NC0004952_Regional Office Historical File Pre 2018 (6)

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2019 (August 2019)
PERMIT VERSION: 4_0.
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
REC
1 V LINTY: Cleveland
SEP G
n 8 2019
Q 9ORC CERT DER: 987732
$RECEIVEDINCDENRIbWR
CENTR, ;L I``ILERrATUS: Processed 5 �- �, 0 2019
DWR SECTION'-
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISi� �R'?WOIVAL OFFICE
�
q
•°'
E
t3
e
u'
�
F°
'2
Q
4
O
O
H
4
O
N
0
O
9
x
50050
00100
QD310
QD5M
31616
CO600
C0665
34496
34SOI
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
BOD -Qty Daily
INS -Qty Daily
FCOLI BR
TOTAL N-
TOTAL P-Couc
1,1-DCE
1,1-DCEY
2400dock
Hn
2400dock
H.
Y111N
mgd
so
Ibs/day
Ibs/day
#/looml
mg/l
mg/l
Ibs/da
lbs/day
1
0600
8
Y
NOFLOW
2
0600
8
Y
NOFLOW
3
0800
1.0
B
NOFLOW
4
0800
2.0
B
NOFLOW
5
10600
8.0
1 Y
0.449
6
0600
8.0
Y
0.411
7 10930
24
0600
8.0
B
1
0.381
7.6
9.9
21
<2
1.1
<0.1
8
0600
8.0
B
0.404
9
0600
6.75
B
0.334
10
0830
1.0
B
0.262
1t
N
NOFLOW
12
10600
8.0
B
INOFLOW
13
0600
8.0
B
NOFLOW
14
0600
8.0
B
NOFLOW
15
0600
3.0
B
NOFLOW
16
0600
8.0
B
NOFLOW
17
1
N
NOFLOW
18
1700
2.0
B
NOFLOW
19
0600
8.0
Y
0.295
20
0600
8.0
Y
0.399
21
0930
24
0430
8.0
Y
0.42
7.9
11.9
41.3
72
22
0600
8.0
Y
0.407
23
Y
0.384
24
0
Y
0.365
25
0
Y
NOFLOW
26
0
Y
0.396
27
JG6008.0
0
Y
0.377
28
0930
24
0
Y
0.374
8.1
20.6
39
4
29
0
Y
0.337
30
0
Y
0.282
31
0
B
0.206
Monthly Average Limit:
OAS
68
124
200
0.071
0.052
MonthlyAvcrag.
0.360167
114.133333
33.766667
6.603854
1.1
0
Daily Maximum:
0.449
8.1
20.6
41.3
172
1.1
0
Daily Minimum:
0.206
7.6
9.9
21
0
11.1
10
s•sa No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2019 (August 2019)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Monthly Avengm
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation— Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2019 (August 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
ON
mill
"7°No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2019 (August 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No,
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation —Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation —Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2019 (August 2019)
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
ssss No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2019 (August 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
O
.2
U
K
e
F
B
E
o
O
in
c
O
g
O
e
K
Z
34147
34461
31694
34469
34475
34010
34376
31626
34220
39700
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITRODEN
PHENANTH
JPHENOL
PYRENE
TETCLETY
TOLUENE IFLUORANT
26DINITR
ANTHRACE
HCD
2400 clock
Hn
2400 dock
In.
YMN
I
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
ug/l
ug/1
119/1
jugA
1
0600
8
Y
NOFLOW
2
0600
8
Y
NOFLOW
3
0800
1.0
B
NOFLOW
4
0800
2.0
B
NOFLOW
5 10600
18.0
Y
6
0600
8.0
Y
7
0930
24
0600
8.0
B
8
0600
8.0
B
9
0600
6.75
B
10
0830
1.0
B
11
N
NOFLOW
12
0600
8.0
B
NOFLOW
13
0600
8.0
B
NOFLOW
14
0600
8.0
JB
I NOFLOW
15
10600
3.0
B
NOFLOW
16
0600
8.0
B
NOFLOW
17
N
NOFLOW
48
1700
2.0
B
NOFLOW
19
10600
8.0
Y
20
1
0600
8.0
Y
21
0930
24
0430
8.0
Y
22
0600
8.0
Y
23
0430
8.0
Y
24
10830
8.0
Y
25
0730
2.0
ly
NOFLOW
26
0500
9.0
Y
27
0600
8.0
Y
28
0930
24
0600
8.0
Y
29
8.0
Y
30
0600
8.0
Y
J1
0800
2.0
B
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.034
Monthly Average
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation -Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2019 (August 2019)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 09/10/2019
•�[/��„�J ��_�f,. 09/10/2019
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
09/10/2019
c
Per - mittee/Submitter Sig a re:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 08-2019 (August 2019)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
Report Comments:
08/07/19 Fecal Coliforms; Below Reporting Limits
08/07/19 Total Phosphorus; Below Reporting Limits
08/21/19 BOD; GGA result is greater than the control limits
08/28/19 BOD; Difference between sample dilutions is greater than 30%. Blank value is outside of control limits.
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2019 (July 2019)
PERMIT VERSION: 4gw,
b l`
CLASS: WW-2 SEP f�,
ORC: Michael D. Sparks {` 01
ORC HAS CHANGED: I fGEN iV\- L PILES
VERSION: 1.0 DWR SECTION]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER:;98-77j9VED/NCDFNR/iD%r>rF,t
STATUS: Processed ° l�
1NG)ROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISC OHAI�€U�� SjpIONAL OFFICE
e
G
U
O
Z
50050
00400
QD310
QD530
31616
C0690
C0665
31496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
DOD -Qty Daily
TSS-Qty Daily
FCOLI BR
TOTAL N-
TOTAL P-Cone
1,1-DCE
1,1-DCEY
2400 clock
H.e
2400 clock
H"
YAWN
mgd
su
Ibs/day
lbs/day
N100ml
mg/l
mg/l
Ibs/day
lbs/day
1
0500
8.0
Y
NOFLOW
2
0600
8.0
Y
NOFLOW
3
0600
8.0
Y
NOFLOW
0830
3.0
B
NOFLOW
5
0600
8.0
Y
NOFLOW
6
0930
1.0
JB
I NOFLOW
7
0930
2.0
B
NOFLOW
8
0600
8.0
Y
0.375
9
0600
8.0
Y
0.393
10
10930
24
0400
8.0
Y
0.395
8.4
113.2
35.6
< 2
11
0600
8.0
Y
0.344
12
0600
8.0
Y
0.27
13
10900
1.0
B
0.214
14
N
NOFLOW
is
0600
8.0
Y
NOFLOW
16
0600
8.0
Y
NOFLOW
17
1
0600
8.0
Y
NOFLOW
18
0600
8.0
Y
NOFLOW
19
0600
3.5
Y
NOFLOW
20
0700
Lo
Y
NOFLOW
21
1000
2.0
Y
NOFLOW
22
0600
8.0
Y
0.399
23
10530
8.0
Y
1
0.432
24
0930
24
0600
8.0
Y
0.409
8
18.8
51.8
<2
25
0600
8.0
Y
0.364
26
0600
8.0
Y
0.294
27
0600
1.0
B
10.177
28
N
NOFLOW
29
0445
8.0
Y
NOFLOW
30
0600
8.0
Y
NOFLOW
31
0600
8.0
NOFLOW
1.Y
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.338833
16
43.7
t
Daily Maximum:
0.432
8.4
18.8
51.8
0
Daily Not mum:
0.177
8
13.2
135.6
10
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2019 (July 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
•;"NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 07-2019 (July 2019)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 08/05/2019
08/02/2019
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
08/05/2019
Permittee/Submitter Signature:*** Ni4l1 /B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories WC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2019 (July 2019)
Report Comments:
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
07/10/19, 07/24/19; Fecal Coliforms; Below Reporting Limits
07/10/16, 07/24/19; BOD; Blank value is outside the control limits.
07/24/19; BOD; Difference between sample dilutions is greater than 30%.
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

t 4
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 06-2019 (June 2019)
PERMIT VERSION: 4.0 PERMIT STATUS: Expired
W CLASS: W -2 F C E I VE ® COUNTY: Cleveland
ORC: Michael D. Sparks JUL 2 3 2019 ORC CERT NUMBER: 987732 ORC HAS CHANGED: No �C�ivEt7/Nc®ENR/[�W�,
CEN
VERSION: 1.0 pWR SECTION STATUS: Processed JUL 2 9 201g
WXNAL
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGl'�:OFFICE
G
H.e
e
fJ
u
F'
a
O
ti
O
v
O
tg'
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semiannually
Annual)
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pd
HOD-Qty Daily
TSS-Qty Daily
FCOLI BR
TOTAL N-
TOTALP-Conc
1,1-DCE
1,1-DCEY
2400 clock
Drs
2400 clock
Rrn
Y/B/N
mgd
su
Ibs/day
Ibs/day
#/100ml
mg/l
mgA
Ibs/day
Ibs/day
1
0830
1.5
B
NOFLOW
2
0700
5.0
B
NOFLOW
3
0600
8.0
Y
NOFLOW
4
0930
24
0600
8.0
B
0.292
8.7
7.1
36.5
1<2
<0.012
<0.012
5
0600
8.0
Y
0,301
6
0600
8.0
B
0.266
7
0600
8.0
Y
0.21
8
0900
1.0
B
0.291
9
1400
2.0
Y
NOFLOW
10
0600
8.0
B
0.268
11
0600
8.0
Y
0.323
12
0930
24
0600
8.0
Y
0.349
8.7
19.9
42.5
<2
13
0600
8.0
Y
0.348
14
0600
6.5
Y
0.28
15
10530
2.0
Y
0.175
16
0530
4.0
Y
NOFLOW
17
0600
8.0
1 Y
NOFLOW
18
1
0600
8.0
Y
I NOFLOW
19
0600
8.0
Y
NOFLOW
28
10600
8.0
Y
NOFLOW
21
0600
4.0
Y
NOFLOW
22
N
NOFLOW
23
1445
1.25
Y
NOFLOW
24
1
0600
8.0
ly
1
0.338
25
0600
8.0
Y
0.434
26
0930
24
10600
9.0
Y
0.421
8.4
15.1
72.3
2
27
0600
8.0
Y
0.422
28
0600
4.0
Y
0.37
29
0700
1.0
Y
0.286
30
1500
1.0
ly
I NOFLOW
}9aathly Avemgc limit:
0.45
68
124
200
0.071
0.052
Monthly Avemgc
0.316119
10.7
50.433333
1.259921
0
0
Daily Mad mum:
0.434
8.7
15.1
72.3
2
0
0
Daily Minimum:
10.175
8.4
17.1
36.5
0
10
0
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation -Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation -Holiday

NPDES PERMIT NO.: NC0004952
VACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 06-2019 (June 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
U
a
.e
F
e
F
<
v
O
F
a
O
v'
a
O
=
Z
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
RNLO-K-F
WE PHTII
CARDNTET
CHLROENZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 clock
Km
2400 clock
H.
WRIN
ug/l
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/1
ug/I
UgA
ug/1
Ibs/day
1
0830
1.5
B
NOFLOW
2
0700
5.0
B
NOFLOW
3
0600
8.0
Y
NOFLOW
4
0930
24
0600
8.0
B
< 10
< 0.024
< 0.012
< 0.012
< 0.024
< 0.012
< 10
< 10
< 20
< 10
< 0.049
5
0600
8.0
Y
6
10600
8.0
B
7
0600
8.0
Y
8
0900
1.0
B
9
1400
2.0
Y
NOFLOW
10
0600
8.0
B
11
0600
8.0
Y
12
0930
24
0600
8.0
Y
13
0600
8.0
Y
14
0600
6.5
Y
15
0530
2.0
Y
16
0530
4.0
Y
NOFLOW
17
1
0600
18.0
Y
INOFLOW
18
0600
8.0
Y
NOFLOW
19
0600
8.0
Y
NOFLOW
20
0600
8.0
Y
NOFLOW
21
0600
4.0
Y
NOFLOW
22
N
INOFLOW
23
1
1445
1.25
Y
NOFLOW
24
0600
8.0
Y
25
0600
8.0
Y
26
0930
24
0600
9.0
Y
27
0600
8.0
ly
28
0600
4.0
Y
29
0700
1.0
Y
30
1500
1.0
Y
NOFLOW
Monthly Avcmgc Limit:
0332
0.058
0.048
U36
0.068
3-W
0.261
Monthly Avcmge
0
0
0
0
0
0
0
0
0
0
0
Daily Maximum:
0
0
10
0
0
0
0
0
10
10
0
Daily Minimum:
0
0
0
0
10
0
0
10
0
0 10
****No Reporting Reason: ENFRUSE =NoFlow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2019 (June 2019)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
v
A
B
u
e
e
U'
E
F
s
.6
u
W
12
8
Q
e
4
O
m
C
F
4
O
-
z
O
e
p
°Ql
,�'
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNBPHTH
JETHYLBEN
FLUORENE
HEXCLBD
ACE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 dock
Ha
2400 clock
H.
WIN
lbs/day
lbs/day
I lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
1
0830
1.5
B
NOFLOW
2
0700
5.0
B
NOFLOW
3
0600
8.0
Y
NOFLOW
4
0930
24
0600
8.0
B
< 0.024
< 0.024
< 0.012
< 0.024
< 0.049
< 0.024
<p.024
< 0.024
< 0.012
< 0.024
< 0.024
5
0600
8.0
Y
6
0600
8.0
B
7
0600
8.0
Y
8
0900
1.0
B
1400
2.0
Y
NOFLOW
10
0600
8.0
B
11
0600
8.0
Y
12
0930
24
0600
8.0
Y
'
13
0600
8.0
Y
14
10600
6.5
Y
'
15
0530
2.0
Y
16
0530
4.0
Y
NOFLOW
17
0600
8.0
Y
INOFLOW
18
0600
8.0
Y
NOFLOW
19
0600
8.0
Y
NOFLOW
20
0600
8.0
Y
NOFLOW
21
0600
4.0
Y
NOFLOW
22
1 N
INOFLOW
23
11445
1.25
Y
NOFLOW
24
0600
8.0
Y
25
0600
8.0
Y
26
0930
24
0600
9.0
Y
27
0600
8.0
Y
28
0600
14.0
Y
29
10700
1.0
1 Y
30
11500
1.0
1 Y
NOFLOW
Monthly Average limit:
0.061
D.087
0.103
0.071
0.065
0.068
7227
0278
0.129
0.071
12846
Monthly Average:
0
0
0
0
0
0
0
0
0
0
0
DailyM=imum:
0
0
0
0
I 0
0
0
0
0
0
0
Daily Minimum:
0
0
0
0
0
0
0
10
0
0
10
**"No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY =No Visitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2019 (June 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
e
3
6
m
m
0
z
34447
00556
TGP3B
34461
34694
34469
34475
34010
34220
39700
34626
Annually
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
OIL-GRSE
CERITDPF
PHENANTII
PHENOL
PYRENE
TETCLETY
TOLUENE
ANTHRACE
HCB
26DINITR
2400 clock
If.
2400 cluck
Hrs
YlB/N
lbs/day
mg/l
pass/fail
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
ug/l
ug/l
ugA
1
0830
1.5
B
NOFLOW
2
0700
5.0
B
NOFLOW
3
0600
8.0
Y
NOFLOW
4
0930
24
0600
8.0
B
<0.024
<5
PASS
<0.024
<0.024
<0.024
<0.012
<0.012
110
<20
<20
5
0600
8.0
Y
6
0600
8.0
B
7
0600
8.0
Y
8
0900
1.0
B
1400
12.0
Y
INOFLOW
10
0600
8.0
B
11
0600
8.0
Y
12
0930
24
0600
8.0
Y
13
0600
8.0
Y
14
1
0600
6.5
Y
is
0530
2.0
Y
16
0530
4.0
Y
NOFLOW
17
0600
8.0
Y
NOFLOW
l8
0600
8.0
Y
NOFLOW
19
0600
8.0
Y
NOFLOW
20
10600
18.0
Y
INOFLOW
21
0600
4.0
Y
NOFLOW
22
N
NOFLOW
23
1445
1.25
Y
NOFLOW
24
0600
8.0
Y
25
10600
8.0
ly
26
0930
24
0600
9.0
Y
27
0600
8.0
Y
28
0600
4.0
Y
29
0700
1.0
Y
30
1500
1.0
ly
I NOFLOW
Monthly Average Limit:
M087
0.071
0.048
0.081
0.071
0.084
Monthly Average:
0
0
0
0
0
0
0
0
0
0
Daily Maximum:
0
0
0
0
0
0
0
0
0
0
Daily Minimum:
0
10
1
0
0
0
0
10
0
10
10
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather, NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2019 (June 2019)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
E
F
E
E
u
E
F
a
F
E
F
E
tfi
o`
'w
C
o'
o
o
ri
34376
Annually
Grab
IFLUORANT
2400 clock
H.
2400 clock
Hrs
Y/D/N
n9A
1
0830
1.5
B
NOFLOW
'
2
0700
5.0
111
NOFLOW
3
0600
8.0
Y
NOFLOW
4
0930
24
0600
8.0
B
< 10
5
0600
8.0
Y
6
0600
8.0
B
7
0600
8.0
ly
8
0900
1.0
B
9
1400
2.0
Y
NOFLOW
10
0600
8.0
B
11
0600
8.0
Y
12
0930
24
0600
8.0
IY
13
0600
8.0
Y
14
0600
6.5
Y
15
0530
2.0
Y
16
10530
4.0
Y
NOFLOW
17
0600
8.0
Y
NOFLOW
18
0600
8.0
Y
NOFLOW
19
0600
8.0
Y
NOFLOW
20
10600
8.0
Y
NOFLOW
21
0600
4.0
Y
NOFLOW
22
N
NOFLOW
23
1445
1.25
Y
NOFLOW
24
0600
8.0
Y
25
0600
8.0
jy
26
0930
24
0600
9.0
Y
27
0600
8.0
Y
28
0600
4.0
Y
29
0700
1.0
Y
so
1
11500
11.0
ly
INCIFLOW
Monthly Avcmgc Limit:
'
Monthly Avemgc
0
Daily Maximum:
0
Daily Minimum:
0
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2019 (June 2019)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 07/09/2019
> 07/09/2019
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part H.E.6 of
the NPDES permit.
9
07/09/2019
v
Permit ee/Submitter Signature:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2019 (June 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
Report Comments:
Below Report Limits (BRL) Results reported as less than (<)
06/04/19, Oil & Grease: Below Repot Limit
06/04/19, 06/12/19, Fecal Coliforms; Below Reporting Limits
06/04/19 BOD; GGA result is less than the control limit. Blank value is outside the control limits.
06/26/16 BOD; Blank value is outside the control limits.
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

1 1.
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2019 (May 2019)
PERMIT VERSION: 4_0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1_0
}� r";PERMIT STATUS: Expired
J U N Z Q 19 COUNTY: Cleveland
ORC CERT NUMBER: 987732
CENTRAL FILES REC€rVEDWDENR/DWR
DWR CEcTION JUL m 2019
STATUS: Processed
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DIS@iUUdLGFQ% XQONAL OFFICE
A
t'J
.E
F
<
O
O
O
1 Z
50050
moo
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
PH
BOD-Qty Daily
TSS -Qty Daily
FCOLI BR
TOTALN-
TOTAL P-Cone
1,LDCE
II-DCEY
2400 clock
lire
2400 clock
Drs
YD1/N
mgd
su
lbs/day
lbs/day
#/loom]
mg/!
mg/1
Ibs/day
ibs/day
1
0930
24
0530
8.0
Y
0.368
8.4
6.4
8
<2
2
0600
8.0
Y
0.328
3
0600
8.0
Y
0.247
4
0830
1.0
B
0.193
5
N
NOFLOW
6
0630
8.0
B
NOFLOW
7
1
1
0600
18.0
B
I NOFLOW
8
0600
8.0
Y
NOFLOW
9
0600
8.0
Y
NOFLOW
10
0500
8.0
Y
NOFLOW
It
1330
4.5
Y
NOFLOW
12
1700
2.0
B
NOFLOW
13
1
10600
18.0
B
1
0.256
14
0600
8.0
B
0.396
15
0930
24
0600
8.0
B
0.392
8.5
6.9
22.2
4
16
0600
8.0
B
0361
17
0600
8.0
B
0.377
18
1
10830
1.0
1 B
1
0.33
19
N
NOFLOW
20
0600
Y
NOFLOW
21
0600
F8.0
Y
NOFLOW
22
0430
Y
NOFLOW
23
0600
8.0
Y
NOFLOW
24 1
10630
6.5
B
NOFLOW
25
0445
1.75
Y
NOFLOW
26
1000
1.50
Y
NOFLOW
27
0830
1.25
Y
0.26
28
0430
10.0 1
Y
0.326
29
0930
24
0430
10.0
Y
0.4
8.5
8.7
28
4
30
0600
8.0
Y
0.399
31
0600
6.5
B
0.327
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average
0.330667
7.333333
19.4
2.519842
Daily Maximum:
0.4
8.5
8,7
28
4
Daily Minimum:
0.193 18.4
16.4
18
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

t
NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2019 (May 2019)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
A
e
U
o
a
F
F
O
O
ao°
d
O
d
u
O
a
2
345M
32103
34541
34546
77163
31566
34571
34601
34606
34616
-11
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
la-DCB
1,2-DCE
1,2-DCP
t42110EY
1.3-DCPE
1,3-DCB
1p-DCB
2p-DCPH
2,4-DMPH
2a1-DNPH
2,4-DNT
2400 clock
Hrs
2400 dock
H.
Y/B/N
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/day
Ibs/day
1
0930
24
0530
8.0
Y
2
0600
8.0
Y
3
0600
8.0
Y
4
10830
1.0
13
5
N
NOFLOW
6
0630
8.0
B
NOFLOW
7
0600
8.0
B
NOFLOW
8
0600
8.0
Y
NOFLOW
9
0600
8.0
Y
NOFLOW
10
0500
8.0
Y
NOFLOW
11
1330
4.5
Y
NOFLOW
12
1700
2.0
B
NOFLOW
13
0600
8.0
B
14
0600
8.0
B
15
0930
24
0600
8.0
B
16
0600
8.0
B
17
0600
8.0
B
18
0830
1.0
B
19
N
I NOFLOW
20
0600
8.0
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0430
8.0
Y
NOFLOW
23
0600
8.0
Y
NOFLOW
24
0630
6.5
B
NOFLOW
25
0445
1.75
Y
NOFLOW
26
1000
1.50
Y
I NOFLOW
27
0830
1.25
Y
28
0430
10.0
Y
29
0930
24
0430
10.0
Y
30
0600
8.0
Y
31
1
10600
165
In
Monthly Average Limit
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0229
0J65
Monthly Average:
Dally Madmum:
Daily Minimum:
sxssNoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2019 (May 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
6
F-
a
g
g
v
q
B
E
in
6
y
O
o
=
x
345%
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
AnnuallyAnnually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPBENOL
2NPBENOL
34-BNZFA
46DN-o-C
4NPBENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 dock
Brx
2400 dock
BM
WHIN
I
lbs/day
I lbs/day
ug/l
I lbs/day
lbs/day
1 lbs/day
lbs/day
ug/l
lbs/day
ug/l
I ug/l
1
0930
24
0530
8.0
Y
2
0600
8.0
Y
3
0600
8.0
Y
4
0830
1.0
B
'
5
N
NOFLOW
6
0630
8.0
B
NOFLOW
7
0600
8.0
B
NOFLOW
8
0600
8.0
Y
NOFLOW
9
10600
8.0
Y
NOFLOW
10
1
0500
18.0
Y
I NOFLOW
11
1330
4.5
Y
NOFLOW
12
1700
2.0
B
NOFLOW
13
0600
8.0
B
14
0600
8.0
B
15
0930
24
0600
8.0
In
16
0600
8.0
B
17
0600
8.0
B
is
0830
1.0
B
19
1
N
NOFLOW
20
0600
8.0
ly
I NOFLOW
21
0600
8.0
Y
NOFLOW
22
0430
8.0
Y
NOFLOW
23
0600
8.0
Y
NOFLOW
24
0630
6.5
B
NOFLOW
25
0445
1.75
ly
NOFLOW
26
1000
1.50
Y
NOFLOW
27
0830
1.25
Y
28
r240430
0430
10.0
Y
29
0930
10.0
Y
30
1
0600
8.0 ly
31
0600
6.5
B
MonthlyA-gel3mit:
&1
0.132
0152
0.232
0.071
0.071
0.119
Monthly Average
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE = No Flow-Rcuse/Recycle; ENVWTHR = No Visitation -Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2019 (May 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
e
e
-
_
.E
u
a
a
a
o
a
e
o
O
,;'
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1 BNZO-K-F
B2E PHTH
CARBNTET
CHLROBNZ
CLROETBA
I CHLRFORM
Cr-TOTAL
CHRYSENE
ICOPPER
CN-TOT
DIETY-PH
2400 clock
Hrs
2409 clock
H.
YRI/N
ugA
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
ug/l
119/1
ugA
ug/l
lbs/day
1
0930
24
0530
8.0
Y
2
0600
8.0
Y
3
0600
8.0
Y
4
0830
1.0
B
5
N
NOFLOW
6
0630
8.0
B
NOFLOW
7
0600
8.0
B
NOFLOW
e
10600
8.0
Y
INOFLOW
9
0600
8.0
Y
NOFLOW
19
10500
8.0
Y
NOFLOW
11
1330
4.5
Y
I NOFLOW
12
1700
2.0
B
NOFLOW
'
13
0600
8.0
B
14
0600
8.0
B
15
0930
24
0600
8.0
B
16
10600
8.0
B
17
0600
8.0
B
1s
0830
1.0
JB
19
N
NOFLOW
20
1
0600
8.0
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0430
8.0
Y
NOFLOW
23
0600
8.0
Y
NOFLOW
24
0630
6.5 1B
I
NOFLOW
25
0445
1.75
Y
NOFLOW
26
1000
1.50
Y
NOFLOW
27
0830
1.25
Y
28
0430
10.0
Y
29
0930
24 10430
110.0
ly
30
0600
8.0
Y
31
0600
6.5
B
Monthly Average limit:
OX2
0.058
0.048
0-w
0.068
3S83
0.261
Monthly Average:
Daily Maximum:
Daily Minimum:
****No Reporting Reason; ENFRUSE =No Flow-Rcuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2019 (May 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
u
e
F
fi
6v
fi
F
u°
`e
E
a
O
'm
C
O
o
U09
O
o
E
�''
2
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNB PHTH
ETHYLBEN
FLUORENE
HEXCLBD
HCE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 dock
Hn
2400 dock
An
Y/WN
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
1
0930
24
0530
8.0
Y
2
0600
8.0
Y
3
0600
8.0
Y
4
0830
1.0
B
5
N
NOFLOW
6
10630
8.0
B
NOFLOW
7 1
0600
8.0
B
I NOFLOW
8
0600
8.0
Y
NOFLOW
9
0600
8.0
Y
NOFLOW
10
0500
8.0
Y
NOFLOW
11
1330
4.5
Y
NOFLOW
12
1700
2.0
B
NOFLOW
13
0600
8.0
B
14
0600
8.0
B
15
0930
24
0600
8.0
B
16
0600
8.0
B
17
0600
8.0 1
B
19 1
0830
1.0
B
19
N
NOFLOW
20
0600
8.0
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0430
8.0
Y
NOFLOW
23
0600
&0
1 Y
I NOFLOW
24
0630
6.5
B
NOFLOW
25
0445
1.75
Y
NOFLOW
26
1000
1.50
Y
NOFLOW
27
0830
1.25
Y
28
0430
10.0
1 Y
29
0930
24
0430
10.0
Y
30
0600
8.0
Y
31
0600
6.5
B
Monthly Avenge Limit:
0.Ml
0.087
10.103
0.071
0.065
0.068
2.227
0.279
0.129
0.071
12.816
Monthly Avenge:
Daily Maximum:
Daily Minimum:
"'47 No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2019 (May 2019)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
F
u
p
O
F
-
u
5
34447
34461
34694
34469
34475
34010
9376
34626
34220
39700
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITRODEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
FLUORANT
26DINITR
ANTHRACE
HCB
2400 clock
H.
2400 d.tk
H.
YlHrN
lbs/day
lbs/day
lbs/day
Ibs/day,
lbs/day
lbs/day
u&q
ug/l
ug/1
ugA
1
0930
24
0530
8.0
Y
2
0600
8.0
Y
3
0600
8.0
Y
4
0830
1.0
B
5
N
NOFLOW
6
10630
8.0
B
NOFLOW
7
0600
8.0
B
NOFLOW
8
0600
8.0
Y
NOFLOW
9
0600
8.0
Y
NOFLOW
10
0500
8.0
Y
NOFLOW
11
1330
4.5
Y
NOFLOW
12
1700
2.0
B
NOFLOW
13
0600
8.0
B
14
0600
18.0
B
15
0930
24
0600
8.0
B
16
0600
8.0
B
17
0600
8.0
B
18
0830
1.0
B
19
1N
INOFLOW
20
0600
8.0
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0430
8.0
Y
NOFLOW
23
0600
8.0
Y
NOFLOW
21 1
10630
6.5
JB
I NOFLOW
25
0445
1.75
Y
NOFLOW
26
1000
1.50
Y
NOFLOW
27
0830
1.25
Y
28
0430
10.0
Y
29
0930
24
0430
10.0
Y
38
1
10600
18.0
ly
31
0600
6.5
B
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.084
Monthly Ava agc:
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2019 (May 2019)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 06/19/2019
✓6C/✓(i��✓ ����/(1� 06/18/2019
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
06/19/2019
Perm ittee/Submitter Signatiye:I�** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Ticaona Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2019 (May 2019)
Report Comments:
05/01/19; Fecal Coliform; Below reporting limit.
05/O1/19: BOD. Blank value is outside of control limits.
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
05/15/19, 05/29/19; BOD, GGA result is less than the control limit.
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPDES PERMUT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2019 (April 2019)
PERMIT VERSION: 4.0 '
CLASS: W W-2 R F r:o ! N/_ E
ORC: Michael D. Sparks J U N 0 6 2019
ORC HAS CHANGED: No
VERSION: lA CENTRAL FILES®VVR SECTION
PERMIT STATUS: Expired 3
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
v
e
O
,''
50050
00400
QD310
QD530
31616
C0600
C0665
37496
34501
Continuous
Weekly
Weekly -
Weekly
Weekly
Semi-annually
Semiannually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
ROD -Qty Daily
TSS-Qty Daily
FCOLI BR
TOTALN-
ITOTAL P-Cone
lj-DCE
II-DCEY
2400 clock
Hts
2400 dock
Hrs
Y/B/N
mgd
su
lbs/day
lbs/day
#/100ml
mg/I
gll
lbs/day
lbs/day
1
0630
10
B
NCIFLOW
2
0630
8
Y
NOFLOW
jE
3
0630
8
Y
NOFLOW
gEIV
AIR
4
0600
8
Y
NOFLOW
5
0600
4.5
Y
NOFLOW
J U N
0 2019
6
0615
4.0
Y
NOFLOW
7
0800
4.0
Y
NOFLOW
w
ROS
a
10430
10.0
1 Y
1
0.448
_
FFICE
9
0630
8.0
Y
0.408
10
0930
24
0630
8.0
Y
0.413
7.9
27.2
9
<2
11
0600
8.0
Y
0.395
12
0630
5.0
Y
0.384
17
0930
1.0
In
1
0.421
14
0900
1.25
Y
0.346
I5
0600
9.0
Y
0.276
16
0630
8.0
Y
0.256
17
0930
24
0600
9.0
Y
0.226
8.2
9.4
5.1
4
18
10600
8.0
1 Y
0.185
19
0730
3.0
B
0.167
20
0900
3.0
B
0.225
21
1
1700
1.5
B
NOFLOW
-
22
0630
8.0
B
NOFLOW
23
0630
11.0
1 Y
I NOFLOW
24
0600
11.0
Y
NOFLOW
25
0600
8.0
Y
NOFLOW
26
1
0600
8.0
Y
NOFLOW
27
0600
4.0
Y
NOFLOW
28
0845
4.0
Y
INOFLow
29
0500
8.0
1 Y
0.358
J0
0500
8.0
Y
0.36
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average
0.324533
18.3
7.05
2
Daily Maximum:
0.448
8.2
272
9
4
Daily Minimum:
0.167
7.9
9.4
5.1
0
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 04-2019 (April 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
u
a
fi
E
U'
3
12
E
O
w
a°
O
U
O
c
%
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
13-DCPE
13-DCB
14-DCB
24-DCPH
2;f-DMPH
2,1-DNPH
24-DNT
2400 dock
Hra
2400 dock
H.
YIBIN
Ibs/da
Ibs/day
Ibs/day
Ibs/day
Ibs/day
lbs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
1
0630
10
B
NOFLOW
2
0630
8
Y
NOFLOW
3
0630
8
Y
NOFLOW
4
0600
8
Y
NOFLOW
5
0600
4.5
Y
NOFLOW
6
10615
4.0
Y
NOFLOW
7
0800
4.0
Y
NOFLOW
8
10430
10.0
ly
9
0630
8.0
Y
10
0930
24
0630
8.0
Y
11
0600
8.0
Y
12
0630
5.0
Y
13
0930
11.0
B
14
0900
1.25
Y
15
0600
9.0
Y
16
0630
8.0
Y
17
0930
24
0600
9.0
Y
18
0600
8.0
Y
19
0730
3.0
B
20
10900
13.0
B
21
1700
1.5
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0630
11.0
Y
NOFLOW
21
06DO
11.0 ..
Y
NOFLOW
25
0600
8.0
Y I
NOFLOW
26
0600
8.0
Y
NOFLOW
27
0600
4.0
Y
NOFLOW
28
0845
4.0
Y
NOFLOW
29
0500
8.0
Y
30
0500
8.0 1
Y
Monthly Average limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0365
Monthly Average:
Daily Maximum:
DailyMinimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2019 (April 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO:: 001 NO DISCHARGE*: NO (Continue)
F
u
9
�
S
6
F
O
p
O
o
O
a
=
Z'
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DNo-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 dock
Hm
2400 cloth
Hrs
YIWN
lbs/day
lbs/day
ug/l
lbs/day
lbs/day
lbs/day
lbs/day
ug/1
lbs/day
ug/I
ug/I
1
0630
10
B
NOFLOW
2
0630
8
Y
NOFLOW
3
0630
8
Y
NOFLOW
4
0600
8
Y
NOFLOW
5
0600
4.5
Y
NOFLOW
6
Y
NOFLOW
7
Y
NOFLOW
8
q0615E4A
Y
9
Y
10
0930
24
Y
I
0600
8.0
Y
12
0630
5.0
Y
13
0930
1.0
B
14
0900
1.25
Y
is
0600
9.0
Y
16
0630
8.0
Y
17
0930
24
0600
9.0
Y
18
0600
8.0
Y
19
0730
3.0
B
20
0900
3.0
B
21
1700
1.5
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0630
11.0
Y
I NOFLOW
24
0600
11.0
Y
NOFLOW
25
0600
8.0
Y
NOFLOW
26
0600 18.0
Y
NOFLOW
27
0600
4.0 _
Y
NOFLOW
28
0845
4.0
NOFLOW
29
0500
8.0
LY
30
0500
8.0
Monthly Avcrage Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Maximum:
Daily Minimum•
s"'" No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPOES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2019 (April 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1_0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
ti
e
C'r
'fi
F
F
O
�
F
O
N
O
m
x
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
112E PHTH JCARBNTET
CHLROBNZ I
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
D1ETY-PH
2400 clock
Hra
2400 clock Illn
Y/B/N
ug/l
Ibs/day
lbs/day
Iba/day
Ibs/day
Ibs/day
ug/l
ug/l
ug/l 111911
lbs/da
1
0630
10
B
NOFLOW
2
0630
8
Y
NOFLOW
'
3
0630
8
Y
NOFLOW
4
0600
8
Y
NOFLOW
5
0600
4.5
Y
NOFLOW
6
0615
4.0
Y
NOFLOW
7
0800
4.0
Y
NOFLOW
8
0430
110.0
Y
9
0630
8.0
Y
10
0930
24
0630
8.0
Y
11
0600
8.0
Y
12
10630
5.0
Y
13
0930
11.0
B
14
0900
1.25
Y
15
0600
9.0
Y
16
0630
8.0
Y
17
10930
24
0600
9.0
Y
18
0600
8.0
Y
19
0730
3.0
B
20
0900
3.0
B
21
1700
1.5
JB
NOFLOW
22
1
0630
&0
B
NOFLOW
23
0630
11.0
Y
NOFLOW
24
0600
11.0
Y
NOFLOW
25
0600
8.0
Y
NOFLOW
26
0600
8.0
Y
NOFLOW
27
0600
4.0
Y
INOFLOW
28
0945
4.0
Y
NOFLOW
29
0500
8.0
Y
30
0500
8.0
Y
Monthly Average Limit:
0.332
0.058
0.049
0336
0.068
3.593
0.261
Monthly Avemgm
Daily Macimum•
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY =No Visitation —Holiday

NPDES PERMIT' NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 04-2019 (April 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
4
lE
9
=
d
F
e
u
F
6
F
a
a
3
O
ti
O
F
a
O
y
a
O
a
x
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
31696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNB PHTH
ETHYLBEN
IFLUORENE
IIEXCLBD
IIICE
LEAD
METHYLCH
MECL2
INAPTHALE
NICKEL
2400 clock
are
2400 clock
H.
YB/N
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
1
0630
10
B
NOFLOW
2
0630
8
Y
NOFLOW
3
0630
8
Y
NOFLOW
4
0600
8
Y
NOFLOW
5
0600
4.5
Y
NOFLOW
6
0615
4.0
Y
NOFLOW
7
0800
4.0
Y
NOFLOW
e
0430
10.0
IY
9
0630
8.0
Y
10
0930
24
0630
8.0
Y
11
0600
8.0
Y
12
0630
5.0
Y
13
0930
1.0
B
14
0900
1.25
Y
15
0600
9.0
Y
16
0630
8.0
Y
17
0930
24
0600
9.0
Y
is
0600
8.0
Y
19
0730
3.0
B
20
0900
3.0
B
21
1700
1.5
B
NOFLOW
22
0630
8.0
IB
NOFLOW
23
0630
11.0
Y
NOFLOW
24
0600
11.0
Y
NOFLOW
25
1
10600
8.0
Y
NOFLOW
26
Y
NOFLOW
27
Y
NOFLOW
28
L08454.0
Y
NOFLOW
29
Y
30
Y
Monthly Average Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.27E
0.129
0.071
12.846
Monthly Average
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVAIM=No Visitation—AdverseWealher; NOFLOW=No Flow; HOLIDAY =NoVisitation—Holiday

NP13ES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2019 (April 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
u
A
9
E
CJ
[+
E
u
3
i=
F
3
C
a
v
O
O
F
a
b
O
o
C
O
aaBj
t
34447
34461
34694
34469
34475
34010
31376
34626
34220
39700
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1 NrrROBEN
PHENANTR
PHENOL
PYRENE
TETCLETY
TOLUENE
FLUORANT
26DINrrR
ANTHRACE
HCB
2400 clock
H.
2400 clack
H.
YHNN
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
ug4
ug/l
ug/1
ug/l
1
0630
10
B
NOFLOW
2
0630
8
Y
NOFLOW
3
0630
8
Y
NOFLOW
4
0600
8
Y
NOFLOW
5
0600
4.5
Y
NOFLOW
6
10615
4.0
Y
NOFLOW
7
0800
4.0
Y
NOFLOW
8
0430
10.0
Y
9
0630
8.0
Y
10
0930
24
0630
8.0
Y
11
10600
8.0
Y
12
0630
5.0
Y
13
0930
1.0
B
14
0900
1.25
Y
15
1
0600
9.0
Y
16
0630
8.0
Y
17
0930
24
0600
9.0
Y
18
0600
8.0
Y
19
0730
3.0
B
20
0900
3.0
B
21
1700
1.5
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0630
11.0
Y
NOFLOW
24
0600
11.0
Y
NOFLOW
25
1
10600
8.0
ly
I NOFLOW
26
0600
8.0
Y
NOFLOW
27
0600
4.0
Y
NOFLOW
28
0845
4.0
Y
NOFLOW
29
0500
8.0
Y
30
0500
8.0
ly
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.094
Monthly Avemge
Daily M.A.=:
Daily Minim.:
a: a No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NP11ES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2019 (April 2019)
COMPLIANCE STATUS: Compliant
coz�__c
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 05/14/2019
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone]
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
05/10/2019
Date
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
J / ti l 05/14/2019
Permittee/Submitter Signa&A:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdear.orgtweb/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
* * ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
* ** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NP13ES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2019 (April 2019)
Report Comments:
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
04/10/19; Fecal Coliform; Below reporting limit.
04/17/19, BOD; Blank value is outside of control limits.Difference between sample dilutions is greater than 30%.
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2019 (March 2019)
PERMIT VERSION: 4.0 PERMIT STATUS: Expired
CLASS: WW-2 RECF!IVED
COUNTY: Clevelan
ORC: Michael D. Sparks ORC CERT R: 98CF_IVED1NCDENR/DWR
ORC HAS CHANGED: No A P P 2 9 2019 f
VERSION:1.0 CEN WC L. FILES STATUS: Processed
DWR SECTION
, WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCH -BvNbREGIONAL OFFIC
5
-
P
O
o
U
09
O
z
50050
00400
QD310
QD530
31616
C0600
C0665
3"96
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
BOD - Qty Daily
TSS - Qty Daily
FCOLr BR
TOTAL N -
TOTAL P - Cone
1.1-DCE
1.1-DCEY
2400 clock
Hm
2400 dock
El.
Y/WN
mgd
su
Ibs/day
lbs/day
t/1100ml
mg/l
mg/I
Ibs/day
Ibs/day
1
0630
8.0
Y
0.414
2
0600
4.0
Y
0.441
3
0600
4.0
Y
0.395
4
0630
8.0
Y
0.406
5
0930
24
0630
8.0
Y
0.401
8.4
< 6.7
8.7
< 2
6
0600
8.0
Y
0.376
7
0430
8.0
Y
0.354
8
0630
3.5
B
0297
9
N
NOFLOW
10
1330
2.0
B
NOFLOW
11
0600
8.0
B
0.233
12
0630
8.0
Y
0.243
13
0930
24
0630
8.0
Y
0.31
8.5
9.6
7.5
<2
14
0600
18.0
Y
0.326
1$
0630
8.0
Y
0.253
16
0600
4.0
Y
0.233
17
0700
4.0
Y
NOFLOW
r8
0430
10.0
Y
NOFLOW
19
0630
10.0
B
NOFLOW
20
1
10630
10.0
Y
JNOFLOW
21
0600
10.0
Y
NOFLOW
22
0630
5.0
Y
NOFLOW
23
0930
3.0
B
NOFLOW
Z4
10
3.0
B
NOFLOW
25
1
0630
110.0
Y
0284
26
0600
10.0
Y
0.372
27
0930
24
0600
10.0
Y
0.383
8.5
18.2
8
<2
29
0600
8.0
Y
0.357
39
0630
6.5
B
0.197
30
0900
2.0
B
0.297
3l
N
I NOFLOW
Monthly Average Limit.
0.45
69
124
200
0.071
0.052
MontblyAverage:
0.3286
9.266667
8.066667
I
Daily Maximum:
0.441
8.5
18.2
8.7
0
Daily Minimum:
0.197
18.4
10
7.5
10
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2019 (March 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
lEE
B
F
u
.e
a
fi
F
n
C
4
o
�
O
Q
a
O
g
�
$
O
e
o
,7°
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
13-DCB
1p-DCB
2,3-DCPH
2,4-DMPH
24-DNPH
24-DNT
2400 do&
Hrs
2400 clock
H.
YMN
lbs/day
lbs/day
Ibs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
1
0630
8.0
Y
2
0600
4.0
Y
3
0600
4.0
Y
4
0630
8.0
Y
5
0930
24
0630
8.0
Y
6
0600
8.0
Y
7
0430
8.0
Y
8
0630
3.5
B
9
N
NOFLOW
10
1330
2.0
B
NOFLOW
11
0600
8.0
B
12
10630
8.0
Y
13
0930
24
0630
18.0
Y
14
0600
8.0
Y
15
0630
8.0
Y
16
0600
4.0
Y
17
0700
4.0
Y
NOFLOW
18
1
0430
10.0
Y
NOFLOW
19
0630
10.0
B
NOFLOW
20
0630
10.0
Y
NOFLOW
21
0600
10.0
Y
NOFLOW
22
0630
5.0
Y
NOFLOW
23
1
0930
3.0
B
NOFLOW
24
10
13.0
B
NOFLOW
25
0630
10.0
Y
26
0600
10.0
Y
27
0930
24
0600
10.0
Y
28
0600
8.0
Y
29
1
0630
16.5
B
30
0900
2.0
B
31
N
NOFLOW
Monthly Average Limit•
0.249
0119
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0-w
Monthly Average:
Daily Maximum:
Daily Minimum:
ssss No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2019 (March 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
J
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
u
E
u
E
8
ea
%
9
m
_
a
O
o
rY
S�'
345M
34591
79531
34657 -
34646
34205
34200
34215
34030
34526
34247
AnnuallyAnnually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46ONo-C
4NPBENOL
JACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
zaOD clock
Rrs
2a00 docJc
Hrs
YMN
lbs/day
Ibs/day
ug/l
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/l
Ibs/day
ug/1
ug/I
1
0630
8.0
Y
2
0600
4.0
Y
3
0600
4.0
Y
4
0630
8.0
Y
5
0930
24
0630
8.0
Y
6
0600
18.0
Y
7
0430
8.0
Y
8
0630
3.5
B
9
N
NOFLOW
10
1330
2.0
B
NOFLOW
11
0600
8.0
B
12
0630
8.0
Y
13
0930
24
0630
8.0
Y
14
0600
1 8.0
Y
15
0630
8.0
Y
16
0600
4.0
Y
17
0700
4.0
Y
NOFLOW
1s
0430
10.0
Y
NOFLOW
19
0630
10.0
B
NOFLOW
20
0630
10.0
Y
NOFLOW
21
0600
10.0
Y
I NOFLOW
22
0630
5.0
Y
NOFLOW
23
0930
3.0
B
NOFLOW
24
10
3.0
B
NOFLOW
25
0630 110.0
Y
26
0600
10.0
Y
27
0930
24
0600
10.0
Y
28
0600
8.0
Y
29
0630
6.5
B
30
0900
2.0
B
31
N INCIFLOW
5lonthly Ai,cmgc Limit:
0.1
0.132
0152
0.232
0.071
0.071
0.119
Monthly Average
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2019 (March 2019)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
�
"
e
e
v
a
u
e
a
o°
3
u
34242
39100
32102
34301
85811
32106
OWN
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab '
Grab
Grab
Grab
BNZO-K-F
112EPRTH
JCARRNTET
CHLRODNZ
I CLROETRA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PA
2400 clods
H s
2400 dock
Hrs
YratN
ugA
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
ug/l
ug/l
ug/I
ug/I
lbs/day
1
0630
8.0
Y
2
0600
4.0
Y
3
0600
4.0
Y
4
0630
8.0
Y
5
0930
24
0630
8.0
Y
6
10600
18.0
Y
7
0430
8.0
Y
e
10630
3.5
B
9
N
NOFLOW
10
1330
2.0
B
NOFLOW
it
0600
8.0
B
12
0630
8.0
Y
13
0930
24
0630
8.0
Y
14
0600
8.0
Y
15
0630
8.0
Y
16
0600
14.0
Y
17
0700
4.0
Y
NOFLOW
18
1
0430
10.0
ly
I NOFLOW
19
0630
10.0
B
NOFLOW
20
0630
10.0
Y
NOFLOW
21
0600
10.0
Y
NOFLOW
22
10630 15.0
Y
NOFLOW
23 1
0930
3.0
B
NOFLOW
24
10
3.0
B
NOFLOW
25
0630
10.0
Y
26
0600
10.0
Y
27
0930
24
0600
10.0
Y
28 1
10600
18.0
Y
29
0630
6.5
B
30
0900
2.0
B
31
N
NOFLOW
Monthly Average Limit:
0.332
0.058
0.048
0.336
0.068
IM
0.261
Monthly Average:
Daily Mira m•
Doily Minimum:
"='NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 03-2019 (March 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
t
F
u
`
e
E
a
E
F
w
ro°
3
o
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DUHET-PH
DNBPHTH
ETHYLBEN
IFLUORENE
HEXCLBD
JHCE
LEAD
METHYLCH
711ECL2
N"THALE
NICKEL
2400 clock
Hrs
2400 Hock
H.
Y/B!N
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
1
0630
8.0
Y
2
0600
4.0
Y
3
0600
4.0
Y
4
0630
18.0
Y
5
0930
24
0630
8.0
Y
6
0600
8.0
Y
7
0430
8.0
Y
8
0630
3.5
B
9
N
NOFLOW
10
1330
2.0
B
NOFLOW
11
0600
8.0
B
12
0630
8.0
Y
13
0930
24
0630
8.0
Y
14
0600
18.0
Y
15
0630
8.0
Y
16
0600
4.0
Y
17
0700
4.0
Y
NOFLOW
18
0430
10.0
Y
NOFLOW
19
0630
10.0
B
NOFLOW
20
0630
10.0
Y
NOFLOW
21
1
10600
110.0
Y
NOFLOW
22
0630
5.0
Y
NOFLOW
23
0930
3.0
B
NOFLOW
74
10
3.0
B
NOFLOW
25
0630
10.0
Y
26
1
0600
110.0
Y
27
0930
24
0600
10.0
Y
28
0600
8.0
Y
29
0630
6.5
B
30
0900
2.0 IB
31
N
NOFLOW
Monthly Avenge Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Avenge:
Daily Marimum:
Daily Minimum:
ass* No Reporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY =No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2019 (March 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
=
e
U'
9
u
a
E'
d
4
O
in
O
F
4
g
y
u
O
o
%
34447
00556
TGP3B
34461
34694
34469
34475
34010
34220
39700
34626
Annually
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
OILGRSE
CER17DPF
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
ANTHRACE
HCB
26DWITR
2400 clock
H.
2400 dock
Dn
YIWN
I
Ibs/day
Intgn
pass/fail
Ibs/day
1 Ibs/day
Ibs/day
Ibs/day
Ibs/day
I ugR
ugA
ug/1
1
0630
8.0
Y
2
0600
4.0
Y
3
0600
4.0
Y
4
0630
8.0
Y
5
0930
24
0630
18.0
Y
< 5
PASS
6
0600
8.0
Y
7
0430
8.0
Y
8
0630
3.5
B
9
N
NOFLOW
10
1330
2.0
B
NOFLOW
11
0600
8.0
B
12
10630
18.0
Y
13
0930
24
0630
8.0
Y
14
0600
8.0
Y
15
0630
8.0
Y
16
0600
4.0
Y
17
0700
4.0
Y
NOFLOW
la
0430
110.0
Y I
NOFLOW
19
0630
10.0
B
NOFLOW
20
0630
10.0
Y
NOFLOW
21
0600
10.0
Y
NOFLOW
22
0630
5.0
Y
NOFLOW
23
0930
3.0
B I
NOFLOW
24
10
3.0
B
NOFLOW
25 1
0630 110.0
Y
26
0600
10.0
Y
27
0930
24
0600
10.0
Y
28
0600
8.0
Y
29
0630
6.5
B
30
0900
2.0
B
31
N
NOFLOW
Monthly Average Limiu
0.087
0.071
0.048
0.081
0.071
0.094
Monthly Average
0
Daily Ma imum:
0
Daily Minimum:
0
s:ss No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2019 (March 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
e
_
uo
a`
O
F
-
c
m
O
34376
Annually
Grab
FLUORANT
2400 clock
Hrs
2300 clock
Hrs
YMN
ugn
1
0630
8.0
Y
2
0600
4.0
Y
3
0600
4.0
Y
4
0630
8.0
Y
5
0930
24
0630
8.0
Y
6
0600
8.0
Y
'
7
0430
8.0
Y
8
0630
3.5
B
9
N
NOFLOW
10
1330
B
NOFLOW
11
0600
B
12
0630
q8.O
Y
13
0930
24
0630
Y
14
1
0600
18.0
Y
25
0630
8.0
Y
16
0600
4.0
Y
17
0700
4.0
Y
NOFLOW
18
0430
10.0
Y
NOFLOW
19
1
0630
10.0
B INOFLOW
20
0630
110.0
Y
NOFLOW
21
0600
10.0
Y
NOFLOW
22
0630
5.0
Y
NOFLOW
23
0930
3.0
B
NOFLOW
24
10
3.0
B INOFLOW
25
0630 110.0
Y
26
0600
10.0
Y
27
0930
24
0600
10.0
Y
28
0600
8.0
Y
29
0630
6.5
B
30
0900
2.0
B
31
N I
NOFLOW
Monthly Average Limit:
Monthly Average:
DaOy Maximum;
Daily Minimum:
ssxs No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2019 (March 2019)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 04/11/2019
✓ 04/11/2019
ORC Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
04/11/2019
Permittee/Submitter Signature:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://porW.nedenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2019 (March 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
Report Comments:
03/05/19, 03/13/19, 03/27/19; Fecal Coliform; Below reporting limit.
03/05/19, Oil & Grease; Below reporting limit.
03/05/19, BOD; Below reporting limit.
03/13/19, BOD; Blank value is outside of control limits
03/27/19, BOD; Blank value is outside of control limits. Difference between sample dilutions is greater than 30%. GGA result is greater than the control limit.

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2019 (February 2019)
SAMPLING LOCATION:
PERMIT VERSION: 4_0 PERMIT STATUS: Expired
CLASS: WW-2 VED COUNTY: Cleveland
ORC: Michael D. Sparks I ORC CERT NUMBER: 987732
ORCHASCHANGED:N1AAR 2 b gnia NECEIVEDlf'CDrzN R IDVVR
VERSION: 1_0 CEN'I`kAL FILES S
DWR SECTION
EFFLUENT DISCHARGE NO.: 001
TATUS: Processed A i, R - , 2. iI',,4
�gop?.Os
NO DISC , l . : Cr�*:,.NIO,Or[_ ;�OFFICE
d
F
-
5
F
i;
u'
<
H
�
iF
O
fi
u
o
O
'e
g
Z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pR
BOD-Qty Daily
TSS-Qty Daily
FCOLIBR
TOTAL N-
TOTALP-Cone
1,1-DCE
1,1-DCEY
2400clock
Hrs
2400dock
H.
URN
mgd
so
Ibs/day
Ibs/day
#/100ml
mg/l
mg/l
Ibs/day
lbs/day
1
0630
8.0
Y
0.4
2
0915
2.0
B
0.38
3
0930
3.25
Y
0.366
4
10630
8.0
Y
0.363
5
0430
18.0
Y
0.352
6
0930
24
0630
8.0
Y
0.354
7.9
<5.9
7.7
<2
<0.6
<0.05
7
0430
8.0
Y
0.336
8
0600
8.0
Y
0.275
9
0845
5.25
Y
0.229
10
0945
15.5
Y
NOFLOW
11
0430
8
Y
NOFLOW
12
0630
8
Y
NOFLOW
13
0630
8
Y
NOFLOW
14
1
0600
8
Y
NOFLOW
15
0630
4.0
Y
NOFLOW
16
N
NOFLOW
17
1400
2.0
B
INOFLOW
18
0630
8.0
Y
0.354
19
1
0630
8.0
Y
0.354
20
0930
24
0630
8.0
Y
0.417
8.3
12.5
10.4
4
21
0600
8.0
Y
0.447
22
0630
8.0
B
0.413
23
10730
4.0
JB
1
0.447
24
0715
4.0
B
0.444
25
0630
8.0
Y
0.422
26
0630
8.0
B
0.43
27
0930
124
0630
8.0
Y
0.418
8.3
7
10.5
<2
28
0630
18.0
ly
1
0.402
Moodily Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average
0.38015
6.5
9.533333
1.587401
0
10
Daily Moaimwn:
0.447
18.3
12.5
110.5
14
10
0
Daily Minimum:
0.229
7.9
10
7.7
0
0
0
**** No Repotting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNED NAME: C N A Holdings LLC
GRADE: WW-3..
eDMR PERIOD: 02-2019 (February 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
e
U
e
F
F
eizo
J...
OAnnual)
zG
O
O
z
34536
32103
34541
34546
77163
34566
34571
34601
1-16
—16
1-11
Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
12-DCE
1,2-DCP
t-12DCEY
1.3-DCPE
1,3-DCB
1,4-DCB
2p-DCPR
2,4-DNPB
2,4-DNPB
24-DNT
z400 clock
Brx
Hrs
YIelN
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
lbs/day
lbs/day
lbs/da
Ibs/day
Ibs/day
Ibs/day
1
0630
8.0
Y
2
0915
2.0
B
3
0930
3.25
Y
4
0630
8.0
Y
5
0430
8.0
Y
6
0930
24
0630
8.0
Y
7
0430
8.0
Y
8
0600
8.0
Y
9
0845
5.25
Y
to
0945
5.5
Y
NOFLOW
11
0430
8
Y
NOFLOW
12
0630
8
Y
NOFLOW
13
0630
8
Y
NOFLOW
14
0600
8
Y
NOFLOW
15
0630
4.0
Y
NOFLOW
16
N
NOFLOW
17
1400
2.0
B
NOFLOW
18
0630
8.0
Y
19
0630
8.0
Y
20
0930
24
0630
8.0
Y
21
0600
8.0
Y
22
0630
8.0
B
23
0730
4.0
B
24
0715
4.0
B
25
0630
8.0
Y
26
0630
8.0
B
27
0930
24
0630
8.0
Y
28
0630
8.0
Y
Monthly Arerage limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly A—ge:
Daily Maximum:
Daily Miuimam:
* * * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNED NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 02-2019 (February 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
E
9
0
f!
a—
O
d
E
O
O°
O
x
345M
34591
79531
U07
34646
34205
31200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZPA
46DNoC
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
DNZO-A-P
2400 clads
1rrs
2400 clock
H.
Y/aiN
lbs/day
Ibs/day
ug I
Ibs/day
lbs/day
Ibs/day
Ibs/day
ug/1
Ibs/day
ug/I
u9/1
1
0630
8.0
Y
2
0915
2.0
B
3
0930
3.25
Y
4
0630
8.0
Y
5
0430
18.0
Y
6
0930
24
0630
8.0
Y
7
0430
8.0
Y
8
0600
8.0
Y
'
9
0845
5.25
Y
18
0945
15.5
Y
NOFLOW
11
0430
8
Y
NOFLOW
12
0630
8
Y
NOFLOW
13
1
0630
8
Y
I NOFLOW
14
0600
8
Y
NOFLOW
15
0630
4.0
Y
NOFLOW
16
N
NOFLOW
17
1400
2.0
B
NOFLOW
18
0630
8.0
Y
19
0630
8.0
Y
20
0930
24
0630
8.0
Y
21
0600
8.0
Y
22
0630
8.0
B
23
0730
4.0
B
24
0715
4.0
JB
25
0630
8.0
Y
26
0630
8.0
B
27
0930
124
10630
8.0
Y
28
0630
8.0
Y
Monthly Average Limit:
0.1
0.132
0252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation —Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNEIg NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2019 (February 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
c:+
�
o°
U
W
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
B2E PHTH
CARBNTET
CHLROBNZ
CLROETHA
I CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 clock
Hrx
2400 clock
Hrx
WHIN
ug/1
Ibs/day
lbs/day
Ibs/day
Ibs/day
Ibs/day
ug/l
ug/1
119/1
ug/l
Ibs/day
1
0630
8.0
Y
2
0915
2.0
B
3
0930
3.25
Y
4
0630
8.0
Y
5
0430
8.0
Y
6
0930
24
0630
8.0
Y
7
0430
8.0
Y
8
0600
8.0
Y
0845
5.25
Y
10
0945
5.5
Y
NOFLOW
11
0430
8
Y
NOFLOW
12
10630
8
Y
NOFLOW
13
0630
8
Y
NOFLOW
14
0600
8
Y
NOFLOW
is
0630
4.0
Y
NOFLOW
16
N
I NOFLOW
17
1400
2.0
B
NOFLOW
19
10630
18.0
Y
19
0630
8.0
Y
20
0930
24
0630
8.0
Y
21
1
0600
8.0
Y
22
0630
8.0
0730
4.0
24
0715
4.0
rB23
25
0630
8.0
26
0630
8.0
B
27
0930
24
'0630
8.0
Y
28
0630
8.0
Y
Monthly Average limit:
0.332
0.058
0.048
0.336
0.068
3583
0.261
Monthly Average:
Daily Maximum:
Daily Minimum: I
+-
I
I
I I
I
I
I
••**NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2019 (February 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
F
u
G
fiig°
r
°
E
_
d`
O
O
F
O
O
°
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DBNET-PH
DNBPHTH
ETIMBEN
FLUORENE
HEXCLBD
ACE
LEAD
hfET[fYI.CH
MECL2
NAPTHALE
NICKEL
2400 clock
are
2400 dock
Hrs
Y/B/N
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
lbs/day
1
0630
8.0
Y
2
0915
2.0
B
3
0930
3.25
Y
4
0630
8.0
Y
5
0430
8.0
Y
6
0930
24
0630
8.0
Y
7
043
88.0
Y
8
0600
8.0
Y
9
0845
5.25
Y
10
0945
5.5
Y
NOFLOW
11
0430
8
Y
NOFLOW
12
0630
8
Y
NOFLOW
13
0630
8
Y
NOFLOW
14
0600
8
Y
NOFLOW
15
0630
4.0
Y
NOFLOW
16
N
NOFLOW
17
1400
2.0
B
INOFLOW
18
0630
8.0
Y
19
0630
8.0
Y
20
0930
24
0630
8.0
Y
21
0600
8o
Y
22
0630
8.0
B
23
0730
4.0
In
24
0715
4.0
B
25
0630
8.0
Y
26
0630
8.0
B
27
10930
24
0630
8.0
Y
28
0630
8.0
ly
Monthly AvemV Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12846
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2019 (February 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
E
d
9
U
F
6
Q
O
=
N
O
6
O
a
O
:
y
�emj
,Z�
34447
34461
34694
34469
34475
34010
34376
34626
34220
39700
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NrrROBEN
PHENANTH
PHENOL
JPYRENE
TETCLETY
TOLUENE
FLUORANT
261HNrTR
ANTHRACE
HCB
2400 dock
H.
2400 dock
Hkx
Y/B/N
Ibs/day
Ibs/day
Ibs/day
lbs/day
Ibs/day
Ibs/day
ug/l
ug/l
ug/l
ug/l
1
0630
8.0
Y
2
0915
2.0
B
3
0930
3.25
Y
4
0630
8.0
Y
5
0430
8.0
Y
6
0930
24
0630
8.0
ly
7
0430
8.0
Y
8
0600
8.0
Y
9
10845
5.25
Y
10
1
0945
5.5
Y
NOFLOW
11
0430
8
Y
NOFLOW
12
0630
8
Y
NOFLOW
13
0630
8
Y
NOFLOW
14
0600
8
Y
NOFLOW
15
0630
4.0
Y
NOFLOW
16
N
NOFLOW
17
1400
2.0
B
NOFLOW
IB
0630
8.0
Y
19
0630
8.0
Y
20
0930
24
0630
8.0
Y
21
0600
8.0
Y
22
0630
8.0
B
23
0730
4.0
B
24
1
0715
4.0
B
25
0630
8.0
Y
26
0630
8.0
B
27
0930
24
0630
8.0
Y
28
0630
18.0
ly
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.084
Munthly Average:
Daily Maximum:
Daily Minimum:
***•NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2019 (February 2019)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 03/13/2019
03/13/2019
ORC/Certifier Signature: Michael D parks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
03/13/2019
Permittee/Submitter Signature Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNED NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2019 (February 2019)
Report Comments:
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
02/06/19, Total Nitrogen, Total Phosphorus; Below Reporting Limit
02/06/19, 02/27/19; Fecal Coliform; Below reporting limit.
02/06/19, BOD; Below reporting limit.
02/20/19, BOD; Blank value is outside of control limits. Difference between sample dilutions is greater than 30%. GGA result is greater than the control limit.

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2019 (January 2019)
PERMIT VERSION: 4.0 g
CLASS: W -2 B� `"} W
ORC: Michael D. Sparks FEB 2 2 2019
ORC HAS CHANGED: No
CEN 1 KAL FILF-a
VERSION: 1.0 D%A/R SECTIO]
PERMIT STATUS: Expired
COUNTY: Clevelandg� E
ORC CERT NUMBERN 773 ®fPdC[3L-"NR/D'NR
STATUS: Processed
MAR -g 4 201y
WQROS
MOORESVILLE REGIONAL OFFICE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
.s
E
'E
E
H
ti
50050
OU400
QD310
QD530
31616
C0600
C0665
31196
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
IPH
HOD - Qty Daily
TSS - Qty Daily
FCOLI BR
TOTAL N -
TOTAL P - Coac
1,1-DCE
II-DCEY
2400 clock
Hrs
2400 dock
H.
YMN
mgd
Sul
Ibs/day
lbs/day,
#/100ml
mg/I
mg/l
Ibs/day
lbs/day
1
0900
1.25
B
0.368
2
0930
24
0630
8.0
Y
0.328
8.1
6
7.9
16
3
0630
8.0
B
0.407
4
0630
110.0
B
0.37
5
0915
1.25
B
0.363
6
0915
3.25
B
0.382
'
7
0630
8.0
Y
0.373
8
0430
10.0
Y
0.382
9
0930
24
0430
10.0
Y
0.379
8.1
9.5
12
2
10
0600
9.0
Y
0.366
11
0630
8.0
Y
0.335
12
1
10700
16.0
Y
0.294
13
0400
9.0
B
0.293
14
0630
8.0
Y
0.305
15
0930
24
0430
10.0
Y
0.295
8.3
14
6.4
<2
16
0430
10.0
Y
0273
17
0600
18.0
Y
0.23
18
0430
10.0
Y
0.262
19
0600
2.50
Y
0.237
20
N
NOFLOW
21
N
I NOFLOW
22
1
0630
19.5
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
0430
10.0
Y
NOFLOW
25
0630
8.0
Y
NOFLOW
26
N
NOFLOW
27
1600
3.0
Y
NOFLOW
28
0430
110.0
Y
NOFLOW
29
0630
8.0
Y
0.383
30
0930
24
0630
10.0
Y
0.39
8.3
<6.5
8.5
<2
31
0600
8.0
1 Y
0.404
Monthly Average limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.337227
7.375
8.7
2.378414
Daily Maximum:
0.407
8.3
14
12
16
Daily Minimum:
0.23
8.1
0
6.4
0
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation -Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2019 (January 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
e
F
u
e
8
u
n
E
u
-
F
e
F
-
'c
<
O
c
O
6
F
O
u
O
.L
L
34536
32103
34541
34W
77163
34566
34571
34601
34606
34616
34611
AnnuallyAnnually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
lj-DCPE
1,3-DCB
1,4-DCB
2,4-DCPH
2A-DMPH
2p-DNPB
2p-DNT
2400 clock
H.
2400 clock
H.
WHIN
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
1
0900
1.25
B
2
0930
24
0630
8.0
Y
3
0630
8.0
B
4
0630
10.0
B
5
0915
1.25
B
6
0915
3.25
B
7
0630
8.0
Y
8
0430
10.0
Y
9
0930
24
0430
10.0
Y
10
10600
19.0
Y
11
0630
8.0
Y
12
0700
6.0
Y
13
0400
9.0
B
14
0630
8.0
Y
15
0930
24
0430
10.0
Y
16
0430
10.0
Y
17
0600
8.0
Y
18
0430
10.0
Y
19
0600
2.50
Y
20
N
NOFLOW
21
N
NOFLOW
22
0630
9.5
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
0430
10.0
Y
NOFLOW
25
0630
8.0
Y
NOFLOW
26
N
NOFLOW
27
1600
3.0
Y
NOFLOW
28
0430
10.0
Y
NOFLOW
29
0630
8.0
Y
30
0930
24
0630
10.0
Y
31
0600
8.0
Y
Monthly Average limit:
0.249
0.119
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0129
0365
Monthly AveragC
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVY rM = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2019 (January 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
O'
E
e`
U'
F`
=
O
_
`
O
O
°e
x
345M
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-o-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZ0-A-A
BNZO-A-P
2400 clock
H.
2400 clock
H.
YINN
Ibs/day
Ibs/day
ug/I
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/1
Ibs/day
ug/1
11911
1
0900
1.25
B
2
0930
24
0630
8.0
Y
3
0630
8.0
B
0630
10.0
1 B
5
0915
1.25
B
6
0915
3.25
B
7
063
88.0
Y
8
0430
10.0
Y
9
0930
24
0430
10.0
Y
to
10600
19.0
Y
11
0630
8.0
Y
12
0700
6.0
Y
13
0400
9.0
B
14
0630
8.0
Y
15
0930
24
0430
10.0
Y
16
10430
10.0
1 Y
17
0600
8.0
Y
18
0430
10.0
Y
19
0600
2.50
Y
20
N
NOFLOW
21
N
NOFLOW
22
0630
9.5
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
0430
110.0
Y
NOFLOW
25
0630
8.0
Y
NOFLOW
26
N
NOFLOW
27
1600
Y
NOFLOW
28
0430
Y
NOFLOW
29
0630
L8.01y
Y
30
0930
24
0630
Y
31
0600
Monthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Macimum•
Daily Minimum:
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2019 (January 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
u
9
E
6
u
8
Q
F
-
-
O
0
,�'
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
112E PHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr_TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 dock
Hrs
2400 clock
Hrs
VA31N
ug/I
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/I
ugll
ug/I
119/1
ibs/day
1
0900
1.25
B
2
0930
24
0630
8.0
Y
3
0630
8.0
B
4
0630
10.0
B
5
0915
1.25
B
6
0915
3.25
B
7
10630
8.0
Y
8
0430
10.0
Y
9
0930
24
0430
10.0
Y
10
0600
9.0
Y
11
0630
8.0
Y
12
1
0700
6.0
Y
13
0400
9.0
B
14
0630
8.0
Y
15
0930
24
0430
10.0
Y
16
0430
10.0
Y
17
0600
8.0
Y
18
0430
10.0
Y
19
0600
2.50
Y
20
N
NOFLOW
21
N
NOFLOW
22
0630
9.5
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
0430
10.0
Y
NOFLOW
25
0630
8.0
Y
NOFLOW
26
N
NOFLOW
27
1600
3.0
1 Y
INCIFLOW
28
0430
10.0
Y
NOFLOW
29
0630
8.0
Y
30
10930
124
10630
10.0
Y
31
0600
8.0
Y
Monthly Average Limit:
0.332
0.058
0.048
0.336
0.068
3.583
0261
Monthly Average
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2019 (January 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
O
§
F
e
d
'P
u
.9
12
F
O
=
y
O
_
�
o
a
O
o
9
cy
2
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNBPHTH
ETHYLBEN
FLUORENE
HEXCLBD
HCE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 dodo
Hrs
2400 door
H.
YMN
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
Ibstday
lbs/day
lbs/day
lbs/day
1
0900
1.25
B
2
0930
24
0630
8.0
Y
3
0630
8.0
B
4
0630
10.0
B
5
0915
11.25
B
6
0915
3.25
B
7
0630
8.0
Y
8
0430
10.0
Y
9
0930
24
0430
10.0
Y
10
1
0600
9.0
ly
11
0630
8.0
Y
12
0700
6.0
Y
13
0400
9.0
B
14
0630
8.0
Y
15
0930
24
0430
10.0
Y
16
0430
110.0
Y
17
0600
8.0
Y
18
0430
10.0
Y
19
0600
2.50
Y
20
N
NOFLOW
21
N
NOFLOW
22
1
0630
19.5
Y
INOFLOW
23
0630
8.0
Y
NOFLOW
24
0430
10.0
Y
NOFLOW
25
0630
8.0
Y
NOFLOW
26
N
NOFLOW
27
1600
3.0
Y
NOFLOW
28
0430
10.0
Y
NOFLOW
29
0630
8.0
Y
30
0930
24
0630
10.0
Y
31
0600
8.0
Y
Monthly Average Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2227
0178
0.129
0.071
12JM
Monthly Avcrag,..
Daily Maximum:
Daily Minimum
••ssNoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 01-2019 (January 2019)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
"
u
a
o
u
O
Z
34447
34461
34694
34469
34475
34010
34376
M26
34220
39700
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
FLUORANT
26DINFTR
ANTHRACE
HCB
2400 clock
Hra
2400 clock
Hr5
Y/nrN
lbs/day
lbs/da
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/I
ugq
ug/l
ug/I
1
0900
1.25
B
2
0930
24
0630
8.0
Y
3
0630
8.0
B
4
0630
10.0
B
5
1
10915
11.25
B
6
0915
3.25
B
7
0630
8.0
Y
8
0430
10.0
Y
9
0930
24
0430
10.0
Y
10
1
10600
19.0
Y
11
0630
8.0
Y
12
0700
6.0
Y
13
0400
9.0
B
14
0630
8.0
Y
r5
0930
24
0430
10.0
Y
16
0430
10.0
Y
17
0600
8.0
Y
18
0430
10.0
Y
19
0600
2.50
Y
20
N
NOFLOW
21
N
NOFLOW
22
0630
9.5
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
0430
10.0
Y
NOFLOW
25
0630
8.0
Y
NOFLOW
26
N
NOFLOW
27
1
1600
13.0
Y
NOFLOW
28
0430
10.0
Y
NOFLOW
29
0630
8.0
Y
30
0930
24
0630
10.0
ly
31
0600
8.0
Y
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.084
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2019 (January 2019)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 02/18/2019
02/ 11 /2019
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
Perm ittee/Submitter Si
02/18/2019
*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2019 (January 2019)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
Report Comments:
1/15/19, 1130/19, Fecal Coliform; Below reporting limit.
1/2/19, BOD; Blank value is outside of control limits.
1/15/19, BOD; Difference between sample dilutions is greater than 30%. Blank value is outside of control limits.
1/30/19, BOD; Below reporting limit. GGA result is greater than the control limit
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
e'-
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2018 (December 2018)
PERMIT VERSION: 4.0
CLASS: WW-2 V
ORC: Michael D. Sparks
ORC HAS CHANGED: No JAN 2
VERSION: 1_0 CEWI 1'�At- FILES
ki
PERMIT STATUS: Expired 3
COUNTY: Cleveland
ORC CERT NUMBER: 9$273,2IVEDACDENR/©WR
STATUS: Processed JA N 2 8 %,91,9
DW R SO,
lh`G1ROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISC�HAffG)ff* FNp,lONAL OFFI(,e
E
rP
F'E
Eo
3
E
z
c
1`
'
Z
50050
004011
QD310
QD530
31616
C0600
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekl
Semi-annually
jCO665
i-annually
Annually
Annuallh
Recorder
Grab
Com osite
Com osite
Grab
Com osite
osite
Grab
Grab
FLOW
1,11
BOD -Qty Daily
T55-Qty Doily
FCOLI BR
TOTAL N-
TOTAL P - Cone
1,1-DCE
1,1-DCEY
2400 clock
Firs
2400 clock
H.
MIN
m d
su
Ibs/day,
Ibs/day
9/100ml
mg/I
mg/l
Ibs/day
Ibs/day
1
N
NOFLOW
2
1615
2
Y
NOFLOW
3
0630
8
Y
0.268
0930 124
0430 1
10
Y 1
0.378
8.4
20.5
12
<2
5
0430
10
Y
0.341
6
0600
8
Y
0.388
7
0600
8
Y
0.342
8
0900
3
Y
0.269
0900
13.5
B 1
0.308
10
0800
4.75
B
0.402
11
0630
8
Y
0.411
12
0930
24
0630
8
Y
0.366
7.9
<6.1
9.2
<2
13
0430
10
Y
0.328
11
1
10600
18
Y
I
0.26
15
0900
4
Y
0.306
16
0930
4.5
Y
NOFLOW
17
0430
8
Y
0.226
18
0630
8
Y
0.234
19
10600
18
Y
1
0.343
20
0930
24
0600
8
Y
0.358
8
11.3
7.8
<2
21
0545
8
Y
0.425
22
0930
2
B
0.411
23
N
NOFLOW
24
N
I NOFLOW
25
N
NOFLOW
26
0630
8
B
NOFLOW
27
0630
8
B
NOFLOW
28
10630
8
B
NOFLOW
29
0930
8
B
NOFLOW
30
0630
2
B
NOFLOW
31
0630
1 7
B
0.447
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.34055
10.6
9.666667
1
Doily Maximum:
0.447
8.4
20.5
12
0
DailyMinicuum
0.226
7.9
0
7.8
0
**** No Reporting Reason: ENFRUSE = No Flow-Retlse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
L"-
OWNER NAME: C N A -Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2018 (December 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
N',n,
U
u
l-
F
a
O
c
E
O
o
O
A
Z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPH
2,4-DMPH
2,1-DNPH
2,4-DNT
2400 clock
R.
2400 clock
I H.
Y/B/N
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/da
Ibs/day
Ibs/da
1
N
NOFLOW
2
1615
2
Y
NOFLOW
3
0630
8
Y
4
0930
24
0430
10
Y
5
10430
1 10
Y
6
0600
8
Y
7
0600
8
Y
8
0900
3
Y
9
0900
3.5
B
l0
0800
14.75
B
11
0630
8
Y
12
0930
24
0630
8
Y
13
0430
10
Y
14
0600
8
Y
15
10900
14
Y
16
0930
4.5
Y
NOFLOW
17
0430
8
Y
18
0630
8
Y
19
0600
8
Y
20
0930
24
0600
8
Y
21
10545
18
Y
22
0930
2
B
23
N
NOFLOW
24
N
NOFLOW
25
N
NOFLOW
26
0630
18
B
I NOFLOW
27
0630
8
B
NOFLOW
28
0630
8
B
NOFLOW
29
0930
8
B
NOFLOW
30
0630
2
B
NOFLOW
31
0630
J7
JB
Monthly Average Limit:
0149
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Retise/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004052
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
L
OWNER NAME: C N A -Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2018 (December 2018)
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001. NO DISCHARGE*: NO (Continue)
v
C
E
i
b
_
E
U'
E
E
3
12
E
?
'E
u
O
_
N
E
F
O
UU
O
e
5
t
Y
Z
34586
34591
79531
34657
34646
34205
34200
34215
34030
34247
Annually
Annual)
Annually
Annual)
Annual)
Annually
Annually
Annually
Annual)
FBNZO-A-A
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPIIENOL
2NPHENOL
34-BNZFA
46DN-a-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-P
2400 crock
H.
2400 c1ach
Hrs
Y/B/N
Ibs/da
Ibs/da
ugA
Ibs/da
Ibs/day
Ibs/day
Ibs/day
u I
Ibs/day
u
ug/I
I
N
NOFLOW
2
1615
2
Y
NOFLOW
3
0630
8
Y
4
0930
24
0430
10
Y
5
0430
10
Y
6
0600
Is
Y
7
0600
8
Y
8
0900
3
Y
9
0900
3.5
B
10
0800
4.75
B
I
0630
18
Y
12
0930
24
0630
8
Y
13
0430
10
Y
14
0600
8
Y
15
0900
4
Y
16
0930
4.5
Y
NOFLOW
17
0430
8
Y
Is
0630
8
Y
19
0600
8
Y
20
0930
24
0600
8
Y
21
0545
8
Y
22
0930
2
B
23
N
NOFLOW
24
N
NOFLOW
25
N
NOFLOW
26
0630
8
B
NOFLOW
27
0630
8
B
NOFLOW
28
0630
8
B
NOFLOW
29
1
10930
18
B
NOFLOW
30
0630
2
B
NOFLOW
31
0630
7
In
Monthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly A%eragc:
Daily M.imum;
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Retise/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A_Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2018 (December 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
`�
E
CJ
I✓
fi
u
s
F'
F'
�
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R
O
m
O
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F
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O
•�
_
a
Z'
34242
39100
3210E
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DNZO-K-F
BEE PHTA
CARBNTET
CRLAOBNZ
CLROETHA
C![LRFORM
Cr-TOTAL
CIIRYSENE
COPPER
CN-TOT
DIETY-PR
2400 clock
H.
2400 clock
H.
Y!B/N
ug/1
Ibs/da
Ibs/day
Ibs/da
Ibs/day
lbs/day
ug/1
ugA
ug/1
ugA
Ibs/da
1
N
NOFLOW
2
1615
2
Y
NOFLOW
3
0630
8
Y
4
0930
24
0430
10
Y
5
0430
10
Y
6
0600
8
Y
7
0600
8
Y
8
0900
13
Y
,q
0900
3.5
B
10
0800
4.75
B
11
0630
8
Y
12
0930
24
0630
8
Y
13
0430
10
Y
14
10600
is
Y
15
0900
4
Y
16
0930
4.5
Y
I NOFLOW
17
0430
8
Y
18
0630
8
Y
19
0600
8
Y
20
0930
24
10600
18
Y
21
0545
8
Y
22
0930
2
B
23
N
NOFLOW
24
N
NOFLOW
25
N
NOFLOW
26
0630
8
B
NOFLOW
27
0630
18
B
NOFLOW
28
0630
8
B
NOFLOW
29
0930
8
B
NOFLOW
30
0630
2
B
NOFLOW
31
0630
7
B
Monthly Average Limit:
0.332
0.058
0.048
0.336
0.068
3.583
0.261
Monthly Average:
Daily Maximum:
Daily Minimum:
* * * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR'= No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER "ME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2018 (December 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION:1.0 1
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
_
E
U
F•
9
1-
a
O
�
o
O
O
u
L
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696 111067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNBPHTH
ETHYLBEN
FLUORENE JHEXCLBD
HCE ILEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 clock
Hrs
2400 clock
Hrs
Y/B/N
Ibs/da
Ibs/day
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/day
Ibs/da
I
N
NOFLOW
2
1615
2
Y
NOFLOW
3
r240430
0630
8
Y
4
0930
10
Y
5
0430
10
Y
6
0600
8
Y
7
0600 18
Y
8
0900
3
Y
9
0900
3.5
B
10
1
0800
4.75
B
11
0630
8
Y
12
0930
24
0630
8
Y
13
0430
10
Y
14
0600
8
Y
15
0900
4
Y
16
1
0930
14.5
Y
NOFLOW
17
0430
8
Y
is
0630
8
Y
19
0600
8
Y
20
0930
24
0600
8
Y
21
10545
18
Y
22
0930
2
B
23
N
NOFLOW
24
N
NOFLOW
25
N
NOFLOW
-
26
0630
8
B
NOFLOW
27
0630
8
B
NOFLOW
28
0630
8
B
NOFLOW
29
0930
8
B
NOFLOW
30
0630
2
B
NOFLOW
31
0630
7
B
Monthly Average Limit:
0.061
0.087
0.103
0.071
10.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Average:
Daily Maximum:
Daily Minimum:
* ** * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2018 (December 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
A
E
E
V
.E
u`
•�
F
!r
a
�
O
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ig
e
O
y
O`
a
O
z
Z
34447
00556
TGP311
34461
34694
34469
34475
34010
34220
39700
34626
Annually
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
OH GRSE
CERI7DPF
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
ANTHRACE
HCB
26DINITR
2400 clock
n.
2400 dacic
Hrs
Y/B/N
Ibs/day
m
ass/fail
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/day
No
ug/1
ug/1
1
N
NOFLOW
2
1615
2
Y
NOFLOW
3
0630
8
Y
4
0930
24
0430
10
Y
<5
PASS
5
1
10430
110
Y
6
0600
8
Y
7
0600
8
Y
8
0900
3
Y
9
0900
3.5
B
10
0800
14.75
B
11
0630
8
Y
12
10930
24
0630
8
Y
13
0430
10
Y
14
0600
8
Y
is
0900
14
Y
16
0930
4.5
Y
NOFLOW
17
0430
8
Y
i5
0630
8
Y
19
0600
8
Y
20
10930
24
10600
18
Y
21
0545
8
Y
22
0930
2
B
23
N
NOFLOW
24
N
NOFLOW
I
25
N
NOFLOW
26
0630
8
B
NOFLOW-'
27
1
0630
8
IB
I NOFLOW
28
0630
8
B
NOFLOW
29
0930
8
B
NOFLOW
38
0630
2
B
NOFLOW
31
0630
17
B
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071 _
0.084
Montbly Average:
0
Daily Maximum:
0
Daily Minimum:
0
** * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3
eDMR PERIOD: 12-2018 (December 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
F
6
E
F
_
r
�
3
O
m
E
O
o
04
O
c
to
2
34376
Annually
Grab
FLUORANT f-
2400 clock
Rrx
2400 clock
H.
Y/D/N
u
1
N
NOFLOW
2
1615
2
Y
NOFLOW
3
0630
8
Y
4
0930
24
0430
10
Y
5
0430
10
Y
6
0600 Is
Y
7
0600
8
Y
8
0900
3
Y
0
0900
3.5
B
10
0800
4.75
B
11
0630
8
Y
0930
24
0630
8
Y
13
0430
10
Y
r1512
14
0600
8
Y
0900
4
Y
16
10930
4.5
Y
NOFLOW
17
0430
8
Y
ie
0630
8
Y
19
0600
8
Y
20
0930
24
0600
8
Y
21
0545
8
Y
22
0930
2
B
23
N
NOFLOW
24
N
NOFLOW
'
25
N
NOFLOW
26
0630
8
B
NOFLOW
27
0630
8
B
NOFLOW
28
0630
8
B
NOFLOW
29
0930
8
B
NOFLOW
30
0630
2
B
NOFLOW
31
0630
7
B
Monthly Average Limit:
,
Monthly M erage:
Daily Maximum:
Daily Minimum:
****NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2018 (December 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 01/17/2019
01/16/2019
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
�1_
6 01/17/2019
Permittee/Submitter Signature: Nicole B Coffee E-Mail:[e-mail] Phone 4:704-480-5729 Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221, 402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2018 (December 2018)
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
Report Comments:
12/4/18, 12/12/18, 12/20/18, Fecal Coliform; Below reporting limit.
12/4/18, 12/20/18, BOD; Blank value is outside of control limits. Difference between sample dilutions is greater than 30%.
12/12/18, BOD; Below reporting limit.
12/4/18, Oil & Grease; Below reporting limit

f r
ETCM,,,1aic. (664) 077fi6942 . rAX (064) B77.4393B
f!fl. Box 16414, Greenville, SC 29606 4 Ctraflsrnan Cuurt, Graer, 5C 29050
Ceriodaphnia dubia Survival and Reproduction Test
EPA-821-R-02-013 Method 1002
Client: CELANESE/CNA
Sample ID: 001 EFFLUENT
NPDES #: NC0004952
Test Date: 05-Dec-18
Laboratory ID #: T52984
Test Reviewed and Approved By:
W 4
Robert W. Kelley, Ph.D.
QA/QC Officer
'�I Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. Included results pertain only to provided'sanVes.
age 1 of 6
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50
Date 17-Dec-18
CNA HOLDINGS TICONA WWTP NPDES# NC0004952 Pipe # 001 County: Cleveland
ry Performing Test: I Comments
X
Signature of Operator i i
X
Signature of Laboratory Su
MAIL ORIGINAL TO Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results
Rank sum= 151
Critical Value= 109
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction= 0.0%
# Young Produced 22 25 26 22 24 22 25 27 22 23 21 24 % Mortality Avg. Reprod.
Adult (L)ive (D)ead L L L L L L L L L L L L 0% 23.6
Control Control
Effluent % 2.13% 0% 23.6
Treatment 2 Treatment 2
Control CV
TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 8.0%
# Young Produced 25 22 27 23 22 23 26 22 26 23 22 22 % 3rd Brood PASS FAIL
Adult (L)Ive (D)ead L L L L L L L L L L L L 100% X
Complete This for Either Test Test Start Date
Collection StartDate 05-Dec-18
pH 1st sample 1st sample 2nd sample Sample 1 03-Dec-18 Sample 2 05-Dec18
Control 7.6 7.8 7.6 8.0 7.7 7.8 Sample Jype (Duration)
Treatment 2 7.6 7.9 7.7 8.1 7.7 7.8 Grab Comp Duration 1st 2nd
Sample 1 X 24hrs. Tox Tox
Sample 2 X 24hrs. Dilution Sample Sample
start end start end start end.
D.O. 1st sam le 1st sam le 2nd sam le Hardness (mg/L) 48.0
Control 6.8 7.8 7.5 7.3 7.7 7.5 Spec. Cond. (Nmhos) 181 576 488
Treatment 2 6.8 7.8 7.7 7.4 7.5 7.3 Chlorine (mg/L) <.05 <.05
Sample Temp. at receipt (°C) � 0.4 0.4
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates)
Concentration
Mortality start/end start/end
LC50 = % Method of Determination Control
95 % Confidence Limits Moving Average Probit I High Conc.
Spearman Kerber ROther pH D.O.
Organism Tested Cerioda hnia dubia
DEM Form AT-1
Page 2 of 6

STATISTICAL ANALYSIS RESULTS
Facility: CNA HOLDINGS
NPDES# NC0004952
Sample ID: TICONA WWTP
ETT# T52984 Date: 05-Dec-18
Laboratory:
Certification #: NCO22
Exp. Date: 11/1/2019
Survival Data
7 Day Survival
Test Used: FISHERS TEST
Control 100%
Test Statistic: P= 1.000
Effluent 100%
Critical Value: P= 0.01
PASS: The effluent does not reduce survival of the test organisms.
Reproduction Data
Raw Data
Test for Normality
Mean young/female
Std. Dev.
Test Used: Shapiro -Wilke Test:
Control 23.6
1.88
Effluent 23.6
1.88
W:
0.876
Critical Value:
0.884
Analysisfor Differences in Reproduction
Test for Homogeneity of Variance
Test Used: Wilcoxon Test
Test Used: F Test
Rank sum=
151.00
F=
1.00
Critical Value=
109.00
Critical Value=
5.32
The data are homogeneous in variance
PASS: The effluent is not chronically toxic.
Page 3 of 6

` Control Mortalityand Reproduction by Test Day ^-
source
rep
1 2 3 4 5 6 7 8
Total
R711-22
1
+4+7
11
22
JJ1 11-28
2
+5+8
12
25
X211-23
3
5
+8+13
26
M1011-2
4
+3+8
11
22
KK711-2
5
+3+9
12
24
U8 11-23
6
+4+7
11
22
06 11-22
7
+3+8
1
141
25
LL3 11-28
8
+4+9
14
27
V4 11-23
9
+3+9
10
22
P511-22
10
+4+8
11
23
117 11-28
11
+4+7
10
21
W 1 11-23
12
+3+9
12
24
13
N/A
0
14
N/A
0
15
N/A
0
16
N/A
0
17
N/A
0
18
N/A
0
19
N/A
o
Mean
20
N/A
0
23.6
Z-13/m. iEffluent:Mortalityand Reproduction by Test'Day
1 2 3 4 5 6 7 8
Total
R7 11-2
1
+3+11
11
25
111 11-
2
+4+8
10
22
X211-2
3
5
+9+13
27
M10 11
4
+4+7
12
z3
KK7 11
5
+3+7
12
22
U8 11-2
6
+5+7
11
23
0611-
7
+5+8
1
131
26
LL3 11-
8
+3+8
11
22
V411-2
9
+3+9
14
26
P5 11-2
10
+3+10
10
23
117 11-2
11
+3+7
12
22
W1 11-1
12
+3+8
11
22
0
13
N/A
0
0
14
N/A
0
0
15
N/A
0
0
16
N/A
0
0
17
N/A
0
0
18
N/A
0
0
19
N/A
o
Mean
0
20
N/A
0
23.6
reneW0
" end _-A4
Jc
Jc
End., ate �<
JG
JC
AM
JC
JC
JC
12-Dec-18
flfnB4tad(&,feneW
03:4e PM
04:19 PM
Oe:4] AM
09:3R AM
09:39 AM
OCH PM
�';ti, �,":'�:�
10Z AM JC
New,temp:..,°C
24.6
24.6
Old temp.'C
24.6
25
24.9
Control New temp. °C
24.61
24.6
Page 4 of 6

�O Box 18414, t;reanv111% BC 2966a-7414
664) 9T7-6942, (HBO)891-2326 Flax (ae4) 077 6938
ihippin9 Addreae: 4 Cragaman Ct, Greer, 6C 29680
4WW.Gr rLr4VmeNN M"rAL.oel&1
Client:
M �. S
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State: L NPDES M AJ C- Y9
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SAMPLE ID 61gorromflosiarinnialnme sampla collection Dale Time
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;ample Custody Transfer Record
Date Time in 'shed Bv 10 nizat)o
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:OMPOSITE SAMPLING PROCEDURES
:olnposite samples must be collected over a 24 hour period.
'Ime Proportional: 1 sample each hour for 24 hours. Equal v
r at minimum 1 sample every 4 hours over 24 hours.
CHAIN 0-- C'US ODD RECORD _
Page
Program
Contniaers
Presemotive
Parameters
tl'boloamaeat Toxlctty
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Samples nparature during collection and transport mustlie behveen
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Secure Reccipt Sample
Area Tcmn aC I Preservcc
:
HOLD TIMEPROCEDURES
For toxicity testing the sample must first be used within 36 hours
ofsample collection (completion orcomposim sample).
Sample mny not be used after 72 hours from sample collection.

CHAIN OF CUSTODY
RECORD
a0 eoa 164 4, OraenAlle, 80 20006-7414
page _L— of _l<
004) OTT-8942, (S00) 091-2325 F=(8641077 M30
MIPpitig Address: 4 Cranaman Ct, Greer, SC 29060
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Program Contalners Preserath'e Parameters
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:OMPOSITE S"PU M PROCEDURES
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HOLD TW FR0CF.DURES
:omposile samples must be collected over a 24 hour period.
Sample
cyaniture during collection and transport mustbo hahveen
For toxicity testing the sample must first be used ►tidiin 36 hours
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0.0 and,
-CI°C, Samples mustnot be frozen. Use water loa In sealed bags.
of sample collection (compaction of composite sample).
'loin Proportional: As per instructions In NPDES VarmIL
Sample may not be used after 72 hours froin sample collection.

NPDE'S PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER'NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2018 (November 2018)
PERMIT VERSION: 4.0
CLASS: WW-2 I F"F I ED
ORC: Michael D. Sparks J nfiN 0 3 2019
ORC HAS CHANGED: No _ G�J
VERSION: 1.0 CEN I RAI. PILES
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
RECEIVEDIINCDENRID`M
STATUS: Processed i/xN 14 019
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*:vli X-60MOORELE REGIONAL OFFICE
w
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F
u
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6
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F
2
w
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_
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C
O
a
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'-
C
Z
S0050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
FH
BOD -Qty Daily
T85-Qty Daily
FCOLIBR
TOTAL N-
TOTAL P-Cant
l,r-DCE
1,1-DCEY
2400 clock
Rrs
2400 clock
Firs
Y/B/N
mgd
su
Ibs/day
Ibs/day
#/loom]
mg/I
mg/I
Ibs/day
Ibs/day
1
0600
8.0
B
0.401
2
0600
8.0
B
0.394
3
N
NOFLOW
4
N
NOFLOW
5
0630
8.0
Y
NOFLOW
6
0600
8.0
Y
0.433
7
0930
24
0630
8.0
Y
0.392
8.1
<6.5
19.9
4
8
0500 19.0
Y 1
0.339
9
0630
8.0
Y
0.342
10
0930
2.0
B
0.368
11
0900
2.0
B
0.307
12
0630
8.0
Y
0.242
13
0630
8.0
Y
0.315
14
0930
24
0630
8.0
Y
0.4
8
10
13
2
15
0600
8.0
Y
0.383
16
0430
lo.o
Y
0.431
17
0800
4.5
Y
0.395
18
0730
4.0
Y
0.381
19
0500
10.0
Y
0.369
211
0930
24
0500
10.0
Y
0.367
7.9
<6.1
10.7
<2
21
0430
9.5
Y
0.346
22
0800
2.0
Y
0.301
23
0745
3.45
Y
0.261
24
N
NOFLOW
25
1615
2.0
Y
NOFLOW
26
10430
1 10.0
Y
1
0.216
27
0630
8.0
Y
0.381
28
0930
24
0630
8.0
Y
0.393
8
29.8
10.8
<2
29
0600
8.0
Y
0.326
30
0630
8.0
Y
NOFLOW
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.353458
9.95
13.6
1.681793
Daily Maximum:
0.433
8.1
29.8
19.9
4
Daily Minimum:
0.216
7.9
0
10.7
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENNWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER'NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2018 (November 2018)
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
F
E
E
E
s
E
'E
O
t
E
-
O
O
UU
O
x
-
C
Z*
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPH
2,4-DMPH
2,4-DNPH
2,4-DNT
2400 clock
Hr.,
2400 clock
Hrs
Y/B/N
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/day
Ibs/day
Ibs/day
1
0600
8.0
B
2
0600
8.0
B
3
N
NOFLOW
4
N
NOFLOW
5
0630
8.0
Y
NOFLOW
6
0600
8.0
Y
7
0930
24
0630
8.0
Y
8
0500
9.0
Y
9
0630
8.0
Y
10
0930
2.0
B
11
0900
2.0
B
12
0630
8.0
Y
13
0630
8.0
Y
14
0930
24
0630
8.0
Y
15
1
10600
18.0
Y
16
0430
10.0
Y
17
0800
4.5
Y
l8
0730
4.0
Y
19
0500
10.0
Y
20
10930
24
0500
10.0
Y
21
0430
19.5
Y
22
0800
2.0
Y
23
0745
3.45
Y
24
N
NOFLOW
25
1615
2.0
Y
NOFLOW
26
0430
1 10.0
Y
27
0630
8.0
Y
28
0930
24
0630
8.0
Y
29
0600
8.0
Y
30
10630
8.0
Y
NOFLOW
Monthly Average Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly Average:
Daily Maximum:
Daily Minimum:
* * * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow, HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER'NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2018 (November 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
G
E
F
E
ti
_
E
U
E
.E
u
A
F
E
F
¢
O
in
EE
O
-
o
m
O
�
=
s
Z
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
12NPHENOL
34-BNZFA
46DN-a-C
4NPIIENOL
ACENAPEN
JACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
I BNZO-A-P
2400 clack
Hrs
2400 clock
H.
Y/B/N
Ibs/da
Ibs/day
ug/l
Ibs/day
Ibs/da
Ibs/day
Ibs/day
ugA
Ibs/day
ug/1
ugA
1
0600
8.0
B
2
0600
8.0
B
3
N
NOFLOW
4
N
I NOFLOW
5
0630
8.0
Y
NOFLOW
6
0600
8.0
Y
7
0930
24
0630
8.0
Y
8
0500
9.0
Y
0630
8.0
Y
10
1
0930
12..0
B
11
0900
2.0
B
12
0630
8.0
Y
13
0630
8.0
Y
14
0930
24
0630
8.0
Y
15
0600
8.0
Y
16
0430
1 10.0
Y
17
0800
4.5
Y
is
0730
4.0
Y
19
0500
10.0
Y
20
0930
24
0500
10.0
Y
21
0430
19.5
Y
22
0800
2.0
Y
23
1
0745
3.45
ly
24
N
NOFLOW
25
1615
2.0
Y
NOFLOW
26
0430
10.0
Y
27
10630
8.0
Y
28
0930
24
0630
8.0
Y
29
0600
18.0
Y
30
0630
8.0
Y
NOFLOW
Monthly Average Limit:
0,
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Macimum:
Daily Minimum:
* * * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: I 1-2018 (November 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
=
y'E
E
(5
F
E
u'
q
[=
E
F
e
O
in
O
E
e
O
o
U
O
°—
ce
Z
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
112EPHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 el-1<
lin
240U claek
Hrs
Y/B/N
ug/l
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/I
ugA
ug/I
ug/I
Ibs/day
1
0600
8.0
B
2
0600
8.0
B
3
N
NOFLOW
4
N
NOFLOW
5
1
10630
18.0
Y
I NOFLOW
6
0600
8.0
Y
7
0930
24
0630
8.0
Y
8
0500
9.0
Y
9
0630
8.0
Y
10
0930
2.0
B
11
1
10900
12.0
B
12
0630
9.0
Y
13
0630
8.0
Y
14
0930
24
0630
8.0
Y
15
0600
8.0
Y
16
0430
10.0
Y
17
0800
4.5
Y
is
0730
14.0
Y
19
0500
10.0
Y
20
10930
24
0500
10.0
Y
21
0430
9.5
Y
22
0800
2.0
Y
23
10745
13.45
Y
24
N
NOFLOW
25
1615
2.0
Y
NOFLOW
26
0430
10.0
Y
27
0630
8.0
Y
28
0930
24
0630
8.0
Y
29
0600
8.0
Y
30
0630
8.0
Y
I NOFLOW
Monthly Average Limit:
0.332
10.058
0.048
0.336
0.068
3.583
0.261
Monthly Average:
Daily M:uimum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Retise/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: I 1-2018 (November 2018)
CLASS: WW-2
ORC: Michael D. Sparks
ORC I-IAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
_
V
E
ci
f=
E
O
E
F
O
o
aao
O
x
L
z'
34341
39110
34371
34381
397112
34396
01051
34418
34423
01067
AnnuallyAnnuall
AnnuallyAnnuallyAnnually
Annually
AnnuallyAnnuallyAnnuallyAnnually
kn.all.,
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNBPHTH
ETHYLBEN
FLUORENE
HEXCLBD
HCE
LEAD
METIIYLCH
NIECL2
NPTH
NICKEL
2400 clock
tirs
2400 clock
firs
MIN
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/da
Ibs/da
lbs/day
Ibs/day
1
0600
8.0
B
2
0600
8.0
B
3
N
NOFLOW
4
N
NOFLOW
5
0630 18.0
Y I
NOFLOW
6
0600
9.0
Y
7
0930
24
0630
8.0
Y
8
0500
9.0
Y
9
0630
8.0
Y
10
0930
2.0
B
it
0900
2.0
B
12
0630
8.0
Y
13
0630
8.0
Y
14
0930
24
0630
8.0
Y
15
0600
8.0
Y
16
0430
10.0
Y
17
0800
4.5
Y
l8
0730
4.0
Y
19
0500
10.0
Y
20
0930
24
0500
10.0
Y
21
0430
9.5
Y
22
0800
2.0
Y
23
0745
3.45
Y
24
N
NOFLOW
25
1615
2.0
Y
NOFLOW
26
0430
10.0
Y
27
10630
18.0
Y
28
0930
24
0630
8.0
Y
29
0600
9.0
Y
3n
0630
8.0
Y
NOFLOW
Monthly Average Limit:
0.061
0.087
0.103
0.071
41.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Average:
Daily M cimmn:
Daily Minimum:
* * * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNERNAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2018 (November 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
u
A
E
u
E
_
E
Q
F
-
E
u'
[-'
E
`
G
-
O
'
O
F
u
O
_
o
C
O
C`
C
C`
Z
34447
34461
34694
34469
34475
34010
34376
34626
34220
39700
Annually
AnnuallyAnnually
AnnuallyAnnuallyAnnuallyAnnuallyAnnually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
FLUORANT
26DINITR
ANTHRACE
HCB
2400 clock
lira
2400 clock
If.
MIN
Ibs/day
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/day
ug/1 I
ug/I
u 1
ug/I
1
0600
8.0
B
2
0600
8.0
B
3
N
NOFLOW
4
N I
NOFLOW
5
0630
8.0
Y
NOFLOW
6
0600
8.0
Y
7
0930
24
0630
8.0
Y
a
0500
9.0
Y
9
0630
8.0
Y
10
0930
2.0
B
11
0900
2.0
B
12
0630
8.0
Y
13
0630
8.0
Y
14
0930
24
0630
8.0
Y
t5
0600
8.0
Y
16
0430
10.0
Y
17
0800
4.5
Y
18
0730
4.0
Y
19
0500
10.0
Y
20
0930
24
0500
10.0
Y
21
0430
9.5
Y
22
0800
2.0
Y
23
0745
3.45
Y
24
N
NOFLOW
25
1615
2.0
Y
NOFLOW
26
0430
10.0
Y
27
0630
8.0
Y
28
0930
24
0630
8.0
Y
29
0600
8.0
Y
30
1
0630
8.0
Y
I NOFLOW
Monthly Average Limit•
0.087
0.071
0.048
0.081
0.071
0.084
Monthly Average:
Daily Maximum:
Daily Minimum:
****No Reporting Reason:ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER -NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2018 (November 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 12/18/2018
12/16/2018
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
12/18/2018
v
Permittee Submitter Signature:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2018 (November 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
Report Comments:
11/20/18, 11/28/18, Fecal Coliform; Below reporting limit.
11/7/18, 11/20/18; BOD; Below reporting limit.
11/14/18 BOD; Blank value is outside of control limits. Difference between
11/28/18 BOD; Difference between sample dilution is greater than 30%
dilutions is
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
than 30%. GGA result is less than the control limit.

NFIDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2018 (October 2018)
PERMIT VERSION: 4.0 � P �r1k,
CLASS: WW-2- -
ORC: Michael D. Sparks Np� 6 2n1a
ORC HAS CHANGED: NorEI\r } `r,f L FILES
VERSION: 1.0 UVVC� SECTION
PERMIT STATUS: Expired 3
COUNTY: Cleveland
ORC CERT NUMBER: 987732
RECEIVED/NCDENW®11 R
STATUS: Processed DEC - 3 2018
OROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCH gV,N � EGIONAL OFFIC
o
U
S
F
E.
O
p
-
g
o°
O
z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pin
BOD -Qty Daily
TSS-Qty Daily
FCOLI BR
TOTAL N-
TOTALP-Cone
1,1-DCE
1,1.DCEY
2400 clock
H.
2400 clock
H.
YIWN
mgd
su
Ibs/day
lbs/day
k/100ml
mg/I
mg/I
Ibs/day
Ibs/day
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0630
8.0
Y
NOFLOW
6
0500
8.0
Y
NOFLOW
7
0930
4.
BB
NOFLOW
8
0500
9.5
Y
0.25
9
0600
8.0
Y
0.249
10
0930
24
10530
8.0
Y
0.252
8
23.1
20
4
11
0600
8.0
Y
0.274
12
0630
8.0
Y
0.391
13
0600
4.5
Y
0.363
14
0600
4.0
Y
0.359
15
0500
10.0
Y
0.306
16
0500
10.0
Y
0.258
17
0930
24
0600
8.0
Y
0.232
8.1
5.4
23.2
<2
1S
0500
9.5
Y
0.229
19
0630
8.0
Y
0.199
20
N
NOFLOW
21
N
NOFLOW
22
0630
8.0
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
0630
8.0
Y
NOFLOW
25
0600
8.0
B
NOFLOW
26
0600
8.0
B
NOFLOW
27
N
NOFLOW
28
1630
1.25
B
NOFLOW
29
0630
8.0
B
0.302
30
0600
8.0
B
0.403
31
0930
24
0600
8.0
B*
0.399
7.8
19.3
17
<2
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.297733
12.6
20.066667
1.587401
Daily Maximum:
0.403
8.1
23.1
23.2
4
Daily Minimum:
0.199
7.8
5.4
17
0
a"' No Repotting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
1
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 10-2018 (October 2018)
PERMIT VERSION: 4_0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
e
.0
u°
71
�
—
�
F
N
o°
a
=
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,7,DCB
1,7-DCE
1,2-DCP
t-12DCEY
II-DCPE
1,3-DCB
]p-DCB
2A-DCPH
24-DMPH
24-DNPH
2A-DNT
2400 clods
R.
2400 dock
H.
YMN
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0630
8.0
Y
NOFLOW
6
0500
8.0
Y
NOFLOW
7
0930
4.0
B
NOFLOW
8
0500
9.5
Y
9
0600
8.0
Y
10
10930
24
0530
8.0
Y
11
0600
8.0
Y
12
0630
8.0
Y
13
0600
4.5
Y
14
0600
4.0
Y
15
0500
Y
16
0500
Y
17
0930
24
0600
F8.0
Y
0500
Y
'
19
0630
8.0
Y
20
N
NOFLOW
21
N
NOFLOW
22
0630
8.0
Y
NOFLOW
23
1
10630
8.0
Y
NOFLOW
24
0630
8.0
1 Y
INOFLOW
25
0600
8.0
B
NOFLOW
26
0600
8.0
B
NOFLOW
27
N
NOFLOW
28
1630
1.25
B
NOFLOW
29
0630
8.0
B
30
0600
18.0
In
31
0930
24
0600
8.0
1 B
Monthly Arcragc Limit:
0.249
0119
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0365
Monthly Armagm
Daily Maximum:
Daily Minimum:
3i**NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2018 (October 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
A
E
E
IJ
_
u
F
6
—
'F
—
O
P
O
E
O
ro°�
O
X
34586
34591
79531
34657
34646
34205
34200
34215
1311311
3026
-247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Crab
Grab
Grab
Grab
Grab
Grab
1 2CPHENOL
2NPHENOL
34-BNZFA
46DNo-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clock
Hm
2400 clock
H.
Y/BN
lbs/day
lbs/day
ug/1
lbs/day
lbs/day
lbs/day
lbs/day
ug/l
lbs/day
jugn
ug/l
1
1
0600
8.0
IY
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
Y
NOFLOW
4
0630
Y
NOFLOW
5
0630
P4.013
Y
NOFLOW
6
0500
Y
NOFLOW
7
0930
NOFLOW
8
0500
9.5
Y
9
0600
8.0
Y
10
0930
24
0530
8.0
Y
11
0600
8.0
Y
12
0630
8.0Y
13
0
Y
14
0600
4.0
Y
15
0500
10.0
Y
16
0500
10.0
Y
17
0930
24
0600
8.0
Y
18
0500
9.5
Y
19
0630
8.0
Y
20
N
I NOFLOW
21
N
NOFLOW
22
0630
8.0
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
1
10630
8.0
Y
NOFLOW
25
0600
8.0
B
NOFLOW
26
0600
8.0
In
I NOFLOW
27
N
NOFLOW
28
1630
1.25
B
NOFLOW
29
1
0630
8.0
B
30
0600
8.0
B
31
0930
24
0600
18.0
In
Monthly Avcragclimit:
0.]
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Ma imum:
Dailyminimum:
ass*NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2018 (October 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
—
g
U
F
'E
A
F°
F
—
�E
a
O
�
O
F
d
O
-
a
O
rY
z
34242
39100
32102
34301
95811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
02E PHTH
CARBNTET
CHLROBNZ
CLROETRA
CHLIO+ORM
Cr-TOTAL
CHRYSENE
COPPER
CTi-TOT
DIETY-PH
2400 dodo
Hrs
2400 dodo
n.
YON
119/1
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
119/1
ug1l
119/1
ug/I I
lbs/day
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0630
8.0
Y
NOFLOW
6
1
0500
8.0
Y
NOFLOW
7
0930
4.0
B
NOFLOW
8
0500
9.5
Y
9
0600
8.0
ly
10
0930
24
0530
8.0
Y
11
0600
8.0
Y
12
0630
8.0
Y
13
0600
4.5
Y
14
10600
4.0
Y
15
0500
10.0
Y
16
0500
110.0
Y
17
0930
24
0600
8.0
Y
18
0500
9.5
Y
19
0630
8.0
Y
20
N
NOFLOW
21
IN
NOFLOW
22
0630
8.0
Y
NOFLOW
23
0630
Y
NOFLOW
24
0630
Y
NOFLOW
25
0600
LIN
B
NOFLOW
26
0600
B
NOFLOW
27
I NOFLOW
28
1630
1.25
B
NOFLOW
29
0630
8.0
B
30
1
10600
8.0
B
31
0930
24
0600
8.0
B
Monthly Average Limit:
0.332
Usti
0.048
0.336
0.068
1 3.583
0.261
Monthly Average:
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY =No Visitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2018 (October 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
�
F
e`
e
u
a
e
F
O
in
O
U
O
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annually
Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Grab
Grab
Grab
Grab
Grab
Grab
Gab
Grab
Grab
Grab
Grab
DUVET -PH
DNBPBTH
ETHYLBEN
FLUORENE
HEXCLBD
HCE
LEAD
METHYLCH
MECL2
N"THALE
NICKEL
2400clock
H.
2400clock
H.
Y/B/N
lbs/day
Ibs/day
Ibs/day
Ibs/day
lbs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
1
0600
8.0
Y
NOFLOW
2
-
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0630
8.0
Y
NOFLOW
6
0500
8.0
Y
NOFLOW
7
10930
4.0
B
I NOFLOW
8
0500
9.5
Y
9
0600
8.0
Y
10
10930
24
0530
8.0
Y
11
0600
8.0
Y
12
0630
8.0
Y
13
0600
4.5
ly
14
0600
4.0
Y
15
0500
10.0
Y
16
0500
10.0
Y
17
0930
24
0600
8.0
Y
18
0500
9.5
Y
19
0630
8.0
Y
20
N
NOFLOW
21
N
NOFLOW
22
0630
8.0
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
0630
Y
NOFLOW
25
0600
NOFLOW
26
0600
F8.0B
B
NOFLOW
27
N
NOFLOW
28
1630
1.25
B
NOFLOW
29
1
0630
18.0
In
30
0600
8.0
B
31
0930
124
10600
18.0
B
Monthly Average Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Montbly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES Put mrr NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 10-2018 (October 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
F
9
U'
5
5
9
d
A
O
t
4
S
65
U
O
'L
Z
34447
34461
34694
34469
34475
31010
39700
34376
34626
34220
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
PHENANTH
PHENOL
PYRENE ITETCLETY
TOLUENE
BCD
FLUORANT
26DINr'1'R
ANTHRACE
2400 clock
H.
2400 dock
H.
Y/BJNN
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
119/1
u8/1
119/1
u9/1
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0630
8.0
Y
NOFLOW
6
10500 18.0
Y
NOFLOW
7
0930
4.0
B
NOFLOW
8
0500
9.5
Y
9
0600
8.0
Y
10
0930
24
0530
8.0
Y
11
0600
8.0
Y
12
0630
8.0
Y
13
0600
4.5
Y
14
0600
4.0
Y
15
0500
10.0
Y
16
0500
10.0
Y
17
0930
24
0600
8.0
Y
18
0500
9.5
Y
19
0630
8.0
Y
20
N
NOFLOW
21
N
NOFLOW
22
0630
8.0
Y
NOFLOW
23
0630
8.0
Y
NOFLOW
24
0630
8.0
Y
NOFLOW
25
0600
8.0
JB
NOFLOW
26
10600
B
NOFLOW
27
N
NOFLOW
28
1630
r25
B
NOFLOW
29
0630
B
30
0600
B
31
0930
124
10600
8.0
B
Monthly Average limit:
0.087
0.071
0.049
0.081
0.071
0.094
Monthly Average:
Daily Maximum:
+
Daily Minimum:
I
I
I
I
I
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation —Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 10-2018 (October 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 11/13/2018
���i�-�� 11/13/2018
aRC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
/ "-Crpa 6, 11/13/2018
Permittee/Submitter Signa e:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PER. NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 10-2018 (October 2018)
Report Comments:
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
10/17/18, 10/31/18, Fecal Coliform; Below reporting limit.
10/10/18, BOD; Blank value is outside of control limits. GGA result is less than the control limit. Difference between sample dilution is greater than 30%. Sample read out on day
6 due to instrument issue. Contacted Ori Tuvia, North Carolina Division of Environmental Quality Mooresville Regional Office on 10/24/18 the day we got the results from Prism
Labs.

CERTIFIED MAIL: 70180040000049150595
Return Receipt to Renee Culler
RECC18:9
November 19, 2018
NCDEQ
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
0 Celanese
The chemistry inside innovation
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerning October 2018, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the October 2018 report has been submitted through the
eDMR system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
Also included are copies of a letter dated October 24, 2018, received from Prism Labs Inc. regarding the DO
reading for BOD sample 2018 Wastewater Permit Analysis, Prism Lab Inc. Case Narrative, Prism Lab Inc.
Sample Receipt Summary, Prism Lab Inc. Laboratory Report, Prism Lab Inc. Wastewater Chain of Custody,
and a letter written to Ori Tuvia notifying him of the letter from Prism Labs Inc. both dated October 24, 2018.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 682-218-6043 (cell), 704/480-5726 (office) or via email at renee.cullerO-celanese.com
Sin erely,
Rene uller
ESHA Manager
Attachments
Duplicate Copies of the signed DMR report
Letter dated October 24, 2018 from Prism Labs Inc.
Prism Lab Inc. Case Narrative
Prism Lab Inc Sample Receipt Summary
Prism Lab Inc. Laboratory Report,
Prism Lab Inc. Wastewater Chain of Custody
Letter dated October 24, 2018 to Ori Tuvia, NCDEQ, Mooresville Regional Office

s
CERTIFIED MAIL: 70170040000049150588
Return Receipt to Renee Culler
RECC18:10
October 24, 2018
NCDEQ
Mooresville Regional Office
Attn.: Ori Tuvia
1617 Mail Service Center
Raleigh, North Carolina 27699A617
j Celanese
The chemistry inside innovation"
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.ce(anese.com
Reference: Prism Labs Inc. DO Reading for BOD Sample 2018 Wastewater Permit Analysis
Permit No. NC 0004952
Dear Mr. Tuvia:
As follow up to the conversation earlier today with Michael Sparks, -Randall Turner, you, and me, this letter is
to formally notify you of the compliance issue at Prism Labs. Inc. concerning the BOD sample for the 2018
Wastewater Permit Analysis project that was collected on October 10, 2018, at 9:30 for Prism Labs. Inc. work
order number 8100194.
Celanese received a letter today notifying .us that the final DO reading was performed on the sixth day (not
within five days as required) due to the Blank value and GGA results being much higher than normal. We
spoke with Terri Cole at Prism Lab. Inc., after receiving the letter. Terri explained that Prism Labs. Inc. has
purchased a second DO probe for reserve to prevent reoccurrence of this issue.
A.copy of this letter along with the Prism Lab. Inc: letter will be included in the eDMR submittal next month.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information, feel free to call me at
682-218-6043 (cell), 704/480-5726 (office) or via email at renee.culler(CDcelanese.com
S'n erely,
U.S. Postal Service"
CERTIFIED MAILP RECEIPT
w onW
co
e Cull rLn
ESHA Manager •fpl2 eiu r
a
Y
0519
%
lun
Certified Mail Fee '$ 3 . r 5
Attachments e�
Prism Lab. Inc. letter dated 10/24/18 ,- ExMaservlces&Fees�(cheaxbOx es leesLIT
rtetum Receipt l p� fl f
Project 2018 Wastewater Permit Analysis O ClR�R�pt(electrOnic) $ t _ "ere 1"
M �Certiff d Mail Restricted Delivery $-
o $ -
�AdultSignatureRe Wct 0)
Adult Signature Restricted Delivery $
110
Pstage •. !�i
oo18�0
O To postage and Few s i
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d] g o r --- -
=-----------
"et and • or P�(' ------
,rQ. --

APRISM
LABORATORIES INC.
Full -Service Analytical &
Environmental Solutions
10/24/18
Celanese
Attn: Michael Sparks
2525 Blacksburg Road
Grover, NC 28073
Mr. Sparks,
Main Office:
449 Springbrook Road
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
1 /800/529-6364
Fax: [phone]
www.prismlabs.com
This letter is in reference to the BOD sample received for your 2018 Wastewater Permit Analysis project
that was collected on 10/10/18 at 09:30 for Prism Labs. Inc. work order number 8100194.
The final DO reading was performed on the sixth day. This was because the Blank value and GGA results
were much higher than normal. The analyst thought the DO probe had malfunctioned, so she performed
maintenance and let it stabilize overnight. On day 6, the results were still high. Results may have a high
bias.
We apologize for any inconvenience this may cause. We are reviewing our procedures to insure that
results are reported accurately and in a timely fashion. We now have a second probe in reserve to use
and we have cleaned our equipment to bring Blank and GGA results back into acceptable range.
Please call me at 704-529-6364 if you have further questions.
Sincerely,
PRISM LABORATORIES, INC.
Terri Cole
Project Manager

s L NC Certification No_ 402 Case Narrative
;D SM I Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions 10/24/2018
L SC Certification No. 99012
Celanese Project: 2018 Wastewater Permit Analysis
Michael Sparks
2525 Blacksburg Road Lab Submittal Date: 10/10/2018
Grover, NC 28073 Prism Work Order. 8100194
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
i
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
Reviewed By Terri W. Cole
Project Manager
A Confirmed positive.
Aa Samples read out on day 6 due to instrument issues.
BB Blank value is outside of the control limits. Validity of the data not affected.
DD Difference between sample dilutions is greater than 30%.
GH GGA result is greater than the control limit.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-8001529-6364-Fax:[phone] Page 1 of5

Full -Service Analytical &
Environmental Solutions
sample Receipt Summary
10/24/2018
Prism Work Order: 8100194
Client Sample ID
Lab Sample ID
Matrix
Daterrime Sampled
DatePTime Received
001 EFF Comp
8100194-01
Water
10/10/18 9:30
10/10/18 15:45
001 EFF Grab
8100194-02
Water
10/10/18 11:45
10/10/18 15:45
Samples were received in good condition at 2.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number. 1.8001529-6364 - Fax: [phone] Page 2 of 5

�
[ S M I
Full -Service Anal Kcal t
Environmental —
Laooratory Kepon
.w ING
Solutions
- 10/24/2018
Celanese
Project: 2018 Wastewater Permit
Client Sample ID: 001 EFF Comp
Attn: Michael Sparks
Analysis
Prism Sample ID: 8100194-01
2525 Blacksburg Road
Prism Work Order. 8100194
Grover, NC 28073
Sample Matrix: Water
Time Collected: 10/10/18 09:30
Time Submitted: 10/10/18 15:45
Parameter
Result Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Daternme ID
General Chemistry Parameters
Biochemical Oxygen Demand
11 Aa, BB, DD, mg/L 2.0
1 `SM5210 B 10/11/18 10:46 CBP PSJ0312
GH
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-8001629-6364 - Fax: 704/52&M9 Page 3 of 5

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
PERMIT VERSION: 4_0 \ PERMIT STATUS: Expired
CLASS: WW-2 RECEIVED COUNTY: Cleveland -3
�+�
ORC: Michael D. Sparks O O T 3 I 2018 ORC CERT NUMBER: 9P7F7gIVE©/NCDENR/DWR
GRADE: WW-3. ORC HAS CHANGED: No N 0 v �� 1
eDMR PERIOD: 09-2018 (September 2018) VERSION: 1.0 CEN kAL FILES STATUS: Processed
DWR SECTION
Vl/QR05
MOORESVILLE REGIONAL OFFICE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
d
G
Fit
e
e`
U'
w
e
11
"a
4
-
O
O
F
-
O
t
y_
o
u
O
44
2
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
BOD-Qty Daily
TSS-Qty Daily
FCOLI BR
TOTAL N-
TOTAL P-Coo.
Ij-DCE
1,1-DCEY
2400 dock
Hrs
2400 dock
H.
Y/WN
mgd
an
Ibs/day
lbs/day
#/100ml
mg/I
mgll
Ibs/day
Ibs/day
2
0830
2.0
B
NOFLOW
2
1545
4.25
Y
NOFLOW
3
0545
4.50
Y
0.233
4
0930
24
0600
8.0
Y
0.296
7.9
<4.9
22.7
<2
5
0630
18.0
Y
1
0.228
6
0600
8.0
Y
0.233
7
0630
8.0
Y
0.19
8
0600
4.0
Y
NOFLOW
9
0545
4.0
Y
NOFLOW
10
10630
18.0
Y
NOFLOW
11
1
0630
8.0
Y
0.269
12
0930
24
0530
9.5
Y
0.288
8
7.9
16.3
<2
13
0600
8.0
Y
0.236
14
0630
8.0
Y
0.172
Is
0925
1.0
B
0.118
16
1
10730
12.75
Y
0.152
17
0500
8.0
Y
0.361
18
0500
8.0
B
0.354
19
0930
24
0545
8.0
B
0.341
7.7
7.1
20.5
<2
20
0600
8.25
B
0.282
21
1
0600
9.5
B
0.217
22
0915
1.0
B
0.159
23
N
NOFLOW
24
0600
18.0
B
INOFLOW
25
0600
8.0
B
NOFLOW
26
0600
9.5
B
NOFLOW
27
0600
9.5
Y
NOFLOW
28
0600
9.5
Y
NOFLOW
29
0630
111.5
1 Y
NOFLOW
30
0630
6.0
1 Y
I NOFLOW
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.242882
5
19.833333
I
Daily Marimum:
0.361
8
7.9
22.7
0
Daily Minimum:
0.118
7.7
0
16.3
1 o
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation -Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2018 (September 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
A
€e.
E
U
e
F
.e
S
F'
Q
1.
O
G
F
1
O
N
o�°
O
3
29
345M
32103
34541
34546
71163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
IZ-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
I 14-DCB
2p-DCPH
2A-DMPH
2kDNPH
gal-DNT
2400 clock
Hn
2400 clock
H.
Y11/N
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
1
0830
2.0
B
NOFLOW
2
1545
4.25
Y
NOFLOW
3
0545
4.50
Y
4
0930
24
0600
8.0
Y
5
0630
8.0
Y
6
10600
18.0
Y
7
0630
8.0
Y
8
0600
4.0
Y
NOFLOW
9
0545
4.0
Y
NOFLOW
10
1
0630
8.0
Y
INOFLOW
11
0630
8.0
Y
12
0930
24
0530
9.5
Y
13
0600
8.0
Y
14
0630
8.0
Y
is
1
0925
1.0
B
16
0730
2.75
Y
17
0500
8.0
Y
1s
0500
8.0
B
19
0930
24
0545
8.0
B
20
1
0600
8.25
B
21
0600
19.5
B
22
0915
1.0
B
23
N
NOFLOW
24
0600
8.0
B
NOFLOW
25
0600
8.0
B
NOFLOW
26
1
0600 19.5
B
I NOFLOW
27
0600
9.5
Y
NOFLOW
28
0600
9.5
Y
NOFLOW
29
0630
11.5
Y
NOFLOW
30
0630
6.0
Y
NOFLOW
Monthly Average Limit:
0.249
0.219
0.494
O.M
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly Averages
Daly Mmrimum:
Daily Minimum:
"" No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 09-2018 (September 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
E
u
B
C
4
Y
Q
-°„0
'm
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Amually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-o-C
4NPBENOL
ACENAPEN
ACENAPYL
ACRYLONI
IBENZENE
BNZO-A-A
BNZO-A-P
2400 dock
Inn
2400 dork
I El.
Y/MQ
I
lbs/day
lbs/day
ug/1
I lbs/day
lbs/day
lbs/day
Ibs/day
ug/l
lbs/day
ug/1
119/1
1
0830
2.0
B
NOFLOW
2
1545
4.25
Y
NOFLOW
3
0545
4.50
Y
4
0930
24
0600
8.0
Y
5
0630
18.0
Y
6
0600
8.0
Y
7
0630
8.0
Y
8
0600
4.0
Y
NOFLOW
9
0545
4.0
Y
NOFLOW
10
1
0630
18.0
Y
NOFLOW
11
0630
8.0
Y
12
0930
24
0530
9.5
Y
13
0600
8.0
Y
14
0630
8.0
Y
15
1
0925
1.0
B
16
0730
2.75
Y
17
0500
8.0
Y
l8
0500
8.0
B
19
0930
24
0545
8.0
B
20
0600
8.25
B
21
10600
9.5
B
22
0915
11.0
B
23
N
NOFLOW
24
0600
8.0
B
NOFLOW
25
0600
8.0
B
NOFLOW
26
0600
9.5
B
NOFLOW
27
0600
19.5
Y
INOFLOW
28
0600
9.5
Y
NOFLOW
29
0630
11.5
Y
NOFLOW
30
0630
6.0
Y
NOFLOW
Monthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Dolly Madonna:
Daily Minimum:
a*axNoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation-AdvelseWeather; NOFLOW=No Flow; HOLIDAY =No Visitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 09-2018 (September 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
#*""NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2018 (September 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Monibly Avenge Limit:
"'#NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 09-2018 (September 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
A
e
H
U'
F
[+°
F
O
"
O
O
X
34447
00556
TGP3B
34461
34694
34469
34475
34010
34220
39700
34626
AnnuallyQuarterly
Q Y
uarterl
Q y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Grab
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1NrrROBEN
OIL-GRSE
CER17DPF
PHENANTH
PHENOL
IrYRENE
TETCLETY
TOLUENE
ANTHRACE
I HCB
26DINITR
2400 crock
Hn
2400 clock
Hn
Y/B/N
Ibs/day
mg/l
pass/fail
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
U911
u9/1
ug/l
1
0830
2.0
B
NOFLOW
2
1545
4.25
Y
NOFLOW
3
0545
4.50
Y
4
0930
24
0600
8.0
Y
<5
PASS
5
10630
18.0
Y
6
0600
8.0
Y
7
0630
8.0
Y
8
0600
4.0
Y
NOFLOW
9
0545
4.0
Y
NOFLOW
10
0630
8.0
Y
NOFLOW
11
0630
8.0
Y
12
10930
24
10530
9.5
Y
13
0600
8.0
Y
14
0630
8.0
Y
15
0925
1.0
B
16
0730
2.75
Y
17
0500
8.0
Y
18
0500
8.0
B
19
0930
24
0545
8.0
B
20
0600
8.25
B
21
0600
9.5
B
22
0915
1.0
B
N
NOFLOW
21
0600
8.0
B
NOFLOW
25
0600
8.0
B
NOFLOW
26
0600
9.5
B
NOFLOW
27
0600
9.5
Y
NOFLOW
28
0600
9.5
Y
NOFLOW
29 10630
111.5
Y
NOFLOW
30
0630
6.0 ly
i NOFLOW
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.094
Monthly Average,
0
Daily Maximum•
0
Daily Minimum:
0
* * * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2018 (September 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
A
e
9
U
K
g
e<
F
'E
O
s
8
F
O
O
c
Z
34376
Annually
Grab
FLDORANT
2400 clock
HM
2400 clock
H.
Y/BNN
U911
1
0830
2.0
B
NOFLOW
2
1545
4.25
Y
NOFLOW
3
0545
4.50
Y
4
10930
24
10600
8.0
Y
5
0630
8.0
Y
6
0600
8.0
Y
7
0630
8.0
Y
8
0600
4.0
ly
I NOFLOW
9
0545
4.0
Y
NOFLOW
10
0630
8.0
Y
NOFLOW
11
0630
8.0
Y
12
0930
24
0530
9.5 -
Y
13
0600
8.0
Y
14
0630
8.0
Y
15
0925
1.0
B
16
0730
2.75
Y
17
0500
8.0
Y
18
0500
8.0
B
19
0930
24
0545
8.0
B
20
0600
8.25
B
21
0600
9.5
B
22
0915
1.0
B
23
N
NOFLOW
24
0600
8.0
B
NOFLOW
25
10600
8.0
B
NOFLOW
26
0600
9.5
B
NOFLOW
27
0600
9.5
Y
NOFLOW
28
0600
9.5
Y
NOFLOW
29
0630
11.5
Y
I NOFLOW
30
1
10630
6.0
Y
NOFLOW
Monthly Average Limit:
Monthly Averagc
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY =No Visitation -Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 09-2018 (September 2018)
Report Comments:
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
9/4/18, 9/12/18, 9/19/18 Fecal Coliform; Below reporting limit.
9/4/18, Oil & Grease; Below reporting limit.
9/4/18, BOD; Below reporting limit. GGA result is less than the control limit.
9/12/18 BOD; Blank value is outside of control limits.
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

�J
4 NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Expired
FACILITY NAME: Celanese -Shelby Facility CLASS: W W-2 Y \' `% ® COUNTY: Cleveland
OWNER NAME: C N A Holdings LLC ORC: Michael D. Sparks ORC CERT NUMBER: 987732
SAP .21 2018 GRADE: WW-3. ORC HAS CHANGED: No RECEIVEQiNMENR/ it'
eDMR PERIOD: 08-2018 (August 2018) VERSION: 1.0 -CENTRAL FILES STATUS: Processed
DWR SECTION L�1,1 201�
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHAI�C*•aRos
lvl e-SVILLE REGIONAL OFFfCI
q
e
y
9
o
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_
e
e
u
y
<
C
O
N
3
O
'
O
O
z
1.-
Z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Anuuall
Recorder
Gmb
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pII
BOD-Qty DAY
TSS-Qty Daily
FCOLI HR
TOTAL N-
TOTAL P-Cone
1,1-DCE
1,1-DCEY
Clack
H.
2400 Clock
H-
WBIN
m d
su
Ibs/da
lbs/day
#/100ml
mg/l
m9/1
lbs/day
Ibs/da
2
0930
24
0600
8.0
Y
0.305
7.5
<5.1
13.7
<2
0.7
<0.05
r42400
2
0600
8.0
Y
0.27
3
0600
8.0
Y
0.29
0445
1.75
Y
0.265
5
N INOFLOW
6
0630
8.0
Y
NOFLOW
7
0630
8.0
Y
NOFLOW
e
0630
8.0
Y
NOFLOW
9
0600
8.0
Y
NOFLOW
10
0630
8.0
Y
INOFLOW
11
0445
4.25
Y
NOFLOW
12
0630
5.0
Y
NOFLOW
13
0500
9.5
Y
0.312
14
0545
12.25
Y
0.266
15
10930
24
0600
8.0
Y
1
0.274
8.5
5
11.9
6
16
0600
8.5
Y
0.33
'
17
0600
8.0
Y
0.318
18
0915
12.50
B
0.311
19
0900
3.25
B
NOFLOW
20
1
0630
8.0
Ill
I NOFLOW
21
0630
8.0
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0600
8.0
B
NOFLOW
24
0630
8.0
B
NOFLOW
25
1
N
NOFLOW
26
1600
2.0
1 B
INOFLOW
27
0630
8.0
Y
0.237
28
0630
8.0
Y
0.401
29
0930
124
10600
8.0
Y
0.375
8
8.1
130.6
2
30
1
0600
8.0
Y
0.404
31
0630
18.0
Y
0.387
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.316333
1
14.366667
18.733333
2.289428
10.7
0
Daily Msaimmm:
0.404
8.5
8.1
30.6
6
0.7
0
Daily Minimum:
0.237
7.5
0
11.9
0
0.7
0
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather, NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday
c+

o NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2018 (August 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Monthly A—ge:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation — AdverseWeather; NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

i NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2018 (August 2018)
PERMIT VERSION: 4_0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
•'"""NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2018 (August 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
fflowwwwwwwwo
Monthly Average:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 08-2018 (August 2018)
PERMIT VERSION• 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2018 (August 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY =No Visitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 08-2018 (August 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 09/14/2018
' "'L/✓�"'� !� 09/12/2018
OR Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
09/14/2018
Permittee/Submitter SignArV" Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221, 402
PERSON(s),COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/fonns.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: WW-2
OWNER NAME: C N A Holdings LLC
ORC: Michael D. Sparks
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 08-2018 (August 2018)
VERSION: 1.0
Report Comments:
8/1/18, Fecal Coliform; Below reporting limit.
8/1/18, BOD; Below reporting limit. Blank value is outside of control limits.
8/1/18, Total Phosphorus; Below Reporting Limit
PERMIT STATUS: Expired
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPDES PERMIT NO. N C 0 0 0 4 9 5 2
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2018 (July 2018)
PERMIT VERSION: 4.0 6= - , 2 PERMIT STATUS: Active 3
PD
CLASS: WW-2 ° r COUNTY: Cleveland
ORC: Michael D. Sparks AUG 2 9 2018 ORC CERT NUMBER: 987732
RECEIVED/NCDENR/DWR
ORC HAS CHANGED: No Ct=ri�`I t L FILE'`J
- 9-{d�+
VERSION: 1.0 D\NR SECTION STATUS: Processed SEP . 4 2018
ROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHAWRIEGIONAL OFFICE
a
q
=
E
U
E
E
a
F
E
P
'�
a
O
E
O
5
z
O
t
z
2
50050
00401)
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annual)
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Cum osite
Grab
Grab
FLOW
PH
BOD -Qty Daily
T55-Qty Daily
FCOLIBR
TOTAL N-
TOTAL P -Cone
1,1-DCE
1,1-DCEY
2400 clack
H.
2400 cluck
Hn
Y/B/N I
m d Isu
Ibs/da
Ibs/day
9/100.1
mg/I
mg/l
Ibs/da
Ibs/day
1
1230
2.0
Y
NOFLOW
2
0500
9.0
Y
0.28
3
0630
8.0
Y
0.362
4
0930
1.0
B
0.411
5
0930
24
0600
8.0
Y
0.373
9.4
12.8
17.4
<2
6
0630
8.0
Y
0.334
0915 12.0
113
0.285
8
1040
2.0
B
NOFLOW
9
0630
9.0
Y
NOFLOW
10
0630
8.0
Y
NOFLOW
11
0630
8.0
Y
NOFLOW
12
-
0600
8.0
Y
NOFLOW
13
0630
18.0
Y
I NOFLOW
14
0500
4.0
Y
NOFLOW
15
1030
3.0
Y
NOFLOW
16
0500
8.0
Y
0.336
17
0630
8.0
Y
0.359
Is
0930
24
10600
8.0
1 Y
1
0.394
8.5
46
28.9
22
19
0600
9.0
Y
0.373
20
0500
8.0
Y
0.356
21
0930
1.0
B
0.338
22
0730
2.0
Y
0.309
23
0500
8.0
Y
0.261
24
0545
8.0
Y
0.379
25
0930
124
0500
18.0
Y
1
0.36
8.2
9.3
22.2
<2
26
0515
8.0
Y
0.382
27
0630
8.0
B
0.326
28
0930
2.75
B
0.316
29
0900
3.5
B
0.329
30
0630
8.0
Y
0.346
31
0600
8.0
Y
0.339
M-11dy A-igc Limlu
0.45
68
124
200
0.071
0.052
Mnnndy A-g�:
0.343091
22.7
22.833333
2.802039
Daily MnxiW-
0.411
8.5
46
28.9
22
Daily Minimwn:
0.261
8.2
9.3
117.4
10
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

pp-
P
NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2018 (July 2018)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
E
E
t-
E
u
a
E
F
-
<
O
Y
n
O
E
-
C
O
0
U
O
e
j
5
t
C
Z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
I,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPH
2,4-DMPH
2,4-DNPH
2,4-DINT
2400 clock
H.
2400 clock
Hn I
Y/B/N I
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
lbs/da
Ibs/da
Ibs/day
1
1230
2.0
Y
NOFLOW
0500
8.0
Y
3
0630
8.0
Y
4
r62
0930
1.0
B
5
0930
24
0600
8.0
Y
0630
8.0
Y
7
0915
2.0
B
8
1040
2.0
B
NOFLOW
0630
8.0
Y
NOFLOW
10
1
0630
8.0
Y
NOFLOW
11
0630
8.0
Y
NOFLOW
12
0600
8.0
Y
NOFLOW
13
0630
8.0
Y
NOFLOW
14
0500
4.0
Y
NOFLOW
15
1030
3.0
1 Y
NOFLOW
16
0500
8.0
Y
17
0630
8.0
Y
r8
0930
24
0600
8.0
Y
19
0600
8.0
Y
20
0500
8.0
Y
21
0930
1.0
B
22
0730
2.0
Y
23
0500
18.0
Y
24
0545
8.0
25
0930
24
0500
8.0
26
0515
8.0
FB
27
0630
8.0
28
0930
2.75
29
0900
3.5
B
30
0630
8.0
Y
31
0600
8.0
Y
Monthly Aremge Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly A -rap:
Daily Maximum:
Way Minimum:
****NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

PNPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2018 (July 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
E
w';
E
U
E
E
u
i-
E
P
a
C
O
w
E
-:'�
O
_
o`
a
O
°
m
_
c
C
2
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-n-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
24000-1,
1It,.,
2400 cinch
H.
Y/B/N
Ibs/da
Ibs/da
ug/I
Ibs/da
Ibs/da
Ibs/da
lbs/day
ugA
I Ibs/day
ug/I I
ug/I
1
1230
2.0
Y
NOFLOW
2
0500
8.0
Y
3
0630
8.0
Y
4
10930
11.0
B
5
0930
24
0600
8.0
Y
6
0630
8.0
Y
7
0915
2.0
B
8
1040
2.0
B
NOFLOW
9
0630
18.0
Y
I NOFLOW
10
0630
8.0
Y
NOFLOW
11
0630
8.0
Y
NOFLOW
12
0600
8.0
Y
NOFLOW
13
0630
8.0
Y
NOFLOW
14
0500
4.0
IY
NOFLOW
35
1030
3.0
Y
NOFLOW
16
0500
9.0
Y
17
0630
8.0
Y
18
0930
124
0600
8.0
Y
19
0600
18.0
Y
20
0500
8.0
Y
21
0930
1.0
B
22
0730
2.0
Y
23
0500
8.0
IY
24
0545
8.0
Y
25
0930
24
0500
8.0
Y
26
0515
8.0
Y
27
0630
8.0
B
28
0930
2.75
B
29
0900
3.5
B
30
0630
8.0
Y
31
0600
8.0
Y
Monthly Average Limit:
0.1
0.132
11.25E
0.232
0.071
0.071
0.119
Monthly Avmvgc:
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2018 (July 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
o
=
~
A
E
U
-
P
-
E
3
F%
E
F
a
O
O
E
i-
O
_
UW O
$
m
L
a
Z.
34242
39100
32102
34301
85811
32106
01034
34320
0104E
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
B2E PHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 0,.&
H.
2400 cluck
Hr.
Y/B/N
ug/I
Ibs/day
Ibs/da
Ibs/day
Ibs/da
lbs/day
UgA
ug/I
u
ug/I
Ibs/da
t
1230
2.0
Y
NOFLOW
2
0500
8.0
Y
3
0630
8.0
Y
4
0930
1.0
B
5
0930
24
0600
8.0
Y
6
0630
8.0
Y
7
0915
2.0
B
8
1040
2.0
B
NOFLOW
9
0630
8.0
Y
NOFLOW
t0
0630
8.0
Y
NOFLOW
11
10630
8.0 ly
NOFLOW
12
0600
8.0
Y
NOFLOW
13
0630
8.0
Y
NOFLOW
14
0500
4.0
Y
NOFLOW
15
1030
3.0
Y
NOFLOW
16
0500
8.0
Y
17
0630
8.0
Y
l8
0930
24
0600
8.0
Y
19
0600
8.0
Y
20
0500
9.0
Y
21
0930
I.0
B
22
0730
2.0
Y
23
0500
8.0
Y
24
0545
8.0
Y
25
0930
24
0500
8.0
Y
26
0515
8.0
ly
27
0630
8.0
B
28
0930
2.75
B
29
0900
3.5
B
30
0630
8.0
Y
31
1
1
0600
8.0
ly
Monthly A,-g. Limit.
0.332
0.058
0.048
0.336
0.068
3.583
0.261
Monthly A -rag.:
Daily Mncimum:
Daily Nat-:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2018 (July 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
:,
o
E
F
-
E
U
E
E
a
1=
E
l
a
O
n
O
P
1 O
y
C
O
L
Y
T. 1
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNBPHTH
ETIIYLBEN
FLUORENE
HEXCLBD
}ICE
LEAD
METRYLCH
MECL2
NAFTHALE
NICKEL
241111 clock
Hrr
M. clock
Hn
YBIN
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/day
Ibs/day
Ibs/da
Ibs/day
Ibs/day
1
1230
2.0
Y
NOFLOW
2
0500
8.0
Y
3
0630
8.0
Y
4
1
0930
1.0
B
5
0930
24
0600
8.0
Y
6
0630
8.0
Y
7
0915
12.0
B
8
1040
2.0
B
NOFLOW
9
0630
8.0 ly
I NOFLOW
10
0630
8.0
Y
NOFLOW
I
0630
8.0
Y
NOFLOW
12
0600
8.0
Y
NOFLOW
13
0630
8.0
Y
NOFLOW
14
0500
4.0
Y
NOFLOW
15
1030
3.0
Y
NOFLOW
16
0500
8.0
Y
17
0630
18.0
Y
18
0930
24
0600
8.0
Y
19
0600
9.0
Y
20
0500
8.0
Y
21
1
0930
1.0
B
22
0730
2.0
Y
23
0500
8.0
Y
24
0545
8.0
Y
25
0930
24
0500
8.0
Y
26
0515
8.0
Y
27
0630
8.0
B
28
2.75
B
29
3.5
B
30
L63
8.0
Y
31
8.0
Y
Monthly A-mge Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Average:
Daily Maxlnmm:
D.Hy Minimum:
****NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPD-ES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2018 (July 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
a
c
F
_
E
E
U
E
F
E
a
F
L
'E
Q
O
n
O
E
F
o
-
U
O
c
5
C
L
a
z',
34447
34461
34694
34469
34475
34010
34376
34626
34220
39700
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
FLUORANT
26DINITR
ANTHRACE
HCD
2400 ciodc
Ilre
2400 c1oci<
11.
YIBIN
Ibs/da
Ibs/da
Ibs/da
lbs/day I
Ibs/da
Ibs/day
ugA
ugA
ugA lum
1
1230
2.0
Y
NOFLOW
2 1
0500
8.0
Y
3
0630
8.0
Y
4
0930
1.0
B
5
0930
24
0600
8.0
Y
6
0630
8.0
Y
7 1
0915
2.0 IB
8
1040
2.0
B
NOFLOW
9
0630
8.0
Y
NOFLOW
10
0630
8.0
Y
NOFLOW
11
0630
8.0
Y
NOFLOW
12
0600
8.0
Y
I NOFLOW
13
0630
8.0
Y
NOFLOW
14
0500
4.0
Y
NOFLOW
15
1030
3.0
Y
NOFLOW
16
0500
8.0
Y
17
0630
8.0
Y
18
0930
24
0600
9.0
Y
19
0600
8.0
Y
20
0500
18.0
Y
21
0930
1.0
B
22
0730
2.0
Y
23
0500
8.0
Y
24
0545
8.0
Y
25
0930
24
0500
9.0
Y
26
0515
8.0
Y
27
0630
8.0
B
29
0930
2.75
1B
29
0900
3.5
B
30
OG30
8.0
Y
31
0600
8.0
Y
Monthly A-mgc Limit:
0.087
0.071
0.048
0.081
0.071
0.084
Monthly Av rap;
Daily M-hri m:
Daily Minimum:
**** No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDNIR PERIOD: 07-2018 (July 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 08/20/2018
08/15/2018
OR /Certifier Signature: Michael D Sparks E-Mail:michae1.sparks a celanese.com Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
08/20/2018
Permittee/Submitter SiVn`�ture:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Penmittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221, 402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2018 (July 2018)
Report Comments:
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
7/5/18, 7/25/18, Fecal Colifonn; below reporting limit.
7/18/18, BOD;Difference between sample dilutions is greater than 30%. Blank value is outside of control limits.
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

1
NFDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
PERMIT STATUS: Active
RECL' �"' E @NTY: Cleveland
JUL 31 ?Qj6ORCCERTNUM�`�//NCDENR/DWR
C1.;-N I'IX,AL RL��''1AUG 6 n Ili
DV'JR SECT Iorj ATUS: Processed
WQROS
QBBp�ssAL
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISQ HA����ECIO OFFICE
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
u
O
E
F
�
2
E
V
E
c
e
F'
E
6
u
O
or
`
O
O
O
-
Y
Z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annual)
Semi-annually
Annually
Annual)
Recorder
Grab
Composite
composite
Grab
Composite
Composite
Grab
Grab
FLOW
PH
BOD -Qly May
TSS -Qly Daily
FCOLI BR
TOTAL N-
TOTAL P -Conc
1,1-DCE
1,1•DCEY
2400 clock
H.
2400 clock
Hn
Y/BIN I
mgd I
su
Ibs/da
lbs/da
4/100mI I
mg/I
mg/I
Ibs/day
lbs/day
1
0600
8.0
B
0.414
2 1
1400
2.0
B
NOFLOW
3
1700
2.0
B
NOFLOW
4
0630
8.0
Y
0.308
5
0930
24
0500
8.0
Y
0.366
8.5
6.4
16.2
< 2
< 0.015
< 0.015
6
0630
8.0
Y
0.428
7
0600
8.0
Y
0.363
8
0630
8.0
Y
0.365
9
0900
1.0
B
0.38
10
0730
2.5
Y
0.324
it
10500
8.0
Y
0.297
12
0630
8.0
Y
0.321
13
0930
24
0630
8.0
Y
1
0.398
8.4
10
10.3
2
14
0600
8.0
Y
0.377
15
0630
8.0
Y
0.335
16
0500
3.0
Y
NOFLOW
17
1400
3.0
Y
NOFLOW
Is
0500
9.5
Y
0.262
19
0600
18.0
Y
1
0.354
20
0930
24
0600
8.0
Y
0.328
9.4
14.8
26.5
1<2
21
0600
9.0
Y
0.253
22
10630
9.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
0600
9.0
Y
NOFLOW
-
26
0600
8.0
Y
NOFLOW
27
0630
9.0
Y
NOFLOW
28
0930
24
0600
9.0
Y
0.415
8.2
17
42.9
10
29
10600
8.0
Y
0.394
31
0530
12.5
ly
1
0.336
Montldy A,e gc Limit:
0.45
68
124
200
0.071
0.052
Monthly A ­ go:
0.3509
12.05
23.975
2.114743
0
0
Daffy Maainmm:
0.428
8.5
17
42.9
10
0
0
Daily Minimum:
0.253
19,2
164
10.3
0
0
0
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
F
-
a
E
E
E•
'
6
lr
�
O
pp
v
E
d
O
o`
z
O
gg
0
5
a
Z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
1-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPH
2,4-DMPH
2,4.DNPH
2,4-DNT
24000.0,
Hrs
2400c1ack
H.
Y/B/N
Ibs/day
Ibs/da
Ibs/da
Ibs/day
Ibs/day
Ibs/da
Ibs/day
Ibs/da
Ibs/day
Ibs/da
Ibs/da
1
0600
8.0
B
2
1400
2.0
B
NOFLOW
3
1
1700
2.0
B
NOFLOW
4
0630
8.0 IY
5
0930
24
0500
8.0
Y
<0.03
<0.015
<0.015
<0.015
<0.015
<0.03
<0.03
<0.03
<0.03
<0.03
<0.03
6
0630
8.0
Y
7
0600
8.0
Y
8
0630
8.0
Y
9
0900
1.0 1
B
10
0730
2.5
Y
11
0500
8.0
Y
12
0630
9.0
Y
13
0930
24
0630
8.0
Y
14
0600
8.0
Y
Is
0630
1 &0
Y
16
0500
3.0
Y
NOFLOW
17
1400
3.0
Y
NOFLOW
is
0500
9.5
Y
19
0600
8.0
Y
20
0930
124
0600
18.0
Y
21
0600
9.0
Y
22
0630
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
0600
9.0
Y
NOFLOW
26
0600
8.0
Y
NOFLOW
27
0630
8.0
Y
NOFLOW
28
0930
24
0600
9.0
Y
29
0600
8.0
Y
30
0530
12.5
Y
Monthly A, ­ go Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly Av go:
0
0
0
0
0
0
0
0
0
0
0
Daily Maximum:
0
0
0
0
0
0
0
0
0
0
0
Daily Minimum:
0
0
0
0
0
0
0
1 11
0
0
0
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2
O
E
-
A
E
U'
E
F
-
E
u
a
F.
E
F
6
,
O
n
O
E
-
O
0
C
O 1
F*
C
z
34586
33591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
AnnuallyAnnually
AnnuallyAnnually
AnnuallyAnnually
AnnuallyAnnually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DNo-C
JNPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clock
H.
2400 clock
H.
Y/B/N
Ibs/day
ibs/day
ug/1
Ibs/day
Ibs/day
Ibs/da
Ibs/day
no
Ibs/day
ugll
ugA
1
0600
8.0
B
2
1400
2.0
B
NOFLOW
3
1700
2.0
B
NOFLOW
4
0630 18.0
Y
5
0930 124
0500
8.0
Y
<0.03
<0.03
<10
<0.03
<0.156
<0.03
<0.03
<10
<0.015
<10
<10
6
0630
8.0
Y
7
0600
8.0
Y
8
0630
8.0
ly
9
0900
1.0
B
10
0730
2.5
Y
it
0500
8.0
Y
12
0630
8.0
Y
t3
0930
24
0630
8.0
Y
14
0600
8.0
Y
15
0630
8.0
Y
16
0500
3.0
Y
NOFLOW
17
1400
3.0
Y
NOFLOW
18
0500
9.5
ly
19
0600
9.0
Y
20
0930
24
0600
8.0
Y
21
0600
9.0
Y
22
0630
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
0600
9.0
Y
NOFLOW
26
0600
8.0
Y
NOFLOW
27
0630
8.0
Y
NOFLOW
28
0930
24
0600
9.0
Y
29
0600
8.0
ly
30
0530
2.5
Y
Monthly A-mgc LInJt:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly M-gc:
0
0
0
0
0
0
0
0
0
0
0
Bony M-h-o:
0
0
0
0
0
0
0
0
0
0
0
Daily Minimum:
0
10
10
0
0
0
0
0
0
0
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NI'DES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
v
q
E
E
U
E
u
8
t=
6
Q
O
F
O
o
C
O
5
L
C'
Z
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
112E PHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 clock
H.
2400 clack
H.
WRIN
ug/1
Ibs/da
Ibs/day I
Ibs/day
Ibs/da
Ibs/da
ug/1
ug/I
ug/1
u
Ibs/day
1
0600
8.0
B
2
1400
2.0
B
NOFLOW
3
1700
2.0
B
NOFLOW
4
0630
&0
Y
5
0930
24
10500
8.0
Y
<10
<0.03 1
<0.015
<0.015
<0.03
<0.015
1<5
<10
<10
<5
10.015
6
0630
8.0
Y
7
0600
8.0
Y
8
0630
8.0
Y
9
0900
1.0
B
10
0730
2.5
Y
11
0500
8.0
Y
12
0630
8.0
Y
13
0930
24
10630
8.0
Y
14
0600
&0
ly
15
0630
8.0
Y
16
0500
3.0
Y
NOFLOW
17
1400
3.0
Y
NOFLOW
i9
0500
9.5
Y
19
0600
8.0
Y
20
0930
24
0600
8.0
ly
21
0600
9.0
Y
22
0630
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
0600
9.0
IY
NOFLOW
26
0600
8.0
Y
NOFLOW
27
0630
8.0
Y
NOFLOW
28
0930
24
10600
9.0
Y
29
0600
8.0
Y
30
0530
2.5
Y
Monthly A-mgc Limit:
0.332
0.058
0.048
0.336
0.068
3.583
0.261
Monthly A-g.:
0
0
0
0
0
0
0
0
0
0
0
Dauy M.A.-:
0
0
0
0
0
0
0
0
0
0
0
Daily Minimum:
0
10
10
10
10
10
10
10
10
0
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
m
q
fi
E+
a
7
'�
O
O
O
o
z
O
o±
x
a
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
'Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNB PHTH
ETHYLBEN
FLUORENE
HEXCLBD
HCE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 cluck
Hr:
2400 cloeic 1Hrs
WHIN
Ibs/day I
Ibs/da
Ibs/da
Ibs/day
Ibs/day
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/day
Ibs/da
1
0600
8.0
B
2
1400
2.0
B
NOFLOW
3
1700
2.0
B
NOFLOW
4
0630
8.0
Y
5
0930
24
0500
8.0
Y
<0.03
<0.03
<0.015
<0.03
<0.01
<0.03
<0.015
<0.03
<0.015
<0.03
0.039
6
0630
8.0
IY
I'
7
0600
8.0
Y
8
0630
8.0
Y
9
0900
1.0
B
10
0730
2.5
Y
11
0500
8.0
Y
12
0630
8.0
Y
13
0930
24
10630
8.0
ly
14
0600
8.0
Y
15
0630
8.0
Y
16
0500
3.0
Y
NOFLOW
17
1400
3.0
Y
NOFLOW
is
0500
9.5
Y
19
0600
8.0
Y
20
0930
124
0600
18.0
Y
21
0600
9.0
Y
22
0630
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
0600
9.0
IY
NOFLOW
26
0600
Y
NOFLOW
27
0630
Y
NOFLOW
28
0930
24
0600
r2.5.
Y
29
0600
Y
30
0530
Y
Monthly Average Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly A-ge:
0
0
0
0
0
0
0
0
0
0.039
Daily Maaimam:
0
0
Eo
0
0
0
0
0
0
0
0.039
Daily Minimum:
0
0
0
0
0
0
0
0
0
0.039
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
v
G
E
_
6
V
E
a
F
O
O
C
O
L
a
Z
34447
00556
TGP3B
34461
34694
34469
34475
34010
34220
39700
34626
Annually
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
OIL-GRSE
CER17DPF
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
ANTHRACE
HCB
26DINITR
2400 d.&
Fin
12400.1-1,
Hrr,
Y/B/N
Ibs/day
mg/1
ass/fail
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/day
ug/I
ugA
ugA
1
0600
8.0
B
2
1400
2.0
B
NOFLOW
3
1700
2.0
B
NOFLOW
4
0630
8.0 ly
5
0930
24
0500
Y
<0.03
<5
PASS
<0.03
<0.03
<0.03
<0.015
<0.015
<10
<10
<10
6
0630
Y
7
0600
r
Y
9
0630
Y
9
0900
.B
10
0730
2.5
Y
I1
0500
8.0
Y
12
0630
8.0
Y
13
0930
24
0630
8.0
Y
14
0600
8.0
ly
15
0630
8.0
Y
16
0500
3.0
Y
NOFLOW
17
1400
3.0
Y
NOFLOW
to
0500
9.5
Y
19
0600
8.0
Y
20
0930
24
0600
8.0
Y
21
0600
9.0
Y
22
0630
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
I NOFLOW
25
0600
9.0
Y
NOFLOW
26
0600
8.0
Y
NOFLOW
27
0630
8.0
Y
NOFLOW
28
0930
24
0600
9.0
Y
29
0600
8.0
Y
30
0530
2.5
Y
Monthly Av mgc Limit:
0.087
0.071
0.048
0.081
0.071
0.084
Manlhly Average:
0
0
0
0
0
0
0
0
0
0
Daily Maximum`
0
0
0
0
0
0
0
0
0
0
Daily Minimum:
0
10
1
10
10
10
10
10
10
0
0
"**No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
E
_
6
U
E
F
E
ci
x
F
E
F
_
4
v
O
-
w
O
F
2
O
U
O
9
C'
Z
34376
Annually
Grab
FLUORANT
2400 clock
H.
2400 cinck
Hr, I
Y/B/N
Bg/I
1
0600
8.0
B
2
1400
2.0
B
NOFLOW
3
1700
2.0
B
NOFLOW
4
0630
8.0
Y
5
0930 124
10500
8.0
ly
< 10
6
0630
8.0
Y
7
0600
8.0
Y
8
0630
8.0
Y
9
0900
1.0
B
10
0730
2.5
Y
11
0500
9.0
Y
12
0630
8.0
Y
13
0930
24
0630
8.0
Y
14
0600
8.0
Y
15
0630
8.0
Y
'
16
0500
3.0
Y
NOFLOW
17
1400
3.0
Y
NOFLOW
18
0500
9.5
Y
19
0600
8.0
Y
20
0930
24
0600
8.0
Y
21
0600
9.0
Y
22
0630
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
0600
9.0
Y
NOFLOW
26
0600
8.0
Y
NOFLOW
27
0630
18.0
Y
NOFLOW
28
0930
24
0600
9.0
Y
29
0600
8.0
Y
30
0530
2.5
Y
Monthly A-gc LImi1:
Mamhly A-,p:
0
Daily Mxxlmum:
0
Daily Minimum:
0
'•*•NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NODES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 07/24/2018
r '! ,4/ �� 07/19/2018
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
c
07/24/2018
Permittee/Submitter Signatu e:� ** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NODES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2018 (June 2018)
'Report Comments:
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
Below Report Limits (BRL) Results reported as less than (<)
6/5/18, Oil & Grease: Below Repot Limit
6/5/18, 6/20/18, Fecal Coliform; below reporting limit.
6/28/18, BODS GGA result is less than the control limit. Blank value is outside of the control limits.
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPSES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2018 (May 2018)
PERMIT VERSION: 4.0RECEIVED
CLASS: W W-2 I I �, I
ORC: Michael D. Sparks U IV 2018
ORC HAS CHANGED: NEE N i KAL FILES
VERSION: 1.0 DWR SECTION
PERMIT STATUS: Active 3
COUNTY: Cleveland
ORC CERT NUMBER: 987732
RECEIVED/NCDENR/DWR
STATUS: Processed
JUL 2 2018
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGEX:vwos
MOORESVILLE REGIONAL OFF CE
q
F
e
I u'
fi
F
g
F'
F
O
m
C
O
O
u
O
s
3
a
a
2
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
Boo -Qty Daily
TSS-Qty Daily
FCOLr BR
TOTAL N-
TOTALP-Coot
LI-DCE
Ll-DCEY
2400 clock
H.
2400 dock
H.
I Y/H/N
mgd
Isu
Ibs/day
Ibs/day
#/100m1
mg/1
1 M94
Ibs/day
Ibs/day
1
0630
8.0
Y
0.324
2
0930
24
0630
8.0
Y
0.365
8.4
8.8
22.2
<2
3
0600
8.0
Y
0.371
4
0600
8.0
Y
1
0.377
5
NOFLOW
6
1700
2.0
Y
NOFLOW
7
0600
8.0
Y
0.239
8
0600
8.0
Y
0.41
9
0930
24
0630
8.0
ly
1
0.363
8.2
16.1
12.1
<2
10
0600
8.0
Y
0.378
11
0600
8.0
Y
0.354
12
0530
2.5
Y
0.289
13
0530
2.5
Y
NOFLOW
la
0600
8.0
Y
NOFLOW
15
0630
8.0
Y
NOFLOW
16
0600
8.0
Y
NOFLOW
17
0600
8.0
Y
NOFLOW
19
0600
8.0
Y
NOFLOW
19
1
N
NOFLOW
20
1430
2.5
Y
NOFLOW
21
0500
18.0
Y
0.298
22
0500
8.0
Y
0.4
23
0930
24
10630
8.0
Y
0.408
8.5
10.9
29.3
4
24
0600
8.0
B
0.34
25
0600
8.0
B
0.439
26
0830
3.0
B
0.373
27
0930
3.0
B
0.352
28
0930
1.5
B
0.403
29
0630
8.0
B
0.447
30
0930
124
0630
8.0
113
0.403
8.5
19.5
18.8
14
31
0630
8.0
B
1
0.386
Monthly Average Limit.
045
68
124
200
0.071
0.05E
Monthly Average:
0.367571
11.325
20.6
2
Daily Maxi mom:
0.447
8.5
19.5
29.3
4
Daily Minimum:
0.239
8.2
6.1 112.1
0
* * * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation -Holiday

NFaES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2018 (May 2018)
PERMPP VERSION: 4_0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
.2
g
u
o
F'
@
O
C
1 O
_
O
u
O
=
w
Z°
34536
32103
34546
77163
31566
34571
34601
31606
34616
34611
34586
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
t-12DCEY
1,3-DCPE
1,3-DCB
1p-DCH
2r4-DCPN
2,4-DMPH
2,4-DNPH
2,4-DNT
2CPHENOL
2400 dock
H.
2400 dock
H.
Y/BIN
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
1
0630
8.0
Y
2
0930
24
0630
8.0
Y
3
10600
8.0
Y
4
0600
8.0
Y
5
NOFLOW
6
1700
2.0
Y
NOFLOW
7
0600
8.0
ly
e
0600
8.0
Y
9
0930
24
0630
8.0
Y
10
0600
8.0
Y
11
0600
8.0
Y
12
0530
2.5
ly
13
0530
2.5
Y
NOFLOW
14
0600
8.0
Y
NOFLOW
'
15
0630
8.0
Y
NOFLOW
16
0600
8.0
Y
NOFLOW
17
0600
8.0
Y
NOFLOW
18
0600
8.0
Y
NOFLOW
19
N
NOFLOW
20
1430
2.5
Y
NOFLOW
21
0500
8.0
Y
22
0500
8.0
Y
23
0930
24
0630
8.0
Y
24
0600
8.0
B
25
0600
8.0
B
26
0830
3.0
B
27
0930
3.0
B
28
1
0930
1.5
B
0630
8.0
B
30
L29
0930
24
0630
8.0
B
31
0630
8.0
B
Monthly A-w Limlu
M249
0.219
0.068
0.094
0.1
0.048
0.126
0.058
0129
0.365
0.1
Monthly Average:
Dolly Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY= No Visitation -Holiday

NPQES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2018 (May 2018)
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather, NOFLOW=No Flow; HOLIDAY= No Visitation —Holiday

NPAES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2018 (May 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
m
p
U'
E
u°
FF
F
a
O
C
1 O
o°
U
O
a
K
:L'
01034
01042
00720
34336
34341
39110
34371
34381
01051
34418
34423
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Cr-TOTAL
COPPER
CN-TOT
DIETY-PH
DIMET-PH
DNBPHTH
ETHYLBEN
FLUORENE
LEAD
I liIETHYLCH
MECL2
2400 clock
Hn
2400 clock
H.
y1wN
ug/t
ug/I
119/1
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
lbs/day
Ibs/day
Ibs/day
1
0630
8.0
Y
2
0930
24
0630
8.0
Y
3
0600
8.0
Y
4
0600
8.0
Y
5
NOFLOW
6
1700
2.0
Y
NOFLOW
7
0600
8.0
Y
e
0600
8.0
Y
9
0930
24
0630
8.0
Y
10
0600
8.0
Y
11
0600
8.0
Y
12
0530
2.5
Y
13
0530
2.5
ly
I NOFLOW
14
0600
8.0
Y
NOFLOW
15
0630
8.0
Y
NOFLOW
16
0600
8.0
Y
NOFLOW
17
0600
8.0
Y
NOFLOW
18
0600
8.0
ly
I NOFLOW
19
N
NOFLOW
20
1430
2.5
Y
NOFLOW
21
r
0500
8.0
Y
22
0500
8.0
Y
23
0930
0630
8.0
Y
24
0600
8.0
B
25
0600
8.0
B
26
0830
3.0
B
27
0930
3.0
B
28
0930
1.5
B
29
0630
8.0
B
70
0930
24
0630
18.0
B
31
1
10630
8.0
B
Monthly Average Llmrt•.
3.583
0.261
0.061
0.987
0.103
0.071
2.227
0.278
0.129
Monthly Avemgc:
D.1ry M-bnma:
Daily Minimum:
****No Reporting Reason: ENFRUSE = No Flow-ReasetRecycle; ENVWTHR = No Visitation -Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation- Holiday

IDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2018 (May 2018)
PERMIT VERSION: 4_0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation —Holiday

NPPES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2018 (May 2018)
PERMIT VERSION: 4_0
CLASS; W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
r
E
E
F
fi
c�
a
E
O
�
O
o°
U
O
¢
K
Z
39700
39702
34247
34242
79531
34220
34526
34626
31320
34376
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Annually
Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
HCB
HEXCLBD
BNZO-A-P
BNZO-K-E
34-BNZFA
ANTHRACE
BNZO-A-A
26DUOM
CHRYSENE
FLUOBANT
2400 crack
H.
2400 dock
H.
Y/B/N
ug/l
Ibs/day
119/1
ug/l
u9/1
ug/l
ug/l
ug/l
u9/1
ug/l
1
0630
8.0
Y
2
0930
24
0630
8.0
Y
3
0600
8.0
Y
4
0600
8.0
ly
5
NOFLOW
6
1700
2.0
Y
NOFLOW
7
0600
8.0
Y
8
0600
8.0
Y
9
0930
24
0630
8.0
Y
10
0600
8.0
Y
21
0600
8.0
Y
12
0530
2.5
ly
13
0530
2.5
Y
NOFLOW
14
1
0600
8.0
Y
NOFLOW
is
0630
8.0
Y
NOFLOW
16
0600
8.0
Y
NOFLOW
17
0600
8.0
Y
NOFLOW
18
0600
8.0
Y
I NOFLOW
19
1
N
NOFLOW
20
1430
2.5
Y
NOFLOW
21
0500
8.0
Y
22
0500
18.0
Y
23
0930
24
10630
8.0
Y
24
0600
8.0
B
25
0600
8.0
B
26
0830
3.0
B
27
0930
3.0
B
28
0930
1.5
B
29
0630
9.0
1B
30
0930
124
10630
8.0
B
3t
0630
8.0
113
Moaarly Avemge Limit.
0.065
Mcm ft Avemgr.
Daily Mmimam•
Daily Maim-
* * * * No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2018 (May 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 06/18/2018
( +K 06/15/2018
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
06/18/2018
Permittee/Submitter SignaturY-* Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221, 402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data-
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NtPES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2018 (May 2018)
Report Comments:
PERMIT VERSION: 4_0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
5/02/18, 5/09/18, Fecal Coliform; below reporting limit.
5/09/18, BODS; below reporting limit.
5/30/18, BODS; Difference between sample dilution is greater than 30%.
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
PERMIT VERSION: 4.0
CLASS: WW-2 ORC: Michael D. Spanks C I \/
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
-J
GRADE: W W-3. ORC HAS CHANGED: N, 9 t l' v 2O 7
eDMR PERIOD: 10-2017 (October 2017) VERSION: 1.0 ` STATUS: Processed
C� ii TP,l_ FILES
E:)VVR SVGTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
O
e
yZ
e
U
E
FF
e
6
O
E
F
O
m
O
m
•�
ae
z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
,
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
BOD-Qty Daily
TSS-Qly Daily
FCOLIBR
TOTAL N-
TOTAL P-Cone
l,l-DCE
1,1-DCEY
2400 clock
Hrs
2400 clock
H.
Y/B/fi
mgd
so
lbs/day
I Ibs/day
#/looml
mg/I
mg/I
I lbs/day
Ibs/day
I
N
NOFLOW
2
0500
10.5
Y
NOFLOW
3
0630
8.5
Y
0.322
37
4
1130
24
0630
8.5
Y
0.323
8.3
111.9
35
1
5
0600
8.5
Y
0.356
n n
6
0630
8.5
Y
0.305
L U I
I
7
N
NOFLOW
8
1815
3.0
Y
NOFLOW
U .,
9
0500
10.50
Y
NOFLOW
10
0630
9.0
Y
0.391
85
11
1130
24
0630
10.5
Y
0.37
7.7
12.3
42.9
12
0600
19.5
Y
0.407
13
0630
8.0
Y
0.413
14
0930
3.0
Y
NOFLOW
15
1700
2.0
Y
NOFLOW
16
0630
8.0
Y
0.316
4
17
1130
24
0630
8.0
Y
0.386
8
10.9
56.7
18
0630
8.0
Y
0.373
19
0630
8.0
Y
0.283
20
0630
8.0
ly
1
0.216
21
N
NOFLOW
22
1230
1
B
NOFLOW
23
0600
8.0
Y
NOFLOW
24
1130
24
0630
8.0
Y
0.363
8.2
<6.1
39.4
28
25
0600
8.0
Y
0.416
26
0600
8.0
Y
0.372
27
0630
8.0
Y
0.296
28
1030
l
B
0.234
29
N
NOFLOW
30
0630
8.0
B
NOFLOW
31
0630
14.0
IB
INOFLOW
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.341222
8.775
43.5
24.361817
Daily Maximum:
0.416
8.3
12.3
56.7
85
DaOynlionnum:
0.216
7.7
10
35
4
"•"" No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: W W-2
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 10-2017 (October 2017)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
e
E
e
L
O
-
F
O
y
O
a
Z°
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
la-DCPE
1,3-DCB
1,4-DCB
2,4-DCPH
2,4-DSIPH
2,4.DNPH
2,4-D.Yr
2400 clock
H.
2400 dock
IH.
YIB/N
Ibs/day
Ibs/day
lbs/day
Ibs/day
lbs/day
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
1
N
NOFLOW
2
0500
10.5
Y
NOFLOW
3
0630
8.5
Y
4
1130
24
0630
8.5
Y
9
0600
8.5
Y
6
0630
18.5
Y
7
N
NOFLOW
8
1815
3.0
Y
NOFLOW
9
0500
10.50
Y
NOFLOW
10
0630
9.0
Y
11
1130
24
0630
10.5
1 Y
12
0600
9.5
Y
13
0630
8.0
Y
14
0930
3.0
Y
NOFLOW
15
1700
2.0
Y
NOFLOW
16
0630
8.0
Y
17
1130
24
0630
8.0
Y
i8
0630
8.0
Y
19
0630
8.0
Y
20
0630
8.0
Y
21
N
NOFLOW
22
1230
1
B
NOFLOW
23
0600
8.0
Y
NOFLOW
24
1130
24
0630
8.0
Y
25
0600
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
28
1030
I
B
29
N
NOFLOW
30
0630
8.0
B
NOFLOW
31
0630
14.0
B
NOFLOW
Monthly Average Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0365
1ltombly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2017 (October 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
s
e
u°
E
u
h
O
O
a
z
O
1.
a
Z*
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-o-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400c1ak iH.
2400dock
H.
YBN
lbs/day
Ibs/day
ug/I
Ibs/day I
Ibs/day
Ibs/day
Ibs/day
ug/I I
Ibs/day
ug/I
ug/l
I
N
NOFLOW
2
0500
10.5
Y
NOFLOW
3
0630
8.5
Y
4
1130
24
10630
8.5
ly
5
0600
8.5
Y
6
0630
8.5
Y
7
N
NOFLOW
8
1815
13.0
Y
NOFLOW
9
0500
10.50
Y
NOFLOW
10
0630
9.0
Y
11
1130
24
0630
10.5
Y
12
0600
9.5
IY
13
0630
8.0
Y
14
0930
3.0
Y
NOFLOW
1s
1700
2.0
Y
NOFLOW
16
0630
8.0
Y
17
1130
24
0630
8.0
Y
IS
0630
18.0
Y
19
0630
8.0
Y
20
0630
8.0
Y
21
N
NOFLOW
22
123
11
B
NOFLOW
27
0600
8.0
Y
NOFLOW
24
1130
24
0630
8.0
Y
25
0600
8.0
Y
26
0600
18.0
Y
27
0630
8.0
Y
28
1030
l
B
29
N
NOFLOW
30
0630
8.0
B
NOFLOW
3t
0630
4.0
B
NOFLOW
Monthly Average Limit:
0.1
0.132
0.252
0.23E
0.071
0.071
0.119
Alomhly Averagr.
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Rcuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2017 (October 2017)
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
fi
U
EG
u
F'
O
O
o°
O
1.
,Z'
34242
39100
32102
34301
95811
32106
01034
34320
01042
11111
34136
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
132E PHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 clock
Hrs
2400 clock
H.
Y/B/N
ug/I
lbs/day
lbs/day
lbs/day I
lbs/day
lbs/day I
ug/I
ug/I
ug/I
ug/1
lbs/day
1
N
NOFLOW
2
0500
10.5
Y
NOFLOW
3
0630
8.5
Y
4
1130
24 10630
8.5
Y
5
0600
8.5
Y
6
0630 18.5
Y
7
N
NOFLOW
8
1815
3.0
Y
NOFLOW
9
0500
10.50
Y
NOFLOW
10
0630
9.0
Y
'
11
1130
24
0630
10.5
Y
12
0600
9.5
Y
13
0630
8.0
Y
la
1
0930
3.0
Y
NOFLOW
15
1700
2.0
Y
NOFLOW
16
0630
18.0
ly
17
1130
24
0630
8.0
Y
18
0630
8.0
Y
19
0630
8.0
Y
20
0630
8.0
Y
21
N
NOFLOW
22
1230
1
B
NOFLOW
23
0600
8.0
Y
NOFLOW
24
1130
24
0630
8.0
Y
25
0600
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
28
1030
1
B
29
N
NOFLOW
30
1
0630
8.0
B
NOFLOW
31
0630
4.0
B
NOFLOW
Monthly Average Limit:
0.332
0.058
0.048
0.336
0.068
3.583
0.261
Monthly Average:
Daily Marhnum:
Daily 1lialmum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 10-2017 (October 2017)
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
m
u
F
F=
a
O
O
`
-
O
s
O
Iee°
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
D151ET-PH
DNB PlITH
ETHYLBEN
FLUORENE
HEXCLBD
HCE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 clock
H.
2400 clock
IH.
Y/R/N
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I ibs/day
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
1
N
NOFLOW
2
0500
10.5
Y
NOFLOW
3
0630
8.5
Y
4
1130
24
0630
8.5
Y
5
0600
8.5
Y
6
0630
18.5
Y
7
N
NOFLOW
8
1815
3.0
Y
NOFLOW
9
0500
10.50
Y
NOFLOW
10
0630
9.0
Y
11
1130
24
0630
10.5
Y
12
0600
19.5
Y
13
0630
8.0
Y
14
0930
3.0
Y
NOFLOW
15
1700
2.0
Y
NOFLOW
16
0630
8.0
Y
17
1130
24
0630
8.0
Y
18
0630
8.0
ly
19
0630
8.0
Y
20
0630
8.0
Y
21
N
NOFLOW
22
1230
I
B
NOFLOW
23
0600
8.0
Y
NOFLOW
24
1130
24
0630
8.0
ly
25
0600
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
28
1030
1
B
29
N
NOFLOW
30
1
0630
8.0
B
NOFLOW
31
0630
4.0
B
NOFLOW
Monthly Average Limlt:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Average:
Daily Ma3lmum:
Daily Mrnimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2017 (October 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
0
"
o
U
F
-
u
o
F
F.
t
O
O
E
O
o°
O
O
wl
aee
ii
a
;9-
34447
34461
34694
34469
34475
34010
39700
34376
34220
34626
00010
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Calculated
NITROBEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
HCB
FLUORANT
ANTHRACE
26DINITR
TEMP-C
2400 clock lH.
2400 clock lH.
Y/B/N
Ibs/day
Ibs/day
Ibs/day I
lbs/day
lbs/day I
Ibs/day
ug/l
ug/l
ug/l I
ug/l
deg c
1
N
NOFLOW
2
0500
10.5
Y
NOFLOW
3
0630
8.5
Y
4
1130
24
0630
8.5 IY
21.6
5
0600
8.5
Y
6
10630
8.5
Y
7
N
NOFLOW
8
1815
3.0
Y
NOFLOW
9
0500
10.50
Y
NOFLOW
10
0630
9.0
Y
11
1130
24
0630
10.5
Y
25.1
12
0600
9.5
Y
13
10630
8.0
IY
14
0930
3.0
Y
NOFLOW
15
11700
2.0
Y
NOFLOW
16
0630
8.0
Y
17
1130
24
0630
8.0
Y
20.6
is
0630
8.0
ly
19
0630
8.0
Y
20
0630
8.0
Y
21
N
NOFLOW
22
1230
1
B
NOFLOW
23
0600
8.0
Y
NOFLOW
24
1130
24
0630
8.0
Y
19.1
25
0600
18.0
Y
26
0600
8.0
27
0630
8.0
28
1030
1
rB
29
NOFLOW
30
0630
8.0
NOFLOW
31
0630
14.0
IB
NOFLOW
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.084
nmuthly Average:
21.6
Daily Maximum:
125.1
Daily 31inimum:
19.1
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2017 (October 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
fi
•`
E
O
O
O
c4
a
Z
00300
Calculated
DO
2400 daek
H.
2400 dock IH.
Y/m
mgtl
1
N
NOFLOW
2
0500
10.5
Y
NOFLOW
3
0630
8.5
Y
4
1130
24
0630
8.5
1 Y
7.7
5
0600
8.5
Y
6
10630
8.5
Y
7
N
NOFLOW
s
1815
3.0
Y
NOFLOW
9
0500
10.50
Y
NOFLOW
10
0630
9.0
Y
11
1130
24
0630
10.5
Y
6.9
12
0600
9.5
Y
13
0630
8.0
Y
14
10930
3.0
Y
NOFLOW
15
1700
2.0
Y
NOFLOW
16
0630
8.0
Y
17
11130
24
0630
8.0
Y
7.8
18
0630
8.0
Y
19
0630
8.0
Y
20
0630
8.0
Y
21
N
NOFLOW
22
1230
1
H
INOFLOW
23
0600
18.0
Y
NOFLOW
24
1130
24
0630
8.0
Y
8.3
25
0600
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
28
1030
1
B
29
N
NOFLOW
30
0630
8.0
B
NOFLOW
31
0630
4.0
B
NOFLOW
M-thly Average Limit:
Monthly Average:
7.675
Daily maim m:
8.3
Daily \Hnlmum:
6.9 '
****NoReporting Reason: ENFRUSE=No Flow-Reusc/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 10-2017 (October 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 11/15/2017
11/15/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
11/15/2017
Permittee/SVbmitter Signature:*** Eric Johnson E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
CLASS: W W-2
COUNTY: Cleveland
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
ORC CERT NUMBER: 987732
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 10-2017 (October 2017)
VERSION: 1.0
STATUS: Processed
Report Comments:
10/17/2017 BOD GGA result is less than the control limit
10/24/2017 BOD Below reporting limit, GGA result is less than the control limit

CERTIFIED MAIL: 7015 1660 0001 0635 4957
Return Receipt to PEM Carter
PEMC17:27
November 20, 2017
NCDEQ
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
rJ'
Celanese
The chemistry inside innovation"
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerning October 2017, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the October's report has been submitted through the eDMR
system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
• 10/17/2017: BOD5 GGA results is less than the control limits.
• 10/24/2017: BOD5 below reporting limits, GGA results is less than the control limit.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(cDcelanese.com.
ely,
PEM Carter
EHS Lead/Environmental Engineer
Attachments

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2017 (September 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
RE'"h
CLASS: W W-2, (s COUNTY: Cleveland
ORC: Michael D. Sparks NOV 0 6 2017 ORC CERT NUMBER: 987732EIVED/NCDE1klR/MA1R
ORC HAS CHANGED: No /^ N O V 13 L 01 ?
VERSION: lA
,-,ENTIIA - FILES STATUS: Processed
®AIR SEC T J(),q
WQROS
hnOrTR�ct,lGi�A!- 0, F iCE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: 1�0-
u
a
y
_
"
E
u
P
E
u
t=
F
E
i
O
o
E
F
O
2m
y
o°
U
O
d
a
n
a
Z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pit
I BOD-Qty Daily
TSS -Qty Daily
FCOLI BR
TOTAL N-
TOTAL P - Cone
l,l-DCE
1,1-DCEY
2400 clock
11.
2400 clock
xrs
YIR/N
mgd
so
lbs/day
Ibs/day
0/100ml
mg/l
mg/1
Ibs/day
lbs/day
I
0630
16
Y
NOFLOW
2
0900
3
Y
NOFLOW
3
0
N
NOFLOW
4
1115
2.75
Y
NOFLOW
5
0630
9.0
Y
0.207
6
11:30
24
0630
9.0
Y
0.347
8.4
13
29.2
42
7
0600
8.5
Y
0.38
S
0630
8.5
1 Y
0.432
9
1100
1.0
B
0.395
10
1015
2.25
Y
0.389
11
0500
10.50
Y
0.34
12
0500
10.5
Y
0.323
13
0600
11.0
Y
0.331
14
11:30
24
10500
10.5
1 Y
1
0.304
8
7.4
42.6
9
Is
0630
6.5
Y
0.257
16
0730
3.0
Y
NOFLOW
17
0500
3.0
Y
NOFLOW
18
0600
11.0
Y
NOFLOW
19
11:30
24
10630
12.0 1
Y
1
0.348
8.4
11.9
51.7
27
20
0630
11.5
Y
0.382
21
0600
9.5
Y
0.35
22
0600
4.75
Y
0.279
23
0
N
NOFLOW
24
1445
2.75
B
NOFLOW
25
0600
8.5 ly
I
NOFLOW
26
0600
8.5
Y
NOFLOW
27
0500
9.5
Y
NOFLOW
28
0600
8.5
Y
NOFLOW
29
0600
8.5
Y
NOFLOW
30
0
N
NOFLOW
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.3376
10.766667
41.166667
21.69128
Daily Matt mum:
0432
8.4
13
51.7
42
Daily Minimum:
0.207
8
7.4 129.2
19
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2017 (September 2017)
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
e
cu
U
E
s
H
F
-
O
O
O
o
O
a
n
Z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Gr46
Gr46
Grab
Glab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPH
2,4-DMPH
2,4-DNPH
2,4-DNT
2400 clock
H.
2400 clock
Hrs
I WIN
I Ibs/day
Ibs/day
I Ibs/day,
lbs/day
lbs/day
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
lbs/day
I lbs/day
1
0630
16
Y
NOFLOW
2
0900
3
Y
NOFLOW
3
0
N
NOFLOW
4
ills
2.75
Y
NOFLOW
5
0630
9.0
1 Y
6
11:30
24
0630
9.0
Y
7
0600
8.5
Y
e
0630
8.5
Y
9
1100
1.0
B
10
1015
2.25
1 Y
11
0500
10.50
Y
12
0500
10.5
Y
13
0600
11.0
Y
14
11:30
24
0500
10.5
Y
is
0630
6.5
Y
16
0730
3.0
Y
NOFLOW
17
0500
3.0
Y
NOFLOW
i8
0600
11.0
1 Y
NOFLOW
19
11:30
24
0630
12.0
Y
20
0630
11.5
Y
21
0600
9.5
Y
22
0600
4.75
Y
23
0
1 N
INOFLOW
24
1445
2.75
B
NOFLOW
25
0600
8.5
Y
NOFLOW
26
0600
8.5
Y
NOFLOW
27
0500
9.5
Y
NOFLOW
28
0600
8.5
Y
NOFLOW
29
0600
8.5
Y
NOFLOW
30
0
N
NOFLOW
Monthly Average Limit:
0.249
0.219
OA94
0.069
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly Average:
Daily Maximum:
Daay \Dnlmum:
""°"NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2017 (September 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
9
F
E
F
s
E
E
�
a
O
w
Oc
iE
1 O
y
O
o
a
7
34596
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-a-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clack
H.
2400 dock
H.
Y/B/N
Ibs/day
Ibs/day
ugfl
I Ibs/day
lbs/day
I Ibs/day
lbs/day
ug/l
Ibs/day
ug/I
ug/l
1
0630
16
Y
NOFLOW
2
0900
3
1 Y
NOFLOW
3
0
N
NOFLOW
4
1115
2.75
Y
NOFLOW
5
0630
9.0
Y
6
11:30
24
0630
9.0
Y
7
0600
8.5
Y
8
0630
8.5
Y
9
1100
1.0
B
10
1015
2.25
Y
11
0500
10.50
Y
12
0500
10.5
Y
13
0600
11.0
IY
14
11:30
24
0500
10.5
Y
15
0630
6.5
Y
16
0730
3.0
Y
NOFLOW
17
1
0500
3.0
Y
NOFLOW
is
0600
11.0
Y
NOFLOW
19
11:30
24
0630
12.0
Y
20
0630
11.5 1
Y
21
0600
9.5
Y
22
0600
4.75
Y
23
0
N
NOFLOW
24
1445
2.75
B
NOFLOW
25
0600
8.5
Y
NOFLOW
26
0600
8.5
Y
NOFLOW
27
0500
9.5
Y
NOFLOW
28
0600
8.5
Y
NOFLOW
29
0600
8.5
Y
NOFLOW
30
0
N
NOFLOW
Monthly Average Limit:
0.1
0.132
0.252
0.132
0.071
0.071
0.119
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: W W-2
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 09-2017 (September 2017)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
e
F
s
E
e
F
C
O
y
O
Z
34242
39100
32102
34301
85811
32106
01034
34310
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grob
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
132E PHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 clock
Ho
2400 clock
Hns
I Y/MN,
ug/I
I Ibs/day
Ibs/day
Ibs/day
I Ibs/day,
Ibs/day
ug/I
I ug/l
ug/1
I ug/I
Ibs/day
1
0630
16
Y
NOFLOW
2
0900
3
Y
NOFLOW
3
0
N
NOFLOW
4
1115
2.75
Y
NOFLOW
5
0630
9.0
Y
6
11:30
24
0630
9.0
Y
7
0600
8.5
Y
8
0630
8.5
Y
9
1100
1.0
B
10
1015
2.25
ly
11
0500
10.50
Y
12
0500
10.5
Y
13
0600
11.0
Y
14
11:30
24
0500
10.5
Y
I5
0630
6.5
Y
16
0730
3.0
Y
NOFLOW
17
0500
3.0
Y
NOFLOW
18
1
0600
11.0
ly
I NOFLOW
19
11:30
24
0630
12.0
Y
Z0
0630
11.5
Y
21
0600
9.5
Y
22
0600
4.75
Y
23
0
N
NOFLOW
24
1
1445
2.75
B
NOFLOW
25
0600
8.5
Y
NOFLOW
26
0600
8.5
Y
NOFLOW
27
0500
9.5
Y
NOFLOW
28
0600
8.5
Y
NOFLOW
29
0600
8.5
Y
NOFLOW
30
1
0
IN
INOFLOW
Monthly Average Limit:
0332
0.058
0.048
0336
0.068
3.593
0.261
Monthly Average:
Daily Maximum:
Daily Minimum:
#°""NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2017 (September 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
t7
F
e
U
2
E
t-
Q
O
O
V
a
O
o
a`
a
,7
34341
39110
34371
34381 .
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DD1tET-PH
DNB KITH
ETHYLBEN
FLDORENE
HEXCLBD
NCE
LEAD
61ETHYLCH
\fECL2
NAPTNALE
NICKEL
2400,N&
Ito
2400 clock
Hn
Y/B/N
Ibs/day
I Ibs/day
lbs/day I
Ibs/day
lbs/day I
Ibs/day
Ibs/day
Ibs/day
Ibs/day I
Ibs/day
Ibs/day
1
0630
16
Y
NOFLOW
2
0900
3
Y
NOFLOW
3
0
N
NOFLOW
4
1115
2.75
Y
NOFLOW
5
0630
9.0
Y
6
11:30
24
0630
9.0
Y
7
0600
8.5
Y
8
0630
8.5
Y
9
1100
1.0
IB
10
1015
2.25
Y
11
0500
10.50
Y
12
0500
10.5
Y
13
0600
11.0
Y
14
11:30
24
0500
10.5
Y
15
0630
6.5
Y
16
0730
3.0
ly
NOFLOW
17
0500
3.0
Y
NOFLOW
18
0600
11.0
Y
NOFLOW
19
11:30
24
0630
12.0
Y
20
0630
11.5
Y
21
0600
9.5
ly
22
0600
4.75
Y
23
0
N
NOFLOW
24
1445
2.75
B
NOFLOW
25
0600
8.5
Y
NOFLOW
26
0600
8.5
Y
NOFLOW
27
0500
9.5
Y
NOFLOW
28
0600
8.5
Y
NOFLOW
29
0600
8.5
Y
NOFLOW
36
0
N
NOFLOW
Monthly Average Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Afmuhiy Average:
Daily Maximum:
Daily' Dalmum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2017 (September 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
8
t
0
E
O
O
Z
34447
00556
TGP311
34461
34694
34469
34475
34010
39700
34376
34220
Annually
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grob
NITROBEN
Olt GRSE
CER17DPF
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
HCB
FLUORANT
ANTHRACE
2400 clock
1H.
2400 clock I
His
Y/BN
Ilbs/day
mg/I I
pass/fail
lbs/day
lbs/day
Ibs/day
Ibs/day I
Ibs/day
ug/1
ug/I
ug/1
1
0630
16
Y
NOFLOW
2
0900
3
Y
NOFLOW
3
0
N
NOFLOW
4
1115
2.75
Y
NOFLOW
5
0630
19.0
Y
6
11:30
24
0630
9.0
Y
7
0600
8.5
Y
S
0630
8.5
Y
9
1100
1.0
B
10
11015
2.25
Y
11
0500
10.50
Y
12
0500
10.5
Y
13
0600
11.0
Y
14
11:30
24
0500
10.5
Y
15
0630
6.5
Y
16
0730
3.0
ly
I NOFLOW
17
0500
3.0
Y
I NOFLOW
18
0600
11.0
Y
NOFLOW
19
11:30
24
0630
12.0
Y
<5
P
20
0630
1 11.5
Y
21
0600
9.5
Y
22
0600
4.75
Y
23
0
N
NOFLOW
24
1445
2.75
B
NOFLOW
25
0600
8.5
Y
NOFLOW
26
0600
8.5
Y
NOFLOW
27
0500
9.5
Y
NOFLOW
28
0600
8.5
Y
NOFLOW
29
0600
8.5
Y
I NOFLOW
30
0
N
I NOFLOW
Monthly Average Limit:
0.N7
0.071
0.0411
0.081
0.071
0.0.
Monthly Average:
0
Daily Mnilmum:
0
DaOy \rinhnum:
0
**** No Reporting Reason: ENFRUSE = No Flow-Rcuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation -Holiday

, NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2017 (September 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
e'
u
r
F=
F
O
°
O
O
u
O
ai
=
z
34626
00010
00300
Annually
Grab
Grab
Calculated
26DINITR
TEMP-C
DO
2400 cloek
H.
2400 clock
IHrs
Y/B/N
ug/1
deg c
mg/I
1
0630
16
Y
NOFLOW
2
0900
3
Y
NOFLOW
3
0
N
NOFLOW
4
1115
2.75
Y
NOFLOW
5
0630
9.0
Y
6
11:30
124
0630
19.0
Y
1
25.6
5.9
7
0600
8.5
Y
8
0630
8.5
Y
9
1100
1.0
B
10
1015
2.25
Y
11
0500
10.50
Y
12
0500
10.5
1 Y
13
0600
11.0
Y
14
11:30
24
0500
10.5
Y
21
7.5
15
0630
6.5
Y
16
0730
3.0
Y
NOFLOW
17
0500
3.0
Y
NOFLOW
18
0600
11.0
Y
NOFLOW
19
11:30
24
0630
12.0
Y
25.1
6.7
20
0630
1 11.5
Y
21
0600
9.5
Y
22
0600
4.75
Y
23
0
N
NOFLOW
24
1445
2.75
B
NOFLOW
25
0600
8.5
Y
NOFLOW
26
0600
8.5
Y
NOFLOW
27
0500
9.5
Y
NOFLOW
28
0600
8.5
Y
NOFLOW
29
0600
8.5
Y
NOFLOW
30
0
N
NOFLOW
Monthly Average Limit:
Monthly Average:
23.9
6.7
Daily Maximum:
25.6
7.5
Daily'M.I. m:
21
15.9
****No Reporting Reason: ENFRUSE=NoFlow-Rcuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2017 (September 2017)
Report Comments:
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
BOD sample 9/6/2017. Difference between sample dilutions is greater than 30%. Blank value is outside of the control limits.

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 09-2017 (September 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 10/20/2017
10/20/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
10/20/2017
Permittee/Submitter Signature:*** Eric J�hnson E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

CERTIFIED MAIL: 70151660 0001 0635 4889
Return Receipt to PEM Carter
PEMC17:25
October 30, 2017
NCDEQ
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
0 Celanese
The chemistry inside innovation
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerning September 2017, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the September's report has been submitted through the
eDMR system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
• Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
• 9/26/2017: BOD5 difference between sample dilutions is greater than 30%.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call meat 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carterO-celanese.com.
ely,
( �
PEM Carter
EHS Lead/Environmental Engineer
Attachments

-3
NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese-ShelbyFacilityCLASS: WW-2 i t O NTY: Cleveland
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks ORC CERT NUMBER: 9`8'1g2:1VED/NCDENR/Dln/s;
GRADE: WW-3. ORC HAS CHANGED: No O C y I ® 4 2'017
OCT 9 2Gir
eDMR PERIOD: 08-2017 (August 2017) VERSION: 1.0 CEII!TRf%L FILEdATUS: Processed
UVVR SECTION WpQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHAOR �1VOGlONAL Os=�fCE
q
6
u
U
E
u
F
g
-
O
O
o
O
e
a
2
50050
00400
QD310
QD530 _
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annual)
Semi-annually
Annually
Annual)
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pit
BOD -Qty Daily
TSS -Qty Daily
FCOLI eR
TOTAL N-
TOTAL P - Cane
1,1-DCE
I,l-DCEY
2400 clock
lic,
2400 clack
Bra
YiBIN
m d
su
lbs/da
lbs/da
#/100ml
m I
mg/I
Ibs/da
Ibs/da
2
0600
12.0
Y
0.237
11
2
1130
24
0600
11.0
Y
0.179
7.8
6.4
13.7
1.1
0.08
3
0600
8.5
Y
0.141
4
0600
6.0
Y
0.085
5
N
NOFLOW
6
N
NOFLOW
7
0600
10.0
Y
NOFLOW
8
0600
10.5
Y
NOFLOW
9
0600
9.0
Y
0.304
83
10
1130
24
0600
8.5
Y
0.325
7.9
10.3
41.7
11
0600
8.5
Y
0.366
12
0700
15.0
Y
1
0.4
13
0815
5.0
Y
0.394
14
0600
10.5
Y
0.402
15
0600
9.5
Y
0.381
83
16
1130
24
0600
9.5
Y
0.381
8
13.3
34.3
17
0600
8.0
Y
0.425
i8
0600
18.0
Y
1
0.369
19
1115
2.0
B
0.371
20
1045
2.0
B
0.337
21
0600
9.0
Y
0.34
22
1130
24
0630
8.5
Y
0.309
7.8
13.4
16.5
3
23
0630
8.5
Y
0.26
24
0600
9.5
Y
0.205
25
0600
8.0
Y
NOFLOW
26
1015
2.0
B
I NOFLOW
27
1045
2.25
B
NOFLOW
28
0630
7.0
B
NOFLOW
29
0630
10.0
Y
NOFLOW
30
0630
8.5
Y
NOFLOW
31
0630
9.5
Y
NOFLOW
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.31055
10.85
26.55
21.835721
1.1
0.08
Daily Maximum:
0.425
8
13.4
41.7
83
1.1
10.08
Daily Minimum:
0.085
7.8
16.4
113.7
3
11.1
0.08
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: W W-2
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 08-2017 (August 2017)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
F
U
6
F
F
H
O
O
O
o
C
O
t
a
iz
2
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annuall
Annuall
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPII
2,4-DMPH
2,4-DNPII
2,4-DNT
2400 clock
Hrs
2400 clack
I W.
Y/BIN
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
1
0600
12.0
Y
2
1130
24
0600
11.0
1 Y
3
0600
8.5
Y
4
0600
6.0
Y
5
N
NOFLOW
6
N
NOFLOW
7
0600
10.0
Y
NOFLOW
8
0600
10.5
Y
NOFLOW
9
0600
9.0
Y
10
1130
24
0600
8.5
Y
11
0600
8.5
Y
12
0700
5.0
1 Y
13
0815
5.0
Y
14
0600
10.5
Y
15
0600
9.5
Y
16
1130
24
0600
9.5
Y
17
0600
8.0
Y
is
0600
18.0
Y
19
1115
2.0
B
30
1045
2.0
B
21
0600
9.0
Y
22
1130
24
0630
8.5
Y
23
0630
8.5
Y
24
0600
9.5
Y
25
0600
8.0
Y
NOFLOW
26
1015
2.0
1 B
I NOFLOW
27
1045
2.25
B
NOFLOW
28
0630
7.0
B
NOFLOW
29
0630
10.0
Y
NOFLOW
70
0630
8.5
Y
NOFLOW
31
0630
9.5
Y
NOFLOW
Monthly Average Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0365
Monthly Average:
Daily Maximum:
Daily llnnimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation-AdverseWeather; NOFLOW=No Flow; HOLIDAY=NoVisitation-Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
F
E
a
U
j
E
u
F
H
O
ul
C
B
O
o
U
O
o
n
m
a
a
Z
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPIIEN01,
2NPIIENOL
34.BNZFA
46DN-o-C
4NPIIENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clock
firs
2400 clock
I tics
Y/B/N
Ibs/da
Ibs/da
u
Ibs/da
Ibs/da
Ibs/da
lbs/day
UFA
lbs/day
Ugfl
u
1
0600
12.0
Y
2
1130
24
0600
11.0
Y
3
0600
8.5
Y
4
0600
6.0
Y
'
5
N
NOFLOW
6
N
NOFLOW
7
10600
10.0
ly
I NOFLOW
e
0600
10.5
Y
NOFLOW
9
0600
9.0
Y
10
1130
24
0600
8.5
Y
11
0600
8.5
Y
12
0700
5.0
ly
13
0815
5.0
Y
14
0600
10.5
Y
is
0600
9.5
Y
16
1130
24
0600
19.5
Y
17
0600
8.0
ly
18
0600
8.0
Y
19
ills
2.0
B
20
1045
2.0
B
21
0600
9.0
Y
22
1130
24
0630
8.5
Y
23
0630
9.5
ly
24
0600
9.5
Y
25
1
0600
8.0
Y
NOFLOW
26
1015
2.0
B
NOFLOW
27
1045
2.25
B
NOFLOW
28
0630
7.0
B
NOFLOW
29
0630
10.0
Y
NOFLOW
30
0630
8.5
Y
NOFLOW
71
0630
9.5
Y
NOFLOW
Monthly Average Limit:
O.l
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 08-2017 (August 2017)
i
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW.=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
p
FZZ
_
E
_
o
U
F
E
u
a
E.
Q
0
O
Q
g
g
O
o
u
O
ii
cc
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Atraually
A=ually
Annually
Annually
Annually
Annually
Annually
Airnually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET•PH
DNB PIITH
ETHYLBEN
FLUORENE
IIEXCLBD
IICE
LEAD
METIIYLCII
MECL2
NAFTIIALE
NICKEL
2400 dock
Iirs
2400 dock
I firs
Y/BM
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/da
1
0600
12.0
Y
2
1130
24
0600
11.0
Y
3
0600
8.5
Y
4
0600
6.0
Y
5
N
NOFLOW
6
N
NOFLOW
7
0600
10.0
Y
NOFLOW
s
0600
10.5
ly
I NOFLOW
9
0600
9.0
Y
10
1130
24
0600
8.5
Y
11
0600
8.5
Y
12
0700
5.0
Y
13
0815
5.0
Y
14
0600
10.5
Y
15
0600
9.5
ly
16
1130
24
0600
9.5
Y
17
0600
8.0
Y
18
0600
8.0
Y
19
ills
2.0
B
20
1045
2.0
1131
21
0600
9.0
Y
22
1130
24
0630
8.5
Y
23
0630
8.5
Y
24
0600
9.5
Y
25
0600
8.0
Y
NOFLOW
26
1015
2.0
IB
I NOFLOW
27
1045
2.25
B
NOFLOW
28
0630
7.0
B
NOFLOW
29
0630
10.0
Y
NOFLOW
30
0630
8.5
Y
NOFLOW
31
1
0630
9.5
Y
NOFLOW
Monthly Average Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
F
u
yE
U
E
v
F
O
w
C
O
o°
O
°
9
ii
Z
34447
34461
34694
34469
34475
34010
34626
39700
34220
34376
00010
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
26DINITR
liCB
ANTHRACE
FLUORANT
TEMP-C
2400 clock
firs
2400 clock
fin
Y/BIN
Ibs/da
Ibs/da
lbs/da
Ibs/da
Ibs/day
Ibs/da
u
ugfl
u
u
deg c
1
0600
12.0
Y
2
1130
24
0600
ILO
Y
29.6
3
0600
8.5
Y
4
0600
6.0
Y
5
N
NOFLOW
6
N
NOFLOW
7
0600
10.0
Y
NOFLOW
s
0600
110.5
Y
INOFLOW
9
0600
9.0
Y
10
1130
24
0600
8.5
Y
26.6
11
0600
8.5
Y
12
0700
5.0
ly
13
0815
5.0
Y
14
1
0600
10.5
Y
15
0600
9.5
Y
16
1130
24
0600
9.5
Y
28.9
17
0600
8.0
Y
18
0600
8.0
Y
19
1115
2.0
B
20
1045
2.0
ID
21
0600
9.0
Y
22
1130
24
0630
8.5
Y
30.4
23
0630
8.5
Y
24
0600
9.5
Y
25
0600
8.0
Y
NOFLOW
26
1015
2.0
IB
I NOFLOW
27
1045
2.25
B
NOFLOW
28
0630
7.0
B
NOFLOW
29
0630
10.0
Y
NOFLOW
30
0630
8.5
Y
NOFLOW
31
0630
9.5
Y
NOFLOW
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.084
Monthly Average:
28.875
Daily Mnrimum•
1
30.4
Daily Minimum:
26.6
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
a
E
U
g
F
fi
9
F
6
O
0m -
F
O
o°
O
c
a
Z
00300
Grab
DO
2400 clack
Hrs
2400 clock
l{rs
IYIDIN
I Mg/1
0600
12.0
Y
2
1130
24
0600
11.0
Y
5
3
r51
0600
8.5
Y
4
0600
6.0
Y
N
NOFLOW
6
N
NOFLOW
7
0600
10.0
Y
NOFLOW
8
0600
10.5
Y
NOFLOW
9
0600
9.0
Y
10
1130
124
10600
8.5
1 Y
6.4
11
0600
8.5
Y
12
0700
5.0
Y
13
0815
5.0
Y
14
0600
10.5
Y
I5
0600
9.5
16
1130
24
0600
9.5
5.4
17
0600
8.0
rB
18
0600
8.0
19
lilts
2.0
20
1045
2.0
B
21
0600
9.0
Y
22
1130
24
0630
8.5
Y
4.7
23
0630
8.5
Y
24
0600
9.5
Y
25
0600
8.0
Y
NOFLOW
26
1
1015
2.0
B
NOFLOW
27
1045
2.25
B
NOFLOW
28
0630
7.0
B
NOFLOW
29
0630
10.0
Y
NOFLOW
30
0630
8.5
Y
NOFLOW
31
0630
9.5
1 Y
NOFLOW
Monthly Average Limit:
Monthly Average:
5.375
Daily Maximum:
6.4
Daily Mlalmnm:
14.7
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 08-2017 (August 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 09/27/2017
e<2:Z� 09/18/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
09/27/2017
Permitte /S bmitter Signature:*** Eric Johnson E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 08-2017 (August 2017) VERSION: 1.0
Report Comments:
8/22/2017 BOD Difference between sample dilutions is greater than 30%.
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

CERTIFIED MAIL: 7015 0640 0007 8479 2033
Return Receipt to PEM Carter
PEMC17:23
September 28, 2017
NCDEQ
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
rJ-1
Celanese
The chemistry inside innovation"
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerning August 2017. DMR for C N A Holdings LLC.- Shelby Facility.
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the August's report has been submitted through the eDMR
system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
• 8/22/2017: BOD5 difference between sample dilutions is greater than 30%.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(&-celanese.com.
PEM Carter
EHS Lead/Environmental Engineer
Attachments

3
NPUES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 07-2017 (July 2017) VERSION: 1.0
_ �q PERMIT STATUS: Active
"� ICOUNTY: Cleveland
AUG 2 9 2017 ORC CERT NUMBER: PEgMIVFD/NCDENRIDWR
CENTRAL FILES SE P - 5 20'a7
DWR SECTION STATUS: Processed
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCfAq'4:LN`dGIONAL OFFICE
o
-
U
E
-
E
a
9
_
O
O
E
:
O
o
U
O
C
a
z
z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annual)
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pit
aOD -Qty Daily
TSS -Qty Daily
FCOL1 art
TOTAL N-
TOTAL P•Conc
1.1-DCE
lj-DCEV
2400 clack
It,,
2400 elect,
urn
vBm
mgd
I su
Ibs/day
Ibs/day
N/I00ml
mg/I
mg/I
I lbs/day
Ibs/day
1
0600
4.0
Y
0.216
2
0500
3.0
Y
NOFLOW
3
0600
9.0
Y
NOFLOW
4
0830
3.5
Y
0.438
5
0600
9.5
Y
0.399
6
1 1130
124
0600
9.5
1 Y
10.31
8
11.4
18.1
129
7
0600
7.5
Y
0.41
8
1030
1.0
B
0.418
9
N
NOFLOW
10
0630
10.0
Y
I NOFLOW
II
0630
9.0
Y
0.44
12
1130
24
0630
9.0
Y
0.343
8.1
15.7
22.9
10
13
0600
9.0
y
0.313
14
0600
9.0
y
0.256
15
1030
1.0 1
B
0.2
16
0830
4.0
B
NOFLOW
17
0600
11.50
Y
NOFLOW
i8
0630
11.0
Y
NOFLOW
19
0630 1
11.0
Y
NOFLOW
20
0600
9.5 1
Y
NOFLOW
21
0600
8.5
y
NOFLOW
22
N
NOFLOW
23
1430
2.5
Y
NOFLOW
24
0630
9.0
Y
0.316
25
0630
8.5
Y
0.399
26
1130
24
0600
9.5
Y
0.344
7.9
17.5
34.4
16
27
0600
9.5
Y
0.358
28
0600
7.0
y
0.349
29
0930
3.0
B
0.331
30
0930
4.0
B
0.314
31
0600
9.0
Y
0.281
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Nlomhly Average:
0.339684
14.866667
25.133333
16.679102
Duur maximum:
0.44
8.1
17.5 134.4
29
Daily Minimum:
0.2 17.9
1
11.4
18.1 1
10
**** No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPbES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2017 (July 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
E
_
E
U
E
u
_
iW
F
O
O
F
O
o
U
O
L
a
z`
Z
34536
31103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCF-
1,2.DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4.DCPII
2,4-DMP1I
2,4-DNPII
2,4-DNT
2400 clock
ur:
2400 dock
❑rs
Y/B/N
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I Ibs/da
Ibs/day
I Ibs/da
Ibs/day
I Ibs/day
1
0600
4.0
Y
2
0500
3.0
Y
NOFLOW
3
0600
9.0
Y
NOFLOW
4
0830
3.5
1 Y
5
0600
9.5
Y
6
1130
24
0600
9.5
Y
7
0600
7.3
Y
8
1030
1.0
B
9
N
NOFLOW
10
0630
10.0
Y
NOFLOW
11
0630
9.0
Y
12
1130
24
0630
9.0
1 Y
13
0600
9.0
Y
14
0600
9.0
Y
15
1 1030
1.0
B
16
0830
4.0
B
NOFLOW
17
0600
11.50
Y
NOFLOW
i8
0630 111.0
Y
INOFLOW
19
0630
11.0
Y
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
8.5
Y
NOFLOW
22
N
NOFLOW
23
1430
2.5
Y
NOFLOW
34
0630
9.0
Y
25
0630
8.5
Y
26
1130
24
0600
9.5
Y
27
0600
9.5
Y
28
0600
7.0
Y
29
0930
3.0
B
30
0930
4.0
B
31
0600
9.0
Y
Monthly Avcrage Limit:
0.249
0.219
0.494
9.068
0.094
0.1
0.048
0.126
0.05E
0.229
0.365
Monthly Avcragc:
Daily Maximum:
Daily 0IW-m:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR= No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY =No Visitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2017 (July 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
-
E
_
E
E
F-
E
u`
E
-
-
1
y
O
e
2
o
c3
C
ii
i`
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPIIENOL
2NPIIENOL
34-BNZFA
46DN-o-C
4NPIIENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 crock
ure
2400 elect,
It,,
Y/BIN
Ibs/da
Ibs/day
I ug/I
Ibs/day
I Ibs/day
Ib0da
Ibs/day
ug/I
I Ibs/da
ug/I
ug/I
0600
14.0
Y
2
0500
3.0
Y
NOFLOW
3
0600
9.0
Y
NOFLOW
4
0830
3.5
5
0600
9.5
6
1130
24
0600
9.5
7
0600
7.5
8
1030
1.0
hy
9
NOFLOW
10
0630
10.0
NOFLOW
It
0630
9.0
12
1130
24
0630
9.0
Y
13
0600
9.0
Y
14
0600
9.0
Y
I5
1030
1.0
B
16
0830
4.0
B
NOFLOW
17
0600
11.50
Y
NOFLOW
is
0630
11.0
Y
NOFLOW
19
0630
11.0
IY
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
8.5
Y
NOFLOW
22
N
NOFLOW
23
1
1 1430
2.5
Y
NOFLOW
24
0630
9.0
Y
25
0630
8.5
Y
26
1130
24
0600
9.5
Y
27
0600
9.5
Y
28
0600
7.0
Y
29
0930
3.0
B
30
0930
4.0
B
31
0600
9.0
Y
Monthly Average Limit:
0.1
0.132
0.252
0.23E 1
D.D71
0.071
0.119
Nlonthly Average:
Daily Maximum:
Daily Minimum:
**** No Rcporting Reason: ENFRUSE = No Flow-Reusc/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPUES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 07-2017 (July 2017) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
E
I
E
U
-
-
E
a
E-
FE
_
O
-
C
E
O
o
U
x
O
n
1
a
C
C
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Amorally
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BN%O-K-F
ME PRTI1
CARBNTET
CIILROBN'L
CLROETHA
CIILRFORM
Cr-TOTAL
CIIRYSENE
COPPER
CN-TOT
n1ETY-Pn
2400 crock
Ilrs
2400 cl.,k
11rr
Y/B/N
ug/I
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/I
ug/I
ug/I
ug/I
Ibs/da
i
0600
4.0
Y
2
0500
3.0
Y
NOFLOW
3
0600
9.0
Y
NOFLOW
4
0830
3.5
Y
5
0600
9.5
Y
6
1 1130
124
0600
9.5
Y
7
0600
7.5
Y
8
1030
1.0
B
9
N
NOFLOW
10
0630
1 10.0
Y
NOFLOW
11
0630
9.0
Y
12
1 1130
24
0630
9.0
Y
13
0600
9.0
Y
14
0600
9.0
Y
15
1030
1.0
B
16
0830
4.0
1 B
NOFLOW
17
0600
11.50
Y
NOFLOW
18
0630
11.0
Y
NOFLOW
19
0630
11.0
Y
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
8.5
Y
NOFLOW
22
N
NOFLOW
23
1430
2.5
Y
NOFLOW
24
0630
9.0
Y
25
0630
8.5
Y
26
1130
24
0600
9.5
Y
27
10600
9.5
Y
28
0600
7.0
Y
29
0930
3.0
B
30
0930
4.0
B
31
0600
9.0
Y
Monthly A).e pUrnh:
0.332
a.058
0.048
0.336
0.068
3.583
0.261
Monthly A-.ga :
DWI). Nb.imum:
Way Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Rcuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW =No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: WW-2 ,
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 07-2017 (July 2017)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
7
B
f-
-
h-
E
U
E
_
E
5
-_
E
-
-
O
m
O
E
-
O
-
o
U
Z
ce
c
Y
.34341
39110
34.371
34.381
.39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-I'll
DNB PI1T11
ET11YLBEN
FLUORENE
IIECCLBD
IICE
LEAD
METIfYLC11
h1ECL2
NAFri1ALE
NICKEL
2400 dock
Dr,
2400 clock
firs
Y/BIN
Ibs/day
Ibs/day
Ibs/da
Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
Ibs/da
Ibs/day
1
0600
4.0
Y
2
0500
3.0
Y
NOFLOW
3
0600
9.0
Y
NOFLOW
4
0830
3.5
Y
5
0600
9.5
Y
6
1130
24
10600
9.5
ly
7
0600
7.5
Y
8
1030
1.0
B
9
N
NOFLOW
10
0630
10.0
Y
NOFLOW
11
0630
9.0
Y
12
1130
24
0630
9.0
Y
13
0600
9.0
Y
14
0600
9.0
Y
i5
1030
1.0
B
16
0830
4.0
B
NOFLOW
17
0600
11.50
Y
NOFLOW
18
0630 111.0
Y I
NOFLOW
19
0630
11.0
Y
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
8.5
Y
NOFLOW
22
N
NOFLOW
23
1430
2.5
Y
NOFLOW
24
0630
9.0
Y
25
0630
8.5
Y
26
1130
24
0600
9.5
Y
27
0600
9.5
Y
28
0600
7.0
Y
29
0930
3.0
B
J0
0930
4.0
B
31
0600
9.0
Y
Monthly Average Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2017 (July 2017)
PERMIT VERSION: 4.0
Facility CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
E
U
E
E
F
E
p
¢
O
u
E
I-
O
-
o°Z
O
t
z
.34447
34461
34694
34469
34475
34010
34220
34626
39700
34376
00010
Annually
Annually
Annually
Annually
Annually
Annuall
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Calculated
NI'1'ItOeEN
YIIENANTII
PHENOL
PYItENE
'fETCLE7'Y
TOLUENE
AN'rI11L10E
26UIMTIi
IICB
FLUOnAN7'
TEMP-C
2400 clock
❑ra
2400 el.&
urs
YiB/N
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
ug/I
ug/l
ug/1
I ug/I
deg c
1
0600
4.0
Y
2
0500
3.0
Y
NOFLOW
3
0600
9.0
Y
NOFLOW
4
0830
3.5
Y
5
0600
9.5
Y
6
1130
24
0600
9.5
Y
27.8
7
1
10600
7.5
IY
8
1030
1.0
D
9
N
NOFLOW
10
0630
10.0
Y
NOFLOW
11
0630
9.0
Y
12
1130
24
10630
9.0
Y
1
30.3
13
0600
9.0
Y
14
0600
9.0
Y
15
1030
1.0
IB
16
0830
4.0
B
NOFLOW
17
0600
11.50
Y
NOFLOW
18
0630
11.0
Y
NOFLOW
19
0630
11.0'
Y
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
8.5
Y
NOFLOW
22
N
I NOFLOW
23
1430
2.5
Y
NOFLOW
24
0630
9.0
Y
25
0630
8.5
Y
26
1130
24
0600
9.5
Y
30.6
27
0600
9.5
Y
28
0600
7.0
Y
29
0930
3.0
B
J0
0930
4.0
B
31
0600
9.0
Y
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.084
Monthly Average:
29.566667
Daily Masimam:
30.6
Daily Minimum:
27.8
**** No Reporting Reason: ENFRUSE = No Flow-Reusc/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2017 (July 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2
o
F
r
V
F
-
7i
-
�
O
O
-
�
O
o
V
O
5
C
00300
Calculated
DO
2400 clack
Ilrs
2400 clock
I Iln
Y/B/N
Mg/I
1
0600
4.0
Y
2
0500
3.0
Y
NOFLOW
3
0600
9.0
Y
NOFLOW
4
0830
3.5
Y
I
5
0600
9.5
Y
6
1130
1 24
0600
9.5
Y
5.5
7
0600
7.5
Y
A
1030
1.0
1 B
9
N
NOFLOW
10
0630
10.0
Y
I NOFLOW
11
0630
9.0
Y
12
1130
24
0630
9.0
Y
4.8
13
0600
9.0
Y
14
0600
9.0
Y
15
1030
1.0
B
16
0830
4.0
B
NOFLOW
17
0600
11.50
Y
NOFLOW
Is
0630
11.0
Y
NOFLOW
19
0630
1 11.0
Y
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
8.5
Y
NOFLOW
22
N
NOFLOW
23
1430
2.5
Y
NOFLOW
24
0630
9.0
Y
25
0630
8.5
Y
26
1130
24
0600
9.5
Y
5.2
37
0600
9.5
Y
29
0600
7.0
Y
29
0930
3.0
B
30
0930
4.0
B
31
0600
9.0
Y
Monthly Average Limit:
Monthly Average:
5.166667
Daily Masimum:
5.5
Daily h7lnimam:
4.8
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NP15ES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2017 (July 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 08/15/2017
08/ 14/2017
/Certifier Signature: Michael D Sparks. E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became. aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
08/15/2017
Permi/ee/Stibmitter SigVttre:*V Rafael Gonzalez E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelb NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 07-2017 (July 2017)
Report Comments:
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
7/12/17 BOD5, Difference between sample dilutions is greater than 30%. Blank value is outside of the control limits.
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

I.
3
NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2 ' " 6..P- IV ®
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks AUG
I I G 1 201 /
GRADE: WW-3. ORC HAS CHANGED: No V I
eDMR PERIOD: 06-2017 (June 2017) VERSION: 1.0 CENTRAL FILES
DWR SECTION
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
..
a
.5
d
_
_
E
U
-
E
u
F
O
a
E
�
O
_
o`
O
v
x
=
7
50050
004011
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
BOD- cryMily
TSS -Qtv Daily
FCOLIBR
TOTAL N-
TOTAL P - Cone
1,1-DCE
1,1-DCEY
2400 clack
Hrx
2400 clack
Firs
Y/B/N
I mgd
su
I Ibs/day
Ibs/day
41100ml
mg/I
mg/I
Ibs/day
I lbs/day
1
0600
9.50
B
0.186
2
0600
5.0
B
0.154
3
N
NOFLOW
4
N
NOFLOW
5
0600
9.5
Y
NOFLOW
6
0630
8.5
Y
0.381
7
1130
24
0600
9.5
Y
0.407
7.9
30.2
71.3
II
a
0600
8.5
Y
0.387
9
0600
7.0
Y
0.307
10
N
NOFLOW
I
N
NOFLOW
12
0500
10.0
Y
NOFLOW
13
1130
24
0500
10.0
Y
0.322
7.9
17.7
64.5
Il
<0.005
<0.0002
14
0630
S.5
Y
0.382
I5
0600
9.0
Y
0.383
16
0630
7.0
Y
0.365
17
0500
6.0
IY
0.292
18
0500
4.5
Y
NOFLOW
19
0445
10.75
Y
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
9.0
Y
NOFLOW
22
0600
19.0
Y
NOFLOW
23
0600
7.0
Y
NOFLOW
24
N
NOFLOW
25
1600
2.0
Y
NOFLOW
26
0630
12.0
Y
0.219
35
27
1130
24
0630
12.5
Y
0.361
8.1
12.6
31.3
2e
0630
8.5
Y
0.402
29
0600
9.0
Y
0.393
30
0600
8.0
Y
0.288
Monthly Merage Limit:
0.45
68
124
200
0.071
0.052
Monddy Aeerage:
0.326812
20.166667
55.7
16.17898
0
0
Mly Maximum:
0A07
8.1
30.2
71.3
35
0
0
Deny Mhdmum:
0.154
7.9
12.6
131.3
1 11
1
1
0
0
**** No Reporting Reason: ENFRUSE = No Flow-Retise/Recycle; ENVWTHR=No Visitation- Adverse Weather, NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday
RECEIVED/NCDENR/DWR
AUG 2 11 2017
WQROS
MOORESVILLE REGIONAL OFFICE

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: W W-3. ORC HAS CHANGED: No
eDMR PERIOD: 06-2017 (June 2017) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
o
E
1=
E
U
E
-
H
F=
'E
O
O
t-
O
O
a
7
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annuall
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,Z-DCE
1,2-DCP
t-I2DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPII
2,4-DNPH
2,4-DNPII
2,4-DNr
2400 el.ek
Hrx
2400 el.ek
Hre
Y/BN
I Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I lbs/day
Ibs/day
1 Ibs/day
Ibs/day
1 Ibs/day
Ibs/day
1
0600
9.50
B
2
0600
5.0
B
3
N
NOFLOW
4
N
NOFLOW
5
0600
9.5
Y
NOFLOW
6
0630
8.5
Y
7
1130
24
0600
9.5
Y
a
0600
8.5
Y
9
0600
7.0
1 Y
10
N
NOFLOW
11
N
NOFLOW
12
0500
10.0
Y
NOFLOW
13
1 130
24
0500
10.0
Y
I
< 0.0002
< 0.0002
< 0.0003
< 0.0003
< 0.0002
< 0.00014
< 0.00013
< 0.0043
< 0.0059
< 0.0035
< 0.0081
14
0630
8.5
Y
15
0600
9.0
Y
16
0630
7.0
Y
17
0500
6.0
Y
1N
0500
4.5
Y
NOFLOW
19
0445
1 10.75
Y
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
9.0
Y
NOFLOW
22
0600
9.0
Y
NOFLOW
23
0600
7.0
Y
NOFLOW
24
N
NOFLOW
25
1600
2.0
1 Y
NOFLOW
26
0630
12.0
Y
27
1130
24
0630
12.5
Y
28
0630
8.5
Y
29
0600
9.0
Y
30
0600
8.0
Y
Me.thly Average Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0J65
Monthly Average:
0
0
0
0
0
0
0
0
0
0
0
Daily M-1-un:
0
0
0
0
0
0
0
0
0
0
0
Daily Olininmmo
0
10
0
D
10
10
0
0
10
10
0
**** No Reporting Reason: ENFRUSE = No Flow-Retlse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday
RECEIVED/NCDENR/DWR
WQROS
MOORESVILLE REGIONAL OFFICE

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 06-2017 (June 2017) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
E
HAnnually
U
E
E
F
B
P
<
-
O
y
f-
O
o
z
O
L
a
c
Z
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DNo-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 Bork
Hr..
2400 clack
Hn
Y/B/N
Ibs/day
I Ibs/day
ug/I
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/I
Ibs/day
I ug/l
no
1
0600
9.50
B
2
0600
5.0
B
3
N
NOFLOW
4
N
NOFLOW
5
0600
9.5
Y
NOFLOW
6
0630
8.5
Y
7
1130
24
0600
9.5
Y
g
0600
8.5
Y
9
0600
7.0
Y
10
N
NOFLOW
II
N
NOFLOW
12
0500
10.0
Y
NOFLOW
13
1130
24
0500
10.0
Y
<0.0032
<0.0038
<3.6
<0.0051
<0.0046
<0.0064
<0.0064
<0.2
<0.0013
<3.2
<3.7
14
0630
8.5
Y
15
0600
9.0
Y
16
0630
7.0
Y
17
0500 16.0
Y
Is
0500
4.5
Y
NOFLOW
19
0445
10.75
IY I
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
9.0
Y
NOFLOW
22
0600
9.0
Y
NOFLOW
27
0600
7.0
Y
NOFLOW
24
N
NOFLOW
25
1600
2.0 ly
I
NOFLOW
26
0630
12.0
Y
27
1130
24
0630
12.5
Y
28
0630
8.5
Y
29
0600
9.0
Y
30
0600
8.0
Y
Monthly Average I.imit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly A,-agt:
0
0
0
0
0
0
0
0
0
0
0
DAY MaAn um:
0 10
0
0
0
0
0
0
0
0
0
D:dly Mlnlmum:
0
0
0
0 10
10
0 to
0
0
0
* * * * No Reporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW =No Flow; HOLIDAY =No Visitation -Holiday
RECEIVEDINCDENR/DWR
AUli 2017
WQROS
MOORESVILLE REGIONAL OFFICE

C
NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: WW-2
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
GRADE: W W-3.
ORC HAS CHANGED: No
eDMR PERIOD: 06-2017 (June 2017)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
E
=
_
E
U
E
F
E
a
F'
E
F-
O
y
p
e
f
O
_
O
U
O
c
a
C
7
34242
3910n
32102
34301
32106
01034
34320
01042
00720
34336
34341
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
132E PHTH
CARBNTET
CHLROBNZ
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
DIMET-PII
2400 doek
Hrs
2400 dnak
Hre
YIB/N
I
ug/I
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
ugA
ug/1
I ug/I
ugA
I Ibs/day
lbs/day
1
0600
9.50
B
2
0600
5.0
B
3
N
NOFLOW
4
N
NOFLOW
5
0600
9.5
Y
NOFLOW
6
0630
8.5
Y
7
1130
24
0600
9.5
Y
e
0600
8.5
IY
9
0600
7.0
Y
10
N
NOFLOW
n
N
NOFLOW
12
0500
10.0
Y
NOFLOW
13
1 130
24
0500
10.0
Y
< 3.9
< 0.0086
< 0.0003
< 0.0002
< 0.0002
< 0.3
< 3.5
17
< 1
< 0.0064
< 0.0043
14
0630
8.5 IY
15
0600
9.0
Y
16
0630
7.0
Y
17
0500
6.0
Y
18
0500
4.5
Y
NOFLOW
19
0445
10.75
Y
NOFLOW
20
0600
9.5 IY
I
N017LOW
21
0600
9.0
Y
NOFLOW
22
0600
9.0
Y
NOFLOW
23
0600
7.0
Y
NOFLOW
24
N
NOFLOW
t
25
1600
2.0
Y
NOFLOW
26
0630
12.0
Y
27
1130
24
0630
12.5
Y
28
0630
8.5
Y
29
0600
9.0
Y
30
0600
8.0
Y
Monthly Average Limit:
0.332
0.058
0.048
0.068
3.583
0.261
0.061
ntonthly,kv... ge:
O 10
0
O
0
O
0
17
0
0
0
Daily atashnum:
0
0 10
0
0
0
0
17
0
0
0
Daily dllnimum:
0
O
0
0
O
O
0
17
0
0
O
**** No Reporting Reason: ENFRUSE= No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW = No Flow; HOLIDAY =No Visitation -Holiday
RECEIVED/NCDENR/DWR
AUG 2 11 2 017
WQROS
MOORESVILLE REGIONAL OFFICE

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 06-2017 (June 2017) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
E
A
U,
E
t-
g
E
t=
E
F.
t
_
O
_
E
O
1z«
o
U
O
°
s
i
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
34447
Annuall Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DNB PIITFI
ETHYLBEN
FLUORENE
HEXCLBD
LICE
LEAD
METLIYLCH
MECL2
NAPTIIALE
NICKEL
NITROBEN
.
2400clock
firs
2400clock
I firs
Y/BN
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
0600
9.50
B
2
0600
5.0
B
3
N
NOFLOW
4
N
NOFLOW
5
0600
9.5
Y
NOFLOW
6
0630
8.5
Y
7
11130
24
0600
9.5
IY
8
0600
8.5
Y
9
0600
7.0
Y
10
N
NOFLOW
II
N
NOFLOW
12
0500
10.0
Y
NOFLOW
13
1 130
24
0500
10.0
Y
< 0.0094
< 0.0002
< 0.0078
< 0.0056
< 0.004
< 0.0024
< 0.0002
< 0.0002
< 0.0056
< 0.0046
< 0.0038
14
0630
S.5
Y
t5
0600
9.0
Y
16
0630
7.0
Y
17
0500
6.0
Y
18
0500
4.5
Y
NOFLOW
19
0445
10.75
Y
NOFLOW
20
0600
9.5 IY
NOFLOW
21
0600
9.0
Y
NOFLOW
22
0600
9.0
Y
NOFLOW
21
0600
7.0
Y
I NOFLOW
24
N
NOFLOW
25
1600
2.0
Y
NOFLOW
26
0630
12.0
Y
27
1130
24
0630
12.5
Y
28
0630
8.5
Y
29
0600 19.0
Y
30
0600
8.0
Y
Monthly Average Limit:
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
0.087
Monthly A-.ge:
0
0
0
0
0
0
0
0
0 10
0
Daily MiWnoun:
0
0
0
0
0
0
0
0
0
0 1
0
Daily 0lhdmam:
0
0
0
0
0
0
0
0 10
0
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday
RECEIVED/NCDENR/DWR
AOG 2 1 NUP
WQROS
MOORESVILLE REGIONAL OFFICE

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 06-2017 (June 2017) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
a
E
n
U
s
H
=
O
=
O
i
O
C
O
C
Z
00556
TGP311
34461
34694
34469
34475
34010
39700
34626
34376
34220
Quarterly
Q Y
uarlcrl
Q Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
OIL-CRSE
CERI7DPF
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
HCD
26DINITR
FLUORANT
ANTHRACE
2400 dock
His
2400 clock
H.
Y/a/N
I mgA
pass/fail
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
Ibs/day
ug/I
ug/I
I ug/I
ug(I
0600
9.50
I3
2
0600
5.0
B
3
N
NOFLOW
4
N
NOFLOW
5
0600
9.5
Y
NOFLOW
6
0630
8.5
ly
7
1130
24
0600
9.5
Y
8
0600
8.5
Y
9
0600
7.0
Y
10
N
NOFLOW
I1
N
NOFLOW
12
0500
10.0
Y
NOFLOW
13
1130
24
0500
10.0
Y
<5
IPASS
<0.0089
1 <0.0013
<0.0096
<0.0003
<0.0001
<2.5
<3
<3.6
<3.3
14
0630
S.5
Y
15
0600
9.0
Y
16
0630
7.0
Y
17
0500
6.0
ly
18
0500
4.5
Y
NOFLOW
19
0445
10.75
Y
NOFLOW
20
0600
9.5
Y
NOFLOW
21
0600
9.0
Y
NOFLOW
22
0600
9.0
Y
NOFLOW
23
0600
17.0
Y
NOFLOW
24
N
NOFLOW
25
1600
2.0
Y
NOFLOW
26
0630
12.0
Y
27
1130
24
0630
12.5
Y
28
0630
8.5
Y
29
11600
9.0
Y
30
0600
8.0
Y
Monthly A,-ga Lhnil:
0.071
0.045
0.081
0.071
0.084
N1..theyA-rtla"
0
0
0
0
0
0
0
0
0
0
D.Ily Maxlnuun:
0
1
10
0
10
0
10
10
0
0
0
Dolly Alinlmumo
1 0
0
0
0
0
0
0
10
10
0
****NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday
i RECEIVED/NCDENR/DWR
AUG 21 2101
WQROS
MOORESVILLE REGIONAL OFFICE

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: WW-2
OWNER NAME: Cna Holdings LLC
ORC: Micliael D. Sparks
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 06-2017 (June 2017)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
a
"
E
E
E
e
E
Fiz°
't
E
F
_
5
O
-
ce
7
34311
00010
00300
Annually
Grab
Calculated
Calculated
CHLOROET
TENIP-C
DO
24011 clack
Hrs
2400 clock
Firs
YIBN
Ib0day
deg
rag/I
1
0600
9.50
B
2
0600
5.0
B
3
N
NOFLOW
4
N
NOFLOW
s
0600
9.5
Y
NOFLOW
6
0630
8.5
Y
7
1130
24
0600
9.5
Y
20.6
5.7
a
0600
8.5
Y
9
0600
7.0
Y
to
N
NOFLOW
II
N
NOFLOW
12
0500
10.0
Y
NOFLOW
13
1130
24
0500
10.0
Y
<0.0006
27.7
5.8
14
0630
S.5
Y
15
0600
9.0
Y
16
0630
7.0
Y
17
0500
6.0
Y
18
0500
4.5
Y
NOFLOW
19
0445
10.75
Y
NOFLOW
20
10600
9.5
Y
NOFLOW
21
0600
9.0
Y
NOFLOW
22
0600
9.0
1 Y
NOFLOW
23
0600
7.0
Y
NOFLOW
24
N
NOFLOW
25
1
1 1600
2.0
Y
NOFLOW
26
0630
12.0
Y
27
1130
24
0630
12.5
Y
27
6.4
28
0630
8.5
Y
29
0600
9.0
Y
30
0600
8.0
Y
Manlhly Average Limit:
0.336
Ntanthly Average:
0
25.1
5.966667
Daily Mast mnm:
0
27.7
6.4
Dilly Nllnhnum:
0
20.6
15.7
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation -Holiday
RECEIVEDINCDENR/DWR
Aa j (, °r ? P 17
WQROS
MOORESVILLE REGIONAL OFFICE

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 06-2017 (June 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 07/29/2017
07/28/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
07/29/2017
Permittee/SubmitterUgnatur�-.* R5pel GAzallz E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to time best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://pottal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the pennittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).
RECEIVED/NCDENR/DWR
AUG I-it1:i
WQROS
MOORESVILLE REGIONAL OFFICE

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: WW-2
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
GRADE: W W-3.
ORC HAS CHANGED: No
eDMR PERIOD: 06-2017 (June 2017)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
Report Comments:
Below Report Limits (BRL) Resuilts reported as less than (<)
Per Ori Tuvia, NC DEQ - DWQ requested the following comment: the parameter Chloroethane has two parameter codes assigned to it: 34311 and 85811.
RECEIVED/NCDENR/DWR
AUG 2 1 Z017
WQROS
MOORESVILLE REGIONAL OFFICE

CERTIFIED MAIL: 7015 1660 0001 0635 4810
Return Receipt to PEM Carter
PEMC17:18
July 10, 2017
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
3
Celanese
The chemistry inside innovation
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
JUL- 14 2017
CENTRAL FILES
DWR SEOTIOYtECEIVEDINCDENRIDWR
JUL 4 7011
ATTN: Central Files WQROS
MOORESVILLE REGIONAL OFFICE
Reference: Revision Request: Concerning March 2017, DMR for C N A Holdings LLC.- Shelby
Facility, Permit No. NC 0004952
To Whom It May Concern:
Per Ori Tuvia, the following revision was made to the submitted March eDMR:
• NOFLOW for March 19, 20 and 27 was entered on the eDMR.
• Comment reflects the request from Ori Tuvia.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(@celanese.com.
PEM Carter
EHS Lead/Environmental Engineer
Attachments

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 3.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
G
2
e
e`
G
E
s
E
1=
E
O
O
f
O
O°
a
O
n
�
a
ce
,Z',
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semiannually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
Boo -Qty Daay
TSS-Qty Daily
FCOLI BR
TOTAL N-
TOTAL P - Cant
Ll-DCE
LI-DCEY
2400 clock
H.
2400 clock
H.
YBNi
I
mgd Isu
Ibs/day
lbs/day
I #/100ml
mp/l
mg/l
Ibs/day
Ibs/day
1
1130
24
0630
8.50
Y
0.386
7.8
15.5
40.9
10
2
0630
8.50
Y
0.382
3
0630
6.00
Y
0.333
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
ly
NOFLOW
7
1130
24
0630
8.50
Y
0.357
7.8
9.2
36.6
S
0630
8.50
Y
0.367
5
9
0630
8.50
Y
0.337
to
0630
8.50
13
0.295
1t
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
Y
INOFLOW
0630
13.25
Y
0.355
9
15
1130
24
0630
8.00
Y
0.333
7.9
9.4
33
16
ris14
0630
8.50
Y
0.382
17
0630
15.50
Y
0.348
0530
4.00
Y
0.247
19
0500
4.00
Y
I NOFLOW
20
0500
10.5
Y
NOFLOW
21
0630
8.50
Y
0.349
1
11
22
1130
24
0630
9.00
Y
0.367
7.9
10.4
33.4
23
0630
6.00
Y
0.352
24
0630
8.00
Y
0.301
25
N
INOFLOW
26
N
NOFLOW
27
0630
9.00
Y
NOFLOW
28
0630
9.00
Y
0.415
19
29
1130
24
0630
10.5
Y
0.421
7.9
10.9
40.7
30
0630
9.00
Y
0.344
31
10630
8.00
Y
1
0.388
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.35295
11.08
36.92
9.878062
DaayMa:lnmto:
0.421
7.9
15.5
40.9
19
Daily Minimum:
0.247
7.8
9.2
33
5
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 3.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2
G
fi
e
3
F
1.
2
'E
E
O
O
E
c
O
O
z
O
a
z
z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
P-DCPE
1,3-DCB
1,4-DCB
2,4-13CPH
2,4-DMPH
2,4-DNPH
2,4-DNT
2400 clerk
Are
2400e1aek
In.
Y/B/N
I
lbs/day
Ibs/day,
lbs/day
lbs/day
lbs/day I
lbs/day
lbs/day I
lbs/day
lbs/day I
lbs/day
lbs/day
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
8
0630
8.50
Y
9
0630
8.50
Y
10
0630
8.50
B
11
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
15
1130
24
0630
8.00
Y
16
1
0630
8.50
Y
17
0630
5.50
Y
is
0530
4.00
Y
19
0500
4.00
Y
NOFLOW
20
0500
10.5
1 Y
INOFLOW
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
23
0630
6.00
Y
24
0630
8.00
Y
25
N
NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
NOFLOW
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
30
0630
9.00
Y
31
0630
18.00
1 Y
Monthly Average Limit:
0.249
0.219
OA94
0.068
0.094
01
0.048
0.126
0.058
0.229
0.365
112anthly Average:
Daay Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 3.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
O
_
o
U
F
E
y
h
F
O
O=
eO°
v
O
'
U
O
•a°
a
K
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
12CF11ENOL
2NPHENOL
34-BNZFA
46DN-o-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
I BNZO-A-P
2400 clack
Hn
2400 clack
H.
YB/N
Ibs/day
Ibs/day
ug/I
Ibs/day
lbs/day
Ibs/day
Ibs/day
ug/1
Ibs/day
ug/1
ug/I
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
8
0630
18.50
Y
9
0630
8.50
Y
to
0630
8.50
B
11
N
NOFLOW
12
N
NOFLOW
13
10630
11.00
Y
NOFLOW
14
0630
13.25
Y
15
1130
24
0630
8.00
Y
16
1
0630
8.50
Y
17
0630
5.50
Y
18
0530
4.00
Y
19
0500
4.00
ly
NOFLOW
20
0500
10.5
Y
NOFLOW
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
23
0630
16.00
Y
24
0630
8.00
IY
25
N
NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
NOFLOW
28
1
0630
9.00
Y
29
1130
24
0630
10.5
Y
30
0630
9.00
Y
31
0630
18.00
ly
Monthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Mazimum:
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 3.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
o
E
l:
m-
a
U
E
F
a
1-
E
~
z
2
e
O
y
O
E
2"
e
O
o
u
O
i
a
a`
Z
34242
39100
32102
34301
32106
01034
34320
01042
00720
34336
34341
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
82E PHTH
CARBNTET
CHLROBNZ
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
DIMET-PH
2400 clock
H.
2400 clock
Ho
YB/N
ug/1
I lbs/day
lbs/day
lbs/day
I lbs/day
ug/1
ug/1
ug/1 I
ug/1
lbs/day
lbs/day
1
1130
24
0630
8.50
Y
2
0630
8.50
ly
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
8
0630
8.50
Y
9
0630
8.50
Y
10
0630
8.50
B
II
N
NOFLOW
12
1
N
I NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
15
1130
24
0630
8.00
Y
16
0630
8.50
Y
17
0630
5.50
Y
18
0530
4.00
Y
19
0500
4.00
IY
I NOFLOW
20
0500
10.5
Y
NOFLOW
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
23
0630
6.00
Y
24
0630
8.00
Y
25
N
NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
NOFLOW
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
30
0630
9.00
Y
M
0630
8.00
Y
Monthly Average Limit:
0332
0.058
0.048
0.068
3.583
0.261
0.061
Monthly Average:
Daily Maximum:
Daily Minimum:
****No Reporting Reason:ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 3.0
PERMIT STATUS: Actica
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Q
o
E
F
e
U
fi
F-
E
P
O
h
C
d
O
a
O
re
z'
39110
34371
34381
39702
34396
01051
34418
34413
34696
01067
34447
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Amually
Annually
Annually
Gob
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DNB PHTH
ETHYLBEN
FLUOBENE
HE%CLBD
HCE
LEAD
I1fETHYLCH
MECL2
NAPI'HALE
NICKEL
MTROBEN
2400 clack
H.
2400 clock
11.
Y/B/N I
Ibs/day
Ibs/day
Ibs/day I
Ibs/day
lbs/day I
Ibs/day
Ibs/day I
lbs/day
lbs/day 1
Ibs/day
Ibs/day
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
8
0630
8.50
Y
9
0630
8.50
Y
to
0630
8.50
II
it
N
NOFLOW
12
N
NOFLOW
'
13
0630
11.00
Y
NOFLOW
14
0630
113.25
Y
is
1130
24
0630
8.00
Y
16
0630
8.50
Y
17
0630
5.50
Y
18
0530
4.00
Y
19
0500
4.00
Y
NOFLOW
20
1
0500
110.5
Y
I NOFLOW
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
23
0630
6.00
Y
24
0630
8.00
Y
25
N
NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
NOFLOW
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
30
0630
9.00
Y
31
0630
8.00
Y
Monthly Average Limit:
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
0.087
Monthly Average:
Daily Maximum:
Daily \Hnlmum:
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 3.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
yE
c
u
o
6
w
u
O
6
O
vi
o'
c4
O
a
a
,Z'
00556
TGP38
34461
34694
34469
34411
34111
34311
34111
31376
31111
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
OILGRSE
CEAI7DPF
PHENANTH
PHENOL
PYAENE
7ETCLETY
TOLUENE
CHLOAOET
ANTHRACE
FLUORANT
HCB
2400 clock
lira
2400 clock
Ho I
Y/B/N
mg/1
pasa/fail 1
Ibs/day
lbs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day I
u9/1
ug/1 I
ug/l
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
<5
PASS
8
0630
8.50
ly
9
0630
8.50
Y
10
0630
8.50
B
11
N
INOFLOW
12
N
NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
15
1130
24
0630
8.00
Y
16
1
0630
8.50
Y
17
0630
15.50
Y
is
0530
4.00
Y
19
0500
4.00
Y
NOFLOW
20
0500
10.5
Y
NOFLOW
21
0630
8.50
Y
22
1130
24
0630
19.00
Y
23
0630
6.00
Y
24
0630
8.00
Y
25
N
NOFLOW
26
N
NOFLOW
27
0630
19.00
Y
INOFLOW
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
30
0630
9.00
Y
31
0630
8.00
Y
Monthly Average Limit:
0.071
0.048
0.081
0.071
0.084
0336
Monthly Average:
0
Daily Maaimum:
0
Daily Minimum:
0
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT -NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 3.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Q
E
fi
F
6
O
w
E
r
O
O
x
y
Z,
34626
00010
00300
Annually
Grab
Calculated
Calculated
26DINITR
TEMP-C
DO
2400 clock
H.
2400 clack
Hrs
Y"
ug/1
deg c
mg/I
1
1130
24
0630
8.50
Y
14.7
9.1
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
1 Y
12.8
9.5
s
0630
18.50
Y
9
0630
8.50
Y
10
0630
8.50
B
11
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
IS
1130
24
0630
8.00
Y
8.7
10.9
16
0630
8.50
Y
17
0630
5.50
Y
i8
0530
4.00
Y
19
0500
4.00
Y
NOFLOW
20
0500
10.5
Y
NOFLOW
21
0630
8.50
Y
22
1130
24
0630
9.00
1 Y
14.6
8.7
23
0630
6.00
Y
24
0630
8.00
Y
25
N
NOFLOW
26
N
NOFLOW
27
0630
19.00
Y
I NOFLOW
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
18.1
7.3
30
0630
9.00
Y
31
0630
8.00
Y
Monthly Average Limit:
Monthly Average:
13.78
9.1
Daily Maaimum:
18.1
10.9
Daily Minimum:
8.7
7.3
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
IFACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 3.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 07/07/2017
07/07/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:michael.sparks @celanese.corn Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
�,� /� 4 0
07/07/2017
.i*�* Rafao �onzalez E-Mail:[e-mail] Phone #:[phone] Date
Permittel/Submitter Signature
Permittee Address: NC Hwy 198 Shelby NC 28150 /Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings, LLC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Mike Queen
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
Report Comments:
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 3.0 STATUS: Processed
1. BOD for 3/1/2017 Difference between sample dilutions is greater than 30%
2. BOD for 3/7/2017 GGA result is less than the control limit.
Per Ori Tuvia, requested NOFLOW for the 19, 20, 27 which were not identified as such on the March 2017 eDMR.

PreDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
PERMIT STATUS: Active
RECEUNTY: Cleveland
IV C CERT NUMBER: 987732
JUN 2 7 2017
eDMR PERIOD: 05-2017 (May 2017) VERSION: 1.0 CENTRAL ZH 4TATUS: Processed
DWR SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
G
E
F
"
(5
E
E
F=
a
6
-
O
=
E
O
o
O
u
c'
`'
7
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pit
DOD-Qty Dolly
TSS -Qty Dolly
FCOLI RR
TOTAL N-
TOTAL P - Cone
1,1-DCE
1,1-13CEY
2400 clock
Hrs
2400 clock
Hrs
WR/N
mgd
su
lbs/day
lbs/day
#/100ml
Ing/I
mg/I 1
lbs/day
lbs/day
1
0630
9.0
Y
0.339
9
2
1130
24
0630
8.5
Y
0.307
7.8
6.4
14.6
3
0600
9.5
Y
0.275
4
0600
9.5
A
10.219
5
0630
9.0
A
0.237
6
N
NOFLOW
7
1100
3.0
Y
NOFLOW
s
0500
9.5
Y
1
0.277
17
9
1130
24
0630
9.0
Y
0.305
8.1
13.2
30
10
0500
9.0
Y
0.315
11
0600
8.5
Y
0.298
12
0630
9.0
Y
0.293
13
0500
5.0
Y
0.184
14
0500
3.5
Y
NOFLOW
15
0600
9.5
Y
NOFLOW
16
0600
9.5
Y
NOFLOW
17
0600
9.0
Y
NOFLOW
1s
0600
8.5
Y
NOFLOW
19
0600
5.5
Y
NOFLOW
20
N
NOFLOW
21
1600
2.0
1 Y
NOFLOW
22
0630
10.0
Y
0.222
19
23
1130
24
10630
9.0
Y
10.363
R
1 11.8
34.5
24
0630
9.0
Y
0.418
25
0600
8.0
➢
0.386
26
0600
S.0
➢
0.341
27
1030
1.5
B
0.336
28
1030
I.5
B
0.363
29
1000
2.0
B
0.335
30
0600
8.0
B
0.3
1
12
J1
1 1130
24
0600
1 13.5
B
0.237
7.9
8.7
36
Monthly Average Limit:
0.45
68
124
200
9.071
0.052
ntonmly Average:
0.302381
10.025
28.775
13.666477
Dolly mw lmmne
0.418
8.1
13.2
136
19
Daily Nlimumm:
0.184
17.8
16.4
14.6
9
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday
RECENED/NCDENR/DWR
JUL �t
WORDS
MOORESVILLE REGICNAL 0MCE

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2017 (May 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2
E
E
ci
E
F
4
?
_
v,
C
p
c
_
p
n
a
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annual) Y
Annual) Y
AnnuallyAnnual)
Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2•DCB
1,2-DCE
1,2-DCP
t-12DCGY
I,.l-DCPE
1,7-DCB
1,4-DCB
2,4-DCPI{
2,4-DMPN
2,4-DNPH
2,4-D\T
2400.lock
Hrs
240n clock
Hrx
Y/BfN
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
I Ibs/day
0630
9.0
Y
2
1130
24
0630
8.5
Y
3
0600
9.5
Y
4
0600
9.5
➢
5
0630
9.0
B
6
N
NOFLOW
7
1100
3.0
Y
NOFLOW
x
0500
9.5
1'Y
9
1130
24
0630
9.0
Y
10
0500
9.0
Y
11
0600
8.5
Y
12
0630
9.0
Y
13
0500
5.0
Y
14
0500
3.5
Y
11,10FLOW
IS
0600
9.5
Y
NOFLOW
16
0600
9.5
Y
NOFLOW
17
0600
9.0
Y
NOFLOW
I8
0600
8.5
Y
NOFLOW
19
0600
5.5
Y
NOFLOW
20
N
NOFLOW
21
1600
2.0
Y
NOFLOW
22
0630
10.0
Y
23
1130
24
0630
9.0
Y
24
0630
9.0
Y
25
0600
8.0
B
26
0600
S.0
B
27
1030
1.5
B
28
1030
1.5
B
29
1000
2.0
B
30
0600
8.0
B
31
1 1130
24
10600
13.5
B
Monthly Average Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0365
Montidv Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Rcuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2017 (May 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
E
a
U
E
-
E
I-'
9
F.
z
O
v
E
C
O
c
? -
Z.
34586
.34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHEN01,
2NPI2ENOL
34-RNZPA
46DNo-C
4NPHENOL
ACENAPCN
ACENAPYL
ACRYLONI
BENZENE.
BNZO•,\•A
BNZO-A-P
2400 clock
Hrs
2400 clack
H.
I YB/N
Ibs/day
Ibs/day
I ug/I
Ibs/day
1 Ibs/day
Ibs/day
I Ibs/day
ug/I
Ibs/day
ug/I
I ug/I
0630
9.0
Y
2
1130
24
0630
8.5
Y
3
0600
9.5
Y
4
0600
9.5
B
5
0630
9.0
B
6
N
NOFLOW
7
1100
3.0
Y
INOFLOW
a
0500
9.5
Y
9
1130
24
0630
9.0
Y
10
0500
9.0
Y
11
0600
8.5
Y
12
0630
9.0
Y
13
0500
5.0
Y
14
0500
3.5
Y
NOFLOW
Is
0600
9.5
Y
NOFLOW
16
0600
9.5
Y
NOFLOW
17
0600
9.0
Y
NOFLOW
18
0600
8.5
Y
NOFLOW
19
0600
5.5
Y
NOFLOW
20
N
NOFLOW
21
1600
2.0
Y
NOFLOW
22
0630
10.0
ly
23
1130
24
0630
9.0
Y
24
0630
9.0
Y
25
0600
8.0
B
26
0600
8.0
B
27
1030
1.5
B
28
1030
1 1.5
IB
29
1000
2.0
B
30
0600
8.0
B
31
1130
24
10600
13.5
B
Monthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
0fanthly Average:
Daily Maxhnum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2017 (May 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
fi
(:
ti
o
U
E
U
1=
E
F
a
-
O
E
=
O
o
U
cd
O
•�
a
ce
7
34242
39100
32102
34301
32106
01034
34320
01042
00720
34336
34341
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
B2E PHTH
CARBNTET
CHLROBNZ
CHLRFORh1
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
DIMET-PH
2400 clock
Hrs
2400 clock
I firs
Y/B/N
ug/1
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
ug/I
ug/I
ug/I
ug/1
I Ibs/day
Ibs/day
1
0630
9.0
Y
2
1130
24
0630
8.5
Y
3
0600
9.5
Y
4
0600
9.5
B
5
0630
9.0
B
6
N
NOFLOW
7
1100
3.0
Y
NOFLOW
e
0500
9.5
ly
9
1130
24
0630
9.0
Y
1D
0500
9.0
Y
11
0600
8.5
Y
12
0630
9.0
Y
13
0500
5.0
ly
14
0500
3.5
Y
NOFLOW
15
0600
9.5
Y
NOFLOW
16
0600
9.5
Y
NOFLOW
17
0600
9.0
Y
NOFLOW
18
0600
18.5
Y
I NOFLOW
19
0600
5.5
Y
NOFLOW
20
N
NOFLOW
21
1600
2.0
Y
NOFLOW
22
0630
10.0
Y
23
1130
24
0630
9.0
Y
24
0630
9.0
Y
25
0600 18.0
D
26
0600
8.0
B
27
1030
1.5
B
28
1030
1.5
B
29
t000
2.0
B
30
0600
8.0
B
31
11130
124
10600 1
13.5
JB
Monthly Average L1mit:
0332
0.058
0.048
0.068
3.583
0.261
0.061
Monody,\vcre>;c
Dolly M-1-co:
Daily Mininmm:
""" No Reporting Reason: ENFRUSE = No Flow-Rcuse/Recycle; ENV WTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2017 (May 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
E
l-i.
_
E
U
-E
n
F=
E
_
o
-
0
u
o
C
O
a
K
7
39110
34371
34391
39702
34396
01051
34418
34423
34696
01067
34447
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DNB PHTH
ETHYLBEN
FLUORENE
HEaCLBD
HCE
LEAD
METIIYLCH
MECL2
NAPTHALE
NICKEL
NITROBEN
2400 clock
Hrs
2400 c1nck
I Hrs
MIN
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
lbs/day
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
1
0630
9.0
Y
2
1130
24
0630
8.5
Y
3
0600
9.5
Y
4
0600
9.5
B
5
0630
9.0
B
6
N
NOFLOW
7
1100
3.0
Y
NOFLOW
e
0500
9.5
Y
9
1130
24
0630
9.0
Y
10
0500
9.0
Y
11
0600
8.5
Y
12
0630
9.0
IY
13
0500
5.0
Y
14
0500
3.5
Y
NOFLOW
15
0600
9.5
Y
NOFLOW
16
0600
9.5
Y
NOFLOW
17
0600
9.0
Y
NOFLOW
18
0600
8.5
Y
NOFLOW
19
0600
5.5
Y
NOFLOW
20
N
NOFLOW
21
1600
2.0
Y
NOFLOW
22
0630
10.0
Y
23
1130
124
0630
9.0
Y
24
0630
9.0
Y
25
0600
8.0
B
26
0600
8.0
B
27
1030
1.5
B
28
1030
29
1000
2.0
B
0600
8.0
B
L3.Ll
0
24
0600
13.5
B
Monthly Average Limit:
0.097
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.946
0.087
111anthly Average:
Daily Macinmm:
Doily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 05-2017 (May 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
F
r
"'
E
F-
E
E
F
_
4
O
in
O
E`_
1-
d
O
-
o
O
n
7
34461
34694
34469
34475
34010
34311
34220
34376
39700
34626
00010
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Calculated
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
CFILOROET
ANTHRACE
FLUORANT
HCB
26DINITR
TEMP-C
2400 clock
I Firs
2400 clock
H.
Y/B N
I
Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
ug/I
ug/1
ug/I
I ug/l
deg c
1
0630
9.0
Y
2
1130
24
0630
8.5
Y
22.3
3
0600
9.5
Y
4
0600
9.5
B
5
0630
9.0
B
6
N
NOFLOW
7
1100
3.0
Y
NOFLOW
a
0500
19.5
Y
9
1130
24
0630
9.0
Y
20.2
10
0500
9.0
Y
11
1
10600
8.5
ly
12
0630
9.0
Y
13
0500
5.0
Y
14
0500
3.5
Y
NOFLOW
15
0600
9.5
Y
NOFLOW
16
0600
9.5
Y
I NOFLOW
17
0600
9.0
Y
I NOFLOW
18
0600
8.5
Y
NOFLOW
19
0600
5.5
Y
NOFLOW
20
N
NOFLOW
21
1600
2.0
Y
NOFLOW
22
0630
10.0
Y
2..1
1130
24
10630
9.0
IY
1
20
24
0630
9.0
Y
25
0600
8.0
B
26
0600
8.0
B
27
1030
1.5
B
29
1030
1.5
B
29
1000
2.0
B
30
0600
8.0
B
31
1130
124
10600
1 13.5
113
1
1
1
1
26.2
Monthly Average Limit:
0.071
0.048
0.081
0.071
0.084
0.336
61on1111r Avvragc:
22.175
Daily Maximum:
26.2
Daily Minimum:
20
"""" No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2017 (May 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
O
E
2
Uo
E
E
v
o
E
H
P
O
'v,
O
ui
ui
O`
U
C
c
L
is
7
00300
Calculated
DO
24n0 clock
Hrs
2400 clock
Hrs
I YB/NI
I Ing/I
1
0630
9.0
Y
2
1130
24
10630
8.5
Y
6.1
3
0600
9.5
Y
4
0600
9.5
B
5
0630
9.0
B
6
N
NOFLOW
7
1100
3.0
Y
NOFLOW
x
0500
9.5
Y
9
1130
24
0630
9.0
Y
6.6
10
0500
9.0
1 Y
I
0600
8.5
Y
12
0630
9.0
Y
13
0500
5.0
Y
14
0500
3.5
Y
NOFLOW
j5
0600
9.5
Y
NOFLOW
16
0600
9.5
Y
NOFLOW
17
0600
9.0
Y
NOFLOW
1s
0600
8.5
Y
NOFLOW
19
0600
5.5
Y
NOFLOW
2U
N
NOFLOW
21
1600
2.0
Y
NOFLOW
22
0630
10.0
Y
23
1130
24
0630
9.0
Y
6.1
24
0630
9.0
Y
25
0600
9.0
B
20
0600
8.0
1 B
27
1030
1.5
B
28
1030
1.5
B
29
1000
2.0
B
30
0600
8.0
B
31
1130
24
0600
1 13.5
1 B
5.5
Monthly Average Limit:
Monthly Avcragco
6.075
Duily Max(mom:
6.6
Daily \tinlmom:
5.5
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 05-2017 (May 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 06/20/2017
06/19/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the pennittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES
06/20/2017
Permitle/Submitter Signa6re:** afael Gonzalez E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the infonnation, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings, INC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/fonns.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the pennittee, then delegation of the signatory authority trust be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

CERTIFIED MAIL: 7015 0640 0007 8479 2040
Return Receipt to PEM Carter
PEMC17:15
June 21, 2017
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
0 Celanese
The chemistry inside innovation
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerning May 2017, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the May's report has been submitted through the eDMR
system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(cD-celanese.com.
Sincerel ,
PEM Carter
EHS Lead/Environmental Engineer
Attachments

4
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2017 (April 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1_0
RECEIVEERMIT STATUS: Active 3
OUNTY: Cleveland
MAY ?, 2 2017 ORC CERT NUMBER; 987732
RECtIVED/NMENR/DWR
CENTRAL FILLS •y
DWR SECTION STATUS: Processed MAY 3 0 2017
WOROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NOD'SC'LA'PU-'ICEN.9GIONIALOFFIcE
O
F
A
"
c
U
E
Es
5
F-
E
F
A
-
y
E
Fv`-,
C
o
U
O
m
c
a
C
ZZ
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
Boo -Qty Daily
TSS -Qty Daily
FCOLI BR
TOTAL N-
I TOTAL P - Cone
1,1-DCE
1,1-DCEY
2400 clack
Hrs
24nu clock
Hrs
Y/B/N
mgd
so
Ibs/day
Ibs/day
#/100ml
mg/I
mg/l
Ibs/day
Ibs/day
1
0630
4.0
B
0.383
2
0630
2.0
B
NOFLOW
3
0630
11.50
Y
NOFLOW
4
0630
8.0
Y
0.418
22
5
1130
24
0630
8.5
Y
10.358
7.7
9.6
15.5
6
0630
8.0
Y
0.44
7
1
0600
8.5
Y
0.40E
8
1100
2.0
B
0.388
9
1 1100
2.0
1 B
0.339
10
0630
9.0
B
0.282
11
1130
24
0630
8.50
B
10.227
7.9
8.5
5.1
14
12
0630
8.00
B
0.2
13
0630
8.50
0.179
14
0630
4.0
0.146
15
0630
4.0
NOFLOW
16
0630
2.0
F
NOFLOW
17
0630
8.5
NOFLOW
18
0630
1.0
0.261
19
1130
24
0630
9.0 IY
0.309
7.9
7.7
112.4
5
20
0630
8.50
Y
0.311
21
0630
8.0
Y
0.261
22
0800
4.0
Y
0.201
23
0530
4.0
Y
NOFLOW
24
0500
10.0
Y
NOFLOW
25
0500
10.0
Y
0.322
7
26
1130
24
0630
9.0
Y
0.348
8.2
10.4
21.S
27
0630
8.5
Y
0.393
28
0500
7.0
Y
0.389
�9
1100
2.0
B
0.41
3a
0945
2.0
Y 1
0.383
Monthly Average Limit:
0.45
6S
124
200
6.071
0.052
hlonmly Average:
0.319739
19.05
113.7
17.449691
Daily Masimnm:
0.44
8.2
10.4
2I.8
22
Daily pOnimumc
0.146
7.7
7.7
5.1
4
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 04-2017 (April 2017) VERSION: 1.0
i
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001
i
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
NO DISCHARGE*: NO (Continue)
E
H
_
E
E
F
E
+
E
F
-
4
`
in
O
F
C
U
O
c
a
7
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
1-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4.DCPH
2,4-DMPH
2,4-DNPH
2,4-DNT
2400 clock
Hrs
2400 clock
firs
YBiN
Ibs/day
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
Ibs/day
lbs/day
Ibs/day
I Ibs/day
1
0630
4.0
B
2
0630
2.0
➢
NOFLOW
3
0630
11.50
Y
NOFLOW
4
0630
8.0
Y
5
1130
24
0630
8.5
Y
6
0630
8.0
Y
7
0600
8.5
Y
8
1100
2.0
B
9
1100
2.0
B
10
0630
9.0
➢
11
1130
24
0630
8.50
B
12
0630
8.00
B
13
0630
8.50
B
14
0630
4.0
B
i5
0630
4.0
B
NOFLOW
16
0630
2.0
B
NOFLOW
17
0630
8.5
Y
NOFLOW
18
0630
1.0
Y
19
1130
24
10630
9.0
Y
20
0630
8.50
Y
21
0630
8.0
Y
22
0800
4.0
Y
23
0530
4.0
Y
NOFLOW
24
0500
10.0
Y
NOFLOW
25
0500
10.0
Y
26
1130
24
0630
9.0
Y
27
0630
8.5
Y
28
0500
7.0
Y
29
1100
2.0
B
30
0945
2.0
Y
Monthly Average. Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly Average;
Daily Maximum:
Doily MiW--
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2017 (April 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
w
-
"
E
<
E
i-
=
-
UU
c
C
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
AnnuallyAnnually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Annually
Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN,-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
HNZO-A-A
BNZO-A-P
2400 cloak
Hn
2400 clock
Hra
Y/B/N
Ibs/day
Ibs/day
ug/I
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I ug/I
Ibs/day
I ug/I
ugH
1
0630
4.0
B
2
0630
2.0
B
NOFLOW
3
0630
11.50
Y
NOFLOW
4
0630
8.0
Y
5
1130
24
0630
8.5
Y
6
0630
8.0
Y
7
0600
8.5
Y
8
1100
2.0
B
9
1 1100
2.0
B
10
0630
9.0
B
11
1130
24
0630
8.50
B
12
0630
8.00
B
13
0630
8.50
B
14
0630
4.0
B
is
10630
4.0
B
NOFLOW
16
0630
2.0
B
NOFLOW
17
0630
18.5
Y
NOFLOW
is
0630
1.0
Y
19
1130
24
0630
9.0
Y
20
0630
8.50
Y
21
0630
8.0
Y
22
0800
4.0
Y
23
0530 '
4.0
Y
NOFLOW
24
0500
10.0
Y
NOFLOW
25
0500
10.0
Y
26
1130,
24
0630
9.0
Y
27
0630
8.5
Y
28
0500
7.0
Y
29
1100
2.0
B
1
30
0945
2.0
Y
Monthly Average Limit
0.1
0.132
0.752
0.232
0.071
0.071
0.119
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2017 (April 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
fi
A
2
U
-
o
U
F
E
it
_
O
e
O
`
o
C
O
a
1
Z
34242
39100
32102
34301
32106
01034
34320
01042
00720
34336
34341
nnuallY
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
B2E PHTH
CARBNTET
CHLROBNZ
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
DIMET-PH
2400 clock
Hts
2400 clock
Hrs
I Y/BM
ug/l
Ibs/day
Ibs/day
Ibs/day
lbs/day
ug/l
ug/l
ug/l
ug/l
lbs/day
Ibs/day
1
0630
4.0
B
2
0630
2.0
B 1
NOFLOW
3
0630
11.50
Y
NOFLOW
4
0630
8.0
Y
5
1130
24
0630
8.5
Y
6
0630
8.0
Y
7
0600
8.5
Y
A
1100
12.0
B
9
1100
2.0
B
10
0630
9.0
B
11
1130
24
0630
8.50
➢
12
0630
8.00
B
13
0630
8.50
B
14
0630
4.0
B
is
0630
4.0
B
NOFLOW
16
0630
2.0
B
NOFLOW
17
0630
8.5
Y
NOFLOW
is
0630
1.0
Y
19
1130
24
0630
9.0
Y
20
0630
8.50
Y
21
0630
8.0
Y
22
0800
4.0
Y
23
0530
4.0
Y
NOFLOW
24
0500
10.0
Y
NOFLOW
25
0500
10.0
Y
26
1130
24
0630
9.0
Y
27
0630
8.5
Y
29
0500
7.0
Y
29
I100
2.0
B
3U
0945
2.0
Y
Monthly Average limit:
0.332
0.058
0.048
0.068
3.583
0.261
0.061
Monthly Average:
Daily Ma:dmnm:
4
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NCO004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2017 (April 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
-
E
y
y
_
E
E
t-
E
v
^
E
F
_
4
-
C
F
-
'L
O
-
-
o`
U
O
o
a
04
7
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
34447
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DNBPHTH
ETHYLBEN
FLUORENE
HENCLBD
HCE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
NITROBEN
2400 rloek
Hrs
2400 dock
firs
Y/e/N
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
lbs/day
lbs/day
1
0630
4.0
B
2
0630
2.0
B
NOFLOW
3
0630
11.50
Y
NOFLOW
4
0630
8.0
Y
5
1130
24
0630
8.5
Y
6
0630
8.0
Y
7
0600
8.5
Y
8
l l00
2.0
B
9
1
1100
2.0
B
10
0630
9.0
B
11
1130
24
0630
8.50
B
12
0630
8.00
B
13
0630
8.50
B
14
0630
14.0
B
is
0630
4.0
B
NOFLOW
16
0630
2.0
B
NOFLOW
17
0630
8.5
Y
NOFLOW
18
0630
1.0
Y
19
1130
24
10630
9.0
Y
20
0630
8.50
Y
21
0630
8.0
Y
22
0800
4.0
Y
23
0530
14.0
Y
NOFLOW
24
0500
10.0
Y
NOFLOW
25
0500
10.0
Y
26
1130
24
0630
9.0
Y
27
0630
8.5
Y
28
0500
7.0
Y
29
1100
2.0
B
30
0945
2.0
Y
Monthly Average Limit:
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
0.087
Mmuhly Average:
Daily Maximum:
Daily Minimum:
****NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2017 (April 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o
G
E
yE
_
fi
IJ
E
n
1-'
E
O
_
o
F
d
1 C
O
a
C
7
34461
34694
34469
34475
34010
34626
34220
34376
39700
34311
00010
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Calculated
PHENANTH
PHENOL
PYREVE
TETCLETY
TOLUENE
26DINITR
ANTHR.\CE
PLUORANT
HCB
CHLOROET
TEMP-C
2400 clack
Hre
2400 clack
H.
YB/N
Ibs/day
Ibs/day
lbs/day
Ibs/day
lbs/day
ug/I
ug/I
ug/I
u9/1
Ibs/day
deg c
1
0630
4.0
B
2
0630
2.0
B
NOFLOW
3
0630
11.50
Y
NOFLOW
4
0630
18.0
Y
5
1130
24
0630
8.5
Y
17.9
6
0630
8.0
Y
7
0600
8.5
Y
8
1100
2.0
JB
9
1100
2.0
B
10
0630
9.0
B
11
1130
24
0630
8.50
B
18.1
12
0630
8.00
B
13
0630
8.50
B
14
0630
4.0
B
15
0630
4.0
B
NOFLOW
16
0630
2.0
B
NOFLOW
17
0630
8.5
Y
NOFLOW
t8
0630
1.0
ly
19
1130
24
0630
9.0
Y
21.5
2°
0630
8.50
Y
21
0630
8.0
Y
22
0800
4.0
Y
23
0530
4.0
Y
NOFLOW
24
0500
10.0
Y
NOFLOW
25
0500
10.0
Y
26
1130
24
0630
9.0
Y
18.4
27
0630
3.5
Y
28
0500
7.0
Y
29
1100
2.0
B
30
0945
2.0
Y
Monthly Average limit:
0.071
0.048
0.081
0.071
0.084
0.336
Monthly Average:
18.975
Daily Maximnm:
21.5
Daily Minimum:
17.9
"""" No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: W W-2
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 04-2017 (April 2017)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
..
G
E
F
E
_
E
U
F
E
U
'n
F-
E
F
`
O
in
O
_
i
O
9
C
O
C
a
C
Z
00300
Calculated
DO
2400 clock
Hrs
2400 deek
Hrs
Y/BIN
Ing/1
l
0630
4.0
B
2
0630 12.0
B
INOFLOW
3
0630
11.50
Y
NOFLOW
4
0630
8.0
Y
5
1130
24
0630
8.5
Y
6.5
6
0630
8.0
Y
0600
18.5
Y
B
1100
2.0
B
9
1100
2.0
B
10
0630
9.0
B
11
1130
24
0630
8.50
B
6.1
12
0630
8.00
JB
13
0630
8.50
➢
14
0630
4.0
B
t5
0630
4.0
B
NOFLOW
16
0630
2.0
B
NOFLOW
17
0630
8.5
Y
NOFLOW
is
0630
1.0
Y
19
1130
24
0630
9.0
Y
16.1
20
0630
8.50
Y
21
0630
8.0
Y
22
0800
4.0
Y
23
0530
4.0
Y
NOFLOW
24
0500
10.0
Y
NOFLOW
25
0500
10.0
Y
26
1130
24
0630
9.0
ly
7.7
27
0630
8.5
Y
28
0500
7.0
Y
29
1100
2.0
B
30
0945
12.0
Y
Monthly Average Limit:
Monthly Average:
6.6
Daily M-inmm:
7.7
Deily Minimum:
6.1
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2017 (April 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION:.1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 05/17/2017
05/15/2017
z
/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
05/17/2017
Permittel/Submitter SignaTure:**UR4fael Gonzalez E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the infonmation, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings, Inc. -Shelby
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks Mike Queen
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for repotting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2017 (April 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
Report Comments:
4/5/2017 BOD Blank value is outside of control limits. Validity of the data not affected.
4/1 1/2017 BOD Difference between sample dilution is greater than 30%
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

CERTIFIED MAIL: 7015 1660 0001 0635 4520
Return Receipt to PEM Carter
PEMC17:14
May 18,' 2017
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
'v,J Celanese
The chemistry inside innovation""
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerninq April 2017, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the April's report has been submitted through the eDMR
system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
All notes are reflected in the eDMR.
• Site continues to experience low flow with no discharge days.
• BOD5 sample 4/5/17: BOD blank value is outside of control limits. Validity of the data not affected.
• BOD5 sample 4/11/17: BOD difference between sample dilution is greater than 30%.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.cartera-celanese.com.
'Sincere
PEM Carter
EHS Lead/Environmental Engineer
Attachments

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: W W-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 03-2017 (March 2017) VERSION: 1.0
t < "" �' P T STATUS: Active
"
CO TY: Cleveland
IMAY 0 � 2 W iC CERT NUMBER: 987732
CCtNTRAI FILE; REFCEIVED/NCDENR/DWR
DWR SECTIC§WTUS: Processed MAY
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCIAWN, : f ps
t ILLE REGIONAL OFFICE
0
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50050
00400
QD310
Q0530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semiannually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pit
BOD-Qp Daily
TSS-Qty Daily
FCOLI BR
TOTAL N-
TOTAL P -Conc
1,1-DCE
1,1-DCEY
2400 clock
H.
2400 clock
H.
Y!B/N
mgd Isu
Ibs/day
lbs/day
#/100ml
mg/I
mg/l
Ibs/day
I Ibs/day
1
1130
24
0630
8.50
Y
0.386
7.8
15.5
40.9
10
2
0630
8.50
Y
0.382
3
0630
6.00
Y
0.333
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
11130
24
0630
8.50
Y
0.357
7.8
9.2
36.6
8
0630
18.50
Y
0.367
5
9
0630
8.50
Y
0.337
10
0630
8.50
B
0.295
11
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
0.355
9
15
1130
124
0630
8.00
Y
0.333
7.9
9.4
33
16
0630
8.50
Y
0.382
17
0630
5.50
Y
0.348
1S
0530
4.00
Y
0.247
19
0500
4.00
Y
20
0500
10.5
Y
21
0630
18.50
Y
1
0.349
11
22
1130
24
0630
9.00
Y
0.367
7.9
10.4
33.4
23
0630
6.00
Y
0.352
24
0630
8.00
Y
0.301
25
N
NOFLOW
26
N
I NOFLOW
27
0630
9.00
Y
28
0630
9.00
Y
0.415
19
29
1130
24
0630
10.5
Y
0.421
7.9
10.9
40.7
30
0630
9.00
Y
0.344
31
0630
8.00
1 Y
1
0.388
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.35295
11.08
36.92
9.878062
Daily Moos...:
0.421
7.9
15.5
40.9
119
Dany MBn;m.m:
0.247
7.8
9.2
33
1 5
**** No Reporting Reason: ENFRUSE = No Flow-Retlse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Anual)Y
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2.DCP
t-12DCEY
,l-DCPE1,3-DCB
I,J-DCB
2,4-DCP
2,DMPH
,
2,4a -DNT
2400 clock
H.
2400 clock
11.
YB/N
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
lbs/day
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
10630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
8
0630
8.50
Y
9
0630
8.50
Y
10
0630
8.50
B
11
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
ly,
I NOFLOW
14
0630
13.25
Y
15
1130
24
0630
8.00
Y
16
0630
8.50
Y
17
0630
5.50
Y
18
10530
4.00
1 Y
19
0500
4.00
Y
20
0500
10.5.
Y
21
10630
8.50
Y
22
1130
24
0630
9.00
Y
23
10630
6.00
1 Y
24
0630
8.00
Y
25
N
NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
30
0630
9.00
Y
31
0630
8.00
Y
Monthly Average Limit:
0.249
0.2.9
OA94
U.
0.0941
O.1
O.N.
0.126
0.058
0.229
O161
Monthly Average:
Daily Maximum:
Daily 3linimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: N00004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN.-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clack
Hrs
12400 clock
Ilya
IY/B/N
Ibs/day I
Ibs/day
ug/I I
Ibs/day
Ibs/day I
Ibs/day
Ibs/day
ug/I
lbs/day
ug/l
ug/1
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
1 -
0630 19.0
Y
NOFLOW
7
11130
24
0630
8.50
Y
8
0630
8.50
Y
9
0630
8.50
Y
10
0630
8.50
B
11
N
NOFLOW
12
N
I NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
15
1130
24
0630
8.00
Y
16
0630
8.50
Y
17
0630
5.50
Y
18
0530
4.00
Y
19
0500
4.00
Y
20
0500
10.5
Y
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
23
10630
6.00
ly
24
0630
8.00
Y
25
N
NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
28
0630
9.00
Y
29
1130
24
10630
1 10.5
ly
30
0630
9.00
Y
31
0630
8.00
Y
Monthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Maximum:
Daily \llnimum:
****NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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39100
32102
34301
32106
01034
34320
01042
00720
34336
34341
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
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G4RBNTE7
CHLROBNZ
CHLRFOR117
Cr-TOTAL
CfIRYBENE
COPPER
CN-TOT
DIETY-PH
DIME? -PH
2400 clock 111rs
2400 clock
H.
Y!B/N
ug/l
Ibs/day
Ibs/day I
lbs/day
Ibs/day I
ug/1
ug/I I
ug/I
ug/1 I
Ibs/day
lbs/day
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
8
0630
18.50
Y
9
0630
8.50
Y
10
0630
8.50
B
11
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
15
1130
24
0630
8.00
Y
16
0630
8.50
Y
17
0630
5.50
Y
18
0530
4.00
Y
19
0500
4.00
Y
20
0500
10.5
Y
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
23
0630
6.00
Y
24
0630
8.00
Y
25
N
NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
28
1
0630
9.00
Y
29
1130
124
10630
10.5
Y
30
0630
9.00
Y
31
0630
8.00
ly
Mauthly Average Limit:
0.332
0.058
0.048
0.068
3.583
0.261
0.061
Monthly Average:
Daily M.dmum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
9
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o
U
E
fi
u
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9
Q
O
iz
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r
O
o°
a
O
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e
n
94
7
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
34447
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DNBPHTH
ETHYLBEN
FLUORENE
HEXCLBD
IICE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
NITROBEN
2400 clock
H.
2400 clock
IH.
Y/B/N
lbs/day
lbs/day
lbs/day
I lbs/day
lbs/day
lbs/day
lbs/day
I lbs/day
lbs/day
I Ibs/day,
lbs/day
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
8
0630
8.50
Y
9
0630
18.50
Y
10
0630
8.50
B
It
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
is
1130
24
0630
8.00
Y
16
0630
8.50
Y
17
0630
5.50
Y
18
0530
4.00
IY
19
0500
4.00
Y
20
0500
10.5
Y
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
23
1
0630
6.00
Y
24
0630
8.00
Y
25
N
I NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
30
1
0630
9.00
IY
31
0630
8.00
Y
Monthly Average Limit:
0.087
0.103
0.071
0.065
0.069
2.227
0.278
0.129
0.071
12.846
0.087
Monthly Avenge:
Dolly Maximum:
Daily \linimum:
****No Reporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
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_
.cifi
o
15
E
F'
a
Q
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O=
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00556
TGP311
34461
34694
34469
34475
34010
34311
34220
34376
39700
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
OIL-GRSE
CERI7DPF
PHENANTII
PHENOL
PYRENE
TETCLETY
TOLUENE
CHLOROET
ANTHRACE
FLUORANT
HCE
2400 dock
Iirs
2400 clock
Hn
Y/B/N
mg/1
I pass/fail
Ibs/day
I Ibs/day
lbs/day I
Ibs/day
Ibs/day
Ibs/day
u9/1
ugA
ug/l
1
1130
24
0630
8.50
Y
2
0630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
19.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
<5
PASS
8
0630
8.50
Y
9
0630
8.50
Y
to
0630
8.50
B
11
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
15
1130
24
10630
8.00
Y
16
0630
8.50
Y
17
0630
5.50
Y
is
0530
4.00
Y
19
0500
4.00
Y
20
0500
10.5
Y
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
23
0630
6.00
Y
24
0630
8.00
ly
25
N
NOFLOW
26
N
NOFLOW
27
0630
9.00
Y
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
30
10630
19.00
Y
31
0630
8.00
Y
Monthly Average Limit:
0.071
0.048
0.081
0.071
0.084
0.336
Monthly Avenge:
0
Daily Maximum:
0
Daily Minimum:
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
t7
9
U'
E
E
v'
F=
~
6
O
O
F
C
O
o°
O
C`
a
n
Z
34626
00010
00300
Annually
Grab
Calculated
Calculated
26DINITR
TEMPO
DO
2400 clock
H.
2400 clock
H.
Y/M
ug/1
deg c
mg/I
1
1130
24
0630
8.50
Y
14.7
9.1
2
10630
8.50
Y
3
0630
6.00
Y
4
N
NOFLOW
5
N
NOFLOW
6
0630
9.0
Y
NOFLOW
7
1130
24
0630
8.50
Y
12.8
9.5
g
0630
8.50
Y
9
0630
8.50
Y
10
0630
8.50
B
11
N
NOFLOW
12
N
NOFLOW
13
0630
11.00
Y
NOFLOW
14
0630
13.25
Y
15
1130
24
0630
18.00
Y
8.7
10.9
16
0630
8.50
Y
17
0630
5.50
Y
10
0530
4.00
Y
19
0500
4.00
Y
20
0500
10.5
1 Y
21
0630
8.50
Y
22
1130
24
0630
9.00
Y
14.6
8.7
23
0630
6.00
Y
24
0630
8.00
Y
25
N
NOFLOW
26
1
N
NOFLOW
27
0630
9.00
Y
28
0630
9.00
Y
29
1130
24
0630
10.5
Y
18.1
7.3
30
0630
9.00
Y
31
0630
8.00
Y
Monthly Average Limit:
6lonthly.lverage:
1
13.78
9.1
Daily Maximum:
18.1
10.9
Daily Miulmum:
18.7
17.3
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 04/20/2017
04/20/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
04/20/2017
Permittle/Submitter Signat(1�e:***Lkaffae1 Gonzalez E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible forgathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings, LLC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Mike Queen
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.nedenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2017 (March 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: W W-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
Report Comments:
1. BOD for 3/1/2017 Difference between sample dilutions is greater than 30%
2. BOD for 3/7/2017 GGA result is less than the control limit.

M
CERTIFIED MAIL: 7015 1660 0001 0635 4346
Return Receipt to PEM Carter
PEMC17:09 RECEIVED/NCDENRIDWR
March 28, 2017
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
APR 10 2017
WQROS
MOORESVILLE REGIONAL OFFICE
'�J7 Celanese
The chemistry inside innovation'
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
MAR 3 1 2017
CENTRAL FILES
DWR SECTION
Reference: Notes Concerning February 2017, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the February's report has been submitted through the eDMR
system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
All notes are reflected in the eDMR.
• Site continues to experience low flow with no discharge days.
• BOD5 sample 2/8/17: difference between sample dilutions is greater than 30% and GGA result is less
than the control limit.
• BOD5 sample 2/8/17: blank value is outside of the control limits. Validity of the data not'affected.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(&-celanese.com,
in ly,
PEM Carter
EHS Lead/Environmental Engineer
Attachments

I e
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 02-2017 (February 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
c
E
F
v
E
U
E
F
E
F
E
F'
F
<
O
-
y
O
E
r
O
a
O
s
m
a
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
Boo -Qty Daily
TSS -Qty Daily
FCOLI BR
TOTAL N-
TOTAL P -Conc
LI-DCE
I,1-DCEY
2400 clock
Hrs
2400 clock
Hrs
YmN
mgd
su
Ibs/da
Ibs/day
0/100ml
Ing/I
I mg/I
Ibs/day
I Ibs/day
1
0630
8.50
Y
0.254
2
0630
8.50
Y
NOFLOW
3
0630
7.00
Y
NOFLOW
4
N
NOFLOW
5
N
NOFLOW
6
0630
8.50
1 Y
NOFLOW
7
0500
10.0
Y
0.355
7
a
1 1130
24
0630
8.50
Y
0.395
8.3
15.2
40.2
1
1.4
0.07
9
0630
8.50
Y
0.381
10
0630
7.00
y
0.376
11
N
NOFLOW
12
N
NOFLOW
13
0630
8.50
Y
NOFLOW
14
0630
8.50
Y
0.384
1 10
i5
1130
24
0630
8.00
Y
0.387
8.2
21
42.9
16
0630
8.00
Y
0.382
17
0630
7.00
Y
0.279
IS
0500
4.00
1 Y
10.246
19
0700
3.00
Y
NOFLOW
2D
0630
8.50
Y
NOFLOW
21
0630
8.50
Y
NOFLOW
22
0630
9.00
Y
NOFLOW
23
0630
10.00 1
Y
NOFLOW
24
0630
5.50
Y
NOFLOW
25
N
NOFLOW
26
1000
4.0
Y
NOFLOW
27
0500
12.00
Y
0.357
2S
0630
8.00
Y
0.393
,Monthly Average Limit:
0.45
68
124
200
0.071
O.D52
hlnmhly Average'
0.349083
18.1
41.55
8.3666
1.4
0.07
Daily Maximum:
0395
8.3
21
42.9
10
1.4
0.07
Daily nuoimum:
0.246
8.2
15.2
40.2
7
1.4
10.07
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NCO004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 02-2017 (February 2017)
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
..
a
E
HE
r
V
E
12
E
O
p
C
O
o
O
_
a
z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
1-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPII
2,4-DMPH
2,4-DNPII
2,4-DM
2400 clock
Hrs
2400 clock
H.
I VIB/N
Ibs/day
Ibs/day
Ibs/day
Ibs/day
I lbs/day
Ibs/day
I Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
1
0630
8.50
Y
2
0630
8.50
Y
NOFLOW
3
0630
7.00
Y
NOFLOW
4
N
NOFLOW
5
N
NOFLOW
6
0630
8.50
Y
NOFLOW
7
0500
10.0
Y
8 1
1130
24
10630
8.50
Y
9
0630
8.50
Y
10
0630
7.00
y
II
N
NOFLOW
12
N
NOFLOW
13
0630
8.50
Y
NOFLOW
14
0630
8.50
Y
i5
1130
24
0630
8.00
Y
16
0630
8.00
Y
17
0630
7.00
Y
Is
0500
4.00
Y
19
0700
3.00
Y
NOFLOW
20
1
10630
8.50
1 Y
NOFLOW
21
0630
8.50
Y
NOFLOW
22
0630
9.00
Y
NOFLOW
23
0630
10.00
Y
NOFLOW
24
0630
5.50
Y
NOFLOW
25
N
NOFLOW
26
1000
4.0
Y
NOFLOW
27
0500
12.00
Y
28
0630
8.00
Y
Monthly Average Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Monthly Average:
Daily Maximum:
Dnlly Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2017 (February 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2
C
F
E
U
E
F=
H
O
in
O
C
O
K
Z
345116
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annually
Y
Annual) Y
Annual) Y
Annual) Y
AnnuallyAnnual)
Y
Annual) Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-o-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clock
Hrs
2400 clock
11.
Ibs/day
Ibs/da
ug/l
Ibs/day
Ibs/day
Ibs/day
lbs/day
ug/I
Ibs/da
ug/I
ug/10630
8.50
2
0630
8.50
JYIBRN
NOFLOW
3
0630
7.00
NOFLOW
4
N
NOFLOW
5
N
NOFLOW
6
0630
8.50
Y
NOFLOW
7
0500
10.0
Y
a
1130
24
0630
18.50
Y
9
0630
8.50
Y
10
0630
7.00
y
II
N
NOFLOW
12
N
NOFLOW
13
0630
8.50
Y
NOFLOW
14
0630
3.50
Y
I5
1130
24
0630
8.00
Y
16
0630
8.00
Y
17
0630
7.00
Y
I6
0500
4.00
Y
19
0700
3.00
ly
NOFLOW
20
0630
8.50
Y
NOFLOW
21
0630
8.50
Y
NOFLOW
22
0630
9.00
Y
NOFLOW
23
0630
10.00
Y
NOFLOW
24
0630
5.50
Y
NOFLOW
25
N
NOFLOW
26
1000
14.0 IY
NOFLOW
27
0500
12.00
Y
2a
0630
1 8.00
Y
Manthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2017 (February 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
1=
A
12
`
V
E
-
E
E
F
r
O
_
in
C
o
_
_
ue
O
�e _
_
a
i
34242
39100
32102
34301
32106
01034
34320
01042
00720
34336
34341
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grabu
BNZO-K-F
WE PHTH
CARBN-rET
CIILRORNZ
CHLRFORIII
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
DIDIET-PH
2400 dark
Hrs
2400 e1ork
fin
Y/BN
I ug/1
Ibs/day
I Ibs/day
lbs/da
Ibs/day
ugA
I ug/l
ug/I
ug/I
Ibs/day
I Ibs/da
11
0630
18.50
Y
2
0630
8.50
Y
NOFLOW
3
0630
7.00
Y
NOFLOW
4
N
NOFLOW
6
N
NOFLOW
6
0630
8.50
Y
NOFLOW
7
0500
10.0
Y
x
1130
24
10630
8.50
Y
9
0630
8.50
Y
10
0630
7.00
11
N
NOFLOW
12
N
NOFLOW
13
0630
8.50
Y
NOFLOW
14
0630
8.50
Y
I5
1130
24
0630
8.00
Y
16
0630
8.00
Y
17
0630
7.00
Y
18
0500
4.00
Y
19
0700
3.00
Y
NOFLOW
20
0630
8.50
Y
NOFLOW
21
0630
18.50
Y
INOFLOW
22
0630
9.00
Y
NOFLOW
23
0630
10.00
Y
NOFLOW
24
0630
5.50
Y
NOFLOW
25
1
N
NOFLOW
26
1000
4.0
Y
NOFLOW
27
0500
Y
28
0630
FOOO
Y
Monthly Average Limit:
0.332
0.058
0.048
0.068
3.583
0.261
0.061
Monthly Average:
Daily Maximum:
Daily 611nimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2017 (February 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
o'
6
F
yz
o
U
E
E
9
E
F
o
-
in
e
i
1 O
U
O
a
1 Z
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
34447
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DNBPHTH
ETHYLBEN
FLUORENE
IIESCLBD
LICE
LEAD
METIIYLCH
MECL2
NAPTHALE
NICKEL
NITROBEN
2400 clack
firs
2400 clock
firs
Y/B/N
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/da
Ibs/day
Ibs/day
lbs/day
Ibs/day
Ibs/day
1
0630
8.50
Y
2
0630
8.50
Y
NOFLOW
3
0630
7.00
Y
NOFLOW
4
N
NOFLOW
5
N
NOFLOW
6
0630
8.50
Y
NOFLOW
7
0500
10.0
Y
s
1130
24
0630
8.50
ly
9
0630
8.50
Y
10
0630
7.00
y
II
N
NOFLOW
12
N
NOFLOW
13
0630
8.50
Y
NOFLOW
14
0630
18.50
ly
IS
1130
24
0630
3.00
Y
16
0630
8.00
Y
17
0630
7.00
Y
18
0500
4.00
Y
19
0700
3.00
Y
NOFLOW
20
0630
8.50
Y
NOFLOW
21
0630
9.50
Y
NOFLOW
22
0630
9.00
Y
NOFLOW
23
0630
10.00
Y
NOFLOW
24
0630
5.50
Y
NOFLOW
25
N
NOFLOW
26
1000
4.0
Y
NOFLOW
27
0500
12.00
Y
28
0630
3.00
Y
Monthly Average Limit:
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12,846
0.087
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2017 (February 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
S
V
_
E
H
E
C
_
F
C
O
-
7
34461
34694
34469
34475
34010
39700
34311
34220
34376
34626
00010
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Calculated
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
HCa
CHLOROET
,WTHRACE
FLUORANT
26DINITR
TEMP-C
2400 dnek
Hrs
2400 dock
Hre
Y/6/N
Ibs/day
I Ibs/da
Ibs/day
I Ibs/day
Ibs/day
ug/l
I Ibs/day
ug/l
I ug/l
ug/l
deg c
1
0630
8.50
Y
2
0630
8.50
Y
NOFLOW
3
0630
7.00
Y
NOFLOW
4
N
NOFLOW
5
N
NOFLOW
6
0630
8.50
Y
NOFLOW
7
0500
10.0
Y
8
11130
24
10630
8.50
Y
1
11.6
9
0630
8.50
Y
10
0630
7.00
y
I
N
NOFLOW
12
N
NOFLOW
13
1
0630
8.50
Y
NOFLOW
14
0630
3.50
Y
15
1130
24
0630
8.00
Y
12.8
16
0630
8.00
Y
17
0630
7.00
ly
18
0500
4.00
Y
19
0700
3.00
Y
NOFLOW
20
0630
8.50
Y
NOFLOW
21
0630
8.50
Y
NOFLOW
22
0630
9.00
Y
NOFLOW
23
0630
10.00
IY
NOFLOW
24
0630
5.50
Y
NOFLOW
25
N
NOFLOW
26
1000
4.0
Y
NOFLOW
27
11500
12.00
Y
28
0630
8.00
ly
Monthly Average Limit
0.071
0.048
0.081
0.071
0.084
0.336
Monthly Average;
12.2
Daily Maximum:
12.8
Daily Minimum:
11.6
****NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2017 (February 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
C
E
F
E
"
E
U
E
F-
E
r-
6
O
_
-
C
O
o
o
=
i
00300
Calculated
DO
2400 clock
H.
2400 clock
Hrs
YBIN
mg/I
1
0630
8.50
Y
2
0630
8.50
Y
NOFLOW
3
0630
7.00
Y
NOFLOW
4
N
NOFLOW
5
N
NOFLOW
6
0630
8.50
1 Y
NOFLOW
7
0500
10.0
Y
8
1130
24
0630
8.50
Y
10.2
9
0630
8.50
Y
10
0630
7.00
y
11
N
NOFLOW
12
N
NOFLOW
13
0630
8.50
Y
NOFLOW
14
0630
8.50
Y
Is
1130
24
0630
8.00
1 Y
9.6
16
0630
8.00
Y
17
0630
7.00
Y
IX
0500
4.00
Y
19
0700
3.00
Y
NOFLOW
20
0630
8.50
Y
NOFLOW
21
0630
8.50
Y
NOFLOW
22
0630
9.00
Y
NOFLOW
23
0630
10.00
Y
NOFLOW
24
0630
5.50
Y
NOFLOW
25
N
NOFLOW
26
1000
14.0
1 Y
INOFLOW
27
0500
12.00
1 Y
28
0630
8.00
1 Y
Monthly Average Limit:
alonthly Average:
99
Daily Maximum:
10.2
Daily \linlmtun:
9.6
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2017 (February 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 03/24/2017
03/17/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The pennittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any infonnation shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
03/24/2017
Permitte4Submitter Signatu:*** WfVel Gonzalez E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings, LLC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks Mike Queen
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 213
.0506(b)(2)(D).

NPDES•PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2017 (February 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
Report Comments:
Prism Laboratories (Charlotte, N.C.) performed BOD5, Total Nitrogen and Total Phosphorus analysis for the month of February.
BOD5 sample 2/8/17:difference between sample dilutions is greater than 30% and GGA result is less than the control limit.
BOD5 sample 2/8/17: blank value is outside of the control limits. Validitv of the data not affected.

P
L NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2017 (January 2017)
PERMIT STATUS: Active
Ce' EYUNTY: Cleveland
ORC CERT NUMBER: 987732
Cr-_ I NTRAL F'LEESTATUS: Processed RECEIVE[)/NCDENR/CWR
DWR SECl10N Vu,R - g LOi7
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
Ros
MOORPRI t
PERMIT VERSION: 4_0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1_0
io
O
d
O
0u
a
O
0
�
a.
tG'
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501I O =1
a
e
U
E
F
V
[-'
e
F
b
O
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Salty
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLODaily
pit
ROD -Qty Da
TSS-Qty Daily
FCOLI BR
TOTAL N-
TOTALP-Cone
i,l-DCE
1,1-DCEY
2400 clock
H.
2400 clock
11.
Y/B/N
mgd
sit
Ibs/day
Ibs/day
#/100m1
mg/1
mg/1
lbs/day
lbs/day
I
N
NOFLOW
2
N
HOLIDAY
3
Y
NOFLOW
4
Y
0.332
7
5
1130
24
0700
8.0
Y
0.43
8.4
17.6
54.9
6
0700
8.0
Y
OA18
7
0700 18.0
N
NOFLOW
8
0700
8.0
N
NOFLOW
9
0700
8.0
B
NOFLOW
10
0700
8.0
B
NOFLOW
1t
1130
24
0700
8.0
B
0.429
8.1
7.2
29.7
4
12
1
0700
8.0
B
0.431
13
0700
8.0
B
OA49
14
0630
4.0
B
0.366
15
0630
2.0
B
NOFLOW
16
N
HOLIDAY
17
0700
8.0
Y
NOFLOW
I8
0700
8.0
Y
0.406
19
1130
24
10700
8.0
1 Y
0.426
8.2
14.6
43
5
20
0700
8.0
Y
0.405
21
N
NOFLOW
22
0930
3.0
Y
NOFLOW
23
0700
8.0
Y
OA43
24
1130
24
10700
8.0
Y
0.356
8.1
9.8
30
25
0700
8.0
Y
0.378
6
26
0700
8.0
Y
0.376
27
0700
8.0
Y
0.376
28
0830
4.0
Y
0.359
29
0900
3.5
Y
0.373
30
0700
8.0
Y
1
0.329
5
31
1130
24
0700
8.0
Y
1
0.285
8.3
6.4
12.1
Monthly Average Limit:
045
68
l24
200
0.071
0.052
Monthly Average:
0387737
I I.12
33.94
5.304566
Daily Maximum:
1 0.449
8.4
17.6
54.9
7
Daily Minimum:
0.285
8.1
6.4
12.1
4
**-**NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW =No Now, HULtuAY=Novlsiiauon-nonuay
'ICE

`NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: W W-3.
eDMR PERIOD: 01-2017 (January 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NOVisitanOn—riouaay

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2017 (January 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
34586
CY
34591
79531
' 34657
34646
34205
34200
34215
34030
34526
34247
G
d
6
F
u°E
F
a
z
v,
O g
c
U
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPIIENOL
2NPllENOL
34-BNZFA
46DN-o-C4NPnENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
HNZO-A•P
2400 clock
H"
lbs/day
lbs/day
ug/I
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ugll
Ibs/day
ug/1
ug/1
I
n
NOFLOW
2
HOLIDAY
3
Y
NOFLOW
4
Y
5
1130
24
0700
8.0
8.0
Y
Y
6
0700
7
0700
8.0
N
NOFLOW
8
0700
8.0
N
NOFLOW
9
0700
8.0
8.0
B
B
NOFLOW
NOFLOW
t0
0700
11
1130
24
0700
8.0
B
12
0700
8.0
B
13
0700
8.0
B
14
0630
4.0
B
15
0630
2.0
B
NOFLOW
16
N
HOLIDAY
17
0700
8.0
Y
NOFLOW
18
0700
8.0
Y
19
1130
24
0700
8.0
Y
20
0700
8.0
Y
21
N
NOFLOW
22
0930
3.0
Y
NOFLOW
23
0700
8.0
Y
24
1130
24
0700
8.0
Y
25
0700
8.0
Y
26
0700
8.0
Y
27
0700
8.0
Y
28
1
0830
14.0
Y
29
0900
3.5
Y
30
0700
8.0
1Y
31
1130
24
0700
8.0
Y
Monthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Av ge:
Daily Maximum%
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation— Holiday

`NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2017 (January 2017)
PERMIT VERSION: 4.0
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation — AdverseWeather; NOFLOW=No Flow; HOLIDAY =No Visitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2017 (January 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Monthly Average Limit:
�■,®�■�
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2017 (January'2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
34461
m
a`
Z
34694
34469
34475
34010
39700
34311
34220
34376
34626
00010
p
U
u
S
Z
O
O
Q
O
s
u
O
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Calculated
PIIENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
IICB
CRLOROLT
MTDRACE
FLUORAMr
26DIhTTR
TEMP-C
2400 clock
On
2400 clock
If.
YB/N
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/l
Ibs/day
U911
ug[l
ugll
deg c
1
N
NOFLOW
2
N
HOLIDAY
3
Y
NOFLOW
4
Y
5
1130
24
0700
0700
9.0
8.0
Y
Y
8
6
7
0700
8.0
N
NOFLOW
8
0700
8.0
N
NOFLOW
9
0700
8.0
B
NOFLOW
10
0700
8.0
B
NOFLOW
it
1130
24
0700
8.0
B
4.3
12
0700
8.0
B
13
0700
8.0
B
14
0630
4.0
B
is
0630
2.0
B
NOFLOW
16
N
HOLIDAY
17
0700
18.0
Y
NOFLOW
18
0700
8.0
Y
19
1 1130
24
0700
8.O
Y
11.4
20
0700
8.0
Y
211
N
NOFLOW
22
0930
3.0
Y
NOFLOW
23
0700
8.0
Y
24
1130
24
0700
8.0
Y
12.1
25
0700
Y
26
0700
Y
27
0700
[8.0
Y
28
0830
Y
29
0900
3.5
ly
30
0700
8.0
Y
31
1130
24
0700
8.0
Y
8
Monthly Average Limit:
0.071
0.048
0.081
0.071
0.084
0J36
Monthly Average:
8.76
Daily Maximum:
12.1
Daily Minimum:
4.3
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation -Holiday

AIPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2017 (January 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
a
6
8
U
6
E
u°
E
Z
V
O
F
g
O
y
p°
U
O
00300
K
a
'
9g
2
Calculated
DO
2409 clock
lira
2400 clock
nrs
YAMN
1119/1
1
N
NOFLOW
2
N
HOLIDAY
3
Y
NOFLOW
4
Y
5
1130
24
0700
8.0
Y
Y
11.5
6
0700
8.0
7
0700
8.0
N
NOFLOW
e
0700
B.0
N
NOFLOW
9
0700
8.0
B
NOFLOW
10
0700
8.0
B
NOFLOW
It
1130
24
0700
8.0
B
13.1
12
0700
8.0
B
13
0700
8.0
B
14
0630
4.0
B
15
0630
2.0
B
NOFLOW
16
N
HOLB)AY
17
0700
8.0
Y
NOFLOW
IR
0700
8.0
Y
19
1130
24
0700
8.0
Y
10.4
20
0700
8.0
Y
21
N
NOFLOW
22
0930
3.0
Y
NOFLOW
23
0700
8.0
Y
24
1130
24
0700
8.0
Y
10
25
0700
8.0
Y
26
0700
8.0
Y
27
0700
8.0
Y
2a
0830
4.0
Y
z9
0900
3.5
Y
30
0700
8.0
Y
31
1130
24
0700
1860
1Y
i
11.2
Monthly Avenge Limit:
Monthly Average:
11.24
Daily M.1comn:
13.1
tinily Miaimom:
10
**** No Reporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW =No Flow; kiuL uAr =No visitauun

1'
1VPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2017 (January 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 02/16/2017
1 02/16/2017
ORC/Certifier Signature: �Michael iD Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
02/16/2017
Permitt a/Submitter Signa re:*** of Gonzalez E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Mike Queen
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.nedenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

' APDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2017 (January 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
Report Comments:
1. Prism Laboratories (Charlotte, N.C.) performed BOD5 analysis for the month of January.
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 997732
STATUS: Processed
2. BOD5 sample 1/5/17: difference between sample dilutions is greater than 30%, should not impact the validity of the test results.
3.BOD5 sample 1/19/17: GGA for this analytical batch was outside the method defined established acceptance limit.

CERTIFIED MAIL: 7015 0640 0005 2820 0985
Return Receipt to PEM Carter
PEMC17:07
February 17, 2017
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
Celanese
The chemistry inside innovation`"
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerning January 2017, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the December's report has been submitted through the
eDMR system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
All notes are reflected in the eDMR.
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
'free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carterCacelanese.com.
Sincerely,
PEM Carter
EHS Lead/Environmental Engineer
Attachments

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
PERMIT STATUS: Active
I� IfCOUNTY: Cleveland
p� ORC CERT NUMBER: 987732
JAN 3 1 2017 RECEIVED/NCDENR/DWR
eDMR PERIOD: 12-2016 (Decernber 2016) VERSION: 1.0 CEN PA,L FILES STATUS: Processed FCB
DWIR SZE 6 2011
CTIO�
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NONQROS
OORESVILLE REGIONAL OFFIC
o
G
E
'+
A
E
U
E
r
E
u
a
F
E
<
n
O
%
e
F
O
o
U
O
Z
a
C
G
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annual)
Semi-annually
Annually
Annual)
Recorder
Crab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
P11
BOD-Qty Daily
TSS -Qty Daily
FCOLI BR
TOTAL N-
TOTAL P - Cant
1,1-DCE
I,[-DCEY
2400 clack
❑rs
2400 clock I
Firs
YBIN I
mgd I
su
Ibs/da
Ibs/day
#/100m1
mg/1 I
mg/1
Ibs/day 1
Ibs/day
1
0700
8.00
Y
NOFLOW
2
0700
8.00
Y
NOFLOW
3
N
NOFLOW
4
1530
2.5
Y
NOFLOW
5
0700
8.0
Y
0.331
6
1130
24 10700
8.0
Y
1
0.448
7.1
19.1
30.3
17
7
0700
8.0
Y
0.367
8
0700
8.0
Y
0.395
9
0700
8.0
Y
0.448
to
0900
3.0
B
0.396
11
0845
3.0
B
0.344
12
0700
8.0
Y
0.321
13
1130
24
0700
8.0
Y
0.278
8.3
7.2
11.6
5
14
0700
8.0
Y
0.236
15
0700
8.0
Y
1
0.206
16
0700
8.0
Y
0.185
17
N
NOFLOW
18
N
NOFLOW
19
0700
8.0
Y
NOFLOW
20
0700
8.0
Y
0.337
3
21
1130
124
0700
8.0
1 Y
0.34
8.2
7.9
1 16.4
22
0700
8.0
Y
0.304
23
0900
3.0
Y
0.252
24
0900
3.0
Y
0.194
25
1715
2.0
Y
NOFLOW
26
0700
2.0
Y
NOFLOW
27
0700
8.0
Y
NOFLOW
28
0700
8.0
Y
NOFLOW
29
0700
8.0
Y
NOFLOW
30
0700
8.0
Y
NOFLOW
31
N
NOFLOW
Monthly Average Limit:
0.45
8
124
200
0.071
0.052
Monthly A -rage:
0.316588
17.2
1.4
19.433333
6.341326
Daily Maxtmmn:
0.448
8.3
9.1
30.3
17
Daily Minimum:
0.185
7.1
11.6
3
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2016 (December 2016)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
13
i
E
(5
E
F
-
.E
(5
F
-
<
-
O
in
p
-
O
O
UU
O
n
&
C
2
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Amorally
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
I,2-DCB
1,2.DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPII
2,4.DMPII
2,4-DNPII
2,4-DNT
2400 clock
Ilrs
2400 clack
llrs
YB/N
Ibs/day I
Ibs/day
Ibs/day I
Ibs/day
Ibs/day
Ibs/day I
Ibs/day
Ibs/day
Ibs/day
Ibs/day 1
Ibs/day
1
0700
8.00
Y
NOFLOW
2
0700
8.00
Y
NOFLOW
3
N
NOFLOW
4
1530
2.5
Y
NOFLOW
5
0700
8.0
Y
6
1130
24
0700
9.0 1
Y
7
0700
8.0
Y
8
0700
8.0
Y
9
0700
8.0
Y
t0
0900
3.0
B
11
0845
3.0
B
12
0700
8.0
Y
13
1130
24
0700
18.0
Y
14
0700
8.0
Y
Is
0700
8.0
Y
16
0700
8.0
Y
17
N
NOFLOW
is
N
NOFLOW
19
0700
8.0
Y
NOFLOW
20
0700
9.0
Y
21
1130
24
0700
8.0
Y
22
0700
8.0
Y
23
0900
3.0
Y
24
0900
3.0
Y
25
1715
2.0
Y
NOFLOW
26
0700
2.0
Y
I NOFLOW
27
0700
8.0
Y
NOFLOW
28
0700
8.0
Y
NOFLOW
29
0700
8.0
Y
NOFLOW
30
0700
8.0
Y
NOFLOW
31
N
NOFLOW
Monthly Aremgc Limit:
1.249
0.219
0.494
0.068
0.094
0.1
0.048
O.t26
0.058
0.229
0.365
Monthly Averagc:
Doily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2016 (December 2016)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
v
o 1
E
F
_
c
U
E
o
u
g
9 1
E
H
O
v
O
`e
O 1
o
C
O 1
n
2
&
C
Z
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Armlially
Annually
Aninually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPIIF.NOL
2NPIIENOL
34-BNZFA
46DN-o-C
4NPIIEN0L
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clock
fire
2400 clock
art
Y/B/N
Ibs/day
Ibs/da
118/I
Ibs/da
Ibs/day
Ibs/day
Ibs/da
u I
Ibs/da
ug/I
u 1
1
0700
8.00
NOFLOW
2
0700
8.00
NOFLOW
3
rN
NOFLOW
4
1530
2.5
NOFLOW
5
0700
8.0
6
1130
24
0700
8.0
Y
7
0700
8.0
Y
8
0700
8.0
Y
9
0700
8.0
Y
10
0900 13.0
D
11
0845
3.0
B
12
0700
8.0
Y
13
1130
24
0700
8.0
Y
14
0700
8.0
Y
15
1
0700
8.0
Y
16
0700
8.0
Y
17
N
NOFLOW
1s
N
NOFLOW
19
0700
8.0
Y
NOFLOW
20
0700
8.0
Y
21
1130
24
0700
8.0
Y
22
0700
8.0
Y
23
0900
3.0
Y
24
0900
3.0
Y
25
1715
2.0
Y
NOFLOW
26
0700
2.0
Y
NOFLOW
27
0700
8.0
Y
I NOFLOW
28
0700
9.0
Y
NOFLOW
29
0700
8.0
Y
NOFLOW
30
0700
8.0
Y
NOFLOW
31
N
NOFLOW
Monthly Avenge Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Avenge:
Daily Mnaimom:
Doily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2016 (December 2016)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
E
_
c
U
E
-
u
F
E
_
0
O
_
v
0
E
e
O
_
o
z
O
t
o
c`
z`
34242
39100
32102
34301
32106
01034
34320
01042
00720
34336
34341
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
112E P11TH
CARBNTET
CHLROBNZ.
CRLRFORM
Cr-TOTAL
CNRYSENE
COPPER
CN-TOT
DIETY-PH
DIMET-PII
2400 clack
Rrs
2400 cloak 1
Rrs
Y/B/n
ug/I
Ibs/day
Ibs/day 1
Ibs/day
Ibs/day I
ug/I
ugll I
ug/1
u I I
Ibs/day
Ibs/day
1
0700
8.00
Y
NOFLOW
2
0700
8.00
Y
NOFLOW
3
N
NOFLOW
4
1530
2.5
Y
NOFLOW
5
0700
8.0
Y
6
1130
24
0700
8.0
Y
7
0700
8.0
Y
8
0700
8.0
Y
9
0700
8.0
Y
10
0900
3.0
B
11
0845
3.0
B
12
0700
8.0
Y
13
1130
24
0700
8.0
Y
14
0700
8.0
Y
t5
0700
8.0
Y
16
0700
8.0
Y
17
N
NOFLOW
Is
N
NOFLOW
19
0700
8.0
Y
NOFLOW
20
0700
18.0
Y
21
1130
24
0700
8.0
Y
22
0700
8.0
Y
23
0900
3.0
Y
24
0900
3.0
Y
25
I715
2.0
Y
NOFLOW
26
0700
2.0
Y
NOFLOW
27
0700
8.0
Y
NOFLOW
28
0700
8.0
Y
NOFLOW
29
0700
8.0
Y
NOFLOW
30
0700
8.0
Y
NOFLOW
31
N
I NOFLOW
Monthly Average Limit:
0.332
0.058
0.048
0.068
3.583
0.261
0.061
Monthly Average:
Daily Maximum:
Daily Minimum:
****NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2016 (December 2016)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
O
E
A
U
E
u°
a
F
E
'E
O
H
f7
E
O
o
U
O
n
Se
z`
z
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
34447
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DNB PIITII
ETIIYLBEN
FLUORENE
IIEXCLBD
DCE
LEAD
METIIYLCII
MECL2
NAPTIIALE
NICKEL
NITROBEN
2400 clock
firs
2400 clock
lirs
Y/BIN
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/da
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
1
0700 18.00
Y I
NOFLOW
2
0700
8.00
Y
NOFLOW
3
N
NOFLOW
4
1530
2.5
Y
NOFLOW
5
0700
8.0
Y
6
1130
24
0700
8.0
Y
7
0700
9.0
Y
8
0700
8.0 1
Y
9
0700
8.0
Y
10
0900
3.0
B
11
0845
3.0
B
12
0700
8.0
Y
13
1130
24
0700
8.0
Y
14
0700
8.0
Y
15
0700
8.0
Y
16
0700
8.0
Y
17
N
NOFLOW
Is
N
NOFLOW
19
0700
8.0
Y
NOFLOW
20
0700
9.0
Y
21
1130
24
0700
8.0
Y
22
0700
8.0
Y
23
0900
3.0
Y
24
0900
3.0
Y
25
1715
2.0
Y
NOFLOW
26
0700
2.0
Y
NOFLOW
27
0700
8.0
Y
NOFLOW
28
0700
8.0
Y
NOFLOW
29
0700
8.0
Y
NOFLOW
30
0700
8.0
Y
NOFLOW
31
N
NOFLOW
Monthly Average Limit:
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
0.087
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2016 (December 2016)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
E
E
E
U
E
a
F
e
P
O
-
v
o
in
C
O
a`
a
C
Z
00556
TGI'3B
34461
34694
34469
34475
34010
34220
34311
34626
39700
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Atmuall
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
OIL-GRSE
CERIMPF
IIIIENAN711
PHENOL
PYRENE
TETCLETY
TOLUENE I
ANTHRACE
CHLOROET
26DINITR
HCB
2400 doek
Ilrs
2400 daeh
Mrs
Y/B/N
mg/1
pass/fail
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/1
Ibs/day
ug/1
ug/1
1
0700
8.00
Y
NOFLOW
2
0700
8.00
Y
NOFLOW
3
N
NOFLOW
4
1530
2.5 IY
NOFLOW
5
0700
8.0
Y
6
1130
24
0700
8.0
Y
<5
PASS
7
0700
8.0
Y
8
0700
8.0
Y
9
0700 18.0
Y
10
0900
3.0
B
11
0845
3.0
B
12
0700
8.0
Y
13
1130
24
0700
8.0
Y
14
1
0700
9.0
IY
15
0700
8.0
Y
16
0700
8.0
Y
17
N
NOFLOW
18
N
NOFLOW
19
1
0700
8.0
Y
NOFLOW
20
0700
8.0
Y
21
1130
24
0700
18.0
IY
22
0700
8.0
Y
23
0900
3.0
Y
z4
0900
3.0
Y
25
1715
2.0
Y
NOFLOW
26
0700
2.0
Y
NOFLOW
27
0700
8.0
Y
NOFLOW
28
0700
8.0
Y
NOFLOW
29
0700
8.0
Y
NOFLOW
30
0700
8.0
Y
NOFLOW
31
N
I NOFLOW
Monthly Average Lfmit:
0.071
0.048
0.081
0.071
0.084
0.336
Monthly Average:
0
Daily Masimum:
0
Daily 31inimum:
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2016 (December 2016)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
E
-
_
U
9
l-
u
f-
E
F
i
O
=
O
O
o
O
C
r
°
C.
34376
00010
00300
THP311
AMDa11
Grab
Calculated
Calculated
Calculated
FLUORANT
TEMP-C
DO
CER7DCIIV
2400 clock
Ilrs
2400 clock I
llrs
Y/a/N
ug/I
deg c
mg/I
percent
1
0700
8.00
Y
NOFLOW
2
0700
8.00
Y
NOFLOW
3
N
NOFLOW
4
1530
2.5
Y
NOFLOW
5
0700 18.0
Y
6
1130
24
0700
8.0
Y
Il
10.8
7
0700
8.0
Y
8
0700
8.0
Y
9
0700
8.0
Y
10
0900
3.0
B
11
1
0845
3.0
D
12
0700
8.0
Y
13
1130
24
0700
8.0
Y
7.8
11.5
14
0700
8.0
Y
15
0700
8.0
Y
16
0700
8.0
Y
17
N
NOFLOW
1s
N
NOFLOW
19
0700
18.0
Y
NOFLOW
20
0700
8.0
Y
21
1130
24
0700
8.0
Y
5.8
12.2
22
0700
8.0
Y
23
0900
3.0
Y
24
0900
3.0
Y
25
1715
12.0
Y
NOFLOW
26
0700
2.0
Y
NOFLOW
27
0700
8.0
Y
NOFLOW
28
1
0700
8.0
Y
NOFLOW
29
0700
8.0
Y
NOFLOW
30
0700
18.0
Y
NOFLOW
31
N
NOFLOW
Monthly Average Limit:
Monthly Average.
9.2
11.5
Daily Maximum:
11
12.2
Daily Minimum:
5.8
110,8
****NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2016 (December 2016)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 01/25/2017
cf* 01/23/2017
ORC/Certifier Signature: Michael D Sparks E-Mail: [e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
01/25/2017
Permitge/Submitter Signature:** qAa'el Gonzalez E-Mail:[e-mail] Phone #:[phone] Date
Penn ittee Address: NC Hwy 198 Slielby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings, LLC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Mike Queen
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting littp://portal.nedenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Pennittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2 COUNTY: Cleveland
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks ORC CERT NUMBER: 987732
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 12-2016 (December 2016) VERSION: 1.0 STATUS: Processed
Report Comments:
BOD5: 12/6/2016 sample was difference between sample dilutions is greater than 30%. Results matches historical results.
BOD5: 12/13/2016 sample performed 1.5 hours outside of holding time. Called Roberta Scheller, NCDEQ - DAQ, to discuss compliance status with this out -of -hold condition
Guidance: compliance box should be checked and notes of this entered on eDMR report. Summary of letter from Prism Laboratory: " There was an oversight made by the lab
analyst. This resulted in the analysis being performed approximately 1.5 hours passed the 48-hour hold time. Because the hold time was only exceeded by approximately 1.5
hours, and the fact that the result (3.1 mg/l) matches historical data, we feel confident that the value is a valid number. "

EFFLUENT
3
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH I NnVPmhPr__J YEAR. 2016
FACILITY NAME CNA Holdings,Inc. - Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdings,Inc. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE= 704-480-5793
CHECK BOX IF ORC HAS CHANGED ® NO FLOW / DISCHARGE FROM SITE
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES x '�ECt I�/ �/` a11=. JOi�I�
DMSION OF WATER QUALITY (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS J A N 3 .2 017
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
0
50050
00010
1 00400
50060
00310
00610
00530
31616
1 00300
00600
00665 00665
TGPJ$`1fO
' 2
E
CL
°1
N
�
O
O
EFFFQ
w
tn
F
Q �
W
La
o
m
Z-cc
�
Z~
O
Q
W
1
O
to
0
U t
LL ONO
WZ
VO
U)
X�
O
Q�
0 It
F-Z
to 1%
a =
O
IL
O, E
ya
s
a°�O
iVILLE
O�
��
EC2 Di
IL
a>0
OC
�
O
AL OFF
MF
o
pU
iV
nfection
HRS
HRS
Y/B/N
MGD
° C
UNITS
UG/L
LB/DAY
MG/L
LB/DAY
#/100ML
MG/L
MG/L
MG/L
MG/L
P/F
UG/L
11
7:00
8.00
`'y
no flow
2
7:00
8.00
Y
no flow
17700
8.00
Y
no flow.
EU..
4
7:00
8.00
Y
no flow
5
6:30
3:00
X
no.flow
_ . .
6
10:00
3.00
Y
no flow
7
'. 7:00
8.00
Y
0.3780
12
L
F(-
8
7:00
8.00
Y
0.4030
15.9
8.5
8.7
32.9
9.0
9
7:00
8.00
Y
0.3680
10
7:00
" 8.00
Y
0.3310
11
7:00
8.001
Y
0.2600
12"
N'
no flow
13
7:30
4.50
Y
no flow
'
14
- `'7:00
8.00
Y
0.2690
7
15
7i00
8.00
Y
0.2600'
11.9
8.1
5.6
11.1
9.9
I L
16
"7:00
:8:00,
Y,.
0.2090
17
7:00
..;8.00
Y
0.1700
18
7:00
8.00
Y
0.1360
191
N'
no flow
20
N
no flow
21
7:00
.8.00
B1Y
no flow
22
7:00
8.00
B/y
no flow
23
:7:00
8.00
B/Y'
no flow,,
24
H
no flow
251,
6:30
<:3.50
H/B
no flow
.
26
N
no flow
27
.'
N
no flow
28
7:00
8.00
Y
no flow
29
7:00
8.00
Y
no flow
30
'.7:00
.,8:00
Y' '-
0.0000
AVERAGE
0.2531
13.9
7.2
22.0
9.17
9.5
- MAXIMUM
0.4030 .
15.9
8.5
.
8.7
32.9
12
9.9
-
m"
MINIMUM
0.0000
11.9
8.1
5.6
11.1
7
9.0
Comp. (C) / crab (G)
G
G
C
C
G .,
G-
C
C
G
C
C,.
Monthly Limit
0.450
6.0-9.0
68.0
124.0
200
Cd4
DWQ Form MR-1 7/12

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) Fv I
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part H.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
,,-Rjrai 1D,-, !
.� _ ) zo 6
Signature of Permittee*** e
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzalez(c�celanese.com 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,Inc. Certification No.
Certified Laboratory (3) ETT Labs Certification No.
Certified Laboratory (4)
Certified Laboratory (5)
PARAMETER CODES
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.ncdenr.org/web/wq/swp/ps/npdes/appforms.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
402
22

pppppp,
EFFLUENT 3
.... ..............
_ _.
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH 0cothPr I YEAR 2016
_........:
FACILITY NAME CNA Holdines,Inc. - Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdings,Inc. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (OR, Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704-480-5793
CHECK BOX IF ORC HAS CHANGED Q NO FLOW / DISCHARGE FROM SITE * 0
Mail ORIGINAL and ONE COPY to: /
CEIVE-D/�ICDERR/DWR
ATTN: CENTRAL FILES x �w,� / 1/1%.S/zo 110
DIVISION OF WATER QUALITY (SIGNATURE OF OPERA701t`IN RESPONSIBLE CHARGE) U t L llA I,E L U
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
vVOR3S
N
50050 1
00010
00400
50060
00310
00610
00530
31G1G
00300
00600
00665 i�006'GS=.'TGP3B:
t=01'0:421
.!AL 07i:
E_
F" Y
voHa
Qo
A
E,
O
k
O
W
EFF FLOW
CO
H
Z
W
�
..
W
0
Q Z
0
Y��
Z
Lu WYLIJ
J
-Uu
O
LLO
U
Z
W
U
X
0
Z
0
O
o�
_
F-
o�
O
❑]
Qa
W
O�
VH
OO
2
00A
Uh
d
O
O0O
Qd
HW
Op
INF
o"
�nfection
HRS
HRS
Y/B/N
MGD
° C
UNITS
UG/L
LB/DAY
MG/L
LB/DAY
9/100ML
MG/L
MG/L
MG/L
MG/L
P/F
UG/L
1
N
no flow
2
N
no flow
3
7:00
8.00
Y
no flow
�.. ,
4
7:00
8.00
Y
0.4490
5
7:00
8.00
Y
0.4260
23.0
8.1
< 7.1
34.8
84
7.6
Q
6
7:00
8.00
Y
0.4350
71
7:00
8.00
Y
0.4150
iLT
8
8:00
5.00
Y
0.3890
R S
9
7:00
5.00
Y
0.3360
10
7:00
8.00
Y
0.2830
11
7:00
8.00
Y
0.2000
18.9
1 7.8
4.3
16.7
1 6
7.9
12
7:00
8.00
Y
0.1370
13
7:00
8.00
Y
0.1190
14
7:00
8.00
Y
0.1060
r, h i
n r m
15
N
no flow
5
16
6:00
4.00
Y
no flow
17
7:00
8.00
Y
no flow
18
7:00
8.00
Y
no flow
19
7:00
8.00
Y
no flow
20
7:00
8.00
Y
no flow
21
7:00
8.00
Y
no flow
22
N
no flow
23
N
no flow
24
7:00
8.00
Y
no flow
25
7:00
8.00
B/Y
0.3790
17
26
7:00
8.00
B/Y
0.3940
16.9
8.4
11.2
41.7
8.7
7:00
8.00
B/Y
0.3620
7:00
8.00
B/Y
0.2930
[30
N
no flow
N .
no flow
7:00
8.00
Y
no flow
AVERAGE
0.3149
19.6
5.2
31.1
20.46
8.1
MAXIMUM
0.4490
23.0
8.4
11.2
41.7
84
8.7
MININIUM
0.1060
1 16.9
7.8
4.3
16.7
6
7.6
Comp. (C) / Grab (G)
O§M
G
G
C
C
G
G
C
C
G
C
C
Monthly Limit
1 0.450
1
1 6.0-9.0
68.0
124.0
200
icE
DWQ Fonn MR-] 7/12

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) Fv I
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
0 2all_
ignat e of Permittee** Date
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzalez(a),celanese.com 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,Ine. Certification No.
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ETT Labs
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.nedenr.org/web/wq/swp/ps/npdes/appforms.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
x* ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
402
22

CERTIFIED MAIL: 7015 0640 0002 9349 2790
Return Receipt to PEM Carter
PEMC16:31
November 18, 2016
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
rJ Celanese
The chemistry inside innovation`"
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerninq October 2016, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report have been
submitted.
• BOD5 for 10/5/2016 was less than the reporting limit of 2.0 mg/I
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(a-celanese.com.
�.7
,
11�
PEM Carter
EHS Lead/Environmental Engineer
Attachments

EFFLUENT
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH I September 2016
FACILITY NAME CNA Holdings,Ine. - Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdinirs,Ine. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this fonn)
OPERATOR IN RESPONSIBLE CHARGE (OR, Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704480-5793
CHECK BOX IF ORC HAS CHANGED ® NO FLOW / DISCHARGE FROM SITE * rig®
AT vORIGINAL andONE COPY to: X �� %IJVJD4j f LOp/&WR
DIVISION OF WATER QUALITY (SIGN TTURE OF OPERATOR IN RESPONSIBLE CHARGE) _rDATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS 0 C I U 16
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
A in1�.l.
m
50050
00010
00400
50060
00310
00610
00530
31 616
00300
00600
00665 00665
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a
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O
i
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disinf Lion
HRS
HRS
YB/N
MGD
0 C
UNITS
UG/L
LB/DAY
M[G/L
LB/DAY
H/100ML
MG/L
MG/L
MG/L
MG/L
P/F
UG/L
1
7:00
8.00
' Y
0.2480
2
7:00
8.00
Y
0.1770
j
3
N
no flow
4
.:
'N
no flow
24
1016
5
H/N
no flow
6
7:00
8.00
B/Y
no flow
CENI
RAL
7
7:00
8.00
.B/Y
no flow,
DWR
SE
8
1:00
8.00
'13/Y
no flow
9
7:00
8.00
BN
no flow
10
6:30
3.00
. B/Y
no flow
11
N,
no flow,•
;
12
7:00
8.00
Y
no flow
13
'7:00
8.00
Y
no flow
14
.7:00
8.00
Y
no flow
�?
15
:, 7:00
8.00
.Y
no flow
° v
16
.` 7:00
8.00
"Y
no flow
17
6:00
3.00
Y
no flow
18
715
8.45
. 'Y
no flow
19
7:00
8.00
Y
0.3680'
20
`7:00
8.00
Y
0.3980
27.1
8.4
13.6
48.8
102
6.3
<5.0
P
21
7:00
8.00
Y
0.4200
22
•, 7:00
8.00
- Y
1 0.3510
23
7:00
8.00
. Y
0.2690
24
N.
no flow
25
N
no flow
26
7:00
8,00
. 'Y
no flow
27
7:00
8.00
Y
no.flow
28
7:00
8.00
Y
no flow
29
7:00
8.00
Y
no flow
30
; 7i00
8.00
`Y,
noflow`
r
AVERAGE
0.3187
27.1
13.6
48.8
102.00
6.3
0.0
P
... MAXIMUM
0.4200.
27.1
8.4- ...
._..
13.6
48.8.
102
_. 6.3
. ,...
<5.0
P
MINIMUM
1 0.17701
27.1
8.4
13.6
48.8
102
6.3
< 5.0
P
Comp: (C) / Grab (G)
G
G
C
C
G'
G
C
C
G
C
C
Monthly Limit
1 0.450
1
1 6.0-9.0
68.0
124.0
200
FICE
DWQ Form MR-1 7/12

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) Fv I
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
Signat re of Permittee** ate
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzal [e-mail] 8/31/2018
Permittee Address Phone Number a -mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,Inc. Certification No.
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ETT Labs
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.nedenr.org/web/wq/swp/ps/npdes/appforms-
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
x No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
402
22

CERTIFIED MAIL: 7015 0640 0005 2818 5633
Return Receipt to PEM Carter
PEMC16:26
September 27, 2016
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
-31
Celanese
The chemistry inside -innovation
RECEIVED/NCDENR/DWR
OCT 11 2016
WQROS
MOORESVILLE REGIONAL OFFICE
RECEIVED
OCT 0 4 2016
Information Processing Uno-
DWQ/BOG
Reference: Notes Concerning August 2016, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004962
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report have been
submitted.
• 8/10/16: BOD5 needs to be qualified due to the oxygen consumption for the blank were outside the
method defined acceptance criteria.
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on the forms, feel free
to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(cD-celanese.com.
(:77('Lu,
PEM Carter
EHS Lead/Environmental Engineer
Attachments
OA
OCT"-:B�
f
UL i 0 5 20

PPP_PPPP_
EFFLUENT
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH pulp„St YEAR. 2016
FACILITY NAME CNA Holdings.Inc. - Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdines,Inc. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (OR, Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704-480-5793
CHECK BOX IF ORC HAS CHANGED ® NO FLOW / DISCHARGE FROM SITE
Mail ORIGINAL and ONE COPY to: o
ATTN: CENTRAL FILES
DIVISION OF WATER QUALITY (SfUNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
N
50050
1 00010
00400
50060
00310
00610
00530
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00300
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0 C
UNITS
UG/L
LB/DAY
MG/L
LB/DAY
N/100ML
MG/L
MG/L
MG/L
MG/L
P/F
UG/L
41
7:00
8.00
Y
noflow
2
7:00
8.00
Y-
noflow
3
7:00
8.00
Y-
noflow
4
7:00
8.00
Y
noflow
5
'7:00
8.00
Y.
noflow
6
N
noflow
,711
N
noflow
8
7:00
8.00
Y.
noflow
`9
7:00
8.00
Y
0.3680
89
10
700
8.00
Y ,..
0.4000
30.0
7.5
12.7
52.7
5.8
1.2
0.2
11
7:00
8.00
Y...
0.4220
12
7:00
8.00
Y
0.3770
1 1 31
3:40
4.25
. Y.
0.2530
o
,
14
7:00
3.00
Y
noflow
15
7:00
8.00
Y
noflow
16
7:00
8.00
Y`
noflow
17
7:00
8.001
Y
noflow
18
7:00
8.00
'Y
noflow
19
7:00
8.00
Y
noflow
20
6:30
3.00
B/Y
noflow
21
6:30
3.00
B/Y "
noflow
22
7:00
8.00
Y
noflow
23
TOO
8.00
Y
0.3070
142,'
24
7:00
8.00
Y
0.3650
20.9
8.4
14.0
21.6
5.9
25
7:00
8.00
Y
0.3730
26
7:00
8.00
Y
0.3160
27A7:OO
N
noflow
28N
noflow
29
Y
noflow
30
Y,`'
0.3660
129
31
Y
0.3260
29.8
8.3
15.2
27.5
5.6
AVERAGE
0.3521
26.9
14.0
33.9
117.69
5.8
12
02
. MAXIMUM' ..
0.4226
30.0
1 8.4
,
15.2.........
...52.7
142
, .:
5.9
_
1.2
,.
02
..
..; ,.�
,
mmvmluM
0.25301
20.9
1 7.5
12.7
21.6
89
5.6
1.2
02
Com . (C) /Grab (G) :.
G
G
C
C
G
G;
r. C
C
, G
C
C
Monthly Limit
0.450
1
6.0-9.0
68.0
124.0
200
DWQ Form MR-1 7/12

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part H.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
11'&q -a'1
Sipa&e o Petro tte * V Date
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzalez(a--)celanese.com 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,lnc. Certification No. 402
Certified Laboratory (3) ETT Labs Certification No. 22
Certified Laboratory (4)
Certified Laboratory (5)
PARAMETER CODES
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.nedenr.org/web/wq/swp/ps/npdes/appforrns.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

ppppppp-
EFFLUENT
3
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH 1i� ,IV YEAR 2016
FACILITY NAME CNA Holdings,Ine. - Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdings,Ine CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704480-5793
CHECK BOX IF ORC HAS CHANGED ® NO FLOW / DISCHARGE FROM SITE
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES x J111101/(
DMSION OF WATER QUALITY (SIONATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE. S E P 13 2016
50050
1 00010
1 00400
50060
00310
00610
00530
31616
00300
00600
00665 00665
TGP3B
010
c
WFA
amsVo
�
«
~C
d
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1-
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(
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JO
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Oa
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m
N
OJ
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W_!x
0
U
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-
Od
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0
11p
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jr
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ORa=EX0E-S
OVu
U
R
ILWUJa
H
GIONA
NF
a
dp�neNct0n
MIS
HRS
YB/N
MGD
° C
UNITS
UG/L
LB/DAY
MG/L
LB/DAY
N/100ML
MG/L
MG/L
MG/L
MG/L
P/F
UG/L
11
7:00
8.00
Y
no flow,
2
10:00
2.50
Y ;
no flow
I k
3
1200
1.00
Y
no flow.
!
4
6'.00
1.50
H/Y
no flown
5
7:00
8.00
Y
no flow
,e
-
;r
6
7:00
8.00
Y `
no flow
71
7:00
8.00
.. Y
no flow
8
7:00
8.00
° Y
no flow
9
9 00
1.25
• yB .;
no flow
10
930
3.00
. YB
no flow
I1
700
8.001
Y
1 0.3450•
64
12
7:00
, 8.00
Y
0.3770
29.3
8.1
12.3
35.5
5.7
131
7:00
8.00
Y
0.3930
14
7:00
' 8.00
Y
0.3780
15
7:00
8.00
Y
0.3020
16
N
no flow
17
N
I no flow
18
7:00
8.00
Y
no flow
19
7:00
8.00
Y
0.4070
29.6
7.6
14.9
39.7 `
12
6:1
20
7:00
8.00
Y
0.4180
21
7:00
8.00
Y
0.3260
22
7:00
. 8.00
" Y "
0.2010
23
N
no flow.
24
N.
no flow
25
7:00
8.00
.. B/Y
no flow-
26
7:00
8.00
B/Y
no flow
27
7:00
8.00
B/Y
no flow.
28
7:00
8.06
- B/Y
no flow"
Cr
'qm
29
7:001
8.00
B/Y
no flow
�' n
301N''
no.flow
31,
N
no..flow
AVERAGE
0.3497
29.5
13.6
37.6
27.71
5.9
MAXIMUM
0.4180
29.6
6.1
14.9
.
39.7 " .
64 ','
61
MINIMUM
0.2010
29.3
7.6
12.3
35.5
12
5.7
Comp. (C) / Grab (G)
G
G
C
C.
,,G
G
C
C
G
Monthly Limit
0.450
6.0-9.0
68.0
124.0
200
OFFI(
DWQ Forth MR-1 7/12

ppppppp-
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F7
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
. A Ad, 0 A , 201L
SignatuV of Permittee***
(Required unless submitted electronica ly)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzalez(&-celanese.com 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,Inc. Certification No.
Certified Laboratory (3) ETT Labs Certification No.
Certified Laboratory (4)
Certified Laboratory (5)
PARAMETER CODES
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.nedenr.org/web/wq/swp/ps/npdes/appfortns.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
402
22

Celanese
The chemistry inside. innovation"
CERTIFIED MAIL: 7015 0640 0005 2818 5619
Return Receipt to PEM Carter
PEMC16:25
August 29, 2016
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
Reference: Notes Concerning June 2016. DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report have been
submitted.
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on the forms, feel free
to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(@-celanese.com.
ely,
PEM Carter
EHS Lead/Environmental Engineer
Attachments

EFFLUENT
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH ,� YEAR 2016
FACILITY NAME CNA HoldinES,Ing. - Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdings,Inc. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (OR, Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704-480-5793
CHECK BOX IF ORC HAS CHANGED Q NO FLOW / DISCHARGE FROM SITE * 0
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES x ?-
DIVISION OF WATER QUALITY (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
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0.3290
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CI
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13
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14
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0.2850
29.1
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0.2450
16
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0.1510
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19
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20
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Y
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21
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Y
no flow
22
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no flow
1
23
7:00
8:00
Y
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24
' 7:00
_
8.00
Y
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25
N
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26
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27
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-
28
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8.001.
"Y
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29
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8.001
Y
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30
7:00
8.00
' Y
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AVERAGE
0.2931
28.0
9.5
34.3
28.57
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26.9
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0.450
6.0-9.0
68.0
124.0
200
RECEIVED/NCDENR/DWR
AUG 0 9 2016
DWQ Forth MR-1 7/12 WQ RO S
MOORESVILLE REGIONAL OFFICE

V
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part H.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
Sigiiattre of Permittee* Date
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzalez(a)-celanese.com 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,Inc. Certification No.
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ETT Labs
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.ncdenr.org/web/wq/swp/ps/npdes/appforrns.
Use only units of measurement designated in the reporting facility's NPDES pemut for reporting data
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
402
22

Celanese
The chemistry inside innovation"
CERTIFIED MAIL: 7015 0640 0005 2820 0961
Return Receipt to PEM Carter
PEMC16:22
July 15, 2016
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
Reference: Notes Concerning June 2016, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report have been
submitted.
• BOD5 sample 6/7/16: Needs to be qualified due to laboratory control standard (GGA) for this analytical
batch was outside the method defined established acceptance limit.
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on the forms, feel free
to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carterO-)celanese.com.
ly,
PEM Carter
EHS Lead/Environmental Engineer
Attachments

MES
JAN 13 2Oi7 EFFLUENT
NPDES PERMIT NO. NC 0004952 DISCHAR ! / _ 001 MONTH May YEAR 2016
FACILITY NAME CNA Holdings.Ine. - Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdings.1ne. I RYWT2A ON NO. 221
(list additional laboratories on the backside/page 2 of this form) �--ul,
OPERATOR IN RESPONSIBLE CHARGE (OR(Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704-480-5793
CHECK BOX IF ORC HAS CHANGED ® O FLOW ! DISCHARGE FROM SITE'r
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES x '�./r✓i"v KOE W1
DIVISION OF WATER QUALITY (S TURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS g,
RALEIG J NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE. A I n I V B 3 2017
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6.0-9.0
68.0
124.0
200
DWQ Form MR-1 7/12
=FICE

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements a
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part H.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am -aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
"Wj,al a" A L14 23, 2016
SignaturP of Permittee*** 0 LUte"
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, .NC 28073 704-480-5728 [e-mail] 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,lnc. Certification No.
Certified Laboratory (3) ETT Labs Certification No.
Certified Laboratory (4)
Certified Laboratory (5)
PARAMETER CODES
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.ncdenr.org/web/wq/swp/ps/npdes/appforms.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DU R for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
402
22

�
4 Celanese
The chemistry inside innovation"
CERTIFIED MAIL: 7015 0640 0005 2820 0909
Return Receipt to PEM Carter
PEMC16:19
June 28, 2016
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-16.17
ATTN: Central Files
Reference: Notes Concerning May 2016, DMR for C N A Holdings LLC - Shelby Facility
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report have been
submitted.
• BOD5 sample 5/10/16: Needs to be qualified due to the oxygen consumption for the blank were outside
the method defined acceptance criteria. ..
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on the forms, feel free
to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.cartera-celanese.com.
incerely,
PEM Carter
EHS Lead/Environmental Engineer
Attachments

EFFLUENT
C 0004952 DISCHARGE NO. 001 MONTH I April I YEAR.
FACILITY NAME CNA Holdines,Inc. Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdinss,Inc. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
2016
OPERATOR IN RESPONSIBLE CHARGE (ORC Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704-480-5793
CHECK BOX IF ORC HAS CHANGED Q NO FLOW / DISCHARGE FROM SITE
Mail ORIGINAL and ONE COPY to: RECEIyIVV/NCB Sir�/EWri
ATTN: CENTRAL FILES x Ss ��`®®
DIVISION OF WATER QUALITY (SIGNATURE OF OPl O RESPONSIBLE CHARGE) ATE r
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS ' °(�/� ' A� T 20 1
RALEIGH NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
1nrnDnc
m
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LB/DAY
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MG/L
MG/L
MG/L
MG/L
P/F
UG/L
1
7:00
8.00
B/Y
no flow
2
N
no flow
3
N
no flow
4
7:00
8.00
Y
no'flow
r•
5
7:00
8.00
Y
no flow
MIA I
61
7:00
8.001
Y
0.2940
7
7
5:00
8.00
Y
0.1490
< 2.7
< 3.1
PEN
8
7:00
8.00
Y
no flow
17.5
7.8
8.6
9
8:15
3.75
Y
0.2910
15.8
7.6
9.1
10
8:30
3.00
Y
no flow
11
7:00
8.00
Y
no flow
121,
7:00
, 8.00
Y . ,
0.3450
16.8
7.5
< 6.3
7.5
15
8.2
13
7:00
8.00
Y
0.3880
jF
14
7:00
8.00
Y
0.3760
15
7:00
8.00
Y
0.3940
16
10:00
2.001
Y
1 0.3860
17
9:45
.2.00
Y
0.3940
18
7:00
8.00
Y
0.3670
17
19
7:00
8.00
Y
0.3170
19.1
7.3
< 5.8
10.8
8.8
20
7:00
' 8.00
Y
0.2560
21
7:00
8.00
Y
0.2050
22.
7:00
8.001
Y
1 0.1880
23
N
no flow
24
20:00
2.00
Y
no flow
25
7:00
8.00
Y
no flow
Lu
iv
26
7:00
8.00
Y
no flow
27
7:00
8.00
.Y
no flow,
28
7:00
8.001
Y
I no flow
29
7:00
8.00
Y
no flow
30
N
no flow
AVERAGE
0.3107
17.3
0.0
1
6.1
1 12.13
8.7
MAXIMUM ..
0.3940
191
7.8..
<8.3
10.8 ,..
...17
9.1
MINIMUM
0.1490
15.8
7.3
<2.7
<3.1
7
8.2
Comp. (C) / Grab (G)
G
G
C
C
G
G
C
C
G
C
C
MontMy Limit
0.450
6.0-9.0
68.0
124.0
200
FICE
DWQ Foam MR-1 7/12

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
SignatqfeofPermtttee*** ate
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 [e-mail] 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,Inc. Certification No.
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ETT Labs
PARAMETER CODES
402
Certification No. 22
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.ncdenr.org/web/wq/swp/ps/npdes/appforms.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the pemrittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

ppprp,
J Celanese
The chemistry inside innovation
CERTIFIED MAIL: 7015 064.0 0005 2820 0879
Return Receipt to PEM Carter
PEMC16:16
May 23, 2016
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
Reference: Notes Concerning April 2016, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report have been
submitted.
• BOD5 sample 4/07/16, 4/12/16 and 4/19/16: was less than the reporting limit of 2.2.
• TSS sample 4/07/2016: less than the reporting limit of 2.4. TSS was performed by Prism Laboratory.
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC-, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on the forms, feel free
to call me at 803/81.8-8683 (cell), 704/480-5726 (office) or via email at pem.carteracelanese.com.
Sincere
PEM Carter
EHS Lead/Environmental Engineer
Attachments

T Ji
Celanese
The chemistry inside innovation"
CERTIFIED MAIL: 7015 0640 0005 2818 5879
Return Receipt to PEM Carter
PEMC16:14
April 22 2016 uA
JAM I
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RECEIVED
.. MAY i. 0 Z016
CENTRAL FILES
DWR SECTION!
RECEIVED/NCDENRIDWR
MAY 2 4 2016
ATTN: Central Files WQROS
MOORESVILLE REGIONAL OFFICE
Reference: Notes Concerning March 2016, DMR for C N A Holdings LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report. have been
submitted.
• BOD5 sample 3/01/16:needs to be qualified due to laboratory control standard (GGA) for this analytical
batch was outside the method defined established acceptance limit.
• BOD5 sample 3/23/2016: less than the reporting limit of 2.4
• BOD5 sample 3/30/2016: less than the reporting limit of 2.2
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC _ Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on the forms, feel free
to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(a-celanese.com.
PEM Carter
EHS Lead/Environmental Engineer
Attachments -
G
MAY .16 2016

•r
EFFLUENT
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH Ma cr her h�� YEAR 2016
FACILITY NAME CNA Holdins sJnc. - Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdinn-s,Inc. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (OR, Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704-480-5793
CHECK BOX IF ORC HAS CHANGED Q NO FLOW / DISCHARGE FROM SITE * M
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES x gl4dl eo i 6
DIVISION OF WATER QUALITY (3 ATURE OFVPERArOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH NC 27699-1617 . ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
0
50050
00010
00400
50060
00310
00610
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HRS
HRS
YB/N
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UNITS
UG/L
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MG/L
LB/DAY
#/100ML
MG/L
MG/L
MG/L
MG/L
P/F
UG/L
1
, 7:0�0
8.00
. Y
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a Il 2.,
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3
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, 0.3520
4
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8.00
` Y `
0.2900
5
N"
no.flow:
-
61
1
N
no, flow
7
'7:00
8.00
Y
no flow
87:00
8.00
Y.
0.3180
13
9
,, 7:00
8.00
` Y
0:383U
-131
8.1 ' , ,
9.9 ,
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10
:"7:00
8:00
' Y
0.3730
11
,_ 7:00
8.00
, Y
0.3460
121,
8:50
2.00
Y. _.
0.3000
13
7:06
2.00
Y .
'no flow
14
`7:00
8.00
" Y
no flow
15
7:00
8.00
Y
0.4070
1.1"
...
16
7:00
8.00
.` Y "
0.3780
19.4
8.4
15.8
31.5
8.6
17
' 7:00
8.00
', Y
0.1200
."
18
7:00
8.00
Y
0.3310
19
7:45
1.75
Y
`no flow
20
7:15
1.75
Y� `
no flow
21
7:00
8.00
r'Y,;
no flow
22
„r7:00
8,00
Y :
0.3620
5
23
.7:00
8.00
Y
0.3280
14.7
7.7 °"
< 6.6
r
. `14.0
;,
9.0 ,.
24
7:00
8.60
Y
0.2580
25
, "'d
H'
no flow
26
°
N
no flow.
27
N
no flow
28
7:00
8.00
B/Y
no flow
29
7:00
8.00
WIT
0.2550 ,
30
"7:00
8.00
= BNY'
0.1990
17.1
7.7
< 3.7
4.1
2
8.4
31
7'.00
8.00
• BN..
,no flow
AVERAGE
0.3191
15.2
`�-, �,;,
,, ,"•^;'..,
6.7
19.4
5.90
9-2
0.0
P
- " MAXIMUM '. �
0.4070
19.4
r . 8:4 .
..-.. ,,
15.8 „
31,5
13
16.5 ...
. � ..
< 5.0
- P
.. ;.�
MINIMUM
0.1200
112
7.7
7.8
4.1
2
8.4
<5.0
P
comp. (C) i drab(G)
G
G
C ;
C"„
G. ,
G
C ;:
C'
G , .
C
C
Monthly Limit
0.450
6.0-9.0
68.0
124.0
200
DWQ Fonn MR-1 7/12

PFP_PPP_
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements a
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
Sign re of Permittee Date
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzalez(cD_celanese.com 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,lnc. Certification No.
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ETT Labs
PARAMETER CODES
402
Certification No. 22
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.ncdenr.org/web/wq/swp/ps/npdes/appforms.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

ppppppp-
EFFLUENT RECEIVEDINCDENP,IDWR
AH 5 2616>
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH YEAR 2016
FACILITY NAME CNA Holdings,Inc. - 7 Celanese CLASS II Mg9 T/1+ I G Clexelandi nGGICE
CERTIFIED LABORATORY (1) CNA Holdines,Inc. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPL Mike Queen, Mike Sparks ORC PHONE_ 704-480-5793
CHECK BOX IF ORC HAS CHANGED ® NO FLOW / DISCHARGE FROM SITE
Mail ORIGINAL and ONE COIRAR: 31 2016
ATTN: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
'3/21/Zo/
d
50050
1 00010
1 00400
1 50060
00310
00610
00530
LRkI6
00300
00600
1 00665 00665
TGP3B
01042
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p
E
a) 0LLIoO
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EFF X
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INF
p
ry
fection
HRS
HRS
Y/B/N
MGD
° C
UNITS
UG/L
LB/DAY
MG/L
LB/DAY
0/100ML
MG/L
MG/L
MG/L
I MG/L
P/F
UG/L
1
7:00,
8.00
Y
no flow
2
7:00
8.00
Y
no flow
3
7:00
8.00
Y
no flow
4
7:00
8.00
Y
no flow
AR
a1
5
` 7:00
8.00
Y
no flow
61
N
no flow
G
K i R
L FILES
7
N
no flow
D\VR
SF
GTIO
q
8
7:00
8.00
Y
no flow
9
7:00
8.00
Y
0.4480
8
10
700
8.00
Y
0.4450
5.9
7.7
8.9
41.6
12.1
1.3
< 0.05
11
,. 7:00
' 8.00
Y
'0.4400
12
7:00,
8.00
Y
0.4320
13
8:00
5.00
Y
0.3600
14
" 7:30
`3.50
Y'
no flow
15
7:00
8.00
Y
no flow
16
7:00
&001
Y
no flow
17
7:00
8.00
Y
no flow
,
18
7:00
8.00
Y
no flow
19
7:00
8.00
Y
no flow
20
6:30'
- 2.00
Y
' no flow
21
9:30
3.00
Y
no flow;
22
7:00
8.00
1 Y
no flow
23
7:00
,8.00
Y
0.4400
8
24
7:00
8.00
Y
0.3420
10.1
7.9
< 11.4
49.6
10.3
25
` 7:00
8.00
B/Y
0'.3960'
26
7:00
8.00
B/Y
0.3290
27
11:00
1.00
B/Y :
0.3570
28
10:00
2.00
B/Y
0.3770
29
7:00
8.00
Y
0.3920
AVERAGE
0.3965
6.0
4.5
45.6
6.00
11.2
1.3
0.0
MAXIMUM ..
0.4480
10.1
7.9
-
a9.
49.6
6
12.1 .•
1.3
<0.05
MINIMUM
1 0.32901
5.9
1 7.7
0.0
1 41.6
1 8
1 10.3
1 1.3
<0.05
Comp. (C) / Grab (G)
G
G
C
C
G
'G
G
C
C
Monthly Limit
0.450
6.0-9.0
68.0
124.0
200
P+L-,
DWQ Form MR-17/12

ppppppp—
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
�a� �LA P, 3 -ZA
Signaitit of Permittee*** 0 We
(Required unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzalez(a_celanese.com 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,Inc. Certification No.
Certified Laboratory (3) ETT Labs Certification No.
Certified Laboratory (4)
Certified Laboratory (5)
PARAMETER CODES
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.ncdenr.org/web/wq/swp/ps/npdes/appforms.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
402
22

pp.ppppp-
CERTIFIED MAIL: 7015 0640 0005 2820 0848
Return Receipt to PEM Carter
PEMC16:13
March 24, 2016
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
Celanese
The chemistry inside innovation -
Reference: Notes Concerninq February 2016. DMR for C N A Holdings LLC.- Shelby Facility.
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report have been
submitted.
• BOD5 sample 2/24/16: less than the reporting limits of 4.0.
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC - Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on the forms, feel free
to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at Dem. carterfc)celanese.com.
(71 L44J,14�
PEM Carter
EHS Lead/Environmental Engineer
Attachments

EFFLUENT
GEAR 1 2016 3
NPDES PERMIT NO. NC 0004952 DISCHARGE NO. 001 MONTH I lanuary ____J YEAR. 2016
FACILITY NAME CNA Holdines,Inc. -'Celanese CLASS II COUNTY Cleveland
CERTIFIED LABORATORY (1) CNA Holdints,Inc. CERTIFICATION NO. 221
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC Michael D. Sparks GRADE III CERTIFICATION NO. 987732
PERSON(S) COLLECTING SAMPLES Mike Queen, Mike Sparks ORC PHONE_ 704-480-5793
CHECK BOX IF ORC HAS CHANGED NO FLOW / DISCHARGE FROM SITE 0
Mail ORIGINAL and ONE COPY to: RECEJVF_D/NCDENRIDWR
ATTN: CENTRAL FILES a /L 2 /Z 0/ 6
DIVISION OF WATER QUALM NATURE OF OPERATOR IN RESPONSIBLE CHARGE) M A l� �DATB')
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
kP,IQROS
d
50050
00010
00400
50060
00310
00610
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31616
00300
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00
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x0
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W
U
0
F-
INF
m
2'
o
p Iry
disinfection
HRS
HRS
YB/N
MGD
° C
UNITS
UG/L
LB/DAY
MG/L
LB/DAY
N/100ML
MG/L
MG/L
MG/L
MG/L
P/F
UG/L
I
H/N
No Flow
2
No Flow
r __
1 �.
•
3
10:20
2.0
Y .
No Flow
e
L
L.
,
4
7:00
8.0
. , Y •
0.4180
12
5
7:00
8.0
. Y
0.3440,
9.0
TO .,
8.9
56.8
11.3
6
7:00
8.0
Y
0.4340
71
7:00
8.0
Y
0.4280
r'1
1 Cm e-
4 t_
^.
.�,
8
7:00
8.0
Y
0.3950
9
N '
No Flow
10
N
No Flow
11
7:00
&6l
Y
No Flow
12
7:00
8.0
Y
0.4130
4
13
7:00
8.0
Y
0.3980 `
6.2
7:4
7.0
29.9
12.2,
14
7:00
8.0
- Y ,
0.3450
15
7:00
8.0
Y
0.2840
16
9:40
2.0
Y
0.3760
17
9:45
2.01
Y
0.3960'
WAN
9' 11
Will;
181
1125
1.0
H/Y
0.3580
19
7:00
&0
Y
0.3020
'
20
7:00
8.0
Y
0.2590
4.6
7.5
< 4.3
15.3
3
12.6
21
7:00
8.0
Y
0.2330'
22
7:00,
8:0
Y
0.0950
23
N .
No Flow
24
N
No Flow
25
7:00
8.0
Y
No Flow
26
7:00
8.0
Y
0.3750
3.8
7.4
< 7.2
33.5
5
12.9
27
7:00
8.0
Y
0.4410
28
7:00
8.0
Y `
0.3980
29
7: 01
8.0
B/Y
0.3240
30
N
No Flow
311
1
1 N
No Flow
'
AVERAGE
0.3508
5.9
�� ;i-
` ^'^ ""+
4.0
33.9
5.18
12.3
MAXIMUM .
_0.4410
1..... 9.0
.. 7.5
8.9
, 56.8
12
12.9..
,.
3
MINIMUM
0.0950
3.8
7.0
0.0
15.3
3
1 11.3
Com . (C) / Grab (G)
G
G
C
C
G
G
C
C
G
C
C
Monthly Limit
0.450
6.0-9.0
68.0
124.0
200
DWQ Form MR-1 7/12

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) Fv I
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines
and imprisonment for knowing violations."
Rafael Gonzalez
Permittee (Please print or type)
Signa eofPermittee*** C/ W
(Requ red unless submitted electronically)
2525 Blacksburg Rd, Grover, NC 28073 704-480-5728 rafael.gonzalez(Cz-)celanese.com 8/31/2018
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Prism Laboratories,Inc. Certification No. 402
Certified Laboratory (3) ETT Labs Certification No. 22
Certified Laboratory (4)
Certified Laboratory (5)
PARAMETER CODES
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting
http://portal.nedenr.org/web/wq/swp/ps/npdes/appforms.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

" Celanese
The chemistry inside innovation -
CERTIFIED MAIL: 7015 0640 0005 2820 1029
Return Receipt to PEM Carter
PEMC16:11
February 24, 2016
NCDENR
Division of Water Quality
1617.Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
Reference: Notes Concerning January 2016, DMR for C N A Holdings, LLC.- Shelby Facility,
Permit No. NC 0004952
To Whom It May Concern:
In accordance with the facility's NPDES Permit, duplicate copies of the signed DMR report have been
submitted.
• BOD5 sample 1/20/16: needs to be qualified due to the oxygen consumption for the blank were outside
the method defined acceptance criteria.
• BOD5 sample 1/20/16 and 1/26/16: less than the reporting limits of 2.0 and 2.3.
• Site continues to experience low flow with no discharge days.
Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information -on -the forms, feel free
to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(a-celanese.com.
rely,
PEM Carter
EHS Lead/Environmental Engineer
Attachments

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2018 (April 2018)
PERMIT VERSION: 4.0 - STATUS: Active
CLASS: WW-2 MAY 2 9 2018 COUNTY: Cleveland
ORC: Michael D. Sparks CEN-ORC CERT NUMBER: 987732
DW
ORC HAS CHANGED: No 6 tYf L FILES
- CVi1R.SECTBa�I
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001
ME
RECEIVED/NCDENR/DWR
NO DISCHARGE*: NO WQROS
MOORESVILLE -r
- - ' L OFFI,
a
G
E
F:
-
E
E
U
E
F
-
u'
a
F
F
a°
O
�+
O
E
O
o`
U14
O
c
m
C
Z
50050
011400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
PH
I
Boo- Q)' Dub)'
TSS• Q tl Daily
FCOLI BR
TOTAL N-
TOTAL P - Cant
1,1-DCE
I,I-DCEY
2400 d.&
tin
2400 dock I
H.
YIBIN
m d I
su
Ibs/da
Ibs/da
#/100mI I
mg/I
mgA 1
Ibs/day
Ibs/day
I
N
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
a
0630
8.0
Y
NOFLOW
5
0600
8.0
Y
NOFLOW
6
0630
8.0
Y
NOFLOW
7
0700
2.5
Y
NOFLOW
8
0730
4.0
Y
NOFLOW
9
0500
8.0
Y
0.335
10
0600
8.0
Y
0.375
11
0930
24
0630
8.0
Y
0.362
8.2
14.8
15.4
<2
12
0600
8.0
Y
0.359
13
0600
8.0
Y
0.354
14
0600
1.5
Y
0.268
15
1300
3.0
Y
NOFLOW
16
0500
9.0
Y
NOFLOW
17
0630
8.0
Y
0.301
18
0930
24
0630
8.0
Y
0.341
9.2
10
12.8
<2
19
0600
8.0
Y
0.326
20
0630
18.0
Y
0.262
21
1015
1.5
B
NOFLOW
22
1230
2.0
B
NOFLOW
23
0630
8.0
Y
0.259
24
0630
8.0
Y
0.368
25
0930
124
0630
8.0
Y
0.359
8.1
9.3
13.8
12
26
0600
8.0
Y
0.355
27
0630
8.0
Y
0.397
28
0900
1.0
B
0.322
29
N
NOFLOW
311
10630
18.0
Y
NOFLOW
Monthly Aycmge Limit:
0.45
68
124
200
0.071
0.052
Ataathly A-gc:
0.333938
11.366667
14
1
-
Daily Maximum:
0.397
8.2
14.8
15.4
0
Daily Minimum:
0.259
8.1
9.3
12.8
0
****NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDrvIR PERIOD: 04-2018 (April 2018)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
O
B
-
E
U
-
E
E
u
i
F
E
F
L
3
y
O
O
L
E
O
=
o`
0
O
e
C
Z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
I,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
I,J-DCB
2,4-DCPH
2,4-DMPH
2,4-DNPH
2,4-DNT
2400 d-1,
Hr
2400c1nch
Hrs
YIB/N
Ibs/da
Ibs/day
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/day 1
Ibs/day
Ibs/day 1
Ibs/da
Ibs/da
1
N
NOFLOW
2
0630
9.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0600
8.0
Y
NOFLOW
6
0630
8.0
Y
NOFLOW
7
0700
2.5
Y
NOFLOW
8
0730
4.0
Y
NOFLOW
0500
8.0
Y
10
0600
8.0
Y
11
0930
24
0630
8.0
Y
12
0600
8.0
Y
13
0600
8.0
Y
14
0600
1.5
Y
15
1300
3.0
Y
NOFLOW
16
0500
9.0
Y
NOFLOW
17
0630
8.0
Y
Is
0930
124
0630
9.0
Y
19
0600
8.0
Y
20
0630
8.0
Y
21
1015
1.5
B
NOFLOW
22
1230
2.0
B
NOFLOW
23
0630
8.0
Y
24
0630
8.0
Y
25
0930
24
0630
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
28
0900
1.0
B
29
1
1N
NOFLOW
30
0630
8.0
Y
NOFLOW
Mmthly A.'crnge Llmin
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.058
0.229
0.365
Munlhlr A-,ge:
D.Hy Mazimum:
DuiW Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2018 (April 2018)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
F
U
F
u
F
F
O
ih
2
O
0
u
O
z
Z
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-o-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 cluck
H. 12400
clock
H. I
YIB/N I
Ibs/da
lbs/day
ugA
Ibs/day I
Ibs/da
Ibs/day I
lbs/day
ugA I
lbs/day
ug/1 lugA
I
N
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0600
8.0
Y
NOFLOW
6
1 10630
18.0
Y
NOFLOW
7
0700
2.5
Y
NOFLOW
8
0730
4.0
Y
NOFLOW
9
0500
8.0
Y
10
0600
8.0
Y
11
0930
24
0630
8.0
Y
12
0600
8.0
Y
13
10600
8.0
Y
14
0600
1.5
ly
Is
1300
3.0
Y
NOFLOW
16
0500
9.0
Y
NOFLOW
17
0630
8.0
Y
18
0930
24
10630
8.0
Y
19
0600
8.0
Y
20
0630
8.0
Y
21
1015
1.5
B
NOFLOW
22
1230
2.0
B
NOFLOW
23
0630
8.0
ly
24
0630
8.0
Y
25
0930
24
0630
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
28
0900
11.0
B
29
1
N
NOFLOW
30
0630
8.0
Y
I NOFLOW
Monthly A-mgc Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly A-gc:
Daily Minimum:
Dully Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2018 (April 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
u
G
=
F
E
h
E
U
6
-
E
u
a
F
E
iJ
'E
¢
E
O
'E
F
@
y
O
`•�
�
U
O
5
t
C
Z
34242
39100
32102
34301
R5811
32106
01034
34320
01042
00720
34336
Annuall
Annually
Annually
Annually
Annually
AnnuallyAnnually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
D2E PHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 clack
H.
2400 clack
H.
VDIN
ug/I
Ibs/da
Ibs/da
Ibs/da
Ibs/da
lbs/day jugA
u
ug/I
ugA I
Ibs/day
1
N
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0600
8.0
Y
NOFLOW
6
0630
8.0
Y
NOFLOW
7
0700
2.5
Y
NOFLOW
8
0730
4.0
Y
NOFLOW
9
0500
8.0
Y
10
0600
8.0
ly
11
0930
24
0630
8.0
Y
12
0600
8.0
Y
13
0600
8.0
Y
14
0600
1.5
Y
15
1300
3.0
Y
NOFLOW
16
0500
9.0
Y
NOFLOW
17
0630
18.0
Y
is
0930
24
0630
8.0
Y
19
0600
8.0
Y
28
0630
8.0
Y
21
1015
1.5
B
NOFLOW
22
1230
2.0
B
NOFLOW
23
0630
8.0
Y
24
0630
8.0
Y
25
0930
24
0630
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
28
0900
1.0
B
29
N
NOFLOW
30
0630
8.0
ly
I NOFLOW
Manlldy Ayemgc Limit:
0,332
0.058
O,U48
0.336
n.068
3.583
0.261
Monikly Aycmge:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2018 (April 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CIiANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
E
U
E
F=
E_
O
n
O
0
t
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNB PIITH
ETHYLBEN
FLUORENE
HEXCLBD
LICE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 ahmk
H.
24000-k
H.
Y/B/N
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/da
Ibs/da
Ibs/day I
Ibs/day
Ibs/da
Ibs/day
1
N
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0600
8.0 IY
I
NOFLOW
6
0630
8.0
Y
NOFLOW
7
0700
2.5
Y
NOFLOW
8
0730
4.0
Y
NOFLOW
9
0500
8.0
Y
10
0600
18.0
IY
11
0930
24
0630
8.0
Y
12
0600
8.0
Y
13
0600
8.0
Y
14
0600
1.5
Y
15
1300
3.0
Y
NOFLOW
16
0500
9.0
Y
NOFLOW
17
10630
8.0
Y
18
0930
24
0630
8.0
Y
19
0600
8.0
Y
20
1
0630
8.0
Y
21
1015
1.5
B
NOFLOW
22
1230
2.0
B
NOFLOW
23
0630
8.0
Y
24
0630
8.0
Y
25
0930
124
0630
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
29
0900
1.0
B
29
N
NOFLOW
30
18.0
IY
I NOFLOW
Monthly A-rtge Limit:
0.061
0.087
0.103
11.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Axemge:
Daily Maximum:
Daily Minimum:
•***NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2018 (April 2018)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q I
E
U
f
E%
E
a
O 1
_
o
O
O
2
2.
34447
34461
34694
34469
34475
34010
34376
34626
34220
39700
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
FLUORANT
26DINITR
ANTHRACE
HCB
2400 clock
Hrr
2400c1nci<
H.
Y/R/N
Ibs/da
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/day
ugh
ug/I
ugA
ugA
I
N
NOFLOW
2
0630
8.0
Y
NOFLOW
3
0630
8.0
Y
NOFLOW
4
0630
8.0
Y
NOFLOW
5
0600
8.0
Y
NOFLOW
6
0630
8.0
Y
NOFLOW
7
0700
2.5
Y
NOFLOW
e
0730
4.0 ly
NOFLOW
9
0500
8.0
Y
10
0600
8.0
Y
11
0930
24 10630
8.0
Y
12
0600
8.0
Y
13
0600
18.0
Y
14
0600
1.5
Y
I5
1300
3.0
Y
NOFLOW
16
0500
9.0
Y
NOFLOW
17
0630
8.0
Y
is
0930
24
0630
8.0
Y
19
1
1
0600
8.0
Y
20
0630
9.0
Y
21
1015
11.5
B
I NOFLOW
22
1230
2.0
B
NOFLOW
23
0630
8.0
Y
24
0630
8.0
Y
25
0930
24
0630
8.0
Y
26
0600
8.0
Y
27
0630
8.0
Y
28
0900
1.0
B
29
N
NOFLOW
30
0630
8.0
Y
NOFLOW
Mnnlhiy A-p Limih
0.087
0.071
0.048
0.081
0.071
0.1184
Mun11J3 M-g.:
Daily Maximum.
Doily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 04-2018 (April 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 05/17/2018
05/15/2018
ORC/Certifier Signature: Michael D Sparks E-Mail:michael.sparks [e-mail] Phone 4:704-480-5793 Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
L_0_iLA 05/17/2018
r
Permittee/Submitter Sign to e:*** Nicole B Coffee E-Mail:[e-mail] celanese.com Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221,402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: C N A Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 04-2018 (April 2018) VERSION: 1.0
Report Comments:
4/11/18, 4/18/18, 4/25/18, Fecal Coliform; below reporting limit.
4/18/18 BOD5 GGA, result is less than control limit.
4/25/18 BOD5 Blank value is outside of control limit.
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4^0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2 R - C F7 "E COUNTY: Cleveland
OWNER NAME: C N A Holdings LLC ORC: Michael D. Spar_ ORC CERT NUMBER: Og� EIVEDINCDENRIDWR
g �R3�?018
GRADE: WW-3. ORC HAS CHANGED: No MAY 0 7 C 111n
eDMRPERIOD: 03-2018 (March VERSION: 1.0 STATUS: Processed
c ) - DV!l13 SECTION WQROS
MOORESVILLE REGIONAL OFFICE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
o I
E
=
E
E
U
E
E
'<
[=
E
F
C
O
H
O
E
F
O 1
0
5
O 1
e
i
C'
Z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annual)
Semi-annually
Annually
Annually .
Recorder
Grab
Composite
m
Coosite
Grab
Composite
Composite
Grab
Grab
FLOW
1.31
Boo -Q1) Daily
TSS -Qty Daily
FCOLI BR
TOTAL N-
TOTAL P -Conc
1,1-DCE
1,l-DCEY
24011 daek
tic
2400.1.0,
H.
YrBIN
mgd
su
Ibs/day
lbs/day
#1100ml
mg/I
mg/I
lbs/day
Ibs/da
1
0530
8.0
Y
NOFLOW
2
0515
8.0
Y
NOFLOW
3
N
NOFLOW
4
1615
2.15
Y
NOFLOW
5
0500
8.0
Y
0.18
18
6
1130
24
0630
8.0
Y
0.257
8.3
8.1
9
7
0630
8.0
Y
0.245
8
0600
8.0
Y
0.211
9
0630
8.0
B
0.201
111
1030
I.0
B
0.206
11
1100
1.0
B
0.217
12
1130
24
0630
8.0
B
0,202
8
4
5.6
22
13
0630
8.0
B
0.258
14
0600
8.0
1 B
0.243
15
0615
8.0
B
0.255
16
0615
8.0
B
0.24
17
1030
1.0
B
0.269
IS
0930
3.0
B
1
0.29
19
1130
24
0630
8.0
Y
1
0.296
8.2
8.4
11.4
17
20
0630
8.0
Y
0.267
21
0630
8.0
Y
0.347
22
0600
8.0
Y
0.343
23
0630
8.0
Y
0.353
24
0945
2.5
1 Y
0.395
25
0900
3.0
0.409
26
0600
8.0
0.394
27
0600
8.0
0,389
20
28
1130
24
0630
8.0
Ny
0.371
8.1
10.8
19.2
29
0600
8.0
0.326
J11
1000
1.5
0.305
31
1000
1.0
B
0.284
Manthtr A-mgc Limit:
0.45
68
124
200
0.071
0.052
Monthly Atcragce
0.287148
7.825
11.3
19.155501
Daily Maximum
0.409
8.3
10.8
19.2
22 '
Daily Minimum:
0.18
8
4
5.6
17
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather, NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2018 (March 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE': NO (Continue)
A
F
V
E
u
F.
F
O
-
O
o`
m
t
Z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
A nnually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
I _-DCB
1,2-DCE
1,2-DCP
I-12DCEY
1,3-DCPE
1,3-DCB
1,4-DC4
2,4-DCPH
2,4.DMPH
2,4-DNPH
2,4-DNT
2400 dock
Wr
2400 clock
It.
Y/B/N
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/da
Ibs/day
Ibs/day
Ibs/da
1
0530
8.0
Y
NOFLOW
2
0515
8.0
Y
NOFLOW
3
N
NOFLOW
4
11615
2.15 1
Y
NOFLOW
5
0500
8.0
Y
6
1130
24
0630
8.0
Y
7
0630
8.0
Y
8
0600
8.0
Y
9
0630
8.0
B
10
1030
1.0
B
11
11100
1.0
B
12
1130
24
0630
18.0
B
13
0630
8.0
B
14
0600
8.0
B
15
0615
8.0
B
16
0615
8.0
B
17
1030
1.0
1 B
1s
0930
3.0
B
19
1130
24
0630
8.0
Y
20
0630
8.0
Y
21
0630
8.0
Y
22
1
10600
18.0
Y
23
Y
24
2.5
Y
25
r638.0
3.0
Y
26
8.0
Y
27
8.0
Y
28
1130
24
0630
8.0
Y
29
0600
8.0
Y
30
1000
1.5
Y
31
1000
1.0
B
Monthly A,-gc Limit:
0.249
0.219
0.494
0.068
n.n94
0.1
0.048
0.126
0.058
0.229
0.365
Monthly A,-gc:
Duiiy M1Liiimum:
Dully Mini--
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility
CLASS: WW-2
OWNER NAME: C N A Holdings LLC
ORC: Michael D. Sparks
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 03-2018 (March 2018)
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE': NO (Continue)
a
G
E
E
E
V
_
a
12 1
E
O
E
O
O
5
C
Z
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPIIENOL
2NPIIENOL
34-BNZFA
46DN-n-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONT
BENZENE
BNZO-A-A
BNZO-A-P
2400 dad<
H.
2400 d-1,
11"
Y/B/N
Ibs/da
Ibs/day;
ug/1
Ibs/day
Ibs/da
Ibs/day
Ibs/da
ug/l
lbs/day
ugA
ugA
1
0530
8.0
Y
NOFLOW
2
0515
8.0
Y
NOFLOW
3
N
NOFLOW
4
1615
2.15
Y
NOFLOW
5
0500
8.0
Y
6
1130
24
0630
8.0 ly
7
0630
8.0
Y
8
0600
8.0
Y
9
0630
8.0
B
111
1030
1.0
B
11
1100
1.0
B
12
1130
24
0630
8.0
B
13
0630
8.0
B
14
0600
8.0
B
'
15
0615
8.0
B
16
0615
8.0
B
17
1030
1.0
B
i9
0930
3.0
B
19
1130
24
0630
8.0
IY
20
0630
8.0
Y
21
0630
8.0
Y
22
0600
8.0
Y
27
0630
8.0
Y
24
0945
2.5
Y
25
0900
3.0
Y
26
0600
9.0
Y
27
0600
8.0
Y
28
1130
24
10630
8.0
Y
29
0600
8.0
Y
30
1000
1.5
Y
31
1000
1 1.0
B
Monthly A-ge Limit:
0.1
0.13E
0.252
0.232
0.071
0.071
0.119
Momhly A-gc:
DMy M..inmm:
Daily Minhnam:
****NoReportingReason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: C N A Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 03-2018 (March 2018) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
u
E
F
_
E
E
a
F
E
E
F
_
a
O
w
O
E
O
o`
U
O
6
t
z
2
34242
3910D
3210E
34301
35811
32106
01034
34320
01042
00720
34336
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
B2EPHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 0-k
Itr.,
240001eeh
Hr.
Y/B/N
ugA
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/da
ugg/I
ugA
ugA
ugA
Ibs/da
1
0530
8.0
Y
NOFLOW
2
0515
8.0
Y
NOFLOW
3
N
NOFLOW
4
1615
2.15
Y
NOFLOW
5 10500
18.0
Y
6
1130
24
0630
8.0
Y
7
0630
8.0
Y
8
0600
8.0
Y
9
0630
8.0
B
10
1030
1.0
B
11
1
11100
11.0
B
12r061130
24
0630
8.0
B
13
30
8.0
B
14
0600
8.0
B
15
0615
8.0
B
l6
0615
18.0
B
17
1030
1.0
B
18
0930
3.0
B
19
1130
24
0630
9.0
Y
20
0630
8.0
Y
21
0630
18.0
Y
22
0600
8.0
Y
23
0630
8.0
Y
24
0945
2.5
Y
25
0900
3.0
Y
26
0600
9.0
Y
27
0600
8.0
28
1130
24
0630
8.0
29
0600
8.0
FBI
30
1000
I.5
31
1000
1.0
Monthly Average Limit:
0.332
0.058
0.049
0.336
0.068
3.583
0.261
Munlhty Avenge:
Doily M..imom:
Dniiy Minlmmn:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: C N A Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 03-2018 (March 2018) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
E
E
E
U
E
E
=
F
E
F
6
-
a
O 1
y
O
e
r
o
O
oL
C
O
5
K
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNBPHTH
ETHYLBEN
FLIIORENE
HEXCLBD
HCE
LEAD
METHYLCH
MECL2
NAPrHALE
NICKEL
2400 clack
Hn
2400 cl-k
Hcc I
Y/B/N
Ibs/day I
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/day
Ibs/da
Ibs/da
Ibs/day
1
0530
8.0
Y
NOFLOW
2
0515
8.0
Y
NOFLOW
3
N
NOFLOW
4
1615
2.15
Y
NOFLOW
5
0500
8.0
Y
6
1130
24
0630 18.0
Y
7
Y
8
8.0
Y
9
r06308.0
8.0
B
10
1.0
B
u
1100
1.0
B
12
1130
24
0630
8.0
B
13
0630
8.0
B
14
0600
8.0
B
15
0615
8.0
B
16
0615
8.0
B
17
1030
1.0
B
18
0930
3.0
B
19
1130
24
0630
8.0
Y
20
0630
8.0
Y
21
0630
8.0
Y
22
0600
8.0
Y
23
0630
8.0
Y
24
0945
2.5
Y
25
0900
3.0
JY
26
0600
9.0
Y
27
0600
8.0
Y
28
1130
24
0630
8.0
Y
29
0600
8.0
Y
30
1000
1 1.5
Y
31
1
1 1000
1.0
B
Monthly Average Limit:
0061
11.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly A, -p:
Doilk Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2018 (March 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
O
E
E
U
=
a
F
fi
O
O
o`
U
C
O
Y
a
Z
34447
00556
TGP3B
34461
34694
34469
34475
34010
39700
34376
34220
Annually
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
NITROBEN
OI4CRSE
CERI7DPP
PHENANTH
PHENOL
PYRENE
T ETCLETY
TOLUENE
HCB
FLUHRACE
.RINT
ANT
2400r1re1,
Hre
2400 0-1,
Hn
Y/B/N
Ibs/da
mg/I
ass/fail
Ibs/day
Ibs/day
Ibs/day
Ibs/da
lbs/day
ugA
ugA
ugA
1
0530
8.0
Y
NOFLOW
2
0515
8.0
Y
NOFLOW
3
N
NOFLOW
4
1615
2.15
Y
NOFLOW
5
0500
8.0
Y
6
1130
24
0630
8.0
Y
<5
PASS
7
0630
8.0
Y
s
1
0600 18.0
Y
9
0630
8.0
10
1030
1.0
I
1100
1.0
rB
12
1130
24
0630
8.0
13
0630
18.0
B
14
8.0
15
8.0
16
r093101
8.0
r-
17
1.0
is
3.0
19
1130
24
0630
8.0
Y
20
0630
8.0
Y
21
0630
8.0
Y
22
0600
8.0
Y
23
0630
8.0
Y
24
1
10945
12.5
Y
25
3.0
Y
26
8.0
Y
27
r0600
8.0
Y
28
1130
24
9.0
Y
29
0600
18.0
IY
30
1000
1.5
1 Y
31
1000
1.0
1 B
Monthly At'enrg* Llmit:
0.087
0.071
0.048
0.081
0.071
0.084
Monthly A-gn
0
Datk M-imom:
0
Daily Minimum:
0
****NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2018 (March 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
E
U
E
E
u
F
E
i
Q
c
O
n
F
O
o`
x
O
L
Z
34626
00010
00300
Annually
Grab
Calculated
Calculated
26DINITR
TEMP-C
DO
2400 clock
Hn
2400 clack
H. I
Y/B/N I
ug/I
deg c
mgA
1
0530
8.0
Y
NOFLOW
2
0515
8.0
Y
NOFLOW
3
N
NOFLOW
4
1615 12.15
Y
NOFLOW
5
0500
8.0
Y
6
1130
24
0630
8.0
Y
12.6
7.6
7
0630
8.0
Y
8
0600
8.0
Y
9
0630
8.0
B
10
1030
1.0
B
11
1100
1.0
B
12
1130
24
0630
8.0
B
9.5
10
13
0630
8.0
B
14
0600
8.0
B
15
0615
8.0
B
16
0615
8.0
B
17
1030
1.0
B
18
0930
3.0
B
19
1130
24
0630
8.0
Y
13.9
8.9
20
0630
8.0
Y
21
10630
8.0
Y
22
0600
8.0
Y
23
0630
8.0
Y
24
0945
2.5
Y
25
0900
3.0
Y
26
1
0600
8.0
ly
27
0600
9.0
Y
28
1130
24
0630
8.0
Y
12.3
9.4
29
0600
8.0
Y
30
1000
1.5
Y
31
1000
1.0
B
M-11dy M-g. Limit:
Monthly A,-p:
12.075
8.975
Dni1y Mn.�imum:
13.9
10
Daily Mi.h--
9.5
17.6
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 03-2018 (March 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 04/16/2018
04/13/2018
ORC/Certifier Signature: Michael D Sparks E-Mail:michae1.sparks rr celanese.com Phone 4:704-480-5793 Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
�:04/16/2018
Permi'Ctee/Submitter SignattYre�*/** Nicole B Coffee E-Mail:nicole. coffee a celanese.corn Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221, 402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.nedenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*-No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2 COUNTY: Cleveland
OWNER NAME: C N A Holdings LLC ORC: Michael D. Sparks ORC CERT NUMBER: 987732
GRADE: WW-3. ORC HAS CHANGED: No
eDMR PERIOD: 03-2018 (March 2018) VERSION: 1.0 STATUS: Processed
Report Comments:
03/06/18 BOD:Difference between sample dilution is greater than 30%. Blank value is outside of the control limits. Oil & Grease is below reporting limits.
03/19/18 BOD:Blank value is outside of the control limits.

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2018 (February 2018)
3
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 @` ® �=��O�7NTY: Cleveland
ORC: Michael D. Sparks sI ORC CERT NUMBER��Ei�/NCE1E( Rfi)VVR
ORC HAS CHANGED: No APR 02 2018
ENI-1.c I
VERSION: 1.0 /'tl. F-OLATUS: Processed
- DWR SECTION
VVQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISC A -V� ►OIONAL OFFICE
E
2
::
E
E
F
E
-n
-
'E
a
O
O
E
O
-
w
u
O
R
m
t
C
Z
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
WeeklyWeekly
Weekly
WeeklySemi-annual)
Semi-annual)
Annual)
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
Boo - Qty Dully
TSS- Qty Daily
FCOLI Bit
TOTAL N -
TOTAL P- Caac
1,1-DCE
1,1-1)CEY
2400 clock
Jim
2400 clock
H.
YfB/N
mgd
su
Ibs/day
Ibs/day
9/100mI
MM
mg/l
Ibs/day
Ibs/day
1
0600
8.0
1 Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
N
NOFLOW
4
1515
2.0
Y
NOFLOW
5
0500
8.0
Y
0.409
18
6
1130
24
0630
8.0
Y
0.341
8.3
< 5.7
7.7
7
1
0500
9.5
Y
0.426
S
0600
8.0
Y
0.408
0630
18.0
Y
1
0.401
10
0830
3.0
Y
0.45
it
0900
3.5
Y
0.429
12
1130
24
0630
8.0
Y
0.439
8.1
19.9
9.5
10
<0.6
<0.05
13
0630
8.0
Y
0.441
14
0630
8.0
Y
0.449
15
0600
8.0
1 Y
10.441
16
0630
8.0
Y
0.447
17
1100
1.0
B
0.424
is
1000
2.0
Y
0.375
19
0630
8.0
Y
0.372
19
20
1130
24
0630
8.0
Y
10.393
8.1
18.8
18.4
21
0530
8.0
Y
0.352
22
0600
8.0
Y
0.315
23
0515
8.0
Y
0.265
24
1000
2.0
Y
0.244
25
1200
2.0
B
NOFLOW
26
0630
Is,0
1B
NOFLOW
27
0630
8.0
Y
NOFLOW
29
0630
8.0
Y
NOFLOW
Monthly Avctaae Limit:
0.45
68
124
200
0.071
0.052
Monthly Avemgv
0.39105
9.533333
11.866667
15.066373
0
0
Dany Maximum:
0.45
8.3
19.8
18.4
19
0
0
Daily Minimum:
0.244
18.1
10
17.7
1 10
0
0
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2018 (February 2018)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
`
E
F
4
•"
E
r
E
u
3
E
'E
6
@
O
2
F
O
-
o
C
O
C
Z
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4.DCPH
2,4-Dh1PH
2,4-DNPH
2,4-DNT
2400 clock
H.
2400 clock
Hrs
YB/N
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/day
Ibs/day
Ibs/day
Ibs/day,
Ibs/da
Ibs/day
Ibs/da
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
N
NOFLOW
4
1515
2.0
Y
NOFLOW
5
0500
9.0
Y
6
1130
24
0630
8.0
Y
7
0500
9.5
1 Y
8
0600
8.0
Y
9
0630
8.0
Y
10
0830
3.0
Y
11
0900
3.5
Y
12
1130
24
0630
8.0
Y
13
0630
18.0
Y
14
0630
8.0
Y
is
0600
8.0
Y
16
0630
8.0
Y
17
1100
1.0
B
18
1000
2.0
Y
19
0630
18.0
Y
20
1130
24
0630
8.0
Y
21
0530
8.0
Y
22
0600
8.0
Y
23
0515
8.0
Y
24
1000
2.0
Y
25
1 1200
12.0
1 B
NOFLOW
26
0630
8.0
B
NOFLOW
27
0630
8.0
Y
NOFLOW
28
0630
8.0
Y
NOFLOW
Monthly A-mitc Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.059
0.229
0.365
Monthly A -p:
rally Minimum;
DOih• Minimum:
****NoReportingReason: ENFRUSE=No Flow-Re11se/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2018 (February 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2
G
E
E
U
-
E
F.
!
2
`E
O
O
O
-
C
O
gg
L
Z
34596
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-oC
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clock
H.
2400 cluck
It.
Y/B/N
Ibs/day
I Ibs/day
um
1 Ibs/day
Ibs/da
Ibs/da
lbs/day
lugA
lbs/day
lugAug/I
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
N
NOFLOW
4
11515
2.0
Y
NOFLOW
5
0500
8.0
Y
6
1130
24
0630
8.0
Y
7
0500
9.5
Y
8
0600
8.0
Y
9
0630
8.0
Y
10
0830
3.0
Y
11
0900
3.5
Y
12
1130
24
0630
8.0
Y
13
0630
8.0
Y
14
0630
8.0
Y
15
0600
8.0
Y
16
0630
8.0
ly
17
1100
1.0
B
is
1000
2.0
Y
19
0630
8.0
Y
20
1130
24
10630
8.0
Y
21
0530
8.0
Y
22
0600
18.0
Y
23
0515
8.0
Y
24
1000
2.0
Y
25
2.0
B
NOFLOW
26
8.0
B
NOFLOW
27
L063
8.0
Y
NOFLOW
28
8.0
Y
NOFLOW
Monthly Arcmgc Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly A-gc:
Dully MWmam:
Dully MO.-
**** No Reporting Reason: ENFRUSE = No Flow-Retise/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2018 (February 2018)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
c
fi
6
E
d
fi
n
F
F
'E
<
O
O
O
_
_
V
O
S
C
z°.
34742
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
Annually
AnnuallyAnnually
AnnuallyAnnuallyAnnually
AnnuallyAnnuallyAnnuallyAnnuallyAnnually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
BNZO-K-F
BZE PHTH
CARBNTET
CHLROBNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CHRYSENE
COPPER
CN-TOT
DIETY-PH
2400 clock
Firs
2400 clock
H.
Y/B/N
ugA
Ibs/da
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/I
ug/I
ugA
u0/I
Ibs/da
1
0600
8.0 ly
NOFLOW
2
0630
8.0
Y
NOFLOW
3
N
NOFLOW
4
1515
2.0
Y
NOFLOW
5
0500
18.0
Y
6
1130
24
0630
9.0
Y
7
10500
9.5
Y
e
0600
8.0
Y
9
0630
8.0
Y
10
0830
3.0
Y
11
0900
3.5
IY
12
1130
24
10630
8.0
Y
13
0630
8.0
Y
14
0630
8.0
Y
15
0600
9.0
Y
16
0630
9.0
Y
17
1100
1.0
B
Is
1000
2.0
Y
19
0630
9.0
Y
20
1130
24
0630
8.0
Y
21
0530
8.0
Y
22
0600
8.0
Y
23
0515
8.0
Y
24
1000
2.0
Y
25
1200
2.0
B
NOFLOW
26
0630
8.0
B
NOFLOW
'
27
0630
8.0
Y
NOFLOW
2s
0630
8.0
Y
NOFLOW
Monthly A—agc Llmin
0.332
0.059
0.049
0.336
0.068
3.583
0.261
Monthly A.'croac:
Dully W.I.—
Dolly Minimum:
•"' No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV WTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2018 (February 2018)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
G
E
u
E
F.
E
u
v
F=
—°�,
O
O
E
O
o
U
O
ryry
C
Z
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNBPHTH
ETHYLBEN
FLUORENE
HEXCLBD
HCE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 dock
It.
2400 dock
n.
YIBIN
I Ibs/day
Ibs/day
I Ibs/day
Ibs/day
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/day
1 Ibs/day
Ibs/day
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
N
NOFLOW
4
1515
2.0
Y
NOFLOW
5
0500
8.0
Y
6
1130
124
0630
18.0
Y
7
0500
9.5
Y
x
0600
8.0
Y
9
0630
8.0
IY
10
0830
3.0
Y
11
0900
3.5
Y
12
1130
24
0630
8.0
Y
13
0630
8.0
Y
14
0630
8.0
Y
15
0600
8.0
Y
16
0630
8.0
Y
17
1100
1.0
B
is
1000
2.0
Y
19
0630
9.0
Y
20
1130
24
0630
9.0
Y
21
0530
9.0
Y
22
0600
8.0
Y
23
0515
9.0
ly
24
1000
2.0
Y
25
1200
2.0
B
NOFLOW
26
0630
8.0
B
NOFLOW
27
0630
8.0
Y
NOFLOW
28
0630
8.0
Y
ILOFLOW
Monthly Avemp Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2,227
0.278
0.129
0.071
12.846
Monthly A -rap:
Daily Mmilru m:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2018 (February 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
°
C
E
F
_
,E�
E
U
E
~
E
u°
F-
<
O
y
1 O
On
U
O
:
f
8
C
Z
34447
34461
34694
34469
34475
34010
39700
34376
34220
34626
00010
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Calculated
NITROBEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
NCB
FLUORANT
ANTHRACE
26DINITR
TEMP-C
2400 clack
H.
2400 clock
Hn
YtBiN
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/day
lbs/day
ugA
ugA
ugA
ugA
deg c
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
N
NOFLOW
4
1515
2.0
Y
NOFLOW
5
0500
8.0
Y
6
1130
124
0630
18.0
Y
7
7
0500
9.5
Y
8
0600
8.0
Y
9
0630
8.0
Y
10
0830
3.0
ly
11
0900
3.5
Y
12
1130
24
10630
8.0
Y
12.3
13
0630
8.0
Y
14
0630
8.0
Y
15
0600
8.0
Y
16
0630
18.0
Y
17
1100
1.0
B
I8
1000
2.0
Y
19
0630
8.0
Y
20
1130
24
0630
8.0
Y
14.1
21
0530
8.0
Y
22
0600
8.0
Y
23
1
0515
18.0
Y
24
1000
2.0
Y
25
1200
2.0
B
NOFLOW
26
0630
8.0
B
NOFLOW
27
0630
8.0
Y
NOFLOW
26
0630
9.0 ly
I NOFLOW
Monthly Me.gu Limit:
0.087
0.071
0.048
0.081
0.071
0.084
M.Ohly Av gc:
11.133333
DAy Maximum:
14.1
Daily Minimum:
7
****No Reporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2018 (February 2018)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
c'
E
U
u°
a
F.
a
O
O
o
s
O
a
ZZ
00300
Calculated
DO
2400 clock
fin
2400 clock
Hr.
MIN
M90
1
0600
8.0
Y
NOFLOW
2
0630
8.0
Y
NOFLOW
3
N
NOFLOW
a
1515
2.0
Y
NOFLOW
s
0500
8.0
Y
6
1130
24
0630
8.0
Y
11.5
%
1
10500
9.5
1 Y
s
0600
8.0
Y
9
0630
8.0
Y
10
0830
3.0
Y
11
0900
3.5
Y
12
1 1130
24
10630
8.0
1 Y
9.9
13
0630
8.0
Y
is
0630
8.0
Y
Is
0600
8.0
Y
16
0630
8.0
Y
17
1100
1.0
B
Is
1000
2.0
Y
19
0630
8.0
Y
20
1130
24
0630
8.0
Y
8.5
21
0530
18.0
Y
22
0600
8.0
Y
23
0515
8,0
Y
24
1000
2.0
Y
25
1200
2.0
B
NOFLOW
26
0630
8.0
B
NOFLOW
27
0630
8.0
Y
NOFLOW
28
1
10630
8.0
Y
NOFLOW
Monthly A-mae Limlt:
Mamhly A -raga :
9.966667
Daily m"Imum:
11.5
Daily Minimum:
8.5
**** No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR= No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY =No Visitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
cDMR PERIOD: 02-2018 (February 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 03/26/2018
03/19/2018
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
03/26/2018
PermAee/Submitter Signature:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Penn ittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221, 402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: C N A Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 02-2018 (February 2018)
Report Comments:
CLASS: W W-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
BOD 02/06/18 Below Reporting Limit, GGA result is less than the control limit
BOD 02/12/18 Difference between sample dilutions is greater than 30%, Blank value is outside of control limits.
Total Nitrogen and Total Phosphorus 02/12/2018 Below Reporting Limit
BOD 02/20/18 GGA result is less than the control limit
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
PERMIT STATUS: Active
3
FACILITY NAME: Celanese -Shelby Facility
CLASS: WW-2
® fCYUNTY: Cleveland
d2018
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
n ^ORC CERT NUMBER: 987732
'VIPs 0
RECEIVEEVNICDENR1DM
GRADE: WW-3.
ORC RAS CHANGED: No
eDMR PERIOD: 01-2018 (January 2018)
VERSION: 1.0
CENTRAL RAL F11-,r. a STATUS: Processed
SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: WROS
MOORESVILLE REGIONAL OFFICI
O
4
m
V
a
fi
F
E
6
O
l-F
O
in
O
i
50050
00400
QD310
QD530
31616
C0600
C0665
3 496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annual)
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
BOD-Qty Daily
TSS-Qty Daily
FCOLI BR
TOTALN-
TOTALP-Cone
l,l-DCE
I,1•DCEY
2400 clock
Hn
2400 clock
IH.
WRIN
m d
so
Ibs/day
Ibs/day
#/100ml
mg/l
mg/I
I Ibs/day
Ibs/day
1
0900
3.5
B
0.429
2
1130
24
0630
8.0
Y
0.379
8.3
<6.3
7.9
7
3
0630
8.0
Y
0.329
4
0600
8.0
Y
0.373
5
0530
10.0
Y
0.33
6
0915
15.5
Y
1
0.268
7
1100
4.50
Y
0.303
8
0500
10.0
Y
10.382
19
9
1130
24
0630
8.0
Y
0.4
8.1
<6.7
8.7
10
0630
8.0
Y
0.397
11
0600
9.0
Y
0.358
12
0630
8.0
Y
0.373
13
1100
1.0
B
0.41
14
0930
2.5
Y
0.387
15
0930
3.0
Y
0.389
16
1130
24
10500
9.0
Y
0.387
18.1
<6.5
9.4
11
17
0630
8.0
Y
0.363
IS
0700
8.0
Y
0.378
19
0600
8.5
Y
0.353
20
1120
2.0
B
NOFLOW
21 1
1630
2.0
B
NOFLOW
22
0630
8.0
Y
0.238
23
1130
24
0630
8.0
Y
0.357
8.1
<6
8
21
24
0630
8.0
Y
0.373
25
0600
8.0
Y
0.347
26
0630
8.0
Y
0.3
27 1
N
NOFLOW
28
1515
1.0
B
NOFLOW
29
0500
9.50
Y
NOFLOW
30
0630
8.0
Y
NOFLOW
31
0630
8.0 1
Y
NOFLOW
Monthly Average Limit:
0.4.
68
124
200
0.071
0.052
Monthly Average:
0.358458
0
8.5
13.239327
Daily Maximum:
0.429
8.3
0
9.4
21
Daily Minimum:
0.238 18.1
10
17.9
7
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather, NOFLOW =No Flow; HOLIDAY =NoVisitation -Holiday

• NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2018 (January 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC. Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Emmommmmmom
****NoReportingReason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather, NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

I
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2018 (January 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Omommmommomm
****No Reporting Reason: ENFRUSE = No Flow-Reuse(Recycle; ENV WTHR= No Visitation —Adverse Weather, NOFLOW = No Flow; HOLIDAY = No Visitation —Holiday

Y
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2018 (January 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
—
R
•**•NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather, NOFLOW=No Flow; HOLIDAY= No Visitation —Holiday

s
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2018 (January 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
mommmmmommm
"*'NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather, NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

I
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2018 (January 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
mommmmommmm
PRIM
Monthly Average:
•"'NoReporting Reason: ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation —Adverse Weather, NOFLOW=No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2018 (January 2018)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
d
3
e`
U
5
F
F
a
O
0
o
O
ti
O
a
ci
z
00300
Calculated
DO
2400 clock
H.
2400 clock
Ilin
wB/N
I
mgfl
1
0900
3.5
B
2
1130
24
0630
8.0
Y
13.6
3
0630
8.0
Y
4
0600
8.0
Y
5
0530
110.0
1 Y
6
0915
5.5
Y
7
1100
4.50
Y
8
0500
10.0
Y
9
1130
124
0630
8.0
Y
1
12.9
10
0630
9.0
Y
11
0600
9.0
Y
12
0630
8.0
Y
13
1100
1.0
B
14
0930
2.5
Y
15
0930
3.0
Y
16
1130
24
0500
9.0
Y
12.1
17
0630
8.0
Y
18 1
0700
8.0
Y
19
0600
8.5
Y
20
1120
2.0
B
NOFLOW
21
1630
2.0
B
NOFLOW
22
0630
8.0
Y
23
1130
24
0630
8.0
Y
11.3
24
0630
8.0
Y
25
0600
8.0
Y
26
0630
8.0
Y
27
N
NOFLOW
28
1515
1.0
B
NOFLOW
29
0500
9.50
Y
NOFLOW
30
0630
8.0
Y
NOFLOW
31
0630
8.0
Y
NOFLOW
Monthly Average Unalh
Monthly Avenge:
12.475
Daily Maximum:
13.6
Daily Minimum:
11.3
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather, NOFLOW =No Flow; HOLIDAY =NoVisitation -Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 01-2018 (January 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 02/23/2018
_C,iC_�: 02/19/2018
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
02/23/2018
Perm6tee/Submitter SignatiVe* Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC, Prism Laboratories INC
CERTIFIED LAB #: 221, 402
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
PERMIT VERSION: 4.0
PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
CLASS: WW-2
COUNTY: Cleveland
OWNER NAME: Cna Holdings LLC
ORC: Michael D. Sparks
ORC CERT NUMBER: 987732
GRADE: WW-3.
ORC HAS CHANGED: No
eDMR PERIOD: 01-2018 (January 2018)
VERSION: 1.0
STATUS: Processed
Report Comments:
BOD 1/02/18 Below Reporting Limit
BOD 1/09/18 Below Reporting Limit
BOD 1/16/18 Below Reporting Limit, GGA result is less than the control limit
BOD 1/23/18 Below Reporting Limit

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2 RECEIVED COUNTY: Cleveland
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks 1� {� f� ORC CERT NUMBER: 987732
GRADE: WW-3. ORC HAS CHANGED: No JAN 2 � ZM RECEIVEDINI-DENR/DWR
eDMR PERIOD: 12-2017 (December 2017) VERSION: 1.0 CEN_I f-,AL FILES STATUS: Processed
rjWR 85CTION FEB 201
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NiQRos
MOORESVILLE REGIONAL OFFICE
C
E
L-
n
V
E
u
w
F-
E
F
'E
-
x
O
y
e
C
O
V
O
m
c
5
Z
50050
00401)
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annually
Semi-annually
Annually
Annually
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pit
ROD -Qty Daily
TSS -Qly Daily
FCOLI BR
TOTAL N-
TOTAL P-Cone
Ll-DCE
1,1-DCEY
2400 dock
urs
2400 clock
lin
W/RIN
mgd
so
Ibs/day
Ibs/day
I #/I00ml
mg/I
mgfl
I Ibs/day
Ibs/day
1
0630
8.0
Y
0.408
2
0600
3.0
Y
NOFLOW
3
1500
3.0
Y
NOFLOW
4
0500
8.0
Y
0.317
5
5
1130
24
10630
8.0
1 Y
0.38
8
1< 6.3
10.5
6
0630
8.0
Y
0.38
7
0600
8.0
Y
0.334
8
0630
8.0
Y
NOFLOW
9
0830
4.0
Y
NOFLOW
to
0730
18.0
Y
NOFLOW
11
0630
8.0
Y
0.308
7
12
1130
24
0630
8.0
Y
0.337
7.9
< 5.6
7
13
10600
8.5
Y
0.357
14
0600
8.0
Y
0.347
15
0630
8.0
Y
0.284
16
0800
1.5
Y
0.208
17
N
NOFLOW
is
0500
8.5
Y
NOFLOW
19
0600
8.5
Y
NOFLOW
20
0600
8.5
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0600
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
2$
N
NOFLOW
26
2.0
B
NOFLOW
27
8.0
B
NOFLOW
28
q13002.0
8.0
B
NOFLOW
29
8.0
B
NOFLOW
30
B
NOFLOW
31
1400
3.0
B
NOFLOW
Monthly Average Limit:
0.45
68
124
200
0.071
0.052
Monthly Average:
0.332727
0
8.75
5.91608
DailyAlaaimum.
0.408
8
0
10.5
7
Daily Miuimnm:
0.208
7.9
0
7
5
**** No Reporting Reason: ENFRUSE = No Flow-Rcuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2017 (December 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
[-
�
E
E
V
E
F-
—
'x
t=
P
>
_
O
C
e
O
o`
O
a
C
2
34536
32103
34541
34M6
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Crab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
la-DCB
1,4-DCB
2,4-DCPII
2,4-DMPn
2,4-DNPII
2,4-DINT
2400 clod:
tlrs
2400 clock
llra
Y/B/N
Ibs/day
I Ibs/day
lbs/day I
Ibs/day
Ibs/day
Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I Ibs/day
1
0630
8.0
Y
2
0600
3.0
Y
NOFLOW
3
1500
3.0
Y
NOFLOW
4
0500
8.0
Y
5
1130
24
10630
8.0
Y
6
0630
8.0
Y
7
0600
8.0
Y
8
0030
18.0
Y
NOFLOW
9
0830
4.0
Y
NOFLOW
10
0730
8.0
Y
NOFLOW
11
0630
8.0
Y
12
1130
24
0630
8.0
Y
13
0600
3.5
Y
14
0600
8.0
Y
15
0630
8.0
Y
16
0800
1.5
Y
17
N
NOFLOW
18
0500
8.5
Y
NOFLOW
19
0600
8.5
Y
NOFLOW
20
0600
18.5
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0600
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
N
NOFLOW
26
11:00
B
NOFLOW
27
0630
B
NOFLOW
2s
0600
L3.O
B
NOFLOW
29
0630
B
NOFLOW
30
1300
B
NOFLOW
31
1400
B
NOFLOW
Monthly Average Urnit:
0.749
0.219
0.494
0.068
0.094
0.1
0.048
0.126
0.0$8
0.229
0.365
Monthly Average:
Dauy Madtnutn:
Dauv nunlntun,:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2017 (December 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
E
F
h
E
V
E
E
T
F
E
'�
-
O
h
E
i-
E
C
_
o
z
C
,=
ii
x
2
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Annual) Y
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPFIENOL
2NPHENOL
34-BNZFA
46ON-o-C
4NPHEN01.
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZ,O-A-A
BNZO-A-P
2400 clock
Hrs
2400 clock
Hrs
Y/B/N
Ibs/day
Ibs/day
ug/l
Ibs/day
Ibs/day
Ibs/day
Ibs/day
ug/I
I Ibs/day
ug/1
I ug/1
1
0630
8.0
Y
2
0600
3.0
Y
NOFLOW
3
1500
3.0
Y
NOFLOW
4
0500
8.0
Y
5
1130
24
0630
9.0
Y
6
0630
8.0
Y
7
10600
8.0
Y
8
0630
8.0
Y
NOFLOW
9
0830
4.0
Y
NOFLOW
to
0730
8.0
Y
NOFLOW
.11
0630
8.0
Y
12
1130
24
0630
8.0
Y
13
0600
18.5
Y
14
0600
8.0
Y
15
0630
8.0
Y
16
0800
1.5
Y
17
N
NOFLOW
18
0500
8.5
Y
NOFLOW
19
0600
8.5
Y
NOFLOW
20
0600
8.5
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0600
8.0
ly
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
xs
N
NOFLOW
26
11:00
2.0
B
NOFLOW
27
0630
8.0
B
NOFLOW
28
0600
8.0
JB
I NOFLOW
29
0630
8.0
B
NOFLOW
30
1300
2.0
B
NOFLOW
31
1400
3.0
B
NOFLOW
Monthly Average Limit:
0.1
0.132
0.252
0.232
0.071
0.071
0.119
Monthly Average:
Daily Maximum:
Daily Minimum:
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2017 (December 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
c
cEE
u
A
-
E
U
E
F
v
F-
E
a
O
n
O
O
O
O
o
n
a
4
34242
39100
32102
34301
85811
32106
01034
34320
01042
00720
34336
A'E nnually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
RNZO-K-F
112E PATH
CARBNTET
CHLRORNZ
CLROETHA
CHLRFORM
Cr-TOTAL
CRRYSENE
COPPER
CN-TOT
D1ETY-PH
2400 cinch
urs
2400 clock
urs
Y/RiN
ug/l
Ibs/day I
lbs/day
lWday I
Ibs/day
Ibs/day I
ug[I
ug/l
ug/l
ug/l
lbs/day
1
0630
8.0
Y
2
0600
3.0
Y
NOFLOW
3
1500
3.0
Y
NOFLOW
4
0500
8.0
Y
5
1130
24
0630
8.0
Y
6
0630
8.0
Y
7
0600
18.0
Y
s
0630
8.0
Y
NOFLOW
9
0830
4.0
Y
NOFLOW
a
0730
8.0
Y
NOFLOW
11
0630
8.0
Y
12
1130
24
0630
8.0
Y
13
0600
8.5
Y
14
0600
8.0
Y
15
0630
8.0
Y
16
0300
L5
Y
17
N
NOFLOW
1s
0500
8.5
Y
NOFLOW
19
0600
8.5
Y
NOFLOW
20
0600
8.5
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0600
8.0
IY
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
N
NOFLOW
26
11:00
2.0
NOFLOW
27
0630
8.0
NOFLOW
28
0600
8.0
JB
NOFLOW
29
0630
8.0
NOFLOW
30
1300
2.0
B
NOFLOW
31
1400
13.0
B
I NOFLOW
Monthly Average Limib
0.33E
0.058
0.048
0.336
0.068
3.583
0.261
Monthly Average:
Daily Maximum:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation— Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2017 (December 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
C
E
_
6
V
FE-,
i
1=
E
i=
O
E
-
0
O
V
O
=
C
C.
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PII
DNB P117'II
ETIIYLHEN
FLUORENE
IIE.XCI,BD
IICE
LEAD
METIIYLCII
NIECL2
NAPTHALE
NICKEL
2400 clock
Hrs
2400 clock
Ilrs
Y/B/N
Ibs/day
Ibs/da
Ibs/day
tbs/day
Ibs/day
Ibs/day
Ibs/day,
Ibs/day
Ibs/day
Ibs/day
1 Ibs/day
1
0630
8.0
Y
2
0600
3.0
Y
NOFLOW
3
1500
3.0
Y
NOFLOW
4
0500
8.0
Y
5
1130
24
0630
8.0
Y
6
0630
8.0
Y
7
0600
8.0
Y
8
0630
8.0
Y
NOFLOW
9
0830
4.0
Y
NOFLOW
10
0730
8.0
Y
NOFLOW
I
0630
8.0
Y
12
1130
24
0630
8.0
Y
13
0600
8.5
Y
14
0600
8.0
Y
15
0630
8.0
Y
16
0800
1.5
Y
17
N
NOFLOW
18
0500
18.5
Y
I NOFLOW
19
0600
8.5
Y
NOFLOW
20
0600
8.5
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0600
8.0
Y
NOFLOW
23
N
I NOFLOW
24
N
NOFLOW
25
N
NOFLOW
26
11:00
2.0
B
NOFLOW
27
0630
8.0
B
NOFLOW
28
0600
8.0
B
NOFLOW -
29
0630
8.0
B
NOFLOW
3a
1300
2.0
IB
NOFLOW
31
1400
1 3.0
D
I NOFLOW
Monthly Avcragc Limir.
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Monthly Avcrage:
Daily Jlasimum:
Daily Mialnmm:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0004952
PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2017 (December 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
E
E
F
E
-<
E—
_
6
O
E
O
o
U
O
5
C
Z
34447
00556
T'GP3B
34461
34694
34469
34475
34010
39700
34376
34220
Annually
Quarterly
Quarterly
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Grab
Grab
Composite
Grab
Grab
Grab
Grab
Grab
Grab
Grob
Grab
NITROBEN
OIL-GILSE
CER17DPF
PIIENANTII
PHENOL
PYRF.NE
TETCLETY
TOLUENE
llCB
FLUORAN'r
ANTIIRACE
2400 clock
Drs
2400 clock
ttrs
Y/B/N
Ibs/day
mg/1
pass/fail
Ibs/day
Ibs/day
Ibs/day
I Ibs/day
Ibs/day
I ug/I
ug/I
I ug/I
0630
8.0
Y
2
0600
3.0
Y
NOFLOW
3
1500
3.0
Y
NOFLOW
4
0500
8.0
Y
5
1130
24
0630
8.0
Y
6
0630
8.0
Y
7
0600
8.0
Y
s
0630
8.0
Y
NOFLOW
9
0830
4.0
Y
NOFLOW
10
0730
8.0
Y
NOFLOW
11
0630
8.0
Y
12
1130
24
0630
8.0
Y
<5
PASS
13
0600
8.5
Y
14
0600
8.0
Y
i5
0630
8.0
Y
16
0800
1.5
Y
17
N
NOFLOW
Is
0500
8.5
Y
NOFLOW
14
0600
8.5
Y
NOFLOW
20
0600
8.5
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0600
8.0 -
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
N
NOFLOW
26
11:00
2.0
B
NOFLOW
27
0630
8.0
B
NOFLOW
28
0600
8.0
B
NOFLOW
29
0630
8.0
B
NOFLOW
30
1300
2.0
B
NOFLOW
31
1400
3.0
B
I NOFLOW
Monthly Average LindC
0.087
0.071
0.048
0.031
0.071
0.084
Monthly Average:
0
Daily Maximum:
0
Daily Minimum:
0
'
****No Reporting Reason: ENFRUSE= No Flow-Rcuse/Recycle; ENVWTHR=No Visitation —Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation—Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2017 (December 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
c
E
E
E
U
_
U`
F-'
E
'E
O
E
O
1z
o`
U
O
C
z'
34626
00010
00300
Annually
Grab
Calculated
Calculated
26DINITR
TEMP-C
DO
2400 clock
11rs
2400 clock
Ilrs
Y/a/N
ug/I
deg a
mg/l
1
0630
8.0
Y
2
0600
3.0
Y
NOFLOW
3
1500
3.0
Y
NOFLOW
4
0500
8.0
Y
5
1 1130
24
0630 18.0
Y
12
10.1
6
0630
8.0
Y
7
-
0600
8.0
Y
8
0630
8.0
1 Y
NOFLOW
9
0830
4.0
Y
NOFLOW
10
0730
8.0
Y
NOFLOW
11
0630
8.0
Y
12
1 1130
24
0630
8.0
Y
7.9
11.2
13
0600
18.5
Y
4
0600
8.0
Y
15
0630
8.0
Y
16
0800
1.5
Y
17
N
NOFLOW
18
0500
8.5
Y
NOFLOW
'
19
0600
8.5
Y
NOFLOW
20
0600
8.5
Y
NOFLOW
21
0600
8.0
Y
NOFLOW
22
0600
8.0
Y
NOFLOW
23
N
NOFLOW
24
N
NOFLOW
25
N
NOFLOW
26
11:00
2.0
B
NOFLOW
27
0630
8.0
B
NOFLOW
28
0600
8.0
B
NOFLOW
29
0630
8.0
B
NOFLOW
30
1300
2.0
B
NOFLOW
31
1400
3.0
B
NOFLOW
Monthly Average Limit:
Monthly Avcragc:
9.95
10.65
Daily Masimum:
12
11.2
Daily Minimum:
7.9
10.1
****NoReporting Reason: ENFRUSE=NoFlow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2017 (December 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 01/18/2018
01 / 16/2018
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The pennittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the peninittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be [Wade as required by part II.E.6 of
the NPDES pennit.
01/18/2018
Perm ttee/Submitter SignUtu e:*** Nicole B Coffee E-Mail;[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting littp://portal.ncdenr.org/web/wq/swp/ps/npdes/fonns.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Pennittee: If signed by other than the permittee, then delegation of the signatory authority mast be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 12-2017 (December 2017)
Report Comments:
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
12/5/2017 BOD : Below Reporting Limit
12/12/2017 Oil & Grease and BOD : Below Reporting Limit

3
NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2017 (November 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS:WW-2COUNTY: Cleveland
�tECEIVE01NCpENFI/®VVR
ORC: Michael D. Sparks JAN 1 fl ..2018 ORC CERT NUMBER: 987732 ORC HAS CHANGED: No j A N 16 2018
VERSION: 1.0 q I • ! pgn�pQgjPJG 1§11 WTUS: Processed
WQROS
MOORESVILLE REGIONAL OFFICE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
q
E
u
6oS
o
0
e
m
F
E
F
x
O
U5
O
O
O
a
O
:
e
&
m
:i'
50050
00400
QD310
QD530
31616
C0600
C0665
34496
34501
Continuous
Weekly
Weekly
Weekly
Weekly
Semi-annual!
Semi-annually
Annually
Annual!
Recorder
Grab
Composite
Composite
Grab
Composite
Composite
Grab
Grab
FLOW
pH
DOD -Qy Daily
TSS-Qy Daily
FCOLI BR
TOTAL N-
TOTAL P-C..,
l,l-DCE
1,1-DCEY
2400 d-k
H.
2400,1o,k
H.
y/m
m d
so
Ibs/da
lbs/da
#/loom!
m
mg/I
lbs/da
Ibs/day
1
0600
8.0
B
NOFLOW
2
0600
8.0
B
NOFLOW
3
0600
8.0
B
NOFLOW
4
1030
2.0
B
NOFLOW
5
1130
2.0
B
I NOFLOW
6
0630 18.0
B
0.317
19
7
1130
24
0630
8.0
B
0.318
7.8
17
23.3
8
0630
8.0
Y
0.377
9
0600
8.0
Y
0.377
10
0600
8.0
1 Y
0.365
11
0800
4.25
Y
I NOFLOW
12
1100
4.0
Y
NOFLOW
13
0630
8.0
Y
0.39
2
14
1130
24
0630
8.0
Y
0.41
7.9
10.9
17.8
15
0600
8.0
Y
0.39
16
0600
8.0
Y
033
17
0630
8.0
Y
0.269
is
1030
1.0
B
0.211
19
N
NOFLOW
20
0630
8.0
B
NOFLOW
21
0630
8.0
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0930
1.0
1 B
NOFLOW
24
1030
1.0
B
NOFLOW
25
N
NOFLOW
26
1130
2.0
B
NOFLOW
27
1
10630
18.0
Y
1
0.373
1
6
28
1130
124
0630
8.0
Y
0.385
7.9
<6.4
13.2
29
0630
8.0
Y
0.416
30
0600
8.0
Y
0.405
Momhly A -mg, Limil:
0.45
68
124
200
0.071
0.052
Monthly A-g,:
0.355533
9.3
18.1
6.109115
Daily Maximum:
0.416
7.9
17
23.3
19
Daily Minimum:
0.211
7.8
0
13.2
2
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2017 (November 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
°
q
9
o
U
2
a
U°
F
a
@
O
O
B
i
E
O
0`
O
gg
m
:Lo
34536
32103
34541
34546
77163
34566
34571
34601
34606
34616
34611
Annually
Annually
Annually
Annually
Annually
Annually
Amually
Annually
Annually
Annually
Annuall
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
1,2-DCB
1,2-DCE
1,2-DCP
t-12DCEY
1,3-DCPE
1,3-DCB
1,4-DCB
2,4-DCPH
2,4-DMPH
2,4-DNPH
2,4-DNT
2400 Mork
H.
2400 clock
I H.
YlBIN
Ibs/da
Ibs/day I
Ibs/day
Ibs/da
Ibs/day
Ibs/day
Ibs/day
Ibs/da
Ibs/da
Ibs/da
lbs/da
1
0600
8.0
B
NOFLOW
2
0600
8.0
B
NOFLOW
3
0600
8.0
B
NOFLOW
4
1030
2.0
B
NOFLOW
5
1130
2.0
B
NOFLOW
6
0630
18.0
B
7
1130
24
0630
8.0
B
8
0630
8.0
Y
9
0600
8.0
Y
10
0600
8.0
Y
11
0800
4.25
Y
NOFLOW
12
1100
4.0
Y
NOFLOW
13
0630
8.0
Y
14
1130
24
0630
8.0
Y
is
0600
8.0
Y
16
0600
8.0
Y
17
0630
8.0
Y
19
1030
1.0
B
19
N
NOFLOW
20
0630
8.0
B
NOFLOW
21
0630
8.0
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0930
1.0
B
NOFLOW
24
1030
1.0
B
NOFLOW
25
N
NOFLOW
26
1130
2.0
B
NOFLOW
27
0630
8.0
Y
28
1130
24
0630
8.0
Y
29
0630
8.0
Y
30
0600
8.0
Y
Monthly Average Limit:
0.249
0.219
0.494
0.068
0.094
0.1
0,048
0.126
0.058
0.229
0.365
Monthly Av,mge:
Daily Maximum:
Daily Minimum:
****NoReportingReason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2017 (November 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
"
F
3
O
O
O
a
O
K
x
Z
34586
34591
79531
34657
34646
34205
34200
34215
34030
34526
34247
Annually
Annually
Annually
Amually
Annually
Annually
Annually
Annually
Armtrally
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
2CPHENOL
2NPHENOL
34-BNZFA
46DN-C
4NPHENOL
ACENAPEN
ACENAPYL
ACRYLONI
BENZENE
BNZO-A-A
BNZO-A-P
2400 clock
K. 12400
clock
H.
YBIN
Ibs/da
Ibs/day
u
Ibs/day
lb5/day I
lbs/day
11M
lbs/day
u
u
1
0600
8.0
B
NOFLOW
2
0600
8.0
B
NOFLOW
3
0600
8.0
B
NOFLOW
4
1030
2.0
B
NOFLOW
5
1130
2.0
B
NOFLOW
6
0630
8.0
B
7 11130
24
0630
8.0
B
e
0630
8.0
Y
9
0600
8.0
Y
io
0600
8.0
Y
11
0800
4.25
Y
NOFLOW
12
1100
4.0
Y
NOFLOW
13
0630
8.0
Y
14
1130
24
0630
8.0
Y
15
10600
8.0
Y
-
-
16
0600
8.0
Y
17
0630
8.0
Y
is
1030
1.0
B
19
N
NOFLOW
20
10630
8.0
B
NOFLOW
21
0630
8.0
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0930
1.0
JB
I NOFLOW
24
1030
1.0
B
NOFLOW
25
N
NOFLOW
26
11130
2.0
B
NOFLOW
27
0630
8.0
Y
28
1130
24
0630
8.0
Y
29
0630
8.0
Y
3a
0600
8.0
Y
Monthly Average Limit:
D.1
0.132
0.252
0.232
0.071
0.071
0.119
M.mbly Average:
Daily 111azimom:
Daily Minimum:
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2017 (November 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1_0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
,
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation— Adverse Weather; NOFLOW=No Flow; HOLIDAY =NoVisitation —Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2017 (November 2017)
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: WW-2 COUNTY: Cleveland
ORC: Michael D. Sparks ORC CERT NUMBER: 987732
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
-
B
G
F
o
fi
F
a`
O
O
is
O
_
o°
O
6
a
a'
2
34341
39110
34371
34381
39702
34396
01051
34418
34423
34696
01067
AnnuallyAnnuallyAnnuallyAnnuallyAnnually
Annuall
Annuall
AnnuallyAnnuallyAnnuallyAnnually
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
DIMET-PH
DNBPHTH
ETHYLBEN
FLUORENE
HEXCLBD
HCE
LEAD
METHYLCH
MECL2
NAPTHALE
NICKEL
2400 clock
Kra
2400 clock
H.
Y/B/N
Ibs/da
Ibs/da
Ibs/da
Ibs/da
Ibs/day
Ibs/da
Ibs/da
lbs/day I
Ibs/da
Ibs/da
Ibs/da
1
0600
8.0
B
NOFLOW
2
0600
8.0
B
NOFLOW
3
0600
8.0
B
NOFLOW
4
1030
2.0
B
NOFLOW
5
1130
2.0
B
NOFLOW
6
0630
8.0
B
7
1130
24
0630
8.0
JB
8
0630
8.0
Y
9
0600
8.0
Y
10
0600
8.0
Y
I
0800
4.25
Y
NOFLOW
12
1100
4.0
Y
NOFLOW
13
0630
8.0
Y
14
1130
24
0630
8.0
Y
15
0600
8.0
IY
16
0600
8.0
Y
17
0630
8.0
Y
i8
1030
1.0
B
19
N
NOFLOW
20
0630
18.0
B
NOFLOW
21
0630
8.0
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0930
1.0
B
NOFLOW
24
1030
1.0
B
NOFLOW
25
N
NOFLOW
26
1130
2.0
B
NOFLOW
27
0630
8.0
Y
28
1130
24
0630
8.0
Y
29
0630
9.0
Y
38
0600
8.0
Y
Monthly Average Limit:
0.061
0.087
0.103
0.071
0.065
0.068
2.227
0.278
0.129
0.071
12.846
Mouthy Average:
Daily Maximum:
Daily Minimum:
****No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather; NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: I 1-2017 (November 2017)
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
F
e
U'
B
e`
9
a`
O
O
H
X
O
y
o°
z
O
y
3
f
8
z
Z
34447
34461
34694
34469
34475
34010
34220
34626
39700
34376
00010
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annually
Annual)
Grab
Grab
Grab
Grab
Grab
Grab
Crab
Grab
Grab
Grab
Calculated
NITROBEN
PHENANTH
PHENOL
PYRENE
TETCLETY
TOLUENE
ANTHRACE
26DIMTR
HCB
FLUORANT
TEMP-C
z400 clock 1H.
2400 crock
H.
I YMN
Ibs/da
Ibs/day I
lbs/da
Ibs/da
Ibs/day
lbs/da
u
ugA
I u
ugA
dee c
1
0600
8.0
B
NOFLOW
2
0600
8.0
B
NOFLOW
3
0600
8.0
B
NOFLOW
4
1030
2.0
B
NOFLOW
5
1130
2.0
B
NOFLOW
6
0630
8.0
IB
7
1130
24
0630
8.0
11
18.6
8
0630
8.0
Y
9
0600
8.0
Y
10
0600
8.0
Y
11
1
0800
4.25
Y
NOFLOW
12
1100
14.0
Y
NOFLOW
13
0630
8.0
Y
14
1130
24
0630
8.0
Y
12.3
15
0600
8.0
Y
16
0600
8.0
Y
17
0630
18.0
Y
18
1030
1.0
B
19
N
NOFLOW
20
0630
8.0
B
NOFLOW
21
0630
8.0
B
I NOFLOW
22
0630
18.0
B
NOFLOW
23
0930
1.0
B
NOFLOW
24
1030
1.0
B
NOFLOW
25
N
NOFLOW
26
1
1130
2.0
B
NOFLOW
27
0630
18.0
Y
28
1130
24
0630
8.0
Y
9.8
29
0630
8.0
Y
30
0600
8.0
Y
Monthly Average Limit:
0.087
0.071
0.048
0.081
0.071
0.084
Monthly Avcngc:
13.566667
Daily Maximum:
18.6
Dauy Minimom:
9.8
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation -Adverse Weather; NOFLOW=No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2017 (November 2017)
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
q
a
e
o
O
d
F
B
Q
F
a
`
6
E
O
_
o
i
C
O
-
O`
z
O
z
t
a
z
Z
00300
Calculated
DO
2400 clock
H.
2400 clock 1H.
YIeM
Ito
1
0600
8.0
B
NOFLOW
2
0600
8.0
B
NOFLOW
3
0600
8.0
B
NOFLOW
4
1030
2.0
B
NOFLOW
5
1130
2.0
1B
I NOFLOW
6
0630
8.0
B
7
1130
24
0630
8.0
B
8.4
8
0630
8.0
Y
9
0600
8.0
Y
10
0600
9.0
Y
11
0800
14.25
1 Y
NOFLOW
12
1100
4.0
Y
NOFLOW
13
0630
8.0
Y
14
1130
24
0630
8.0
Y
9.7
15
0600
8.0
Y
16
0600
8.0
Y
17
0630
8.0
Y
is
1030
1.0
B
19
N
NOFLOW
20
0630
8.0
B
NOFLOW
21
0630
8.0
B
NOFLOW
22
0630
8.0
B
NOFLOW
23
0930
1.0
B
NOFLOW
24
1030
1.0
B
NOFLOW
25
N
NOFLOW
26
1130
2.0
B
NOFLOW
27
0630
8.0
Y
28
1130
24
0630
8.0
Y
10.6
29
0630
8.0
Y
30
0600
8.0
Y
Monthly Average Until:
Monthly Average:
9.566667
Daily Mnamum:
10.6
Dauy Minimum:
18.4
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR=No Visitation- Adverse Weather, NOFLOW =No Flow; HOLIDAY=NoVisitation- Holiday

NPDES PERMIT NO.: NC0004952
FACILITY NAME: Celanese -Shelby Facility
OWNER NAME: Cna Holdings LLC
GRADE: WW-3.
eDMR PERIOD: 11-2017 (November 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW-2
ORC: Michael D. Sparks
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed
SUBMISSION DATE: 12/19/2017
( 4Lj.�,.�� �..4 12/14/2017
ORC/Certifier Signature: Michael D Sparks E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within.24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
w'e.Z • cau__Q Q 12/19/2017
Permittee/Submitter SigVaMtre:*** Nicole B Coffee E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: NC Hwy 198 Shelby NC 28150 Permit Expiration Date: 08/31/2018
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: CNA Holdings INC
CERTIFIED LAB #: 221
PERSON(s) COLLECTING SAMPLES: Michael Sparks, Randy Turner
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(DI.

NPDES PERMIT NO.: NC0004952 PERMIT VERSION: 4.0
FACILITY NAME: Celanese -Shelby Facility CLASS: WW-2
OWNER NAME: Cna Holdings LLC ORC: Michael D. Sparks
GRADE: WW-3. ORC HAS CHANGED: No
eD1VIR PERIOD: 11-2017 (November 2017) VERSION: 1.0
Report Comments:
11/7/2017 BOD Difference between sample dilutions is greater than 30%
11/28/2017 BOD Below Reporting Limits
PERMIT STATUS: Active
COUNTY: Cleveland
ORC CERT NUMBER: 987732
STATUS: Processed

CERTIFIED MAIL: 70151660 0001 0635 4988
Return Receipt to PEM Carter
PEMC17:28
December21, 2017
NCDEQ
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
ATTN: Central Files
.i Celanese
The chemistry inside innovation"
Celanese Corporation
2525 Blacksburg Road
Grover, NC 28073-9641
www.celanese.com
Reference: Notes Concerning November 2017. DMR for C N A Holdings LLC: Shelby Facility,
Permit No. NC 0004962
To Whom It May Concern:
In accordance with the facility's NPDES Permit, the Novembers report has been submitted through the
eDMR system and duplicate copies of the signed DMR report have been attached to this letter as part of the
requirements.
• Prism Laboratories of Charlotte, NC, continues to provide certified contract laboratory services.
• 11/7/2017: BOD5 Difference between sample dilutions is greater than 30%
• 11/28/2017: BOD5 below reporting limits.
C N A Holding LLC — Shelby Facility is committed to ensuring compliance with all County, State, and Federal
regulations. Should there be a need for further discussion pertaining to the information on these forms, feel
free to call me at 803/818-8683 (cell), 704/480-5726 (office) or via email at pem.carter(@-celanese.com.
ely,
PEM Carter
EHS Lead/Environmental Engineer
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