• an influent wet well with lime addition;
• influent pumps;
• a surge tank;
• an equalization tank;
• a flash mix tank with aluminum chloride addition;
• coagulant and polymer addition;
• two primary clarifiers;
• two aeration basins with bentonite clay addition;
• a splitter box and floc tank;
• three secondary clarifiers with ferric chloride addition;
• a sand filter;
• an effluent holding tank;
• a sludge thickener tank; and
• a sludge belt press.
These treatment works are located at PPG's " Shelby facility on NCSR 1313, west of Shelby,
Cleveland County and discharge treated process wastewater, stormwater, sanitary sewage,
cooling water, and landfill leachate, at the location specified on the attached map, through
outfall 001 into Brushy Creek, a class C water in the Broad River Basin; and
2. Discharge non -contact cooling water and stormwater through outfall 002, at the location
specified on the attached map, into Overflow Branch, a class C water in the Broad River Basin.

�Z, lg
f�1 AMEO � i
11�
V )IT
4 j
V,
�V
'.
% I T
-I'll. 7�-
JA
A
. . .
. . . . . . . �U. L
Outfall 001 to Brushy Creek X
'N_r Latitude: 35020'25"
f
Longitu de: 81036'58
T
V
46,
-7
Vr ff
Y y
CA
;0
- 01
A
j
/j i f
NI
V,
77- 46
4 # IT
.77
J2,
3N)
TIN - I V*j
4-
z
_g
V�
r �T
rj
•
X-,
y
iv
Outfall 002 to Overflow Branch -, : I c
L
J
Latitude: 35019'27"
Longitude: 81037'50"
V
y7.
4)
�'z
(j fir L }
A
7,
V
Y(
'I
NJ A
1AW
PPG Indtistrie's'. - NC0004685
Tkilit
Location J1,
USES Quad Name: Shelby SE/SW
Receiving Stream: see Above T
Stream Class':'C
-Ndith 40t t0' SCAL E
Subbasin: Broad - 03,0804

Permit NC0004685
Part I. Section A
1. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Beginning on the effective date of this permit and lasting until permit expiration, the Pen-nittee is authorized to
discharge from Outfall 001. Such discharges shall be limited and monitored by the Permittee as specified below:
:
PARAMETER'
EFFLUENT. LIMITATIONS F
MONITOY2ING.
REQUIRE
Monthly
Aver a
Daily
";`Maximum } :
Measurement
Fre uenc '
Sample,
..,
Saffiple.:;
1Location...:_
Flow (MGD)
1.3
Continuous
Recording
I or E
BOD, 5-day, 20oC (mass)
217.0 lbs/day
325.5 lbs/day
Weekly
Composite
E
BOD, 5-day, 200C (conc.)
20.0 mg/L
30.0 mg/L
Weekly
Composite
E
Total Suspended Solids
20.0 mg/L
146.0 mg/L
Weekly
Composite
E
NH3-N (mass)
65.0 lbs/day
97.5 lbs/day
Weekly
Composite
E
NH3-N (conc.)
6.0 mg/L
9.0 mg/L
Weekly
Composite
E
Dissolved Oxygen
Daily Average >_5.0 mg/L
Daily
Grab
E
Dissolved Oxygen (instream)
Monitor & Report
See Note 1
Grab
U,D
pH
>_6.0 to <_9.0 Standard Units
Daily
Grab
E
Temperature, oC
Daily
Grab
E
Temperature, oC (instream)
See Note 1
Grab
U,D
Fecal Coliform
Weekly
Grab
E
Total Nitrogen
Quarterly
Composite
E
Total Phosphorus
Quarterly
Composite
E
Conductivity
See Note 1
Grab
U,D
Oil and Grease
10.0 mg/L
15.0 mg/L
Weekly
Grab
E
Total Lead
Monthly
Composite
E
Fluoride
5.4 mg/L
Weekly
Composite
E
Total Zinc
2/Month
Composite
E
Total Copper
2/Month
Composite
E
Chloride
2/Month
Composite
E
Total Residual Chlorine2
17 µg/L
Weekly
Grab
E
Chronic Toxicity3
Quarterly
Composite
E
NOTES:
1 E - Effluent, I - Influent, U - Upstream at NCSR 1323, D - Downstream at NCSR 1305; upstream and downstream samples
shall be grab samples collected three times per week during June, July, August, and September and weekly during the
remainder of the year.
2 The limitation for TRC becomes effective 18 months from the effective date of this permit. Monitoring and effluent limitation
for TRC apply only if chlorine is added for disinfection.
3 Chronic Toxicity (Ceriodaphnia) P/F @ 33%; January, April, July, October. See Part I, A. 3 of this permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.

Permit NC0004685
Part I. Section A
2. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is authorized to
discharge from Outfall 002. Such discharges shall be limited and monitored by the Permittee as specified -below:
:.
EFFLUENT LIMITATIONS
MONITORING
RE UIREMENTS
PARAMETER
Montlily Daily
lVdeasurement'
Saffiple Sample
,.
Maximum _
.Fre uenc
e Location
Avera e. ,
,
Flow (MGD)
Semi -Annually
Estimate
Effluent
Temperature
See Note 1
Semi -Annually
Grab
Effluent
Total Residual Chlorine2
28 µg/L _
Semi -Annually
Grab
Effluent
pH
Between 6.0 and 9.0 Standard Units
Semi -Annually
Grab
Effluent
NOTES:
1 The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of
more than 2.8oC and in no case cause the ambient water temperature to exceed 290C.
2 The effluent limitation for chlorine shall become effective 18 months after the effective date of this permit. /)1Y4 / 20D I/
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.
THE PERMITTEE SHALL OBTAIN AUTHORIZATION FROM THE DIVISION OF WATER QUALITY PRIOR TO UTILIZING ANY BIOCIDE IN THE
COOLING WATER - SEE PART I, A. 4 OF THIS PERMIT.
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER.

Permit NC0004685
Part I. Section A
3. CHRONIC TOXICITY PERMIT LIMIT (QUARTERLY) - OUTFALL 001
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 33%.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent
versions. The tests will be performed during the months of January, April, July, and October. Effluent sampling
for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit
limit, then multiple -concentration testing shall be performed at a minimum, in each of the two following months
as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998)
or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the
pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the
following address:
Attention: Environmental Sciences Branch
North Carolina Division of
Water Quality
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no later than 30
days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
Concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity (An test form indicating the
facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No
Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences Branch at
the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include
alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival, minimum control organism. reproduction, and appropriate environmental controls, shall constitute an
invalid test and will require immediate follow-up testing to be completed no later than the last day of the month
following the month of the initial monitoring.

Permit NC0004685
Part I. Section A
4. BIOCIDE CONDITION
The Permittee shall not use any biocides except those approved in conjunction with the permit application. The
Permittee shall notify the Director in writing not later than ninety (90) days prior to instituting use of any
additional biocide used in cooling systems which may be toxic to aquatic life other than those previously reported
to the Division of Water Quality. Such notification shall include completion of Biocide Worksheet Form 101 and a
map locating the discharge point and receiving stream.
5. DISINFECTION CONDITION — OUTFALL 001
In the event that violations of North Carolina's water quality standards for fecal coliform occur as a result of this
discharge, disinfection will immediately be required and the permit amended to establish a fecal coliform effluent
limitation.

NPDES Permit Requirements
Page 1 of 16
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
Section A. Definitions
2/Month
Samples are collected twice per month with at least ten calendar days between sampling events.
3/Week
Samples are collected three times per week on three separate calendar days.
Act or "the Act"
The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended, 33 USC 1251, et. seq.
Annual Average
The arithmetic mean of all "daily* discharges" of a pollutant measured during the calendar year. In the case of fecal
coliform, the geometric mean of such discharges.
Arithmetic Mean
The summation of the individual values divided by the number of individual values.
Bypass
The known diversion of waste streams from any portion of a treatment facility including the collection system, which
is not a designed or established or operating mode for the facility.
Calendar Da�q
The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any
consecutive 24-hour period that reasonably represents the calendar day may be used for sampling.
Calendar Quarter
One of the following distinct periods: January through March, April through June, July through September, and
October through December.
Composite Sample
A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 ml in
such a manner as to result in a total sample representative of the wastewater discharge during the sample period. The
Director may designate the most appropriate method (specific number and size of aliquots necessary, the time
interval between grab samples, etc.) on a case -by -case basis. Samples may be collected manually or automatically.
Composite samples may be obtained by the following methods:
(1) Continuous: a single, continuous sample collected over a 24-hour period proportional to the rate of flow.
(2) Constant time/variable volume: a series of grab samples collected at equal time intervals over a 24.hour
period of discharge and combined proportional to the rate of flow measured at the time of individual sample
collection, or
(3) .Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period
with the time intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow recorder and
totalizer, and the preset gallon interval between sample collection fixed at no greater than 1 /24 of the
expected total daily flow at the -treatment system, or
(4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period at
a constant time interval. This method may only be used in situations where effluent flow rates vary
less than 15 percent. The grab samples shall be taken at intervals of no greater than 20 minutes apart
during any 24-hour period and must be of equal size and of no less than 100 milliliters. Use of this method
requires prior approval by the Director.
Version 612012003

NPDES Permit Requirements'
Page 2 of 16
In accordance with (4) above, influent grab samples shall not be collected more than once per hour.
Effluent grab samples shall not be collected more than once per hour except at wastewater treatment systems
having a detention time of greater than 24 hours. In such cases, effluent grab samples may be collected at
intervals evenly spaced over the 24hour period that are equal in number of hours to the detention time of the
system in number of days. However, the interval between effluent grab samples may not exceed six hours nor
the number of samples less than four during a 24-hour sampling period.
Continuous flow measurement
Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance
activities on the flow device.
Daily Discharge
The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the
calendar day for purposes of sampling. For pollutants measured in units of mass, the "daily discharge" is calculated as
the total mass of the pollutant discharged over the day. The "daily discharge' concentration comprises the mean
concentration for a 24-hour sampling period as either a composite 'sample concentration or the arithmetic mean of all
grab samples collected during that period. (40 CFR 122.3)
Daily Maximum
The highest "daily discharge" during the calendar month.
Daily Satnphng
Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the
permit. The Division expects that sampling shall be conducted on weekdays except where holidays or other
disruptions of normal operations prevent weekday sampling. If sampling is required for all seven days of the week
for any permit parameter(s), that requirement will be so noted on the Effluent Limitations and Monitoring Page(s).
DWO or "the Division"
The Division of Water Quality, Department of Environment and Natural Resources.
EMC
The North Carolina Environmental Management Commission.
Facility Closure
The cessation of wastewater treatment at a permitted facility, or the cessation of all activities that require coverage
under the NPDES. Completion of facility closure will allow this permit to be rescinded.
Geometric Mean
The Nth root of the product of the individual values where N = the number of individual values. For purposes of
calculating the geometric mean, values of "0" (or "< [detection level]' shall be considered =1.
Grab Sample
Individual samples of at least 100 ml collected over a period of time not exceeding 15 minutes. Grab samples can be
collected manually. Grab samples must be representative of the discharge (or the receiving stream, for instreatn
samples).
Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
Instantarieous flow measurement
A measure of flow taken at the time of sampling, when both the sample and flow will be representative of the total
discharge.
Version 612012003

NPDES Permit Requirements
Page 3 of 16
Months Average (concentration limitl
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar month. In the case of fecal
coliform, the geometric mean of such discharges.
Permit Issuing Authority
The Director of the Division of Water Quality.
Quarterly Average (concentration limit)
The average of all samples taken over a calendar quarter.
Severe property damage
Substantial physical damage to property, damage to the treatment facilities which causes them to become inoperable,
or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage excludes economic loss caused by delays in production.
Toxic Pollutant:
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
Upset
An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance with
permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance caused by
operational . error, improperly. designed treatment facilities, inadequate treatment facilities, lack of preventive
maintenance, or careless or improper operation.
Weekly Average (concentration limitl
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar week. In the case of fecal
coliform, the geometric mean of such -discharges.
Section B. General Conditions
1. Dui to COMI
The Permittee must comply with all conditions of this permit. Any permit noncompliance constitutes a violation
of the Clean Water Act and is grounds for enforcement action; for permit termination, revocation and reissuance,
or modification; or denial of a permit renewal application [40 CFR 122.41].
a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants and with standards for sewage sludge use or disposal established under
section 405(d) of the Clean Water Act within the time provided in the regulations that establish these
standards or prohibitions or standards for sewage sludge use or disposal, even if the permit has not yet been
modified to incorporate the requirement.
b. The Clean Water Act provides that any person who violates section 301, 302, 306, 307, 308, 318 or 405 of the
Act, or any permit condition or limitation implementing any such sections in a permit issued under section
402, or any requirement imposed in a pretreatment program approved under sections 402(a)(3) or 402(b)(8)
of the Act, is subject to a civil penalty not to exceed $25,000 per day for each violation. [40 CFR 122.41 (a)
(2)]
c. The Clean Water Act provides that any person who negligently violates sections 301, 302, 306, 307, 308, 318, or
405 of the Act, or any condition or limitation implementing any of such sections in a permit issued under
section 402 of the Act, or any requirement imposed in a pretreatment program approved under section
402(a)(3) or 402(b)(8) of the Act, is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment of not more than 1 year, or both. In the case of a second or subsequent conviction for a
negligent violation, a person shall be subject to criminal penalties of not more than $50,000 per day of
violation, or by imprisonment of not more than 2 years, or both. [40 CFR 122.41 (a) (2)]
Version 612012003

NPDES Permit Requirements
Page 4 of 16
d. Any person who knowing violates such sections, or such conditions or limitations is subject to criminal
penalties of $5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. In
the case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal
penalties of not more than $100,000 per day of violation, or imprisonment of not more than 6 years, or both.
[40 CFR 122.41 (a) (2)]
e. Any person who knowingly violates section 301, 302, 303, 306, 307, 308, 318 or 405 of the Act, or any permit
condition or limitation implementing any of such sections in a permit issued under section 402 of the Act,
and who knows at that time that he thereby places another person in imminent danger of death or serious
bodily injury, shall, upon conviction, be subject to a fine of not more than $250,000 or imprisonment of not
more than 15 years, or both. In the case of a second or subsequent conviction for a knowing endangerment
violation, a person shall be subject to a fine of not more than $500,000 or by imprisonment of not more than
30 years, or both. An organization, as defined in section 309(c)(3)(13)(iii) of the CWA, shall, upon conviction
of violating the imminent danger provision, be subject to a fine of not more than $1,000,000 and can be fined
up to $2,000,000 for second or subsequent convictions. [40 CFR 122.41 (a) (2)]
f. Under state law, a civil penalty of not more than $25,000 per violation may be assessed against any person
who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North
Carolina General Statutes § 143-215.6A]
g. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302,
306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such
sections in a permit issued under section 402 of this Act. Administrative penalties for Class I violations are
not to exceed $10,000 per violation, with the maximum amount of any Class I penalty assessed not to exceed
$25,000. Penalties for Class II violations are not to exceed $10,000 per day for each- day during. which. the
violation continues, with the maximum amount of any Class II penalty not to exceed $125,000. [40 CFR
122.41 (a) (3)]
2. Duty to Mitigate
The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in
violation of this permit which has a reasonable likelihood of adversely affecting human health or the environment
[40 CFR 122.41 (d)].
3. Civil and Criminal Liability
Except as provided in permit conditions on "Bypassing" (Part II. C. 4), "Upsets" (Part II. C. 5) and "Power
Failures" (Part II. C. 7), nothing in this permit shall be construed to relieve the Permittee from any
responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309
of the Federal Act, 33 USC 1319. Furthermore, the Permittee is responsible for consequential damages, such as
fish kills, even though the responsibility for effective compliance may be temporarily suspended.
4. OR and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee
from any responsibilities, liabilities, or penalties to which the Permittee is or may be subject to under NCGS 143-
215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for
consequential damages; such as fish kills, _even though the responsibility for effective compliance may, be
temporarily suspended.
5. Property Rights
The issuance of this permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion- of personal rights, nor
any infringement of Federal, State or local laws or regulations [40 CFR 122.41 (g)].
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical structures or
facilities or the undertaking of any work in any navigable waters.
Varcinn R/9nMnnQ

NPDES Permit Requirements
Page 5 of 16
7. Severability
The provisions of this permit are severable. If any provision of this permit, or the application of any provision of thi
permit to any circumstances, is held invalid, the application of such provision to other circumstances, and the remainde
of this permit, shall not be affected thereby [NCGS 150B-23].
8. Duty to Provide Information
The Permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any information which the
Permit Issuing; Authority may request to determine whether cause exists for modifying, revoking and reissuing, or
terminating this permit or to determine compliance with this permit. The Permittee shall also furnish to the
Permit Issuing Authority upon request, copies of records required by this pemut [40 CFR 122.41 (h)].
9. Duty to Reapply
If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit, the
Permittee must apply for and obtain a new permit [40 CFR 122.41 (b)].
10. Expiration of Permit
The Permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the Permittee shall submit such information, forms, and
fees as are required by the agency authorized to issue permits no later than 180 days prior to the expiration date.
Any Permittee that has not requested renewal at least 180 days prior to expiration, or any Permittee that does not
have a permit after the expiration and has not requested renewal at least 180 days prior to expiration, will subject
the Permittee to enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and certified
[40 CFR 122.41 (k)].
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible
corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in
charge of a principal business function, or any other person who performs similar policy or decision
making functions for the corporation, or (b) the manager of one or more manufacturing, production, or
operating facilities, provided, the manager is authorized to make management decisions which govern the
operation of the regulated facility including having the explicit or implicit duty of making major capital
investment recommendations, and initiating and directing other comprehensive measures to assure long
term environmental compliance with environmental laws and regulations; the manager can ensure that
the necessary systems are established or actions taken to gather complete and accurate information for
permit application requirements; and where authority to sign documents has been assigned or delegated
to the manager in accordance with corporate procedures .
(2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or
ranking elected official [40 CFR 122.22].
b.. All reports required by the permit and other information requested by the Permit Issuing Authority shall be
signed by a person described in paragraph a. above or by a duly authorized representative of that person. A
person is a duly authorized representative only if
1. The authorization is made in writing by a person described above;
2. The authorization specified either an individual or a position having responsibility for the overall
operation of the regulated facility or activity, such as the position of plant manager, operator of a well or
well field, superintendent, a position of equivalent responsibility, or an individual or position having
overall responsibility for environmental matters for the company. (A duly authorized representative may
thus be either a named individual or any individual occupying a named position); and
3. The written authorization is submitted to the Permit Issuing Authority [40 CFR 122.22]
Version 612012003

NPDES Permit Requirements .
Page 6 of 16
c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate
because a different individual or position has responsibility for the overall operation of the facility, a new
authorization satisfying the requirements of paragraph (b) of this section must be submitted to the Director
prior to or together with any reports, information, or applications to be signed by an authorized
representative [40 CFR 122.22]
d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the
following certification [40 CFR 122.22]:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the
Pern ittee for a permit modification, revocation and reissuance, or termination, or a notification of planned
changes or anticipated noncompliance does not stay any permit condition [40 CFR 122.41 (0].
13: Permit Modification Revocation and Reissuance or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the
permit, revoking and reissuing the permit, or terminating the permit as allowed by the laws, rules, and regulations
contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina
Administrative Code, Subchapter 2H .0100; and North Carolina General Statute 143-215.1 et. al.
14. Annual Administering and Compliance Monitoring Fee Requirements
The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being
billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 2H.0105 (b) (4)
may cause this Division to initiate action to revoke the permit.
Section C. - Operation and Maintenance of Pollution Controls
1. Certified Operatbr
Upon classification of the permitted facility by the Certification Commission, the Permittee shall employ a
certified water pollution control treatment system operator in responsible charge (ORC) of the water pollution
control treatment system. Such operator must hold a certification of the grade equivalent to or greater than the
classification assigned to the water pollution control treatment system by the Certification Commission. The
Permittee must also employ one or more certified Back-up .ORCs who possess a currently valid certificate of the
type of the system. Back-up ORCs must possess a grade equal to (or no more than one grade less than) the grade
of the system [15A NCAC 8G.02011.
The ORC of each Class I facility must:
➢ Visit the facility at least weekly
➢ Comply with all other conditions of 15A NCAC 8G.0204.
The ORC of each Class II, III and IV facility must:
➢ Visit the facility at least daily, excluding weekends and holidays
➢ Properly manage and document daily operation and maintenance of the facility
➢ Comply with all other conditions of 15A NCAC 8G.0204.
Once the facility is classified, the Permittee shall submit a letter to the Certification Commission designating the
operator in responsible charge:
a. Within 60 calendar days prior to wastewater being introduced into a new system
Version 612012003

NPDES Permit Requirements
Page 7 of 16
b. Within 120 calendar days of:
➢ Receiving notification of a change in the classification of the system requiring the designation of a
new ORC and back-up ORC
➢ A vacancy in the position of ORC or back-up ORC.
2. Proper Operation and Maintenance
The Pem-ittee shall at all times provide the operation and maintenance resources necessary to operate the existing
facilities at optimum efficiency. The Pemuttee shall at all times properly operate and maintain all facilities and
systems of treatment and control (and related appurtenances) which are installed or used by the Permittee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the Permittee to install
and operate backup or auxiliary facilities only when necessary to achieve compliance with the conditions of the
permit [40 CFR 122.41 (e)].
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a Permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this permit [40 CFR 122.41
(c)]
4. Bypassing of Treatment Facilities
a. Bypass not exceeding limitations [40 CFR 122.41 (m) (2)]
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but
only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject to the
provisions of Paragraphs b. and c. of this section.
b. Notice [40 CFR 122.41 (m)' (3)]
(1) Anticipated bypass. If the Permittee knows in advance of the need for a bypass, it shall submit prior
notice, if possible at least ten days before the date of the bypass; including an evaluation of the
anticipated quality and effect of the bypass.
(2) Unanticipated bypass. The Permittee shall submit notice of an unanticipated bypass as required in Part
II. E. 6. (24-hour notice).
c. Prohibition of Bypass
(1) Bypass from the treatment facility is prohibited and the Permit Issuing Authority, may take enforcement
action against a Permittee for bypass, unless:
(A) Bypass was unavoidable to'prevent loss of life, personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the.use of auxiliary treatment facilities,
retention of untreated wastes or maintenance during normal periods of equipment downtime. This
condition is not satisfied if adequate backup equipment should have been installed in the exercise of
reasonable engineering judgment to prevent a bypass which occurred during normal periods of
equipment downtime or preventive maintenance; and
(C) The Permittee submitted notices as required under Paragraph b. of this section.
(2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for a bypass as provided in any current or future system -wide collection system
permit associated with the treatment facility.
(3) The Permit Issuing Authority may approve an anticipated bypass, after considering its adverse effects, if
the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph c.
(1) of this section.
5. Upsets
a. Effect of an upset [40 CFR 122.41 (n) (2)1: An upset constitutes an affirmative defense to an action
brought for noncompliance with such technology based permit effluent limitations if the requirements of
paragraph b. of this condition are met. No determination made during administrative review of claims that
Version 612012003

NPDES Permit Requirements
Page 8 of 16
noncompliance was caused by upset, and before an action for noncompliance, is final administrative action
subject to judicial review.
b. Conditions necessary for a demonstration of upset: A Permittee who wishes to establish the
affirmative defense of upset shall demonstrate, through properly signed, contemporaneous operating logs, or
other relevant evidence that:
(1) An upset occurred and that the Permittee can identify the cause(s) of the upset;
(2) The Permittee facility was at the time being properly operated; and
(3) The Permittee submitted notice of the upset as required in Part II. E. 6. (b) (B) of this permit.
(4) The Permittee complied with any remedial measures required under Part II. B. 2. of this permit.
d. Burden of proof [40 CFR 122.41 (n) (4)]: The Permittee seeking to establish the occurrence of an
upset has the burden of proof in any enforcement proceeding.
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters
shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant
from such materials from entering waters of the State or navigable waters of the United States. The Permittee
shall comply with all existing Federal regulations governing the disposal of sewage sludge. Upon promulgation of
40 CFR Part 503, any permit issued by the Permit Issuing Authority for the utilization/disposal of sludge may be
reopened and modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR 503. The
Permittee shall comply with applicable 40 CFR 503 Standards for the Use and Disposal of Sewage Sludge (when
promulgated) within the time provided in the regulation, even if the permit is not modified to incorporate the
requirement. The Permittee shall notify. the Permit Issuing Authority of any significant change in its sludge use
or disposal practices.
7. Power Failures
The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 2H.0124 —
Reliability) to prevent the discharge of untreated or inadequately treated wastes during electrical power failures
either by means of alternate power sources, standby generators or retention of inadequately treated effluent.
Section D. Monitoring and Records
1. Representative Sg=llinng
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and nature of
the permitted discharge. Samples collected at a frequency less than daily shall be taken on a day and time that is
characteristic of the discharge over the entire period the sample represents. All samples shall be taken at the
monitoring points specified in this permit and, unless otherwise specified, before the effluent joins or is diluted
by any other wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to and the approval of the Permit Issuing Authority [40 CFR 122.41 (j)].
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each month and reported on a
monthly Discharge Monitoring Report (DMR) Form (MR 1, 1.1, 2, 3) or alternative forms approved by the
Director, postmarked no later than the 28th day following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of
these, and all other reports required herein, shall be submitted to the following address:
NC DENR / Division of Water Quality / Water Quality Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Version 6/20/2003

NPDES Permit Requirements
Page 9 of 16
3. Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected
and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. The
devices shall be installed, calibrated and maintained to ensure that the accuracy of the measurements is consistent
with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a
maximum deviation of less than 10% from the true discharge rates throughout the range of expected discharge
volumes. Flow measurement devices shall be accurately calibrated at a minimum of once per year and maintained
to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device.
The Director shall approve the flow measurement device and monitoring location prior to installation.
Once -through condenser cooling water flow monitored by pump logs, or pump hour meters as specified in Part I
of this permit and based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations (published pursuant to
NCGS 143-215.63 et. seq.), the Water and Air Quality Reporting Acts, and to regulations published pursuant to
Section 304(p), 33 USC 1314, of the Federal Water Pollution Control Act (as Amended), and 40 CFR 136; or in
the case of sludge use or disposal, approved under 40 CFR 136, unless otherwise specified in 40 CFR 503, unless
other test procedures have been specified in this permit [40 CFR 122.41].
To meet the intent of the monitoring required by this permit, all test procedures must produce minimum
detection and reporting levels that are below the permit discharge requirements and all data generated must be
reported down to the minimum detection or lower reporting level of the procedure. If no approved methods are
determined capable of achieving minimum detection and reporting levels below permit discharge requirements,
then the most sensitive (method with the lowest possible detection and reporting level) approved method must
be used.
5. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any
monitoring device or method required to be maintained under this permit shall, upon conviction, be punished by
a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or
by both. If a conviction of a person is for a violation committed after a first conviction of such person under this
paragraph, punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not more
than 4 years, or both [40 CFR 122.411.
6. Records Retention
Except for records of monitoring information required by this permit related to the Permittee's sewage sludge
use and disposal activities, which shall be retained for a period of at least five years (or longer as required by 40
CFR 503), the Permittee shall retain records of all monitoring information, including.
➢ all calibration and maintenance records
➢ all original strip chart recordings for continuous monitoring instrumentation
➢ copies of all reports required by this permit
➢ copies of all data used to complete the application for this permit
These records or copies shall be maintained for a period of at least 3 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time [40 CFR
122.41].
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the Permittee shall record
the following information [40 CFR 122.411:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
Version 612012003

NPDES Permit Requirements
Page 10 of 16
e. The analytical techniques or methods used; and
f. The results of such analyses.
8. Inspection and Entry
The Permittee shall allow the Director, or an authorized representative (including an authorized contractor acting
as a representative of the Director), upon the presentation of credentials and other documents as may be required
by law, to;
a. Enter upon the Permittee's premises where a regulated facility or activity is located or conducted, or where
records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this
permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices,
or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise
authorized by the Clean Water Act, any substances or parameters at any location [40 CFR 122.41 (i)].
Section E Reporting Requirements
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit. The discharge
of any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall
constitute a violation of the permit.
2. Planned Changes
The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or
additions to the permitted facility [40 CFR 122.410)]. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR
122.29 (b); or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged. This notification applies to pollutants subject neither to effluent limitations in the permit, nor to
notification requirements under 40 CFR 122.42 (a) 0).
c. The alteration or addition results in a significant change in the Permittee's sludge use or disposal practices,
and such alternation, addition or change may justify the application of permit conditions that are different
from or absent in the existing permit, including notification of additional use or disposal sites not reported
during the permit application process or not reported pursuant to an approved land application plan.
3. Anticipated Noncompliance
The Permittee shall give advance notice to'the Director of any planned changes to the permitted facility or other
activities that might result in noncompliance with the permit [40 CFR 122.410) (2)].
4. Transfers
This permit is not transferable to any person except after notice to the Director. The Director may require
modification or revocation and reissuance of the permit to document the change of ownership. Any such action
may incorporate other requirements as may be necessary under the Clean Water Act [40 CFR 122.410) (3)].
5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit [40 CFR 122.410) (4)].
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part II. D. 2) or forms
provided by the Director for reporting results of monitoring of sludge use or disposal practices.
b. If the Permittee monitors any pollutant more frequently than required by this permit, the results of such
monitoring shall be included in the calculation and reporting of the data submitted on the DMK
Version 612012003

NPDES Permit Requirements
Page 11 of 16
6. Twenty-four Hour Reporting
a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that
potentially threatens public health or the environment. Any information shall be provided orally within 24
hours from the time the Permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the Permittee becomes aware of the circumstances. The written
submission shall contain a description of the noncompliance, and its cause; the period of noncompliance,
including exact dates and times, and if the noncompliance has not been corrected, the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the
noncompliance [40 CFR 122.410) (6)].
b. The Director may waive the written report on a case -by -case basis for reports under this section if the oral
report has been received within 24 hours.
c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response
personnel at [phone], [phone] or [phone].
7. Other Noncompliance
The Permittee shall report all instances of noncompliance not reported -under Part II. E. 5 and 6. of this permit at
the time monitoring reports are submitted. The reports shall contain the information listed in Part II. E. 6. of
this permit [40 CFR 122.41 p) (7)].
8. Other Information
Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or
submitted incorrect information in a permit application or in any report to the Director, it shall promptly submit
such facts or information [40 CFR 122.410) (8)].
9. Noncompliance Notification "
The Permittee shall report by telephone to either the central office or the appropriate regional office of the
Division as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge 6f the occurrence of any of the following.
a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of
wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge
digester; the known passage of a slug of hazardous substance through the facility; or any" other unusual
circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps, aerators, compressors, etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass directly to receiving
waters without treatment of all or any portion of the influent to such station or facility.
Persons reporting such occurrences by telephone shall also file a written report within 5 days following first
knowledge of the occurrence.
10. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act, 33
USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the offices
of the Division of Water Quality. As required by the Act, effluent data shall not be considered confidential.
Knowingly making any false statement on any such report may result in the imposition of criminal penalties as
provided for in NCGS 143-215.1(b)(2) or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this permit, including
monitoring reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of
Version 612012003

NPDES Permit Requirements
Page 12 of 16
not more than $25,000 per violation, or by imprisonment for not more than two years per violation, or by both
[40 CFR 122.41].
12. Annual Performance Reports
Permittees who own or operate facilities that collect or treat municipal or domestic waste shall provide an annual
report to the Permit Issuing Authority and to the users/customers served by the Permittee (NCGS 143-215.1C).
The report shall summarize the performance of the collection or treatment system, as well as the extent to which
the facility was compliant with applicable Federal or State laws, regulations and rules pertaining. to water quality.
The report shall be provided no later than sixty days after the end of the calendar or fiscal year, depending upon
which annual period is used for evaluation.
PART III
OTHER REQUIREMENTS
Section A. Construction
The Permittee shall not commence construction of wastewater treatment facilities, nor add to the plant's treatment
capacity, nor change the treatment process(es) utilized at the treatment plant unless the Division has issued an
Authorization to Construct (AtC) permit. Issuance of an AtC will not occur until Final Plans and Specifications for
the proposed construction have been submitted by the Permittee and approved by the Division.
Section B. Groundwater Monitoring
The Pennittee shall, upon written notice from the Director of the Division of Water Quality, conduct groundwater
monitoring as may be required to determine the compliance of this NPDES permitted facility with the current
groundwater standards.
Section C. Changes in Discharges of Toxic Substances
The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe (40 CFR 122.42):
a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent
basis, of any toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the
following "notification levels";
0) One hundred micrograms per liter 000 µg/L);
(2) Two hundred micrograms per liter (200 µg/L) for acrolein and acrylonitrile; five hundred micrograms
per liter (500 µg/L) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol; and one milligram per liter
0 mg/L) for antimony;
(3) Five times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge, on a non -routine 'or
infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the
highest of the following "notification levels";
(1) Five hundred micrograms per liter (500 µg/L);
(2) One milligram per liter 0 mg/L) for antimony; —
(3) Ten times the maximum concentration value reported for that pollutant in the permit application.
Section D. Evaluation of Wastewater Discharge Alternatives
The Permittee shall evaluate all wastewater disposal alternatives and pursue the most environmentally sound
alternative of the reasonably cost effective alternatives. If the facility is in substantial non-compliance with the terms
and conditions of the NPDES permit or governing rules, regulations or laws, the Permittee shall submit a report in
such form and detail as required by the Division evaluating these alternatives and a plan of action within 60 days of
notification by the Division.
Section E. Facility Closure Requirements
The Permittee must notify the Division at least 90 days prior to the closure of any wastewater treatment system
covered by this permit. The Division may require specific measures during deactivation of the system to prevent
Version 612012003

NPDES Permit Requirements
Page 13 of 16
adverse impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit
continue at the permitted facility.
PART IV
SPECIAL CONDITIONS FOR MUNCIPAL FACILITIES
Section A Publicly Owned Treatment Works (POTWsI
All POTWs must provide adequate notice to the Director of the following.
1. Any new introduction of pollutants into the POTW from an indirect discharger which would be subject to
section 301 or 306 of CWA if it were directly discharging those pollutants; and
2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger
as influent to that POTW at the time of issuance of the permit.
3. For purposes of this paragraph, adequate notice shall include information on (1) the quality and quantity of
effluent introduced into the POTW, and (2) any anticipated impact of the change on the quantity or quality
of effluent to be discharged from the POTW.
Section B. Municipal Control of Pollutants from Industrial Users.
1. Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs from
industries using the municipal system may be present in the Permittee's discharge. At such time as
sufficient information becomes available to establish limitations for such pollutants, this permit may be
revised to specify effluent limitations for any or all of such other pollutants in accordance with best
practicable technology or water quality standards.
2. Under no circumstances shall the Permittee allow introduction of the following wastes in the waste
treatment system:
a. Pollutants which create a fire or explosion hazard ,in the POTW, including, but not limited to,
wastestreams with a closed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees
Centigrade using the test methods specified in 40 CFR 261.21;
b. Pollutants which will cause corrosive structural damage to the POTW, but in no case Discharges
with pH lower than 5.0, unless the works is specifically designed to accommodate such Discharges;
C. Solid or viscous pollutants in amounts which will cause obstruction to the flow in the POTW
resulting in Interference;
d. Any pollutant, including oxygen demanding pollutants (BOD, etc.) released in a Discharge at a flow
rate and/or pollutant concentration which will cause Interference with the POTW;
e. Heat in amounts which will inhibit biological activity in the POTW resulting in Interference, but in
no case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C
(104°F) unless the Division, upon request of the POTW, approves alternate temperature limits;
f. Petroleum oil, nonbiodegradable cutting oil, or products of mineral oil origin in amounts that will
cause interference or pass through;
g. Pollutants which result in the presence of toxic gases, vapors, or fumes within the POTW in a
quantity that may cause acute worker health and safety problems;
h. Any trucked or hauled pollutants, except at discharge points designated by the POTW.
3. With regard to the effluent requirements listed in Part I of this permit, it may be necessary for the
Permittee to supplement the requirements of the Federal Pretreatment Standards (40 CFR, Part 403) to
ensure compliance by the Permittee with all applicable effluent limitations. Such actions by the Permittee
may be necessary regarding some or all of the industries discharging to the municipal system.
4. The Permittee shall require any industrial discharges sending influent to the permitted system to meet
Federal Pretreatment Standards promulgated in response to Section 307(b) of the Act. Prior to accepting
wastewater from any significant industrial user, the Permittee shall either develop and submit to the
Version 612012003

NPDES Permit Requirements '
Page 14 of 16
Division a Pretreatment Program for approval per 15A NCAC 2H .0907(a) or modify an existing
Pretreatment Program per 15A NCAC 2H .0907(b).
This permit shall be modified, or alternatively, revoked and reissued, to incorporate or modify an approved
POW Pretreatment Program or to include a compliance schedule for the development of a POW
Pretreatment Program as required under Section 402(b)(8) of the Clean Water Act and implementing
regulations or by the requirements of the approved State pretreatment program, as appropriate.
Section C. Pretreatment Programs
Under authority of sections 307(b) and (c) and 402(b)(8) of the Clean Water Act and implementing regulations 40
CFR Part 403, North Carolina General Statute 143-215.3 (14) and implementing regulations 15A NCAC 2H
.0900, and in accordance with the approved pretreatment program, all provisions and regulations contained and
referenced in the Pretreatment Program Submittal are an enforceable part of this permit.
The Permittee shall operate its approved pretreatment program in accordance with Section 402(b)(8) of the Clean
Water Act, the Federal Pretreatment Regulations 40 CFR Part 403, the State Pretreatment Regulations 15A
NCAC 2H .0900, and the legal authorities, policies, procedures, and financial provisions contained in its
pretreatment program submission and Division approved modifications there of. Such operation shall include
but is not limited to the implementation of the following conditions and requirements:
1. Sewer Use Ordinance (SUP)
The Permittee shall maintain adequate legal authority to implement its approved pretreatment program.
2. Industrial Waste Survey (IWS)
The Permittee shall update its Industrial Waste Survey (IWS) to include all users of the sewer collection
system at least once every five years.
3. Monitoring Plan
The Permittee shall implement a Division approved Monitoring Plan for the collection of facility specific
data to be used in a wastewater treatment plant Headworks Analysis (HWA) for the development of
specific pretreatment local limits. Effluent data from the Plan shall be reported on the DMRs (as required
by Part II, Section D, and Section E.5.).
4. Headworks Analysis a A) and Local Limits
The Permittee shall obtain Division approval of a Headworks Analysis (HWA) at least once every five
years, and as required by the Division. Within 180 days of the effective date of this permit (or any
subsequent permit modification) the Permittee shall submit to the Division a written technical evaluation
of the need to revise local limits (i e., an updated HWA or documentation of why one is not needed) [40
CFR 122.42]. The Pennittee shall develop, in accordance with 40 CFR 403.5(c) and 15A NCAC 2H -.0909,
specific Local Limits to implement the prohibitions listed in 40 CFR 403.5(a) and (b) and 15A NCAC 2H
.0909.
5. Industrial User Pretreatment Permits am & Allocation Tables
In accordance with NCGS 143-215.1, the Permittee shall issue to all significant industrial users, permits for
operation of pretreatment equipment and discharge to the Permittee's treatment works. These permits
shall contain limitations, sampling protocols, reporting requirements, appropriate standard and special
conditions, and compliance schedules as necessary for the installation of treatment and control
technologies to assure that their wastewater discharge will meet all applicable pretreatment standards and
requirements. The Permittee shall maintain a current Allocation Table (AT) which summarizes the results
of the Headworks Analysis (HWA) and the limits from all Industrial User Pretreatment Permits (IUP).
Permitted IUP loadings for each parameter cannot exceed the treatment capacity of the POW as
determined by the HWA.
Version &20/2003

NPDES Permit Requirements
Page 15 of 16
6. Authorization to Construct (A to C)
The Permittee shall ensure that an Authorization to Construct permit (AtC) is issued to all applicable
industrial users for the construction or modification of any pretreatment facility. Prior to the issuance of
an AtC, the proposed pretreatment facility and treatment process must be evaluated for its capacity to
comply with all Industrial User Pretreatment Permit (IUP) limitations.
POTW Inspection & Monitoring of their SIUs
The Permittee shall conduct inspection, surveillance, and monitoring activities as described in its Division
approved pretreatment program in order to determine, independent of information supplied by industrial
users, compliance with applicable pretreatment standards. The Permittee must:
a. Inspect all Significant Industrial Users (SIUs) at least once per calendar year; and
b. Sample all Significant Industrial Users (SIUs) at least twice per calendar year for all permit -
limited pollutants, once during the period from January 1 through June 30 and once during the
period from July 1 through December 31, except for organic compounds which shall be sampled
once per calendar year;
8. SIU Self Monitoring and Reporting
The Permittee shall require all industrial users to comply with the applicable monitoring and reporting
requirements outlined in the Division approved pretreatment program, the industry's pretreatment permit,
or in 15A NCAC 2H .0908.
9. Enforcement Response Plan (ERP)
The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards
promulgated pursuant to section 307(b) and (c) of the Clean Water Act (40 CFR 405 et. seq.), prohibitive
discharge standards as set forth in 40 CFR 403.5 and 15A NCAC 2H .0909, and specific local limitations.
All enforcement actions shall be consistent with the Enforcement Response Plan (ERP) approved by the
Division.
10. Pretreatment Annual Reports (PAR)
The Permittee shall report to the Division in accordance with 15A NCAC 2H .0908. In lieu of submitting
annual reports, Modified Pretreatment Programs developed under 15A NCAC 2H .0904 (b) may be
required to meet with Division personnel periodically to discuss enforcement of pretreatment requirements
and other pretreatment implementation issues.
For all other active pretreatment programs, the Permittee shall submit two copies of a Pretreatment Annual
Report (PAR) describing its pretreatment activities over the previous twelve months to the Division at the
following address:
NC DENR / DWQ / Pretreatment Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
These reports shall be submitted according to a schedule established by the Director and shall contain the
following.
a.) Narrative
A brief discussion of reasons for, status of, and actions taken for all Significant Industrial
Users (SIUs) in Significant Non -Compliance (SNC);
b.) Pretreatment Program Summaa (PPS)
A pretreatment program summary (PPS) on specific forms approved by the Division;
c.) Significant Non -Compliance Report (SNCR)
The nature of the violations and the actions taken or proposed to correct the violations on
specific forms approved by. the Division;
d.) Industrial Data Summary Forms DS4
Version 612012003

NPDES Permit Requirements
Page 16 of 16
Monitoring data from samples collected by both the POTW and the Significant Industrial
User (SIU). These analytical results must be reported on Industrial Data Summary Forms
(IDSF) or other specific format approved by the Division;
e.) Other Information
Copies of the POTW's allocation table, new or modified enforcement compliance schedules,
public notice of SIUs in SNC, and any other information, upon request, which in the
opinion of the Director is needed to determine compliance with the pretreatment
implementation requirements of this permit;
11. Public Notice
The Permittee shall publish annually a list of Significant Industrial Users (SIUs) that were in Significant
Non -Compliance (SNC) as defined in the Permittee's Division approved Sewer Use Ordinance with
applicable pretreatment requirements and standards during the previous twelve month period. This list
shall be published within four months of the applicable twelve-month period.
12. Record Keeping
The Permittee shall retain for a minimum of three years records of monitoring activities and results, along
with support information including general records, water quality records, and records of industrial impact
on the POTW.
13. Funding; and Financial Report
The Permittee shall maintain adequate funding and staffing levels to accomplish the objectives of its
approved pretreatment program.
14. Modification to Pretreatment Programs
Modifications to the approved pretreatment program including but not limited to local limits
modifications, POTW monitoring of their Significant Industrial Users (SIUs), and Monitoring Plan
modifications, shall be considered a permit modification and shall be governed by 15 NCAC 2H .0114 and
15A NCAC 2H.0907..
Version 612012003

1r
SOC Priority Project: No
To: NPDES Unit
Water Quality Section
Attention: Charles Weaver
Date: July 30, 2003
NPDES STAFF REPORT AND RECOMMENDATION
MRO No.: 03-09
County: Cleveland
Permit No. NC0004685
PART I - GENERAL INFORMATION
1. Facility and address: PPG Industries, Inc.
940 Washburn Switch Road
Shelby, North Carolina 28150
2. Date of investigation: June 18, 2003
3. Report prepared by: Michael L. Parker, Environmental Engineer II
4. Persons contacted and telephone number: Todd Winn, [phone], ext. 359.
5. Directions to site: From the intersection of US Hwy 74 and SR 1313 (Washburn Switch Road)
just west of the City of Shelby, travel north on SR 1313 approximately 3.0 miles. The PPG plant
is located on the left side of the road.
6. Discharge point(s), list for all discharge points:
Outfall 001:
Latitude: 35° 20' 43" Longitude: 81° 37' 02"
Outfall 002:
Latitude: 35' 19' 28" Longitude: 810 37' 51"
Attach a USGS map extract and indicate treatment facility site and discharge point on map.
WWTP:
U.S.G.S. Quad No.: F12SW
U.S.G.S. Quad Name: Boiling Springs North, NC
Discharge point:
U.S.G.S. Quad No.: F12SE U.S.G.S. Quad Name: Shelby, NC
7. Site size and expansion area are consistent with application? Yes. There is ample area for
additional WWTP construction, if necessary.

Page Two
Topography (relationship to flood plain included): Flat to moderate slopes; the WWTP is not
located within a 100-year flood plain.
9. Location of nearest dwelling: None within 500 feet of the plant
10. Receiving stream or affected surface waters: Brushy Creek (outfall 001), Overflow Branch
(outfall 002)
a. Classification: C (both receiving streams)
b. River Basin and Subbasin No.: Broad 030804
C. Describe receiving stream features and pertinent downstream uses: Brushy Creek is of
moderate size (15-25 feet wide) with a sandy bottom. General "C" classification uses
downstream. Overflow Branch is = 3 - 4 feet wide, and downstream uses are primarily
agricultural in nature.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
a. Volume of wastewater to be permitted: 1.3 MGD (outfall 001), Flow is intermittent at
outfall 002.
Current permitted capacity of the wastewater treatment facility: 1.3 MGD
Actual treatment capacity of the current facility (current design capacity): 1.3 MGD
d. Date(s) and construction activities allowed by previous Authorizations to Construct issued
in the previous two years: There have been no ATCs issued in the past 2 years, however,
this facility was authorized to conduct a pilot testing program where treated effluent was
recycled back through the facility for use as non -contact cooling water (see Part IV).
e. Please provide a description of existing or substantially constructed wastewater treatment
facilities: Existing treatment facilities consists of an influent overflow/storage basin,
influent screening with grinder, wet well with lime addition, a surge tank, an equalization
tank, a flash mix tank for aluminum chloride, coagulant and polymer addition, two (2)
primary clarifiers, two (2) aeration basins with diffused air and bentonite clay addition, a
floc tank with ferric chloride addition, three (3) secondary clarifiers with ferric chloride
addition, a chlorine contact tank being used as an effluent pump tank (no chlorine is added
at this time), traveling bridge sand filter, defoamer addition, gravity sludge thickener, belt
filter press, and an overflow lagoon. Stand-by power is provided for the industrial process
and the WWTP through on -site generators. The permittee has received approval from the
Division to use of bentonite clay for effluent toxicity reduction and the addition of
aluminum chloride as a reactant for fluoride removal, chemical precipitation, and floc
formation. There is no treatment provided at outfall 002.
f. Please provide a description of proposed wastewater treatment facilities: There are no
proposed WWT facilities at this time.

Irr-age Three
g. Possible toxic impacts to surface waters: Information contained in the files -of this office
indicates that this facility is in compliance with it's toxicity testing requirements.
h. Pretreatment Program (POTWs only): N/A
2. Residuals handling and utilization/disposal scheme: Residuals are currently land filled at the JMN
private landfill. PPG has a non -discharge permit for the land application of residuals
(WQ0001055), however, no residuals have ever been applied.
Treatment plant classification: Class IV (no change from previous rating)
4. SIC Code(s): 3229 (PPG), 3083 (Azdel)
Wastewater Code(s) Primary: 64 Secondary: 02, 73, 15, 14, 36
Main Treatment Unit Code: 01602
PART III - OTHER PERTINENT INFORMATION
Is this facility being constructed with Construction Grant Funds or are any public monies involved
(municipals only)? No public monies were involved in the construction of this facility.
2.. Special monitoring or limitations (including toxicity) requests: None at this time.
Important SOC, JOC or Compliance Schedule dates: N/A
4. Alternative Analysis Evaluation:
Spray Irrigation: Insufficient area
Connection to Regional Sewer System: There is none presently available to serve this site.
Subsurface: Insufficient area
5. Air quality and/or groundwater concerns or hazardous materials utilized at this facility that may
impact water quality, air quality, or groundwater: No GW concerns at this time. The facility has
obtained the necessary air quality permits. There are no known hazardous materials concerns.
PART IV - EVALUATION AND RECOMMENDATIONS
The permittee, PPG Industries, Inc., has applied for permit renewal. The WWTP serves the
industrial and domestic needs for PPG and a nearby company; Azdel, Inc.. Azdel is located on the PPG
property and uses the fiberglass produced at PPG in part of their industrial process. Azdel contributes
10,000 gpd to the PPG WWTP.
Outfall 001 is the outfall from the WWTP that treats the industrial, domestic, some of the
stormwater from the two sites, and at this time all non -contact cooling wastewater. Outfall 002 consists
of non -contact cooling water and stormwater.

Page Four
11
In late August 2002, PPG submitted a request to conduct a pilot study whereby the effluent from
its WWT facility would be recycled back into the non -contact process water treatment system. The
reason for the study was due to an ongoing drought that had severely affected the amount of water
available to the City of Shelby which is where PPG obtains its process water. The pilot study would help
determine whether or not the recycling of PPG's WWTP effluent would be acceptable to use in its non -
contact cooling water process. It was PPG's intention that if the resulting data from the pilot study
indicated no detrimental effects as a result of the reuse of this water, the company would request that the
subject permit be amended to include the reuse of treated effluent. An approval letter was sent to the
company on August 5, 2002 authorizing the pilot study.
Based on the results of the study, PPG has found that the recycling of up to 100% of their effluent
to be a beneficial reuse of their wastewater, and they have requested that language be added to their
permit that allows this activity to continue. PPG also would like to have the option of installing a
filtration system on the non -contact process water waste stream to filter the recycled waste water prior to
its use. Should there be any need to discharge any of this non -contact process water it would be routed
back to the WWTP for recycling. Based on the information provided, this Office has no objection to this
request and recommends that the necessary language be included in the permit permanently authorizing
this activity.
PPG has also obtained coverage under SW general permit number NCG070015, which contains
outfalls, 003, 004, 005, 006, 007, and 008. Prior to reissuance of the subject NPDES permit, the staff of
the NPDES Unit should consider combining the two (2) permits for simplicity's sake, and to eliminate
any confusion that may arise between the two NPDES permits.
Based on the WWT facilities that are available, PPG should be able to continue to meet the existing
and proposed permit effluent limitations, provided there are no significant changes in the current waste
stream.
It is recommended that the permit be renewed as requested.
24�
Signature of report preparer Date
Water Quality 0,4ional Supervisor Date
h:\dsr\dsr03\ppg.sr

W q TF9QG
r
-";
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P. E. Director
Division of Water Quality
DIVISION OF WATER QUALITY
Mr. Tim Mathis, Manufacturing Manager
PPG Industries Fiber Glass Products, Inc.
940 Washburn Road
Shelby, North Carolina 28150
Dear Mr. Mathis:
November 10, 2005
Subject: NPDES Permit NC0004685
Shelby Facility
Cleveland County
Our records indicate that NPDES Permit No. NC0004685 was issued on November 4,
2005 for the discharge of wastewater to the surface waters of the State from your facility. The
purpose of this letter is to advise you of the importance of the Permit and the liabilities in the
event of failure to comply with the terms and conditions of the Permit. If you have not already
done so, it is suggested that you thoroughly read the Permit. Of particular importance are Pages
4and 5.
Pages 4 and 5 sets forth the effluent limitations and monitoring requirements for your
discharge. Your discharge must not exceed any of the limitations set forth. The section headed
"Monitoring Requirements" describes the measurement frequencies, sample types and sampling
locations. Upon commencement of your discharge (or operation), you must initiate the required
monitoring. The monitoring results must be entered on reporting forms furnished or approved by
this Agency. For new permits/facilities, the Division may supply an initial small stock of these
forms; however, if you fail to receive the forms, please contact this Office as quickly as possible.
The forms, including directions for their completion, and other important information are also
available at http://h2o.enr.state.ne.us/NPDES/documents.html. It is imperative that all applicable
parts be completed, and the original and one copy be submitted as required.
Please be advised that an annual fee may be required for your facility; if so, you will
receive a statement from our Raleigh Office. It is imperative that the fee be paid in a timely
manner so as to prevent enforcement action or possible revocation of your permit.
Noe Carolina
Nturally
N. C. Division of Water Quality, Mooresville Regional Office, 610 E. Center Ave. Suite 301, Mooresville NC 28115 [phone] Customer Service
1-877-623-6748

The remaining parts of the Permit set forth definitions, general conditions and special
conditions applicable to the operation of wastewater treatment facilities and/or discharge(s). The
conditions include special reporting requirements in the event of noncompliance, bypasses,
treatment unit/process failures, etc. Also addressed are requirements for a certified wastewater
treatment plant operator if you are operating wastewater treatment facilities. Any changes in
operation of wastewater treatment facilities, quantity and type of wastewater being treated or
discharged, expansions and/or upgrading of wastewater treatment facilities must be permitted or
approved by this Agency.
To maintain compliance with discharge limitations, proper operation and maintenance of
a wastewater treatment facility and the development of a process control program are essential.
For those facilities having chlorine tablet disinfection, please be advised that chlorine tablets
approved for wastewater treatment use must be used; swimming pool tablets are not approved.
Also, be advised that DWQ staff need to have access to the facility's discharge point into the
receiving stream; please maintain a path along the outfall line to facilitate that access.
Failure to comply with the terms and conditions of an NPDES Permit subjects the
Permittee to enforcement action pursuant to Section 143-215.6 of the North Carolina General
Statutes. A civil penalty of up to $25,000 per violation (and/or criminal penalties) may be
assessed for such violations. If you find at any time that you are unable to comply with the terms
and conditions of the Permit, you should contact this Office immediately. A Special Order by
Consent (SOC) may be necessary while pursuing action to obtain compliance.
As a final note, an NPDES Permit is normally issued for a five-year period. Permits are
not automatically renewed. Renewal requests must be submitted to this Agency no later than 180
days prior to expiration. Please make note of the expiration date of your Permit. This date is set
forth on Page 1 of the Permit. Also note that NPDES Permits are not automatically transferable.
If you, as the Permittee, cease to need this Permit, then you should request that the Division of
Water Quality rescind the Permit or request that DWQ reissue the Permit to another party, if
necessary.
As mentioned previously, the purpose of this letter is to advise you of the importance of
your NPDES Permit. Please read the Permit and contact this Office at 704/663-1699 in
Mooresville if you have any questions or need clarification. We look forward to providing any
assistance.
Sincerely,
r"t ID. Rex Gleason, P.E.
Surface Water Protection Regional Supervisor
l?

C� WAT �9QG
� r
�a ,?A• W� • ,fir ,.Wichpel F. Easley
®F'w,t, 1 ' d 0 IRCES
William:G4$'Ros�;FJ,'CASecretary
NCDENR "`�''`'
North Carolina Department of Environment an ,Natural Resources
Alan W. imek, P.E., Director
Division of Water Quality
Mr. Tim Mathis, Manufacturing Manager
PPG Industries Fiber Glass Products, Inc.
940 Washburn Road
Shelby, North Carolina 28150
Dear Mr. Mathis:
NOV 0 8 2005
November 4, 2005
IV SECTION
Subject: Issuance of NPDES Permit
NC0004685
Shelby Facility
Cleveland County
Division personnel have reviewed and approved your application for renewal of the subject permit.
Accordingly, we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to
the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between North Carolina and the U.S. Environmental Protection Agency dated May 9, 1994 (or as
subsequently amended).
This final permit includes following changes from the draft permit sent to you on June 1, 2004:
• In the supplement.to the permit cover sheet "a chlorine contact tank" was replaced with "an
effluent holding tank Change was done because chlorine is no longer used as a disinfecting agent.
• The total lead measurement frequency was changed from 2/month to 1/month to correct an error.
• The daily maximum TSS limit was changed from 30 mg/L to 146 mg/L to correct an error.
• The pH effluent limitations language was changed to ">6.0 to d" to be consistent with the
previous permit.
The Division has reviewed your request for a revision of the OR and Grease limit. The
request cannot be granted. Review of the Oil and Grease effluent data indicates that since February
2001 when the new analytical procedure became effective only violations of the Oil and Grease
limit have occurred. The vast majority of the measurements were below detection levels. In order to
change the limit, you will need to conduct a side -by -side method comparison in accordance with the
procedure described in the Section 2 of the document "Analytical Method Guidance for EPA
Method 1664A Implementation and Use (40 CFR Part 136), February 2000" and submit results to
the Division.
The Division cannot grant your request to reduce the monitoring frequency for BOD and NH, from
weekly to 2/month. Your facility is classified as a Class III facility and the current monitoring frequency for
oxygen consuming substances for your facility reflects a reduction in the standard monitoring frequency of
3/week for Class III facilities. In addition, both BOD and NH, are major operational parameters that
N. C. Division of Water Quality / NPDES Unit Phone: [phone]
1617 Mail Service Center, Raleigh, NC 27699-1617 fax: [phone]
Internet: h2o.enr.state.nc.us DENR Customer Service Center..1 800 623-7748

indicate effectiveness of treatment system operation and should be monitored frequently to prevent
deficiencies and limit violations and assure protection of the water quality in the receiving stream.
The Division is also unable to grant your request for adding the following statement to the effluent
page for Outfall 002: "Monitoring is required only when non -contact cooling water is discharged to outfall
002". The Outfall 002 is a non -contact cooling water outfall and is permitted in accordance with the general
permit for non -contact cooling water. Provisions in the General Permit for non -contact cooling water do
not allow the modification you have requested.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30)
days following receipt of this letter. This request must be in the form of a written petition, conforming to
Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings
(6714 Mail Service Center, Raleigh, North Carolina 27699-6714). Unless such demand is made, this
decision shall be final and binding.
Please note that this permit is not transferable except after notice to the Division. The Division
may require modification or revocation and reissuance of the permit. This permit does not affect the legal
requirements to obtain other permits which may be required by the Division of Water Quality or permits
required by the Division of Land Resources, the Coastal Area Management Act or any other Federal or
Local governmental permit that may be required. If you have any questions concerning this permit, please
contact Sergei Chernikov at telephone number [phone], extension 594.
Sincerely,
ov-, "Alan W. Klimek, P.E.
cc: NPDES files
Central Files
Mooresville Regional Office / Surface Water Protection
Aquatic Toxicology Unit
Roosevelt Childress, EPA Region 4

uoissi =OD 4ua1110�17BUUW luluauzuoJinug aql Jo Aluoglny gig
Ailun6 ia4LAA, jo uoisinlQ
Joloa IG "g.d '3lauzi�l •m uelV.
n9/1M Al w
-90OZ `-p jaquzanoN A'Op STIR pau�iig
800Z `I£ 4sn$nV uo 4q�11upiuz;u aiidxa llugs ajiiugosip o-juor;uzpoglnu atp puu liuuad sigi,
'S00Z I -iaquzaoa(I aniloajja ouiooaq liuus liuuad @%L
Joaxatl AI puu `III `II `I
sad ui llPOJ las suoilipuoo 131llo puu `sluauia.zinbas �uuoliuoui `suoilu HUTI luanpla ti}im aouupi000u
ui uisug JaAPd puozg aril ui tlouusg IAOUJanp puu xaajo Agsniq su paluu�31sap s-ialum �?uintaoai of
A:jUno0 puEianai0
Agiagg jo Isam
EIEI 2 93M u0
A3fiara AglazlS
lu paluool f4ii?ou3 u uzo.�l ialumtu cols puu-iolumalsum o�ljugosip of pazi toglnu �ga.zatl si
pa;Eaodzoaul 'slanpoid sselo aagi3 sau3snpul odd
`papuauiu su pV to quoD uoi4nllod-194utlA lu.zapa3 atll puu `uoissi =OD
luatua�uu7aW luluauiuoilAug uugo iuD MjoN aql Aq poldopu puu palu lnutoid suoiluln ai ptre
sp iupuuls in3mul satllo ` I ' S I Z-ot,l alnlulS lu.iauaD uugo-iu;D MJoN to suoisinoid aql tllim aouuilduioo uI
ma,tsAS mouvximiriH aouvHOSIa Lxv.La i Tod ivmoixvm
2Hi x2[aNn x2[,LVMa SVM ZOUVHOSIG of
All'IVfl60 2H3,LV A 30 MOISIAM
SH31MOS H WHfIJLVN UMV ZAi2WMOHlAM3 30 .LM3-LHVdHa
VNI'IOHVO HILMON 30 alLV.LS
989fi000ON liu-uad

Permit NC0004685
SUPPLEMENT TO PERAUT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby
revoked, and as of this issuance, any previously issued permit bearing this number is no longer
effective. Therefore, the exclusive authority to operate and discharge from this facility arises under the
permit conditions, requirements, terms, and provisions included herein.
PPG Industries Fiber Glass Products, Incorporated is hereby authorized to:
Continue operation of a 1.3 MGD wastewater treatment facility consisting of:
• an overflow/storage basin;
• bar screen and grinder;
• an influent wet well with lime addition;
• influent pumps;
• a surge tank;
• an equalization tank;
• a flash mix tank with aluminum chloride addition;
• coagulant and polymer addition;
• two primary clarifiers;
• two aeration basins with bentonite clay addition;
• a splitter box and floc tank;
• three secondary clarifiers with ferric chloride addition;
• a sand filter;
• an effluent holding tank;
• a sludge thickener tank; and
• a sludge belt press.
These treatment works are located at PPG's Shelby facility on NCSR 1313, west of Shelby,
Cleveland County and discharge treated, process wastewater, stormwater, sanitary sewage,
cooling water, and landfill leachate, at the location specified on the attached map, through
outfall 001 into Brushy Creek, a class C water in the Broad River Basin; and
2. Discharge non -contact cooling water and stormwater through outfall 002, at the location
specified on the attached map, into Overflow Branch, a class C water in the Broad River Basin.

IV
L/
G7)�
Outfall 001 to Brushy Creek
Latitude: 35120'25" J
\N
Longitude: 81136'5811
in
V
7
\V
1-7
40 J.
0
X• A
.
'Ji
31 NZ
YV
S" HIM)
Ify
?
4V
I L I
)-4
7
M I V
V
IN
7)(-
17*
7
4
Outfall 002 to Overflow Branch
Latitude: 35019'27"
Longitude: 81037'50"
-T d
Vi
. . ...........
X-
71
PPG Industries. - NC0004685 Facility
A I
L M
USGS Quad Name: Shelby SE/SW
Receiving Stream: See Above
Stream Class: C Not to SCALE
Subbasin: Broad - 030804 North I I

Permit NC0004685
Part I. Section A
1. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is authorized to
discharge from Outfall 001. Such discharges shall be limited and monitored by the Permittee as specified below:
PARAMETER
EFFLUENT. LIMITATIONS
MONITORING
REQUIREMENTS
Monthly, : ' ,
Aver a `' :
Daily
Maximum
Measurement
Frequency,, , ,
Sample
a
"Sample.
Location'
Flow (MGD)
1.3
Continuous
Recording
I or E
BOD, 5-day, 20oC (mass)
217.0 lbs/day
325.5 lbs/day
Weekly
Composite
E
BOD, 5-day, 20oC (conc.)
20.0 mg/L
30.0 mg/L
Weekly
Composite
E
Total Suspended Solids
20.0 mg/L
146.0 mg/L
Weekly
Composite
E
NH3-N (mass)
65.0 Ibs/day
97.5 lbs/day
Weekly
Composite
E
NH3-N (conc.)
6.0 mg/L
9.0 mg/L
Weekly
Composite
E
Dissolved Oxygen
Daily Average >_5.0 mg/L
Daily
Grab
E
Dissolved Oxygen (instream)
Monitor & Report
See Note 1
Grab
U,D
pH
>-6.0 to :59.0 Standard Units
Daily
Grab
E
Temperature, oC
—
Daily
Grab
E
Temperature, oC (instream)
See Note 1
Grab
U,D
Fecal Coliform
Weekly
Grab
E
Total Nitrogen
Quarterly
Composite
E
Total Phosphorus
Quarterly
Composite
E
Conductivity �^
See Note 1
Grab
U,D
Oil and Grease
10.0 mg/L
15.0 mg/L
Weekly
Grab
E
Total Lead
Monthly
Composite
E
Fluoride
-
—5.4 mg/L
Weekly
Composite
E
Total Zinc
2/Month'
Composite
E
Total Copper
2/Month
Composite
E
Chloride
2/Month
Composite
E
Total Residual Chlorine2
17 µg/L
Weekly
Grab
E
Chronic Toxicity3
Quarterly
Composite
E
NOTES:
1 E - Effluent, I - Influent, U - Upstream at NCSR 1323, D - Downstream at NCSR 1305; upstream and downstream samples
shall be grab samples collected three times per week during June, July, August, and September and weekly during the
remainder of the year.
2 The limitation for TRC becomes effective 18 months from the effective date of this permit. Monitoring and effluent limitation
for TRC apply only if chlorine is added for disinfection.
3 Chronic Toxicity (Ceriodaphnia) P/F @ 33%; January, April, July, October. See Part I, A. 3 of this permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.

Pem-At NC0004685
Part I. Section A
2. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is authorized to
discharge from Outfall 002. Such discharges shall be limited and monitored by the Permittee as specified below:
PARAMETER
EFFLUENT'LYMITATIONS
MONITORING REQUIREMENTS
Monthly,-
Avera e,..--
Daily
: _ .Magiffium.:
Measurement
Fre uency
- Sample.; ,
a
Sample
,Location_
Flow (MGD)
Semi -Annually
Estimate
Effluent
Temperature
See Note 1
Semi -Annually
Grab
Effluent
Total Residual Chlorine2
28 µg/L
Semi -Annually
Grab
Effluent
pH
Between 6.0 and 9.0 Standard Units
Semi -Annually
Grab
Effluent
NOTES:
1 The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of
more than 2.80C and in no case cause the ambient water temperature to exceed 29°C.
2 The effluent limitation for chlorine shall become effective 18 months after the effective date of this permit.
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.
THE PERMITTEE SHALL OBTAIN AUTHORIZATION FROM THE DIVISION OF WATER QUALITY PRIOR TO UTILIZING ANY BIOCIDE IN THE
COOLING WATER — SEE PART I, A. 4 OF THIS PERMIT.
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER.

Permit NC0004685
Part Io Section A
3. CHRONIC TOXICITY PERMIT LIMIT (QUARTERLY) — OUTFALL 001
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 33%.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent
versions. The tests will be performed during the months of January, April, July, and October. Effluent sampling
for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit
limit, then multiple -concentration testing shall be performed at a minimum, in each of the two following months
as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998)
or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the
pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the
following address:
Attention: Environmental Sciences Branch
North Carolina Division of
Water Quality
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no later than 30
days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the
facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No
Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences Branch at
the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include
alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival, minimum control organism. reproduction, and appropriate environmental controls, shall constitute an
invalid test and will require immediate follow-up testing to be completed no later than the last day of the month
following the month of the initial monitoring.

Permit NC0004685
Part I. Section A
4. BIOCIDE CONDITION
The Permittee shall not use any biocides except those approved in conjunction with the permit application. The
Permittee shall notify the Director in writing not later than ninety (90) days prior to instituting use of any
additional biocide used in cooling systems which may be toxic to aquatic life other than those previously reported
to the Division of Water Quality. Such notification shall include completion of Biocide Worksheet Form 101 and a
map locating the discharge point and receiving stream.
5. DISINFECTION CONDITION — OUTFALL 001
In the event that violations of North Carolina's water quality standards for fecal coliform occur as a result of this
discharge, disinfection will immediately be required and the permit amended to establish a fecal coliform effluent
limitation.

DENR/DWQ FACT SHEET FOR NPDES PERMIT DEVELOPMENT
NPDES No. NC0004685
"� rzy pk v^* kx '° 5 9 ..C. .y,. eh. '` ``42"{. G } 'C'rv,
�a��, , <.. s �rF a,.� . ,_ ��. o�,, za t� Facil�t Informs �lonn.�:,
Applicant/Facility Name:
PPG Industries Fiber Glass Products, Inc.
Applicant Address:
940 Washburn Switch Road, Shelby, NC
Facility Address:
940 Washburn Switch Road, Shelby, NC
Permitted Flow
1.3 MGD
Type of Waste:
95% Industrial, 5% Domestic
Facility/Permit Status:
Existing renewal without expansion
County:
Cleveland
..a`t h .. x w €m ,,
.a Stream Characterist.�csks',ri .,., ..M . .'
Receiving Stream
Brushy Creek (001) and Overflow Branch (002)
303(d) Listed?
No
Stream Classification
C
Sub -basin
03-08-04
Drainage Area (mi2):
15.1
Summer 7Q 10 (cfs)
4.0
Winter 7Q 10 (cfs) :
7.6
Average Flow (cfs) :
21.0
IWC (%) Q 3.0 MGD:
133
Regional Office:
Mooresville
USGS Topo Quad:
F12SE
Permit Writer:
Mark McIntire
Date
June 1, 2004
LO Proposed Changes
• Addition of total residual chlorine limits for both outfalls with an 18 month
schedule of compliance.
• Removal of instream fecal coliform monitoring.
• Monitoring frequency for lead has been reduced from 2/month to monthly.
2.0 Background
PPG Industries Fiber Glass Products, Inc. operates a fiberglass fiber manufacturing facility in
Shelby, NC. The Shelby plant currently concentrates the bulk of its fiberglass manufacturing
on the reinforced plastics market.
Manufacturing begins with glass raw materials including limestone, silica, boron, clay and
fluorspar. These raw materials are blended in powder form and added to melt furnaces. The
batch melt furnaces, operating at 28000F, transform the batch into molten glass. The molten
glass is then drawn from the furnaces through electrically heated platinum bushings into
continuous fibers. These fibers are gathered into strands and either spooled or chopped into
specified lengths. Water sprays cool the glass and keep strand contact points clean during the
winding process.
A "binder", which is water based, is applied to the individual fibergaas they are drawn from the
furnaces before being gathered into strands. The binder is a proprietary mixture of resins, film
formers, lubricants, surfactants and coupling agents emulsified in a water base. The majority of
the wastewater treated by the treatment plant is spray water, lost binder and cleaningmater.
PPG Industries Fact Sheet
NPDES Renewal
Page 1

Additional wastewater is received from Azdel, Inc. Azdel is a PPG joint venture with GE and
produces a fiber glass reinforced polypropylene sheet material that is sold to molders. This is
considered a plastics laminating process and is cover under 40 CFR 463. The manufacturing
process is dry, so that the wastewater sent to PPG is either cooling water, cleaning water or
domestic wastewater. Therefore, no allocation based on 463 is proposed.
3. Wasteload Allocation Summary
This permit was first issued on May 31, 1978. The permit was summarily adjudicated. It is not
entirely evident why the permit was adjudicated, however a review of historical files seems to
indicate that the adjudication was filed because of a disagreement with limit development. At
issuance, final effluent limitations were based on 40 CFR 410.32, Subpart C: Textile Dry
Processing. While the permit was being adjudicated, interim limits were established based on
the results of a field calibrated water quality model. Upon resolution of the adjudication (it was
determined that textile guidelines did not apply to PPG's discharge), the permit was reissued in
August of 1979 with water -quality limitations based on the results of the model. This original
series of wasteload allocations was based on a discharge flow of 0.875 MGD.
The permit was renewed in 1985 with a change in allocation, however the reason for the
change is not evidenced in the files. In 1988, Jackie Nowell completed a wasteload allocation
for this facility at an expanded flow of 1.3 MGD. The increase in flow was based on process
modifications in the manufacturing facility. - Jackie evaluated PPG's discharge with a level B
model and developed appropriate water quality -based limitations for BOD5 and NH3-N.
The current effluent limitations for BOD5 and NH3-N are based on the level B model run in
1988, while the current TSS limits are BPJ, apparently based on the BOD5 limits developed as
resolution to the 1978/79 adjudication.
Extensive research was conducted during the previous renewal process to. determine if any
federal guidelines exist for such a manufacturing operation. Lacy Ballard of PPG was contacted
for a detailed description of the manufacturing process and associated end products. Don
Anderson and Hugh Wise were contacted at EPA in D.C. regarding the applicability of textile
and glass guidelines. After conversations with both, it was determined that neither set of
guidelines applies to PPG's process. As stated earlier, PPG does accept wastewater from Azdel,
Inc. Azdel's operation falls under the authority of 40 CFR 463, Plastics Laminating. However,
manufacturing at Azdel is a dry process. Azdel's wastewater is largely cooling water, cleaning
water and domestic wastewater. Therefore, guidelines do not apply to this aspect of PPG's
effluent either.
PPG operates two outfalls, 001 and 002.
Outfall 001
Outfall 001 is the effluent from the wastewater treatment plant and receives the following kinds
of wastewater:
• Sanitary
• Research
• Boilers
• Miscellaneous
• Forming
• Fabrication
• Coating
• Process WW
• Storm drains/garage pads
• Azdel, Inc. WW
Outfall 002
Outfall 002 is a non -contact cooling water outfall and is permitted in accordance with the
general permit for non -contact cooling water.
PPG Industries Fact Sheet
NPDES Renewal
Page 2

Reasonable potential analyses were conducted for lead, copper, zinc, and fluoride for outfall
001. While the maximum predicted concentration for copper and zinc exceeded the allowable
concentration, no limits are proposed as the facility is not experiencing whole effluent toxicity.
The monitoring frequency for lead has been reduced from 2/month to monthly because of a
single detection in 2 years worth of sampling.
4.0 Compliance Summary
A review of DMR data has indicated that compliance with permit conditions is excellent.
While the facility had a history of toxicity .failures prior to 1996, installation of bentonite
addition facilities in 1998 appear to have fixed the problem. The facility has passed all whole
effluent toxicity tests since at least January 2000.
5.0 Instream Monitoring Requirements
PPG currently monitors dissolved oxygen, fecal coliform, temperature and conductivity
instream. This renewal recommends maintaining instream monitoring for DO, temperature,
and conductivity. As this stream is not 303(d) listed for fecal coliform, current strategy
recommends removal of instream monitoring for such.
6.0 Proposed Schedule for Permit Issuance
Draft Permit to Public Notice: June 1, 2004
Permit Scheduled to Issue: July 26, 2004
7.0 State Contact
If you have any questions regarding any of the above information or the attached permit, please
contact Sergei Chernikov at [phone] ext. 594.
CHANGES TO THE FINAL PERMIT:
• In the supplement to permit cover sheet "a chlorine contact tank" was replaced with "an
effluent holding tank. Change was done because chlorine is no longer used as a
disinfecting agent.
• The total lead measurement frequency was changed from 2/month to 1/month to
correct an error.
• The daily maximum TSS limit was changed from 30 mg/L to 146 mg/L to correct an
error.
• The monitoring frequency for BOD was changed from weekly to 2/month based on the
review of the effluent data and a response to the permittee request.
• The monitoring frequency for NHs was changed from weekly to 2/month based on the
review of the effluent data and a response to the permittee request.
• The pH effluent limitations language was changed to ">6.0 to <9" to be consistent with
the previous permit.
PPG Industries Fact Sheet
NPDES Ren.e%Nal
Page 3

qt ° f
June 1, 2004
_�
Mry J. T. Scruggs, • anufacturing Manager
PPG Industries -Fiber Glass Products, Inc.
940 Washburn Road
Shelby, North Carolina 28150
Dear Mr. Scruggs:
NL DEPT. QF O6 'R"Wtgle11F. Easley, Governor
AND fir" ACTT.^; _ RESOl1RCEiState of North Carolina
Al / �,. i lam floss, Jr., Secretary
Department of Erivir' ent and Natural Resources
Alan W. Klimek, P.E., Director
4 Division of Water Quality
WATER CIVAILIRYSECyloN
Subject: Draft NPDES Permit
Permit NC0004685
Shelby Facility
Cleveland County
Enclosed with this letter is a copy of the draft permit for your facility. Please review the draft carefully to
ensure thorough understanding of the conditions and requirements it contains. Changes to your existing
permit are summarized below.
• A daily maximum total residual chlorine (TRC) limitation has been included for both outfalls to
reflect recently adopted implementation strategy for a recently adopted freshwater standard for
TRC. An 18 month schedule of compliance.has been included for both outfalls.
• The instream monitoring requirement for fecal coliform has been deleted.
• The monitoring frequency for total lead has been reduced from 2/month to monthly.
In your permit application package you requested that the NPDES permit authorize the subject facility to
reuse treated effluent in the manufacturing processes. While the Division of Water Quality encourages
PPG to institute reuse at it's facilities, a Reuse Permit is required before instituting reuse on a long-term
basis. I have discussed this matter with Shannon Thornburg of the Division's Non -Discharge Permitting
Unit. She is generally familiar with this matter and can provide you with details regarding the Reuse
permitting process. She can be reached at [phone], extension 353.
Submit any comments to me no later than thirty days following your receipt of the draft. Comments
should be sent to my attention at the address listed at the bottom of this page. If you have any comments,
questions, or concerns regarding this draft permit, call me at [phone], extension 508.
Sincerely,
Mark D. McIntire, P.E.
NPDES, Unit
enclosures
cc: NPDES Unit
Moo`r_esville: Regional Office: /.-WateiQua'Iity Section (d'raff prmit,; fa_ct-sheet)g
Aquatic Toxicology Unit (draft permit)
Roosevelt Childress, EPA Region 4 (draft permit, fact sheet, permit application)
Shannon Thornburg, Non -Discharge Permitting Unit
1617 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1617 - TELEPHONE [phone]/FAX [phone]
VISIT US ON THE WEB AT http://h2o.enr.state.nc.us/NPDES

A
Permit NC0004685
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER DUALITY
M -7o I� k
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
The permit shall become effective
This permit and the authorization to discharge shall expire at midnight on August 31, 2008.
Signed this day
Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

Permit NC0004685
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby
revoked, and as of this issuance, any previously issued permit bearing this number is no longer
effective. Therefore, the exclusive authority to operate and discharge from this facility arises under the
permit conditions, requirements, terms, and provisions included herein.
PPG Industries Fiber Glass Products, Incorporated is hereby authorized to:
Continue operation of a 1.3 MGD wastewater treatment facility consisting of:
• an overflow/storage basin;
• bar screen and grinder;
• an influent wet well with lime addition;
• influent pumps;
• a surge tank;
• an equalization tank;
• a flash mix tank with aluminum chloride addition;
• coagulant and polymer addition;
• two primary clarifiers;
• two aeration .basins with.bentonite clay addition; --.--- --
• a splitter box and floc. tank;
• three secondary clarifiers with ferric chloride addition.
• a sand filter;
• a chlorine contact basin;
• a sludge thickener tank; and"
• a sludge belt press.;
These treatment works are locatedat PPG's Shelby facility on NCSR 1313, west of Shelby,
Cleveland:. County and discharge treated process wastewater, stormwater; sanitary sewage,
cooling water, and landfill leachate, at: the -location' specified on the attached map, through
outfall 001 into Brushy Creek; a class C water in the Broad River Basin; and
2. Discharge non -contact cooling water and stormwater through outfall 002, at the location
specified on the attached map, into Overflow Branch, a class C water in the Broad River Basin.

a
PPG Industries. - NC0004685
Facility
y u
Location
USGS Quad Name: Shelby SE/SW
Receiving Stream: See Above
Stream Class: C
Subbasin: Broad - 030804
N®%I i
Not to SCALE

Permit NC0004685
Part I. Section A
1. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is authorized to
discharge from Outfall 001. Such discharges shall be limited and monitored by the Permittee as specified below:
EFFLUENT, LIMITATIONS
_ _.
MONITORING >REQUIREMENTS
PARAMETER .
Monthly
DOW
Measuremient
Sample
Sample::
Aver " e :
Masim un
Ere" it ey.
Tne
l ocationl
Flow (MGD)
1.3
Continuous
Recording
I or E
BOD, 5-day, 20oC (mass)
217.0 lbs/day
325.5 lbs/day
Weekly
Composite
E
BOD, 5-day, 20 C (cone.)
20.0 mg/L
30.0 mg/L
Weekly
Composite
E
Total Suspended Solids
20.0 mg/L
30.0 mg/L
Weekly
Composite
E
NH3-N (mass) —...._......... --
65.0 lbs/day
97.5 lbs/day
--- - ....__...._.._....
Weekly
_... -- — --- ....... - ..._._.._...._
Composite
...----...
E
----- ....—..__...
-- ------ --.....-
NH3-N (cone.)
6.0 mg/L
9.0 mg/L _
Weekly
Composite
E
Dissolved Oxygen -
Daily Average >- 5.0 mg/L
Daily
Grab
E
Dissolved Oxygen (instream)
_.............. ---------- - - --- --...
Monitor & Report
--- ---....... - -- ---- - -- -- ...
See Note 1
-------
Grab
----
U,D
--- -
_
pH
Between 6.0 and 9.0 Standard Units
Daily
Grab
E
Temperature, OC .......... ... _.
_...Daily.-,.,
Grab.._
E
Temperature, OC (instream) ..........
See Note;l;
Grab
U,D
----
_...- -- -- -- - - -
Fecal Coliform
Weekly
Grab
E
Total NitrogenQuarterly
..... _..... _.. ....... _.... --- ................ ---. .......... _.........
_._ ............... --.....
----
Composite
- -- - ...--. -
E
--- - -...._...._...--
Total Phosphorus
Quarterly
Composite
E
Conductivity
See Note 1
Grab
U,D
Oil and Grease
10.0 ng/L
15.0 mg/L'.
Weekly .
Grab
.......---------
E
---- --
------...-.._..------.... ---_
Total Lead
.._._. :._. __—
_-....__._._.....---.-----....._.--._
...__....--------
2/Month
Composite
-
E
Fluoride
--
5.4-mg/L
.__-------._.... ---------
Weekly
----- _----
Composite
-,---,._.........
E
- ---------------- _
--....._...... -—.._..... __...... _......_..------- -----
Total Zinc
...-=-----.u.___.._._
.._._
2/Month
Composite
E
Total Copper
2/Month
Composite
E
Chloride
----.._._.._....._._.__..._.__......
_.._........._...__..._...- --
2/Month
-- - -- --------
Composite
--
E
-.-...-------....
_._.......... _.......... .......... _._... _..._.._....--- ...-...._._..._........-- ..... _..
Total Residual Chlorine2
.... ..........
17 µg/L
Weekly
---
Grab
--------.
E
_.....---....---------
-----...-------..__...--
Chronic Toxicity3
---------___-_-
_---------
Quarterly
Composite
E
NOTES:
1 E - Effluent, I - Influent, U - Upstream at NCSR 1323, D - Downstream at NCSR 1305; upstream and downstream samples
shall be grab samples collected three times per week during June, July, August, and September and weekly during the
remainder of the year.
2 The limitation for TRC becomes effective 18 months from the effective date of this permit. Monitoring and effluent limitation
for TRC apply only if chlorine is added for disinfection.
3 Chronic Tonicity (Ceriodaphnia) P/F ® 33%; January, April, July, October. See Part I, A. 3 of this permit_
THERE SHALL BE NO DISCHARGE OF FLOATING SOLIDS OR VISIBLE FOAM IN OTHER THAN TRACE AMOUNTS.

_•
Permit NC0004685
Part I. Section A
2. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Beginning on the effective date of this permit and lasting until permit expiration, the Permittee is authorized to
discharge from OutfaU 002. Such discharges shall be limited and monitored by the Permittee as specified below:
PARAMETER
Average
Maximum
Frequency
a
Location
Flow (MGD)
Semi -Annually
Estimate
Effluent
Temperature
_._._.._._...._..._._.._._._.__.....__.._.._..... - ._...__._.....—
See Note 1
-..._......_._......._..._..-.. ---- — ._.. _—...-- --..._.._.._..-...................----._
Semi -Annually
..—.__._....__..-------
Grab
Effluent
Total Residual Chlorine2
, 28 µg/L
........... ....
Semi -Annually
_......... ........... .........
Grab
Effluent
pH
Between 6.0 and 9.0 Standard Units
Semi -Annually
Grab
Effluent
NOTES:
1 The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of
more than 2.80C and in no case cause the ambient water temperature to exceed 29oC.
2 The effluent limitation for chlorine shall become effective 18 months after the effective date of this permit.
THERE SHALL BE NO DISCHARGE OF FLOATING -SOLIDS OR VISIBLE FOAM' IN_ OTHER THAN TRACE AMOUNTS.
THE PERMITTEE SHALL OBTAIN AUTHORIZATION FROM THE DIVISION OF WATER :QUALITY PRIOR TO UTILIZING ANY BIOCIDE IN THE
COOLING WATER — SEE PART l;,A. 4 OF THIS PERMIT.
THERE SHALL BE NO CHROMIUM, ZINC, ,OR'COPPER ADDED;TO THE COOLING WATER. ___

Permit NC0004685
Part I. Section A
3. CHROMIC TOXICITY PERMIT LIMIT (QUARTERLY) — OUTFALL 001
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 33%.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent
versions. The tests will be performed during the months of January, April, July, and October. Effluent sampling
for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the permit
limit, then multiple -concentration testing shall be performed at a minimum, in each of the two following months
as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998)
or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
All toxicity testing results required as` part of .phis permit ' condition = Will" be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP313 for the
pass/fail results acid THP313 for the Chronic Value. Additionally, DWQ Form AT=3 (original) is to be sent to the
following address:
Attention: Environmental Sciences'Branch
North Carolina Division of
Water :Quality
1621 Mail Seivice` Center
Raleigh,`North Carolina 27699=1621
Completed Aquatici Toxicity Test Forms shall be filed with the Environmental Sciences $ranch no later than 30
days after the end of the reporting period', for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature.
Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the
facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No
Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences Branch at
the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water
Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include
alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an
invalid test and will require immediate follow-up testing to be completed no later than the last day of the month
following the month of the initial monitoring.

4
Permit NC0004685
Part I. Section A
4. BIOCIDE CONDITION
The Permittee shall not use any biocides except those approved in conjunction with the permit application. The
Permittee shall notify the Director in writing not later than ninety (90) days prior to instituting use of any
additional biocide used in cooling systems which may be toxic to aquatic life other than those previously reported
to the Division of Water Quality. Such notification shall include completion of Biocide Worksheet Form 101 and a
map locating the discharge point and receiving stream.
5. DISINFECTION CONDITION — OUTFALL 001
In the event that violations of North Carolina's water quality standards for fecal coliform occur as a result of this
discharge, disinfection will immediately be required and the permit amended to establish a fecal coliform effluent
limitation.

DENR/DWQ FACT SHEET FOR NPDES PERMIT DEVELOPMENT
NPDES No. NC0004685
)F'aeilit Immformatioai ;_. n .
Applicant/Facility Name:
PPG Industries Fiber Glass Products, Inc.
Applicant Address:
940 Washburn Switch Road, Shelby, NC
Facility Address:
940 Washburn Switch Road, Shelby, NC
Permitted Flow
1.3 MGD
Type of Waste:
95% Industrial, 5% Domestic
Facility/Permit Status:
Existing renewal without expansion
County:
Cleveland
StreaYn Characteristics .. ,
Receiving Stream
Brushy Creek (001) and Overflow Branch (002)
303(d) Listed?
No
Stream Classification
C
Sub -basin
03-08-04
Drainage Area (mi2):
15.1
Summer 7Q 10 (cfs)
4.0
Winter 7Q10 (cfs):
7.6
Average Flow (cfs):
21.0
IWC (%) @ 3.0 MGD:
33
Miscellaneous
Regional Office:
Mooresville
USGS Topo Quad:
F12SE
Permit Writer:
Mark McIntire
Date
June 1, 2004
1.0 . Proposed Changes
Addition of total residual chlorine limits for both outfalls with an 18 month
schedule of compliance.
Removal of instream fecal coliform monitoring.
Monitoring frequency for lead has been reduced from 2/month to monthly.
2.0 Background
PPG Industries Fiber Glass Products, Inc. operates a fiberglass fiber manufacturing facility in
Shelby, NC. The Shelby plant currently concentrates the bulk of its fiberglass manufacturing
on the reinforced plastics market.
Manufacturing begins with glass raw materials including limestone, silica, boron, clay and
fluorspar. These raw materials are blended in powder form and added to melt furnaces. The
batch melt furnaces, operating at 2800oF, transform the batch into molten glass. The molten
glass is then drawn from the furnaces through electrically heated platinum bushings into
continuous fibers. These fibers are gathered into strands and either spooled or chopped into
specified lengths. Water sprays cool the glass and keep strand contact points clean during the
winding process.
A "binder", which is water based, is applied to the individual fibers as they are drawn from the
furnaces before being gathered into strands. The binder is a proprietary mixture of resins, film
formers, lubricants, surfactants and coupling agents emulsified in a water base. The majority of
the wastewater treated by the treatment plant is spray water, lost binder and cleaning water.
PP(; ine:lus_ries P;�::,. SE;eet
'ti 11DES Renewal
l i!gc

Additional wastewater is received from Azdel, Inc. Azdel is a PPG joint venture with GE and
produces a fiber glass reinforced polypropylene sheet material that is sold to molders. This is
considered a plastics laminating process and is cover under 40 CFR 463. The manufacturing
process is dry, so that the wastewater sent to PPG is either cooling water, cleaning water or
domestic wastewater. Therefore, no allocation based on 463 is proposed.
3. Wasteload Allocation Summ
This permit was first issued on May 31, 1978. The permit was summarily adjudicated. It is not
entirely evident why the permit was adjudicated, however a review of historical files seems to
indicate that the adjudication was filed because of a disagreement with limit development. At
issuance, final effluent limitations were based on 40 CFR 410.32, Subpart C: Textile Dry
Processing. While the permit was being adjudicated, interim limits were established based on
the results of a field calibrated water quality model. Upon resolution of the adjudication (it was
determined that textile guidelines did not apply to PPG's discharge), the permit was reissued in
August of 1979 with water -quality limitations based on the results of the model. This original
series of wasteload allocations was based on a discharge flow of 0.875 MGD.
The permit was renewed in 1985 with a change in allocation, however the reason for the
change is not evidenced in the files. In 1988, Jackie Nowell completed a wasteload allocation
for this facility at an expanded flow of 1.3 MGD. The increase in flow was based on process
modifications in the manufacturing facility. Jackie evaluated PPG's discharge with a level B
model and developed appropriate water quality -based limitations for BOD5 and NH3-N.
The current effluent limitations for BOD5 and NH3-N are based on the level B model run in
1988, while the current TSS limits are BPJ, apparently based on the BOD5 limits developed as
resolution to the 1978/79 adjudication.
Extensive research was conducted during the previous renewal process to determine if any
federal guidelines exist for such a manufacturing operation. Lacy Ballard of PPG was contacted
for a detailed description of the manufacturing process and associated end products. Don
Anderson and Hugh Wise were contacted at EPA in D.C. regarding the applicability of textile
and glass guidelines. After conversations with both, it was determined that neither set of
guidelines applies to PPG's process. As stated earlier, PPG does accept wastewater from Azdel,
Inc. Azdel's operation falls under the authority of 40 CFR 463, Plastics Laminating. However,
manufacturing at Azdel is a dry process. Azdel's wastewater is largely cooling water, cleaning
water and domestic wastewater. Therefore, guidelines do not apply to this aspect of PPG's
effluent either.
PPG operates two outfalls, 001 and 002.
Outfall 001
Outfall 001 is the effluent from the wastewater treatment plant and receives the following kinds
of wastewater:
• Sanitary
• Research
• Boilers
• Miscellaneous
• Forming
• Fabrication
• Coating
• Process WW
• Storm drains/garage pads
• Azdel, Inc. WW
Outfall 002
Outfall 002 is a non -contact cooling water outfall and is permitted in accordance with the
general permit for non -contact cooling water.
;NME;S Rc,nc'xal
P:,,:. 1.

Reasonable potential analyses were conducted for lead, copper, zinc, and fluoride for outfall
001. While the maximum predicted concentration for copper and zinc exceeded the allowable
concentration, no limits are proposed as the facility is not experiencing whole effluent toxicity.
The monitoring frequency for lead has been reduced from 2/month to monthly because of a .
single detection in 2 years worth of sampling.
4.0 Compliance Summary
A review of DMR data has indicated that compliance with permit conditions is excellent.
While the facility had a history of toxicity failures prior to 1996, installation of bentonite
addition facilities in 1998 appear to have fixed the problem. The facility has passed all whole
effluent toxicity tests since at least January 2000.
5.0 Instream Monitoring Requirements
PPG currently monitors dissolved oxygen, fecal coliform,
instream. This renewal recommends maintaining instream
and conductivity. As this stream is not 303(d) listed for
recommends removal of instream monitoring for such.
6.0 Proposed Schedule for Permit Issuance
Draft Permit to Public Notice: June 1, 2004
Permit Scheduled to Issue: July 26, 2004
temperature and conductivity
monitoring for DO, temperature,
fecal coliform, current strategy
7.0 State Contact
If you have any questions regarding any of the above information or the attached permit, please
contact Mark McIntire at (919) 33-5038 ext. 508.
NPDES UNIT SIGNOFF: 0G� n DATE:
REGIONAL OFFICE COMMENT:
NAME:
TE:
NPIDIFS
Page 3

�K-P
Michael F. Easley, Governor
William G. Ross, -Jr., Secretary
Department of Environment and Natural Resources
Alan Klimek, P.E. Director
Division of Water Quality
August 5, 2002
Mr. J. T. Scruggs, Manufacturing Manager
PPG Industries Fiber Glass Products
940 Washburn Switch Road
Shelby, N.C. 28150
Subject: Pilot Study Request
Recycle of WWTP Effluent
PPG Industries Fiber Glass Products- Shelby Plant
NPDES Permit No. NC0004685
Cleveland County
-D-ear_Mb . Scruggs:
This Office is in receipt of your letter dated August 6, 2002 concerning a request to
conduct a pilot study whereby the effluent from your WWT facility would be recycled back into
your process water treatment system. In your letter you indicated that the reason for this study is
due to the ongoing drought that has affected this part of the State, which has severely affected the
amount of water available to the City of Shelby where your current process water is obtained.
Once completed, the results of the pilot study will help determine whether or not the recycling of
your WWTP effluent would be acceptable in your manufacturing process. You also requested
that the pilot study begin from the date of your letter and continue through December 31, 2002.
Should the resulting data from the pilot study indicate no detrimental effects as a result of the
reuse of this water, a request for an amendment to the company's NPDES Permit will be
forthcoming.
This Office has no objection to PPG conducting a pilot study involving the recycle of
WWTP effluent back into the company's manufacturing process. This approval is effective from
the date of this letter through December 31, 2002. Please note that'under no circumstances should
this approval be construed to allow KoSa to exceed any existing NPDES permit limitation or to
by-pass any existing wastewater treatment process.
NCDENR
Customer Service
1 800 623-7748
Division of Water Quality
919 North Main Street Mooresville, NC.28115 Phone [phone]
Fax [phone]

Mr. J. T. Scruggs
August 5, 2002
Page Two
If you have any questions regarding this matter, please contact Mr. Michael Parker or me
at 704-663-1699.
cc: Dave Goodrich
/mlp
h\gen\pilotstd.doc
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Post -it® Fax Note 76-1 Date j j� pages►
rFax
d From '
VV '� v1�
Co./Dept. /_ Co.
# %l1� Phone #

PPFFP� . '
PPG Industries Fiber Glass Products, Inc.
940 Washburn Switch Road
Shelby, N.C. 28150
Mr. Michael Parker
Division of Water Quality
NC DENR
919 North Main Street
Mooresville, NC 28115
Re: Pilot Study
Dear Mr. Parker:
RECEIVED
AUG 5 2002
August 6, 2002
NC DEPT OF EH4'RO'%' Er?T
AND NATU`tA L RE- O' RC'U': a
M)OFESVILLE RECIWIAL 0i=a itiE
Due to the existing drought affecting Cleveland County, we are submitting a request to conduct a
pilot study to recycle treated effluent at our facility. This pilot study will involve the recycle of
up to 100% of our treated effluent. The treated water, now being discharged to Brushy Creek
(NPDES permit # NC0004685), will be reused as non -potable, process water only. We are
requesting that the approval for this pilot study run through December 31, 2002.
Upon the conclusion of this study, we will determine the overall feasibility of this recycling
effort.
If the results of this study are favorable, we will submit an application to your department to
modify our existing permit to include this recycling effort.
If you have any questions concerning this request, please contact Todd Winn, Environmental
Engineer, at 704-474-2261 extension 359.
Sincerely,
1 /,
J.T. Scruggs
Manufacturing Manager
cc: file

State of North Carolina \
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor'
Wayne McDevitt, Secretary
Kerr T. Stevens, Director
April 12, 1999
Mr. Lacy Ballard
PPG Industries Fiber Glass Products, Inc.
940 Washburn Switch Road
Shelby, North Carolina 28150
Dear Mr. Ballard:
NCDENR
Subject: NPDES Permit Correction
Permit No. NC0004685
Shelby Facility
Cleveland County
On March 29, 1999 the Division of Water Quality issued NPDES Permit No. NC0004685 to PPG
Industries for their Shelby facility. In response to your request received April 6, 1999, the permit has been
corrected to include weekly monitoring for BOD, and NHS-N as was required in the previously issued permit.
Please find enclosed an amended effluent limitations page for outfall 001. This page should be
inserted into your permit and the old one discarded. All other terms and conditions contained in the original
permit remain unchanged and in full effect. This permit correction is issued pursuant to the requirements of
North Carolina General Statutes 143-215.1 and the Memorandum of Agreement between North Carolina and
the U. S. Environmental Protection Agency.
If you have any questions concerning this permit modification, please contact Mr. Mark McIntire at
telephone number [phone],' extension 553.
Sincerely,
err T. Stevens
Cc: Central Files _
A�looresville Regional`Office % Water.Quality Section_ .�
NPDES-Unit-Files
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50 % Recycled / 10 % Post -consumer paper
A

PPP'�.
A. (1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - FINAL Permit No. NC0004685
During the period beginning on the effective date of the permit and lasting until permit expiration, the Permittee is authorized to discharge from
outfall(s) serial number 001. Such discharges shall be limited and monitored by the Permittee as specified below:
EFFL S 1VIONiTORING REQUIlEMEN 1S
.,
ont yDaily, Monthly Daily
. Average. Maximum Average;Maximum Measurement SainpleSample „�
r ",.; lb%day , Ib/day Coneentration zConcentration FFrequencY �'YPe Location';`
Flow Continuous Recordink T I or E
Total• • • • itill[ITiT7/1��[[�1i'T7/11♦ • • • •
�i►1:lQ► �•T.XII♦Sy�.��:�ll ,�/�S!�1 •i'"iT7/1� �� • - • • •
ores
/-inc
m
m
Notes:
I Sample Locations: E - Effluent, I - Influent, U - Upstream at NCSR 1323, D - Downstream at NCSR 1305; upstream and downstream samples shall be grab samples. Stream samples shall
be collected three times per week during June, July, August, and September and once per week during the remaining months of the year. z
'- The daily average dissolved oxygen effluent concentration shall not be less than 5.0 mg/L.
3 The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
r" 4 Chronic Toxicity (Ceriodaphnia) P/F @ 33 %; January, April, July, October; See A(3) of the Supplement to Effluent Limitations page; collection of the composite toxicity sample shall
coincide with composite samples for lead, fluoride, zinc, copper, and chloride.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
L-1

State of North Carolina
Department of Environmen.
and Natural Resources
Division of Water Quality
1994
James B. Hunt, Jr., Governor NCDENR
Wayne McDevitt Secretary
;,t
ORTH CAROLINA DEPARTMENT OF
Kerr T. Stevens, Director °"' =:fl r {,ENVIRONMENT AND NATURAL RESOURCES
March 29, 1999
Mr. Lacy Ballard
PPG Industries Fiber Glass Products, Inc.
940 Washburn Switch Road
Shelby, North Carolina 28150
Subject: NPDES Permit Issuance
Shelby Facility
Permit Number NC0004685
Cleveland County
Dear Mr_ Ballard:
In accordance with the application for discharge permit received on July 1, 1997, the Division
is forwarding herewith the subject state - NPDES permit. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between North Carolina and the U.S. Environmental Protection Agency dated December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty
(30) days following receipt of this letter. This request must be in the form of a written petition,
conforming to Chapter 150B of the North Carolina General Statutes, and filed with the office of
Administrative Hearings, Post Office Drawer 27447, Raleigh, North Carolina 27611-7447. Unless
such a demand is made, this permit shall be final and binding.
This permit does not affect the legal requirements to obtain other permits which may be
required by the Division of Water Quality or permits required by the Division of Land Resources,
Coastal Area Management Act, or any other Federal or Local governmental permits which may be
required.
If you have any questions or comments regarding these speculative limitations, please do not
hesitate to contact Mark McIntire at telephone number [phone], extension 553.
Sincerely
Original Signed By
®avid A. Goodrich
Kerr T. Stevens
Cc: Central Files
NPDES Permit File _
Mooresvil]e_Regional..Off'ce`—W__ It Quality
Aquatic Toxicology Unit
EPA, Roosevelt Childress
P.O. Box 29535, RALEIGH, NORTH CAROLINA 27626-0535 TELEPHONE [phone]/FAX [phone]
AN EQUAL OPPORTUNITY AFFIRMATIVE ACTION EMPLOYER 50% RECYCLED/ 10% POST -CONSUMER PAPER

r
Permit No. NC0004685
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
PPG Industries Fiber Glass Products, Incorporated
is hereby authorized to discharge treated wastewater from a facility located at
Shelby Facility
On NCSR 1313
West of Shelby
Cleveland County
to receiving waters designated as Brushy Creek and Overflow Branch in the Broad River Basin
in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I,
II, III and IV hereof.
The permit shall become effective May 1, 1999
This permit and the authorization to discharge shall expire at midnight on August 31, 2003
Signed this day March 29, 1999
Original Signed By
David A. Goodrich
KerrT. Stevens, Director
Division of Water Quality
By Authority of the Environmental Management Commission

Permit No. NC0004685
SUPPLEMENT TO PERMIT COVER SHEET
PPG Industries Fiber Glass Products, Incorporated
is hereby authorized to:
1. Continue operation of a 1.3 MGD wastewater treatment facility consisting of an
overflow/storage basin, bar screen and grinder, an influent wet well with lime addition,
influent pumps, a surge tank, an equalization tank; a flash mix tank with aluminum
chloride addition, coagulant and polymer addition, two primary clarifiers, two aeration
basins with bentonite clay addition, a splitter box and floc tank, three secondary clarifiers
with ferric chloride addition, a sand filter, a chlorine contact basin, a sludge thickener
tank, and a sludge belt press located at PPG's Shelby facility ' on NCSR 1313, west of
Shelby, Cleveland County (see Part III, A of this permit), discharging treated process
wastewater, stormwater, sanitary sewage, cooling water, and landfill leachate from said
treatment works,. at the location specified on the attached map, through outfall 001 into
Brushy Creek, a class C water in the Broad River Basin; and
2. Discharge non -contact cooling water and stormwater through outfall 002, at the location
specified on the attached map, into Overflow Branch, a class C water in the Broad River
Basin.

�
•��^ I �• •��
1,337 � o I \
'�
I I yj
/ ) /�
96
J -r
Do968
uble Sftint/
. S \�t
\ -� .n
00
� ice• O
323
washDurn
a
�Substati51_n 1313
7 ♦^
Cl
INER
BM
�\ 2
o
0 132
J' �- 1 -
Bogy
CP
17
e '
1314r
kayo
rr�"BLA
In
`r
lsx
132
J
c'
Ifer
ARO
Scale 1: 24 000
Latitude: 35'20'43"
Longitude: 81°37'02"
Quad #. F12SE
Stream Class: C
Receiving Stream: Brushy Creek (001) d`? Overflow Branch (002)
Permitted Flow: 1.3 MGD (001)
/'wzz
4 6
art "eK4'. cl'i
PPG Industries, Inc.
NC0004685
Cleveland County

A. (1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - FINAL Permit No. NC0004685L
During the period beginning on the effective date of the permit and lasting until permit expiration, the Permittee is authorized to discharge from
outfall(s) serial number 001. Such discharges shall be limited and monitored by the Permittee as specified below:
EFFLUENCHARAC
„.
montill y
Average
Daily,.,
Maximum
lbLday"l
; . ont i y
Average
oncentration
Daily,
;Maximum
Concentration
Measurement
.. ;rFrequency
Sample.,; ,t
....
Sample .-
rLocation'
oW7MGM
1.3
Continuous
Kecorclmg
lorE
5-day,
mg
mg
Daily
Composite
otal SuspendedResidue
20.0 m
mg
Daily
ompostte
,-
mg
mg
Daily
ompostte
Dissolved xygen
Daily
6rab
pHj
Daily
Grab
Temperature °C
Daily
Grab,
Fecal o i orm geometric mean
Weekly
Grab,
Total Nitrogen + Z+
—Quarterly
Composite
Total Phosphorus
Quarterly
ompostte
Conductivity
6ee Note '
I Urab
I U, D—
Oil and Grease
100 m a
m n
ee v
,ra
m
tc
e
Notes:
t Sample Locations: E - Effluent, I — Influent, U — Upstream at NCSR 1323, D — Downstream at NCSR 1305; upstream and downstream samples shall be grab samples. Stream samples shall
be collected three times per week during June, July, August, and September and once per week during the remaining months of' the year.
z The daily average dissolved oxygen effluent concentration shall not be less than 5.0 mg/L.
3 The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
4 Chronic Toxicity (Ceriodaphnia) P/F @ 33 %; January, April, July, October; See A(3) of the Supplement to Effluent Limitations page; collection of the composite toxicity sample shall
coincide with composite samples for lead, nickel, fluoride, zinc, copper, and chloride.
There shall be no discharge of floating solids or visible foam in other than trace amounts.

A. (2) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - FINAL Permit No. NC0004685
During the period beginning on the effective date of the permit and lasting until permit expiration, the Permittee is authorized to discharge from
outfall(s) serial number 002. Such discharges shall be limited and monitored by the Permittee as specified below:
Ts
�
r
-,.> r,"5 s, ��' :..� •.his ,J�,-':,
E� I, Y s
.,.v'"* §
aF"% % y
gbh`
on i y
at
y� r�
�, y
rMdy�� a
Maximum
Aveia a
"
Maztmuiri
t?MeasuienrentS.
le">��Sam1
;1. «
ab/day
�:, �, ..z3
Ib/day
ConceiitCatton
'Concentration
rFrequency
_FTow
,E.
;{;
Types
I;ocationl.
(MGD)
Semi -Annually
sttmate
emperature
See Note
See Note
eml- nnua y
Cirab
otal ResidualChlorine
I 6enli-Annually
Grab
Notes
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER.
t Sample Locations: E - Effluent
2 The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of more than 2.80C and in no case cause the ambient water temperature to
exceed 290C.
The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
The Permittee shall obtain authorization from the Division of Water Quality prior to utilizing any biocide in the cooling water (See A(4) of the Supplement to Effluent Limitations Page).
There shall be no discharge of floating solids or visible foam in other than trace amounts.

PPG Industries Fiber Glass Products, Incorporated
Permit No. NC0004685
SUPPLEMENT TO EFFLUENT LIMITATIONS
AND MONITORING REQUIREMENTS
SPECIAL CONDITIONS
A_ (3) CHRONIC TOXICITY PASS/FAIL PERMIT LIMIT (QUARTERLY)
The effluent discharge shall at no time exhibit chronic toxicity using test procedures outlined in the "North Carolina
Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised November 1995, or subsequent versions.
The effluent concentration at which there may be no observable inhibition of reproduction or significant mortality is 33%
(defined as treatment two in the procedure document). The permit holder shall perform quarterly monitoring using this
procedure to establish compliance with the permit condition. The tests will be performed during the months of January, April,
July and October. Effluent sampling for this testing shall be performed at the NPDES permitted final effluent discharge below
all treatment processes.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring Form
(MR-1) for the month in which it was performed, using the parameter code TGP3B. Additionally, DWQ Form AT-1 (original)
is to be sent to the following address:
Attention: Environmental Sciences Branch
North Carolina Division of
Water Quality
4401 Reedy Creek Rd.
Raleigh, N.C. 27607
Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in association
with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity sample must be
measured and reported if chlorine is employed for disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the Permittee
will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, permit
number, pipe number, county, and the month/year of the report with the notation of "No Flow" in the comment area of the
form. The report shall be submitted to the Environmental Sciences Branch at the address cited above.
Should any single quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring will begin
immediately until such time that a single test is passed. Upon passing, this monthly test requirement will revert to quarterly in
the months specified above.
Should the Permittee fail to monitor during a month in which toxicity monitoring is required, then monthly monitoring will
begin immediately until such time that a single test is passed. Upon passing, this monthly test requirement will revert to
quarterly in the months specified above.
Should any test data from this,monitoring requirement or tests performed by the North Carolina Division of Water Quality
indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring
requirements or limits.
NOTE: Failure to achieve test conditions as specified in the. cited document, such as minimum control organism survival,
minimum control organism reproduction, and appropriate environmental controls, shall constitute an invalid test and will
require immediate follow-up testing to be completed no later than the last day of the month following the month of the initial
monitoring.

PPG Industries Fiber Glass Products, Incorporated
Permit No. NC0004685
SUPPLEMENT TO EFFLUENT LIMITATIONS
AND MONITORING REQUIREMENTS
SPECIAL CONDITIONS (Continued)
A. (4) BIOCIDE CONDITION
The Permittee shall not use any biocides except those approved in conjunction with the permit application. The Permittee
shall notify the Director in writing not later than ninety (90) days prior to instituting use of any additional biocide used in
cooling systems which may be toxic to aquatic life other than those previously reported to the Division of Water Quality.
Such notification shall include completion of Biocide Worksheet Form 101 and a map locating the discharge point and
receiving stream.
A. (5) DISINFECTION CONDITION
In the event that violations of North Carolina's water quality standards for fecal coliform occur as a result of this discharge,
disinfection will immediately be required and the permit amended to establish a fecal coliform effluent limitation.

PART I
Section B. Schedule of Compliance
1. The permittee shall comply with Final Effluent Limitations specified for discharges in accordance
with the following schedule:
Permittee shall comply with Final Effluent Limitations by the effective date of the permit unless
specified below.
2. Permittee shall at all times provide the operation and maintenance necessary to operate the
existing facilities at optimum efficiency.
3. No later than 14 calendar days following a date identified in the above schedule of compliance,
the permittee shall submit either a report of progress or, in the case of specific actions being
required by identified dates, a written notice of compliance or noncompliance. In the latter case,
the notice shall include the cause of noncompliance, any remedial actions taken, and the
probability of meeting the next schedule requirements.

Part II
Page I of 14
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
SECTION A. DEFINITIONS'
1. Permit Issuing Authority
The Director of the Division of Water Quality.
2. DEM or "the Division"
Means the Division of Water Quality, Department of Environment, Health and Natural Resources.
3. EMC
Used herein means the North Carolina Environmental Management Commission.
4. Act or "the Act -'.-
The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended, 33 USC
1251, et. seq.
5. Mass/Dav Measurements
a. The "monthly average discharge" is defined as the total mass of all daily discharges sampled
and/or measured during a calendar month on which daily discharges are sampled and
measured, divided by the number of daily discharges sampled and/or measured during such
month. It is therefore, an arithmetic mean found by adding the weights of the pollutant found
each day of the month and then dividing this sum by the number of days the tests were
reported. The limitation is identified as "Monthly Average" in Part I of the permit.
b. The "weekly average discharge" is defined as the total mass of all daily discharges sampled
and/or measured during the calendar week (Sunday - Saturday) on which daily discharges are
sampled and measured, divided by the number of daily discharges sampled and/or measured
during such week. It is, therefore, an arithmetic mean found by adding the weights of
pollutants found each day of the week and then dividing this sum by the number of days the
tests were reported. This limitation is identified as "Weekly Average" in Part I of the permit.
c. The "maximum daily discharge" is the total mass (weight) of a pollutant discharged during a
calendar day. _If only one sample is taken during any calendar day the weight of pollutant
calculated from it is the "maximum daily discharge." This limitation is identified as "Daily
Maximum," in Part I of the permit.
d. The "average annual discharge" is defined as the total mass of all daily discharges sampled
and/or measured during the calendar year on which daily discharges are sampled and
measured, divided by the number of daily discharges sampled and/or measured during such
year. It is, therefore, an arithmetic mean found by adding the weights of pollutants found each
day of the year and then dividing this sum by the number of days the tests were reported. This
limitation is defined as "Annual Average" in Part I of the permit.

Part II
Page 2 of 14
6. Concentration Measurement
a. The "average monthly concentration," other than for fecal coliform bacteria, . is the sum of the
concentrations of all daily discharges sampled and/or measured during_ a calendar month on
which daily discharges are sampled and measured, divided by the number of daily discharges
sampled and/or measured during such month (arithmetic mean of the daily concentration
values). The daily concentration value is equal to the concentration of a composite sample or in
the case of grab samples is the arithmetic mean (weighted by flow value) of all the samples
collected during that calendar day. The average monthly count for fecal coliform bacteria is
the geometric mean of the counts for samples collected during a calendar month. This
limitation is identified as "Monthly Average" under "Other Limits" in Part I of the permit.
b. The "average weekly concentration," other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges sampled and/or measured during a calendar week
(Sunday/Saturday) on which daily discharges are sampled and measured divided by the
number of daily discharges sampled and/or measured during such week (arithmetic mean of the
daily concentration values). The daily concentration value is equal to the concentration of a
composite sample or in the case of grab samples is the arithmetic mean (weighted by flow
value) of all the samples collected during that .calendar day. The average weekly count for
fecal coliform bacteria is the geometric mean of the counts for samples collected during a
calendar week. This limitation is identified as "Weekly Average" under "Other Limits" in
Part I of the permit..
c. The "maximum daily concentration" is the concentration of a pollutant discharge during a
calendar day. If only one sample is taken during any calendar day the concentration of
pollutant calculated from it is the "Maximum Daily Concentration". It is identified as "Daily
Maximum" under "Other Limits" in Part I of the permit.
d. The "average annual concentration," other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges sampled and/or measured during a calendar year on
which daily discharges are sampled and measured divided by the, number of daily discharges
sampled and/or measured during such year (arithmetic mean of the daily concentration
values). The daily concentration value is equal to the concentration of a composite sample or in
the case of grab samples is the arithmetic mean (weighted by flow value) of all the samples
collected during that calendar day . The average yearly count for fecal coliform bacteria is the
geometric mean of the counts for samples collected during a calendar year. This limitation is
identified as "Annual Average" under "Other Limits" in Part I of the permit.
e. The "daily average concentration" (for dissolved oxygen) is the minimum allowable amount of
dissolved oxygen required to be available in the effluent prior to discharge averaged over a
calendar day. If only one dissolved oxygen sample is taken over a calendar day, the sample is
considered to be the "daily average concentration" for the discharge. It is identified as "daily
average" in the text of Part I.
f .. The "quarterly average concentration". is . the average of, all samples taken over a calendar
quarter. It is identified as "Quarterly Average Limitation" in the text of Part 1 of the permit.
g. A calendar quarter is defined as one of the following distinct periods. January through March,
April through June, July through September, and October through December.

Part II
Page 3 of 14
7. Other Measurements
a. Flow, (MGD): The flow limit expressed in this permit is the 24 hours average flow, averaged
monthly. It is determined as the arithmetic mean of the total daily flows recorded during the
calendar month.
b. An "instantaneous flow measurement" is a measure of flow taken at the time of sampling, when
both the sample and flow will be representative of the total discharge.
c. A "continuous flow measurement" is a measure of discharge flow from the facility which occurs
continually without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for
infrequent maintenance activities on the flow device.
8. Types of Samples
a. Composite Sample: A composite sample shall consist of:
(1) a series of grab samples collected at equal time intervals over a 24 hour period of discharge
and combined proportional to the rate of flow measured at the time of individual sample
collection, or
(2) a series of grab samples of equal volume collected over a 24 hour period with the time
intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow
recorder and totalizer, and the present gallon interval between sample collection fixed at
no greater than 1 /24 of the expected total daily flow at the treatment system, or
(3) a single, continuous sample collected over a 24 hour period proportional to the rate of flow.
In accordance with (1) above, the time interval between influent grab samples shall be no
greater than once per hour, and the time interval between effluent grab samples shall be no
greater than once per hour except at wastewater treatment systems having a detention time of
greater than 24 hours. In such cases, effluent grab samples may be collected at time intervals
evenly spaced over the 24 hour period which are equal in number of hours to the detention time
of the system in number of days. However, in no case may the time interval between effluent
grab samples be greater than six (6) hours nor the number of samples less than four (4) during a
24 hour sampling period.
b. Grab Sample: Grab samples are individual samples collected over a period of time not
exceeding 15 minutes; the grab sample can be taken manually. Grab samples must be
representative of the discharge or the receiving waters.
9. Calculation of Means
a Arithmetic Mean: The arithmetic mean of any set of values is the summation of the individual
values divided by the number of individual values.
b. Geometric Mean: The geometric mean of any set of values is the Nth root of the product of the
individual values where N is equal to the number of individual values. The geometric mean is
equivalent to the ant ilog of the arithmetic mean of the logarithms of the individual values.
For purposes of calculating the geometric mean, values of zero (0) shall be considered to be one
(1).
c. Weighted by Flow Value: Weighted by flow value means the summation of each concentration
times its respective flow divided by the summation of the respective flows.

Part II
Page 4 of 14
10. Calendar Day
A calendar day is defined as the period from midnight of one day until midnight of the next day.
However, for purposes of this per any consecutive 24-hour period that reasonably represents
the calendar day may be used for sampling.
11. Hazardous Substance
A hazardous substance means any substance designated under 40 CFR Part 116 pursuant to Section
311 of the Clean Water Act.
12. Toxic Pollutant
A toxic pollutant is any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
SECTION B. GENERAL CONDITIONS
1. Duty to Compiv
The permittee must comply with all conditions of this permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit renewal application.
a. The permittee shall comply with effluent standards or prohibitions established under section
307(a) of the Clean Water Act for toxic pollutants and with standards for sewage sludge use or
disposal established under section 405(d) of the Clean Water Act within the time provided in
the regulations that establish these standards or prohibitions or standards for sewage sludge
use or disposal, even if the permit has not yet been modified to incorporate the requiremgnt.
b. The Clean Water Act provides that any person who violates a permit condition is subject to a
civil penalty not to exceed $25,000 per day .for each violation. Any person who negligently
violates any permit condition is subject to criminal penalties'of $2,500 to $25,000 per day of
violation, or imprisonment for not more than 1 year, or both. Any person who knowingly
violates permit conditions is subject to criminal penalties of $5,000 to $50,000 per day of
violation, or imprisonment for not more than 3 years, or both. Also,_any person who violates a
permit condition may be assessed an administrative penalty not to exceed $10,000 per violation
with the maximum amount not to 'exceed $125,000. [Ref: Section 309 of the Federal Act 33
U.S.C. 1319 and 40 CFR 122.41 (a)]
c. Under state law, a civil penalty of not more than ten thousand dollars ($10,000) per violation
- may be assessed against any person who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit. [Ref: North Carolina General Statutes § 143-215.6A]
d. Any person may be assessed an administrative penalty by the Administrator for violating
section 301, 302, 306, 307, 308, 318, or 405 of the Act, 'or any permit condition or limitation
implementing any of such sections in a permit issued under section 402 of the Act.
Administrative penalties for Class l violations are not to exceed $10,000 per violation, with
the maximum amount of any Class I penalty assessed not to exceed $25,000: Penalties for Class
II violations are not to exceed $10,000 per day for each day during which the violation
continues, with the maximum amount of any Class 11 penalty not to exceed $125,0M.

Part II
Page 5 of 14
2. Duty to Mitigate
The permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or
disposal in violation of this permit which has a reasonable likelihood of adversely affecting
human health or the environment.
3. Civil and Criminal Liability
Except as provided in permit conditions on 'Bypassing" (Part II, C-4) and 'Tower Failures" (Part III
C-7), nothing in this permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309 of
the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for consequential damages,
such as fish kills, even though the responsibility for effective compliance may be temporarily
suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities, or penalties to which the permittee is or may
be subject to under NCGS 143-215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321.
Furthermore, the permittee is responsible for consequential damages, such as fish kills, even
though the responsibility for effective compliance may be temporarily suspended.
5. Property Rights
The issuance of this permit does not convey any property rights in either real or personal property,
or any exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights, nor any infringement of Federal, State or local laws or regulations.
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical
structures or facilities or the undertaking of any work in any navigable waters.
7. Severability
The provisions of this permit are severable, and if any provision of this permit, or the application
of any provision of this permit to any circumstances, is held invalid, the application of such
provision to other circumstances, and the remainder of this permit, shall not be affected thereby.
8. Duty to Provide Information
The permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any
information which the Permit Issuing Authority may request to determine whether cause exists for
modifying, revoking and reissuing, or terminating this permit or to determine compliance with this
permit. The permittee shall also furnish to the Permit Issuing Authority upon request, copies of
records required to be kept by this permit.
9. Duty to Reapply
If the permittee wishes to continue an activity regulated by this permit after the expiration date of
this permit, the permittee must apply for and obtain a new permit.

Pan II
Page 6 of 14
10. Expiration of Permit
The permittee is not authorized to discharge after the expiration date. In order to receive
automatic authorization to discharge beyond the expiration date, the permittee shall submit such
information, forms, and fees as are required by the agency authorized to issue permits no later than
180 days prior to the expiration date. Any permittee that has not requested renewal at least 180
days prior to expiration, or any permittee that does not have a permit after the expiration and has
not requested renewal at least 180 days prior to expiration, will subject the permittee to enforcement
procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed
and certified.
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a
responsible corporate officer means: (a) a president, secretary, treasurer or vice president
of the corporation in charge of a principal business function, or any other person who
performs similar policy or decision making functions for the corporation, or (b) the manager
of one or more manufacturing production or operating facilities employing more than 250
persons or having gross annual sales or expenditures exceeding 25 million (in second quarter
1980 dollars), if authority to sign documents has been assigned or delegated to the manager
in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive
officer or ranking elected official.
b. All reports required by the permit and other information requested by the Permit Issuing
Authority shall be signed by a person described above or by a duly authorized representative of
that person. A person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or apposition having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
responsibility, or an individual or position having overall responsibility for environmental
matters for the company. (A duly authorized representative may thus be either a named
individual or any individual occupying a named position.); and
(3) The written authorizationis submitted to the Permit Issuing Authority.
c. Certification. Any person signing a document under paragraphs a. or b. of this section shall
make the following certification:
"I certify, under penalty of law; that this document and all attachments were prepared .under
my direction or supervision in accordance with a system designed to 'assure that qualified
personnel properly gather and evaluate the information submitted.' Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering
the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."

Pan II
Page 7 of 14
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request
by the permittee for a permit modification, revocation and reissuance, or termination, or a
notification of planned changes or anticipated noncompliance does not stay any permit condition.
13. Permit Modification Revocation and Reissuance, or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and
modifying the permit, revoking and reissuing the permit, or terminating the permit as allowed by
the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122 and
123; Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North
Carolina General Statute 143-215.1 et. al.
14. Previous Permits
All previous National Pollutant Discharge Elimination System Permits issued to this facility,
whether for operation or discharge, are hereby revoked by issuance of this permit. IThe exclusive
authority to operate this facility arises under this permit. The authority to operate the facility
under previously issued permits bearing this number is no longer effective. I The conditions,
requirements, terms, and provisions of this permit authorizing discharge under the National
Pollutant Discharge Elimination System govern discharges from this facility.
SECTION C. OPERATION AND MAINTENANCE OF POLLUTION CONTROLS
1. Certified Operator
Pursuant to Chapter 90A-44 of North Carolina General Statutes, and upon classification of the
facility by the Certification Commission, the permittee shall employ a certified wastewater
treatment plant operator in responsible charge (ORC) of the wastewater treatment facilities. Such
operator must hold a certification of the grade equivalent to or greater than the classification
assigned to the wastewater treatment facilities by the Certification Commission. The pem-dttee
must also employ a certified back-up operator of the appropriate type and any grade to comply
with the conditions of Title 15A, Chapter 8A .0202. The ORC of the facility must visit each Class I
facility at least weekly and each Class II, III, and IV facility at least daily, excluding weekends
and holidays, and must properly manage and document daily operation and maintenance of the
facility and must comply with all other conditions of Title 15A, Chapter 8A .0202. Once the
facility is classified, the permittee shall submit a letter to the Certification Commission which
designates the operator in responsible charge within thirty days after the wastewater treatment
facilities are 50%,complete.
2. Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of
treatment and control (and related appurtenances) which are installed or used by the permittee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also
includes adequate laboratory controls and appropriate quality assurance procedures. This provision
requires the operation of back-up or auxiliary facilities or similar systems which are installed by a
permittee only when the operation is necessary to achieve compliance with the conditions of the
permit.

Part II
Page 8 of 14
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary
to halt or reduce the permitted activity in order to maintain compliance with the condition of this
permit.
4. Bypassing of Treatment Facilities
a. Definitions
(1) 'Bypass" means the known diversion of waste streams from any portion of a treatment
facility including the collection system, which is not a designed or established or operating
mode for the facility.
(2) "Severe property damage" means substantial physical damage to property, damage to the
treatment facilities which causes them to become inoperable, or substantial and permanent
loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage does not mean economic loss caused by delays in
production.
b. Bypass not exceeding limitations.
The permittee may allow any bypass to occur which does not cause effluent limitations to be
exceeded, but only if it also is for essential maintenance to assure efficient operation. These
bypasses are not subject to the provisions of Paragraphs c. and d. of this section.
c. Notice
(1) Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall
submit prior notice, if possible at least ten days before the date of the bypass; including an
evaluation of the anticipated quality and affect of the bypass.
(2) Unanticipated bypass. The permittee shall submit notice of an unanticipated bypass as
required in Part II, E. 6. of this permit: (24 hour notice).
d. Prohibition of Bypass
(1) Bypass is prohibited and the Permit Issuing Authority may take enforcement action against
. a permittee for bypass, unless:
(A) Bypass was unavoidable to prevent loss of life, personal injury or severe property
damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment
facilities, retention of untreated_ wastes or maintenance during normal periods of
equipment downtime. This condition is not satisfied if adequate backup equipment should
have been installed in the exercise of reasonable engineering judgment to prevent a bypass
which occurred during normal periods of equipment downtime or preventive maintenance;
and
(C) The permittee submitted notices as required under Paragraph c. of this section.
(2) The Permit Issuing Authority may approve an anticipated bypass, after considering its
adverse affects, if the Permit Issuing Authority determines that it will meet the three
conditions listed above in Paragraph d. (1) of this section.

Part II
Page 9 of 14
5. Upsets
a. Definition.
"Upset " means an exceptional incident in which there is unintentional and temporary
noncompliance .with technology based permit effluent limitations because of factors beyond the
reasonable control of the permittee. An upset does not include noncompliance to the extent
caused by operational error, improperly designed treatment facilities, inadequate treatment
facilities, lack of preventive maintenance, or careless or improper operation.
b. Effect of an upset.
An upset constitutes an affirmative defense to an action brought for noncompliance with such
technology based permit effluent limitations if the requirements of paragraph c. of this
condition are met. No determination made during administrative review of claims that
noncompliance was caused by upset, and before an action for noncompliance, is final
administrative action subject to judicial review.
c. Conditions necessary for a demonstration of upset
A permittee who wishes to establish the affirmative defense of upset shall demonstrate,
through properly signed, contemporaneous operating logs, or other relevant evidence that:
(1) An upset occurred and that the permittee can identify the cause(s) of the upset;
(2) The permittee facility was at the time being properly operated; and
(3) The permittee submitted notice of the upset as required in Part II, E. 6. (b) (B) of this permit.
(4) The permittee complied with any remedial measures required under Part I1, B. 2. of this
permit.
d. Burden of proof.
In any enforcement proceeding the permittee seeking to establish the occurrence of an upset has
the burden of proof.
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of
wastewaters shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such
as to prevent any pollutant from such materials from entering waters of the State or navigable
waters of the United States. The permittee shall comply with all existing federal regulations
governing the disposal of sewage sludge. Upon promulgation of 40 CFR Part 503, any permit issued
by the Permit Issuing Authority for the utilization/disposal of sludge may be reopened and
modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR Part 503. The
permittee shall comply with applicable 40 CFR Part 503 Standards for the .Use and Disposal of
Sewage Sludge (when promulgated) within the time provided in the regulation, even if the permit
is not modified to incorporate the requirement. The permittee shall notify the Permit Issuing
Authority of any significant change in its sludge use or disposal practices.
7. Power Failures
The permittee is responsible for maintaining adequate safeguards as required by DEM Regulation,
Title 15A, North Carolina Administrative Code, Subchapter 2H, .0124 Reliability, to prevent the
discharge of untreated or inadequately treated wastes during electrical power -failures either by
means of alternate power sources, standby generators or retention of inadequately treated effluent.

Part II
Page 10 of 14
SECTION D. MONITORING AND RECORDS
1. Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the
volume and nature of the permitted discharge. Samples collected at a frequency less than daily
shall be taken on a day and time that is characteristic of the discharge over .the entire period
which the sample represents. All samples shall be taken at the monitoring points specified in this
permit and, unless otherwise specified, before the effluent joins or is diluted by any other
wastestream, body of water, or substance. Monitoring points shall . not be changed without
notification to and the approval of the Permit Issuing Authority.
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each month and
reported on a,monthly Discharge Monitoring Report (DMR) Form (DEM No. MR 1, 1.1, 2, 3) or
alternative forms approved by the Director,. DEM, postmarked no later than the 30th day
following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case
of a new facility, on the last day of the month following the commencement of discharge.
Duplicate signed copies of these, and all other reports required herein, shall be submitted to the
following address:
Division of Water Quality
Water Quality Section
ATTENTION: Central Files
Post Office Box 29535
Raleigh, North Carolina 27626-0535
3. Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific practices
shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges. The devices shall be installed, calibrated and maintained to ensure that the
accuracy of the measurements are consistent with the accepted capability of that type of device.
Devices selected shall be capable of measuring flows with a maximum deviation of less than + 10%
from the true discharge rates throughout the range of expected discharge volumes. Once -through
condenser cooling water flow which is monitored by pump logs, or pump hour meters as specified in
Part I of this permit and based on the manufacturer's pump curves shall not be subject to this
requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published
pursuant to NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations
published pursuant to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as
Amended, and Regulation 40 CFR 136; or in the case of sludge use or disposal, approved under 40
CFR 136, unless otherwise specified in 40 CFR 503, unless other test procedures have been specified
in this permit.
To meet the intent of the monitoring required by this permit, all test procedures must produce
minimum detection and reporting levels that are below the permit discharge requirements and all
data generated must. be reported down to the minimum detection or lower reporting level of the
procedure. If no approved methods are determined capable of achieving minimum detection and

Part lI
Page 11 of 14
reporting levels below permit discharge requirements, then the most sensitive (method with the
lowest possible detection and reporting level) approved method must be used.
5. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders
inaccurate, any monitoring device or method required to be maintained under this permit shall,
upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for
not more than two years per violation, or by both. If a conviction of a person is for a violation
committed after a first conviction of such person under this paragraph, punishment is a fine of not
more than $20,000 per day of violation, or by imprisonment of not more than 4 years, or both.
6. Records Retention
Except for records of monitoring information required by this permit related to the permittee's
sewage sludge use and disposal activities, which shall be retained for a period of at least five
years (or longer as required by 40 CFR 503), the permittee shall retain records of all monitoring
information, including all calibration and maintenance records and all original strip chart
recordings for continuous monitoring instrumentation, copies of all reports required by this permit,
for a period of at least 3 years from the date of the sample, measurement, report or application.
This period may be extended by request of the Director at any time.
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the permittee
shall record the following information:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f . The results of such analyses.
8. Inspection and Entry
The permittee shall allow the Director, or an authorized representative (including an authorized
contractor acting as a representative of the Director), upon the presentation of credentials and other
documents as may be required by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or
conducted, or where records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions
of this permit;
C. Inspect at reasonable times any facilities, equipment (including monitoring and control
equipment), practices, or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as
otherwise authorized by the Clean Water Act, any substances or parameters at any location.

Part II
Page 12 of 14
SECTION E. REPORTING REQUIREMENTS
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit.
The discharge of any pollutant identified in this permit more frequently than or at a level in excess
of that authorized shall constitute a violation of the permit.
2. Planned Changes
The permittee shall give notice to the Director as soon as possible of any planned physical
alterations or additions to the permitted facility. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for determining
whether a facility is a new source in 40 CFR Part 122.29 (b); or
b. The alteration or addition could significantly change the nature or increase the quantity of
pollutants discharged. This notification applies to pollutants which are subject neither to
effluent limitations in the permit, nor to notification requirements under 40 CFR Part 122.42 (a)
(1).
c. The alteration or addition results in a significant change in the permittee's sludge use or
disposal practices, and such alternation, addition or change may justify the application of
permit conditions that are different from or absent in the existing permit, including notification
of additional use or disposal sites not reported during the permit application process or not
reported pursuant to an approved land application plan.
3. Anticipated Noncompliance
The permittee shall give advance notice to the Director of any planned changes in the permitted
facility or activity which may result in noncompliance with permit requirements.
4. Transfers
This permit is not transferable to any person except after notice to the Director. The Director may
require modification or revocation and reissuance of the permittee and incorporate such other
.requirements as may be necessary under the Clean Water Act.
5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit.
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part 11. D. 2
of this permit)'or forms provided by the Director for reporting results of monitoring of sludge use
or disposal practices.
b. If the permittee monitors any pollutant more frequently than required by the permit, using test
procedures specified in Part II, D. 4. of this permit or in the case of sludge use or disposal,
approved under 40 CFR 503, or as specified in this permit, the results of this monitoring shall be
included in the calculation and reporting of the data submitted in the DMR.
c. Calculations for all limitations which require averaging of measurements shall utilize an
arithmetic mean unless otherwise specified by the Director in the permit.

Part II
Page 13 of 14
6. Twenty-four Hour Reporting
a- The permittee shall report to the central office or the appropriate regional office any
noncompliance which may endanger health or the environment. Any information shall be
provided orally within 24 hours from the time the permittee became aware of the
circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances. The written submission shall contain a
description of the noncompliance, and its cause; the period of noncompliance, including exact
dates and times, and if the noncompliance has not been corrected, the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence
of the noncompliance.
b. The following shall be included as information which must be reported within 24 hours under
this paragraph:
(1) Any unanticipated bypass which exceeds any effluent limitation in the permit.
(2) Any upset which exceeds any effluent limitation in the permit.
(3) Violation of a maximum daily discharge limitation for any of the pollutants listed by the
Director in the permit to be reported within 24 hours.
c. The Director may waive the written report on a case -by -case basis for reports under paragraph
b. above of this condition if the oral report has been received within 24 hours.
7. Other Noncompliance
The permittee shall report all instances of noncompliance not reported under Part II. E. 5 and 6. of
this permit at the time monitoring reports are submitted. The reports shall contain the information
listed in Part II. E. 6. of this permit.
8. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in a permit
application, or submitted incorrect information in a permit application or in any report to the
Director, it shall promptly submit such facts or information.
9. Noncompliance Notification
The permittee shall report by telephone to either the central office or the appropriate regional
office of the Division as soon as possible, but in no case more than 24 hours or on the next working
day following the occurrence or first knowledge of the occurrence'of any of the following:
a. Any occurrence at the water pollution control facility which results in the discharge of
significant amounts of wastes which are abnormal in quantity or characteristic, such as the
dumping of the contents of a sludge digester; the known passage of a slug of hazardous substance
through the facility; or any other unusual circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of
adequate wastewater treatment such as mechanical or electrical failures of pumps, aerators,
compressors, etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass
directly to receiving waters without treatment of all or any portion of the influent to such
station or facility.

Pan II
Page 14 of 14
Persons reporting such occurrences by telephone shall also file a written report in letter form within
5 days following first knowledge of the occurrence.
10. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the
Federal Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for
public inspection at the offices of the Division of Water Quality. As required by the Act, effluent
data shall not be considered confidential. Knowingly making any false statement on any such
report may result in the imposition of criminal penalties as provided for in NCGS 143-215.1(b)(2) or
in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement,
representation, or certification in any record or other .document submitted or required to be
maintained under this permit, including monitoring reports or reports of compliance or
noncompliance shall, upon conviction, be punished by a fine of not more than $10,000 per violation,
or by imprisonment for not more than two years per violation, or by both.

PART III
OTHER REQUIREMENTS
A. Construction
No construction of wastewater treatment facilities or additions to add to the plant's treatment
capacity or to change the type of process utilized at the treatment plant shall be begun until Final
Plans and Specifications have been submitted to the Division of Water Quality and written approval
and Authorization to Construct has been issued.
B. Groundwater Monitoring
The permittee shall, upon written notice from the Director of the Division of Water Quality, conduct
groundwater monitoring as may be required to determine the compliance of this NPDES permitted
facility with the current groundwater standards.
C. Changes in Discharges of Toxic Substances
The permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe:
a.That any activity has occurred or will occur which would result in the discharge, on a routine or
frequent basis, of any toxic pollutant which is not limited in the permit, if that discharge will
exceed the highest of the following "notification levels';
(1) One hundred micrograms per liter (100 ug/1);
(2)Two hundred micrograms per liter (200 ug/1) for acrolein and acrylonitrile; five hundred
micrograms per liter (500 ug/1) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol; and
one milligram per liter (1 mg/1) for antimony;
(3) Five (5) times the maximum concentration value reported for that pollutant in the permit
application.
b. That any activity has occurred or will occur which would result in any discharge, on a non -routine
or infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will
exceed the highest of the following "notification levels';
(1) Five hundred micrograms per liter (500 ug/1);
(2) One milligram per liter (I mg/1) for antimony;
(3) Ten (10) times the maximum concentration value reported for that pollutant in the permit
application.
D. Requirement to Continually Evaluate Alternatives to Wastewater Discharges
The permittee shall continually evaluate all wastewater disposal alternatives and pursue the most
environmentally sound alternative of the reasonably cost effective alternatives. If the facility is in
substantial non-compliance with the terms and conditions of the NPDES permit or governing rules,
regulations or laws, the permittee shall submit a report in such form and detail as required by the
Division evaluating these alternatives and a plan of action within sixty (60) days of notification by the
Division.

PART IV
ANNUAL ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
A. The permittee must pay the annual administering and compliance monitoring fee
within 30 (thirty) days after being billed by the Division. Failure to pay the fee in
a timely manner in accordance with 15A NCAC 2H .0105(b)(4) may cause this
Division to initiate action to revoke the permit.

To: -Permits and Engineering Unit
Water Quality Section
Attention: Mark McIntyre
SOC Priority Project: No
Date: August 10, 1998
NPDES STAFF REPORT AND RECOMMENDATION
MRO No.: 98-50
County: Cleveland
Permit No. NC0004685
1. Facility and Address: PPG Industries, Inc.
940 Washburn Switch Road
Shelby, North Carolina 28150
2. Date of Investigation: August 6, 1998
3. Report Prepared by: Michael L. Parker, Environmental Engineer H
4. Persons Contacted and Telephone Number: Lacy Ballard, [phone], ext. 544.
5. Directions to Site: From the intersection of US Hwy 74 and SR ,1313 (Washburn Switch Road)
just west of the City of Shelby, travel north on SR 1313 approximately 3.0 miles. The PPG plant
is located on the left side of the road.
6. Discharge Point(s), List for all discharge points:
001:
Latitude: 35° 20' 43" Longitude: 81° 37' 02"
002:
Latitude: -35° 19' 28" Longitude: 81° 37' 51"
Attach a USGS map extract and indicate treatment facility site and discharge point on map.
WWTP:
U.S.G.S. Quad No.: F12SW
U.S.G.S. Quad Name: Boiling Springs North, NC
Discharge Point:
U.S.G.S. Quad No.: F12SE U.S.G.S. Quad Name: Shelby, NC
7. Site size and expansion area consistent with application? Yes. There is ample area for additional
WWTP construction, if necessary.

PPP1
Fr,
Page Two
Topography (relationship to flood plain included): Flat to moderate slopes; the WWTP is not
located within the 100 year flood plain.
9. Location of nearest dwelling: None within 500 feet.
10. Receiving stream or affected surface waters: Brushy Creek
a. Classification: C
b. River Basin and Subbasin No.: Broad 030804
C. Describe receiving stream features and pertinent downstream uses: Receiving stream is
of moderate size (15-25 feet wide) with a sandy bottom. General "C" classification uses
downstream.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
a. Volume of wastewater to be permitted: 1.3 MGD (ultimate design capacity)
b. Current permitted capacity of the wastewater treatment facility: 1.3 MGD
Actual treatment capacity of the current facility (current design capacity): 1.3 MGD
d. Date(s) and construction activities allowed by previous Authorizations to Construct
issued in the previous two years: N/A
Please provide a description of existing or substantially constructed wastewater treatment
facilities: Existing treatment facilities consists of influent screening, lime addition, surge
tank, equalization tank, flash tank with aluminum chloride addition, polymer addition,
primary clarification, aeration basins with diffused air, secondary clarifiers with ferric
chloride addition, tertiary filters, chlorine contact tank (no chlorine is added at this time),
traveling bridge sand filter, defoamer addition, gravity sludge thickener, belt filter press,
and an overflow lagoon. Stand-by power is provided for the industrial process and the
WWTP through on -site generators. Since the Permit was last issued, the permittee has
received approval from the Division to use of bentonite clay for effluent toxicity
reduction and the addition of aluminum chloride as a reactant for flouride removal,
chemical precipitation, and floc formation.
f. Please provide a description of proposed wastewater treatment facilities: N/A
g. Possible toxic impacts to surface waters: In the past few years, this facility has had
difficulty passing it's toxicity tests. As a result, PPG entered into an SOC (96-24), which
contained a compliance schedule that required full compliance with final effluent
limitations by June 30, 1998. The SOC is due to expire on September 30, 1998.
Information contained in the files of this office indicates that compliance has been
achieved.
h. Pretreatment Program (POTWs only): N/A

Fp7r,
I
Page Three
2. Residuals handling and utilization/disposal scheme: Residuals are currently landfilled at the
Cleveland Container Company private landfill. PPG has a non -discharge permit for the land
application of residuals (WQ0001055), however, no residuals have ever been applied.
3. Treatment plant classification: Class IV (no change from previous rating)
4. SIC Code(s): 3229 (PPG), 3083 (Azdel)
Wastewater Code(s) Primary: 64 Secondary: 02, 73, 15, 14, 36
Main Treatment Unit Code: 01602
PART III - OTHER PERTINENT INFORMATION
l . Is this facility being constructed with Construction Grant Funds or are any public monies involved
(municipals only)? No public monies involved.
2.. Special monitoring or limitations (including toxicity) requests: None at this time.
I Important SOC, JOC or Compliance Schedule dates: PPG has met all SOC compliance dates.
4. Alternative Analysis Evaluation:
Spray Irrigation: N/A
Connection to Regional Sewer System: There is none presently available.
Subsurface: N/A
5. Air quality and/or groundwater concerns or hazardous materials utilized at this facility that may
impact water quality, air quality, or groundwater: No GW concerns at this time. The facility has
obtained the necessary air quality permits. There are no known hazardous materials concerns.
PART IV - EVALUATION AND RECOMMENDATIONS
The permittee, PPG Industries, Inc., has applied for permit renewal. The WWTP serves the
industrial and domestic needs for PPG and a nearby company; Azdel, Inc.. Azdel is located on the PPG
property and uses the fiberglass produced at PPG in part of their industrial process.
Outfall 001 is the outfall from the WWTP that treats the industrial, domestic, some of the
stormwater from the two sites, and at this time all non -contact cooling wastewater. Outfall 002 consists
of non -contact cooling water and stormwater.

pp!r�
I
Page Four
Based on the WWT facilities that are available, PPG should be able to continue to meet the
existing and proposed permit effluent limitations, provided there are no significant changes.
It is recommended that the permit be renewed as requested.
Signature of report preparer Date
Water Quali ' egional Superv6 Date
h:\dsr\dsr98\ppg.sr

PPP1
SOC Priority Project: No
To: Permits and Engineering Unit
Water Quality Section
Attention: Mark Mclnoxe
Date: August 10, 1998
NPDES STAFF REPORT AND RECOMMENDATION
MRO No.: 98-50
County: Cleveland
Permit No. NC0004685
PART I - GENERAL INFORMATION
1. Facility and Address: PPG Industries, Inc.
940 Washburn Switch Road
Shelby, North Carolina 28150
2. Date of Investigation: August 6, 1998
3. Report Prepared by: Michael L. Parker, Environmental Engineer H
4. Persons Contacted and Telephone Number: Lacy Ballard, [phone], ext. 544.
5. Directions to Site: From the intersection of US Hwy 74 and SR 1313 (Washburn Switch Road)
just west of the City of Shelby, travel north on SR 1313 approximately 3.0 miles. The PPG plant
is located on the left side of the road.
6. Discharge Point(s), List for all discharge points:
001:
Latitude: 35' 20' 43" Longitude: 81' 3702"
002:
Latitude: 35' 19' 28" Longitude: 81' 3751"
Attach a USGS map extract and indicate treatment facility site and discharge point on map.
WWTP:
U.S.G.S. Quad No.: F12SW
U.S.G.S. Quad Name: Boiling Springs North, NC
Discharge Point:
U.S.G.S. Quad No.: F12SE U.S.G.S. Quad Name: Shelby, NC
7. Site size and expansion area consistent with application? Yes. There is ample area for additional
WWTP construction, if necessary.

PFFIF,
Page Two
8. Topography (relationship to flood plain included): Flat to moderate slopes; the WWTP is not
located within the 100 year flood plain.
9. Location of nearest dwelling: None within 500 feet.
10. Receiving stream or affected surface waters: Brushy Creek
a. Classification: C
b. River Basin and Subbasin No.: Broad 030804
Describe receiving stream features and pertinent downstream uses: Receiving stream is
of moderate size (15-25 feet wide) with a sandy bottom. General "C" classification uses
downstream.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
1. a. Volume of wastewater to be permitted: 1.3 MGD (ultimate design capacity)
b. Current permitted capacity of the wastewater treatment facility: 1.3 MGD
C. Actual treatment capacity of the current facility (current design capacity): 1.3 MGD
d. Date(s) and construction activities allowed by previous Authorizations to Construct
issued in the previous two years: N/A
e. Please provide a description of existing or substantially constructed wastewater treatment
facilities: Existing treatment facilities consists of influent screening, lime addition, surge
tank, equalization tank, flash tank with aluminum chloride addition, polymer addition,
primary clarification, aeration basins with diffused air, secondary clarifiers with ferric
chloride addition, tertiary filters, chlorine contact tank (no chlorine is added at this time),
traveling bridge sand filter, defoamer addition, gravity sludge thickener, belt filter press,
and an overflow lagoon. Stand-by power is provided for the industrial process and the
WWTP through on -site generators. Since the Permit was last issued, the permittee has
received approval from the Division to use of bentonite clay for effluent toxicity
reduction and the addition of aluminum chloride as a reactant for flouride removal,
chemical precipitation, and floc formation.
f. Please provide a description of proposed wastewater treatment facilities: N/A
g. Possible toxic impacts to surface waters: In the past few years, this facility has had
difficulty passing it's toxicity tests. As a result, PPG entered into an SOC (96-24), which
contained a compliance schedule that required full compliance with final effluent
limitations by June 30, 1998. The SOC is due to expire on September 30, 1998.
Information contained in the files of this office indicates that compliance has been
achieved.
h. Pretreatment Program (POTWs only): N/A

pppplp"' I
Page Three
2. Residuals handling and utilization/disposal scheme: Residuals are currently landfilled at the
Cleveland Container Company private landfill. PPG has a non -discharge permit for the land
application of residuals (WQ0001055), however, no residuals have ever been applied.
3. Treatment plant classification: Class IV (no change from previous rating)
4. SIC Code(s): 3229 (PPG), 3083 (Azdel)
Wastewater Code(s) Primary: 64 Secondary: 02, 73, 15, 14, 36
Main Treatment Unit Code: 01602
PART III - OTHER PERTINENT INFORMATION
1. Is this facility being constructed with Construction Grant Funds or are any public monies involved
(municipals only)? No public monies involved.
2.. Special monitoring or limitations (including toxicity) requests: None at this time.
3. Important SOC, JOC or Compliance Schedule dates: PPG has met all SOC compliance dates.
4. Alternative Analysis Evaluation:
Spray Irrigation: N/A
Connection to Regional Sewer System: There is none presently available.
Subsurface: N/A
5. Air quality and/or groundwater concerns or hazardous materials utilized at this facility that may
impact water quality, air quality, or groundwater: No GW concerns at this time. The facility has
obtained the necessary air quality permits. There are no known hazardous materials concerns.
PART IV - EVALUATION AND RECOMMENDATIONS
The permittee, PPG Industries, Inc., has applied for permit renewal. The WWTP serves the
industrial and domestic needs for PPG and a nearby company; Azdel, Inc.. Azdel is located on the PPG
property and uses the fiberglass produced at PPG in part of their industrial process.
Outfall 001 is the outfall from the WWTP that treats the industrial, domestic, some of the
stormwater from the two sites, and at this time all non -contact cooling wastewater. Outfall 002 consists
of non -contact cooling water and stormwater.

PPPP'P" I
Page Four
Based on the WWT facilities that are available, PPG should be able to continue to meet the
existing and proposed permit effluent limitations, provided there are no significant changes.
It is recommended that the permit be renewed as requested.
'g e�� -- I �el
Signature of report preparer Date
Water Quah ' egional Supervi Date
h:\dsr\dsr98\ppg.sr

" State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. Lacy Ballard
PPG Industries
940 Washburn Switch Road
Shelby, North Carolina ' 28150
Dear Mr. Ballard:
�U
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
July 6, 1998 MC. Dll&?!. G_V
�!-I� E;q' :A.f:17,B;
iJU i:Ci %3
JUL 10 1998
09020 OF Ejlgj'atl, Eff1
Subject: NPDES Permit Renewal Application
Permit NC0004685
PPG Industries - Shelby
Cleveland County
The Division received your permit renewal application and renewal fee of $300.00 (paid by
check #0003733028) on July 6, 1998. Thank you for submitting this package in a timely fashion.
. The permit renewal for this facility has been assigned to Mark McIntire of the NPDES Unit.
Mr. McIntire will contact you if further information is needed to complete the permit renewal. If
you have any additional questions concerning renewal of the subject permit, please contact Mr.
McIntire at [phone], extension 553.
Sincerely,
Charles H. Weaver, Jr.
NPDES Unit
cc: Central Files
'ooresville Regional Officce, Water Qualty'Section
NPDES File
P.O. Box 29535, Raleigh, North Carolina 27626-0535 919 733-5083, extension 511 (fax) 919 733-0719
An Equal Opportunity Affirmative Action Employer [e-mail]

J
PPG Industries, 940 Washburn Switch Road, Shelby, N.C. 28150
July 2, 1998
Lacy Ballard, R. E. M.
Staff Engineer, Environmental
Fiber Glass Products
Mr. Charles H. Weaver, Jr.
N.C. DENR/DWQ/NPDES
P.O. Box 29535
Raleigh, North Carolina 27626-0535
Subject: Permit renewal
NC0004685
Dear Mr. Weaver:
704-434-2261
Extension 544
[e-mail]
The Shelby plant of PPG Industries request renewal of the NPDES discharge permit
number NC0004685. Enclosed are the application forms, sludge management
description, signature authorization, and maps, along with the $300 fee.
The major changes in treatment plant operation/facility since the last permit application
is the addition of aluminum chloride as a reactant to remove fluoride and the use of
bentonite clay for the removal of effluent toxicity. Attached is a listing of the changes
and a suggested description of the facility.
If additional information is needed, please give me a call.
Sincerely,
Lacy Ballard
cc: M. LeCroy
H. Blackwell
W.Schenck

Changes from previous permit application:
1. the addition of aluminum chloride and coagulants in the primary chemical treatment
system for the removal of fluoride and for chemical precipitation and floc formation
2. the use of bentonite clay as an additive to the biological system for effluent toxicity
removal
3. the replacement of four sand filters with one traveling bridge filter
Suggested descriptive paragraph:
Continue to discharge non -contact cooling water and stormwater from outfall 002 into
Overflow Branch which is classified Class C waters in the Broad River Basin, and
continue to discharge process water, stormwater, sanitary sewage, cooling water, and
landfill leachate from outfall 001 from the existing wastewater treatment facility consisting
of an overflow/storage basin, bar screen and grinder, an influent wet will with lime
addition, influent pumps, a surge tank, an equalization tank, a flash mix tank with
aluminum chloride, coagulant and polymer addition, two primary clarifiers, two aeration
basins, with bentonite clay addition, a splitter box and floc tank, three secondary clarifiers
with ferric chloride addition, a sand filter, a chlorine contact basin, a sludge thickener tank,
and a sludge belt press located at Shelby Facility, on NCSR 1313, west of Shelby,
Cleveland County.

NORTH CAROLINA DEPT. OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
ENVIRONMENTAL MANAGEMENT COMMISSION
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
STANDARD FORM C - MANUFACTURING AND COMMERCIAL
SECTION 1. APPLICATION AND FACILITY DESCRIPTION
Unless otherwise specified on this form ell hems are to be completed. B an hem is not applicable indicate 'NA'.
ADDITIONAL INSTRUCTIONS FOR SELECTED ITEMS APPEAR IN SEPARATE INSTRUCTION BOOKLETAS INDICATED. REFERTO BOOKLET
BEFORE FILLING OUT THESE ITEMS.
1.
Legal Name of Applicant
101
(see instructions)
2
Mailing Address of Applicant
(see Instructions)
Number & Street
102a
City
102b
state
102c
Zp Code
102d
a
AppBranrs Authorized Agent
(see Instructions)
Name and Tide
103a
Number & Street
103b
City
103C
Ste-
103d
Zip Code'
103a
Telephone
103f
4.
Previous Application
If a previous application for a
permit under the National
Pollutant Discharge Elimination
System has been made, give
the date of application.
104
Please Pant or Type
PPG Industires, Inc.
940 Washburn Switch Road
Shelby
North Carolina
28150
Lacy Ballard
Staff Engineer
940 Washburn Switch Road
o,Shelby, t
-
North Carolina
28150
704' 434-2261
Area Number
Code
93 .8 4
Y R MO DAY
I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete,
and ac✓Jrate.
Lacy Ballard 102e Staff Engineer
Printed Name of Person Signing Title
ton 98 6 30
Signature f Apo[Zafit or Authorized Agent YR MO DAY
Date Application Signed
North Carolina General statue 143-215.6 (bj(2) provides that Any person who knowingy makes any false statement representation, or certification in any
application, record report plan, or other doaunent files a required m be maintained under Amide 21 or regulations of the Envirorxr►ental Management
Commission implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate ary recordng or monitoring device or method required
m be operated or maintained under Article 21 or regulations of the Environmental Management Commission implementing that Artfde, shall be guilty of a
misdemeanor punishable by a fine oat fo exceed 510,000, or by imprisonment not to exceed six months, or by both. (1 S U.S.C. Section 1001 provdes a
punishment by a fate or not more than $10,000 or imprisonment not more than 5 years, or both, for a similar offense.)
0

FOR AGENG
Facility (see instructions)
Give e narne, ownership, and
physical location of the plant or
other operating facility where
dscharge(s) presently occur(s)
or will occur.
Name
105a
PPG Industries, Inc.
Ownership (Public, Private
or both Pubic and Private)
105b
PUS gPRV BPP
Check block if a Federal
facility
1050
FED
and give GSA Inventory
Control Number
105d
Location:
Number & Street
10Ee
940 Washburn Switch Road
city
icsf
Shelby
Cointy
10eg
Cleveland
State
10Eh
North Carolina
6. Nature of Business State the nature
106a
Fiber glass manufacturing
of the business conducted at the
plant or operating facility.
10Eb
AGENCY USE
7. Facility Intake Water (see
ons) Indicate water intake
instructions)
volume per day by sources.
Estimate average volume per day
in thousand gallons per day.
1300
Municipal or private water system
107a
thousand gallom per day
Sudam water
107b
0 _thousand gallons per day
Groundwater
107c
0 ft- galJorts per day
Othe
107d
320 _thcusand gaIk= per day
Total Item 7
1076
1620 fiwusand gak= per day
• If there is intake water from 'other',
107f
Stormwater
specify the source.
8. Water Use Estimate average
=
per day in thousand gallons
per day for the following types of
water usage at the tacility.
(See instructions)
113
Noncontact cooling water
108a
gakx*s per day
Boiler feed water
106b
55 thou sand ga,11cm per day
Process water (including contact
108c
1158 gailkm per day
cooling water)
Sanitary water
10ed
70 ---A"jsand gallons per day
Other
105e
224 _thousand gallons per day
Total Item 8
Icef
1620 sand gajbns per day
• If them are dsdiarges lo'othee,
Stormwater'
specify
10ag
If there is 'Sanitary' water use,
iceh,
18 0 0 peopL- served
give the number of people served.
a

FOH AU NUY U-=-
9. All Faciill Discharges and other Losses. Number
and nstructions)Volume Specify the
)i= (Sae
a Discharge
number of discharge points and the volume of water
10 the
discharged or lost from the facility according
categories below. Estimate average volume per day in
thousand gallons per day Number of
Total Volume Discharged,
Discharge Points
Million Gallons Per Lay
Surface Water
109a1
109a2
Sanitary wastewater transport sYsten
109161
109b2
Storm water transport system
109c1
109a
Combined sanitary and storm water
109d1
109C12
transport system
Surface impoundment with no
losel
109e2
effluent
Underground percolation
1109H
Well injection
loggi
109g2
Waste acceptance firm
109h1
109h2
Evaporation
logil
30+
10M
388
Consumption
icsil
109j2
Other
109k1
109k2
Facility dischargers and volume
1090
10912
Total item 9
*If there are discharges to'cithee,
109m1
specify.
.10. Permits, Licenses and Appliaitions
List all existing, pending or denied permits, licenses and applications related to discharges from this facility (see _instructions)
Issuing
For Type of
Data
Filed
Data
Issued
Date
Denied
Expiration
Date
Agency
Agency Permit or
Use License
10 Number
YR/MO/DA
YRIMOIDA
YR/MOIDA
YR/MC/DA
.AT
... I -D n-P. -q
in A R 1;
n nd
q R — R-- J;
I 1'N.C. �0700151 08-4-30 103-3-3
-01 , , "' , E -.* - Fannon 0 f) 1A Q — 1 — I '11Q 0 — I — 1 A "AT 0 lr-.,,q 199-19— 1
11. Maps and Drawings
Attach all required maps and drawings to the back of this application. (see instructions)
12- Additional Information

STANDARD FORM C - MANUFACTURING AND COMMERCIAL
SECTION II. BASIC DISCHARGE DESCRIPTION
Complete this section for each discharge indicated in Section
which the waste water does not go through a treatment works
also discharges to surface waters from this facility. SEPARAT
ORIGINATE IN THE SAME FACILITY. All values for an existi
discharge, values should reflect best engineering estimates.
ADDITIONAL INSTRUCTIONS FOR SELECTED ITEMS r
BEFORE FILLING OUT THESE ITEMS.
1. Discharge Serial No. and Name
a D scharge Serial No. 201a
(see instructions)
b. Discharge Name 201b
Give the name of discharge, ff
any (see insructions)
c. Previous Discharge Serial No 201c
If a previous permit
appl''cation was made for this ds
charge (Item 4, Section 1) provide
previous dsdharge serial
number.
2: Discharge Operating Dates .
a Discharge Began Date 202a
If tiv discharge described below
is in operation, gore the data
(within best estimate) the
discharge began
b. Discharge to Begin Date 202b
If the 'discharge has never
occurred but is planned for some
future date, give the data the
discharge will begin.
c. Discharge to End Date If the M
discharge is scheduled to be
discontinued within the next 5
years, give the date (within best
estimate) the discharge will end.
3. Engineering Report Available
Chedd'rf an engineervhg report is
available to reviewing agency
upon request (see instructions) 203
4. Di�ar�e Location Name the
polit'cal boundaries within which
the pant of discharge -is located:
crane
County
(If applicable) City or Town
5 Discharge Point Description
(see insmx-dons)
Discharge into (check one)
Stream (ndudes cWhes, arroyos,
and other watercourses
I"
Osman
Muniidpal Sanitary wastewater
Transport System
Municipal Combined Sanitary
and Storm Transport System
EKE
1, Items 9, that is to surface waters. This includes discharges to municipal sewerage aystema in
xior to being discharged to surface waters. Discharges to wells must be described where there are
E DESCRIPTIONS OF EACH DISCHARGE ARE REQUIRED EVEN IF SEVERAL DISCHARGES
ig discharge should be representative of the twelve previous months of operation. If this is a proposed
1PPEAR IN SEPARATE INSTRUCTION BOOKLET AS INDICATED. REFER TO BOOKLET
001
Treatment plant effluent
001
.59 1
NA
YR MO :
NA
YR MO
Agency Use
North Carolina 2Xd.
Cleveland 204e
204
® STR
❑ LKE
OCE
❑ MTS
MCS .

W1
Municipal Storm Water Transport
System
Well (injection)
Cew
If 'odW is checked, specify type
66 Discharge Point - LattLong. .
Give the Precise location of the
point of T= to the nearest
second.
Lanxis
Longitude
7. Dis—chaige PA)o6iving Watei Nime
Name the waterway at the point of
discharge. (see instructions)
If the d e h an outfall that extends
shoreline
beyond =dw no is below the
moan low
water line, complete item 8,
arAcela'U tumor X Ni—L
x...... ........
For Acercy Use
I 3Me
8. Offshore Discharge
a. Discharge Distance from Shore
b. . Discharge Depth Below Water
Discharge Type and Occurrence
a Type of Discharge Check
whether the discharge is
continuous or intermittent
(See instructions)
b. Discharge Occurrence Days
per Week. Enter the average
number of days per week
(during periods of discharge)
this discharge occurs.
c. Discharge Occurrence- Months
It this discharge normally oper-
ates (either intermittently or
continuously) on less than a yez
around basis (excluding shut-
downs for routine maintenance)
check the months during the ye;
when the discharge is operating
(see instructions)
Complete Items 10 and 11 -if intermittentis
checked in Item 9.a. Otherwise, proceed to
hem 12
10. Intermittent Discharge Ouanthy
State the average volume per d1s-
charge occurrence in thousands of
gal"
11. Intermittent Discharge Duration
and Frequency
a- Intermittent Discharge Duratior
Per Day State the average
number of hours per day the
discharge is operating
b. Intermittent Discharge
e
Frequency State the average
number of discharge o= manc
per day " days when
disdMGk1g
12. Maximum Flow Period Give the
time period in which the -maximum
flow of this discharge occurs
DISCHARGfHRIAL NUMBER
❑ STS
n WEL
❑ OTH
205b
206a _L7_DEG. 37 MIN. L._SEC;
20Eb 35 DEG. _2L__MIN. 2 6 _SEC
207a Brushy Creek
1 2070 1
IFE--l—KI
11111F.K22-
210
21 la
211b
212
NA
feet
NA
❑ (con) Continuous
(rnt) Intermittent
days per week
❑ JAN
E] FES
E] APR
E] MAY
❑ JUL
C] AUG
❑ OCT
[-] NOV
[]MAR
❑ JUN
❑ SEP
❑ DEC
5 6 - _jhousand gallons per day
20
—hours per day
18 - discharge occurrences per day
From Apr 10 S
month month

DT-4'SPTd
TOO
Pi)4sTT
40M
paqpuTuipq
C80C
APTD'SS'2T
TOO
a-4STT-40N
auo-4s
6ZZE
(Z)
paqLunN FuPaS) U URE.I. Utti) rt:ul4uiluujv
seBmWs.0 peje4S ijun ujnLu.mmN
%onpoid q
S[MMM MMd 'o
(Suoqm4sul em)
u=xipoid Supmew x4 pasn Ap=ou sv6n uo.ampoid
jo lepeaew mpi esn 'I elqiU ui peisa lou sepoo OIS jo:j
19151009 uo.V-=sLq eLp jo I elqeLL ui poWoms spun eLp ui
(clpL well) peonpoid ionpok! &4 jo tiv i. wE41) pawnsuco
leueqvw mm eLp jetpie jo junom wnwpmw pue edA
et;t Alddns 'eBm4osp rt; Bu!snm A.V=e eLp se9uosep
4P.4m OPOO OIS qm � eNuLpsia Butsmo A;!A.Py
UPTq-eaedo
bUTqUUTMVT 4GGqS 'Dul --Lapzv
U10-T J-T 9-472Ma-4 S '2M.'-S9pnT OUT OSTV
buTanqDPjnuPUI SSPTb aaqTg aoi
AqTTTDPJ qu9m4Paa4 aaqpmaqspb& EEtZ
TOO
idaevm WU3S 3EANHOSI4
(suoqorLqstm.
em) 8BM.Psp sm &=TOA
14;A=e jo uoQd=sep &v
L, eAn uoqduosea /4!A.=y
z
,ft
MAN

is Waste Abatement
a. Waste Abatement Practices
Describe to waste abaternent
practices used an this dis-
charge With a brief ranative
(see instructions)
b. Waste Abatement Codes
Using the codes listed in Table
11 of the Instruction Booklet
describe the waste abatement
proo_es;as for this discharge in
--the order in which they occur
..if possible.
215a
. 215b
DISCHARGE SERIAL NUMBER
001
Narrative- Recycle of process cooling water
and wash water; use of effluent in
bel t press sprays
(i) ESEPAR
_j2)ESEGRE
(3) EMERGE
(41 RF.COV'F,
—ISIRUSEOR
(6) RECYCL
(9)
(13)
—(14)
-(is)
(16)
(17)
_(18)
(19)
(20)
_(21)
(22)--------(23)
(24)
(25)
I

DISCHARGE SERIAL NUMBER
001
16. Wastewater Characteristics
Check the box beside each constituent which is present in She effluent (disdwp water). This determination is to be based on acb Ld analysis
or best estimaie.(see instructions)
Parameter
PreseM
Parameter
msent
216
216
Color
copper
00080
01042
X
Ammia
0
X
01045
X
Org00605 is nvogen
LOW
X
X
01051
iTale
Magnes&urri
00620
X
009V
ante
00615
01055
mercury
00665
X
719M
molybdenum
00945
01062
-Suirloa
tc e
X
00745
01057
aurtrte
tenium
00740
01147
timmloa
bilver
71870
01077
ionoe
Potassium
00940
X
'00937
yanSodium
00720
00929
ruronoe
X
uum
00951
0105 9
Aluminum
I itanium
01105
X
01152
Anum01097�y
01102
Arsenic1-inc:
X
01002
01092
beryllium
Algiades,
01012
L
74051
Banum
Urdonnalea organic compounas
01007
74052
boron
esvaoes
01022
X
74053
a mtum
t a"o 9mase
X
01027
0�
a aum
00916
X
32730
X
ctanL5
01037
'8
X
Chromium
X
c
01034
•`
t orm bacteria
X
ioactwity
74055
74050
Specify substances, compounds and/or elements in hem 26.
Pesticides ('tnsectiddes, fungicides, and rodenticides) must be reported in berms of the acceptable common names specified in Aoceptabie Common Names
and Chemicafnames for the ingredent Statement on Pesticide Labeis, 2nd Edition, Environmental Protectiori Agency, Washington, D.C. 20250, June 197Z as
required by Subsection 162.7(b) of the Regulations for the Enforcement of the Federal Insecticide, Fungicide, and Roden6cide Act.

■zrtr_�aaayn7
1
DISCHARGE SERIAL NUMBER
) 001
17. Description of Intake and Discharge
For each of the parameters fisted below, enter in the appropriate box the value or code letter answer caged for (see instructions)
In adcition, enter the parameter name and code and all required values for any of the following parameters if they ere checked in item 16:
ammonia, cyanide, aluminum, arsenic, beryllium, cadmium, chromium, copper, lead, mercury, nickel, selenium, zinc, phenols, oil and grease, and.
chlorine (residual).
Innuent
t
n
t
Uaily
minimum
axrmum
requency
umoer osample
Parameter and Code
Intake
Treated
Average
Value
Value
of Analysis
Analyses
Type
Water
Intake
Observed or
Observed or
217
(Daily
Water
Expected
Expected
average)
(Daily
During
During
average)
Discharge
Discharge
Activity
ct ty
1
2)
3)
6
8)
ww
Gallons per day
00056
0.88
0.63
1.26
Cont.
365
-
pH.
Units
00400
6.3
7.8
7 7
260
G
Temperature winter
,F
74CM
2
195
i emperanire summer
OF
7"/
24.5.
20.4
26.9
7 7'
65
G
xtchemc al gen
Demand
(SOD 5-Day)
mg/I
00310
7.4
16.4
1. 4
1/ 7
52
C
Chemical oxygen
Demand (COD)
mgA
00340
otai Sispenow
(nonfilterable) Solids
mg/I
005M
8.5
1.1.
32:9
7/7
260
C
Specific
micromhos/cm at 25°C
00095
meacie Matter
(residue)
ml/1
00545
• Other discharges sharing intake flow (serial numbers) (see instructions)
Copper 0.057 0.10 0.120 2/30 24 C mg/l
01042
Oil & Grease 1.9 '1.0 7.0 1/7 52 G mg/l
00556

ri
T/bUI
T/.6n
T/bn
spunocT
T /BuI
T/BuI
T/BuI
OOT
CLOOE
AM*-'I[d M0110H."[00aE TSTS
UMOPCEI
my
SdV
AAT :M X2921 UO P9SPC
0%3 1
(MM4 Imem jo SLqR5 Uo!ll!tu
jed peppe spunod) AAULro 'D
... jaimowum
qSLZ to nerve Pue &xeN I
(S)PI.PenuA Jo aumN 'B
: BLRMOIIC4 et 4 jamsus
119miBre jo'jqlq!Liu!'-jauoatpuco
Aii L;pm Pepa.4 sl 881ELPS.tp
W;l SGA4 PPV lue"Wij J--w-m
pesn am setappe
lua=az imem pus ucqp-jaua6
imlem Welms io/pLri BuIpco
M.4 s, e5juLpsp p. 6L WmI (neldwoo
eingel jueuxd nbe jo jemod
x4 einpwojd Aoue8nuie jo wiew
A�.Ipq bu!dLund
jofew iq =nos ismod elRwew
ez BBMLPS1.p -
siLp iq ejq2feAV WE sloquco zueld
OupM61jq eL; ppe4o sj0-4L*0 Wqd M
.-P-41ep ;DAOqV :LTZ UI94I
..3
vz
0 E/Z
LVO-.
9010
1110
Z6010 DUTZ
F—
—o 7—z
L
-s>
s y
TSOTO P'29rl
D
7v z
o c7z
fiiT
0 1 >
0 T -P
E: 0
zs
L/T
9
6'T
U L9UU &�uuLuLuV
�o
TT
OE/z.
0
SO, ;r
SO -a
L90TO T;9xc)-rN
7-D
-f, Z
0 E/ Z-
MOO. 8PT-loltr.
D.
ZS
&L
OS600 @PTIOTIT�
(S)
(9)
95jutpsla
eamLps!a
'I
Bupna
13u!l rK3
Alm)
(eBweA'e
pmoed-I
ixa
pep9d
JKLIM
Apea)
L.lz
adAl
SeSABW
p
jo peA"qo
GnPA
JO PMM90
WRA
p
8 Be"y
Sul
peweil
JMIBM
emem
epDo PUB J%BwEmd
eou�mq
JqawnN
I k-yier&w
I wnwixevy
j
I wnwiui
Aimn
im+ui
I PMMZuO
r" nil
TOO
id39vqnN Wbl3S 3E)IdVHOSIC
Illl�il�ll�l

d Chemical composition of these I 219d
additives (see instructions)
Complete Items 20-25 if there is a thermal discharge
(e.g., associated with a steam andror power generation
plant steel mill, petroleum refinery, or any other
manufacturing process) and the mtal discharge flow is
10 million galbns per day or more. (see instructions)
20. Thermal Discharge Source_ Check 220
the appropriate item(s) indicating
the source of the discharge (see
instructions)
Boiler Blowdown
Baler Chemical Cleaning
Ash Pond Overflow
Boiler Water Treatment -
Evaporator Blowdown
Oil and Coal Fired Plants -Effluent
from Air Pollution Control Devices
Condense Cooling Water
Cooling Tower Blowdown
Manufacturing Process
Other
21. Discharge/Receiving Water
Temperature Difference
Give the maximum temperature
difference between the ctisclarga
and receiving waters for summer
and winter operating conditions
(see instructions)
Summer 221a
Winter 221b
22 Discharge Temperature. Rate of
Change Per Hour 222
Give the maximum possible rate of
temperature change per hour of
discharge under operating
conditions (see instructions)
23. Water Temperature, Percentile
Report(Frequency of Occurrence)
In the labia below, enter the
temperature which is exceeded 109/6
of the year, 5% of the year, 1% of
the year and not at all (maximum
yearly temperature). (see
instructions)
Frequency of occurrence
a. Intake Water Temperature 223a
(subject to natural changes
b. Discharge Water Temperature 22313
24. Water Intake Velocity 224
(see instructions)
25. Retention Time GW-thelength of 225
time, in minutes, from start of
water temperature rise to discharge
of cooling water. (see instructions)
DISCHARGE SERIAL NUMBER
001
See MSDS Attached
BLBD
BCCL
APOF
EPBD
OCFP
COND
CTBD
MFPR
OTHR
OF
OF
°Ffiour
Maximum
OF OF OF OF
'°F OF OF OF
feet/sec.
minutes

STANDARD FORM C - MANUFACTURING AND COMMERCIAL
SECTION Ill. BASIC DISCHARGE DESCRIPTION
Complete this section for each discharge indicated in Section I, Items 9, that is to surface waters. This includes discharges to municipal sewerage systems in
which the waste water does not go through a ireatrnent works prior to being discharged to surface waters. Discharges to wells must be described where there are
also discharges to surface waters from this facility. SEPARATE DESCRIPTIONS OF EACH DISCHARGE ARE REQUIRED EVEN IF SEVERAL DISCHARGES
ORIGINATE IN THE SAME FACILITY. All values for an existing discharge should be representative of the twelve previous months of operation. ff this is a proposed
discharge, values should reflect best engineering estimates.
ADDITIONAL INSTRUCTIONS FOR SELECTED ITEMS APPEAR IN SEPARATE INSTRUCTION BOOKLET AS INDICATED. REFER TO BOOKLET
BEFORE FILLING OUT THESE ITEMS.
1. Discharge Serial No. and Name
002
a Discharge Serial No. 201a
(see instructions)
,b. Discharge Name 201b
Overflow branch
Give the name of discharge, if
any (see instructions)
c. Previous Discharge Serial No 201c
002
If a previous permit
ds
a''cation was made for this
WSwdort 1)
c(Item 4, provide
discharge serial
previous
number.
2 Disch ge Operating Dates
a. Diarscharge Began Date 202a
87 05
If the discharge described below
is in operation, give the data
(within best estimate) the
discharge began
b. Discharge to Begin Date 20b
NA :...
If the'disc harge has never
YR. ...:.: :. ..
occurred but is planned for some
_.
future date, give the date the
discharge will begin.
NA
c. Discharge to End Date If the 202c
discharge is scheduled to be
YR. .. MO. • ..:... .
discontinued within the next 5
years, give the date (within best
estimate) the discharge will end.
3. Engineering Report Available
Check if an engineering report is
available to reviewing agency
upon request (see instructions) 203
❑
4. Dissdch,aarr�ge Location Name the
politticalboundaries within which
the point of disctiarg" located:
Agency Use
State 2Xa
North Carolina 204d,
Courity 204b
Cleveland 2134e
(if applicable) City or Town 204c
204
S. Discharge Point Description
(see instructions)
Discharge into (check one)
Stream (includes ditches, arroyos, 205a
:E] STR
and other watercourses
Lake
❑ LKE
Ocean
❑ OCE
Municipal Sanitary wastewater
❑ MTS
Transport System
Municipal Combined Sanitary
and Storm Transport System
❑ MCS

MIMI
111111111
—on7in,
Municipal Storm Water Transport
System
Well (injection)
Other
If 'cd-& is checked, specify type
6. Discharge Point - Lat(Long.
Give the precise location of the
point of discharge io the nearest
second.
Latitude
Lx)g . itude
7. Discharge Receiving Water Nime
Name the waterway at the point of
discharge. (see instructions)
If the cfisd-kxge is through an outfal that extends
beyond the shoreline or is below the mew low
water line, complete item 8,
For Acency Use
3C3a
X.,
8.
X
offshore Discharge
a. Discharge Distance from Shore
b. Discharge Depth Below Water
Discharge Type and Occurrence
a. Type of Discharge Check
whet" the discharge is
continuous or intermittent
(See instructions)
b. Discharge Occurrence Days
per Week. Enter the average
number of days per week
(during periods of discharge)
this discharge occurs.
c. Discharge Occurrence- Niondr.
If this ds--hwge normally oper-
ates (either intermittently or
continuously) on less than a yw
around basis (excluding shut-
downs for routine maintenance)
check the months during the y&
when the discharge is operating
(see instructions)
Complete Items 10 and 11 If 'intermittent' is
checked in Item 9.a. Otherwise, proceed lo
Item 151
10. Intermittent Discharge Quantity
State the average volume per dis-
charge occurrence in thousands of
gallons
11. Intermittent Discharge Duration
and Frequency
a Intennitteent Discharge Duration
Per Day State, the average
number of hours per day the
discharge is operating
b. Intermittent Discharge
Frequency State the average
number of dis�iarge o= nenc
Par day during days when
dis&—gbg
12. Maximum Flow Period Give the
time period in which the -maximum
flow of this discharge occurs
OF-=&z.
207b
1 2070 1
11111F.-I—LA
210
21 la
211b
s
212
DISCHARGE bF�kl-.NUMBER
E] STS
C] WEL
M OTH
-15 DEG. _2-0—MIN. —LQ—_SEC
81 DEG. —U—M I N. 4 5 --JSEC
None
-days per week
[] JAN
❑ FEB
E] MAR
C] APR
❑ MAY
❑ JUN
C] JUL
C] AUG
❑ SEP
[) OCT
[:] NOV
❑ DEC
thousand gallons per day
_—hours per day
—dzdmrge occurrences per day
From — to
month month
11

1-UHAUaNL,T
DISCHARGE SERIAL NUMBER
002
13. Activity Description Give a 213a Non contact cooling water
narrative description of activity without chemical treatment
producing this discharge (we
instructions)
14. . Causing Discharge For each SIC Code which
=s the activity causing this dschwge, supply the
" and maximum amount of either the raw material
consumed (Item 14a) or the product produced (Item 14b)
in the units specified in Table I of the Instruction Booklet.
For SIC Codes not listed in Table 1, use raw material or
production units normally used for measuring production
(see instructions)
a Raw Materials
Maximum Unit
Shared Discharges
b. Products
Maximum Unit Shared Discharges
SIC Code Name Amount(Day (See Table 1) (Serial Number)
b (1) (2) (J) 1 14? 1 (5)
3229 Stone, Not listkid
Glass.Clax:

15 Waste Abatement
a Waste Abatement Practices
Desabe to waste abatement
pracdces; used an this dr,
clusage with a brief narrative
(see instructions)
b. Waste Abatement Codes
Using the codes listed in Table
11 of the Instruction Booklet
-describe the waste abatement
processes for this discharge in
the -order in which they occur
N Possible.
215a
215b
DISCHARGE SERIAL NUMBER
002
Nan,aj,6. Minimize water usage in sprays
when operating. Spray water used to
rnol- exterior of furnaces as a -..temporary
measure for temperature 'control and
fhr rnn1j'ra'hnt, g1 ass drained from
fu-mar,p, Tn use two to three times
per year.
(4)
(10)
(13) (14)
(16) 117)
(19) (20)
121
(22)(214)
0

WV -p=uW% pue'epeof6und 'ePP oesul Raped ll � etll Jo lumeaqu3 etsuopEln5vd eyt p (q)LZ9l uop�esgnS Aq pannbal
se w6l em b9ZOZ '0'4 '=BuigseM 'Aoua6`d uogo%oid Ieluawuwu3 'uop1.P3 PuZ 'sNge7 ePO4sad uo �uswel 2S 7ua•�aJ6u! 9t4 -q saweu�iwaY0 PUv
s9uJeN uoww00 elgmdeooy u pey!oeds seweu uowwoo elgelde= eyl jo sulk ul peuodej eq lsnw (seplopuepa pue 'sepal6ur4 'sepapoesul) sapp4sad
-93 we41 ul sluewele jo�pue spunoduoo 'sammsgns 4padS .
09017L
990bL
kIA!Pml
-vuereq wlo 1 oo
09009
v=0
ep-UO140
wnlwoj
09Z9E
L£010
slue=un
O6LM
91600
wnrn s
09m0
LZOIO
esmwg pue in
wnlwpe
ESOM
ZMLO
sep=se
u
MOM
LOOLO
sounodwoo olue5io pmemown
wn .
t
Z�l10
sepol
tun 10
Z8010
Mo
ou17
auaw
ZOM
L60LO
ul
Auowauy
Z5110
90M
wnluell i
Lunuiwniv
6m10
19500
Lunipq i
eauonla
6Z600
07LOO
wnipoS
sauei(
Lewo
wnlssmo
Orem
eouofLlo
LLOW
0ML
-
J9AIIR
eoiwwp
LbllO
0vLoo
wrnuel
euunc
L9010
moo
MOIN
eoulrtq
Z9010
94600
wnue=Aim
aPfl
eVq
tin
srua�dsou
l0
919M
81U11
ujntsoubeV4
GISAIN
1pveegi
�
U88o alu DI
MLO
O1900
toil
eluowurd
MLO
08000
Jol
92,
91Z
vjeswd
isleuieJeel
umaid
Jmeweme
(suoG.=sul ees)'elewpse lseq jo
s!sllleue ler»e uo peseq eq of 9! uopeu!umetep st m e&eLpsp) lueMe et; ut luesard s! VLjm luerapsuoo 4=8 eplseq xoq 84 it *Lr3
•quauigvaaq TVaTuraua ON sapspe3��4� a e1sEM 9l
zoo
�39W(1N WUBS BOUVHOSIQ

(suoq rt4su! ees) (sjegwnu pues) MN eMMul 6uue4s se6leyosQ sey;O .
SC900
mw
(anplsai)
JMTM aiasatn
56000
009Z 4s wo/so 4LUOMIw
eouez2rpu000u
OES00
V6w
"oS (epp-je41Buou)
pepmeds-,R _.o
OK=
l/6w
(000) Puswacl
U96AX0 rmweqo
OXCO
l/6w
(As0-S 009)
PumuaO
ua6P*WaLpcqq
LZ04L
de
jeuiwns eirnsjedwe i
6�L
• do
(Jejum-) eimL-jgdwB
OOV00
szlun
d
.
ESJ00
lisp jed suopM
•
nna
6
g
S
b
E
Z
l
k!n4otl
a6J21PS,0
6
66ieyos!0
6P
(e6s�enB
JaMm
(a6
e&a
3
JaleM
Alle0)
1pa)
LlZ
edA.L
sesAMW
sts� MWjo
JO pe�uesgO
en(eA
�o Pe uesgO
OMA
efteny
Wmul
Pe1Ewl
JMsM
e4mul
epco PUB Je4ewe�ed
aid
o M' wn
�uenbw
wnwi
wnwiui
Aim
u
luenmi "
•(lenplsei) euucnLp
Pue'esm6Puello'spueyd'purz'wnwetes'le5p+u 'AnoJew'peel'ieddoo'wniuiojLp'wruwpw'wrnlllieq'owes�e'wnuwnle'ap!ueAo'swowwe
:% u+eq u! pe4mp am ALB p! sxneweied 6uuwollgl et; do Aue -q semen peanbei Qs PUe ePoo Pus eweu Je4e� ey; ie4ue 'uogPPa ul
(suogon4su ees) xy Peffm JeMsue JMSI epoO Jo enleA ey1 xoq e4eudadde eye u! je4ue 'Ngeg pels!I veleumed et; jo Lpee jo:l
e5m4wb pue eMmul p ucgduose0 LL

DISCHARGE SERIAL NUMBER
002
.-Y
Parameter and Code
217
nvsa
Intake
Water
(Daily
average)
1
t
Treated
Intake
Water
(Daily
average)
2
Daily
Average
3
-Minimum
Value
Observed or
Expected
During
Discharge
Activity.
4
maximum
Value
Observed or
ExPeclad
During
Discharge
Activity8
5
reWency
of Analysis
6
NUMOW
of
Analyses
Type
18. Plant Controls Check if the following
plant controls are available for this
discharge 218
Alternate power source for major
pumping facility
Alarm or emergency procedure for
power or equipment failure
Complete Item 191 discharge is torr
coding and/or steam water
generation and water treatment
additives are used
19. Water Treatment Additives If the
discharge is treated with any
conditioner, inhibitor, or algiade,
answer the following:
a. Name of Material(s) 219a
b. Name and address of 219b
manufacturer
c, Ouanthy (pounds added per 219c
million gallons of water treated)
None

Permit No. NC0004685
Renewal application 6-30-98
Sludge Management Plan Narrative
The wastewater treatment plant sludge generated by the Shelby facility is a mixture of
primary and secondary sludges. The primary sludge is the result of clarification using
lime, aluminum chloride, polymers and coagulants to achieve floc formation and settling.
The secondary sludge is waste activated sludge from the biological treatment system. The
secondary sludge also containes bentonite clay and a small amount of ferric chloride.
Both sludges are combined in a sludge thickener/storage tank prior to dewatering.
Polymer addition and mechanical mixing, along with dilution water, is required to prepare
the sludge for the belt press. The sludge is then pumped to a belt press for dewatering.
The belt press has both a gravity drain section and a pressure section where the water is
removed. Typically, the solids are increased from 4-5% as it leaves the storage tank, to 25
to 30% solids discharged from the belt press. The dewatered sludge is transported by
screw conveyors to a roll -off box which is handled by a local hauling and waste disposal
contractor.
Dewatered sludge is disposed of, off -site, at a private landfill owned by Cleveland
Container Service (JM Landfill). The sludge is incorporated into the cover dirt.
As an alternative disposal method, the Shelby plant has acreage permitted for land
application of sludge (Permit No. WQ0001055) but has elected not to use this option.

An
L
� .
PPG Industries, Inc.
Works No. 52 940 Washburn Switch Road Shelby, North Carolina 28150 USA
January 24, 1997
WPCSOCC
N.C. DEHNR, Water Quality
P.O. Box 29535
Raleigh, N.C. 27626-0535
Dear Sirs:
Subject: Change in Operator in Responsible Charge
NPDES Permit No. NC0004685
PPG Industries, Shelby
This letter is to notify you of a change in Operator in Responsible Charge (ORC) and
backup operators for our wastewater -treatment plant.
Operator in Responsible Charge:
Henry F. Blackwell
Grade IV, Certification number 19514.
Backup operators:
William Schenck
Grade IV, Certification number 15216 .
Lacy Ballard
Grade IV, Certification number 4282
Signature authority under 15A NCAC 2B.0506 continues to be delegated to Lacy Ballard,
Staff Engineer. If additional information is needed, please contact Lacy Ballard at 704-
434-2261, ex. 544.
Sincerely,
A. A. stroth
Manufacturing Manager
cc: J. Lesley, Mooresville Regional Office
M. LeCroy
R Fletcher

SCENIC OF WATER FLOW
PPG INDUSTRIES,
INC.
FCityHaterStormSupply
Drainage
,'00,000
North &
cpd
South
Non—
Sanitary
Forming
orging
Cooling
60,000
847,000
113,000
opd
apd
gpd
R2s'e�rch
Fzbi-i cati-o'n
To Rt-osphere
1000.
15,000
gpd
gpd
vaporation
i 335,000
Discharge No.
80i 1 E1-5
Coating
gpd
002
43,000
1000
gpd
gpd
Product
I300
grd
Storm
(;isc.
Process
hater
Drainage
3000
.
74,000
Garage/pads
185,000_
gpd
gpd
To Custcmer
To atTosphere
3],200 bpd
S1Udae -
Landfi ] 1 S1 edge f-la
s tc raterAzde1, mac.Deirateri nq reatr.;ent
2u)G
�gl:d
gpd
Discharge NO,
001 Brushy Creek
1,300,000 normal gpd
1,500,000 maximum gpd

�Rehoth — . - \�-
ch � • O \
/ 900
NZ
i _ ..;. !� /(,�, - :' -` �� _\:•�%-ice — .I .. .900
3912
251
I000337
988
Double Springy x9 B i'
ACO
1336
900 U.
323
SO
` �, , - \�� . •�' I "s'a Washburn
_ •� ( I t t ! Subst lion 1 13`�
91.3
x /� •I• ., . q ` i..ce•.. -37
l3
CO
Lattimore • ,�, —�- �� i� $ D a
•:� `�.,/ d' .i� �• ' SEpBOASO is ,, i j. l „ 9U
f 13I) ''� i • ,(
�• 1em
190-1
1l
.� . %� 9W •I. _ J 7 r sF
N

A
� ,, V je-c, -�— �'IcZ 3
Customer No. 716706 0i
Ticket No. ' 074313
Material Safety Data Sheet 7Emergency Phone
08 438 1800
Section r • • • _
TRADE NAME EXFOAM 494 Was�eWwa ePr treatment C099IDENT
DOT SHIPPING NAME 4V44
Compound, Industrial Process Water Treating, Liquid
'' v.,
Section 2F.M..�. �.. ►.-�4�� •I.�.a ��
CAS NUMBER % EXPOSURE CRITERIA
'goes not contain hazardous cons;.ituents
..rider 29CFR 1910.1200, d(3)S(4).
Section 3
white liquid -
Section 4
FLASH POINT (& METHOD USED) FLAMMABLE LIMITS IN AIR % BY VOLUME ' AUTO IGNITION
ER
LOWER . UPPER TEMPATURE
} 200 F. PMCC f A 9A ha€�
EXTINGUISHING MEDIA:
SPECIAL FIRE FIGHTING PROCEDURES:
':ool exposed containers with w.er spray. Firefighters should wear full
Protective gear.
UNUSUAL FIRE AND EXPLOSION HAZARD:
None known
Section 5 •<�e't 50n4
STABILITY (NORMAL CONDITIONS) CONDITIONS TO AVOID
Stable �fot determined
INCOMPATIBILITY (MATERIALS TO AVOID)
Strong oxidizing agents_
HAZARDOUS DECOMPOSITION PRODUCTS
CC, CO2
HAZARDOUS POLYMERIZATION CONDITIONS TO AVOID
Will not occur Not applicable
GRADE :.

wF<uFCIIUF OURVIly FJutu JF 1%=1 (connnuee)
Section 6 - • a
TOXICITY INFORMATION:
See Section
EFFECTS OF OVEREXPOSURE:
INHALATION: ' Prolonged exposure to vapors or mist may irritate naseT passages.
INGESTION: Product may cause irritation of gastro-intestinal tract if large
amounts are swallowed.
SKIN OR EYE CONTACT: Prolonged or frequent skin contact can cause irritation.
EMERGENCY AND FIRST AID PROCEDURES
INHALATION: Remove affected persons to fresh air and treat symptoms.
INGESTION: DO NOT INDUCE VOMITING. Seek medical attention immediately.
SKIN CONTACT: Wash with soap and water. Remove contaminated clothing and wash
before reuse.
EYE CONTACT: Flush eyes immediately with water and seek medical attention.
Section . « . , �a�:: ;::gib Tows.., .::X• a
VENTILATION REQUIREMMZNTS
'lechanical ventzla•Lion should be adequate.
RE,
)PIRATORY PROTEECTION (SPECIFY TYPE)
one special
EY9 PROJECTION GLOVES
uogg es Rubber or plastic
OTHER PROTECTIVE CLOTHING AND EQUIPMENT
Long sleeve work shirt and pants.
Section 8
STEPS TO TAKE IF MATERIAL IS RELEASED OR SPILLED
olleot using absorbent, place in container for proper disposal. Flush area
Of spill with water.
WAS It DISPOSAL METHOD
Dispose usin chemical scavenq er service in authorized landfill. For additional
disposal instructions, contact your state water pollution control agency.
Section 9 `~
PRECAUTIONS TO BE TAKEN IN HANDLING AND STORAGE
;:eepp container closed when not in use.
50 F. is recommended.
V I HtR PRECAUTION5
Por industrial use only.
Protect from freezing. Storage above
PREPARED BY: F 11or5s DATE: `''• ''
The date included herein are presented accordingg to W. R. Grace d Co.'s practices current at the time of preparation hereof, are made available solely For the consideration, im,estigation and
verification of the original recipients hereof and do not constitute a representation or warranty For which Grace assumes legal responsibility. lr is the responsibility of a recipient of this data to
remain currently informed on chemical hazard information, to design and update its own safety program and to comply with all national, Federal, state, and local laws and regulations applicable
to safety, occupational health, right to know and emriromental protection.
GRACE