WI0300210_Injection Event Record_20120118

. , -
INJECTION EVENT RECORD
North Carolina Department of Environment and Natural Resources - Division of Water Quality
Permit Number WI-0300210
1. Permit Information
NCDOT-Roadside Environmental Unit
Permittee
>rmer NCDOT Asphalt Testinq Site: No. 2-66
Facilityy Name
164 Bostian Bridge .Road,
Statesville, NC
Facility -Address
2: Injection Contractor Information
Hart & Hickman, PC
Injection Contractor / Company Name
Street Address 29.23 S Tryon St, Ste 100
Charlotte NC 28203
City State Zip Code
(7:04) 586-0007
Area code - Phone number
3. _, Well Information
Number of wells used.:for injection 36
Well names B-1 through B-35 + B-2B -
Were any new wells installed during this injection
event?
- n Yes ❑ No
If yes, please provide the following information:
.N.M. of.M.9pitorin ,.Wells
Number of Injection Wells see below
Type of Well Installed (Check applicable type);.
❑ Bored - ❑ Drilled ❑X Direct -Push'
❑ Hand -Augured ❑ Otber (specify),
Please include two copies of the .G W-1 b.for each`
well inst�lled
36.-In3ecte - Staz,glessh;Saeel Extractable -Well,
Scr2errS.=in Qeosahe. Bore Hole'
Were any wells abandoned during this injection
event?
❑x Yes ❑ No
If .yes, please provide the following information:
Number of Monitoring Wells
Number of Injection Wells 36
Please include two copies of the GW-30 for each
well abandoned.
4. .Injectant Information
'EOS 598B42 with B12 Supplement
Injectant Type 13-2=B-10= --,20 a EOS/--80o Water
:13-1, B-11-B-35, + B-213=
Concentration -14 o EOS/-86 6 water
If the injectant is diluted please indicate the source
dilution fluid. Public Water 1A
-1,618 gallons. EOS 'I,< e
-Total Volume Injected -10, 666 gallons Water✓
-46 gallons. EOS
Volume Injected -per well-276-460 gallons. Water
G�.
5. Injection History
Injection number (e.g. 3 of 5) 1
Is -this the last injection at this site_?
0 Yes ❑ No
I DO HEREBY CERTIFY THAT ALL THE
INFORMATION QN:.THIS, FORM IS. CORRECT TO
THE BEST OF MY KNOWLEDGE AND THAT THE
INJECTION WAS PERFORMED WITHIN THE
STANDA OUT IN THE PERMIT.
T
yk?
SIGNATURVOF INJECTION CONTRACTOR ATE
_Stivve L:ibbey for Hart &Hickman, PC
PRINT NAME OF PERSON. PERFORMING THE INJECT"
Submit the original"of this form to.the Divisiwbf-Waier Quahgi within 30 days of injection.
Attnr-UIC Program, 1636 Mail Service Center, Raleigh; NC 21690-1636, Phone No. 919-733-3221
Form UIC-IER
Rev. 11/06
r el
r

.Via US Mail
January 18-, 2012
North Carolina DepArtment of Environment'and Natural Resources
Aquifer Protection Section — UIC Program'
DENR - Division of Water Quality
1,636,Mail,Service'Center
Raleigh, NC 27699-1636
Attention.. -Mr. David Goodrich
Re: Injection Event Record (Form .:UIC4ER)
NC DOTT-Asphalt Testing SfteVo. 2-66
164 Bostiaft Bridge Road
Statesville, North Carolina
H&H Job No. DOT-404.
Dear Mr. Goodrich:
On behalf of the ,NCDOT Roadside Environmental Unit, Hart & Hickman, PC (H&H) is
submitting the, enclosed Injection Event Record,for the EOS` injection event performed on
er 40 through 19 2: All
Decenib 012 at the �roferenced', fa6ility. injection wells were abandoned
with Portland cement after, the event. Should d you have any questions or need any
additional information, please feel free to `contact me: at 4 (704) -586-0007.-
Very truly y(?Urs,'
Hart & Hickman, PC
Mad Brambleti,'PE
Principal 4
4:1/.? JYUU I'll YVt*,ak[t=tf_t ?U L -?UCCL
Charlotte; NE292E13 Meig'h, NC 27607
w
Daain 919,a47,444 .586WO7
1-main.-
-www.haithkkman.COM
nbOT4m sw=�iikmmos w, � idmid,
S.VAk-MaVer�ra4cL%ANC DOT -Do cd edion Evint RcwrdkU[C-IER Cova Lcumdoe

Rogers, Michael -
From: Matt Bramblett [[e-mail]]
Sent: Thursday, March 05, 2015 1:04 PM
To: Rogers, Michael
Subject: DOT Statesville Injection Well Forms
Attachments: Injection Event Record_01-2013.pdf
Per our discussion, here -you go. Let me know if you have further questions or need more information.
Matt
Matt Bramblett, PE, Principal
Hart & Hickman, PC 12923 South_Tryon_Street-Suite 100 1 Charlotte, NC 28203
Direct 704-887-4620 1 Mobile [phone] Main 704-586-0007
www.harthickman.com
hart r hickman

fy A` NON E .� SIDENT
s . North Carolina De arunentofEnvironme
'�'� """" �•, " WELL CONTRACTOR CERTii
hti k tout � -
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individuan Name
GEOLOGIC EXPLORATION, INC
Well"Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
7f 04 l 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-1
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injectionid
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision. Lot No., Parcel. Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley Q(Flat []Ridge ❑Other
LATITUDE 35 ^ 45 56.6500 " DMS OR DD
LONGITUDE 80 ° 55 • 2.5700 " DMS OR DD
Latitudellongilude source: i, 3PS Qropographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
IfI
L WELL CONSTRUCTION RECORD
nt and Natural Resources- Division of Water Quality
iCATION # 3552
d. TOP OF CASING IS
0.0 FT. Above Land Surface'
`Top of casing terminated at/or below land surface may require
a variance In accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): N/A
METHOD OF TEST N/A
f. DISINFECTION: Type
N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness!
7. CASING: Depth
Diameter Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
9. SCREEN:_ Depth
Diameter Slot Size Material
Top Bottom
Ft. In. in.
Top Bottom
Ft. in. In.
= Top Bottom
Ft. in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
MAYMEAD ASPHALT PLANT
NIA
0.0 / 42.0
Facility Name,
Facility ID# (if applicable)
/
164 BOSTIAN BRIDGE DRIVE
/
Street Address
-/
STATESVILLE
NC
28677
/
City or Town
State
Zip Code
/
NCDOT
/
Contact Name
/
164 BOSTIAN BRIDGE! DRIVE :'
Mailing Address
/
STATESVILLE
NC
28677
/
City or Town
State
Zip Code
12. REMARKS:
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH_ 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO Cal
I
c. WATER LEVEL Below Top of,Casing: 21.0. FT.
(Use "+" if Above Top of Casing)
Formation Description
DIRECT PUSH
:I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NCAC 2C. WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS
: RECORD BEEN PROVIDED TO THE WELL OWNER.
\ _ . 01/17/13
L SIGN A lfJ�" RTIF ED WEL R — DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW 1b -
ef,QUailty Information Processing;= Rev_ 2/09

WELL ABANDONMENT RECORD
North Carolina Department of Environment
and Natuml Resources- Division of Water Quality
r' WELL CONTRACTOR CERTIFICATION # 3552
I
1. WELL CONTRACTOR:
s. WELL DETAILS:
VINCE FEDERLE
a.Total Depth 42.0 ft. Diameter. in.
Well Contractor (Individual) Name,
b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC
Measuring point Is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
6. CASING: Length Diameter
1 Street Address
STATESVILLE W 28625
a. Casing Depth (f known): NIA ft. in.
City or Town State Zip Code
b. Casing Removed: NIA ft. in.
.
704 872-7686
.Ares a Phone number
7. DISINFECTION: NIA
l
2. WELL INFORMATION:
(Amount of 65%75% calcium hypochlorite used)
t
SITE WELL ID # (if applicable) B'1
8. SEALING MATERIAL:
Neat Cement Sand Cement
STATE WELL PERMIT # (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
Water gal. Water gal.
Bentonite
'
i.
DWQ or OTHER PERMIT # (if applicable)
Bentonite 3wo lb.
i WELL USE (Check applicable use).=] Monitoring ❑ Residential
Type: ❑ Slurry ❑ Pellets
❑ Municipal/Public ❑Industrial/Commercial ❑ Agricultural
Water gal.
❑ Recovery Z Injection ❑ Irrigation
Other
f ❑ Other (list use)
Type material PORTLAND CEMENT
j
Amount 8.5 GALLONS
3. WELL LOCATION:
+ COUNTY IREDELL QUADRANGLE NAME
i
+i+ NEAREST TOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
.164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
1 .
(Slreel/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) :
j TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley V Flat ❑ Ridge❑ Other
(Check appropriate selling)
; 10. WELL DIAGRAM : Draw a detailed sketch of liwall on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
<LATITUDE 35 _� 45 56.6500 ^DMS OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 __' 55 ' 2.5700 ^ DMS OR DO
types of fill materffels:sed
Latitude/longitude source: &�,PS ❑Topographic map
12M 8/12
(location of well must be shown on a USGS topo map andattached to .
11. D'A'fE WELL ABANDONED
this form if not using GPS)
"
1 DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
:. WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a:
THVRORD HASSBEEN POVIDED TO THE WELL OWNER.
(Ifa residential well, skip 4a: complete 4b, well ownerinformallon only.)h
� �,,
FACILITY ID # (if applicable)
G�Zn/{
! �.t71X2�2— 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
:' SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL "DATE
City or.Town State Zip Code
; (The private well owner must be an individual wbersonallWbandons His/her residential wen
in accoNance with 15A NCAC 2C .0113.)
'Ab. CONTACT PERSON/WELL OWNER
VINCE FEDERLE'
NAME )NCDOT
PRINTED NAME OF'P.ERSON ABANDONING THE WE LL
STRADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE: NQ 28677
" '
Silbrn�t a copy to the owner and the orlgina(to Division
of Vilater Quality information Processing, ' Form GW-30
-' 161 fvlali Service Cente[, Raleigh NC 27699'1617 Phone{ (919)
�... .
J
Rev. 5/i0
807663(10' t r y

��A]Q�'T• \
NON-RESIDENTIAL ON -RESIDENTIAL WELL CONSTRUCTION RECORD
'• '" o North Carolina Department of Environment and Natural Resources- Division of Water Quality
`�' � r •�, r P Q tY
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(tf applicable)
SITE WELL ID #(If applicable) B-2
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Induslrial(Commercial ❑ Agricultural ❑ Recovery ❑ Injection If
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/10/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel. Zip Code)
CITY. STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley VFlal ❑Ridge ❑Other
LATITUDE 35 -45-56.6500 „ DMS OR DD
LONGITUDE 80 0 55 • 2.5700 " DMS OR DD
Latitude/longitude source:. W3PS Oropographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 38.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO LJ(
c. WATER LEVEL Below Top of Casing: 21.0 F-E
(Use "+' if Above' Top of Casing)
d. TOP OF CASING IS 0.0 FT. Above Land Surface`
'Top of casing terminated allor below land surface may require
a variance in accordance with I6A NCAC 2C .0118.
G. YIELD (gpm): N/A
METHOD OF TEST N/A
= f. DISINFECTION: Type
N/A
Amount N/A
g. WATER ZONES (depth):
Top Bottom
Top
Bottom
Top Bottom
Top
Bottom
Top Bottom
Top
Bottom
Thickness/
7. CASING: Depth
Diameter
Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material
Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
FI-
9. SCREEN: Depth
Diameter Slot
Size Material
Top Bottom
Ff.
in.
in.
Top Bottom
Ft.
in.
in.
Top Bottom
Ft. '
in.
in.
10. SANDIGRAVEL PACK:
Depth
Size
Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
11. DRILLING LOG -
Top Bottom
0.0 / 38.0
/
12. REMARKS:
Formation Description
DIRECT PUSH
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• M NCAC PC. WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECORD S BEEN PROVIDED O THE L OWNER.
01/17/13
SIGNATURE OF CERTIFIED WE L ACTOR DATE
VINCE FEDERLE•
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

•r•d a n
�•,� J ,Z.`- WELL ABANDONMENT RECORD
a, rq Imo° North Carolina Department of Environment and Natuml Resources- Division of Water Quality
WI+:Li, rnNT)?ArrnR rRRTr7i rt"ATrnN if. 3552
1. WELL CONTRACTOR:
5.
WELL DETAILS:
VINCE FEDERLE
a.Total Depth 38.0 ft. Diameter. in.
Well Contractor (Individual) Name
b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC
Measuring point is 0.0 IL above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
6.
CASING: Length Diameter
` Street Address
STATESVILLE NC 28625
a. Casing Depth ()f known): NIA ft. in.
City or Town State Zip Code
b. Casing Removed: N/A ft. In.
704 ) 872-7686
N/A
Area code Phone number
7.
DISINFECTION:
2 WELL INFORMATION:
(Amount of 65%75% calcium hypochlorite used)
SITE WELL ID # (if applicable) B-2
= 8.
SEALING MATERIAL.:
Neat Cement Sand Cement
STATE WELL PERMIT# (ifappricable)
Cement lb. Cement lb.
COUNTY WELL PERMIT' # [f applicable]
Water gal. Water oat.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonite 300.0 lb.
WELL USE (Check applicable use)D Monitoring ❑ Residential
Type:❑ Slurry ❑ Pellets
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
Water gal.
❑ Recovery 0 Injection ❑ Irrigation
Other
❑ Other (list use)
Type material PORTLAND CEMENT
Amount 7.5 GALLONS
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
9.
- EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC [LAND SETTING:
❑ Slope ❑ Valley F1 Flat ❑ Ridge❑ Other
(Check appropriate setting)
10.
WELL DIAGRAM :Draw a detailed sklatch of theell on the back of this
form showing total -depth, depth and diameter of screens (if any) remaining
LATITUDE 35 _^ 45 56-6500 ^ DMS OR DD
in the well, gravel interval, intervals of easing perforations, and depths and
LONGITUDE 80 - 55 2.5700 ° DMS OR DD
types of fill materialstsed
Latitudellongitude source: &!�3PS (3ropographic map
12/10/12
(lodation ofwe/N rust be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form if not using GPS)
4a. FACILITY - The name of the business where the well Is located. Complete 4a;
(If a residential well, skip 4a: complete 4b, well owner information only.)
FACILITY ID # (if applicable)
NAME OF FACILITY MAYMEAD ASPHALT PLANT
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE . NC 28677
City or, Town State . Zip Code
4b. CONTACT PERSON/WELL OWNER:
NAME`-_ NCDOT
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT COPY OF
THIS RECORD HAS BEEN PIDVIDED TO THE WELL OWNER.
01/
SIGNATUREc-O F C RTIFIE� D W�n-IrACTOR . DATE
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATI'_
(The private well owner must be an individual wUersonalhebandons his/her residential well,.
in accordance with 15A NCAC 2C .o113.) `
VINCE FEDERLE. ~ .
PRIUTED NAME OF PERSON ABANDONING THE WE LL
Form GW-30
Rev. 5110.

NONRESIDENTIAL ONRESIDENTIAL
WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
• "�•°°'
WELL CONTRACTOR CERTIFCCATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 ) 872-7686
Area code Phone number
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
*Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST N/A
f. DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
2. WELL INFORMATION:
: 7. CASING:
Depth
Diameter Weight Material
WELL CONSTRUCTION PERMIT#
Top
Bottom
Ft.
OTHER ASSOCIATED PERMIT#(tf applicable)
: Top
Bottom
FL
SITE WELL ID #(if applicable) B-28
: Top
Bottom
Ft.
i
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
: 8. GROUT-
Depth
Material Method
Indusidal/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Ffi
Top
Bottom
Ft.
Irrigation❑ Other ❑ (list use)
: Top
Bottom
Ft.
DATE DRILLED 12/18/12
; Top
Bottom
Ft.
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley !;(Flat []Ridge ❑Other
LATITUDE 35 . ° 45 ' 56.6500 ^ DMS OR DD
LONGITUDE 80 ° 55 ' 2.5700 " DMS OR DD
Latitude/longitude source: 03PS propographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE -
Street Address
STATESVILLE
NC
28677'
City or Town
Stale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
- Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 36.0 FEET
b. DOES WELL REPLACE EXISTING INF,LL? YES
NO Ej'/
c. WATER LEVEL Below Top of Casing:
21.0
FT. .
(Use "+^ if Above Top of Casing)
: 9. SCREEN-. Depth Diameter
Top Bottom Ft. in.
Top Bottom Ft. in.
Top Bottom R. in.
10. SAND/GRAVEL PACK:
Depth Size
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
11. DRILLING LOG
Top Bottom
0.0 / 36.0
/
12. REMARKS:
Slot Size Material
In.
in -
in.
Material
Formation Description
DIRECT PUSH
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCA912C. WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
: REC,7HAS,BEEN V! O THE LL O NER.
' �0� 01/17/13
: SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
: PRINTED NAME OF PERSON -CONSTRUCTING THE WELL
Form GW-1 b
Rev. 2109

m SG1TF•o `., 1
WELL ABANDONMENT RECORD
_. ' o:
North Carolina .Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR: a. WELL DETAILS:
VINCE FEDERLE a.Total Depth 36.0 It Diameter: in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-2B
STATE WELL PERMIT #' (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable usep Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery Z Injection ❑ Irrigation
❑ Otherpist use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME _
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC / LAND SE_UING.
❑ Slope ❑ Valley G Flat _ _13 Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 45 56.6500 " DMS OR DD
LONGITUDE 80 55 2.5700 ^ DMS OR DD
6. CASING: Length
a. Casing Depth (if known): NIA
b. Casing Removed: NIA
Diameter
fL in.
ft. in.
7. DISINFECTION: N/A
(Amount of 65°/a75% calcium hypochionte used)
8. SEALING MATERIAL:
Neat comp Sand Cerro,nt
Cement lb. Cement lb,.
Water gal. Water gal.
Bentonite
Bentonite lb.
Type: ❑ Slurry 0 Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 7.25 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TRFMIF
10. WELL DIAGRAM : Draw a detailed sketch of th®ell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materlallsed
Latitude/longitude source: Rf;PS Oropographic map
12/18/12
(location of well must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form if not using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a- FACILITY- The name of the business where the well is located. Complete 4a r
THIS RECORD HAS BEEN PIDVIDED TO THE WELL OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.)
FACILITY ID # (if applicable)
�1/ 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE - NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town Slate Zip Code
(The private well owner must be an individual w Er onall bandons his/her residential well .
in accordance with 15A NCAC 2C .0113.)
4b:,CONTACT PERSONMELL OWNER:
S
VINCE FEDERLE '
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
-STREET-ADDRESS '164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Form GW-30
Rev. 5110

•y.N $TArFgW
aid
'.; NONRESIDENTIAL WELL coNsrRucrtoN RE, coRn
North Carolina Department ofGnvironment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-3
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural p Recovery❑ Injection E(
Irrigation[] Other ❑ (list use)
DATE DRILLED 12/19/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No.. Parcel. Zip Code)
CITY. STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley KdFlat ❑Ridge 'p01her
LATITUDE 35 ^ 45 ' 56.6500 „ DMS OR DO
LONGITUDE80 ^ 55, 2-5700 "DMS.OR DO
Lalitudefiongitude source: 03PS Qropographic map
(locatlon of well must be shown on a USGS tope map andattached to
this fomt ifnot using GPS)
5. FACILITY (Name of the business where the well Is located.)
MAYMEAD ASPHALT PLANT
NIA
Facility Name
Facility ID# (if
applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NOW
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use'+' if Above Top of Casing)
d. TOP OF CASING IS
0.0 FT. Above Land Surface'
'Top of casing terminated at/or below land surface may require
a variance In accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): N/A
METHOD OF TEST N/A
f. DISINFECTION: Type
N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness/
: 7. CASING: Depth
Diameter Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material Method
Top Bottom
Ft.
: Top Bottom
FL
Top Bottom
Ft.
9. SCREEN: Depth
Diameter Slot Size Material
:TOP Bottom
Ft. in. In.
Top Bottom
Ft. in. in.
Top Bottom
Ft. in. in.
10. SANDIGRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
: Top Bottom
FL
Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
0.0 / 42.0
/
12. REMARKS:
Formation Description
DIRECT PUSH
- 190 HERE Y CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A N A C. WELL CO STRUON S7yAAAAA�1NNNN!pppppARDS. AND THAT A COPY OF THIS
: RECO BEEN PI IOED,(LO THE
((Q00// ��`11 rip 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev- 2109

WELL ABANDONMENT RECORD
s.
North Carolina Department of Environment and Natural Resources- Division of Water Quality
P� Q lY
WELL CONTRACTOR CERTIFICATION # 3552
1: WELL CONTRACTOR: 5. WELL DETAILS:
VINCE FEDERLE a.Total Depth 42.0 ft. Diameter: in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
CilyorTown Slate Zip Code
704 1 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-3
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)D Monitoring ❑ Residential
i❑ M unicipal/Public ❑ IndustriallCommercial 0 Agricultural
❑ Recovery M Injection ❑ Irrigation
i
❑ Other (fist use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(Streel/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
0 Slope ❑ Valley G Flat ❑ Ridge❑ Other
6. CASING: Length Diameter
a. Casing Depth (if known): NIA (L
b. Casing Removed: N/A A.
7. DISINFECTION: N/A`
(Amount of 65%76% calcium hypochiorite used)
8. SEALING MATERIAL:
[gat Cament Sand Ceme t
Cement lb. Cement lb.
Water gal. Water aal.
Bentonite
Bentonite 300.e lb.
Type:0 Slurry 0 Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
In.
In.
(Check appropriate selling)
10. WELL DIAGRAM : Draw a detailed sketch of th eell on the back of this
- _
form showing total depth, depth and diameter of screens (if any) remaining
j LATITUDE _35 _^ 45 , 56.6500 • DMS OR DD
_ in the well, gravel interval, Intervals of casing perforations, and depths and
I{ i LONGITUDE 80 � — 2.5700 ^.DM5 OR DD
types of rill matedalwsed"
f j Lalitudellongilude source: VGPS Qropographic map
12/1 g/12
(location of well must be shown on.a'USGS topo map andattached to
11. DATE WELL ABANDONED
this form if not using GPSJ -
1 DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH ISA NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT COPY OF
' 4a. FACILITY -The name of the business where the well is located. Complete 4a r
THIS CORD HAS BEEN P®VIDED TO THE WELL OWNER.
' (if a residential well, skip'4a; complete 4b, well owner inrorrnation only.)
I
/J
�(��Gi.P�t
FACILITY ID # (f applicable)
l 01/17/13
1 MAYMEAD ASPHALT PLANT
NAME OF FACILITY
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL • DATE
�. City or Town State Zip Code
(The private well owner must be an individual w orsonall bandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
4b..C_ONTACT PERSONIWELL OWNER:
VINCE FEDERCE
NAME NCDOT
1
PRINTED NAME OF PERSON ABANDONING THE WELL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE NC 28677
Form GW-30
1aliServtce Centel `Raleigh NC2Tli99 11i 7, Phone [phone]bb r> Rev. 5110
S
,. :-.: a:.... .' r. .. .. c-- _... _.. .:'.S+.r .vv.. �... r...r - .. ,_-v.+.-.
,'
i
., ..v. .r .. . .a. ar. n .� ..e _..r .. .,.�. .a

yt
a o` $rAiFo``k s
NONRESIDENTIAL WELL CONSTRUCTION RECORD
1(` North Carolina Department of Environment and Natural Resources- Division of WaterQuality
5 WELL CONTRACTOR CERTIFICATION # 3552
.w.2' r
w-" e
N.'
1. WELL CONTRACTOR:
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
VINCE FEDERLE
*Top of casing terminated atfor below land surface may require
Well Contractor (Individual) Name
a variance in accordance With 15A NCAC 2C .0118.
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
: e. YIELD (gpm): NIA METHOD OF TEST NIA
176 COMMERCE BLVD
L DISINFECTION: Type N/A Amount NIA
Street Address
g. WATER ZONES (depth):
STATESVILLE NC 28625
Top Bottom Top Bottom
City or Town State Zip Code
: Top Bottom Top Bottom
70( 4 1 872-7686
: Top Bottom Top Bottom
Area code Phone number
Thickness/
2. WELL INFORMATION:
: 7. CASING: Depth Diameter Weight Material
WELL CONSTRUCTION PERMIT#
Top Bottom Ft.
OTHER ASSOCIATED PERMIT#(ii applicable)
: Top Bolton FL -
SITE WELL ID #(if applicable) B-4
: Top Bottom Ft.
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
: 8• GROUT: Depth Material Method
InduslriallCommercial ❑ Agricultural ❑ Recovery Injection d
Tap Bollom Ft.
Irrigation❑ Other ❑ (list use)
: Top Bottom FL
DATE DRILLED 12/11/12
: Top Bollom Ft.
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel. Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley VFW ❑Ridge []Other
LATITUDE 35 ^ 45 ' 56.6500 " DMS OR DD
LONGITUDE 80 ^ 55, 2.5700 "DMS OR DO
Lalitude/longitude source: 'W3PS Oropographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable).
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
Area code Phone number
6. WELL DETAILS:
a_ TOTAL DEPTH: 41.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO [�
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+" If Above Top of Casing)
9. SCREEN: Depth Diameter SlotSize Material
Top Bottom Ft_ in. in.
Top Bottom Ft. in. in.
Top Bottom FL -in. in.
10• SAND/GRAVEL PACK:
Depth Size
Top Bottom Ft.
Top Bottom Ft.
Top Bolton Ft.
11. DRILLING LOG
Top Bottom
0.0 / 41.0
/
12. REMARKS:
Material -
Formation Description
DIRECT PUSH '
I Do HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• ISA NCAC 2C• WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECO(2O HJfS 13EEN�PROVIDED TA THE I�L OWNER.
01/17/13
SIGNATURE OF CERTIFIED WELL COITMACOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
lualliy Information ' rocessing�;,_. _ Rev. 2/09

I
WELL ABANDONMENT RECORD
2
--r� North Carolina Department of Environment and Natural Resources- Division of Water Quality
L L
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
s. WELL DETAILS:
VINCE FEDERLE
a.Total Depth 41.0 ft. Diameter: in.
Well Contractor (Individual) Name
b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC
Measuring point Is 0.B ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
6. CASING: Length Diameter
Street Address
STATESVILLE NC 28625
a. Casing Depth (if known): N/A R in.
City or Town Stale Zip Code
b. Casing Removed: N/A 0. in,
704 ) 872-
NIA
Area code Phonee number
7. DISINFECTION:
(Amount of 65%75% calcium hypochlorite used)
2. WELL INFORMATION: -
SITE WELL ID # (if applicable) B4
8. SEALING MATERIAL:
Neat Cement Sand Cement
STATE WELL PERMIT # (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
Water gal. Water oat.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonite 300-0 lb.
WELL USE (Check applicable usep Monitoring ❑ Residential
Type:❑ Slurry ❑ Pellets
M unicipal/Public U Industrial/Commercial ❑ Agricultural
Water gal.
❑ Recovery M Injection ❑ Irrigation
Other
❑ Other (list use)
Type material PORTLAND CEMENT
Amount 8.25 GALLONS
3. WEL OCATION.
COUNTY IRE DELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
(StreeURoad Name, Number, Community, Subdivision, Lot No., Parcel,-Zlp Code)
TOPOGRAPHC I LAND SETTING:
❑ Slope ❑ Valley U Rat ❑ Ridge❑ Other
(Check appropriate setting)
10. WELL DIAGRAM : Draw a detailed sketch of theeil on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE _35_ _^ 45 56.6500 - DMS OR DO
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _ = 55 2.5700 - DMS OR DD
types of fill materialsised
Latitude/longitude source: &63PS 01-opographic map
12/11/12
(location of well must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form -if not using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C. WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY -The name of the business where the well is located- Complete 4a.
THIS RECORD HAS BEEN PRVIDED TO THE WELL OWNER.
(If a residential well, skip 4a; Eomplele 4b, well owner information only.)
FACILITY ID # (if applicable)
/ J� 01/17/13
NAME OF FACILITY -MAYMEAD ASPHALT PLANT"
SIG ERTI IE WELL DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
:. SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE'
City Or Town State Zip Code
(The private well owner must be an individual w ersonali bandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSONlWELL OWNER:
VINCE FEDERLE
NAME-. NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
' STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
-
Su6mlt ado" py to the owner and the ongInai1 o Division- of Water Quality ilnformatton Processing
:..- ; Forni GW-3D
107. Mail Servici: Center;_Raleigh, NG 27699,-1617 Phone':'(919j'807=6300 ',....... `•,;c ": Rev. 5110

'mod rim � •
1 ' t(• Sr NONRESIDENTIAL ONRESIDENTIAL WELL CONSTRUCTION RECORD
7 01 North Carolina Department of Environment and Natural Resources- Division or Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor pndividual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-5
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Tap of casing terminated allor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): N/A METHOD OF TEST N/A
f. DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
:7. CASING: Depth Diameter Weight Material
Top Bottom Ft.
Top Bottom Fl.
Top - Bottom Ft.
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑ : 8. GROUT: Depth Material Method
Industrial/Commercial_ ❑ Agricultural ❑ Recovery❑ Injection Top Bottom Ft.
Irrigation❑ Other ❑ (list use) : Top Bottom Ft.
DATE DRILLED 12/11/12 : Top Bottom Ft.
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope []Valley 9Flat ❑Ridge ❑Other
LATITUDE 35 ^ 45 - 56.6500 " DMS OR DID
LONGITUDE 80 ^ 55, 2.5700 " DMS OR DD
Latilude/iongitude source: 03PS aopographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located_)
MAYMEAD ASPHALT PLANT NIA
Facility Name Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE NC 28677
City or Town Stale Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC 28677
City or Town Slate Zip Code
Area code Phone number
'6. WELL DETAILS:
a. TOTAL DEPTH: 41.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO E/
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+' if Above Top of Casing)
:9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. in. in.
Top Bottom IFt. in. in.
Top Bottom Ft. in. in.
10. SANDIGRAVEL PACK:
Depth Size
Top Bottom FL
Top Bottom FL -
Top Bottom Ft.
11. DRILLING LOG
Top Bottom
0.0 / 41.0
12. REMARKS:
Material
Formation Description
DIRECT PUSH
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC C, WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS
RE RD AS BEEN PR VIDESR THE L OWNER.
(ffC\�(P�� 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-lb
Rev. 2/09

' 4 WELL ABANDO&MENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
•..;„ ,".:'�' y WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR: 6. WELL DETAILS:
VINCE FEDERLE a. Total Depth 41.0 ft. Diameter. in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 ) 872-7666
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-5
6• CASING: Length Diameter
a. Casing Depth (Ifknown): WA ft
b. Casing Removed: N/A ft.
7. DISINFECTION: NIA
(Amount of 65%75% calcium hypochlorile used)
8. SEALING MATERIAL:
in.
in.
i
Neat .em .nt Sand Cement
T
STATE WELL PERMIT # (if applicable}
Cement lb. Cement lb.
COUNTY WELL PERMIT # Cf applicable)
Water gal. Water oal.
DWQ or OTHER PERMIT # (if applicable)
Bentonite
WELL USE (Check applicable use)D Monitoring ❑ Residential
Benlonite 300.0 lb.
Type: ❑ Slurry ❑ Pellets
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
Water gal.
i
❑ Recovery 0 Injection ❑ Irrigation
Other
❑ Other (list use)
Type material PORTLAND CEMENT
I
3. WELL LOCATION:
-
Amount 8.25 GALLONS
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE :
9. - EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
i
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Slreel/Road Name, Number, Community. Subdivision, Lot No., Parcel, Zip Code)
- TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley fG Fiat. ❑ Ridge❑ Other
(Check appropriate setting)
10. WELL DIAGRAM : Draw a detailed sketch of [heel[ on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 35 _� 45 56.6500 ^ DMS OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 55 2.5700 . DMS OR ' DD
types of rill materialsrsed
Latitude/longitude source: Rf.-PS Oropographic map
(location of well mustbe shown on a USGS topo map andatfached to
11. DATE WELL ABANDONED 12/11/12
this farm if not using GPS)
100 HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
4a. FACILITY - The name of the business where the well is located. Complete 4a :
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT COPY OF
THIS RECORD HAS BEEN P®VIDED TO THE WELL OWNER.
(If a residential well, skip 4a: complete 4b, well owner information only.)
FACILITY ID # (if applicable)
�f �^ 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNXt{l' ERTt IED WEL DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an Individual w ersanap bandons his/her residential well
"
in accardancewilh 15A NCAC 2C .0113.)
41). CONTACT PERSON/WELL OWN I
VINCE-FEDERLE J
NAME NCDOT,:.
PRINTED NAME OF PERSON ABANDONING THE WELL
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Submit a copy tDtth`e�awner and the dH§ina! to Division of Watet• Quality Information Processing "
:,. Form Gw-sD
Phgne
1617 Ma11 Service Cerite� ;Raleigh IVC 27699 161i', Rev. 5/10

a ` • :. NONRESIDENT)
S
North Carolina Department of Environmer
q�CVaue•ph:r WELL CONTRACTOR CERTIF
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(ir applicable)
SITE WELL ID #(inapplicable) 13-6
3. WELL USE (Check One Box) Monitoring 0 Municipal/Public 0
Industrial/Commercial ❑ Agricultural ❑ Recovery 0 Injection [u�
Irrigation0 Other 0 (list use)
DATE DRILLED 12/11/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel. Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope Malley ,VFlat ORidge ❑Other
LATITUDE 35 ° 45 56.6500 " DMS OR DO
LONGITUDE 80 ^ 55 • 2.5700 " DMS OR DD
Latilude/longitude source: 03PS Oropographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located)
MAYMEAD ASPHALT PLANT
NIA
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
U
Area code Phone number
S. WELL DETAILS:
a. TOTAL DEPTH: 41.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO E/'
c. WATER LEVEL Below Top of Casing: . 21.0 FT,
(Use "+" if Above Top of Casing)
WELL CONSTRUCTION RECORD
it and Natural Resources- Division or Water Quality
ICATION # 3552
d. TOP OF CASING IS
0.0 FT. Above Land Surface*
'Top of casing terminated at/or below land surface may require
a variance In accordance with 15A NCAC 2C .0118.
'a. YIELD (gpm): N/A
METHOD OF TEST N/A
E DISINFECTION: Type
N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness/
:7. CASING: Depth
Diameter Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
: 8. GROUT., Depth
Material Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
:9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft. in. in.
Top Bottom
Ft. in. in.
: TOP Bottom
Ft. in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top Bollom
Ft.
: Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
Formation Description
0.0 1 41.0
DIRECT PUSH
1
1
. 1
12. REMARKS:
100 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2 ,WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECO D 5 BEEN PROVIDED THE WE�L OWNNER.
l PIN Pn �� 01/17/13
: SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2109

WELL ABANDONMENT. RE CORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
";""'„ •�'"' WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
s. WELL DETAILS:
VINCE FEDERLE
a.Total Depth 41.0 R Diameter: in.
Well Contractor (Individual) Name
b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC
Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name
((( 176 COMMERCE BLVD
6. CASING: Length Diameter
I Street Address
STATESVILLE NC 28625
a. Casing Depth (if known): N/A IL in.
i City or Town Stale Zip Code
b. Casing Removed: NIA g• in.
l 704 ) 872-7686
Area code Phone number
7• DISINFECTION: NIA
2. WELL INFORMATION:
(Amount of 65%75% calcium hypochlorite used)
SITE WELL ID # (if applicable) B 6
8. SEALING MATERIAL:
Neat Cement Sand Cat
STATE WELL PERMIT# (if applicable)
'
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
Water gal. Water oat.
j DWQorOTHER PERMIT # (if applicable)
Bentonite
i
WELL USE (Check applicable use)D Monitoring ❑ Residential
Bentonite 300-e ib.
Type: ❑ Slurry ❑ Pellets
❑ Municipal/Public 0 industrial/Commercial 0 Agricultural
Water gal.
❑ Recovery M injection 0 Irrigation
Other
0 Other (list use)
Type material PORTLAND CEMENT
3. WELL LOCATION:
Amount 8.25 GALLONS
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:.
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Street/Road Name, Number, Conumrnity, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley CA. Flat ❑ RidgeO Other
(Check appropriate setting)
LATITUDE 35. _' 45 56.6500 ^ DiVLS OR DD
LONGITUDE 80 55 • 2.5700 ^ DMS OR OD
10. WELL DIAGRAM : Draw a detailed sketch of theall on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materialsrsed
Lalifud=longllude source, g(GPS ul opographic map
(location of well must be shown on a USGS lopo map andattached to
11. DATE WELL ABANDONED 12/11/12
this form if not using GPS)
100 HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
da. FACILITY - The mama or the business where the well is located. Complete 4a r
(If a residential well, skip 4a; complete 4b, well owner information only.)
THI-9,REYORD HAS 13EEN P VIDED�p THEWELL ER.
.l.,t� -
�
FACILITY ID # (if applicable)
•
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE 'NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town Stale - Zip Code
'(The private well owner must be an individual wpersonalhabandons his/her residential well
in accordance with 15A NCAC 2C.0113.) -
4b.CONTACT PERSON/WELLOWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET,ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
..
r •-Form G 3
617 Mail Service. Center, Raleigh NC`27699 1617, Phone_ (9?9j 807 6300+ , r� Rev. 5/10

1 V ONRESIDENTL4L WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTII+ICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(ir applicable)
SITE WELL ID #(if applicable) B-7'
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection J?(
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/19/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel. Zip Code)
CITY: STATESVILLE COUNTY 1REDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley SifFlat ❑Ridge ❑Other
LATITUDE 35 -45 - 56.6500 ., DMS OR DD
LONGITUDE 80 ` 55 • 2.5700 " DMS OR DD
Latitude/longitude source: 03PS Uopographic map
(location of well must be shown on a USGS lopo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
f
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 38.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO C�
c. WATER LEVEL;BelowTop of Casing: 21.0 FT.
(Use '+"'if Above Top of Casing)
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST NIA
f. DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top
Bottom
Top
Bottom
Top
Bottom
Thickness/
:7. CASING:
Depth
Diameter
Weight Material
Top
Bottom
Ft.
Top
Bottom
Ft.
Top
Bottom
FL
: 8. GROUT:
Depth
Material
Method
Top
Bottom
FL
: Top
Bottom
Ft.
Top
Bottom
Ft.
9. SCREEN:
Depth
Diameter Slot Size Material
Top
Bottom
Ft.
in.
in.
Top.
Bottom
Ft.
in.
in.
Top
Bottom
Ft.
in.
in.
10.. SAND/GRAVEL PACK:
Depth
Size
Material
Top
Bottom
Ft.
Top
Bottom
Ft.
Tap
Bottom
Ft.
11. DRILLING LOG
Top Bottom
0.0 / 38.0
. 1
12. REMARKS:
Formation Description
DIRECT PUSH
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
I 5A NQ5C : R 2 NSIONSJ�fWDARONERTAOPYOFTHIS
OVI0TT(O TH 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE.FEDERLE
: PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

""`�SrAiE •• .
�, V•�n h
WELL ABANDONMENT RE, CORD
Norlh Carolina Department of Environment and Natural Resources- Division of Water Quality
�d,�4q Wau Y-� R•p",F
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
704 1 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-7
S. WELL DETAILS:
a.Total Depth 38.0 ft. Diameter in.
b. Water Level (Below Measuring Point): 21.0 fL
Measuring point is 0.0 ft. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): N/A ft in.
b. Casing Removed: NIA ft. in.
7. DISINFECTION: N/A
(Amount of 651/675°% calcium hypochlodle used)
8. SEALING MATERIAL:
Nnat Cement
STATE WELL PERMIT # (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable) Water gal Water nal
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Cheat applicable use)D Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial -❑ Agricultural
❑ Recovery Z Injection ❑ Irrigation
❑ Other (fist use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
_ 164 BOSTIAN BRIDGE DRIVE 28677
`. (Street/Road Name, Number, Community, Subdivision, Lot No.. Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley V Flat ❑ Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 _ 45 56.6500 • DMS OR DD-
LONGITUDE 80 _ 55 • 2.5700 • DMS - OR DO
Bentonite
Bentonite 300-0 lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTIAND CEMENT
Amount 7.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL: -
TREMIE
10. WELL DIAGRAM :Draw a detailed sketch of theall on the back of this
form showing total depth, depth and diameter of screens (f any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materiakused
Latitude/longitude source: ' 17s-PS Qropographic map
(location of well must be sholvn on a USGS topo map andattached to
11. DATE WELL ABANDONED 12/19/12
this fonn if not using GPS)
1 DO HEREBY CERTIFY THATTHIS WELL WAS ABANDONED IN ACCORDANCE
le qa
4a. FACILITY -The name of the business where the well is located. only.)
(If a residential well, side qa; complete 4b, well owner information only.)
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THATA COPY OF
THIS �REC S BEEN P®Vlt TO T OWNER.
\\\\YY
FACILITY ID #.
a��J
(if applicable)
01/17/13
NAMEOF FACILITY MAYMEAD ASPHALT PLANT
: SIGNATURE OF CERTIFIED WELL CONTRACTOR - DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
Cily or Town Slate Zip Code
(The private well owner must be an Individual wba—rsonathpbandons histher residential well
4b. CONTACT PERSONNVELL OWNER:
in accordance with 15A NCAC,2C .0113.)
NAME NCDOT
VINCE FEDERLE
PRINTED NAME OF PERSON ABANDONING THE WE LL
.STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Form GW-30
Rev. 5/10

I NONRESIDENT
North Carolina Department of Environnlet
WELL CONTRACTOR CERTIF1
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (individuaq Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(ff applicable)
SITE WELL ID #(trapplicable) B-8
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ injection vd
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/12112
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY; STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley VFiat ❑Ridge ❑Other
LATITUDE 35 -45 • 56.6500 " DMS OR DD
LONGITUDE 80 - 55 • 2.5700 " DMS OR DD
Latitudefiongitude source: V3PS Qropographic map
(location of well must be shown on a USGS topo map andatlached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
- Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
U
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO L-)(
c. WATER LEVEL Below.Top of Casing: 21.0 FT.
(Use "+" if Above Top of Casing)
IA
L WELL CONSTRUCTION RECORD
1t and Natural Resources- Division of Water Quality
CATION # 3552
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Top of casing tennlnated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST N/A
f. DISINFECTION: Type NIA Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Boltom Top Bottom
Top Bottom Top Bottom
Thickness/
: 7. CASING: Depth Diameter Weight Material
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
8. GROUT: Depth Material Method
Top Bottom Ft.
Top Bottom Ft.
Top Bottom R.
: 9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. in, in.
Top Bottom Ft. in. in.
Top Bottom Ft. in. in.
10. SAND/GRAVEL PACK:
Depth Size
Top Boltom FL
Top Bottom FL
Top Bottom Ft.
Material
11. DRILLING LOG
Top Bottom Formation Description
0.0 / 42.0 DIRECT PUSH
/
12. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NW 2C. WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
REFOOVlpgq TO THLL OWNER
R.
01/17/73
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
)ANCE FEDERLE
: PRINTED NAME OF PERSON CONSTRUCTING THE WELL
< 1Fo
Subit wlthln 30idays>of cotnpletlon to > Dlytston of Water Quaftiy (nformairon Processing,.' Rev 2los GW-1b
m
r
+=••1617 Mail Service Center Rater h NC 2769g 164 Phone; (919) 807 630U ; "'
i

-
�d�r•'y1° + a�
rr WELL ABANDONMENT RECORD
a� =.•.1r- of.
,, f'I •. f. �°' �� North Carolina Department oFEnvironment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR: 5. WELL DETAILS:
VINCE FEDERLE a.Total Depth 42.0 fl. Diameter. in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21-0 ft.
GEOLOGIC EXPLORATION, INC Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
8. CASING: Length Diameter
Sheet Address
STATESVILLE NC 28625
a. Casing Depth (if known): N/A ft. in.
I City or Town Stale Zip Code
b. Casing Removed: NIA ft. in.
704 872-7686
N/A
Area Phone number
- 7. DISINFECTION:
t
(Amount of 65%75% calcium hypochlorite used)
1 2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-8
i
: 8. SEALING MATERIAL:
Neat Cement Sand Cement
STATE WELL PERMIT # (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
t Water gal. Water gal.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonite •e lb.
WELL USE (Check applicable use)❑ Monitoring 0 Residential
Type: ❑ Slurry 0 Pellets
❑ M unicipallPubiic ❑ IndustriallCommercial ❑ Agricultural
Water gal.
0 Recovery Z Injection ❑ Irrigation
i
Other
❑ Other (list use)
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
j 3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NFARESTTOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
1 ' 164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC / LAND SETTING:
` 0 Slope 0 Valley F/, Flat 0 Ridge❑ Other
I
(Check appropriate setting)
10. WELL DIAGRAM :Draw a detailed sketch of ttwdl on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
1
LATITUDE 35 _^ 45 56.6500 ^ DMS OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
1.
LONGITUDE 80 = 55 • 2.5700 • DMS OR DD
types of fill materials,sed
!
Latitude/longitude source: , Ii3PS Dropographic map
12/12/12
(location ofwe#must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form if not using GPS) r
1 DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a i
THIS RECORD HAS BEEN P®VIDED TO THE WELL OWNER.
(If a residential well, skip 4a; complete 46, well owner information only.)
, �
�
- i
FACILITY ID # (if applicable)
i/xjL(f(// 01/17/13
� ,�7i
NAME OF -FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 80STIAN BRIDGE HIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an individual whersona%abandons his/her residential well
(((
in accordance with 15A NCAC 2C .0113-)
!
4b. CONTACT PERSON/WELL OWNER:
VINCE FEDERLE
* jl
NAME NCDOT`
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677 '
t
ualt Form GW-30
adeora76;=PlDiolnvels::
rma: t.o. n
. h NC 27fi99=161Ftotheowner
(9n19ot
:......, i._ .... ::
)f'a3W07=t6e3r0Q0 .n.f..o
Rev.5/101617MaifCente;>Raig

6 y
e,'k�r ouaw"-
I. WELL CONTRACTOR:
VINCE FEDERLE -
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-9
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/12/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel. Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley !(Flat ❑Ridge []Other
LATITUDE 35 " 45 56.6500 " DMS OR DO
LONGITUDE 80 " 55 ' 2.5700 " DMS OR DO
Lalitude/longitude source: IZ3PS plbpographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (f
applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
L.�
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO C�
c. WATER LEVEL Below Top of Casing: 21.0 FT,
(Use "+" if Above Top of Casing)
NONRESIDENTIAL ONRErSIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division or Water Quality
WELL CONTRACTOR CERTIFICATION # 3SS2
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
: e. YIELD (gpm): NIA METHOD OF TEST N/A
L DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
7. CASING: Depth Diameter Weight Material
= Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
:8. GROUT: Depth Material Method
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
: 9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. in. in.
Top Bottom Ft. in. in.
Top Bottom Ft. in. in.
10. SANDIGRAVEL PACK:
Depth Size Material
Top Bottom FL
Top Bolton Ft. -
Top Bottom Ft.
11. DRILLING LOG
Top Bottom Formation Description
0.0 / 42.0 DIRECT PUSH
/
/
12. REMARKS.
: 1 DO HEREBY CERTIFY THAT THIS.WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C. WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS
fjECoKDHAS BEEN PRO OTO WELL/OWNER.
tirt-c� �- 01117/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

fr. `p S3•��: WELL ABANDONMENT RECORD
i.s
North Carolina Department of Environment and Natural Resources- Division of Water Qualify
h `C ......�= ^" WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-9
STATE WELL PERMIT# (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # Of applicable)
WELL USE (Check applicable use)' Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery 9 Injection ❑ Irrigation
❑ Other (fist use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
6. WELL DETAILS:
a.Total Depth 42.0 ft. Diameter in.
b. Water Level (Below Measuring Point): 21.0 %
Measuring point is 0.0 fL above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): NIA ft. in.
b. Casing Removed: NIA fl. in.
7. DISINFECTION: NIA
(Amount of 65%75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb- Cement lb.
Water gal. Water gal.
Bentonite
Bentonite 3ao.0 lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
n—u,t 8.5 GALLONS
9.. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC / LAND SETTING:
0-Slope ❑ Valley V Flat ❑ Ridge❑ Other
(Check appropriate setting) 10. WELL DIAGRAM : Draw a detailed sketch of lheell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 35 _' 45 56.6500 ^ DMS OR DD in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _y 55 2.5700 ^ DMS OR Dp types of fill materialmsed
j Latitude/longilude source: IMPS pfopographic map
(location ofwall must be shown on a USGS topo map andallached to
this form if not using GPS)
11. DATE WELL ABANDONED
12/12/12
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THATA COPY OF
4a. FACILITY -The name of the business where the well is located. Complete 4a: THIS RECORD HAS BEEN POVIDED TO THE WELL OWNER.
(li a residential well, skip 4a; complete 4b, well owner information only.)
h. FACILITY 10 # (if applicable) 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT SI TURe OF CERTIFIE�CMDATE
164 BOSTIAN BRIDGE DRIVE
STREETADDRESS -
.t STATESVILLE NC 28677 : SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
_ Cily or Town Stale Zip Code (The private well owner must be an individual wbersonalhebandons his/her residential well
In accordance with 15A NCAC 2C .0113.} '
4b. CONTACT PERSONIWELL OWNER: VINCE FEDERLE
NAME ' NCDOT PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS t64 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Subtnit a Copyo the owner and the ortglnal io Drvt§ion of Water QDality Information Processrng, Form GW-30
` 1617 Mail Service Center, Rah gh, NC 27699 1617 Phone' (919} 8Q7 6300 Rev. 5110
;- :.-.-..s i.�.v :::..., .roar• ....:.....::.....:. :..:.•.. :. - 1 , 4 J
f '

, » SiArC6
NONREaDENT
North Carolina Department of Environme
WELL CONTRACTOR CERTIFI
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-10
3, WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Eli
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12112/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY. STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley VFlat ❑Ridge ❑Other
LATITUDE 35 ' 45 56.6500 " DMS OR OD
LONGITUDE 80 " 55, 2.5700 " DMS OR DD
Latiludellongitude source: W3PS Qropographic map
(location of welt must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Slate
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO[/
c. WATER LEVEL Below Top of Casing: 21.0 FT
(Use "+' if Above Top of Casing)
IAL
WELL CONSTRUCTION RECORD
nt and Natural Resources- Division of Water Quality
CATION # .3552
: d. TOP OF CASING IS 0.0 FT. Above Land Surface'
*Top of casing terminated atfor below land surface may require
a variance in accordance with 15A NCAC.2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST N/A
f. DISINFECTION: Type N/A- Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
: 7. CASING: Depth Diameter Weight Material
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
: 8. GROUT: Depth Material Method
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
:9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. in. in.
Top Bottom Ff. in, in.
Top Bottom Ft. in. in.
10..SANDIGRAVEL PACK:
Depth Size
: Top Bottom Ft.
Top Bottom Ft.
Top Bottom FL
11. DRILLING LOG
Top Bottom
0.0 / 42.0
/
: 12. REMARKS:
Material
Formation Description
DIRECT PUSH
:I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RE OR D70 THE-V4�LL OWNER
(f ' 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE.
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1 b
Rev_ 2/09

WELL ABANDONMENT RECORD
fMhi
' d••~ - ° North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
- Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-10
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable used Monitoring ❑ Residential
0 Municipal/Public ❑ IndustriallCommerciai ❑ Agricultural
❑ Recovery 71 Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGIE NAME
NEAREST TOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:_
❑ Slope ❑ Valley Vi Fiat ❑ Ridge❑ Other
(Check appropriate setting)
& WELLDETAILS:
a.Totai Depth 42.0 ft. Diameter in.
b. Water Level (Below Measuring Point): 21.0 ft. —
Measuring point is 0.0 ft. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): N/A fL in.
b. Casing Removed: N/A ft. In.
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlorile used)
: 8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb. Cement lb.
Water gat. Water cal.
Bentonite
Bentonite 300.0 lb.
Type:❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
9• EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
SREMIE
10• WELL DIAGRAM : Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE _35_ _ 45 56.6500 " DMS OR DD
In the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80. = 55 2.5700 ^ DMS OR DD
types of fill malerialsised
LatitudeAongitude source: �GPS Qfopographic map-
12/12/12
f/ocalion of well must be shown on a USGS lopo map andattached to
- 11. DATE WELL ABANDONED
this form if not using GPS)
100 HEREBY CERTIFY THATTHIS WELL WAS ABANDONED IN ACCORDANCE
: WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY -The name of the business where the well is located. Complete 4a i
THIS RECORD HAS BEEN P®VIDED TO THE WELL OWNER.
(If a residential weti, skip 4a; complete 4b, well owner information only.)
FACILITY ID # (;f applicable)
� 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
Clly of Town - _ - Stale Zip Codas •.
(Theer private well owner must be an individual w sonall bandons his/her residential well
in accordance With 1SA'NCAC 2C .0113.)
4b. CONTACT PERSONIWELL OWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PER30N ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Form GW-30
Rev. 5/10

�a� SrArF�'�1
.T NONRESIDENT
Norlli Carolina Department of Environmei
WELL CONTRACTOR CERTIFI
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
17f COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERM IT#(iiapplicable)
SITE WELL ID #(it applicable) B-11
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Induslrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Id
Irrigation[] Other ❑ (list use)
DATE DRILLED 12/13/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC 1 LAND SETTING: (check appropriate box)
❑Slope ❑Valley U'Rat ❑Ridge ❑Other
LATITUDE 35 ° 45 ' 56.6500 " DMS OR DO
LONGITUDE 80 ° 55 ' 2.5700 " DMS OR DD
Lalitudellongitude source: W3PS pfopographic map
(location of well must be shown on a USGS topo map andattached to this form if not using GPS)
5. FACILITY (Name of the business where the well is located_)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN 13RIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City of Town ,
State
Zip Code
t—�
Area code Phone number -
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELT?-NtSQ'"NO E/
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use'+' if Above Top of Casing)
If�
L WELL CONSTRUCTION RECORD
it and Natural Resources- Division of Water Quality
CATION # 3552
d. TOP OF CASING,IS
0.0 FT. Above Land Surface
'Top of casinoenninated at/or below land surface may require
a variance In accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA
METHOD OF TEST NIA
f. DISINFECTION: Type
N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness/
7. CASING: Depth
Diameter Weight Material
= Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
FL
: 8. GROUT: Depth
Material Method
Top Bottom
Ft.
Top Bottom -
Ft.
Top Bottom
Ft.
: 9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft. in. in.
Top Bottom
Ft. in. in.
Top - Bottom
Ft. in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top Bottom
FL
Top Bottom
FL
11_ DRILLING LOG
Top Bottom Formation Description
0.0 / 42.0
/
12. REMARKS:
DIRECT PUSH
' 1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAV2C. WELL CONSTRU TIONrdST NDARDS, AND THAT A COPY OF THIS
: REC�RHAS.9EENP VIOTHE�j.IO NE�
V /7� 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-ib
Rev. 2/09 .

J�+STATt'a4
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
P Q ty
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-11
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable usep Monitoring ❑ Residential
❑ M unlcipaifPublic ❑ Industrial/Commercial ❑ Agricultural
p Recovery M Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
5. WELL DETAILS:
a.Total Depth 42.0 ft. Diameter. In.
b. Water Level (Below Measuring Point): 21.0 ft.
Measuring point is 0.0 ft. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): N/A ft. in.
b. Casing Removed: N/A It. in.
7. DISINFECTION: NIA
(Amount of 65%75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement
Cement lb.
Water gal.
Bentonite
Bentonite 3.3 lb.
Type. ❑ Slurry ❑ Pellets
Water gal.
Sand Cement
Cement Ill.
Water aaL
Other
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel. Zip Code)
TOPOGRAPHIC / LAND SETTING:
❑ Slope ❑ Valley G Flat ❑ Ridge❑ Other -
(Check appropriate selling) 10. WELL DIAGRAM : Draw a detailed sketch of thuell on the back of this
form showingtotal depth, depth and diameter of screens (if any) remaining
LATITUDE 35 45 56.6500 DMS OR DD in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 55 2.5700 • DMS OR DO types of flit materiaisised
Latitude/longitude source: &!J�PS ❑Topographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
11. DATE WELL ABANDONED 12/13112
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WEL LCONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a
(If a residential well, skip 4a; complete 4b• well owner information only.)
S RECORD HAS B N PI3V ED TO THE WELL OWNER.
FACILITY ID # (f applicable)
��
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR
DATE
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677 - --
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE .
City or Town '.. State Zip Code
(The private well owner must be an individual whersm�allsabandons his/her'residentlal well
in accordance with 15A NCAC 2C .0113.)
4b.CONTACT PERSON/WELL OWNER:
VINCE FEDERLE
�'-
Fla;. ...
NAME NCDOT -
PRINTED NAME OF PERSON ABANDONING THE WELL
-
;.
STREET.ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Subtnit'a copyto (F1e owner and the ortgfnal to Division of
Water Qiiality Information Processing _
Form 6w-3o
"16 i7 Mall Service Center Ralei h NC 27699 161 Phone=:' 919
807 6300 >>
Rev. 5110

£°A• m 4
s 5 .NON-RESIDENT
North Carolina Department ofEnvironmet
WELL CONTRACTOR CERTIr
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70f 4 1 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(ir applicable) B-12
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection R(
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/13/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY_ STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
[]Slope []Valley JJFlat ❑Ridge pOther
LATITUDE 35 -45 56.6500 'DMS OR DO
LONGITUDE 80 ^ 55 , 2.5700 " DMS OR DD
Latitude/longitude source: MPS OFopographic map
(location of well must be shown on a USGS topo map andattached to
this form lfnot using GPS)
5. FACILITY (Name of the business where the well Is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (f applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO U /
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use'+" if Above Top of Casing)
IA
L WELL CONSTRUCTION RECORD
it and Natural Resources- Division of Water Quality
ICATION # 3552
' d. TOP OF CASING IS
0.0 FT. Above Land Surface'
'Top of casing terminated allor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
: e. YIELD (gpm): NIA
METHOD OF TEST N/A
f. DISINFECTION: Type
N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness!
7. CASING: Depth
Diameter Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Fl.
8. GROUT: Depth
Material Method
Top Bottom
Ft.
Top Bottom
Ft.
= Top Bottom
Ft.
9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft. - in. in.
Top Bottom
Ft. in. in.
Top Bottom
Ft. in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
: Top Bottom
Ft.
m Top Botto
Ft.
Top Bottom
Ft.
11. DRILLING LOG
Top, Bottom
Formation Description
0.0 / 42.0
DIRECT PUSH
/
/
12. REMARKS:
1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECOnp Iif S eEEfJ PROV,IDEDXTHE OWN/ER.
V ljlr (A�t/ill f/J(� /Qr7(?n � 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

'x3• �y4: WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
5. WELL DETAILS:
a.Total Depth 42.0 IL Diameter: in.
b. Water Level (Below Measuring Point): 21.0 ft.
Measuring point is 0.0 ft. above land surface.
6. CASING: Length Diameter
Street Address -
STATESVILLE NC 28625
a. Casing Depth (if known): NIA fl. in.
— -- - - City or Town - Slate Zip Code
b. Casing Removed: N/A ft. in.
704 - - 872-7686 - - - --
N/A
-)
_ Area code Phone number
7. DISINFECTION:
2. WELL INFORMATION:
(Amount of 65°/n75% calcium hypochiorite used)
SITE WELL ID # (if applicable) B-12
8. SEALING MATERIAL:
Neat Cement Sand CPmPnt
STATE WELL PERMIT # (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
Water gal. Watergal.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonite 300•e lb.
WELL USE (Check applicable usey.. Monitoring ❑ Residential
Type: ❑ Slurry ❑ Pellets
❑ Murilcipal/Public ❑ Industrial/Commercial ❑ Agricultural
Water gal.
Recovery tG Injection ❑ Irrigation
Other
❑ Other (fist use)
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Slreel/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) :
- TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley V Flat ❑ Ridge❑ Other
- (Check appropriate setting)
: 10. WELL DIAGRAM :Draw a detailed sketch of the -lion the back of this
- - -
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 35 -45 56.6500 ^ DMS OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 __ 55 • 2.5700 ^ DMS OR DD
types of fill materialsised
Lalitudenongitude source: RJ�PS C Topographic map
12/13/12
(location of well must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form if not using GPS)
100 HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF
4a. FACILITY -The name or the business where the well is located. Complete 4aIS
(If a residential well, skip 4a; complete 4b, well owner information only)
HAS $EEN P(�VIDEO WELL OWNER.
_7L
FACILITY ID# (if applicable)
/!!+ CA�++/j a�J\
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28577
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town Slate Zip Code
(The private well owner must be an individual w ersonal bandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSON/WELL OWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Form GW-30
Rev. 5/10

NON-RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department orEnvironment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
�''......,- -
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
d. TOP OF CASING IS 0.0 FT. Above Land Surface*
'Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): N/A METHOD OF TEST N/A
f. DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
2. WELL INFORMATION:
: 7. CASING:
Depth
Diameter Weight Material
WELL CONSTRUCTION PERMIT#
Top
Bottom
Ft.
OTHER ASSOCIATED PERMIT#(if applicable)
:Top
Bottom
Ft.
SITE WELL ID #(ir applicable) B-13
: Top
Bottom
Ft.
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
: 8. GROUT:
Depth
Material Method
IndustriallCommerciai ❑ Agricultural ❑ Recovery ❑ Injection V
Top
Bottom
Ft.
Irrigation❑ Other ❑ (list use)
: Top
Bottom
Ff.
DATE DRILLED 12/13/12
: Top
Bottom
Ft.
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY. STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley t;(Fiat ❑Ridge ❑Other
LATITUDE 35 ^ 45 56.6500 -DIVISOR DD
LONGITUDE 80 ° 55, 2.5700 ' DMS OR DO
Latitudellongitude source: W3PS propographle map
(location of well, must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town_
Stale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
U
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 41.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO Cl
c. WATER LEVEL -Below Top of Casing: 21.0 FT.
(Use "+' if Above Top of Casing) -
9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. in. in.
Top Bottom Ft. in. in.
Top Bottom Ft. in. In.
Ia. SANDIGRAVEL PACK:
Depth Size
Top Bottom Ft.
Top Bottom FL
Top Bottom Ft.
11. DRILLING LOG
Top Bottom
0.0 / 41.0
12. REMARKS:
Material
. Formation Description
DIRECT PUSH
100 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. ANQ THAT A COPY OF THIS
RECOR iAS BEEN PROVIDE To THE�l1 E.LL OWNER.
i�ru" 7 • / o Cpq 4� 01/17/13
SIGNATURE OF C/ELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-ib
Rev. 2/09

.s. � �•C D 1,
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION
# 3552
1. WELL CONTRACTOR:.
6. WELL DETAILS:
VINCE FEDERLE
a.Total Depth 41.0 ft. Diameter. in.
Well Contractor (IndividuaQ Name
b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC
Measuring point is 0.0 fL above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
6. CASING: Length Diameter
Street Address
STATESVILLE NC 28625
a. Casing Depth (if known): NIA fL in.
City or Town Stale Zip Code
b. Casing Removed: NIA It. in.
704 1 872-7686
Area code Phone number
7. DISINFECTION: N/A
2. WELL INFORMATION:
(Amount of 65%75% calcium hypochlodte used)
SITE WELL ID # (if applicable) B-13
8. SEALING MATERIAL:
Neat Cement Sand Cement
STATE WELL PERMIT # (if applicable)
Cement lb. Cement Ib.
COUNTY WELL PERMIT # (if applicable)
Water gal. Water gal.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonile 300.0 lb.
WELL USE (Check applicable use).7 Monitoring 0 Residential
Type: 0 Slurry ❑ Pellets
0 Municipal/Public ❑ industrial/Commercial ❑ Agricultural
Water gal.
❑ Recovery M Injection ❑ Irrigation
Other
0 Other (list use)
Type material PORTLAND CEMENT
Amount 8.25 GALLONS
i
3. WELL LOCATION:
'
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Street/Road Name, Number, Community, Subdivision, Lot No.. Parcel, lip Code)
;
i
TOPOGRAPHC / LAND SETTING:
0 Slope 0 Valley IZ Flat I7 RidgeL7 Other
r
(Check appropriate setting)
10. WELL DIAGRAM : Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (if any) remaininE
i
LATITUDE 35 _^ 45 , 56.6500 DMS OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
�.
LONGITUDE 80 _ - 55 • 2.5700 [)MS OR DD
types of fill materials,sed
I
Latitude/ton ilude source: g 03PS []topographic map
(location of welt must be showB on a USGS topo map andattached to
11. DATE WELL ABANDONED 12/13/12
l
this form it not using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
:y
4a. FACILITY - The name of the business where the well is located. Complete 4a
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
THIS CO`RD, HAS BEEN
r
(If a residential well, skip 4a; complete 4b, well owner Information only.)
R ®VIDED TO THE WE��/LL/ OWNER.
` ���``�'�""
FACILITY ID #
1
Y ��?�7�X/l.C�
a
(if applicable)
NAME OF FACILITY MAYMEAD ASPHALT PLANT
01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE'
STREEtADDRESS 164.BOSTIAN BRIDGE DRIVE
'1=
f ' .
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an individual w orsonal bandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
.. 4b. CONTACT PERSON/WELL OWNER:
VINCE FEDERLE -
s"�`
"
NAME;'NCD.OT.
PRINTED NAME OF PERSON ABANDONING THE WE LL
r
STREET ADDRESS 164 BDSTIAN BRIDGE DRIVE STATESVILLE, NC 28577
_
- -
Ubinit a copg to tkle ownerrand the onglnal to Dl�islon,of WaterQua(tt�/ Informatt,p;eng, N
1:617rMal15eivfce Centdr, Ratetgh, NC 27699 1617, Phon
Form GW-30
Rev. 5110
:..,

V NN 7
'17-
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, ING
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-14
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industriai/Commercial ❑ Agricultural ❑ Recovery ❑ Injection a,
Irrigation❑ Other[] (list use)
DATE DRILLED 12/19/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope []Valley fir✓,FW ❑RIdge []Other
LATITUDE 35 ^ 45 •56.6500 "DMS OR 'Do
LONGITUDE 80 ^ 55 - 2.5700 " DMS OR DD
LaliludeAongitude source: VGPS propographic map
flocation of well must be shown on a USGS topo map andaltached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (f
applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
U
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 38.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO U/
c. WATER LEVEL Below Top of Casing: 21.0 FT
(Use -+" If Above Top of Casing) .
1 '4r ONRE,SZDiNTIAL WELL CONSTRUCTION RECORD
North Carolina Department orEnvironnlent and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # _ 3552
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Top of casing terminated at/or below land surface may require
a variance In accordance with 15A NCAC 2C .0118.
G. YIELD (gpm): N/A
METHOD OF TEST N/A
= f. DISINFECTION: Type
NIA
Amount NIA
g. WATER ZONES (depth):
: Top Bottom
Top Bottom
Top Bollorr
Top Bottom
Top Bottom
Top Bottom
Thickness/
: 7. CASING: Depth
Diameter
Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material Method
Top Bottom -
Ft.T
: Top Bottom
Ft.
Top Bottom
Ft.
9. SCREEN: Depth
Diameter
Slot Size Material
Top Bottom
Ft.
in. in.
Top Bottom
Ft.
in. in.
Top Bottom
Ft.
in. in.
- 10. SAND/GRAVEL PACK:
Depth
Size Material
Tap Bottom
Ft.
m Top Botto
Ft.
Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
Formation Description
0.0 / 38.0
DIRECT PUSH
12. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C. WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS
RECORD BEEN PROVIDED T THEW JI LL OWNER.
/17113
SIGNATURE OF CERTIFIED WELL CO - CT R 01DATE
VINCE FEDERLE
PRINTED NAME.QF PERSON CONSTRUCTING THE WELL
Form GW-1 b
Rev. 2/09

1� Ni.ST if''4`t•..
NT RECORD
WELL ABANDONME
North Carolina Department of Environment and Naturui Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
i. WELL CONTRACTOR: 6. WELL DETAILS-
VINCE FEDERLE a.Total Depth 38.0 ft. Diameter. in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC Measuring paint is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD = 6. CASING: Length Diameter
Street Address
STATESVILLE NC 28625 a. Casing Depth (if known): N/A fit. in.
City or Town _. -State Zip Code b. Casing Removed: N/A ft, in.
_ - - 7! 04 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-14
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable usep Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery M Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(Slreel/Road Name, Number, Community, Subdivision, Lot No., Parcel. Zip Code)
TOPOGRAPHC / LAND SETTING:
Slope ❑ Valley V Flat ❑ Ridge❑ Other -
(Check appropriate selling)
LATITUDE 35 45 • 56.6500 •DMS OR DD
LONGITUDE-80 55 , 2.5700 -DMS ..OR DD
Latitudeflon nude source• c7f--'PS pf hi
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb. Cement lb.
Water gal. Water oat.
Bentonite
Benlonile 300-0 lb.
Type: El Slurry ❑ Pellets
Water. gal.
Other
Type material PORTLAND CEMENT
Amount 7.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
10. WELL DIAGRAM : Draw a detailed sketch of lheell on the back of this
form showing total depth• depth and diameter of screens (if any) remaining
In the well, gravel interval, intervals of casing perforations, and depths and
types of fill malerialstsed
g opograp c map
(location of well must be shown on a USGS tope map andaltached to
11. DATE WELL ABANDONED 12119/1,2 _
this form if not using GPS)
100 HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
"
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
°. 4a. FACILITY - The name of the business where the well is located. Complete 4a:
1SSS ECORD HAS BEEN POVIDED TO�THE OWNER.
r (II a residential well, skip 4a; complete 4b, well owner Information only.)
WELL
`T
� •`L�2�7ia'/KX�
FACILITY ID # (if applicable)
V 7 01/17/13
NAME OF FACILffY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL . DATE
City or Town Stale Zip Code
(The private well owner must bean individual wdersonalltabandons hLJher residential well
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSONANELL OWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
`STREETADDRES5164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Su6mif a copy to fhe owner and the onglnal to Dlvlsron of Wafer Quality Information Processing,
A= Form GW-3O
;:'.1617 MaU Service Center,: E2ateigh, NC 27y699 1617, Phone {9 t9) 807 6300 Rev. 5/10

r, a.
A.
.ter 3.'y NON-RESIDENT)
North Carolina Department of Environme
'�,�" , ; .••;,�` WE, CONTRACTOR CERTIFI
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
P
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(ir appllcable) B-15
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Lei
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/13/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No.,.Parcel, Zip Code)
CITY; STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley UrFlat ❑Ridge ❑Other
LATITUDE 35 " 45 - 56.6500 " DMS OR DO
LONGITUDE 80 0 55 • 2.5700 " DMS OR DD
Latitude/longitude source: BPS ❑Topographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
NCDOT
Contact Name,;
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
L�
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 39.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO I ✓
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+" if Above Top of Casing)
A
L WELL CONSTRUCTION RECORD
nt and Natural Resources- Division of Water Quality
CATION # 3552
d. TOP OF CASING IS 0.0 FT. Above Land Surface*
'Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): N/A METHOD OF TEST N/A
f. DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thicknessf
: 7. CASING: Depth Diameter Weight Material
Top Bottom FL
Top Bottom Ft.
Top Bottom R.
:8. GROUT: Depth Material Method
Top Bottom Ft.
Top Bottom Fl.
Top Bottom Ft.
9. SCREEN: Depth Diameter Slot Size, Material
Top Bottom Ft. -In- in.
Top Bottom Ft. in. in.
Top Bottom Ft. In. In.
10. SAND/GRAVEL PACK:
Depth Size Material
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
11. DRILLING LOG
Top Bottom Formation Description
0.0 / 39.0 DIRECT PUSH
12- REMARKS:
106 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
:REC07 BEEN PROVIDED TO THE WELL OWNER.
01/17/13
SIGNA RTIFiED WEI!1t!4WNTV.4WM DATE
VINCE FEDERLE
: PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Fort GW-1 b
Rev. 2/09

STArfa`'b\
1. WELL CONTRACTOR:
VINCE FEDERLE
WELL ABANDONMENT RECORD
North Carolina Department or Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
s. WELL DETAILS:
a.Total Depth. 39.0 ft. Diameter. in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC Measuring point Is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 1 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-15
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)❑ Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery Z Injection ❑ irrigation
❑ Other Oust use)
6. CASING:
Length Diameter
a. Casing Depth Of known):-
NIA ft. in.
b. Casing Removed:
NIA ft. in.
- 7. DISINFECTION: NIA
(Amount of 650/675% calcium
hypochlonte used)
8. SEALING MATERIAL:
Neat Cement
Sand Cement
Cement -lb.
Cement - lb. _
Water gal.
Water clal.
Bentonite
Bentonite 300.0 lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT -
Amount 7.75 GALLONS
3. WELL LOCATION:
I
j
IREDELL
COUNTY QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Streel/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC I LAND SETTING:
❑ Slope ❑ Valley p Flat ❑ Ridge❑ Other
i
(Check appropriate selling)
: 10. WELL DIAGRAM : Draw a detailed sketch of th®ell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
!
LATITUDE 35 _^ 45 • 56.6500 • DMS OR DO
in the well, gravel Interval, intervals of casing perforations, and depths and
LONGITUDE 80 • 55, 2.5700 ^ DMS OR DO
types of fill materials,sed
Lalitudellongitude source: &63PS ❑ropographic map
12/13/12
`l
(location of well must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form ffnot using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
-
4a. FACILITY -The name of the business where the well is located. Complete 4a;'
(if a residential well, skip 4a; complete 4b, well owner information only.)
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
-Q110ECORD HAS BEEN PDVI D TO THE WELL OWNER.
�(ff(` -
-
FACILITY I # Of applicable)�Lj�
01/17/13
:I • : `
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS .164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE'
II�
City Or Town State Zip Code
(The Private well owner must be an individual w ersonall bandons his/her residential well .
J
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSON/WELL OWNER:
VINCE FEDERLE
NAME NCDOT
: PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
SubrniY a copy to the owner` and the onglna[ Eo Dlvtston of Water Quality tnformatlbn Processing, Form GW-30'
-
1617Mail Service Center= Raleigfi; NC 27699=1ti17, Phone . [phone]' Rev.5/10

xv w
�a STAin "A
P
NONRESIDENT]
i-' ; North Carolina Department of Environmei
WELL CONTRACTOR CERT(F
1. WELL CONTRACTOR:
VINCE FEDERLE
W611 Contractor (individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
CityorTown Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(ifapplicable)
SITE WELL ID #(if applicable) B-16
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery❑ Injection 91
irrigation❑ Other ❑ (list use)
DATE DRILLED 12/13/12 - 12/14/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel. Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC 1 LAND SETTING: (check appropriate box)
[]Slope ❑Valley SifFlat ❑Ridge ❑Other
LATITUDE 35 -45 56.6500 " DMS OR DO
LONGITUDE 80 ^ 55 • 2.5700 " DMS OR DO
Lalitudellongitude source: I,Z3PS Uopographic map
(location of well must be shown on a USGS topo map andaltached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Slate
Zip Code
NCOOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO Cv/
c. WATER LEVEL Below Top of Casing: 21.0 FT,
(Use'+" If Above Top of Casing)
A
.L WELL CONSTRUCTION RECORD
it and Natural Resources- Division of Water Quality
ICATION # 3552
d. TOP OF CASING IS 0.0 FT. Above Land Surface•
'Top of casing terminated atlor below land surface may require
a variance in accordance With 15A NCAC 2C .0118.
e. YIELD (gpm): N/A METHOD OF TEST N/A
L DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
: 7. CASING: Depth Diameter Weight Material
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
: 8. GROUT: Depth Material Method
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. -in. in.
Top Bottom Ft. in. in.
Top Bottom Ft. in. In.
10. SAND/GRAVEL PACK:
Depth Size
Top Bottom - Ft.
Top Bottom Ft.
Top Bottom Ft.
Material
11. DRILLING LOG
Top Bottom Formation Description
0-0 / 42.0
• 12. REMARKS:
DIRECT PUSH
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS
RECOR BEEN PROVIDED TO THE WELL OWNER
01/17/13
SIGNATORE OF CERTIFIED WCIL C TOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form G /U-1 b
Rev. 2/09

n
.3 WELL ABANDONME
RECORD
�i�1••t �„ ' -c°O' North Carolina Department of Environment
1•r +' ; •- • fir"
and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
s. WELL DETAILS:
VINCE FEDERLE
a.Total Depth 42.0 fL Diameter. in.
Well Contractor (individual) Name
b. Water Level (Below Measuring Point): 21.0 a.
GEOLOGIC EXPLORATION, INC
Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
6. CASING: Length Diameter
Street Address
STATESVILLE NC 28625
a. Casing Depth (if known): N/A R. in.
City or Town State Zip Code
b. Casing Removed: NIA ft. in.
704 ) 872-7686
Area code Phone number
7. DISINFECTION: N/A
2. WELL INFORMATION:
(Amount of 650/.75%a calcium hypochlodle used)
SITE WELL 1D # (if applicable) 8-16
= 8. SEALING MATERIAL:
Neat Cement Sand Cement
STATE WELL PERMIT# (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
Water gal. Water gal.
DWQ or OTHER PERMIT # (if applicable)
Bentonite
WELL USE (Check applicable use)-] Monitoring ❑ Residential
Bentonite 300-0 lb.
Type:0 Slurry ❑ Pellets
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
Water gal.
❑ Recovery M Injection ❑ Irrigation
Other
❑ Other (list use)
Type material PORTLAND CEMENT
3 WELL LOCATION
Amount 8.5 GALLONS
COUNTY IREDELL QUADRANGLE NAME
NEAREST -TOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley f/ Flat ❑ Ridge❑ Other
(Check appropriate setting)
10. WELL DIAGRAM : Draw a detailed sketch of lheell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 35 _^ 45 , 56.6500 • DMS OR OD
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 __ 55 - 2.5700 ^ DMS OR DD
types of fill materialsised
Latitudeflongitude source: 03PS Dropographic map
12/14l12
(location of well must be shown on a USGS topo map andattached to :
11. DATE WELL ABANDONED
this form if not using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
4a. FACILITY - The name of the business where the well is located. Complete 4a; :
WITH 15A NCAG 2C, WELL CONSTRUCTION STANDARDS, AND THATA COPY OF
THIS RECORD HAS BEEN PIDVIDED TO THE WELL OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.)
%FACILITY ID # (tf applicable)
61117/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE' NC 28677 :
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an individual wbersonalhabandons his/her residential wen
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSON/WELL OWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Form GW-30
Rev. 5110

„•',' as STAT n^`4Y
ties 3 _
.L Y ON -RESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
? ' "'k :J WELL CONTRACTOR cERTII• [CATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Sheet Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(irapplicable)
SITE WELL ID #(If applicable) B-17
3. WELL USE (Check One Box) Monitoring ❑ MLnicipal/Public ❑
IndustriallCommercial ❑ Agricultural ❑ Recovery ❑ Injection R(
Irrigation[] Other ❑ (list use)
DATE DRILLED 12114/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY; STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
[]Slope []Valley FiFlat ❑Ridge ❑Other
LATITUDE 35 ^ 45 ' 56.6500 ” DMS OR DO
LONGITUDE 80 0 55 • 2.5700 " DMS OR DO
Latitudetlongitude source: BPS Uopographic map
(location of well must be shown on a USGS topo map andattached to
this form ifnot using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
NIA
Facility Name
Facility ID# (if
applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
- STATESVILLE
NC
28677
City or Town
Stale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO LJ(
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+• if Above Top of Casing)
= d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Top of casing terminated attor below land surface may require
a variance 1n accordance with I SA NCAC 2C .0118.
e. YIELD (gpm): N/A METHOD OF TEST N/A
f. DISINFECTION: Type N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
: 7. CASING: Depth Diameter Weight Material
Top Bottom Fl.
Top Bottom Ft.
Top Bottom Ft.
: 8. GROUT: Depth Material Method
Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
: 9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. In. in.
Top Bottom Ft. in. in.
: Tap Bottom. Ft. in. in.
10. SAND/GRAVEL PACK:
Depth Size
Top Bottom Ft.
Top Bottom Ft.
Top . Bottom Ft.
11. DRILLING LOG
Top Bottom
0.0 / 42.0
r
12. REMARKS:
Material
Formation Description
DIRECT PUSH
:I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 29 WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
- RECORQ HP BEFtJ PROVIDED HE WEM OWN/ER. /f
V !/7r CZs✓fx t�Kt pllLQit,Yg— 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

WELL ABANDONMENT RECORD
North Carolina Department of Environment and Naluml Resources- Division of Water Quality
WELL CONTRACTOR CERTWICATION # 3552
1. WELL CONTRACTOR: s. WELL DETAILS:
VINCE FEDERLE a.Total Depth 42.0 ft. Diameter. in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 ft..
GEOLOGIC EXPLORATION, INC Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD 6. CASING: Lenqth Diameter
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-17 -
a. Casing Depth (if known): WA ft, in.
b. Casing Removed: NIA ft. in.
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlorite used)
: 8. SEALING MATERIAL:
Neat Cement 'Sand Cement
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (If applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable usef) Monitoring ❑ Residential
Municipal/Public D Industrial/Commercial ❑ Agricultural
❑ Recovery Z injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / (AND SETTING:
❑ Slope ❑ Valley G Flat ❑ Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 45 56.6500 ^ DMS OR DD
LONGITUDE 80 ° 55 ' 2.5700 ^ DMS OR .DD
Latitude/longitude source: lyr-PS Qro o ra hie ma
Cement lb. Cement lb.
Water gal. Water oat.
Bentonite
Sentonite 300A lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
10. WELL DIAGRAM :Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (If any) remaining
In the well, gravel interval, intervals of casing perforations, and depths and
types of fill malerialsised
p p F: 11. DATE WELL ABANDONED 12/14/12 .
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
I.DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a + THIS RECORD HAS BEEN POVIDED TO THE WELL OWNER.
(if a residential well, skip 4a; complete 4b, well owner information only.)
FACILITY ID # (if applicable) / n 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT sli TUR5 CERTIFIED W R DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677 : SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code (The private well owner must be an individual w gMgnap bandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSON/WELL OWNER: VINCE FEEJERLE
NAME NCDOT - PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE. NC 28677
Form GW-30
Rev. 5110

,pry �,1 SrAr�a
g
1. WELL CONTRACTOR: -
VINCE FEDERLE
Well Contractor (Individuan Name
GEOLOGIC EXPLORATION. ING
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-18 ?
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection d
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/19/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate lox)
[]Slope ❑Valley @(Flat ❑Ridge ❑Other
LATITUDE 35 ^ 45 56.6500 " DMS OR DO
LONGITUDE 80 0 55, 2.5700 " DMS OR DD
Latitude/longitude source: W3PS pfopographic map
(location of welt must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if
applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE--,-'
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
Area code Phone number
S. WELL DETAILS:
a. TOTAL DEPTH: 40.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO q/
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+• if Above Top of Casing)
NON-RESIDENTIAL WE, LL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
d. TOP OF CASING IS 0.0 FT. Above Land Surface*
'Top of casing lerminated at/or below land surface may require
a variance In accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): N/A
METHOD OFTEST N/A
L DISINFECTION: Type
N/A
Amount N/A
g. WATER ZONES (depth):
Top Bottom
Top
Bottom
Top Bottom
Top
Bottom
Top Bottom
Top
Bottom
Thickness/
7. CASING: Depth
Diameter
Weight Material
= Top Bollom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material
Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
:9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft.
in. in.
Top Bottom
Ft.
in. in.
Top Bottom
FL
in. in.
10. SAND/GRAVEL PACK:
"
. Depth
Size Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
Formation Description
0.0 / 40.0
DIRECT PUSH
/
12. REMARKS:
100 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
- REC RD S BEEN PR VIDEj�/Tj0 THE�L OWNER
(/xt 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
: PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-lb
Rev. 2/09

y;,•. srnTe�,
1 -fv�pr d ry '�•
1. WELL CONTRACTOR:
VINCE FEDERLE
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
s. WELL DETAILS:
a.Tolal Depth 40.0 f(, Diameter: In.
Well Contractor (individual) Name
b. Water Level (Below Measuring Point): 21.0 It.
GEOLOGIC EXPLORATION, INC
Measuring point is 0.0 IL above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
6. CASING: Length Diameter
Street Address
STATESVILLE NC 28625
a. Casing Depth (If known): N/A ft. in.
City or Town Stale Zip Code
b. Casing Removed: N/A ft. in.
704 ) 872-7686
NIA
i Area code Phone number
7. DISINFECTION:
I
(Amount of 65%75% calcium hypochlorite used)
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-18
i
: B. SEALING MATERIAL:
f
Neat Cement Sand Cempt
STATE WELL PERMIT # (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
Water gal. Water aal.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonite 3a-0 lb.
WELL USE (Check applicable use)D Monitoring ❑ Residential
Type: ❑ Slurry ❑ Pellets
❑ M uniclpallPublic ❑ Industrial/Commercial ❑ Agricultural.
Water gal.
1
❑ Recovery CG Injection ❑. Irrigation
Other
i ❑ Other (list use)
Type material PORTLAND CEMENT
Amount 8.0 GALLONS
3. WELL LOCATION:
ICOUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
t
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
i
TOPOGRAPHC / LAND SETTING:
i ❑ Slope D Valley LG Flat ❑ Ridge❑ Other
(Check appropriate setting) -
10. WELL DIAGRAM: Draw a detailed sketch of t1well on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 35 _^ 45 56.6500 • DMS OR DO
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _ ^ 55 , 2.5700 ° DMS OR DD
types of (6I materiaisrsed
} Latitude/longitude source: &!f,-PS Oropographic map
12/19/12
(location of well must be shown on a USGS topo map andatlached to
11• DATE WELL ABANDONED
this form if not using GPS)
li
t
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THATA COPY OF
j. 4a. FACILITY -The name or the business where the wep is located. Complete 4a;
(If a residential well, skip 4a; complete 4b, well owner Information only.)
TH RECORD HAS 8 N P®V ED TO THE WELL OWNER.
FACILITY ID # (if applicable)�?�7C�
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
- STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town Slate Zip Code ."
(The private well ownermusl be an individual wpersonalitabandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSONfWELL OWNER:
VINCE FEDERLE
" NAME NCDOT
_
PRINTED NAME OF PERSON ABANDONING THE WELL
STREET ADDRESS 161 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
.,,
..
Submita copyto the owner and the ong►nal_to Dtvlslon of Water Quality Information Processing, ,- Form GW-30
1617 Mai(Service Center; Raleigh,, NC 27699 9617, Phone [phone] ; ; . Rev. 5110

.�•••�SrAIl•`K`
Vd�e7 4 L�
3 " ' 1 i' ON-RESIDENTML WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CICATION # 3552
C>;RTIC
1 1 1
I. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
StreetAddress
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(If applicable)
SITE WELL ID #(If applicable) B-19
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Top of casing terminated allor below land surface may require
a variance in accordance With 15A NCAC 2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST N/A
E DISINFECTION: Type N/A Amount NIA
g.. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness!
7. CASING: Depth Diameter Weight Material
Top Bottom Ft. -
Top Bottom Ft.
Top BoUom Ft.
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑ : 8. GROUT: Depth Material Method
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Ci Top Bottom Ft.
Irrigation❑ Other ❑ (list use) ; Top Bottom Ft.
DATE DRILLED 12/14/12 : Top Bottom Ft.
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel -Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley VFiat ❑Ridge []Other
LATITUDE 35 ° 45 56.6500 "DMS OR DD
LONGITUDE80 " 55 1 2.5700 "DMS OR DD
Latitudeilongitude source: MPS aopographic map
(location ofwell must he shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
C-�
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 41.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO E/
c. WATER LEVEL Below Top of Casing: 21.0 FT -
(Use "+" if Above Top of Casing)
:9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. in. in.
Top Bottom FL in. in.
Top Bottom Ft. In. in.
10. SAND/GRAVEL PACK:
Depth Size
Top Bottom Ft.
Top Bollom Ft.
Top Bottom Ft.
11. DRILLING LOG
Top Bottom
0.0 / 41.0
12. REMARKS:
Material
Formation Description
DIRECT PUSH
1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NC C 2X, WELL CONSTRUCTJJJJJIQQQQQN STANRDS, AND THAT A COPY OF THIS
RECOR h S BEEN PR DED-PHE WEL(.JJWNN
oofl 77� 01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

sinrf�w�.,
r � �J!
�;: � w;a.cw•.:
1. WELL CONTRACTOR:
VINCE FEDERLE
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-19
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)!] Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial CI Agricultural
❑ Recovery 0 Injection ❑ Irrigation-
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE.DRIVE 28677
6. WELL DETAILS:
a.Total Depth 41.0 ft. Diameter. in.
b. Water Level (Below Measuring Point): 21.0 fL
Measuring point is 0.0 ft. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): N/A ft. in.
b. Casing Removed: NIA ft. in.
7. DISINFECTION: NIA
(Amount of 650/675% calcium hypochlorile used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb. Cement lb.
Water gat. Water gal.
Bentonite
Bentonite 300.0 lb.
Type. ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 8.25 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
t
(Streel/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) :
TOPOGRAPHC / LAND SETTING:
I
❑ Slope ❑ Valley rG Fiat ❑ Ridge❑ Other
I
(Check appropriate setting)
= 10. WELL DIAGRAM : Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 35 _^ 45 , 56.6500 - DM5 OR DD
in the well. gravel interval, intervals of casing perforations, and depths and
i
LONGITUDE 80 ° 55 - 2.5700 ^ DMS OR DO
types of fill malerials,sed
Lalitude/longilude source: V.GPS Qfopographic map
12/14/12
'•
(location of well must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form ifnot using GPS)
I
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY -The name of the business where the well is located. Complete 4a :
THI RECORD HAS BEEN POVIDED TO THE WELL OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.)
•
FACILITY ID# Of applicable)
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE "
j
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELLOWNER ABANDONING THE WELL DATE
I"
City or Town i . -- State Zip Code
(The private well owner must be an individdal ersonail bandons his/her residential wen
fo accordance with 15A NCAC 2C .0113.)
- 4b. CONTACT PERSON7WELL OWNER:
VINCE FEDERLE .'
NAME..NCDOT
-
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREETAODRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
ua}r Inrormauon rrocessmg ;:; Form GW-30
_ . Rev. 5/10

t � J
1��I-�� Ir �•
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 1 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-20
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
InduslrlaUCommercial ❑ Agricultural ❑ Recovery ❑ Injection 9(
Irrigation❑ Other ❑ (list use)
DATE DRILLED . 12/14/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley &Flat ❑Ridge []Other
LATITUDE 35 0 45 •56.6500 " DMS OR DO
LONGITUDE 80 a 55, 2.5700 " DMS OR DD
Latitude/longitude source: 03PS []Topographic map
(location of well must be shown on a USGS topo map andattached to
this font if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# Cif applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
f )
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 38.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NOW
c. WATER LEVEL Below Top of Casing: 21.0 FT
(Use '+" if Above Top of Casing)
NONRESIDENTIAL ONRESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTir,[CATION # 3552
• d. TOP OF CASING IS 0.0 FT. Above Land Surface`
'Top of casing terminated at/or below land surface may require
a variance in accordance with i5A NCAC 2C .0118.
: e. YIELD (gpin): NIA METHOD OF TEST N/A
f. DISINFECTION: Type NIA Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thicknesst
: 7. CASING: Depth Diameter Weight Material
Top Bottom Ft -
Top Bottom Ft.
Top Bottom Ft.
: 8. GROUT: Depth Material "" Method
- Top Bottom Ft. _
Top Bottom Ft.
Top Bottom Ft.
9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. In. in.
Top Bottom Ft. in. in.
Top Bottom Ft. in. in.
10. SAND/GRAVEL PACK:
Depth Size
Top Bottom FL
Top Bottom . Ft.
Top Bottom Ft.
Material
11. DRILLING LOG
Top Bottom Formation Description
0.0 / 38.0
/
12. REMARKS:
DIRECT PUSH
1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15ANCAC2C WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS
RECOR� BEEN PROVIDED T THE OWNER.
01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

k,-
fF�r"7 t
1. WELL CONTRACTOR:
VINCE FEDERLE
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
6. WELL DETAILS:
a.Total Depth 38.0 Ill. Diameter. in.
Well Contractor (Individuao Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (f applicable) B-20
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (If applicable)
DWQ or OTHER PERMIT # (if applicable)
—WELL USE (Check applicable use)9 Monitoring ❑ Residential
0 M unicipai/Public 0 Industrial/Commercial 0 Agricultural
0 Recovery 0 Injection ❑ Irrigation
Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
h. Water Level (Below Measuring Point): 21.0 ft.
Measuring point is 0.0 ft. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): NIA ft.
b. Casing Removed: N/A ft.
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlorite used)
8. SEALING MATERIAL.:
Neat Cement Sand Cement
Cement Ib. Cement lb.
Water gal. Water gal.
Bentonite
Senlonite 300.0 lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 7.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
(Street/Road Name, Number, Community, Subdivision. Lot No.. Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley V Flat ❑ Ridge❑ Other
(Check appropriate selling)
LATITUDE 35 _° 45 - 56.6500 ° DMS OR DD
LONGITUDE 80 ° 55 - 2.5700 ^ DMS OR DD
Lalilude/longitude source: &63PS Uopographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
in.
in.
10. WELL DIAGRAM : Draw a detailed sketch of ttleell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval• intervals of casing perforations, and depths and
types of fill matedals,sed
11. DATE WELL ABANDONED 12/14/12
100 HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a r
THIS CORD HAS BEEN POVIDED TO THE WELL OWNER.
(If a residential well, skip 4a: complete 4b, well owner information only)
�' �LOL
FACILITY ID # (if applicable)
F� 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR - DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an individual wbersonall�abandons his/her residential well
inaccordance wiihll5A NCAC 2C .0113_) -
4b. CONTACT PERSONMELL OWNER:
VINCE FEDERLE
-.:NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
'.STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Fort GW-30
Rev. 5110

i '.
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
,GEOLOGIC EXPLORATION, INC
Well Contractor Company Name _
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(ir applicable)
SITE WELL ID #(irapplicable) B-21
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Ed
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/17/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision. Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley ig'Flal []Ridge []Other
LATITUDE 35 ^ 45 • 56.6500 " DMS OR DD
LONGITUDE 80 " 55 2.5700 ^ DMS OR DD
Latitude/longitude source: BPS pfopographic map
(location of well must be shown on a USGS topo map andattached to
this form lfnot using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT NIA
Facility Name Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE - NC 28677
City or Town State Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC 28677
City or Town State Zip Code
U
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
c. WATER LEVEL Below Top of Casing: 21.0 FT
(Use "+" if Above Top of Casing)
NONRESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natuml Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
d. TOP OF CASING IS 0.0 FT. Above Land Surface
`Top of casing terminated allor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST N/A
E DISINFECTION: Type N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
7. CASING: Depth Diameter Weight Material
= Top Bottom Ft.
Top Bottom Ft.
Top Bottom Ft.
8. GROUT. Depth Material Method
Top Bottom Fl.
Top Bottom FL
Top Bottom Ft.
: 9. SCREEN: Depth Diameter Slot Size Material
Top Bottom FL_in. in.
Top Bottom Ft. in. in.
Top Bottom Ft. in. in.
10. SAND/GRAVEL PACK:
Depth Size
Top Bottom Ft.
Top Bottom Ft.
Top Bottom FL
Material
11. DRILLING LOG
Top Bottom Formation Description
0.0 / 42.0
12. REMARKS:
DIRECT PUSH
• 1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
E D HAS BEEN PROM O TO TWELLOWNER.
- 1LLZCONTRA(5T=0—R
01/17/13
SIGNATURE OF CERTIFIED DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

Y
"
A
C� 11 Or
•y.,,N
VL.4'H'�C4
1
1. WELL CONTRACTOR:
VINCE FEDERLE,
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 26625
City or Town State Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-21
STATE WELL PERMIT # (if applicable)
S. WELL DETAILS:
a.Total Depth 42.0 ft. Diameter in.
b. Water Level (Below Measuring Point): 21.0 ft.
Measuring point is 0.0 ft. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): N/A ft. in.
b. Casing Removed: N/A ft. in.
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable) Water gal. Wafergal.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonite 300.0 lb.
WELL USE (Check applicable used Monitoring ❑ Residential
Type:O Slurry ❑ Peliels
0 M unicipal/Public 0 Industrial/Commercial ❑ Agricultural Water gal.
0 Recovery M Injection 0 Irrigation Other
❑ Other (list use) Type material PORTLAND CEMENT
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
Amount 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
(Street/Road Name, Number, Community. Subdivision. Lot No., Parcel, Zip Code) ;
TOPOGRAPHC l LAND SETTING:
❑ Slope 0 Valley 121 Flat 0 RidgeO Other
(Check appropriate setting)
: 10. WELL DIAGRAM : Draw a detailed sketch of theall on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE _35 45 , 56.6500 ° DMS OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _ 55 - 2.5700 ^ DMS OR DD
types of fill materialsised
Latitudellongilude source: S63PS propographic map
11. DATE WELL ABANDONED 12/17/12
(location of well must he shown on a USGS topo map andattached to
this roan if not using GPS)
100 HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
: WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THATA COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a;
THIS RECORD HAS BEEN POVIDED TO THE WELL OWNER.
(If a residential wen, skip 4a; complete 4b, well owner Information only.)
FACILITY ID # (if applicable)
Q� �p� 0 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CON RACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must bean Individual whqrsonall bandons his/her residential well
in accordance. with 15A NCAC 2C .0113.)
4b. CONTACT PERSONANELL OWNER:
VINCE FEDERLE
NAME . NCDOT '
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
quauty ; intormation rrocessing . Form GW-30
r , Rev. 5/10
a

9,�e,k 4+tx�p rr
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name .
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 ) 872-7686 - - -- - T
Area code Phone number _
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #of applicable) B-22
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industdal/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Ef
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/17/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY; STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley KdFlal ❑Ridge ❑Other
LATITUDE 35 " 45 ' 56.6500 " DMS OR DD
LONGITUDE 80 ^ 55 , 2.5700 " DMS OR DD
Latitudeilongitude source: MPS (]Topographic map
(location of well must be shown on a USGS topo map andattached to
this form ifnot using GPS) _- -
S. FACILITY (Name of the business where the well Is located.)
MAYMEAD ASPHALT PLANT N/A
Facility Name Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE -
Street Address
STATESVILLE NC 28677
City or Town State Zip Code
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC 28677
City or Town Stale Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO C/
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+" if Above Top of Casing) ,
NON .ES`IDENTIA L WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources -Division of Water Quality
- WELL CONTRACTOR CE, RTIFICATION # 3552
d. TOP OF CASING IS
0.0 FT. Above Land Surface'
*Top of casing terminated atfor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA
METHOD OF TEST N/A
- E DISINFECTION: Type
NIA Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
.Top Bottom
Thickness/
7. CASING: Depth
Diameter Weight Material
= Top Bottom
Ft.
Top Bottom
Fl.
Top Bottom
FL
8. GROUT: Depth
Material Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
:9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
A. in. in.
Top Bottom
Ft. in_ in.
Top Bottom
Ft. in. in.
10. SAND/GRAVEL PACK -
Depth
Size Material
Top Bottom
Ft
Top Bottom
Ft_
Top Bottom
Ft.
11. DRILLING LOG
Top Bottom Formation Description
0.0 / 42.0 DIRECT PUSH
12_ REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NNCC//llC 2C, WELL CONSTFFFFFFjjjjjj,,,,,,UCTIONSTANDARDS , AND THAT A COPY OF THIS
R4CQrt�BEENROTOTHE LL WN� VV Fnnrrllidid �D 01/17/13
- SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
rty =_ Information Processing,.: Rev.2/09

J
..tlh <iw rfi S
1. WELL CONTRACTOR:
VINCE FEDERLE
WELL ABANDONMENT RECORD
North Carolina Department of Environment rend Natural Resources- Division. of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
6. WELL DETAILS:
a.Total Depth 42.0 ft. Diameter. In.
Well Contractor (individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, ING Measuring point is 0.0 fL above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-22
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable) .
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)D Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery lG Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGIE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
G. CASING: Length Diameter
a. Casing Depth Of known): N/A ft, in.
b. Casing Removed: N/A ft. in.
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlorite used)
.8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb. Cement lb.
Water gal. Water oat.
Bentonite
Benlonile =-0 lb.
Type: ❑ Slurry ❑ Pellets
Water gal -
Other
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
(Streel/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) :
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley fG Flat ❑ Ridge❑" Other
(Check appropriate selling) 10. WELL DIAGRAM : Draw a detailed sketch of t1well on the back of [his
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 35 _• 45 , 56.6500 " DMS OR DO in the well, gravel interval, intervals of casing perforations, and depths and
'
LONGITUDE 80 • 55' - 2,5700 " DMS OR DD
types of fill materialsised
1
Latitude/longitude source: VGPS Oropographic map
12/17/12
(location of wet! must be shown on a USGS tope map andaRached to
11. DATE WELL ABANDONED
this form ifnot using GPS)
4 ' �•
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND THATA COPY OF
4a. FACILITY - The name of The business where the well is located. Complete 4a r
THIS RECORD HAS BEEN POVIDED TO THE WELL OWNER.
s!
(If a residential well, skip 4a; complele 4b, well owner information only.)
FACILITY ID # (if applicable)
01/17/13
.NAME OF FACILITY MAYMEAD ASPHALT PLANT .:
SIGNAT RTIFIED WELL CONTRACTOR DATE
("
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE
.:
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City,or Town - Slate Zip Code
(the private well owner must be an individual whersonalitebandons his/her residen[!at well
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSON/WELL OWNER:
VINCE FEDERLE
NAME NCDOT
- PRINTED NAME OF PERSON ABANDONING THE WE LL
:+
STREErADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE. NC 28677
Submit a copy to.1 the ownerand the or►glnal to Division of WaterQuahty Information Processing,y FormGiN-3o
_
Malf Service Center, Rale►gh, NC 27699 1617; Phdne (919) 807 630d Rev. 5110
,Fti17
r ,� ,

''�A4i' NONRESIDENT]
A�
North Carolina Department ofEnvironmel
�s'� •. ^:l air
WELL CONTRACTOR CERTIF
1. WELL CONTRACTOR:
JAMES HESS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Sheet Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(II applicable)
SITE WELL ID #(if applicable) B-23
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public D
industrial/Commercial ❑ Agricultural ❑ Recovery D Injection E�
IrrigationD Other D (list use)
DATE DRILLED 12/17/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley 'Q(Ftat DRidge ❑Other
LATITUDE 35 0 45 -56.6500 " DMS OR DD
LONGITUDE 80 ' 55 1 2.5700 " DMS OR' DD
Latitude/longitude source: ,(BPS Qfopographic map
(location of well must be shown on a USGS topo map andattached to
this form /f not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT N/A
Facility Name Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE NC 28677
City or Town Slate Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC 28677
City or Town State Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b_ DOES WELL REPLACE EXISTING WELL? YES ❑ NO E/
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+' if Above Top of Casing)
L WELL CONSTRUCTION RECORD
it and Natural Resources- Division of Water Quality
ICATION # 3550
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Top of casing terminated al/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST NIA
L DISINFECTION: Type NIA Amount N/A
g. WATER ZONES (depth):
: Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
: 7. CASING: Depth Diameter Weight Material
Top Bottom Ft.
Top Bottom Ft_
Top Bottom Ft.
: 8_ GROUT: Depth Material Method
Top Bottom Ft_
Top Bottom FL
Top Bolton FL
9. SCREEN: Depth Diameter Slot Size Material
Top Bottom FL in. In.
Top Bottom Ft. In. in.
Top Bottom Ft. in. In.
10. SANDIGRAVEL PACK:
Depth Size
Top Bottom Ft_
: Top Bottom Ft_
Top Bottom Ft.
Material
11. DRILLING LOG
: Top Bottom Formation Description
0.0 / 42.0
12. REMARKS:
DIRECT PUSH
• 1-HE
..,REBYCERTI THAT THIS WELL WAS CONSTR O IN ACCORDANCE WITH
• 1AC 2C, WE ONSTRUCTTII 1J'1 SW11
ARDS, AN AT A COPY OF THIS
RECORD HAS B PROVIDE O�Q THE OWNER
/» 01/17/13
SIGNA E OF CERTIFIED WELL C NTRACTOR DATE
JA rES HESS
: PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

WELL ABANDONMENT RECORD
o=
North Carolina Department of Environment and Natural Resources- Division of Water Quality
=-tiVGLL CONTRACTOR CGRTII+ICAT[ON # 3550
1. WELL CONTRACTOR:
' JAMES HESS.- -- - Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC -
Well Contractor Company Name
176 COMMERCE BLVD
-- Street Address
STATESVILLE. NC 28625
City or Town== - - - State Zip Code
_ 704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-23
-_ STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)-] Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery 0 Injection ❑ Irrigation -
❑ Other (list use)
3. WELL LOCATION: -
COUNTY IREDELL QUADRANGIE NAME
'NEAREST TOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
-__ :-_ _ (Slreel/Road Name, -Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:-
❑ Slope ❑ Valley Vi Flat ❑ Ridge❑ Other
(Check appropriate selling)
-LATITUDE 35. ^45 56.6500 • DMS OR DD
LONGITUDE 80 ^ 55 2.5700 • DMS OR DD
S. WELL DETAILS:
a.Total Depth 42.0
ft. Diameter. In.
b. Water Level (Below Measuring
Point):- 21.0 ft.
Measuring point is 0.0
ft. above land surface.
6. CASING:
Length Diameter --
a. Casing Depth (f known):.
NIA ft. in.
b. Casing Removed:
N/A ft. in.
7. DISINFECTION: NIA
(Amount of 651/675% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb. Cement lb.
Water gal. Water oat.
Bentonite
Bentonite 700.0 lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
10. WELL DIAGRAM : Draw a detailed sketch of tiieell on the back of this
- form showing total depth, depth and diameter of screens (f any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill material3,sed
Latilude/longitude source: 663PS propographic map 12/17/12
(location of well must be shown on a USGS topo map andattached to - 11. DATE WELL ABANDONED
this form if not using GPS)
4a. FACILITY - The name of the business where the well Is located. Complete 4a
(If a residential well. skip 4a; complete 4b, well owner information only.)
FACILITY ID # (if applicable) '
NAME OF FACILITY MAYMEAD ASPHALT PLANT
STREETADDRESS 164-BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
City orTown Stale Zip Code
4b. CONTACT PERSONANELL OWNER:.
NAME -NCDOT
STREETADDRESS
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C LL CONSTRUCTION STAND S.
AND THATA COPY OF
THIS RECORD EEN PSTD TN HE WELL ER.
/,Jn�Jt f� 01/17/13
SIGNATUY
OF CERTIFIED WELL CONTRACTOR DATE
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
(The private well owner must be an Individual wbersonall�l3abandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
JAMES HESS
PRINTED NAME OF PERSON ABANDONING 11Ht vve LL
164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677 -
Form GW-30
Rev. 5L10

�d r.0
NONI&SIDENTIAL WELL CONSTRUCTION RECORD
S
North Carolina Department of Environment and Natural Resources- Division of Water Quality
,,� �•1• c
1 �rF
WELL CONTRACTOR CERTIFICATION it3550
1. WELL CONTRACTOR:
JAMES HESS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Narne
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(ir applicable)
SITE WELL ID #(it applicable) B-24
3. WELL USE (Check One Box) Monitoring ❑ MunicipaltPubiic ❑
InduslriallCommercial ❑ Agricultural ❑ Recovery ❑ Injection Rr
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/17/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC 1 LAND SETTING: (check appropriate box)
❑Slope ❑Valley QfFiat []Ridge ❑Other
LATITUDE 35 " 45 - 56.6500 " DMS OR DO
LONGITUDE 80 ^ 55 :, 2.5700 " DMS OR DD
Latitude/longitude source: U3PS pfopographic map
(location of well must be shown on a USGS topo map andaltached to
this form ifnot using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT N/A
Facility Name Facility ID# (f applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE NC 28677
City or Town State Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC 28677
City or Town Stale Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO C✓
c. WATER LEVEL Below Top of Casing: 21.0 FT
(Use "+' if Above Top of Casing)
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
"Top of casing terminated at/or below land surface may require
a variance in accordance with IBA NCAC 2C .0118.
e. YIELD (gpm): N/A METHOD OF TEST N/A
f. DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Boltom
Top Boltom
Top Bottom
Top
Bottom
Top
Bottom
Top
Bottom
Thickness/
7. CASING: Depth
Diameter
Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
: 8. GROUT: Depth
Material
Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft.
In.
in.
Top Bottom
Ft.
in.
in.
Top Bottom
Ft.
in.
in.
- 10. SAND/GRAVEL PACK:
Depth
Size
Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
0.0 ! 42.0
12. REMARKS:
Formation Description
DIRECT PUSH
• 1 DO HEREBY E'r{TIF¢CYGQTH�AT-THITW ttyyADDSCONST TED IN ACCORDANCE WITH
: R CORDC Z f;kf�l+iIDE�TO TH1.71 S, R lHAT A COPY OF THIS
01/17/13
SIG TURE OF CERTIFIED WELL CONTRACTOR DATE
JAMES HESS
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GWAb
Rev. 2/09

�c,,l��% �FV3•;
1i 11�
•R'�v.�w.u.r�•;'
1. WELL CONTRACTOR:
JAMES HESS
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION #
Well Contractor (IndividuaQ Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28525
City or Town Slate Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-24
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable usep Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery M Injection ❑ Irrigation
❑ Other (list use)
3550
S. WELL DETAILS:
a.Tolal Depth 42.0
ft. Diameter in.
b. Water Level (Below Measuring Point): 21.0 R
Measuring point is 0.0
ft. above land surface.
6. CASING:
Length Diameter
a. Casing Depth (if known):
N/A ft. in.
b. Casing Removed:
N/A ft. in.
7. DISINFECTION: NIA
(Amount of 650/675% calcium hypochlorite used)
: 8. SEALING MATERIAL:
Neat Cement Sand Cem�t
Cement lb. Cement lb.
Water gal. Water gal.
Bentonite
Bentonite _ -3�:o lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE 9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677 TREMIE
(SlreettRoad Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley V Flat ❑ Ridge❑ Other
(Check appropriate setting) 10. WELL DIAGRAM : Draw a detailed sketch of Itleell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 35 _' 45 56.6500 • DM5 OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _ ^ 55 2.5700 • [)MS OR DD
types of fill materials,sed
Lalitude/longilude source: MPS pfopographic map
12/17/12
(location ofwefl must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form if not using GPS)
I DO HERI.8Y CE IFY THAT THIS WELL WAS ABAN ONED IN ACCORDANCE
WITH 15A NCAC ,WELL CONSTRUCTION STAN RDS, AND THAT A COPY OF
'.
'
4a. FACILITY - The name of the business where the well is located. Complete 4a;
(If a residential well. skip 4a: complete 4b, well owner information only.)
: THIS RECORD/AS BEEN PrDE13%rp THE WE OWNER.
N�
I'
FACILITY ID # (if applicable)
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGN RE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town Slate Zip Code
(The private well owner must be an individual w ersonall bandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
r:
4b. CONTACT PERSONiWELL OWNER:
DAMES HESS
NC
NAME: I
: PRINTED NAME OF PERSON ABANDONING THE WE LL
SfiREETADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
=
Submit a copy to the owner and the original to Otvfston of Water Qua(It' Information Processing, ° GW-30
Form
9617 Mall Service Center,'Ralelgh, NC 27699 iti17, Phone 9,19 :807 6300 `� } r •, Rev. 5l10
l
., •• •. \

A,crvrj
1. WELL CONTRACTOR.
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(it applicable)
SITE WELL ID #(if applicable) B-25
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection N
Irrigation[] Other ❑ (list use)
DATE DRILLED 12/17/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: ' STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley VFlat ❑Ridge []Other
LATITUDE 35 " 45 - 56.6500 " DMS OR DD
LONGITUDE 80 " 55 , 2.5700 " DMS OR DD
Latitudellongilude source: BPS Qfopographle map
(location of well must be shown on aUSGS topo map andattached to
this form if not using GPS) _
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT NIA
Facility Name Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE NC - 28677
City or Town Slate Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC 28677
City or Town State Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: - 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+" if Above Top of Casing)
NON ESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
d. TOP OF CASING IS 0.0 FT. Above Land Surface*
'Top of casing terminated allor below land surface may require
a variance In accordance with 15A NCAC 2C .011 B.
e. YIELD (gpm): NIA
METHOD OF TEST N/A
f. DISINFECTION: Type
N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness/
T. CASING: Depth
Diameter Weight Material
Top Bottom
Ft.
Top Bottom
R.
Top Bottom
Ft.
: 8. GROUT: Depth
Material Method
- Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
FL
9. SCREEN: Depth
Diameter SlotSlze Material
Top Bottom
Ft. In. in.
Top Bottom
Ft. in. in.
Top Bottom
Ft. in. in.
- 10. SANDIGRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top Bottom
Fl.
Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
Formation Description
0.0 / 42.0 DIRECT PUSH
/
12. REMARKS:
• 100 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECOR HAS BEEN PROVIDED TO THE WELL OWNER.
�7 _ ? �, /% 01/17/13
SIGN CER IFIED L R DATE
VINCE FEDERLE
- PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev, 2109

Aj
WELL ABANDONMENT RECORD
ib
North Carolina Department of Environment and Natural Resources- Division of Water Quality
-WELL CONTRACTOR CERTIrICATION # - 3552 -
1. WELL CONTRACTOR: _ _ _ - _ ._ - - _ •_. 5. WELL DETAILS:
_ _VINCE FEDERLE — -_ = =_ a.Total Depth 42.0 R. Diameter. In.
Well Contractor (Individual) Name _ - b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC - Measuring point Is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD -6. CASING: Length Diameter
- - Street Address
STATESVILLE: - ' - NC 28625 a. Casing Depth (if known): NIA g,_ in.
_ - City of Town- - - - - -- -- - - - State Zip Code b. Casing Removed: N/A ft. in.
-- - - 1
704= _ =872=7686
Areac d__P_(A
Phone - - 7. DISINFECTION: N/A
- mount of 65%75% calcium hypochlorite used)
2. WELL INFORMATION:
SITE WELL ID # (ifapplicable)
8-25 8. SEALING MATERIAL:
STATE WELL PERMIT# ((fapplicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable usep Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery M Injection ❑ Irrigation
0 Other (list use)
3, WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(StreetlRoad Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) :
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley [/, Flat ❑ Ridge❑ Other
Neat Cement Sand Cement
Cement lb. Cement lb.
Water gal. Water oat.
Bentonite
Sentonite Me lb.
Type: ❑ Slurry 0 Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
_ (Check appropriate setting)
10. WELL DIAGRAM :Draw a detailed sketch of theell on the back of this
_
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE _35_ _= 45 56.6500 DMS OR DD
'in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _ 55 - 2.5700 - DMS OR DD
types of fill materialsrsed
Latiiudenongitude source: A. -PS propographic map
12/17/12
(location of well must be shown on a USGS topo map andattached to
- 11. DATE WELL ABANDONED
this form if not using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH t 5A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF -
4a. FACILITY - The name of the business where the well is located, Complete 4a ;
THIS RE OR-D HASOWNER.
BEEN POVIDED TO THE WELL OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.)il>z
FACILITY ID # (if applicable)
p 01/17/13
CrE�/f CX�
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an individual wbersonalhabandons his/her residential well
in accordance with 15ANCAC 2C .0113.)
4b. CONTACT PERSON/WELL OWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOS11AN BRIDGE DRIVE STATESVILLE, NG20677
Form GW-30
Rev. 5110

NONRESIDENTIAL ONRESIDENTIAL WELL CONSTRUCTION RECORD
Nortli Carolina Department ofEnvironment and Natural Resources- Division of Water Quality
RT[FICATION#
3552WELL CONTRACIOiCE
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872, 7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-26
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
IndustrialtCommercial ❑ Agricultural ❑ Recovery ❑ Injection f�
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/17/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY; STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope []Valley en Flat ❑Ridge ❑Other
LATITUDE 35 ^ 45 56.6500 - DMS OR DO
LONGITUDE 80 ^ 55 , 2.5700 " DMS OR DD
Latitudellongitude source: I0GPS . pfopographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677-
City or Town
State
Zip Code
l)
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO L�
c. WATER LEVEL Below Top of Casing: 21.0 FT,
(Use '+' if Above Top of Casing)
d. TOP OF CASING IS 0.0 FT. Above Land Surface`
'Top of casing terminated at/or below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpin): N/A METHOD OF TEST N/A
f. DISINFECTION: Type N/A Amount NIA
g. WATERZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bolton Top Bottom
Thickness/
:7. CASING: Depth Diameter Weight Material
Top Bottom Ft.
Top Bottom FL
Top Bottom Ft.
8. GROUT: Depth Material Method
Top Bottom FL
Top Bottom Ft.
Top Bottom Ft.
: 9. SCREEN: Depth Diameter Slot Size Material
Top Bottom FL In. in.
Top Bottom Ft. in. In.
Top Bottom Ft. in. in.
10. SAND/GRAVEL PACK:
Depth Size Material
Top Bottom Ft.
Top Bottom Ft.
Top Bottom FL
11. DRILLING LOG
Top Bottom Formation Description
0.0 / 42.0 DIRECT PUSH
/
12. REMARKS:
100 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RE OR S BEEN PROVID TO THE LL OWNER.
01/17/13
- SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
: PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1ii
Rev. 2109

srnt
WELL ABANDONMENT RECORD
i i i
North Carolina Department olEnvironment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor. Company Name
176 COMMERCE BLVD
Sheet Address
STATESVILLE NC 28625
S. WELL DETAILS:
a.Tolal Depth 42.0 ft. Diameter. in,
b. Water Level (Below Measuring Potnl): 21.0 ft.
Measudng point is 0.0 ft. above land surface. -
6. CASING: Length Diameter
a- Casing Depth Of known): NIA ft.
City or Town State Zip Code U. Casing Removed: N/A ft.
704 1 872-7686 7. DISINFECTION: N/A
Area code Phone number
(Amount of 65%75% calcium hypochlorite used)
2. WELL INFORMATION:
SITE WELL ID # (if applicable)
B-26 : 8. SEALING MATERIAL:
Neat Cement Sand Cement
STATE WELL PERMIT # (If applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # Cf applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable usef] Monitoring 0 Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery ,G Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(Streel/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) :
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley G, Flat ❑ Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 0 45 56.6500 ^ DMS OR DO
LONGITUDE 80 - 55 2.5700 ^ DMS OR DO
Latitudellongitude source: Rf�PS Qlopographic map
flocalion of well must be shown on a USGS topo map andattached to
this form it not using GPS)
Water gal. Watergal.
Bentonite
Bentonite a000 lb.
Type:❑ Slurry ❑Pellets
Water gal.
Other
Type material PORTLAND CEMENT
n— -f 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
in.
in.
10• WELL DIAGRAM Draw a detailed sketch of thee8 on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materialsised
11. DATE WELL ABANDONED,
12/17/12
: 1 DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
" ?
4a- FACILITY -The name of the business where the well is located. Complete 4a i
THIS f3ECORDHASBEEN P®VIDEO TO THE WELL OWNER.
1
(If a residential well, skip 4a; complete 4b, well owner information only.)
��p AV
FACILITY. ID# (if applicable)- _ -
— 01/17113
'
- ..-NAME OF FACILITY MAYMEAD ASPHALT PLANT
: SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
. ..
' STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an individual wbersonalkebandons his/her residential well. -
in accordance with 15A NCAC 2C .0113.)
4b, CONTACT PERSONlWELL OWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
I
STREET ADDRESS 164-BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Submit a�copy fo the owner and the original to Division of
' - •- -
Water Quality Information Processing, +` Form GW-30
I". L 1.....
1
1617•.M If le Cehteh••Ralei ih NC 27699'.9697. Phone : (919i807.'6300
_> _ ... _ _" __. !. ;_ ..:= Rev. 5110

i vA °ra nA�o � j
7 1 `Y ONRESIDENTIAL WELL CONSTRUCTION RECORD.
•`' ; 'y o� North Carolina Department of Environment and Natural Resources- Division of Water Quality
""u�'.•r WELL CONTRACTOR CERTIFICATION # 3552
W..
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(it applicable)
SITE WELL ID #(if applicable) B-27
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection fft
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/17/12 - 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community. Subdivision. Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope []Valley VFlal ❑Ridge ❑Other
LATITUDE 35 ° 45 - 56.6500 " DMS OR DD
LONGITUDE 80 - 55 , 2.5700 " DMS OR DD
Latitude/longttude source: BPS pfopographic map
(location of well must be shown on a USGS topo map andaltached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Slate
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
L�
Area code Phone number
G. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO Ei✓
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+" if Above Top of Casing),
d. TOP OF CASING IS
0.0 FT. Above Land Surface'
'Top of casing terminated at/or below land surface may require
a variance in accordance With 15A NCAC 2C .0118.
e. YIELD (gpm): N/A
METHOD OF TEST N/A
L DISINFECTION: Type
N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Tap Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness/
:7. CASING: Depth
Diameter Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
: 8. GROUT: Depth
Material Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft. In. in.
Top Bottom
Ft. in. in.
Top Bottom
Ft. in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
11. DRILLING LOG
: Top Bottom
0.0 / 42.0
1
/
12. REMARKS:
Formation Description
DIRECT PUSH
' 100 HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C. WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECO�RD% BEEN PR�tOVIDED O THE LL OWNER.
�J
V BEEN
01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE.
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2109

i
-
I T• ��'t -_ WELL ABANDONMENT RECORD
o:
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION !# . 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
_ - -Street Address
STATESVILLE NC 28625
== City or Town- - State Zip Code
704 872 7686
s. WELL DETAILS:
a.Total Depth 42.0 ft. Diameter. in.
b. Water Level (Below Measuring Point): 21.0 ft.
Measuring point is 0.0 ft, above land surface.
S. CASING: Length Diameter
a. Casing Depth Of known): NIA R in.
b. Casing Removed: NIA ft. in.
Area code Phone number 7. DISINFECTION: NIA
2. WELL INFO(Amount of 65%75% calcium hypochlorile used)
RMATION:
B-27 : 8. SEALING MATERIAL:
-- - _-- -- - SITE WELL ID # (if applicable)
Neat Cement Sand Cement
STATE WELL PERMIT # Of applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable) Water gal. Watergal;
Bentonite -
DWQ or OTHER PERMIT # (if applicable)
Bentonite Man lb.
WELL USE (Check applicable use)'] Monitoring ❑ Residential
Type:❑ Slurry ❑ Pellets
D Municipal/Public ❑ Industrial/Commercial ❑ Agricultural Water gal.
❑ Recovery. 0 Injection ❑ Irrigation Other
❑ Other (list use) Type material PORTLAND CEMENT
A 1 8.5 GALLONS
3. WELL LOCATION:
noun
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC / LAND SETIING9 -
EJ Slope ❑ Valley V Flat D RidgeD Other
(Check appropriate setting)
10. WELL DIAGRAM :Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens Of any) remaining
LATITUDE 35--- _^ 45 , 56.6500 - ^ DMS OR DO
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _ ^ 55 - 2.5700 - DMS OR DO
types of fill materialsised
Lalitude/longilude source: Rf.PS Dropographic map
12/18/12
(location of well must be shown on a VSGS topo map andattached to
11. DATE WELL ABANDONED
this form if not using GPS)
: I DO HEREBY CERTIFY THATTHIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a i
(If a residential well, skip 4a; complete 4b,'Wbh owner information only.)
THIS CORD HAS BEEN RVIDE TO THE WELL OWNER.
FACILITY ID # (if applicable)
a���71 - 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
: SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
Clly or Town Slate Zip Code
(The private well owner must be an Individual w ersonal bandons his/her residential well
- in accordance with 15A NCAC 2C.0113.)
4b.CONTACT PERSONMELL OWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 161 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
hit`a copy`fo the owner and the or'lginal to Dwtsfon of Wafer Qualify iriformafIon Processing, Form GW-30
Mail Sernce Ce(lter Ralergfl NC 27699 1117' Phone [phone] r r Rev. 5110

NONRESIDENTIAL ONRESIDENTIAL WE, LL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
<f WELL CONTRACTOR CERTIFICATION #
� i' 3550
1. WELL CONTRACTOR:
JAMES HESS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMITNif applicable)
SITE WELL ID #(if applicable) B-28
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
IndustriallCommercial ❑ Agricultural ❑ Recovery ❑ Injection R(
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/17/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers. Community, Subdivision, Lot No., Parcel, Zip Code)
CITY. STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley SVFlat ❑Ridge ❑Other
LATITUDE 35 -45 - 56.6500 DMS OR DO
LONGITUDE 80 " 55 ' 2.5700 " DMS OR DO
Latilude/longilude source: 03PS pfopographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located_)
MAYMEAD ASPHALT PLANT NIA
Facility Name Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE NC 28677
City or Town State Zip Code
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC 28677
City or Town State Zip Code
U
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET .
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO L7�
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+" if Above Top of Casing)
d. TOP OF CASING IS
0.0 FT. Above Land Surface'
`Top of casing terminated at/or below land surface may require
a variance in accordance
with 15A NCAC 2C .0118.
e. YIELD (gpm): N/A
METHOD OF TEST. N/A
f. DISINFECTION: Type
N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness/
7. CASING: Depth
Diameter Weight Material
Top Bottom
Ft.
Top Bottom
FL
Top Bottom
Ft.
: 8. GROUT. Depth
Material Method
= Top Bottom
Ft.
Top Bottom
FL
Top Boltom
FL
9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
FL in. in.
Top Bottom
Ft. in. in.
Top Bottom
Ft. in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
FL
11. DRILLING LOG
Top Bottom
Formation Description
0.0 1 42.0
DIRECT PUSH
12. REMARKS:
' 100 HEREBY CE FY THAT THIS WELL WAS CONST TED IN ACCORDANCE WITH
• 15A NCAC 2C. LCONSTRWrTbN ! NOARDS. THAT A COPY OF THIS
RECORD DEEYTO THFiI vN
01/17/13
SIG ' URE OF CERTIFIED WELL CONTRACTOR DATE
JAMES HESS
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1 b
Rev. 2109

w"
3•
WELL ABANDONMENT RECORD
o;.
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3550
1. WELL CONTRACTOR:
s. WELL DETAILS:
JAMES HESS
a.Total Depth 42.0 ft. Diameter: in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 a.
GEOLOGIC EXPLORATION, ING Measuring point is 0.0 R. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 y 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-28
STATE WELL PERMIT # (if applicable)
6. CASING: Length Diameter
a. Casing Depth (f known): NIA g. in.
b. Casing Removed: WA ft. in.
7. DISINFECTION- WA
(Amount of 650/675% calcium hypochlorite used)
: 8. SEALING MATERIAL:
NP,•ttCerra? nt Sand Cement
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable) Water gal. Water __-__gal.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonite ana•a lb.
WELL USE (Check applicable Use)!] Monitoring ❑ Residential
Type:❑ Slurry ❑ Pellets
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural Water gal.
❑ Recovery 9 Injection ❑ Irrigation Other
❑ Other (list use) Type material PORTLAND CEMENT
n­,„t 8.5 GALLONS
3. WELL LOCATION:
COUNTY IREDELL QUADRANGIE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(Street/Road Name, Number, Community. Subdivision, Lot No., Parcel, Zip Code) -
TOPOGRAPHC / LAND SETTING: -
❑ Slope ❑ Valley G Flat ❑ Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 . ^ 45 - 56.6500 ' DMS OR DO
LONGITUDE 80 ^ 55 - 2.5760 DMS OR DD
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
10. WELL DIAGRAM : Draw a detailed sketch of lhsell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of rill materiaisised
Latttude/longilude source. PS pfopographic map
(location ofweU must be shown on a USGS topo map andattached to
- 11. DATE WELL ABANDONED 12/17/12
this form it not using GPS) .
: I DO HEREBY CE TIFY THAT THIS WELL WAS AB DOARDMED IN ACCORDANCE
WITH 15A NCA C, WELL CONSTRUCTION ST S, AND THAT A COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a;
THIS RECOR AS BEE DEtp )fTH W L OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.)
FACILITY ID # (if applicable)
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
: SIGN RE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE -DRIVE
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an individual wbersonalipbandons his/her residential well
' - - -
in accordance with 15A NCAC 2C .0113.)
4b-CONTACT PERSONANELL"OWNER:
JAMES HESS
NAME NCOOT.'
PRINTED NAME OF PERSON ABANDONING THE WE LL
c mccT nnnocec 164 BOSTIAN BRIDGE DRIVE STATESVILLE. NC 28677
-
Form GW-30
Rev. 5/10

N- ONRESIDENTML
fr I ` ;•.''
WELL CONSTRUCTION RECORD
North Carolina Deparhnent of Environment and Nntural Resources- Division of Water Quality
�o
V.
WELL CONTRACTOR CERTIFICATION # 3550
1. WELL CONTRACTOR:
JAMES HESS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 1 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(it applicable)
SITE WELL ID #(if applicable) B-29
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery❑ Injection Id
irrigation❑ Other ❑ (list use)
DATE DRILLED 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley &(Flat []Ridge ❑Other
LATITUDE 35 ° 45 56.6500 " DMS OR DO
LONGITUDE 80 ° 55, 2.5700 " DMS OR DE
Latitude/longitude source: BPS Qropographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS) -
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT N/A
Facility Name Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE NC 28677
City or Town State Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC 28677
City or Town Slate Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 32.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO C✓
c. WATER LEVEL Below Top of Casing: 21.0 Fr.
(Use'+" if Above Top of Casing)
d. TOP OF CASING IS 0.0 FT. Above Land Surface'
'Top of casing terminated aUor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
o. YIELD (gpm): N/A
METHOD OF TEST N/A
f. DISINFECTION: Type
N/A
Amount N/A
g. WATER ZONES (depth):
Top Bottom
Top
Bolcom
Top Bottom
Top
Bottom
Top Bottom
Top
Bottom
Thickness/
: 7. CASING: Depth
Diameter
Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
:8. GROUT: Depth
Material Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
:9. SCREEN: Depth
Diameter
Slot Size Material
Top Bottom
Ft.
in. in.
Top Bottom
Ft.
in. in.
Top Bottom
Ft.
in. in.
10. SANDlGRAVEL-PACK:
Depth
Size Material
Top Bottom
FL
Top Bottom
Ft.
Top Bottom
Ft.
- 11. DRILLING LOG
Top Bottom
Formation Description
0.0 / 32.0
DIRECT PUSH
/
: 12. REMARKS:
I DO HEREBY CER Y THAT THIS WELL WAS CONSTR ED IN ACCORDANCE WITH
• 11A NCAC 2C, CONSTR; N DARDS, A T A COPY OF THIS
RECORD Ftf� N PRO IDEJO THE LL O NE
01/17/13
: SIGN RE OF CERTIFIED WELL CONTRACTOR DATE
JA ES HESS
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2109

SfAT♦: as ,
a,:ar.
V Y��
rr w
WELL ABANDONMENT RECORD
�
�,, +•1 ' � t- North Carolina Department of Gnvironroent m1d Natural Resources- Division of Water Qualify
N•„„r
WELL CONTRACTOR CERTIFICATION # 3550
1. WELL CONTRACTOR:
5. WELL DETAILS:
JAMES HESS
a.Total Depth 32.0 ft. Diameter. in.
Well Contractor (Individual) Name
b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC
Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name =
176 COMMERCE BLVD
6. CASING: Length Diameter
Street Address
STATESVILLE-
NC 28625 a. Casing Depth Of known): N/A ft. in.
---- - City or Town - -- -
State Zip Code b. Casing Removed: NIA ft. In.
704 872-7686
NIA
Area a _Phone number
7. DISINFECTION:
_
(Amount of 65%75% calcium hypochlorite used)
2. WELL INFORMATION: -
SITE WELL ID # (if applicable) B-29
B. SEALING MATERIAL:
_
Neat Cement Sand Cement
STATE WELL PERMIT# (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # Of applicable)
WELL USE (Check applicable usep Monitoring ❑ Residential
❑ M unicipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery 0 Injection ❑ Irrigation
❑ Other (list use)
Cement lb. Cement lb.
Water gal. Water aat.
Bentonite
Bentonite 30-0 lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
6 5 GALLONS
3. WELL LOCATION:
Amount
COUNTY IREDELL QUADRANGLE NAME
-
NEAREST TOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
- - (Streel/Road Name, Number, Community, SubdlV6iDn, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC / LAND SETTING: --- — - - -
—
❑ Slope ❑ Valley V Flat ❑ Ridge❑ Other
-- (Check appropriate selling) _
10. WELL DIAGRAM.: Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE _35 -- _'-45 56.6500 • DMS-OR DD
-in [he well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _ 0 55 , 2.5700 • DMS OR DD
types of fill materialssed
Latitude/longitude source: RfGPS Qropographic map
12/18112
(location of well must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form if not using GPS)
- -
I DO HEREBY RTIFY THAT THIS WELL WAS A NDONED IN ACCORDANCE
WITH 15A N 2C, WELL CONSTRUCTIONS KNDARDS. AND THAT A COPY OF
4a. FACILITY -The name of the business where the well Is located_ Complete 4a
THIS REC HAS B P® TO THE LL OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.)
A �{%l%
FACILITY ID # (if applicable)
01/17/13
NAME OF'FACILITY MAYMEAD ASPHALT PLANT
SI ATURE OF CERTIFIED WELL CONTRACTOR DATE
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City of Town State Zip Code
(The private well owner must be an individual wbersonalhabandons his/her residential well
- in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSONIWELL OWNER: _
JAMES HESS
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WELL
STRUT ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE. NC 28677
Form GW-30
Rev. 5/10

��: siArEo
x �•{r'VV. 3.�_.�3E
1. WELL CONTRACTOR:
JAMES HESS
Well Contractor (individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(ir applicable) B-30
3. WELL USE (Check One Box) Monitoring ❑ MunicipaUPublic ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery D Injection
Irrigation[] Other ❑ (list use)
DATE DRILLED 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY. STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley tIFlat ❑Ridge ❑Other
LATITUDE 35 ^ 45 - 56.6500 " DMS OR DO
LONGITUDE 80 ^ 55 , 2.5700 " DMS OR DO
Latitude/iongitude source: [,BPS Oropographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS) - _
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
NIA
Facility Name
Facility ID# (f
applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
CityorTown
State
Zip Code
NCOOT
Contact Name
164 BOSTIAN BRIDGE DRIVE "
Mailing Address
STATESVILLE
NC
28677
City or Town
State .
Zip Code
U
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 38.0 FEET .
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO E/
c. WATER LEVEL Below Top of Casing: 21.0 FT
(Use "+" if Above Top of Casing)
NONRESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department orEnviroument and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 35SO
d. TOP OF CASING IS
0.0 FT. Above Land Surface'
*Top of casing terminated at/or below land surface may require
a variance in accordance vailh 15A NCAC 2C .0118.
e. YIELD (gpm): N/A
METHOD OF TEST N/A
f. DISINFECTION: Type
N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bollom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness/
7. CASING: Depth
Diameter Weight Material
Top Bottom
FL
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material Method
Top Bottom
FL_
Top Bottom
Ft.
Top Bottom
Ft.
9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft. in" in.
Top "Bottom
Ft. in. in.
Top Bollom
Ft. in" in.
10. SAND/GRAVEL PACK:
Depth Size
Top Bottom Ft.
Top Bolton Ft.
Top Bolcom Ft.
Material
11. DRILLING LOG
Top Bottom Formation Description
0.0 / 38.0 DIRECT PUSH
/
/
12. REMARKS:
• 100 HEREBY CFAIFY THAT THIS WELL WAS CONS CTED IN ACCORDANCE WITH
• 15A NCAC 2C,,VyELL CONS IHI nWP fANDAROS, D THAT A COPY OF THIS
: RECORD HA EEN P VIdEp TO
01/17/13
SIG URE OF CERTIFIED WELL CONTRACTOR DATE
JAMES HESS
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

`STnrfo"W
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water uali
WELL CONTRACTOR OR CERTIFICATION /# 3550
1. WELL CONTRACTOR:
JAMES HESS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Sheet Address,
STATESVILLE NC 28625
City or Town Slate Zip Code
704 1 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-30
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (f applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)7 Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
0 Recovery M Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGIENAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
S. WELL DETAILS:
a.Tolal Depth 38.0 It. Diameter: in.
b. Water Level (Below Measuring Point): 21.0 ft.
Measuring point is 0.0 ft, above land surface.
6. CASING: Length Diameter
a. Casing Depth Of known): N/A ft. in.
b. Casing Removed: N/A ft. in.
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlodte used)
: 8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb. Cement lb.
Water gal. Water gal.
Bentonite
Bentonite 30e•e lb.
Type: ❑ Slurry Cl Pellets
Water gal_
Other
Type material- PORTLAND CEMENT
Amount 7.5 GALLONS
S. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
(StreelfRoad Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
i
TOPOGRAPHC / LAND SETTING: -
❑ Slope ❑ Valley F/ Flat ❑ Ridge❑ Other
(Check appropriate setting) 10. WELL DIAGRAM : Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE _35_ 45 1 56.6500 - DMS OR DD in the well, gravel interval, intervals ofcasing perforations, and depths and
LONGITUDE 80 55 • 2.5700 ^ DM5 OR DD types of fill malerialsised
Latitude/longitude source: S633PS Qfopographic map 12/18/12
(location of well must be shown on a USGS topo map andattached to 11 • DATE WELL ABANDONED
this form ifnot using GPS)
I DO HEREBY ERTIFY THAT THIS WELL WAS ANDONED IN ACCORDANCE
WffH 15A C 2C, WELL CONSTRUCTION ANDARDS, AND THAT A COPY OF
4a. FACILITY - The name of the business where the well is located. Complete 4a i THIS REC D HAS 13G /C�lj O TH ^ LL OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.) '�QJ�1 Y /�{
FACILITY ID # (If applicable) 01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT 5 ATURE OF CERTIFIED WELL CONTRACTOR DATE
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677 : SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City Or Town Slate . Zip Code (The private well owner must he an individual w e sonal bandons his/her residential well
in accordance with 15A NCAC 2C .0113_)
4b. CONTACT PERSON/WELL OWNER: JAMES"HESS
NAME NCDOT PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 161 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
Form GW-30
Rev. 5110

.I NONRESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division Of Water Quality
•< ezWELT, CONTRACTOR CERTIFICATION # 35S2
k
' �-� `ter, . _
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Stale Zip Code
70( 4 f 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(it applicable)
SITE WELL ID #(inapplicable) B-31
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection d
Irrigaffon❑ Other ❑ (list use)
DATE DRILLED 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
[]Slope ❑Valley dFlat ❑Ridge ❑Other
LATITUDE 35 ^ 45 156.6500 " DMS OR DD
LONGITUDE 80 ^ 55 1 2.5700 " DMS OR DO
Latitude/longitude source: W3PS Qropographic map
(location ot-well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
- MAYMEAD ASPHALT PLANT NIA
Facility Name Facility ID# (if
applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE NC
28677
City or Town State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE NC
28677
City or Town Stale "
Zip Code
U
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 27.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑
NO G/
c. WATER LEVEL Below Top of Casing: 21.0
FT.
(Use "+' if Above Top of Casing)
: d. TOP OF CASING IS
0.0 FT. Above Land Surface'
'Top of casing terminated allor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): N/A
METHOD OF TEST N/A
f. DISINFECTION: Type
N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bollam
Thickness/
: 7. CASING: Depth
Diameter Weight Material
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material Method
Top Bottom
Ft.
Top Bottom
Ft.
: Top Bottom
Ft.
9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft - In. in.
Top Bottom
Ft. in. in.
Top Bottom
Ft. in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top_______Bottom-
Ft.
Top Bolton
Ft.
11. DRILLING LOG
Top Bottom
0.0 / 27.0
12. REMARKS:
Formation Description
DIRECT PUSH
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C-WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS
RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
01/17/13
SI d CER I IED OR DATE
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2109
1

britYs WELL ABANDONMENT RECORD
as
North Carolina Deparhnent of Gnvironmenl and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTII+ICATION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address -
STATESVILLE NC 28625
City or Town State Zip Code
704 1 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-31
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)D Monitoring ❑ Residential
❑ M unicipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ 'Recovery M Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE .
164 BOSTIAN BRIDGE DRIVE 28677
(StreetrRoad Name, Number, Community, Subdivision, Lot No.. Parcel, Zip Code)
TOPOGRAPHC I LAND SETTING: -- — -_ — —
O Slope ❑ Valley V Flat ❑ Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 245 56.6500 `.DMS OR - DO
LONGITUDE 80 55 • 2.5700 • DMS OR DO
Latitudellongitude source: 03PS Ofbpographic map 12/18I12
(location of well must be shown on a USGS topo map andattached to 11. DATE WELL ABANDONED
this form if not using GPS)
s. WELL DETAILS:
a.Tolal Depth 27.0 ft. Diameter in.
b. Water Level (Below Measuring Point): 21.0 ft.
Measuring point is 0.0 fL above land surface,
6. CASING: Length Diameter
a. Casing Depth (if known): N/A ft. in.
b. Casing Removed: NIA ft. in.
7. DISINFECTION' N/A
(Amount of 65%75% calcium hypochiodle used)
: - 8. SEALING MATERIAL:
Neat Cement SandCement
Cement —lb. Cement lb.
Water gal_ Water gal.
Bentonite
Bentonite 7a0.0 lb.
Type:❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
Amount 5.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TRFMIF
10. WELL DIAGRAM :Draw a detailed sketch of Iheell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill malerialsised
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY -The name of the business where the well Is located. Complete 4a i
: THIS REC- RD_HAS P®VIDED TO THE WELL OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.)
BEEN
��%Mtl{
FACILITY ID # (if applicable)
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner must be an individual w ersonall)abandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
4b. CONTACT PERSONANELL OWNER:
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
'-"•'••••"""'r7it:�",..�},:�.._,`!�!�..c,.a„ui Iu,q1 W. IJIY WIVII V6. YY O LGr; WUAI r L H]rOrmaUUn-t'e .rOCSsln -
Form G 3D
761TMai1 Service Center Ralelgh.NCs27699 1617 Phone (919) 807=630Q _ Rev_ 5/10

-•da STAi��y_
y� j' ]�
r�, '�;{�• M �F 1 'Y ONA@�ESIDENTIAL WELLCONSTRUCTION RECORD
North Carolina Department off;nvironment and Natural Resources- Division of Water Quality
��` ," .. •fir
WELL CONTRACTOR CERTII�[Cr1TION # 3552
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #pf applicable) B-32
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery❑ Injection d
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley ldFlat ❑Ridge ❑Other
LATITUDE 35 ° 45 ' 56.6500 „ DMS OR DD
LONGITUDE 80 , 55 ' 2.5700 " DMS OR DD
Latilude/longitude source: 03PS Oropographic map
(location of wel/must be shown on a USGS topo map andattached to
this form irnot using GPS)
5. FACILITY (Name of the business where the well is located.)
d. TOP OF CASING IS 0.0 FT. Above Land Surface
'Top of casing terminated atfor below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST N/A
f. DISINFECTION: Typo NIA Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top
Bottom
Top "
Bottom
Top
Bottom
Thickness/
: 7. CASING: Depth Diameter Weight Material
Top Bottom
FL
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material Method
Top . Bottom
Ft.
: Top Bottom
Ft.
Top Bottom
Ft.
9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft.
in. in.
Top Bottom
Ft.
in. in.
Top Bottom
Ft.
In. In.
10. SAND/GRAVEL PACK:
Depth .
Size Material
Tap Bollom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
MAYMEAD ASPHALT PLANT
NIA
0.0 I 42.0
Facility Name
Facility ID// (if applicable)
/
164 BOSTIAN BRILIgE DRIVE
/
Street Address
/
STATESVILLE
NC
28677
/
City or Town
State
Zip Code
/
14CDOT
/
Contact Name
/
164 BOSTIAN BRIDGE DRIVE
/
Mailing Address
/
STATESVILLE
NC
28677
/
City or Town
State
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REP -LACE EXISTING WELL? YES ❑ NO L�r
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+" if Above Top of Casing)
12. REMARKS:
Formation Description
DIRECT PUSH
' I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• NCl192CJIDIEX CONSTRUCTIONST DAROJ ACOPY OF THIS
RE
: RECppVVpO�rHASpEEN P VID O THE L O NER.
01/17/13
SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
VINCE FEDERLE
= PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1b
Rev. 2/09

WELL ABANDONIVIENT RECORD
North Carolina Department of"Environment and Natural Resources- Division or Water Quality
l `�•aM;:��•�'•
WELL CONTRACTOR CERTIFICATION # 3552
1. WELL CONTRACTOR:
5. WELL DETAILS:
VINCE FEDERLE
a.Totai Depth 42.0 ft. Diameter. in.
Well Contractor (individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC Measuring point is 0 0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-32
STATE WELL PERMIT# (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)!] Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Cornmerc(al 0 Agricultural
❑ Recovery rlr Injection 0 Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGIE NAME
NEAREST TOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
6. CASING:
Length Diameter
a. Casing Depth (if known):
NIA ft.
b. Casing Removed:
N/A ft,
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement
Sand Cement
Cement lb.
Cement lb.
Water gal.
Water gaL
Bentonite
Bentonite 300-0 lb.
Type: ❑ Slurry 0 Pellets
Water gal.
Other
Type material PORTLAND CEMENT
e­r r 8.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
in.
in.
(S(reelfRoad Name, Number, Community, Subdivision, Lot No.. Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
- -
❑ Slope ❑ Valley V Flat 0 Ridge(] Other
(Check appropriate selling)
10. WELL DIAGRAM : Draw a detailed sketch of theeli on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE _35 _^ 45 56.6500 ° DMS OR DD
in the well, gravel interval, Intervals of casing perforations, and depths and
LONGITUDE 80 _ ^ 55 2.5700 ° DMS OR DD
types of rill malerialsrsed
Latitude/longitude source: Rfsps pfopographic map
12/18/12
(location of weft must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form ff not using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY - The name or the business where the well is located. Complete 4a : :
THIS RECORD HAS BEEN PfDVIDED TO THE WELL OWNER.
(If a residential well, skip 4a: complete 4b, well owner information only.)
FACILITY ID # (if applicable)
[ m P� 01 /17113
NAME OF FACILITY MAYMEAD ASPHALT PLANT :
SIG14ATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
Cily or Town State Zip Code
(The private well owner must be an individual w orsonai bandons his/her residential well
in accordance with 15A NCAC 2C _0113.)
4b. CONTACT PERSONNVELL OWNER: -
VINCE FEDERLE
NAME NCDOT
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE,-NC 28677
5ubmlt a copy to the'owner and the orlgrnal to Divtswn of Water Qua6ty4 Information Processing, Form GW-30
i617, ItAall Service Center Ratergh NC 27699 1617 Pfiorte [phone] r t r , Rev. 5/10

�a SrATE o'�
f. ' (NONRESIDENT
• �j a
�'k G North Carolina Department ofEnvironniei
WELL CONTRACTOR CERTIF
1. WELL CONTRACTOR:
VINCE FEDERLE
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
.City or Town Stale Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#--
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(if applicable) B-33
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection 9(
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE .28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope ❑Valley JIFlat ❑Ridge ❑Other
LATITUDE 35 ° 45 ' 56.6500 " DMS OR DD
LONGITUDE 80 ' 55 • 2.5700 " DMS OR DD
Latiludellongilude source: W3PS Qfopographic map
(location of well must be shown on a USGS topo map andatfached to
this farm if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
NIA
Facility Name
Facility ID# (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Scale
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b_ DOES WELL REPLACE EXISTING WELL? YES❑ NOW
c. WATER LEVEL Below Top of Casing: 21.0 FT. _
(Use "+' if Above Top of Casing)
Ift
L WE, LL CONSTRUCTION RECORD
it and Natural Resources- Division of Water Quality
(CATION # 3552
d. TOP OF CASING IS
0.0 Ff. Above Land Surface'
'Top of casing terminated atior below land surface may require
a variance in accordance with 15A NCAC 2C .0118.
e. YIELD (gpm): NIA
METHOD OF TEST N/A
f. DISINFECTION: Type
N/A Amount NIA
g. WATER ZONES (depth):
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Top Bottom
Thickness/
7. CASING: Depth
Diameter Weight Material
= Top Bottom
FL
Top Bottom
Ft.
Top Bottom
Ft.
8. GROUT: Depth
Material Method
Top Bottom
Ft.
Top Bottom
Ft.
Top Bottom
Ft.
: 9. SCREEN: Depth
Diameter Slot Size Material
Top Bottom
Ft. in. in.
Top Bottom
Fl. in. in -
Top Bottom
Ft. in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top Bollom
Ft.
= Top Bottom
Ft.
11. DRILLING LOG
Top Bottom
Formation Description
0.0 / 42.0
DIRECT PUSH
12. REMARKS:
I DD HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH
• 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS
RECO;:S BEENPROVIDEDTO THE WELL OWNER.
SIGNAATO F CERTIFIED W � DATE
013
VINCE FEDERLE
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW=1b
Rev. 2109

' �,• STArFcA
WELL ABANDONMENT RECORD
.. f North Carolina Department of Environinent and Natural Resources- Division or Water Quality
o; p Q ty
.....,.. WELL CONTRACTOR CGRTII+ICr\TION # 3552
1. WELL CONTRACTOR:
6. WELL DETAILS:
VINCE FEDERLE
a.Total Depth 42.0 ft. Diameter. in.
Well Contractor (Individual) Name
b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC
Measuring point is 0.0 fL above (and surface.
Well Contractor Company Name
176 COMMERCE BLVD
6. CASING: Length Diameter
Street Address
STATESVILLE NC 26625
a. Casing Depth (if known): NIA ft. in.
City or Town State Zip Code
b. Casing Removed: N/A ft. in.
704 ) 872-7686
N/A
Area code Phone number
7. DISINFECTION:
(Amount of 65%75% calcium hypochlorite used)
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-33
8. SEALING MATERIAL:
Neat Cement Sand Cement
STATE WELL PERMIT # (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
Water gal. Water gal.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Sentonite 30.0 lb.
WELL USE (Check applicable usef] Monitoring ❑ Residential
Type:O Slurry 0 Pellets
0 Municipal/Public 0 Industrial/Commercial ❑ Agricultural
Water gal.
0 Recovery M Injection ❑ Irrigation
Other
❑ Other (list use)
Type material PORTLAND CEMENT
Amounl 8.5 GALLONS
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
(Slreel/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
❑ Slope 0 Valley f/ Flat ❑'RidgeO Other
(Check appropriate setting)
: 10. WELL DIAGRAM :Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
LATITUDE 735_ _^ 45 56.6500 - DMS OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 < 55 2.5700 " DMS OR DD
types of fill materials,sed
Latitudellongitude source: + ,PS Qfopographic map
12/18/12
(location of well must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
this form /f not using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C; WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF
4a. FACILITY -The name of the business where the well is located. Complete 431THIS
RECORD HAS BEEN P®VIDEO TO THE WELL OWNER.
(If a residential welt, skip 4a; complete 4b, well owner information only.)
FACILITY ID # (if applicable)
�e p^�� .01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGtfATLJRE OF CERTIFIED WELL CONTRACTOR DATE
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
SIGNATURE OF PRIVATBV7Ei.@:U"IOR#1BAt*DDN1NG THE WELL DATE
City orTown State Zip Code
(The private well owner must be an individual w ersoriall bandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
4b.CONTACT PERSONIWELL OWNER:
VINCE FEDERLE
NAME NCDOT -
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE, NC 28677
"=Submit a copy a the ownet arrd the onglnal to'Dlulston of WalerQuahty Information P�ocesstng,,- Form GW-30
:.11i17 Mail Service Center, Ralelgti NC 27699 1617 Phone (9t9)�O7 6300 Rev. 5110

' 4k Hux Kta•
1. WELL CONTRACTOR:
JAMES HESS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
70( 4 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
WELL CONSTRUCTION PERMIT#
OTHER ASSOCIATED PERMIT#(if applicable)
SITE WELL ID #(If applicable) B-34
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Id
Irrigation❑ Other ❑ (list use)
DATE DRILLED 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name. Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC / LAND SETTING: (check appropriate box)
❑Slope [Walley VFlat ❑Ridge ❑Other
LATITUDE 35 -45 ' 56.6500 " DMS OR DD
LONGITUDE 80 , 55 - 2.5700 " DMS OR _DO
LatitudeAongitudesource: 03PS pfopographicmap
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility IDfE (if applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
State
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
Cily or Town
Stale -
Zip Code
L—)
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO E/
c. WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+' if Above Top of Casing)
-NONRESIDENTIAL WELL CONSTRUCTION REcoRD
North Carolinu Deparbncnl of Environment and Natuml Resources- Division of Writer Quality
WELL CONTRACTOR cERTw1CATION # 3550
d. TOP OF CASING IS 0.0 FT. Above Land Surface -
'Top of casing terminated al/or below land surface may require
a variance In accordance with 15A NCAC 2C .0118.
o. YIELD (gpm): NIA METHOD OF TEST N/A
f. DISINFECTION: Type N/A Amount N/A
g. WATER ZONES (depth):
Top Bottom Top Bottom
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
7. CASING: Depth Diameter Weight Material
Top Bottom Ft.
Top Bottom FL
Top Bottom R.
: 8. GROUT: Depth Material Method
Top Bottom Ft.
Tap Bottom FL
Top Bottom Ft.
:9. SCREEN: Depth Diameter Slot Size Material
Top Bottom Ft. in. in.
Top Bottom Ft. in. in.
Top Bottom Ft. in. in.
10. SAND/GRAVEL PACK:
Depth Size Material
: Top Bottom Ft.
: Top Bottom Ft.
Top Bottom Ft.
11. DRILLING LOG
: Top Bottom Formation Description
0.0 / 42.0 DIRECT PUSH
/
- 12. REMARKS:
I DO HEREBY CEPOY THAT THIS WELL WAS CONSTRPPED IN ACCORDANCE WITH
• 15A NCAC 2C, ' CONSTRLCMO SJ/�NDARDS, A THAT A COPY OF THIS
RECORD HAS NPR VIOE�TO T"H.E/Vj'ELf„(�WNE
[ /�{�Y� 01/17/13
SIGN RE OF CERTIFIED WELL CONTRACTOR DATE
JAMES HESS
: PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW=1b
Rev. 2/09

r
i �' I r`• r Ot
1. WELL CONTRACTOR:
JAMES HESS
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3550
5. WELL DETAILS:
a.Total Depth 42.0 ft. Diameter. in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
704 ) 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) B-34
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use}.'] Monitoring ❑ Residential
❑ M unicipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery G Injection ❑ Irrigation -
❑ Other (list use)
6. CASING: Length Diameter
a. Casing Depth (if known): N/A IL in.
b. Casing Removed: N/A ft. in.
7. DISINFECTION: N/A
(Amount of 65%75% calcium hypochlor(te used)
8. SEALING MATERIAL:
Neat cament Sand Cement
Cement lb. Cement lb.
Water gal. Water gaL
Bentonite
Benlonile 300.e lb.
Type: ❑ Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND CEMENT
I
Amount 8.5 GALLONS
3. WELL LOCATION:
i COUNTY IREDELL QUADRANGLE NAME
NEAREST TOWN: STATESVILLE
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
i 164 BOSTIAN BRIDGE DRIVE 28677
TREMIE
I (Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley V Flat ❑ Ridge❑ Other
(Check appropriate setting)
10. WELL DIAGRAM : Draw a detailed sketch of lheell on the back of [his
form shoving total depth, depth and diameter of screens (if any) remaining
i LATITUDE _35_ _• 45 , 56.6500 ^ DMS OR DD
in the well, gravel interval, intervals of casing perforations, and depths and
- t LONGITUDE 80 • 55 • 2.5700 • DMS OR DD
types of fill materiaissed
Latiludellongi(ude source: QGPS Qropographic map
12/18/12
! (location of we/f must be shown on a USGS topo map andattached to
11. DATE WELL ABANDONED
I this form if not using GPS)
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
l
: WITH ISA NCA013EEN LL CONSTRUCTION STAND S, AND THATA COPY OF
I, 4a. FACILITY - The name of [he business where the well is located. Complete 4a;
THiS RECORD P9LW6ED WEL NER.
(If a residential well, skip 4a; complete 4b, well owner information only.)
;THE
Y �,, '
FACILITY ID # (if applicable)
01/17113
--NA
!, NAME OF FACILITY MAYMEAD ASPHALT PLANT
FIG _ OF CERTIFIED WELL CONTRACTOR DATE
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE
_ STATESVILLE NC .28677
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
! City or Town State Zip Code
(The private well owner must be an individual wpersonalltebandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
{ 46. CONTACT PERSONiWELL OWNER:
i
JAMES HESS
NAME NCDOT
- PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 164 BOSTIAN BRIDGE DRIVE STATESVILLE. NC 28677
Subd thoi WQua' fraionoesgmt a copy othwane a , Form GW-30
- 1617 Marl Service Center,. Raleigh NC 27699 1617 Phone [phone] Rev. 5/10
.. r,,
t

NONRESIDENTIAL WELL CONSTRUCTION RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 3550
1. WELL CONTRACTOR:
JAMES HESS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town Slate Zip Code
70( 4 ) 872-7686
Area code Phone number
d. TOP OF CASING IS 0.0 FT. Above Land Surface"
'Top of casing terminated aUor below land surface may require
a variance in accordance with ISA NCAC 2C .0118.
e. YIELD (gpm): NIA METHOD OF TEST NIA
L DISINFECTION: Type NIA Amount WA
g. WATER ZONES (depth):
Top Bottom Top Bottom.
Top Bottom Top Bottom
Top Bottom Top Bottom
Thickness/
2. WELL INFORMATION: : 7. CASING: Depth Diameter Weight Material
WELL CONSTRUCTION PERMIT# - Top Bottom Ft.
OTHER ASSOCIATED PERMIT#(if applicable) ; Top Bollom Fl.
SITE WELL ID #(if applicable) B-35 : Top Bottom Ft.
3. WELL USE (Check One Box) Monitoring ❑ Municipal/Public ❑
Industrial/Commercial ❑ Agricultural ❑ Recovery ❑ Injection Ed
irrigalion❑ Other ❑ (list use)
DATE DRILLED 12/18/12
4. WELL LOCATION:
164 BOSTIAN BRIDGE DRIVE 28677
(Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code)
CITY: STATESVILLE COUNTY IREDELL
TOPOGRAPHIC I LAND SETTING: (check appropriate box)
❑Slope ❑Valley ,Flat ❑Ridge ❑Other
LATITUDE 35 " 45 ' 56.6500 " DMS OR DD
LONGITUDE 80 ^ 55 1 2.5700 "DMS OR DD
Latilude/tongitude source: VGPS ❑topographic map
(location of well must be shown on a USGS topo map andattached to
this form if not using GPS)
5. FACILITY (Name of the business where the well is located.)-
MAYMEAD ASPHALT PLANT
N/A
Facility Name
Facility ID# (if
applicable)
164 BOSTIAN BRIDGE DRIVE
Street Address
STATESVILLE
NC
28677
City or Town
Slate
Zip Code
NCDOT
Contact Name
164 BOSTIAN BRIDGE DRIVE
Mailing Address
STATESVILLE
NC
28677
City or Town
Stale
Zip Code
U
Area code Phone number
6. WELL DETAILS:
a. TOTAL DEPTH: 42.0 FEET
b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO I,/
-c. WATER LEVEL Below Top of Casing: 21.0 FT,
(Use "+" if Above Top of Casing)
:8. GROUT: Depth
Material
Top Bollom
Ft.
_
Top Bottom
Ft.
Top Bottom
Ft.
_
: 9. SCREEN: Depth
Diameter Slot Size
Top Bottom
Ft.
in. In.
Top Bolcom
Ft,
in. in.
Tap Bottom
Ft.
in. in.
10. SAND/GRAVEL PACK:
Depth
Size Material
Top Bottom
Ft.
Top Bottom
Ft.
Tap Bottom
Ft.
- 11. DRILLING LOG
Top Bottom
Formation Description
0.0 / 42.0 -
12. REMARKS:
DIRECT PUSH
Method
Material
1 DO HEREBY C TIFY THAT THIS WELL WAS CONST CTED IN ACCORDANCE WITH
• 15A NC AC 2C LL CONSTTI ANDARDS D THAT A COPY OF THIS
RECORD EEN P OV1Q�0 70 T . WF,LL OW R.
01/17/13
SI TURE OF CERTIFIED WELL CONTRACTOR DATE
JAMES HESS
PRINTED NAME OF PERSON CONSTRUCTING THE WELL
Form GW-1 b
Rev. 2109

r ` . '3• -� K
�� - �l fly:;:• :� �
WELL ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division or Water Quality
WELL CONTRACTOR CERTIFICATION # 3550
1. WELL CONTRACTOR:
5. WELL DETAILS:
JAMES HESS
a.Total Depth 42.0 ft. Diameter. in.
Well Contractor (Individual) Name b. Water Level (Below Measuring Point): 21.0 ft.
GEOLOGIC EXPLORATION, INC Measuring point is 0.0 ft. above land surface.
Well Contractor Company Name .
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
6. CASING: Length Diameter
a. Casing Depth (if known): N/A ft. in.
City or Town State Zip Code
b. Casing Removed: N/A ft. in.
704 ) 872-7685
- N/A
Area code Phone number
7. DISINFECTION:
2. WELL INFORMATION:
(Amount of65%75% calcium hypochlodte used)
SITE WELL ID # (if applicable) B-35
6. SEALING MATERIAL:
Neat Cement Sand CPmPnt
STATE WELL PERMIT# (if applicable)
Cement lb. Cement lb.
COUNTY WELL PERMIT # (if applicable)
Water gal. Water gal.
Bentonite
DWQ or OTHER PERMIT # (if applicable)
Bentonite 300.0 lb.
WELL USE (Check applicable use)D Monitoring ❑ Residential
Type:❑ Slurry ❑Pellets
❑ M unicipaUPublic ❑ IndustriallCommercial ❑ Agricultural
Water gal.
❑ Recovery fG Injection ❑ Irrigation
Other
❑ Other (list use)
Type material PORTLAND CEMENT
3 WELL LOCATION•
- Amount 8.5 GALLONS
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
164 BOSTIAN BRIDGE DRIVE 28677
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) :
TOPOGRAPHC / LAND SETTING:
❑ Slope O Valley . G Flat ❑ Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 45 56.6500 ° DIAS OR DD
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
TREMIE
10. WELL DIAGRAM :Draw a detailed sketch of thiaell on the back of this
form showing total depth, depth and diameter of screens (tf any) remaining
In the well, gravel interval, intervals of casing perforations, and depths and
LONGITUDE 80 _ 55 • 2.5700 - DMS OR DO
L
types of fill matedals,sed
Latitudellongitude source: Rf.PS Qfopographic map
12/18/12
(location of well must be shown on a USGS topo map andattached to
: 11. DATE WELL ABANDONED _
this form ifnot using GPS)
100 HEREBY CERT),FY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
4a. FACILITY -The name of the business where the well is located. Complete 4a;
(If a residential well, skip 4a: complete 4b, well owner information only.)
WITH 15A NCAC , WELL CONSTRUCTION STANqADS, AND THAT A COPY OF
: THIS RECORD BEEN FiH6ED $Q THE WE WNER.
Y N
FACIUTYID# (if.applicable)
01/17/13
NAME OF FACILITY MAYMEAD ASPHALT PLANT
SIGNAT E OF CERTIFIED WELL CONTRACTOR DATE
STREETAIDDRESS 164 BOSTIAN BRIDGE DRIVE
STATESVILLE NC 28677
: SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State Zip Code
(The private well owner, must be an individual wharsonallwbandons his/her residential well
In accordance with 15A NCAC 2C .0113.) .
4b. CONTACT PERSON/WELL OWNER:
JAMES HESS -
NAME NCDOT..
- PRINTED NAME OF PERSON ABANDONING THE WE LL
154 BOSTIAN BRIDGE DRIVE STATESVI
STREETADDRESS L E. NC 28677
Submtta capy to the owner and the orlgfnal to Division of Water Qualltyr' Informatlon Processing,Form
1617 Mall Service Center, RaleigF►, NC 27699 1617 Ffi`one [phone] r Rev.
/56 -3D
_ ,
y
• ®- ` • .. _

Via Email
February 16, 2015
NC DOT — Roadside Environmental
4809 Beryl Road
Raleigh, NC 27606
Attention: Mr. Ethan Caldwell, LG and PE
Re: Semi -Annual Monitoring Report
NC DOT Site No. 2-66 03©0���
Statesville, North Carolina W:T
H&H Job No. DOT-504
Dear Ethan:
Per your request, please find the attached EOS®
Monitoring Report for the above -referenced site.
information, please do not hesitate to contact me.
Sincerely,
Hart & Hickman, PC
//X/ r4644to
Matt Bramblett, PE
Principal
Attachment
hart R hickman
SMARTER ENVIRONMENTAL SOLUTIONS
RECEIVEDIDENRIDWR
FEB 2 3 2015
Water Quality Regional
Operations Section
Injection and Semi -Annual Groundwater
If you have any questions or need further
cc: Mr. David Goodrich, DWR UIC Program (via certified mail and email)
Mr. Andrew Pitner, Mooresville DWR (via certified mail)
Mr. Allen Johnson, Property Owner (via certified mail)
Ms. Jane Murray, Iredell County Health Department (via certified mail)
2923 South Tryon Street, Suite 100 3334 Hillsborough Street
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

EOS® Injection and Semi -Annual
Groundwater Monitoring Report
Former ATL Site No. 2-66
®o� 0 CAR �s��r
�e CR..•......••• s
oQ• �FESS/0�• �����s
O
SEAL °
25069 J
m-���:� �1� lam•.: �� .
®� ,a
•.INE••. 0
�ssV R ��
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007 main
164 Bostian Bridge Road
Statesville, North Carolina
H&H Job No. DOT-504
February 16, 2015
hart -4 hickman
SMARTER ENVIRONMENTAL SOLUTIONS
#C-1269 Engineering
#-245 Geology
3334 Hillsborough Street
Raleigh, NC 27607 www.harthickman.com
919.847.4241 main

EOS® Injection and Semi -Annual
Groundwater Monitoring Report
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
Table of Contents .
Section
Page No.
1.0 Introduction.................................................................................................................................. I
2.0 Potential Receptor Survey Update.............................................................................................3
2.1 Water Supply Wells.................................................................................................................... 3
2.2 Surface Water..............................................................................................................................4
3.0 Groundwater/Surface Water Monitoring.................................................................................5
3.1 Data Collection Procedures........................................................................................................ 5
3.2 Groundwater Levels and Flow Direction................................................................................... 6
3.3 Surface Water Measurements and Analytical Data.................................................................... 6
3.4 Groundwater Analytical Data..................................................................................................... 7
4.0 Evaluation of Natural Attenuation Parameters........................................................................9
4.1 Competing Electron Acceptors................................................................................................... 9
4.2 Geochemical Indicator Parameters...........................................................................................12
4.3 Electron Donor..........................................................................................................................13
4.4 Presence of Degradation Daughter Products............................................................................14
5.0 Summary and Conclusions.......................................................................................................15
1 hart 'I` hickman
SAAAA-Master Pmjects\NC DOT-DOT\DOT-500s Contract\DOT-504 Statesville 66\September 2014 Report\Semi-Annual GWM Report.doc •
SMARTER WARONMEWAL-SOLUTIONS

List of Tables
Table 1
Water Supply Well Inventory
Table 2
Water Supply Well Analytical Data Summary
Table 3
Water Level Data Summary
Table 4
Surface Water Analytical Data Summary
Table 5
Saprolite Monitoring Well Analytical Data Summary
Table 6
Shallow Bedrock Monitoring Well Analytical Data Summary
Table 7
Summary of Natural Attenuation Indicator Data
Table 8
Surface Water Parameters
List of Figures
Figure 1
Site Location Map
Figure 2
Site Map
Figure 3
Water Supply Well Location Map
Figure 4
EOS® Injection Point Locations
Figure 5
Estimated Shallow Groundwater Potentiometric Map (July 2014)
Figure 6
Target VOC Concentrations in Saprolite Groundwater
Figure 7
Target VOC Concentrations in Bedrock Groundwater
List of Appendices
Appendix A Laboratory Analytical Data
ii hart hickman
SAAAA-Master ProjectsUQC DOT-DOT\DOT-500s Contract\DOT-504 Statesville 66VSeptember 2014 Report\Semi-Annual GWM Report.doc
SMARTER ENVIRONMENTAL SOLUTIONS

EOS® Injection and Semi -Annual
Groundwater Monitoring Report
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
1.0 Introduction
On behalf of the North Carolina Department of Transportation (DOT), Hart & Hickman, PC
(H&H) has prepared this report to present bioenhancement post -injection groundwater
monitoring data for the former Asphalt Testing Laboratory Site No. 2-66. The site is located at
164 Bostian Bridge Road, which is near Buffalo Shoals Road (State Road 1004) in Statesville,
North Carolina (Figure 1). A site map is provided as Figure 2.
Soil and groundwater impacts from former asphalt testing operations were previously identified
at the site. The asphalt testing utilized trichloroethene (TCE), 1, 1, 1 -trichloroethane (1,1,1-TCA),
and/or carbon tetrachloride pp
CTC . The approved CAP included excavation for source area soil
( )
and monitored natural attenuation (MNA) for groundwater impacts. Approximately 162 tons of
impacted soils were removed from the source area in September 2001 as reported in H&H's
Semi -Annual Monitoring and Soil Remediation Report dated February 19, 2002. Confirmation
soil samples indicated that soils were adequately removed. Monitored natural attenuation,
consisting of semi-annual or annual groundwater monitoring, was conducted at the site from
2002 until prior to the bioenhancement injection in December 2012.
Because TCE concentrations remained more than two orders of magnitude above the
groundwater standard, a stream is located near the plume, and there is no public water available
in the area of the site, H&H recommended that a bioenhancement event be conducted in shallow
groundwater where TCE concentrations were the highest. Bioenhancement improves subsurface
conditions for more efficient natural attenuation by reductive dechlorination.
On behalf of DOT, H&H prepared an Underground Injection Control (UIC) Permit Application
dated August 24, 2012 to conduct a bioenhancement injection at the site. The injectant selected
I hart hickman
S:\AAA-Master Projects\NC DOT-DOIIDOT-500s Contract\DOT-504 Statesville 66\September 2014 Report\Semi-Annual GWM Report.doc
- SMARTER ENVIRONMENTAL SOLUTIONS

for the bioenhancement injection event was Emulsified Oil Substrate (EOS®). DENR issued the
UIC permit on November 9, 2012. The bioenhancement injection activities were conducted in
December 2012.
The injection event included 36 temporary direct push technology (DPT) injection points and
injecting the EOS® into the upper 20 ft of the saturated zone. The 36 temporary DPT injection
wells were installed approximately 20 ft apart perpendicular to groundwater flow and
approximately 35 ft apart parallel to groundwater flow within the target treatment area. The DPT
temporary injection wells were advanced to depths ranging from approximately 27 ft to 42 ft
below ground surface (bgs). The injection area and injection well locations are depicted on
Figure 4.
_- The EOS® concentrate was mixed with water prior to injection using an approximate mixing
ratio of 1:6 (EOS® to water). For the project, a total of approximately 1,618 gallons of EOS®
concentrate were mixed with approximately 10,666 gallons of potable water and injected into the
subsurface. The quantity of EOS® was determined using EOS Remediation, LLC's EOS®
Design Tool (Version 3.0) software. Approximately 323 to 508 gallons of diluted EOS® mixture
were injected into each injection well.
This post -injection semi-annual groundwater monitoring report includes a summary of post -
injection groundwater monitoring between October 2013 and July 2014.
2 hart hickman
SAAAA-Master ProjectsM DOT-DOTtDOT-500s ContracADOT-504 Statesville 66\September 2014 Report\Semi-Annual GWM Report.doc
SMARTER ENVIRONMENTAL SOLUTIONS

2.0 Potential Receptor Survey Update
A summary of area receptors is described below and was last updated in August 2013. An
annual receptor survey update will be provided in the next report.
2.1 Water Supply Wells
The August 2013 receptor survey update was performed by reconnaissance within 1,500 ft of the
former asphalt -testing laboratory and by contacting the local utility department to confirm that no
municipal wells are in the area. During the August 2013 receptor update, no additional water
supply wells were identified within 1,500 ft of the site.
A total of 18 water supply wells (active, inactive, or abandoned) are located within a 1,500-ft
radius of the former asphalt -testing laboratory. The locations of the water supply wells are
indicated on Figure 3, and a summary of water supply well information is provided in Table 1.
Of the 18 water supply wells, four wells are located on -site and are designated as WSW-1,
WSW-2, WSW-4, and WSW-4A. In accordance with the approved CAP, H&H abandoned water
supply wells WSW-1 and WSW-2 in September 2001. Water supply wells WSW-4 (deeper) and
WSW-4A (shallow) are located approximately 500 ft southeast and upgradient of the source area.
WSW-4 serves the entire subject property and WSW-4A is inactive. Target volatile organic
compounds (VOCs) have not been detected in WSW-4 including during the May 2014 sampling
event (Table 2).
No off -site water supply wells are located downgradient of the former asphalt -testing laboratory.
Each of the 14 off -site water supply wells is located upgradient or cross -gradient of the former
asphalt laboratory. The closest off -site water supply well (WSW-5) is situated cross -gradient of
the site approximately 650 ft southwest of the former asphalt laboratory.
One of the 14 off -site water supply wells (WSW-3) is located cross -gradient of the former
asphalt -testing laboratory on the Dorothy Davis property (across an unnamed tributary of
Third Creek and approximately 1,200 ft northeast of the former laboratory). WSW-3 was
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it
sampled in September 1997 and again in October 1998. No target compounds were identified in
either sample. Further, a deep saprolite monitoring well (DMW-8), located on the same side of
the tributary as WSW-3, is not impacted. The lack of impacts in DMW-8 indicates that the
tributary acts as an effective hydraulic barrier.
Based on the distance from the former laboratory, the known extent of the contaminant plume,
and topographic and hydraulic gradient considerations, the potential for site groundwater impacts
to affect the off -site water supply wells is considered to be low.
2.2 Surface Water
Two surface water bodies are located within a 0.25-mile radius of the subject site (Figures 1
and 3). An unnamed tributary to Third Creek is located approximately 400 ft north of the former
laboratory and borders the northern property boundary. In addition, Third Creek is located
approximately 600 ft west of the former laboratory and borders the western property boundary.
Both of these surface water bodies appear to be discharge locations for site groundwater.
In February 1999, surface water samples were collected from both the unnamed tributary and
Third Creek at locations along the northern and western property boundaries of the site. In
addition, H&H collected a surface water sample (labeled SS-2) in May 2014 from the unnamed
tributary of Third Creek (Table 4 and Figure 2). The surface water sample was analyzed for
purgeable halocarbons by EPA Method 6200B. Target compounds were not detected in the
surface water sample. In addition, groundwater modeling conducted as part of the CAP indicates
that target compounds will not be present in these surface waters above surface water quality
standards in the future. Recent surface water sampling activities are discussed further in
Section 3.
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f '

3.0 Groundwater/Surface Water Monitoring
As outlined in the UIC permit, H&H conducted a pre -injection groundwater monitoring events on
February 2 and 3, 2012 and December 7, 2012 to finalize the injection area and to establish a
baseline for comparison with post -injection monitoring data. Additionally, H&H performed
quarterly post -injection monitoring events in February 2013, April 2013, June 2013, October 2013,
January 2014, May 2014, and July 2014 to assess the performance of the implemented enhanced
bioremediation remedy. The April 2013, October 2013, and May 2014 quarterly sampling events
were comprehensive events as outlined in the UIC permit application. The groundwater sampling
procedures and monitoring results for the most recent monitoring event in July 2014 are
discussed below. The locations of the monitoring and temporary injection wells are indicated on
Figure 4, and monitoring well construction information is provided in Table 3.
3.1 Data Collection Procedures
H&H sampled deeper saprolite monitoring wells DMW-1, DMW-2, DMW-6, DMW-8, DMW-9,
DMW-10, and DMW-11 and bedrock monitoring well DMW-7. Samples from these wells were
submitted for laboratory analysis of VOCs by Environmental Protection Agency (EPA) Method
6200B (reporting the EPA Method 601 list). Eight Resource Conservation and Recovery Act
(RCRA) metals (arsenic, barium, cadmium, chromium, lead, selenium, silver, and mercury) were
analyzed by EPA Methods 6010/7470, as well as nitrate, sulfate, sulfide, metabolic acids,
methane, ethane, ethene, and total organic carbon (TOC). Field measurements were also collected
from these wells and the unnamed tributary of Third Creek for dissolved oxygen (DO), oxidation-
reduction potential (ORP), specific conductivity, ferrous iron, pH, and temperature. In addition,
one surface water sample was collected from the unnamed tributary of Third Creek located north
of the site for laboratory analysis of VOCs by EPA Method 6200B (reporting the EPA
Method 601 list).
The sampling event was conducted using the following procedures. After well water levels were
gauged, DO concentrations were measured using a downhole probe. Following DO
measurements and prior to collection of groundwater samples, the target wells were purged using
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dedicated disposable bailers until pH, temperature, and specific conductivity values stabilized. If
a well went dry during purging, the purging process was considered to be complete. Groundwater
samples were collected with dedicated disposable bailers.
Groundwater samples were submitted for laboratory analyses of VOCs using methods listed
above. Pace Analytical Laboratories, Inc., a North Carolina -certified laboratory, conducted
laboratory analyses. Dedicated laboratory -supplied sample bottles were used for sample
collection. A chain -of -custody record was completed for samples collected and included sample
description, date collected, time collected, matrix, sample container information, and analyses
required. The chain -of -custody was signed by H&H and placed along with the samples in a
chilled cooler for hand delivery to the laboratory by H&H. Copies of the laboratory analytical
data sheets and chain -of -custody records are provided in Appendix A.
3.2 Groundwater Levels and Flow Direction
Water levels in site monitoring wells were gauged using an electronic water level meter on
July 30, 2014 (Table 3). The estimated saprolite potentiometric map constructed from the
July 2014 groundwater elevation data is presented as Figure 5. The potentiometric map was
constructed using both shallow and deeper saprolite water levels. Consistent with previous data,
groundwater flow in the saprolite aquifer i generall
y to the northwest in the direction of
�' p q g Y
Third Creek and its tributary. The shallow groundwater has a calculated horizontal hydraulic
gradient of approximately 0.02 ft/ft.
3.3 Surface Water Measurements and Analytical Data
As required in the UIC permit, quarterly surface water measurements were collected from the
unnamed tributary of Third Creek at locations upstream (SS-1) and downstream (SS-2) of the
injection area to determine if the bioenhancement injection activities are adversely impacting the
creek. The locations of SS-1 and SS-2 are depicted on Figure 2. Based on similar data between
g
the two locations during each sampling event, the bioenhancment injection has not adversely
impacted the tributary (Table 8).
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1

H&H will continue to collect surface water field measurements at locations upstream and
downstream of the injection area on a quarterly basis. Should field measurements indicate
impacts to the tributary, surface water samples would be collected from the tributary and
analyzed for various parameters as outlined in the UIC permit.
As noted in the UIC permit application, during the quarterly post -injection comprehensive
sampling event in May 2014, a surface water sample was collected from the unnamed tributary of
Third Creek at a location (SS-2) downgradient of the injection area. The sample was collected
by lowering a bailer into the streambed. No VOCs were detected in the surface water sample
(Table 4).
3.4 Groundwater Analytical Data
Deeper Saprolite
Analytical results from the July 2014 sampling event indicate groundwater impacts above
groundwater standards in deeper saprolite monitoring wells DMW-6 and DMW-11 (Table 5 and
Figure 6). TCE and 1, 1 -dichloroethane were the only two compounds detected above groundwater
standards. The most elevated COC concentrations were detected in DMW-6. TCE was detected
in monitoring well DMW-6 at a concentration of 43.2 µg/l, which is above the groundwater
standard for TCE of 3 µg/l. 1,1-DCA was detected in monitoring well DMW-6 at a concentration
of 40.6 µg/l, which is above the groundwater standard for of 6 µg/1
Consistent with previous sampling events, target compounds were not detected in deeper
saprolite well DMW-8. Monitoring well DMW-8 is situated on the northern side of the unnamed
tributary of Third Creek. The absence of groundwater impacts in DMW-8 indicates that the
tributary is acting as an effective hydraulic barrier.
Bedrock
The bedrock monitoring wells were last sampled in May 2014. In May 2014, target
compounds were not detected above laboratory reporting limits in bedrock wells DMW-3, DMW-4,
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and DMW-7 (Table 6 and Figure 7), or in the on -site water supply well WSW-4 (Table 2).
Bedrock well DMW-7 is located adjacent to deep saprolite well DMW-6, which is the monitoring
well with the highest target compound concentrations. Although only approximately 25 ft separates
the DMW-6 and DMW-7 well screens, the concentrations decrease with depth to non -detectable
levels in DMW-7.
TCE is the most widespread target VOC detected above standards. Post -injection July 2014 data
indicate that TCE levels decreased from 68.5 µg/1 to 43.3 µg/l in DMW-6, 3.3 µg/1 to 2.9 µg/1 in
DMW-9, and 10.8 µg/1 to 7.9 µg/1 in DMW-11. These trends indicate that the EOS® injection
has resulted in enhanced bioremediation within portions of the groundwater plume area.
Concentration trends will continue to be evaluated during future sampling events.
Concentrations of key VOCs in saprolite and bedrock groundwater are depicted on Figures 6
and 7.
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4.0 Evaluation of Natural Attenuation Parameters
Natural attenuation of groundwater contaminants occurs by physical, chemical, and biological
processes. Biodegradation by reductive dechlorination is a primary degradation pathway for the
type of constituents present at the site. Additional data on reductive dechlorination including
indicator parameter data and daughter product concentrations are discussed below.
The target potential DOT compounds at the site are amenable to natural attenuation. 1,1,1-TCA
and TCE predominantly biodegrade under anaerobic conditions by a process known as reductive
dechlorination. 1,1,1-TCA also degrades abiotically to 1,1-DCE. Historically, there was some
evidence of natural degradation of these compounds based on the presence of potential daughter
products: l,l-DCE, 1,1-DCA, and cis-1,2-DCE. However, natural site conditions were not
highly favorable for reductive dechlorination.
{
The EOS® injection was designed to enhance conditions for biodegradation of the constituents of
concern, and general favorable results in concentrations trends are being observed since the
injection of EOS® in December 2012. Recent and historical biodegradation data are presented in
Table 7. A discussion of the recent indicator parameter data from July 2014 is provided below.
4.1 Competing Electron Acceptors
Various electron acceptors can potentially compete with reductive dechlorination, including DO,
nitrate, sulfate, iron (III), and carbon dioxide (methanogenesis). Each sequential reaction reduces
the ORP of the groundwater into the range within which anaerobic reductive dechlorination can
occur most efficiently. These parameters or their byproducts (e.g., Fe(II) and methane) were
measured to assess the prevailing redox conditions at the site. A brief discussion of each
parameter is provided below.
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Dissolved Oxygen
DO is used by microbes as an electron acceptor for the biodegradation of organic carbon.
r-
Reductive dechlorination occurs under anaerobic or low DO conditions. DO concentrations of
less than 5 mg/1 may be acceptable, while concentrations less than 0.5 mg/l are ideal.
Dissolved oxygen measurements ranged from 0.82 mg/l (DMW-2) to 2.70 mg/l (DMW-7) in
July 2014. Monitoring wells with dissolved oxygen levels close to or less than 1.0 mg/l included
monitoring wells DMW-1, DMW-2, and DMW-6. The measured dissolved oxygen
concentrations in most impacted monitoring wells indicate conditions conducive for reductive
dechlorination to occur.
Nitrate/Nitrite
Nitrate may be used as an electron acceptor for anaerobic biodegradation via denitrification. In
this process, nitrate is reduced and nitrite is produced. In general, nitrate concentrations in the
plume less than background are considered indicative of anaerobic biodegradation. At
concentrations greater than 1 mg/l, nitrate may compete with the reductive dechlorination
process.
Nitrate was detected at concentrations which ranged from <0.020 mg/l (DMW-6, DMW-10 and
DMW-11) to 2.30 mg/1 (DMW-2) in July 2014. These data suggest that nitrate reduction may be
occurring in the plume, indicating the presence of anaerobic conditions favorable for reductive
dechlorination. Most nitrate levels were less than 1 mg/l, and the potential for significant
competition with reductive dechlorination is low.
Sulfate/Sulfide
Sulfate also may be used as an electron acceptor for anaerobic biodegradation. This process is
known as sulfate reduction and results in the depletion of sulfate and production of sulfide in the
aquifer. Sulfate concentrations within the plume below background concentrations and sulfide
concentrations within the plume above background concentrations are indicative of anaerobic
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degradation by sulfate reduction. In addition, sulfate at concentrations greater than 20 mg/1 may
compete with reductive dechlorination processes.
Sulfate was detected at concentrations that ranged from <2.0 mg/l (DMW-8) to 81.8 mg/l
(DMW-2) in July 2014. Sulfate concentrations in the plume wells were generally greater than
the concentration (<20 mg/1) considered most favorable for reductive dechlorination. In general,
sulfate concentrations in the plume wells appear to indicate the potential for competition with
reductive dechlorination.
Sulfide was not detected above the laboratory detection limit (<0.10 mg/1) in July 2014. The lack
of sulfide concentrations in the plume wells appear to indicate that sulfate reduction is not
significant anaerobic process at the site.
Iron II
Iron reduction is an anaerobic process in which Fe3+ is reduced to Fee+. The reduced form of iron
is soluble. The presence of ferrous iron in groundwater greater than 1.0 mg/l is typically
considered an indication of iron -reducing conditions. In July 2014, ferrous iron was generally
not detected (<0.2 mg/1), other than 5.4 mg/1 in DMW-10 and 9 mg/l in MW-11. Therefore, iron
reduction appears to be occurring in some portions of the groundwater plume.
Methane
The presence of methane above background conditions indicates microbial degradation
(methanogenesis) is occurring and strongly reducing conditions have been established. The
fastest rates of anaerobic dechlorination typically occur under methanogenic conditions.
Methane was detected at concentrations which ranged from <6.6 µg/l (DMW-2, DMW-6, DMW-
7, and DMW-8) to 4,070 µg/l (DMW-11) in July 2014. These results indicate that strongly
reducing conditions are present in portions of the plume.
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4.2 Geochemical Indicator Parameters
Parameters that are indicators of conditions favorable for anaerobic biodegradation of chlorinated
solvents include ORP, pH, and temperature. Ethene/ethane (end products) can also serve as
indicators of complete reductive dechlorination. At the request of DENR, site wells also were
sampled for eight RCRA (metals arsenic, barium, cadmium, chromium, lead, selenium, silver,
and mercury). A summary of these data and recent previous natural attenuation indicator and
target COC data are provided in Table 7. These parameters (July 2014 data) were evaluated to
assess biodegradation processes at the site, and the results are discussed below.
Redox Conditions (ORP)
The ORP of groundwater is a measure of electron activity and is an indicator of the relative
tendency of a solution to accept or transfer electrons. ORP of a groundwater system affects
biodegradation rates. Reductive dechlorination is most efficient in the ORP range corresponding
to sulfate reduction and methanogenesis (<-100 mV), but reductive dechlorination also occurs in
the ORP range associated with nitrate, manganese, and iron reduction (-50 mV to 740 mV).
ORP ranged from -17 mV (DMW-10) to 319 mV (DMW-1) in July 2014. ORP data are
generally lower in impacted wells and are within the range in which reductive dechlorination
may occur.
pH and Temperature
Groundwater pH values ranging from six to eight standard units are generally preferable for
anaerobic biodegradation. The pH of groundwater affects the presence and activity of microbial
populations. Acid generated during reductive dechlorination can decrease pH levels after a
bioenhancement injection. Groundwater pH ranged from 4.99 to 7.46 in July 2014. The site pH
values are within or close to the range, which is considered favorable for reductive
dechlorination.
Temperature does not greatly influence reductive dechlorination, but temperatures greater than
20 °C may accelerate biochemical processes. In July 2014, temperatures ranged from 15.7 °C to
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18.7 C. The average shallow groundwater temperature for the site is approximately 16.4 C.
These temperatures are in the range, which is considered satisfactory for biodegradation.
Ethene and Ethane
The dissolved gases ethene and ethane are non -toxic end products of reductive dechlorination of
chlorinated solvents. Apart from ethane in DMW-6 and DMW-11, dissolved ethene and ethane
were not detected in the site wells in the pre -injection or post -injection monitoring events.
Ethane was detected in DMW-11 during pre -injection sampling in February 2012 and post -
injection sampling in February and April 2013. Additionally, ethane was detected in DMW-6
during the post -injection sampling in October 2013 and January 2014. These results indicate that
reductive dechlorination may be occurring in the vicinity of DMW-6 and DMW-11. Because
ethene and ethane are highly volatile, it is not usual that these compounds were not detected in
the remaining plume groundwater samples even if they may have been present.
Eight RCRA Metals
In July 2014, the only RCRA metal detected in the site wells included barium in all sampled
wells. Post -injection metals concentrations are similar to pre -injection metals concentrations
detected in February 2012.
4.3 Electron Donor
TOC
TOC is utilized as an electron donor in the reductive dechlorination process and, therefore, is
needed to drive the process. Organic carbon can be either naturally occurring or introduced
artificially. The goal of the EOS injection was to provide a carbon source to drive the reductive
dechlorination process.
The presence of TOC at concentrations greater than 20 mg/L is considered ideal
for biodegradation of chlorinated solvents. In July 2014, TOC levels ranged from 2.7 mg/1
(DMW-7) to 27.9 mg/l (DMW-10). H&H will continue to will monitor for the presence of TOC
in other portions of the plume during future monitoring events.
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Metabolic Acids
In groundwater, fermentation of EOS produces metabolic acids including lactic, pyruvic, acetic,
propionic, and butyric acids. The production of these acids releases hydrogen into groundwater,
which is then utilized by indigenous microbes in reductive dechlorination. In January 2014,
groundwater samples were analyzed for metabolic acids to evaluate the presence of EOS
breakdown products. The metabolic acid results are summarized in Tables 8. Metabolic acids
were generally not detected in plume wells in January 2014. In accordance with the UIC
monitoring plan, the first year of post -injection sampling has been completed; therefore,
metabolic acids will no longer be monitored.
4.4 Presence of Degradation Daughter Products
Degradation or daughter products have been detected in site groundwater. The presence of the
1,1,1-TCA daughter product 1,1-DCA and TCE daughter product cis-1,2-dicholorethene (cis-1,2-
DCE) provide direct evidence that biodegradation by reductive dechlorination of the parent
VOCs has occurred. In general, daughter product concentrations continue to be present in higher
concentrations relative to parent products. The continued presence of these daughter products
indicates that reductive dechlorination is occurring.
In addition to reductive dechlorination, 1,1,1-TCA also undergoes significant degradation by
abiotic processes in which it is transformed to 1,1-DCE or acetate in the presence of water. The
presence of significant 1,1-DCE concentrations compared to TCA in well DMW-6 indicates that
abiotic degradation of TCA is also occurring in the plume area.
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I

5.0 Summary and Conclusions
H&H has implemented an enhanced bioremediation remedy and completed the pre -injection
baseline and quarterly post -injection performance monitoring ' events at the former Asphalt
Testing Laboratory Site No. 2-66 in Statesville, NC. The purpose of the remedial action was to
address chlorinated solvents in groundwater. The pre -injection baseline monitoring event was
completed in February/December 2012 and quarterly post -injection performance monitoring
events are currently being conducted. The following summarizes the results of the sampling
events and performance of the bioenhancement injection activities:
• Groundwater impacts, including TCE, 1,1,1-TCA, and their daughter products, are
present near and downgradient of the former asphalt testing laboratory. Groundwater
impacts exceed groundwater standards in two deeper saprolite monitoring wells. No
impacts above standards were detected in bedrock monitoring wells.
• No ground water impacts were detected in monitoring well DMW-8 located on the opposite
side of the unnamed tributary of Third Creek from the former asphalt -testing laboratory.
The absence of ground water impacts in DMW-8 indicates that the tributary is acting as an
effective hydraulic barrier.
• Target compounds were not detected in the active, upgradient on -site water supply well or
in the unnamed tributary of Third Creek in May 2014.
• A bioenhancement agent (EOS®) was injected into 36 injection wells in December 2012.
Post -injection data collected most recently in July 2014 indicate that TCE concentrations
are decreasing in plume wells DMW-6, DMW-9, and DMW-11. These trends indicate
that the EOS® injection has resulted in enhanced bioremediation within portions of the
groundwater plume area. Concentration trends will continue to be evaluated during
future sampling events.
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In accordance with the UIC permit, H&H recommends continuing performance monitoring to
include two years of post -injection quarterly sampling to evaluate the effectiveness of the EOS®
injection at reducing groundwater concentrations. Quarterly monitoring events are being
completed in November 2014 and January 2015. An injection performance evaluation report
will be submitted to the DENR UIC Program in March 2015, which will present the results of the
November 2014 and January 2015 quarterly sampling events, an updated receptor survey, an
updated evaluation of the effectiveness of the enhanced biodegradation, and recommendations
for future monitoring and/or site activities.
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Table 1
Water Supply Well Inventory
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
Map ID
Well Owner & Address
Well Status
Distance and Direction from Former Asphalt
Testing Laboratory
WSW-1
Maymead, Inc., 164 Bostian Bridge Drive, Statesville
Abandoned
On -site, near former asphalt laboratory
WSW-2
Maymead, Inc., 164 Bostian Bridge Drive, Statesville
Abandoned
On -site, near former asphalt laboratory
WSW-3
Dorothy Davis, 124 Bostian Bridge Drive, Statesville
Active
—1,200 ft, cross -gradient
WSW-4
Maymead, Inc., 164 Bostian Bridge Drive, Statesville
Active
On -site, —500 ft, upgradient
WSW-4A
Maymead, Inc., 164 Bostian Bridge Drive, Statesville
Inactive
On -site, —500 ft, upgradient
WSW-5
Lance & Melissa Lingle, 913 Buffalo Shoals Road, Statesville
Active
—650.ft, cross -gradient
WSW-6
Fred Davis, Buffalo Shoals Road, Statesville
Active
—800 ft, upgradient
WSW-7
Fred Davis Estate, Buffalo Shoals Road, Statesville
Active
—1,000 ft, upgradient
WSW-8
Dorothy Davis, 868 Buffalo Shoals Road, Statesville
Active
—1,100 ft, upgradient
WSW-9
Dorothy Davis, 868 Buffalo Shoals Road, Statesville
Active
—1,100 ft, upgradient
WSW-10
Jerry Hinson, 917 Buffalo Shoals Road, Statesville
Active
—900 ft, upgradient
WSW-11
Jack & Betty Wooten, 897 Buffalo Shoals Road, Statesville
Active
—1,000 ft, upgradient
WSW-12
Margaret Cloer, 881 Buffalo Shoals Road, Statesville
Active
—1,200 ft, upgradient
WSW-13
Jack & Betty Wooten, 871 Buffalo Shoals Road, Statesville
Active
--1,200 ft, upgradient
WSW-14
Jack & Betty Wooten, 865 Buffalo Shoals Road, Statesville
Active
—1,400 ft upgradient
WSW-15
Jerry Hinson, 911 Buffalo Shoals Road, Statesville
Active
—900 ft, upgradient
WSW-16
Wooten Family of NC, 847 Buffalo Shoals Road, Statesville
Active
—1,200 ft, upgradient
WSW-17
Garland Cloer, 889 Buffalo Shoals Road, Statesville
Active
—1,200 ft, upgradient
Notes:
Owner and address information based on Iredell County GIS Database and Recent H&H windshield survey.
WSW-15 and WSW-16 were located during the updated receptor survey in August 2006.
WSW-17 was located during the updated receptor survey in August 2010.
Water supply well locations are provided on Figure 3.
Table 1 (Page 1 of 1)
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Date: 211612015

COMPOUNDS
NC GW
Standard
1, 1, 1 -Trichloroethane
200
Trichloroethene
3
1,1-Dichloroethane
6
1,1-Dichloroethene
7
Methyl-tert butyl ether
20
m/p-xylenes
500
1,2,4-Trimethylbenzene
400
n-Propylbenzene
70
Naphthalene
6
1,4-Dioxane
3
1,2-Dichloroethane
0.4
Diisopropyl ether
70
Ethylbenzene
600
Table 2
Water Supply Well Analytical Data Summary (pg/L)
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
WSW-1 (-213')
WSW-2
WSW-3 (100')
WSW-4 (-165')
WSW-4
(-100')
Abandoned Site Well
Abandoned
Site Well
Davis Residential Well
Site Well (potable)
Inactive site well
6230D
6230D
601
601(Dup)
601
6230D
601
6230D
601
601
601
601
601
601
1 601
601
601
601
601
601
601
1 601
601
1 601
601
6200B
6200B
6200B
6200B
601
Oct-96
Sep-97
Oct-98
Oct-98
Oct-98
Sep-97
Oct-98
Jan-99
Aug-01
Feb-02
Aug-02
Feb-03
Aug-03
Feb-04
Aug-04
Feb-05
Aug-05
Feb-06
Aug-06
Feb-07
Aug-07
Feb-08
Aug-08
Aug-09
Aug-10
Aug-11
Apr-13
Oct-13
May-14
Feb-09
2
<0.5
<1
<1
<1
<0.5
<1
<0.5
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
0.7
<0.5
<1
<1
<1
<0.5
<1
<0.5
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
<1.0'
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
0.9
<0.5
<1
<1
<1
<0.5
<1
<0.5
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
I <1.0
0.8
<0.5
<1
<1
<1
<0.5
<1
<0.5
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
1
0.7
NA
NA
NA
<0.5
NA
<0.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.5
<0.5
NA
NA
NA
<0.5
NA
<0.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA,
NA
NA
NA
NA
NA
NA
NA
1
<0.5
NA
NA
NA
<0.5
NA
<0.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA.
NA
NA
NA
NA
NA
NA
NA
0.9
<0.5
NA
NA
NA
<0.5
NA
<0.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.7
<0.5
NA
NA
NA
<0.5
NA
<0.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
<5.0
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.9
<0.5
<1
<1
<1
<0.5
<1
<0.5
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
0.8
<0.5
NA
NA
NA
<0.5
NA
<0.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.5
<0.5
NA
NA
NA
<0.5
NA
1 <0.5
NA
NA
NA
NA
NA
NA
NA
NA
I NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Notes:
Analytical method numbers are shown below sample IDs.
NA - Not Analyzed for this parameter.
Bold indicates concentration exceeds standard.
Dup - Duplicate sample
GW - Ground Water
Well depth is shown in parenthesis
1,4-Dioxane was analyzed by Method SW846-8260B/SIM
p
File: $:\AA,Q-Master Projects\NC DOT-DOTIDOT-500s Contract\DOT-504 Statesville 66\September 2014 Report\Tables\Tables\T2-WSW data Table 2 (Page 1 of 1)
Date: 2/16/2015 Hart & Hickman, PC

Table 3
Water Level Data Summary
Former ATL Site No. 2-66
Statesville, North Carolina
H& Job No. DOT-504
February 5, 2013
April 11,
2013
June 25, 2013
October 23, 2013
January 27, 2014
May 8, 2014
July 30, 2014
Well I.D.
Depth (ft)
Screen (ft)
Screened
Aquifer
Zone
Elevation
TOC (ft)
(100 ftDatum)
Static
Water Table
(ft below TOC)
Water Table
Elevation (ft)
(100 ft Datum)
Static
Water Table
(ft below TOC)
Water Table
Elevation (ft)
(100 ft Datum)
Static
Water Table
(ft below TOC)
Water Table
Elevation (ft)
(100 ft Datum)
Static
Water Table
(ft below TOC)
Water Table
Elevation (ft)
(100 ft Datum)
Static
Water Table
(ft below TOC)
Water Table
Elevation (ft)
(100 ft Datum)
Static
Water Table
(ft below TOC)
Water Table
Elevation (ft)
(100 ft Datum)
Static
Water Table
(ft below TOC)
Water Table
Elevation (ft)
(100 ft Datum)
SMW-1
30
20-30
Shallow Saprolite
90.73
26.38
64.35
1 26.38
64.35
26.29
64.44
26.70
64.03
27.02
63.71
25.95
64.78
26.87
63.86
SMW-2
35
25-35
Shallow Saprolite
93.92
28.96
64.96
28.90
65.02
28.70
65.22
29.09
64.83
29.30
64.62
28.30
65.62
29.22
64.70
SMW-3
40
30-40
Shallow Saprolite
98.79
32.62
66.17
32.42
66.37
32.05
66.74
32.39
66.40
29.74
69.05
31.29
67.50
32.44
66.36
SMW-4
35
25 - 35
Shallow Saprolite
100.52
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
SMW-5A
30
20 - 30
Shallow Saprolite
95.14
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
DMW-1
50
45 - 50
Deep Saprolite
98.11
32.64
65.47
32.49
65.62
32.13
65.98
32.64
65.47
29.91
68.20
31.62
66.49
32.77
65.34
DMW-2
40
35-40
Deep Saprolite
92.72
28.19
64.53
28.16
64.56
27.98
64.74
28.39
64.33
28.79
63.93
27.68
65.04
28.55
64.17
DMW-3
60
55 - 60
Shallow Bedrock
101.15
30.17
70.98
29.04
72.11
28.70
72.45
26.90
74.25
24.16
76.99
24.73
76.42
NM
NA
DMW-4
70
65 - 70
Shallow Bedrock
98.08
NM
NA
32.48
65.60
32.13
65.95
32.60
65.48
29.85
68.23
31.66
66.42
32.64
65.44
DMW-5
38.5
28.5 - 38.5
Deep Saprolite
78.57
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
NM
NA
DMW-6
36.25
26.25 - 36.25
Deep Saprolite
79.60
18.42
61.18
18.51
61.09
18.48
61.12
18.75
60.85
18.42
61.18
18.54
61.06
18.88
60.72
DMW-7
65
60 - 65
Shallow Bedrock
79.00
17.54
61.46
17.62
61.38
17.66
61.34
17.92
61.08
17.57
61.43
NM
NA
NM
NA
DMW-8
24
14 - 24
Deep Saprolite
68.34
7.59
60.75
7.65
60.69
7.76
60.58
8.00
60.34
7.70
60.64
7.77
60.57
8.20
60.14
DMW-9
40
30-40
Deep Saprolite
88.72
25.62
1 63.10
1 25.63
63.09
1 25.53
163.19
25.84
62.88
25.38
63.34
25.42
63.30
NM
NA
DMW-10
38
28-38
Deep Saprolite
86.24
25.30
60.94
25.40
60.84
25.32
60.92
25.68
60.56
25.36
60.88
25.61
60.63
25.86
1 60.38
DMW-11
40
1 30-40
1 Deep Saprolite
85.13
23.30
61.83
23.34
1 61.79
23.30
61.83
23.49
61.64
23.21
61.92
23.29
61.84
23.47
1 61.66
Notes:
TOC = Top of PVC well casing.
All wells referenced to an assumed datum of 100 feet.
NA - Not Available/Not Applicable
NM - Not Measured
SMW-5Awas abandoned March 21, 2002
DMW-3; DMW-4 and DMW-7 are Type III double -cased wells.
*DMW-1, DMW-3 and DMW-4 were repaired on 7124/06 and re -surveyed for TOC elevations on 8/17/06
DMW-5 discovered damaged in August 2008 and could not be sampled.
SMW-4 could not be located since December 2012.
File: SAAAA-MasterProjectsM DOT -DOT\DOT-500sContract\DOT-504Statesville 66\September2014Report\Tables\TablesM-Water Table Table 3 (Page 1 of 1)
Date: 2/162015 Hart & Hickman, PC

Table 4
Surface Water Analytical Data Summary
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
Compound
SS-1
Upgradient
Tributary
SS-2
Downgradient
Tributary
SS-3
Upgradient
Third Creek
SS-4
Mid -Point
ThirdCreek
SS-5
Downgradient
Third Creek
Feb-99
Feb-99
Au -01
Au -02
Au -03
Au -04
Au -05
Au -06
Au -07
Au -08
Feb-09
Au -09
Au -10
Au -11
A r-13
Oct-13
Ma -14
Feb-99
Feb-99
Feb-99
14-Dioxane
NA
NA
NA
NA
NA
<5.0
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
111-Trichloroethane
<0.5
<0.5
<1
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
c1.0
<1.0
<1.0
<0.5
<0.5
c0.5
Tichooroethene
<0.5
<0.5
<1
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<0.5
<0.5
<0.5
11-Dichloroethane
<0.5
<0.5
<t
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<0.5
<0.5
<0.5
cis-l2-Dichloroethene
<0.5
<0.5
<t
<1
c1
<t
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<0.5
<0.5
<0.5
11-Dichloroethene
<0.5
<0.5
et
c1
<t
<t
<1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<0.5
<0.5
<0.5
Chloroform
<0.5
<0.5
<1
<1
<1
<1
<1
<1.0
<1.0
<1.0
<1.0
I <1.0
<1.0
<1.0
<1.0
<1.0
1 <1.0
c0.5
<0.5
<0.5
Results are in pgA
"<^ indicates compound was not detected above the analytical detection limit
NA - Not Analyzed for this parameter.
File: SAAAA-Master Projects\NC DOT -DOT\DOT-500s Contract\DOT-504 Statesville 66\September 2014 Report\Tables\Tables\T4-Surface Water Summary Table 4 (Page 1 of 1)
Date: 2/16/2015 Hart &Hickman, PC

Table 5 (Page 1 of 6)
Saprolite Monitoring Well Analytical Data Summary (pg/1)
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
JDOT Target Compounds
Non -Target
1,1,1-Trlchloroethane
Trichloroethene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-131chloroethene
cis-1,2-Dichloroethene
1,4-Dloxane
Methylene
Chloride
Chlorobenzene
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
<5.0
<5
<1
NS
NS
NS
NS
NS
NS
NS
NS
NS
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
<1
<1
<1
<1
NA
<5
<1
<1
<1
4.3
<1
1.9
<1
NA
<5
<1
<1
<1
3.7
<1
<1
<1
NA
<5
<1
<1
<1
4.8
<1
1.8
<1
NA
<5
<1
<1
<1
8.1
<1
2.7
<1
NA
<5
<1
<1
<1
11
<1
<1
<1
NA
<5
<1
<1
<1
8.9
<1
1.4
<1
NA
<5
<1
<1
<1
8.2
<1
0.961
<1
<5.0
<5
<1
<1.0
<1.0
5.9
<1.0
<1.0
<1
NA
<1.0
<1.0
<1
<1
8.6
<1
<1
<1
NA
<2
<1
<1
<1
6.7
<1
<1
<1
NA
<2
<1
<1.0
<1.0
5.6
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
4.7
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
3.5
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
3.8
<1.0
<1.0
o.0
NA
<1.0
<1.0
<1.0
<1.0
3.1
<1.0
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
3.5
<1.0
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
1.9
<1.0
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
5.8
<1.0
<1.0
<1.0
NA
<5.0
<1.0
<1.0
<1.0
5.8
<1.0
<1.0
<1.0
NA
<5.0
<1.0
<1.0
<1.0
2.1
<1.0
<1.0
<1.0
NA
<2.0
<1.0
<1.0
<1.0
2.2
<1.0
<1.0
<1.0
NA
<2.0
- <1.0
<1.0
<1.0
2.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
3.1
<1.0
<1.0
<1.0
4EiEl
<2.0
<1.0
200
3
6
0.4
350
70
5
50
Bold indicates concentration exceeds standard
Analytical method numbers are shown beside sample IDs. 1,4-Dioxane was analyzed by Select Ion Monitoring
SS - Shallow Saprolite; DS - Deep Saprolite; GW - Groundwater, NA = Not Analyzed for this parameter, NS = Well not sampled
J= The analyte was positively identified but the value is estimated below the reporting limit
SMW-5A was abandoned March 21, 2002
SMW-4 is damaged and could not be sampled, August 2004; SMW-4 repaired July 2006
DMW-2 reported Chloroform at an estimated value = 0.78J µg/l, August 2004
Vinyl chloride (1.7 ug/1) and 1,1,2-trichloroethane (1.8 ug/I) were detected in DMW-6 in February 2005
Chloroform (3 ug/1), and ,1,1,2-trichloroethane (3.5 ug/1) were detected in DMW-6 in February 2006
1,1,2,2-Trlchloroethane (2.2 ug/1) was detected in DMW-6 in February 2008
Chloroform (3.5 ug/I), and ,1,1,2-trichloroethane (2.5 ug/I) were detected in DMW-6 in August 2009
1,1,2-trichloroethane (1.2 ug/1) was detected in DMW-6 in August 2011
WELL
SCREEN
SS (15'-25')
3S (20'-30')
Table 5 (Page 1 of 6)
File: SA AA -Master Projects\NC DOT -DOT\DOT-500s ContractlDOT-504 Statesville 66\September 2014 Report\Tables%Tables\T5-New sap data
Date: 2/16/2015 Hart & Hickman, PC

Table 5 (Page 2 of 6)
Saprolite Monitoring Well Analytical Data Summary (pg/1)
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
DOT Target Compounds
Non -Target
COMPOUND
1,1,1-Trichloroethane
Trichlorcethene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,4-Dioxane
Methylene
Chloride
Chlorobenzene
WELL
SCREEN
Well ID
Analysis
Sample DateINTERVAL
601
Dec-96
4
1
1
<1
2
6
NA
<5
<1
601
Oct-98
3
<1
10
<1
<1
7
NA
<5
<1
601
Au -01
4.4
<1
6.2
<1
<1
<1
NA
<5
<1
601
Feb-02
2.3
1.5
8.3
<1
<1
<1
NA
<5
<1
601
Au -02
1.6
2.1
11
<1
1.5
2.8
NA
<5
<1
601
Feb-03
4.0
1.6
11
<1
<1
1.3
NA
<5
<1
601
Au -03
1.1
<1
12
<1
<1
<1
NA
<5
<1
601
Feb-04
<1
<1
7.1
<1
<1
2.9
NA
<5
<1
601
Au -04
<1
<1
4.7
<1
<1
1.7
<5.0
<5
<1
601
Feb-05
<1.0
<1.0
3.1
<1.0
<1.0
1.9
NA
<1.0
<1.0
601
Au -05
<1
<1
5.7
<1
<1
2.8
NA
<2
<1
SMW-3
601
Feb-06
<1
<1
7.7
<1
<1
3.0
NA
<2
<1
601
Au -06
<1.0
<1.0
6.9
<1.0
<1.0
2.8
NA
<2.0
<1.0
SS (30'-40')
601
Feb-07
<1.0
<1.0
7.7
<1.0
<1.0
2.7
NA
<2.0
<1.0
601
Au -07
<1.0
<1.0
6.7
<1.0
<1.0
3.4
NA
<2.0
<1.0
601
Feb-08
<1.0
<1.0
8.7
<1.0
<1.0
2.3
NA
<1.0
<1.0
601
Au -08
<1.0
1.5
7.9
<1.0
<1.0
1.9
NA
<1.0
<1.0
601
Feb-09
<1.0
<1.0
8.8
<1.0
<1.0
3.7
NA
<1.0
<1.0
601
Au -09
<1.0
<1.0
4.5
<1.0
<1.0
2.8
NA
<1.0
<1.0
601
Aug-1 0
<1.0
<1.0
4.7
<1.0
<1.0
2.1
NA
<5.0
<1.0
6200B
Aug-1 1
<1.0
<1.0
3.7
<1.0
<1.0
1.4
NA
<2.0
<1.0
6200B
Apr-1 3
<1.0
<1.0
4.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
62008
Oct-13
<1.0
<1.0
4.3
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200E
Ma -14
<1.0
<1.0
2.1
<1.0
<1.0
<1.0
NA
<2.0
<1.0
SMW-4
601
Dec-96
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Oct-98
<1
<1
<1
<1
<1
<1
NA
<5
<1
SS (25'-35')
SMW-5A
601
Dec-96
1
<1
<1
- <1
6
<1
NA
<5
<1
SS (20'-30')
NC GW Standard
200
3
6
0.4
350
70
3
5
50
11-5.
Bold indicates concentration exceeds standard
Analytical method numbers are shown beside sample IDs. 1,4-Dioxane was analyzed by Select Ion Monitoring
SS - Shallow Saprolite; DS - Deep Saprolite; GW - Groundwater; NA = Not Analyzed for this parameter, NS = Well not sampled
J= The analyte was positively identified but the value is estimated below the reporting limit
SMW-5A was abandoned March 21, 2002
SMW-4 is damaged and could not be sampled, August 2004; SMW-4 repaired July 2006
DMW-2 reported Chloroform at an estimated value = 0.78J µg/l, August 2004
Vinyl chloride (1.7 ug/I) and 1,1,2-trichloroethane (1.8 ug/1) were detected in DMW-6 in February 2005
Chloroform (3 ug/1), and ,1,1,2-trichloroethane (3.5 ug/1) were detected in DMW-6 in February 2006
1,1,2,2-Trichloroethane (2.2 ug/I) was detected in DMW-6 in February 2008
Chloroform (3.5 ug/I), and ,1,1,2-trichloroethane (2.5 ug/1) were detected in DMW-6 in August 2009
1,1,2-trichloroethane (1.2 ug/I) was detected in DMW-6 in August 2011
Table 5 (Page, 2 of 6)
File: SAAAA-Master Projects\NC DOT-DOnDOT-500s Contract\DOT-504 Statesville 66\September 2014 Report\Tables\Tables\T5-New sap data
Date: 2/16/2015 Hart & Hickman, PC

Table 5 (Page 3 of 6)
Saprolite Monitoring Well Analytical Data Summary (Ng/1)
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
DOT Target Compounds
Non -Target
COMPOUND
1,1,1-Trichloroethane
Trichloroethene
1,1.Dlchloroethane
1,2-Dlchloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,4-Dioxane
Methylene
Chloride
Chlorobenzene
WELL
SCREEN
Well ID
Analysis
Sample DateINTERVAL
601
Dec-96
53
47
26
<1
37
53
NA
<5
1
8260E
Jan-97
59
54
28
<5
51
59
NA
<5
<5
601
Oct-98
30
41
28
<1
40
59
NA
<5
<1
601
Au -01
110
110
61
<1
51
56
NA
<5
<1
601
Feb-02
66
84
31
<1
64
58
NA
<5
<1
601
Au -02
42
51
23
<1
36
30
NA
<5
<1
601
Feb-03
17
26
16
<1
17
21
NA
<5
<1
601
Au -03
27
49
30
<1
27
39
NA
<5
<1
601
Feb-04
4.2
8.9
9.1
<1
6.8
10
NA
<5
<1
601
Au -04
2.6
6.6
5.3
<1
4.5
7.4
<5.0
<5
<1
601
Feb-05
2.7
7.4
6.1
<1.0
6.3
9.7
NA
<2.0
<1.0
NS
Au-05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Feb-06
NS
NS
NS
NS
NS
NS
NS
NS
NS
601
Au -06
1.5
6.8
4.9
<1.0
2.4
4.9
NA
<2.0
<1.0
DMW-1
601
Feb-07
1.8
5.3
4.9
<1.0
3.0
7.2
NA
<2.0
<1.0
601
Au -07
<1.0
1.4
2.0
<1.0
1.2
2.7
NA
<2.0
<1.0
DS (45'-50')
601
Feb -OS
<1.0
2.1
1.7
<1.0
1.2
2.7
NA
<1.0
<1.0
601
Au -08
<1.0
2.4
1.2
<1.0
2.0
1.8
NA
<1.0
<1.0
601
Feb-09
1.2
3.8
4.7
<1.0
3.2
4.4
NA
<1.0
<1.0
601
Au -09
<1.0
2.9
1.9
<1.0
1.8
2.5
NA
<1.0
<1.0
601
Au -10
4.0
3.5
4.7
<1.0
3.8
4.8
NA
<5.0
<1.0
6200B
Au -11
<1.0
2.4
3.7
<1.0
1.7
3.5
NA
<2.0
<1.0
6200B
Feb-12
<1.0
1.3
1.8
<1.0
<1.0
1.6
NA
<2.0
<1.0
62008
Feb-13
<1.0
1.0
1.3
<1.0
<1.0
1.1
NA
<2.0
<1.0
6200B
Apr-1 3
<1.0
1.0
1.6
<1.0
<1.0
1.1
NA
<2.0
<1.0
6200E
Jun-13
<1.0
1.0
2.8
<1.0
<1.0
2.0
NA
<2.0
<1.0
6200E
Oct-13
<1.0
1.9
3.7
<1.0
1.3
2.8
NA
<2.0
<1.0
6200B
Jan-14
<1.0
3.0
4.5
<1.0
<1.0
3.3
NA
<2.0
<1.0
6200B
Ma -14
<1.0
1.6
2.9
<1.0
<1.0
2.0
NA
<2.0
<1.0
6200B
Jul-14
<1.0
2.1
4.2
<1.0
1.3
3.5
NA
<2.0
<1.0
NC GW Standard
200
3
6
0.4
350
70
3
5
50
Notes:
Bold indicates concentration exceeds standard
Analytical method numbers are shown beside sample IDs. 1,4-Dioxane was analyzed by Select Ion Monitoring
SS - Shallow Saprolite; DS - Deep Saprolite; GW - Groundwater, NA = Not Analyzed for this parameter; NS = Well not sampled
J= The analyte was positively identified but the value is estimated below the reporting limit
SMW-5A was abandoned March 21, 2002
SMW-4 is damaged and could not be sampled, August 2004; SMW-4 repaired July 2006
DMW-2 reported Chloroform at an estimated value = 0.78J µg/l, August 2004
Vinyl chloride (1.7 ug/1) and 1,1,2-trichloroethane (1.8 ug/1) were detected in DMW-6 in February 2005
Chloroform (3 ugh), and ,1,1,2-trichloroethane (3.5 ug/1) were detected in DMW-6 in February 2006
1,1,2,2-Trichloroethane (2.2 ug/1) was detected in DMW-6 in February 2008
Chloroform (3.5 ug/1), and ,1,1,2-trichloroethane (2.5 ugll) were detected in DMW-6 in August 2009
1,1,2-trichloroethane (1.2 ug/I) was detected in DMW-6 in August 2011
Table 5 (Page_ 3 of 6)
File: S:WAA-Master Projects\NC DOT -DOT\DOT-500s Contract\DOT-504 Statesville 66\September 2014 Repart\Tables\Tables\T5-New sap data Hart & Hickman, PC
Date: 2/16/2015

Table 5 (Page 4 of 6)
Saprolite Monitoring Well Analytical Data Summary (Ng/1)
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
DOT Target Compounds
Non -Target
COMPOUND
1,1,1-Trichloroethane
Trichloroethene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,4-Dioxane
Methylene
Chloride
Chlorobenzene
WELL
SCREEN
INTERVAL
Well ID
Analysis
Sample Dat
601
Mar-97
210
120
72
<2.5
130
<2.5
NA
<12.5
<2.5
601
Oct-98
29
18
48
<1
39
<1
NA
<5
<1
601
Au -01
9.9
11
43
<1
17
1.7
NA
1 <5
<1
601
Feb-02
23
18
49
<1
32
<1
NA
<5
<1
601
Au -02
21
22
55
<1
32
5.1
NA
<5
<1
601
Feb-03
12
17
23
<1
13
2.8
NA
<5
<1
601
Au -03
21
37
94
<1
23
<1
NA
<5
<1
601
Feb-04
13
28
73
<1
18
6.6
NA
<5
<1
601
Au -04
27
48
86
<1
38
15
<5.0
<5
<1
601
Feb-05
18
38
40
<1.0
32
12
NA
<2.0
<1.0
601
Au -05
20
36
67
<1
19
12
NA
<2
<1
601
Feb-06
15
42
59
<1
19
9.1
NA
<2
<1
601
Au -06
13
29
58
<1.0
14
12
NA
<2.0
<1.0
601
Feb-07
8.2
19
40
<1.0
11
8.3
NA
<2.0
<1.0
DMW-2
601
Au -07
4.3
10
37.8
<1.0
6.2
4.2
NA
<2.0
<1.0
DS (35'-40')
601
Feb-08
2.1
6.6
22
<1.0
3.0
2.8
NA
<1.0
<1.0
601
Au -08
1.4
6.0
17
<1.0
3.2
2.1
NA
<1.0
<1.0
601
Feb-09
2.1
5.8
16
<1.0
4.5
3.0
NA
<1.0
<1.0
601
Au -09
1.6
5.6
9.2
<1.0
3.2
1.9
NA
<1.0
<1.0
601
Au -10
4.8
4.3
8.9
<1.0
3.5
1.9
NA
<5.0
<1.0
6200B
Au -11
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200E
Feb-12
<1.0
<1.0
2.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Feb-13
<1.0
<1.0
1.6
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200E
Apr-1 3
<1.0
<1.0
2.1
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Jun-13
<1.0
<1.0
1.8
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Oct-13
<1.0
<1.0
1.8
<1.0
<1.0
<1.0
NA
-2.0
<1.0
6200E
Jan-14
<1.0
<1.0
1.3
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Ma -14
<1.0
<1.0
1.3
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Jul-14
<1.0
<1.0
1.1
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6230D
Jan-99
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
NA
<5
<0.5
601
Au -01
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Feb-02
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Au -02
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Feb-03
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Au -03
<1
<1
<1
<1
<1
<1
NA
<5
<1
DS (28.5'-
DMW-5
601
Feb-04
<1
<1
<1
<1
<1
<1
NA
<5
<1
38.5')
601
Au -04
<1
<1
<1
<1
<1
<1
<5.0
<5
<1
601
Feb-05
<1.0
<1.0
<1.0
<1.0
<1.0
<1
NA
<2.0
<1.0
601
Au -05
<1
<1
<1
<1
<1
<1
NA
<2
<1
601
Feb-06
<1
<1
<1 I
<1
<1
<1
NA
<2
<1
601
Au -06
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
NC GW Standard
200
3
6
0.4
350
70
3
5
50
Notes:
Bold indicates concentration exceeds standard
Analytical method numbers are shown beside sample IDs. 1,4-Dioxane was analyzed by Select Ion Monitoring
SS - Shallow Saprolite; DS - Deep Saprolite; GW - Groundwater; NA = Not Analyzed for this parameter; NS = Well not sampled
J= The analyte was positively identified but the value is estimated below the reporting limit
SMW-5A was abandoned March 21, 2002
SMW-4 is damaged and could not be sampled, August 2004; SMW-4 repaired July 2006
DMW-2 reported Chloroform at an estimated value = 0.78J µgh, August 2004
Vinyl chloride (1.7 ug/I) and 1,1,2-trichloroethane (1.8 ug/I) were detected in DMW-6 in February 2005
Chloroform (3 ug/I), and ,1,1,2-trichloroethane (3.5 ug/I) were detected in DMW-6 in February 2006
1,1,2,2-Trichloroethane (2.2 ug/I) was detected in DMW-6 in February 2008
Chloroform (3.5 ug/1), and ,1,1,2-trichloroethane (2.5 ug/1) were detected in DMW-6 in August 2009
1,1,2-trichloroethane (1.2 ug/1) was detected in DMW-6 in August 2011
Table 5 (Page 4 of 6)
File: SAAAA-Master Projects\NC DOT -DOT\DOT-500s Contract\DOT-504 Statesville 66\September 2014 Report\Tables\Tables\T5-New sap data Hart &Hickman PC
Date: 2/16/2015

Table 5 (Page 5 of 6)
Saprolite Monitoring Well Analytical Data Summary (Ng/1)
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
DOT Target Compounds
Non -Target
COMPOUND
1,1,1-Trichloroethane
Trichloroethene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
1,4-Dioxane
Methylene
Chloride
Chlorobenzene
WELL
SCREEN
INTERVAL
Well ID
Analysis
at
Sample Date'
6230D
Jan-99
74
67
42
<0.5
160
1.5
NA
<5
<0.5
601
Au -01
95
57
60
<1
93
4.5
NA
<5
<1
601
Feb-02
140
170
89
<1
500
<10
NA
<5
<10
601
Au -02
140
190
120
<1
590
18
NA
<5
<10
601
Feb-03
100
180
77
<1
430
<10
NA
<5
<10
601
Au -03
97
170
80
4.3
420
14
NA
8.5
<1
601
Feb-04
63
140
74
<1
350
10
NA
<5
<1
601
Au -04
61
150
74
<10
380
8.1J
180
<50
<10
601
Feb-05
49
150
69
7.8
250
10
NA
6.6
<1.0
601
Au -05
65
170
83
<5
290
12
NA
<10
<5
601
Feb-06
44
220
98
1.8
390
9.2
180
5.8
<1
601
Au -06
19
190
83
<5
270
9.0
NA
<10
<5.0
601
Feb-07
39
170
81
<5
330
12.0
180
<10
<5.0
DMW-6
601
Au -07
40.3
167
100
<10.0
290
<10.0
NA
<20.0
<10.0
DS (26.26%
601
Feb-08
33
130
77
<1.0
200
6.9
170
<1.0
<1.0
36.25')
601
Au -08
24
100
77
3.6
180
6.1
NA
<1.0
<1.0
601
Feb-09
18
96
67
<1.0
220
6.7
NA
<1.0
<1.0
601
Aug- 9
23
120
83
4.9
220
6.6
NA
<1.0
<1.0
601
Aug-10
16
100
79
<1.0
200
8.6
NA
<5.0
<1.0
6200E
Aug-1 1
10.6
100
75.9
1.3
147
3.9
NA
<2.0
<1.0
6200E
Feb-12
5.9
68.5
63.1
<1.0
90.5
3.0
NA
<2.0
<1.0
6200E
Feb-13
5.2
71.8
61.6
<1.0
92.1
3.7
NA
<2.0
<1.0
6200B
Apr-1 3
5.5
71.4
65.0
1.1
99.2
3.8
NA
<2.0
<1.0
6200B
Jun-13
5.1
67.1
67.8
<1.0
92.7
3.0
NA
-2.0
<1.0
6200B
Oct-13
5.0
69.9
71.1
1.1
97.7
4.3
NA
<2.0
<1.0
6200B
Jan-14
3.6
62.5
50.9
1.2
73.2
3.5
NA
<2.0
<1.0
6200E
Ma -14
3.1
64.9
57.2
<1.0
67.7
1.9
NA
<2.0
<1.0
6200E
Jul-14
1.9
43.2
40.6
<1.0
52.0
2.5
NA
<2.0
<1.0
601
Au -01
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Feb-02
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Au -02
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Feb-03
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Au -03
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Feb-04
<1
<1
<1
<1
<1
<1
NA
<5
<1
601
Au -04
<1
<1
<1
<1
<1
<1
<5.0
<5
<1
601
Feb-05
<1
<1
<1
<1
<1
<1
NA
<1.0
<1
601
Au -05
<1
<1
<1
<1
<1
<1
NA
<2
<1
601
Feb-06
<1
<1
<1
<1
<1
<1
NA
<2
<1
601
Au -06
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<2.0
601
Feb-07
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<2.0
601
Au -07
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
DMW-8
601
Feb-08
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1,0
DS (14'-24')
601
Au -08
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1.0
601
Feb-09
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1.0
601
Au -09
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
- <1.0
601 1
Aug-10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<5.0
<1.0
6200E
Au -11
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Feb-12
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Feb-13
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
A r-13
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Jun-13
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
Oct-1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
Jan-14
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
L
Ma -14
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
Jul-14
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
NC GW Standard
200
3
6
0.4
350
70
3
5
50
Notes:
Bold indicates concentration exceeds standard
Analytical method numbers are shown beside sample Ds. 1,4-Dioxane was analyzed by Select Ion Monitoring
SS - Shallow Saprolite; DS - Deep Saprolite; GW - Groundwater; NA = Not Analyzed for this parameter; NS = Well not sampled
J= The analyte was positively identified but the value is estimated below the reporting limit
SMW-5A was abandoned March 21, 2002
SMW-4 is damaged and could not be sampled, August 2004; SMW-4 repaired July 2006
DMW-2 reported Chloroform at an estimated value = 0.78J µg/l, August 2004
Vinyl chloride (1.7 ug/1) and 1,1,2-trichloroethane (1.8 ugA) were detected in DMW-6 in February 2005
Chloroform (3 ug/1), and ,1,1,2-trichloroethane (3.5 ugA) were detected in DMW-6 in February 2006
1,1,2,2-Trichloroethane (2.2 ugA) was detected in DMW-6 in February 2008
Chloroform (3.5 ug/1), and ,1,1,2-trichloroethane (2.5 ugh) were detected in DMW-6 in August 2009
1,1,2-trichloroethane (1.2 ugA) was detected in DMW-6 in August 2011
Table 5 (Page 5 of 6)
File: S:WAA-Master Projects\NC DOT -DOT\DOT-500s Contract\DOT-504 Statesville 66\September 2014 Report\Tables\Tables\T5-New sap data
Date: 2/1612015 Hart & Hickman, PC

Table 5 (Page 6 of 6)
Saprolite Monitoring Well Analytical Data Summary (pg/1)
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
DOT Target Compounds
Non -Target
COMPOUND
1,1,1-Trichloroethane
Trichloroethene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dlchloroethene
cis-1,2-Dichloroethene
1,4-Dioxane
Methylene
Chloride
Chlorobenzene
WELL
SCREEN
INTERVAL
Well ID
Analysis
Sample Datc
6200B
Feb-12
<1.0
3.3
4.5
<1.0
2.1
<1.0
NA
<2.0
<1.0
6200B
Feb-13
<1.0
5.8
8.5
<1.0
3.6
<1.0
NA
<2.0
<1.0
6200B
Apr-13
<1.0
6.4
7.7
<1.0
4.4
1.1
NA
<2.0
<1.0
DMW-9
62008
Jun-13
<1.0
5.6
6.7
<1.0
3.6
1.2
NA
<2.0
<1.0
DS (30'-40')
6200B
Oct-13
<1.0
4.9
4.9
<1.0
3.4
1.2
NA
<2.0
<1.0
62008
Jan-14
<1.0
2.9
2.6
<1.0
1.9
<1.0
NA
-2.0
<1.0
6200B
Ma -14
<1.0
2.9
2.3
<1.0
1.9
<1.0
NA
<2.0
<1.0
6200B
Feb-12
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200E
Feb-13
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Apr-1 3
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
DMW-10
6200B
Jun-13
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Oct-13
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
DS (30'40)
6200B
Jan-14
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200B
Ma -14
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200E
Jul-14
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<2.0
<1.0
6200E
Feb-12
<1.0
10.E
10.9
<1.0
15.0
<1.0
NA
<2.0
<1.0
6200E
Feb-13
<1.0
8.0
7.0
<1.0
10.5
<1.0
NA
<2.0
<1.0
6200B
Apr-13
<1.0
9.0
7.6
<1.0
11.9
<1.0
NA
<2.0
<1.0
DMW-11
6200B
Jun-13
<1.0
6.7
4.9
<1.0
7.4
1.4
NA
<2.0
<1.0
6200B
Oct-13
<1.0
6.3
6.6
<1.0
9.0
<1.0
NA
<2.0
<1.0
DS (30'-40')
6200B
Jan-14
<1.0
8.1
6.8
<1.0
9.5
<1.0
NA
<2.0
<1.0
62008
May-14
<1.0
6.3
6.4
<1.0
7.5
<1.0
NA
<2.0
<1.0
6200E
Jul-14
<1.0
7.9
8.6
<1.0
11.0
<1.0
NA
<2.0
<1.0
NC GW Standard
200
3
6
0.4
350
70
3
5
50
ivuroa.
Bold indicates concentration exceeds standard
Analytical method numbers are shown beside sample IDs. 1,4-Dioxane was analyzed by Select Ion Monitoring
SS - Shallow Saprolite; DS - Deep Saprolite; GW - Groundwater; NA = Not Analyzed for this parameter; NS = Well not sampled
J= The analyte was positively identified but the value is estimated below the reporting limit
SMW-5Awas abandoned March 21, 2002
SMW-4 is damaged and could not be sampled, August 2004; SMW-4 repaired July 2006
DMW-2 reported Chloroform at an estimated value = 0.78J µgh, August 2004
Vinyl chloride (1.7 ug/1) and 1,1,2-trichloroethane (1.8 ug/1) were detected in DMW-6 in February 2005
Chloroform (3 ug/1), and ,1,1,2-trichloroethane (3.5 ug/1) were detected in DMW-6 in February 2006
1,1,2,2-Trichloroethane (2.2 ug/1) was detected in DMW-6 in February 2008
Chloroform (3.5 ug/1), and ,1,1,2-trichloroethane (2.5 ug/1) were detected in DMW-6 in August 2009
1,1,2-trichloroethane (1.2 ug/1) was detected in DMW-6 in August 2011
Table 5 (Page 6 of 6)
File: S:WAA-Master Projects\NC DOT -DOT\DOT-500s Contract\DOT-504 Statesville 66\September 2014 Report\Tables\Tables\T5-New sap data
Hart &Hickman, PC
Date: 2/16/2015

Table 6
Shallow Bedrock Monitoring Well Analytical Data Summary (mg/l)
Former ATL Site No. 2.66
Statesville, North Carolina
'i H&H Job No. DOT-504
COMPOUND
Trichloroethane
Trichloroethene
1,1-
Dichloroethane
1,1-
Dichloroethene
cis-1,2-
Dichloroethene
1,4-0ioxane
Chlorobenzene
WELL
SCREEN
INTERVAL
Well ID
Analysis
Sample Date
601
Mar-97
<1
<1
<i
<7
<1
NA
<1
601
Oct-98
<1
<1
<i
<t
<1
NA
<7
601
Feb-03
<t
<1
<1
<1
<1
NA
<1
Set
Au -03
<1
<t
<i
<1
<1
NA
c1
601
Feb-04
<1
<1
<1
<1
<1
NA
<1
601/8260
Au -04
<1
<1
<1
<t
<1
<5.0
<1
601
Feb-05
<1
c1
<1
<1.
<1
NA
<t
601
Au 5
c1
<1
<1
c1
<1
NA
<1
601
Feb-06
<1
<1
<1
<1
<1
NA
<1
DMW-3
601
Au -06
<1.0
<1.0
<1.0
<1.0
<1.0
NA
-1.0
(55'-60')
601
Feb-07
<1.0
<1.0
c1.0
<1.0
<7.0
NA
<1.0
601
Au -07
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
601
Feb-08
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
601
Au -08
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
601
Feb-09
<1.0
<1.0
-1.0
<1.0
<1.0
NA
<1.0
601
Au -10
<1.0
<1.0
<1.0
-1.0
<1.0
NA
<1.0
6200B
Aug-1 I
<1.0
<7.0
c1.0
<1.0
<1.0
NA
<1.0
6200B
A r-13
<1.0
<1.0
<1.0
c1.0
<1.0
NA
<1.0
6200E
Oct-13
-1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
5/92014
Ma -14
<1.0
<1.0
<1.0
c1.0
<1.0
NA
<1.0
601
Mar-97
<1
<1
<1
<1
<1
NA
<1
601
1 Oct-98
<i
<1
<1
<t
<1
NA
<t
601
Au -01
<1
<1
<1
<1
<1
NA
<t
601
Feb-02
<1
<1
c1
<1
<1
NA
<1
601
Au -02
<1
<1
<1
<1
<1
NA
<1
601
Feb-03
<1
<1
<1
<1
<1
NA
<1
601
Au 3'
<1
c1
<1
c1
<1
NA
<1
601
Feb-04
<1
c1
<1
<1
<1
NA
c1
601/8260
Au -04
<1
<1
<1
<1
<1
c5.0
<1
601
Feb-05
<1
<1
<1
<7
<1
NA
<t
601
Au -05
<i
<t
c1
<1
<1
NA
<1
DMW4
601
Feb-06
<t
<1
c1
<1
<1
NA
<1
(65-70')
601
Au -06
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
601
Feb-07
<1.0
<1.0
<1.0
<1.0
<1.0
NA
-1.0
601
Au -07
<1.0
<1.0
<1.0
<1.0
<1.0
NA
-1.0
601
Feb-08
<7.0
<7.0
<1.0
<1.0
<1.0
NA
<1.0
601
Au -08
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
601
Au -09
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
601
Au -10
<1.0
<1.0
<1.0
c1.0
<1.0
NA
<1.0
6200E
Aug-1 I
<1.0
<7.0
<1.0
-1.0
<1.0
NA
<1.0
6200B
A r-13
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
6200E
Oct-13
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
6200B
Ma -14
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
601
Au -01
<1
<1
c1
<1
<1 -
NA
<1
601
Feb-02
<1
<1
<1
1.9
<1
NA
c1
601
Au -02
2A
6.3
1.6
14
<1
NA
ct
601
Feb-03
2.1
2.4
<1
2.8
<t
NA
<t
601
Au -03
3.8
7.0
1.5
12
<1
NA
ct
601
Feb-04
<1
1.5
<1
2.6
<t
NA
<7
601/8260
Au -04
0.81J
2.2
0.70J
3.6
<i
<5.0
<t
601
Feb-05
<1
2.1
-1.0
3.9
<1
NA
<1
601
Au -05
<1
1.6
<1
1.9
<i
NA
<1
601
Feb-06
<1
3.7
1.5
3
<1
NA
<1
601
Au -06
<1.0
4.6
1.3
3.3
c1.0
NA
<1.0
601
Feb-07
<1.0
2.2
1.8
2.5
<1.0
NA
<1.0
601
Au -07
<1.0 1
2.7
1.2
3.5
<1.0
NA
<1.0
DMW-7
601
Feb-08
<1.0
2.2
<1.0
1.6
<1.0
NA
<1.0
(60'-65')
601
Au -08
<1.0
3.1
<1.0
2.6
<1.0
NA
<1.0
601
Feb-09
<1.0
2.3
1.4
2.8
<1.0
NA
<1.0
601
Au -09
<1.0
2.1
c1.0
1.3
<1.0
NA
<1.0
601 1
Au -10
<1.0
3.2
1.1
2.8
<1.0
NA
c1.0
6200B
Au -11
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
6200B
Feb-12
<1.0
c1.0
<1.0
<1.0
<1.0
NA
<1.0
6200B
Feb-131
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
6200B
A r-13
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
6200B
Jun-13
<1.0
<1.0
<1.0
I <1.0 I
<1.0
NA
-1.0
6200B
Oct-13
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
6200E
Jan-14
<1.0
<7.0
<1.0
<1.0
<1.0
NA
<1.0
62008
<1.0
<1 0
<1.0
<1.0
<1.0
0<1.
62008
Ja-14
ul-14
<1
<10
<1.0
<1.0
NA
IF -NC
GW STANDARD
200 13
6
350
70
3
50
Analytical method numbers are shown beside sample IDs.
Bold indicates concentration exceeds standard
GIN- Ground Water
J= The analyte was positively identified but the value is estimated below the reporting limit
NA = Not Analyzed for this parameter
1,4-0ioxane was analyzed by Method SW846-8260BISIM
r = Methylene chloride detected at a concentration of 2.7 (µg/Q in February 2013
<..r�.�wc ooraorommmc.,,..�oorew smr.,d�b ssss.wm...mr. n.,mra.n..�r.n.amJa..eemm Table (Page 1 of 1)
mm. memis Hart & Hickman, PC

Table 7 (Page 1 of 6)
Summary of Natural Attenuation Indicator Data
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-604
Monitoring Well ED
SMW-1
SMW-2
Sampling Date
Aug-10
Aug-11
Apr-13
Oct-13
May-14
Aug-10
Aug-11
Apr-13
Oct-13
May-14
Field Measurements
Dissolved Oxygen (mg/1)
1.83
3.13
3.50
1.35
1.61
0.34
0.98
3.20
1.17
1.04
Ferrous Iron (mg/1)
NA
NA
<0.2
<0.2
<0.2
NA
NA
<0.2
<0.2
1.00 '
Redox(mV)
277
278
144.2
320
368
384
521
280
406
370
Conductivity (µS/cm)
130.0
160.0
123.0
157.8
298.0
288.0
220.0
263.0
270.1
344.9
pH (standard units)
5.27
5.21
5.13
5.39
5.76
5.31
5.03
5.22
5.29
5.55
Temperature (°C)
18.0
18.1
19.3
17.5
18.0
18.6
19.0
19.6
17.3
18.0
Labortaory Analytical Parameters
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Nitrate (mg/1)
Sulfate (mg/1)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
TOC (mg/1)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Methane (µg/l)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Ethane (µg/l)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Ethene (µg/1)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Metals 601017470 (,ell)
Arsenic
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Barium
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Cadmium
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Chromium
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Lead
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Selenium
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Silver
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Mercury
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Metabolic Acids (m0)
Acetic Acid
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Butyric Acid
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Lactic Acid
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Propionic Acid
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Pyruvic Acid
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Notes:
TOC = Total Organic Carbon; DO = Dissolved Oxygen; NA = Not Analyzed
1 = Sulfide and metals samples collected on July 17, 2013.
RW S:~.MastwPrajmt WC Dar D0TWT-WNCantre MOT-504Sta v le6Weptember2014RepwffabksVablee\T7-Nat.Atten.nm Table 7 (Page 1 of 6)
Date: 2M64015
Hart &Hickman, PC

1
Table 7 (Page 2 of 6)
Summary of Natural Attenuation Indicator Data
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
Monitoring Wel1ID
SMW-3
DMW-1
Sampling Date
Aug-10
Aug-11
Apr-13
Oct-13
May-14
Feb-12
Dec-12
Feb-13
Apr-13
Jun-13'
Oct-13
Jan-14
May-14
Jul-14
Field Measurements
Dissolved Oxygen (mg/1)
0.31
0.97
2.22
1.70
1.22
0.68
NA
2.40
2.48
0.86
1.20
1.11
1.37
1.61
Ferrous Iron (mg/1)
NA
NA
<0.2
<0.2
<0.2
<0.2
NA
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
Redox(mV)
121
84
107
106
124
310
NA
296
116
414
320
206
300
319
Conductivity (µS/cm)
128.0
110.0
123.0
127.1
196.7
96.4
NA
106.3
73.0
71.4
157.8
70.0
125.5
302.7
pH (standard units)
5.34
5.70
5.51
5.58
5.98
5.64
NA
5.63
5.50
5.56
5.39
5.57
5.25
4.99
Temperature (°C)
18.6
19.0
18.2
16.4
16.4
18.3
NA
18.3
18.2
19.8
17.5
15.7
16.0
15.7
Labortaory Analytical Parameters
0.28
NA
NA
NA
NA
<0.20
NA
0.076
0.079
0.07
0.11
0.23
0.32
0.24
Nitrate (mg/1)
Sulfate (mg/1)
48
NA
NA
NA
NA
<5.0
NA
5.2
4.2
4.6
4.2
4.5
3.9
3.6
Sulfide (mg/1)
NA
NA
NA
NA
NA
NA
<0.10
<0.10
NA
<0.10
<0.10
<O.IO
<0.10
<0.10
TOC (mg/1)
2.5
NA
NA
NA
NA
4.9
NA
26.7
4.9
5.7
4.5
5.5
4.4
6.1
Methane (µg/1)
NA
NA
NA
NA
NA
15.7
NA
12.8
7.3
8.2
9.3
15.4
14.2
10.2
Ethane (µg/1)
NA
NA
NA
NA
NA
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
Ethene (µg/1)
NA
NA
NA
NA
NA
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
Metals 601017470 (ur/1)
Arsenic
NA
NA
NA
NA
NA
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
Barium
NA
NA
NA
NA
NA
NA
56.7
58.1
NA
57.5
56.8
60.2
59.8
61.8
Cadmium
NA
NA
NA
NA
NA
NA
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
<1.0
Chromium
NA
NA
NA
NA
NA
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
Lead
NA
NA
NA
NA
NA
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
Selenium
NA
NA
NA
NA
NA
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
Silver
NA
NA
NA
NA
NA
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
Mercury
NA
NA
NA
NA
NA
NA
<0.20
<0.20
NA
<0.20
<0.20
<0.20
<0.20
<0.20
Metabolic Acids (m¢/1)
Acetic Acid
NA
NA
NA
NA
NA
<5.0
NA
<1.8
1.91
<0.67
<0.67
<0.67
NA
NA
Butyric Acid
NA
NA
NA
NA
NA
<5.0
NA
<0.87
<0.87
<0.10
<0.10
<0.10
NA
NA
Lactic Acid
NA
NA
NA
NA
NA
<25
NA
<2.3
<2.3
<2.0
<2.0
<2.0
NA
NA
Propionic Acid
NA
NA
NA
NA
NA
<5.0
NA
<1.0
<1.0
<0.25
<0.25
<0.25
NA
NA
Pyruvic Acid
NA
NA
NA I
NA
NA 1
<10 1
NA I
<2.0
<2.0
<0.53
<0.53
<0.53
NA
NA
Notes:
TOC = Total Organic Carbon; DO = Dissolved Oxygen; NA = Not Analyzed
t = Sulfide and metals samples collected on July 17, 2013.
Table 7 (Page 2 of 6)
Dee: 2hr2015 ter P,geclsWC WT-OOT�DOT+ CmUxt\00T-500 Statwrille fiSVSeptembcr 2014 Report\TaEka\Tables\T7-Nat. Atten. nex (1)
Date: v1e¢o1s Hart &Hickman, PC

Table 7 (Page 3 of 6)
Summary of Natural Attenuation Indicator Data
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
Monitoring Well ID
DMW-2
DMW-6
Sampling Date
Feb-12
Dec-12
Feb-13
Apr-13
Jun-131
Oct-13
Jan-14
May-14
Jul-14
Feb-12
Dec-12
Feb-13
Apr-13
Jun-131
Oct-13
Jan-14
May-14
Jul-14
Field Measurements
Dissolved Oxygen (mg/1)
0.41
NA
2.83
3.08
0.83
1.17
1.16
1.66
0.82
1.24
NA
3.23
3.32
0.76
1.17
1.06
0.41
1.44
Ferrous Iron (mg/1)
<0.2
NA
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
NA
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
Redox(mV)
207
NA
324
242
372
286
197
210
195
174
NA
91
131
410
136
49
87
106
Conductivity (µS/cm)
281.6
NA
243.6
263.0
253.9
282.3
234.0
445.6
490.9
418.9
NA
363.3
385.0
364.7
410.9
330.0
409.7
425.8
pH (standard units)
5.18
NA
5.06
4.84
5.02
5.06
4.94
5.30
5.31
6.11
NA
6.26
5.33
6.11
6.15
6.16
6.61
6.97
Temperature (°C)
18.6
NA
18.3
18.6
19.6
16.2
15.7
17.1
17.0
16.4
NA
16.3
16.7
16.3
15.6
16.0
16.4
17.0
Labortaory Analytical Parameters
4.50
NA
3.20
5.40
2.90
3.50
3.70
2.40
2.30
<0.20
NA
0.59
0.74
0.33
0.86
0.54
<0.020
<0.020
Nitrate (mg/1)
Sulfate (mg/1)
66.8
NA
79.1
60.6
79.5
72.7
79.1
83.3
81.8
81.3
NA
62.7
86.9
70.3
54.3
58.2
59.5
45.9
Sulfide (mg/1)
NA
<0.10
<0.10
NA
<0.10
<0.10
<0.10
<0.10
<0.10
NA
<0.10
<0.10
NA
<0.10
<0.10
<0.10
<0.10
<0.10
TOC (mg/1)
6.0
NA
5.4
11.4
42.6
5.8
7.0
5.3
5.8
10.3
NA
11.8
11.8
11.0
46.0
17.1
11.1
14.2
Methane (µg/1)
76.4
NA
105
124
110
62.8
61.9
30.3
<6.6
22.2
NA
19.2
18.9
<6.6
93.8
49.4
17.4
<6.6
Ethane (µg/1)
<I0.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<10.0
NA
<6.2
<6.2
<6.2
7.0
7.0
<6.2
<6.2
Ethene (µg/1)
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
Metals 601017470 (ue/1)
Arsenic
NA
<10.0
<I0.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
Barium
NA
32.3
27.6
NA
28.4
28.3
28.2
27.2
28.2
NA
117
216
NA
114
ill
195
109
108
Cadmium
NA
<1.0
<1.0
NA
<1.0
<1.0
1.0
<I.0
<1.0
NA
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
<1.0
Chromium
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
37.9
NA
<5.0
<5.0
35.7
<5.0
<5.0
Lead
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
10.3
NA
<5.0
<5.0
10.6
<5.0
<5.0
Selenium
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
Silver
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
Mercury
NA
<0.20
<0.20
NA
<0.20
0.22
<0.20
<0.20
<0.20
NA
<0.20
<0.20
NA
<0.20.
<0.20
<0.20
<0.20
<0.20
Metabolic Acids (mjz1V
Acetic Acid
<5.0
NA
<1.8
<1.8
<0.67
<0.67
<0.67
NA
NA
<5.0
NA
<1.8
1.8J
<0.67
<0.67
<0.67
NA
NA
Butyric Acid
<5.0
NA
<0.87
<0.87
<0.10
<0.10
<0.10
NA
NA
<5.0
NA
<0.87
<0.87
<0.10
<0.10
<0.10
NA
NA
Lactic Acid
<25
NA
<2.3
<2.3
<2.0
<2.0
<2.0
NA
NA
<25
NA
<2.3
<2.3
<2.0
<2.0
<2.0
NA
NA
Propionic Acid
<5.0
NA
<1.0
<1.0
<0.25
<0.25
<0.25
NA
NA
<5.0
NA
<1.0
<1.0
<0.25
<0.25
<0.25
NA
NA
Pyruvic Acid
<10
NA
<2.0
<2.0
<0.53
<0.53
<0.53
NA
NA
<10
NA
<2.0
<2.0
<0.53
<0.53
<0.53
NA
NA
Notes:
TOC = Total Organic Carbon; DO = Dissolved Oxygen; NA = Not Analyzed
( = Sulfide and metals samples collected on July 17, 2013.
File: S:YVN-Master PrysebW C DOT-DOTtDOTE00s CanVacttDOT-506 StatesWlle fi6\SeptemEe, 2010 RepaM1\Tables\Table\77-Nat. Allen. nea (3) Table 7 (Page 3 of 6)
Date: vteaots Hart & Hickman, PC

Table 7 (Page 4 of 6)
Summary of Natural Attenuation Indicator Data
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-604
Monitoring Well El)
DMW-8
DMW-9
Sampling Date
Feb-12
Dec-12
Feb-13
Apr-13
Jun-131
Oct-13
Jan-14
May-14
Jul-14
Feb-12
Dec-12
Feb-13
Apr-13
Jun-131
Oct-13
Jan-14
May-14
Field Measurements
Dissolved Oxygen (mg/1)
4.44
NA
4.86
4.98
4.76
3.55
3.10
2.86
2.04
0.95
NA
1.01
1.09
1.11
2.45
2.32
2.07
Ferrous Iron (mg/1)
<0.2
NA
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
0.5
NA
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
Redox(mV)
258
NA
94
101
103
116
237
220
197
111
NA
293
139
314
184
116
112
Conductivity (µS/cm)
159.8
NA
147.3
150.0
146.0
168.7
142.0
162.8
170.9
290.1
NA
245.4
268.0
249.8
283.0
240.0
270.6
pH (standard units)
6.51
NA
6.78
6.16
6.10
6.54
6.51
6.62
6.44
5.70
NA
5.62
5.40
5.88
5.47
5.53
5.69
Temperature (°C)
14.6
NA
16.1
15.0
17.6
16.2
12.6
14.5
15.0
18.2
NA
18.6
18.6
18.4
18.4
17.9
17.8
Labortaory Analytical Parameters
0.76
NA
0.77
0.56
0.73
0.72
0.88
0.80
0.79
2.1
NA
1.7
1.6
1.5
1.5
1.4
1.5
Nitrate (mg/1)
Sulfate (mg/1)
<5.0
NA
2.6
2.2
2.4
2.3
3.0
2.1
<2.0
61.5
NA
66.7
65.6
85.1
65.8
76.3
71.3
Sulfide (mg/1)
NA
<0.10
<0.10
NA
<0.10
<0.10
<0.10
<0.10
<0.10
NA
<0.10
<0.10
NA
<0.10
<0.50
<0.50
<0.50
TOC (mg/1)
22.2
NA
2.2
22.1
3.0
2.5
2.1
3.4
24.4
7.1
NA
5.7
7.2
5.5
5.5
8.1
5.6
Methane (µg/1)
<10.0
NA
<6.6
<6.6
<6.6
8.3
<6.6
<6.6
<6.6
147
NA
151
153
24.6
40.6
175
116
Ethane (µg/1)
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
Ethene (µg/1)
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
Metals 601017470 gljl
Arsenic
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
Barium
NA
60.4
33.8
NA
36.1
35.9
33.6
28.9
30.7
NA
100
91.0
NA
84.3
86.2
85.0
82.0
Cadmium
NA
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
Chromium
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
Lead
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
Selenium
NA
<10.0
<I0.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
Silver
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
Mercury
NA
<0.20
<0.20
NA
<0.20
<0.20
<0.20
<0.20
<0.20
NA
<0.20
<0.20
NA
<0.20
<0.20
<0.20
<0.20
Metabolic Acids (me/1)
Acetic Acid
<5.0
NA
<1.8
<1.8
<0.67
<0.67
<0.67
NA
NA
<5.0
NA
<1.8
<1.8
<0.67
<0.67
NA
NA
Butyric Acid
<5.0
NA
<0.87
<0.87
<0.10
<0.10
<0.10
NA
NA
<5.0
NA
<0.87
<0.87
<0.10
<0.10
NA
NA
Lactic Acid
<25
NA
<2.3
<2.3
<2.0
<2.0
<2.0
NA
NA
<25
NA
<2.3
<2.3
<2.0
<2.0
NA
NA
Propionic Acid
<5.0
NA
<1.0
<1.0
<0.25
<0.25
<0.25
NA
NA
<5.0
NA
<1.0
<1.0
<0.25
<0.25
NA
NA
Pyruvic Acid
<10
NA
<2.0
<2.0
<0.53
<0.53
<0.53
NA
NA
<10
NA
<2.0
<2.0
<0.53
<0.53
NA
NA
Notes:
TOC = Total Organic Carbon; DO = Dissolved Oxygen; NA = Not Analyzed
t = Sulfide and metals samples collected on July 17, 2013.
J = estimated concentration greater than the method deletion limit, but below the reporting limit.
Table 7 (Page 4 of 6)
Re: S:~-Master Projwts\NC DOT-DOTDOTZi CmVa MOT-504 Statesville 66\Sept=ber 2014 aepoMTab \TWWT7-Nat. Allen. nm (4) Hart &Hickman, PC
Data: z162015

Table 7 (Page 5 of 6)
Summary of Natural Attenuation Indicator Data
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
Monitoring Well ED
DMW-10
DMW-I I
Sampling Date
Feb-12
Dec-12
Feb-13
Apr-13
Jun-131
Oct-13
Jan-14
May-14
Jul-14
Feb-12
Dec-12
Feb-13
Apr-13
Jun-131
Oct-13
Jan-14
May-14
Jul-14
Field Measurements
Dissolved Oxygen (mg/l)
2.25
NA
0.88
0.92
0.52
0.82
0.80
1.11
2.01
1.03
NA
1.13
1.20
0.83
2.24
2.19
1.99
2.16
Ferrous Iron (mg/1)
<0.2
NA
5.0
5.0
4.5
5.0
5.0
6.0
5.4
0.5
NA
7.5
8.0
8.0
8.5
9.0
10.0
9.0
Redox (mV)
22
NA
-58
-27
4
-37
-34
-17
-17
18
NA
54
76
116
12
66.4
71.4
93
Conductivity (µS/cm)
463.2
NA
440.0
440.0
428.4
490.6
400.0
381.2
480.1
666.8
NA
500.3
556.0
490.4
576.1
492.0
448.9
502.3
pH (standard units)
6.51
NA
6.47
6.24
6.34
6.35
6.39
6.61
6.71
6.67
NA
6.32
5.70
6.23
6.30
6.15
6.20
6.29
Temperature (°C)
18.3
NA
18.9
18.6
18.4
17.6
17.3
17.9
17.0
1.7.3
NA
18.3
17.1
17.3 '
17.6
16.6
16.8
16.4
Labortaory Analytical Parameters
<0.20
NA
<0.020
<0.020
<0.020
0.12
<0.020
<0.020
<0.020
<0.20
NA
<0.020
<0.020
<0.020
<0.020
<0.020
<0.020
<0.020
Nitrate (mg/1)
Sulfate (mg/1)
19.0
NA
27.4
22.4
24.9
35.3
20.8
20.2
17.6
114
NA
99.7
106
103
75
108
47.9
80.3
Sulfide (mg/1)
NA
<0.10
0.15
NA
<0.10
<0.10
<0.10
<0.10
<0.10
NA
<0.10
<0.10
NA
<0.10
<0.50
<0.10
<0.10
<0.10
TOC (mg/1)
21.4
NA
24.9
26.0
22.8
18.3
21.6
23.6
27.9
23.9
NA
24.2
26.9
25.0
18.4
23.4
23.8
21.9
Methane (µg/1)
945
NA
1,040
839
389
701
<6.6
555
1160
1,640
NA
347
260
65.3
663
3,790
2,140
4,070
Ethane (µg/1)
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
14.5
NA
6.5
7.7
<6.2
<6.2
<6.2
<6.2
<6.2
Ethene (µg/l)
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<10.0
NA
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
<6.2
Metals 601017470 (uzll)
Arsenic
NA
<10.0
<10.0
NA
<I0.0
<10.0
<10.0
<10.0
<10.0
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<I0.0
<10.0
Barium
NA
140
707
NA
144
136
141
252
143
NA
88.3
89.7
NA
70.0
69.8
66.5
58.9
69.5
Cadmium
NA
<1.0
8.2
NA
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<1.0
<1.0
NA
<1.0
<1.0
<1.0
<1.0
<1.0
Chromium
NA
<5.0
224
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
Lead
NA
<5.0
92.7
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
Selenium
NA
<10.0
10.8
NA
<10.0
<10.0
<10.0
<10.0
<10.0
NA
<10.0
<10.0
NA
<10.0
<10.0
<10.0
<10.0
<10.0
Silver
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
NA
<5.0
<5.0
NA
<5.0
<5.0
<5.0
<5.0
<5.0
Mercury
NA
<0.20
<0.20
NA
<0.20
<0.20
<0.20
<0.20
<0.20
NA
<0.20
<0.20
NA
<0.20
<0.20
<0.20
<0.20
<0.20
Metabolic Acids (me/1)
Acetic Acid
<5.0
NA
<1.8
1.91
<0.67
<0.67
0.67J
NA
NA
<5.0
NA
<1.8
<1.8
<0.67
<0.67
<0.67
NA
NA
Butyric Acid
<5.0
NA
<0.87
<0.87
<0.10
<0.10
<0.10
NA
NA
<5.0
NA
<0.87
<0.87
<0.10
<0.10
<0.10
NA
NA
Lactic Acid
<25
NA
<2.3
<2.3
<2.0
<2.0
<2.0
NA
NA
<25
NA
<2.3
<2.3
<2.0
<2.0
<2.0
NA
NA
Propionic Acid
<5.0
NA
<1.0
<1.0
<0.25
<0.25
<0.25
NA
NA
<5.0
NA
<1.0
<1.0
<0.25
<0.25
<0.25
NA
NA
Pyruvic Acid
<10
NA
<2.0
<2.0
<0.53
1 <0.53
<0.53
1 NA
NA
<10
NA
<2.0
<2.0
1 <0.53
<0.53
<0.53
NA
NA
Notes:
TOC = Total Organic Carbon; DO = Dissolved Oxygen; NA = Not Analyzed
1 = Sulfide and metals samples collected on July 17, 2013.
J = estimated concentration greater than the method detetion limit, but below the reporting limit.
Table 7 (Page 5 of 6)
Re: SRAM -Master PrejectsWC DOT -DOTMTb C-b t\DOT4+ Stetnv!W 66NSWpl 2014 Repot\Tab1es\Tab1n\T7-NaL Aaen. nm(5)
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Table 8
Surface Water Parameters
Former ATL Site No. 2-66
Statesville, North Carolina
H&H Job No. DOT-504
Surface Water Location
SS-1 (u)stream)
SS-2 (downstream
Sampling Date
Dec-12
Feb-13
Apr-13
Jun-13
Oct-13
Jan-14
May-14
Jul-14
Dec-12
Feb-13
Apr-13
Jun-13
Oct-13
Jan-14
May-14
Jul-14
Field Measurements
Dissolved Oxygen (mg/1)
10.83
10.10
9.86
6.45
8.66
9.30
9.00
9.70
10.96
10.40
10.06
6.79
9.50
10.20
9.68
10.00
Ferrous Iron (mg/1)
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
<0.2
Redox (mV)
190
174
168
43
66.6
70.4
98
182
194
163
170
34
69
69
108
277
Conductivity (µS/cm)
136.4
116.6
121.4
33.5
123.6
131.3
120.1
118.1
128.9
115.5
133.9
43.4
130.3
136.1
85.4
135.4
pH (standard units)
7.04
7.00
7.02
6.78
7.18
7.20
7.32
6.98
7.02
6.90
6.96
7.00
7.16
7.18
7.22
6.43
Temperature (°C)
10.6
12.0
13.3
16.4
14.2
13.0
20.4
22.9
10.9
11.1
14.0
16.1
14.2
13.1
22.4
24.0
Notes:
TOC = Total Organic Carbon; DO = Dissolved Oxygen; NA = Not Analyzed
1 = Sulfide and metals samples collected on July 17, 2013.
Table 8 (Page 1 of 1)
R.: S:WM-Master PrqectaWC DOT-DOTIDOT£AOa Cantraei\DOT300 SIeteaW0e fi6�September 2014 Report\Tablea\Tables\TSSurlxe Water Paramclem
Date: X164015 Hart & Hickman, PC

APPROXIMATE TITLE
0 2000 4000 SITE LOCATION MAP
w
P
SCALE IN FEET PROJECT
FORMER ATL SITE #2-66
U.S.G.S. QUADRANGLE MAP STATESVILLE, NORTH CAROLINA
hart hiekman 2923 S. Trvon Street Suite 100
Charlotte, NC 28203
SMARTER ENVIRONMENTA I. SOLUTIONS 704.586.0007(p) 704.586.0373(f)
DATE: 10-06-14 REVISION NO: 0
JOB NO: DOT-504 FIGURE NO: 1
STATESVILLE WEST, NC 1993
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)

QDMW-8
— — ' — TRIBUTARY
�✓ I
DMW-6 TREES I
Q
TREES *DMW-7 DMW-11
DMW-10 I.
DMW-5Q I
DMW-9 MAIN
Q GARAGE I
AGGEGRATE I
STOCK PILES
FORMER ASPHALT DMW-2Q : P-6
TESTING LABORATORIES -S I
:�
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® WSW �j AW-4A
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# HOPPER
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AGGEGRATE
STOCK PILES
TREES ME
LEGEND
SITE PROPERTY BOUNDARY
— — — STREAM
SHALLOW MONITORING WELL
Q DEEP MONITORING WELL
t- MONITORING WELL BEDROCK
® WATER SUPPLY WELL
as ABANDONED WATER SUPPLY
WELL
SURFACE WATER SAMPLE
TEMPORARY MONITORING WELL
• SOIL BORING
APPROXIMATE
0 100 200
SCALE IN FEET
SITE MAP
PROJECT
FORMER ATL SITE #2-66
STATESVILLE, NORTH CAROLINA
' SOUTHERN RAILROAD
hart hickman2923 South Tryon Street -Suite
Charlotte, North Carolina 28203 0
704-586-0007(p) 704-586-0373(i)
SNWtI9l BiYRO1LYlENDLL SOW�IONS License # C-1269 / #C-245 Geolc
DATE: 10-06-14 REVISION NO. 0
JOB NO. DOT-504 FIGURE NO. 2

OUKf p
OwFR ,Sqs NT
FORMER ASPHALT I
TESTING LABORATOR
WSW -1 WSW-2 I /
WSW-4A ;
WSW-
- — - ---- - --
omm
I I WSW-7 i WS 1
iWSW-6 f WSW-8 ;
WSW-5 \ / I WSW-9!*
i
LEGEND
WATER SUPPLY WELL
ABANDONED WATER SUPPLY WELL
---- SITE PROPERTY BOUNDARY
---- OTHER PROPERTY BOUNDARY
—� ESTIMATED GROUND WATER FLOW DIRECTION
NOTES:
1. MAP BASED ON RICHARD CATLIN & ASSOCIATES JUNE
1997 CSA & IREDELL COUNTY GIS DATABASE
2. WATER SUPPLY WELLS ARE KEYED TO TABLE 1
k; WSW-15 f 1
sf- 10 WSWO
11 / / 1
APPROXIMATE
o soo l000
SCALE IN FEET
WATER SUPPLY WELL LOCATION MAP
Pr4a`r FORMER ATL
SITE #2-66
STATESVILLE, NORTH CAROLINA
•
had hickman
2923 South Tryon Street -Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(1)
SMARfFR ENVRONYIENUIL SOLUTIONS
License # C-1269 / #C-245 Geology
DATE: 10-06-14
REVISION NO. 0
JOB NO: DOT-504
FIGURE NO. 3

LEGEND
I — — — — SITE PROPERTY BOUNDARY
STREAM
SHALLOW MONITORING WELL...
Q DEEP MONITORING WELL
\1 + BEDROCK MONITORING WELL
0°MW"8
(60.14) ® WATER SUPPLY WELL
SS-1 ABANDONED WATER SUPPLY
WELL
I _ • . • — ' — TRIBUTARY
/ SS-2 . • � �� A SURFACE WATER SAMPLE
MONITORING WELL SHALLOW
/ 62 I SAPROLITE
I
TEMPORARY MONITORING WELL
TREES
DMW-6 I
(60.72) G SOIL BORING
TREES DMW-7 DMW-11 I
(61.66) I (63.86) SAPROLITE GROUNDWATER
ELEVATION (FT) (JULY 2014)
DMW-10 64— GROUNDWATER
(60.38) 66 I POTENTIOMETRIC CONTOUR (FT)
ESTIMATED FLOW DIRECTION
/ Q I NM NM NOT MEASURED
DMW-5
(NM) DMW-9
I G (NM) MAIN
GARAGE
AGGEGRATE I
STOCK PILES
F MER ASPHALT DMW-2 GP-6
TESTING LABORATORIES (64.17) +
6470 TW-4 2�
SMW-1 tj% I
U TW-3 Llj
GP-5 /�.
6 PARKING
/TGFI-Al GP-3
AGGEGRATE GP 16 L(66.35) WS� WSW-2 ASTs
�
STOCK PILES SMW-3 TVV-6 I
65.34 �TW 1-
(65.34) TW5 QQ
AGGEGRATE
STOCK PILES 64/ DMW 4#
(65.44) O I
66 I
SMW-4
® nonvEl NWAW"I APPROXIMATE
DMW � 0 100 200
(NM) HOPPER \- OFFICE
AGGEGRATE
STOCK PILES i SCALE IN FEET
TREES
""E ESTIMATED SHALLOW GROUNDWATER
POTENTIOMETRIC MAP - JULY 2014
11 I I i7.—_
SOUTHERN RAILROAD
TREES
PROJECT
J FORMER ATL SITE #2-66
STATESVILLE, NORTH CAROLINA
2923 South Tryon Street -Suite 100
hart hickman Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(o
SMAR19i B�VRONMENfAL SOLL1110NS license # C-1269 / #C-245 Geolc
DATE: 10-06-14 REVISION NO. 0
JOB NO. DOT-504 FIGURE NO. 5

DMW-8 DS
10/13
1/14
5/14
7/14
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
I <1
I <1
DMW-10 (DS)
10/13 1/14 5/14 7/14
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
DMW-6 (DS)
10/13
1/14
5/14
7/14
69.9
62.5
64.9
43.2
5.0
3.6
3.1
1.9
97.7
73.2
67.7
52.0
71.1
50.9
57.2
40.6
4_3
3_5
1.9
9.5
TREES
DMW-1l
DMW-5�
AGGEGRATE
STOCK PILES
SMW-1
SS
8/11
4/13
10/13
5/14
<1
<1
<1
I <1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
I <1
<1
<1
DMW-1 (DS)
10/13
1/14
5/14
7/14
1.9
3
1.6
2.1
<1
<1
<1
<1
1.3
<1
<1
1.3
3.7
4.5
2.9
4.2
2.8
1 3.3
1 2
3.5
77, I I I I -- _
DMW-11 (DS)
10/13
1/14
5/14
7/14
6.3
1 8.1
6.3
7.9
<1
<1
<1
<1
9.0
9.5
7.5
11.0
6.6
6.8
5.4
8.6
<1.0
<1.0
<1.0
<1A
SOUTHERN RAILROAD
� I
<1
I � I
<1
I -� I
<1
I \ I
<1
3.7
4.0
1 4.3
2.1
1.4
<1
I <1
<1
I
I
I
I
I
.ES I
I
714 I
.1 I:1
.1 I
.1
.1 I
I
I
I
I
I
I
PARKING I
I
I
I
I
I
I
WSW-4�/�WSW 4A
(ACTIVE) 00(INACTIVE)
)FFICE I
-I
1
I
TREES I
LEGEND
SITE PROPERTY BOUNDARY
- - - STREAM
SHALLOW MONITORING WELL
Q DEEP MONITORING WELL
T MONITORING WELL BEDROCK
® WATER SUPPLY WELL
ABANDONED WATER SUPPLY
WELL
SURFACE WATER SAMPLE
TEMPORARY MONITORING WELL
_ ESTIMATED GROUND WATER
FLOW DIRECTION
3 TCEISOCONCENTRATION
CONTOUR (pg/I)
7/14 = DATE
<1=TRICHLOROETHENE (Ng/1)
<1=1,1,1-TRICHLOROETHANE (pg/1)
<1 =1,1-DICHLOROETHENE (Ng/1)
3.7 =1,1-DICHLOROETHANE (1.1g/1)
1.4 I =CIS-1,2-DICHLOROETHENE (Ng/1)
APPROXIMATE
0 100 200
SCALE IN FEET
I"` TARGET VOC CONCENTRATIONS IN
SAPROLITE GROUNDWATER
-Ralrcr
FORMER ATL SITE #2-66
STATESVILLE, NORTH CAROLINA
: 2923 South Tryon Street -Suite 100
hart hickman Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(i)
SNW{ItE� @l11RONMEIldL SOWipNS License # C-1269 / #C-245 Geol(
DATE: 10-06-14 REVISION NO. 0
JOB NO. DOT-504 FIGURE NO. 6

QDMW-8
TRIBUTARY
/ ASS-2—
DMW-7 (SBR)
10/13
1/14
5/14
7/1.4
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
/
DMW-6
DMW-11
i<
• U
2
/
/
/
TREES
SOUTHERN RAILROAD
LEGEND
SITE PROPERTY BOUNDARY
STREAM
SHALLOW MONITORING WELL
Q DEEP MONITORING WELL
T MONITORING WELL BEDROCK
® WATER SUPPLY WELL
�`--� ABANDONED WATER SUPPLY
WELL
I
SURFACE WATER SAMPLE
I A- TEMPORARY MONITORING WELL
I
I0
SOIL BORING
TREES I
I
I
I
I
7/14
= DATE
<1
=TRICHLOROETHENE (pg/1)
MAIN
<1
=1,1,1-TRICHLOROETHANE (pg/1)
GARAGE I
WSW-4A
2/09
<1
<1
=1,1-DICHLOROETHENE (Ng/1)
=1,1-DICHLOROETHANE (pg/1)
<1
=CIS-1,2-DICHLOROETHENE (lug/1)
DMW-3 SBR
8/11
4/13
10/13
5/14
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
WSW-4
/11
4/13
10/13
5/14
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1
<1 I
<1
<1 I<1
<1
I
I
I
I
I ti
I
WSW-4 WAW-4A
Inceve> (INACTIVE) APPROXIMATE
0 100 200
OFFICE
I SCALE IN FEET
TARGET VOC CONCENTRATIONS
IN BEDROCK GROUNDWATER
PROJECT
TREES I FORMER ATL SITE #2-66
STATESVILLE, NORTH CAROLINA
• 2923 South Tryon Street -Suite 100
hart hiekman Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(t
SMARM @AIRONMOiTAL SOWIIONS Incense # C-1269 / #C-245 Geok
DATE: 10-06-14 REVISION NO. 0
JOB NO DOT-504
FIGURE NO. 7

Appendix A
Laboratory Analytical Data
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

aceAnalytical
www.pacelabs.com
November 06, 2013
Chemical Testing Engineer
NCDOT
Materials & Tests Unit
1801 Blue Ridge Road
Raleigh, NC 27607
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
RE: Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Dear Chemical Engineer:
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on October 24, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
4 Q'
REPORT OF LABORATORY ANALYSIS
k
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc..
a00 -
[phone]
Page 1 of 45

_ lacieAnalytical
/ wwwpacelabs.com
November 06, 2013
Page 2
cc: JeffAlbano, Hart & Hickman
l pCt:'q_
ft
.i
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 45

�wmvpacelabs.comeAnalyiical
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
DOT 404 34613.3.26
92177010
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92177010001
DMW-6
RSK 175
DL1
3
PASI-M
EPA6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
92177010002
DMW-7
RSK 175
DL1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310E
SAE
1
PASI-A
92177010003
DMW-10
RSK 175
DL1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S21)
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310E
SAE
1
PASI-A
92177010004
DMW-9
RSK 175
DL1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S213
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
92177010005
DMW-11
RSK 175
DL1
3
PASI-M
EPA 6010
JMW
7
PASI-A
_
EPA 7470
MTS
1
PASI-A
SM 6200E
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 45

� I
,��acceAnalyfical
www.pacelabs.com
I
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
A2LA Certification #: 2926.01
Alaska Certification #: UST-078
Alaska Certification #MN00064
Arizona Certification #: AZ-0014
Arkansas Certification #: 88-0680
California Certification #: 01155CA
Colorado Certification #Pace
Connecticut Certification M PH-0256
EPA Region 8 Certification #: Pace
Florida/NELAP Certification #: E87605
Georgia Certification #: 959
Hawaii Certification #Pace
Idaho Certification #: MN00064
Illinois Certification #: 200011
Kansas Certification #: E-10167
Louisiana Certification #: 03086
Louisiana Certification #: LA080009
Maine Certification #: 2007029
Maryland Certification M 322
Michigan DEQ Certification At: 9909
Minnesota Certification #: 027-053-137
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #:12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Mississippi Certification #: Pace
Montana Certification #: MT CERT0092
Nebraska Certification #: Pace
Nevada Certification #: MN00064
New Jersey Certification #: MN-002
New York Certification #: 11647
North Carolina Certification #: 530
North Dakota Certification#: R-036
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Certification #: MN200001
Oregon Certification #: MN300001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification
Tennessee Certification #: 02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Virginia/DCLS Certification #: 002521
VirginiaNELAP Certification M 460163
Washington Certification #: C754
West Virginia Certification #: 382
Wisconsin Certification #: 999407970
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiafVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 45

,�aceAnalytical
'.pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
92177010006
DMW-8
RSK 175
DI-1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
NITS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
92177010007
DMW-2
RSK 175
DI-1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
NITS
1
PASI-A
SM 62008
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
92177010008
DMW-1
RSK 175
DI-1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
92177010009
CREEK
SM 6200B
CAH
33
PASI-C
92177010010
WSW-4
SM 6200E
CAH
33
PASI-C
92177010011
SMW-2
SM 6200E
CAH
33
PASI-C
92177010012
SMW-1
SM 6200E
CAH
33
PASI-C
92177010013
DMW-3
SM 6200B
CAH
33
PASI-C
92177010014
SMW-3
SM 6200E
CAH
33
PASI-C
92177010016
TRIP
SM 6200B
CAH
33
PASI-C
92177010016
DMW-4
SM 6200B
CAH
33
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 45

axAnalytical
wwwpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road -Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-6
Lab ID: 92177010001 Collected:
10/23/13
09:40 Received: 10/24/13 12:57 Matrix: Water
Parameters
Results Units
Report Limit
DF Prepared
Analyzed CAS No. Qual
RSK 176 AIR Headspace
Analytical Method: RSK 175
Ethane
7.0 ug/L
6.2
1
10/29/1318:03 74-84-0
Ethene
ND ug/L
6.2
1
10129/1318:03 74-85-1
Methane
93.8 ug/L
6.6
1
10/29/13 18:03 74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1 10/2511310:25
1012811319:57 7440-38-2
Barium
111 ug/L
5.0
1 10/25/1310:25
10/2811319:57 7440-39-3
Cadmium
ND ug/L
1.0
1 10/25/1310:25
10/28/1319:57 7440-43-9
Chromium
NO ug/L
5.0
1 10/25/1310:25
10/28/13 19:57 7440-47-3
Lead
ND ug/L
5.0
1 10/25/1310:25
10/2911314:14 7439-92-1
Selenium
ND ug/L
10.0
1 10/2511310:25
10/28/1319:57 7782-49-2
Silver
ND ug/L
5.0
1 10/25/1310:25
10/2811319:57 7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1 10/25/13 20:15
10/28/13 22:19 7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
71.1 ug/L
1.0
1
10/26/13 08:04 75-34-3
1,1-Dichloroethene
97.7 ug/L
1.0
1
10/26/13 08:04 75-35-4
1,1,1-Trichloroethane
5.0 ug/L
1.0
1
10/26/13 08:04 71-55-6
1,1,2-Trichloroethane
NO ug/L
1.0
1
10/26/13 08:04 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 08:04 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 08:04 95-50-1
1,2-Dichloroethane
1.1 ug/L
1.0
1
10/26/13 08:04 107-06-2
1,2-Dichloropropane
NO ug/L
1.0
1
10/26/13 08:04 78-87-5
1,3-Dichlorobenzene
NO ug/L
1.0
1
10/26/13 08:04 541-73-1
1,4-Dichlorobenzene
NO ug/L
1.0
1
10/26/13 08:04 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 08:04 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 08:04 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 08:04 75-25-2
cis-1,2-Dichloroethene
4.3 ug/L
1.0
1
10/26/13 08:04 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 08:04 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 08:04 56-23-5
Chlorobenzene
NO ug/L
1.0
1
10/26/13 08:04 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 08:04 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 08:04 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 08:04 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 08:04 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 08:04 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 08:04 75-09-2
trans-1,2-Dichloroethene
NO ug/L
1.0
1
10/26/13 08:04 156-60-5
trans-1,3-Dichloropropene
NO ug/L
1.0
1
10/26/13 08:04 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 08:04 127-18-4
Trichloroethene
69.9 ug/L
1.0
1
10/26/13 08:04 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 08:04 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 08:04 75-01-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM
without the written consent of Pace Analytical Services, Inc..
Page 6 of 45

�aceAnalydcal
rwa¢pacefabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-6
Lab ID: 92177010001 Collected:
10/23113 09:40
Received: 10/24/13 12:57 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 08:04
106-93-4
Surrogates
4-Bromof)uorobenzene (S)
94 %
70-130
1
10/26/13 08:04
460-00-4
1,2-Dichloroethane-d4 (S)
105 %
70-130
1
10/26/13 08:04
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
10/26/13 08:04
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
10/29/1315:42
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
54.3 mg/L
4.0
2
10/3011311:22
14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.86 mg/L
0.020
1
10/25/13 03:48
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
46.0 mg/L
1.0
1
10/30/13 18:11
7440-44-0
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 45

,�aceAnalydcal
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-7 Lab ID: 92177010002 Collected: 10/23/13 10:20 Received: 10/24/13 12:57 Matrix: Water
Parameters Results Units Report Limit . DF Prepared Analyzed CAS No. Qua!
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
10/29/1318:35
74-84-0
Ethene
ND ug/L
6.2
1
10/29/13 18:35
74-85-1
Methane
ND ug/L
6.6
1
10/29/1318:35
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method:
EPA 3010
Arsenic
ND ug/L
10.0
1 10/25/13 10:25
10/28/13 20:00
7440-38-2
Barium
28.2 ug/L
5.0
1 10/25/13 10:25
10/28/13 20:00
7440-39-3
Cadmium
NO ug/L
1.0
1 10/25/13 10:25
10/28/13 20:00
7440-43-9
Chromium
NO ug/L
5.0
1 10/25/13 10:25
10/28/13 20:00
7440-47-3
Lead
NO ug/L
5.0
1 10/2511310:25
10/2911314:17
7439-92-1
Selenium
NO ug/L
10.0
1 10/2511310:25
10/28/13 20:00
7782-49-2
Silver
NO ug/L
5.0
1 10/25/13 10:25
10/28/13 20:00
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1 10/25/13 20:15
10/28/13 22:22
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
10/26/13 03:41
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 03:41
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 03:41
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 03:41
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 03:41
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 03:41
95-50-1
1,2-Dichloroethane
NO ug/L
1.0
1
10/26/13 03:41
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 03:41
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 03:41
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 03:41
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 03:41
75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 03:41
74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 03:41
75-25-2
cis-1,2-Dichloroethene
NO ug/L
1.0
1
10/26/13 03:41
166-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/2611303:41
10061-01-5
Carbon tetrachloride
NO ug/L
1.0
1
10/26/13 03:41
56-23-5
Chlorobenzene
NO ug/L
1.0
1
10/26/13 03:41
108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 03:41
75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 03:41
67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 03:41
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 03:41
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 03:41
75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 03:41
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 03:41
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 03:41
10061-02-6
Tetra chloroethene
ND ug/L
1.0
1
10/26/13 03:41
127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 03:41
79-01-6 -
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 03:41
75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 03:41
75-01-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 11/06/2013 04:59 PM
without the written consent of Pace Analytical Services, Inc..
Page 8 of 45 _ "

aceAnalytical
www.pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-7
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (EDB)
- Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
5310E TOC
Total Organic Carbon
�I
-' Date: 11/06/2013 04:59 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 92177010002 Collected: 10/23/13 10:20
Results Units Report Limit DF
Received: 10/24/13 12:57 Matrix: Water
Prepared Analyzed CAS No. Qual
Analytical Method: SM 6200B
ND ug/L
1.0
1
10/26/13 03:41
106-93-4
95 %
70-130
1
10/26/13 03:41
460-00-4
102 %
70-130
1
10/26/13 03:41
17060-07-0
100 %
70-130
1
10/26/13 03:41
2037-26-5
Analytical Method: SM 4500-S2D
NO mg/L
0.10
1
10129/1315:42
18496-25-8
Analytical Method: EPA 300.0
10.9 mg/L
2.0
1
10/30/13 04:09
14808-79-8
Analytical Method: EPA 353.2
0.032 mg/L
0.020
1
10/25/13 03:57
Analytical Method: SM 6310B
6.7 mg/L
1.0
1
10/3011318:22
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 9 of 45

AceAnalXical
vvmv pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-10
Parameters
Lab ID: 92177010003 Collected: 10/23/13 11:00
Results Units Report Limit DF
Received: 10/24/13 12:57 Matrix: Water
Prepared Analyzed CAS No.
RSK 175 AIR Headspace
Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
10/29/13 18:46 74-84-0
Ethane
ND ug/L
6.2
1
10/2911318:46 74-85-1
Methane
701 ug/L
6.6
1
10129/1318:46 74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:12 7440-38-2
Barium
136 ug/L
5.0
1
10/25/13 10:25
10/28/13 20:12 7440-39-3
Cadmium
ND ug/L
1.0
1
10/25/1310`:25
10/28/13 20:12 7440A3-9
Chromium
ND ug/L
5.0
1
10/25/1310:25
10/28/13 20:12 7440-47-3
Lead
ND ug/L
5.0
1
10/25/1310:25
10/29/13 14:30 7439-92-1
Selenium
ND ug/L
10.0
1
10/25/1310:25
10/28/13 20:12 7782-49-2
Silver
ND ug/L
5.0
1
10/25/13 10:25
10/28/13 20:12 7440-22A
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.26
1
10/25/13 20:16
10/28/13 22:30 7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
10/26/13 03:57 75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 03:57 75-35A
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 03:57 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 03:57 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 03:57 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 03:57 95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 03:57 107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26113 03:57 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 03:57 541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 03:57 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 03:57 75-27-4
Bromometliane
ND ug/L
5.0
1
10/26/13 03:57 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 03:57 75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 03:57 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 03:57 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 03:57 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 03:57 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 03:57 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 03:57 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 03:57 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 03:57 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 03:57 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 03:57 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 03:57 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 03:57 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 03:57 127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 03:57 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 03:57 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 03:57 75-014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc..
Qua]
Page 10 of 45

aceAnalXical
wrwpacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-10
Parameters
Lab ID: 92177010003 Collected: 10/23113 11:00
Results Units Report Limit DF
Received: 10/24/13 12:57 Matrix: Water
Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 03:57 106-93-4
Surrogates
4-Bromofluorobenzene (S)
95 %
70-130
1
10/26/13 03:57 460-00-4
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
10/26/13 03:57 17060-07-0
Toluene-d8 (S)
100 %
70-130
1
10/26/13 03:57 2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S21)
Sulfide
ND mg/L
0.10
1
10/29/13 15:42 18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
35.3 mg/L
2.0
1
10/30/13 04:50 14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.12 mg/L
0.020
1
10/25/13 03:59
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
18.3 mg/L
1.0
1
10/30/13 18:36 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 45

P aceAnalytical
wwwpacerabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
I
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-9 Lab ID: 92177010004 Collected: 10/23/13 11:40 Received: 10/24/13 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
10/2911318:57 74-84-0
Ethene
ND ug/L
6.2
1
10/29/1318:57 74-85-1
Methane
40.6 ug/L
6.6
1
10/29/1318:57 74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:15 7440-38-2
Barium
86.2 ug/L
5.0
1
10/25f13 10:25
10/28113 20:15 7440-39-3
Cadmium
NO ug/L
1.0
1
10/25/13 10:25
10/28/13 20:15 7440A3-9
Chromium
ND ug/L
5.0
1
10/25/13 10:25
10/28/13 20:15 7440-47-3
Lead
ND ug/L
5.0
1
10/25/13 10:25
10/29/13 14:34 7439-92-1
Selenium
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:15 7782-49-2
Silver
ND ug/L
5.0
1
10/25/13 10:25
10/28/13 20:15 7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation
Method:
EPA 7470
Mercury
ND ug/L
0.20
1'
10/25113 20:15
10/28/13 22:33 7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
4.9 ug/L
1.0
1
10/26/13 04:14 75-34-3
1,1-Dichloroethene
3.4 ug/L
1.0
1
10/26/13 04:14 75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 04:14 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10126/1304:14 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 04:14 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 04:14 95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/2611304:14 107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/2611304:14 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 04:14 541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/2611304:14 106-46-7
Bromodichloro methane
ND ug/L
1.0
1
10/26/13 04:14 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26113 04:14 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 04:14 75-25-2
cis-1,2-Dichloroethene
1.2 ug/L
1.0
1
10/26/13 04:14 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26113 04:14 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 04:14 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 04:14 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 04:14 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 04:14 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26113 04:14 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 04:14 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 04:14 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 04:14 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 04:14 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 04:14 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 04:14 127-18-4
Trichloroethene
4.9 ug/L
1.0
1
10/26/13 04:14 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 04:14 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 04:14 75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 45

�aceAnalXicalo
www.pacelabs.mm
i
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-9
Lab ID: 92177010004 Collected:
10/23/13 11:40
Received: 10/24/13 12:57 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 04:14 106-93-4
Surrogates
4-Bromofluorobenzene (S)
95 %
70-130
1
10/26/13 04:14 460-00-4
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
10/26/13 04:14 17060-07-0
Toluene-d8 (S)
100 %
70-130
1
10/26/13 04:14 2037-26-5
4500S21D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.50
5
10/2911315:42 18496-25-8 D3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
65.8 mg/L
4.0
2
10/30/1311:36 14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
1.5 mg/L
0.020
1
10/25/13 04:00
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
5.6 mg/L
1.0
1
10/30/13 18:50 7440-44-0
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 45

,�ac'eAnalyticalo
www.pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100 -'
Huntersville, NC 28078
I
[phone]
Sample: DMW-11 Lab ID: 92177010006 Collected: 10/23/13 12:20 Received: 10124/13 12:67 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
10/2911319:07 74-84-0
Ethene
ND ug/L
6.2
1
10/29/1319:07 74-85-1
Methane
663 ug/L
6.6
1
10/29/1319:07 74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:19 7440-38-2
Barium
69.8 ug/L
5.0
1
10/25/13 10:25
10/28/13 20:19 7440-39-3
Cadmium
ND ug/L
1.0
1
10125/13 10:25
10/28/13 20:19 7440-43-9
Chromium
ND ug/L
5.0
1
10/25/13 10:25
10/28/13 20:19 7440-47-3
Lead
ND ug/L
5.0
1
10/25/13 10:25
10/29/1314:37 7439-92-1
Selenium
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:19 7782-49-2
Silver
ND ug/L
5.0
1
10/2511310:25
10/28/13 20:19 7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
10/25/13 20:15
10/28/13 22:35 7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 62008
1,1-Dichloroethane
6.6 ug/L
1.0
1
10/26/13 04:30 75-34-3
1,1-Dichloroethene
9.0 ug/L
1.0
1
10/26/13 04:30 75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 04:30 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 04:30 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 04:30 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 04:30 95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 04:30 107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 04:30 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 04:30 641-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 04:30 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 04:30 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 04:30 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 04:30 75-25-2
cis- 1.2-Dichloroethene
ND ug/L
1.0
1
10/26/13 04:30 156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 04:30 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 04:30 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 04:30 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 04:30 75-00-3
Chloroform
NO ug/L
1.0
1
10/26/13 04:30 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 04:30 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 04:30 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 04:30 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 04:30 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 04:30 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 04:30 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 04:30 127-18-4
Trichloroethene
6.3 ug/L
1.0
1
10/26/13 04:30 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 04:30 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 04:30 75-01-4
REPORT OF LABORATORY ANALYSIS --
1
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 45

I
(�aneAnalytical
wvmpace/abs.com
i
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-11
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, N021NO3 unpres
Nitrogen, Nitrate
5310E TOC
Total Organic Carbon
Date: 11/06/2013 04:59 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 92177010005 Collected: 10/23/13 12:20
Results Units Report Limit DF
Received: 10/24113 12:57 Matrix: Water
Prepared Analyzed CAS No. Qual
Analytical Method: SM 6200B
ND ug/L
1.0
1
10/26/13 04:30 106-93-4
95 %
70-130
1
10/26/13 04:30 460-00-4
103 %
70-130
1
10/26/13 04:30 17060-07-0
99 %
70-130
1
10/26/13 04:30 2037-26-5
Analytical Method: SM 4500-S2D
ND mg/L
0.50
5
10/29/1315:42 18496-25-8 D3
Analytical Method: EPA 300.0
75.3 mg/L
10.0
5
10/30/1311:49 14808-79-8
Analytical Method: EPA 353.2
ND mg/L
0.020
1
10/25/13 04:04
Analytical Method: SM 5310B
18.4 mg/L
1.0
1
10/30/13 19:03 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 45

��aceAnalytical
wwwpacelabsxom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-8 Lab ID: 92177010006 Collected: 10123/13 13:15 Received: 10/24/13 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
10/2911319:18 74-84-0
Ethene
ND ug/L
6.2
1
10/29/1319:18 74-85-1
Methane
8.3 ug/L
6.6
1
10/29/13 19:18 74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:22 7440-38-2
Barium
35.9 ug/L
5.0
1
10/25/13 10:25
10/28/13 20:22 7440-39-3
Cadmium
ND ug/L
1.0
1
10/25/13 10:25
10/28/13 20:22 7440-43-9
Chromium
ND ug/L
5.0
1
10/25/13 10:25
10/28/13 20:22 7440-47-3
Lead
ND ug/L
5.0
1
10/25/13 10:25
10/2911314:40 7439-92-1
Selenium
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:22 7782-49-2
Silver
ND ug/L
6.0
1
10/25/13 10:25
10/28/13 20:22 7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
10/25/13 20:15
10/28/13 22:38 7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
10/26/13 04:47 75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 04:47 75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 04:47 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 04:47 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 04:47 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 04:47 95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 04:47 107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 04:47 78.87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 04:47 541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/2611304:47 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 04:47 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26113 04:47 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 04:47 75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 04:47 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 04:47 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 04:47 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 04:47 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 04:47 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 04:47 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 04:47 74-87-3
Dibromochlorom ethane
ND ug/L
1.0
1
10/26/13 04:47 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 04:47 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 04:47 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 04:47 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 04:47 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 04:47 127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 04:47 79-01-6
Trichlorofluoromethane
NO ug/L
1.0
1
10/26/13 04:47 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 04:47 75-01-4
REPORT OF LABORATORY ANALYSIS
i
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 45

r
�aceAnalytical"
' 1mv.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-8
Lab ID: 92177010006 Collected:
10/23113 13:15
Received: 10/24/13 12:57 Matrix: Water
Parameters
Results Units Report
Limit
DF
Prepared Analyzed CAS No.
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 04:47 106-93-4
- Surrogates
4-Bromofluorobenzene (S)
94 %
70-130
1
10/26/13 04:47 460-00-4
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
10/26/13 04:47 17060-07-0
Toluene-d8 (S)
100 %
70-130
1
10/26/13 04:47 2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
10/2911315:42 18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
2.3 mg/L
2.0
1
10/30/13 05:30 14808-79-8
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA353.2
Nitrogen, Nitrate
0.72 mg/L
0.020
1
10/25/13 04:05
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
2.5 mg/L
1.0
1
10/30/13 19:58 7440-44-0
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 17 of 45

_ aOAnalytical
-pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-2
Parameters
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 92177010007 Collected: 10/24/13 07:15 Received: 10/24/13 12:57 Matrix: Water
Results . Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
10129/1319:29 74-84-0
Ethene
ND ug/L
6.2
1
10/29/1319:29 74-85-1
Methane
62.8 ug/L
6.6
1
10/29/1319:29 74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:25 7440-38-2
Barium
28.3 ug/L
5.0
1
10/25/13 10:25
10/28/13 20:25 7440-39-3
Cadmium
ND ug/L
1.0
1
10/25/13 10:25
10/28/13 20:25 7440-43-9
Chromium
ND ug/L
5.0
1
10/25/13 10:25
10/28/13 20:25 7440-47-3
Lead
ND ug/L
6.0
1
10/2511310:25
10/29/1314:43 7439-92-1
Selenium
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:25 7782-49-2
Silver
ND ug/L
5.0
1
10/25/13 10:25
10/28/13 20:25 7440-224
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
0.22 ug/L
0.20
1
10/25/13 20:15
10/28/13 22:41 7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
1.9 ug/L
1.0
1
10126/13 05:03 75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 05:03 75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 05:03 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 05:03 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 05:03 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 05:03 95-50-1
1,2-Dichloroethane
NO ug/L
1.0
1
10/26/13 05:03 107-06-2
1,2-Dichloropropane
NO ug/L
1.0
1
10/26/13 05:03 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 05:03 541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 05:03 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 05:03 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 05:03 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 05:03 75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 05:03 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 05:03 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 05:03 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 05:03 108-90-7
Chloroethane
NO ug/L
1.0
1
10/26/13 05:03 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 05:03 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 05:03 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 05:03 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 05:03 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 05:03 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 05:03 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 05:03 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 05:03 127-18-4
Trchloroethene
ND ug/L
1.0
1
10/26/13 05:03 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 05:03 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 05:03 75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, f
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 45 n

�aceAnalydcal
wwwpacelab.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-2
Lab ID: 92177010007 Collected:
10/24/13 07:15
Received: 10/24/13 12:57 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qua]
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 05:03 106-93-4
Surrogates
4-Bromofluorobenzene (S)
95 %
70-130
1
10/26/13 05:03 460-00-4
1,2-Dichloroethane-d4 (S)
104 %
70-130
1
10/26/13 05:03 17060-07-0
Toluene-d8 (S)
100 %
70-130
1
10/26/13 05:03 2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
10/29/1315:42 18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA300.0
Sulfate
72.7 mg/L
10.0
5
10/30/13 12:03 14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
3.5 mg/L
0.020
1
10/25/13 04:13
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
5.8 mg/L
1.0
1
10/30/13 20:08 7440-44-0
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 45

,�aceAnalyfical
wmv.pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-1
Parameters
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 92177010008 Collected: 10/24/13 09:00 Received: 10124/13 12:57 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
NO ug1L
6.2
1
10/29/13 19:39 74-84-0
Ethene
ND ug/L
6.2
1
10/2911319:39 74-85-1
Methane
9.3 ug/L
6.6
1
10/29/13 19:39 74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:28 7440-38-2
Barium
56.8 ug/L
5.0
1
10/25/13 10:25
10/28/13 20:28 7440-39-3
Cadmium
ND ug/L
1.0
1
10/25/13 10:25
10/28/13 20:28 7440-43-9
Chromium
ND ug/L
5.0
1
10/26/13 10:25
10/28/13 20:28 7440-47-3
Lead
ND ug/L
5.0
1
10/25/13 10:25
10/29/13 14:47 7439-92-1
Selenium
ND ug/L
10.0
1
10/25/13 10:25
10/28/13 20:28 7782-49-2
Silver
ND ug/L
5.0
1
10/25/13 10:25
10/28/13 20:28 7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
10/25/13 20:15
10/28/13 22:43 7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
3.7 ug/L
1.0
1
10/26113 05:20 75-34-3
1,1-Dichloroethene
1.3 ug/L
1.0
1
10/2611305:20 75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 05:20 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 05:20 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 05:20 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 05:20 95-50-1
1,2-Dichloroethane
NO ug/L
1.0
1
10/2611305:20 107-06-2
1,2-Dichloropropane
NO ug/L
1.0
1
10/26/13 05:20 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/2611305:20 541-73-1
1,4-Dichlorobenzene
NO ug/L
1.0
1
10/26/13 05:20 106-46-7
Bromodichloromethane
NO ug/L
1.0
1
10/26/13 05:20 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 05:20 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 05:20 75-25-2
cis-1,2-Dichloroethene
2.8 ug/L
1.0
1
10126/1305:20 156-59-2
cis- 1,3-Dichloropropene
NO ug/L
1.0
1
10/26/13 05:20 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 05:20 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 05:20 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 05:20 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 05:20 67-66-3
Chloromethane
NO ug/L
1.0
1
10/26/13 05:20 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 05:20 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 05:20 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 05:20 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/2611305:20 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 05:20 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 05:20 127-18-4
Trichloroethene
1.9 ug/L
1.0
1
10/26/13 05:20 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 05:20 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 05:20 75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc..
Page 20 of 45

�aceAnalydcal
www.pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-1
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (ED13)
- Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, N021NO3 unpres
Nitrogen, Nitrate
5310E TOC
Total Organic Carbon
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 92177010003 Collected:
Analytical
Analytical
Analytical
Analytical
Analytical
10/24/13 09:00
Received: 10/24/13 12:57 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
Method: SM 6200B
ND ug/L
1.0
1
10/26/13 05:20
106-93-4
97 %
70-130
1
10/26/13 05:20
460-00-4
104 %
70-130
1
10/26/13 05:20
17060-07-0
103 %
70-130
1
10/26/13 05:20
2037-26-5
Method: SM 4500-S2D
ND mg/L
0.10
1
10/29/13 15:42
18496-26-8
Method: EPA 300.0
4.2 mg/L
2.0
1
10/30/13 05:58
14808-79-8
Method: EPA 353.2
0.11 mg/L
0.020
1
10/25/13 04:14
Method: SM 5310B
4.5 mg/L
1.0
1
10/30/13 20:19
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc..
Qual
Page 21 of 45

��aceAnalytical
www.pacelabs.com
Project: . DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - SuileA
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Sample: CREEK
Parameters
Lab ID: 92177010009 Collected: 10/23/13 13:40
. Results Units Report Limit DF
Received: 10124/13 12:57 Matrix: Water
Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
10/26/13 05:36 75-34-3
1,1-Dichloroethene
NO ug/L
1.0
1
10/26/13 05:36 75-35-4
1,1,1-Trichloroethane
NO ug/L
1.0
1
10/26/13 05:36 71-55-6
1,1,2-Trichloroethane
NO ug/L
1.0
1
10/26/13 05:36 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 05:36 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 05:36 95-50-1
1,2-Dichloroethane
NO ug/L
1.0
1
10/26/13 05:36 107-06-2
1,2-Dichloropropane
NO ug/L
1.0
1
10/26/13 05:36 78-87-5
1,3-Dichlorobenzene
NO ug/L
1.0
1
10/26/13 05:36 541-73-1
1,4-Dichlorobenzene
NO ug/L
1.0
1
10/26/13 05:36 106-46-7
Bromodichloromethane
NO ug/L
1.0
1
10/26/13 05:36 75-27-4
Bromomethane
NO ug/L
5.0
1
10/26/13 05:36 74-83-9
Bromoform
ND ug/L
1-0
1
10/26/13 05:36 75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 05:36 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 05:36 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 05:36 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 05:36 108-90-7
Chloroethane
ND ug/L
1.0
1
1.0/26/13 05:36 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 05:36 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 05:36 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 05:36 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 05:36 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 05:36 75-09-2
trans-1,2-Dichloroethene
NO ug/L
1.0
1
10/26/13 05:36 156-60-5
trans-1,3-Dichloropropene
NO ug/L
1.0
1
10/26/13 05:36 10061-02-6
Tetrachloroethene
NO ug/L
1.0
1
10/26/13 05:36 127-18-4
Trichloroethene
NO ug/L
1.0
1
10/26/13 05:36 79-01-6
Trichlorofluoromelhane
ND ug/L
1.0
1
10/26/13 05:36 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 05:36 75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 05:36 106-93-4
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
1
10/26/13 05:36 460-00-4
1,2-Dichloroethane-d4 (S)
105 %
70-130
1
10/26/13 05:36 17060-07-0
Toluene-d8 (S)
99 %
70-130
1
10/26/13 05:36 2037-26-5
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 22 of 45

'an
eAnalytical
www.pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WSW-4
Parameters
Lab ID: 92177010010 Collected: 10/23/13 14:00
Results Units Report Limit DF
Received: 10/24/13 12:57 Matrix: Water
Prepared Analyzed CAS No_ Qua]
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
NO ug/L
1.0
1
10/26/13 05:52 75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 05:52 75-354
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 05:52 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 05:52 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 05:52 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 05:52 95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 05:52 107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 05:52 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 05:52 541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 05:52 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 05:52 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 05:52 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 05:52 75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 05:52 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 05:52 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 05:52 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26113 05:52 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 05:52 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 05:52 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 05:52 74-87-3
Dibromochloromelhane
ND ug/L
1.0
1
10/26/13 05:52 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 05:52 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 05:52 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 05:52 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 05:52 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 05:52 127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 05:52 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 05:52 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 05:52 75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 05:52 166-93-4
Surrogates
4-Bromofluorobenzene (S)
95 %
70-130
1
10/26/13 05:52 460-00-4
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
10/26/13 05:52 17060-07-0
Toluene-d8 (S)
100 %
70-130
1
10/26/13 05:52 2037-26-5
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 23 of 45

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: SMW-2 Lab ID: 92177010011 Collected: 10/24/13 07:45 Received: 10/24/13 12:57 Matrix: Water
Parameters Results Units Report,Limit DF Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200 Analytical Method: SM 6200B
1,1-Dichloroethane
2.0 ug/L
1.0
1
10/2611306:09 75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:09 75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 06:09 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 06:09 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/2611306:09 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:09 95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 06:09 107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 06:09 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:09 541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:09 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 06:09 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 06:09 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 06:09 75-25-2
cis-1,2-Dichloroethene
NO ug/L
1.0
1
10/26/13 06:09 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 06:09 10061-01-5
Carbon tetrachloride
NO ug/L
1.0
1
10/26/13 06:09 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 06:09 108-90-7
Chloroethane
NO ug/L
1.0
1
10/26/13 06:09 75-00-3
Chloroform
NO ug/L
1.0
1
10/26/13 06:09 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 06:09 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 06:09 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 06:09 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 06:09 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:09 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 06:09 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 06:09 127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 06:09 79-01-6
Tdchlorofluoromethane
ND ug/L
1.0
1
10/26/13 06:09 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 06:09 75-01-4
1,2-Dibromoethane (EDB)
NO ug/L
1.0
1
10/26/13 06:09 106-93-4
Surrogates
4-Bromofluorobenzene(S)
95 %
70-130
1
10/26/13 06:09 460-00-4
1,2-Dichloroethane-d4 (S)
104 %
70-130
1
10/26/13 06:09 17060-07-0
Toluene-d8 (S)
100 %
70-130
1
10/26/13 06:09 2037-26-5
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 24 of 45

--1
aceAnal ical0
rwmvpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: SMW-1
Lab ID: 92177010012 Collected: 10/24113 08:20
Received: 10/24/13 12:57 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qua]
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
10/26/13 06:25
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:25
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10/26/13 06:25
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 06:25
79-00-5
1,1,2,2-Tetrach]oroethane
ND ug/L
1.0
1
10/2611306:25
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:25
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/2611306:25
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 06:25
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:25
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:25
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 06:25
75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 06:25
74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 06:25
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:25
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 06:25
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 06:25
56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 06:25
108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 06:25
75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 06:25
67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 06:25
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 06:25
124-48-1
Dichlorodifluoro methane
ND ug/L
1.0
1
10/26/13 06:25
75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 06:25
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:25
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 06:25
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 06:25
127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 06:25
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 06:25
75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 06:25
75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 06:25
106-93-4
Surrogates
4-Bromofluorobenzene (S)
93 %
70-130
1
10/26/13 06:25
460-00-4
1,2-Dichloroethane-d4 (S)
106 %
70-130
1
10/26/13 06:25
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
10/26/13 06:25
2037-26-5
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 25 of 45

,�aceAnalydcal
wrnvpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 2a078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-3 Lab ID: 92177010013 Collected: 10124/13 10:50 Received: 10124113 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200 Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
10/26/13 06:42 75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:42 75-35-4
1,1,1-Trichloroethane
NO ug/L
1.0
1
10/26/13 06:42 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 06:42 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 06:42 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:42 95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 06:42 107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 06:42 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:42 541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:42 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 06:42 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 06:42 74-83-9
Bromoform
ND ug/L
1.0
1
/
10/26/13 06:42 7 5-2 - 5 2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:42 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 06:42 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 06:42 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 06:42 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 06:42 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 06:42 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 06:42 74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 06:42 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 06:42 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 06:42 75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:42 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 06:42 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 06:42 127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 06:42 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 06:42 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 06:42 75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 06:42 106-93-4
-'
Surrogates
4-Bromofluorobenzene (S)
94 %
70-130
1
10/26/13 06:42 460-00-4
1,2-Dichloroethane-d4 (S)
104 %
70-130
1
10/26/13 06:42 17060-07-0
Toluene-d8 (S)
99 %
70-130
1
10/26/13 06:42 2037-26-5
'
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 26 of 45

�aceAnalytical
mmpacelabs.=
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: SMW-3
Lab ID: 92177010014 Collected: 10/24/13 11:30
Received: 10/24/13 12:57 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
4.3 ug/L
1.0
1
10/26/13 06:58
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10126/1306:68
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
10126/1306:58
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 06:58
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 06:58
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:58
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 06:58
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 06:58
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:58
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 06:58
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 06:58
75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 06:58
74-834
Bromoform
ND ug/L
1.0
1
10/26/13 06:58
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:58
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 06:58
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 06:58
56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 06:58
108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 06:58
75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 06:58
67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 06:58
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 06:58
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 06:58
75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 06:58
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 06:58
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 06:58
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 06:58
127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 06:58
79-01-6
Trichlorofluoromethane
ND ug/L
1.0'
1
10/26/13 06:58
75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 06:58
75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 06:58
106-93-4
Surrogates
4-Bromofluorobenzene (S)
95 %
70-130
1
10/26/13 06:58
460-00-4
1,2-Dichloroethane-d4 (S)
107 %
70-130
1
10/26/13 06:58
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
10/26/13 06:58
2037-26-5
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 27 of 45

1�;a'ceAnalXicals
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 i
[phone] I -
Project* DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: TRIP Lab ID: 92177010015 Collected: 10/23/13 00:00 Received: 10/24/13 12:57 Matrix: Water
Parameters Results Units . Report Limit DF Prepared Analyzed CAS No. Qua]
601 Volatiles by SM 6200 Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
10/26/13 07:15 75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 07:15 75-35-4
11,1-Trichloroethane
NO ug/L
1.0
1
10/26/13 07:15 71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 07:15 79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10/26/13 07:15 79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 07:15 95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 07:15 107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 07:15 78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 07:15 541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 07:15 106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 07:15 75-27-4
Bromomethane
ND ug/L
5.0
1
10/26/13 07:15 74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 07:15 75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 07:15 156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 07:15 10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 07:15 56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 07:15 108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 07:15 75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 07:15 67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 07:15 74-87-3
Dibromochlorom ethane
ND ug/L
1.0
1
10/26/13 07:15 124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
10/26/13 07:15 75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 07:15 75-09-2
trans-1,2-Dichloroethene
NO ug/L
1.0
1
10/26/13 07:15 156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 07:15 10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 07:15 127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 07:15 79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 07:15 75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 07:15 75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 07:16 106-93-4
Surrogates
4-Bromofluorobenzene (S)
94 %
70-130
1
10/26/13 07:15 460-00-4
1,2-Dichloroethane-d4 (S)
105 %
70-130
1
10/26/13 07:15 17060-07-0
Toluene-d8 (S)
101 %
70-130
1
10/26/13 07:15 2037-26-5
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 28 of 45

4AceAnalyfical'9
wvmpace/abs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Sample: DMW-4 Lab ID: 92177010016 Collected: 10/24/13 10:00 Received: 10/24/13 12:57 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200 Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
10/26/13 07:31
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
10/26/13 07:31
75-35-4
1,1,1-Tdchloroethane
ND ug/L
1.0
1
10/26/13 07:31
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
10/26/13 07:31
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
10126/1307:31
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 07:31
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
10/26/13 07:31
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
10/26/13 07:31
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 07:31
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
10/26/13 07:31
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
10/26/13 07:31
75-27-4
Bromomethane
ND ug/L
5.0.
1
10/26/13 07:31
74-83-9
Bromoform
ND ug/L
1.0
1
10/26/13 07:31
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 07:31
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 07:31
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
10/26/13 07:31
56-23-5
Chlorobenzene
ND ug/L
1.0
1
10/26/13 07:31
108-90-7
Chloroethane
ND ug/L
1.0
1
10/26/13 07:31
75-00-3
Chloroform
ND ug/L
1.0
1
10/26/13 07:31
67-66-3
Chloromethane
ND ug/L
1.0
1
10/26/13 07:31
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
10/26/13 07:31
124-48-1
Dichlorodifluoromelhane
ND ug/L
1.0
1
10/26/13 07:31
75-71-8
Methylene Chloride
ND ug/L
2.0
1
10/26/13 07:31
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
10/26/13 07:31
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
10/26/13 07:31
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
10/26/13 07:31
127-18-4
Trichloroethene
ND ug/L
1.0
1
10/26/13 07:31
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
10/26/13 07:31
75-69-4
Vinyl chloride
ND ug/L
1.0
1
10/26/13 07:31
75-014
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
10/26/13 07:31
106-93-4
Surrogates
4-Bromofluorobenzene (S)
94 %
70-130
1
10/26/13 07:31
460-00-4
1,2-Dichloroethane-d4 (S)
108 %
70-130
1
10/26/13 07:31
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
10/26/13 07:31
2037-26-5
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 29 of 45

aceAnalyiical
wwwpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
QC Batch: AIR/18600
Analysis Method: RSK 175
QC Batch Method: RSK 175
Analysis Description: RSK 175 AIR HEADSPACE
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
METHOD BLANK: 1564311
Matrix: Water
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Ethane ug/L
ND 6.2 10/29/1317:53
Ethene ug/L
ND 6.2 10/29/1317:53
Methane ug/L
ND 6.6 10/29/1317:53
LABORATORY CONTROL SAMPLE & LCSD: 156431.2
1564313
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qualifiers
Ethane ug/L
114
114
113
100
100
85-115
.5 20
Ethene ug/L
106
106
106
100
100
85-115
.3 20
Methane ug/L
60.7
59.2
58.9
98
97
85-115
.5 20
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 30 of 45

i p
® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
(�5aneAnaljdical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wym.pacelab&com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
- " QC Batch: MERP/5743 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
METHOD BLANK: 1073464 Matrix: Water
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 10/28/13 21:58
LABORATORY CONTROL SAMPLE: 1073465
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1073466 1073467
MS MSD
92177214001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Mercury ug/L ND 2.5 2.5 2.2 2.1 84 79 75-125 6
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 31 of 45

m Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
laceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Hunlersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: DOT 404,34613.3.26
Pace Project No.: 92177010
QC Batch: MPRP/14512 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Associated Lab Samples: 92177010001,92177010002,92177010003,92177010004,92177010005,92177010006,92177010007,
92177010008
METHOD BLANK: 1072581
Matrix: Water
Associated Lab Samples:
92177010001, 92177010002, 92177010003, 92177010004, 92177010005,
92177010006, 92177010007,
92177010008
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
ug/L
ND
10.0
10/28/1319:20
Barium
ug/L
ND
6.0
10%28/1319:20
Cadmium
ug/L
ND
1.0
10/28/1319:20
Chromium
ug/L
ND
5.0
10/28/1319:20
Lead
ug/L
ND
5.0
10/28/13 19 20
Selenium
ug/L
ND
10.0
10/28/1319:20
Silver
ug/L
ND
5.0
10128/1319:20
LABORATORY CONTROL SAMPLE:
Parameter
1072582
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
ug/L
500
516
103
80-120
Barium
ug/L
500
488
98
80-120
Cadmium
ug/L
500
501
100
80-120
Chromium
ug/L
500
488
98
80-120
Lead
ug/L
500
486
97
80-120
Selenium
ug/L
500
516
103
80-120
Silver
ug/L
250
246
98
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1072583
1072584
MS
MSD
92176977001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
Arsenic
ug/L
ND
500
500
528
533
105
106
75-125
1
Barium
ug/L
13.0
500
500
503
503
98
98
75-125
0
Cadmium
ug/L
ND
500
500
506
508
101
102
75-125
0
Chromium
ug/L
ND
500
500
488
490
97
97
75-125
1
Lead
ug/L
ND
500
500
483
485
96
97
75-125
0
Selenium
ug/L
NO
500
500
526
525
104
104
75-125
0
Silver
ug/L
ND
250
250
246
247
99
99
75-125
0
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 32 of 45

f ;
�aceAnalytical
wwwpacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MSV/24691 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 601 by 6200E
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008,92177010009,92177010010,92177010011,92177010012,92177010013,92177010014,
92177010015,92177010016
METHOD BLANK: 1073012 Matrix: Water
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008,92177010009,92177010010,92177010011,92177010012,92177010013,92177010014,
92177010015,92177010016
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1-Trichloroethane
ug/L
ND
1.0
10/26/13 03:24
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
10/26/13 03:24
1,1,2-Trichloroethane
ug/L
ND
1.0
10/26/13 03:24
1,1-Dichloroethane
ug/L
ND
1.0
10/26/13 03:24
1,1-Dichloroethene
ug/L
ND
1.0
10/26/13 03:24
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
10/26/13 03:24
1,2-Dichlorobenzene
ug/L
ND
1.0
10/26/13 03:24
1,2-Dichloroethane
ug/L
ND
1.0
10/26/13 03:24
1,2-Dichloropropane
ug/L
ND
1.0
10/26/13 03:24
1,3-Dichlorobenzene
ug/L
ND
1.0
10/26/13 03:24
1,4-Dichlorobenzene
ug/L
ND
1.0
10/2611303:24
Bromodichloromethane
ug/L
ND
1.0
10/26/13 03:24
Bromoform
ug/L
ND
1.0
10/26/13 03:24
Bromomethane
ug/L
ND
5.0
10/26/13 03:24
Carbon tetrachloride
ug/L
ND
1.0
10/26/13 03:24
Chlorobenzene
ug/L
ND
1.0
10/26/13 03:24
Chloroethane
ug/L
ND
1.0
10/26/13 03:24
Chloroform
ug/L
ND
1.0
10/26/13 03:24
Chloromethane
ug/L
ND
1.0
10/26/13 03:24
cis-1,2-Dichloroethene
ug/L
ND
1.0
10/26/13 03:24
cis-1,3-Dichloropropene
ug/L
ND
1.0
10/26/13 03:24
Dibromochloromethane
ug/L
ND
1.0
10/26/13 03:24
Dichlorodifluoromethane
uglL
ND
1.0
10/26/13 03:24
Methylene Chloride
ug/L
ND
2.0
10/26/13 03:24
Tetrachloroethene
ug/L
ND
1.0
10/26/13 03:24
trans-1,2-Dichloroethene
ug/L
ND
1.0
10/26/13 03:24
trans-1,3-Dichloroprope ne
ug/L
ND
1.0
10/26/13 03:24
Trchloroethene
ug/L
ND
1.0
10/26/13 03:24
Trichlorofluoromethane
ug/L
ND
1.0
10/26/13 03:24
Vinyl chloride
ug/L
ND
1.0
10/26/13 03:24
1,2-Dichloroethane-d4(S)
%
102
70-130
10126/1303:24
4-Bromofluorobenzene (S)
%
96
70-130
10/26/13 03:24
Toluene-d8 (S)
%
100
70-130
10/26/13 03:24
LABORATORY CONTROL SAMPLE: 1073013
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 50 55.1 110 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
_ Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc..
Page 33 of 45

1�;a'ceAnaljdical'
wvnvpacela6s.rnm
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
LABORATORY CONTROL SAMPLE: 1073013
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,2,2-Tetrachloroethane
ug/L
50
55.1
110
60-140
1,1,2-Trichloroethane
ug/L
50
55.9
112
60-140
1,1-Dichloroethane
ug/L
50
51.4
103
60-140
1,1-Dichloroethene
ug/L
50
52.8
106
60-140
1,2-Dibromoethane (EDB)
ug/L
50
57.2
114
60-140
1,2-Dichlorobenzene
ug/L
50
56.8
114
60-140
1,2-Dichloroethane
ug/L
50
49.2
98
60-140
1,2-Dichloropropane
ug/L
50
55.8
112
60-140
1,3-Dichlorobenzene
ug/L
50
54.6
109
60-140
1,4-Dichlorobenzene
ug/L
50
53.2
106
60-140
Bromodichloromethane
ug/L
50
57.4
115
60-140
Bromoform
ug/L
50
48.5
97
60-140
Bromomethane
ug/L
50
53.4
107
60-140
Carbon tetrachloride
ug/L
50
54.7
109
60-140
Chlorobenzene
ug/L
50
54.2
108
60-140
Chloroethane
ug/L
50
43.5
87
60-140
Chloroform
ug/L
50
52.6
105
60-140
Chloromethane
ug/L
50
44.1
88
60-140
cis-1,2-Dichloroethene
ug/L
50
51.3
103
60-140
cis-1,3-Dichloropropene
ug/L
50
61.7
123
60-140
Dibromochloromethane
ug/L
50
50.6
101
60-140
Dichlorodifluoromethane
ug/L
50
49.7
99
60-140
Methylene Chloride
ug/L
50
56.7
113
60-140
Tetrachloroethene
ug/L
50
54.6
109
60-140
trans-1,2-Dichloroethene
ug/L
50
50.6
101
60-140
trans-1,3-Dichloropropene
ug/L
50
56.7
113
60-140
Trichloroethene
ug/L
50
51.9
104
60-140
Trichlorofluoro methane
ug/L
50
45.7
91
60-140
Vinyl chloride
ug/L
50
46.8
94
60-140
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 1073014
1073015
MS
MSD
92177010010
Spike
Spike
MS
MSD
MS MSD % Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec Limits RPD
1,1,1-Trichloroethane
ug/L
ND
20
20
23.8.
24.6
119
123 60-140 3
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
23.0
22.9
115
114 60-140 0
1,1,2-Trichloroethane
ug/L
ND
20
20
22.9
23.8
115
119 60-140 4
1,1-Dichloroethane
ug/L
ND
20
20
22.8
23.3
114
116 60-140 2
1,1-Dichloroethene
ug/L
ND
20
20
24.1
23.9
120
120 60-140 1
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
23.2
23.2
116
116 60-140 0
1,2-Dichlorobenzene
ug/L
ND
20
20
24.0
25.0
120
125 60-140 4
1,2-Dichloroethane
ug/L
NO
20
20
21.5
22.3
107
111 60-140 4
1,2-Dichloropropane
ug/L
ND
20
20
23.9
25.0
119
125 60-140 5
1,3-Dichlorobenzene
ug/L
ND
20
20
23.2
23.8
116
119 60-140 2
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in full,
Date: 11/06/2013 04:59 PM
without
the written consent of Pace Analytical Services, Inc..
Qual
Page 34 of 45
I

_�aceAnaljdical
mmpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1073014
MS
92177010010
Spike
Parameter
Units
Result
Conc.
1,4-Dichlorobenzene
ug/L
ND
20
Bromodichloro methane
ug/L
ND
20
Bromoform
ug/L
ND
20
Bromomethane
ug/L
ND
20
Carbon tetrachloride
ug/L
ND
20
Chlorobenzene
ug/L
ND
20
Chloroethane
ug/L
ND
20
Chloroform
ug/L
ND
20
Chloromethane
ug/L
ND
20
cis-1,2-Dichloroethene
ug/L
ND
20
cis-1,3-Dichloropropene
ug/L
ND
20
Dibromochloromethane
ug/L
ND
20
Dichlorodifluoromethane
ug/L
ND
20
Methylene Chloride
ug/L
ND
20
Tetrachloroethene
ug/L
ND
20
trans-1,2-Dichloroethene
ug/L
ND
20
trans-1,3-Dichloropropene
ug/L
ND
20
Tichloroethene
ug/L
ND
20
Trichlorofluoromethane
ug/L
ND
20
Vinyl chloride
ug/L
ND
20
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville; NC 28078
[phone]
MSD
Spike
Conc.
1073015
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
20
22.6
23.5
113
117
60-140
4
20
23.1
24.0
116
120
60-140
4
20
19.3
19.3
97
96
60-140
0
20
20.1
22.4
100
112
60-140
11
20
23.8
24.2
119
121
60-140
1
20
22.9
23.6
114
118
60-140
3
20
24.3
23.8
121
119
60-140
2
20
23.1
23.6
115
118
60-140
2
20
18.8
19.0
94
95
60-140
1
20
22.1
22.5
110
113
60-140
2
20
22.5
23.3
112
117
60-140
4
20
21.0
21.1
105
105
60-140
0
20
22.8
23.4
114
117
60-140
2
20
22.9
23.7
115
119
60-140
4
20
23.2
24.4
116
122
60-140
5
20
22.2
22.9
111
115
60-140
3
20
21.6
22.6
108
113
60-140
5
20
22.8
23.0
114
115
60-140
1
20
22.7
22.8
113
114
60-140
1
20
20.5
21.2
102
106
60-140
4
99
96
70-130
102
99
70-130
98
98
70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc..
Qual
Page 35 of 45

o
Analytical
imw.pacefabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
QC Batch: WET/27828 Analysis Method: SM 4500-S2D
QC Batch Method: SM 4500-S21) Analysis Description: 4500S2D Sulfide Water
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004. 92177010005, 92177010006, 92177010007,
92177010008
METHOD BLANK: 1074375 Matrix: Water
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide mg/L ND 0.10 10/29/1315:42
LABORATORY CONTROL SAMPLE: 1074376
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide mg/L .5 0.54 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1074377 1074378
MS MSD
92176757002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Sulfide mg/L ND .5 .5 0.52 0.52 105 105 75-125 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1074379
1074380
MS
MSD
92176996002 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qual
Sulfide mg/L ND .5
.5
0.52
0.52 105 105 75-125 0
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 36 of 45

�aceAnalyticalo
W"zPacelabs.cvm
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
QC Batch: WETA/16840 Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
METHOD BLANK: 1072206 Matrix: Water
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 2.0 10/29/13 23:24
LABORATORY CONTROL SAMPLE: 1072207
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate mg/L 20 20.2 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1072208 1072209
MS MSD
92176714001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Sulfate mg/L 4.8 20 20 22.2 22.2 87 87 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1073864 1073865
MS MSD
92176543001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 5.1 20 20 27.3 28.7 111 118 90-110 5 M1
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 37 of 45

��aceAnalyfical
www.pacelabscom
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: WETA/16844
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92177010001, 92177010002.
92177010003, 92177010004, 92177010005, 92177010006, 92177010007.
92177010008
METHOD BLANK: 1072500
Matrix: Water
Associated Lab Samples: 92177010001, 92177010002,
92177010003. 92177010004, 92177010005, 92177010006. 92177010007,
92177010008
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L
ND 0.020 10/26/13 03:35
LABORATORY CONTROL SAMPLE: 1072501
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
2.5 2.4 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1072502 1072503
MS MSD
92177071010
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits
RPD Qual
Nitrogen, Nitrate mg/L 1.8
2.5 2.5 4.0 4.0 88 89 90-110
0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1072504 1072505
MS MSD
92177010001
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits
RPD Qual
Nitrogen, Nitrate mg/L 0.86
2.5 2.5 3.1 3.1 92 90 90-110
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59 PM without the written consent of Pace Analytical Services, Inc.. Page 38 of 45

r
All Iff
/�acceAnalytical
rwnxpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
- QC Batch: WETA/16839 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: 5310E TOC
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
METHOD BLANK: 1072193 Matrix: Water
Associated Lab Samples: 92177010001, 92177010002, 92177010003, 92177010004, 92177010005, 92177010006, 92177010007,
92177010008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L ND 1.0 10/30/13 16:59
LABORATORY CONTROL SAMPLE: 1072194
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 25 25.3 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1072195 1072196
MS MSD
92176634002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 2.1 25 25 24.3 24.3 89 89 75-125 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1072197 1072198
MS MSD
92177035002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 467 25 25 461 466 -27 -6 75-125 1 M6
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 39 of 45

acmnalytical
www.pacelabs.com
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 j
[phone]
DF -Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PRL- Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
PASI-M Pace Analytical Services - Minneapolis
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 40 of 45 - J

9 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wympacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92177010001
DMW-6
RSK 175
AIR/18600
92177010002
DMW-7
RSK 175
AIR/18600
92177010003
DMW-10
RSK 175
AIR/18600
92177010004
DMW-9
RSK 175
AIR/18600
92177010005
DMW-11
RSK 175
AIR/18600
_ 92177010006
DMW-8
RSK 175
AIR/18600
92177010007
DMW-2
RSK 175
AIR/18600
r- 92177010008
DMW-1
RSK 175
AIR/18600
92177010001
DMW-6
EPA 3010
MPRP/14512
EPA6010
ICP/13195
92177010002
DMW-7
EPA 3010
MPRP/14512
EPA 6010
ICP/13195
92177010003
DMW-10
EPA 3010
MPRP/14512
EPA 6010
ICP/13195
92177010004
DMW-9
EPA 3010
MPRP/14512
EPA 6010
ICP/13195
92177010005
DMW-11
EPA 3010
MPRP/14512
EPA 6010
ICP/13195
92177010006
DMW-8
EPA3010
MPRP/14512
EPA6010
ICP/13195
92177010007
DMW-2
EPA 3010
MPRP/14512
EPA 6010
ICP/13195
92177010008
I
DMW-1
EPA 3010
MPRP/14512
EPA 6010
ICP/13195
92177010001
DMW-6
EPA 7470
MERP/5743
EPA 7470
MERC/5558
92177010002
DMW-7
EPA 7470
MERP15743
EPA 7470
MERC/5558
92177010003
DMW-10
EPA 7470
MERP/5743
EPA 7470
MERC/5558
92177010004
DMW-9
EPA 7470
MERP/5743
EPA 7470
MERC/5558
92177010005
DMW-11
EPA 7470
MERP15743
EPA 7470
MERC/5558
92177010006
DMW-8
EPA 7470
MERP/5743
EPA 7470
MERC/5558
_ 92177010007
DMW-2
EPA 7470
MERP/5743
EPA 7470
MERC/5558
92177010008
DMW-1
EPA 7470
MERP/5743
EPA 7470
MERC/5558
92177010001
DMW-6
SM 6200B
MSV/24691
92177010002
DMW-7
SM 6200E
MSV/24691
- 92177010003
DMW-10
SM 6200E
MSV/24691
" 92177010004
DMW-9
SM 6200E
MSV/24691
92177010005
DMW-11
SM 6200E
MSV/24691
92177010006
DMW-8
SM 6200E
MSV/24691
92177010007
DMW-2
SM 6200B
MSV/24691
92177010008
DMW-1
SM 6200E
MSV/24691
92177010009
CREEK
SM 6200B
MSV/24691
92177010010
WSW-4
SM 6200E
MSV/24691
92177010011
SMW-2
SM 6200E
MSV/24691
92177010012
SMW-1
SM 6200B
MSV/24691
92177010013
DMW-3
SM 6200E
MSV/24691
92177010014
SMW-3
SM 6200E
MSV/24691
92177010015
TRIP
SM 6200B
MSV/24691
92177010016
DMW-4
SM 6200E
MSV/24691
92177010001
DMW-6
SM 4500-S2D
WET/27828
92177010002
DMW-7
SM 4500-S2D
WET/27828
92177010003
DMW-10
SM 4500-S2D
WET/27828
92177010004
DMW-9
SM 4500-S2D
WET/27828
92177010005
DMW-11
SM 4500-S2D
WET/27828
92177010006
DMW-8
SM 4500-S2D
WET/27828
92177010007
DMW-2
SM 4500-S2D
WET/27828
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2013 04:59
PM
without the written consent of Pace Analytical Services, Inc..
Page 41 of 45

0 Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr.
iwnvpacefabs.com Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DOT 404 34613.3.26
Pace Project No.: 92177010
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92177010008
DMW-1
SM 4500-S213
WET/27828
92177010001
DMW-6
EPA 300.0
WETA/16840
92177010002
DMW-7
EPA 300.0
WETA/16840
92177010003
DMW-10
EPA 300.0
WETA/16840
92177010004
DMW-9
EPA 300.0
WETA/16840
92177010005
DMW-11
EPA 300.0
WETA/16840
92177010006
DMW-8
EPA 300.0
WETA/16840
92177010007
DMW-2
EPA 300.0
WETA116840
92177010008
DMW-1
EPA 300.0
WETA/16840
92177010001
DMW-6
EPA 353.2
WETA/16844
92177010002
DMW-7
EPA 353.2
WETA/16844
92177010003
DMW-10
EPA 353.2
WETA/16844
92177010004
DMW-9
EPA 353.2
WETA/16844
92177010005
DMW-11
EPA 353.2
WETA/16844
92177010006
DMW-8
EPA 353.2
WETA/16844
92177010007
DMW-2
EPA 353.2
WETA/16844
92177010008
DMW-1
EPA 353.2
WETA/16844
92177010001
DMW-6
SM 5310E
WETAI16839
92177010002
DMW-7
SM 5310E
WETA116839
92177010003
DMW-10
SM 5310E
WETA/16839
92177010004
DMW-9
SM 5310E
WETA/16839
92177010005
DMW-11
SM 5310E
WETA/16839
92177010006
DMW-8
SM5310B
WETA/16839
92177010007
DMW-2
SM 5310E
WETA/16839
92177010008
DMW-1
SM 5310B
WETA/16839
Date: 11/06/2013 04:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 42 of 45

11-11'ra°aceAnalyGcal
Sample Condition Upon Recei
Document Number:
F-CHR-CS-03-rev.11
Page 1 of 2
Issuing Authority:
Pace Huntersville Quality Office
Client Name:
Where Received: Huntersville ❑ Asheville ❑ Eden [] Raleigh
Courier: ❑ Fed Ex ❑ UPS❑ USPS[4 Client❑ Commercial❑ Pace Other
Pro D =D'fer
Custody Seal on Cooler/Box Present: ❑ yes [� no Seals intact: ❑ yes ❑ no
Proj-Name
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None Other
Thermometer Used: IR Gun T1102 1301 Type of Ice: Wet Blue None aSamples on ice, cooling process has begun
Temp Correction Factor T1102: No Correction T1301: No Correction _.
�
Corrected Cooler Temp.: ( C
Biolo ical Tissue is Frozen: Yes No N1A
g
Date and Initi I of pers exfining
3
Temp should be above freezing to 6°C
Comments:
contents: d
Chain of Custody Present:
Yes []No
❑N/A
1.
Chain of Custody Filled Out:
Yes ❑No
❑NIA
2.
Chain of Custody Relinquished:
OYes ❑No
❑N/A
3.
Sampler Name & Signature on COC:
PYes ❑No
❑N/A
4.
Samples Arrived within Hold Time:
t FlYes ❑No
❑N/A
5.
Short Hold Time Analysis (<72hr):
Yes ❑No
❑N/A
6,
Rush Turn Around Time Requested:
Dyes No
❑N/A
7.
Sufficient Volume:
Yes ❑No
❑NIA
8.
Correct Containers Used:
Yes ❑No
❑NIA
g,
-Pace Containers Used:
( Yes ❑No
❑N/A
Containers Intact:
PYes ❑No
❑N/A
10,
Filtered volume received for Dissolved tests
❑Yes ❑No
NIA
11.
Sample Labels match COC:
Yes ONo
❑NIA
-Includes date/time/ID/Analysis Matrix:
✓S —
c
All containers needing preservation have been checked.
Yes ❑No
❑NIA
13.
All containers needing preservation are found to be in
Yes ❑No
❑NIA
compliance vrilh EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
PYes ❑No
Samples checked for dechlorination:
Yes ❑No
❑NIA
14.
Headspace in VOA Vials >6mm):
4( No
❑N/A
15.
Trip Blank Present:
Yes ❑No
❑NIA
16.
Trip Blank Custody Seals Present
t Yes ❑No
❑NIA
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: �s e [`j u •„ Date/Time: / , •,, y j
Comments/Resolution:
SCURF Review: Date: 1 "'' 2 °/ 's o'---
SRF Review: ' ) Date: k 2 `/ %J WO# : 92177 ®10
Note: Whenever there- a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR II�II�I�III IIIIIII IIII
Certification Office ( Le out of hold, incorrect preservative, out of temp, I
incorrect containers) 92177010
Page 43 of 45

i
ato
y CHAIN -OF -CUSTODY / Analytical Request Document
/ f rlreAnalvPiral The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. o
www.pacelaes.com
Page: of
Section A Section B Section C
�>, /f ^
Required Client Information; Required Project Information: Invoice Information:
Company: r ( Report TO: t �/ Attention:
bey l G
2 4 L/ 93
Address: Copy
To:
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REGULATQRYAGENCY
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(- NPDES i GROUND WATER DRINKING WATER
F UST ? RCRA T OTHER
Email To: / Purchase
S ltOnP1! I�J1 iCii�ii'tZ�
Order No.:
Pace Quote
Reference:
FPh,,.l,IFax:
Project
Name: { q G�
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Location'L^Manager:aProj
STATE:
jV
ted Due Date[TAT: Project
Number: U
Paw ProfAa 4:
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RaquirodClienl Information MATRIX ! CODE
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DATE
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SA61PLE CONDITIONS
IF
SAMPLER NAME AND SIGNATURE
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'FaceAnalyt of e
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Ln
v
0
Page: of �f---
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information:
Company: j Report To: 1 Attention:
1724294
' 3 ( �ij _
L y
Address:
Copy To:
CompanyN�me M;
REGULATORY AGENCY
Address: �y � 7 aA _
7 Y�
r- NPDES i— GROUNDWATER r DRINKING WATER
(` UST F- RCRA i - OTHER
Email TD• + • < /� t,,,r,�,,�/
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Reference:
Ph ne:
�7Ctt GW"�
Fax:
Project Name: �`
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Pace Protect
Manager.
Site Location
STATE:
��
Requested Duo Date/TAT: L,
Project Number. ^ UL o 11
\J _
Paco Proflc 11:
Requested
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Filtered
(Y/N)
Section D Matrix Codes
o
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Raquired Client Information MATRIX I CODE
c
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RELINQUISHED BY I AFFILIATION
DATE
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DATE
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SAMPLER NAME AND SIGNATURE
Q
c
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ORIGINAL
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SIGNATURE of SAMP
DATE Signed
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(MMIDD/YY): aZy
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'hnportant Note: By signing this fomt you am accepting Paca s NET 30 day payment term: and agreeing to late charges of 1.5ffi per many invoices not paid %VWK30 days. r F-ALL-O.020rev.07, 15-May-2007
�1

J
micro seeps,-,.-,
November 4, 2013
Kevin Godwin
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Microseeps
220 VJlliam Pitt Way
Pittsburgh. PA 15238
Phone: [phone]
Fax: [phone]
RE: DOT STATESVILLE / 92177010
Microseeps Workorder.10479
Dear Kevin Godwin:
Enclosed are the analytical results for sample(s) received by the laboratory on Friday, October 25, 2013.
- Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise
narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Robbin Robl 11/04/2013
[e-mail]
Customer Service Representative
Enclosures
Report ID: 10479 - 450376
As a valued client we would appreciate your comments on our service.
Please email [e-mail].
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
vrithout the written consent of Microseeps.
Total Number of Pages
Page 1 of 14

1 £
inicroseeps '
LABORATORY ACCREDITATIONS & CERTIFICATIONS
Microsecps
220 l°filliam Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Accreditor:
Pennsylvania Department of Environmental Protection, Bureau of Laboratories
Accreditation ID:
02-00538
Scope:
NELAP Non -Potable Water and Solid & Hazardous Waste
Accreditor:
NELAP: State of Florida, Department of Health, Bureau of Laboratories
Accreditation ID:
E87832
Scope:
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
South Carolina Department of Health and Environmental Control, Office of Environmental
Laboratory Certification
Accreditation ID:
89009003
Scope:
Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA)
Accreditor:
NELAP: State of Louisiana, Department of Environmental Quality
Accreditation ID:
04104
Scope:
Solid and Chemical Materials; Non -Potable Water
Accreditor:
NELAP: New Jersey, Department of Environmental Protection
Accreditation ID:
PA026
Scope:
Non -Potable Water; Solid and Chemical Materials
Accreditor:
NELAP: New York, Department of Health Wadsworth Center
Accreditation ID:
11815
Scope:
Non -Potable Water; Solid and Hazardous Waste
Accreditor:
State of Connecticut, Department of Public Health, Division of Environmental Health
Accreditation ID:
PH-0263
Scope:
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
NELAP: Texas, Commission on Environmental Quality
Accreditation ID:
T104704453-09-TX
Scope:
Non -Potable Water
Accreditor:
State of New Hampshire
Accreditation ID:
299409
Scope:
Non -potable water
Accreditor:
State of Georgia
Accreditation ID:
Chapter 391-3-26
Scope:
As per the Georgia EPD Rules and Regulations for Commercial Laboratories, Microseeps is
accredited by the Pennsylvania Department of Environmental Protection Bureau of
Laboratories under the National Environmental Laboratory Approval Program (NELAC).
Report ID: 10479 • 450376
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except ir. full,
without the written consent of fdlicroseeps,
nedn' =>
Page 2 of 14

j microseeps-}
SAMPLE SUMMARY
Workorder: 10479 DOT STATESVILLE / 92177010
hlicroseeps
220 William Pitt 1aby
Pittsburgh, PA15238
Phone: [phone]
Fax: [phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Received
104790001
DMW-6
Water
10/23/2013 09:40
10/25/2013 IV00
104790002
DMW-7
Water
10/23/2013 10:20
101251201311:00
104790003
DMW-10
Water
10/23/2013 11:00
10/251201311:00
104790004
DMW-9
Water
10123/201311:40
10125/201311:00
104790005
DMW-11
Water
10/23/201312:20
10/25/2013 11:00
104790006-
DMW-8
Water
10/23/2013 13:15
10125/201311;00
104790001
DMW 2
Water
10/24/2013 07:15
101251201311t00
104790008 -
DMW-1
Water
10/24/.2013:09:00
10125/201311:00
Report ID: 10479 - 450376
CERTIFICATE OF ANALYSIS
ibis report shall not be reproduced, except in full,
without the written consent of Microseeps.
.`nel�ac=
Page 3 of 14

ANALYTICAL RESULTS
Workorder: 10479 DOT STATESVILLE 192177010
Microseeps
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 104790001
Sample ID: DMW6
Date Received: 10/25/2013 11:00
Date Collected: 10/23/2013 09:40
Matrix: Water
Parameters
Results Units
PQL
MDL DFPrepared By
Analyzed
By Qual
EDonors - MICR
Analysis Desc: AM21 G
Analytical Method: AM21 G
Acetic Acid
0.67U mg/I
5.0
0.67 1
11/1/201311:46
BW
PropionicAcid
0.25U mg/I
5.0
0.25 1
11/1/201311:46
BW
PyruvicAcid
0.53U mg/I
10
0.53 1
11/1/201311:46
BW
Butyric Acid
0.10U mg/I
5.0
0.10 1
11/11201311:46
BW
Lactic Acid
2.OU mg/I
25
2.0 1
11111201311:46
BW
Report ID: 10479 - 450376 Page 4 of 14
CERTIFICATE OF ANALYSIS
This report shall not be reproduced• except in full.
without the written consent of Microseeps.
nP[a r"

Ic
ANALYTICAL RESULTS
Workorder. 10479 DOT STATESVILLE / 92177010
Microseeps
220 William Pitt Way
Pit(sWrgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 104796002 Date Received: 10/25/2013 11:00 Matrix: Water
Sample ID: DMW-7 Date Collected: 10123/2013 10:20
Parameters Results Units PQL MDL ' DIF Prepared By Artalyzed By Qual
ElDonors - MICR
Analysts_,
AdeiicA'cid
0.671.11 mg/l
5.0
0.67
1
111/1/2011312M
BW
Prop tonic'Acid
0.28U mg1l
5.0
0.25
1
11111201312:52
BW
PyruvIdAcid
0.53U Mon
10 .
0.53 3
1
111/1/2013:112:52
Butyric Acid
0s10u mg(l
5.0
0;10
1
11/1 , 12'013 12:52,
BW
Lactic Acid
2.'OU m'gli,
25
2.0
1
1111111/2011312f52
BW
Report ID: 10479 - 450376
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the w6tten consent of Microseeps.
Jine A
Page 5 of, 14

f «/
microseeps
ANALYTICAL RESULTS
Workorder: 10479 DOT STATESVILLE / 92177010
Nlicroseeps
220 William Pitt Way
Pittsburgh, PA 15238
Phone. [phone]
Fax: [phone]
Lab ID: 104790003
Sample ID: DMW-10
Date Received: i oi25/2013 11:00
Date Collected: 10/23/2013 11:00
Matrix: Water
Parameters
Results Units
PQL
MDL DFPrepared By
Analyzed
By Qual
EDonors - MICR
Analysis Desc: AM21G
Analytical Method: AM21G
Acetic Acid
0.67U mg/I
5.0
0.67 1
11/1/201313:14
BW
PropionicAcid
0.25U mg/I
5.0
0.25 1
11/1/201313:14
BW
PyruvicAcid
0.53U mg/I
10
0.53 1
11/1/201313:14
BW
Butyric Acid
0.10U mg/I
5.0
0.10 1
11111201313:14
BW
Lactic Acid
2.0U mg/I
25
2.0 1
11/1/201313:14
SW
Report ID: 10479 - 450376 Page 6 of 14
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Microseeps.
'rlelac"=.

s r d�L, t:,
mlcroseepsF°=
ANA. LYTICAL RESULTS
Workorder. 10479 DOT STATESVILLE / 92177010
Microseeps
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 104790004
Sample ID: OMW-9
Date Received: 10/25/2013 11:00
Date Collected: 10/23/201311:40
Matrix: Water
Parameters
Results Units
PQL
MDL DFPrepared By
'Analyzed
By Qual
EDonors - MICR
Analysis Dek:AM21G
Anaty6cal Methtid':AM21G.. m
AceticAcid
0.6711 mall
5.0
G.67 1
11/11201313:36
BW
Propioni.aAcid
0.25U mgA
5.0
0.25, 1
11111201313:36,
BW
Pyruvic Acid
0.53U mgll
10
0.53 1
11/1/2013'13:36
BW
Butyric Acid
0.1011 mall
5:0
0.10, 1
11/`1/201313:361
BW
Lactic Acid
2.01.11. mg/l
25
2.'0 1
11/1/2613 13:36
BW
Report ID: 10479 - 450376 Page 7 of 14
CERTIFICATE OF ANALYSIS
This report shall not be -reproduced. except in full.
vAlhout the written consent of Microseeps.

-
�
Microseeps
220 William Pitt Way
1`
Pittsburgh, PA 15238
f111CfOSt'C(1S
Phone:
[phone]
Fax: [phone]
ANALYTICAL
RESULTS
Workorder: 10479 DOT STATESVILLE / 92-177010
Lab ID: 104790005
Date Received: 10/25/2013 11:00
Matrix: Water
Sample ID: DMW-11
Date Collected: 10/23/2013 12:20
Parameters
Results Units
PQL
MDL DFPrepared By
Analyzed
By Qual
EDonors - MICR
Analysis Desc: AM21 G
Analytical Method: AM21 G
Acetic Acid
0.67U mgA
5.0
0.67 1
11/1/2013 13:58
BW
PropionicAcid
0.25U mg/I
5.0
0.25 1
11/1/2013 13:58
BW
Pyruvic Acid
0.53U mg/I
10
0.53 1
11/1/201313:58
BW
Butyric Acid
O.10U mg/l
5.0
0.10 1
11/1/201313:58
BW
LacticAcid
2.OU mg/l
25
2.0 1
11/1/201313:58
BW
Report ID: 10479 - 450376 Page 8 of 14
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Microseeps.
:''rie(ar

�� rl
I � �
micros oseeps
ANALYTICAL RESULTS
Workorder: 10479 DOT STATESVILLE 192177010
Alicroseeps
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 104790006
Sample ID: DMW-8
Date Received: 10/25/2013 11:00
Date Collected: 10/23/2013 13:15
Matrix: Water
Parameters
Results Units
PQL
MDL DFPrepared By
Analyzed
By Qual
EDonors - MICR
Analysis Desc: AM21 G
Analytical Method: AM21 G
Acetic Acid
0.67U mg/I
5.0
0.67 1
11/1/201314:20
BW
PropionicAcid
0.251.1 mgA
5.0
0.25 1
11/1/201314:20
BW
PyruvicAcid
0.53U mg/I
10
0.53 1
11/1/201314:20
BW
Butyric Acid
0.101.11 mg/I
5.0
0.10 1
1111/201314:20
BW
Lactic Acid
2.01.1 mg/I
25
2.0 1
11/1/201314:20
BW
Report ID: 10479 - 450376 Page 9 of 14
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Microseeps.
riPiar`

Microseeps
. }
i !
220 William Pitt Way
Pittsburgh. PA 15238
'- j
_
tltlCfUSEEpS
Phone: [phone]
Fax [phone]
ANALYTICAL RESULTS
Workorder: 10479 DOT STATESVILLE 192177010
Lab ID: 104790007
Date Received: 10/25/2013 11:00
Matrix: Water
Sample ID: DMW-2
Date Collected: 10/24/2013 07:15
Parameters
Results Units
PQL
MDL DF Prepared By
Analyzed
By Qual
EDonors - MICR
Analysis Desc: AM21G
Analytical Method: AM21G
Acetic Acid
0.67U mg/l
5.0
0.67 1
11/1/201314:42
BW
PropionicAcid
0.25U mg/1
5.0
0.25 1
1111/201314:42
BW
PyruvicAcid
0.531J mg/I
10
0.53 1
11/11201314:42
BW
Butyric Acid
0.10U mg/I
5.0
0.10 1
11/1/201314:42
BW
Lactic Acid
2.OU mg/I
25
2.0 1
11111201314:42
BW
Report ID: 10479 - 450376 Page 10 of 14
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in lull,
without the written consent of Microseeps.
nPlac_--.

Microseeps
l
220 William Pitt Way
Pittsburgh. PA 15238
microseeps"°
Phone:
(412) 826.52 45
_fits=
Fax: [phone]
ANALYTICAL RESULTS
Workorder: 10479 DOT STATESVILLE / 92177010
Lab ID: 104790008
Date Received: 10/25/,2013 11:60
Matrix: Water
Sample ID: DMW 1
Date Collected: 10/24/2013 09:00
Parameters
Risults, Units
PQL
MDL DFPrepared By
Analyzed
By Qual
EDonors - MICR
Analysis-Desc: AM21G
Analytical Method: AM21'G-
Acetic Acid
0.67U mgn
5.0
0.67 1
11/112013,15:04
BW
PropionleAcid
U5U mg/l•
5.0
0.25 1
11111201315:04
BW.
Pyruvid Arid
0.53U mgp
10
0.53 1
111112013.15:04
BW
Butyric Acid
0.10U ,mg/l
5.0
0.10 1
11/i/201'3-15:04
BW
LactIcAcfd
2:0U mg/l
25
2.'0 1
11/1/2013.15iO4
BW
Report ID: 10479 - 450316 Page 11 of 14
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
e+ithout the written consent of Microseeps.
. `"relate=

t
z t�
microseeps,
ANALYTICAL RESULTS QUALIFIERS
Workorder: 10479 DOT STATESVILLE / 92177010
DEFINITIONS/QUALIFIERS
Microseeps
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Disclaimer: The Pennsylvania Department of Environmental Protection (PADEP) has decided to no longer recognize analyses that do not
produce data for primary compliance, for NELAP accreditation. The methods affected by this decision are AM20GAx, AM21 G,
SW846 7199 and AM4.02. The laboratory shall continue to administer the NELAPlTNI standard requirements in the performance
of these methods.
MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection.
PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation.
ND Not detected at or above reporting limit.
DF Dilution Factor.
S Surrogate.
RPD Relative Percent Difference.
% Rec Percent Recovery.
U Indicates the compound was analyzed for, but not detected at or above the noted concentration.
J Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL),
Report ID: 10479 - 450376
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Microseeps.
`rie[ac=P=
Page 12 of 14

r-
°34�A7
-
T:' u
micros eeps_ .
QUALITY CONTROL DATA
Workorder: 10479 DOT STATESVILLE / 92177010
Microseeps
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Far.: [phone]
QC Batch. EDON/1902
Analysis Method:
AM21G
QC Batch Method: AM21G
Associated Lab Samples:
104790001, 104790002. 104790003,
104790004, 104790005, 104790006, 104790007, 104790008
METHOD BLANK: 23805
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
EDonors
Acetic Acid
mg/I
0.67U
0.67
PropionicAcid
mg/I
0.25U
0.25
PyruvicAcid
mg/I
0.531.1
0.53
Butyric Acid
mg/I
0.10U
0.10
Lactic Acid
mg/I
2.01.1
2.0
LABORATORY CONTROL SAMPLE:
23806
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result %
Rec
Limits Qualifiers
EDonors
Acetic Acid
mg/I
100
98
98
70-130
PropionicAcid
mg/I
100
93
93
70-130
Pyruvic Acid
mg/I
100
87
87
70-130
Butyric Acid
mg/I
100
97
97
70-130
Lactic Acid
mg/I
100
120
116
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 23807
23808
Original:
104790001
Original
Spike
MS MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Result Result
% Rec
% Rec
Limit
RPD
RPD Qualifiers
EDonors
Acetic Acid
mg/I
0
100
95 95
95
95
70-130
0
20
PropionicAcid
mg/I
0
100
91 91
91
91
70-130
0
20
PyruvicAcid
mg/I
0
100
85 87
85
87
70-130
2.3
20
BulyricAcid
mg/I
0
100
96 94
96
94
70-130
2.1
20
Lactic Acid
mgil
0
100
110 120
113
115
70-130
1.8
20
Report ID: 10479 - 450376
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Microseeps.
''riplatc
Page 13 of 14

Microseeps
f
220 William Pitt Way
Pittsburgh, PA 15238
` t
R11Cf6SCCpS
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder: 10479 DOT STATESVILLE / 92177010
Lab ID
Sample ID
Prep Method Prep Batch Analysis Method
Analysis
Batch
104790001
DMW-6
AM21G
EDON/1902
104790002
DMW-7
AM21G
EDON/1902
104790003
DMW-10
AM21G
EDON/1902
104790004
DMW-9
AM21G
EDON/1902
104790005
DMW-11
AM21G
EDON/1902
104790006
DMW-8
AM21G
EDON11902
104790007
DMW-2
AM21G
EDON11902
104790008
DMW-1
AM21G
EDON/1902
Report ID: 10479 - 450376
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Microseeps.
Page 14 of 14

i7(
Chain of Custody
Workorder: 92177010 Workorder Name: DOT STATESVILLE Results Requested 11/4/2013
_ aceAnaljltical
Ya"Y.pacelab&com
.r,
Re{iort'((rivoice To r ,' '::Sulieonfract 7oY. , ;
.A ,�-y t' �- , r..11:+RegiiesteilrAnatysist
Kevin Godwin
Pace Analytical Charlotte i r '�
�C—
PO
9800 KinceyAve. Suite 100 D
Huntersville, NC 28078
Phone [phone]
n
Email: [e-mail]
S
1
:�'tP'te"seniedjiro'niafners;'x
•
+��s
J �'�
{�:Clt
-
gT
@
item
- a"fit . +.t
Samplo ID; �, ` + �.' .' yDaf�
b ID
a
LAB USE ONLY
1
DMW-6
10/23/2013 09:40
92177010001
Water
2
DMW-7
10/231201310:20
92177010002
Water
3
DMW-10
101231201311:00
92177010003
Water
4
DMW-9
10/231201311:40
92177010004
Water
5
DMW-11
10/23/201312:20
92177010005
Water
6
DMW-8
10/23/201313:15
92177010006
Water
7
DMW-2
10/2412013 07:15
92177010007
Water
8
DMW-1
10/24/2013 09:00
92177010008
Water
9
10
11
12
,. ... .. Comments
Transfers
Rel ased By
Date/Time
Received By
DateMirne
3
3
Cooler Temperature on Receipt OF CustodySeal
Y or N
Received on Ice Y or N samples Intact Y or N
FMT-ALL-C-002rev.00 24March2009 page 'i of i
Thursday, October 24, 2013 2:19:08 PM

Cooler Receipt Form
Client Name: Project: Dot t ���� r ���'L��i ab Work Order: z
A. Shipping/Container Information -(circle appropriate response) v
Courier: FedEx UPS LISPS Client Other: Air bill Present: Yes No
Tracking Number:
Custody Seal on Cooler/Box Present: Yes'. 'Z Seals Intact: Yes No
f
Cooler/Box Packing Material: ubble Wr' Absorbent Foam Other:
Type of Ice: Wet) Blue None Ice Intact:(Yes, Melted
Cooler Temperature: Radiation Screened: Ye oNoChain of Custody Presen : Yoe
Comments
B. Laboratory Assignment/Log-in-.(check appropriate response) - - - -
YES
NO
N/A
Comment -
Reference non -Conformance
Chain of Custody properly filled out
Chain of Custody relinquished
Sampler Name & Signature on CO
Containers intact
Were samples in separate bags
Sample container labels match COC
Sample name/date and time collected----
Sufficient volume provided
Microseeps containers used
Are containers properly preserved for the requested testing?
(as labeled) _
If an unknown preservation state, were containers checked?
Exception: VOA's coliform--- - -
✓
Af yes, see pH form.
Was volume for dissolved testing field filtered, as noted on
the COG? Was volume received in a preserved container?
Comments:
Cooler contents examined/received by : Z `yrr Date: `0169--IK f3
Project Manager Review Date: 1,9 /d;'3

aceAnalytical o
�nvw.pacelaos.com
(
February 10, 2014
Chemical Testing Engineer
NCDOT
Materials & Tests Unit
1801 Blue Ridge Road
Raleigh, NC 27607
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Dear Chemical Engineer:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 28, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
PCcft
REPORT OF LABORATORY ANALYSIS
r '
This report shall not be reproduced, except in full,
y
9gORAtp�
without the written consent of Pace Analytical Services, Inc..
Pagel of 37

acmnalytical
www.pacelabs.com
February 10, 2014
Page 2
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
cc: Mr. Stephen Libbey, Hart & Hickman
pCCRp0�
1Nf
9e�RA�pQ,
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�CGn n��in�' ® 205 East Meadow Road - Suite A 2225 Riverside Dr.
t eAn V Eden, NC 27288 Asheville, NC 28804
wwwpacelabs.com [phone] [phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
A2LA Certification #: 2926.01
Alabama Dept of Environmental Management #40770
Alaska Certification M UST-078
Alaska Certification #MN00064
Arizona Certification M AZ-0014
Arkansas Certification #: 88-0680
California Certification #: 01155CA
Colorado Certification #Pace
Connecticut Certification #: PH-0256
EPA Region 5 #WD-15J
EPA Region 8 Certification #: Pace
Florida/NELAP Certification #: E87605
Georgia Certification M 959
Hawaii Certification #Pace
Idaho Certification #: MN00064
Illinois Certification M 200011
Indiana Certification#C-MN-01
Iowa Certification M 368
Kansas Certification #: E-10167
Kentucky Dept of Envi. Protection - DW #90062
Louisiana Certification #: 03086
Louisiana Certification M LA080009
Maine Certification #: 2007029
Maryland Certification #: 322
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Michigan DEQ Certification #: 9909
Minnesota Certification #: 027-053-137
Mississippi Certification #: Pace
Montana Certification #: MT CERT0092
Nevada Certification #: MN00064
Nebraska Certification #: Pace
New Jersey Certification #: MN-002
New York Certification #: 11647
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North Dakota Certification #: R-036
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Oregon Certification M MN200001
Oregon Certification #: MN300001
Pennsylvania Certification M 68-00563
Puerto Rico Certification
Tennessee Certification #: 02818
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Utah Certification #: MN00064
Virginia/DCLS Certification #: 002521
Virginia/VELAP Certification #: 460163
Washington Certification #: C754
West Virginia Certification #: 382
Wisconsin Certification #: 999407970
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaIVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
i
l I
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical ® 205 East MeadoEden, NC 27288 Asheville, NC Riverside28804
www.pagelabs.com [phone] (828)2544176
SAMPLE ANALYTE COUNT
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92187846001
DMW-7
RSK 175
DI-1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
EWS
1
PASI-A
SM 5310B
SAE
1
PASI-A
92187846002
DMW-6
RSK 175
DI-1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
EWS
1
PASI-A
SM 531013
SAE
1
PASI-A
92187846003
DMW-10
RSK 175
DI-1
3
PASI-M
EPA6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
EWS
1
PASI-A
SM 531013
SAE
1
PASI-A
92187846004
DMW-9
RSK 175
DI-1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
EWS
1
PASI-A
SM 5310B
SAE
1
PASI-A
92187846005
DMW-11
RSK 175
DL1
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 37

i
aceAnalytical
www.pacelabs.com
I
i
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: DOT STATESVILLE 34613.3.26
i
Pace Project No.: 92187846
Lab ID Sample ID
92187846006 DMW-2
92187846007 DMW-1
92187846008 DMW-8
92187846009 TRIP
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
EPA 300.0
EPA 353.2
SM 5310B
RSK 175
EPA 6010
EPA 7470
SM 6200B
SM 4500-S2D
EPA 300.0
EPA 353.2
SM 5310B
RSK 175
EPA 6010
EPA 7470
SM 6200B
SM 4500-S2D
EPA 300.0
EPA 353.2
SM 5310E
RSK 175
EPA 6010
EPA 7470
SM 6200B
SM 4500-S2D
EPA 300.0
EPA 353.2
SM 5310B
SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analysts
Analytes
Reported
Laboratory
SAE
1
PASI-A
EWS
1
PASI-A
SAE
1
PASI-A
DL1
3
PASI-M
JMW
7
PASI-A
MTS
1
PASI-A
CAH
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
EWS
1
PASI-A
SAE
1
PASI-A
DL1
3
PASI-M
JMW
7
PASI-A
MTS
1
PASI-A
CAH
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
EWS
1
PASI-A
SAE
1
PASI-A
DL1
3
PASI-M
JMW
7
PASI-A
MTS
1
PASI-A
CAH
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
EWS
1
PASI-A
SAE
1
PASI-A
CAH
33
PASI-C
Page 5 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Analytical ®
205 East MeadoEden,
de Dr.
Suite
9800Huntersv
NC 272 8
Asheville, NC'28 04
Ile, NC28078
www.pacelabs.com
[phone]
[phone]
[phone]
ANALYTICAL RESULTS
Project: DOT STATESVILLE
34613.3.26
Pace Project No.: 92187846 .
Sample: DMW-7
Lab ID: 92187846001 Collected: 01/27/14 13:00
Received: 01/28/14 11:41
Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed
CAS No. Qua[
as
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
01/30/14 11:37
74-84-0
Ethene
ND ug/L
6.2
1
01/30/14 11:37
74-85-1 -
Methane
ND ug/L
6.6
1
01/30/14 11:37
74-82-8
6010 MET ICP
Analytical Method: EPA6010 Preparation Method: EPA3010
Arsenic
ND ug/L
10.0
1 01/29/1414:20
02/04/1419:10
7440-38-2
Barium
21.2 ug/L
5.0
1 01/29/1414:20
02/04/1419:10
7440-39-3
Cadmium
ND ug/L
1.0
1 01/29/1414:20
02/0411419:10
7440-43-9
Chromium
ND ug/L
5.0
1 01/29/1414:20
02/04/1419:10
7440-47-3
Lead
ND ug/L
5.0
1 01/29/1414:20
02/04/14 19:10
7439-92-1
Selenium
ND ug/L
10.0
1 01/29/1414:20
02/04/1419:10
7782-49-2
Silver
ND ug/L
5.0
1 01/29/1414:20
02/0411419.10
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1 01/29/14 19:00
01/31/14 20:37
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
01/29/14 22:27
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
01/29/14 22:27
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
01/29/14 22:27
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/29/14 22:27
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/29/14 22:27
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 22:27
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
01/29/14 22:27
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/29/14 22:27
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 22:27
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 22:27
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/29/14 22:27
75-27-4
Bromomethane
ND ug/L
5.0
1
01/29/14 22:27
74-83-9
Bromoform
ND ug/L
1.0
1
01/29/14 22:27
75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 22:27
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 22:27
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/29/14 22:27
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/29/14 22:27
108-90-7
Chloroethane
ND ug/L
1.0
1
01/29/14 22:27
75-00-3
Chloroform
ND ug/L
1.0
1
01/29/14 22:27
67-66-3
Chloromethane
ND ug/L
1.0
1
01/29/14 22:27
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/29/14 22:27
124-48-1 j
Dichlorodifluoromethane
ND ug/L
1.0
1
01/29/14 22:27
75-71-8 `
Methylene Chloride
ND ug/L
2.0
1
01/29/14 22:27
75-09-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 22:27
156-60-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 22:27
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/29/14 22:27
127-18-4 -
Trichloroethene
ND ug/L
1.0
1
01/29/14 22:27
79-01-6 _
Trichlorofluoromethane
ND ug/L
1.0
1
01/29/14 22:27
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/29/14 22:27
75-01-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 02/10/2014 03:24 PM
without the written consent of Pace Analytical Services, Inc..
Page 6 of 37

aceAnalytical
- www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Sample: DMW-7
Lab ID: 92187846001 Collected:
01/27/14 13:00
Received: 01/28/14 11:41 Matrix:
Water
Parameters
Results Units Report
Limit
DF
Prepared Analyzed
CAS No. Qua[
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane(EDB)
ND ug/L
1.0
1
01/29/14 22:27
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
01/29/14 22:27
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
01/29/14 22:27
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
01/29/14 22:27
2037-26-5
4500S21) Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
02/03/1416:17
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
3.8 mg/L
2.0
1
02/05/14 01:06
14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.58 mg/L
0.020
1
01/29/14 08:59
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
2.4 mg/L
1.0
1
02/04/14 14:40
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 37
I

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Sample: DMW-6 Lab ID: 92187846002 Collected: 01/27/14 13:45 Received: 01/28/14 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
7.0 ug/L
6.2
1
01/30/1411:56
74-84-0
Ethene
ND ug/L
6.2
1
01/30/1411:56
74-85-1
Methane
49.4 ug/L
6.6
1
01/30/14 11:56
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1 01/29/1414:20
02/04/1419:13
7440-38-2
Barium
195 ug/L
5.0
1 01/29/1414:20
02/04/1419:13
7440-39-3
Cadmium
ND ug/L
1.0
1 01/29/1414:20
02/04/1419:13
7440-43-9
Chromium
35.7 ug/L
5.0
1 01/29/1414:20
02/04/1419:13
7440-47-3
Lead
10.6 ug/L
5.0
1 01/29/14 14:20
02/04/14 19:13
7439-92-1
Selenium
ND ug/L
10.0
1 01/29/1414:20
02/04/1419:13
7782-49-2
Silver
ND ug/L
5.0
1 01/29/1414:20
02/04/1419:13
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1 01/29/14 19:00
'01/31/14 20:40
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
50.9 ug/L
1.0
1
01/30/14 02:52
75-34-3
1,1-Dichloroethene
73.2 ug/L
1.0
1
01/30/14 02:52
75-35-4
1, 1, 1 -Trichloroethane
3.6 ug/L
1.0
1
01/30/14 02:52
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/30/14 02:52
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/30/14 02:52
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 02:52
95-50-1
1,2-Dichloroethane
1.2 ug/L
1.0
1
01/30/14 02:52
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/30/14 02:52
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 02:52
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 02:52
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/30/14 02:52
75-27-4
Bromomethane
ND ug/L
5.0
1
01/30/14 02:52
74-83-9
Bromoform
ND ug/L
1.0
1
01/30/14 02:52
75-25-2
cis-1,2-Dichloroethene
3.5 ug/L
1.0
1
01/30/14 02:52
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
01/30/14 02:52
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/30/14 02:52
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/30/14 02:52
108-90-7
Chloroethane
ND ug/L
1.0
1
01/30/14 02:52
75-00-3
Chloroform
ND ug/L
1.0
1
01/30/14 02:52
67-66-3
Chloromethane
ND ug/L
1.0
1
01/30/14 02:52
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/30/14 02:52
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
01/30/14 02:52
75-71-8
Methylene Chloride
ND ug/L
2.0
1
01/30/14 02:52
75-09-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
01/30/14 02:52
156-60-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
01/30/14 02:52
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/30/14 02:52
127-18-4
Trichloroethene
62.5 ug/L
1.0
1
01/30/14 02:52
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
01/30/14 02:52
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/30/14 02:52
75-01-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 02/10/2014 03:24 PM
without the written consent of Pace Analytical Services, Inc..
Page 8 of 37

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Sample: DMW-6
Lab ID: 92187846002 Collected:
01/27/14 13:45
Received: 01/28/14 11:41 Matrix: Water
Parameters
Results Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
01/30/14 02:52
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
01/30/14 02:52
460-00-4
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
01/30/14 02:52
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
01/30/14 02:52
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
02/03/1416:17
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
58.2 mg/L
10.0
5
02/05/14 01:38
14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA353.2
Nitrogen, Nitrate
0.54 mg/L
0.020
1
01/29/14 09:09
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
17.1 mg/L
2.0
2
02/05/14 10:42
7440-44-0
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical ® 205 East Meadow Road - Suite 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
www.pacelabs.com [phone] [phone]
ANALYTICAL RESULTS
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-10 Lab ID: 92187846003 Collected: 01/27/14 14:30 Received: 01/28/14 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
01/30/1412:06
74-84-0
Ethene
ND ug/L
6.2
1
01/30/1412:06
74-85-1
Methane
ND ug/L
6.6
1
01/30/1412:06
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
01/29/1414:20
02/04/1419:16
7440-38-2
Barium
141 ug/L
5.0
1
01/29/1414:20
02/04/1419:16
7440-39-3
Cadmium
ND ug/L
1.0
1
01/29/1414:20
02/04/1419:16
7440-43-9
Chromium
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:16
7440-47-3
Lead
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:16
7439-92-1
Selenium
ND ug/L
10.0
1
01/29/1414:20
02/04/1419:16
7782-49-2
Silver
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:16
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
01/29/14 19:00
01/31/14 20:43'
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
01/29/14 22:44
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
01/29/14 22:44
75-35-4
1, 1, 1 -Trichloroethane
ND ug/L
1.0
1
01/29/14 22:44
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/29/14 22:44
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/29/14 22:44
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 22:44
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
01/29/14 22:44
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/29/14 22:44
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 22:44
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 22:44
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/29/14 22:44
75-27-4
Bromomethane
ND ug/L
5.0
1
01/29/14 22:44
74-83-9
Bromoform
ND ug/L
1.0
1
01/29/14 22:44
75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 22:44
156-59-2
cis- 1, 3-Dichloropropene
ND ug/L
1.0
1
01/29/14 22:44
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/29/14 22:44
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/29/14 22:44
108-90-7
Chloroethane
ND ug/L
1.0
1
01/29/14 22:44
75-00-3
Chloroform
ND ug/L
1.0
1
01/29/14 22:44
67-66-3
Chloromethane
ND ug/L
1.0
1
01/29/14 22:44
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/29/14 22:44
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
01/29/14 22:44
75-71-8
Methylene Chloride
ND ug/L
2.0
1
01/29/14 22:44
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 22:44
156-60-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 22:44
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/29/14 22:44
127-18-4
Trichloroethene
ND ug/L
1.0
1
01/29/14 22:44
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
01/29/14 22:44
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/29/14 22:44
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 37

1 �
aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
li
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Sample: DMW-10
I
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, N021NO3 unpres
Nitrogen, Nitrate
5310B TOC
Total Organic Carbon
i
Date: 02/10/2014 03:24 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 92187846003 Collected:
01/27/14 14:30
Received: 01/28/14 11:41 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
Analytical Method: SM 6200B
ND ug/L
1.0
1
01/29/14 22:44
106-93-4
99 %
70-130
1
01/29/14 22:44
460-00-4
98 %
70-130
1
01/29/14 22:44
17060-07-0
101 %
70-130
1
01/29/14 22:44
2037-26-5
Analytical Method: SM 4500-S2D
ND mg/L
0.10
1
02/03/1416:17
18496-25-8
Analytical Method: EPA 300.0
20.8 mg/L
2.0
1
02/05/14 16:52
14808-79-8
Analytical Method: EPA 353.2
ND mg/L
0.020
1
01/29/14 09:10
Analytical Method: SM 5310B
21.6 mg/L
1.0
1
02/04/14 15:23
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qua[
Page 11 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 205 East Meadow Road - Suite A 2225 Riverside Dr.
acmnalytical Eden, NC 27288 Asheville, NC 28804
www.pacelabs.com [phone] [phone]
ANALYTICAL RESULTS
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-9 Lab ID: 92187846004 Collected: 01/27/14 15:15 Received: 01/28/14 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 176 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
01/30/1412:16
74-84-0
Ethene
ND ug/L
6.2
1
01/30/1412:16
74-85-1
Methane
116 ug/L
6.6
1
01/30/1412:16
74-82-8
6010 MET ICP
Analytical Method: EPA6010 Preparation Method: EPA3010
Arsenic
ND ug/L
10.0
1
01/29/1414:20
02/04/1419:19
7440-38-2
Barium
82.0 ug/L
5.0
1
01/29/1414:20
02/04/1419:19
7440-39-3
Cadmium
ND ug/L
1.0
1
01/29/1414:20
02/04/1419:19
7440-43-9
Chromium
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:19
7440-47-3
Lead
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:19
7439-92-1
Selenium
ND ug/L
10.0
1
01/29/1414:20
02/04/1419:19
7782-49-2
Silver
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:19
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
01/29/14 19:00
01/31/14 20:45
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
2.6 ug/L
1.0
1
01/29/14 23:00
75-34-3
1,1-Dichloroethene
1.9 ug/L
1.0
1
01/29/14 23:00
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
01/29/14 23:00
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/29/14 23:00
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/29/14 23:00
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:00
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
01/29/14 23:00
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/29/14 23:00
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:00
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:00
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/29/14 23:00
75-27-4
Bromomethane
ND ug/L
5.0
1
01/29/14 23:00
74-83-9
Bromoform
ND ug/L
1.0
1
01/29/14 23:00
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 23:00
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 23:00
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/29/14 23:00
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/29/14 23:00
108-90-7
Chloroethane
ND ug/L
1.0
1
01/29/14 23:00
75-00-3
Chloroform
ND ug/L
1.0
1
01/29/14 23:00
67-66-3
Chloromethane
ND ug/L
1.0
1
01/29/14 23:00
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/29/14 23:00
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
01/29/14 23:00
75-71-8
Methylene Chloride
ND ug/L
2.0
1
01/29/14 23:00
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 23:00
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 23:00
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/29/14 23:00
127-18-4
Trichloroethene
2.9 ug/L
1.0
1
01/29/14 23:00
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
01/29/14 23:00
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/29/14 23:00
75-01-4
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalytical Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
www.pacelabs.com [phone] [phone] [phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Sample: DMW-9
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
5310E TOC
Total Organic Carbon
I
Date: 02/10/2014 03:24 PM
ANALYTICAL RESULTS
Lab ID: 92187846004 Collected: 01/27/14 15:15
Results Units Report Limit DF
Received: 01/28/14 11:41 Matrix: Water
Prepared Analyzed CAS No. Qua[
Analytical Method: SM 6200B
ND ug/L
1.0
1
01/29/14 23:00
106-93-4
99 %
70-130
1
01/29/14 23:00
460-00-4
99 %
70-130
1
01/29/14 23:00
17060-07-0
101 %
70-130
1
01/29/14 23:00
2037-26-5
Analytical Method: SM 4500-S2D
ND mg/L
0.50
1
02/03/1416:17 18496-25-8 D3
Analytical Method: EPA 300.0
71.3 mg/L
10.0
5
02/05/14 03:48 14808-79-8
Analytical Method: EPA 353.2
1.5 mg/L
0.020
1
01/29/14 09:11
Analytical Method: SM 5310B
5.6 mg/L
1.0
1
02/04/14 15:35 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 37

acmnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
r�
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]--
i
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
i
Sample: DMW-11 Lab ID: 92187846005 Collected: 01/28/14 09:00 Received: 01/28/14 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
01/30/1412:25
74-84-0
Ethene
ND ug/L
6.2
1
01/30/1412:25
74-85-1
Methane
3790 ug/L
6.6
1
01/30/1412:25
74-82-8
6010 MET ICP
Analytical Method: EPA6010 Preparation Method: EPA3010
Arsenic
ND ug/L
10.0
1
01/29/14 14:20
02/04/1419:22
7440-38-2
Barium
66.5 ug/L
5.0
1
01/29/14 14:20
02/04/1419:22
7440-39-3
Cadmium
ND ug/L
1.0
1
01/29/14 14:20
02/04/1419:22
7440-43-9
Chromium
ND ug/L
5.0
1
01/29/14 14:20
02/04/1419:22
7440-47-3
Lead
ND ug/L
5.0
1
01/29/14 14:20
02/04/1419:22
7439-92-1
Selenium
ND ug/L
10.0
1
01/29/14 14:20
02/04/1419:22
7782-49-2
Silver
ND ug/L
5.0
1
01/29/14 14:20
02/04/1419:22
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20 '
1
01/29/14 19:00
01/31/14 20:48
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
6.8 ug/L
1.0
1
01129/1423:17
75-34-3
1,1-Dichloroethene
9.5 ug/L
1.0
1
01/29/14 23:17
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
01/29/14 23:17
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/29/14 23:17
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/29/14 23:17
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:17
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
01/29/14 23:17
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/29/14 23:17
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:17
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:17
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/29/14 23:17
75-27-4
Bromomethane
ND ug/L
5.0
1
01/29/14 23:17
74-83-9
Bromoform
ND ug/L
1.0
1
01/29/14 23:17
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 23:17
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 23:17
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/29/14 23:17
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/29/14 23:17
108-90-7
Chloroethane
ND ug/L
1.0
1
01/29/14 23:17
75-00-3
Chloroform
ND ug/L
1.0
1
01/29/14 23:17
67-66-3
Chloromethane
ND ug/L
1.0
1
01/29/14 23:17
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/29/14 23:17
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
01/29/14 23:17
75-71-8
Methylene Chloride
ND ug/L
2.0
1
01/29/14 23:17
75-09-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 23:17
156-60-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 23:17
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/29/14 23:17
127-18-4
Trichloroethene
8.1 ug/L
1.0
1
01/29/14 23:17
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
01/29/14 23:17
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/29/14 23:17
75-01-4
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 37 -
I
i

- aceAnalytical
— www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: DOT STATESVILLE 34613.3.26
j Pace Project No.: 92187846
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-11
Lab ID: 92187846005 Collected:
01/28/14 09:00
Received: 01/28/14 11:41 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
601 Volatiles by SM 6200,
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND 1
1.0
1
01/29/14 23:17
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
01/29/14 23:17
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
01/29/14 23:17
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
01/29/14 23:17
2037-26-5
4500S2D Sulfide Water
Analytical D
Method: SM 4500 S2
Sulfide
ND 11
0.10
1
02/03/1416:17
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
108 mg/L
10.0
5
02/05/14 04:20
14808-79-8
353.2 Nitrogen, NO2/i unpres
Analytical Method: EPA353.2
Nitrogen, Nitrate
ND ni
0.020
1
01/29/14 12:13
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
23.4 11
1.0
1
02/04/14 15:46
7440-44-0
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 15 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow
de Dr.
® Eden, NC 272 8 Asheville, lle, NC 1 acmnalytical 28804
www.pacelabs.com [phone] [phone]
ANALYTICAL RESULTS
Project: DOT STATESVILLE 34613.3.26
Pace Project No.:. 92187846
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone] I
i I
Sample: DMW-2 Lab ID: 92187846006 Collected: 01/28/14 09:35 Received: 01/28/14 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
01/30/14 12:35
74-84-0
Ethene
ND ug/L
6.2
1
01/30/14 12:35
74-85-1
Methane
61.9 ug/L
6.6
1
01/30/14 12:35
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
01/29/1414:20
02/04/1419:25
7440-38-2
Barium
28.2 ug/L
5.0
1
01/29/1414:20
02/04/1419:25
7440-39-3
Cadmium
1.0 ug/L
1.0
1
01/29/1414:20
02/04/1419:25
7440-43-9
Chromium
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:25
7440-47-3
Lead
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:25
7439-92-1
Selenium
ND ug/L
10.0
1
01/29/1414:20
02/04/1419:25
7782-49-2
Silver
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:25
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
01/29/14 19:00
01/31/14 20:50
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
1.3 ug/L
1.0
1
01/29/14 23:33
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
01/29/14 23:33
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
01/29/14 23:33
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/2911423:33
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/29/14 23:33
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:33
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
01/29/14 23:33
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/29/14 23:33
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:33
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:33
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/29/14 23:33
75-27-4
Bromomethane
ND ug/L
5.0
1
01/29/14 23:33
74-83-9
Bromoform
ND ug/L
1.0
1
01/29/14 23:33
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
01129/1423:33
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 23:33
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/29/14 23:33
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/29/14 23:33
108-90-7
Chloroethane
ND ug/L
1.0
1
01/29/14 23:33
75-00-3
Chloroform
ND ug/L
1.0
1
01/29/14 23:33
67-66-3
Chloromethane
ND ug/L
1.0
1
01/29/14 23:33
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/29/14 23:33
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
01/29/14 23:33
75-71-8
Methylene Chloride
ND ug/L
2.0
1
01/29/14 23:33
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 23:33
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 23:33
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/29/14 23:33
127-18-4
Trichloroethene
ND ug/L
1.0
1
01/29/14 23:33
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
01/29/14 23:33
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/29/14 23:33
75-01-4
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 37

aceAnaljftal
www.pagelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
,
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: DMW-2
Lab ID: 92187846006 Collected:
01/28/14 09:35
Received: 01/28/14 11:41 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane(EDB)
ND ug/L
1.0
1
01/29/14 23:33
106-93-4
_ Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
01/29/14 23:33
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
01/29/14 23:33
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
01/29/14 23:33
2037-26-5
4500S21D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
02/03/1416:17
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
79.1 mg/L
10.0
5
02/05/14 04:53
14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA353.2
Nitrogen, Nitrate
3.7 mg/L
0.020
1
01/29/14 12:14
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
7.0 mg/L
1.0
1
02/04/14 15:56
7440-44-0
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 17 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
aceAnalyticai
Eden, NC 27288 Asheville, NC 28804
www.pacelabs.com [phone] [phone]
ANALYTICAL RESULTS
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
i
Sample: DMW-1 Lab ID: 92187846007 Collected: 01/28/14 10:10 Received: 01/28/14 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 176 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
01/3011412:45
74-84-0
Ethene
ND ug/L
6.2
1
01/30/1412:45
74-85-1
Methane
15.4 ug/L
6.6
1
01/30/1412:45
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
01/2911414:20
02/0411419:28
7440-38-2
Barium
60.2 ug/L
5.0
1
01/29/1414:20
02/04/1419:28
7440-39-3
Cadmium
ND ug/L
1.0
1
01/29/1414:20
02/04/1419:28
7440-43-9
Chromium
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:28
7440-47-3
Lead
ND ug/L
5.0
1
01/29/1414:20
02104/1419:28
7439-92-1
Selenium
ND ug/L
10.0
1
01/29/1414:20
02/04/1419:28
7782-49-2
Silver
ND ug/L
5.0
1
01/29/1414:20
02104/1419:28
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
' ND ug/L
0.20
1
01/29/14 19:00
01/31/14 20:53
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
4.5 ug/L
1.0
1
01129/1423:50
75-34-3
1,1-Dichloroethene
1.5 ug/L
1.0
1
01/29/14 23:50
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
01/29/14 23:50
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/29/14 23:50
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/29/14 23:50
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:50
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
01129/1423:50
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/29/14 23:50
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:50
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/29/14 23:50
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/29/14 23:50
75-27-4
Bromomethane
ND ug/L
5.0
1
01/29/14 23:50
74-83-9
Bromoform
ND ug/L
1.0
1
01/29/14 23:50
75-25-2
cis-1,2-Dichloroethene
3.3 ug/L
1.0
1
01/29/14 23:50
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 23:50
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/29/14 23:50
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/29/14 23:50
108-90-7
Chloroethane
ND ug/L
1.0
1
01/29/14 23:50
75-00-3
Chloroform
ND ug/L
1.0
1
01/29/14 23:50
67-66-3
Chloromethane
ND ug/L
1.0
1
01/29/14 23:50
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/29/14 23:50
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
01/29/14 23:50
75-71-8
Methylene Chloride
ND ug/L
2.0
1
01/29/14 23:50
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
01/29/14 23:50
156-60-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
01/29/14 23:50
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/29/14 23:50
127-18-4
Trichloroethene
3.0 ug/L
1.0
1
01/29/14 23:50
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
01/29/14 23:50
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/29/14 23:50
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc..
Page 18 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
RCG nna'�Inal® 205 East MeadoEden, NC 27288 Asheville, NC 128 04 9800Hunte sville, NC128078
— www.pacelabs.com [phone] [phone] [phone]
ANALYTICAL RESULTS
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Sample: DMW-1
Parameters
Lab ID: 92187846007 Collected: 01/28/14 10:10
Results Units Report Limit DF
Received: 01/28/14 11:41 Matrix: Water
Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane(EDB)
ND ug/L
1.0
1
01/29/14 23:50
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
01/29/14 23:50
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
01/29/14 23:50
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
01/29/14 23:50
2037-26-5
4500S213 Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
02/03/1416:17
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
4.6 mg/L
2.0
1
02/05/14 05:25
14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.23 mg/L
0.020
1
01/29/14 13:47
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
5.5 mg/L
1.0
1
02/04/14 16:30
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
aceAnalytical
Eden, NC 27288 Asheville, NC 28804
www.pacelabs.com [phone] [phone]
ANALYTICAL RESULTS
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
I
Sample: DMW-8 Lab ID: 92187846008 Collected: 01/28/14 11:00 Received: 01/28/14 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
01/30/1412:55
74-84-0
Ethene
ND ug/L
6.2
1
01/30/1412:55
74-85-1
Methane
ND ug/L
6.6
1
01/30/1412:55
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
01/2911414:20
02/0411419:32
7440-38-2
Barium
33.6 ug/L
5.0
1
01/29/1414:20
02/04/1419:32
7440-39-3
Cadmium
ND ug/L
1.0
1
01/29/1414:20
02/04/1419:32
7440-43-9
Chromium
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:32
7440-47-3
Lead
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:32
7439-92-1
Selenium
ND ug/L
10.0
1
01/29/1414:20
02/04/1419:32
7782-49-2
Silver
ND ug/L
5.0
1
01/29/1414:20
02/04/1419:32
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
01/29/14 19:00
01/31/14 21:01
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
01/30/14 00:06
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
01/30/14 00:06
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
01/30/14 00:06
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/30/14 00:06
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/30/14 00:06
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 00:06
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
01/30/14 00:06
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/30/14 00:06
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 00:06
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 00:06
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/30/14 00:06
75-27-4
Bromomethane
ND ug/L
5.0
1
01/30/14 00:06
74-83-9
Bromoform
ND ug/L
1.0
1
01/30/14 00:06
75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
01/30/14 00:06
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
01/30/14 00:06
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/30/14 00:06
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/30/14 00:06
108-90-7
Chloroethane
ND ug/L
1.0
1
01/30/14 00:06
75-00-3
Chloroform
ND ug/L
1.0
1
01/30/14 00:06
67-66-3
Chloromethane
ND ug/L
1.0
1
01/30/14 00:06
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/30/14 00:06
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
01/30/14 00:06
75-71-8
Methylene Chloride
ND ug/L
2.0
1
01/30/14 00:06
75-09-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
01/30/14 00:06
156-60-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
01/30/14 00:06
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/30/14 00:06
127-18-4
Trichloroethene
ND ug/L
1.0
1
01/30/14 00:06
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
01/30/14 00:06
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/30/14 00:06
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc..
Page 20 of 37

I
aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Sample: DMW-8
Lab ID: 92187846008 Collected:
01/28/14 11:00
Received: 01/28/14 11:41 Matrix: Water
Parameters
Results Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
01/30/14 00:06
106-93-4
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
01/30/14 00:06
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
01/30/14 00:06
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
01/30/14 00:06
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S21D
Sulfide
ND mg/L
0.10
1
02103/1416:17
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
3.0 mg/L
2.0
1
02/05/14 05:57
14808-79-8
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA353.2
Nitrogen, Nitrate
0.88 mg/L
0.020
1
01/29/14 13:49
631013 TOC
Analytical Method: SM 5310B
Total Organic Carbon
I f
4
2.1 mg/L
1.0
1
02/04/14 16:41
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 37

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Sample: TRIP Lab ID: 92187846009 Collected: 01/27/14 00:00 Received: 01/28/14 11:41 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
601 Volatiles by SM 6200 Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
01/30/14 00:23
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
01/30/14 00:23
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
01/30/14 00:23
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
01/30/14 00:23
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
01/30/14 00:23
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 00:23
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
01/30/14 00:23
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
01/30/14 00:23
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 00:23
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
01/30/14 00:23
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
01/30/14 00:23
75-27-4
Bromomethane
ND ug/L
5.0
1
01/30/14 00:23
74-83-9
Bromoform
ND ug/L
1.0
1
01/30/14 00:23
75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
01/30/14 00:23
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
01/30/14 00:23
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
01/30/14 00:23
56-23-5
Chlorobenzene
ND ug/L
1.0
1
01/30/14 00:23
108-90-7
Chloroethane
ND ug/L
1.0
1
01/30/14 00:23
75-00-3
Chloroform
ND ug/L
1.0
1
01/30/14 00:23
67-66-3
Chloromethane
ND ug/L
1.0
1
01/30/14 00:23
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
01/30/14 00:23
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
01/30/14 00:23
75-71-8
Methylene Chloride
ND ug/L
2.0
1
01/30/14 00:23
75-09-2
trans- 1,2-Dichloroethene
ND ug/L
1.0
1
01/30/14 00:23
156-60-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
1
01/30/14 00:23
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
01/30/14 00:23
127-18-4
Trichloroethene
ND ug/L
1.0
1
01/30/14 00:23
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
01/30/14 00:23
75-69-4
Vinyl chloride
ND ug/L
1.0
1
01/30/14 00:23
75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
01/30/14 00:23
106-93-4
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
01/30/14 00:23
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
01/30/14 00:23
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
01/30/14 00:23
2037-26-5
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 22 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
-- w 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
aceAnalytical Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
www.pacelabs.com [phone] [phone] [phone]
i
QUALITY CONTROL DATA
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187946
QC Batch: AIR/19319 Analysis Method: RSK 175
QC Batch Method: RSK 175 Analysis Description: RSK 175 AIR HEADSPACE
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008
METHOD BLANK: 1617728
Matrix: Water
Associated Lab Samples:
92187846001, 92187846002, 92187846003, 92187846004, 92187846005,
92187846006, 92187846007,
92187846008
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Ethane
ug/L
ND 6.2
01/30/1411:19
Ethene
ug/L
ND 6.2
01/30/1411:19
Methane
ug/L
ND 6.6
01/30/1411:19
LABORATORY CONTROL SAMPLE & LCSD: 1617729
1617730
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec % Rec
Limits RPD RPD
Ethane
ug/L
114
107 104
94 91
85-115 3 .20
Ethene
ug/L
106
99.4 97.2
94 92
85-115 2 20
Methane
ug/L
60.7
56.5 55.6
93 92
85-115 2 20
SAMPLE DUPLICATE. 1617731
Parameter
Ethane
Ethene
Methane
Date: 02/10/2014 03:24 PM
92187846001 Dup
Units Result Result
ug/L ND ND
ug/L ND ND
ug/L ND 4.1J
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 23 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
de Dr.
aceAnalytical ® 205 East MeadoEden, NC 27288 Asheville, NC'28 04
www.pacelabs.com [phone] [phone]
QUALITY CONTROL DATA
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
�I
i
QC Batch: MERP/6120 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 921.87846007, i
92187846008
METHOD BLANK: 1129910 Matrix: Water
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 01/31/14 21:57
LABORATORY CONTROL SAMPLE: 1129911
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.4 97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1129912 1129913
MS MSD
92187753003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.2 2.2 86 86 75-125 .0
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 24 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Kincey Ave.
te 100
5a?neAnalXical ® 205 East MeadoEden, NC 272 8 Asheville, NC Riverside28804 9800Huntersville, NC1280778
www.pacelabs.com [phone] [phone] [phone]
QUALITY CONTROL DATA
1
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
QC Batch: MPRP/15153 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008
METHOD BLANK: 1129633
Matrix: Water
P i Associated Lab Samples:
92187846001, 92187846002, 92187846003, 92187846004, 92187846005,
92187846006, 92187846007,
92187846008
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
ug/L
ND
10.0
02/04/1418:42
Barium
ug/L
ND
5.0
02/04/1418:42
Cadmium
ug/L
ND
1.0
02/04/1418:42
Chromium
ug/L
ND
5.0
02/04/1418:42
Lead
ug/L
ND
5.0
02/04/1418:42
Selenium
ug/L
ND
10.0
02/04/1418:42
Silver
ug/L
ND
5.0
02104/1418:42
LABORATORY CONTROL SAMPLE:
1129634
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Arsenic
ug/L
500
501
100
80-120
Barium
ug/L
500
512
102
80-120
Cadmium
ug/L
500
506
101
80-120
Chromium
ug/L
500
513
103
80-120
Lead
ug/L
500
511
102
80-120
Selenium
ug/L
500
508
102
80-120
Silver
ug/L
250
256
102
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1129635 1129636
MS MSD
92187845001 Spike Spike MS MSD
MS
MSD
% Rec
Parameter
Units
Result Cone. Cone. Result Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
ug/L
ND 500 500 328 321
64
62
75-125
2 M1
Barium
ug/L
2390 500 500 3120 3040
145
129
75-125
3 M1
Cadmium
ug/L
1.6 500 500 440 441
88
88
75-125
0
—' Chromium
uglL
50.4 500 500 506 506
91
91
75-125
0
Lead
ug/L
49.1 500 500 488 484
88
87
75-125
1
Selenium
ug/L
ND 500 500 259 248
52
50
75-125
4 M1
Silver
ug/L
ND 250 250 225 226
90
91
75-125
1
i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM
without the written consent of Pace Analytical Services, Inc..
Page 25 of 37

aceAnalytical
wmpacelabs.00m
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone] i
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
QC Batch: MSV/25645 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 601 by 6200B
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008,92187846009
METHOD BLANK: 1129754 Matrix: Water
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008,92187846009
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1,1-Trichloroethane
ug/L
ND
1.0
01/29/14 22:10
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
01/29/14 22:10
1,1,2-Trichloroethane
ug/L
ND
1.0
01/29/14 22:10
1,1-Dichloroethane
ug/L
ND
1.0
01/29/14 22:10
1,1-Dichloroethene
ug/L
ND
1.0
01/29/14 22:10
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
01/29/14 22:10
1,2-Dichlorobenzene
ug/L
ND
1.0
01/29/14 22:10
1,2-Dichloroethane
ug/L
ND
1.0
01/29/14 22:10
1,2-Dichloropropane
ug/L
ND
1.0
01/29/14 22:10
1,3-Dichlorobenzene
ug/L
ND
1.d
01/29/14 22:10
1,4-Dichlorobenzene
ug/L
ND
1.0
01/29/14 22:10
Bromodichloromethane
ug/L
ND
1.0
01/29/14 22:10
Bromoform
ug/L
ND
1.0
01/29/14 22:10
Bromomethane
ug/L
ND
5.0
01/29/14 22:10
Carbon tetrachloride
ug/L
ND
1.0
01/29/14 22:10
Chlorobenzene
ug/L
ND
1.0
01/29/14 22:10
Chloroethane
ug/L
ND
1.0
01/29/14 22:10
Chloroform
ug/L
ND
1.0
01/29/14 22:10
Chloromethane
ug/L
ND
1.0
01/29/14 22:10
cis- 1,2-Dichloroethene
ug/L
ND
1.0
01/29/14 22:10
cis- 1,3-Dichloropropene
ug/L
ND
1.0
01/29/14 22:10
Dibromochloromethane
ug/L
ND
1.0
01/29/14 22:10
Dichlorodifluoromethane
ug/L
ND
1.0
01/29/14 22:10
Methylene Chloride
ug/L
ND
2.0
01/29/14 22:10
Tetrachloroethene
ug/L
ND
1.0
01/29/14 22:10
trans-1,2-Dichloroethene
ug/L
ND
1.0
01/29/14 22:10
trans- 1,3-Dichloropropene
ug/L
ND
1.0
01/29/14 22:10
Trichloroethene
ug/L
ND
1.0
01/29/14 22:10
Trichlorofluoromethane
ug/L
ND
1.0
01/29/14 22:10
Vinyl chloride
ug/L
ND
1.0
01/29/14 22:10
1,2-Dichloroethane-d4 (S)
%
99
70-130
01/29/14 22:10
4-Bromofluorobenzene (S)
%
100
70-130
01/29/14 22:10
Toluene-d8 (S)
%
100
70-130
01/29/14 22:10
LABORATORY CONTROL SAMPLE: 1129755
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 50 47.9 96 60-140
1,1,2,2-Tetrachloroethane ug/L 50 47.3 95 60-140
1,1,2-Trichloroethane ug/L 50 49.4 99 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc.. Page 26 of 37

aceAnal�/tical
J`
wwwpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
LABORATORY CONTROL SAMPLE:
1129755
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,1-Dichloroethane
ug/L
50
44.9
90
60-140
1,1-Diehl oroethene
ug/L
50
44.1
88
60-140
1,2-Dibromoethane (EDB)
ug/L
50
49.5
99
60-140
1,2-Dichlorobenzene
ug/L
50
47.0
94
60-140
1,2-Dichloroethane
ug/L
50
46.0
92
60-140
1,2-Dichloropropane
ug/L
50
47.8
96
60-140
1,3-Dichlorobenzene
ug/L
50
45.6
91
60-140
1,4-Dichlorobenzene
ug/L
50
45.9
92
60-140
Bromodichloromethane
ug/L
50
52.3
105
60-140
Bromoform
ug/L
50
53.7
107
60-140
Bromomethane
ug/L
50
53.2
106
60-140
Carbon tetrachloride
ug/L
50
52.5
105
60-140
Chlorobenzene
ug/L
50
47.8
96
60-140
Chloroethane
ug/L
50
47.0
94
60-140
Chloroform
ug/L
50
46.6
93
60-140
Chloromethane
ug/L
50
42.0
84
60-140
cis-1,2-Dichloroethene
ug/L
50
45.8
92
60-140
cis- 1,3-Dichloropropene
ug/L
50
53.9
108
60-140
Dibromochloromethane
ug/L
50
52.5
105
60-140
Dichlorodifluoromethane
ug/L
50
42.2
84
60-140
Methylene Chloride
ug/L
50
44.8
90
60-140
Tetrachloroethene
ug/L
50
47.4
95
60-140
trans-1,2-Dichloroethene
ug/L
50
43.7
87
60-140
trans-1,3-Dichloropropene
ug/L
50
56.1
112
60-140
Trichloroethene
ug/L
50
47.7
95
60-140
Trichlorofluoromethane
ug/L
50
45.5
91
60-140
Vinyl chloride
ug/L
50
46.5
93
60-140
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
101
70-130
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 27 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalyficai ® 205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
www.pacelabs.com [phone] [phone]
QUALITY CONTROL DATA
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: WET/29362 Analysis Method: SM 4500-S2D
QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008
METHOD BLANK: 1131620 Matrix: Water
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide mg/L
ND 0.10
02/03/1416:17
LABORATORY CONTROL SAMPLE: 1131621
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Rec
Limits Qualifiers
Sulfide mg/L
.5
0.53
106
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1131622
1131623
MS
MSD
92187846001
Spike
Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Conc.
Conc. Result
Result
% Rec % Rec Limits RPD Qual
Sulfide mg/L ND
.5
.5 0.54
0.54
107 107 75-125 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1131624 1131625
MS MSD
92187986002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfide mg/L ND .5 .5 0.46 0.46 92 92 75-125 0
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 28 of 37

I
- aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
QC Batch: WETA/17949 Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008
METHOD BLANK: 1131604 Matrix: Water
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 2.0 02/04/1414:17
LABORATORY CONTROL SAMPLE: 1131605
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate mg/L 20 20.8 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1131606 1131607
MS MSD
92186894001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 79.6 20 20 99.2 106 98 130 90-110 6 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1131614 1131615
MS MSD
92187383001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Sulfate mg/L 3120J 20 20 21.2 19.8 90 84 90-110 6 M1
ug/L
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 29 of 37

ace Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA/17900 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004
METHOD BLANK: 1129439 Matrix: Water
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.020 01/29/14 08:39
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1129440
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 2.5 2.6 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1129441 1129442
MS MSD
92187795001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD
Nitrogen, Nitrate mg/L 0.64 2.5 2.5 3.2 3.2 102 101 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1129443 1129444
MS MSD
92187799001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD
Nitrogen, Nitrate mg/L ND 2.5 2.5 2.6 2.6 104 103 90-110 1
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Qual
i
I
Page 30 of 37

�5aneAnalyticalo
wwvw.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
i
QC Batch: WETA/17902 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92187846005, 92187846006, 92187846007, 92187846008
METHOD BLANK: 1129495 Matrix: Water
Associated Lab Samples: 92187846005, 92187846006, 92187846007, 92187846008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.020 01/29/14 11:58
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1129496
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 2.5 2.5 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1129497 1129498
MS MSD
92187941002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD
Nitrogen, Nitrate mg/L 8.3 2.5 2.5 11.0 10.9 109 108 90-110 0
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 31 of 37

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
,�aneAnalyfical" 205 East MeadoEden, NC 27288 Asheville, NC128 04 9800Hunte svlle, NC128078
www.pageiabs.com [phone] [phone] [phone]
QUALITY CONTROL DATA
Project: DOT STATESVILLE.34613.3.26
Pace Project No.: 92187846
QC Batch: WETA/17930 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: 5310B TOC
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007, .
92187846008
METHOD BLANK: 1130807 Matrix: Water
Associated Lab Samples: 92187846001, 92187846002, 92187846003, 92187846004, 92187846005, 92187846006, 92187846007,
92187846008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L ND 1.0 02/04/14 14:12
LABORATORY CONTROL SAMPLE: 1130808
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 25 24.9 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1130809 1130810
MS MSD
92187846001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 2.4 25 25 25.0 24.8 91 90 75-125 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1130811 1130812
MS MSD
92187795002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 2.4 25 25 25.4 25.5 92 92 75-125 0
Date: 02/10/2014 03:24 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 32 of 37

Pace Analytical Services, Inc.
aceAnalytica! ® 205 East Meadow Road - Suite A
Eden, NC 27288
www.pacelabs.com [phone]
QUALIFIERS
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-M Pace Analytical Services - Minneapolis
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24 PM without the written consent of Pace Analytical Services, Inc.. Page 33 of 37

7 ci
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
® 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Analytical Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
wmpace/abs.com [phone] [phone] [phone]
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92187846001
DMW-7
RSK 175
AIR/19319
92187846002
DMW-6
RSK 175
AIR/19319
92187846003
DMW-10
RSK 175
AIR/19319
92187846004
DMW-9
RSK 175
AIR/19319
92187846005
DMW-11
RSK 175
AIR/19319
92187846006
DMW-2
RSK 175
AIR/19319
92187846007
DMW-1
RSK 175
AIR/19319
92187846008
DMW-8
RSK 175
AIR/19319
-
92187846001
DMW-7
EPA 3010
MPRP/15153
EPA 6010
ICP/13753
92187846002
DMW-6
EPA 3010
MPRP/15153
EPA 6010
ICP/13753
92187846003
DMW-10
EPA 3010
MPRP/15153
EPA 6010
ICP/13753
92187846004
DMW-9
EPA 3010
MPRP/15153
EPA 6010
ICP/13753
92187846005
DMW-11
EPA 3010
MPRP/15153
EPA 6010
ICP/13753
92187846006
DMW-2
EPA 3010
MPRP/15153
EPA 6010
ICP/13753 _-
92187846007
DMW-1
EPA 3010
MPRP/15153
EPA 6010
ICP/13753
92187846008
DMW-8
EPA 3010
MPRP/15153
EPA 6010
ICP/13753
I•
92187846001
DMW-7
EPA 7470
MERP/6120
EPA 7470
MERC/5907
92187846002
DMW-6
EPA 7470
MERP/6120
EPA 7470
MERC/5907
92187846003
DMW-10
EPA 7470
MERP/6120
EPA 7470
MERC/5907
92187846004
DMW-9
EPA 7470
MERP/6120
EPA 7470
MERC/5907
92187846005
DMW-11
EPA 7470
MERP/6120
EPA 7470
MERC/5907
92187846006
DMW-2
EPA 7470
MERP/6120
EPA 7470
MERC/5907
92187846007
DMW-1
EPA 7470
MERP/6120
EPA 7470
MERC/5907
92187846008
DMW-8
EPA 7470
MERP/6120
EPA 7470
MERC/5907
92187846001
DMW-7
SM 6200B
MSV/25645
92187846002
DMW-6
SM 6200E
MSV/25645
92187846003
DMW-10
SM 6200B
MSV/25645
92187846004
DMW-9
SM 6200B
MSV/25645
_
92187846005
DMW-11
SM 6200B
MSV/25645
92187846006
DMW-2
SM 6200E
MSV/25645
92187846007
DMW-1
SM 6200E
MSV/25645
92187846008
DMW-8
SM 6200B
MSV/25645
92187846009
TRIP
SM 6200B
MSV/25645
92187846001
DMW-7
SM 4500-S2D
WET/29362
92187846002
DMW-6
SM 4500-S2D
WET/29362
92187846003
DMW-10
SM 4500-S2D
WET/29362
92187846004
DMW-9
SM 4500-S2D
WET/29362
_-
92187846005
DMW-11
SM 4500-S2D
WET/29362
92187846006
DMW-2
SM 4500-S2D
WET/29362
92187846007
DMW-1
SM 4500-S2D
WET/29362
92187846008
Dli
SM 4500-S2D
WET/29362
92187846001
DMW-7
EPA 300.0
WETA/17949
92187846002
DMW-6
EPA 300.0
WETA/17949
`-
92187846003
DMW-10
EPA 300.0
WETA/17949
92187846004
DMW-9
EPA 300.0
WETA/17949
92187846005
DMW-11
EPA 300.0
WETA/17949
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/10/2014 03:24
PM
without the written consent of Pace Analytical Services, Inc..
Page 34 of 37

aceAnalytical
"mpace/abs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DOT STATESVILLE 34613.3.26
Pace Project No.: 92187846
Lab ID
Sample ID
92187846006
DMW-2
92187846007
DMW-1
92187846008
DMW-8
-- 92187846001
DMW-7
92187846002
DMW-6
92187846003
DMW-10
92187846004
DMW-9
92187846005
DMW-11
92187846006
DMW-2
92187846007
DMW-1
92187846008
DMW-8
f 92187846001
DMW-7
92187846002
DMW-6
92187846003
DMW-10
92187846004
DMW-9
92187846005
DMW-11
92187846006
DMW-2
92187846007
DMW-1
92187846008
DMW-8
Date: 02/10/2014 03:24 PM
QC Batch Method
EPA 300.0
EPA 300.0
EPA 300.0
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
SM 5310B
SM 5310B
SM 5310B
SM 5310B
SM 5310B
SM 5310B
SM 5310B
SM 5310B
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch Analytical Method
WETA/17949
WETA/17949
WETA/17949
WETA/17900
WETA/17900
WETA117900
WETA/17900
WETA/17902
WETA/17902
WETA/17902
WETA/17902
WETA117930
WETA117930
WETA/17930
WETA/17930
WETA/17930
WETA/17930
WETA/17930
WETA/17930
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 35 of 37

UOCument Name: UUCUf l lenl rXcwacu, vUuul 11— 1,
Sample Condition Upon Receipt SCUR Page 1 of 2
;aceAnalyfrcaf Document Number: Issuing Authority:
F-CHR-CS-03-rev.13 Pace Huntersville Quality Office
Client Name:
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial❑ Pace Other Optional
Proj. Due Date:
Custody Seal on Cooler/Box Present: ❑ yes no Seals intact: ❑ yes ❑ no
Proj. Name:
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1102 Type of Ice: 16/et Blue None [Samples on ice, cooling process has begun
T_�.- /a ,4:..... C....4..• Td4A )9 Ain ( nrrantinn -113n� Nn (:nrrpr•.tion
V 1.
Biological Tissue is Frozen: Yes No
Date and lmt' Is of person examining
1 ig
Corrected Cooler Tem p• C
�!-AA
contents:ZLI/-
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
Yes ONO
❑N/A
1.
Chain of Custody Filled Out:
es ONO
❑NIA
2.
----------....
Chain of Custody Relinquished:
- Yes �t DMT
o
Sampler Name & Signature on COC:
IJYes ONO
❑N/A
4.
Samples Arrived within Hold Time:
2Yes ONO
❑N/A
5.
.-,�tarIU
N/A
6.
Short Hold Time Analysis (<72hr):
Yes o
Rush Turn Around Time Requested:
❑Yes J2/No
❑N/A
7.
Sufficient Volume:
Yes ONO
❑N/A
8.
Correct Containers Used:
F Yes ❑No
❑NIA
9.
-Pace Containers Used:
Oyes ONO
❑NIA
Containers Intact:
►dyes ONO
El N/A
10.
Filtered volume received for Dissolved tests
❑Yes ONO
0N/A
11.
Sample Labels match COC:
P�-'s ONO
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
,ZYes ON.
❑N!A
13.
All containers needing preservation are found to be in
Yes ❑No
❑NIA
compliance with EPA recommendation.
/J
exceptions: VOA, eoliform, TOC, 0&G, WI-DRO (water)
Yes ❑ No
Samples checked for dechlorination:
Yes ONO
❑N/A
14.
Headspace in VOA Vials (>6mm):
❑O�Yes o
❑NIA
15.
1LIYes ONO
❑N/A
16. /
Trip Blank Present:
Trip Blank Custody Seals Present
Yes ONO
❑N/A
Pace Trio Blank Lot # (if purchased): _
Client Notification/ Resolution: Field Data Required? Y /
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: Date: f Z.
SRF Review: / Date:
Note: Whenever the ' a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
WOp:92187846
92187846
I
Page 36 of 37

CHAIN -OF -CUSTODY / Analytical Request Document
^ A--h 43....1 ° The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
,.%,
UVV/,1141y t,vul
www.pacelabs.com
Page;
of
Section A
Section B
Section C
Required Client Information:
Required Project Information:
Invoice Information:
•
178 gpq
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Company:
tt ''
Report To:
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Attention: '` +�
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Address:
Copy To:
Company Name:
REGULATORY AGENCY
9k-
Address:
r
NPDES r GROUND WATER j— DRINKING WATER
C t^�
ieLk fJC^ 5
(
UST r RCRA
OTHER
Email To:
Purchase Order No.:
Pace Quote
`�
Reference:
Phon
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Fax:
Project Name: �` rr ff --
a4-A.-S L �:.,c+
Pace Project
Manager.
$Ite"Location
Q�
Requested Due Date/TAT:
Project Number. —� t �O
�.+Ot^
Pace Profile #:-STATE•
`�—
Requested Analysis'Filteretl(Y/N)-"
-
Section D
Required Client information
Matrix Codes
MATRIX 1 CODE
o 0 COLLECTED
Preservatives
.K:
=r.:
Drinking Water DW
_ (
O
Water WT
Waste Water WW
U COMPOSITE COMPOSITE. 1`-
a m START ENO!GRAB
Product P"
SoillSofid SL
SAMPLE ID
Oil OL
�=
W,
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(A-Z, 0-9l ;)
Wipe WP
Air AR
p Lu
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Sample
IDS MUST BE UNIQUE
Tissue TS
Other OT
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ADDITIONXL,60MMENTS
f2ELINQUISHEOBY/AFFILIATION
DATE"
TIME
AC CEPTEDBY;lAFFILIATION
DATE
TIME
SAMPLE CONDITIONS
t
j
SAMPLER NAME AND SIGNATURE
U
o
ORIGINAL PRINT Name of SAMPLER:
v'
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5
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d
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SIGNATURE of SAMPI.IER:
/
DATE Signed
(MM/DDI"YY): %
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N
'hnportant Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per on or any invoices not paid tvilhin Vays. F-ALL-t.f-UZUreV.0 -May-ZUU / /, 9 b

i
:fcciMyrrrar
mlcrosceps'���
February 10, 2014
Kevin Godwin
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Microseeps/Pace Analytical Energy Services, LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
RE: DOT STATESVILLE / 92187846
Microseeps Workorder.- 11286
Dear Kevin Godwin:
Enclosed are the analytical results for sample(s) received by the laboratory on Wednesday, January 29, 2014.
Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise
narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Robbin Robl 02/10/2014
[e-mail]
Customer Service Representative
Enclosures
Report ID: 11286 - 486275
As a valued client we would appreciate your comments on our service.
Please email [e-mail].
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Microseeps/Pace Analytical Energy Services, LLC.
Total Number of Pages -L
Page 1 of 14

Microseeps/Pace Analytical Energy Services, LLC
y acoAnslrlca�'
"
220 William Pitt Way
r? �s
Pittsburgh, PA 15238
Phone: [phone]
m crosccpsu:
Fax: [phone]
LABORATORY ACCREDITATIONS & CERTIFICATIONS
Accreditor:
Pennsylvania Department of Environmental Protection, Bureau of Laboratories
Accreditation ID:
02-00538
Scope:
NELAP Non -Potable Water and Solid & Hazardous Waste
Accreditor:
NELAP: State of Florida, Department of Health, Bureau of Laboratories
Accreditation ID:
E87832
Scope:
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
South Carolina Department of Health and Environmental Control, Office of Environmental
Laboratory Certification
Accreditation ID:
89009003
Scope:
Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA)
Accreditor:
NELAP: State of Louisiana, Department of Environmental Quality
Accreditation ID:
04104
Scope:
Solid and Chemical Materials; Non -Potable Water
Accreditor:
NELAP: New Jersey, Department of Environmental Protection
Accreditation ID:
PA026
Scope:
Non -Potable Water, Solid and Chemical Materials
Accreditor:
NELAP: New York, Department of Health Wadsworth Center
Accreditation ID:
11815
Scope:
Non -Potable Water; Solid and Hazardous Waste
Accreditor:
State of Connecticut, Department of Public Health, Division of Environmental Health
Accreditation ID:
PH-0263
Scope:
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
NELAP: Texas, Commission on Environmental Quality
Accreditation ID:
T104704453-09-TX
Scope:
Non -Potable Water
Accreditor:
State of New Hampshire
Accreditation ID:
299409
Scope:
Non -potable water
Accreditor:
State of Georgia
Accreditation ID:
Chapter 391-3-26
Scope:
As per the Georgia EPD Rules and Regulations for Commercial Laboratories, Microseeps is
accredited by the Pennsylvania Department of Environmental Protection Bureau of
Laboratories under the National Environmental Laboratory Approval Program (NELAC).
Report ID: 11286 - 486275
,N AC-�i1ry0j CERTIFICATE OF ANALYSIS
_:1.11~a'elac This report shall not be reproduced, except in full,
without the written consent of Microseeps/Pace Analytical Energy Services, I.I.C.
Page 2 of 14

SAMPLE SUMMARY
Workorder: 11286.DOT STATESVILLE / 92187846
Microseeps/Pace Analytical Energy Services, LLC
220 William Pitt Way
Pittsburgh, PA 15236
Phone: [phone]
Fax: [phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Received
112860001
DMW 7
Water
1/27/2014 13:00
1/29/2014 11:45
112860002
DMW-6
Water
1/27/2014 13:45
1/29/2014 11:45
112860003
DMW-10
Water
1/27/2014 14:30
1/29/201411:45
112860004
DMW 9
Water
1/27/201415:15
1/29/201411:45
112860005
DMW 11
Water
1/28/2014 09:00
1/29/2014 11:45
112860006
DMW-2
Water
1/28/2014 09:35
1/29/2014 11:45
112860007
DMW-1
Water
1128/2014 10:10
1/29/2014 11:45
112860008
DMW-8
Water
1/28/2014 11:00
1/29/2014 11:45
Report ID: 11286 - 486275
^ ^? CERTIFICATE OF ANALYSIS
-�.i . a
d' This report shall not be reproduced, except in full,
without the written consent of Microseeps/Pace Analytical Energy Services, LLC.
Page 3 of 14

% �•P:3Co�Lrdy11AM1'
F ?�
ffli
crnscepsE%'
ins^�
ANALYTICAL RESULTS
Microseeps/Pace Analytical Energy Services, LLC
220 William Pitt Way
Pittsburgh, PA 1523:8
Phone: [phone]
Fax: [phone]
Workorder: 11286 DOT STATESVILLE/92187846
Lab ID: 112860001 Date Received://2912014 11:46 Matrix: Water
Sample ID: DMW 7 . Date.Collecled 1/27/201.4 13:00
Parameters Results Units PQL MDL DF.Prepared By Analyzed By Qual
EDonors -MICR
Analysts Desc AM21G:
Analytical Method: AM21G
AceticAcid
0.67U moil
5.'0 0.67
1;
2/6I201412:47
BW
PropionicAcid
0.251.1 'moil
5.0 .0.25
1.
2/6/2014 12:47
BW
Pytuvickid
0.53U mgli
10 0.53
1
2%6/201412:47
BW
Butyric Acid
0:10U moil
5.0 0.10
1
2/6/201412:47
BW
Lactic Acid
2.OU mg/l
25 2.0
1
2/6/201412:47
BW
Report ID: 11286 - 486275 Page 4 of 14
- CERTIFICATE OF ANALYSIS
r1e��C This repgr(shall not be reproduced, except In full,
without the wrillen consent or Microseeps/PaceAnaiylical Energy Services, LLC.

�/ 210A lyrical-
.
m�croscepsy�'
ANALYTICAL RESULTS
Workorder: 11286 DOT STATESVILLE 192187846
MicroseepslPace Analytical Energy Services, LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 112860062
Sample ID: DMW 6.
Date Received: 1/29/2.014 11:45
Date Collected: 1/27/2014.1.3:45
Matrix: Water
Parameters.
Results Units
POL
MDL:
DFPrepared By
An
By Qual
EDonors - MICR
Analysts Desc AM2:1.G .
Analy'hcalMethod AM21G
Ace6cAcid
0.67U mg/I
5 0
0-67,
1
2/6/2014 13:53
6W
PropionicAcid
6 25U mg/I
5:0
.25
1
2/6/2014 13:53
BW
PyruvicAcid
0.531.1 rrig/I
10'
0.53.
1
2/6/2014.13:53
BW
Butyric -Acid.
6.10U rr gll
5:0.
0..10;
1
'2/6/2014.13:53
BW
Lactici4eid
2.0U mg/I
21:
2.0
1
2/6/201413:53
BW
Report ID: It 286 - 486275 Page 5 of 14
CERTIFICATE OF ANALYSIS
j rj�1 •, This report shall not be reproduced, except in full,
without the written consent of Microseeps/PaceAnalylicat Energy Services, LLC:

M,
y, T � V-- ; ff B,
m1crosee s, ,
ANALYTICAL RESULTS
MiCfGseepsiPace Analytical Energy Services. LLC
226 William Pitt Way
PIROburgh, PA 15238
Phone: [phone]
Fax: [phone]
Workordqr. 11286 DOT STATIESMILLE.1 92 187846.
Lab ID: 112860003 Date Received: 1/29/201411:45 Matrix: Water
.Sample 10: DMW-I 0 Date Collected: 1/27=11414:30
Paramet&s. R esmlis Units POL MDL DIF Prepared 'By Analyzed By Qual
EDonors MICR
Analysis base AM21G
Analytical M,e.t.h.6-d,:.AM.21 G
A.ceficAcid
0.67J mgtl
5 6.67 1
OfopionicAcid
0.'25.Ij mg/l
5.0 015
PyruvicAcid
0.53u m4A
10 0.53, 1
ButyricAcid
Ojou nign
5.0 0.1.0 1
Lactic Acid
2..OU tholl
25 2.0 1
Report ID:11266=486275
216/2014 14:15
BW
2/6/2014 14:15
BW
2i661.4 1*4:15
BW.
216/2014 14:15
'BW;
2.16/2014 1.4:15
BW
CERTIFICATE OF ANALYSIS
This report shall not be rbot6duced, except In full,
la, without the written consent of Mic-ro.0,eps/Pa.6e Analytical Energy Services, LLG..
Fagg q of 14.

- Vj
- YP4-
tZacleol-111014MV
Wbrkdrder: 11286 DOT STATESVILLE 92187846
1-010: 112860004
Sample ID: DMW-9
Pirannetees Results Units
EDonors, - MICR
MicroseepslPaceAnalyiical Energy Services, LLC
2.20 William Pill Way
Pittsburgh. PA 15238
Phone: [phone]
Fax: [phone]
ANALYMAILIRMILT$
Date Received! 11291201.4 11:45 Matrix: Water
Date Collected: 1127/2014. 15:15
PQl- MbL bFPrepared By AnalyziBd BY . QU61
AiWY KIZkSj#'A 21'G
!A691yjkal Method AM21'13
AdeticAcid
. .
0.6 8
- . —.4 rno-11
5..0
0;67
Firopiqn,icAcid
0.25U mg/I
54
0.25-
Pyruvic Acid
0.531.1 mgjl
10
.0.53:
Butyric Acid
6.1101.11 mg/I
6.0
.010
LactiqAti&
2..OU mg/l
25
2.0.
Report ID:. 11 24P - 486275
2/612014 141:37
BW
216/2014 14:37
BW
2/6/2 . 014 14:3!
8W
2/60.14 f4:37
BW
1 216/2014 14:37
BW
CERTIFICATE OF ANALYSIS
This rep6rt shall hot be teprbdumd, except in full,
without the written consent.of Mid6se.epi/Pade Ahalyll 'Cal Energy Services* LLC.
Page 7 of 14

r : �.- .rCaMalyrfcaf'
n1crosceprP-
ANALYTICAL RESULTS
Workorder: 11.286 DOT STATESVILLE / 92187846
Microseeps/Pace Analytical Energy Services, LLC
220 William Pill Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab, ID: 112860005 Dale Received: 1/29%2014 11:46 Matrix: Water
Sample ID: . DMW-11 Date Collected' 1/2812014, 09:00
Parameters: Results Units PQL MDL DF:Prepair By. Analyzed By Qual
EDoriors - MICR
Qrialysls Desc AM21G: =
Arlalyodbl Metfi'od1,AM2fG: "
AceticAcid
0 67U mg/1
510 0.67 1
2/61.201414:59
BW
PropronicAcid
0.25U mg/l
5.0 0:25 1
2/61201414:59
BW
PyruvicAcid
0.53U mg/I
10 0.53 1
2161201414 59
BW
Butyric Acid
010U nigh
5.0 0.10 1
216/20141459
BW
LacEicAcid
2.OU Y11g/1
25. 2.0. 1
2/6/20141.4:59
BW
Report ID: 1124,- 48.6275 Page 8 of 14
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Microseeps/Pace Analytical Energy Services, LLC.

_,. �Coilavtyr/ral
mferosecps_='
ANALYTICAL RESULTS
Workor&c 11286 DOT STATESVILLE % 52187846
MicroseepslPaceAnalytical Energy Services. LLC
220. William Pitt Way
Pillsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 112860006 Date Received: 1/29/2014 11:45 Matrix: Water
.Sample ID: - DMW-2 Date Collected: 1/28/2014 09:35
Parameters :Results Units PQL MDL DF Prepared By Analyzed By Qual
EDonors:--MICR
Analysts Di c:-,AM21'G:.
Analytical Method:AM210
Acetic Acid
0:67U mgll
5.0 0.67
1
216/201415c21
BW
PropionicAcid
0:25U Yrigll
5.0, 0.25
1
visikm 15:21
BW
PyruvicAcid
6.53U mgA
10 0.53
1
216120141$:21
BW
Butyric Acid
0.10U mg/I
5.0 0.10
1
2/61201415-:21
BW
Lactic Acid
YAU mgll
25 2:0
1
216/201415i21
BW
Repod ID:` 11286 - 486275
CERTIFICATE OFANALYSIS
r This report shall not be reproduced, except in rult,
:'lhe�ace. wilhoultt a vrtilten consent of tuticroseepslPaceAnalplical Energy Services, LLC.
Page 9 of 14

d.K�CcilnaFjr/uv/'
y�_,,..
m1croseeps,A: -
�y
ANALYTICAL RESULTS
Workordbr: 11286 DOT STATESVILLE / 92187846
Microseeps/Pace Analytical Energy Services, LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 112860007 Date Received: 1/29/2.014 11:45 Matrix: Water
Sample ID: DMW4 Date Collected: 1/28/201410:10
Parameters Results Units PQL MDL DFPrepared By Analyzed I3yQual
EDonors - MICR
Analysis Dgsc AM21;G Analytical Method AM21;G
AceticAcid.
0.671.1 'mg/I.
54
0.67
1
216/201415:43
BW
ProMonleAcid
0.25U mgll
5.0
0.25
1
2/6/201416:43'
BW
P.yruvicAcid
0.53U mg/I
10
0.53
1
2M&b1416:43
BW
Baty�ia.Aciii
0.10U mg/I
5 0
0.10
1
2/6/2014 16:43
BW
LkNcAi id
2.OU mgll
25
2.0
1
2/6/201415:43
BW
Report ID: 11286 - 486275
CERTIFICATE OF ANALYSIS
:='nelac5: This report shall not be reproduced, except In full,
without the written consent of Microseeps/Pace Analytical Energy Services, LLC.
Page 10 of 14

Analytical
rm
3
6-lcseqps;>"
1!,ro
Workorder: 11286 DOT STATESVILLE/ 92187846
Lab ID: 112860008
Sample ID: DMW-8
Parameters
EDonors; - MICR
AH*tid. Qok.- AM71 G,
Acetic Acid
Pro p.ion-icAdi.d
PyruvidAcid
ButyricAcid
Laalc-Acid
Report ID: 11286 - 486275
1—hel'
1.
Microseeps/Pace Analytical Energy Services, LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax [phone]
ANALYTICAL RESULTS
Date Received: 1/29/2014 11:45 Matrix: Water
Date Collected. 1/28/2014 11:00
Results Units PQL MDL DFPrepared By Analyzed By Qual
Analytical Method; AM21,G
0..67U mg/l
5;0 0.07
1
2!6RQ14 16:05
BW
0..25U mg1I
5..0 0.25.
1
2A6q014 16:05
BW
0.53U mgjI
16 0.53
1
216/2011 *4 16'.:0'5
BW
0.10U mg/I
5.0 6.10
1
2/612014 16-05
BW
2.01.1 mii/I
25 40
1
2(612014 16:05
BW
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Microseeps/Pace Analytical Energy Services, I-I.C.
Page 11 of 14

__... ,iC•C/il7.iryrlC:Ir-
i
m croseepr;>
ANALYTICAL RESULTS QUALIFIERS
Microseeps/Pace Analytical Energy Services, LLC
220 Wiliam Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Workorder. 11286 DOT STATESVILLE 192187846
DEFINITIONS/QUALIFIERS
Disclaimer; The Pennsylvania Department of Environmental Protection (PADEP) has decided to no longer recognize analyses that do not
produce data for primary compliance, for NELAP accreditation. The methods affected by this decision are AM20GAx, AM21 G,
SW846 7199 and AM4.02. The laboratory shall continue to administer the NELAP/TNI standard requirements in the performance
of these methods.
MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection.
PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation.
NO Not detected at or above reporting limit.
DF Dilution Factor.
S Surrogate.
RPD Relative Percent Difference.
% Rec Percent Recovery.
U Indicates the compound was analyzed for, but not detected at or above the noted concentration.
J Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL).
Report ID: 11286 - 486275
.. worn
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Microseeps/Pace Analytical Energy Services, LLC.
Page 12 of 14

Microseeps/Pace Analytical Energy Services, LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Workorder: 11286 DOT STATESVILLE / 92187846
QC Batch: EDON/1992 Analysis Method: AM21 G
QC Batch Method: AM21 G
Associated Lab Samples: 112860001, 112860002, 112860003,'l12860004, 112880005. 112860006, 112860007,'112860008
METHOD BLANK: 25639
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
EDonors
Acetic Acid
mg/1
0.67U
0.67
PropionicAcid
mg/I
0.25U
0.25
Pyruvic Acid
mg/I
0.53U
0.53
ButyricAcid
mg/I
0.10U
0.10
Lactic Acid
mg/I
2.OU
2.0
LABORATORY CONTROL SAMPLE: 25640
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
EDonors
AceticAcid
mg/I
100
100
102
70-130
PropionicAcid
mg/I
100
92
92
70-130
Pyruvic Acid
mg/l
100
110
111
70-130
ButyricAcid
mg/I
100
84
84
70-130
Lactic Acid
mg/I
100
120
125
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 25641
25642
Original:
112860001
Original
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Result
Result
% Rec
% Rec
Limit RPD
RPD Qualifiers
EDonors
AceticAcid
mg/I
0
100
99
100
99
100
70-130
1
20
PropionicAcid
mg/I
0
100
94
97
95
97
70-130
2.1
20
PyruvicAcid
mg/l
0
100
87
92
87
92
70-130
5.6
20
ButyricAcid
mg/I
0
100
98
100
99
101
70-130
2
20
Lactic Acid
mg/1
0
100
100
100
101
103
70-130
2
20
Report ID: 11286 - 486275
CERTIFICATE OF ANALYSIS
?'i nela%c This report shall not be reproduced, except in full,
without the written consent of Microseeps/Pace Analytical Energy Services, LLC.
Page 13 of 14

�J
r% PacoAnayrrcor'
MicroseepsrPaceAnalytical Energy Services, LLC
220 William Pill Way
r
Pittsburgh, PA 15238
Phone: [phone]
mleroseepsr av
Fax: [phone]
(QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder: 11286 DOT STATESVILLE! 92187846
i
Analysis
Lab; ID
Sample I.D.
PTep.Method Prep Batch Analysis Method
Batch
112860001
DMW 7
AM21G
EDON/1992
112860002
DMW-6
AM21G
EDON/1992
112860003
DMW-1.0
AM210
EDUN/1992
112860004
DMW-9
AM21G
EDON/1992
112860005
DMW-11
AM21G
EDON/1992
112860006
DMW2
AM21G
EDON/1992
112860007
DMW 1
AM21G
EDON/1992
112860008
DMW 8
AM21 G
EDON/1992
Report ID: 11285 - 486275
CERTIFICATE OF ANALYSIS
Y` This report dhell not be reproduced, except in full,
h'elacwithout the written consent of Microseeps/Pace Analytical Energy Services, LLC.
Page 14 of 14

Chain of Custody
Workorder: 92187846 Workorder Name: DOT STATESVILLE 34613.3.26
acekldi vt
ical
www.pacelabs.com
Results Requested 2/6/2014
Repoit'IlnvoiceTo. `':' Subcontract To `
"`� Requested Anal sis
Kevin Godwin
Pace Analytical Charlotte P.O..
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
�1rC
Phone [phone] %Sc'�PS
Email: [e-mail] 1
Cj
`PreseniedcContainers '
Collect
t
N
m .
Item
Sample lD
DatefTime
Lab ID
Matrix
LAB USE ONLY
1
DMW-7
1/27/201413:00
92187846001
Water
Z
�(
2
DMW-6
1/271201413:45
92187846002
Water
Z
>(
3
DMW-10
1/27/201414:30
92187846003
Water
4
DMW-9
1/27/201415:15
92187846004
Water
2-
5
DMW-11
1/28/2014 09:00
92187846005
Water
-2
6
DMW-2
1/28/201409:35
92187846006
Water
Z
7
DMW-1
1/28/201410:10
92187846007
Water
Z
8
DMW-8
1/28/201411:00
92187846008
Water
'z
K
9
10
11
12
Commenfs
Transfers
Relea ed By
DatefTirpe
Received By
Date/Time
to
r
I L-7 y
2
3
Cooler Temperature on Receipt 3. °CI
CustodV Seal Y or N .•
Received on Ic Y or N Sam les Intac Y or N .
Tuesday, January 28, 2014 2:25:12 PM FMT-ALL-G002rev.00 24March2009 Page 1 of 1

NON-CONFORMANCE FORM
Microseeps Project Number:
Date: 2` Time of Receipt: 1/ / Receiver: Z�
Client: eC�_
REASON FOR NON-CONFORMANCE: ,
wa, (J ?� awe. I� w W.
illa is
ACTION TAKEN:
Client name: -- -� '+ ip�inn �CiC� Date:/ _ / : Time:
C � � ¢.�t�- i 5 C{,G1la✓' 2.� r �� (� _ �� -f'✓'OG� et� ` I �L� �—
a0a ski d e--M a
Customer Service Initials:cam/ Date:

Chris Thomas
From: Kevin Godwin <[e-mail]>
Sent: Wednesday, January 29, 20141:15 PM
To: Chris Thomas
Subject: Re: DOT STATESVILLE 3.4613.3.26
Hi Chris,
- The client's sample IDs begin with DMW.
Kevin Godwin
Project Manager
Pace Analytical
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
Phone: [phone] ext. 237
Fax: [phone]
www.pacelabs.com
>>> "Chris Thomas" <CThomasOmicroseeps.com> 1/29/201412:18 PM >>>
Kevin,
We received samples for the DOT STATESVILLE 34613.3.26 project. I have attached a copy of the COC/Non-
Conformance. The COC sample ID's start with DMW. All vials with Pace ID's are DWW. Client labels on vials -look like
DMW. We just need to confirm what ID's are correct for log -in so we can proceed with the analysis.
Thanks,
Chris
Christopher Thomas
Microseeps, a Division of Pace Analytical Energy Services, LLC
220 William Pitt Way
Pittsburgh, PA 15238
Office: 412-826-5245
Direct: 412-826-4481
Disclaimer: This message contains confidential information and is intended only for the individual(s) named. If you are
not the named addressee, you should permanently delete this e-mail from your system and should not disseminate,
distribute or copy this e-mail. E-mail transmission cannot be guaranteed to be secure or error -free as information
delivered over the internet could be corrupted, lost, destroyed, delayed, or contain viruses
rhis email has been scanned by the Symantec Email Security.cloud service.
For more information please visit http://www.symanteccloud.com
r�
1

Cooler Receipt Form
Client Name: Project: TVF S WO_WI I Lab Work Order:
A. Shipping/Container Information (circle appropriate response)
Courier: EEd x UPS USPS 'Client Other: Air bill Present: ^ Y se No
Tracking Number:
Custody Seal on Cooler/Box Present: Y No Seals Intact: Yes No
Cooler/Box Packing Materia ; Bubble WrraaP. Absorbent Foam Other:
Type of IceBlue ' No Ice Intac . ^Ye Melted
Cooler Temperature: Radiation Screened: Yes No Chain of Custody Present Ye No -
Comments:
B. Laboratory Assignment/Log-in (check appropriate response)
YES NO
JN/Alto_mrffe­ft---
Reference non=Conformance
Chain of Custody properly filled out
r
Chain of Custody relinquished -
=->--
Sampler Name & Signature on CDC
Containers intact
Were samples in separate bags
Sample container labels match CDC
ample name/date and time collected
-
Sufficient volume provided
Microseeps containers used
Are containers properly preserved for the requested testing?
(as labeled)
-
If an unknown preservation state, were containers checked?
Exception: VOA's coliform
!Eyes, see pH form.
—
Was volume for dissolved testing field filtered, as noted on
the.000? Was volume received in a preserved container?
1_4
Comments:
Cooler contents examined/received by: Date:`
Project Manager Review: C)aZ- Date:

aceAnallXical
J`
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
May 19, 2014
Chemical Testing Engineer
NCDOT
Materials & Tests Unit
1801 Blue Ridge Road
Raleigh, NC 27607
RE: Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Dear Chemical Engineer:
Enclosed are the analytical results for sample(s) received by the laboratory on May 09, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc: Mr. Stephen Libbey, Hart & Hickman
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pagel of 44

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 _
[phone]
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
A21-A Certification #: 2926.01
Alabama Certification #40770
Alabama Certification #40770
Alaska Certification #: UST 078
Alaska Certification #MN00064
Arizona Certification #: AZ-0014
Arkansas Certification #: 88-0680
California Certification M 01155CA
Colorado Certification #Pace
Connecticut Certification #: PH-0256
EPA Region 8 Certification #: 8TMS-L
Florida/NELAP Certification #: E87605
Guam Certification #: Pace
Georgia Certification #: 959
Idaho Certification M MN00064
Hawaii Certification #MN00064
Illinois Certification #: 200011
Indiana Certification#C-MN-01
Iowa Certification #: 368
Kansas Certification M E-10167
Kentucky Dept of Envi. Protection - DW #90062
Kentucky Dept of Envi. Protection - WW #:90062
Louisiana DEQ Certification #: 3086
Louisiana DHH #: LA140001
Maine Certification #: 2013011
Maryland Certification #: 322
Michigan DEPH Certification #: 9909
Minnesota Certification #: 027-053-137
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification * 5342
North Carolina Wastewater Certification M 12
South Carolina Certification M 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Mississippi Certification #: Pace
Montana Certification #: MT0092
Nebraska Certification #: Pace
New Jersey Certification #: MN-002
New Jersey Certification #: MN-002
New York Certification #: 11647
North Carolina Certification #: 530
North Carolina State Public Health #: 27700
North Dakota Certification M R-036
Ohio EPAM 4150
Ohio VAP Certification #: CL101
Oklahoma Certification M 9507
Oregon Certification #: MN200001
Oregon Certification * MN300001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification
Saipan (CNMI) #:MP0003
South Carolina #:74003001
Texas Certification #: T104704192
Tennessee Certification #: 02818
Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251
VirginiaNELAP Certification * Pace
Washington Certification #: C486
Wisconsin Certification #: 999407970
West Virginia Certification #: 382
West Virginia TO-15 Approval
West Virginia DHHR #:9952C
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 44

�,AceAnalydcal
www.pacelabs.com
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
SAMPLE ANALYTE COUNT
Lab ID
Sample ID
Method
92200731001
DMW-3
SM 6200E
92200731002
DMW-4
SM 6200B
92200731003
SMW-3
SM 6200B
92200731004
SMW-2
SM 6200E
92200731005
SMW-1
SM 6200E
92200731006
DMW-1
RSK 175
EPA 6010
EPA 7470
SM 6200B
SM 4500-S21)
EPA 300.0
EPA 353.2
SM 5310B
92200731007
DMW-2
RSK 175
EPA 6010
EPA 7470
SM 6200B
SM 4500-S21)
EPA 300.0
EPA 353.2
-
SM 5310E
92200731008
DMW 9
RSK 175
EPA 6010
-
EPA 7470
SM 6200B
SM 4500-S2D
EPA 300.0
EPA 353.2
SM 5310B
92200731009
DMW-10
RSK 175
EPA 6010
EPA 7470
SM 6200B
SM 4500-S21)
EPA 300.0
EPA 353.2
SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analysts
Analytes
Reported
Laboratory
CAH
33
PASI-C
CAH
33
PASI-C
CAH
33
PASI-C
CAH
33
PASI-C
CAH
33
PASI-C
JRB
3
PASI-M
JMW
7
PASI-A
MTS
1
PASI-A
CAH
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
DMN
1
PASI-A
SAE
1
PASI-A
JRB
3
PASI-M
JMW
7
PASI-A
MTS
1
PASI-A
CAH
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
DMN
1
PASI-A
SAE
1
PASI-A
JRB
3
PASI-M
JMW
7
PASI-A
MTS
1
PASI-A
CAH
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
DMN
1
PASI-A
SAE
1
PASI-A
JRB
3
PASI-M
JMW
7
PASI-A
MTS
1
PASI-A
CAH
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
DMN
1
PASI-A
SAE
1
PASI-A
Page 3 of 44

aceAnalytical
www.pacelabs.cam
Pace Analytical Services, Inc. -
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 --
[phone]
Project: DOT 404 WBS#34613.3.26
Pace Project No.: 92200731
Lab ID Sample ID
92200731010 DMW 11
92200731011 DMW-6
92200731012 DMW-7
92200731013 DMW-8
92200731014 SS-2
92200731015 WSW-4
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
RSK 175
JRB
3
PASI-M -
EPA 6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
RSK 175
JRB
3
PASI-M
EPA6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM, 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
RSK 175
JRB
3
PASI-M
EPA6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 4500-S21)
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A _
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
RSK 175
JRB
3
PASI-M
EPA6010
JMW
7
PASI-A
EPA 7470
MTS
1
PASI-A
SM 62006
CAH
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
SM 6200B
CAH
33
PASI-C
SM 6200B
CAH
33
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 44

�� aceAnal tical
J
www.pacelabs.com
1
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
- Sample: DMW 3 Lab ID: 92200731001 Collected: 05/09/14 07:10 Received: 05/09/14 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
601 Volatiles by SM 6200 Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
05/12/14 23:59
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/12/14 23:59
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/12/14 23:59
71-55-6
1,1,2-Trchloroethane
ND ug/L
1.0
1
05/12/14 23:59
79-00-5
_I 1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/12/14 23:59
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/12/14 23:59
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/12/14 23:59
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/12/14 23:59
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/12/14 23:59
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/12/14 23:59
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/12/14 23:59
75-27-4
Bromomethane
ND ug/L
5.0
1
05/12/14 23:59
74-83-9
- Bromoform
ND ug/L
1.0
1
05/12/14 23:59
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/12/14 23:59
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/12/14 23:59
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/12/14 23:59
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/12/14 23:59
108-90-7
Chloroethane
ND ug/L
1.0
1
05/12/14 23:59
75-00-3
Chloroform
ND ug/L
1.0
1
05/12/14 23:59
67-66-3
Chloromethane
ND ug/L
1.0
1
05/12/14 23:59
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/12/14 23:59
124-48-1
- Dichlorodifluoromethane
ND ug/L
1.0
1
05/12/14 23:59
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/12/14 23:59
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/12/14 23:59
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/12/14 23:59
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/12/14 23:59
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/12/14 23:59
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/12/14 23:59
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/12/14 23:59
75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/12/14 23:59
106-93-4
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
1
05/12/14 23:59
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
05/12/14 23:59
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/12/14 23:59
2037-26-5
REPORT OF LABORATORY ANALYSIS
_ This report shall not be reproduced, except in full,
Date: 05/19/2014 12:16 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 44

aceAnalXical
www.pacelabs.com
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
i
Sample: DMW-4
Parameters
Lab ID: 92200731002 Collected: 05/09/14 07:25
Results Units Report Limit DF
Received: 05/09/14 13:12 Matrix: Water
Prepared Analyzed CAS No. Qua[
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
05/13/14 00:15
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:15
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 00:15
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 00:15
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 00:15
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:15
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 00:15
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 00:15
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:15
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:15
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 00:15
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 00:15
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 00:15
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:15
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 00:15
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 00:15
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 00:15
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 00:15
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 00:15
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 00:15
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 00:15
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 00:15
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 00:15
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:15
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 00:15
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 00:15
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 00:15
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 00:15
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 00:15
75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 00:15
106-93-4
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
05/13/14 00:15
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
05/13/14 00:15
17060-07-0
Toluene-d8 (S)
102 %
70-130
1
05/13/14 00:15
2037-26-5
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 44 ,

aceAnalXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: SMW-3 Lab ID: 92200731003 Collected: 05/09/14 07:40 Received: 05/09/14 13:12 Matrix: Water .
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
-, 601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
2.1 ug/L
1.0
1
05/13/14 00:32
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:32
75-35-4
- 1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 00:32
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 00:32
79-00-5
__. 1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 00:32
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:32
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 00:32
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 00:32
78.87-5
- 1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:32
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:32
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 00:32
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 00:32
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 00:32
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:32
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 00:32
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 00:32
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 00:32
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 00:32
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 00:32
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 00:32
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 00:32
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 00:32
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 00:32
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:32
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 00:32
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 00:32
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 00:32
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 00:32
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 00:32
75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 00:32
106-93-4
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
05/13/14 00:32
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
05/13/14 00:32
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
05/13/14 00:32
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/19/2014 12:16 PM without the written consent of Pace Analytical Services, Inc:.
Page 7 of 44

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc. -
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731.
Sample: SMW-2
Parameters
Lab ID: 92200731004 Collected: 05/09/14 07:55
Results Units Report Limit DF
Received: 05/09/14 13:12 Matrix: Water
Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200
Analytical Method:.SM 6200E
1,1-Dichloroethane
3.1 ug/L
1.0
1
05/13/14 00:48
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:48
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 00:48
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 00:48
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 00:48
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:48
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 00:48
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 00:48
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:48
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 00:48
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 00:48
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 00:48
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 00:48
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:48
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 00:48
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 00:48
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 00:48
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 00:48
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 00:48
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 00:48
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 00:48
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 00:48
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 00:48
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 00:48
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 00:48
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 00:48
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 00:48
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 00:48
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 00:48
75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 00:48
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
05/13/14 00:48
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
05/13/14 00:48
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
05/13/14 00:48
2037-26-5
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 44

�AceAnalydcalo
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: SMW-1 Lab ID: 92200731005 . Collected: 05/09/14 08:10 Received: 05/09/14 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200 Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
05/13/14 01:05
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:05
75-35-4
-- 1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 01:05
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 01:05
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 01:05
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:05
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 01:05
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 01:05
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:05
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:05
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 01:05
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 01:05
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 01:05
75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:05
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 01:05
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 01:05
56-23-5 '
Chlorobenzene
ND ug/L
1.0
1
05/13/14 01:05
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 01:05
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 01:05
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 01:05
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 01:05
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 01:05
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 01:05
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:05
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 01:05
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 01:05
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 01:05
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 01:05
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 01:05
75-01-4
1 1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 01:05
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
05/13/14 01:05
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
05/13/14 01:05
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/13/14 01:05
2037-26-5
- REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/19/2014 12:16 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 44

aceAnalydcal
www.pacelabs.com
Pace Analytical Services, Inc. -,
9800 Kincey Ave. Suite 100 j
Huntersville, NC 28078 iL'
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: DMW-1
Parameters
Lab ID: 92200731006 Collected: 05/09/14 08:40
Results Units Report Limit DF
Received: 05/09/14 13:12 Matrix: Water
Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace
Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
05/15/14 21:44
74-84-0
Ethene
ND ug/L
6.2
1
05/15/14 21:44
74-85-1
Methane
14.2 ug/L
6.6
1
05/15/14 21:44
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
05/12/14 15:45
05/13/1416:03
7440-38-2
Barium
59.8 ug/L
5.0
1
05/12/14 15:45
05113/1416:03
7440-39-3
Cadmium
ND ug/L
1.0
1
05/12/14 15:45
05/13/1416:03
7440-43-9
Chromium
ND ug/L
5.0
1
05/12/14 15:45
05/13/1416:03
7440-47-3
Lead
ND ug/L
5.0
1
05/12/14 15:45
05/13/1416:03
7439-92-1
Selenium
ND ug/L
10.0
1
05/12/14 15:45
05/1311416:03
7782-49-2
Silver
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:03
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
05/12114 23:00
05/14/14 18:21
7439-97-6 M1
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
2.9 ug/L
1.0
1
05/13/14 01:22
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:22
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 01:22
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 01:22
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 01:22
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:22
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 01:22
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 01:22
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:22
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:22
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 01:22
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 01:22
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 01:22
75-25-2
cis-1,2-Dichloroethene
2.0 ug/L
1.0
1
05/13/14 01:22
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 01:22
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 01:22
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 01:22
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 01:22
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 01:22
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 01:22
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 01:22
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 01:22
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 01:22
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:22
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 01:22
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 01:22
127-18-4
Trichloroethene
1.6 ug/L
1.0
1
05/13/14 01:22
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 01:22
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 01:22
75-01-4
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 44 {

, aceAnal�/tical
J`
www.pacelabs.com
S i
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: DMW-1
Parameters
— 601 Volatiles by SM 6200
1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
' 5310E TOC
Total Organic Carbon
Date: 05/19/2014 12:16 PM
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92200731006 Collected:
05/09/14 08:40
Received: 05/09/14 13:12 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
Analytical Method: SM 6200B
ND ug/L
1.0
1
05/13/14 01:22
106-93-4
97 %
70-130
1
05/13/14 01:22
460-00-4
99 %
70-130
1
05/13/14 01:22
17060-07-0
101 %
70-130
1
05/13/14 01:22
2037-26-5
Analytical Method: SM 4500-S2D
ND mg/L
0.10
1
05/16/14 16:13
18496-25-8
Analytical Method: EPA 300.0
3.9 mg/L
2.0
1
05/15/14 15:36
14808-79-8
Analytical Method: EPA 353.2
0.32 mg/L
0.020
1
05/09/14 22:55
Analytical Method: SM 5310B
4.4 mg/L
1.0
1
05/13/14 19:13
744044-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 11 of 44

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 _.
[phone]
I
Sample: DMW-2 Lab ID: 92200731007 Collected: 05/09/14 09:00 Received: 05/09/14 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical. Method: RSK 175
Ethane
ND ug/L
6.2
1
05/15/14 21:55
74-84-0
Ethene
ND ug/L
6.2
1
05/15/14 21:55
74-85-1
Methane
30.3 ug/L
6.6
1
05/15/14 21:55
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
05/12/1415:45
05/13/1416:13
7440-38-2
Barium
27.2 ug/L
5.0
1
05/12/1415:45
05/13/1416:13
7440-39-3
Cadmium
ND ug/L
1.0
1
05/12/14 15:45
05/13/1416:13
7440-43-9
Chromium
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:13
7440-47-3
Lead
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:13
7439-92-1
Selenium
ND ug/L
10.0
1
05/12/1415:45
05/13/1416:13
7782-49-2
Silver
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:13
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/12/14 23:00
05/14/14 18:29
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
1.3 ug/L
1.0
1
05/13/14 01:38
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:38
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 01:38
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 01:38
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 01:38
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:38
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 01:38
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 01:38
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:38
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:38
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 01:38
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 01:38
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 01:38
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:38
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 01:38
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 01:38
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 01:38
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 01:38
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 01:38
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 01:38
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 01:38
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 01:38
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 01:38
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:38
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 01:38
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 01:38
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 01:38
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 01:38
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 01:38
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/19/2014 12:16 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 44

�AceAnalydcaloD
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: DMW-2
Lab ID: 92200731007 Collected:
05/09/14 09:00
Received: 05/09/14 13:12 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
— 601 Volatiles by SM 6200
Analytical Method: SM 6200B
1 2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 01:38
106-93-4
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
1
05/13/14 01:38
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
05/13/14 01:38
17060-07-C
Toluene-d8 (S)
101 %
70-130
1
05/13/14 01:38
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
'Sulfide
ND mg/L
0.10
1
05/16/14 16:13
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
83.3 mg/L
10.0
5
05/15/14 15:50
14808-79-8
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2
-- Nitrogen, Nitrate
2.4 mg/L
0.020
1
05/09/1422:57
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
5.3 mg/L
1.0
1
05/13/14 19:46
7440-44-0
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 13 of 44

aceftiXicai®
www.pacelab.com
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Pace Analytical Services, Inc. -
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
I i
Sample: DMW 9
Parameters
Lab ID: 92200731008 Collected: 05/09/14 09:20
Results Units Report Limit DF
Received: 05/09/14 13:12 Matrix: Water
Prepared Analyzed CAS No. Qua[
RSK 175 AIR Headspace
Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
05/15/14 22:07
74-84-0
Ethene
ND ug/L
6.2
1
05/15/14 22:07
74-85-1
Methane
175 ug/L
6.6
1
05/15/14 22:07
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
05/12/1415:45
05/1311416:16
7440-38-2
Barium
85.0 ug/L
5.0
1
05/12/1415:45
05/1311416:16
7440-39-3
Cadmium
ND ug/L
1.0
1
05/12/1415:45
05/13/14 16:16
7440-43-9
Chromium
ND ug/L
5.0
1
05/12/1415:45
05/13/14 16:16
7440-47-3
Lead
ND ug/L
5.0
1
05/12/14 15:45
05/13/14 16:16
7439-92-1
Selenium
ND ug/L
10.0
1
05/12/1415:45
05/1311416:16
7782-49-2
Silver
ND ug/L
5.0
. 1
05/12/1415:45
05/131/14 16:16
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
05/12/14 23:00
05/14/14 18:37
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
2.3 ug/L
1.0
1
05/13/14 01:54
75-34-3
1,1-Dichloroethene
1.9 ug/L
1.0
1
05/13/14 01:54
75-35-4
1,1,1-Trich[oroethane
ND. ug/L
1.0
1
05/13/14 01:54
71-55-6
1,1,2-Trich[oroethane
ND ug/L
1.0
1
05/13/14 01:54
79-00-5
1,1,2,2-Tetrach[oroethane
ND ug/L
1.0
1
05/13/14 01:54
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:54
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 01:54
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 01:54
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:54
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 01:54
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 01:54
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 01:54
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 01:54
75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:54
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 01:54
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 01:54
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 01:54
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 01:54
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 01:54
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 01:54
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 01:54
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 01:54
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 01:54
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 01:54
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 01:54
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 01:54
127-18-4
Trichloroethene
2.9 ug/L
1.0
1
05/13/14 01:54
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 01:54
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 01:54
75-01-4
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 44

aceAnalytical
j mw,pacelabs.cam
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: DMW 9
Lab ID: 92200731008 Collected:
05/09/14 09:20
Received: 05/09/14 13:12 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 01:54
106-93-4
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
05/13/14 01:54
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
05/13/14 01:54
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
05/13/14 01:54
2037-26-5
4500213 Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
05/16/1416:13
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
76.3 mg/L
4.0
2
05/15/14 16:31
14808-79-8
-' 3512 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
- Nitrogen, Nitrate
1.4 mg/L
0.020
1
05/09/14 23:01
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
8.1 mg/L
1.0
1
05/13/14 19:57
7440-44-0
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 15 of 44

aceAnalyical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: DMW-10 Lab ID: 92200731009 Collected: 05/09/14 09:40 Received: 05/09/14 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
05/15/14 22:18
74-84-0
Ethene
ND ug/L
6.2
1
05/15/14 22:18
74-85-1
Methane
555 ug/L
6.6
1
05/15/14 22:18
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
05/12/14 15:45
05/13/14 16:22
7440-38-2
Barium
252 ug/L
5.0
1
05/12/14 15:45
05/13/14 16:22
7440-39-3
Cadmium
ND ug/L
1.0
1
05/12/14 15:45
05/13/14 16:22
7440-43-9
Chromium
ND ug/L
5.0
1
05/12/14 15:45
05/13/14 16:22
7440-47-3
Lead
ND ug/L
5.0
1
05/12/14 15:45
05/13/14 16:22
7439-92-1
Selenium
ND ug/L
10.0
1
05/12/14 15:45
05/13/14 16:22
7782-49-2
Silver
ND ug/L
5.0
1
05/12/14 15:45
05/13/14 16:22
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/12/14 23:00
05/14/14 18:39
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
05/13/14 02:11
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 02:11
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 02:11
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 02:11
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 02:11
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:11
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 02:11
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 02:11
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:11
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:11
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 02:11
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 02:11
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 02:11
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 02:11
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 02:11
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 02:11
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 02:11
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 02:11
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 02:11
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 02:11
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 02:11
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 02:11
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 02:11
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 02:11
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 02:11
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 02:11
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 02:11
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 02:11
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 02:11
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05119/2014 12:16 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 44

,AeAnalXical
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Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
)ampie: uiviw-1 u
i
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
5310B TOC
Total Organic Carbon
Date: 05/19/2014 12:16 PM
ANALYTICAL RESULTS
Lab ID: 92200731009 Collected:
05/09/14 09:40
Received:. 05/09/14 13:12 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
Analytical Method: SM 6200B
ND ug/L
1.0
1
05/13/14 02:11
106-93-4
98 %
70-130
1
05/13/14 02:11
460-00-4
99 %
70-130
1
05/13/14 02:11
17060-07-0
100 %
70-130
1
05/13/14 02:11
2037-26-5
Analytical Method: SM 4500-S21)
ND mg/L
0.10
1
05/16/14 16:13
18496-25-8
Analytical Method: EPA 300.0
20.2 mg/L
2.0
1
05/15/14 16:44
14808-79-8
Analytical Method: EPA 353.2
ND mg/L
0.020
1
05/09/14 23:02
Analytical Method: SM 5310B
23.6 mg/L
1.0
1
05/13/14 20:07
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qua[
Page 17 of 44

aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 26078 • _
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: DMW-11
Parameters
Lab ID: 92200731010 Collected: 05/09/14 10:00
Results Units Report Limit DF
Received: 05/09/14 13:12 Matrix: Water
Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace
Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
05/16/1412:08
74-84-0
Ethene
ND ug/L
6.2
1
05/16/1412:08
74-85-1
Methane
2140 ug/L
6.6
1
05/16/1412:08
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
05/12/1415:45
05/13/1416:25
7440-38-2
Barium
58.9 ug/L
5.0
1
05112/1415:45
05/13/1416:25
7440-39-3
Cadmium
ND ug/L
1.0
1
05/12/1415:45
05/13/1416:25
7440-43-9
Chromium
ND ug/L
5.0
1
05/1211415:45
05/13/1416:25
7440-47-3
Lead
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:25
7439-92-1
Selenium
ND ug/L
10.0
1
05/12/1415:45
05/13/1416:25
7782-49-2
Silver
ND ug/L
5.0
1
05/12/1415:45
05/13/14 16:25
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
05/12/14 23:00
05/14/14 18:42
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
6.4 ug/L
1.0
1
05/13/14 02:27
75-34-3
1,1-Dichloroethene
7.6 ug/L
1.0
1
05/13/14 02:27
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 02:27
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 02:27
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 02:27
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:27
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 02:27
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 02:27
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:27
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:27
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 02:27
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 02:27
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 02:27
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 02:27
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 02:27
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 02:27
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 02:27
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 02:27
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 02:27
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 02:27
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 02:27
12448-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 02:27
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 02:27
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 02:27
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 02:27
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 02:27
127-18-4
Trichloroethene
6.3 ug/L
1.0
1
05/13/14 02:27
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 02:27
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 02:27
75-01-4
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 18 of 44 a

�,AceAnalyticalo
www.pacelabs.com
�l
i
Project: DOT 404 WBS#34613.3.26
Pace Project No.: 92200731
--,Sample: DMW 11
Parameters
601 Volatiles by SM 6200
i
j 1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
i
531013TOC
Total Organic Carbon
)ate: 05/19/2014 12:16 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92200731010 Collected:
05/09/14 10:00
Received: 05/09/14 13:12 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qua[
Analytical Method: SM 6200B
ND ug/L
1.0
1
05/13/14 02:27
106-93-4
97 %
70-130
1
05/13/14 02:27
460-00-4
100 %
70-130
1
05/13/14 02:27
17060-07-0
102 %
70-130
1
05/13/14 02:27
2037-26-5
Analytical Method: SM 4500-S2D
ND mg/L
0.10
1
05/16/14 16:13
18496-25-8
Analytical Method: EPA 300.0
47.9 mg/L
4.0
2
05/15/14 16:58
14808-79-8
Analytical Method: EPA 353.2
ND mg/L
0.020
1
05/09/14 23:04
Analytical Method: SM 5310B
23.8 mg/L
1.0
1
05/13/14 20:17
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 44

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Pace Analytical Services, Inc. --I
9800 KinceyAve. Suite 100 +'
Huntersville, NC 28078 �.
[phone]
I
I
Sample: DMW-6
Parameters
Lab ID: 92200731011 Collected: 05/09/14 10:20
Results Units Report Limit DF
Received: 05/09/14 13:12 Matrix: Water
Prepared Analyzed CAS No.
RSK 175 AIR Headspace
Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
05/16/1412:31
74-84-0
Ethene
ND ug/L
6.2
1
05/16/1412:31
74-85-1
Methane
17.4 ug/L
6.6
1
05/16/14 12:31
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
05/12/1415:45
05/13/1416:28
7440-38-2
Barium
109 ug/L
5.0
1
05/12/14 15:45
05/13/1416:28
7440-39-3
Cadmium
ND ug/L
1.0
1
05/12/1415:45
05/13/1416:28
7440-43-9
Chromium
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:28
7440-47-3
Lead
ND ug/L
5.0
1
05/1211415:45
05/13/1416:28
7439-92-1
Selenium
ND ug/L
10.0
1
05/12/1415:45
05/13/1416:28
7782-49-2
Silver
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:28
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/12/14 23:00
05/14/14 18:44
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
57.2 ug/L
1.0
1
05/13/14 03:50
75-34-3
1,1-Dichloroethene
67.7 ug/L
1.0
1
05/13/14 03:50
75-35-4
1,1,1-Trichloroethane
3.1 ug/L
1.0
1
05/13/14 03:50
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 03:50
79-00-5
1,1,2,2-Tetrachlorcethane
ND ug/L
1.0
1
05/13/14 03:50
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:50
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 03:50
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 03:50
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:50
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:50
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 03:50
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 03:50
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 03:50
75-25-2
cis-1,2-Dichloroethene
1.9 ug/L
1.0
1
05/13/14 03:50
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 03:50
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 03:50
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 03:50
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 03:50
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 03:50
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 03:50
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 03:50
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 03:50
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 03:50
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 03:50
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 03:50
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 03:50
127-18-4
Trichloroethene
64.9 ug/L
1.0
1
05/13/14 03:50
79-01-6
Trich lo roflu oro methane
ND ug/L
1.0
1
05/13/14 03:50
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 03:50
75-01-4
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
i
Page 20 of 44 j

�,AceAnalydcalo
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
- Sample:
le: DMW-6
Lab ID: 92200731011 Collected:
05/09/14 10:20
Received: 05/09/1413.12 Matrix. Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
- 601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 03:50
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
05/13/14 03:50
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
05/13/14 03:50
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
05/13/14 03:50
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S21)
Sulfide
ND mg/L
0.10
1
05/16/14 16:13
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
59.5 mg/L
4.0
2
05/15/14 17:11
14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/L
0.020
1
05/09/14 23:05
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
11.1 mg/L
1.0
1
05/13/14 20:28
7440-44-0
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 44

aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 +_
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: DMW 7 Lab ID: 92200731012 Collected: 05/09/14 11:00 Received: 05/09/14 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
RSK 176AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
05/16/14 12:42
74-84-0
Ethene
ND ug/L
6.2
1
05/16/14 12:42
74-85-1
Methane
15.8 ug/L
6.6
1
05/16/14 12:42
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
05/12/1415:45
05/13/1416:41
7440-38-2
Barium
52.4 ug/L
5.0
1
05/12/1415:45
05/13/1416:41
7440-39-3
Cadmium
ND ug/L
1.0
1
05/12/1415:45
05/13/1416:41
7440-43-9
Chromium
6.9 ug/L
5.0
1
05/12/1415:45
05/13/1416:41
7440-47-3
Lead
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:41
7439-92-1
Selenium
ND ug/L
10.0
1
05/12/1415:45
05/13/1416:41
7782-49-2
Silver
ND ug/L
5.0
1
05/12/1415:45
05/13/1416:41
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND. ug/L
0.20
1
05/12/14 23:00
05/14/14 18:47
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
05/13/14 02:44
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 02:44
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 02:44
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 02:44
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 02:44
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:44
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 02:44
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 02:44
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:44
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 02:44
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 02:44
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 02:44
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 02:44
75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 02:44
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 02:44
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 02:44
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 02:44
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 02:44
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 02:44
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 02:44
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 02:44
124-48-1
Dichlorodiftuoromethane
ND ug/L
1.0
1
05/13/14 02:44
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 02:44
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 02:44
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 02:44
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 02:44
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 02:44
79-01-6
TrichloroFluoromethane
ND ug/L
1.0
1
05/13/14 02:44
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 02:44
75-01-4
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qua[
Page 22 of 44 i

aceAnal dcal
J
www.pacelabs.com
i
I
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
- Sample: DMW 7
Lab ID: 92200731012 Collected:
05/09/14 11:00
Received: 05/09/14 13:12 Matrix:.Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 02:44
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
05/13/14 02:44
460-00-4
r
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
05/13/14 02:44
17060-07-0
Toluene-d8 (S)
102 %
70-130
1
05/13/14 02:44
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
05/16/14 16:13
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
4.4 mg/L
2.0
1
05/15/14 17:25
14808-79-8
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.18 mg/L
0.020
1
05/09/14 23:06
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
17.2 mg/L
1.0
1
05/13/14 20:55
7440-44-0
,Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 23 of 44

acmnalytical
www.pacelabs.com
Pace Analytical Services, Inc. -
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 -
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: DMW 8 Lab ID: 92200731013 Collected: 05/09/14 11:40 Received: 05/09/14 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 176 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
05/16/1412:53
74-84-0
Ethene
ND ug/L
6.2
1
05/16/1412:53
74-85-1
Methane
ND ug/L
6.6
1
05/16/1412:53
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
05/12/1415:45
05/13/14 16:44
7440-38-2
Barium
28.9 ug/L
5.0
1
05/12/1415:45
05/13/14 16:44
7440-39-3
Cadmium
ND ug/L
1.0
1
05/12/14 15:45
05/13/14 16:44
7440-43-9
Chromium
ND ug/L
5.0
1
05/12/1415:45
05/13/14 16:44
7440-47-3
Lead
ND ug/L
5.0
1
05/12/1415:45
05/13/14 16:44
7439-92-1
Selenium
ND ug/L
10.0
1
05/12/1415:45
05/13/14 16:44
7782-49-2
Silver
ND ug/L
5.0
1
05/12/1415:45
05/13/14 16:44
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
05/12/14 23:00
05/14/14 18:50
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
05/13/14 03:00
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 03:00
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 03:00
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 03:00
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 03:00
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:00
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 03:00
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 03:00
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:00
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:00
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 03:00
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 03:00
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 03:00
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 03:00
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 03:00
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 03:00
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 03:00
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 03:00
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 03:00
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 03:00
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 03:00
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 03:00
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 03:00
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 03:00
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 03:00
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 03:00
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 03:00
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
05/13/14 03:00
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 03:00
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/19/2014 12:16 PM without the written consent of Pace Analytical Services, Inc..
Page 24 of 44

aceAnalytical
-/ wwvapace/abs.ccm
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
oampie: uivivv-u
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (ED13)
Surrogates
— 4-Bromofluorobenzene (S)
j 1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
I1
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, N021NO3 unpres
— Nitrogen, Nitrate
5310B TOG
Total Organic Carbon
Date: 05/19/2014 12:16 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92200731013 Collected:
05/09/14 11:40
Received: 05/09/14 13:12 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: SM 6200B
ND ug/L
1.0
1
05/13/14 03:00
106-93-4
97 %
70-130
1
05/13/14 03:00
460-00-4
98 %
70-130
1
05/13/14 03:00
17060-07-0
101 %
70-130
1
05/13/14 03:00
2037-26-5
Analytical Method: SM 4500-S2D
ND mg/L
0.10
1
05/16/14 16:13
18496-25-8
Analytical Method: EPA 300.0
2.1 mg/L
2.0
1
05/15/1418:06
14808-79-8
Analytical Method: EPA 353.2
0.80 mg/L
0.020
1
05/09/14 23:07
Analytical Method: SM 5310B ,
3.4 mg/L
1.0
1
05/13/14 21:06
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Services, Inc..
Page 25 of 44

aceAnalytical
www.pacelabs,cam
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
Sample: SS-2 Lab ID: 92200731014 Collected: 05/09/14 11:50 Received: 05/09/14 13:12 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200 Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
05/13/14 03:17
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
05/13/14 03:17
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
05/13/14 03:17
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
05/13/14 03:17
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
05/13/14 03:17
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:17
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
05/13/14 03:17
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
05/13/14 03:17
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:17
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
05/13/14 03:17
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
05/13/14 03:17
75-27-4
Bromomethane
ND ug/L
5.0
1
05/13/14 03:17
74-83-9
Bromoform
ND ug/L
1.0
1
05/13/14 03:17
75-25-2
cis- 1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 03:17
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 03:17
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
05/13/14 03:17
56-23-5
Chlorobenzene
ND ug/L
1.0
1
05/13/14 03:17
108-90-7
Chloroethane
ND ug/L
1.0
1
05/13/14 03:17
75-00-3
Chloroform
ND ug/L
1.0
1
05/13/14 03:17
67-66-3
Chloromethane
ND ug/L
1.0
1
05/13/14 03:17
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
05/13/14 03:17
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
05/13/14 03:17
75-71-8
Methylene Chloride
ND ug/L
2.0
1
05/13/14 03:17
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
05/13/14 03:17
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
05/13/14 03:17
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
05/13/14 03:17
127-18-4
Trichloroethene
ND ug/L
1.0
1
05/13/14 03:17
79-01-6
Trich lorofluoro methane
ND ug/L
1.0
1
05/13/14 03:17
75-69-4
Vinyl chloride
ND ug/L
1.0
1
05/13/14 03:17
75-01-4
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
05/13/14 03:17
106-93-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
05/13/14 03:17
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
05/13/14 03:17
17060-07-0
Toluene-d8 (S)
99 %
70-130
1
05/13/14 03:17
2037-26-5
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 26 of 44

1111�IaceAnalydcal
j" wwwpace/abs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
-, Sample: WSW-4 Lab ID: 92200731015. Collected: 05/09/14 12:20 Received: 05/09/14 13:12 . Matrix: Water
__ Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
601 Volatiles by SM 6200
1,1-Dichloroethane
1,1-Dichloroethene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
1,1,2,2-Tetrachloroethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromomethane
Bromoform
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromoch loromethane
Dichlorodifluoromethane
Methylene Chloride
- trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Tetrachloroethene
Trichloroethene
Trichlo roflu oro methane
Vinyl chloride
1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 05/19/2014 12:16 PM
Analytical Method: SM 6200B
ND ug/L
1.0
1
05/13/14 03:34
75-34-3
ND ug/L
1.0
1
05/13/14 03:34
75-35-4
ND ug/L
1.0
1
05/13/14 03:34
71-55-6
ND ug/L
1.0
1
05/13/14 03:34
79-00-5
ND ug/L
1.0
1
05/13/14 03:34
79-34-5
ND ug/L
1.0
1
05/13/14 03:34
95-50-1
ND ug/L
1.0
1
05/13/14 03:34
107-06-2
ND ug/L
1.0
1
05/13/14 03:34
78-87-5
ND ug/L
1.0
1
05/13/14 03:34
541-73-1
ND ug/L
1.0
1
05/13/14 03:34
106-46-7
ND ug/L
1.0
1
05/13/14 03:34
75-27-4
ND ug/L
5.0
1
05/13/14 03:34
74-83-9
ND ug/L
1.0
1
05/13/14 03:34
75-25-2
ND ug/L
1.0
1
05/13/14 03:34
156-59-2
ND ug/L
1.0
1
05/13/14 03:34
10061-01-5
ND ug/L
1.0
1
05/13/14 03:34
56-23-5
ND ug/L
1.0
1
05/13/14 03:34
108-90-7
ND ug/L
1.0
1
05/13/14 03:34
75-00-3
ND ug/L
1.0
1
05/13/14 03:34
67-66-3
ND ug/L
1.0
1
05/13/14 03:34
74-87-3
ND ug/L
1.0
1
05/13/14 03:34
124-48-1
ND ug/L
1.0
1
05/13/14 03:34
75-71-8
ND ug/L
2.0
1
05/13/14 03:34
75-09-2
ND ug/L
1.0
1
05/13/14 03:34
156-60-5
ND ug/L
1.0
1
05/13/14 03:34
10061-02-6
ND ug/L
1.0
1
05/13/14 03:34
127-18-4
ND ug/L
1.0
1
05/13/14 03:34
79-01-6
ND ug/L
1.0
1
05/13/14 03:34
75-69-4
ND ug/L
1.0
1
05/13/14 03:34
75-01-4
ND ug/L
1.0
1
05/13/14 03:34
106-93-4
97 %
70-130
1
05/13/14 03:34
460-00-4
99 %
70-130
1
05/13/14 03:34
17060-07-0
100 %
70-130
1
05/13/14 03:34
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 27 of 44

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 I_ -
[phone]
QUALITY CONTROL DATA
Project: DOT--404 WBS#34613.3.26
Pace Project No.: 92200731
QC Batch: AIR/20267 Analysis Method: RSK 175
QC Batch Method: RSK 175 Analysis Description: RSK 175 AIR HEADSPACE
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009
METHOD BLANK: 1682230 Matrix: Water
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethane ug/L ND 6.2 05/15/14 20:22
Ethene ug/L ND 6.2 05/15/14 20:22
Methane ug/L ND 6.6 05/15/14 20:22
LABORATORY CONTROL SAMPLE & LCSD: 1682231
1682232
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter Units
Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Ethane ug/L
114
111 109
97 96
85-115 2 20
Ethene ug/L
106
103 102
97 96
85-115 1 20
Methane ug/L
60.7
60.0 ' 59.1
99 97
85-115 2 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1682233
1682234
MS
MSD
60168831004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
Ethane ug/L
ND
114
114
117
132
103
116
63-147
12
Ethene ug/L
ND
106
106
107
121
100
114
42-149
13
Methane ug/L
ND
60.7
60.7
64.4
72.0
101
114
30-150
11
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 28 of 44

aceAnalXical
www.pacelabs.com
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
QC Batch: AIR/20273 Analysis Method: RSK 175
QC Batch Method: RSK 175 Analysis Description: RSK 175 AIR HEADSPACE
Associated Lab Samples: 92200731010, 92200731011, 92200731012, 92200731013
METHOD BLANK: 1683130 Matrix: Water
Associated Lab Samples: 92200731010, 92200731011, 92200731012, 92200731013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethane
ug/L
ND
6.2
05/16/1411:41
Ethene
ug/L
ND
6.2
05/16/1411:41
Methane
ug/L
ND
6.6
05/16/1411:41
LABORATORY CONTROL SAMPLE & LCSD: 1683131
1683132
Spike
LCS
LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits
Ethane
ug/L
114
107
108
94 95
85-11
Ethene
ug/L
106
100
100
94 94
85-11
Methane
ug/L
60.7
58.1
58.1
96 96
85-11
SAMPLE DUPLICATE: 1683133
92200731010 Dup
Parameter Units Result Result RPD Qualifiers
- Ethane
ug/L
ND
ND
Ethene
ug/L
ND
ND
Methane
ug/L
2140
2620
_ REPORT OF LABORATORY ANALYSIS
_ This report shall not be reproduced, except in full,
'Date: 05/19/2014 12:16 PM without the written consent of Pace Analytical Services, Inc..
J
20
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD RPD Qualifiers
.5 20
.1 20
0 20
Page 29 of 44

�aceAnalXical
www.pacelabs.com
Pace Analytical Services, Inc. ,
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 ! _
[phone]
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
QC Batch: MERP/6595 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
METHOD BLANK: 1197002 Matrix: Water
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 05/14/1418:15
LABORATORY CONTROL SAMPLE: 1197003
Parameter Units
Mercury
ug/L
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.6 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1197004 1197005
MS MSD
92200731006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 1.8 1.8 73 70 75-125 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1197012 1197013
MS MSD
92200295015 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 1.8 1.8 73 72 75-125 1 M1
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 30 of 44

aceAnalylical0
7 www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 1oo
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
J Pace Project No.: 92200731
QC Batch: MPRP/15931
Analysis Method:
EPA 6010
QC Batch Method: EPA 3010
Analysis Description:
6010 MET
Associated Lab Samples: 92200731006, 92200731007. 92200731008, 92200731009,
92200731010, 92200731011. 92200731012,
92200731013
METHOD BLANK: 1196639
Matrix: Water
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009,
92200731010, 92200731011, 92200731012,
92200731013
Blank Reporting
_- Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
ug/L
ND
10.0 05/13/1415:56
Barium
ug/L
ND
5.0 05/13/1415:56
Cadmium
ug/L
ND
1.0 05/13/1415:56
Chromium
ug/L
ND
5.0 05/13/1415:56
Lead
ug/L
ND
5.0 05/13/1415:56
Selenium
ug/L
ND
10.0 05/1311415:56
Silver
ug/L
ND
5.0 05/13/1415:56
LABORATORY CONTROL SAMPLE:,
1196640
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Arsenic
ug/L
500 471
94 80-120
Barium
ug/L
500 475
95 80-120
Cadmium
ug/L
500 473
95 80-120
—, Chromium
ug/L
500 474
95 80-120
Lead
ug/L
500 481
96 80-120
Selenium
ug/L
500 468
94 80-120
Silver
ug/L
250 242
97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1196641
MS
92200731006
Spike
Parameter
Units
Result
Conc.
Arsenic
ug/L
ND
500
Barium
ug/L
59.8
500
Cadmium
ug/L
ND
500
Chromium
ug/L
ND
500
Lead
ug/L
ND
500
Selenium
ug/L
ND
500
Silver
ug/L
ND
250
Date: 05/19/2014 12:16 PM
1196642
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
490
490
98
98
75-125
0
500
541
549
96
98
75-125
1
500
483
494
97
99
75-125
2
500
486
497
97
99
75-125
2
500
485
493
97
99
75-125
2
500
470
487
94
97
75-125
4
250
248
253
99
.101
75-125
2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 31 of 44

aceAnalXical
www.pacelab&cam
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
QC Batch: MSW26782 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 601 by 6200B
Associated Lab Samples: 92200731001, 92200731002, 92200731003, 92200731004, 92200731005, 92200731006, 92200731007,
92200731008,92200731009,92200731010,92200731011,92200731012,92200731013,92200731014,
92200731015
METHOD BLANK: 1196800 Matrix: Water
Associated Lab Samples: 92200731001, 92200731002, 92200731003, 92200731004, 92200731005, 92200731006, 92200731007,
92200731008, 92200731009, 92200731010, 92200731011, 92200731012, 92200731013, 92200731014,
92200731015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1-Trichloroethane
ug/L
ND
1.0
05/12/14 23:42
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/12/14 23:42
1,1,2-Trichloroethane
ug/L
ND
1.0
05/12/14 23:42
1,1-Dichloroethane
ug/L
ND
1.0
05/12/14 23:42
1,1-Dichloroethene
ug/L
ND
1.0
05/12/14 23:42
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/12/14 23:42
1,2-Dichlorobenzene
ug/L
ND
1.0
05/12/14 23:42
1,2-Dichloroethane
ug/L
ND
1.0
05/12/14 23:42
1,2-Dichloropropane
ug/L
ND
1.0
05/12/14 23:42
1,3-Dichlorobenzene
ug/L
ND
1.0
05/12/14 23:42
1,4-Dichlorobenzene
ug/L
ND
1.0
05/12/14 23:42
Bromodichloromethane
ug/L
ND
1.0
05/12/14 23:42
Bromoform
ug/L
ND
1.0
05/12/14 23:42
Bromomethane
ug/L
ND
5.0
05/12/14 23:42
Carbon tetrachloride
ug/L
ND
1.0
05/12/14 23:42
Chlorobenzene
ug/L
ND
1.0
05/12/14 23:42
Chloroethane
ug/L
ND
1.0
05/12/14 23:42
Chloroform
ug/L
ND
1.0
05/12/14 23:42
Chloromethane
ug/L
ND
1.0
05/12/14 23:42
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/12/14 23:42
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/12/14 23:42
Dibromochloromethane
ug/L
ND
1.0
05/12/14 23:42
Dichlorodifluoromethane
ug/L
ND
1.0
05/12/14 23:42
Methylene Chloride
ug/L
ND
2.0
05/12/14 23:42
Tetrachloroethene
ug/L
ND
1.0
05/12/14 23:42
trans-1,2-Dichloroethene
ug/L
ND
1.0
05/12/14 23:42
trans-1,3-Dichloropropene
ug/L
ND
1.0
05/12/14 23:42
Trichloroethene
ug/L
ND
1.0
05/12/14 23:42
Trichlorofluoromethane
ug/L
ND
1.0
05/12/14 23:42
Vinyl chloride
ug/L
ND
1.0
05/12/14 23:42
1,2-Dichloroethane-d4 (S)
%
99
70-130
05/12/14 23:42
4-Bromofluorobenzene (S)
%
98
70-130
05/12/14 23:42
Toluene-d8 (S)
%
102
70-130
05/12/14 23:42
LABORATORY CONTROL SAMPLE: 1196801
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 50 53.1 106 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/19/2014 12:16 PM without the written consent of Pace Analytical Services, Inc..
� I
Page 32 of 44

�,AceAnalXical"
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
LABORATORY CONTROL SAMPLE: 1196801
Parameter
1,1,2,2-Tetrachloroethane
ug/L
1,1,2-Trichloroethane
ug/L
1,1-Dichloroethane
ug/L
1,1-Dichloroethene
ug/L
1,2-Dibromoethane (EDB)
ug/L
1,2-Dichlorobenzene
ug/L
1,2-Dichloroethane
ug/L
1,2-Dichloropropane
ug/L
j 1,3-Dichlorobenzene
ug/L
1,4-Dichlorobenzene
ug/L
Bromodichloromethane
ug/L
Bromoform
ug/L
Bromomethane
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroethane
ug/L
Chloroform
ug/L
Chloromethane
ug/L
cis- 1,2-Dichloroethene
ug/L
cis-1,3-Dichloropropene
ug/L
Dibromochloromethane
ug/L
Dichlorodifluoromethane
ug/L
Methylene Chloride
ug/L
Tetrachloroethene
ug/L
trans-1,2-Dichloroethene
ug/L
trans-1,3-Dichloropropene
ug/L
Trichloroethene
ug/L
Trichlorofluoromethane
ug/L
vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
Units
QUALITY CONTROL DATA
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
50.
52.5
105
60-140
50
51.8
104
60-140
50
50.7
101
60-140
50
50.6
101
60-140
50
51.2
102
60-140
50
50.2
100
60-140
50
52.2
104
60-140
50
50.1
100
60-140
50
48.7
97
60-140
50
48.2
96
60-140
50
52.9
106
60-140
50
45.1
90
60-140
50
41.5
83
60-140
50
53.3
107
60-140
50
48.0
96
60-140
50
46.9
94
60-140
50
50.1
100
60-140
50
51.6
103
60-140
50
50.6
101
60-140
50
53.6
107
60-140
50
44.3
89
60-140
50
52.8
106
60-140
50
54.0
108
60-140
50
50.0
100
60-140
50
51.4
103
60-140
50
47.4
95
60-140
50
53.0
106
60-140
50
46.5
93
60-140
50
58.0
116
60-140
100
70-130
99
70-130
99
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1197169
l
MS
Parameter
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
Date: 05/19/2014 12:16 PM
92200731001
Spike
Units
Result
Conc.
ug/L
ND
20
ug/L
ND
20
ug/L
ND
20
ug/L
ND
20
ug/L
ND
20
ug/L
ND
20
ug/L
ND
20
ug/L
ND
20
ug/L
ND
20
ug/L
ND
20
Qualifiers
MSD
Spike
Conc.
1197170
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
20
24.3
24.4
121
122
60-140
1
20
22.3
22.9
112
114
60-140
2
20
23.1
23.2
115
116
60-140
1
20
22.4
22.5
112
113
60-140
1
20
23.8
23.7
119
118
60-140
1
20
22.2
22.2
111
111
60-140
0
20
22.4
21.9
112
110
60-140
2
20
22.8
22.9
114
114
60-140
0
20
22.6
22.7
113
114
60-140
1
20
22.3
21.7
112
108
60-140
3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 33 of 44

aceAnalytical
xawipacelabs.cam
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 L_
[phone]
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1197169
MS
92200731001
Spike
Parameter
Units
Result
Conc.
1,4-Dichlorobenzene
ug/L
ND
20
Bromodichloromethane
ug/L
ND
20
Bromoform
ug/L
ND
20
Bromomethane
ug/L
ND
20
Carbon tetrachloride
ug/L
ND
20
Chlorobenzene
ug/L
ND
20
Chloroethane
ug/L
ND
20
Chloroform
ug/L
ND
20
Chloromethane
ug/L
ND
20
cis-1,2-Dichloroethene
ug/L
ND
20
cis-1,3-Dichloropropene
ug/L
ND
20
Dibromochloromethane
ug/L
ND
20
Dichlorodifluoromethane
ug/L
ND
20
Methylene Chloride
ug/L
ND
20
Tetrachloroethene
ug/L
ND
20
trans-1,2-Dichloroethene
ug/L
ND
20
trans-1,3-Dichloropropene
ug/L
ND
20
Trichloroethene
ug/L
ND
20
Trichlorofluoromethane
ug/L
ND
20
Vinyl chloride
ug/L
ND
20
1,2-Dichloroethane-d4 (S)
%
4-13romofluorobenzene (S)
%
Toluene-d8 (S)
%
Date: 05/19/2014 12:16 PM
1197170
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result .
% Rec
% Rec
Limits
RPD
20
22.1
21.5
110
108
60-140
2
20
23.3
23.3
116
116
60-140
0
20
19.4
19.5
97
97
60-140
1
20
18.7
17.9
93
89
60-140
4
20
26.3
26.2
132
131
60-140
1
20
21.7
21.4
109
107
60-140
1
20
21.3
21.7
107
108
60-140
2
20
22.4
22.4
112
112
60-140
0
20
15.2
17.1
76
85
60-140
11
20
22.3
22.5
112
113
60-140
1
20
23.4
23.5
117
117
60-140
1
20
20.1
19.8
100
99
60-140
1
20
23.1
22.9
115
114
60-140
1
20
21.8
22.3
109
112
60-140
3
20
23.9
23.8
120
119
60-140
0
20
23.6
23.3
118
117
60-140
1
20
20.7
21.0
104
105
60-140
1
20
24.9
24.7
125
124
60-140
1
20
23.8
23.4
119
117
60-140
2
20
25.6
25.3
128
127
60-140
1
98
97
70-130
101
100
70-130
100
101
70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, Inc..
Qua[
Page 34 of 44

Pace Analytical Services, Inc.
® 9800 Kincey Ave. Suite 100
6,PaceAnalyical Huntersville, NC 28078
/ www.pacelabs.com [phone]
1
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
QC Batch: WET/31071 Analysis Method: SM 4500-S2D
QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
METHOD BLANK: 1200824 Matrix: Water
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide mg/L ND 0.10 05/16/1416:13
LABORATORY CONTROL SAMPLE: 1200825
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide mg/L .5 0.53 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1200826
1200827
MS
MSD
92200731006 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Sulfide mg/L ND .5
.5
0.44
0.44
88
88
75-125
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1200828
1200829
MS
MSD
92201026007 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Sulfide mg/L ND .5
.5
0.49
0.49
98
98
75-125
0
9 �
I
V
I
�0ate: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 35 of 44

Pace Analytical
Services, Inc. ,-
®
aceAnalydcal
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www..pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
QC Batch: WETA/18970
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92200731006, 92200731007,
92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
METHOD BLANK: 1196860
Matrix: Water
Associated Lab Samples: 92200731006, 92200731007,
92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Sulfate mg/L
ND 2.0 05/15/1413:47
LABORATORY CONTROL SAMPLE: 1196861
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Sulfate mg/L
20 18.9 95 90-110
I
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1196862 1196863
MS MSD
92200594001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits
RPD Qual
Sulfate mg/L ND
20 20 20.4 20.3 96 96
90-110
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1196864 1196865
-
MS MSD
92200731012
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits
RPD Qua[
Sulfate mg/L 4.4
20 20 23.4 23.5 95 95
90-110
0
i
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 36 of 44

Pace Analytical Services, Inc.
® 9800 Kincey Ave. Suite 100
aceAnalyica! Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
QC Batch: WETA/18950 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
METHOD BLANK: 1196199 Matrix: Water
Associated Lab Samples: 92200731006, 92200731007, 92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
-- 92200731013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.020 05/09/14 22:46
i
LABORATORY CONTROL SAMPLE: 1196200
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 2.5 2.5 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1196201 1196202
MS MSD
92200295015 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate m9 /L 0.040 2.5 2.5 2.2 2.2 86 87 90-110 1 M1
'L
'Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 37 of 44

Pace Analytical Services, Inc.
®
aceAnalytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelab.com
[phone]
QUALITY CONTROL DATA
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731.
QC Batch: WETA/18972
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92200731006, 92200731007,
92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
METHOD BLANK: 1196879
Matrix: Water
Associated Lab Samples: 92200731006, 92200731007,
92200731008, 92200731009, 92200731010, 92200731011, 92200731012,
92200731013
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0 05/13/14 17:32
i
LABORATORY CONTROL SAMPLE: 1196880
Spike LCS LCS % Rec
i
Parameter Units
Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L
25 24.8 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1196881 1196882
MS MSD
92200563001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits
RPD Qua[
Total Organic Carbon mg/L 2.3
25 25 27.0 27.1 99 99
75-125
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1196883 1196884
MS MSD
92200731011
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits
RPD Qual
Total Organic Carbon mg/L 11.1
25 25 34.9 34.4 95 93
75-125
1
Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 38 of 44

aceAna,(Xical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: DOT-404 WBS#34613.3.26
Pace Project No.: 92200731
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
- ' PRL - Pace Reporting Limit.
i RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-M Pace Analytical Services - Minneapolis
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
!Date: 05/19/2014 12:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 39 of 44

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DOT 404 WBS#34613.3.26
Pace Project No.: 92200731
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92200731006
DMW 1
RSK 175
AIR/20267
92200731007
DMW-2
RSK 175
AIR/20267
92200731008
DMW 9
RSK 175
AIR/20267
92200731009
DMW-10
RSK 175
AIR/20267
92200731010
DMW 11
RSK 175
AIR/20273
92200731011
DMW-6
RSK 175
AIR/20273
92200731012
DMW-7
RSK 175
AIR/20273
92200731013
DMW-8
RSK 175
AIR/20273
92200731006
DMW 1
EPA 3010
MPRP/15931
EPA 6010
92200731007
DMW 2
EPA 3010
MPRP/15931
EPA 6010
92200731008
DMW 9
EPA 3010
MPRP/15931
EPA 6010
92200731009
DMW 10
EPA 3010
MPRP/15931
EPA 6010
92200731010
DMW 11
EPA 3010
MPRP/15931
EPA 6010
92200731011
DMW 6
EPA 3010
MPRP/15931
EPA 6010
92200731012
DMW 7
EPA 3010
MPRP/15931
EPA 6010
92200731013
DMW-8
EPA 3010
MPRP/15931
EPA 6010
92200731006
DMW-1
EPA 7470
MERP/6595
EPA 7470
92200731007
DMW2
EPA 7470
MERP/6595
EPA 7470
92200731008
DMW9
EPA 7470
MERP/6595
EPA 7470
92200731009
DMW 10
EPA 7470
MERP/6595
EPA 7470
92200731010
DMW-11
EPA 7470
MERP/6595
EPA 7470
92200731011
DMW-6
EPA 7470
MERP/6595
EPA 7410
92200731012
DMW7
EPA 7470
MERP/6595
EPA 7470
92200731013
DMW 8
EPA 7470
MERP/6595
EPA 7470
92200731001
DMW 3
SM 6200E
MSV/26782
92200731002
DMW-4
SM 6200E
MSV/26782
92200731003
SMW-3
SM 6200E
MSV/26782
92200731004
SMW-2
SM 6200E
MSV/26782
92200731005
SMW 1
SM 6200B
MSV/26782
92200731006
DMW 1
SM 6200E
MSV/26782
92200731007
DMW2
SM 6200B
MSV/26782
92200731008
DMW-9
SM 6200B
MSV/26782
92200731009
DMW-10
SM 6200B
MSV/26782
92200731010
DMW-11
SM 6200B
MSV/26782
92200731011
DMW-6
SM 6200B
MSV/26782
92200731012
DMW7
SM 6200B
MSV/26782
92200731013
DMW-8
SM 6200B
MSV/26782
92200731014
SS-2
SM 6200B
MSV/26782
92200731015
WSW-4
SM 6200B
MSV/26782
92200731006
DMW-1
SM 4500-S2D
WET/31071
92200731007
DMW-2
SM 4500-S2D
WET/31071
92200731008
DMW-9
SM 4500-S2D
WET/31071
92200731009
DMW-10
SM 4500-S2D
WET/31071
92200731010
DMW-11
SM 4500-S2D
WET/31071
92200731011
DMW-6
SM 4500-S2D
WET/31071
92200731012
DMW-7
SM 4500-S2D
WET/31071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/19/2014 12:16 PM without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/14416
ICP/14416
ICP/14416
ICP/14416
ICP/14416
ICP/14416
ICP/14416
ICP/14416
MERC/6359
MERC/6359
MERC/6359
MERC/6359
MERC/6359
MERC/6359
MERC/6359
MERC/6359
Page 40 of 44 1

r aceAnal�/�'lcal
J`
j' www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 10o
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DOT-404 WBS#34613.3.26
—' Pace Project No.: 92200731
Lab ID
92200731013
92200731006
92200731007
92200731008
92200731009
92200731010
92200731011
92200731012
- 92200731013
92200731006
92200731007
-- 92200731008
92200731009
92200731010
92200731011
92200731012
92200731013
92200731006
- 92200731007
92200731008
92200731009
92200731010
92200731011
92200731012
92200731013
Sample ID
DMW-8
DMW 1
DMW-2
DMW-9
DMW 10
DMW 11
DMW-6
DMW 7
DMW-8
DMW-1
DMW-2
DMW 9
DMW-10
DMW-11
DMW-6
DMW-7
DMW-8 .
DMW 1
DMW 2
DMW-9
DMW-10
DMW 11
DMW 6
DMW-7
DMW 8
)ate: 05/19/2014 12:16 PM
QC Batch Method
SM 4500-S2D
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
EPA 353.2
SM 5310B
SM 5310B
SM 5310B
SM 5310B
SM 5310B
SM 5310B
SM 5310B
SM 5310B
QC Batch Analytical Method
WET/31071
WETA/18970
WETA/18970
WETA/18970
WETA/18970
WETA/18970
WETA/18970
WETA/18970
WETA/18970
WETA/18950
WETA/18950
WETA/18950
WETA/18950
WETA/18950
WETA/18950
WETA/18950
WETA/18950
WETA/18972
WETA/18972
WETA/18972
WETA/18972
WETA/18972
WETA/18972
WETA/18972
WETA/18972
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 41 of 44

�,,lceAftalytical` sample Condition Upon Receipt SCUR
j Document Number:
F-CHR-CS-003-rev.14
Client Name:��
Page 1 of 2
Issuing Authority:
Pace Huntersville Quality Office
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ gLePt❑ Commercial[] Pace Other
Custody Seat on Cooler/Box Present: ❑ yes ❑L2 Seals intact: ❑ yes ❑ no
f '
Packing Material: ❑ Bubble Wrap ❑ BubblOB gs ❑ None ❑ Other
Thermometer Used: IR Gun T1102 T 40 Type of Ice: � Blue None Samples on ice, cooling process has begun
Tamn Cnrrpctinn Factnr T11n9- Kin (nrrartinn T13n1• Nn r.nrrartinn
�C
Corrected Cooler Temp.:Biological
Tissue is Frozen: Yes
No N/A
Date and Initials of person examining
contents:
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
--UYes
❑No
El N/A
1.
Chain of Custody Filled Out:
---Dryes
❑No
❑NIA
2.
Chain of Custody Relinquished:
Yes
❑No
❑N/A
3.
Sampler Name & Signature on COC:
Yes
❑No
❑N/A
4.
Samples Arrived within Hold Time:
des
El No
❑N/A
5.
Short Hold Time Analysis (<72hr):
--ffYes
❑�Noo
ON/A
6.
Rush Turn Around Time Requested:
❑Yes
CWo-
LJN/A
7.
Sufficient Volume:
es
❑No
❑NIA
8. ` Z,. 1�
-�`t<<�'( E''0-i'
Correct Containers Used:
des
❑No
❑N/A
9. c' (Vy-
-Pace Containers Used:
- Yes
❑No
❑NIA
Containers Intact:
-t:IYes
❑No
❑N/A
10.
Filtered- volume received for -Dissolved tests----
- ❑Yes -❑No
-E191A
1T. -
- - -
Sample Labels match COC:
es ❑No
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
s
❑No
❑NIA
13.
/� tev
A/%
,
All containers needing preservation are found to be in
❑Peso
❑N/A
compliance with EPA recommendation.
/t
exceptions: VOA, coliform, TOC, 0&G, WI•DRO (water)
/LIYes
❑No
Samples checked for dechlorination:
Yes
❑_No❑N/A
14.
Headspace in VOA Vials (>6mm):
❑Yes..EIwNo ❑_NIA
15.
Trip Blank Present:
❑Yes
[]No
" N/A
16.
Trip Blank Custody Seals Present
❑Yes
❑No
❑
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
Date/Time:
SCURF Review: Date: I
SRF Review: Date:
Note: Whenever th r . a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
Field Data Required? Y / N
Page 42 of 44

CHAIWOF-CUSTODY / Analytical Request Document
f .•ceAnalyt/eal The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
0
M
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Section A Section B Section C
Page: of
Required Client Information: Required Project Information: Invoice Information:
�w
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8 . '6 4 3 4
-ompany:
Report To:
Attention:
Y� L'F!`G�Ecica
, `
4ddress:. 9�i
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Copy To:
Company Name:
j /
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REGULATORY AGENCY
03
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1 NPDES f GROUND WATER gBkDRINKING WATER
I" UST I- RCRA I OTHER
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Project Name:
Pace PrcJe
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Manager.
STATE:
/.
Requested Due DaterrAT:s
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Project Number:
"
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(Y/N)
Section D Matrix Codes
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_
_...._........ ... ,,. r--ALL-Q-020rev.07, 15-May-2007

,a ceAnalXical °
www.pacelabs.com
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
1
l
0
v
Section A Section B Section C Page: cc` -of D
Required Client Information: Required Project Information: Invoice Inftrmation:
Company /L ate. ro Report To: Attention:1806433
Address: a e L e 6
loL3 5. P otrL S� S4 , Copy To: Company lame: l
14 REGULATORY AGENCY
Address: —NPDES F6-'1 ROUND WATER j DRINKING WATER
Email Toss �(r� �.G Purchase Order No.: Pace Quote '
e Reference: I F' UST r— RCRA IF OTHER
Phone: Fax: Project Name: Pace Project)
04 - - d Manager. Site Location
Requested Due Date1TAT: N Project Number: Pace Profile # ,t-A ware:
Gs.•'
Requested
Analysis
Filtered
(Y/N)
j
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Required Client Information MATRIX / CODE
Drinking Water DW
Water WT
Waste Water WW
Product P
Soil/Solid St.
SAMPLE ID oil e wP
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(A-Z, 0.9 / ;) Air AR
Sample IDs MUST BE UNIQUE Tissue TS
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SIGNATURE of SAMPLER:
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�AeAnalydcal
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 12, 2014
Chemical Testing Engineer
NCDOT
Materials & Tests Unit
1801 Blue Ridge Road
Raleigh, NC 27607
RE: Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Dear Chemical Engineer:
Enclosed are the analytical results for sample(s) received by the laboratory on July 31, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Per client request, report revised 11/12/14 to remove EPA 602 results and report EPA 601 results.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
J",g!� -
Kevin Godwin
[e-mail]
Project Manager
Enclosures
�e pCCRFO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 33

aceAnalyiical
wmpacelabs.com
Pace Analytical Services, Inc. -
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Huntersville, NC 28078
[phone]
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
A21-A Certification #: 2926.01
Alaska Certification #: UST-078
Alaska Certification #MN00064
Alabama Certification #40770
Arizona Certification M AZ-0014
Arkansas Certification #: 88-0680
California Certification #: 01155CA
Colorado Certification #Pace
Connecticut Certification M PH-0256
EPA Region 8 Certification #: 8TMS-L
Florida/NELAP Certification M E87605
Guam Certification #:14-008r
Georgia Certification #: 959
Georgia EPD #: Pace
Idaho Certification M MN00064
Hawaii Certification #MN00064
Illinois Certification #: 200011
Indiana Certification#C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky Dept of Envi. Protection - DW #90062
Kentucky Dept of Envi. Protection - WW #:90062
Louisiana DEQ Certification #: 3086
Louisiana DHH #: LA140001
Maine Certification #: 2013011
Maryland Certification #: 322
Michigan DEPH Certification #: 9909
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Minnesota Certification #: 027-053-137
Mississippi Certification M Pace
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Ohio EPAM 4150
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Puerto Rico Certification
Saipan (CNMI) #:MP0003
South Carolina #:74003001
Texas Certification M T104704192
Tennessee Certification #: 02818
Utah Certification * MN000642013-4
Virginia DGS Certification M 251
Virginia/VELAP Certification M Pace
Washington Certification #: C486
West Virginia Certification #: 382
West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
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REPORT OF LABORATORY ANALYSIS
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aV� /I��'r��J�
lily I (
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: DOT NO 2-66 WBS#34613.3.26
- Pace Project No.: 92211527
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92211527001 DMW-10
RSK 175
JRB
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
HVK
1
PASI-A
SM 6200E
MCK
33
PASI-C
SM 4500-S21)
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
-
EPA 353.2
DMN
1
PASI-A
SM 5310E
SAE
1
PASI-A
92211527002 DMW 11
RSK 175
JRB
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
HVK
1
PASI-A
SM 6200B
MCK
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310E
SAE
1
PASI-A
92211527003 DMW-2
RSK 175
JRB
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
HVK
1
PASI-A
SM 6200B
MCK
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
92211527004 DMW 1
RSK 175
JRB
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
HVK
1
PASI-A
_
SM 6200E
MCK
33
PASI-C
SM 4500-S21)
SAE
1
PASI-A
EPA 300.0
SAE
1
PASI-A
-
EPA 353.2
DMN
1
PASI-A
SM 5310B
SAE
1
PASI-A
92211527005 DMW 8
RSK 175
JRB
3
PASI-M
EPA 6010
JMW
7
PASI-A
EPA 7470
HVK
1
PASI-A
SM 6200E
MCK
33
PASI-C
SM 4500-S2D
SAE
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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aceAnalydcal
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Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Lab ID Sample ID
92211627006 DMW 6
92211627007 DMW 7
SAMPLE ANALYTE COUNT
Method
EPA 300.0
EPA 353.2
SM 5310B
RSK 175
EPA 6010
EPA 7470
SM 6200B
SM 4500-S21)
EPA 300.0
EPA 353.2
SM 5310B
RSK 175
EPA 6010
EPA 7470
SM 6200B
SM 4500-S21)
EPA 300.0
EPA 353.2
SM 5310B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytes
Analysts Reported Laboratory
SAE
1
PASI-A —
DMN
1
PASI-A
SAE
1
PASI-A
JRB
3
PASI-M
JMW
7
PASI-A
HVK
1
PASI-A
MCK
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
DMN
1
PASI-A
SAE
1
PASI-A
JRB
3
PASI-M
JMW
7
PASI-A
HVK
1
PASI-A
MCK
33
PASI-C
SAE
1
PASI-A
SAE
1
PASI-A
DMN
1
PASI-A
SAE
1
PASI-A
Page 4 of 33

�AceAnalytical
www.pacelabs.com
I �-
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT NO 2-66 WBS#34613.3.26
—� Pace Project No.: 92211527
Sample. DMW-10
Lab ID: 92211627001 Collected:
07/30/14 10:00
Received: 07/31/14 16:40 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
08/05/14 18:29
106-93-4
Surrogates
4-Bromofluorobenzene (S)
129 %
70-130
1
08/05/14 18:29
460-00-4
1,2-Dichloroethane-d4 (S)
87 %
70-130
1
08/05/14 18:29
17060-07-0
Toluene-d8 (S)
103 %
70-130
1
08/05/14 18:29
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
08/05/14 15:48
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
17.6 mg/L
2.0
1
08/06/14 18:53
14808-79-8
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/L
0.020
1
07/31/14 21:48
M1
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
27.9 mg/L
1.0
1
08/05/14 19:59
7440-44-0
Date: 11 /12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page 6 of 33

Pace Analytical Services, Inc.
®
a9800Suite
ceAnalytca! Huntesvile, NC
`
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW-10 Lab ID: 92211527001 Collected: 07/3011410:00 Received: 07/31/1416:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
RSK 175 AIR Headspace
Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
08/04h414:56
74-84-0
Ethene
ND ug/L
6.2
1
08/04/14 14:56
74-85-1
Methane
1160 ug/L
6.6
1
08/04/14 14:56
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:05
7440-38-2
Barium
143 ug/L
5.0
1
08/01/14 15:35
08/05/14 00:05
7440-39-3
Cadmium
ND ug/L
1.0
1
08/01/14 15:35
08/05/14 00:05
7440-43-9
Chromium
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:05
7440-47-3
Lead
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:05
7439-92-1
Selenium
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:05
7782-49-2
Silver
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:05
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
Q.20
1
08/01/1412:45
08/01/1415:29
7439-97-6 M1
601.Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
08/05/14 18:29
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
08/05/14 18:29
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
08/05/14 18:29
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
08/05/14 18:29
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
08/05/14 18:29
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
08105/1418:29
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
08/05/14 18:29
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
08/05/14 18:29
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 18:29
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 18:29
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
08/05/14 18:29
75-27-4
Bromomethane
ND ug/L
5.0
1
08/05/14 18:29
74-83-9
Bromoform
ND ug/L
1.0
1
08/05/14 18:29
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
08/0511418:29
156-59-2
cis- 1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 18:29
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
08/05/14 18:29
56-23-5
Chlorobenzene
NO ug/L
1.0
1
08/05/14 18:29
108-90-7
Chloroethane
ND ug/L
1.0
1
08/05/14 18:29
75-00-3
Chloroform
ND ug/L
1.0
1
08/05/14 18:29
67-66-3
Chloromethane
ND ug/L
1.0
1
08/05/14 18:29
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
08/05/14 18:29
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
08105/1418:29
75-71-8
Methylene Chloride
ND ug/L
2.0
1
08/05/14 18:29
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 18:29
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 18:29
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
08/05/14 18:29
127-18-4 .
Trichloroethene
ND ug/L
1.0
1
08/05/14 18:29
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
08/05/14 18:29
75-69-4
Vinyl chloride
ND ug/L
1.0
1
08/05/14 18:29
75-01-4
Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 33

l �'�,aceAnal�/�'ical
J`
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
�P►LL�'f�C�l_�T���1_ri��
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211627
- Sample: DMW-11 Lab ID: 92211527002 Collected: 07/30/14 12:30 Received: 07/31/14 16:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace
Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
08/04/14 16:11
74-84-0
Ethene
ND ug/L
6.2
1
08/04/14 16:11
74-85-1
Methane
4070 ug/L
6.6
1
08/04/14 16:11
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:17
7440-38-2
- Barium
69.5 ug/L
5.0
1
08/01/14 15:35
08/05/14 00:17
7440-39-3
Cadmium
ND ug/L
1.0
1
08/01/14 15:35
08/05/14 00:17
7440-43-9
Chromium
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:17
7440-47-3
Lead
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:17
7439-92-1
Selenium
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:17
7782-49-2
Silver
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:17
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation
Method: EPA 7470
j Mercury
ND ug/L
0.20
1
08/01/1412:45
08/01/1415:37
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
8.6 ug/L
1.0
1
08/05/14 18:46
75-34-3
1,1-Dichloroethene
11.0 ug/L
1.0
1
08/05/14 18:46
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
08/05/14 18:46
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
08/05/14 18:46
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
08/05/14 18:46
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
08105/1418:46
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
08/05/14 18:46
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
08/05/14 18:46
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 18:46
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 18:46
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
08/05/14 18:46
75-27-4
Bromomethane
ND ug/L
5.0
1
08/05/14 18:46
74-83-9
Bromoform
ND ug/L
1.0
1
08/05/14 18:46
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 18:46
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 18:46
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
08/05/14 18:46
56-23-5
Chlorobenzene
ND ug/L
1.0
1
08/05/14 18:46
108-90-7
Chloroethane
ND ug/L
1.0
1
08/05/14 18:46
75-00-3
Chloroform
ND ug/L
1.0
1
08105/1418:46
67-66-3
Chloromethane
ND ug/L
1.0
1
08/05/14 18:46
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
08/05/14 18:46
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
08/05/14 18:46
75-71-8
Methylene Chloride
ND ug/L
2.0
1
08/05/14 18:46
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 18:46
156-60-5
' trans-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 18:46
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
08/05/14 18:46
127-18-4
Trichloroethene
7.9 ug/L
1.0
1
08/05/14 18:46
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
08/0511418:46
75-69-4
Vinyl chloride
ND ug/L
1.0
1
08/05/14 18:46
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2014 12:36 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 33

aceAnalytical
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Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW-11
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S2D Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
5310B TOC
Total Organic Carbon
Date: 11/12/2014 12:36 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92211527002 Collected:
07/30/14 12:30
Received: 07/31/1416:40 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qua[
Analytical Method: SM 6200B
ND ug/L
1.0
1
08/05/14 18:46
106-93-4
126 %
70-130
1
08/05/14 18:46
460-00-4 -
88 %
70-130
1
08/05/14 18:46
17060-07-0
104 %
70-130
1
08/05/14 18:46
2037-26-5 -
Analytical Method: SM 4500-S2D
-,
ND mg/L
0.10
1
08/05/14 15:48
18496-25-8
Analytical Method: EPA 300.0
80.3 mg/L 10.0 5 08/06/14 19:06 14808-79-8
Analytical Method: EPA 353.2
ND mg/L 0.020 1 07/31/14 21:58
Analytical Method: SM 5316B
21.9 mg/L 1.0 1 08/05/14 20:10 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 33

/AeAnalytical
/ www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW 2 Lab ID: 92211527003 Collected: 07/30/14 13:20 Received: 07/31/14 16:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
i Ethane
ND ug/L
6.2
1
08/04/14 16:23
74-84-0
Ethene
ND ug/L
6.2
1
08/04/1416:23
74-85-1
Methane
ND ug/L
6.6
1
08104/1416:23
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation
Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:20
7440-38-2
Barium
28.2 ug/L
5.0
1
08/01/14 15:35
08/05/14 00:20
7440-39-3
Cadmium
ND ug/L
1.0
1
08/01/14 15:35
08/05/14 00:20
7440-43-9
" Chromium
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:20
7440-47-3
Lead
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:20
7439-92-1
Selenium
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:20
7782-49-2
Silver
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:20
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
08/01/14 12:45
08/01/14 15:39
.7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
1.1 ug/L
1.0
1
08/05/14 19:03
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
08/05/14 19:03
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
08/05/14 19:03
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
08/05/14 19:03
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
08/05/14 19:03
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 19:03
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
08/05/14 19:03
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
08/05/14 19:03
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
08105/1419:03
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 19:03
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
08/05/14 19:03
75-27-4
Bromomethane
ND ug/L
5.0
1
08/05/14 19:03
74-83-9
Bromoform
ND ug/L
1.0
1
08/05/14 19:03
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 19:03
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 19:03
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
08/05/14 19:03
56-23-5
Chlorobenzene
ND ug/L
1.0
1
08/05/14 19:03
108-90-7
Chloroethane
ND ug/L
1.0
1
08/05/14 19:03
75-00-3
Chloroform
ND ug/L
1.0
1
08/05/14 19:03
67-66-3
Chloromethane
ND ug/L
1.0
1
08/05/14 19:03
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
08/05/14 19:03
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
08/05/14 19:03
75-71-8
Methylene Chloride
ND ug/L
2.0
1
08/05/14 19:03
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 19:03
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 19:03
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
08/05/14 19:03
127-18-4
Trichloroethene
ND ug/L
1.0
1
08/05/14 19:03
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
08/05/14 19:03
75-69-4
Vinyl chloride
ND ug/L
1.0
1
08/05/14 19:03
75-01-4
j :Date: 11/12/201412:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 33

aceAnalytical
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Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW-2
Parameters
601 Volatiles by SM 6200
1,2-Dibromoethane (EDB)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4500S213 Sulfide Water
Sulfide
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
5310E TOC
Total Organic Carbon
Date: 11/12/2014 12:36 PM
ANALYTICAL RESULTS
Lab ID: 92211527003 Collected: 07/30/14 13:20
Received: 07/31/14 16:40 Matrix: Water
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: SM 6200B
ND ug/L
1.0
1
08/05/14 19:03
106-93-4
127 %
70-130
1
08/05/14 19:03
460-00-4
87 %
70-130
1
08/05/14 19:03
9 03
17060-07-0
2037 26 5
102 /o
70-130
1
08/05/1-t - -
Analytical Method: SM 4500-S213
ND mg/L
0.10
1
08/05/1415:48 18496-25-8
Analytical Method: EPA 300.0
81.8 mg/L
10.0
5
08/06/14 19:20 14808-79-8
Analytical Method: EPA 353.2
2.3 mg/L
0.020
1
07/31/14 21:59
Analytical Method: SM 5310B
5.8 mg/L
1.0
1
08/05/14 20:24 7440A4-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�I
i I
� I
Page 10 of 33

�AeAnalyfical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
VO4)875-9092
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW 1 Lab ID: 92211527004 Collected: 07/30/14 15:00 Received: 07/31/14 16:40 Matrix:.Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
08/04/1416:34
74-84-0
Ethene
ND ug/L
6.2
1
08/04/1416:34
74-85-1
- Methane
10.2 ug/L
6.6
1
08/04/14 16:34
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:23
7440-38-2
Barium
61.8 ug/L
5.0
1
08/01/14 15:35
08/05/14 00:23
7440-39-3
Cadmium
ND ug/L
1.0
1
08/01/14 15:35
08/05/14 00:23
7440-43-9
Chromium
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:23
7440-47-3
Lead
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:23
7439-92-1
Selenium
NO ug/L
10.0
1
08/01/14 15:35
08/05/14 00:23
7782-49-2
Silver
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:23
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
08101/1412:45
08/01/1415:42
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
4.2 ug/L
1.0
1
08105/1419:20
75-34-3
i 1,1-Dichloroethene
1.3 ug/L
1.0
1
08/05/14 19:20
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
0810511419:20
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
08/05/14 19:20
79-00-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
08105/1419:20
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 19:20
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
08/05/14 19:20
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
08/05/14 19:20
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
08105/1419:20
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 19:20
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
08/05/14 19:20
75-27-4
Bromomethane
ND ug/L
5.0
1
08/05/14 19:20
74-83-9
Bromoform
ND ug/L
1.0
1
08/05/14 19:20
75-25-2
cis-1,2-Dichloroethene
3.6 ug/L
1.0
1
08/05/14 19:20
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 19:20
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
08/05/14 19:20
56-23-5
Chlorobenzene
ND ug/L
1.0
1
08/05/14 19:20
108-90-7
Chloroethane
ND ug/L
1.0
1
08/05/14 19:20
75-00-3
Chloroform
ND ug/L
1.0
1
08/05/14 19:20
67-66-3
Chloromethane
ND ug/L
1.0
1
08/05/14 19:20
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
08/05/14 19:20
124-48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
08/05/14 19:20
75-71-8
Methylene Chloride
ND ug/L
2.0
1
08/05/14 19:20
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 19:20
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 19:20
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
08/05/14 19:20
127-18-4
Trichloroethene
2.1 ug/L
1.0
1
08/05/14 19:20
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
08105/1419:20
75-69-4
Vinyl chloride
ND ug/L
1.0
1
08/05/14 19:20
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2014 12:36 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 33

aceAnalytkal
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078 t_
[phone]
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW 1
Lab ID: 92211527004 Collected:
07/30/14 15:00
Received: 07/31/14 16:40 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
08/05/14 19:20
106-93-4
Surrogates
4-Bromofluorobenzene (S)
131 %
70-130
1
08/05/14 19:20
460-00-4
1,2-Dichloroethane-d4 (S)
87 %
70-130
1
08/05/14 19:20
17060-07-0
Toluene-d8 (S)
104 %
70-130
1
08/05/14 19:20
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
08/05/14 15:48
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
3.6 mg/L
2.0
1
08/06/14 19:33
14808-79-8
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.24 mg/L
0.020
1
07/31/14 22:00
531013 TOC
Analytical Method: SM 531013
Total Organic Carbon
6.1 mg/L
1.0
1
08/05/14 20:37
7440-44-0
Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 33

�aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9B00 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW-8 Lab ID: 92211527005 Collected: 07/30/14 16:30 Received: 07/31/14 16:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
08/04/14 16:45
74-84-0
Ethene
ND ug/L
6.2
1
08/04/14 16:45
74-85-1
- Methane
ND ug/L
6.6
1
08/04/14 16:45
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:27
7440-38-2
Barium
30.7 ug/L
5.0
1
08/01/14 15:35
08/05/14 00:27
7440-39-3
Cadmium
ND ug/L
1.0
1
08/01/14 15:35
08/05/14 00:27
7440-43-9
Chromium
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:27
7440-47-3
Lead
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:27
7439-92-1
Selenium
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:27
7782-49-2
Silver
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:27
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Mercury
ND ug/L
0.20
1
08/01/1412:45
08/01/1415:45
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
08/05/14 19:36
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
08105/1419:36
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
08/05/14 19:36
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
08/05/14 19:36
79-00-5
i 1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
08/05/14 19:36
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 19:36
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
08/05/14 19:36
107-06-2
_ 1,2-Dichloropropane
ND ug/L
1.0
1
08/05/14 19:36
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 19:36
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
08/0511419:36
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
08/05/14 19:36
75-27-4
Bromomethane
ND ug/L
5.0
1
08/05/14 19:36
74-83-9
Bromoform
ND ug/L
1.0
1
08/05/14 19:36
75-25-2
cis-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 19:36
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
08/0511419:36
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
08/05/14 19:36
56-23-5
Chlorobenzene
ND ug/L
1.0
1
08/05/14 19:36
108-90-7
` Chloroethane
ND ug/L
1.0
1
08/05/14 19:36
75-00-3
Chloroform
ND ug/L
1.0
1
08/05/14 19:36
67-66-3
Chloromethane
ND ug/L
1.0
1
08/05/14 19:36
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
08/05/14 19:36
12448-1
Dichlorodifluoromethane
ND ug/L
1.0
1
08/05/14 19:36
75-71-8
Methylene Chloride
ND ug/L
2.0
1
08/05/14 19:36
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 19:36
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 19:36
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
08/05/14 19:36
127-18-4
Trichloroethene
ND ug/L
1.0
1
08105/1419:36
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
08/05/14 19:36
75-69-4
-' Vinyl chloride
ND ug/L
1.0
1
08/05/14 19:36
75-01-4
Date: 11/12/201412:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 33

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100 I
Huntersviile, NC 28078 (,
[phone]
I
I
Sample: DMW 8
Lab ID: 92211527006 Collected:
07/30/14 16:30
Received: 07/31/14 16:40 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qua[
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
08/05/14 19:36
106-93-4
Surrogates
4-Bromofluorobenzene (S)
129 %
70-130
1
08/05/14 19:36
460-00-4
1,2-Dich[oroethane-d4 (S)
87 %
70-130
1
08/05/14 19:36
17060-07-0
Toluene-d8 (S)
106 %
70-130
1
08/05/14 19:36
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
-.
Sulfide
ND mg/L
0.10
1
08/05/1415:48
18496-25-8 j
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
ND mg/L
2.0
1
08/06/14 20:14
14808-79-8
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.79 mg/L
0.020
1
07/31/14 22:01
5310B TOC
Analytical Method: SM 5310B
-
Total Organic Carbon
24.4 mg/L
1.0
1
08/05/14 21:05
7440-44-0
Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 33 ,

P , aceAnal Ical
% www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW 6 Lab ID: 92211527006 Collected: 07/31/14 11:15 Received: 07/31/14 16:40 Matrix: Water
_ Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace
Ethane
Ethene
Methane
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury
Mercury
601 Volatiles by SM 6200
1,1-Dichloroethane
1,1-Dichloroethene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
1,1,2, 2-Tetrachloroethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromod ich loromethane
Bromomethane
Bromoform
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromoch loromethane
Dichlorod ifluoromethane
Methylene Chloride
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Tetrachloroethene
Trichloroethene
Trichlo rolluoromethane
- Vinyl chloride
Date: 11 /12/2014 12:36 PM
i
Analytical Method: RSK 175
ND ug/L
6.2
1
08/04/14 16:57
74-84-0
ND ug/L
6.2
1
08/04/14 16:57
74-85-1
ND ug/L
6.6
1
08/04/1416:57
74-82-8
Analytical Method: EPA 6010 Preparation Method: EPA 3010
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:30
7440-38-2
108 ug/L
5.0
1
08/01/14 15:35
08/05/14 00:30
7440-39-3
ND ug/L
1.0
1
08/01/14 15:35
08/05/14 00:30
7440-43-9
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:30
7440-47-3
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:30
7439-92-1
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:30
7782-49-2
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:30
7440-22-4
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L
0.20
1
08/01/1412:45
08101/1415:47
7439-97-6
Analytical Method: SM 6200B
40.6 ug/L
1.0
1
08/05/14 19:53
75-34-3
52.0 ug/L
1.0
1
08/05/14 19:53
75-35-4
1.9 ug/L
1.0
1
08/05/14 19:53
71-55-6
ND ug/L
1.0
1
08/05/14 19:53
79-00-5
ND ug/L
1.0
1
08/05/14 19:53
79-34-5
ND ug/L
1.0
1
08/05/14 19:53
95-50-1
ND ug/L
1.0
1
08/05/14 19:53
107-06-2
ND ug/L
1.0
1
08/05/14 19:53
78-87-5
ND ug/L
1.0
1
08/05/14 19:53
541-73-1
ND ug/L
1.0
1
08105/1419:53
106-46-7
ND ug/L
1.0
1
08/05/14 19:53
75-27-4
ND ug/L
5.0
1
08/05/14 19:53
74-83-9
ND ug/L
1.0
1
08/05/14 19:53
75-25-2
2.5 ug/L
1.0
1
08/05/14 19:53
156-59-2
ND ug/L
1.0
1
08/05/14 19:53
10061-01-5
ND ug/L
1.0
1
08/05/14 19:53
56-23-5
ND ug/L
1.0
1
08/05/14 19:53
108-90-7
ND ug/L
1.0
1
08/05/14 19:53
75-00-3
ND ug/L
1.0
1
08/05/14 19:53
67-66-3
ND ug/L
1.0
1
08/05/14 19:53
74-87-3
ND ug/L
1.0
1
0810511419:53
124-48-1
ND ug/L
1.0
1
08/05/14 19:53
75-71-8
ND ug/L
2.0
1
08/0511419:53
75-09-2
ND ug/L
1.0
1
08/05/14 19:53
156-60-5
ND ug/L
1.0
1
08/05/14 19:53
10061-02-6
ND ug/L
1.0
1
08/05/14 19:53
127-18-4
43.2 ug/L
1.0
1
08/05/14 19:53
79-01-6
ND ug/L
1.0
1
08/05/14 19:53
75-69-4
ND ug/L
1.0
1
08/05/14 19:53
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 33

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc. --
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW 6
Lab ID: 92211527006 Collected:
07/31/14 11:15
Received: 07/31/14 16:40 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
08/05/14 19:53
106-93-4
Surrogates
4-13romofluorobenzene (S)
129 %
70-130
1
08/05/14 19:53
460-00-4
1,2-Dichloroethane-d4 (S)
88 %
70-130
1
08/05/14 19:53
17060-07-0
Toluene-d8 (S)
105 %
70-130
1
08/05/14 19:53
2037-26-5
4500S213 Sulfide Water
Analytical Method: SM 4500-S213
Sulfide
ND mg/L
0.10
1
08/07/14 16:34
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
45.9 mg/L
10.0
5
08/06/14 20:28
14808-79-8
363.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/L
0.020
1
07/31/14 22:02
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
14.2 mg/L
1.0
1
08/05/14 21:15
7440-44-0
Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 33

/ aceAnal fical
J
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Sample: DMW-7 Lab ID: 92211627007 Collected: 07/31/14 12:30 Received: 07/31/14 16:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
RSK 175 AIR Headspace Analytical Method: RSK 175
Ethane
ND ug/L
6.2
1
08/04/14 17:08
74-84-0
Ethene
ND ug/L
6.2
1
08/04/1417:08
74-85-1
Methane
ND ug/L
6.6
1
08/04/1417:08
74-82-8
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Arsenic
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:33
7440-38-2
Barium
37.4 ug/L
5.0
1
08/01/14 15:35
08/05/14 00:33
7440-39-3
Cadmium
ND ug/L
1.0
1
08/01/14 15:35
08/05/14 00:33
7440-43-9
Chromium
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:33
7440-47-3
Lead
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:33
7439-92-1
Selenium
ND ug/L
10.0
1
08/01/14 15:35
08/05/14 00:33
7782-49-2
Silver
ND ug/L
5.0
1
08/01/14 15:35
08/05/14 00:33
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
1
08/01/1412:45
08/01/1415:55
7439-97-6
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,1-Dichloroethane
ND ug/L
1.0
1
08/05/14 20:10
75-34-3
1,1-Dichloroethene
ND ug/L
1.0
1
08/05/14 20:10
75-35-4
1,1,1-Trichloroethane
ND ug/L
1.0
1
08/05/14 20:10
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
1
08/05/14 20:10
79-60-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
1
08/05/14 20:10
79-34-5
1,2-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 20:10
95-50-1
1,2-Dichloroethane
ND ug/L
1.0
1
08/05/14 20:10
107-06-2
1,2-Dichloropropane
ND ug/L
1.0
1
08/05/14 20:10
78-87-5
1,3-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 20:10
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
1
08/05/14 20:10
106-46-7
Bromodichloromethane
ND ug/L
1.0
1
08/05/14 20:10
75-27-4
Bromomethane
ND ug/L
5.0
1
08/05/14 20:10
74-83-9
Bromoform
ND ug/L
1.0
1
08/05/14 20:10
75-25-2
' cis-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 20:10
156-59-2
cis-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 20:10
10061-01-5
Carbon tetrachloride
ND ug/L
1.0
1
08/05/14 20:10
56-23-5
Chlorobenzene
ND ug/L
1.0
1
08/05/14 20:10
108-90-7
Chloroethane
ND ug/L
1.0
1
08/05/14 20:10
75-00-3
Chloroform
ND ug/L
1.0
1
08/05/14 20:10
67-66-3
Chloromethane
ND ug/L
1.0
1
08/05/14 20:10
74-87-3
Dibromochloromethane
ND ug/L
1.0
1
08/05/14 20:10
124 48-1
Dichlorodifluoromethane
ND ug/L
1.0
1
08/05/14 20:10
75-71-8
Methylene Chloride
ND ug/L
2.0
1
08/05/14 20:10
75-09-2
trans-1,2-Dichloroethene
ND ug/L
1.0
1
08/05/14 20:10
156-60-5
trans-1,3-Dichloropropene
ND ug/L
1.0
1
08/05/14 20:10
10061-02-6
Tetrachloroethene
ND ug/L
1.0
1
08/05/14 20:10
127-18-4
- Trichloroethene
ND ug/L
1.0
1
08/05/14 20:10
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
08/05/14 20:10
75-69-4
- i Vinyl chloride
ND ug/L
1.0
1
08/05/14 20:10
75-01-4
bate: 11/12/201412:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 33

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc. —
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.:. 92211527
Sample: DMW-7
Lab ID: 92211527007 Collected:
07/31/14 12:30
Received: 07/31/14 16:40 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
601 Volatiles by SM 6200
Analytical Method: SM 6200B
1,2-Dibromoethane(EDB)
ND ug/L
1.0
1
08/05/14 20:10
106-93-4
Surrogates
4-Bromofluorobenzene (S)
127 %
70-130
1
08/05/14 20:10
460-00-4
1,2-Dichloroethane-d4 (S)
85 %
70-130
1
08/05/14 20:10
17060-07-0
Toluene-d8 (S)
103 %
70-130
1
08/05/14 20:10
2037-26-5
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
08/07/1416:34
18496-25-8
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
5.2 mg/L
2.0
1
08/06/14 20:41
14808-79-8
363.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.61 mg/L
0.020
1
07/31/14 22:03
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
2.7 mg/L
1.0
1
08/05/14 21:30
7440-44-0
Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 18 of 33

Pace Analytical Services, Inc.
0
aceAnalytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
VO4)875-9092
QUALITY CONTROL DATA
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
QC Batch: AIR/20958 Analysis Method: RSK 175
QC Batch Method: RSK 175 Analysis Description: RSK 175 AIR HEADSPACE
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
x` I
METHOD BLANK: 1751477 Matrix: Water
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211627007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethane ug/L ND 6.2 08/04/1412:14
Ethene ug/L NO 6.2 08/04/1412:14
Methane ug/L ND 6.6 08/04/1412:14
LABORATORY CONTROL SAMPLE & LCSD: 1751478
1751479
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Ethane ug/L
114
111
118
98
104
85-115 6 20
r, Ethene ug/L
106
103
110
97
104
85-115 7 20
Methane ug/L
60.7
59.0
62.9
97
104
85-115 6 20
.�nwr�� vvru�.r�� �. � is �•rov
10276005001 Dup
Parameter Units Result Result
Ethane ug/L ND ND
Ethene ug/L ND ND
Methane ug/L ND ND
SAMPLE DUPLICATE: 1751481
Parameter
Ethane
Ethene
Methane
RPD Qualifiers
92211527001 Dup
Units Result Result RPD Qualifiers
ug/L ND ND
ug/L ND ND
ug/L 1160 926 22 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
;,Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 33

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MERP/6925 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
METHOD BLANK: 1254740 Matrix: Water
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
Blank Reporting -
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 08/01/1415:24
1 r
LABORATORY CONTROL SAMPLE: 1254741
Parameter Units
Mercuryug/L
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.5 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1254742 1254743
MS MSD
92211527001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 1.4 1.2 54 49 75-125 10 M1 d
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /12/2014 12:36 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 33

aJceAnalltical
`
�� www.pacelabs.com
QUALITY CONTROL DATA
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/16580
Analysis Method:
EPA 6010
QC Batch Method: EPA 3010
Analysis Description:
6010 MET
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
{
METHOD BLANK: 1255119
Matrix: Water
Associated Lab Samples: 92211527001,
92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
ug/L
ND
10.0 08/04/14 23:08
Barium
ug/L
ND
5.0 08/04/14 23:08
Cadmium
ug/L
ND
1.0 08/04/14 23:08
Chromium
ug/L
ND
5.0 08/04/14 23:08
Lead
ug/L
ND
5.0 08/04/14 23:08
Selenium
ug/L
ND
10.0 08/04/14 23:08
Silver
ug/L
ND
5.0 08/04/14 23:08
LABORATORY CONTROL SAMPLE: 1255120
Parameter Units
Arsenic
Barium
Cadmium
Chromium
_ Lead
Selenium
Silver
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
500
524
105
80-120
500
510
102
80-120
500
539
108
80-120
500
509
102
80-120
500
519
104
80-120
500
591
118
80-120
250
256
103
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1255121
MS
92211494001
Spike
Parameter
Units
Result
Conc.
_ Arsenic
ug/L
ND
500
Barium
ug/L
1180
500
Cadmium
ug/L
ND
500
Chromium
ug/L
69.6
500
Lead
ug/L
92.5
500
Selenium
ug/L
ND
500
'. Silver
1
ug/L
ND
250
1255122
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
423
425
85
85
75-125
1
500
1680
1690
100
103
75-125
1
500
480
480
96
96
75-125
0
500
542
546
94
95
75-125
1
500
540
546
89
91
75-125
1
500
440
444
88
89
75-125
1
250
238
237
95
95
75-125
0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
'Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qua[
Page 21 of 33

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
QC Batch: MSV/29204 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 601 by 6200E
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
METHOD BLANK: 1327549 Matrix: Water
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1-Trichloroethane
ug/L
ND
1.0
08/05/14 17:56
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
08/0511417:56
1,1,2-Trichloroethane
ug/L
ND
1.0
08/0511417:56
1,1-Dichloroethane
ug/L
ND
1.0
08/05/14 17:56
1,1-Dichloroethene
ug/L
ND
1.0
08/05/14 17:56
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
08/05/14 17:56
1,2-Dichlorobenzene
ug/L
ND
1.0
08/05/14 17:56
1,2-Dichloroethane
ug/L
ND
1.0
08/05/14 17:56
1,2-Dichloropropane
ug/L
ND
1.0
08/05/1417:56
1,3-Dichlorobenzene
ug/L
ND
1.0
08/05/14 17:56
1,4-Dichlorobenzene
ug/L
ND
1.0
08/05/14 17:56
Bromodichloromethane
ug/L
ND
1.0
08/05/14 17:56
Bromoform
ug/L
ND
1.0
08/0511417:56
Bromomethane
ug/L
ND
5.0
08/05/14 17:56
Carbon tetrachloride
ug/L
ND
1.0
08/05/14 17:56
Chlorobenzene
ug/L
ND
1.0
08/05/14 17:56
Chloroethane
ug/L
ND
1.0
08/05/14 17:56
Chloroform
ug/L
ND
1.0
08/05/14 17:56
Chloromethane
ug/L
ND
1.0
08/05/14 17:56
cis-1,2-Dichloroethene
ug/L
ND
1.0
08/05/14 17:56
cis-1,3-Dichloropropene
ug/L
ND
1.0
08/05/14 17:56
Dibromochloromethane
ug/L
ND
1.0
08/05/14 17:56
Dichlorodifluoromethane
ug/L
ND
1.0
08/05/14 17:56
Methylene Chloride
ug/L
ND
2.0
08/05/14 17:56
Tetrachloroethene
ug/L
ND
1.0
08/05/14 17:56
trans-1,2-Dichloroethene
ug/L
ND
1.0
08/05/14 17:56
trans-1,3-Dichloropropene
ug/L
ND
1.0
08/05/14 17:56
Trichloroethene
ug/L
ND
1.0
08/05/14 17:56
Trichlorofluoromethane
ug/L
ND
1.0
08/05/14 17:56
Vinyl chloride
ug/L
ND
1.0
08/05/14 17:56
1,2-Dichloroethane-d4 (S)
%
87
70-130
08/05/14 17:56
4-Bromofluorobenzene (S)
%
127
70-130
08/05/14 17:56
Toluene-d8 (S)
%
107
70-130
08/05/14 17:56
LABORATORY CONTROL SAMPLE: 1327550
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
1,1,1-Trichloroethane
ug/L
50
39.3 79 60-140
1,1,2,2-Tetrachloroethane
ug/L
50
45.4 91 60-140
1,1,2-Trichloroethane
ug/L
50
46.3 93 60-140
Results presented
on this page are in the units indicated
by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS _'
This report shall not be reproduced, except in full,
Date: 11/12/2014 12:36 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 33 ';

aceAnal�/�'ical
J`
j www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
LABORATORY CONTROL SAMPLE: 1327550
Parameter
1,1-Dichloroethane
ug/L
1,1-Dichloroethene
ug/L
1,2-Dibromoethane (EDB)
ug/L
1,2-Dichlorobenzene
ug/L
1,2-Dichloroethane
ug/L
1,2-Dichloropropane
ug/L
1,3-Dichlorobenzene
ug/L
1,4-Dichlorobenzene
ug/L
Bromodichloromethane
ug/L
Bromoform
ug/L
Bromomethane
ug/L
- Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
--' Chloroethane
ug/L
Chloroform
ug/L
-" Chloromethane
ug/L
cis- 1,2-Dichloroethene
ug/L
- cis-1,3-Dichloropropene
ug/L
Dibromochloromethane
ug/L
Dichlorodifluoromethane
ug/L
Methylene Chloride
ug/L
Tetrachloroethene
ug/L
trans-1,2-Dichloroethene
ug/L
trans-1,3-Dichloropropene
ug/L
Trichloroethene
ug/L
Trichlorofluoromethane
ug/L
- Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene -dB (S)
%
Units
QUALITY CONTROL DATA
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
50
38.1
76
60-140
50
41.8
84
60-140
50
45.9
92
60-140
50
43.0
86
60-140
50
39.3
79
60-140
50
45.5
91
60-140
50
43.2
86
60-140
50
42.7
85
60-140
50
48.8
98
60-140
50
61.2
122
60-140
50
39.8
80
60-140
50
49.0
98
60-140
50
45.7
91
60-140
50
38.4
77
60-140
50
44.4
89
60-140
50
37.2
74
60-140
50
42.4
85
60-140
50
45.6
91
60-140
50
53.4
107
60-140
50
40.0
80
60-140
50
40.9
82
60-140
50
51.7
103
60-140
50
42.4
85
60-140
50
44.5
89
60-140
50
46.3
93
60-140
50
43.0
86
60-140
50
38.5
77
60-140
88
70-130
120
70-130
98
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
Date: 11/12/2014 12:36 PM
f+, i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 23 of 33

Pace Analytical Services, Inc.
®
aceAnalytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 _
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
-
QC Batch: WET/32458 Analysis Method: SM 4500-S2D
QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005
METHOD BLANK: 1256548 Matrix: Water
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
I,
Sulfide mg/L ND 0.10 08105/1415:48
i
LABORATORY CONTROL SAMPLE: 1256549
i
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Sulfide mg/L .5 0.48 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1256550 1256551
MS MSD
92211156003 Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec
Limits RPD Qual
Sulfide mg/L ND .5 .5 0.56 0.56 108 108
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1256552 1256553
MS MSD
92211527004 Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec
Limits RPD Qual
Sulfide mg/L ND .5 .5 0.51 0.51 102 102
90-110 0
i
I
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
-i
REPORT OF LABORATORY ANALYSIS
=
This report shall not be reproduced, except in full,
Date: 11/12/2014 12:36 PM without the written consent of Pace Analytical Services, Inc..
Page 24 of 33 1

'� aceAnalJfical
i
www.pacefaftcom
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
QUALITY CONTROL DATA
QC Batch: WET/32521 Analysis Method: SM 4500-S2D
QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water
Associated Lab Samples: 92211527006, 92211527007
METHOD BLANK: 1258576
Associated Lab Samples: 92211527006, 92211527007
Parameter Units
Sulfide mg/L
LABORATORY CONTROL SAMPLE: 1258577
Parameter Units
Sulfide mg/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 08/07/1416:34
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.5 0.52 . 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1258578 1258579
MS , MSD
92211527006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD
Sulfide mg/L ND .5 .5 0.50 0.50 100 100 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1258580 1258581
MS MSD
92212055015 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD
Sulfide mg/L ND .5 .5 0.49 0.49 99 99 90-110 0
w
I
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
y,
)ate: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Qual
Page 25 of 33

aceAnalytical
wwwpacelab&com
QUALITY CONTROL DATA
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Pace Analytical Services, Inc. ..
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
1
QC Batch: WETA/19812 Analysis Method: EPA 300.0
I
QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
METHOD BLANK: 1257094 Matrix: Water
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers I
Sulfate mg/L ND 2.0 08/06/1417:31
LABORATORY CONTROL SAMPLE: 1257095
Parameter Units
Sulfate mg/L
i
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 19.0 95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1257096 1257097
MS MSD
92210975018 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND 20 20 20.3 20.4 102 102 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1257098 1257099
MS MSD
92211589001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 27.4 20 20 50.0 51.4 113 120 90-110 3 M1
}
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2014 12:36 PM without the written consent of Pace Analytical Services, Inc.. Page 26 of 33

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
QC Batch: WETA/19766 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
METHOD BLANK: 1254508 Matrix: Water
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
Blank Reporting
j Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.020 07/31/14 21:45
LABORATORY CONTROL SAMPLE: 1254509
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 2.5 2.4 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1254510 1254511
MS MSD
92211527001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L ND 2.5 2.5 1.7 1.7 66 66 90-110 0 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
,Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 27 of 33

aceAnalydcal
www.pacelabs.com
QUALITY CONTROL DATA
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 t �i
[phone]
!I
QC Batch: WETA/19774 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: 531013 TOC
Associated Lab Samples: 92211527001, 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
METHOD BLANK: 1255079 Matrix: Water
Associated Lab Samples: 92211527001. 92211527002, 92211527003, 92211527004, 92211527005, 92211527006, 92211527007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers 4
Total Organic Carbon mg/L ND 1.0 08/05/14 17:04
LABORATORY CONTROL SAMPLE: 1255080
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 25 24.6 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1255081 1255082
MS MSD
92211131005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 2120 25 25 2180 2200 260 348 90-110 1 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1255083 1255084
MS MSD
92211527004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 6.1 25 25 29.8 29.0 95 92 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
Date: 11/12/2014 12:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
h
Page 28 of 33

Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
aceAnalytical Huntersville, NC 28078
�l' www.pacelabs.com [phone]
QUALIFIERS
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
- PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
- each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A
PASI-C
PASI-M
Pace Analytical Services -Asheville
Pace Analytical Services - Charlotte
Pace Analytical Services - Minneapolis
ANALYTE QUALIFIERS
11
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2014 12:36 PM without the written consent of Pace Analytical Services, Inc.. Page 29 of 33
I

aceAnal fical
J
www.pacelabs.cem
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
Lab ID
92211527001
92211627002
92211527003
92211527004
92211627005
92211527006
92211527007
92211527001
92211527002
92211527003
92211527004
92211527005
92211527006
92211527007
92211527001
92211527002
92211527003
92211527004
92211527005
92211527006
92211527007
92211527001
92211527002
92211627003
92211527004
92211527005
92211527006
92211627007
92211527001
92211527002
92211527003
92211527004
92211527005
92211527006
92211527007
92211527001
92211527002
92211627003
92211527004
92211527005
92211527006
92211527007
92211527001
92211527002
92211527003
Sample ID
DMW 10
DMW-11
DMW-2
DMW-1
DMW 8
DMW-6
DMW 7
DMW-10
DMW-11
DMW-2
DMW-1
DMW 8
DMW-6
DMW7
DMW 10
DMW 11
DMW 2
DMW 1
DMW8
DMW 6
DMW-7
DMW-10
DMW 11
DMW-2
DMW-1
DMW8
DMW-6
DMW7
DMW 10
DMW 11
DMW2
DMW 1
DMW8
DMW6
DMW7
DMW 10
DMW 11
DMW-2
DMW-1
DMW-8
DMW-6
DMW7
DMW 10
DMW 11
DMW-2
Date: 11/12/2014 12:36 PM
QC Batch Method
RSK 175
RSK 175
RSK 175
RSK 175
RSK 175
RSK 175
RSK 175
EPA 3010
EPA 3010
EPA 3010
EPA 3010
EPA 3010
EPA 3010
EPA 3010
EPA 7470
EPA 7470
EPA 7470
EPA 7470
EPA 7470
EPA 7470
EPA 7470
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 4500-S2D
SM 4500-S2D
SM 4500-S2D
SM 4500-S2D
SM 4500-S2D
SM 4500-S2D
SM 4500-S2D
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 300.0
EPA 353.2
EPA 353.2
EPA 353.2
QC Batch Analytical Method
AIR/20958
AIR/20958
AIR/20958
AIR/20958
AIR/20958
AIR/20958
AIR/20958
MPRP/16580
EPA 6010
MPRP/16580
EPA 6010
MPRP/16580
EPA 6010
MPRP/16580
EPA 6010
MPRP/16580
EPA 6010
MPRP/16580
EPA 6010
MPRP/16580
EPA 6010
MERP/6925
EPA 7470
MERP/6925
EPA 7470
MERP/6925
EPA 7470
MERP/6925
EPA 7470
MERP/6925
EPA 7470
MERP/6925
EPA 7470
MERP/6925
EPA 7470
MSV/29204
MSV/29204
MSV/29204
MSV/29204
MSV/29204
MSV/29204
MSV/29204
WET/32458
WET/32458
WET/32458
WET/32458
WET/32458
WET/32521
WET/32521
WETA/19812
WETA/19812
WETA/19812
WETA/19812
WETA/19812
WETA/19812
WETA/19812
WETA/19766
WETA/19766
WETA/19766
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/14972
ICP/14972 fi
ICP/14972
ICP/14972
ICP/14972
ICP/14972
ICP/14972
MERC/6666
MERC/6666 d
MERC/6666
MERC/6666
MERC/6666
MERC/6666
MERC/6666
Page 30 of 33

aceAnalytical
i www.pacelabacom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DOT NO 2-66 WBS#34613.3.26
Pace Project No.: 92211527
t
Lab ID
92211527004
92211627005
92211527006
92211627007
92211527001
92211627002
92211527003
92211527004
92211527005
92211527006
�92211527007
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample ID QC Batch Method QC Batch Analytical Method
DMW 1
EPA 353.2
WETA/19766
DMW-8
EPA 353.2
WETA/19766
DMW-6
EPA 353.2
WETA/19766
DMW 7
EPA 353.2
WETA/19766
DMW-10
SM 5310E
WETA/19774
DMW-11
SM 53106
WETA/19774
DMW-2
SM 5310E
WETA/19774
DMW 1
SM 5310B
WETA/19774
DMW-8
SM 5310B
WETA/19774
DMW-6
SM 5310B
WETA/19774
DMW 7
SM 5310B
WETA/19774
)ate: 11/12/2014 12:36 PM
i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 31 of 33

�AilceAn Jyfical"
Sample Condition Upon Receil
Document Number:
F-CHR-CS-003-rev.14
Nage i or z
Issuing Authority:
Pace Huntersville Quality Office
Client Name: H CLvv ' P(_
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial Pace Other
Custody Seal on Cooler/Box Present: ❑ yes ,Pno Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1102 T1 0 Type of Ice: Wet Blue None �ERamples on ice, cooling process has begun
r w nn. TA RAA • AI'. ('nrronFinrl
I CIII tJ I,Vll Clill Vll •vim.. Div vv.. vv.v.
Corrected Cooler Temp.: a D •C
.��.. ..� ��.. __-._..
Biological Tissue is Frozen: YesANoN/A
Date and I itials of pq son examining
contents: 31
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
IER es
❑No
❑N/A
1.
Chain of Custody Filled Out:
9,?es
❑No
❑N/A
2.
Chain of Custody Relinquished:
(Yes
❑No
❑N/A
3.
Sampler Name & Signature on COC:
`s
❑No
❑NIA
4.
Samples Arrived within Hold Time:
es
ONo
❑N/A
5.
Short Hold Time Analysis (<72hr):
es
❑No
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
Wo
❑N/A
7.
Sufficient Volume:
Wes
ONo
ON/A
8.
Correct Containers Used:
Wes
El No
El NIA
9.
-Pace Containers Used:
es
❑No
❑N/A
Containers Intact:
Wes
❑No
El NIA
10.
Filtered volume received for Dissolved tests
OYes
❑No
WA
11.
Sample Labels matchCOC:
-Includes date/time/ID/Analysis Matrix:
❑Yes �o
❑N/A
12. �PIe I� - �1t ��be�S SCt�,�(I �j�
COS- 'S "1 S l a3D
All containers needing preservation have been checked.
Wes
❑No
ON/A
13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
Wes
❑No
ON/A
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
1,09s.
El No
Samples checked for dechlorination:
Headspace in VOA Vials (>6mm):
❑Yes
❑No
�o
ON/A
14.
15.Akk Me
Trip Blank Present:
❑Yes
❑No
'S�a
16.
Trip Blank Custody Seals Present
❑Yes
❑NoIA
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: Date: 3J ifs
SRF Review: P /L Date: `
Note: Whenever they • a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( 1.e out of hold, incorrect preservative, out of temp,
incorrect containers)
Field Data Required? Y / N
1�
WIN.►' �',�. !�►��
ll 11181�11�lflillll 11 l
92" 1,113w7
1 e..
Page 32 of 33

CHAIN -OF -CUSTODY / Analytical Request Document
co
a The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. O
RLAnalytical Cl)
www.pacelabs.cem N
Section A Section B Section C
Page: of EL
Required Client Information: Required Project Information: Invoice Information:
Company: \ Report To: Attention:
1843301
ddress,. `
.S• t c- c n ST. S4 G r o3
Copy To:
Company Name:
REGULATORY AGENCY
C�Ct, ,e
Address:
t NPDES 1 GROUND WATER I— DRINKING WATER
i UST I— RCRA {— OTHER
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Purchase Order No.:
Pace Quote
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Requested Due Date/TAT:
Project Number: 'Ltf ;+� J y i� y c
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