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HomeMy WebLinkAboutWI0300345_TWELVE-MONTH POST INJECTION_20200514TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER MONITORING REPORT TREX PROPERTIES 3114 and 3124 Cullman Avenue Charlotte, North Carolina Mecklenburg County EPA ID: NCD049773245 Prepared for: TREX PROPERTIES, LLC Prepared by: � EnviroAnalytics Group EnviroAnalytics Group, LLC 1515 Des Peres Road, Suite 300 St. Louis, MO 63131 May 2020 /EnviroAnafytics Group TABLE OF CONTENTS 1 INTRODUCTION......................................................................................................1 2 INJECTION OF IRON -ACTIVATED PERSULFATE................................................ 2 3 WATER QUALITY MONITORING............................................................................2 3.1 Monitoring Well Construction............................................................................. 2 3.2 Groundwater Sampling Procedures................................................................... 2 3.3 Groundwater Sampling Results..........................................................................4 3.3.1 Tetrachloroethylene (PCE).......................................................................... 4 3.3.2 Trichloroethylene(TCE)............................................................................... 5 3.3.3 Cis 1,2 Dichloroethene (Cis 1,2 DCE)......................................................... 6 3.4 Surface Water Sampling Procedures................................................................. 6 3.5 Surface Water Analytical Results....................................................................... 6 4 OBSERVATIONS..................................................................................................... 7 EnviraAnalytics Group FIGURES 1 Site Location Map 2 Monitoring Well Location and Topographic Map 3 Trex Injection Strategy 4 Water Table Elevation Contour Map (January 2020) 5 Tetrachloroethene in Groundwater (January 2020) 6 Trichloroethene in Groundwater (January 2020) 7 Cis 1,2 Dichloroethene in Groundwater (January 2020) 8 Cross Section A -A' 9 Cross Section B-B' 10 Cross Section C-C' TABLES 1 Summary of Monitoring Well Construction Information and Water Level Data 2 Summary of Groundwater Analytical Results 3 Summary of Surface Water Analytical Results APPENDICES A Injection Event Records and Photo Documentation B Groundwater and Surface Water Sampling Forms C Laboratory Reports and Chain of Custody Records D Graphs of Contaminant Concentrations Versus Time Trends E IET 360-Day Data Evaluation F SVE System Graphs EnviroAnalytics Group 1 INTRODUCTION This report has been prepared as required by NCDEQ UIC Program Injection Permit No. W10300345, specifically Part IV — Monitoring and Reporting Requirements. The permit was issued to Trex Properties, LLC (Trex) on July 21, 2017 in response to an Application for Permit to Construct and/or Use a Well(s) for Injection, for In -Situ Groundwater Remediation dated January 18, 2017. The injection and monitoring work are being conducted by Trex to satisfy environmental remediation requirements of the NCDEQ Hazardous Waste Section (HWS). The Trex site consists of two properties that together comprise +/-1.68 acres and accommodate two warehouse structures each approximately 11,000 square feet in size that were constructed in the early 1960s. The building at 3114 Cullman Avenue was previously used by Detrex, Inc. to store various hazardous waste (HW) codes and recycle HW codes F001 & F002 under a Resource Conservation and Recovery Act (RCRA) Part B permit issued in 1983. Products, storage containers, and non-RCRA/non-hazardous solid wastes such as used oil were previously stored at the adjacent building located at 3124 Cullman Avenue. Both properties were acquired by Trex on June 18, 2013 and are located east of but within the limits of the City of Charlotte. All of the hazardous and non -hazardous wastes were removed from the two buildings in 2014 and both are currently unoccupied. The general locations of the properties and surrounding topography, roads and railways are shown on the Site Location Map provided as Figure 1. The aerial photograph in Figure 2 shows the general land use within the immediate vicinity of the properties, local topography, and the locations of permanent monitoring wells installed as part of the RCRA Facility Investigation. Past incidental spills of solvents resulted in contamination of unsaturated materials occurring beneath and adjacent to the two buildings, and underlying groundwater. Solvent contaminated groundwater has slowly migrated to vacant downgradient properties to the north, and threatens a perennial stream known as Little Sugar Creek. The soil and groundwater remediation activities for the site were described in the Conceptual Approach to Remediation (CAR) prepared by WR and dated July 15, 2016. The NCDEQ HWS approved these activities in a letter dated October 24, 2016. A soil vapor extraction (SVE) system consisting of 30 extraction wells was constructed within the two Trex buildings and began operating in August 2017. The SVE system has operated since that time resulting in significant reduction of soil contaminant concentrations, and alleviation of vapor intrusion issues at adjacent properties. Trex provides monthly reports to the NCDEQ HWS to document and track the soil remediation process. Graphs visibly illustrate the decreasing trends in Photo Ionization Detector (PID) readings, at some of the vacuum extraction wells having the highest readings in 2017, are presented in Appendix F. The approved CAR included injection of iron -activated sodium persulfate at locations on the Trex properties and adjacent properties to the north. Figure 3 illustrates the UIC Program approved TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER Page 11 MONITORING REPORT — May 2020 TREX PROPERTIES — 3114 and 3124 Cullman Avenue, Charlotte, North Carolina 1_­� EnviroAnafytics Group injection strategy and the approximate locations where nineteen of the twenty proposed injection wells were installed by Innovative Environmental Technologies, Inc. (IET) on behalf of Trex in 2018. Description of the injection activities are provided in Section 2 of this report, and the results of post -injection groundwater and surface water monitoring activities are discussed in Section 3. 2 INJECTION OF IRON -ACTIVATED PERSULFATE IET implemented the oxidant injection strategy described in the UIC application and permit for the site using the product "Ferric Oxide activated Sodium Persulfate" between January 7th and 17th, 2019 and on behalf of Trex. This product combines a self -activating oxidation persulfate chemistry while providing components for a longer lasting biological attenuation process following the initial oxidation event. A copy of the Injection Event Record (IER) dated January 24, 2019 that IET submitted to the UIC Program is included in Appendix A. A copy of IET's Technology Discussion and Field Report dated January 2019 is also included in Appendix A, with photographs to document the event. Details of the injection event including descriptive logs for each injection point are included in IET's January 2019 reports. A total of approximately 159,000 pounds of sodium persulfate were mixed with approximately 14,000 pounds of ferric oxide powder and municipal water to create about 69,500 gallons of injectant that was introduced into nineteen of the twenty injection wells referenced previously. Several attempts were made to install injection well IW-16; however, subsurface obstacles encountered prior to reaching the targeted injection depth prevented installation of that well. Day -lighting of injectant in the vicinity of wells IW-1 and IW-2 was noted to the south of the building at 3114 Cullman Avenue. IET consequently utilized direct -push machinery to inject the prescribed amount of injectant into the subsurface at seven nearby locations. More detailed descriptions and information regarding the injection event are included in Appendix A. 3 WATER QUALITY MONITORING 3.1 Monitoring Well Construction Type II monitoring wells screened in the saprolite include PMW-1A, PMW-2A, PMW-3A, PMW- 4A, PMW-5A, PMW-6A, PMW-7A, PMW-8A, PMW-9A & 9B, PMW-10A, and PMW-11A. Type III monitoring wells screened in bedrock include PMW-1 B, PMW-2B, PMW-7B, PMW-8B, PMW-9C, PMW-10B, PMW-11 B, and PMW-13B, Type III monitoring wells have an outer casing that extends into and is grouted in the top of bedrock to prevent infiltration of water from the saprolite. Table 1 provides construction information for all of the active monitoring wells at the site. 3.2 Groundwater Sampling Procedures The monitoring plan contained in the UIC application and permit prescribed collection of pre - injection groundwater and surface water samples that were collected between the dates of TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER Page 12 MONITORING REPORT — May 2020 TREX PROPERTIES — 3114 and 3124 Cullman Avenue, Charlotte, North Carolina EnviroAnalytics Group November 26th and 29th, 2018. Groundwater samples were obtained from twenty permanent monitoring wells, specifically: PMW-1A & 1B, PMW-2A & 2B, PMW-3A, PMW-4A, PMW-5A, PMW-6A, PMW-7A & 7B, PMW-8A & 8B, PMW-9A, 9B, & 9C, PMW-10A & 10B, PMW-11A & 11 B, and PMW-13B. The sampling locations are shown on Figure 2. Post -injection samples from these wells were collected approximately one month following the injection event (February 19th and 20th, 2019), approximately six months following the injection event (July 23rd and 24th, 2019) and approximately twelve months following the injection event (January 14th and 15th, 2020). The following procedures were utilized during each of the three sampling events. Each well's identity and location were confirmed. The depth to the static groundwater level within the well to be sampled was measured from the reference point on top of the well casing. Field measurements of volatile organic vapors in the air space at the well head using a calibrated Photo Ionization Detector (PID) were recorded on the sampling form for the well. The well was then purged according to the EPA -approved low flow methods using a peristaltic pump equipped with a variable speed flow controller capable of limiting the purge rate to less than one-half liter per minute. Field parameters including; water level during purging, volume of water removed, dissolved oxygen (DO), temperature (degrees 'Celsius), electrical conductivity (or EC in milli - Siemens per centimeter, mS/cm), pH, oxidation-reduction potential (ORP), and turbidity (NTU) were monitored during purging and recorded on the sampling forms included in Appendix B. The post -injection groundwater samples were also field tested for persulfate content using an assay kit consisting of colorimetric strips, and the test results were also recorded on the sampling forms. Field parameter measurements were observed to stabilize (less than 10% variance over three consecutive readings) prior to collecting groundwater samples by decanting directly into laboratory prepared containers in the order shown below, stored in an ice -chilled cooler, and transported under standard chain -of -custody protocols to the Pace Analytical Services (Pace) laboratory located in Huntersville, NC. Each sample was analyzed as follows: • Volatile Organic Compounds (VOCs) via EPA Test Method 8260D • Ethene via RSK 175 Method • Iron via EPA Method 6010D with Preparation Method EPA 3010A • Chloride and Sulfate by EPA Method 300.0 Rev 2.1 1993 • Total Organic Carbon via Standard Method 531OB-2011 Table 1 also provides depth to groundwater measurements obtained on January 13, 2020 from the 20 monitoring wells referenced in this section. The depth to groundwater measurements were used to determine the groundwater elevations shown on Table 1 and in Figure 4. The piezometric contours depicting equal shallow groundwater elevation shown in Figure 4 indicate that the direction of groundwater flow is northerly towards Little Sugar Creek. This makes intuitive sense and is consistent with previous determinations of groundwater flow direction at the site. TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER Page 13 MONITORING REPORT — May 2020 TREX PROPERTIES — 3114 and 3124 Cullman Avenue, Charlotte, North Carolina EnviroAnalytics Group 3.3 Groundwater Sampling Results Table 2 provides a summary of the laboratory analytical results for the pre -injection monitoring event in November 2018, and the three post -injection monitoring events conducted in February, July 2019 and January 2020. The laboratory analytical reports and chain of custody records for these events are included in Appendix C. The January 2020 samples contain concentrations of ten VOCs exceeding their respective North Carolina Groundwater Standards established in Title 15A of the NC Administrative Code Subchapter 2L (21- Standards) at one or more locations. The VOCs and locations where their concentrations exceed their 2L Standards are shown in the table below: VOC Location where Concentration Exceeds 2L Standard 1,1,2,2 - Tetrachloroethane PMW-4A 1,1 Dichloroethane PMW-10A 1,1 Dichloroethene PMW-9C, PMW-10A, PMW-13B 1,2,4-Trichlorobenzene PMW-9A, PMW-9B Benzene PMW-9A, PMW-9B Cis 1,2 Dichloroethene PMW-1A, PMW-2A, PMW-3A, PMW-4A, PMW-5A, PMW-6A, PMW-7A, PMW-9A, PMW-9B, PMW-9C, PMW-10A, PMW-10B, PMW-13B Tetrachloroethene PMW-1A, PMW-1B, PMW-2A, PMW-2B, PMW-3A, PMW-4A, PMW-5A, PMW-6A, PMW-7A, PMW-7B, PMW-8A, PMW-8B, PMW-9A, PMW-9B, PMW-9C, PMW-10A, PMW-10B, PMW-11A, PMW-11B, PMW-13B Trans-1,2-Dichloroethene PMW-3A, PMW-6A Trichloroethene PMW-1A, PMW-lB, PMW-2A, PMW-2B, PMW-3A, PMW-4A, PMW-5A, PMW-6A, PMW-7A, PMW-7B, PMW-8A, PMW-8B, PMW-9A, PMW-9B, PMW-9C, PMW-10A, PMW-10B, PMW-11A, PMW-11B, PMW-13B Vinyl Chloride I PMW-1A, PMW-9A, PMW-9B, PMW-11A The VOCs Tetrachloroethene (PCE), Trichloroethene (TCE) and Cis 1,2 Dichlorothene (Cis 1,2 DCE) were reported above lab detection limits at most monitoring well locations and are considered the primary contaminants of concern (COCs) at the site. The extent and concentrations of these three VOCs in groundwater is discussed in the following sections. 3.3.1 Tetrachloroethylene (PCE) PCE is considered to be a primary COC in groundwater at the site. The January 2020 monitoring event reported PCE concentrations that exceeded its 2L Standard of 0.7 pg/L at all of the twenty groundwater monitoring locations. The January 2020 PCE concentrations are shown in Table 2 and are depicted spatially on Figure 5. The PCE concentrations that exceeded the 2L Standard (0.7 pg/L) ranged from 2.6 pg/L (PMW-9A) to 29,900 pg/L (PMW-6A). The highest PCE concentrations are present in the central portion of the site immediately down -gradient from presumed source(s) near monitoring wells PMW-5A, PMW-6A and PMW-13B, and in the northern portion near the PMW-9 and PMW-10 well clusters. TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER Page 14 MONITORING REPORT - May 2020 TREX PROPERTIES - 3114 and 3124 Cullman Avenue, Charlotte, North Carolina EnviroAnalytics Group Concentration versus time graphs for each VOC detected at a concentration exceeding its 2L standard are included in Appendix D. The graphs of PCE concentration versus time for shallow groundwater visually illustrate stable or decreasing concentration trends in all cases. The PCE concentration versus time graphs for deeper groundwater document stable concentration trends in all cases except that for deep downgradient monitoring wells PMW- 9C and PMW-13B. In the case of 9C, this well is installed within the treatment zone and downgradient of the treatment area so migration of PCE maybe occurring from the IW-13, IW-9 area. PMW-13B is screened from 98 to 103 feet below ground surface, approximately 25 feet deeper than the deepest injection well, although within the treatment area. This is the only monitoring well within the treatment area screened in bedrock. PCE could potentially be migrating down a compromised grout seal at PMW-13B, or the groundwater from the highly impacted area around PMW-5A has possibly migrated down vertical fractures into this deeper well screen. 3.3.2 Trichloroethylene (TCE) TCE is also considered to be a primary COC in groundwater at the site. The January 2020 monitoring event detected TCE concentrations that exceeded its 2L Standard at all twenty groundwater monitoring locations. The January 2020 TCE concentrations are shown in Table 2 and are depicted spatially on Figure 6. The TCE concentrations that exceeded the 2L Standard of 3 pg/L ranged from 14.3 pg/L (PMW-2B) to 93,600 pg/L (PMW-5A). The highest TCE concentrations are present in the central portion of the site near wells PMW-5A and PMW-6, and in the northern portions near PMW-13B and the PMW-9 and PMW-10 well clusters, similar to the occurrence of PCE. TCE is a possible degradation product of PCE. Concentration versus time graphs for each VOC detected at a concentration exceeding its 2L standard are included in Appendix D. The graphs of TCE concentration versus time for shallow groundwater visually indicate stable or decreasing concentration trends in all cases except that for PMW-5A, which shows an increasing trend. The TCE concentration versus time graphs for deeper groundwater also show stable concentration trends in all cases except that for locations PMW-9C and PMW-13B. In the case of 9C, this well is installed within the treatment zone and downgradient of the treatment area so migration of TCE maybe occurring from the IW-13, IW-9 area. PMW-13B is screened from 98 to 103 feet below ground surface, approximately 25 feet deeper than the deepest injection well, although within the treatment area. This is the only monitoring well within the treatment area screened in bedrock. TCE could potentially be migrating down a compromised grout seal at PMW-13B, or the groundwater from the highly impacted area around PMW-5A has possibly migrated down vertical fractures into this deeper well screen. TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER Page 15 MONITORING REPORT — May 2020 TREX PROPERTIES — 3114 and 3124 Cullman Avenue, Charlotte, North Carolina EnviroAnalytics Group 3.3.3 Cis 1,2 Dichloroethene (Cis 1,2 DCE) PCE and TCE degradation product Cis 1,2 DCE was detected at concentrations that exceeded its 2L Standard at thirteen of the twenty groundwater monitoring locations. The January 2020 Cis 1,2 DCE concentrations are shown in Table 2 and are depicted spatially on Figure 7. The Cis 1,2 DCE concentrations that exceeded the 2L Standard of 70 pg/L ranged from 94.2 pg/L (PMW-1 B) to 2,610 pg/L (PMW-6A). The highest Cis 1,2 DCE concentrations are also present in the central portion of the site near wells PMW-5A and PMW-6, and in the northern portions near PMW-13B and the PMW-9 and PMW-10 well clusters. The graphs of Cis 1,2 DCE concentration versus time for shallow groundwater reveal the same stable or decreasing concentration trends in all cases. The Cis 1,2 DCE concentration versus time graphs for deeper groundwater also show stable concentration trends in all cases except for deep downgradient locations PMW-9B, PMW-9C and PMW-13B. Concentration versus time graphs for the all of the VOCs detected in site groundwater by individual well location are included in Appendix D. 3.4 Surface Water Sampling Procedures Three surface water samples (SW-1 through SW-3) were collected from Little Sugar Creek (Class C stream) during the pre and post injection monitoring events at the locations shown in Figure 2. Each sample was collected by submerging a laboratory -cleaned, non -preserved, one -liter glass container into the stream and then decanting the water into the laboratory -prepared bottleware containing the appropriate amount of preservative for the analysis to be conducted. The samples were stored on ice and transported under standard chain -of -custody protocol to Pace for analysis of VOCs by EPA Method 8260D. The post -injection surface water samples were field tested for: persulfate, temperature, pH, electrical conductance, dissolved oxygen, and redox. The field readings are included on the sampling forms in Appendix B and are summarized in Table 3. 3.5 Surface Water Analytical Results PCE concentrations in excess of its North Carolina Surface Water Standard established in Title 15A of the NC Administrative Code Subchapter 2B (213 Standard) of 3.3 pg/L were detected in the January 2020 surface water samples from locations SW-2 and SW-3 (see Table 3). The detected PCE concentrations in surface water samples from these locations were 12.1 pg/L (SW- 2) and 8.2 pg/L (SW-3). TCE concentrations exceeding the 2B Standard of 30 pg/L were also identified in the surface water samples from location SW-2 (55.4 pg/L) and SW-3 (35.3 pg/L). The concentration of TCE TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER Page 16 MONITORING REPORT — May 2020 TREX PROPERTIES — 3114 and 3124 Cullman Avenue, Charlotte, North Carolina EnviraAnalytics Group at upstream surface water location SW-1 (26.4 pg/L) was slightly less than the 2B Standard of 30 pg/L. Detectable concentration of Cis 1,2 DCE were also identified in all three of the surface water samples; however, all of the concentrations were below the EPA Tap Water Screening level of 36 pg/L. A 2B Standard for Cis 1,2 DCE has not been established. The surface water sampling locations and analytical results are also illustrated on Figures 2 through Figure 7. Table 3 summarizes the current and historic surface water analytical results. Copies of the laboratory analytical reports and chains of custody are included in Appendix C. 4 OBSERVATIONS A copy of IET's 360-day data evaluation report to Trex is included as Appendix E. IET's report contains more detailed discussion of the results of the injection in terms of chemical parameter changes observed in the post -injection analytical results. Tables 2 and 3 provide comparisons of pre- and post -injection total VOC concentrations at all of the groundwater and surface water sample locations. The aggregated VOC concentration comparisons indicate substantial contaminant concentration decreases as a result of the injection activities documented in this report. Graphs of total VOC concentrations versus time trends since groundwater monitoring began at the site in 2012 are included in Appendix D. Overall decreasing VOC concentration trends over time are apparent at all twenty of the groundwater monitoring locations that are part of the post - injection monitoring program for the site. Graphs of pre- and post -injection PCE, TCE and Cis 1,2 DCE concentrations versus time for each of the surface water samples are included in Appendix D. The graphs of VOC concentrations versus time for the three surface water samples indicate decreasing or stable concentrations over the post -injection monitoring period thus far. Cross -sections showing monitoring and injection wells within the treatment area are provided as Figures 8 through 10. PCE, PCE and Cis 1,2 DCE concentrations detected in the January 2020 samples are shown by monitoring well location on these cross -sections. According to IET, chemical oxidation reactions via production of sulfate free radicals appears to have diminished across the treatment area, overall degradation of total VOCs has been observed; however, concentrations of primary COCs exceeding target levels remain in most wells. TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER Page 17 MONITORING REPORT — May 2020 TREX PROPERTIES — 3114 and 3124 Cullman Avenue, Charlotte, North Carolina EnviroAnalytics Group According to the UIC injection permit requirements, monitoring of injection related byproducts should continue until their concentrations attenuate to pre -injection conditions or to below the applicable 2L Standard, whichever is greater. TWELVE-MONTH POST INJECTION GROUNDWATER AND SURFACE WATER Page 18 MONITORING REPORT — May 2020 TREX PROPERTIES — 3114 and 3124 Cullman Avenue, Charlotte, North Carolina EnviraAnalytics Group FIGURES '!'Fier BEEN � t :��►� 1, � �►1. NO � ..'sk!-Tr-,�-, il o ,. 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MONITORING WELL NOT INCLUDED IN INJECTION PERMIT SAMPLING SURFACE WATER SAMPLE LOCATION / PARCEL LINE \ TOPOGRAPHIC ELEVATION LINES (CONTOUR INTERVAL 2 FEET) LPMWVV-9A 1 V U \rl M N -- ( V ` PMW-16A PMW-16B,— r . / 1 .. PMW-7A � . . PMW-76 PMW-21B . PMW-21A Al NOTES 1. ELEVATION CONTOURS OBTAINED FROM ARCGIS ONLINE OPEN DATA 2. AERIAL IMAGE OBTAINED FROM GOOGLE EARTH PRO, 2018 \ 3 LAND PARCELS OBTAINED FROM j MECKLENBURG COUNTY GIS DATA CENTER <https://vfww.mecknc.gov/LUESA/GIS/ Pages/GIS-Data-Center.aspx > PMW 5A 3124 Vl CULLMAN AVE i 3114 PMW-20B PMW-20A CULLMAN AVE` PMW-4A PMW-18B , _ ..� PMW PMW-2A PMW-3A PMW-1A <y PMW-16 •p,�a�� 0 50 100 200 . \ ? III r # �Jhk�^i�?�� ;'•• FEET DRAWN BY: KA REVISION DATE OF BY: DESCRIPTION: PROJECT SHEET NUMBER. REVISION: FIGURE 2 NUMBER: NUMBER: APPROVED BY: MD #1 NA KA NA NA 1 OF 1 EnviroAnalytics MONITORING WELL LOCATION AND TOPOGRAPHIC MAP DATE: 03-30-2020 #2 NA NA NA TREX PROPERTIES, LLC DRAWING FIGURE Group DATE: NUMBER: SCALE: AS SHOWN #3 NA NA NA CHARLOTTE, NC 03-30-2020 2 'ork\20200330_Trex - Charlotte.dwg, 3/30/2020 3:50:35 PM / tilt,n) / TREATMENT ZONE r- LEGEND $ TYPE II SHALLOW MONITORING WELL TYPE III DEEP WELL LOCATION + PROPOSED TREX INJECTION WELL WITH AREA OF INFLUENCE f \ QCE 10.000 ug/L ISOGONCENTRATION LINE ICE 10,000 ug,/L 15000NCENTRAlION LANE `1' \ t;s 1.2 DICE 10,000 ug/L ISOCONCE NTRATION LINE (e,I80) TCE CONCENTRATIONS 1+ TCE ISOCONCENTRATION LINE GROUNDWATER ELEVATION CON OUR? r� DTE S WELL LAST SAMPLED IN SEPTEMBER 2015 HELLS PMW-4, PWM- 1 4 PAIR, PMW-16 PAIR, PWM- 17 PAIR, AND PWM-18A COULD NOT BE SAMPLED IN 2015 —RESULTS ARE FROM THE PREVIOUS 2012 SAMPLING EVENT ALL RESULTS ARE IN pug/L ^ DRAWN BY: KA EnviroAnalyticS APPROVED BY: MD Group DATE: 03-30-2020 SCALE: AS SHOWN IA r I 1 f P4 I r 1 �w - f .a._f Ig; 1 R4-1 1:00[t .� 4 pN souace � • AREA FOit THE x - _-- ` CONTAMINATION REVISION DATE OF NUMBER: REVISION: BY: DESCRIPTION: #1 NA KA NA #2 NA NA NA #3 NA NA NA PMjD - Pww-2W 100,000 t0 1 Y I —2g11 I h2 PMW— 16A "JDMJr— [aaW _ CROUNDWATER ONTAMINATION F ROM OFF -SITE I FIGURE 3 TREX INJECTION STRATEGY TREX PROPERTIES, LLC CHARLOTTE, NC NOTES 1. BASE MAP OBTAINED FROM 6-MONTH POST INJECTION GROUNDWATER MONITORING REPORT PREPARED BY WITHERSRAVENEL, 2016. 0 50 100 200 iiii FEET PROJECT SHEET NUMBER: NUMBER: NA 1 OF 1 DRAWING FIGURE DATE: NUMBER: 03-30-2020 3 \KA Work\20200330_Trex - Charlotte.dwg, 3/30/202010:S8:26 AM LEGEND PROPERTY BOUNDARY PARCEL LINE Y TYPE II MONITORING WELL tj TYPE III MONITORING WELL MONITORING WELL NOT INCLUDED IN INJECTION PERMIT SAMPLING PMW-12B SW _ I SURFACE WATER SAMPLE LOCATION PMW-12A (100) SHALLOW GROUNDWATER ELEVATION PMW-10-A PMW-9C PMW-9A _ V (FT AMSL) (675.47) (676.67) (675.62) PMW-9B -� N P v E DEEP GROUNDWATER ELEVATION (FT AMSL) PMW-10B \ PMW_ SHALLOW GROUNDWATER ELEVATION PMW-11A G PMW-` A CONTOUR (FT AMSL) "' PMW-11B 6jSS 4— IMPLIED GROUNDWATER FLOW PMW (676.70) (677.00) - PMW-21B PMW-13B PMW-21A _t (673.39) NOTES . %. ♦ .+ a 1. DEPTH TO WATER MEASUREMENTS PMW . } a� •� r r Or i (665.50) PMW-6A RECORDED ON 01/13/2020. PMW 8A 1'(679.02) (676.23) t \ 2. AERIAL IMAGE OBTAINED FROM \ GOOGLE EARTH PRO, 2018 14A PMW-146 3. LAND PARCELS OBTAINED FROM �l MECKLENBURG COUNTY GIS DATA CENTER PMW-5A <https://www.mecknc.gov/LUESA/GIS/ C� (679.64) �1b� 3124 Pages/GIS-Data-Center.aspx > 61� r CULLMAN AVE 3114 PMW-206 PMW-20A PMW-18A 6a� CULLMA 6b�3 PMW-4A PMW-18B , 6g1 ti (681.77) ` � 6g15� _ - _- PMW-21B (681.05) PMW-3A PMW-2A (680.99),(681.09) Er PMW-1A _ PMvv- I t3 0 40 80 160 (680.93) FEET REVISION DATE OF PROJECT SHEET ^ DRAWN BY: KA NUMBER: REVISION: BY: DESCRIPTION: NUMBER: NUMBER: ` FIGURE 4 APPROVED BY: MD #1 NA KA NA NA 1 OF 1 /nviroAna Elytics WATER TABLE ELEVATION CONTOUR MAP DATE: 03-30-2020 #2 NA NA NA TREX PROPERTIES, LLC DRAWING FIGURE Group CHARLOTTE NC 0 -3 -2020 NUMBER: SCALE: AS SHOWN #3 NA NA NA , C:\KA Work\20200330_Trex - Charlotte.dwg, 3/30/2020 3:41:11 PM (<O.16) , LEGEND -- — PROPERTY BOUNDARY $ PARCEL LINE ' J TYPE II MONITORING WELL \ TYPE III MONITORING WELL \ \SURFACE WATER SAMPLE LOCATION 'i (100) PCE CONCENTRATION (ug/L) a' � • � ' —100— PCE CONCENTRATION ISOPLETH (ug/L) PMW-10A PMW-9A PCE CONCENTRATION 100-1,000 ug/L / (6,880) (22,100 NF (2.6) �j 0 PMW' 300B PMW 9B M P N P PCE CONCENTRATION 1,000-9,999 ug/L PMW-11A Ci V 0 PCE CONCENTRATION 10,000+ ug/L (30.5) PMW-11 F 1 0 (8.2) (124) pp� g �o PMW-7A (634) PMW (1,290) PMW-13B o00 NOTES (9,960) / 1. AERIAL IMAGE OBTAINED FROM / \ GOOGLE EARTH PRO, 2018 f (19.8) / PMW-6A \ 2. LAND PARCELS OBTAINED FROM PMW-8A /� (29,900) o \ MECKLENBURG COUNTY GIS DATA / \ o CENTER (67 9) / ^oo \ < https://www.mecknc.gov/LUESA/GIS/ Pages/GIS-Data-Center.aspx > 3. SAMPLES COLLECTED PMW-5A JANUARY, 2020. (10,900) \ r PMW-4A \ 700 (84.3) 1,0oo PMW-2B --- ' (891) �� PMW-2A \ PMW) (1,120) MW-1A ,, (P71.7) PMW-1B� \0* 0 40 80 160 \ FEET DRAWN BY: KA REVISION DATE OF BY: DESCRIPTION:PROJECT SHEET NUMBER: REVISION: FIGURE 5 NUMBER: NUMBER: APPROVED BY: MD #1 NA KA NA NA 1 OF 1 EnviroAnalytics TETRACHLOROETHENE (PCE) IN GROUNDWATER DATE: 03-30-2020 #2 NA NA NA TREX PROPERTIES, LLC DRAWING FIGURE Group CHARLOTTE NC 0 -3 -2020 NUMBER: SCALE: AS SHOWN #3 NA NA NA , 'ork\20200330_Trex - Charlotte.dwg, 3/30/20204:13:58 PM Ei (35) ^ DRAWN BY: KA EnviroAnalyticS APPROVED BY: MD Group DATE: 03-30-2020 SCALE: AS SHOWN PMW-8A (516) 0(55.4)l PMW-1 74 10A IL(48,600) PMW 9A 900) (90 2) PMW-96 6,80o) (1,720)� I (26.4) 1 PMW-7A \ (1,670) AV (2130) \ I, 000 _---1 / PMW-6A o° iA o0 o \ \ o PMW-4A (233) (14.3) %PMW-2A A. PMW-3A/ (133) (363) PMW-1 A (218) (37.2) REVISION NUMBER: DATE OF REVISION: BY: DESCRIPTION: #1 NA KA NA #2 NA NA NA #3 NA NA NA LEGEND PROPERTY BOUNDARY t� Y` PARCEL LINE TYPE II MONITORING WELL TYPE III MONITORING WELL t SURFACE WATER SAMPLE LOCATION �^ (100) TCE CONCENTRATION (ug/L) —100— TCE CONCENTRATION ISOPLETH (ug/L) v v E 0 TCE CONCENTRATION 100-1,000 ug/L P TCE CONCENTRATION 1,000-9,999 ug/L j ' 0 TCE CONCENTRATION 10,000+ ug/L •� NOTES 'v\we' �ao FIGURE 6 TRICHLOROETHENE (TCE) IN GROUNDWATER TREX PROPERTIES, LLC CHARLOTTE, NC 1. AERIAL IMAGE OBTAINED FROM GOOGLE EARTH PRO, 2018 2. LAND PARCELS OBTAINED FROM MECKLENBURG COUNTY GIS DATA CENTER < https://www.mecknc.gov/LUESA/GIS/ Pages/GIS-Data-Center.aspx > 3. SAMPLES COLLECTED JANUARY, 2020. 0 40 80 160 iiii FEET PROJECT SHEET NUMBER: NUMBER: NA 1 OF 1 DRAWING FIGURE DATE: NUMBER: 03-30-2020 6 \KA Work\20200330_Trex - Charlotte.dwg, 3/30/20204:17:07 PM (4.7) / \ LEGEND PROPERTY BOUNDARY PARCEL LINE TYPE II MONITORING WELL _ TYPE III MONITORING WELL L SURFACE WATER SAMPLE LOCATION (7.6) (100) CIS 1,2-DCE CONCENTRATION (ug/L) —100— CIS 1,2-DCE CONCENTRATION ISOPLETH (ug/L) r PMW-10A (1,690) (96M0W 9C PM 8) ' s E N U E O CIS 1,2-DCE CONCENTRATION 100-1,000 ug/L P v PMWPMW-9B 10B (1,170) \ ` M P N / 0 CIS 1,2-DCE CONCENTRATION 1,000-9,999 ug/L (1,330) - PMW-11A (4.4) o PMW-11 B (59.0) g PMW-7A (357) 4 PMW-7B 00 7 (34.2) 0 PMW-13B NOTES Al (2,020) / 1. AERIAL IMAGE OBTAINED FROM GOOGLE EARTH PRO, 2018 JW-8B "(35.4) PMW-6A 2. LAND PARCELS OBTAINED FROM PMW-8A (2,610) ^ MECKLENBURG COUNTY GIS DATA (28.2) \ �� ` CENTER \ < https://www.mecknc.gov/LUESA/GIS/ 100, Pages/GIS-Data-Center.aspx > 3. SAMPLES COLLECTED PMW 5Aw JANUARY, 2020. PMW-4A T \ PMW-2A \ PMW 3A (845) (94.2) � 14 PMW-1Ao .04 (598) PMW-1R 0 40 80 160 \ (69.5) FEET DRAWN BY: KA REVISION DATE OF BY: DESCRIPTION:PROJECT NUMBER: REVISION: FIGURE 7 NUMBER NUMBER: APPROVED BY: MD #1 NA KA NA CIS 1,2-DICHLOROETHENE IN GROUNDWATER NA 1oF1 rnxroAnalytics DRAWING FIGURE Group DATE: 04-08-2020 #2 NA NA NA TREX PROPERTIES, LLC DDATE: NUMBER: SCALE: AS SHOWN #3 NA I NA NA CHARLOTTE, NC 04-08-2020 7 ,A Work\20200408_Trex - Charlotte.dwg, 4/8/2020 2:19:21 PM LEGEND OUTER WELL CASING INTERVAL WELL SCREEN INTERVAL aINNER WELL CASING INTERVAL INJECTION WELL _v_ SHALLOW GROUNDWATER ELEVATION (100) PCE CONCENTRATION IN ug/L (JANUARY 2020) (100) TCE CONCENTRATION IN ug/L (JANUARY 2020) (100) CIS 1,2 DCE CONCENTRATION IN ug/L (JANUARY 2020) RESIDUAL SOIL/SAPROLITE PARTIALLY WEATHERED BEDROCK COMPETENT ROCK A' Pr1",-8A 0 80 16C FE DRAWN BY: KA EnviroAnalyticS APPROVED BY: MD Group DATE: 05-05-2020 SCALE: AS SHOWN A SOUTH 700 690 < � a m a 680 _ (71.7) = _ 670 (218) 598) — — — — ' 660 650 sao / / 630 (44.1) (37.2)/ (69.5) 620 610 600 590 580 REVISION DATE OF NUMBER: REVISION: BY: DESCRIPTION: #1 NA KA NA #2 NA NA NA #3 NA NA NA NOTES 1. INFERRED BOUNDARIES BETWEEN GEOLOGIC UNITS ARE TRANSITIONAL 0 40 80 160 iiii FEET A' NORTH PROJECT SHEET FIGURE 8 NUMBER: NUMBER: CROSS SECTION A -A' NA 1 OF 1 DRAWING FIGURE TREX PROPERTIES LLC , DATE: NUMBER: CHARLOTTE, NC 05-06-2020 8 CA Work 2\20200513_Trex - Charlotte_Post Injection GW Monitoring.di EAG FIG 8 (2), 5/13/2020 11:11:11 AM LEGEND OUTER WELL CASING INTERVAL WELL SCREEN INTERVAL INNER WELL CASING INTERVAL INJECTION WELL SHALLOW GROUNDWATER ELEVATION (100) PCE CONCENTRATION IN ug/L (JANUARY 2020) (100) TCE CONCENTRATION IN ug/L (JANUARY 2020) (100) CIS 1,2 DCE CONCENTRATION IN ug/L (JANUARY 2020) RESIDUAL SOIL/SAPROLITE PARTIALLY WEATHERED BEDROCK COMPETENT ROCK NOTES 1. INFERRED BOUNDARIES BETWEEN GEOLOGIC UNITS ARE TRANSITIONAL 0 40 80 160 iiii FEET B B, WEST EAST 3114 CULLMAN AVE 3124 CULLMAN AVE — 3144 CULLMAN AVE 3154 CULLMAN AVER 3162 CULLMAN AVE 3200 CULLMAN AVE 700 � r 670 680 670 660 650 640 630 620 610 DRAWN BY: KA REVISION NUMBER: I DATE OF REVISION: BY: DESCRIPTION:PROJECT FIGURE 9 NUMBER: SHEET NUMBER: EnviroAnalytics APPROVED BY: MD #1 NA KA Nq 1 SECTION BLC NA 1 OF 1 DATE: OS-OS-2020 #2 NA NA NA DRAWING DATE: FIGURE NUMBER: Group TRERXOPROPERTIIES LSS CHARLOTTE, 1C 05-05-2020 9 SCALE: AS SHOWN #3 NA NA NA C:\KA Work 2\20200513_Trex - Charlotte Post Injection GW Monitoring.di EAG FIG 9 (2), 5/13/2020 11:12:43 AM PMW- PMW-13B P PMW-21A �- MWAB PMW-BA EnviraAnalytics Group TABLES TABLE 1 SUMMARY OF MONITORING WELL CONSTRUCTION INFORMATION AND WATER LEVEL DATA TREX PROPERTIES, LLC CHARLOTTE, NC Well ID Date Installed Well Type Total Depth of Well Casing (ft bgs) Total Depth of Outer Casing (ft bgs) Screened Interval (ft bgs) Screened Material Height of Top of Casing (ft ags) Depth to PWR (ft bgs) Top of PWR Elevation (ft msl) Depth to Bedrck o (ft bgs) Top of Bedrock Elevation (ft msl) Ground Surface Elevation (ft msl) Top of Casing Elevation (ft msl) Depth to Groundwater on 1/13/20 (ft btoc) Groundwater Elevation on 1/13/20 (ft msl) PMW-IA 09/14/12 Type II 12 -- 7-12 Saprolite 3.33 10 676.95 -- -- 683.62 686.95 5.03 681.92 PMW-113 1 09/13/12 Type I11 54 44 1 49-54 PWR 3.75 1 10 676.87 1 55 631.87 683.12 1 686.87 5.94 680.93 PMW-2A 09/14/12 Type II 30 -- 20-30 Saprolite 3.58 30 657.34 -- -- 683.76 687.34 6.25 681.09 PMW-2B 09/13/12 Type III 55 37 50-55 PWR 3.56 30 656.98 55 631.98 683.42 686.98 5.93 681.05 PMW-3A 09/14/12 Type II 25 -- 15-25 Saprolite 3.58 25 662.00 -- -- 683.42 687.00 6.01 680.99 PMW-4A 06/14/12 Type ll 12 2-12 Saprolite 3.41 -- -- 687.45 690.86 9.09 681.77 PMW-5A 06/13/12 Type II 39 29-39 PWR -0.28 25 658.60 683.88 683.60 3.96 679.64 PMW-6A 06/12/12 Type II 38 28-38 PWR -0.31 30 653.76 684.07 683.76 4.74 679.02 PMW-7A 06/12/12 Type II 38 28-38 PWR -0.25 30 653.67 683.92 683.67 6.97 676.70 PMW-713 06/25/12 Type II1 55 40 50-55 PWR -0.30 30 654.04 684.34 684.04 7.04 677.00 PMW-8A 06/11/12 Type II 42 -- 32-42 PWR -0.34 35 649.76 685.10 684.76 8.53 676.23 PMW-8B 06/21/12 Type III 58 43 53-58 PWR -0.33 35 649.98 685.31 684.98 19.48 665.50 PMW-9A 06/08/12 Type II 19 -- 9-19 Saprolite -0.29 -- -- 683.61 683.32 7.85 675.47 PMW-913 06/13/12 Type II 34 -- 24-34 Saprolite -0.25 30 653.41 683.66 683.41 7.95 675.46 PMW-9C 06/21/12 Type II1 50 35 45-50 PWR -0.26 30 653.57 683.83 683.57 7.95 675.62 PMW-10A 06/11/12 Type II 63 -- 53-63 PWR -0.31 55 627.94 683.25 682.94 6.27 676.67 PMW-1013 06/21/12 Type II1 73 64 68-73 PWR -0.32 55 628.17 73 610.17 683.49 683.17 6.38 676.79 PMW-11A 06/12/12 Type II 63 -- 53-63 PWR -0.29 55 627.62 -- -- 682.91 682.62 6.43 676.19 PMW-1 lB 06/21/12 Type III 78 63 73-78 PWR -0.30 55 627.81 78 604.81 683.11 682.81 6.66 676.15 PMW-12A 06/25/12 Type II 40 30-40 PWR -0.32 20 661.57 -- -- 681.89 681.57 NM -- PMW-12B 06/25/12 Type II1 49 42 44-49 PWR -0.31 20 661.70 49 632.70 682.01 681.70 NM -- PMW-13B 07/12/12 Type II1 103 88 98-103 Bedrock -0.28 50 635.27 88 597.27 685.55 685.27 11.88 673.39 PMW-14A 09/19/12 Type II 30 -- 20-30 Saprolite 2.89 25 656.14 -- -- 678.25 681.14 NM -- PMW-14B 09/19/12 Type III 50 32 45-50 PWR 2.85 25 656.00 678.15 681.00 NM PMW-16A 09/19/12 Type II 22 -- 12-22 PWR -0.28 5 678.26 683.54 683.26 NM PMW-16B 09/19/12 Type II1 55 24 50-55 PWR -0.30 5 678.37 55 628.37 683.67 683.37 NM PMW-17A 09/19/12 Type II 22 -- 12-22 PWR -0.31 5.5 680.72 -- -- 686.53 686.22 NM PMW-17B 09/12/12 Type II 50 45-50 PWR -0.29 5.5 680.82 55 631.32 686.61 686.32 NM PMW-18A 09/14/12 Type II 22 12-22 Saprolite 3.58 22 664.27 -- -- 682.69 686.27 NM PMW-18B 09/14/12 Type II1 43 22 38-43 PWR 3.50 22 664.40 43 643.40 682.90 686.40 NM PMW-20A 12/11/14 Type II 39 -- 34-39 Saprolite 2.75 39 -- -- 643.98 683.28 686.03 NM PMW-20B 12/09/14 Type III 60 45 55-60 Rock 3.32 -- -- 39 644.02 683.32 686.64 NM PMW-21A 12/02/14 Type II 35 -- 30-35 Saprolite -0.41 35 648.31 -- -- 683.62 683.21 NM PMW-21B 12/03/14 Type II1 67 40 62-67 PWR -0.31 35 648.27 67 616.27 683.57 683.26 NM PMW-22A 12/08/14 Type II 63 -- 58-63 Saprolite 3.10 63 620.81 -- -- 683.95 687.03 NM PMW-22B 12/09/14 Type III 86 70 81-86 PWR 2.64 63 621.15 85 599.15 684.26 686.88 NM Notes 1. ft bgs = Feet below ground surface 2. ft toc = Feet below top of casing 3. ft ags = Feet above ground surface 4. ft msl = Feet above mean sea level 5. PWR = Partially Weathered Rock. 6. -- = Not Applicable TABLE2 SUMMARY OF GROUNDWATER ANALYTICAL RESULTS TREX PROPERTIES, LLC CHARLOTTE, NC N,IW Designation NC 2L Standard PMW-1A PMW-lA PMW-1A PMW-1A PMW-113 PMW IB (PMW-DUP2) PMW-1B PMW-DUP1 PMW-1B PMW-1B PMW-1B (DUP2) pMW-2A PMW-2A PMW-2A PMW-2A PMW-2B PMW-2B PMW-2B PMW-2B PMW-3A PMW-3A PMW-3A PMW-3A Depth or EPA Tap TD = 12 ft. TD = 12 ft. TD = 12 ft. TD = 12 ft. TD = 54 ft. TD = 54 ft. TD = 54 ft. TD = 54 ft. TD = 54 ft. TD = 54 ft. TD = 54 ft. TD = 30 ft. TD = 30 ft. TD = 30 ft. TD = 30 ft. TD = 55 ft. TD = 55 ft. TD = 55 ft. TD = 55 ft. TD = 25 ft. TD = 25 ft. TD = 25 ft. TD = 25 ft. Lab ID Water SL 92409026001 92418554011 92438460001 92461009001 92409026002 92409026022 92418554012 TD = 54 ft. 92438460002 92461009002 92461009022 92409026003 92418554013 92438460003 92461009003 92409026004 92418554014 92438460004 92461009004 92409026005 92418554015 92438460005 92461009005 Date 11/27/2018 2/20/2019 7/24/2019 1/15/2020 11/27/2018 11/27/2018 2/20/2019 2/19/2019 7/24/2019 1/15/2020 1/15/2020 11/27/2018 2/20/2019 7/24/2019 1/15/2020 11/27/2018 2/20/2019 7/24/2019 1/15/2020 11/27/2018 2/20/2019 7/24/2019 1/15/2020 Volatile Organic Compound Pre -Injection I-M post 6-M post 12-M post Pre -Injection Pre -Injection 1-M post 1-M post 6-M post 12-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection I-M post 6-M post 12-M post Pre -Injection I-M post 6-M post 12-M post 1,1,1,2-Tetrachloroethane 1 <3.3 <5.0 <6.8 <1.7 <0.82 <0.82 <].0 <I.0 <0.34 <0.34 <0.34 <3.3 <10.0 <3.4 <3.4 <1.3 <2.5 <1.7 <.7 <41.2 <I00 <4.2 <17.0 1,1,1-Trichloroethane 200 <4.8 276 <3.5 16.3 <1.2 <.2 <1.0 <I.0 <0.18 <0.18 <0.18 7.8 J 5.7 J <.8 <1.8 <.9 <12.5 <0.88 <0.88 <60.0 <100 <2.2 <8.8 1, 1,2,2-Tetrachloroethane 0.2 <4.0 78.6 22.0 <.1 <1.0 <.0 <.0 <1.0 <0.22 <0.22 <0.22 <4,0 <10.0 <22 <2.2 <1.6 <12.5 <1.1 <l.l <50.0 <100 25.4 <11.1 1,1,2-Trichloroethane 0.6 <2.9 5.6 <4,7 <12 <0.72 <0.72 <.0 <1.0 <024 <0.24 <0.24 <2.9 <10.0 <2.4 <2.4 <1.2 <12.5 <12 <1.2 <36.2 <100 3.8 J <11.8 1,1-Dichloroethane 6 <3.2 18.7 18.3 J 5.8 <0.80 <0.80 <.0 <.0 <0.27 0.38 J 0.40 J <3.2 <10.0 <2.7 <2.7 <13 <12.5 <1.3 <13 <40.0 <100 <3.4 <13.4 1,1-Dichloroethene 350 <5.6 2 J 13.4 J <12 <.4 <1.4 <1.0 <1.0 <024 <0.24 <0.24 8 J 7.2 J <2.4 <2.4 <2.2 <12.5 <.2 <.2 <70.0 <100 <3.1 <12.2 1,1-Dichloropropene NSL <4.9 <5.0 <4.3 <l.l <1.2 <1.2 <1.0 <I.0 <0.21 <0.21 <0.21 <4.9 <10.0 <2.1 <2.1 <2.0 <12.5 <LI <1.1 <61.2 <100 <2.7 <10.6 1,2,3-Trichlorobenzene 7 <3.3 <5.0 <6.9 <1.7 <0.82 <0.82 1 <1.0 <I.0 <0.34 <0.34 <0.34 1 <3.3 <10.0 <3.4 <3.4 <13 <12.5 <1.7 <1.7 <41.2 <100 <4.3 <17.2 1,2,3-Trichloropropane 0.005 <4,1 <5.0 <6.9 <1.7 <1.0 <1.0 <1.0 <I.0 <0.35 <0.35 <0.35 <4.1 <10.0 <3.5 <3.5 <.6 <12.5 <1.7 <1.7 <51.2 <100 <4.3 <17.4 1,2,4-Trichlorobenzene 400 <3.5 <5.0 <4,4 <1.1 <0.88 <0.88 0.57 J 0.68 J 0.56 J 0.39 J 0.39 J <3.5 <10.0 <2.2 <22 <1.4 <12.5 <1.1 <.1 <43.8 <100 <2.7 <10.9 1,2-Dibromo-3-chloropropane 0.04 <20.0 <10.0 <5.1 <13 <5.0 <5.0 <2.0 <2.0 <0.26 <0.26 <0.26 <20.0 <20.0 <2.6 <2.6 <8.0 <25.0 <13 <1.3 <250 <200 <3.2 <12.8 1,2-Dibromoethane (EDB) 0.02 <2.7 <5.0 <5.2 <13 <0.68 <0.68 <1.0 <1.0 <0.26 <0.26 <0.26 <2.7 <10.0 <2.6 <2.6 <1.1 <12.5 <13 <1.3 <33.8 <100 <3.2 <12.9 1,2-Dichlorobenzene 20 <3.0 <5.0 <5.8 <.5 <0.75 <0.75 <1.0 <.0 <0.29 <0.29 <0.29 <3.0 <10.0 <2.9 <2.9 <.2 <12.5 <.5 <1.5 <37.5 <100 <3.6 <14.6 1,2-Dichloroethane 0.4 <2.4 <5.0 <6.7 <.7 <0.60 <0.60 <1.0 <.0 <0.34 <0.34 <0.34 <2.4 <10.0 <3.4 <3.4 <0.96 <12.5 <13 <1.7 <30.0 <100 <4.2 <16.8 1,2-Dichloropropane 0.6 <2.7 <5.0 <3.7 <0.94 <0.68 <0.68 <1.0 <1.0 <0.19 <0.19 <0.19 <2.7 <10.0 <.9 <1.9 <1.1 <12.5 <0.94 <0.94 <33.8 <100 <2.3 <9.4 1,3-Dichlorobenzene 200 <2.4 <5.0 <4.3 <1.1 <0.60 <0.60 <1.0 <1.0 <0.22 <0.22 <0.22 <2.4 <10.0 <22 <22 <0.96 <12.5 <1.1 <.1 <30.0 <100 <2.7 <10.8 1,3-Dichloropropane 0.6 <2.8 <5.0 <3.2 <0.79 <030 <0.70 <1.0 <.0 <0.16 <0.16 <0.16 <2.8 <10.0 <1.6 <.6 <.1 <12.5 <0.79 <0.79 <35.0 <100 <2.0 <7.9 1,4-Dichlorobenzene 6 <3.3 <5.0 <5.2 <13 <0.82 <0.82 <1.0 <1.0 <0.26 <0.26 <0.26 <3.3 <10.0 <2.6 <2.6 <13 <12.5 <1.3 <1.3 <41.2 <100 <3.2 <12.9 2,2-Dichloropropane NSL <.3 <5.0 <5.4 <1.4 <0.32 <0.32 <1.0 <.0 <0.27 <0.27 <0.27 <1.3 <10.0 <2.7 <2.7 <0.52 <12.5 <.4 <1.4 <16.2 <100 <3.4 <13.5 2-Butanone (MEK) 4,000 <9.6 <25.0 1 1 <66.6 <16.6 <2.4 <2.4 <5.0 <5.0 <3.3 <3.3 <3.3 <9.6 <50.0 <33.3 <33.3 <3.8 <62.5 1 <16.6 <16.6 <120 <500 <41.6 <166 2-Chlorotoluene 100 <3.5 <5.0 <4.1 <1.0 <0.88 <0.88 <1.0 <.0 <0.20 <0.20 <0.20 <3.5 <10.0 <2.0 <2.0 <.4 <12.5 <.0 <1.0 <43.8 <100 <2.5 <10.2 2-11exanone 40 <4.6 <25.0 <11.4 <2.8 <1.2 <.2 <5.0 <5.0 <0.57 <0.57 <0.57 <4.6 <50.0 <5.7 <5.7 <1.8 <62.5 <2.8 <2.8 <57.5 <500 <7.1 <28.4 4-Chlorotoluene 24 <3.1 <5.0 <4.1 <.0 <0.78 <0.78 <1.0 <.0 <0.20 <0.20 <0.20 <3.1 <10.0 <2.0 <2.0 <.2 <12.5 <.0 <1.0 <38.8 <100 <2.6 <10.2 4-Methyl-2-pentanone (M[lBK) 100 <3.3 <25.0 <90.6 <22.6 <0.82 <0.82 <5.0 <5.0 <4.5 <4.5 <4.5 <3.3 <50.0 <45.3 <45.3 <1.3 <62.5 <22.6 <22.6 <41.2 <500 <56.6 <226 Acetone 6,000 <100 78.8 J <123 69.2 J <25.0 1 <25.0 <25.0 <25.0 <6.2 <6.2 <6.2 <100 <250 1 <61.7 <61.7 1 <40.0 <312 <30.8 1 <30.8 <1250 <2500 1 343 953 J Benzene 1 <2.5 <5.0 <3.0 <0.75 <0.62 <0.62 <1.0 I <1.0 11 <0,15 <0.15 <0.15 <2.5 <10.0 <1.5 <1.5 1 <1.0 <12.5 <0.75 1 <0.75 <31.2 <100 I <1.9 <7.5 Bromobenzene 62 <3.0 <5.0 <4.4 <1.1 <0.75 <0.75 <1.0 <1.0 <0.22 <0.22 <0.22 <3.0 <10.0 <22 <22 <1.2 <12.5 Bromochloromethane 83 <.7 <5.0 <6.9 <1.7 <0.42 <0.42 <1.0 <1.0 <0.34 <0.34 <0.34 <1.7 <10.0 <3.4 <3.4 <0.68 <12.5 <1.7 <.7 <21.2 <100 <4.3 <17.2 Bromodichloromethane 0.6 <.g <5.0 <5.1 <1.3 <0.45 <0.45 <1.0 <.0 <0.26 <0.26 <0.26 <1.8 Bromofom 4 <2.6 <5.0 <12.3 <3.1 <0.65 <0.65 <1.0 <1.0 <0.62 <0.62 <0.62 <2.6 <10.0 <6.2 <6.2 <.0 <12.5 <3.1 <3.1 <32.5 <100 <7.7 <30.8 Bromomethane 100 <2.9 <10.0 <12.4 <3.1 <0.72 <0.72 <2.0 <2.0 <0.62 <0.62 <0.62 <2.9 <20.0 <6.2 <6.2 <.2 <25.0 <3.1 <3.1 <36.2 <200 <7.8 <31.0 Carbon tetrachloride 0.3 <2.5 <5.0 <4,5 <1.1 <0.62 <0.62 <1.0 <1.0 <0.22 <0.22 <0.22 <2.5 <10.0 <2.2 <22 <1.0 <12.5 <.1 <.1 <31.2 <100 <2.8 <11.2 Chlorobenzene 50 <2.3 <5.0 <4.7 <.2 <0.58 <0.58 <1.0 <.0 <0.23 <0.23 <0.23 <2.3 <10.0 <2.3 <2.3 <0.92 <12.5 <.2 <1.2 <28.8 <100 <2.9 <11.6 Chloroethane 3,000 <5.4 <5.0 <9.8 <2.4 <1.4 <1.4 <.0 <I.0 <0.49 1 <0.49 1 <0.49 1 11 <5.4 1 <10.0 1 <4.9 1 1 <4.9 <2.2 <12.5 <2.4 <2.4 1 <67.5 <100 <6.1 <24.5 Chloroform 70 <.4 <25.0 <46.8 <11.7 <0.35 <0.35 <5.0 <5.0 1 <2.3 <2.3 <2.3 <1.4 <50.0 <23.4 <23.4 1 <0.56 <62.5 <11.7 <11.7 <17.5 <500 <29.2 11 <117 Chloromethane 3 <.1 13.1 <7.8 <.9 11<0.28 <0.28 0.7 J 0.93 J 0,56 J 0.73 J <0.39 <l.l <10.0 <3.9 <3.9 <0.44 <12.5 <.9 <1.9 <13.8 <100 31.5 <19.4 cis-1,2-Dichloroethene 70 1,170 206 1,280 598 301 314 187 175 91.9 69.5 64.9 92.4 82.0 34.7 94.2 <0.76 <12.5 <.5 <1.5 1,030 243 48.1 845 cis-1,3-Dichloropropene 0.4 1.3 <5.0 <5.9 <1.5 <0.32 <0.32 <1.0 <I.0 <0.30 <0.30 <0.30 <1.3 <10.0 <3.0 <3.0 <0.52 <12.5 1 <1.5 <1.5 <16.2 <100 <3.7 <14.8 Dibromochloromethane 0.4 <2.1 <5.0 <8.3 <2.1 <0.52 <0.52 <1.0 <.0 <0.41 <0.41 <0.41 <2.1 <10.0 <4.1 <4.1 <0.84 <12.5 <2.1 <23 <26.2 <100 <5.2 <20.6 Dibromomethane 70 <2.1 <5.0 <9.2 1 <23 <0.52 <0.52 <1.0 <I.0 <0.46 <0.46 <0.46 <2.1 <10.0 <4.6 <4,6 <0,84 <12.5 <2.3 <2.3 <26.2 <I00 <5.7 <23.0 Dichlorodifluoromethane 1,000 <2.1 <5.0 <4.5 <.1 <0.52 <0.52 <1.0 <1.0 <0.23 <0.23 <0.23 <2.1 <10.0 <2.3 <2.3 <0.84 <12.5 <.1 <13 <26.2 <100 <2.8 <11.3 Diisopropyl ether 1,500 <.2 <5.0 <4.4 <.1 <0.30 <0.30 <1.0 <1.0 <0.22 <0.22 <0.22 <1.2 <10.0 <2.2 -2.2 <0.48 <12.5 <.1 <1.1 <15.0 <100 <2.7 110.9 Ethylbenzene 600 <3.0 <5.0 <5.1 <13 <0.75 <0.75 <1.0 <LO <0.26 <0.26 <0.26 11 <3.0 <10.0 <2.6 1 <2.6 <12 <12.5 <13 <1.3 <37.5 <100 <3.2 <12.8 Hexachloro-1,3-butadiene 0.4 <7.1 <5.0 <8.8 <2.2 <.g <1.8 <1.0 <1.0 1 <0.44 <0.44 <0.44 <7.1 <10.0 <4.4 <4.4 <2.8 <12.5 Methyl-tert-butyl ether 20 <2.1 <5.0 <5.5 <1.4 <0.52 <0.52 <1.0 <.0 <0.28 <0.28 <0.28 <2.1 <10.0 <2.8 <2.8 <0.84 <12.5 <.4 <1.4 <26.2 <100 <3.4 <13.8 Methylene Chloride 5 11.4 J <25.0 <73.8 <18.4 <2.4 <2.4 <5.0 <5.0 <3.7 <3.7 <3.7 <93 <50.0 <36.9 <36.9 <3.9 <62.5 <18.4 <18.4 <121 <500 <46.1 <184 Naphthalene 6 <2.4 <5.0 <7,0 <1.8 <0.60 <0.60 <1.0 <1.0 <0.35 <0.35 <0.35 <2.4 <10.0 <3.5 <3.5 <0.96 <12.5 <1.8 <1.8 <30.0 <100 <4.4 <17.6 Styrene 70 <2.6 <5.0 <5.3 <13 <0.65 <0.65 <1.0 <.0 <0.27 <0.27 <0.27 <2.6 <10.0 <23 <2.7 <1.0 <12.5 <1.3 <1.3 <32.5 <100 <3.3 <13.4 Tetrachloroethene 0.7 <4.6 181 282 71.7 22.5 22.4 51.3 53.5 44.4 44.1 45 1,260 1,070 935 1,120 714 1,290 821 891 20,600 7,610 1,500 3,870 Toluene 600 <2.6 <5.0 <4.9 <1.2 <0.65 <0.65 <1.0 <I.0 <0.24 <0.24 <0.24 <2.6 <10.0 <2.4 <2.4 1,0 <12.5 <1.2 <1.2 <32.5 <100 <3.0 <12.2 trans-1,2-Dichloroethene 100 <4.9 13.9 <5.1 <13 <1.2 <.2 0.8 J 0.8 J 1.1 1.2 1.0 <49 <10.0 <2.5 <2.5 <2.0 <12.5 <1.3 <1.3 <61.2 <100 7.3 J 110 trans-1,3-Dichloropropene 0.4 <2.6 <5.0 -6.2 <.5 <0.65 <0.65 <1.0 <.0 <0.31 <0.31 <0.31 <2.6 <10.0 <3.1 <3.1 <1.0 <12.5 <1.5 <1.5 <32.5 <100 1 <3.9 <15.4 Trichloroethee 3 <43 480 2,180 218 11.3 12.0 18.9 17.0 23.4 37.2 39.0 127 157 130 133 31.3 24.5 18.6 14.3 1,860 494 48.5 363 Trichlorofluoromethane 2,000 <2.0 <5.0 <6.2 <1.6 <0.50 <0.50 <1.0 <.0 <0.31 <0.31 <0.31 <2.0 <10.0 <3.1 <3.1 <0,80 <12.5 <1.6 <1.6 <25.0 <100 <3.9 <15.6 Vinyl acetate 88 <3.5 <10.0 <29.0 <7.2 <0.88 <0.88 <2.0 <2.0 <1.4 <1.4 <.4 <3.5 <20.0 <14.5 <14.5 <.4 <25.0 <7.2 <7.2 <43.8 <200 <18.1 <72.5 Vinyl chloride 0.03 226 10.7 75.6 19.0 <1.6 <1.6 <1.0 <.0 <0.24 <0.24 <0.24 <6.2 <10.0 <2.4 <2.4 <2.5 <12.5 <.2 <1.2 <77.5 <100 <3.0 <12.1 Xylene (total) 500 <10.0 <5.0 <12.6 <3.2 <.5 <2.5 <1.0 <.0 <0.63 <0.63 <0.63 <10.0 <10.0 <6.3 <6.3 <4.0 <12.5 <3.2 <3.2 <125 <100 <7.9 <31.5 m&p-Xylene 500 <6.6 Ill <8.2 <2.0 <16 <1.6 <2.0 <2.0 <0.41 <0.41 <0.41 <6.6 <20.0 <43 <4.1 <2.6 <25.0 <2.0 <2.0 <82.5 <200 <5.1 <20.5 o-Xylene 500 <2.3 <5.0 <4.4 <.1 <0.58 <0.58 <1.0 <.0 <0.22 <0.22 <0.22 <2.3 <10.0 <2.2 <2.2 <0.92 <12.5 <.1 <l.l <28.8 <100 <2.8 <11.0 p-Isopropyltoluene 25 <3.1 <5.0 <4.2 <1.1 <0.78 <0.78 <1.0 <I.0 <0.21 <0.21 <0.21 <3.1 <10.0 <2.1 <2.1 <L2 <12.5 -1 <.1 <38.8 <100 <2.6 rTolal.VOC, e(green=%decrease, red=%increase) L,407 1,364 �� 3,871 175% 998 29% 335 348 259 26°/ 248 29°<.. 162 52% 154 569s� 150 55% 1,495 ],322 12°4. 1,100 26°/ 1,347 10°6 745 1,315 76% 840 13% 905 21% 23,490 8,347 64°/� 2,008 91% 6,141 74% Other Parameters Persulfate (mg/L) NSL NA >70.0 0.7 1.4 NA NA 5.6 NA >70.0 49.0 49.0 NA 0.0 0.0 0.0 NA 0.0 0.0 2.8 NA >70.0 >70.0 >70.0 Iron (µg/L) 300 7,750 5,710 22,200 5,060 110 83.1 29.4 J 50 U 19.5 U 19.5 U 19.5 U 269 28.5 J 26.3 J 39.3 J 52.2 31.5 J 35.4 J 35.4 1,720 1,300 1,520 2,010 Chloride (mg/L) 250,000 14,500 14,300 10,000 9,000 7,500 7,500 7,700 7,800 7,400 7,800 8,300 10,600 10,600 9,600 10,000 7,800 8,200 7,600 7,900 10,600 22,200 19,800 15,800 Ethene (µg/L) NSL 53.9 10.0 U 19.70 4.26 U <10.0 <10.0 10.0 U 10.0 U 1.2 U 4.26 U 4.26 U 10.0 U 10.0 U 1.2 U 4.26 U <10.0 10.0 U 1.2 U 4.26 U <10.0 10.0 U 1.2 U 4.26 U Sulfate (mg/L) 250,000 20,000 1,380,000 414,000 634,000 8,300 8,600 54,800 81,700 141,000 265,000 265,000 14,700 15,500 12,200 19,100 9,500 11,000 10,300 10,000 10,100 458,000 505,000 232,000 Total Organic Carbon (mg/L) NSL 15,000 28,900 12,200 10,900 1,300 1,300 1,300 1,200 1,300 1,400 1,200 1,500 1,500 950 J 1,600 <500 620 J 530 J 500 U 2,800 5,300 4,000 3,300 Temperature CQ NSL 14.32 12.46 23.20 19.05 14.98 1 14.98 14.40 12.46 21.32 19.02 19.02 16.47 14.41 18.76 17.58 16.29 14.42 20.60 17.60 16.45 15.26 22.30 19.93 pH (standard) 6.5 to 8.5 6.25 3.06 4.88 5.58 7.31 7.31 7.15 3.06 6.54 9.51 9.51 5.63 6.11 6.00 5.69 5.76 6.22 5.88 5.86 5.61 4.18 4.25 5.16 Specific Conductance (µS/cm) NSL 367 2.10 1.10 1.27 430 430 0.368 2.100 0.733 0.931 0.931 172 0.138 0.190 0.198 214 0.177 0.240 0.242 155 4.48 2.87 0.764 Dissolved Oxygen (mg/L) NSL 0.98 0.23 0.00 0.00 0.10 0.10 0.21 0.32 3.69 1.27 1.27 1.94 0.84 0.00 0.17 0.30 0.91 0.29 0.48 0.60 0.18 0.00 4.14 Redox Potential(mV) NSL -64.0 411.7 123.0 130.0 -51.0 51.0 148.7 411.7 210.0 233.0 233.0 226.0 145.6 122.0 263.0 230.0 138.7 98.0 295.0 191.0 300.1 471.0 450.0 TABLE2 SUMMARY OF GROUNDWATER ANALYTICAL RESULTS TREX PROPERTIES, LLC CHARLOTTE, NC MW Designation NC 2L Standard PMW4A PMW-4A PMW4A PMW4A PMW-5A PMW-5A PMW-5A PMW-5A PMW-6A PMW-6A PMW-6A PMW-6A PMW-7A PMW-7A PMW-7A PMW-7A PMW-7B PMW-7B PMW-7B PMW-7B Depth or EPA Tap TD = 12 B. TD = 12 ft. TD = 12 B. TD = 12 B. TD = 39 ft. TD = 39 B. TD = 39 ft. TD = 39 B. TD = 38 B. TD = 38 ft. TD = 38 B. TD = 38 ft. TD = 38 B. TD = 38 ft. TD = 38 ft. TD = 38 ft. TD = 55 ft. TD = 55 B. TD = 55 ft. TD = 55 ft. Lab ID Water SL 92409026006 92418554016 92438460006 92461009006 92409026007 92418554017 92438460007 92461009007 92409026008 92418554018 92438460008 92461009008 92409026009 92418554019 92438460009 92461009009 92409026010 92418554020 92438460010 92461009010 Date 11/27/2018 2/20/2019 7/23/2019 1/15/2020 11/26/2018 2/19/2019 7/24/2019 1/14/2020 11/27/2018 2/19/2019 7/24/2019 1/14/2020 11/28/2018 2/20/2019 7/24/2019 1/14/2020 11/28/2018 2/20/2019 7/24/2019 1/14/2020 Volatile Organic Compound Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 12M ost 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post 1, 1, 1,2-Tetrachloroethane 1 <1.3 <2.0 <1.4 <0.68 <165 <500 <170 <340 <165 <500 <170 <170 <4.1 <12.5 <8,5 <6.8 <16.5 <10.0 <13.6 <8.5 1,1,1-Trichloroethane 200 28.1 27.2 44.5 21.4 1,630 <500 <87.5 6,710 <240 823.0 <87.5 820 <6.0 <12.5 <4.4 <3.5 <24.0 <10.0 <7.0 <4.4 1, 1,2,2-Tetrachloroethane 0.2 <1.6 6.2 27.0 10.6 <200 <500 <111 <222 <200 <500 <I11 <I11 <5.0 <12.5 <5.6 <4.4 <20.0 <10.0 <8.9 <5.6 1,1,2-Trichloroethane 0.6 <1.2 <2.0 <0.94 <0.47 <145 <500 <118 <236 <145 <500 <I18 <118 <3.6 <12.5 <5.9 <4,7 <14.5 <10.0 <9.4 <5.9 1,1-Dichloroethane 6 3 J 2.2 4.2 1.9 J <160 <500 <134 <268 <160 <500 <134 <134 <4.0 <12.5 <6.7 <5.4 <16.0 <10.0 <10.7 <6.7 1,1-Dichloroethene 350 4.7 <2.0 <0.98 <0.49 1,900 <500 <122 <245 3,330 <500 <122 <122 <7.0 <12.5 <6.1 <4.9 <28.0 <10.0 <9.8 <6.1 1,1-Dichloropropene NSL <2.0 <2.0 <0.85 <0.43 <245 <500 <106 <213 <245 <500 <106 <106 <6.1 <12.5 <5.3 <4.3 <24.5 <10.0 <8.5 <5.3 1,2,3-Trichlorobenzene 7 <1.3 <2.0 <1.4 <0.69 <165 <500 <172 <344 <165 <500 <172 <172 <4.1 <12.5 <8.6 <6.9 <16.5 11 <10.0 <13.8 <8.6 1,2,3-Trichloropropane 0.005 <1.6 <2.0 <1.4 <0.69 <205 <500 <174 <347 <205 <500 <174 <174 <5.1 <12.5 <8.7 <6.9 <20.5 <10.0 <13.9 <8.7 1,2,4-Trichlorobenzene 400 <1.4 <2.0 <0.87 <0.44 <175 <500 <109 <218 <175 <500 <109 <109 <4,4 <12.5 1,2-Dibromo-3-chloropropane 0.04 <8.0 <4.0 <1.0 <0.51 <1000 <1000 <128 <257 <1000 <1000 <128 <128 <25.0 <25.0 <6.4 <5.1 <100 <20.0 <10.3 <6.4 1,2-Dibromoethane (EDB) 0.02 <1.1 <2.0 <1.0 <0.52 <135 <500 <129 <258 <135 <500 <129 <129 <3.4 <12.5 <6.4 <5.2 <13.5 <I0.0 <10.3 <6.4 1,2-Dichlombenzene 20 <1.2 <2.0 <1.2 <0.58 <150 <500 <146 <291 <150 <500 <146 <146 <3.8 <12.5 <7.3 <5.8 <15.0 <10.0 <11.6 <7.3 1,2-Dichloroethane 0.4 <0.96 <2.0 <1.3 <0.67 <120 <500 <168 <336 <120 <500 <168 <168 <3.0 <12.5 <8.4 <6.7 <12.0 <10.0 <13.4 <8.4 1,2-Dichloropropane 0.6 <1.1 <2.0 <0.75 <0.37 <135 <500 <93.5 <187 <135 <500 <93.5 <93.5 <3.4 <12.5 <4.7 <3.7 <13.5 <10.0 <7,5 <4.7 1,3-Dichlorobenzene 200 <0.96 <2.0 <0.87 <0.43 <120 <500 <108 <217 <120 <500 <108 <108 <3.0 <12.5 <5.4 <4.3 <12.0 <10.0 <8,7 <5.4 1,3-Dichloropropane 0.6 <l.l <2.0 <0.63 <0.32 <140 <500 <79.0 <158 <140 <500 <79.0 <79.0 <3.5 <12.5 <4.0 <3.2 <14.0 <10.0 <6.3 <4.0 1,4-Dichlorobenzene 6 <1.3 <2.0 <1.0 <0.52 <165 <500 <129 <258 <165 <500 <129 <129 <4.1 <12.5 <6.4 <5.2 <16.5 <10.0 <10.3 <6.4 2,2-Dichloropropane NSL <0.52 <2.0 <l.l <0.54 <65.0 <500 <135 <270 <65.0 <500 <135 2-Butanone (MEK) 4,000 <3.8 <10.0 <13.3 <6.7 <480 <2500 <1660 <3330 <480 <2500 <1660 <1660 <12.0 <62.5 <83.2 <66.6 <48.0 <50.0 <133 <83.2 2-Chlorotoluene 100 <1.4 <2.0 <0.81 <0.41 <175 <500 <102 <203 <175 <500 <102 <102 <4.4 <12.5 <5.1 <4.1 <17.5 <10.0 <8.1 <5.1 2-Hexanone 40 <1.8 <10.0 <2.3 <1.1 <230 <2500 <284 <568 <230 <2500 <284 <284 <5.8 <62.5 <14.2 <I 1.4 <23.0 <50.0 <22.7 <14.2 4-Chlorotoluene 24 <1.2 <2.0 <0.82 <0.41 <155 <500 <102 <204 <155 <500 <102 <102 <3.9 <12.5 <5.1 <4.1 <15.5 <10.0 <8.2 <5.1 4-Methyl-2-pentanone (MIBK) 100 <1.3 <10.0 <18.1 <9.1 <165 <2500 <2260 <4530 <165 <2500 <2260 <2260 <4.1 <62.5 <113 1 <90.6 <16.5 <50.0 <181 <113 Acetone 6,000 <40.0 <50.0 <24.7 <12.3 <5000 <12500 <3080 19,600 J <5000 <12500 <3080 <3080 <125 <312 <154 351 J <500 <250 <247 464 J Benzene 1 <1.0 <2.0 4.6 <0.30 <125 <500 <75.0 <150 <125 <500 <75.0 <75.0 <3.1 5.4 J <3.8 6.7 il <12.5 1 <10.0 <6.0 <3.8 Bromobenzene 62 <1.2 1 <2.0 1 <0.88 <0.44 <150 <500 1 <110 <220 450 <500 <110 <110 <3.8 <12.5 <5.5 <q,q 45.0 <I0.0 <g,g <5.5 Bromochloromethane 83 <0.68 <2.0 <1.4 <0.69 <85.0 <500 <172 <343 <85.0 <500 <172 <172 <2.1 <12.5 <8.6 <6.9 <8,5 <I0.0 <13.7 <8.6 Bromodichloromethane 0.6 <0.72 <2.0 <1.0 <0.51 <90.0 <500 <128 <256 <90.0 <500 <128 <128 <2.2 <12.5 <6.4 <5.1 <9.0 <10.0 <10.2 <6.4 Bromoform 4 <1.0 <2.0 <2.5 <1.2 <130 <500 <308 <617 <130 <500 <308 <308 <3.2 <12.5 <15.4 <123 <13.0 <I0.0 <24.7 <15.4 Bromomethane 100 <1.2 <4.0 <2.5 <1.2 <145 <1000 <310 <620 <145 <1000 <310 <310 <3.6 <25.0 <15.5 <12.4 <14.5 <20.0 <24.8 <15.5 Carbon tetrachloride 0.3 <1.0 <2.0 <0.90 <0.45 <125 <500 <112 <224 <125 <500 <112 <112 <3.1 <12.5 <5.6 <4.5 <12.5 <10.0 <9.0 <5.6 Chlorobenzene 50 <0.92 <2.0 <0.93 <0.47 <115 <500 <116 <233 <115 <500 <116 <116 <2.9 <12.5 <5.8 <4.7 <11.5 <10.0 <9.3 <5.8 Chloroethane 3,000 <2.2 <2.0 <2.0 <0.98 <270 <500 <245 <490 <270 <500 <245 <245 <6.8 <12.5 <12.2 <9.8 <27.0 1 <10.0 <19.6 42.2 Chloroform 70 <0.56 <10.0 <9.4 1 <4.7 1 1 <70.0 <2500 1 <1170 <2340 <70.0 <2500 <I170 <I170 <1.8 1 <62.5 <58.5 <46.8 <7,0 <50.0 <93.6 <58.5 Chloromethane 3 <0.44 <2.0 <1.6 <0.78 <55.0 <500 <194 <389 <55.0 <500 <194 <194 <1.4 <12.5 <9.7 <7.8 <5.5 <10.0 <15.6 <9.7 cis-1,2-Dichloroethene 70 299 92.7 195 95.9 3,530 2300 1,990 1,400 5,350 2,330 2,710 2,610 249 340 239 357 47.1 J <10.0 38.6 J 34.2 cis-1,3-Dichloropropene 0.4 <0.52 <2.0 <1.2 <0.59 <65.0 <500 <148 <296 <65.0 <500 <148 <148 <1.6 <12.5 <7,4 <5.9 <6.5 <10.0 <11.8 <7.4 Dibromochloromethane 0.4 <0.84 <2.0 <1.7 <0.83 <105 <500 <206 <413 <105 <500 <206 <206 <2.6 <12.5 <10.3 <8.3 <10.5 <10.0 <16.5 <10.3 Dibromomethane 70 <0.84 <2.0 <1.8 <0.92 <105 <500 <230 <459 <105 <500 <230 <230 <2.6 <12.5 <11.5 <9.2 <10.5 <10.0 <18.4 <11.5 Dichlorodifluoromethane 1,000 <0.84 <2.0 <0.90 <0.45 <105 <500 <113 <226 <105 <500 <113 <113 <2.6 <12.5 <5.6 <4.5 <10.5 <10.0 <9.0 <5.6 Diisopropyl ether 1,500 <0.48 <2.0 <0.87 <0.44 <60.0 <500 <109 <218 <60.0 <500 <109 1 <109 <1.5 <12.5 <5.4 <4.4 <6.0 <10.0 <8.7 <5.4 Ethylbenzene 600 <1.2 <2.0 <1.0 <0.51 <150 <500 <128 <256 <150 <500 <128 <128 <3.8 <12.5 <6.4 <5.1 <15.0 <I0.0 <10.2 <6.4 Hexachloro-1,3-butadiene 0.4 <2.8 <2.0 <1.8 1 <0.88 1 <355 <500 <219 1 <438 <355 <500 <219 <219 <8.9 1 <12.5 <11.0 <8.8 <35.5 <10.0 <17.5 <11.0 Methyl-tert-butyl ether 20 <0.84 <2.0 <l.l <0.55 <105 <500 <138 <275 <105 <500 438 438 <2.6 <12.5 <6.9 <5.5 <10.5 <10.0 <11.0 <6.9 Methylene Chloride 5 <3.9 <10.0 <14.8 <7.4 <485 <2500 <1840 <3690 <485 <2500 <1840 <1840 <12.1 <62.5 <92.2 <73.8 <48.5 <50.0 <148 <92.2 Naphthalene 6 <0.96 <2.0 <1.4 <0.70 <120 <500 <176 <352 <120 <500 <176 <176 <3.0 <12.5 <8.8 <7.0 <12.0 <10.0 <14.1 <8.8 Styrene 70 <1.0 <2.0 <1.1 <0.53 <130 <500 <134 <267 <130 <500 434 1134 <3.2 <12.5 <6.7 <5.3 <13.0 <10.0 <10.7 <6.7 Tetrachloroethene 0.7 169 94.4 153 84.3 15,000 10,800 13,300 10,900 41,200 26,800 34,000 29,900 652 717 1,010 634 3,910 673 3,570 1,290 Toluene 600 <1.0 <2.0 <0,98 <0.49 <130 <500 <122 <244 <130 <500 <122 <122 3.2 <12.5 <6.1 <4.9 <13.0 <I0.0 <9.8 <6.1 trans- l,2-Dichloroethene 100 <2.0 3.9 7.0 2.3 <245 325 J 292 J <254 <245 349 J 419 J 398 J <6.1 <12.5 <6.4 <5.1 <24.5 <10.0 <10.2 <6.4 trans-1,3-Dichloropropene 0.4 <1.0 <2.0 <1.2 <0.62 <130 <500 <154 <309 <130 <500 454 <154 <3.2 <12.5 7.7 <6.2 <13.0 <10.0 <12.4 <7.7 Trichloroethene 3 583 252 381 233 75,900 50,500 98,900 93,600 86,000 48,400 57,400 49,700 1,690 2,200 2,560 1,670 8,280 1,280 5,330 2,130 Trichlorofluoromethane 2,000 <0.80 <2.0 4.2 <0.62 <100 <500 <156 <311 290 J 180 J 197 J <156 <2.5 <12.5 <7.8 <6.2 <10.0 <I0.0 <12.4 <7.8 Vinyl acetate 88 <1.4 <4.0 <5.8 <2.9 <175 <1000 <725 <1450 <175 <1000 <725 <725 <4.4 <25.0 <36.2 <29.0 <17.5 QO.0 <58.0 <36.2 Vinyl chloride 0.03 <2.5 <2.0 <0.97 <0.48 <310 <500 <121 <242 <310 <500 <121 <121 <7.8 <12.5 <6.0 <4.8 <31.0 <10.0 <9.7 <6.0 Xylene (total) 500 <4.0 <2.0 <2.5 <1.3 <500 <500 <315 <630 <500 <500 <315 <315 <12.5 <12.5 <15.8 <12.6 <50.0 <10.0 <25.2 <15.8 m&p-Xylene 500 <2.6 <4.0 <1.6 <0.82 <330 <1000 <205 <410 <330 <1000 <205 <205 <8.2 <25.0 <10.2 <8.2 <33.0 <20.0 <16.4 <10.2 o-Xylene 500 <0.92 <2.0 <0.88 <0.44 <115 <500 <110 <220 <115 <500 <110 <110 <2.9 <12.5 <5.5 <4.4 <11.5 <10.0 <8.8 <5.5 p-Isopropyltoluene 25 <1.2 <2.0 <0.85 <0.42 <155 <500 <106 <212 <155 <500 <106 <106 <3.9 <12.5 <5.3 <q.2 <15.5 <10.0 <8.5 <5.3 Total VOCs Change (green =%decrease, red =%increase) 1,087 479 56'% 816 25"/0 449 59"!� 97,960 63,925 35"/0 114,482 17% 132,210 35% 136,170 78,882 42% 94,726 30°/� 83,428 39% 2,591 3,262 26% 3,809 47% 3,019 17% 12,237 1,953 8,939 2T% 3,918 6R"' Other Parameters Persulfate (mg/L) NSL NA >70.0 14.0 0.0 NA >70.0 >70.0 >70.0 NA >70.0 >70.0 >70.0 NA 0.0 35.0 0.0 NA 0.0 0.5 0.0 Iron (µg/L) 300 623 337 93.5 242 6,330 387 215 449 9,940 3,290 7,090 663 402 1,400 472 1,030 345 1,420 1,550 725 Chloride (mg/L) 250,000 5,000 5,100 8,003 6,200 16,700 55,100 64,100 67,600 30,400 69,500 67,900 58,700 14,400 14,200 12,400 15,000 5,900 2,000 6,000 3,000 Ethene (µg/L) NSL 10.0 U 10.0 U 1.2 U 4.26 l; 10.0 U 10.0 U 1.2 U 4.26 U 10.0 U 10.0 U 1.2 U 4.26 U 10.0 U 10.0 U 1.2 U 4.26 U 10.0 U 10.0 U 1.4 J 4.26 U Sulfate (mg/L) 250,000 32,500 133,000 182,000 120,000 12,200 526,000 410,000 527,000 21,500 817,000 622,000 541,000 16,400 17,200 16,500 15,800 10,200 6,700 9,600 5,800 Total Organic Carbon (mg/L) NSL 1,400 2,400 3,100 1,500 2,000 8,000 8,600 9,000 3,600 9,300 7,400 8,200 710 J 940 J 860 J 690 J 500 J 7,300 1,500 3,600 Temperature (°C) NSL 17.50 13.01 21.16 17.06 19.22 16.02 23.11 19.45 18.50 16.23 23.21 20.43 16.68 16.52 21.22 19.50 17.10 15.49 1 21.26 18.69 pH (standard) 6.5 to 8.5 6.00 6.10 5.78 5.73 6.60 5.34 5.55 5.15 6.10 3.86 4.56 4.75 5.94 6.38 5.87 5.87 1 6.17 7.19 6.33 6.34 Specific Conductance (µS/cm) NSL 178.0 0.383 0.621 0.385 0.243 4.078 2.05 1.86 0.255 11.25 4.73 2.02 215 0.180 0.235 0.223 235.0 0.100 63 0.196 Dissolved Oxygen (mg/L) NSL 3.47 2.32 1.68 3.97 0.30 0.34 0.00 0.00 0.75 0.24 0.00 0.00 0.10 0.34 0.00 0.00 0.10 4.79 %. 0.00 1.09 Redox Potential (mV) NSL 234.0 132.5 90.0 217.0 10.2 359.8 237.0 366.0 -21.7 431.3 453.0 491.0 211.0 131.3 260.0 166.0 212.0 117.8 108.0 156.0 TABLE2 SUMMARY OF GROUNDWATER ANALYTICAL RESULTS TREX PROPERTIES, LLC CHARLOTTE, NC MW Designation NC 2L Standard PMW-8A PMW-8A PMW-8A PMW-8A PMW-8B PMW-8B PMW-8B PMW-8B PMW-9A PMW-9A PMW-9A PMW-9A PMW-9B PMW-9B PMW-9B PMW-9B PMW-9C PMW-9C PMW-9C PMW-9C Depth or EPA Tap TD = 42 ft. TD = 42 ft. TD = 42 B. TD = 42 ft. TD = 58 ft. TD = 58 ft. TD = 58 ft. TD = 58 ft. TD = 19 B. TD = 19 ft. TD = 19 B. TD = 19 B. TD = 34 B. TD = 34 B. TD = 34 ft. TD = 34 ft. TD = 50 ft. TD = 50 ft. TD = 50 ft. TD = 50 ft. Lab ID Water SL 92409026011 92418554021 92438460011 92461009011 92409026012 92418554022 92438460012 92461009012 92409026013 92418554001 92438460013 92461009013 92409026014 92418554002 92438460014 92461009014 92409026015 92418554003 92438460015 92461009015 Date 11/26/2018 2/20/2019 7/23/2019 1/14/2020 11/26/2018 2/20/2019 7/23/2019 1/15/2020 11/27/2018 2/19/2019 7/23/2019 1/15/2020 11/27/2018 2/19/2019 7/23/2019 1/15/2020 11/27/2018 2/19/2019 7/23/2019 1/15/2020 Volatile Organic Compound Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post 1, 1, 1,2-Tetrachloroethane 1 <1.6 <5.0 <1.7 <1.7 <1.6 <5.0 <1.7 <1.7 <1.6 <4.0 <0.85 <0.85 <3.3 <I0.0 <3.4 <6.8 <33.0 <5.0 <85.0 <85.0 1,1,1-Trichloroethane 200 <2.4 <5.0 <0.88 <0.88 <2.4 <5.0 <0.88 <0.88 <2.4 <4.0 <0.44 <0.44 <4.8 <10.0 <1.8 <3.5 <48.0 <5.0 <43.8 <43.8 1, 1,2,2-Tetrachloroethane 0.2 <2.0 <5.0 <1.1 <l.l <2.0 <5.0 <1.1 <l.l <2.0 <4.0 <0.56 <0.56 <4.0 <10.0 <2.2 <4,4 <40.0 <5.0 <55.5 <55.5 1,1,2-Trichloroethane 0.6 <1.4 <5.0 <1.2 <1.2 11.4 <5.0 <1.2 <1.2 <1.4 <4.0 <0.59 <0.59 <2.9 <10.0 <2.4 <4.7 <29.0 <5.0 <59.0 <59.0 1,1-Dichloroethane 6 <1.6 <5.0 <1.3 <1.3 3.3 J 3.3 J 3.0 J 2.5 J 8.5 7 5.8 4.3 <3.2 3.9 J 4.5 J <5.4 <32.0 <5.0 <67.0 <67.0 1,1-Dichloroethene 350 10.4 11.7 8.9 6.7 16 12.9 8.3 5.7 3.5 J 3.3 J 3.1 2.6 11.5 25.3 31.2 33.6 535 26.2 2,260 2,400 1,1-Dichloropropene NSL <2.4 <5.0 <l.l <l.l <2.4 <5.0 <I.1 <l.l <2.4 <4.0 <0.53 <0.53 <4.9 <10.0 <2.1 <4.3 <49.0 <5.0 <53.2 1,2,3-Trichlorobenzene 7 <1.6 <5.0 <1.7 <1.7 <1.6 <5.0 <1.7 <1.7 <1.6 <4.0 <0.86 <0.86 <3.3 <10.0 <3.4 <6.9 <33.0 <5.0 <86.0 <86.0 1,2,3-Trichloropropane 0.005 <2.0 <5.0 <1.7 <1.7 <2.0 <5.0 <1.7 <1.7 <2.0 <4.0 <0.87 <0.87 <4.1 <10.0 <3.5 <6.9 <41.0 <5.0 <86.8 <86.8 1,2,4-Trichlorobenzene 400 <1.8 <5.0 <l.l <l.l <1.8 <5.0 <I.1 <1.1 3.9 J 4.3 4.4 3.8 28.8 44.0 42.4 64.0 <35.0 <5.0 <54.5 <54.5 1,2-Dibromo-3-chloropropane 0.04 <10.0 <10.0 <1.3 <1.3 <10.0 <10.0 <1.3 <1.3 <10.0 <8.0 <0.64 <0.64 <20.0 <20.0 <2.6 <5.1 <200 <10.0 <64.2 <64.2 1,2-Dibromoethane (EDB) 0.02 <1.4 <5.0 <1.3 <1.3 <1.4 <5.0 <1.3 <1.3 <1.4 <4.0 <0.64 <0.64 <2.7 <10.0 <2.6 <5.2 <27.0 <5.0 <64.5 <64.5 1,2-Dichlorobenzene 20 <1.5 <5.0 <1.5 <1.5 <1.5 <5.0 <1.5 <1.5 <1.5 <4.0 <0.73 <0.73 <3.0 <10.0 <2.9 <5.8 <30.0 <5.0 <72.8 <72.8 1,2-Dichloroethane 0.4 <1.2 <5.0 <1.7 <1.7 <1.2 <5.0 <1.7 <1.7 <1.2 <4.0 <0.84 <0.84 <2.4 <10.0 <3.4 <6.7 <24.0 <5.0 <84.0 <84.0 1,2-Dichloropropane 0.6 <1.4 <5.0 <0.94 <0.94 <1.4 <5.0 <0.94 <0.94 <1.4 <4,0 <0.47 <0.47 <2.7 <10.0 <1.9 <3.7 <27.0 <5.0 <46.8 <46.8 1,3-Dichlorobenzene 200 <1.2 <5.0 <1.1 <l.l <1.2 <5.0 <l.l <1.1 1.5 J 1.5 J 1.9 J <0.54 4.7 J 7.1 J 8.1 J 10.2 J <24.0 <5.0 <54.2 <54.2 1,3-Dichloropropane 0.6 <1.4 <5.0 <0.79 <0.79 <1.4 <5.0 <0.79 <0.79 <1.4 <4.0 <0.40 <0.40 <2.8 <10.0 <1.6 <3.2 <28.0 <5.0 <39.5 <39.5 1,4-Dichlorobenzene 6 <1.6 <5.0 <1.3 <1.3 <1.6 <5.0 <1.3 <1.3 13.0 <4.0 17.1 <0.64 <3.3 <10.0 <2.6 <5.2 <33.0 <5.0 <64.5 <64.5 2,2-Dichloropropane NSL <0.65 <5.0 <1.4 <1.4 <0.65 <5.0 <1.4 <1.4 <0.65 <4.0 <0.68 <0.68 <1.3 <10.0 <2.7 <5.4 <13.0 <5.0 <67.5 <67.5 2-Butanone (MEK) 4,000 <4.8 <25.0 <16.6 <16.6 <4,8 <25.0 <16.6 <16.6 <4,8 <20.0 <8,3 <83 <9.6 <50.0 <33.3 <66.6 <96.0 <25.0 <832 <832 2-Chlorotoluene 100 <1.8 <5.0 <1.0 <1.0 <1.8 <5.0 <1.0 <1.0 <1.8 <4.0 <0.51 <0.51 <3.5 <10.0 <2.0 <4.1 <35.0 <5.0 <50.8 <50.8 2-Hexanone 40 <2.3 <25.0 <2.8 <2.8 <2.3 <25.0 <2.8 <2.8 <2.3 <20.0 <1.4 <1.4 <4.6 <50.0 <5.7 <11.4 <46.0 <25.0 <142 <142 4-Chlorotoluene 24 <1.6 <5.0 <1.0 <1.0 <1.6 <5.0 <1.0 <1.0 <1.6 <4.0 <0.51 <0.51 <3.1 <10.0 <2.0 <4.1 <31.0 <5.0 <51.0 <51.0 4-Methyl-2-pentanone (MIBK) 100 <1.6 <25.0 <22.6 <22.6 <1.6 <25.0 <22.6 <22.6 <1.6 <20.0 <11.3 <I 1.3 <3.3 <50.0 <45.3 <90.6 <33.0 <25.0 <1130 <1130 Acetone 6,000 <50.0 <125 <30.8 <30.8 <50.0 <125 <30.8 <30.8 <50.0 <100 <15.4 <15.4 <100 <250 1 1 <61.7 353 J J <1000 <125 <1540 <1540 Benzene 1 <1.2 <5.0 <0.75 <0,75 <1.2 1 1 <5.0 <0.75 <0.75 6 4.5 1 4.5 4.0 10.9 1 15.5 15.2 15.8 J <25.0 <5.0 <37.5 <37.5 Bromobenzene 62 <1.5 <5.0 <1.1 <l.l <1.5 <5.0 1 <1.1 <l.l <1.5 <4.0 <0.55 <0.55 <3.0 <10.0 <22 Bromochloromethane 83 <0.85 <5.0 <1.7 <1.7 <0.85 <5.0 <1.7 <1.7 <0.85 <4.0 <0.86 <0.86 <1.7 <10.0 <3.4 <6.9 <17.0 <5.0 <85.8 <85.8 Bromodichloromethane 0.6 <0.90 <5.0 <1.3 <1.3 <0.90 <5.0 <1.3 <1.3 <0.90 <4.0 <0.64 <0.64 <1.8 <10.0 <2.6 <5.1 <18.0 <5.0 <64.0 <64.0 Bromoform 4 <1.3 <5.0 <3.1 <3.1 <1.3 <5.0 <3.1 <3.1 <1.3 <4.0 <1.5 <1.5 <2.6 <10.0 <6.2 <12.3 <26.0 <5.0 <154 <154 Bromomethane 100 <1.4 <10.0 <3.1 <3.1 <1.4 <10.0 <3.1 <3.1 <1.4 <8.0 <1.6 <1.6 <2.9 <20.0 <6.2 <12.4 <29.0 <10.0 <155 <155 Carbon tetrachloride 0.3 <1.2 <5.0 <1.1 <l.l <1.2 <5.0 <1.1 <l.l <1.2 <4.0 <0.56 <0.56 <2.5 <10.0 <22 <4,5 <25.0 <5.0 <56.0 <56.0 Chlorobenzene 50 <1.2 <5.0 <1.2 <1.2 <1.2 <5.0 <1.2 <1.2 1.3 J <4.0 <0.58 <0.58 20.2 <10.0 <2.3 <4.7 <23.0 <5.0 <58.2 <58.2 Chloroethane 3,000 <2.7 <5.0 <2.4 <2.4 <2.7 <5.0 <2.4 <2.4 <2.7 <4.0 <1.2 <1.2 <5.4 <10.0 <4.9 <9.8 <54.0 <5.0 <122 <122 Chloroform 70 8.3 13.6 J <11.7 <] 1.7 1.7 JJJ <25.0 1 <11.7 <11.7 <0.70 <20.0 <5.8 <5.8 <1.4 <50.0 1 <23.4 <46.8 <14.0 <25.0 1 <585 <585 Chloromethane 3 <0.55 <5.0 <1.9 <1.9 <0.55 <5.0 <1.9 <1.9 <0.55 <4.0 <0.97 <0.97 <l.l <10.0 <3.9 <7.8 <11.0 <5.0 <97.2 <97.2 cis-1,2-Dichloroethene 70 28.2 1 41.5 1 31.1 28.2 52.0 51.5 39.3 35.4 515 413 364 408 1,150 1,200 1,690 1,170 1 308 105 871 960 cis-1,3-Dichloropropene 0.4 <0.65 <5.0 <1.5 <1.5 <0.65 <5.0 <1.5 <1.5 <0.65 <4,0 <0.74 <0.74 <1.3 <10.0 <3.0 <5.9 <13.0 <5.0 <74.0 <74.0 Dibromochloromethane 0.4 <1.0 <5.0 <2.1 <2.1 <1.0 <5.0 <2.1 <2.1 <1.0 <4.0 <1.0 <1.0 <2.1 <10.0 <4.1 <8.3 <21.0 <5.0 <103 <103 Dibromomethane 70 <1.0 <5.0 <2.3 <2.3 <1.0 <5.0 <2.3 <2.3 <1.0 <4.0 <1.1 <1.1 <2.1 <10.0 <4.6 <9.2 <21.0 <5.0 <115 <115 Dichlorodifluoromethane 1,000 <1.0 <5.0 <l.l <l.l <1.0 <5.0 <1.1 <l.l <1.0 <4.0 <0.56 <0.56 <2.1 1 <10.0 <2.3 <4.5 1 <21.0 <5.0 <56.5 <56.5 Diisopropyl ether 1,500 <0.60 <5.0 <l.l <l.l <0.60 <5.0 <1.1 <l.l <0.60 <4.0 <0.54 <0.54 <1.2 <10.0 <2.2 <4.4 <12.0 <5.0 <54.5 <54.5 Ethylbenzene 600 <1.5 <5.0 <1.3 <1.3 <1.5 <5.0 <1.3 <1.3 <1.5 <4.0 <0.64 <0.64 <3.0 <10.0 <2.6 <5.1 <30.0 <5.0 <64.0 <64.0 Hexachloro-1,3-butadiene 0.4 <3.6 <5.0 <2.2 <2.2 <3.6 <5.0 1 <2.2 1 <2.2 <3.6 <4.0 <l.l <l.l <7.1 <10.0 <4.4 <8.8 <71.0 <5.0 <110 <110 Methyl-tert-butyl ether 20 <1.0 <5.0 <1.4 <1.4 <1.0 <5.0 <1.4 <1.4 <1.0 <4.0 <0.69 <0.69 <2.1 <10.0 <2.8 <5.5 <21.0 <5.0 <68.8 <68.8 Methylene Chloride 5 <4.8 <25.0 <18.4 <18.4 <4.8 <25.0 <18.4 <18.4 <4.8 <20.0 <9.2 <9.2 <9.7 <50.0 <36.9 <73.8 <97.0 <25.0 <922 <922 Naphthalene 6 <1.2 <5.0 <1.8 <1.8 <1.2 <5.0 <1.8 <1.8 <1.2 <4.0 <0.88 <0.88 <2.4 <10.0 <3.5 <7.0 <24.0 <5.0 <88.0 <88.0 Styrene 70 <1.3 15.0 <1.3 <1.3 <1.3 <5.0 <1.3 <1.3 <1.3 <4.0 <0.67 <0.67 <2.6 <I 0.0 <2.7 <5.3 <26.0 <5.0 <66.8 <66.8 Tetrachloroethene 0.7 52.3 67.8 62.1 67.9 81.8 24.5 39.5 19.8 <2.3 2.5 J <0.40 2.6 180 665 523 731 4,480 389 16,900 22,100 Toluene 600 <1.3 <5.0 <1.2 1,2 <1.3 <5.0 <12 <1.2 <1.3 <4.0 <0.61 <0.61 <2.6 <I0.0 <2.4 <4,9 <26,0 <5.0 <61.0 <61.0 trans-1,2-Dichloroethene 100 <2.4 <5.0 <1.3 <1.3 <24 <5.0 <1.3 <1.3 12.7 7.4 5.5 4.2 <4.9 <10.0 5.7 J <51 <49.0 <5.0 <63.5 <63.5 trans-1,3-Dichloropropene 0.4 <1.3 -5.0 <1.5 <1.5 <1.3 <5.0 <1.5 <1.5 <1.3 <4.0 <0.77 <0.77 <2.6 <10.0 <3.1 <6.2 <26.0 <5.0 <77.2 <77.2 Trichloroethene 3 597 590 565 516 995 598 589 474 36.9 37.1 17.4 90.2 590 1,730 1,230 1,720 12,300 785 42,600 48,600 Trichlorofluoromethane 2,000 <1.0 <5.0 <1,6 <.L6 <LO <5.0 <1.6 <1.6 <1.0 <4,0 <0.78 <0.78 <2.0 <10.0 <3.1 <6.2 <20.0 <5.0 <77.8 <77.8 Vinyl acetate 88 <1.8 <10.0 <7.2 <7.2 <1.8 <10.0 <7.2 <7.2 <1.8 <8.0 <3.6 <3.6 <3.5 <20.0 <14.5 <29.0 <35.0 <10.0 <362 1 <362 Vinyl chloride 0.03 <3.1 <5.0 <1.2 <1.2 <3.1 <5.0 <1.2 4.2 98.1 94.2 82.0 61.2 96.5 80.2 90.3 56.9 <62.0 <5.0 <60.5 <60.5 Xylene (total) 500 <5.0 <5.0 <3.2 <3.2 <5.0 <5.0 <3.2 <3.2 <5.0 <4.0 <1.6 <1.6 40.0 40.p <6.3 <12.6 <100 <5.0 <158 <158 m&p-Xylene 500 <3.3 <10.0 <2.0 <2.0 <3.3 <10.0 <2.0 <2.0 <3.3 <8.0 <1.0 <1.0 <6.6 <20.0 <4.1 <8.2 <66.0 40.p <102 <102 o-Xylene 500 <12 <5.0 <l.l <l.l <1.2 <5.0 4.1 <l.l <1.2 <4.0 <0.55 <0.55 <2.3 40.0 <2.2 <4.4 <23.0 <5.0 <55.0 <55.0 p-Isopropyltoluene 25 <1.6 <5.0 <].1 <l.l <L6 <5.0 <Ll <],I <],6 <4.0 <0.53 <0.53 <3.1 <I0.0 <2.1 <4.2 <31.0 <5.0 <53.0 <53.0 Total VOCs Change(green=%decrease, red=%increase) 696 725 4% 667 4°/, 619 II''� 1,150 690 100/, 679 41°,. 537 53% 700 575 18% 506 28% 581 170i6 2,093 3,771 80% 3,640 74% 3,802 821% 17,623 1,305 930. 62,631 _--' 74,060 - Other Parameters Persulfate (mg/L) NSL NA 0.0 0.0 0.0 NA 0.0 0.0 0.0 NA 0.0 0.0 4.2 NA 0.0 0.0 0.0 NA 0.0 0.0 4.2 Iron (µg/L) 300 308 1,120 2,160 646 931 1,370 646 2,040 19,000 19,200 18,600 16,600 1,840 594 1,180 655 4,190 2,720 2,610 1,250 Chloride (mg/L) 250,000 6,900 6,900 7,000 6,900 7,000 6,800 6,500 6,300 33,200 29,500 26,700 38,400 42,400 33,400 35,700 32,700 8,500 2,000 23,900 31,100 Ethene (µg/L) NSL 10.0 U 10.0 U 1.2 U 4.26 U 10.0 U 10.0 U 2.4 J 4.26 U 36.1 37.1 33.4 17 10.6 10.0 13.5 4.26 U 10.0 U 10.0 U 2.2 J 4.26 U Sulfate (mg/L) 250,000 13,500 13,900 14,400 13,800 83,800 72,300 63,400 60,700 1,300 1,200 2,200 2,000 3,900 5,100 4,900 5,300 3,300 16,600 6,700 35,800 Total Organic Carbon (mg/L) NSL 2,400 1,000 U 500 U 500 U 2,000 2,800 3,100 1,500 5,900 7,600 7,600 5,100 1,600 2,300 2,000 1,100 2,300 3,900 2,300 2,100 Temperature (°C) NSL 17.72 16.29 20.49 19.17 17.72 15.52 20.90 18.65 18.29 14.69 22.84 17.03 17.05 15.64 19.75 17.64 16.51 15.44 19.52 18.48 pH (standard) 6.5 to 8.5 6.70 6.82 5.91 5.39 8.10 8.28 7.46 7.69 6.50 6.85 6.29 5.89 6.40 6.50 6.15 5.86 6.90 7.25 6.45 Specific Conductance (µS/cm) NSL 0.172 0.160 0.217 0.205 0.123 0.660 0.856 0.780 0.489 0.465 0.621 0.580 0.402 0.337 4.540 0.422 0.101 0.126 0.330 Dissolved Oxygen (mg/L) NSL 1.00 1.40 0.00 3.67 OA4 2.05 0.00 0.00 0.36 1.75 0.00 0.16 1.00 0.45 0.00 0.34 1.00 3.96 0.00 rn� Redox Potential (mV) NSL -17.8 126.0 157.0 249.0 -92.2 175.3 30.0 -15.0 -125.4 -32.4 -90.0 -17.0 -50.7 69.0 -7.11 46.0 -68.0 51.2 -36.0 TABLE2 SUMMARY OF GROUNDWATER ANALYTICAL RESULTS TREX PROPERTIES, LLC CHARLOTTE, NC MW Designation NC 2L PMW-10A PMW-10A PMW-DUP2 PMW-10A PMW-10A PMW-10A (DUPI) PMW-10B PMW-10B PMW-10B PMW-10B PMW-11A PMW-11A PMW-11A PMW-11A PMW-11B PMW-11B PMW-11B PMW-11B PMW-13B PMW-13B (PMW-DUPI) PMW-13B PMW-13B PMW-13B Depth Standard or EPA Tap TD = 63 ft. TD = 63 ft. TD = 63 ft. TD = 63 ft. TD = 63 ft. TD = 63 ft. TD = 73 ft. TD = 73 ft. TD = 73 ft. TD = 73 ft. TD = 63 ft. TD = 63 ft. TD = 63 ft. TD = 63 ft. TD = 78 ft. TD = 78 ft. TD = 78 ft. TD = 78 ft. TD =103 ft. TD =103 ft. TD =103 ft. TD =103 ft. TD =103 ft. Lab ID Water SL 92409026016 92418554004 92418554010 92438460016 92461009016 92461009021 92409026018 92418554005 92438460017 92461009017 92409026016 92418554006 92438460018 92461009018 92409026019 92418554007 92438460019 92461009019 92409026020 92409026021 92418554008 92438460020 92461009020 Date 11/27/2018 2/19/2019 2/19/2019 7/23/2019 1/15/2020 1/15/2020 11/27/2018 2/19/2019 7/23/2019 1/15/2020 11/27/2018 2/20/2019 7/23/2019 1/14/2020 11/26/2018 2/20/2019 7/23/2019 1/14/2020 11/27/2018 11/27/2018 2/19/2019 7/23/2019 1/14/2020 Volatile Organic Compound Pre -Injection 1-M post 1-M post 6-M post 12-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection 1-M post 6-M post 12-M post Pre -Injection Pre -Injection 1-M post 6-M post 12-M post 1, 1, 1,2-Tetrachloroethane 1 <165 <250 <200 <85.0 <85.0 <85.0 <132 <50.0 <85.0 <85.0 <6.6 <5.0 <1.4 <0.34 <4.1 <5.0 <1.7 <3.4 <3.3 <3.3 <I0.0 <3.4 <85.0 1,1,1-Trichloroethane 200 653 524 499 <43.8 <43.8 430 <192 211 <43.8 <43.8 <9.6 3.8 J <0.70 15.9 <6.0 <5.0 <0.88 5.8 J 1, 1,2,2-Tetrachloroethane 0.2 <200 <250 <200 <55.5 <55.5 <55.5 <160 <50.0 <55.5 <55.5 <8.0 <5.0 <0.89 <0.22 <5.0 <5.0 <1.1 <22 <4.0 <4,0 <10.0 <2.2 <55.5 1,1,2-Trichloroethane 0.6 <145 <250 <200 <59.0 <59.0 <59.0 <116 <50.0 <59.0 <59.0 <5.8 <5.0 <0.94 <0.24 <3.6 <5.0 <1.2 <2.4 <2.9 <2.9 <10.0 <2.4 <59.0 1,1-Dichloroethane 6 <160 <250 <200 <67.0 <67.0 86.4 J <128 40.9 J <67.0 <67.0 <6.4 <5.0 7.1 3.9 <4.0 <5.0 2.7 J 4.0 J <3.2 <3.2 <10.0 <2.7 <67.0 1,1-Dichloroethene 350 2,110 <251 <200 <61.2 454 422 1,380 <50.1 <61.2 209 J 39.1 7.3 <0.98 <0.24 22.2 5.0 13.7 12.2 27.5 26.6 27.4 17.9 471 1,1-Dichloropropene NSL <245 <250 <200 <53.2 <53.2 <53.2 <196 <50.0 <53.2 <53.2 <9.8 <5.0 <0.85 <0.21 <6.1 <5.0 <l.l <2.1 <4.9 <4.9 <10.0 <2.1 <53.2 1,2,3-Trichlorobenzene 7 <165 <250 <200 <86.0 <86.0 <86.0 <132 <50.0 <86.0 <86.0 <6.6 <5.0 <1.4 <0.34 <4.1 <5.0 <1.7 <3.4 <3.3 <3.3 <I0.0 <3.4 <86.0 1,2,3-Trichloropropane 0.005 <205 <250 <200 <86.8 <86.8 <86.8 <164 <50.0 <86.8 <86.8 <82 <5.0 <1.4 <0.35 <5.1 <5.0 <1.7 <3.5 <4.1 <4.1 <I0.0 <3.5 <86.8 1,2,4-Trichlorobenzene 400 <175 <250 <200 <54.5 <54.5 <54.5 <140 <50.0 <54.5 <54.5 <7.0 <5.0 <0.87 <0.22 <4.4 <5.0 <l.l <2.2 1,2-Dibromo-3-chloropropane 0.04 <1000 <500 <400 <64.2 <64.2 <64.2 <800 <100 <64.2 <64.2 <40.0 <10.0 <1.0 <0.26 <25.0 <10.0 <1.3 <2.6 <20.0 <20.0 <20.0 <2.6 <64.2 1,2-Dibromoethane (EDB) 0.02 <135 <250 <200 <64.5 <64.5 <64.5 <108 <50.0 <64.5 <64.5 <5.4 <5.0 <1.0 <0.26 <3.4 <5.0 <1.3 <2.6 <2.7 <2.7 <I0.0 <2.6 <64.5 1,2-Dichlorobenzene 20 <150 <250 <200 <72.8 <72.8 <72.8 <120 <50.0 <72.8 <72.8 <6.0 <5.0 <1.2 <0.29 <3.8 <5.0 <1.5 <2.9 <3.0 <3.0 <10.0 <2.9 <72.8 1,2-Dichloroethane 0.4 <120 <250 <200 <84.0 <84.0 <84.0 <96.0 <50.0 <84.0 <84.0 <4.8 <5.0 1.9 J 0.89 J <3.0 <5.0 <1.7 <3.4 <2.4 <2.4 <10.0 <3.4 <84.0 1,2-Dichloropropane 0.6 <135 <250 <200 <46.8 <46.8 <46.8 <108 <50.0 <46.8 <46.8 <5.4 <5.0 <0.75 <0.19 <3.4 <5.0 <0.94 <1.9 <2.7 <2.7 <10.0 <1.9 <46.8 1,3-Dichlorobenzene 200 <120 <250 <200 <54.2 <54.2 <54.2 <96.0 <50.0 <54.2 <54.2 <4.8 <5.0 <0.87 <0.22 <3.0 <5.0 <1.1 <2.2 <2.4 <2.4 <I0.0 <2.2 <54.2 1,3-Dichloropropane 0.6 <140 <250 <200 <39.5 <39.5 <39.5 <112 <50.0 <39.5 <39.5 <5.6 <5.0 <0.63 <0.16 <3.5 <5.0 <0.79 <1.6 <2.8 <2.8 <10.0 <1.6 <39.5 1,4-Dichlorobenzene 6 <165 <250 <200 <64.5 <64.5 <64.5 <132 <50.0 <64.5 <64.5 <6.6 <5.0 <1.0 <0.26 <4.1 <5.0 <1.3 <2.6 <3.3 <3.3 <10.0 <2.6 <64.5 2,2-Dichloropropane NSL <65.0 <250 <200 <67.5 <67.5 <67.5 <52.0 <50.0 <67.5 <67.5 <2.6 <5.0 <1.1 <0.27 <1.6 <5.0 <1.4 <2.7 <1.3 <1.3 <10.0 <2.7 <67.5 2-Butanone (MEK) 4,000 <480 <1250 <1000 <832 <832 <832 <384 <250 <832 <832 <19.2 <25.0 <13.3 <3.3 <12.0 <25.0 <16.6 <33.3 <9.6 <9.6 <50.0 <33.3 <832 2-Chlorotoluene 100 <175 <250 <200 <50.8 <50.8 <50.8 <140 <50.0 <50.8 <50.8 <7.0 <5.0 <0.81 <0.20 <4.4 <5.0 <1.0 2-Hexanone 40 <230 <1250 <1000 <142 <I42 <142 <184 <250 <142 <142 <9.2 <25.0 <2.3 <0.57 <5.8 <25.0 <2.8 <5.7 <4.6 <4.6 <50.0 <5.7 <142 4-Chlorotoluene 24 <155 <250 <200 <51.0 <51.0 <51.0 <124 <50.0 <51.0 <51.0 <6.2 <5.0 <0.82 <0.20 <3.9 <5.0 <1.0 <2.0 <3.1 <3.1 <10.0 <2.0 <51.0 4-Methyl-2-pentanone (MIBK) 100 <165 <1250 <1000 <1130 <1130 <1130 <132 <250 <1130 <1130 <6.6 <25.0 <18.1 1 <4.5 <4.1 <25.0 <22.6 <45.3 <3.3 <3.3 <50.0 <45.3 <1130 Acetone 6,000 <5000 <6250 <5000 1 1 <1540 <1540 <1540 <4000 1,340 <1540 <1540 <200 <125 <24.7 <6.2 1 <125 <125 <30.8 161 J <100 <100 <250 <61.7 4,670 J Benzene 1 <125 <250 <200 <37.5 <37.5 <37.5 <100 <50.0 <37.5 <37.5 <5.0 <5.0 <0.60 <0.15 <3.1 <5.0 <0.75 <1.5 <2.5 <2.5 <10.0 <1.5 <37.5 Bromobenzene 62 <150 <250 <200 <55.0 <55.0 <55.0 <120 <50.0 <55.0 <55.0 <6.0 <5.0 <0.88 <0.22 <3.8 <5.0 <l.l <22 <3.0 <3.0 <10.0 <22 <55.0 Bromochloromethane 83 <85.0 <250 <200 <85.8 <85.8 <85.8 <68.0 <50.0 <85.8 <85.8 <3.4 <5.0 <1.4 <0.34 <2.1 <5.0 <1.7 <3.4 <1.7 <1.7 <10.0 <3,4 <85.8 Bromodichloromethane 0.6 <90.0 <250 <200 <64.0 <64.0 <64.0 <72.0 <50.0 <64.0 <64.0 <3.6 <5.0 <1.0 <0.26 <2.2 <5.0 <1.3 <2.6 <1.8 <1.8 <10.0 <2.6 <64.0 Bromoform 4 <130 <250 <200 <154 <154 <154 <104 <50.0 <154 <154 <5.2 <5.0 <2.5 <0.62 <3.2 <5.0 <3.1 <6.2 <2.6 <2.6 <10.0 <6.2 <154 Bromomethane 100 <145 <500 <400 <155 <155 <155 <116 <100 <155 <155 <5.8 <10.0 <2.5 <0.62 <3.6 <10.0 <3.1 <6.2 <2.9 <2.9 Q0.0 <6.2 <155 Carbon tetrachloride 0.3 <125 <250 <200 <56.0 <56.0 <56.0 <100 <50.0 <56.0 <56.0 <5.0 <5.0 <0.90 <0.22 <3.1 <5.0 <l.l <22 <2.5 <2.5 <10.0 <22 <56.0 Chlorobenzene 50 <115 <250 <200 <58.2 <58.2 <58.2 <92.0 <50.0 <58.2 <58.2 <4.6 <5.0 <0.93 <0.23 <2.9 <5.0 <1.2 <2.3 <2.3 <2.3 <10.0 <2.3 <58.2 Chloroethane 3,000 <270 <250 <200 <122 <122 <122 <216 <50.0 <122 <122 <10.8 <5.0 <2.0 <0.49 <6.8 <5.0 <2.4 <4.9 <5.4 <5.4 <10.0 <4.9 <122 Chloroform 70 <70.0 <1250 <1000 <585 <585 <585 <56.0 <250 <585 <585 <2.8 <25.0 <9.4 <2.3 Chloromethane 3 <55.0 <250 <200 <97.2 <97.2 <97.2 <44.0 <50.0 <97.2 <97.2 <2.2 <5.0 <1.6 <0.39 <1.4 <5.0 <1.9 <3.9 <l.l <1.1 <10.0 <3.9 <97.2 cis-1,2-Dichloroethene 70 3,260 908 879 1,400 1,690 1,770 2,300 222 1,140 1,330 163 75.6 35.5 4.4 70.3 19.9 41.6 59.0 67.9 66.8 80.1 63.0 2,020 cis-1,3-Dichloropropene 0.4 <65.0 <250 <200 <74.0 <74.0 <74.0 <52.0 <50.0 <74.0 <74.0 <2.6 <5.0 <1.2 <0.30 <1.6 <5.0 <1.5 <3.0 <1.3 <1.3 <I0.0 <3.0 <74.0 Dibromochloromethane 0.4 <105 <250 <200 <103 <103 <103 <84.0 <50.0 <103 <103 <4.2 <5.0 <1.7 <0.41 <2.6 <5.0 <2.1 <4.1 <2.1 <2.1 <10.0 <4.1 <103 Dibromomethane 70 <105 <250 <200 <115 <I15 <115 <84.0 <50.0 <I15 <I15 <4.2 <5.0 <1.8 <0.46 <2.6 <5.0 <2.3 <4.6 <2.1 <2.1 <I0.0 <4,6 <115 Dichlorodifluoromethane 1,000 <105 <250 <200 <56.5 <56.5 <56.5 <84.0 <50.0 <56.5 <56.5 <4.2 <5.0 <0.90 <0.23 <2.6 <5.0 <l.l <2.3 <2.1 <2.1 <10.0 <2.3 <56.5 Diisopropyl ether 1,500 <60.0 <250 <200 <54.5 <54.5 <54.5 <48.0 <50.0 <54.5 <54.5 <2.4 <5.0 <0.87 <0.22 <1.5 <5.0 <l.l <2.2 <1.2 <1.2 <10.0 <2.2 <54.5 Ethylbenzene 600 <150 <250 <200 <64.0 <64.0 <64.0 <120 <50.0 <64.0 <64.0 <6.0 <5.0 <1.0 <0.26 <3.8 <5.0 <1.3 <2.6 <3.0 <3.0 <10.0 <2.6 <64.0 Hexachloro-1,3-butadiene 0.4 <355 <250 <200 <110 <110 <110 <284 <50.0 <110 <110 <14.2 <5.0 <1.8 <0.44 <8.9 <5.0 <2.2 <4.4 <7.1 <7.1 1 <10.0 <4.4 <110 Methyl-tert-butyl ether 20 <105 <250 <200 <68.8 <68.8 <68.8 <84.0 <50.0 <68.8 <68.8 <4.2 <5.0 <1.1 <0.28 <2.6 <5.0 <1.4 <2.8 <2.1 <2.1 <10.0 <2.8 <68.8 Methylene Chloride 5 <485 <1250 <1000 <922 <922 <922 <388 <250 <922 <922 30.8 <25.0 <14.8 <3.7 <12.1 <25.0 <18.4 <36.9 <9.7 <9.7 <50.0 <36.9 <922 Naphthalene 6 <120 <250 <200 <88.0 <88.0 <88.0 <96.0 <50.0 <88.0 <88.0 <4.8 <5.0 <1.4 <0.35 <3.0 <5.0 <Lg <3.5 <2.4 <2.4 <10.0 <3.5 <88,0 Styrene 70 <130 1250 <200 <66.8 <66.8 <66.8 <104 <50.0 <66.8 <66.8 <5.2 <5.0 <1.1 <0.27 <3.2 <5.0 <1.3 <2.7 <2.6 <2.6 <10.0 <2.7 <66.8 Tetrachloroethene 0.7 11,400 5,110 4,060 6,870 6,880 7,380 6,370 1,150 5,720 5,030 346 91.3 200 30.5 202 25.8 71.0 124 434 444 174 159 9,960 Toluene 600 <130 <250 <200 <61.0 <61.0 <61.0 <104 <50.0 <61.0 <6L0 <5.2 <5.0 <0.98 <0.24 <3.2 <5,0 <1.2 <2.4 <2.6 <2.6 <10.0 <2.4 <61.0 trans-1,2-Dichloroethene 100 <245 132 J 143 J 187 J <63.5 <63.5 <196 32.6 J <63.5 <63.5 <9.8 <5.0 3.7 J <0.25 <6.1 <5.0 <1.3 <2.5 <4.9 <4.9 <I0.0 <2.5 <63.5 trans-1,3-Dichloropropene 0.4 <130 <250 <200 <77.2 <77.2 <77.2 <104 <50.0 <77.2 <77.2 <5.2 <5.0 <1.2 <0.31 <3.2 -5.0 <1.5 <3.1 <2.6 <2.6 <10.0 <3.1 <77.2 Trichloroethee 3 66,100 27,500 23,600 38,100 37,900 41,100 48,400 7,110 27,300 26,800 2,060 494 660 67.5 1,910 580 983 1,170 1,440 1,420 1,150 939 39,400 Trichlorofluoromethane 2,000 <100 <250 <200 <77.8 <77.8 <77.8 <80.0 <50.0 <77.8 <77.8 <4.0 <5.0 <1.2 <0.31 <2.5 <5.0 <L6 <3,1 <2.0 <2.0 <10.0 <3.1 <77.8 Vinyl acetate 88 <175 <500 <400 <362 <362 <362 <140 <100 <362 <362 <7.0 <10.0 <5.8 <1.4 <4.4 <10.0 <7.2 <14.5 <3.5 <3.5 <20.0 <14.5 <362 Vinyl chloride 0.03 <310 <250 <200 <60.5 <60.5 <60.5 <248 <50.0 <60.5 <60.5 <12.4 <5.0 <0.97 0.56 J <7.8 <5.0 <1.2 <2.4 <6.2 <6.2 <10.0 <2.4 660.5 Xylene (total) 500 <500 <250 <200 <158 <159 <158 <400 <50.0 <158 <158 <20.0 <5.0 <2.5 <0.63 <12.5 <5.0 <3.2 <6.3 <10.0 <10.0 <10.0 <6.3 <158 m&p-Xylene 500 <330 <500 <400 <102 <102 <102 <264 <100 <102 <102 <13.2 <10.0 <1.6 <0.41 <8.2 Q0.0 <2.0 <4.1 <6.6 <6.6 <20.0 <4.1 <102 o-Xylene 500 <115 <250 <200 <55.0 <55.0 <55.0 <92.0 <50.0 <55.0 <55.0 <4.6 <5.0 <0.88 <0.22 <2.9 <5.0 <l.l <2.2 <2.3 <2.3 <10.0 <2.2 <55.0 p-Isopropyltoluene 25 <155 <250 <200 <53.0 <53.0 <53.0 <124 <50.0 <53.0 <53.0 <6.2 <5.0 <0.85 <0.21 <3.9 <5.0 <].l <2.1 <3.1 <3.1 <10.0 <21 <53.0 Total VOCs Change (green =%decrease, red=%increase) 83,523 34,174 59% 29,181 65% 46,557 4q% 46,924 44% 51,188 39% 58,450 10,107 83g4 34,160 12°/, 33,369 43% 2,639 672 759,E 908 66% 124 95% 2,205 631 719,E 1,112 50% 1,536 3 1,969 1,957 I% 1,432 27% 1,179 4011., 56,729 2781% Other Parameters Persulfate (mg/L) NSL NA >70.0 >70.0 >70.0 >70.0 >70.0 NA >70.0 >70.0 >70.0 NA 2.1 >70.0 >70.0 NA 1.4 0.0 14.0 NA NA 3.0 7.0 7.0 Iron (µg/L) 300 25 U 292 7,710 66.3 44.8 J 43.1 J 154 61.5 176 128 481 10,200 227 309 577 4,200 490 302 1,620 1,760 892 399 1,430 Chloride (mg/L) 250,000 19,800 55,700 55,200 32,000 25,200 25,400 17,800 48,800 26,000 23,000 4,800 1,600 7,700 6,300 7,100 4,400 4,700 7,600 3,600 3,500 3,900 3,700 13,200 Ethene (µg/L) NSL 10.0 U 10.0 U 10.0 U 2.3 J 4.3 U 4.26 U 10.0 U 10.0 U 1.2 U 4.26 U 10.0 U 10.0 U 1.2 U 4.26 U 10.0 U 10.0 U 3.4 J 5.25 J 10.0 U 10.0 U 10.0 U 1.2 U 95.6 Sulfate (mg/L) 250,000 15,500 349,000 344,000 120,000 99,200 99,100 15,800 84,700 91,700 88,600 15,800 3,300 57,700 85,900 19,300 11,900 12,800 22,200 9,100 9,200 10,700 10,000 15,400 Total Organic Carbon (mg/L) NSL 1,500 5,600 5,800 3,200 2,100 2,000 1,200 4,400 2,500 1,700 1,200 9,200 820 J 2,400 500 U 5,600 1,600 730 J 1,000 930 J 1,100 940 J 610 J Temperature (°C) NSL 1 17.09 15.53 15.53 21.50 17.78 17.78 15.49 15.20 20.77 17.91 14.95 15.69 19.17 17.80 16.54 15.40 19.22 17.84 16.23 16.23 17.19 21.27 18.79 pH (standard) 6.5 to 8.5 6.60 5.40 5.40 6.19 6.21 6.21 6.70 5.72 6.13 6.15 6.70 5.93 6.20 6.06 7.00 7.31 6.32 5.97 6.40 6.40 6.40 6.24 7.35 Specific Conductance (µS/cm) NSL 0.261 6.733 6.733 1.340 0.753 0.753 0.244 0.901 0.112 0.724 0.194 0.080 0.841 0.939 0.249 0.153 0.144 0.299 0.126 0.126 0.128 0.167 0.408 Dissolved Oxygen (mg/L) NSL 1.00 0.18 0.18 0.00 0.00 0.00 0.75 2.68 0.00 0.00 1.62 2.89 0.10 0.97 3.29 4.67 0.00 0.00 1.38 1.38 0.21 0.81 4.03 Redox Potential (mV) NSL 9.8 359.2 359.2 289.0 323.0 323.0 -24.2 243.5 280.0 224.0 29.3 136.4 230.0 447.0 -33.1 1748.7 12.0 58.0 62.3 62.3 171.3 185.0 -14.0 Notes: 1. Concentrations shown in µg/L. 2. 2L Standard = Groundwater Standard established in Title 15A of the North Carolina Administrative Code Subchapter 2L section .0202, last amended April 1, 2013. 3. EPA TAP SL = Tap water screening level established in EPA Regional Screening Level Summary Table (TR=1E-6, HQ =1) January 2015 4. NSL = No Standard or Screening Level Listed. 5. Bold values indicate detected concentration above the laboratory reporting limit. 6. Shaded values indicate a concentration above the 2L Standard or EPA TAP SL. 7. C9-Common Laboratory Contaminant 8. 136-The relative percent difference between the sample and the sample duplicate exceeded laboratory control limits 9. MI -Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample recovery 10. UJ = Undetected; quantitation limit is imprecise 11. JH = Estimated quantitation; possibly biased high 12. Well PMW-4 was dry at the time of sampling 13. Off -site wells PMW-14A and PMW-14B are in deep woods to the west of the site and could not be found 14. Wells PMW-16A, PMW-16B, PMW-17A, and PMW-17B are in rail construction equipment storage area and were not accessible at the time of sampling. 15. Well PMW-18A outside protective casing was bent. Field sampling equipment could not be advanced beyond 5.5 feet below top of casing. Therefore, PMW-18A was not sampled. 16. NA = Not Analyzed for this compound 17. MS/MSD (09/26/12) sample collected for PMW-12B. % of 11/27/18 total VOC concentration Well ID pre -injection post -injection (Nov 2018) 1-month (Feb 2019) 6-month (July 2019) 12-month (Jan 2020) PMW-IA 1,407 1,364 3% 3,871 175% 998 29% PMW-1B 348 259 26% 162 54% 154 56% PMW-2A 1,495 1,322 12% 1,100 26% 1,347 10% PMW-2B 745 1,315 76% 840 13% 905 21% PMW-3A 23,490 8,347 64% 2,000 91% 6,141 74% PMW-4A 1,087 479 56% 816 25% 449 59% PMW-5A 97,960 63,600 35% 114,482 17% 132,210 35% PMW-6A 136,170 78,882 42% 94,726 30% 83,428 39% PMW-7A 2,591 3,262 26% 3,809 47% 3,019 17% PMW-7B 12,237 1,953 84% 8,939 27% 3,454 72% PMW-8A 696 725 4% 667 4% 619 11% PMW-8B 1,150 690 40% 679 41% 537 53% PMW-9A 700 575 18% 506 28% 581 17% PMW-9B 2,093 3,771 80% 3,640 74% 3,802 82% PMW-9C 17,623 1,305 93% 62,631 255% 74,060 320% PMW-IOA 83,523 34,174 59% 46,557 44% 46,924 44% PMW-IOB 58,450 10,107 83% 34,160 42% 33,369 43% PMW-11A 2,639 672 75% 903 66% 124 95% PMW-11B 2,205 631 71% 1,112 50% 1,536 30% PMW-13B 1,957 1,432 27% 1,179 40% 56,729 2798% Decrease Range 3% to 93% 4% to 91% 10% to 95% Decrease Average 49% 41% 45% Increase Range 4% to 80% 13% to 255% 17% to 2978% Increase Average 47% 97% 546% TABLE 3 SUMMARY OF SURFACE WATER ANALYTICAL RESULTS TREX PROPERTIES, LLC CHARLOTTE,NC Volatile Organic Compound 15A NCAC 2B SW-1 SW-1 SW-1 SW-1 SW-2 SW-2 SW-2 SW-2 SW-3 SW-3 SW-3 SW-3 Standard or Name EPA TAP SL 92409026040 92418554023 92438460023 92461009023 92409026041 92418554024 92438460024 92461009023 92409026042 92418554025 92438460025 92461009025 11/28/2018 2/20/2019 7/24/2019 1/15/2020 11/28/2018 2/20/2019 7/24/2019 1/15/2020 11/28/2018 2/20/2019 7/24/2019 1/15/2020 Pre -Injection 1-M post inject 6-M post inject 1-yr post inject Pre -Injection I-M post inject 6-M post inject 1-YR post inject Pre -Injection 1-M post inject 6-M post inject 1-YRpostinject 1,1,1,2-Tetrachloroethane 0.57 <0.33 <1.0 <0.34 <0.34 <0.33 <1.0 <0.34 <0.34 <0.33 <1.0 <0.34 <0.34 1,1,1-Trichloroethane 200 <0.48 <1.0 <0.18 <0.18 <0.48 <1.0 <0.18 <0.18 <0.48 <1.0 <0.18 <0.18 1,1,2-Trichloroethane 0.28 <0.29 <1.0 <0.24 <0.24 <0.29 <1.0 <0.24 <0.24 <0.29 <1.0 <0.24 <0.24 1, 1 -Dichloroethane 2.8 <0.32 <1.0 <0.27 <0.27 <0.32 <1.0 <0.27 <0.27 <0.32 <1.0 <0.27 <0.27 1,1-Dichloroethene 280 <0.56 <1.0 <0.24 <0.24 1.9 <1.0 <0.24 <0.24 1.6 <1.0 <0.24 <0.24 1, 1 -Dichloropropene NSL <0.49 <1.0 <0.21 <0.21 <0.49 <1.0 <0.21 <0.21 <0.49 <1.0 <0.21 <0.21 1,2,4-Trichlorobenzene 1.2 <0.35 <1.0 <0.22 <0.22 <0.35 <1.0 <0.22 <0.22 <0.35 <1.0 <0.22 <0.22 1,2-Dichlorobenzene 1.9 <0.30 <1.0 <0.29 <0.29 <0.30 <1.0 <0.29 <0.29 <0.30 <1.0 <0.29 <0.29 1,2-Dichloroethane 0.17 <0.24 <1.0 <0.34 <0.34 <0.24 <1.0 <0.34 <0.34 <0.24 <1.0 <0.34 <0.34 1,2-Dichloropropane 0.14 <0.27 <1.0 <0.19 <0.19 <0.27 <1.0 <0.19 <0.19 <0.27 <1.0 <0.19 <0.19 1,3-Dichlorobenzene NSL <0.24 <1.0 <0.22 <0.22 <0.24 <1.0 <0.22 <0.22 <0.24 <1.0 <0.22 <0.22 1,4-Dichlorobenzene 0.48 <0.33 <1.0 <0.26 <0.26 <0.33 <1.0 <0.26 <0.26 <0.33 <1.0 <0.26 <0.26 Benzene 51 <0.25 <1.0 <0.15 <0.15 <0.25 <1.0 <0.15 <0.15 <0.25 <1.0 <0.15 <0.15 Bromodichloromethane 0.13 <0.18 <1.0 <0.26 <0.26 1 1 <0.18 <1.0 <0.26 <0.26 <0.18 <1.0 <0.26 <0.26 Bromoform 4 <0.26 <1.0 <0.62 <0.62 <0.26 <1.0 <0.62 <0.62 <0.26 <1.0 <0.62 <0.62 Carbon tetrachloride 1.6 <0.25 <1.0 <0.22 <0.22 <0.25 <1.0 <0.22 <0.22 <0.25 <1.0 <0.22 <0.22 Chlorobenzene 488 <0.23 <1.0 <0.23 <0.23 <0.23 <1.0 <0.23 <0.23 <0.23 <1.0 <0.23 <0.23 Chloroform 0.22 0.24 J <5.0 <2.3 <2.3 0.30 J <5.0 <2.3 <2.3 0.24 J <5.0 <23 <2.3 Chloromethane 190 <0.11 <1.0 <0.39 <0.39 <0.11 <1.0 <0.39 <0.39 <0.11 <1.0 <0.39 <0.39 cis-1,2-Dichloroethene 36 7.5 1.9 6.5 4.7 23.9 3.6 13.9 7.6 21.0 1 3.8 10.5 5.2 Ethylbenzene 1.5 <0.30 <1.0 <0.26 <0.26 11 <0.30 1 <1.0 <0.26 <0.26 <0.30 <1.0 <0.26 <0.26 Methyl-tert-butyl ether 14 <0.21 <1.0 <0.28 <0.28 <0.21 <1.0 <0.28 <0.28 <0.21 <1.0 <0.28 <0.28 Methylene Chloride 11 <0.97 <5.0 <3.7 <3.7 <0.97 <5.0 <3.7 <3.7 <0.97 <5.0 <3.7 <3.7 Naphthalene 0.17 <0.24 <1.0 <0.35 <0.35 <0.24 <1.0 <0.35 <0.35 <0.24 <1.0 <0.35 <0.35 Tetrachloroethene 3.3 0.9 J <1.0 <0.16 <0.16 28.1 7.1 11.6 12.1 20.2 7.5 7.9 8.2 Toluene 11 <0.26 <1.0 <0.24 0.26 J <0.26 <1.0 <0.24 <0.24 <0.26 <1.0 <0.24 <0.24 trans-1,2-Dichloroethene 360 <0.49 <1.0 <0.25 <0.25 <0.49 <1.0 <0.25 <0.25 <0.49 <1.0 <0.25 <0.25 Trichloroethene 30 72.2 14.3 28.2 26.4 145 29 48.9 55.4 114 25 35.2 35.3 Trichlorofluoromethane 5,200 <0.20 <1.0 <0.31 <0.31 <0.20 <1.0 <0.31 <0.31 <0.20 <1.0 <0.31 <0.31 Vinyl chloride 2.4 <0.62 <1.0 <0.24 <0.24 <0.62 <1.0 0.93 J <0.24 <0.62 <1.0 0.61 J <0.24 m&p-Xylene 190 <0.66 <2.0 <0.41 <0.41 <0.66 <2.0 <0.41 <0.41 <0.66 <2.0 <0.41 <0.41 o-Xylene 1 190 <0.23 <1.0 <0.22 <0.22 <0.23 <1.0 <0.22 <0.22 <0.23 <1.0 <0.22 <0.22 p-Isopropyto uene I NSL 1 < < <0.21 <0.21 <0.31 <1.0 <0.21 <0.21 <0.31 <1.0 <0.21 <0.21 Total VOCs Change (green =%decrease, red %increase) 81 31 62% 35 57% 31 61% 199 54 73% 75 62% 75 62% 157 57 63% 54 65% 49 69% Other Parameters Persulfate (mg/L) NA 6.0 0.0 0.0 NA 5.6 0.0 0.0 NA 3.5 0.0 0.0 Temperature (°C) NA 7.46 26.08 16.30 NA 7.56 27.09 16.33 NA 7.55 26.94 16.19 pH (standard) NA 6.63 6.86 6.40 NA 6.80 7.01 6.23 NA 7.08 7.11 6.37 Specific Conductance (µS/cm) NA 0.091 0.185 0.208 NA 0.095 0.189 0.212 NA 0.093 0.183 0.212 Disolved Oxygem (mg/L) NA 178.70 6.70 7.35 NA 12.21 6.07 7.66 NA 12.36 6.32 8.12 Redox Potential (mV) I I NA 178.7 51.0 166.0 NA 169.4 41.0 185.0 NA 163.2 16.0 210.0 Notes: 1. Concentrations shown in µg/L. 2. 2L Standard = Groundwater Standard established in Title 15A of the North Carolina Administrative Code Subchapter 2L section .0202, last amended April 1, 2013. 3. EPA TAP SL = Tap water screening level established in EPA Regional Screening Level Summary Table (TR=1E-6, HQ =1) January 2015 4. NSL = No Standard or Screening Level Listed. 5. Bold values indicate detected concentration above the laboratory reporting limit. 6. Shaded values indicate a concentration above the 2L Standard or EPA TAP SL. 7. NA = Not Analyzed for this compound 1/1 EnviroAnafytics Group APPENDICES EnvirQAnafytics Group APPENDIX A INJECTION EVENT RECORDS AND PHOTO DOCUMENTATION North Carolina Department of Environmental Quality — Division of Water Resources INJECTION EVENT RECORD (IER) Permit Number WI0300345 1. Permit Information Trex Properties Permittee Trex-Charlotte Facility Name 3114 Cullman Ave. Charlotte, NC. Mecklenburg Co. Facility Address (include County) 2. Injection Contractor Information Innovative Environmental Tech. Inc. Injection Contractor / Company Name Street Address: 6071 Easton rd. Pipersville, PA 18947 City State Zip Code (888)721-8283 Area code — Phone number 3. Well Information Number of wells used for injection 19 Well IDs: IW-1 through IW-20 Were any new wells installed during this injection event? ❑ Yes X No (7 addtnl temp. dpt.) If yes, please provide the following information: Number of Monitoring Wells Number of Injection Wells. Type of Well Installed (Check applicable type): ❑ Bored ❑ Drilled ❑ Direct -Push ❑ Hand -Augured ❑ Other (specify) Please include a copy of the GW-1 form for each well installed. Were any wells abandoned during this injection event? ❑ Yes X No If yes, please provide the following information: Number of Monitoring Wells Number of Injection Wells. Please include a copy of the GW-30 for each well abandoned. 4. Injectant Information Sodium Persulfate, Ferric Oxide Powder, Water Injectant(s) Type (can use separate additional sheets if necessary Concentration 25-30% NPS, 2-5% Fe0 If the injectant is diluted please indicate the source dilution fluid: City of Charlotte Fire Hydrant Total Volume Injected (gal) 69,536 Volume Injected per well (gal) 1,400-10,232 5. Injection History Injection date(s): 1/7-1/17/2019 Injection number (e.g. 3 of 5):1 of 1 Is this the last injection at this site? X Yes ❑ No I DO HEREBY CERTIFY THAT ALL THE INFORMATION ON THIS FORM IS CORRECT TO THE BEST OF MY KNOWLEDGE AND THAT THE INJECTION WAS PERFORMED WITHIN THE STANDARDS LAID OUT IN THE PERMIT. _ 1/24/2019 SIGNATURE OF INJECTION CONTRACTOR DATE Ian H. Connor Submit the original of this form to the Division of Water Resources within 30 days of injection. Form UIC-IER Attn: UIC Program, 1636 Mail Service Center, Raleigh, NC 27699-1636, Phone No. 919-807-6464 Rev. 3-1-2016 IPFmwjT Innovative Environmental U&nologies, Inc. Technology Discussion and Field Report To Trex Properties For The Application Of "Ferric Oxide activated Persulfate" At 3114 Cullman Ave. Charlotte, NC NCDEQ UIC Permit #-WI0300345 January 2019 Innovative Environmental Technologies, Inc. 6071 Easton Road Pipersville, PA 18947 (888) 721-8283 www.iet-inc.net Pipersville, PA . Columbus, OH . Concord, NC QET Contents ExecutiveSummary.................................................................................................................................. 2 Introduction............................................................................................................................................... 2 Remediation Implementation................................................................................................................ 2 InjectionProcedures............................................................................................................................2 Direct -Push -Driven Perforated Rod Placement.............................................................................. 3 Subsurface Pathway Development.................................................................................................... 3 Provect-OX Injection............................................................................................................................ 3 LiquidRinse........................................................................................................................................... 3 PostInjection Line Purge..................................................................................................................... 3 SiteMap.......................................................................................................................................................4 Conclusion.................................................................................................................................................. 5 AppendixA - Injection Logs.................................................................................................................... 5 1 1 P a g e Trex Properties - Cullman Ave. QET Executive Summary On behalf of Trex Properties, Innovative Environmental Technologies, Inc. (IET) has prepared the following injection report. This report has been prepared to document remediation activities conducted at the site. The injection program was implemented from January 7t" to 17t" 2019. The remedial approach employed the oxidation remediation product "Ferric Oxide activated Persulfate". This product pairs a self -activating oxidation persulfate chemistry while providing the appropriate components for a longer lasting biological attenuation process following the initial oxidation event. The materials introduced across 19 of 20 injection wells included 158,858 pounds of sodium persulfate, 13,826 pounds of ferric oxide powder in approximately 69,536 gallons of solution. Although several attempts were made IW-16 was not installed due to obstacles encountered prior to reaching the desired depth. Surfacing of remedial material was encountered during the implementation of the design at several of the Injection Wells; namely (IW-1, IW-2, IW-3, IW-6, IW-7, IW-10, IW-11 and IW-13). Ultimately full dosages were applied to IW-3, IW-6 and IW-7 using decreased flow and pressure and revisiting the location multiple times. IW-1 and IW-2 were not completed in full, but 7 direct push locations were installed in the area around these two locations in order to distribute the material via injection. IW-10, IW-11 and IW-13 did not receive a full dosage but IW-12 received the materials left over from these wells. IW-12 is immediately upgradient of the uninstalled IW-16 location and 10, 11 and 13 were not accepting any more volume without excessive daylighting occurring in and along the road (Cullman Ave). IW-12 shares a screened interval with IW-13 so the extra material was added there. The point by point dosages along with instances of surfacing and other field notes are noted in the attached field logs. Introduction The Cullman Ave site located in Charlotte, NC, was identified as having soils and groundwater impacted by the historical release of chlorinated hydrocarbons. An injection program was conducted by IET for the remediation of CVOC impacts in both soil and groundwater throughout the designated areas utilizing advanced oxidation technologies. Remediation Implementation Injection Procedures IET injected a total of injection wells and 7 direct push locations at the Cullman Ave. site. Details regarding each injection attempt are provided in the field logs in the Appendix. 2 1 P a g e Trex Properties — Cullman Ave. GET Direct -Push -Driven Perforated Rod Placement A Powerprobe 9500 unit comparable to the one pictured in Figure 1, was utilized to drive the injection screen (as seen in Figure 2) to depths ranging from 5 to 27 feet below ground surface (bgs). It is at these depths, that the likelihood exists of being in close proximity to the targeted waters in the more permeable layers that were identified during FIGURE 1: AMS POWER PROBE 9500 VTR characterization of the site. These more permeable layers are those believed to have historically provided the preferential pathways taken by the dissolved -phase CVOCs. Subsurface Pathway Development Compressed air was used to propel all injectants into the subsurface. Compressed air was first injected into the subsurface at approximately 150 pounds per square inch (psi) until a significant pressure drop was observed at the injection pressure vessel. This process is referred to as pathway development. The intent of this step is to open pathways in the subsurface for FIGURE 2: RETRACTABLE INJECTION SCREEN the injectants to follow. These pathways are believed to be those more permeable pathways along which VOCs are more likely to have migrated, both in the vadose and saturated zones. Liquid and liquid -entrained injectants are then delivered with pressurized gas to the pathways that were produced during the development step. Liquid Injection A predetermined volume of the sodium persulfate and ferric oxide material was immediately injected into the subsurface fractures and voids that were developed during the compressed air injection step. Liquid Rinse A small amount of water was injected to clear the injection lines and sand packs of the injectant. Post Injection Line Purge Compressed air was injected to clear the lines of all material and to force the remedial components further into the formation before moving to the next injection location. 3 1 P a g e Trex Properties — Cullman Ave. �T Site Map A +w— ■ _ IW-15 -4i5 _ P —7 W - .20) PWW-21 PY11V-2SA a ' 1 oo,00a PMM1 *p 76 . rt yaH ■ . SOURCE AREAFOR AZ" - -� COO NTTAMINATION - _ 3A7 pWw 2A ' MW 06 !2° Pam- ❑PT Lacatiarr� FIGURE 3: GENERAL INJECTION IMPLEMENTATION — INJECTION LOCATIONS 4 1 P a g e Trex Properties — Cullman Ave. �T Conclusion The injection program at the Cullman Ave. site was implemented based on the proposed design with slight field modifications. All proposed injectants were introduced at the targeted depths. It is expected that the injection event will yield positive results and IET looks forward the assessing the data following future sampling events. Appendix A - Injection Logs 5 1 P a g e Trex Properties — Cullman Ave. ITT 12 AIL TECHNJOLO.EiIES, LNC.. Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/10, 1/12/2019 Time of Injection: to Well ID IW-1 Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 6-26' 6-26' Duration of Fracture (seconds): 20 Pressure of Pre -injection pathway development 75 Estimated Radius of Influence 12.5 Pounds of Sodium Persulfate 8363 8363 Pounds of Ferric Oxide 725 725 Gallons of Solution 3658 3658 Pressure of Post -injection pathway dev. 50 Odors: Field Observations: Well was attempted 1/10 daylighting immediately from around well casing with bentonite and re -attempted 1/12 daylighting immediatle utilized in place of this infection well. to seal ton of Direct hush iniection points ITT 12 AIL TECHNJOLO.EiIES, LNC.. Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/10,1/12/2019 Well ID IW-2 Time of Injection: 14:16 to 17:45 Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 6-26' 6-26' 6-26' 6-26' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 3200 8363 3200 8363 Pounds of Ferric Oxide 277 725 277 725 Gallons of Solution 1400 3658 1400 3658 Pressure of Post -injection pathway dev. 50 50 Odors: Field Observations: Daylighting occurred from mulitiple locations after 1000 gallons injected 1/10, well was revisited 1 /12 and 400 Gallons was iniected before davli6tin2 occurred. DPT locations were installed in order to apply the remaining iniectate. ITT ATIVE ENVIRONMENTAL TECHNOLDERES, M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date/Time of Injection: 1/8/2019 1/10/2019 1/11/2019 1/12/2019 1/15/2019 10:38 9:30 12:30 8:45 8:46 WellID IW-3 to to to to to 12:30 13:00 16:45 11:42 9:11 Odors: Field Observations: Daylighting occurred from the edge of the building, well was revisited multiple times in order to apply full volume Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 11-31' 11-31' 11-31' 11-31' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 ITT ATIVE ENVIRONMENTAL TECHNOLDER , M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date/Time of Injection: 1/7/2019 1/8/2019 15:02 8:50 Well ID IW-4 to to 16:48 10:34 Odors: Field Observations: Summary Injection Point Summary Actual Proposed Proposed Proposed Well Screen 18-38' 19-39' 18-38' 19-39' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 ITT 12 Job Name: Date of Injection: AIL TECHNJOLO.EiIES, LNC.. Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate 1/7/2019 Well ID IW-5 Time of Injection: 10:13 to 14:49 Summary Injection Point Summary Proposed Proposed Actual Proposed Well Screen 18-38' 19-39' 18-38' 19-39' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 Odors: Field Observations: Slight surface escape. 15' northeast of well. let pressure dissipate at 12:30. finished iniection at 14:00 ITT 12 AIL TECHNJOLO.EiIES, LNC.. Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date/Time of Injection: 1/9/2019 1/10/2019 1/11/2019 12:26 8:51 9:54 Well ID IW-6 Sum] Injection Point Summary Actual Proposed Actual Well Screen 18-38' 19-39' 18-38' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 Gallons of Solution 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 Odors: Field Observations: to to to 16:42 9:20 12:30 occurred 20' west of well. revisited well twice in order to finish under decreased pressure (20 ITT 12 1L TECHNJOLO.EiIES, LNC.. Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Well ID IW-7 Date/Time of Injection: 1/10/2019 1/11/2019 1/12/2019 1/15/2019 14:45 13:05 9:07 9:18 to to to to 16:15 14:45 11:05 11:10 Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 18.5-38.5' 19-39' 18.5-38.5' 19-39' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 Odors: Field Observations: Davli6tin2 occurred 1/10 15' east of infection i well was revisited 3 times to complete under decreased ITT ATIVE ENVIRONMENTAL TECHNOLDER , M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/8/2019 Time of Injection: 12:45 to Well ID IW-8 16:04 Odors: Field Observations: Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 27-47' 27-47' 27-47' 27-47' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 ITT ATIVE ENVIRONMENTAL TECHNOLDER , M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/9/2019 Time of Injection: 8:53 to Well ID IW-9 12:04 Odors: Field Observations: Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 31-51' 31-51' 31-51' 31-51' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 ITT 12 Job Name: Well ID AIL TECHNJOLO.EiIES, LNC.. Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate IW-10 Date/Time of Injection: 1/10/2019 1/11/2019 1/16/2019 15:29 9:10 8:18 to to to 16:30 10:13 8:36 Summary Injection Point Summary Proposed Proposed Actual Proposed Well Screen 31-51' 31-51' 31-51' 31-51' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 3657 8363 3657 8363 Pounds of Ferric Oxide 317 725 317 725 Gallons of Solution 1600 3658 1600 3658 Pressure of Post -injection pathway dev. 50 50 Odors: Field Observations: Davli6tin2 occurred 20' south of IW-10 on 1/10. well was revisited twice under decreased pressure (20 occurred both times ITT 12 AIL TECHNJOLO.EiIES, LNC.. Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Well ID IW-11 Date/Time of Injection: 1/11/2019 1/15/2019 1/16/2019 9:50 12:00 40:29 to to to 11,00 14:45 11:22 Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 31-51' 31-51' 31-51' 31-51' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 4516 8363 4516 8363 Pounds of Ferric Oxide 396 725 396 725 Gallons of Solution 2000 3658 2000 3658 Pressure of Post -injection pathway dev. 50 50 Odors: Field Observations: Daylighting occurred 1/11 after 400 under reduced pressure (20 psi). daN injected, 25' northeast of injection well, well was revisited twice continued from same area. 1600 additional eallons iniected. ITT ATIVE ENVIRONMENTAL TECHNOLDER , I-IVC., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Time of Injection: 1/7/2019 1/15/2019 1/16/2019 11:20 14:55 8:38 WellID IW-12 to to to 17:00 16:47 15:30 Odors: Field Observations: Left over materials from IW-10, IW-11 and IW-13 were added here due to screened interval being common w' IW-13 and upgradient proximity to uninstalled IW-16 Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 44-64' 44-64' 44-64' 44-64' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 23392 8363 23392 8363 Pounds of Ferric Oxide 2028 725 2028 725 Gallons of Solution 10,232 3658 10232 3658 Pressure of Post -injection pathway dev. 50 50 ITT 12 AIL TECHNJOLO.EiIES, LNC.. Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Well ID IW-13 Date/Time of Injection: 1/7/2019 1/12/2019 1/16/2019 10:30 16:00 12:20 to to to 11:00 17:20 12:45 Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 44-64' 44-64' 44-64' 44-64' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 1829 8363 1829 8363 Pounds of Ferric Oxide 158 725 158 725 Gallons of Solution 800 3658 800 3658 Pressure of Post -injection pathway dev. 50 50 Odors: Field Observations: Daylighting occurred 1/7 from previously abandoned casing 3' north of well, old casing was over drilled and grouted from 0-20' on 1/9/2019, grout was allowed to set and well was revisited twice under reduced pressure (20 psi), davli,2htin2 occurred 10' east of well both times ITT ATIVE ENVIRONMENTAL TECHNOLDER , M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date/Time of Injection: 11:31 8:32 Well ID IW-14 to to 16:57 11:09 Odors: Field Observations: Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 52-72' 53-73' 52-72' 53-73' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 ITT ATIVE ENVIRONMENTAL TECHNOLDER , M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/12/2019 Time of Injection: 11:17 to Well ID IW-15 15:07 Odors: Field Observations: Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 53-73' 53-73' 53-73' 53-73' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 ITT 12 AIL TECHNJOLO.EiIES, LNC.. Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: Time of Injection: to Well ID IW-16 Summary Injection Point Summary Actual Actual Well Screen Duration of Fracture (seconds): Pressure of Pre -injection pathway development Estimated Radius of Influence Pounds of Sodium Persulfate Pounds of Ferric Oxide Gallons of Solution Pressure of Post -injection pathway dev. Odors: Field Observations: Well not installed ITT ATIVE ENVIRONMENTAL TECHNOLDERES, M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Date/Time of Injection: 1/9/2019 1/10/2019 11:30 8:35 Well ID IW-17 to to 16:37 11:22 Odors: Field Observations: Slight surface escapes observed around well, stopped for night and finished 1/10. Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 53-73' 53-73' 53-73' 53-73' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 ITT ATIVE ENVIRONMENTAL TECHNOLDER , M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Time of Injection: 1/7/2019 1/8/2019 15:30 8:56 Well ID IW-18 to to 17:03 10:50 Odors: Field Observations: Summary Injection Point Summary Actual Proposed Actual Proposed Well Screen 53-73' 53-73' 53-73' 53-73' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 ITT 12 Job Name: Date of Injection: AIL TECHNJOLO.EiIES, LNC.. Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate 1/10/2019 Well ID IW-19 Time of Injection: 11:32 to 15:18 Summary Injection Point Summary Actual Proposed Proposed Proposed Well Screen 53-73' 53-73' 53-73' 53-73' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 Odors: Field Observations: Influence observed at PMW-10A and PMW-10B. replaced J plugs and continued ITT ATIVE ENVIRONMENTAL TECHNOLDERES, M., Job Name: Trex - Cullman Ave. - Charlotte, NC 2019 Injections Permanent Well Application of Ferric Oxide Activated Persulfate Time of Injection: 1/8/2019 1/9/2019 10:57 8:18 Well ID IW-20 to to 17:23 11:10 Odors: Field Observations: Slight surface escapes observed around well, stopped for night and finished 1/9 Summary Injection Point Summary Actual Proposed Proposed Proposed Well Screen 53-73' 53-73' 53-73' 53-73' Duration of Fracture (seconds): 20 20 Pressure of Pre -injection pathway development 75 75 Estimated Radius of Influence 12.5 12.5 Pounds of Sodium Persulfate 8363 8363 8363 8363 Pounds of Ferric Oxide 725 725 725 725 Gallons of Solution 3658 3658 3658 3658 Pressure of Post -injection pathway dev. 50 50 IET L i INNOVATIVE ENVIRONMENTAL TECHNOLOGIES, INC Job Name: Trex - Cullman Ave. - Charlotte, NC Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/17/2019 Well ID DPT-1 2019 Injections Time of Injection: 9:56 to 11:37 Summary Injection Point Summary Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Injection Interval (ft.bgs.) 8-10' 10-12' 12-14' 16-18' 19-21' 8-21' Duration of Fracture (seconds): 3 3 3 3 3 Pressure of Pre -injection pathway developmeni 150 150 150 150 150 Estimated Radius of Influence 12.5 12.5 12.5 12.5 12.5 Pounds of Sodium Persulfate 387 387 387 387 387 1935 Pounds of Ferric Oxide 35 35 35 35 35 175 Gallons of Solution 170 170 170 170 170 850 Pressure of Post -injection pathway dev. 50 50 50 50 50 Odors: Field Observations: DPT refusal @ 22', location installed —10' west of IW-1 ET L I INNOVATIVE ENVIRONMENTA L. TECHNOLOGIES, INC.. Job Name: Trex - Cullman Ave. - Charlotte, NC Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/17/2019 Well ID DPT-2 2019 Injections Time of Injection: 11:46 to 13:22 Summary Injection Point Summary Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Injection Interval (ft.bgs.) 8-10' 10-12' 12-14' 16-18' 18-20' 8-20' Duration of Fracture (seconds): 3 3 3 3 3 Pressure of Pre -injection pathway developmeni 150 150 150 150 150 Estimated Radius of Influence 12.5 12.5 12.5 12.5 12.5 Pounds of Sodium Persulfate 387 387 387 387 387 1935 Pounds of Ferric Oxide 35 35 35 35 35 175 Gallons of Solution 170 170 170 170 170 850 Pressure of Post -injection pathway dev. 50 50 50 50 50 Odors: Field Observations: DPT refusal @ 22', location installed —10' southwest of IW-1 ET L I INNOVATIVE ENVIRONMENTAL TECHNOLOGIES, INC.. Job Name: Trex - Cullman Ave. - Charlotte, NC Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/14/2019 Well ID DPT-3 2019 Injections Time of Injection: 16:55 to 18:45 Summary Injection Point Summary Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Injection Interval (ft.bgs.) 8-10, 10-12' 12-14' 14-16' 16-18' 8-18' Duration of Fracture (seconds): 3 3 3 3 3 Pressure of Pre -injection pathway developmeni 150 150 150 150 150 Estimated Radius of Influence 12.5 12.5 12.5 12.5 12.5 Pounds of Sodium Persulfate 387 387 387 387 387 1935 Pounds of Ferric Oxide 35 35 35 35 35 175 Gallons of Solution 170 170 170 170 170 850 Pressure of Post -injection pathway dev. 50 50 50 50 50 Odors: Field Observations: DPT refusal @ 19', location installed —15' east of IW-1 ET L I INNOVATIVE ENVIRONMENTAL TECHNOLOGIES, INC.. Job Name: Trex - Cullman Ave. - Charlotte, NC Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/14/2019 Well ID DPT-4 2019 Injections Time of Injection: 16:00 to 16:55 Summary Injection Point Summary Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Injection Interval (ft.bgs.) 5-7' 8-10, 11-13' 14-16' 17-19' 5-19' Duration of Fracture (seconds): 3 3 3 3 3 Pressure of Pre -injection pathway developmeni 150 150 150 150 150 Estimated Radius of Influence 12.5 12.5 12.5 12.5 12.5 Pounds of Sodium Persulfate 387 387 387 387 387 1935 Pounds of Ferric Oxide 35 35 35 35 35 175 Gallons of Solution 170 170 170 170 170 850 Pressure of Post -injection pathway dev. 50 50 50 50 50 Odors: Field Observations: DPT refusal @ 20', location installed —15' southeast of IW-1 ET L I INNOVATIVE ENVIRONMENTAL TECHNOLOGIES, INC.. Job Name: Trex - Cullman Ave. - Charlotte, NC Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/14/2019 Well ID DPT-5 2019 Injections Time of Injection: 13:50 to 15:05 Summary Injection Point Summary Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Injection Interval (ft.bgs.) 5-7' 8-10, 11-13' 14-16' 17-19' 5-19' Duration of Fracture (seconds): 3 3 3 3 3 Pressure of Pre -injection pathway developmeni 150 150 150 150 150 Estimated Radius of Influence 12.5 12.5 12.5 12.5 12.5 Pounds of Sodium Persulfate 387 387 387 387 387 1935 Pounds of Ferric Oxide 35 35 35 35 35 175 Gallons of Solution 170 170 170 170 170 850 Pressure of Post -injection pathway dev. 50 50 50 50 50 Odors: Field Observations: DPT refusal @ 20', location installed —15' west of IW-2 ET L I INNOVATIVE ENVIRONMENTAL TECHNOLOGIES, INC.. Job Name: Trex - Cullman Ave. - Charlotte, NC Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/14/2019 Well ID DPT-6 2019 Injections Time of Injection: 12:01 to 13:36 Summary Injection Point Summary Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Injection Interval (ft.bgs.) 14-16' 16-18' 18-20' 20-22' 22-24' 14-24' Duration of Fracture (seconds): 3 3 3 3 3 Pressure of Pre -injection pathway developmeni 150 150 150 150 150 Estimated Radius of Influence 12.5 12.5 12.5 12.5 12.5 Pounds of Sodium Persulfate 387 387 387 387 387 1935 Pounds of Ferric Oxide 35 35 35 35 35 175 Gallons of Solution 170 170 170 170 170 850 Pressure of Post -injection pathway dev. 50 50 50 50 50 Odors: Field Observations: DPT refusal @ 25', location installed —15' southwest of IW-2 ET L I INNOVATIVE ENVIRONMENTAL TECHNOLOGIES, INC.. Job Name: Trex - Cullman Ave. - Charlotte, NC Permanent Well Application of Ferric Oxide Activated Persulfate Date of Injection: 1/14/2019 Well ID DPT-7 2019 Injections Time of Injection: 9:47 to 11:58 Summary Injection Point Summary Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Actual Proposed Injection Interval (ft.bgs.) 17-19' 19-21' 21-23' 23-25' 25-27' 17-27' Duration of Fracture (seconds): 3 3 3 3 3 Pressure of Pre -injection pathway developmeni 150 150 150 150 150 Estimated Radius of Influence 12.5 12.5 12.5 12.5 12.5 Pounds of Sodium Persulfate 387 387 387 387 387 1935 Pounds of Ferric Oxide 35 35 35 35 35 175 Gallons of Solution 170 170 170 170 170 850 Pressure of Post -injection pathway dev. 50 50 50 50 50 Odors: Field Observations: DPT refusal @ 25', location installed —15' southwest of IW-2 ti 1 IE, INNOVATIVE ENVIRONMENTAL TECHNOLOGIES, INC. Job Name: Trex-Cullman Ave. 2019 Injections In -Situ Chemical Oxidation using Ferric Oxide activated Persulfate Date of Injections: 1/7-1/17/2019 Injection Summary Injection Summary Injection Point Summary Actual Proposed Pounds of Sodium Persulfate 158858 158900 Pounds of Ferric Oxide 13826 13780 Gallons of Solution 69536 69500 January 9, 2019 WR Project No. 03130430.12 Activated Persulfate Injection Observations Trex Properties, LLC 3114 & 3124 Cullman Ave, Charlotte NC IET-INC,NET 888.721.8283 Photo #1: Innovative Environmental Technologies (IET) injection trailer rig set up in front of 3114 Cullman Avenue. Each of the 20 injection locations is to receive ^3,700 gallons of activated persulfate solution, in about 17-200 gallon batches. Nine 55 pounds of Klozur persulfate and one 50 pound bag of ferric oxide are mixed with municipal water to create each 200 gallon batch. Each pallet holds 40 bags of either persulfate (white bags) or ferric iron (red bags). Photo #2: Mixing room (left) and injection control room (right). Each empty pallet on left represents 2,200 pounds of persulfate mixed and injected since injection work started on January 7, 2019. Page 1 of 6 Activated Persulfate Injection Observations January 9, 2019 Trex Properties, LLC 3114 & 3124 Cullman Ave, Charlotte NC WR Project No. 03130430.12 Photo #3: Storage of persulfate and ferric iron in 3124 Cullman Ave. As of January 9, 2019 there were 41 pallets of persulfate (1,640 bags) and two pallets of ferric iron (80 bags) stored within the building. Photo #4: Connection to municipal water supply equipped with flow totalizer. Water hose leading towards top of photo is connected to injection trailer in front of 3114 Cullman Avenue. Hose leading towards bottom of photo is connected to a second injection trailer on the north side of Cullman Avenue. Page 2 of 6 Activated Persulfate Injection Observations January 9, 2019 Trex Properties, LLC 3114 & 3124 Cullman Ave, Charlotte NC WR Project No. 03130430.12 Photo #5: Water hose protector leading across Cullman Avenue to second injection trailer. �a Photo 6: Mixing tank and injection pump and related equipment in injection trailer. Page 3 of 6 Activated Persulfate Injection Observations January 9, 2019 Trex Properties, LLC 3114 & 3124 Cullman Ave, Charlotte NC WR Project No. 03130430.12 Photo #7: Injection hose connection into IW-17 on north side of Cullman Avenue. Photo #8: Injection hose connection into IW-9 on south side of Cullman Avenue. Page 4 of 6 Activated Persulfate Injection Observations January 9, 2019 Trex Properties, LLC 3114 & 3124 Cullman Ave, Charlotte NC WR Project No. 03130430.12 Photo #9: Flags marking location of surface water sampling point SW-2. A sample of the surface water from Little Sugar Creek was field tested for the presence of persulfate during the January 9, 2019 site visit. Photo #10: Colorimetric field test kit used to check for the presence of sodium persulfate in surface water. Page 5 of 6 Activated Persulfate Injection Observations January 9, 2019 Trex Properties, LLC 3114 & 3124 Cullman Ave, Charlotte NC WR Project No. 03130430.12 Fr tedium persu4fate, pp}h2 49 56 STORE 1K l+x+s+tl THE DARK CAS• NC) C-7870 Photo #11: Sample of Little Sugar Creek surface water mixed with indicator chemical within testing ampoule. No color change was observed indicating the absence of sodium persulfate in the surface water. �1�� 4L } + t Photo #12: East looking view of sodium persulfate field test ampoule with Little Sugar Creek in the background. Page 6 of 6 S i6 EnviroAnafytics Group APPENDIX B GROUNDWATER AND SURFACE WATER SAMPLING FORMS Monitoring Well Gauging Form Trex Properties • Charlotte, NC Well ID Zone Screened Screened Interval k b Well Diameter In Sample Parameters Total Depth h b Depth to Water k BT Measured Total Depth ft BTOC Time ate PMW-1A Saprolite 7-12 2 VOCs+MNAs 12 5, oT 1 6. 15 r 5 23 13 PMW1B PWR 49-54 2 VOCs+MNAs 54 � �,q� t 5-j,51 1525 13 PMW-2A Saprolite 20-30 2 VOCs + MNAs 30 Z t 3 -1, K 2t 1511 ( 3 PMW-2B PWR SO -SS 2 VOCs+MNAs 55 rj,g7�t 54,3ot )51S i r3 PMW-3A Saprolite 15-25 2 VOCs+MNAs 25 6,o i Zq,38t 1r.20 t f3 PMW-4A Saprolite 2-12 2 VOCS +MNAs 12 9,09l 15.10, ISIO I )3 PMW-5A PWR 29.39 2 VOCs+MNAs 39 1.96' 59.81, )50-] � )3 PMW6A PWR 28-38 2 VOCs+MNAs 38 q.-Iq 39 Sot 1505 11)3 PMW-7A PWR 28-38 2 VOCS +MNAs 38 6,91, 31,`♦�� 1455' 1 )3 PMW-7B PWR 50.55 2 VOCs+MNAs 55 -1. OW 5q.95i 1500 ) 13 PMW-8A PWR 32-42 2 VOCs+MNAs 42 8, SJ t q' Z 5 I I 12 5 ) 13 PMW-88 PWR 53-58 2 VOCs+MNAs 58 t 1, q 0' 1 L13 Q 1 3 PMW-9A Saprolite 9-19 2 VOCS+ MNAs 19 '� t77 19 , 1 p r + q S5 1 ) 3 PMW-9B Saprolite 24.34 2 VOCs+MNAs 34 �,9rj` 33,g51 19;?- 113 PMW-9C PWR 45.50 2 VOCs+MNAs 50 1, 9$ I 400. a2t I q So 1 r3 PMW-10A PWR 53-63 2 VOCs+MNAs 63 G. 2-11 6 3, 55 t 1 � y 5 ,) 3 PMW-108 PWR 68-73 2 VOCs+MNAs 73 6,381 �3.051 1KW1 /13 PMW-11A PWR 53.63 2 VOCs+MNAs 63 6,Li3`1�315 ti 13 PMW-118 PWR 73-79 2 VOCs+MNAs 78 to 6 r 8, rjZ 3; PMW-12A PWR 30-40 2 VOCS 40 ---- PMW-128 PWR 44.49 2 VOCS 49 ---- PMW-136 Bedrock 98.103 2 VOCs+WAS 103 `I'O"gt 103.Dt 1 r PMW-14A Saprolite 20-30 2 VOC$ 30 PMW-14B PWR 45-50 2 VOCS 50 ---- PMW-16A PWR 12-22 2 VOCS 22 -- PMW-16B PWR 50-55 2 VOCS 55 ---- PMW-17A PWR 12-22 2 VOCS 22 -- PMW-17B PWR 45.50 2 VOCS 50 - PMW-18A Saprolite 12.22 2 VOCS 22 -- PMW-18B PWR 38-43 2 VOCS 43 ---- PMW-20A Saprolite 34-39 2 VOCS 39 - PMW-208 Rock 55.60 2 VOCs 60 ---- PMW-21A Saprolite 30-35 2 VOCs 35 -- PMW-218 PWR 62.67 2 VOCS 67 ---- PMW-22A Saprolite 58.63 2 VOCS 63 -- PMW-22B PWR 81-86 j 2 j VOCs 86 ---- Notes: k - feet bgs - below ground surface in = inches BTOC - below top of casing PWR = Partially weathered rack MNA analytes = Persulfate, TOC, sulfate, iron, chloride, and ethenes r■ ither aver �� Our People, Your Success Page 1 of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-1A Site Name Trex Properties, Charlotte NC Date 1 / S zo a,, Well Depth I Depth to Water 5, ;'� Well Diameter 2" Casing Material PVC Screen Length 5' Well Water Volume Sampling Crew K d M. rf. Pump Type Peristaltic Tubing Type 114" Poly LDPE Intake set at ov $ Weather Conditions Ow to c s+ 1 b ° F Notes (eg. odor or color) �0 a 4•'t& 6 4 nao r V It: 61y Clse.r Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m /L Temp °C(PS/cm) EC pH standard ORP m Turbidity NTU 22 5. D.l2 4 19 cf. 1.I7- $ qq Sys 4 IW25 5.8s, 1. tis , 2. 7 Ig 2$ 5.%, 0.3 0 .1Z 7 Iq3l 6.4 o 19-111 1.15o 1,76 Z7 1 3 �,al` O r $ 0,q ,a 1,2.0 6,01 4z Zfb I►I3-1 0,2Z 18.14 1, t3 5.64 161 Iq3 1448 %3' a 17 r18,91 1.25 Z 14 z Z3 1443 51213, O' 8 6,66 1q.06 I,26 .bq -1 7-23 t 5. %V ),9 o.e)q 19.091.74 . 6G 131 ZI y i .0 0.00 1 Iq, 5 I'ti S.58 1 - v3 00 Other Parameters Sampled at I Svc, Parameter. Samples delivered to 4 C-10, by Y_ Q , at o 4 -� Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass :1 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic I 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other YID. 96,3 Prem v+� ttd a rcd 51; kit WEAL ProjectslTrex Properties LLC - DETREX - TlCharlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)1Field FormslWR Groundwater Sampling Form for Trex Properties -All 8 9 40 Our People, Your Success Page 1 of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-1B Site Name Trex Properties, Charlotte NC Date Well Depth 5 w Depth to Water 5 Well Diameter 2" Casing Material PVC Screen Length 5' Well Water Volume Sampling Crew )t,A, M, N, Pump Type Peristaltic Tubing Type 114" Poly LDPE Intake set at -.,5t� Weather Conditions bvtrca s; . — (.0 1- Notes (eg. odor or color) No ✓ia 1-; cs.�i� Q16r Vf'5"b)•1 Glen r Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C ECj Slcm ORP mV Turbidity NTIJ 2. b 9, a, 6-to 16.1 ' pay , I O l l .tz 0.137 3,5 C. ' 0, I.1N MIS 0.905 7, 134 , q I' v. a . 5 9 c l () A qqZ4S o.0 3S2 1' .0 19'.06 95q 37 q, 53 .1 7Z9 v.o 58 1' 0 1q,01 0,9gto ./6 7, zz 0•6 1401 ' Z 19.0I 0.939 57 ILI o 1' Z " oz +9. 733 qbS . 1t Other Parameters Sampled at I 4 Parameters taken with Samples delivered to by y, 4, at 09417 owl r 1l i Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other H / I S z 6 U:IEAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)1Field FormslWR Groundwater Sampling Form for Trex Properties -All W .� Page Our People, Your Success Groundwater Sampling Form Job Number Of 1 03130430.11 State ID NCD049773245 Well ID PMW-2A Site Name TrexPropetWes, CharlotfeNC Date S 2-8f Well Depth 3a' Depth to Water - Well Diameter 2" Casing Material PVC Screen Length 10' Well Water Volume Sampling Crew X. A, ,V 44, Al, Pump Type Peristaltic Tubing Type 114" Poly !_DPE Intake set at " 7,6' Weather Conditions Qvercat4., Notes (eg odor or color) P6 ar �s:bl Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m /L Temp °C(PS/Cm) EC pH standard ORP m Turbidity NTU z 5 S. 1' b. Z 11,36 69 5.94 zq!8.1 Ing 5.+10, G .15 M39 z SA1 Z86 a.a 4 q0,l3 5.�9 Zsl v,o 173'.10 a, yq -7, T o. # 3 S.-1 $ Z-71 D. o o' 1, o 7 51 b, 117 y 6,-7 Z7 D, o :24o 5. qn, Z o,'Zcj)1,1,q t>,194 S.73 Z to 8 Izq3 0' O.zZ 0, q7 Sal 5 6.0 tZ4 S `i0' 0.01 1-1.58 0.198 5. bq Z43 rtsp �M a Other Parameters Sampled at vs Parameters taken with U Samples delivered to �, « � �by 1[, at 04 y 7 a Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic l 180 Days SO4 None 250 ml plastic 1 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other >' : %9 M M tsu) w ' &- U:IEAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injectionff ield FormslWR Groundwater Sampling Form for Trex Properties -All 9 410 lipOur People, Your Success Page 1 of 1 Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well1D PMW-213 Site Name Trex Properties, Charlotte NC Date i I S f 202 a Well Depth 55 Depth to Water S_61' Well Diameter 2" Casing Material PVC Screen Length 5' Well Water Volume Sampling Crew u, M,Al Pump Type Peristaltic Tubing Type 1/4" Poly LDPE Intake set at N 3 Weather Conditions Ove cas+� 65 r Notes (eg. odor or color) �Vp,�ofrcFl,la Oder 1�'tl.l... Llti r Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m li_ Temp °C EC Slcm pH standard ORP m Turbidity NTU b•!I' 1 ,01 IY.4z O,2#s 5.96 361 cc 11,50 0.3 o 0. 6 rl.,59 0. zyz S.83 350 53 6. 1' b.#IC 641 11,3 L o.Zq] 5.'01 Sq3 1166 3 01 6.66 6,10 `)• ! O.zq I 5. t 33 0 1159 4.,50' [).75 IS I I-v,4 L 6 ZHI S. 3 3zW 4 c2 6' O. qo D-$ 1-1,56 D. MI 5,84 315 0 )-Cos . 05 0.4I ?, Sal o.zy 0 to a, 30' f, I S . 3 q -7.5 O, Z 85 30 Z Izrl ,30' l 30 6.4 'I, bo 0. zq-L S, afa Tq 5 vtner rarameters Sampled at Samples delivered to I Z SParameters taken with Hor, bk U 5z z Pac. Am" g� c., by 1LA at 0? 1?'r on t/fi Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other i D ! q.,7 rpm Sod: .A �S 1 c4c U:IEAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injectionffield FormslWR Groundwater Sampling Form for Trex Properties -All OPage 1 of 1 Our People. Your Success Job Number 03130430.11 Groundwater Sampling Fonn State ID NCD049773245 Well ID PMW-3A Site Name Trex Properties, Charlotte NC Date 1 I 15 I iozo Well Depth 7,5' Depth to Water 6.1 Well Diameter 2" Casing Material PVC Screen Length 10, Well Water Volume Sampling Crew 9A. a- NJ, /,l, Pump Type Peristaltic Tubing Type 114" Poly LDPE Intake set at t0� Weather Conditions byc rca s + . — tpo c F Notes (eg odor or color) Alp *w h; c. Lj, radof VI S,'bILA G1 tc<< Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C(PS/cm) EC pH standard ORP m Turbidity NTU 1303 L b 9 &.1r 9.01 18.199 1.00 14 S q S69&l$ 1366 6, W G. a +5.00 14.0q D. 0` S,tD +170 13et 1309 6, ► ' D 4S 4. Z 111.1 0.78a 5,71 o Jao 110 , o o 1q, z 1 0,-176 1. Z'? qsq 9"7.6 gQ 19.z9 0.769 Y so 92,1? 32o a, t. J S 3 111,311 0.1767 S, zo yy $o, 23 4. TV i, se 4111S 11,51 0,1765 5, Iq q50 17 , J 33p Other Parameters Sampled at Samples delivered to by Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 0 180 Days SO4 None 250 ml plastic a 28 Days TOC 1­131304 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other 1 ' 7-13, L1 12PA, o iv 0" 1/16 U:IEAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)1Field FormslWR Groundwater Sampling Form for Trex Properties -All Page Our People, Your Success Of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-4A Site Name Trex Properties, Charloffe NC Date _ � t $ s os o Well Depth IZ Depth to Water q,yg Well Diameter 2+' Casing Material PVC Screen Length 5- Well Water Volume Sampling Crew M.N. Pump Type Peristaltic Tubing Type 1/4" Poly LDPE Intake set at N)#1 Weather Conditions • 1- Wr 1,,,4cf.ars Notes(eg odororcoloo Ne, ra�ea..41e, odor L.' At .► for , Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C(PS/CM) EC pH standard ORP mV Turbidity NTU ISO-1 5 b I q,5! j j, 31 D, 4VI3 0 1510 C1, 5 ' 14, qo ri.33o,yo9 1,16 )SS zqg Si3 9,SS' qi 'Z9 i 0,401 4106 1617 91,0 151 b .Sq 11,714 0. V.1 q 5,9,7 1 2 Zq,q 51 7' q.15 0390 SIC13 f 519 22- ,57 0 11,I D C. S 4 we ISzs q-01 0,385 5,50 7,01 "1, jVZ8 0.2 4,00 11.4DS o.3,bW S.-7-7 zl?- 4.3 1531 58 5,-73 21,7 S.K SLID q Ie Other Parameters Sampled at Samples delivered to taken with by k. A . at ogWT or, V/ d Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other o ;u ../ U:IEAG ProjectslTrex Properties LLC - DETREX - T1Charlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injectionff ield FormslWR Groundwater Sampling Form for Trex Properties -All Page Our People, Your Success Of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-5A Site Name Trex Properties, Charlotte NC Date zot0 Well Depth 314 Depth to Water Well Diameter 2" Casing Material PVC Screen Length 10' Well Water Volume Sampling Crew 1C. A. 4. m , d, Pump Type Peristaltic Tubing Type 114" Poly LDPE Intake set at 3 �1 Weather Conditions 0yerC4x5t , --V 43°F' Notes (eg odor or color) Nc ne+:c"I& od&.- v,,c;b1H GIsAr Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C(PS/cm) EC pH standard ORP mV Turbidity NTU SUL IS. M % 01 tit A.4'1 1, 4f 5 3, s z 465 z 9 -t IS s -6Ss' 6.;o 6,06 1 R.q-r 1.41 4.5'7 k21 31-6 5 '* 6 4C 0.00 6 1. 5 L q, It 389 30. 551 S' 0.60 6,00 0,30 1,10 S.aZ 374 1111 sq ' a-7S 4r00 1 ,q3 I. t 5,11 3170 7z,I ISS, 14,190.90 ,oa ,CIS �5 366 t.� Other Parameters Sampled at Samples delivered to 01 Parameters taken witt e c , by at 69Y7 car+ Oic Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days Ethenes None 40 ml VOAs glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other 1D 1 by7 At If, ljt, 4 .- ltok3 5 d #L% d s I h+I for e S k w it a U:IEAG ProjectslTrex Properties LLC - DETREX - T1Charlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injectioriffield FormslWR Groundwater Sampling Form for Trex Properties -All 40- lip People, Your Success Page 1 of 1 Job Number 03130430.99 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-6A Site Name Trex Properties, Charlotte NC Date_I liq Izoto Well Depth 3 g Depth to Water ;; , 6 3 : Well Diameter 2" Casing Material PVC Screen Length 10, Well Water Volume Sampling Crew g A k- M.N. Pump Type Peristaltic Tubing Type 1/4" Poly LDPE Intake set at 33 Weather Conditions 6 V, rca► s i •v 4 3 o F Notes (eg odor or color) NO rtet. cdo le- e.f V. <-tl.., rl.-- Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C(PS/cm) EC pH standard ORP mV Turbidity NTU 1600 5,31, 2 1.33 20. qz I. -IS 4,5,1 470 147 563 Zn' a• 1 Ze. Z I - 1B I W.65 411 9'i 06 01& 0115Z0.3% 1.88 y. 7o y 8t it. 15o9 0.08 20,40 1.93 4111 L49C IS-1 512 4,4%, 1,o 0,oq Ze.gd I, q1. 4113 N $ it) ► I -0' 1. r 0, eZ to, Ztoo q..IH90 11101 IS1% 4, 11 b.00 in,q Z 2.01 14.-Ig 11,11 I � '� ,9'►+ 1. 6 0 00 �0, 4 , r: �[.'15 Lill -I 5,,- P i utner varameters Sampled at 1 5 3 0 Samples delivered to po-c,_ _Si by at A, at —R7 d.r IN Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic i 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other 1p: 374.1 ppm r 7 70 Nine 5fetA late rid s AP U:IEAG Projects\Trex Properties LLC - DETREX - T\Charlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)1Field Forms\WR Groundwater Sampling Form for Trex Properties -All too .. Our People, Your Success Page 1 of 1 Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-7A Site Name Trex Properties, Charloffe NC Date r 1 Z6 Well Depth 3 Depth to Water 6 _ $ Well Diameter 2" Casing Material PVC Screen Length 10, Well Water Volume Sampling Crew K A. j- Pump Type Peristaltic Tubing Type 1/4" Poly LDPE Intake set at Weather Conditions 19A t r..n , rob F Notes (eg. odor or color) We ne4.r.,.h1L ndor iTT-1 - r1-..r Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C(PS/cm) EC pH standard ORP m Turbidity NTU 10 1.$9' 01Z 0,01 14.26 O,z%% 5let 1 11711 131 ILI13 1. r b• y a 0.ZZ3 3 1-11 lit ILll "1.9a' 0, d.oa 19.3z 0.tz3 i69 y. 14la .90' .8 0,00 q.31 . VZ3 S. o 14S 5, 142z `1 , CtZ' 16 0, bc> lq.q4 D. VL3 S.S4 10 q31 1425 -1, 9 1 I• Y o.00 4.41 0.'123 17.199 1 6 5, t 8 �, 9' 1.41 O,00 y 9 o' 35. Z a !� o.db 9.�1"I 0.7z 3 %-1 166 33.1 0100 1q.5o o.zZ 81 ILC '3 z jq M 1i Other Parameters Sampled at Parameters taken with pr,l7cl -5z Samples delivered to P"r] ., j . r by Ae, q , at�t/0 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass ----3- 14 Days Ethenes None 40 ml VOAs glass _ 3 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other 63.6 piem U:IEAG ProjectslTrex Properties LLC - DETREX --RCharlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)1Field Forms\WR Groundwater Sampling Form for Trex Properties -All Our People, Your Success Page Of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-713 Site Name Trex Properties, Charlotte NC Date + 4 ' Zs 20 Well Depth 5; Depth to Water 6,76 Well Diameter 2" Casing Material PVC Screen Length 5' Well Water Volume Sampling Crew K.O. j-- M.N. Pump Type Peristaltic Tubing Type 1/4" Poly LDPE Intake set at . 51 ' Weather Conditions 1-r 4 ra .., r b 5 F Notes (eg odor or color) o ho j; A I, t er Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C(PS/cm) EC pH standard ORP mV Turbidity NTU 1330 L1,01 Is. gq 0.1 Wt 4.53 134 33 8' 0,111 1,55 l 9 q5.4 1336 6,99, 0.4 2116 1 t. 16 11, a 11 .5 14 III 33 9 6 2,13 I$.6S 0.1-1 �.5 4 'i 3 4 n 4 I A Z. I q fit. 0, j 5 b 156 13H5 1 MLL 6,194 C,qS 15t 13Z 1344 f. yI 3t 1 7 61 19D %,940 I , 1 1,,: M Z q 6,193 (1,34 15 1354 It) 15'4 7 Hot, Other Parameters Sampled at 9.6 Parameters taken with er;b o, a-5,Z,T Samples delivered to o,,, wt.a by at oyy pr +r�4 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic # 180 Days SO4 None 250 ml plastic M 28 Days TOC H31304 40 ml VOAs glass _ 7 days Pesticides None 1 Liter glass 7 Days Other 4 b', 3,9 RRAA t M U:IEAG ProjectslTrex Properties LLC - DETREX - T1Charlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injectioriffield FormslWR Groundwater Sampling Form for Trex Properties -All 40 Page Our People, Your Success of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well I PMW-8A Site Name Trex Properties, Charlotte NC Date 114 1-0ZO Well Depth y2. 01 Depth to Water 1 $ Well Dia eter 2" Casing Material PVC Screen Length 10' Well Water Volume Sampling Crew X. A. k A4. N, Pump Type Peristaltic Tubing Type 1/4" Poly LOPE Intake set at -. 317 Weather Conditions Dvc rG, s k ii Z ` F Notes (eg. odor or color) 5 i... k.F 0d. o, Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m /L Temp °C EC S/cm) pH standard ORP m Turbidity NTU 08 18. 9 0.7,1- 4.28 z3G 0 91z' a.q 10.63 0-te") 5 cl I US 1.Z 0836 q.2 R, 0•f/ 1110 t8.so �.Z0? 0,00 Z4D 2t.L. oS34 q, 4 2' 5� I 9 �•209 S. J3 24 6 111.3 0 42- G.56, t.0 '1 t 5.53 Zy Li 2 , 0134S 4,69, f•'t 4 1 1q.64 O.Zot 5.45 Z 0'94 $ 9.19 1 1,'1* 6 19, oq D . t oS S. S ' 14 0051 911, C 6 4.2 16 19.1, D.ZOS S.yo S50 - 5 .61' 1, 3 S 5 19.15 0, taS !;, 101 1+1 9 0961 10.01' 5 '9 z4 64 3 0 1` Other Parameters Sampled at Samples delivered to meters taken with H f.6o, by at 6041 0.,, (116 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 1 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other PM: '7. C 1 04 U:IEAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NC1NC - RFI, TREXIGW Monitodng12020-01 (Post- Injectioriff ield >=ormslWR Groundwater Sampling Form for Trex Properties -All 40- lipOur People, Your Success Page 1 of 1 Job Number 03130430.99 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-8B Site Name Trex Properties, Charlotte NC Date s iy Well Depth lk Depth to Water Well Diameter 2" Casing Material PVC Screen Length 5' Well Water Volume Sampling Crew 9 A/ M. N Pump Type Peristaltic Tubing Type 1/4" Poly LDPE Intake set at.-5G` Weather Conditions {%Ytf fw s 4 /n F Notes (eg odororcolor) _�✓p ✓la�tw6lr, ader Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m /L Temp °C EC (PS/cm)rd R-7, ORP m Turbidity NTU 1220 Z2. (0 D. b. 15,12 o.69, ZZ3 r--*� v.y 0.10 u.-r09 -22 8 zz 6 3.Z' O.L D.13 8• Q -21 lob }t2 S, I' t). 09 i '1 0.11 — 19 r2�2 ►2" 1. a b c3 8_ Z 6,136 S -)-1 55 235 Z6,'iZ` oo I Z 0.-7q-1 7,'t -� I I238 2"1 1. y rs.00 2 0.~1 -I 2y I Z7, 4 6, 1. 6 0,00 3 6.18 -1173 . ILA I-M Z%.5LA' !•S t,0 -73 utner varameters Sampled at Samples delivered to by oK Ih 6 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic I 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other 04. ,A p" dirl ko -2 0 f-ras so ,u,,.• P-cfs 1 w W QpPAAI feM / As 1 (57 20 I lien 111VIEd. vM ,&d brog. — C41#0' 6 I740 0.+ //ry'io - DTw; 3d, so` 6'` PeeAe e j 0T6**11% Z4, sot e f 6Sa a^ I/s. 11:lEAG ProjectslTrex Properties LLC - DETREX - T1Charlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injectiori ff ield FormslWR Groundwater Sampling Form for Trex Properties -All Our People, You, Success Groundwater Sampling Form Page 1 of Job Number 03130430.11 State ID NCD049773245 Well ID PMW-9A Site Name Trex Properties, Charlotte NC Date Z , T 0 Well Depth I , Depth to Water $, I Well Diameter' 2" Casing Material PVC Screen Length 10' Well Water Volume Sampling Crew Pump Type Peristaltic Tubing Type 114" Poly LDPE Intake set at Weather Conditions e a a . Lae 14 Notes (eg. odor or color) !0 . �% r Other Parameters Sampled at p Parameters taken witt Samples delivered to by �L�-, )/it Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic I 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 7 days Pesticides None 1 Liter glass 7 Days Other Pito, M.2 M T63 - @ s rrj.r� w7 op WEAL ProjectslTrex Properties LLC - DETREX - TlCharlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injectionffield Forms\WR Groundwater Sampling Form for Trex Properties -All �. Our People. Your Success Groundwater Sampling Form Page 1 of Job Number 03130430.11 State ID NCD049773245 Well ID PMW-9B Site Name Trex Properties, Charlotte NC Date Well Depth 3y Depth to Water g, Well Diameter 2" Casing Material PVC Screen Length 10, Well Water Volume Sampling Crew K + A N. Pump Type Peristaltic Tubing Type 114" Poly LD_PE Intake set at .v Z 9 ` Weather Conditions Over [As+- , - 6 Notes (eg. odor or color) No aaalr "61 of Other Parameters Sampled at Samples delivered to Parameters taken with____bter �,L u 5 % Rb.. -,•s t`cul by at O 7 nn Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 180 Days 804 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other I i�` 50 . to r i A U:%EAG ProjectslTrex Properties LLC - DETREX - T1Charlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injectionffield FormslWR Groundwater Sampling Form for Trex Properties -All J� Our People, Your Success Page Groundwater Sampling Form Of Job Number 03130430.11 State ID NCD049773245 Well ID PMW-9C Site Name Trex Properties, Charloffe NC Date 1 / 1 S /2 0 z o Well Depth S.,- Depth to Water R .3 W Well Diameter 2" Casing Material PVC Screen Length 5' Well Water Volume Sampling Crew X„ Q . 4- M. iv. Pump Type Peristaltic Tubing Type 114" Poly LDPE Intake set at !L f Weather Conditions nw rr ' S • F Notes (eg odor or color) /N _Ode,.' 11 Time 24 Fir. Water Level from TOG)Gals. Volume Purged DO m IL Temp °C EC (PS/cm)standard pH ORP m Turbidity NTU 119,31 O7 34i ;112 S,� b94 2` o a 1%40 0.,?q A &z5 4,1,9 Iq :I q 10' 0,61 D.00 19.3q 0-353 4 zi; 73 t4.s (3gSW ,)a 6.60 6,00 0, 743 .z-1 3y, 2 .0951 b,7f 0.00 10AS 0,34"? b.za zl • 5 1000 0,90 0.60 K.qb 0,311 G,2G z0, a poi 1:OS 6,00 I '{g A.3-7-1 ^/, 1 Other Parameters Sampled at Samples delivered to 1010 Parameters taken with Pace n�!„�,ru 1 by, at L!7 4—f r�,6 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOG H3PO4 40 ml VOAs glass 7 days Pesticides None 1 Liter glass 7 Days Other Pip: Hl.%i vmm s Pry • tlt P M U:IEAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)IField FormslWR Groundwater Sampling Form for Trex Properties -All Page 1 of Our People Your Success Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-10A Site Name Trex Properties, Charloffe NC Date 1 �� Za Well Depth 3' _ Depth to Water 6 Well Diameter 2" Casing Material PVC Screen Length 10' Well Water Volume Sampling Crew K. TAi.tj , � P, � J p Pump Type Peristaltic Tubing Type 1/4" Poly LDPE Intake set at g(p ""�" Weather Conditions Ovc r c.. s 4 . N b5 ° F` Notes (eg odor or color) ft y404.j S. A. h4 Lit.� Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C EC S/cm) pH ORP (mV Turbidity NTU In5v 6 0.10 0. CS 0.795 G.II Sit lo 53 C.11 0.36 b 167, 11. t 4 611-1L 3, 4 e n. S 6,00 1-1, 0.-747 6,19 310 b. Ds-, 7h{ 0.6.0 0,00 -1.70 b.la 3zo 0.0 DZ '1'1' ,yS ao 1-1,'13 6,159 (0.1q 7, z1 0,0 95 L. 77 d,9a 6.06 1111b 6.15 b.zo 31Z 0.0 .-Y7' 1. 65 A.p o -1 -1'1 1 6.'15 ,zo zz 010 ro��i' 95 r7.00 '1.-7 0.0 I a�n I s Other Parameters Sampled at Samples delivered to ► Parameters taken with r r1 hl, ca / by, at o9l,r ter► I/6 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 1 180 Days SO4 None 250 ml plastic 1 _ 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other lv' L ► 5 A-W to U:IEAG ProjectslTrex Properties LLC - DETREX - T1Charlotte, NC1NC - RFI, TREXIGW Monitodng12020-01 (Post- Injectioriffield FormslWR Groundwater Sampling Form for Trex Properties -All NIP Our People, Your Success Page Groundwater Sampling Form Site Name Trex Properties, Charloffe NC Well Depth -is, Depth to Water Casing Material PVC Screen Length 5- Sampling Crew K•A 4- M.,4, Pump Type Peristaltic Tubing Type 1/4" Poly Weather Conditions r)VCX CA-54-, ti 65°r Noti Of Job Number 03130430.11 State ID NCD049773245 Well ID PMW-10B Date , rS Zo2D _ Well Diameter 2" Well Water Volume DIRE Intake set at'— -11 (eg odororcolor) A/p Nei};ak�,ft Ddel, V,'s;blH c1t�� Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C(PS/cm) EC pH standard ORP m Turbidity NTU )bI5 6.-77` OBI U.-I I-' Ss d. 0 5.5 a 2 o O-L 0111 17,8 0,153 5,96 Iq3 011 ' o. 0,04, I-1-S9 6"13q 6.08 jqt 6, o2y 6,74` 6f 6.00 111,M 6.13o (p,fl 701 6,0 IbZ7 -1 F 0.5 b.DD I'1.90 0,7zb .Is1 zf2 .O 030 0. A,00 h. o.72s (,.Iy 2.f`1 O.O '33 0 1-7,11 6.-1z 6. IS 2zy o, r Other Parameters Sampled at y0 Parameters taken with Nor. &G i S x Samples delivered to a G I by K.A at o q-? I 6 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic I 180 Days SO4 None 250 ml plastic + 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other : 246.3 P Pv r U:%EAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)1Field FormslWR Groundwater Sampling Form for Trex Properties -All Our People, Your Success Page Of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-11A Site Name Trex Properfles, Charlotte NC Date ! ro /z o z o Well Depth 63' Depth to Water ,1 x Well Diameter 2" Casing Material PVC Screen Length 10' Well Water Volume Sampling Crew 14, A. T /4. , Pump Type Peristaltic Tubing Type 1/4" Poly LDPE Intake set at• Weather Conditions p vc+ c e► 1i , 2' Notes (eg odor or color) �{/� �,� ;Gal +t o d •� Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m IL Temp °C(PS/Cm) EC pH standard ORP m Turbidity NTU &I ,Sq 9 o,761 9,72 /i, 1 6.y .cal ).571 or S,9,1 I za, jolt G,'7a r 6-15 .42 4,01 10" 6.8:3 r.a 0.11 I'IA 0.94t 6.d3 7 4 0e1 6,q6 11.19 o e05 4.Dq b Other Parameters Sampled at Parameters taken with • Z Samples delivered to p At ,� } c by at 64y7 e-i r//6 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 1 180 Days SO4 None 250 ml plastic 1 28 Days TOC H3PO4 40 ml VOAs glass 7 days Pesticides None 1 Liter glass 7 Days Other U:IEAG ProjectslTrex Properties LLC - DETREX - T\Chadotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injectionff ield Form51WR Groundwater Sampling Form for Trex Properties -All fto.1#'i$rrAr�a4r Page Our People, Your Success Of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-11 B Site Name Trex Properfles, Charlotte NC Date 1 I 101.0 Well Depth 11a. 0 ` Depth to Water -1, t r Well Diameter 2" Casing Material PVC Screen Length 5' Well Water Volume Sampling Crew K.A. d' HI, k Pump Type Peristaltic Tubing Type 1/4" Poly LDPE !' Intake set at — 7 b Weather Conditions 4vcicSLs4 , w 6Z6F Notes (eg. odor or color) A/�, rIO�:Ia61t eder V:S�t~IM Glta�` Time 24 Hr. Water Level from TOC Volume Purged Gals. DO m /L Temp °C(PS/Cm) EC pH standard ORP m Turbidity NTU 411 't . Z G 111. 6 9 ; I 930 -1, 6, Y 0,3 I -I Ag 5.b 1 R0,0 0433 1. o. o.a '1.'14 6,244 L;m 7.3 G„o 36 B 0-2f,to 5-Fts i1 0.4 3 -111 11. 2 S, q 2 go 0Q N2 4' z o, t 11.16 0.2$R SA3 NY b 0•0 Irlb 43 5",55 "t 0 48 H 1.(0 0.0 11,94 17 09 SCI SOLIAPI Other Parameters Sampled at Samples delivered to 0 R S_0 Parameters taken with Pace 44 by, at-&Pyy „ 114 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCS HCL 40 ml VOAs glass 14 Days Ethenes None 40 ml VOAs glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 7 days Pesticides None 1 Liter glass 7 Days Other Ptr): 14.1 M PumP S ec.d t*& St 51 �p k4 U:IEAG ProjectslTrex Properties LLC - DETREX - T\Charlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)1Field FormslWR Groundwater Sampling Form for Trex Properties -All 40 .Page 1 of 1 Our People, Your Success Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID PMW-13B Site Name Trex Properties, Charlotte NC Date / V z0 Well Depth J 3 _ Depth to Water ^I Well Diameter 2" Casing Material PVC Screen Length 5' Well Water Volume .�. Sampling Crew X, A. 4- A4. n! Pump Type Peristaltic Tubing Type 114" Poly LDPE Intake set at Weather Conditions �- coo F Notes (eg odor or color) /Vo rfa�rc.61. AE sr I/'srbly cicoar Other Parameters Sampled at V Parameters taken with k1bri 6f, tt-SZ Samples delivered to by X A , at y7 G Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 3 14 Days Ethenes None 40 ml VOAs glass 3 7 Days Metals Nitric Acid 250 ml plastic 1 180 Days 804 None 250 ml plastic 1 28 Days TOC H3PO4 40 ml VOAs glass 3 7 days Pesticides None 1 Liter glass 7 Days Other ID.' /9.8 prA, !;,,el, PcrS-I i,ie .'-7.o AA4t r 4epe , # {, • N.R. r�, K C f d i�14 U:IEAG ProjectslTrex Properties LLC - DETREX - RCharlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injectiori (field FormslWR Groundwater Sampling Form for Trex Properties -All "0 Page 1 of 1 Our People, Your Success Groundwater Sampling Form Job Number 03130430.11 State ID NCD049773245 Well ID SW-1 Site Name Trex Properties, Charlotte NC Date I+ 5 f 1-a z 0 Well Depth Depth to Water Well Diameter Casing Material Screen Length Well Water Volume Sampling Crew , N Pump Type Tubing Type Intake set at Weather Conditions nvcrc, S4 . ^' b- F Notes (eg odor or color) Other Parameters Sampled at 16ZC4 Parameters taken with Samples delivered to sacs rrFl_ by M N at a 9 q 7 e.4 1�/6 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days Ethenes None 40 ml VOAs glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 7 days Pesticides None 1 Liter glass 7 Days Other s �'v oK d- f U:%EAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NCINC - RFI, TREXIGW Monitodng12020-01 (Post- Injectionff ield FormslWR Groundwater Sampling Form for Trex Properties -All Page 1 of 1 mRPP Our People Your Success Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID SW-2 Site Name Trex Properties, Charlotte NC Date i 115 Z o z a Well Depth Depth to Water Well Diameter Casing Material Screen Length Well Water Volume Sampling Crew )C A ,L M, jy. Pump Type Tubing Type Intake set at Weather Conditions Querar, S ♦ o 6 F Notes (eg odor or color) Other Parameters Sampled at 1615 Parameters taken with Samples delivered to %{ by M,N, at d 9y7 0+t (If,( Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days Ethenes None 40 ml VOAs glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 7 days Pesticides None 1 Liter glass 7 Days Other U:IEAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NCINC - RFI, TREXIGW Monitoring12020-01 (Post- Injection)1Field FormslWR Groundwater Sampling Form for Trex Properties -All Page Our People, Your Success Of Job Number 03130430.11 Groundwater Sampling Form State ID NCD049773245 Well ID SW-3 Site Name Trex Properties, Charlotte NC Date I t s x o 2 o Well Depth Depth to Water Well Dia eter Casing Material Screen Length Well Water Volume Sampling Crew A, - M, Al, Pump Type Tubing Type Intake set at Weather Conditions OYir ca S+ .1 w 6 o ° F Notes (eg odor or color) • . �• �M •--Turbidity Other Parameters Sampled at Samples delivered to os Parameters taKen with c .fY4,-c./ by 1A,1J at pgyy O., t//6 Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days Ethenes None 40 ml VOAs glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days SO4 None 250 ml plastic 28 Days TOC H3PO4 40 ml VOAs glass 7 days Pesticides None 1 Liter glass 7 Days Other U:IEAG ProjectslTrex Properties LLC - DETREX - TlCharlotte, NC1NC - RFI, TREXIGW Monitoring12020-01 (Post- InjectEoriffield FormslWR Groundwater Sampling Form for Trex Properties -All EnvirQAnafytics Group APPENDIX C LABORATORY REPORTS AND CHAIN OF CUSTODY RECORDS leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 23, 2020 David Craig EnviroAnalytics Group 1650 Des Peres Road Suite 303 Saint Louis, MO 63131 RE: Project: Trex-Charlotte GW Pace Project No.: 92461009 Dear David Craig: Enclosed are the analytical results for sample(s) received by the laboratory on January 16, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, p Taylor Ezell taylor.ezell@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Matthew Dostal, EnviroAnalytical Group REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 114 lacieAnalyfica(' www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Trex-Charlotte GW Pace Project No.: 92461009 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Mold Certification #: LAB0152 Texas Certification #: T 104704245-17-14 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Virginia Certification #: VT2006 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 9980939910 Wyoming UST Certification #: via A21-A 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Trex-Charlotte GW Pace Project No.: 92461009 Lab ID Sample ID Matrix Date Collected Date Received 92461009001 PMW-1A Water 01/15/20 15:00 01/16/20 09:47 92461009002 PMW-1B Water 01/15/2014:05 01/16/20 09:47 92461009003 PMW-2A Water 01/15/20 12:50 01/16/20 09:47 92461009004 PMW-2B Water 01/15/20 12:15 01/16/20 09:47 92461009005 PMW-3A Water 01/15/20 13:30 01/16/20 09:47 92461009006 PMW-4A Water 01/15/20 15:40 01/16/20 09:47 92461009007 PMW-5A Water 01/14/20 16:00 01/16/20 09:47 92461009008 PMW-6A Water 01/14/20 15:30 01/16/20 09:47 92461009009 PMW-7A Water 01/14/20 14:40 01/16/20 09:47 92461009010 PMW-7B Water 01/14/20 14:00 01/16/20 09:47 92461009011 PMW-8A Water 01/14/20 09:00 01/16/20 09:47 92461009012 PMW-8B Water 01/15/20 16:55 01/16/20 09:47 92461009013 PMW-9A Water 01/15/20 09:00 01/16/20 09:47 92461009014 PMW-9B Water 01/15/20 09:40 01/16/20 09:47 92461009015 PMW-9C Water 01/15/20 10:10 01/16/20 09:47 92461009016 PMW-10A Water 01/15/20 11:15 01/16/20 09:47 92461009017 PMW-10B Water 01/15/20 10:40 01/16/20 09:47 92461009018 PMW-11A Water 01/14/20 10:40 01/16/20 09:47 92461009019 PMW-11 B Water 01/14/20 09:50 01/16/20 09:47 92461009020 PMW-13B Water 01/14/20 11:50 01/16/20 09:47 92461009021 PMW-DUP1 Water 01/15/20 11:15 01/16/20 09:47 92461009022 PMW-DUP2 Water 01/15/20 14:05 01/16/20 09:47 92461009023 SW-1 Water 01/15/20 16:25 01/16/20 09:47 92461009024 SW-2 Water 01/15/20 16:15 01/16/20 09:47 92461009025 SW-3 Water 01/15/20 16:05 01/16/20 09:47 92461009026 EB-1 Water 01/14/20 16:15 01/16/20 09:47 92461009027 EB-2 Water 01/15/20 17:05 01/16/20 09:47 92461009028 Trip Blank 1 Water 01/14/20 08:00 01/16/20 09:47 92461009029 Trip Blank 2 Water 01/14/20 16:20 01/16/20 09:47 92461009030 Trip Blank 3 Water 01/15/20 08:00 01/16/20 09:47 92461009031 Trip Blank 4 Water 01/15/20 17:10 01/16/20 09:47 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Trex-Charlotte GW 92461009 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92461009001 PMW-1A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009002 PMW-1 B RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D CL 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009003 PMW-2A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009004 PMW-213 RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009005 PMW-3A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009006 PMW-4A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009007 PMW-5A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009008 PMW-6A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Trex-Charlotte GW Pace Project No.: 92461009 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009009 PMW-7A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009010 PMW-713 RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009011 PMW-8A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009012 PMW-813 RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009013 PMW-9A RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009014 PMW-913 RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009015 PMW-9C RSK-175 DAH 1 PAN EPA 6010D SH1 1 PASI-A EPA 8260D CL 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Trex-Charlotte GW 92461009 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SM 5310B-2011 ECH 1 PASI-A 92461009016 PMW-10A RSK-175 DAH 1 PAN EPA 6010D IDS 1 PASI-A EPA 8260D CL 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009017 PMW-10B RSK-175 DAH 1 PAN EPA 6010D IDS 1 PASI-A EPA 8260D CL 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009018 PMW-11A RSK-175 DAH 1 PAN EPA 6010D DS 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009019 PMW-11 B RSK-175 DAH 1 PAN EPA 6010D IDS 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009020 PMW-13B RSK-175 DAH 1 PAN EPA 6010D IDS 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009021 PMW-DUP1 RSK-175 DAH 1 PAN EPA 6010D IDS 1 PASI-A EPA 8260D CL 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009022 PMW-DUP2 RSK-175 DAH 1 PAN EPA 6010D IDS 1 PASI-A EPA 8260D SAS 63 PASI-C EPA 300.0 Rev 2.1 1993 BRJ 2 PASI-A SM 5310B-2011 ECH 1 PASI-A 92461009023 SW-1 EPA 8260D CL 63 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Trex-Charlotte GW 92461009 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92461009024 SW-2 EPA 8260D SAS 63 PASI-C 92461009025 SW-3 EPA 8260D SAS 63 PASI-C 92461009026 EB-1 EPA 8260D SAS 63 PASI-C 92461009027 EB-2 EPA 8260D SAS 63 PASI-C 92461009028 Trip Blank 1 EPA 8260D SAS 63 PASI-C 92461009029 Trip Blank 2 EPA 8260D SAS 63 PASI-C 92461009030 Trip Blank 3 EPA 8260D SAS 63 PASI-C 92461009031 Trip Blank 4 EPA 8260D SAS 63 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-1A Lab ID: 92461009001 Collected: 01/15/20 15:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:11 01/20/2014:11 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 5060 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 22:55 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone 69.2J ug/L 125 30.8 5 01/20/20 13:14 67-64-1 Benzene ND ug/L 5.0 0.75 5 01/20/20 13:14 71-43-2 Bromobenzene ND ug/L 5.0 1.1 5 01/20/20 13:14 108-86-1 Bromochloromethane ND ug/L 5.0 1.7 5 01/20/20 13:14 74-97-5 Bromodichloromethane ND ug/L 5.0 1.3 5 01/20/20 13:14 75-27-4 Bromoform ND ug/L 5.0 3.1 5 01/20/20 13:14 75-25-2 Bromomethane ND ug/L 10.0 3.1 5 01/20/20 13:14 74-83-9 IK 2-Butanone (MEK) ND ug/L 25.0 16.6 5 01/20/20 13:14 78-93-3 Carbon tetrachloride ND ug/L 5.0 1.1 5 01/20/20 13:14 56-23-5 Chlorobenzene ND ug/L 5.0 1.2 5 01/20/20 13:14 108-90-7 Chloroethane ND ug/L 5.0 2.4 5 01/20/20 13:14 75-00-3 v2 Chloroform ND ug/L 25.0 11.7 5 01/20/20 13:14 67-66-3 Chloromethane ND ug/L 5.0 1.9 5 01/20/20 13:14 74-87-3 v2 2-Chlorotoluene ND ug/L 5.0 1.0 5 01/20/20 13:14 95-49-8 4-Chlorotoluene ND ug/L 5.0 1.0 5 01/20/20 13:14 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 25.0 1.3 5 01/20/20 13:14 96-12-8 Dibromochloromethane ND ug/L 5.0 2.1 5 01/20/20 13:14 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 1.3 5 01/20/20 13:14 106-93-4 Dibromomethane ND ug/L 5.0 2.3 5 01/20/20 13:14 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 1.5 5 01/20/20 13:14 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 1.1 5 01/20/20 13:14 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 1.3 5 01/20/20 13:14 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 1.1 5 01/20/20 13:14 75-71-8 1,1-Dichloroethane 5.8 ug/L 5.0 1.3 5 01/20/20 13:14 75-34-3 1,2-Dichloroethane ND ug/L 5.0 1.7 5 01/20/20 13:14 107-06-2 1,1-Dichloroethene ND ug/L 5.0 1.2 5 01/20/20 13:14 75-35-4 cis-1,2-Dichloroethene 598 ug/L 5.0 1.5 5 01/20/20 13:14 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 1.3 5 01/20/20 13:14 156-60-5 1,2-Dichloropropane ND ug/L 5.0 0.94 5 01/20/20 13:14 78-87-5 1,3-Dichloropropane ND ug/L 5.0 0.79 5 01/20/20 13:14 142-28-9 2,2-Dichloropropane ND ug/L 5.0 1.4 5 01/20/20 13:14 594-20-7 1,1-Dichloropropene ND ug/L 5.0 1.1 5 01/20/20 13:14 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 1.5 5 01/20/20 13:14 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 5.0 1.5 5 01/20/20 13:14 10061-02-6 Diisopropyl ether ND ug/L 5.0 1.1 5 01/20/20 13:14 108-20-3 Ethylbenzene ND ug/L 5.0 1.3 5 01/20/20 13:14 100-41-4 Hexachloro-1,3-butadiene ND ug/L 5.0 2.2 5 01/20/20 13:14 87-68-3 2-Hexanone ND ug/L 25.0 2.8 5 01/20/20 13:14 591-78-6 p-Isopropyltoluene ND ug/L 5.0 1.1 5 01/20/20 13:14 99-87-6 Methylene Chloride ND ug/L 25.0 18.4 5 01/20/20 13:14 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-1A Lab ID: 92461009001 Collected: 01/15/20 15:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 22.6 5 01/20/2013:14 108-10-1 ND ug/L 5.0 1.4 5 01/20/2013:14 1634-04-4 ND ug/L 5.0 1.8 5 01 /20/20 13:14 91-20-3 ND ug/L 5.0 1.3 5 01/20/2013:14 100-42-5 ND ug/L 5.0 1.7 5 01/20/2013:14 630-20-6 ND ug/L 5.0 1.1 5 01/20/2013:14 79-34-5 71.7 ug/L 5.0 0.81 5 01/20/2013:14 127-18-4 ND ug/L 5.0 1.2 5 01/20/2013:14 108-88-3 ND ug/L 5.0 1.7 5 01 /20/20 13:14 87-61-6 ND ug/L 5.0 1.1 5 01/20/2013:14 120-82-1 16.3 ug/L 5.0 0.88 5 01/20/2013:14 71-55-6 ND ug/L 5.0 1.2 5 01/20/2013:14 79-00-5 218 ug/L 5.0 1.1 5 01/20/2013:14 79-01-6 ND ug/L 5.0 1.6 5 01/20/2013:14 75-69-4 ND ug/L 5.0 1.7 5 01/20/2013:14 96-18-4 ND ug/L 10.0 7.2 5 01/20/2013:14 108-05-4 IK 19.0 ug/L 5.0 1.2 5 01/20/2013:14 75-01-4 ND ug/L 5.0 3.2 5 01/20/2013:14 1330-20-7 ND ug/L 10.0 2.0 5 01/20/2013:14 179601-23-1 ND ug/L 5.0 1.1 5 01/20/2013:14 95-47-6 100 % 70-130 5 01/20/2013:14 460-00-4 95 % 70-130 5 01/20/2013:14 17060-07-0 102 % 70-130 5 01/20/2013:14 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 9.0 mg/L 1.0 0.60 1 01/18/20 02:56 16887-00-6 634 mg/L 12.0 6.0 12 01/18/2017:03 14808-79-8 Analytical Method: SM 531OB-2011 10.9 mg/L 1.0 0.50 1 01/20/20 22:21 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-1B Lab ID: 92461009002 Collected: 01/15/20 14:05 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Ethene 6010 MET ICP Iron 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride Date: 01/23/2020 03:52 PM Analytical Method: RSK-175 Preparation Method: RSK175 ND ug/L 13.0 4.26 1 01/20/2014:27 01/20/2014:27 74-85-1 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A ND ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 22:58 7439-89-6 Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/18/20 23:48 67-64-1 ND ug/L 1.0 0.15 1 01/18/20 23:48 71-43-2 ND ug/L 1.0 0.22 1 01/18/20 23:48 108-86-1 ND ug/L 1.0 0.34 1 01/18/20 23:48 74-97-5 ND ug/L 1.0 0.26 1 01/18/20 23:48 75-27-4 ND ug/L 1.0 0.62 1 01/18/20 23:48 75-25-2 ND ug/L 2.0 0.62 1 01/18/20 23:48 74-83-9 ND ug/L 5.0 3.3 1 01/18/20 23:48 78-93-3 ND ug/L 1.0 0.22 1 01/18/20 23:48 56-23-5 ND ug/L 1.0 0.23 1 01/18/20 23:48 108-90-7 ND ug/L 1.0 0.49 1 01/18/20 23:48 75-00-3 ND ug/L 5.0 2.3 1 01/18/20 23:48 67-66-3 0.73J ug/L 1.0 0.39 1 01/18/20 23:48 74-87-3 ND ug/L 1.0 0.20 1 01/18/20 23:48 95-49-8 ND ug/L 1.0 0.20 1 01/18/20 23:48 106-43-4 ND ug/L 5.0 0.26 1 01/18/20 23:48 96-12-8 ND ug/L 1.0 0.41 1 01/18/20 23:48 124-48-1 ND ug/L 1.0 0.26 1 01/18/20 23:48 106-93-4 ND ug/L 1.0 0.46 1 01/18/20 23:48 74-95-3 ND ug/L 1.0 0.29 1 01/18/20 23:48 95-50-1 ND ug/L 1.0 0.22 1 01/18/20 23:48 541-73-1 ND ug/L 1.0 0.26 1 01/18/20 23:48 106-46-7 ND ug/L 1.0 0.23 1 01/18/20 23:48 75-71-8 0.38J ug/L 1.0 0.27 1 01/18/20 23:48 75-34-3 ND ug/L 1.0 0.34 1 01/18/20 23:48 107-06-2 ND ug/L 1.0 0.24 1 01/18/20 23:48 75-35-4 69.5 ug/L 1.0 0.29 1 01/18/20 23:48 156-59-2 1.2 ug/L 1.0 0.25 1 01/18/20 23:48 156-60-5 ND ug/L 1.0 0.19 1 01/18/20 23:48 78-87-5 ND ug/L 1.0 0.16 1 01/18/20 23:48 142-28-9 ND ug/L 1.0 0.27 1 01/18/20 23:48 594-20-7 ND ug/L 1.0 0.21 1 01/18/20 23:48 563-58-6 ND ug/L 1.0 0.30 1 01/18/20 23:48 10061-01-5 ND ug/L 1.0 0.31 1 01/18/20 23:48 10061-02-6 ND ug/L 1.0 0.22 1 01/18/20 23:48 108-20-3 ND ug/L 1.0 0.26 1 01/18/20 23:48 100-41-4 ND ug/L 1.0 0.44 1 01/18/20 23:48 87-68-3 ND ug/L 5.0 0.57 1 01/18/20 23:48 591-78-6 ND ug/L 1.0 0.21 1 01/18/20 23:48 99-87-6 ND ug/L 5.0 3.7 1 01/18/20 23:48 75-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 IL v2 v2 Page 10 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-113 Lab ID: 92461009002 Collected: 01/15/20 14:05 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 5.0 4.5 1 01/18/20 23:48 108-10-1 ND ug/L 1.0 0.28 1 01/18/20 23:48 1634-04-4 ND ug/L 1.0 0.35 1 01/18/20 23:48 91-20-3 ND ug/L 1.0 0.27 1 01/18/20 23:48 100-42-5 ND ug/L 1.0 0.34 1 01/18/20 23:48 630-20-6 ND ug/L 1.0 0.22 1 01/18/20 23:48 79-34-5 44.1 ug/L 1.0 0.16 1 01/18/20 23:48 127-18-4 ND ug/L 1.0 0.24 1 01/18/20 23:48 108-88-3 ND ug/L 1.0 0.34 1 01/18/20 23:48 87-61-6 0.39J ug/L 1.0 0.22 1 01/18/20 23:48 120-82-1 ND ug/L 1.0 0.18 1 01/18/20 23:48 71-55-6 ND ug/L 1.0 0.24 1 01/18/20 23:48 79-00-5 37.2 ug/L 1.0 0.22 1 01/18/20 23:48 79-01-6 ND ug/L 1.0 0.31 1 01/18/20 23:48 75-69-4 ND ug/L 1.0 0.35 1 01/18/20 23:48 96-18-4 ND ug/L 2.0 1.4 1 01/18/20 23:48 108-05-4 IK ND ug/L 1.0 0.24 1 01/18/20 23:48 75-01-4 v2 ND ug/L 1.0 0.63 1 01/18/20 23:48 1330-20-7 ND ug/L 2.0 0.41 1 01/18/20 23:48 179601-23-1 ND ug/L 1.0 0.22 1 01/18/20 23:48 95-47-6 100 % 70-130 1 01/18/20 23:48 460-00-4 95 % 70-130 1 01/18/20 23:48 17060-07-0 99 % 70-130 1 01/18/20 23:48 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 7.8 mg/L 1.0 0.60 1 01/18/20 03:11 16887-00-6 265 mg/L 5.0 2.5 5 01/18/2017:18 14808-79-8 Analytical Method: SM 531OB-2011 1.4 mg/L 1.0 0.50 1 01/20/20 23:12 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-2A Lab ID: 92461009003 Collected: 01/15/20 12:50 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:29 01/20/2014:29 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 39.3J ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:01 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 250 61.7 10 01/19/20 05:36 67-64-1 Benzene ND ug/L 10.0 1.5 10 01/19/20 05:36 71-43-2 Bromobenzene ND ug/L 10.0 2.2 10 01/19/20 05:36 108-86-1 Bromochloromethane ND ug/L 10.0 3.4 10 01/19/20 05:36 74-97-5 Bromodichloromethane ND ug/L 10.0 2.6 10 01/19/20 05:36 75-27-4 Bromoform ND ug/L 10.0 6.2 10 01/19/20 05:36 75-25-2 Bromomethane ND ug/L 20.0 6.2 10 01/19/20 05:36 74-83-9 IK 2-Butanone (MEK) ND ug/L 50.0 33.3 10 01/19/20 05:36 78-93-3 Carbon tetrachloride ND ug/L 10.0 2.2 10 01/19/20 05:36 56-23-5 Chlorobenzene ND ug/L 10.0 2.3 10 01/19/20 05:36 108-90-7 Chloroethane ND ug/L 10.0 4.9 10 01/19/20 05:36 75-00-3 v2 Chloroform ND ug/L 50.0 23.4 10 01/19/20 05:36 67-66-3 Chloromethane ND ug/L 10.0 3.9 10 01/19/20 05:36 74-87-3 v2 2-Chlorotoluene ND ug/L 10.0 2.0 10 01/19/20 05:36 95-49-8 4-Chlorotoluene ND ug/L 10.0 2.0 10 01/19/20 05:36 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 50.0 2.6 10 01/19/20 05:36 96-12-8 Dibromochloromethane ND ug/L 10.0 4.1 10 01/19/20 05:36 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 10.0 2.6 10 01/19/20 05:36 106-93-4 Dibromomethane ND ug/L 10.0 4.6 10 01/19/20 05:36 74-95-3 1,2-Dichlorobenzene ND ug/L 10.0 2.9 10 01/19/20 05:36 95-50-1 1,3-Dichlorobenzene ND ug/L 10.0 2.2 10 01/19/20 05:36 541-73-1 1,4-Dichlorobenzene ND ug/L 10.0 2.6 10 01/19/20 05:36 106-46-7 Dichlorodifluoromethane ND ug/L 10.0 2.3 10 01/19/20 05:36 75-71-8 1,1-Dichloroethane ND ug/L 10.0 2.7 10 01/19/20 05:36 75-34-3 1,2-Dichloroethane ND ug/L 10.0 3.4 10 01/19/20 05:36 107-06-2 1,1-Dichloroethene ND ug/L 10.0 2.4 10 01/19/20 05:36 75-35-4 cis-1,2-Dichloroethene 94.2 ug/L 10.0 2.9 10 01/19/20 05:36 156-59-2 trans-1,2-Dichloroethene ND ug/L 10.0 2.5 10 01/19/20 05:36 156-60-5 1,2-Dichloropropane ND ug/L 10.0 1.9 10 01/19/20 05:36 78-87-5 1,3-Dichloropropane ND ug/L 10.0 1.6 10 01/19/20 05:36 142-28-9 2,2-Dichloropropane ND ug/L 10.0 2.7 10 01/19/20 05:36 594-20-7 1,1-Dichloropropene ND ug/L 10.0 2.1 10 01/19/20 05:36 563-58-6 cis-1,3-Dichloropropene ND ug/L 10.0 3.0 10 01/19/20 05:36 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 10.0 3.1 10 01/19/20 05:36 10061-02-6 Diisopropyl ether ND ug/L 10.0 2.2 10 01/19/20 05:36 108-20-3 Ethylbenzene ND ug/L 10.0 2.6 10 01/19/20 05:36 100-41-4 Hexachloro-1,3-butadiene ND ug/L 10.0 4.4 10 01/19/20 05:36 87-68-3 2-Hexanone ND ug/L 50.0 5.7 10 01/19/20 05:36 591-78-6 p-Isopropyltoluene ND ug/L 10.0 2.1 10 01/19/20 05:36 99-87-6 Methylene Chloride ND ug/L 50.0 36.9 10 01/19/20 05:36 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-2A Lab ID: 92461009003 Collected: 01/15/20 12:50 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 50.0 45.3 10 01/19/20 05:36 108-10-1 ND ug/L 10.0 2.8 10 01/19/20 05:36 1634-04-4 ND ug/L 10.0 3.5 10 01/19/20 05:36 91-20-3 ND ug/L 10.0 2.7 10 01/19/20 05:36 100-42-5 ND ug/L 10.0 3.4 10 01/19/20 05:36 630-20-6 ND ug/L 10.0 2.2 10 01/19/20 05:36 79-34-5 1120 ug/L 10.0 1.6 10 01/19/20 05:36 127-18-4 ND ug/L 10.0 2.4 10 01/19/20 05:36 108-88-3 ND ug/L 10.0 3.4 10 01/19/20 05:36 87-61-6 ND ug/L 10.0 2.2 10 01/19/20 05:36 120-82-1 ND ug/L 10.0 1.8 10 01/19/20 05:36 71-55-6 ND ug/L 10.0 2.4 10 01/19/20 05:36 79-00-5 133 ug/L 10.0 2.2 10 01/19/20 05:36 79-01-6 ND ug/L 10.0 3.1 10 01/19/20 05:36 75-69-4 ND ug/L 10.0 3.5 10 01/19/20 05:36 96-18-4 ND ug/L 20.0 14.5 10 01/19/20 05:36 108-05-4 IK ND ug/L 10.0 2.4 10 01/19/20 05:36 75-01-4 v3 ND ug/L 10.0 6.3 10 01/19/20 05:36 1330-20-7 ND ug/L 20.0 4.1 10 01/19/20 05:36 179601-23-1 ND ug/L 10.0 2.2 10 01/19/20 05:36 95-47-6 99 % 70-130 10 01/19/20 05:36 460-00-4 89 % 70-130 10 01/19/20 05:36 17060-07-0 102 % 70-130 10 01/19/20 05:36 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 10 mg/L 1.0 0.60 1 01/18/20 04:06 16887-00-6 19.1 mg/L 1.0 0.50 1 01/18/20 04:06 14808-79-8 Analytical Method: SM 531OB-2011 1.6 mg/L 1.0 0.50 1 01/20/20 23:29 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-2B Lab ID: 92461009004 Collected: 01/15/20 12:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:32 01/20/2014:32 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 26.7J ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:04 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 125 30.8 5 01/19/20 05:18 67-64-1 Benzene ND ug/L 5.0 0.75 5 01/19/20 05:18 71-43-2 Bromobenzene ND ug/L 5.0 1.1 5 01/19/20 05:18 108-86-1 Bromochloromethane ND ug/L 5.0 1.7 5 01/19/20 05:18 74-97-5 Bromodichloromethane ND ug/L 5.0 1.3 5 01/19/20 05:18 75-27-4 Bromoform ND ug/L 5.0 3.1 5 01/19/20 05:18 75-25-2 Bromomethane ND ug/L 10.0 3.1 5 01/19/20 05:18 74-83-9 IK 2-Butanone (MEK) ND ug/L 25.0 16.6 5 01/19/20 05:18 78-93-3 Carbon tetrachloride ND ug/L 5.0 1.1 5 01/19/20 05:18 56-23-5 Chlorobenzene ND ug/L 5.0 1.2 5 01/19/20 05:18 108-90-7 Chloroethane ND ug/L 5.0 2.4 5 01/19/20 05:18 75-00-3 v2 Chloroform ND ug/L 25.0 11.7 5 01/19/20 05:18 67-66-3 Chloromethane ND ug/L 5.0 1.9 5 01/19/20 05:18 74-87-3 v2 2-Chlorotoluene ND ug/L 5.0 1.0 5 01/19/20 05:18 95-49-8 4-Chlorotoluene ND ug/L 5.0 1.0 5 01/19/20 05:18 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 25.0 1.3 5 01/19/20 05:18 96-12-8 Dibromochloromethane ND ug/L 5.0 2.1 5 01/19/20 05:18 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 1.3 5 01/19/20 05:18 106-93-4 Dibromomethane ND ug/L 5.0 2.3 5 01/19/20 05:18 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 1.5 5 01/19/20 05:18 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 1.1 5 01/19/20 05:18 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 1.3 5 01/19/20 05:18 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 1.1 5 01/19/20 05:18 75-71-8 1,1-Dichloroethane ND ug/L 5.0 1.3 5 01/19/20 05:18 75-34-3 1,2-Dichloroethane ND ug/L 5.0 1.7 5 01/19/20 05:18 107-06-2 1,1-Dichloroethene ND ug/L 5.0 1.2 5 01/19/20 05:18 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 1.5 5 01/19/20 05:18 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 1.3 5 01/19/20 05:18 156-60-5 1,2-Dichloropropane ND ug/L 5.0 0.94 5 01/19/20 05:18 78-87-5 1,3-Dichloropropane ND ug/L 5.0 0.79 5 01/19/20 05:18 142-28-9 2,2-Dichloropropane ND ug/L 5.0 1.4 5 01/19/20 05:18 594-20-7 1,1-Dichloropropene ND ug/L 5.0 1.1 5 01/19/20 05:18 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 1.5 5 01/19/20 05:18 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 5.0 1.5 5 01/19/20 05:18 10061-02-6 Diisopropyl ether ND ug/L 5.0 1.1 5 01/19/20 05:18 108-20-3 Ethylbenzene ND ug/L 5.0 1.3 5 01/19/20 05:18 100-41-4 Hexachloro-1,3-butadiene ND ug/L 5.0 2.2 5 01/19/20 05:18 87-68-3 2-Hexanone ND ug/L 25.0 2.8 5 01/19/20 05:18 591-78-6 p-Isopropyltoluene ND ug/L 5.0 1.1 5 01/19/20 05:18 99-87-6 Methylene Chloride ND ug/L 25.0 18.4 5 01/19/20 05:18 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-213 Lab ID: 92461009004 Collected: 01/15/20 12:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 22.6 5 01/19/20 05:18 108-10-1 ND ug/L 5.0 1.4 5 01/19/20 05:18 1634-04-4 ND ug/L 5.0 1.8 5 01/19/20 05:18 91-20-3 ND ug/L 5.0 1.3 5 01/19/20 05:18 100-42-5 ND ug/L 5.0 1.7 5 01/19/20 05:18 630-20-6 ND ug/L 5.0 1.1 5 01/19/20 05:18 79-34-5 891 ug/L 5.0 0.81 5 01/19/20 05:18 127-18-4 ND ug/L 5.0 1.2 5 01/19/20 05:18 108-88-3 ND ug/L 5.0 1.7 5 01/19/20 05:18 87-61-6 ND ug/L 5.0 1.1 5 01/19/20 05:18 120-82-1 ND ug/L 5.0 0.88 5 01/19/20 05:18 71-55-6 ND ug/L 5.0 1.2 5 01/19/20 05:18 79-00-5 14.3 ug/L 5.0 1.1 5 01/19/20 05:18 79-01-6 ND ug/L 5.0 1.6 5 01/19/20 05:18 75-69-4 ND ug/L 5.0 1.7 5 01/19/20 05:18 96-18-4 ND ug/L 10.0 7.2 5 01/19/20 05:18 108-05-4 IK ND ug/L 5.0 1.2 5 01/19/20 05:18 75-01-4 ND ug/L 5.0 3.2 5 01/19/20 05:18 1330-20-7 ND ug/L 10.0 2.0 5 01/19/20 05:18 179601-23-1 ND ug/L 5.0 1.1 5 01/19/20 05:18 95-47-6 98 % 70-130 5 01/19/20 05:18 460-00-4 89 % 70-130 5 01/19/20 05:18 17060-07-0 100 % 70-130 5 01/19/20 05:18 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 7.9 mg/L 1.0 0.60 1 01/18/20 04:20 16887-00-6 10 mg/L 1.0 0.50 1 01/18/20 04:20 14808-79-8 Analytical Method: SM 531OB-2011 ND mg/L 1.0 0.50 1 01/20/20 23:49 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-3A Lab ID: 92461009005 Collected: 01/15/20 13:30 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:34 01/20/2014:34 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 2010 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:07 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone 953J ug/L 1250 308 50 01/20/20 14:44 67-64-1 Benzene ND ug/L 50.0 7.5 50 01/20/20 14:44 71-43-2 Bromobenzene ND ug/L 50.0 11.0 50 01/20/20 14:44 108-86-1 Bromochloromethane ND ug/L 50.0 17.2 50 01/20/20 14:44 74-97-5 Bromodichloromethane ND ug/L 50.0 12.8 50 01/20/20 14:44 75-27-4 Bromoform ND ug/L 50.0 30.8 50 01/20/20 14:44 75-25-2 Bromomethane ND ug/L 100 31.0 50 01/20/20 14:44 74-83-9 IK 2-Butanone (MEK) ND ug/L 250 166 50 01/20/20 14:44 78-93-3 Carbon tetrachloride ND ug/L 50.0 11.2 50 01/20/20 14:44 56-23-5 Chlorobenzene ND ug/L 50.0 11.6 50 01/20/20 14:44 108-90-7 Chloroethane ND ug/L 50.0 24.5 50 01/20/20 14:44 75-00-3 v2 Chloroform ND ug/L 250 117 50 01/20/20 14:44 67-66-3 Chloromethane ND ug/L 50.0 19.4 50 01/20/20 14:44 74-87-3 v2 2-Chlorotoluene ND ug/L 50.0 10.2 50 01/20/20 14:44 95-49-8 4-Chlorotoluene ND ug/L 50.0 10.2 50 01/20/20 14:44 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 250 12.8 50 01/20/20 14:44 96-12-8 Dibromochloromethane ND ug/L 50.0 20.6 50 01/20/20 14:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 50.0 12.9 50 01/20/20 14:44 106-93-4 Dibromomethane ND ug/L 50.0 23.0 50 01/20/20 14:44 74-95-3 1,2-Dichlorobenzene ND ug/L 50.0 14.6 50 01/20/20 14:44 95-50-1 1,3-Dichlorobenzene ND ug/L 50.0 10.8 50 01/20/20 14:44 541-73-1 1,4-Dichlorobenzene ND ug/L 50.0 12.9 50 01/20/20 14:44 106-46-7 Dichlorodifluoromethane ND ug/L 50.0 11.3 50 01/20/20 14:44 75-71-8 1,1-Dichloroethane ND ug/L 50.0 13.4 50 01/20/20 14:44 75-34-3 1,2-Dichloroethane ND ug/L 50.0 16.8 50 01/20/20 14:44 107-06-2 1,1-Dichloroethene ND ug/L 50.0 12.2 50 01/20/20 14:44 75-35-4 cis-1,2-Dichloroethene 845 ug/L 50.0 14.6 50 01/20/20 14:44 156-59-2 trans-1,2-Dichloroethene 110 ug/L 50.0 12.7 50 01/20/20 14:44 156-60-5 1,2-Dichloropropane ND ug/L 50.0 9.4 50 01/20/20 14:44 78-87-5 1,3-Dichloropropane ND ug/L 50.0 7.9 50 01/20/20 14:44 142-28-9 2,2-Dichloropropane ND ug/L 50.0 13.5 50 01/20/20 14:44 594-20-7 1,1-Dichloropropene ND ug/L 50.0 10.6 50 01/20/20 14:44 563-58-6 cis-1,3-Dichloropropene ND ug/L 50.0 14.8 50 01/20/20 14:44 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 50.0 15.4 50 01/20/20 14:44 10061-02-6 Diisopropyl ether ND ug/L 50.0 10.9 50 01/20/20 14:44 108-20-3 Ethylbenzene ND ug/L 50.0 12.8 50 01/20/20 14:44 100-41-4 Hexachloro-1,3-butadiene ND ug/L 50.0 21.9 50 01/20/20 14:44 87-68-3 2-Hexanone ND ug/L 250 28.4 50 01/20/20 14:44 591-78-6 p-Isopropyltoluene ND ug/L 50.0 10.6 50 01/20/20 14:44 99-87-6 Methylene Chloride ND ug/L 250 184 50 01/20/20 14:44 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-3A Lab ID: 92461009005 Collected: 01/15/20 13:30 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D 4-Methyl-2-pentanone (MIBK) ND ug/L 250 226 50 01/20/20 14:44 108-10-1 Methyl-tert-butyl ether ND ug/L 50.0 13.8 50 01/20/20 14:44 1634-04-4 Naphthalene ND ug/L 50.0 17.6 50 01/20/20 14:44 91-20-3 Styrene ND ug/L 50.0 13.4 50 01/20/20 14:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 50.0 17.0 50 01/20/20 14:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 50.0 11.1 50 01/20/20 14:44 79-34-5 Tetrachloroethene 3870 ug/L 50.0 8.1 50 01/20/20 14:44 127-18-4 Toluene ND ug/L 50.0 12.2 50 01/20/20 14:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 50.0 17.2 50 01/20/20 14:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 50.0 10.9 50 01/20/20 14:44 120-82-1 1,1,1-Trichloroethane ND ug/L 50.0 8.8 50 01/20/20 14:44 71-55-6 1,1,2-Trichloroethane ND ug/L 50.0 11.8 50 01/20/20 14:44 79-00-5 Trichloroethene 363 ug/L 50.0 11.0 50 01/20/20 14:44 79-01-6 Trichlorofluoromethane ND ug/L 50.0 15.6 50 01/20/20 14:44 75-69-4 1,2,3-Trichloropropane ND ug/L 50.0 17.4 50 01/20/20 14:44 96-18-4 Vinyl acetate ND ug/L 100 72.5 50 01/20/20 14:44 108-05-4 IK Vinyl chloride ND ug/L 50.0 12.1 50 01/20/20 14:44 75-01-4 Xylene (Total) ND ug/L 50.0 31.5 50 01/20/20 14:44 1330-20-7 m&p-Xylene ND ug/L 100 20.5 50 01/20/20 14:44 179601-23-1 o-Xylene ND ug/L 50.0 11.0 50 01/20/20 14:44 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 50 01/20/20 14:44 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 50 01/20/20 14:44 17060-07-0 Toluene-d8 (S) 101 % 70-130 50 01/20/20 14:44 2037-26-5 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Chloride 15.8 mg/L 1.0 0.60 1 01/18/20 04:34 16887-00-6 Sulfate 232 mg/L 5.0 2.5 5 01/18/2017:33 14808-79-8 531013 TOC Analytical Method: SM 531 OB-2011 Total Organic Carbon 3.3 mg/L 1.0 0.50 1 01/21/20 00:04 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-4A Lab ID: 92461009006 Collected: 01/15/20 15:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Ethene 6010 MET ICP Iron 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride Date: 01/23/2020 03:52 PM Analytical Method: RSK-175 Preparation Method: RSK175 ND ug/L 13.0 4.26 1 01/20/2014:37 01/20/2014:37 74-85-1 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A 242 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:10 7439-89-6 Analytical Method: EPA 8260D ND ug/L 50.0 12.3 2 01/20/2012:56 67-64-1 ND ug/L 2.0 0.30 2 01 /20/20 12:56 71-43-2 ND ug/L 2.0 0.44 2 01/20/2012:56 108-86-1 ND ug/L 2.0 0.69 2 01/20/2012:56 74-97-5 ND ug/L 2.0 0.51 2 01/20/2012:56 75-27-4 ND ug/L 2.0 1.2 2 01/20/2012:56 75-25-2 ND ug/L 4.0 1.2 2 01/20/2012:56 74-83-9 ND ug/L 10.0 6.7 2 01/20/2012:56 78-93-3 ND ug/L 2.0 0.45 2 01/20/2012:56 56-23-5 ND ug/L 2.0 0.47 2 01/20/2012:56 108-90-7 ND ug/L 2.0 0.98 2 01/20/2012:56 75-00-3 ND ug/L 10.0 4.7 2 01/20/2012:56 67-66-3 ND ug/L 2.0 0.78 2 01/20/2012:56 74-87-3 ND ug/L 2.0 0.41 2 01/20/2012:56 95-49-8 ND ug/L 2.0 0.41 2 01/20/2012:56 106-43-4 ND ug/L 10.0 0.51 2 01/20/2012:56 96-12-8 ND ug/L 2.0 0.83 2 01/20/2012:56 124-48-1 ND ug/L 2.0 0.52 2 01/20/2012:56 106-93-4 ND ug/L 2.0 0.92 2 01/20/2012:56 74-95-3 ND ug/L 2.0 0.58 2 01/20/2012:56 95-50-1 ND ug/L 2.0 0.43 2 01/20/2012:56 541-73-1 ND ug/L 2.0 0.52 2 01/20/2012:56 106-46-7 ND ug/L 2.0 0.45 2 01 /20/20 12:56 75-71-8 1.91 ug/L 2.0 0.54 2 01/20/2012:56 75-34-3 ND ug/L 2.0 0.67 2 01/20/2012:56 107-06-2 ND ug/L 2.0 0.49 2 01/20/2012:56 75-35-4 95.9 ug/L 2.0 0.58 2 01/20/2012:56 156-59-2 2.3 ug/L 2.0 0.51 2 01/20/2012:56 156-60-5 ND ug/L 2.0 0.37 2 01/20/2012:56 78-87-5 ND ug/L 2.0 0.32 2 01/20/2012:56 142-28-9 ND ug/L 2.0 0.54 2 01/20/2012:56 594-20-7 ND ug/L 2.0 0.43 2 01/20/2012:56 563-58-6 ND ug/L 2.0 0.59 2 01 /20/20 12:56 10061-01-5 ND ug/L 2.0 0.62 2 01 /20/20 12:56 10061-02-6 ND ug/L 2.0 0.44 2 01/20/2012:56 108-20-3 ND ug/L 2.0 0.51 2 01 /20/20 12:56 100-41-4 ND ug/L 2.0 0.88 2 01/20/2012:56 87-68-3 ND ug/L 10.0 1.1 2 01 /20/20 12:56 591-78-6 ND ug/L 2.0 0.42 2 01/20/2012:56 99-87-6 ND ug/L 10.0 7.4 2 01/20/2012:56 75-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 Page 18 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-4A Lab ID: 92461009006 Collected: 01/15/20 15:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 10.0 9.1 2 01/20/2012:56 108-10-1 ND ug/L 2.0 0.55 2 01/20/2012:56 1634-04-4 ND ug/L 2.0 0.70 2 01 /20/20 12:56 91-20-3 ND ug/L 2.0 0.53 2 01/20/2012:56 100-42-5 ND ug/L 2.0 0.68 2 01/20/2012:56 630-20-6 10.6 ug/L 2.0 0.44 2 01/20/2012:56 79-34-5 84.3 ug/L 2.0 0.32 2 01/20/2012:56 127-18-4 ND ug/L 2.0 0.49 2 01/20/2012:56 108-88-3 ND ug/L 2.0 0.69 2 01 /20/20 12:56 87-61-6 ND ug/L 2.0 0.44 2 01/20/2012:56 120-82-1 21.4 ug/L 2.0 0.35 2 01/20/2012:56 71-55-6 ND ug/L 2.0 0.47 2 01/20/2012:56 79-00-5 233 ug/L 2.0 0.44 2 01/20/2012:56 79-01-6 ND ug/L 2.0 0.62 2 01/20/2012:56 75-69-4 ND ug/L 2.0 0.69 2 01/20/2012:56 96-18-4 ND ug/L 4.0 2.9 2 01/20/2012:56 108-05-4 IK ND ug/L 2.0 0.48 2 01 /20/20 12:56 75-01-4 ND ug/L 2.0 1.3 2 01/20/2012:56 1330-20-7 ND ug/L 4.0 0.82 2 01/20/2012:56 179601-23-1 ND ug/L 2.0 0.44 2 01/20/2012:56 95-47-6 99 % 70-130 2 01/20/2012:56 460-00-4 92 % 70-130 2 01/20/2012:56 17060-07-0 101 % 70-130 2 01/20/2012:56 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 6.2 mg/L 1.0 0.60 1 01/18/20 04:48 16887-00-6 120 mg/L 2.0 1.0 2 01/18/2017:49 14808-79-8 Analytical Method: SM 531OB-2011 1.5 mg/L 1.0 0.50 1 01/21/20 00:56 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 19 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-5A Lab ID: 92461009007 Collected: 01/14/20 16:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:39 01/20/2014:39 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 449 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:13 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone 19600J ug/L 25000 6170 1000 01/20/20 15:37 67-64-1 Benzene ND ug/L 1000 150 1000 01/20/20 15:37 71-43-2 Bromobenzene ND ug/L 1000 220 1000 01/20/20 15:37 108-86-1 Bromochloromethane ND ug/L 1000 343 1000 01/20/20 15:37 74-97-5 Bromodichloromethane ND ug/L 1000 256 1000 01/20/20 15:37 75-27-4 Bromoform ND ug/L 1000 617 1000 01/20/20 15:37 75-25-2 Bromomethane ND ug/L 2000 620 1000 01/20/20 15:37 74-83-9 IK 2-Butanone (MEK) ND ug/L 5000 3330 1000 01/20/20 15:37 78-93-3 Carbon tetrachloride ND ug/L 1000 224 1000 01/20/20 15:37 56-23-5 Chlorobenzene ND ug/L 1000 233 1000 01/20/20 15:37 108-90-7 Chloroethane ND ug/L 1000 490 1000 01/20/20 15:37 75-00-3 v2 Chloroform ND ug/L 5000 2340 1000 01/20/20 15:37 67-66-3 Chloromethane ND ug/L 1000 389 1000 01/20/20 15:37 74-87-3 v2 2-Chlorotoluene ND ug/L 1000 203 1000 01/20/20 15:37 95-49-8 4-Chlorotoluene ND ug/L 1000 204 1000 01/20/20 15:37 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5000 257 1000 01/20/20 15:37 96-12-8 Dibromochloromethane ND ug/L 1000 413 1000 01/20/20 15:37 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1000 258 1000 01/20/20 15:37 106-93-4 Dibromomethane ND ug/L 1000 459 1000 01/20/20 15:37 74-95-3 1,2-Dichlorobenzene ND ug/L 1000 291 1000 01/20/20 15:37 95-50-1 1,3-Dichlorobenzene ND ug/L 1000 217 1000 01/20/20 15:37 541-73-1 1,4-Dichlorobenzene ND ug/L 1000 258 1000 01/20/20 15:37 106-46-7 Dichlorodifluoromethane ND ug/L 1000 226 1000 01/20/20 15:37 75-71-8 1,1-Dichloroethane ND ug/L 1000 268 1000 01/20/20 15:37 75-34-3 1,2-Dichloroethane ND ug/L 1000 336 1000 01/20/20 15:37 107-06-2 1,1-Dichloroethene ND ug/L 1000 245 1000 01/20/20 15:37 75-35-4 cis-1,2-Dichloroethene 1400 ug/L 1000 291 1000 01/20/20 15:37 156-59-2 trans-1,2-Dichloroethene ND ug/L 1000 254 1000 01/20/20 15:37 156-60-5 1,2-Dichloropropane ND ug/L 1000 187 1000 01/20/20 15:37 78-87-5 1,3-Dichloropropane ND ug/L 1000 158 1000 01/20/20 15:37 142-28-9 2,2-Dichloropropane ND ug/L 1000 270 1000 01/20/20 15:37 594-20-7 1,1-Dichloropropene ND ug/L 1000 213 1000 01/20/20 15:37 563-58-6 cis-1,3-Dichloropropene ND ug/L 1000 296 1000 01/20/20 15:37 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1000 309 1000 01/20/20 15:37 10061-02-6 Diisopropyl ether ND ug/L 1000 218 1000 01/20/20 15:37 108-20-3 Ethylbenzene ND ug/L 1000 256 1000 01/20/20 15:37 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1000 438 1000 01/20/20 15:37 87-68-3 2-Hexanone ND ug/L 5000 568 1000 01/20/20 15:37 591-78-6 p-Isopropyltoluene ND ug/L 1000 212 1000 01/20/20 15:37 99-87-6 Methylene Chloride ND ug/L 5000 3690 1000 01/20/20 15:37 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-5A Lab ID: 92461009007 Collected: 01/14/20 16:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 5000 4530 1000 01/20/2015:37 108-10-1 ND ug/L 1000 275 1000 01/20/2015:37 1634-04-4 ND ug/L 1000 352 1000 01 /20/20 15:37 91-20-3 ND ug/L 1000 267 1000 01/20/2015:37 100-42-5 ND ug/L 1000 340 1000 01/20/2015:37 630-20-6 ND ug/L 1000 222 1000 01/20/2015:37 79-34-5 10900 ug/L 1000 162 1000 01/20/2015:37 127-18-4 ND ug/L 1000 244 1000 01/20/2015:37 108-88-3 ND ug/L 1000 344 1000 01 /20/20 15:37 87-61-6 ND ug/L 1000 218 1000 01/20/2015:37 120-82-1 6710 ug/L 1000 175 1000 01/20/2015:37 71-55-6 ND ug/L 1000 236 1000 01/20/2015:37 79-00-5 93600 ug/L 1000 220 1000 01/20/2015:37 79-01-6 ND ug/L 1000 311 1000 01/20/2015:37 75-69-4 ND ug/L 1000 347 1000 01/20/2015:37 96-18-4 ND ug/L 2000 1450 1000 01/20/2015:37 108-05-4 IK ND ug/L 1000 242 1000 01 /20/20 15:37 75-01-4 ND ug/L 1000 630 1000 01/20/2015:37 1330-20-7 ND ug/L 2000 410 1000 01/20/2015:37 179601-23-1 ND ug/L 1000 220 1000 01/20/2015:37 95-47-6 99 % 70-130 1000 01/20/2015:37 460-00-4 93 % 70-130 1000 01/20/2015:37 17060-07-0 104 % 70-130 1000 01/20/2015:37 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 67.6 mg/L 1.0 0.60 1 01/18/20 05:02 16887-00-6 527 mg/L 10.0 5.0 10 01/18/2018:03 14808-79-8 Analytical Method: SM 531OB-2011 9.0 mg/L 1.0 0.50 1 01/21/20 01:15 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-6A Lab ID: 92461009008 Collected: 01/14/20 15:30 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:41 01/20/2014:41 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 663 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:22 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 12500 3080 500 01/19/20 04:24 67-64-1 Benzene ND ug/L 500 75.0 500 01/19/20 04:24 71-43-2 Bromobenzene ND ug/L 500 110 500 01/19/20 04:24 108-86-1 Bromochloromethane ND ug/L 500 172 500 01/19/20 04:24 74-97-5 Bromodichloromethane ND ug/L 500 128 500 01/19/20 04:24 75-27-4 Bromoform ND ug/L 500 308 500 01/19/20 04:24 75-25-2 Bromomethane ND ug/L 1000 310 500 01/19/20 04:24 74-83-9 IK 2-Butanone (MEK) ND ug/L 2500 1660 500 01/19/20 04:24 78-93-3 Carbon tetrachloride ND ug/L 500 112 500 01/19/20 04:24 56-23-5 Chlorobenzene ND ug/L 500 116 500 01/19/20 04:24 108-90-7 Chloroethane ND ug/L 500 245 500 01/19/20 04:24 75-00-3 v2,v3 Chloroform ND ug/L 2500 1170 500 01/19/20 04:24 67-66-3 Chloromethane ND ug/L 500 194 500 01/19/20 04:24 74-87-3 v2,v3 2-Chlorotoluene ND ug/L 500 102 500 01/19/20 04:24 95-49-8 4-Chlorotoluene ND ug/L 500 102 500 01/19/20 04:24 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2500 128 500 01/19/20 04:24 96-12-8 Dibromochloromethane ND ug/L 500 206 500 01/19/20 04:24 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 500 129 500 01/19/20 04:24 106-93-4 Dibromomethane ND ug/L 500 230 500 01/19/20 04:24 74-95-3 1,2-Dichlorobenzene ND ug/L 500 146 500 01/19/20 04:24 95-50-1 1,3-Dichlorobenzene ND ug/L 500 108 500 01/19/20 04:24 541-73-1 1,4-Dichlorobenzene ND ug/L 500 129 500 01/19/20 04:24 106-46-7 Dichlorodifluoromethane ND ug/L 500 113 500 01/19/20 04:24 75-71-8 1,1-Dichloroethane ND ug/L 500 134 500 01/19/20 04:24 75-34-3 1,2-Dichloroethane ND ug/L 500 168 500 01/19/20 04:24 107-06-2 1,1-Dichloroethene ND ug/L 500 122 500 01/19/20 04:24 75-35-4 cis-1,2-Dichloroethene 2610 ug/L 500 146 500 01/19/20 04:24 156-59-2 trans-1,2-Dichloroethene 398J ug/L 500 127 500 01/19/20 04:24 156-60-5 1,2-Dichloropropane ND ug/L 500 93.5 500 01/19/20 04:24 78-87-5 1,3-Dichloropropane ND ug/L 500 79.0 500 01/19/20 04:24 142-28-9 2,2-Dichloropropane ND ug/L 500 135 500 01/19/20 04:24 594-20-7 1,1-Dichloropropene ND ug/L 500 106 500 01/19/20 04:24 563-58-6 cis-1,3-Dichloropropene ND ug/L 500 148 500 01/19/20 04:24 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 500 154 500 01/19/20 04:24 10061-02-6 Diisopropyl ether ND ug/L 500 109 500 01/19/20 04:24 108-20-3 Ethylbenzene ND ug/L 500 128 500 01/19/20 04:24 100-41-4 Hexachloro-1,3-butadiene ND ug/L 500 219 500 01/19/20 04:24 87-68-3 2-Hexanone ND ug/L 2500 284 500 01/19/20 04:24 591-78-6 p-Isopropyltoluene ND ug/L 500 106 500 01/19/20 04:24 99-87-6 Methylene Chloride ND ug/L 2500 1840 500 01/19/20 04:24 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 22 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-6A Lab ID: 92461009008 Collected: 01/14/20 15:30 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 2500 2260 500 01/19/20 04:24 108-10-1 ND ug/L 500 138 500 01/19/20 04:24 1634-04-4 ND ug/L 500 176 500 01/19/20 04:24 91-20-3 ND ug/L 500 134 500 01/19/20 04:24 100-42-5 ND ug/L 500 170 500 01/19/20 04:24 630-20-6 ND ug/L 500 111 500 01/19/20 04:24 79-34-5 29900 ug/L 500 81.0 500 01/19/20 04:24 127-18-4 ND ug/L 500 122 500 01/19/20 04:24 108-88-3 ND ug/L 500 172 500 01/19/20 04:24 87-61-6 ND ug/L 500 109 500 01/19/20 04:24 120-82-1 820 ug/L 500 87.5 500 01/19/20 04:24 71-55-6 ND ug/L 500 118 500 01/19/20 04:24 79-00-5 49700 ug/L 500 110 500 01/19/20 04:24 79-01-6 ND ug/L 500 156 500 01/19/20 04:24 75-69-4 ND ug/L 500 174 500 01/19/20 04:24 96-18-4 ND ug/L 1000 725 500 01/19/20 04:24 108-05-4 ND ug/L 500 121 500 01/19/20 04:24 75-01-4 ND ug/L 500 315 500 01/19/20 04:24 1330-20-7 ND ug/L 1000 205 500 01/19/20 04:24 179601-23-1 ND ug/L 500 110 500 01/19/20 04:24 95-47-6 100 % 70-130 500 01/19/20 04:24 460-00-4 93 % 70-130 500 01/19/20 04:24 17060-07-0 101 % 70-130 500 01/19/20 04:24 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 58.7 mg/L 1.0 0.60 1 01/18/20 05:16 16887-00-6 541 mg/L 11.0 5.5 11 01/18/2018:17 14808-79-8 Analytical Method: SM 531OB-2011 8.2 mg/L 1.0 0.50 1 01/21/20 01:31 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. M1 IK Page 23 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-7A Lab ID: 92461009009 Collected: 01/14/20 14:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:44 01/20/2014:44 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 1030 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:25 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone 351J ug/L 500 123 20 01/20/20 13:50 67-64-1 Benzene 6.7J ug/L 20.0 3.0 20 01/20/20 13:50 71-43-2 Bromobenzene ND ug/L 20.0 4.4 20 01/20/20 13:50 108-86-1 Bromochloromethane ND ug/L 20.0 6.9 20 01/20/20 13:50 74-97-5 Bromodichloromethane ND ug/L 20.0 5.1 20 01/20/20 13:50 75-27-4 Bromoform ND ug/L 20.0 12.3 20 01/20/20 13:50 75-25-2 Bromomethane ND ug/L 40.0 12.4 20 01/20/20 13:50 74-83-9 IK 2-Butanone (MEK) ND ug/L 100 66.6 20 01/20/20 13:50 78-93-3 Carbon tetrachloride ND ug/L 20.0 4.5 20 01/20/20 13:50 56-23-5 Chlorobenzene ND ug/L 20.0 4.7 20 01/20/20 13:50 108-90-7 Chloroethane ND ug/L 20.0 9.8 20 01/20/20 13:50 75-00-3 v2 Chloroform ND ug/L 100 46.8 20 01/20/20 13:50 67-66-3 Chloromethane ND ug/L 20.0 7.8 20 01/20/20 13:50 74-87-3 v2 2-Chlorotoluene ND ug/L 20.0 4.1 20 01/20/20 13:50 95-49-8 4-Chlorotoluene ND ug/L 20.0 4.1 20 01/20/20 13:50 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 100 5.1 20 01/20/20 13:50 96-12-8 Dibromochloromethane ND ug/L 20.0 8.3 20 01/20/20 13:50 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 20.0 5.2 20 01/20/20 13:50 106-93-4 Dibromomethane ND ug/L 20.0 9.2 20 01/20/20 13:50 74-95-3 1,2-Dichlorobenzene ND ug/L 20.0 5.8 20 01/20/20 13:50 95-50-1 1,3-Dichlorobenzene ND ug/L 20.0 4.3 20 01/20/20 13:50 541-73-1 1,4-Dichlorobenzene ND ug/L 20.0 5.2 20 01/20/20 13:50 106-46-7 Dichlorodifluoromethane ND ug/L 20.0 4.5 20 01/20/20 13:50 75-71-8 1,1-Dichloroethane ND ug/L 20.0 5.4 20 01/20/20 13:50 75-34-3 1,2-Dichloroethane ND ug/L 20.0 6.7 20 01/20/20 13:50 107-06-2 1,1-Dichloroethene ND ug/L 20.0 4.9 20 01/20/20 13:50 75-35-4 cis-1,2-Dichloroethene 357 ug/L 20.0 5.8 20 01/20/20 13:50 156-59-2 trans-1,2-Dichloroethene ND ug/L 20.0 5.1 20 01/20/20 13:50 156-60-5 1,2-Dichloropropane ND ug/L 20.0 3.7 20 01/20/20 13:50 78-87-5 1,3-Dichloropropane ND ug/L 20.0 3.2 20 01/20/20 13:50 142-28-9 2,2-Dichloropropane ND ug/L 20.0 5.4 20 01/20/20 13:50 594-20-7 1,1-Dichloropropene ND ug/L 20.0 4.3 20 01/20/20 13:50 563-58-6 cis-1,3-Dichloropropene ND ug/L 20.0 5.9 20 01/20/20 13:50 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 20.0 6.2 20 01/20/20 13:50 10061-02-6 Diisopropyl ether ND ug/L 20.0 4.4 20 01/20/20 13:50 108-20-3 Ethylbenzene ND ug/L 20.0 5.1 20 01/20/20 13:50 100-41-4 Hexachloro-1,3-butadiene ND ug/L 20.0 8.8 20 01/20/20 13:50 87-68-3 2-Hexanone ND ug/L 100 11.4 20 01/20/20 13:50 591-78-6 p-Isopropyltoluene ND ug/L 20.0 4.2 20 01/20/20 13:50 99-87-6 Methylene Chloride ND ug/L 100 73.8 20 01/20/20 13:50 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 24 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-7A Lab ID: 92461009009 Collected: 01/14/20 14:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D 4-Methyl-2-pentanone (MIBK) ND ug/L 100 90.6 20 01/20/20 13:50 108-10-1 Methyl-tert-butyl ether ND ug/L 20.0 5.5 20 01/20/20 13:50 1634-04-4 Naphthalene ND ug/L 20.0 7.0 20 01/20/20 13:50 91-20-3 Styrene ND ug/L 20.0 5.3 20 01/20/20 13:50 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 20.0 6.8 20 01/20/20 13:50 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 20.0 4.4 20 01/20/20 13:50 79-34-5 Tetrachloroethene 634 ug/L 20.0 3.2 20 01/20/20 13:50 127-18-4 Toluene ND ug/L 20.0 4.9 20 01/20/20 13:50 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 6.9 20 01/20/20 13:50 87-61-6 1,2,4-Trichlorobenzene ND ug/L 20.0 4.4 20 01/20/20 13:50 120-82-1 1,1,1-Trichloroethane ND ug/L 20.0 3.5 20 01/20/20 13:50 71-55-6 1,1,2-Trichloroethane ND ug/L 20.0 4.7 20 01/20/20 13:50 79-00-5 Trichloroethene 1670 ug/L 20.0 4.4 20 01/20/20 13:50 79-01-6 Trichlorofluoromethane ND ug/L 20.0 6.2 20 01/20/20 13:50 75-69-4 1,2,3-Trichloropropane ND ug/L 20.0 6.9 20 01/20/20 13:50 96-18-4 Vinyl acetate ND ug/L 40.0 29.0 20 01/20/20 13:50 108-05-4 IK Vinyl chloride ND ug/L 20.0 4.8 20 01/20/20 13:50 75-01-4 Xylene (Total) ND ug/L 20.0 12.6 20 01/20/20 13:50 1330-20-7 m&p-Xylene ND ug/L 40.0 8.2 20 01/20/20 13:50 179601-23-1 o-Xylene ND ug/L 20.0 4.4 20 01/20/20 13:50 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 20 01/20/20 13:50 460-00-4 1,2-Dichloroethane-d4 (S) 94 % 70-130 20 01/20/20 13:50 17060-07-0 Toluene-d8 (S) 102 % 70-130 20 01/20/20 13:50 2037-26-5 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Chloride 15.0 mg/L 1.0 0.60 1 01/18/20 05:30 16887-00-6 Sulfate 15.8 mg/L 1.0 0.50 1 01/18/20 05:30 14808-79-8 531013 TOC Analytical Method: SM 531 OB-2011 Total Organic Carbon 0.69J mg/L 1.0 0.50 1 01/21/20 01:48 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-7B Lab ID: 92461009010 Collected: 01/14/20 14:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:51 01/20/2014:51 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 725 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:28 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone 464J ug/L 625 154 25 01/20/20 14:26 67-64-1 Benzene ND ug/L 25.0 3.8 25 01/20/20 14:26 71-43-2 Bromobenzene ND ug/L 25.0 5.5 25 01/20/20 14:26 108-86-1 Bromochloromethane ND ug/L 25.0 8.6 25 01/20/20 14:26 74-97-5 Bromodichloromethane ND ug/L 25.0 6.4 25 01/20/20 14:26 75-27-4 Bromoform ND ug/L 25.0 15.4 25 01/20/20 14:26 75-25-2 Bromomethane ND ug/L 50.0 15.5 25 01/20/20 14:26 74-83-9 IK 2-Butanone (MEK) ND ug/L 125 83.2 25 01/20/20 14:26 78-93-3 Carbon tetrachloride ND ug/L 25.0 5.6 25 01/20/20 14:26 56-23-5 Chlorobenzene ND ug/L 25.0 5.8 25 01/20/20 14:26 108-90-7 Chloroethane ND ug/L 25.0 12.2 25 01/20/20 14:26 75-00-3 v2 Chloroform ND ug/L 125 58.5 25 01/20/20 14:26 67-66-3 Chloromethane ND ug/L 25.0 9.7 25 01/20/20 14:26 74-87-3 v2 2-Chlorotoluene ND ug/L 25.0 5.1 25 01/20/20 14:26 95-49-8 4-Chlorotoluene ND ug/L 25.0 5.1 25 01/20/20 14:26 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 125 6.4 25 01/20/20 14:26 96-12-8 Dibromochloromethane ND ug/L 25.0 10.3 25 01/20/20 14:26 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 25.0 6.4 25 01/20/20 14:26 106-93-4 Dibromomethane ND ug/L 25.0 11.5 25 01/20/20 14:26 74-95-3 1,2-Dichlorobenzene ND ug/L 25.0 7.3 25 01/20/20 14:26 95-50-1 1,3-Dichlorobenzene ND ug/L 25.0 5.4 25 01/20/20 14:26 541-73-1 1,4-Dichlorobenzene ND ug/L 25.0 6.4 25 01/20/20 14:26 106-46-7 Dichlorodifluoromethane ND ug/L 25.0 5.6 25 01/20/20 14:26 75-71-8 1,1-Dichloroethane ND ug/L 25.0 6.7 25 01/20/20 14:26 75-34-3 1,2-Dichloroethane ND ug/L 25.0 8.4 25 01/20/20 14:26 107-06-2 1,1-Dichloroethene ND ug/L 25.0 6.1 25 01/20/20 14:26 75-35-4 cis-1,2-Dichloroethene 34.2 ug/L 25.0 7.3 25 01/20/20 14:26 156-59-2 trans-1,2-Dichloroethene ND ug/L 25.0 6.4 25 01/20/20 14:26 156-60-5 1,2-Dichloropropane ND ug/L 25.0 4.7 25 01/20/20 14:26 78-87-5 1,3-Dichloropropane ND ug/L 25.0 4.0 25 01/20/20 14:26 142-28-9 2,2-Dichloropropane ND ug/L 25.0 6.8 25 01/20/20 14:26 594-20-7 1,1-Dichloropropene ND ug/L 25.0 5.3 25 01/20/20 14:26 563-58-6 cis-1,3-Dichloropropene ND ug/L 25.0 7.4 25 01/20/20 14:26 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 25.0 7.7 25 01/20/20 14:26 10061-02-6 Diisopropyl ether ND ug/L 25.0 5.4 25 01/20/20 14:26 108-20-3 Ethylbenzene ND ug/L 25.0 6.4 25 01/20/20 14:26 100-41-4 Hexachloro-1,3-butadiene ND ug/L 25.0 11.0 25 01/20/20 14:26 87-68-3 2-Hexanone ND ug/L 125 14.2 25 01/20/20 14:26 591-78-6 p-Isopropyltoluene ND ug/L 25.0 5.3 25 01/20/20 14:26 99-87-6 Methylene Chloride ND ug/L 125 92.2 25 01/20/20 14:26 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 26 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-713 Lab ID: 92461009010 Collected: 01/14/20 14:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D 4-Methyl-2-pentanone (MIBK) ND ug/L 125 113 25 01/20/20 14:26 108-10-1 Methyl-tert-butyl ether ND ug/L 25.0 6.9 25 01/20/20 14:26 1634-04-4 Naphthalene ND ug/L 25.0 8.8 25 01/20/20 14:26 91-20-3 Styrene ND ug/L 25.0 6.7 25 01/20/20 14:26 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 25.0 8.5 25 01/20/20 14:26 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 25.0 5.6 25 01/20/20 14:26 79-34-5 Tetrachloroethene 1290 ug/L 25.0 4.0 25 01/20/20 14:26 127-18-4 Toluene ND ug/L 25.0 6.1 25 01/20/20 14:26 108-88-3 1,2,3-Trichlorobenzene ND ug/L 25.0 8.6 25 01/20/20 14:26 87-61-6 1,2,4-Trichlorobenzene ND ug/L 25.0 5.4 25 01/20/20 14:26 120-82-1 1,1,1-Trichloroethane ND ug/L 25.0 4.4 25 01/20/20 14:26 71-55-6 1,1,2-Trichloroethane ND ug/L 25.0 5.9 25 01/20/20 14:26 79-00-5 Trichloroethene 2130 ug/L 25.0 5.5 25 01/20/20 14:26 79-01-6 Trichlorofluoromethane ND ug/L 25.0 7.8 25 01/20/20 14:26 75-69-4 1,2,3-Trichloropropane ND ug/L 25.0 8.7 25 01/20/20 14:26 96-18-4 Vinyl acetate ND ug/L 50.0 36.2 25 01/20/20 14:26 108-05-4 IK Vinyl chloride ND ug/L 25.0 6.0 25 01/20/20 14:26 75-01-4 Xylene (Total) ND ug/L 25.0 15.8 25 01/20/20 14:26 1330-20-7 m&p-Xylene ND ug/L 50.0 10.2 25 01/20/20 14:26 179601-23-1 o-Xylene ND ug/L 25.0 5.5 25 01/20/20 14:26 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 25 01/20/20 14:26 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 25 01/20/20 14:26 17060-07-0 Toluene-d8 (S) 102 % 70-130 25 01/20/20 14:26 2037-26-5 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Chloride 3.0 mg/L 1.0 0.60 1 01/18/20 06:12 16887-00-6 M1 Sulfate 5.8 mg/L 1.0 0.50 1 01/18/20 06:12 14808-79-8 M1 531013 TOC Analytical Method: SM 531 OB-2011 Total Organic Carbon 3.6 mg/L 1.0 0.50 1 01/21/20 02:06 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-8A Lab ID: 92461009011 Collected: 01/14/20 09:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2014:58 01/20/2014:58 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 646 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:31 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 125 30.8 5 01/19/20 03:49 67-64-1 Benzene ND ug/L 5.0 0.75 5 01/19/20 03:49 71-43-2 Bromobenzene ND ug/L 5.0 1.1 5 01/19/20 03:49 108-86-1 Bromochloromethane ND ug/L 5.0 1.7 5 01/19/20 03:49 74-97-5 Bromodichloromethane ND ug/L 5.0 1.3 5 01/19/20 03:49 75-27-4 Bromoform ND ug/L 5.0 3.1 5 01/19/20 03:49 75-25-2 Bromomethane ND ug/L 10.0 3.1 5 01/19/20 03:49 74-83-9 IK 2-Butanone (MEK) ND ug/L 25.0 16.6 5 01/19/20 03:49 78-93-3 Carbon tetrachloride ND ug/L 5.0 1.1 5 01/19/20 03:49 56-23-5 Chlorobenzene ND ug/L 5.0 1.2 5 01/19/20 03:49 108-90-7 Chloroethane ND ug/L 5.0 2.4 5 01/19/20 03:49 75-00-3 v2 Chloroform ND ug/L 25.0 11.7 5 01/19/20 03:49 67-66-3 Chloromethane ND ug/L 5.0 1.9 5 01/19/20 03:49 74-87-3 v2 2-Chlorotoluene ND ug/L 5.0 1.0 5 01/19/20 03:49 95-49-8 4-Chlorotoluene ND ug/L 5.0 1.0 5 01/19/20 03:49 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 25.0 1.3 5 01/19/20 03:49 96-12-8 Dibromochloromethane ND ug/L 5.0 2.1 5 01/19/20 03:49 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 1.3 5 01/19/20 03:49 106-93-4 Dibromomethane ND ug/L 5.0 2.3 5 01/19/20 03:49 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 1.5 5 01/19/20 03:49 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 1.1 5 01/19/20 03:49 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 1.3 5 01/19/20 03:49 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 1.1 5 01/19/20 03:49 75-71-8 1,1-Dichloroethane ND ug/L 5.0 1.3 5 01/19/20 03:49 75-34-3 1,2-Dichloroethane ND ug/L 5.0 1.7 5 01/19/20 03:49 107-06-2 1,1-Dichloroethene 6.7 ug/L 5.0 1.2 5 01/19/20 03:49 75-35-4 cis-1,2-Dichloroethene 28.2 ug/L 5.0 1.5 5 01/19/20 03:49 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 1.3 5 01/19/20 03:49 156-60-5 1,2-Dichloropropane ND ug/L 5.0 0.94 5 01/19/20 03:49 78-87-5 1,3-Dichloropropane ND ug/L 5.0 0.79 5 01/19/20 03:49 142-28-9 2,2-Dichloropropane ND ug/L 5.0 1.4 5 01/19/20 03:49 594-20-7 1,1-Dichloropropene ND ug/L 5.0 1.1 5 01/19/20 03:49 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 1.5 5 01/19/20 03:49 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 5.0 1.5 5 01/19/20 03:49 10061-02-6 Diisopropyl ether ND ug/L 5.0 1.1 5 01/19/20 03:49 108-20-3 Ethylbenzene ND ug/L 5.0 1.3 5 01/19/20 03:49 100-41-4 Hexachloro-1,3-butadiene ND ug/L 5.0 2.2 5 01/19/20 03:49 87-68-3 2-Hexanone ND ug/L 25.0 2.8 5 01/19/20 03:49 591-78-6 p-Isopropyltoluene ND ug/L 5.0 1.1 5 01/19/20 03:49 99-87-6 Methylene Chloride ND ug/L 25.0 18.4 5 01/19/20 03:49 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-8A Lab ID: 92461009011 Collected: 01/14/20 09:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 22.6 5 01/19/20 03:49 108-10-1 ND ug/L 5.0 1.4 5 01/19/20 03:49 1634-04-4 ND ug/L 5.0 1.8 5 01/19/20 03:49 91-20-3 ND ug/L 5.0 1.3 5 01/19/20 03:49 100-42-5 ND ug/L 5.0 1.7 5 01/19/20 03:49 630-20-6 ND ug/L 5.0 1.1 5 01/19/20 03:49 79-34-5 67.9 ug/L 5.0 0.81 5 01/19/20 03:49 127-18-4 ND ug/L 5.0 1.2 5 01/19/20 03:49 108-88-3 ND ug/L 5.0 1.7 5 01/19/20 03:49 87-61-6 ND ug/L 5.0 1.1 5 01/19/20 03:49 120-82-1 ND ug/L 5.0 0.88 5 01/19/20 03:49 71-55-6 ND ug/L 5.0 1.2 5 01/19/20 03:49 79-00-5 516 ug/L 5.0 1.1 5 01/19/20 03:49 79-01-6 ND ug/L 5.0 1.6 5 01/19/20 03:49 75-69-4 ND ug/L 5.0 1.7 5 01/19/20 03:49 96-18-4 ND ug/L 10.0 7.2 5 01/19/20 03:49 108-05-4 IK ND ug/L 5.0 1.2 5 01/19/20 03:49 75-01-4 ND ug/L 5.0 3.2 5 01/19/20 03:49 1330-20-7 ND ug/L 10.0 2.0 5 01/19/20 03:49 179601-23-1 ND ug/L 5.0 1.1 5 01/19/20 03:49 95-47-6 101 % 70-130 5 01/19/20 03:49 460-00-4 90 % 70-130 5 01/19/20 03:49 17060-07-0 104 % 70-130 5 01/19/20 03:49 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 6.9 mg/L 1.0 0.60 1 01/18/20 07:36 16887-00-6 13.8 mg/L 1.0 0.50 1 01/18/20 07:36 14808-79-8 Analytical Method: SM 531OB-2011 ND mg/L 1.0 0.50 1 01 /21 /20 02:24 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-8B Lab ID: 92461009012 Collected: 01/15/20 16:55 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/20/2015:00 01/20/2015:00 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 2040 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:34 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 125 30.8 5 01/19/20 05:00 67-64-1 Benzene ND ug/L 5.0 0.75 5 01/19/20 05:00 71-43-2 Bromobenzene ND ug/L 5.0 1.1 5 01/19/20 05:00 108-86-1 Bromochloromethane ND ug/L 5.0 1.7 5 01/19/20 05:00 74-97-5 Bromodichloromethane ND ug/L 5.0 1.3 5 01/19/20 05:00 75-27-4 Bromoform ND ug/L 5.0 3.1 5 01/19/20 05:00 75-25-2 Bromomethane ND ug/L 10.0 3.1 5 01/19/20 05:00 74-83-9 IK 2-Butanone (MEK) ND ug/L 25.0 16.6 5 01/19/20 05:00 78-93-3 Carbon tetrachloride ND ug/L 5.0 1.1 5 01/19/20 05:00 56-23-5 Chlorobenzene ND ug/L 5.0 1.2 5 01/19/20 05:00 108-90-7 Chloroethane ND ug/L 5.0 2.4 5 01/19/20 05:00 75-00-3 v2 Chloroform ND ug/L 25.0 11.7 5 01/19/20 05:00 67-66-3 Chloromethane ND ug/L 5.0 1.9 5 01/19/20 05:00 74-87-3 v2 2-Chlorotoluene ND ug/L 5.0 1.0 5 01/19/20 05:00 95-49-8 4-Chlorotoluene ND ug/L 5.0 1.0 5 01/19/20 05:00 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 25.0 1.3 5 01/19/20 05:00 96-12-8 Dibromochloromethane ND ug/L 5.0 2.1 5 01/19/20 05:00 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 1.3 5 01/19/20 05:00 106-93-4 Dibromomethane ND ug/L 5.0 2.3 5 01/19/20 05:00 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 1.5 5 01/19/20 05:00 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 1.1 5 01/19/20 05:00 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 1.3 5 01/19/20 05:00 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 1.1 5 01/19/20 05:00 75-71-8 1,1-Dichloroethane 2.5J ug/L 5.0 1.3 5 01/19/20 05:00 75-34-3 1,2-Dichloroethane ND ug/L 5.0 1.7 5 01/19/20 05:00 107-06-2 1,1-Dichloroethene 5.7 ug/L 5.0 1.2 5 01/19/20 05:00 75-35-4 cis-1,2-Dichloroethene 35.4 ug/L 5.0 1.5 5 01/19/20 05:00 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 1.3 5 01/19/20 05:00 156-60-5 1,2-Dichloropropane ND ug/L 5.0 0.94 5 01/19/20 05:00 78-87-5 1,3-Dichloropropane ND ug/L 5.0 0.79 5 01/19/20 05:00 142-28-9 2,2-Dichloropropane ND ug/L 5.0 1.4 5 01/19/20 05:00 594-20-7 1,1-Dichloropropene ND ug/L 5.0 1.1 5 01/19/20 05:00 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 1.5 5 01/19/20 05:00 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 5.0 1.5 5 01/19/20 05:00 10061-02-6 Diisopropyl ether ND ug/L 5.0 1.1 5 01/19/20 05:00 108-20-3 Ethylbenzene ND ug/L 5.0 1.3 5 01/19/20 05:00 100-41-4 Hexachloro-1,3-butadiene ND ug/L 5.0 2.2 5 01/19/20 05:00 87-68-3 2-Hexanone ND ug/L 25.0 2.8 5 01/19/20 05:00 591-78-6 p-Isopropyltoluene ND ug/L 5.0 1.1 5 01/19/20 05:00 99-87-6 Methylene Chloride ND ug/L 25.0 18.4 5 01/19/20 05:00 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-813 Lab ID: 92461009012 Collected: 01/15/20 16:55 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 22.6 5 01/19/20 05:00 108-10-1 ND ug/L 5.0 1.4 5 01/19/20 05:00 1634-04-4 ND ug/L 5.0 1.8 5 01/19/20 05:00 91-20-3 ND ug/L 5.0 1.3 5 01/19/20 05:00 100-42-5 ND ug/L 5.0 1.7 5 01/19/20 05:00 630-20-6 ND ug/L 5.0 1.1 5 01/19/20 05:00 79-34-5 19.8 ug/L 5.0 0.81 5 01/19/20 05:00 127-18-4 ND ug/L 5.0 1.2 5 01/19/20 05:00 108-88-3 ND ug/L 5.0 1.7 5 01/19/20 05:00 87-61-6 ND ug/L 5.0 1.1 5 01/19/20 05:00 120-82-1 ND ug/L 5.0 0.88 5 01/19/20 05:00 71-55-6 ND ug/L 5.0 1.2 5 01/19/20 05:00 79-00-5 474 ug/L 5.0 1.1 5 01/19/20 05:00 79-01-6 ND ug/L 5.0 1.6 5 01/19/20 05:00 75-69-4 ND ug/L 5.0 1.7 5 01/19/20 05:00 96-18-4 ND ug/L 10.0 7.2 5 01/19/20 05:00 108-05-4 IK ND ug/L 5.0 1.2 5 01/19/20 05:00 75-01-4 ND ug/L 5.0 3.2 5 01/19/20 05:00 1330-20-7 ND ug/L 10.0 2.0 5 01/19/20 05:00 179601-23-1 ND ug/L 5.0 1.1 5 01/19/20 05:00 95-47-6 100 % 70-130 5 01/19/20 05:00 460-00-4 93 % 70-130 5 01/19/20 05:00 17060-07-0 104 % 70-130 5 01/19/20 05:00 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 6.3 mg/L 1.0 0.60 1 01/18/20 07:49 16887-00-6 60.7 mg/L 1.0 0.50 1 01/18/20 07:49 14808-79-8 Analytical Method: SM 531OB-2011 1.5 mg/L 1.0 0.50 1 01/21/20 03:19 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-9A Lab ID: 92461009013 Collected: 01/15/20 09:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene 17.2 ug/L 13.0 4.26 1 01/21/2013:04 01/21/2013:04 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 16600 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:37 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 62.5 15.4 2.5 01/19/20 02:55 67-64-1 Benzene 4.0 ug/L 2.5 0.38 2.5 01/19/20 02:55 71-43-2 Bromobenzene ND ug/L 2.5 0.55 2.5 01/19/20 02:55 108-86-1 Bromochloromethane ND ug/L 2.5 0.86 2.5 01/19/20 02:55 74-97-5 Bromodichloromethane ND ug/L 2.5 0.64 2.5 01/19/20 02:55 75-27-4 Bromoform ND ug/L 2.5 1.5 2.5 01/19/20 02:55 75-25-2 Bromomethane ND ug/L 5.0 1.6 2.5 01/19/20 02:55 74-83-9 IK 2-Butanone (MEK) ND ug/L 12.5 8.3 2.5 01/19/20 02:55 78-93-3 Carbon tetrachloride ND ug/L 2.5 0.56 2.5 01/19/20 02:55 56-23-5 Chlorobenzene ND ug/L 2.5 0.58 2.5 01/19/20 02:55 108-90-7 Chloroethane ND ug/L 2.5 1.2 2.5 01/19/20 02:55 75-00-3 v2 Chloroform ND ug/L 12.5 5.8 2.5 01/19/20 02:55 67-66-3 Chloromethane ND ug/L 2.5 0.97 2.5 01/19/20 02:55 74-87-3 v2 2-Chlorotoluene ND ug/L 2.5 0.51 2.5 01/19/20 02:55 95-49-8 4-Chlorotoluene ND ug/L 2.5 0.51 2.5 01/19/20 02:55 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 12.5 0.64 2.5 01/19/20 02:55 96-12-8 Dibromochloromethane ND ug/L 2.5 1.0 2.5 01/19/20 02:55 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 2.5 0.64 2.5 01/19/20 02:55 106-93-4 Dibromomethane ND ug/L 2.5 1.1 2.5 01/19/20 02:55 74-95-3 1,2-Dichlorobenzene ND ug/L 2.5 0.73 2.5 01/19/20 02:55 95-50-1 1,3-Dichlorobenzene ND ug/L 2.5 0.54 2.5 01/19/20 02:55 541-73-1 1,4-Dichlorobenzene ND ug/L 2.5 0.64 2.5 01/19/20 02:55 106-46-7 Dichlorodifluoromethane ND ug/L 2.5 0.56 2.5 01/19/20 02:55 75-71-8 1,1-Dichloroethane 4.3 ug/L 2.5 0.67 2.5 01/19/20 02:55 75-34-3 1,2-Dichloroethane ND ug/L 2.5 0.84 2.5 01/19/20 02:55 107-06-2 1,1-Dichloroethene 2.6 ug/L 2.5 0.61 2.5 01/19/20 02:55 75-35-4 cis-1,2-Dichloroethene 408 ug/L 2.5 0.73 2.5 01/19/20 02:55 156-59-2 trans-1,2-Dichloroethene 4.2 ug/L 2.5 0.64 2.5 01/19/20 02:55 156-60-5 1,2-Dichloropropane ND ug/L 2.5 0.47 2.5 01/19/20 02:55 78-87-5 1,3-Dichloropropane ND ug/L 2.5 0.40 2.5 01/19/20 02:55 142-28-9 2,2-Dichloropropane ND ug/L 2.5 0.68 2.5 01/19/20 02:55 594-20-7 1,1-Dichloropropene ND ug/L 2.5 0.53 2.5 01/19/20 02:55 563-58-6 cis-1,3-Dichloropropene ND ug/L 2.5 0.74 2.5 01/19/20 02:55 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 2.5 0.77 2.5 01/19/20 02:55 10061-02-6 Diisopropyl ether ND ug/L 2.5 0.54 2.5 01/19/20 02:55 108-20-3 Ethylbenzene ND ug/L 2.5 0.64 2.5 01/19/20 02:55 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.5 1.1 2.5 01/19/20 02:55 87-68-3 2-Hexanone ND ug/L 12.5 1.4 2.5 01/19/20 02:55 591-78-6 p-Isopropyltoluene ND ug/L 2.5 0.53 2.5 01/19/20 02:55 99-87-6 Methylene Chloride ND ug/L 12.5 9.2 2.5 01/19/20 02:55 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 32 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-9A Lab ID: 92461009013 Collected: 01/15/20 09:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 12.5 11.3 2.5 01/19/20 02:55 108-10-1 ND ug/L 2.5 0.69 2.5 01/19/20 02:55 1634-04-4 ND ug/L 2.5 0.88 2.5 01/19/20 02:55 91-20-3 ND ug/L 2.5 0.67 2.5 01/19/20 02:55 100-42-5 ND ug/L 2.5 0.85 2.5 01/19/20 02:55 630-20-6 ND ug/L 2.5 0.56 2.5 01/19/20 02:55 79-34-5 2.6 ug/L 2.5 0.40 2.5 01/19/20 02:55 127-18-4 ND ug/L 2.5 0.61 2.5 01/19/20 02:55 108-88-3 ND ug/L 2.5 0.86 2.5 01/19/20 02:55 87-61-6 3.8 ug/L 2.5 0.54 2.5 01/19/20 02:55 120-82-1 ND ug/L 2.5 0.44 2.5 01/19/20 02:55 71-55-6 ND ug/L 2.5 0.59 2.5 01/19/20 02:55 79-00-5 90.2 ug/L 2.5 0.55 2.5 01/19/20 02:55 79-01-6 ND ug/L 2.5 0.78 2.5 01/19/20 02:55 75-69-4 ND ug/L 2.5 0.87 2.5 01/19/20 02:55 96-18-4 ND ug/L 5.0 3.6 2.5 01/19/20 02:55 108-05-4 IK 61.2 ug/L 2.5 0.60 2.5 01/19/20 02:55 75-01-4 ND ug/L 2.5 1.6 2.5 01/19/20 02:55 1330-20-7 ND ug/L 5.0 1.0 2.5 01/19/20 02:55 179601-23-1 ND ug/L 2.5 0.55 2.5 01/19/20 02:55 95-47-6 97 % 70-130 2.5 01/19/20 02:55 460-00-4 93 % 70-130 2.5 01/19/20 02:55 17060-07-0 104 % 70-130 2.5 01/19/20 02:55 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 38.4 mg/L 1.0 0.60 1 01/18/20 08:03 16887-00-6 2.0 mg/L 1.0 0.50 1 01/18/20 08:03 14808-79-8 Analytical Method: SM 531OB-2011 5.1 mg/L 1.0 0.50 1 01/21/20 03:36 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 33 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-9B Lab ID: 92461009014 Collected: 01/15/20 09:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/21/2013:08 01/21/2013:08 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 655 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:40 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone 353J ug/L 500 123 20 01/20/20 14:08 67-64-1 Benzene 15.8J ug/L 20.0 3.0 20 01/20/20 14:08 71-43-2 Bromobenzene ND ug/L 20.0 4.4 20 01/20/20 14:08 108-86-1 Bromochloromethane ND ug/L 20.0 6.9 20 01/20/20 14:08 74-97-5 Bromodichloromethane ND ug/L 20.0 5.1 20 01/20/20 14:08 75-27-4 Bromoform ND ug/L 20.0 12.3 20 01/20/20 14:08 75-25-2 Bromomethane ND ug/L 40.0 12.4 20 01/20/20 14:08 74-83-9 IK 2-Butanone (MEK) ND ug/L 100 66.6 20 01/20/20 14:08 78-93-3 Carbon tetrachloride ND ug/L 20.0 4.5 20 01/20/20 14:08 56-23-5 Chlorobenzene ND ug/L 20.0 4.7 20 01/20/20 14:08 108-90-7 Chloroethane ND ug/L 20.0 9.8 20 01/20/20 14:08 75-00-3 v2 Chloroform ND ug/L 100 46.8 20 01/20/20 14:08 67-66-3 Chloromethane ND ug/L 20.0 7.8 20 01/20/20 14:08 74-87-3 v2 2-Chlorotoluene ND ug/L 20.0 4.1 20 01/20/20 14:08 95-49-8 4-Chlorotoluene ND ug/L 20.0 4.1 20 01/20/20 14:08 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 100 5.1 20 01/20/20 14:08 96-12-8 Dibromochloromethane ND ug/L 20.0 8.3 20 01/20/20 14:08 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 20.0 5.2 20 01/20/20 14:08 106-93-4 Dibromomethane ND ug/L 20.0 9.2 20 01/20/20 14:08 74-95-3 1,2-Dichlorobenzene ND ug/L 20.0 5.8 20 01/20/20 14:08 95-50-1 1,3-Dichlorobenzene 10.2J ug/L 20.0 4.3 20 01/20/20 14:08 541-73-1 1,4-Dichlorobenzene ND ug/L 20.0 5.2 20 01/20/20 14:08 106-46-7 Dichlorodifluoromethane ND ug/L 20.0 4.5 20 01/20/20 14:08 75-71-8 1,1-Dichloroethane ND ug/L 20.0 5.4 20 01/20/20 14:08 75-34-3 1,2-Dichloroethane ND ug/L 20.0 6.7 20 01/20/20 14:08 107-06-2 1,1-Dichloroethene 33.6 ug/L 20.0 4.9 20 01/20/20 14:08 75-35-4 cis-1,2-Dichloroethene 1170 ug/L 20.0 5.8 20 01/20/20 14:08 156-59-2 trans-1,2-Dichloroethene ND ug/L 20.0 5.1 20 01/20/20 14:08 156-60-5 1,2-Dichloropropane ND ug/L 20.0 3.7 20 01/20/20 14:08 78-87-5 1,3-Dichloropropane ND ug/L 20.0 3.2 20 01/20/20 14:08 142-28-9 2,2-Dichloropropane ND ug/L 20.0 5.4 20 01/20/20 14:08 594-20-7 1,1-Dichloropropene ND ug/L 20.0 4.3 20 01/20/20 14:08 563-58-6 cis-1,3-Dichloropropene ND ug/L 20.0 5.9 20 01/20/20 14:08 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 20.0 6.2 20 01/20/20 14:08 10061-02-6 Diisopropyl ether ND ug/L 20.0 4.4 20 01/20/20 14:08 108-20-3 Ethylbenzene ND ug/L 20.0 5.1 20 01/20/20 14:08 100-41-4 Hexachloro-1,3-butadiene ND ug/L 20.0 8.8 20 01/20/20 14:08 87-68-3 2-Hexanone ND ug/L 100 11.4 20 01/20/20 14:08 591-78-6 p-Isopropyltoluene ND ug/L 20.0 4.2 20 01/20/20 14:08 99-87-6 Methylene Chloride ND ug/L 100 73.8 20 01/20/20 14:08 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 34 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-913 Lab ID: 92461009014 Collected: 01/15/20 09:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D 4-Methyl-2-pentanone (MIBK) ND ug/L 100 90.6 20 01/20/20 14:08 108-10-1 Methyl-tert-butyl ether ND ug/L 20.0 5.5 20 01/20/20 14:08 1634-04-4 Naphthalene ND ug/L 20.0 7.0 20 01/20/20 14:08 91-20-3 Styrene ND ug/L 20.0 5.3 20 01/20/20 14:08 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 20.0 6.8 20 01/20/20 14:08 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 20.0 4.4 20 01/20/20 14:08 79-34-5 Tetrachloroethene 731 ug/L 20.0 3.2 20 01/20/20 14:08 127-18-4 Toluene ND ug/L 20.0 4.9 20 01/20/20 14:08 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 6.9 20 01/20/20 14:08 87-61-6 1,2,4-Trichlorobenzene 64.0 ug/L 20.0 4.4 20 01/20/20 14:08 120-82-1 1,1,1-Trichloroethane ND ug/L 20.0 3.5 20 01/20/20 14:08 71-55-6 1,1,2-Trichloroethane ND ug/L 20.0 4.7 20 01/20/20 14:08 79-00-5 Trichloroethene 1720 ug/L 20.0 4.4 20 01/20/20 14:08 79-01-6 Trichlorofluoromethane ND ug/L 20.0 6.2 20 01/20/20 14:08 75-69-4 1,2,3-Trichloropropane ND ug/L 20.0 6.9 20 01/20/20 14:08 96-18-4 Vinyl acetate ND ug/L 40.0 29.0 20 01/20/20 14:08 108-05-4 IK Vinyl chloride 56.9 ug/L 20.0 4.8 20 01/20/20 14:08 75-01-4 Xylene (Total) ND ug/L 20.0 12.6 20 01/20/20 14:08 1330-20-7 m&p-Xylene ND ug/L 40.0 8.2 20 01/20/20 14:08 179601-23-1 o-Xylene ND ug/L 20.0 4.4 20 01/20/20 14:08 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 20 01/20/20 14:08 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 20 01/20/20 14:08 17060-07-0 Toluene-d8 (S) 102 % 70-130 20 01/20/20 14:08 2037-26-5 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Chloride 32.7 mg/L 1.0 0.60 1 01/18/20 08:17 16887-00-6 Sulfate 5.3 mg/L 1.0 0.50 1 01/18/20 08:17 14808-79-8 531013 TOC Analytical Method: SM 531 OB-2011 Total Organic Carbon 1.1 mg/L 1.0 0.50 1 01/21/20 04:28 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-9C Lab ID: 92461009015 Collected: 01/15/20 10:10 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/21/2013:15 01/21/2013:15 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 1250 ug/L 50.0 19.5 1 01/17/20 01:06 01/17/20 23:43 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 6250 1540 250 01/19/20 03:46 67-64-1 Benzene ND ug/L 250 37.5 250 01/19/20 03:46 71-43-2 Bromobenzene ND ug/L 250 55.0 250 01/19/20 03:46 108-86-1 Bromochloromethane ND ug/L 250 85.8 250 01/19/20 03:46 74-97-5 Bromodichloromethane ND ug/L 250 64.0 250 01/19/20 03:46 75-27-4 Bromoform ND ug/L 250 154 250 01/19/20 03:46 75-25-2 Bromomethane ND ug/L 500 155 250 01/19/20 03:46 74-83-9 v2 2-Butanone (MEK) ND ug/L 1250 832 250 01/19/20 03:46 78-93-3 Carbon tetrachloride ND ug/L 250 56.0 250 01/19/20 03:46 56-23-5 Chlorobenzene ND ug/L 250 58.2 250 01/19/20 03:46 108-90-7 Chloroethane ND ug/L 250 122 250 01/19/20 03:46 75-00-3 IL Chloroform ND ug/L 1250 585 250 01/19/20 03:46 67-66-3 Chloromethane ND ug/L 250 97.2 250 01/19/20 03:46 74-87-3 v2 2-Chlorotoluene ND ug/L 250 50.8 250 01/19/20 03:46 95-49-8 4-Chlorotoluene ND ug/L 250 51.0 250 01/19/20 03:46 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1250 64.2 250 01/19/20 03:46 96-12-8 Dibromochloromethane ND ug/L 250 103 250 01/19/20 03:46 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 250 64.5 250 01/19/20 03:46 106-93-4 Dibromomethane ND ug/L 250 115 250 01/19/20 03:46 74-95-3 1,2-Dichlorobenzene ND ug/L 250 72.8 250 01/19/20 03:46 95-50-1 1,3-Dichlorobenzene ND ug/L 250 54.2 250 01/19/20 03:46 541-73-1 1,4-Dichlorobenzene ND ug/L 250 64.5 250 01/19/20 03:46 106-46-7 Dichlorodifluoromethane ND ug/L 250 56.5 250 01/19/20 03:46 75-71-8 v2 1,1-Dichloroethane ND ug/L 250 67.0 250 01/19/20 03:46 75-34-3 1,2-Dichloroethane ND ug/L 250 84.0 250 01/19/20 03:46 107-06-2 1,1-Dichloroethene 2400 ug/L 250 61.2 250 01/19/20 03:46 75-35-4 cis-1,2-Dichloroethene 960 ug/L 250 72.8 250 01/19/20 03:46 156-59-2 trans-1,2-Dichloroethene ND ug/L 250 63.5 250 01/19/20 03:46 156-60-5 1,2-Dichloropropane ND ug/L 250 46.8 250 01/19/20 03:46 78-87-5 1,3-Dichloropropane ND ug/L 250 39.5 250 01/19/20 03:46 142-28-9 2,2-Dichloropropane ND ug/L 250 67.5 250 01/19/20 03:46 594-20-7 1,1-Dichloropropene ND ug/L 250 53.2 250 01/19/20 03:46 563-58-6 cis-1,3-Dichloropropene ND ug/L 250 74.0 250 01/19/20 03:46 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 250 77.2 250 01/19/20 03:46 10061-02-6 Diisopropyl ether ND ug/L 250 54.5 250 01/19/20 03:46 108-20-3 Ethylbenzene ND ug/L 250 64.0 250 01/19/20 03:46 100-41-4 Hexachloro-1,3-butadiene ND ug/L 250 110 250 01/19/20 03:46 87-68-3 2-Hexanone ND ug/L 1250 142 250 01/19/20 03:46 591-78-6 p-Isopropyltoluene ND ug/L 250 53.0 250 01/19/20 03:46 99-87-6 Methylene Chloride ND ug/L 1250 922 250 01/19/20 03:46 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-9C Lab ID: 92461009015 Collected: 01/15/20 10:10 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 1250 1130 250 01/19/20 03:46 108-10-1 ND ug/L 250 68.8 250 01/19/20 03:46 1634-04-4 ND ug/L 250 88.0 250 01/19/20 03:46 91-20-3 ND ug/L 250 66.8 250 01/19/20 03:46 100-42-5 ND ug/L 250 85.0 250 01/19/20 03:46 630-20-6 ND ug/L 250 55.5 250 01/19/20 03:46 79-34-5 22100 ug/L 250 40.5 250 01/19/20 03:46 127-18-4 ND ug/L 250 61.0 250 01/19/20 03:46 108-88-3 ND ug/L 250 86.0 250 01/19/20 03:46 87-61-6 ND ug/L 250 54.5 250 01/19/20 03:46 120-82-1 ND ug/L 250 43.8 250 01/19/20 03:46 71-55-6 ND ug/L 250 59.0 250 01/19/20 03:46 79-00-5 48600 ug/L 250 55.0 250 01/19/20 03:46 79-01-6 ND ug/L 250 77.8 250 01/19/20 03:46 75-69-4 ND ug/L 250 86.8 250 01/19/20 03:46 96-18-4 ND ug/L 500 362 250 01/19/20 03:46 108-05-4 IK ND ug/L 250 60.5 250 01/19/20 03:46 75-01-4 v2 ND ug/L 250 158 250 01/19/20 03:46 1330-20-7 ND ug/L 500 102 250 01/19/20 03:46 179601-23-1 ND ug/L 250 55.0 250 01/19/20 03:46 95-47-6 100 % 70-130 250 01/19/20 03:46 460-00-4 94 % 70-130 250 01/19/20 03:46 17060-07-0 98 % 70-130 250 01/19/20 03:46 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 31.1 mg/L 1.0 0.60 1 01/18/20 08:31 16887-00-6 35.8 mg/L 1.0 0.50 1 01/18/20 08:31 14808-79-8 Analytical Method: SM 531OB-2011 2.1 mg/L 1.0 0.50 1 01/21/20 04:45 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 37 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-10A Lab ID: 92461009016 Collected: 01/15/20 11:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/21/2013:17 01/21/2013:17 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 44.8J ug/L 50.0 19.5 1 01/21/20 01:33 01/22/20 05:09 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 6250 1540 250 01/19/20 04:04 67-64-1 Benzene ND ug/L 250 37.5 250 01/19/20 04:04 71-43-2 Bromobenzene ND ug/L 250 55.0 250 01/19/20 04:04 108-86-1 Bromochloromethane ND ug/L 250 85.8 250 01/19/20 04:04 74-97-5 Bromodichloromethane ND ug/L 250 64.0 250 01/19/20 04:04 75-27-4 Bromoform ND ug/L 250 154 250 01/19/20 04:04 75-25-2 Bromomethane ND ug/L 500 155 250 01/19/20 04:04 74-83-9 v2 2-Butanone (MEK) ND ug/L 1250 832 250 01/19/20 04:04 78-93-3 Carbon tetrachloride ND ug/L 250 56.0 250 01/19/20 04:04 56-23-5 Chlorobenzene ND ug/L 250 58.2 250 01/19/20 04:04 108-90-7 Chloroethane ND ug/L 250 122 250 01/19/20 04:04 75-00-3 IL Chloroform ND ug/L 1250 585 250 01/19/20 04:04 67-66-3 Chloromethane ND ug/L 250 97.2 250 01/19/20 04:04 74-87-3 v2 2-Chlorotoluene ND ug/L 250 50.8 250 01/19/20 04:04 95-49-8 4-Chlorotoluene ND ug/L 250 51.0 250 01/19/20 04:04 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1250 64.2 250 01/19/20 04:04 96-12-8 Dibromochloromethane ND ug/L 250 103 250 01/19/20 04:04 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 250 64.5 250 01/19/20 04:04 106-93-4 Dibromomethane ND ug/L 250 115 250 01/19/20 04:04 74-95-3 1,2-Dichlorobenzene ND ug/L 250 72.8 250 01/19/20 04:04 95-50-1 1,3-Dichlorobenzene ND ug/L 250 54.2 250 01/19/20 04:04 541-73-1 1,4-Dichlorobenzene ND ug/L 250 64.5 250 01/19/20 04:04 106-46-7 Dichlorodifluoromethane ND ug/L 250 56.5 250 01/19/20 04:04 75-71-8 v2 1,1-Dichloroethane ND ug/L 250 67.0 250 01/19/20 04:04 75-34-3 1,2-Dichloroethane ND ug/L 250 84.0 250 01/19/20 04:04 107-06-2 1,1-Dichloroethene 454 ug/L 250 61.2 250 01/19/20 04:04 75-35-4 cis-1,2-Dichloroethene 1690 ug/L 250 72.8 250 01/19/20 04:04 156-59-2 trans-1,2-Dichloroethene ND ug/L 250 63.5 250 01/19/20 04:04 156-60-5 1,2-Dichloropropane ND ug/L 250 46.8 250 01/19/20 04:04 78-87-5 1,3-Dichloropropane ND ug/L 250 39.5 250 01/19/20 04:04 142-28-9 2,2-Dichloropropane ND ug/L 250 67.5 250 01/19/20 04:04 594-20-7 1,1-Dichloropropene ND ug/L 250 53.2 250 01/19/20 04:04 563-58-6 cis-1,3-Dichloropropene ND ug/L 250 74.0 250 01/19/20 04:04 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 250 77.2 250 01/19/20 04:04 10061-02-6 Diisopropyl ether ND ug/L 250 54.5 250 01/19/20 04:04 108-20-3 Ethylbenzene ND ug/L 250 64.0 250 01/19/20 04:04 100-41-4 Hexachloro-1,3-butadiene ND ug/L 250 110 250 01/19/20 04:04 87-68-3 2-Hexanone ND ug/L 1250 142 250 01/19/20 04:04 591-78-6 p-Isopropyltoluene ND ug/L 250 53.0 250 01/19/20 04:04 99-87-6 Methylene Chloride ND ug/L 1250 922 250 01/19/20 04:04 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 38 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-10A Lab ID: 92461009016 Collected: 01/15/20 11:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 1250 1130 250 01/19/20 04:04 108-10-1 ND ug/L 250 68.8 250 01/19/20 04:04 1634-04-4 ND ug/L 250 88.0 250 01/19/20 04:04 91-20-3 ND ug/L 250 66.8 250 01/19/20 04:04 100-42-5 ND ug/L 250 85.0 250 01/19/20 04:04 630-20-6 ND ug/L 250 55.5 250 01/19/20 04:04 79-34-5 6880 ug/L 250 40.5 250 01/19/20 04:04 127-18-4 ND ug/L 250 61.0 250 01/19/20 04:04 108-88-3 ND ug/L 250 86.0 250 01/19/20 04:04 87-61-6 ND ug/L 250 54.5 250 01/19/20 04:04 120-82-1 ND ug/L 250 43.8 250 01/19/20 04:04 71-55-6 ND ug/L 250 59.0 250 01/19/20 04:04 79-00-5 37900 ug/L 250 55.0 250 01/19/20 04:04 79-01-6 ND ug/L 250 77.8 250 01/19/20 04:04 75-69-4 ND ug/L 250 86.8 250 01/19/20 04:04 96-18-4 ND ug/L 500 362 250 01/19/20 04:04 108-05-4 IK ND ug/L 250 60.5 250 01/19/20 04:04 75-01-4 v2 ND ug/L 250 158 250 01/19/20 04:04 1330-20-7 ND ug/L 500 102 250 01/19/20 04:04 179601-23-1 ND ug/L 250 55.0 250 01/19/20 04:04 95-47-6 100 % 70-130 250 01/19/20 04:04 460-00-4 95 % 70-130 250 01/19/20 04:04 17060-07-0 104 % 70-130 250 01/19/20 04:04 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 25.2 mg/L 1.0 0.60 1 01/18/20 08:45 16887-00-6 99.2 mg/L 1.0 0.50 1 01/18/20 08:45 14808-79-8 Analytical Method: SM 531OB-2011 2.1 mg/L 1.0 0.50 1 01/21/20 05:03 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 39 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-10B Lab ID: 92461009017 Collected: 01/15/20 10:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/21/2013:20 01/21/2013:20 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 128 ug/L 50.0 19.5 1 01/21/20 01:33 01/22/20 05:12 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 6250 1540 250 01/19/20 04:22 67-64-1 Benzene ND ug/L 250 37.5 250 01/19/20 04:22 71-43-2 Bromobenzene ND ug/L 250 55.0 250 01/19/20 04:22 108-86-1 Bromochloromethane ND ug/L 250 85.8 250 01/19/20 04:22 74-97-5 Bromodichloromethane ND ug/L 250 64.0 250 01/19/20 04:22 75-27-4 Bromoform ND ug/L 250 154 250 01/19/20 04:22 75-25-2 Bromomethane ND ug/L 500 155 250 01/19/20 04:22 74-83-9 v2 2-Butanone (MEK) ND ug/L 1250 832 250 01/19/20 04:22 78-93-3 Carbon tetrachloride ND ug/L 250 56.0 250 01/19/20 04:22 56-23-5 Chlorobenzene ND ug/L 250 58.2 250 01/19/20 04:22 108-90-7 Chloroethane ND ug/L 250 122 250 01/19/20 04:22 75-00-3 IL Chloroform ND ug/L 1250 585 250 01/19/20 04:22 67-66-3 Chloromethane ND ug/L 250 97.2 250 01/19/20 04:22 74-87-3 v2 2-Chlorotoluene ND ug/L 250 50.8 250 01/19/20 04:22 95-49-8 4-Chlorotoluene ND ug/L 250 51.0 250 01/19/20 04:22 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1250 64.2 250 01/19/20 04:22 96-12-8 Dibromochloromethane ND ug/L 250 103 250 01/19/20 04:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 250 64.5 250 01/19/20 04:22 106-93-4 Dibromomethane ND ug/L 250 115 250 01/19/20 04:22 74-95-3 1,2-Dichlorobenzene ND ug/L 250 72.8 250 01/19/20 04:22 95-50-1 1,3-Dichlorobenzene ND ug/L 250 54.2 250 01/19/20 04:22 541-73-1 1,4-Dichlorobenzene ND ug/L 250 64.5 250 01/19/20 04:22 106-46-7 Dichlorodifluoromethane ND ug/L 250 56.5 250 01/19/20 04:22 75-71-8 v2 1,1-Dichloroethane ND ug/L 250 67.0 250 01/19/20 04:22 75-34-3 1,2-Dichloroethane ND ug/L 250 84.0 250 01/19/20 04:22 107-06-2 1,1-Dichloroethene 209J ug/L 250 61.2 250 01/19/20 04:22 75-35-4 cis-1,2-Dichloroethene 1330 ug/L 250 72.8 250 01/19/20 04:22 156-59-2 trans-1,2-Dichloroethene ND ug/L 250 63.5 250 01/19/20 04:22 156-60-5 1,2-Dichloropropane ND ug/L 250 46.8 250 01/19/20 04:22 78-87-5 1,3-Dichloropropane ND ug/L 250 39.5 250 01/19/20 04:22 142-28-9 2,2-Dichloropropane ND ug/L 250 67.5 250 01/19/20 04:22 594-20-7 1,1-Dichloropropene ND ug/L 250 53.2 250 01/19/20 04:22 563-58-6 cis-1,3-Dichloropropene ND ug/L 250 74.0 250 01/19/20 04:22 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 250 77.2 250 01/19/20 04:22 10061-02-6 Diisopropyl ether ND ug/L 250 54.5 250 01/19/20 04:22 108-20-3 Ethylbenzene ND ug/L 250 64.0 250 01/19/20 04:22 100-41-4 Hexachloro-1,3-butadiene ND ug/L 250 110 250 01/19/20 04:22 87-68-3 2-Hexanone ND ug/L 1250 142 250 01/19/20 04:22 591-78-6 p-Isopropyltoluene ND ug/L 250 53.0 250 01/19/20 04:22 99-87-6 Methylene Chloride ND ug/L 1250 922 250 01/19/20 04:22 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 40 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-10B Lab ID: 92461009017 Collected: 01/15/20 10:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 1250 1130 250 01/19/20 04:22 108-10-1 ND ug/L 250 68.8 250 01/19/20 04:22 1634-04-4 ND ug/L 250 88.0 250 01/19/20 04:22 91-20-3 ND ug/L 250 66.8 250 01/19/20 04:22 100-42-5 ND ug/L 250 85.0 250 01/19/20 04:22 630-20-6 ND ug/L 250 55.5 250 01/19/20 04:22 79-34-5 5030 ug/L 250 40.5 250 01/19/20 04:22 127-18-4 ND ug/L 250 61.0 250 01/19/20 04:22 108-88-3 ND ug/L 250 86.0 250 01/19/20 04:22 87-61-6 ND ug/L 250 54.5 250 01/19/20 04:22 120-82-1 ND ug/L 250 43.8 250 01/19/20 04:22 71-55-6 ND ug/L 250 59.0 250 01/19/20 04:22 79-00-5 26800 ug/L 250 55.0 250 01/19/20 04:22 79-01-6 ND ug/L 250 77.8 250 01/19/20 04:22 75-69-4 ND ug/L 250 86.8 250 01/19/20 04:22 96-18-4 ND ug/L 500 362 250 01/19/20 04:22 108-05-4 IK ND ug/L 250 60.5 250 01/19/20 04:22 75-01-4 v2 ND ug/L 250 158 250 01/19/20 04:22 1330-20-7 ND ug/L 500 102 250 01/19/20 04:22 179601-23-1 ND ug/L 250 55.0 250 01/19/20 04:22 95-47-6 101 % 70-130 250 01/19/20 04:22 460-00-4 95 % 70-130 250 01/19/20 04:22 17060-07-0 100 % 70-130 250 01/19/20 04:22 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 23.0 mg/L 1.0 0.60 1 01/18/20 08:59 16887-00-6 88.6 mg/L 1.0 0.50 1 01/18/20 08:59 14808-79-8 Analytical Method: SM 531OB-2011 1.7 mg/L 1.0 0.50 1 01/21/20 05:22 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 41 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-11A Lab ID: 92461009018 Collected: 01/14/20 10:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene ND ug/L 13.0 4.26 1 01/21/2013:22 01/21/2013:22 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 309 ug/L 50.0 19.5 1 01/21/20 01:33 01/22/20 05:15 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone ND ug/L 25.0 6.2 1 01/20/20 12:03 67-64-1 Benzene ND ug/L 1.0 0.15 1 01/20/20 12:03 71-43-2 Bromobenzene ND ug/L 1.0 0.22 1 01/20/20 12:03 108-86-1 Bromochloromethane ND ug/L 1.0 0.34 1 01/20/20 12:03 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 01/20/20 12:03 75-27-4 Bromoform ND ug/L 1.0 0.62 1 01/20/20 12:03 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 01/20/20 12:03 74-83-9 IK 2-Butanone (MEK) ND ug/L 5.0 3.3 1 01/20/20 12:03 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.22 1 01/20/20 12:03 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 01/20/20 12:03 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 01/20/20 12:03 75-00-3 v2 Chloroform ND ug/L 5.0 2.3 1 01/20/20 12:03 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 01/20/20 12:03 74-87-3 v2 2-Chlorotoluene ND ug/L 1.0 0.20 1 01/20/20 12:03 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.20 1 01/20/20 12:03 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 01/20/20 12:03 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 01/20/20 12:03 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 01/20/20 12:03 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 01/20/20 12:03 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 01/20/20 12:03 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.22 1 01/20/20 12:03 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 01/20/20 12:03 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.23 1 01/20/20 12:03 75-71-8 1,1-Dichloroethane 3.9 ug/L 1.0 0.27 1 01/20/20 12:03 75-34-3 1,2-Dichloroethane 0.89J ug/L 1.0 0.34 1 01/20/20 12:03 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 01/20/20 12:03 75-35-4 cis-1,2-Dichloroethene 4.4 ug/L 1.0 0.29 1 01/20/20 12:03 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.25 1 01/20/20 12:03 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.19 1 01/20/20 12:03 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.16 1 01/20/20 12:03 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.27 1 01/20/20 12:03 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.21 1 01/20/20 12:03 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.30 1 01/20/20 12:03 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.31 1 01/20/20 12:03 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.22 1 01/20/20 12:03 108-20-3 Ethylbenzene ND ug/L 1.0 0.26 1 01/20/20 12:03 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.44 1 01/20/20 12:03 87-68-3 2-Hexanone ND ug/L 5.0 0.57 1 01/20/20 12:03 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.21 1 01/20/20 12:03 99-87-6 Methylene Chloride ND ug/L 5.0 3.7 1 01/20/20 12:03 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 42 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-11A Lab ID: 92461009018 Collected: 01/14/20 10:40 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 5.0 4.5 1 01/20/2012:03 108-10-1 ND ug/L 1.0 0.28 1 01/20/2012:03 1634-04-4 ND ug/L 1.0 0.35 1 01/20/2012:03 91-20-3 ND ug/L 1.0 0.27 1 01/20/2012:03 100-42-5 ND ug/L 1.0 0.34 1 01/20/2012:03 630-20-6 ND ug/L 1.0 0.22 1 01/20/2012:03 79-34-5 30.5 ug/L 1.0 0.16 1 01/20/2012:03 127-18-4 ND ug/L 1.0 0.24 1 01/20/2012:03 108-88-3 ND ug/L 1.0 0.34 1 01/20/2012:03 87-61-6 ND ug/L 1.0 0.22 1 01/20/2012:03 120-82-1 15.9 ug/L 1.0 0.18 1 01/20/2012:03 71-55-6 ND ug/L 1.0 0.24 1 01/20/2012:03 79-00-5 67.5 ug/L 1.0 0.22 1 01/20/2012:03 79-01-6 ND ug/L 1.0 0.31 1 01/20/2012:03 75-69-4 ND ug/L 1.0 0.35 1 01/20/2012:03 96-18-4 ND ug/L 2.0 1.4 1 01/20/2012:03 108-05-4 IK 0.56J ug/L 1.0 0.24 1 01/20/2012:03 75-01-4 ND ug/L 1.0 0.63 1 01/20/2012:03 1330-20-7 ND ug/L 2.0 0.41 1 01/20/2012:03 179601-23-1 ND ug/L 1.0 0.22 1 01/20/2012:03 95-47-6 99 % 70-130 1 01/20/2012:03 460-00-4 94 % 70-130 1 01/20/2012:03 17060-07-0 102 % 70-130 1 01/20/2012:03 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 6.3 mg/L 1.0 0.60 1 01/18/20 09:13 16887-00-6 85.9 mg/L 1.0 0.50 1 01/18/20 09:13 14808-79-8 Analytical Method: SM 531OB-2011 2.4 mg/L 1.0 0.50 1 01/21/20 05:42 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 43 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-11B Lab ID: 92461009019 Collected: 01/14/20 09:50 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene 5.25J ug/L 13.0 4.26 1 01/21/2013:25 01/21/2013:25 74-85-1 J 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 302 ug/L 50.0 19.5 1 01/21/20 01:33 01/22/20 05:18 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone 161J ug/L 250 61.7 10 01/20/20 13:32 67-64-1 Benzene ND ug/L 10.0 1.5 10 01/20/20 13:32 71-43-2 Bromobenzene ND ug/L 10.0 2.2 10 01/20/20 13:32 108-86-1 Bromochloromethane ND ug/L 10.0 3.4 10 01/20/20 13:32 74-97-5 Bromodichloromethane ND ug/L 10.0 2.6 10 01/20/20 13:32 75-27-4 Bromoform ND ug/L 10.0 6.2 10 01/20/20 13:32 75-25-2 Bromomethane ND ug/L 20.0 6.2 10 01/20/20 13:32 74-83-9 IK 2-Butanone (MEK) ND ug/L 50.0 33.3 10 01/20/20 13:32 78-93-3 Carbon tetrachloride ND ug/L 10.0 2.2 10 01/20/20 13:32 56-23-5 Chlorobenzene ND ug/L 10.0 2.3 10 01/20/20 13:32 108-90-7 Chloroethane ND ug/L 10.0 4.9 10 01/20/20 13:32 75-00-3 v2 Chloroform ND ug/L 50.0 23.4 10 01/20/20 13:32 67-66-3 Chloromethane ND ug/L 10.0 3.9 10 01/20/20 13:32 74-87-3 v2 2-Chlorotoluene ND ug/L 10.0 2.0 10 01/20/20 13:32 95-49-8 4-Chlorotoluene ND ug/L 10.0 2.0 10 01/20/20 13:32 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 50.0 2.6 10 01/20/20 13:32 96-12-8 Dibromochloromethane ND ug/L 10.0 4.1 10 01/20/20 13:32 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 10.0 2.6 10 01/20/20 13:32 106-93-4 Dibromomethane ND ug/L 10.0 4.6 10 01/20/20 13:32 74-95-3 1,2-Dichlorobenzene ND ug/L 10.0 2.9 10 01/20/20 13:32 95-50-1 1,3-Dichlorobenzene ND ug/L 10.0 2.2 10 01/20/20 13:32 541-73-1 1,4-Dichlorobenzene ND ug/L 10.0 2.6 10 01/20/20 13:32 106-46-7 Dichlorodifluoromethane ND ug/L 10.0 2.3 10 01/20/20 13:32 75-71-8 1,1-Dichloroethane 4.OJ ug/L 10.0 2.7 10 01/20/20 13:32 75-34-3 1,2-Dichloroethane ND ug/L 10.0 3.4 10 01/20/20 13:32 107-06-2 1,1-Dichloroethene 12.2 ug/L 10.0 2.4 10 01/20/20 13:32 75-35-4 cis-1,2-Dichloroethene 59.0 ug/L 10.0 2.9 10 01/20/20 13:32 156-59-2 trans-1,2-Dichloroethene ND ug/L 10.0 2.5 10 01/20/20 13:32 156-60-5 1,2-Dichloropropane ND ug/L 10.0 1.9 10 01/20/20 13:32 78-87-5 1,3-Dichloropropane ND ug/L 10.0 1.6 10 01/20/20 13:32 142-28-9 2,2-Dichloropropane ND ug/L 10.0 2.7 10 01/20/20 13:32 594-20-7 1,1-Dichloropropene ND ug/L 10.0 2.1 10 01/20/20 13:32 563-58-6 cis-1,3-Dichloropropene ND ug/L 10.0 3.0 10 01/20/20 13:32 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 10.0 3.1 10 01/20/20 13:32 10061-02-6 Diisopropyl ether ND ug/L 10.0 2.2 10 01/20/20 13:32 108-20-3 Ethylbenzene ND ug/L 10.0 2.6 10 01/20/20 13:32 100-41-4 Hexachloro-1,3-butadiene ND ug/L 10.0 4.4 10 01/20/20 13:32 87-68-3 2-Hexanone ND ug/L 50.0 5.7 10 01/20/20 13:32 591-78-6 p-Isopropyltoluene ND ug/L 10.0 2.1 10 01/20/20 13:32 99-87-6 Methylene Chloride ND ug/L 50.0 36.9 10 01/20/20 13:32 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 44 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-11B Lab ID: 92461009019 Collected: 01/14/20 09:50 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 50.0 45.3 10 01/20/2013:32 108-10-1 ND ug/L 10.0 2.8 10 01/20/2013:32 1634-04-4 ND ug/L 10.0 3.5 10 01 /20/20 13:32 91-20-3 ND ug/L 10.0 2.7 10 01/20/2013:32 100-42-5 ND ug/L 10.0 3.4 10 01/20/2013:32 630-20-6 ND ug/L 10.0 2.2 10 01/20/2013:32 79-34-5 124 ug/L 10.0 1.6 10 01/20/2013:32 127-18-4 ND ug/L 10.0 2.4 10 01/20/2013:32 108-88-3 ND ug/L 10.0 3.4 10 01 /20/20 13:32 87-61-6 ND ug/L 10.0 2.2 10 01/20/2013:32 120-82-1 5.8J ug/L 10.0 1.8 10 01/20/2013:32 71-55-6 ND ug/L 10.0 2.4 10 01/20/2013:32 79-00-5 1170 ug/L 10.0 2.2 10 01/20/2013:32 79-01-6 ND ug/L 10.0 3.1 10 01/20/2013:32 75-69-4 ND ug/L 10.0 3.5 10 01/20/2013:32 96-18-4 ND ug/L 20.0 14.5 10 01/20/2013:32 108-05-4 ND ug/L 10.0 2.4 10 01 /20/20 13:32 75-01-4 ND ug/L 10.0 6.3 10 01/20/2013:32 1330-20-7 ND ug/L 20.0 4.1 10 01/20/2013:32 179601-23-1 ND ug/L 10.0 2.2 10 01/20/2013:32 95-47-6 98 % 70-130 10 01/20/2013:32 460-00-4 94 % 70-130 10 01/20/2013:32 17060-07-0 102 % 70-130 10 01/20/2013:32 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 7.6 mg/L 1.0 0.60 1 01/18/20 09:55 16887-00-6 22.2 mg/L 1.0 0.50 1 01/18/20 09:55 14808-79-8 Analytical Method: SM 531OB-2011 0.73J mg/L 1.0 0.50 1 01/21/20 05:59 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. M1 IK Page 45 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-13B Lab ID: 92461009020 Collected: 01/14/20 11:50 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Analytical Method: RSK-175 Preparation Method: RSK175 Ethene 95.6 ug/L 13.0 4.26 1 01/21/2013:28 01/21/2013:28 74-85-1 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Iron 1430 ug/L 50.0 19.5 1 01/21/20 01:33 01/22/20 05:21 7439-89-6 8260D MSV Low Level Analytical Method: EPA 8260D Acetone 4670J ug/L 6250 1540 250 01/20/20 15:19 67-64-1 Benzene ND ug/L 250 37.5 250 01/20/20 15:19 71-43-2 Bromobenzene ND ug/L 250 55.0 250 01/20/20 15:19 108-86-1 Bromochloromethane ND ug/L 250 85.8 250 01/20/20 15:19 74-97-5 Bromodichloromethane ND ug/L 250 64.0 250 01/20/20 15:19 75-27-4 Bromoform ND ug/L 250 154 250 01/20/20 15:19 75-25-2 Bromomethane ND ug/L 500 155 250 01/20/20 15:19 74-83-9 IK 2-Butanone (MEK) ND ug/L 1250 832 250 01/20/20 15:19 78-93-3 Carbon tetrachloride ND ug/L 250 56.0 250 01/20/20 15:19 56-23-5 Chlorobenzene ND ug/L 250 58.2 250 01/20/20 15:19 108-90-7 Chloroethane ND ug/L 250 122 250 01/20/20 15:19 75-00-3 v2 Chloroform ND ug/L 1250 585 250 01/20/20 15:19 67-66-3 Chloromethane ND ug/L 250 97.2 250 01/20/20 15:19 74-87-3 v2 2-Chlorotoluene ND ug/L 250 50.8 250 01/20/20 15:19 95-49-8 4-Chlorotoluene ND ug/L 250 51.0 250 01/20/20 15:19 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1250 64.2 250 01/20/20 15:19 96-12-8 Dibromochloromethane ND ug/L 250 103 250 01/20/20 15:19 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 250 64.5 250 01/20/20 15:19 106-93-4 Dibromomethane ND ug/L 250 115 250 01/20/20 15:19 74-95-3 1,2-Dichlorobenzene ND ug/L 250 72.8 250 01/20/20 15:19 95-50-1 1,3-Dichlorobenzene ND ug/L 250 54.2 250 01/20/20 15:19 541-73-1 1,4-Dichlorobenzene ND ug/L 250 64.5 250 01/20/20 15:19 106-46-7 Dichlorodifluoromethane ND ug/L 250 56.5 250 01/20/20 15:19 75-71-8 1,1-Dichloroethane ND ug/L 250 67.0 250 01/20/20 15:19 75-34-3 1,2-Dichloroethane ND ug/L 250 84.0 250 01/20/20 15:19 107-06-2 1,1-Dichloroethene 471 ug/L 250 61.2 250 01/20/20 15:19 75-35-4 cis-1,2-Dichloroethene 2020 ug/L 250 72.8 250 01/20/20 15:19 156-59-2 trans-1,2-Dichloroethene ND ug/L 250 63.5 250 01/20/20 15:19 156-60-5 1,2-Dichloropropane ND ug/L 250 46.8 250 01/20/20 15:19 78-87-5 1,3-Dichloropropane ND ug/L 250 39.5 250 01/20/20 15:19 142-28-9 2,2-Dichloropropane ND ug/L 250 67.5 250 01/20/20 15:19 594-20-7 1,1-Dichloropropene ND ug/L 250 53.2 250 01/20/20 15:19 563-58-6 cis-1,3-Dichloropropene ND ug/L 250 74.0 250 01/20/20 15:19 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 250 77.2 250 01/20/20 15:19 10061-02-6 Diisopropyl ether ND ug/L 250 54.5 250 01/20/20 15:19 108-20-3 Ethylbenzene ND ug/L 250 64.0 250 01/20/20 15:19 100-41-4 Hexachloro-1,3-butadiene ND ug/L 250 110 250 01/20/20 15:19 87-68-3 2-Hexanone ND ug/L 1250 142 250 01/20/20 15:19 591-78-6 p-Isopropyltoluene ND ug/L 250 53.0 250 01/20/20 15:19 99-87-6 Methylene Chloride ND ug/L 1250 922 250 01/20/20 15:19 75-09-2 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 46 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-13B Lab ID: 92461009020 Collected: 01/14/20 11:50 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 1250 1130 250 01/20/20 15:19 108-10-1 ND ug/L 250 68.8 250 01/20/20 15:19 1634-04-4 ND ug/L 250 88.0 250 01/20/20 15:19 91-20-3 ND ug/L 250 66.8 250 01/20/20 15:19 100-42-5 ND ug/L 250 85.0 250 01/20/20 15:19 630-20-6 ND ug/L 250 55.5 250 01/20/20 15:19 79-34-5 9960 ug/L 250 40.5 250 01/20/20 15:19 127-18-4 ND ug/L 250 61.0 250 01/20/20 15:19 108-88-3 ND ug/L 250 86.0 250 01/20/20 15:19 87-61-6 ND ug/L 250 54.5 250 01/20/20 15:19 120-82-1 208J ug/L 250 43.8 250 01/20/20 15:19 71-55-6 ND ug/L 250 59.0 250 01/20/20 15:19 79-00-5 39400 ug/L 250 55.0 250 01/20/20 15:19 79-01-6 ND ug/L 250 77.8 250 01/20/20 15:19 75-69-4 ND ug/L 250 86.8 250 01/20/20 15:19 96-18-4 ND ug/L 500 362 250 01/20/20 15:19 108-05-4 IK ND ug/L 250 60.5 250 01/20/20 15:19 75-01-4 ND ug/L 250 158 250 01/20/20 15:19 1330-20-7 ND ug/L 500 102 250 01/20/20 15:19 179601-23-1 ND ug/L 250 55.0 250 01/20/20 15:19 95-47-6 99 % 70-130 250 01/20/20 15:19 460-00-4 94 % 70-130 250 01/20/20 15:19 17060-07-0 101 % 70-130 250 01/20/20 15:19 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 13.2 mg/L 1.0 0.60 1 01/18/2010:09 16887-00-6 M1 15.4 mg/L 1.0 0.50 1 01/18/2010:09 14808-79-8 M1 Analytical Method: SM 531OB-2011 0.61 J mg/L 1.0 0.50 1 01 /21 /20 06:17 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 47 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-DUP1 Lab ID: 92461009021 Collected: 01/15/20 11:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Ethene 6010 MET ICP Iron 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Date: 01/23/2020 03:52 PM Analytical Method: RSK-175 Preparation Method: RSK175 ND ug/L 13.0 4.26 1 01 /21 /20 14:46 01 /21 /20 14:46 74-85-1 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A 43.1 J ug/L 50.0 19.5 1 01 /21 /20 01:33 01 /22/20 05:25 7439-89-6 Analytical Method: EPA 8260D ND ug/L 6250 1540 250 01/23/20 01:31 67-64-1 ND ug/L 250 37.5 250 01/23/20 01:31 71-43-2 ND ug/L 250 55.0 250 01/23/20 01:31 108-86-1 ND ug/L 250 85.8 250 01/23/20 01:31 74-97-5 ND ug/L 250 64.0 250 01/23/20 01:31 75-27-4 ND ug/L 250 154 250 01/23/20 01:31 75-25-2 ND ug/L 500 155 250 01/23/20 01:31 74-83-9 ND ug/L 1250 832 250 01/23/20 01:31 78-93-3 ND ug/L 250 56.0 250 01/23/20 01:31 56-23-5 ND ug/L 250 58.2 250 01/23/20 01:31 108-90-7 ND ug/L 250 122 250 01/23/20 01:31 75-00-3 ND ug/L 1250 585 250 01/23/20 01:31 67-66-3 ND ug/L 250 97.2 250 01/23/20 01:31 74-87-3 ND ug/L 250 50.8 250 01/23/20 01:31 95-49-8 ND ug/L 250 51.0 250 01/23/20 01:31 106-43-4 ND ug/L 1250 64.2 250 01/23/20 01:31 96-12-8 ND ug/L 250 103 250 01/23/20 01:31 124-48-1 ND ug/L 250 64.5 250 01/23/20 01:31 106-93-4 ND ug/L 250 115 250 01/23/20 01:31 74-95-3 ND ug/L 250 72.8 250 01/23/20 01:31 95-50-1 ND ug/L 250 54.2 250 01/23/20 01:31 541-73-1 ND ug/L 250 64.5 250 01/23/20 01:31 106-46-7 ND ug/L 250 56.5 250 01/23/20 01:31 75-71-8 86.4.1 ug/L 250 67.0 250 01/23/20 01:31 75-34-3 ND ug/L 250 84.0 250 01/23/20 01:31 107-06-2 422 ug/L 250 61.2 250 01/23/20 01:31 75-35-4 1770 ug/L 250 72.8 250 01/23/20 01:31 156-59-2 ND ug/L 250 63.5 250 01/23/20 01:31 156-60-5 ND ug/L 250 46.8 250 01/23/20 01:31 78-87-5 ND ug/L 250 39.5 250 01/23/20 01:31 142-28-9 ND ug/L 250 67.5 250 01/23/20 01:31 594-20-7 ND ug/L 250 53.2 250 01/23/20 01:31 563-58-6 ND ug/L 250 74.0 250 01/23/20 01:31 10061-01-5 ND ug/L 250 77.2 250 01/23/20 01:31 10061-02-6 ND ug/L 250 54.5 250 01/23/20 01:31 108-20-3 ND ug/L 250 64.0 250 01/23/20 01:31 100-41-4 ND ug/L 250 110 250 01/23/20 01:31 87-68-3 ND ug/L 1250 142 250 01/23/20 01:31 591-78-6 ND ug/L 250 53.0 250 01/23/20 01:31 99-87-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IH,IK, L1.v1 Page 48 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-DUP1 Lab ID: 92461009021 Collected: 01/15/20 11:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 5310B TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 1250 922 250 01/23/20 01:31 75-09-2 ND ug/L 1250 1130 250 01/23/20 01:31 108-10-1 ND ug/L 250 68.8 250 01/23/20 01:31 1634-04-4 ND ug/L 250 88.0 250 01/23/20 01:31 91-20-3 ND ug/L 250 66.8 250 01/23/20 01:31 100-42-5 ND ug/L 250 85.0 250 01/23/20 01:31 630-20-6 ND ug/L 250 55.5 250 01/23/20 01:31 79-34-5 7380 ug/L 250 40.5 250 01/23/20 01:31 127-18-4 ND ug/L 250 61.0 250 01/23/20 01:31 108-88-3 ND ug/L 250 86.0 250 01/23/20 01:31 87-61-6 ND ug/L 250 54.5 250 01/23/20 01:31 120-82-1 430 ug/L 250 43.8 250 01/23/20 01:31 71-55-6 ND ug/L 250 59.0 250 01/23/20 01:31 79-00-5 41100 ug/L 250 55.0 250 01/23/20 01:31 79-01-6 ND ug/L 250 77.8 250 01/23/20 01:31 75-69-4 ND ug/L 250 86.8 250 01/23/20 01:31 96-18-4 ND ug/L 500 362 250 01/23/20 01:31 108-05-4 ND ug/L 250 60.5 250 01/23/20 01:31 75-01-4 ND ug/L 250 158 250 01/23/20 01:31 1330-20-7 ND ug/L 500 102 250 01/23/20 01:31 179601-23-1 ND ug/L 250 55.0 250 01/23/20 01:31 95-47-6 105 % 70-130 250 01/23/20 01:31 460-00-4 107 % 70-130 250 01/23/20 01:31 17060-07-0 98 % 70-130 250 01/23/20 01:31 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 25.4 mg/L 1.0 0.60 1 01/18/2010:51 16887-00-6 99.1 mg/L 2.0 1.0 2 01/18/2019:36 14808-79-8 Analytical Method: SM 531OB-2011 2.0 mg/L 1.0 0.50 1 01/21/2016:01 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 49 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-DUP2 Lab ID: 92461009022 Collected: 01/15/20 14:05 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual VOA (GC) RSK175 Ethene 6010 MET ICP Iron 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride Date: 01/23/2020 03:52 PM Analytical Method: RSK-175 Preparation Method: RSK175 ND ug/L 13.0 4.26 1 01 /21 /20 14:50 01 /21 /20 14:50 74-85-1 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A N D ug/L 50.0 19.5 1 01 /21 /20 01:33 01 /22/20 05:28 7439-89-6 Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/20/2012:38 67-64-1 ND ug/L 1.0 0.15 1 01 /20/20 12:38 71-43-2 ND ug/L 1.0 0.22 1 01/20/2012:38 108-86-1 ND ug/L 1.0 0.34 1 01/20/2012:38 74-97-5 ND ug/L 1.0 0.26 1 01/20/2012:38 75-27-4 ND ug/L 1.0 0.62 1 01/20/2012:38 75-25-2 ND ug/L 2.0 0.62 1 01/20/2012:38 74-83-9 ND ug/L 5.0 3.3 1 01/20/2012:38 78-93-3 ND ug/L 1.0 0.22 1 01/20/2012:38 56-23-5 ND ug/L 1.0 0.23 1 01/20/2012:38 108-90-7 ND ug/L 1.0 0.49 1 01/20/2012:38 75-00-3 ND ug/L 5.0 2.3 1 01/20/2012:38 67-66-3 ND ug/L 1.0 0.39 1 01/20/2012:38 74-87-3 ND ug/L 1.0 0.20 1 01/20/2012:38 95-49-8 ND ug/L 1.0 0.20 1 01/20/2012:38 106-43-4 ND ug/L 5.0 0.26 1 01/20/2012:38 96-12-8 ND ug/L 1.0 0.41 1 01/20/2012:38 124-48-1 ND ug/L 1.0 0.26 1 01/20/2012:38 106-93-4 ND ug/L 1.0 0.46 1 01/20/2012:38 74-95-3 ND ug/L 1.0 0.29 1 01/20/2012:38 95-50-1 ND ug/L 1.0 0.22 1 01/20/2012:38 541-73-1 ND ug/L 1.0 0.26 1 01/20/2012:38 106-46-7 ND ug/L 1.0 0.23 1 01 /20/20 12:38 75-71-8 0.40J ug/L 1.0 0.27 1 01/20/2012:38 75-34-3 ND ug/L 1.0 0.34 1 01/20/2012:38 107-06-2 ND ug/L 1.0 0.24 1 01/20/2012:38 75-35-4 64.9 ug/L 1.0 0.29 1 01/20/2012:38 156-59-2 1.0 ug/L 1.0 0.25 1 01/20/2012:38 156-60-5 ND ug/L 1.0 0.19 1 01/20/2012:38 78-87-5 ND ug/L 1.0 0.16 1 01/20/2012:38 142-28-9 ND ug/L 1.0 0.27 1 01/20/2012:38 594-20-7 ND ug/L 1.0 0.21 1 01/20/2012:38 563-58-6 ND ug/L 1.0 0.30 1 01 /20/20 12:38 10061-01-5 ND ug/L 1.0 0.31 1 01 /20/20 12:38 10061-02-6 ND ug/L 1.0 0.22 1 01/20/2012:38 108-20-3 ND ug/L 1.0 0.26 1 01 /20/20 12:38 100-41-4 ND ug/L 1.0 0.44 1 01/20/2012:38 87-68-3 ND ug/L 5.0 0.57 1 01 /20/20 12:38 591-78-6 ND ug/L 1.0 0.21 1 01/20/2012:38 99-87-6 ND ug/L 5.0 3.7 1 01/20/2012:38 75-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 v2 Page 50 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: PMW-DUP2 Lab ID: 92461009022 Collected: 01/15/20 14:05 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 300.0 IC Anions 28 Days Chloride Sulfate 531013 TOC Total Organic Carbon Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 5.0 4.5 1 01/20/2012:38 108-10-1 ND ug/L 1.0 0.28 1 01/20/2012:38 1634-04-4 ND ug/L 1.0 0.35 1 01 /20/20 12:38 91-20-3 ND ug/L 1.0 0.27 1 01/20/2012:38 100-42-5 ND ug/L 1.0 0.34 1 01/20/2012:38 630-20-6 ND ug/L 1.0 0.22 1 01/20/2012:38 79-34-5 44.5 ug/L 1.0 0.16 1 01/20/2012:38 127-18-4 ND ug/L 1.0 0.24 1 01/20/2012:38 108-88-3 ND ug/L 1.0 0.34 1 01 /20/20 12:38 87-61-6 0.39J ug/L 1.0 0.22 1 01/20/2012:38 120-82-1 ND ug/L 1.0 0.18 1 01 /20/20 12:38 71-55-6 ND ug/L 1.0 0.24 1 01/20/2012:38 79-00-5 39.0 ug/L 1.0 0.22 1 01/20/2012:38 79-01-6 ND ug/L 1.0 0.31 1 01/20/2012:38 75-69-4 ND ug/L 1.0 0.35 1 01/20/2012:38 96-18-4 ND ug/L 2.0 1.4 1 01/20/2012:38 108-05-4 IK ND ug/L 1.0 0.24 1 01 /20/20 12:38 75-01-4 ND ug/L 1.0 0.63 1 01/20/2012:38 1330-20-7 ND ug/L 2.0 0.41 1 01/20/2012:38 179601-23-1 ND ug/L 1.0 0.22 1 01/20/2012:38 95-47-6 100 % 70-130 1 01/20/2012:38 460-00-4 93 % 70-130 1 01/20/2012:38 17060-07-0 102 % 70-130 1 01/20/2012:38 2037-26-5 Analytical Method: EPA 300.0 Rev 2.1 1993 8.3 mg/L 1.0 0.60 1 01/18/2011:05 16887-00-6 265 mg/L 5.0 2.5 5 01/18/2019:51 14808-79-8 Analytical Method: SM 531OB-2011 1.2 mg/L 1.0 0.50 1 01/21/2016:53 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 51 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: SW-1 Lab ID: 92461009023 Collected: 01/15/20 16:25 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/19/20 00:06 67-64-1 ND ug/L 1.0 0.15 1 01/19/20 00:06 71-43-2 ND ug/L 1.0 0.22 1 01/19/20 00:06 108-86-1 ND ug/L 1.0 0.34 1 01/19/20 00:06 74-97-5 ND ug/L 1.0 0.26 1 01/19/20 00:06 75-27-4 ND ug/L 1.0 0.62 1 01/19/20 00:06 75-25-2 ND ug/L 2.0 0.62 1 01/19/20 00:06 74-83-9 ND ug/L 5.0 3.3 1 01/19/20 00:06 78-93-3 ND ug/L 1.0 0.22 1 01/19/20 00:06 56-23-5 ND ug/L 1.0 0.23 1 01/19/20 00:06 108-90-7 ND ug/L 1.0 0.49 1 01/19/20 00:06 75-00-3 ND ug/L 5.0 2.3 1 01/19/20 00:06 67-66-3 ND ug/L 1.0 0.39 1 01/19/20 00:06 74-87-3 ND ug/L 1.0 0.20 1 01/19/20 00:06 95-49-8 ND ug/L 1.0 0.20 1 01/19/20 00:06 106-43-4 ND ug/L 5.0 0.26 1 01/19/20 00:06 96-12-8 ND ug/L 1.0 0.41 1 01/19/20 00:06 124-48-1 ND ug/L 1.0 0.26 1 01/19/20 00:06 106-93-4 ND ug/L 1.0 0.46 1 01/19/20 00:06 74-95-3 ND ug/L 1.0 0.29 1 01/19/20 00:06 95-50-1 ND ug/L 1.0 0.22 1 01/19/20 00:06 541-73-1 ND ug/L 1.0 0.26 1 01/19/20 00:06 106-46-7 ND ug/L 1.0 0.23 1 01/19/20 00:06 75-71-8 ND ug/L 1.0 0.27 1 01/19/20 00:06 75-34-3 ND ug/L 1.0 0.34 1 01/19/20 00:06 107-06-2 ND ug/L 1.0 0.24 1 01/19/20 00:06 75-35-4 4.7 ug/L 1.0 0.29 1 01/19/20 00:06 156-59-2 ND ug/L 1.0 0.25 1 01/19/20 00:06 156-60-5 ND ug/L 1.0 0.19 1 01/19/20 00:06 78-87-5 ND ug/L 1.0 0.16 1 01/19/20 00:06 142-28-9 ND ug/L 1.0 0.27 1 01/19/20 00:06 594-20-7 ND ug/L 1.0 0.21 1 01/19/20 00:06 563-58-6 ND ug/L 1.0 0.30 1 01/19/20 00:06 10061-01-5 ND ug/L 1.0 0.31 1 01/19/20 00:06 10061-02-6 ND ug/L 1.0 0.22 1 01/19/20 00:06 108-20-3 ND ug/L 1.0 0.26 1 01/19/20 00:06 100-41-4 ND ug/L 1.0 0.44 1 01/19/20 00:06 87-68-3 ND ug/L 5.0 0.57 1 01/19/20 00:06 591-78-6 ND ug/L 1.0 0.21 1 01/19/20 00:06 99-87-6 ND ug/L 5.0 3.7 1 01/19/20 00:06 75-09-2 ND ug/L 5.0 4.5 1 01/19/20 00:06 108-10-1 ND ug/L 1.0 0.28 1 01/19/20 00:06 1634-04-4 ND ug/L 1.0 0.35 1 01/19/20 00:06 91-20-3 ND ug/L 1.0 0.27 1 01/19/20 00:06 100-42-5 ND ug/L 1.0 0.34 1 01/19/20 00:06 630-20-6 ND ug/L 1.0 0.22 1 01/19/20 00:06 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2 IL v2 v2 Page 52 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: SW-1 Lab ID: 92461009023 Collected: 01/15/20 16:25 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene ND ug/L 1.0 0.16 1 01/19/20 00:06 127-18-4 Toluene 0.26J ug/L 1.0 0.24 1 01/19/20 00:06 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/19/20 00:06 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/19/20 00:06 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/19/20 00:06 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/19/20 00:06 79-00-5 Trichloroethene 26.4 ug/L 1.0 0.22 1 01/19/20 00:06 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/19/20 00:06 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/19/20 00:06 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/19/20 00:06 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/19/20 00:06 75-01-4 v2 Xylene (Total) ND ug/L 1.0 0.63 1 01/19/20 00:06 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/19/20 00:06 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/19/20 00:06 95-47-6 Surrogates 4-Bromofluorobenzene (S) 104 % 70-130 1 01/19/20 00:06 460-00-4 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 01/19/20 00:06 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 01/19/20 00:06 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 53 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: SW-2 Lab ID: 92461009024 Collected: 01/15/20 16:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/19/20 02:20 67-64-1 ND ug/L 1.0 0.15 1 01/19/20 02:20 71-43-2 ND ug/L 1.0 0.22 1 01/19/20 02:20 108-86-1 ND ug/L 1.0 0.34 1 01/19/20 02:20 74-97-5 ND ug/L 1.0 0.26 1 01/19/20 02:20 75-27-4 ND ug/L 1.0 0.62 1 01/19/20 02:20 75-25-2 ND ug/L 2.0 0.62 1 01/19/20 02:20 74-83-9 ND ug/L 5.0 3.3 1 01/19/20 02:20 78-93-3 ND ug/L 1.0 0.22 1 01/19/20 02:20 56-23-5 ND ug/L 1.0 0.23 1 01/19/20 02:20 108-90-7 ND ug/L 1.0 0.49 1 01/19/20 02:20 75-00-3 ND ug/L 5.0 2.3 1 01/19/20 02:20 67-66-3 ND ug/L 1.0 0.39 1 01/19/20 02:20 74-87-3 ND ug/L 1.0 0.20 1 01/19/20 02:20 95-49-8 ND ug/L 1.0 0.20 1 01/19/20 02:20 106-43-4 ND ug/L 5.0 0.26 1 01/19/20 02:20 96-12-8 ND ug/L 1.0 0.41 1 01/19/20 02:20 124-48-1 ND ug/L 1.0 0.26 1 01/19/20 02:20 106-93-4 ND ug/L 1.0 0.46 1 01/19/20 02:20 74-95-3 ND ug/L 1.0 0.29 1 01/19/20 02:20 95-50-1 ND ug/L 1.0 0.22 1 01/19/20 02:20 541-73-1 ND ug/L 1.0 0.26 1 01/19/20 02:20 106-46-7 ND ug/L 1.0 0.23 1 01/19/20 02:20 75-71-8 ND ug/L 1.0 0.27 1 01/19/20 02:20 75-34-3 ND ug/L 1.0 0.34 1 01/19/20 02:20 107-06-2 ND ug/L 1.0 0.24 1 01/19/20 02:20 75-35-4 7.6 ug/L 1.0 0.29 1 01/19/20 02:20 156-59-2 ND ug/L 1.0 0.25 1 01/19/20 02:20 156-60-5 ND ug/L 1.0 0.19 1 01/19/20 02:20 78-87-5 ND ug/L 1.0 0.16 1 01/19/20 02:20 142-28-9 ND ug/L 1.0 0.27 1 01/19/20 02:20 594-20-7 ND ug/L 1.0 0.21 1 01/19/20 02:20 563-58-6 ND ug/L 1.0 0.30 1 01/19/20 02:20 10061-01-5 ND ug/L 1.0 0.31 1 01/19/20 02:20 10061-02-6 ND ug/L 1.0 0.22 1 01/19/20 02:20 108-20-3 ND ug/L 1.0 0.26 1 01/19/20 02:20 100-41-4 ND ug/L 1.0 0.44 1 01/19/20 02:20 87-68-3 ND ug/L 5.0 0.57 1 01/19/20 02:20 591-78-6 ND ug/L 1.0 0.21 1 01/19/20 02:20 99-87-6 ND ug/L 5.0 3.7 1 01/19/20 02:20 75-09-2 ND ug/L 5.0 4.5 1 01/19/20 02:20 108-10-1 ND ug/L 1.0 0.28 1 01/19/20 02:20 1634-04-4 ND ug/L 1.0 0.35 1 01/19/20 02:20 91-20-3 ND ug/L 1.0 0.27 1 01/19/20 02:20 100-42-5 ND ug/L 1.0 0.34 1 01/19/20 02:20 630-20-6 ND ug/L 1.0 0.22 1 01/19/20 02:20 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 115 v2 v2 Page 54 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: SW-2 Lab ID: 92461009024 Collected: 01/15/20 16:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene 12.1 ug/L 1.0 0.16 1 01/19/20 02:20 127-18-4 Toluene ND ug/L 1.0 0.24 1 01/19/20 02:20 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/19/20 02:20 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/19/20 02:20 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/19/20 02:20 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/19/20 02:20 79-00-5 Trichloroethene 55.4 ug/L 1.0 0.22 1 01/19/20 02:20 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/19/20 02:20 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/19/20 02:20 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/19/20 02:20 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/19/20 02:20 75-01-4 Xylene (Total) ND ug/L 1.0 0.63 1 01/19/20 02:20 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/19/20 02:20 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/19/20 02:20 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 01/19/20 02:20 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 01/19/20 02:20 17060-07-0 Toluene-d8 (S) 104 % 70-130 1 01/19/20 02:20 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 55 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: SW-3 Lab ID: 92461009025 Collected: 01/15/20 16:05 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/19/20 02:37 67-64-1 ND ug/L 1.0 0.15 1 01/19/20 02:37 71-43-2 ND ug/L 1.0 0.22 1 01/19/20 02:37 108-86-1 ND ug/L 1.0 0.34 1 01/19/20 02:37 74-97-5 ND ug/L 1.0 0.26 1 01/19/20 02:37 75-27-4 ND ug/L 1.0 0.62 1 01/19/20 02:37 75-25-2 ND ug/L 2.0 0.62 1 01/19/20 02:37 74-83-9 ND ug/L 5.0 3.3 1 01/19/20 02:37 78-93-3 ND ug/L 1.0 0.22 1 01/19/20 02:37 56-23-5 ND ug/L 1.0 0.23 1 01/19/20 02:37 108-90-7 ND ug/L 1.0 0.49 1 01/19/20 02:37 75-00-3 ND ug/L 5.0 2.3 1 01/19/20 02:37 67-66-3 ND ug/L 1.0 0.39 1 01/19/20 02:37 74-87-3 ND ug/L 1.0 0.20 1 01/19/20 02:37 95-49-8 ND ug/L 1.0 0.20 1 01/19/20 02:37 106-43-4 ND ug/L 5.0 0.26 1 01/19/20 02:37 96-12-8 ND ug/L 1.0 0.41 1 01/19/20 02:37 124-48-1 ND ug/L 1.0 0.26 1 01/19/20 02:37 106-93-4 ND ug/L 1.0 0.46 1 01/19/20 02:37 74-95-3 ND ug/L 1.0 0.29 1 01/19/20 02:37 95-50-1 ND ug/L 1.0 0.22 1 01/19/20 02:37 541-73-1 ND ug/L 1.0 0.26 1 01/19/20 02:37 106-46-7 ND ug/L 1.0 0.23 1 01/19/20 02:37 75-71-8 ND ug/L 1.0 0.27 1 01/19/20 02:37 75-34-3 ND ug/L 1.0 0.34 1 01/19/20 02:37 107-06-2 ND ug/L 1.0 0.24 1 01/19/20 02:37 75-35-4 5.2 ug/L 1.0 0.29 1 01/19/20 02:37 156-59-2 ND ug/L 1.0 0.25 1 01/19/20 02:37 156-60-5 ND ug/L 1.0 0.19 1 01/19/20 02:37 78-87-5 ND ug/L 1.0 0.16 1 01/19/20 02:37 142-28-9 ND ug/L 1.0 0.27 1 01/19/20 02:37 594-20-7 ND ug/L 1.0 0.21 1 01/19/20 02:37 563-58-6 ND ug/L 1.0 0.30 1 01/19/20 02:37 10061-01-5 ND ug/L 1.0 0.31 1 01/19/20 02:37 10061-02-6 ND ug/L 1.0 0.22 1 01/19/20 02:37 108-20-3 ND ug/L 1.0 0.26 1 01/19/20 02:37 100-41-4 ND ug/L 1.0 0.44 1 01/19/20 02:37 87-68-3 ND ug/L 5.0 0.57 1 01/19/20 02:37 591-78-6 ND ug/L 1.0 0.21 1 01/19/20 02:37 99-87-6 ND ug/L 5.0 3.7 1 01/19/20 02:37 75-09-2 ND ug/L 5.0 4.5 1 01/19/20 02:37 108-10-1 ND ug/L 1.0 0.28 1 01/19/20 02:37 1634-04-4 ND ug/L 1.0 0.35 1 01/19/20 02:37 91-20-3 ND ug/L 1.0 0.27 1 01/19/20 02:37 100-42-5 ND ug/L 1.0 0.34 1 01/19/20 02:37 630-20-6 ND ug/L 1.0 0.22 1 01/19/20 02:37 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 115 v2 v2 Page 56 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: SW-3 Lab ID: 92461009025 Collected: 01/15/20 16:05 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene 8.2 ug/L 1.0 0.16 1 01/19/20 02:37 127-18-4 Toluene ND ug/L 1.0 0.24 1 01/19/20 02:37 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/19/20 02:37 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/19/20 02:37 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/19/20 02:37 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/19/20 02:37 79-00-5 Trichloroethene 35.3 ug/L 1.0 0.22 1 01/19/20 02:37 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/19/20 02:37 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/19/20 02:37 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/19/20 02:37 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/19/20 02:37 75-01-4 Xylene (Total) ND ug/L 1.0 0.63 1 01/19/20 02:37 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/19/20 02:37 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/19/20 02:37 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 01/19/20 02:37 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 01/19/20 02:37 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 01/19/20 02:37 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 57 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: EB-1 Lab ID: 92461009026 Collected: 01/14/20 16:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/18/20 22:46 67-64-1 ND ug/L 1.0 0.15 1 01/18/20 22:46 71-43-2 ND ug/L 1.0 0.22 1 01/18/20 22:46 108-86-1 ND ug/L 1.0 0.34 1 01/18/20 22:46 74-97-5 ND ug/L 1.0 0.26 1 01/18/20 22:46 75-27-4 ND ug/L 1.0 0.62 1 01/18/20 22:46 75-25-2 ND ug/L 2.0 0.62 1 01/18/20 22:46 74-83-9 ND ug/L 5.0 3.3 1 01/18/20 22:46 78-93-3 ND ug/L 1.0 0.22 1 01/18/20 22:46 56-23-5 ND ug/L 1.0 0.23 1 01/18/20 22:46 108-90-7 ND ug/L 1.0 0.49 1 01/18/20 22:46 75-00-3 ND ug/L 5.0 2.3 1 01/18/20 22:46 67-66-3 ND ug/L 1.0 0.39 1 01/18/20 22:46 74-87-3 ND ug/L 1.0 0.20 1 01/18/20 22:46 95-49-8 ND ug/L 1.0 0.20 1 01/18/20 22:46 106-43-4 ND ug/L 5.0 0.26 1 01/18/20 22:46 96-12-8 ND ug/L 1.0 0.41 1 01/18/20 22:46 124-48-1 ND ug/L 1.0 0.26 1 01/18/20 22:46 106-93-4 ND ug/L 1.0 0.46 1 01/18/20 22:46 74-95-3 ND ug/L 1.0 0.29 1 01/18/20 22:46 95-50-1 ND ug/L 1.0 0.22 1 01/18/20 22:46 541-73-1 ND ug/L 1.0 0.26 1 01/18/20 22:46 106-46-7 ND ug/L 1.0 0.23 1 01/18/20 22:46 75-71-8 ND ug/L 1.0 0.27 1 01/18/20 22:46 75-34-3 ND ug/L 1.0 0.34 1 01/18/20 22:46 107-06-2 ND ug/L 1.0 0.24 1 01/18/20 22:46 75-35-4 ND ug/L 1.0 0.29 1 01/18/20 22:46 156-59-2 ND ug/L 1.0 0.25 1 01/18/20 22:46 156-60-5 ND ug/L 1.0 0.19 1 01/18/20 22:46 78-87-5 ND ug/L 1.0 0.16 1 01/18/20 22:46 142-28-9 ND ug/L 1.0 0.27 1 01/18/20 22:46 594-20-7 ND ug/L 1.0 0.21 1 01/18/20 22:46 563-58-6 ND ug/L 1.0 0.30 1 01/18/20 22:46 10061-01-5 ND ug/L 1.0 0.31 1 01/18/20 22:46 10061-02-6 ND ug/L 1.0 0.22 1 01/18/20 22:46 108-20-3 ND ug/L 1.0 0.26 1 01/18/20 22:46 100-41-4 ND ug/L 1.0 0.44 1 01/18/20 22:46 87-68-3 ND ug/L 5.0 0.57 1 01/18/20 22:46 591-78-6 ND ug/L 1.0 0.21 1 01/18/20 22:46 99-87-6 ND ug/L 5.0 3.7 1 01/18/20 22:46 75-09-2 ND ug/L 5.0 4.5 1 01/18/20 22:46 108-10-1 ND ug/L 1.0 0.28 1 01/18/20 22:46 1634-04-4 ND ug/L 1.0 0.35 1 01/18/20 22:46 91-20-3 ND ug/L 1.0 0.27 1 01/18/20 22:46 100-42-5 ND ug/L 1.0 0.34 1 01/18/20 22:46 630-20-6 ND ug/L 1.0 0.22 1 01/18/20 22:46 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 115 v2 v2 Page 58 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: E13-1 Lab ID: 92461009026 Collected: 01/14/20 16:15 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene ND ug/L 1.0 0.16 1 01/18/20 22:46 127-18-4 Toluene ND ug/L 1.0 0.24 1 01/18/20 22:46 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/18/20 22:46 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/18/20 22:46 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/18/20 22:46 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/18/20 22:46 79-00-5 Trichloroethene ND ug/L 1.0 0.22 1 01/18/20 22:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/18/20 22:46 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/18/20 22:46 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/18/20 22:46 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/18/20 22:46 75-01-4 Xylene (Total) ND ug/L 1.0 0.63 1 01/18/20 22:46 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/18/20 22:46 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/18/20 22:46 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 01/18/20 22:46 460-00-4 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 01/18/20 22:46 17060-07-0 Toluene-d8 (S) 104 % 70-130 1 01/18/20 22:46 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 59 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: EB-2 Lab ID: 92461009027 Collected: 01/15/20 17:05 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/18/20 23:04 67-64-1 ND ug/L 1.0 0.15 1 01/18/20 23:04 71-43-2 ND ug/L 1.0 0.22 1 01/18/20 23:04 108-86-1 ND ug/L 1.0 0.34 1 01/18/20 23:04 74-97-5 ND ug/L 1.0 0.26 1 01/18/20 23:04 75-27-4 ND ug/L 1.0 0.62 1 01/18/20 23:04 75-25-2 ND ug/L 2.0 0.62 1 01/18/20 23:04 74-83-9 ND ug/L 5.0 3.3 1 01/18/20 23:04 78-93-3 ND ug/L 1.0 0.22 1 01/18/20 23:04 56-23-5 ND ug/L 1.0 0.23 1 01/18/20 23:04 108-90-7 ND ug/L 1.0 0.49 1 01/18/20 23:04 75-00-3 ND ug/L 5.0 2.3 1 01/18/20 23:04 67-66-3 ND ug/L 1.0 0.39 1 01/18/20 23:04 74-87-3 ND ug/L 1.0 0.20 1 01/18/20 23:04 95-49-8 ND ug/L 1.0 0.20 1 01/18/20 23:04 106-43-4 ND ug/L 5.0 0.26 1 01/18/20 23:04 96-12-8 ND ug/L 1.0 0.41 1 01/18/20 23:04 124-48-1 ND ug/L 1.0 0.26 1 01/18/20 23:04 106-93-4 ND ug/L 1.0 0.46 1 01/18/20 23:04 74-95-3 ND ug/L 1.0 0.29 1 01/18/20 23:04 95-50-1 ND ug/L 1.0 0.22 1 01/18/20 23:04 541-73-1 ND ug/L 1.0 0.26 1 01/18/20 23:04 106-46-7 ND ug/L 1.0 0.23 1 01/18/20 23:04 75-71-8 ND ug/L 1.0 0.27 1 01/18/20 23:04 75-34-3 ND ug/L 1.0 0.34 1 01/18/20 23:04 107-06-2 ND ug/L 1.0 0.24 1 01/18/20 23:04 75-35-4 ND ug/L 1.0 0.29 1 01/18/20 23:04 156-59-2 ND ug/L 1.0 0.25 1 01/18/20 23:04 156-60-5 ND ug/L 1.0 0.19 1 01/18/20 23:04 78-87-5 ND ug/L 1.0 0.16 1 01/18/20 23:04 142-28-9 ND ug/L 1.0 0.27 1 01/18/20 23:04 594-20-7 ND ug/L 1.0 0.21 1 01/18/20 23:04 563-58-6 ND ug/L 1.0 0.30 1 01/18/20 23:04 10061-01-5 ND ug/L 1.0 0.31 1 01/18/20 23:04 10061-02-6 ND ug/L 1.0 0.22 1 01/18/20 23:04 108-20-3 ND ug/L 1.0 0.26 1 01/18/20 23:04 100-41-4 ND ug/L 1.0 0.44 1 01/18/20 23:04 87-68-3 ND ug/L 5.0 0.57 1 01/18/20 23:04 591-78-6 ND ug/L 1.0 0.21 1 01/18/20 23:04 99-87-6 ND ug/L 5.0 3.7 1 01/18/20 23:04 75-09-2 ND ug/L 5.0 4.5 1 01/18/20 23:04 108-10-1 ND ug/L 1.0 0.28 1 01/18/20 23:04 1634-04-4 ND ug/L 1.0 0.35 1 01/18/20 23:04 91-20-3 ND ug/L 1.0 0.27 1 01/18/20 23:04 100-42-5 ND ug/L 1.0 0.34 1 01/18/20 23:04 630-20-6 ND ug/L 1.0 0.22 1 01/18/20 23:04 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 115 v2 v2 Page 60 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: E13-2 Lab ID: 92461009027 Collected: 01/15/20 17:05 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene ND ug/L 1.0 0.16 1 01/18/20 23:04 127-18-4 Toluene ND ug/L 1.0 0.24 1 01/18/20 23:04 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/18/20 23:04 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/18/20 23:04 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/18/20 23:04 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/18/20 23:04 79-00-5 Trichloroethene ND ug/L 1.0 0.22 1 01/18/20 23:04 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/18/20 23:04 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/18/20 23:04 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/18/20 23:04 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/18/20 23:04 75-01-4 Xylene (Total) ND ug/L 1.0 0.63 1 01/18/20 23:04 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/18/20 23:04 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/18/20 23:04 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 01/18/20 23:04 460-00-4 1,2-Dichloroethane-d4 (S) 86 % 70-130 1 01/18/20 23:04 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 01/18/20 23:04 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 61 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: Trip Blank 1 Lab ID: 92461009028 Collected: 01/14/20 08:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/18/20 23:22 67-64-1 ND ug/L 1.0 0.15 1 01/18/20 23:22 71-43-2 ND ug/L 1.0 0.22 1 01/18/20 23:22 108-86-1 ND ug/L 1.0 0.34 1 01/18/20 23:22 74-97-5 ND ug/L 1.0 0.26 1 01/18/20 23:22 75-27-4 ND ug/L 1.0 0.62 1 01/18/20 23:22 75-25-2 ND ug/L 2.0 0.62 1 01/18/20 23:22 74-83-9 ND ug/L 5.0 3.3 1 01/18/20 23:22 78-93-3 ND ug/L 1.0 0.22 1 01/18/20 23:22 56-23-5 ND ug/L 1.0 0.23 1 01/18/20 23:22 108-90-7 ND ug/L 1.0 0.49 1 01/18/20 23:22 75-00-3 ND ug/L 5.0 2.3 1 01/18/20 23:22 67-66-3 ND ug/L 1.0 0.39 1 01/18/20 23:22 74-87-3 ND ug/L 1.0 0.20 1 01/18/20 23:22 95-49-8 ND ug/L 1.0 0.20 1 01/18/20 23:22 106-43-4 ND ug/L 5.0 0.26 1 01/18/20 23:22 96-12-8 ND ug/L 1.0 0.41 1 01/18/20 23:22 124-48-1 ND ug/L 1.0 0.26 1 01/18/20 23:22 106-93-4 ND ug/L 1.0 0.46 1 01/18/20 23:22 74-95-3 ND ug/L 1.0 0.29 1 01/18/20 23:22 95-50-1 ND ug/L 1.0 0.22 1 01/18/20 23:22 541-73-1 ND ug/L 1.0 0.26 1 01/18/20 23:22 106-46-7 ND ug/L 1.0 0.23 1 01/18/20 23:22 75-71-8 ND ug/L 1.0 0.27 1 01/18/20 23:22 75-34-3 ND ug/L 1.0 0.34 1 01/18/20 23:22 107-06-2 ND ug/L 1.0 0.24 1 01/18/20 23:22 75-35-4 ND ug/L 1.0 0.29 1 01/18/20 23:22 156-59-2 ND ug/L 1.0 0.25 1 01/18/20 23:22 156-60-5 ND ug/L 1.0 0.19 1 01/18/20 23:22 78-87-5 ND ug/L 1.0 0.16 1 01/18/20 23:22 142-28-9 ND ug/L 1.0 0.27 1 01/18/20 23:22 594-20-7 ND ug/L 1.0 0.21 1 01/18/20 23:22 563-58-6 ND ug/L 1.0 0.30 1 01/18/20 23:22 10061-01-5 ND ug/L 1.0 0.31 1 01/18/20 23:22 10061-02-6 ND ug/L 1.0 0.22 1 01/18/20 23:22 108-20-3 ND ug/L 1.0 0.26 1 01/18/20 23:22 100-41-4 ND ug/L 1.0 0.44 1 01/18/20 23:22 87-68-3 ND ug/L 5.0 0.57 1 01/18/20 23:22 591-78-6 ND ug/L 1.0 0.21 1 01/18/20 23:22 99-87-6 ND ug/L 5.0 3.7 1 01/18/20 23:22 75-09-2 ND ug/L 5.0 4.5 1 01/18/20 23:22 108-10-1 ND ug/L 1.0 0.28 1 01/18/20 23:22 1634-04-4 ND ug/L 1.0 0.35 1 01/18/20 23:22 91-20-3 ND ug/L 1.0 0.27 1 01/18/20 23:22 100-42-5 ND ug/L 1.0 0.34 1 01/18/20 23:22 630-20-6 ND ug/L 1.0 0.22 1 01/18/20 23:22 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 115 v2 v2 Page 62 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: Trip Blank 1 Lab ID: 92461009028 Collected: 01/14/20 08:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene ND ug/L 1.0 0.16 1 01/18/20 23:22 127-18-4 Toluene ND ug/L 1.0 0.24 1 01/18/20 23:22 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/18/20 23:22 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/18/20 23:22 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/18/20 23:22 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/18/20 23:22 79-00-5 Trichloroethene ND ug/L 1.0 0.22 1 01/18/20 23:22 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/18/20 23:22 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/18/20 23:22 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/18/20 23:22 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/18/20 23:22 75-01-4 Xylene (Total) ND ug/L 1.0 0.63 1 01/18/20 23:22 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/18/20 23:22 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/18/20 23:22 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 01/18/20 23:22 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 01/18/20 23:22 17060-07-0 Toluene-d8 (S) 103 % 70-130 1 01/18/20 23:22 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 63 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: Trip Blank 2 Lab ID: 92461009029 Collected: 01/14/20 16:20 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/18/20 23:39 67-64-1 ND ug/L 1.0 0.15 1 01/18/20 23:39 71-43-2 ND ug/L 1.0 0.22 1 01/18/20 23:39 108-86-1 ND ug/L 1.0 0.34 1 01/18/20 23:39 74-97-5 ND ug/L 1.0 0.26 1 01/18/20 23:39 75-27-4 ND ug/L 1.0 0.62 1 01/18/20 23:39 75-25-2 ND ug/L 2.0 0.62 1 01/18/20 23:39 74-83-9 ND ug/L 5.0 3.3 1 01/18/20 23:39 78-93-3 ND ug/L 1.0 0.22 1 01/18/20 23:39 56-23-5 ND ug/L 1.0 0.23 1 01/18/20 23:39 108-90-7 ND ug/L 1.0 0.49 1 01/18/20 23:39 75-00-3 ND ug/L 5.0 2.3 1 01/18/20 23:39 67-66-3 ND ug/L 1.0 0.39 1 01/18/20 23:39 74-87-3 ND ug/L 1.0 0.20 1 01/18/20 23:39 95-49-8 ND ug/L 1.0 0.20 1 01/18/20 23:39 106-43-4 ND ug/L 5.0 0.26 1 01/18/20 23:39 96-12-8 ND ug/L 1.0 0.41 1 01/18/20 23:39 124-48-1 ND ug/L 1.0 0.26 1 01/18/20 23:39 106-93-4 ND ug/L 1.0 0.46 1 01/18/20 23:39 74-95-3 ND ug/L 1.0 0.29 1 01/18/20 23:39 95-50-1 ND ug/L 1.0 0.22 1 01/18/20 23:39 541-73-1 ND ug/L 1.0 0.26 1 01/18/20 23:39 106-46-7 ND ug/L 1.0 0.23 1 01/18/20 23:39 75-71-8 ND ug/L 1.0 0.27 1 01/18/20 23:39 75-34-3 ND ug/L 1.0 0.34 1 01/18/20 23:39 107-06-2 ND ug/L 1.0 0.24 1 01/18/20 23:39 75-35-4 ND ug/L 1.0 0.29 1 01/18/20 23:39 156-59-2 ND ug/L 1.0 0.25 1 01/18/20 23:39 156-60-5 ND ug/L 1.0 0.19 1 01/18/20 23:39 78-87-5 ND ug/L 1.0 0.16 1 01/18/20 23:39 142-28-9 ND ug/L 1.0 0.27 1 01/18/20 23:39 594-20-7 ND ug/L 1.0 0.21 1 01/18/20 23:39 563-58-6 ND ug/L 1.0 0.30 1 01/18/20 23:39 10061-01-5 ND ug/L 1.0 0.31 1 01/18/20 23:39 10061-02-6 ND ug/L 1.0 0.22 1 01/18/20 23:39 108-20-3 ND ug/L 1.0 0.26 1 01/18/20 23:39 100-41-4 ND ug/L 1.0 0.44 1 01/18/20 23:39 87-68-3 ND ug/L 5.0 0.57 1 01/18/20 23:39 591-78-6 ND ug/L 1.0 0.21 1 01/18/20 23:39 99-87-6 ND ug/L 5.0 3.7 1 01/18/20 23:39 75-09-2 ND ug/L 5.0 4.5 1 01/18/20 23:39 108-10-1 ND ug/L 1.0 0.28 1 01/18/20 23:39 1634-04-4 ND ug/L 1.0 0.35 1 01/18/20 23:39 91-20-3 ND ug/L 1.0 0.27 1 01/18/20 23:39 100-42-5 ND ug/L 1.0 0.34 1 01/18/20 23:39 630-20-6 ND ug/L 1.0 0.22 1 01/18/20 23:39 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 115 v2 v2 Page 64 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: Trip Blank 2 Lab ID: 92461009029 Collected: 01/14/20 16:20 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene ND ug/L 1.0 0.16 1 01/18/20 23:39 127-18-4 Toluene ND ug/L 1.0 0.24 1 01/18/20 23:39 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/18/20 23:39 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/18/20 23:39 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/18/20 23:39 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/18/20 23:39 79-00-5 Trichloroethene ND ug/L 1.0 0.22 1 01/18/20 23:39 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/18/20 23:39 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/18/20 23:39 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/18/20 23:39 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/18/20 23:39 75-01-4 Xylene (Total) ND ug/L 1.0 0.63 1 01/18/20 23:39 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/18/20 23:39 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/18/20 23:39 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 01/18/20 23:39 460-00-4 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 01/18/20 23:39 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 01/18/20 23:39 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 65 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: Trip Blank 3 Lab ID: 92461009030 Collected: 01/15/20 08:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/18/20 23:57 67-64-1 ND ug/L 1.0 0.15 1 01/18/20 23:57 71-43-2 ND ug/L 1.0 0.22 1 01/18/20 23:57 108-86-1 ND ug/L 1.0 0.34 1 01/18/20 23:57 74-97-5 ND ug/L 1.0 0.26 1 01/18/20 23:57 75-27-4 ND ug/L 1.0 0.62 1 01/18/20 23:57 75-25-2 ND ug/L 2.0 0.62 1 01/18/20 23:57 74-83-9 ND ug/L 5.0 3.3 1 01/18/20 23:57 78-93-3 ND ug/L 1.0 0.22 1 01/18/20 23:57 56-23-5 ND ug/L 1.0 0.23 1 01/18/20 23:57 108-90-7 ND ug/L 1.0 0.49 1 01/18/20 23:57 75-00-3 ND ug/L 5.0 2.3 1 01/18/20 23:57 67-66-3 ND ug/L 1.0 0.39 1 01/18/20 23:57 74-87-3 ND ug/L 1.0 0.20 1 01/18/20 23:57 95-49-8 ND ug/L 1.0 0.20 1 01/18/20 23:57 106-43-4 ND ug/L 5.0 0.26 1 01/18/20 23:57 96-12-8 ND ug/L 1.0 0.41 1 01/18/20 23:57 124-48-1 ND ug/L 1.0 0.26 1 01/18/20 23:57 106-93-4 ND ug/L 1.0 0.46 1 01/18/20 23:57 74-95-3 ND ug/L 1.0 0.29 1 01/18/20 23:57 95-50-1 ND ug/L 1.0 0.22 1 01/18/20 23:57 541-73-1 ND ug/L 1.0 0.26 1 01/18/20 23:57 106-46-7 ND ug/L 1.0 0.23 1 01/18/20 23:57 75-71-8 ND ug/L 1.0 0.27 1 01/18/20 23:57 75-34-3 ND ug/L 1.0 0.34 1 01/18/20 23:57 107-06-2 ND ug/L 1.0 0.24 1 01/18/20 23:57 75-35-4 ND ug/L 1.0 0.29 1 01/18/20 23:57 156-59-2 ND ug/L 1.0 0.25 1 01/18/20 23:57 156-60-5 ND ug/L 1.0 0.19 1 01/18/20 23:57 78-87-5 ND ug/L 1.0 0.16 1 01/18/20 23:57 142-28-9 ND ug/L 1.0 0.27 1 01/18/20 23:57 594-20-7 ND ug/L 1.0 0.21 1 01/18/20 23:57 563-58-6 ND ug/L 1.0 0.30 1 01/18/20 23:57 10061-01-5 ND ug/L 1.0 0.31 1 01/18/20 23:57 10061-02-6 ND ug/L 1.0 0.22 1 01/18/20 23:57 108-20-3 ND ug/L 1.0 0.26 1 01/18/20 23:57 100-41-4 ND ug/L 1.0 0.44 1 01/18/20 23:57 87-68-3 ND ug/L 5.0 0.57 1 01/18/20 23:57 591-78-6 ND ug/L 1.0 0.21 1 01/18/20 23:57 99-87-6 ND ug/L 5.0 3.7 1 01/18/20 23:57 75-09-2 ND ug/L 5.0 4.5 1 01/18/20 23:57 108-10-1 ND ug/L 1.0 0.28 1 01/18/20 23:57 1634-04-4 ND ug/L 1.0 0.35 1 01/18/20 23:57 91-20-3 ND ug/L 1.0 0.27 1 01/18/20 23:57 100-42-5 ND ug/L 1.0 0.34 1 01/18/20 23:57 630-20-6 ND ug/L 1.0 0.22 1 01/18/20 23:57 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 115 v2 v2 Page 66 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: Trip Blank 3 Lab ID: 92461009030 Collected: 01/15/20 08:00 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene ND ug/L 1.0 0.16 1 01/18/20 23:57 127-18-4 Toluene ND ug/L 1.0 0.24 1 01/18/20 23:57 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/18/20 23:57 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/18/20 23:57 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/18/20 23:57 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/18/20 23:57 79-00-5 Trichloroethene ND ug/L 1.0 0.22 1 01/18/20 23:57 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/18/20 23:57 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/18/20 23:57 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/18/20 23:57 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/18/20 23:57 75-01-4 Xylene (Total) ND ug/L 1.0 0.63 1 01/18/20 23:57 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/18/20 23:57 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/18/20 23:57 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 01/18/20 23:57 460-00-4 1,2-Dichloroethane-d4 (S) 90 % 70-130 1 01/18/20 23:57 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 01/18/20 23:57 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 67 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: Trip Blank 4 Lab ID: 92461009031 Collected: 01/15/20 17:10 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 01/23/2020 03:52 PM Analytical Method: EPA 8260D ND ug/L 25.0 6.2 1 01/19/20 00:15 67-64-1 ND ug/L 1.0 0.15 1 01/19/20 00:15 71-43-2 ND ug/L 1.0 0.22 1 01/19/20 00:15 108-86-1 ND ug/L 1.0 0.34 1 01/19/20 00:15 74-97-5 ND ug/L 1.0 0.26 1 01/19/20 00:15 75-27-4 ND ug/L 1.0 0.62 1 01/19/20 00:15 75-25-2 ND ug/L 2.0 0.62 1 01/19/20 00:15 74-83-9 ND ug/L 5.0 3.3 1 01/19/20 00:15 78-93-3 ND ug/L 1.0 0.22 1 01/19/20 00:15 56-23-5 ND ug/L 1.0 0.23 1 01/19/20 00:15 108-90-7 ND ug/L 1.0 0.49 1 01/19/20 00:15 75-00-3 ND ug/L 5.0 2.3 1 01/19/20 00:15 67-66-3 ND ug/L 1.0 0.39 1 01/19/20 00:15 74-87-3 ND ug/L 1.0 0.20 1 01/19/20 00:15 95-49-8 ND ug/L 1.0 0.20 1 01/19/20 00:15 106-43-4 ND ug/L 5.0 0.26 1 01/19/20 00:15 96-12-8 ND ug/L 1.0 0.41 1 01/19/20 00:15 124-48-1 ND ug/L 1.0 0.26 1 01/19/20 00:15 106-93-4 ND ug/L 1.0 0.46 1 01/19/20 00:15 74-95-3 ND ug/L 1.0 0.29 1 01/19/20 00:15 95-50-1 ND ug/L 1.0 0.22 1 01/19/20 00:15 541-73-1 ND ug/L 1.0 0.26 1 01/19/20 00:15 106-46-7 ND ug/L 1.0 0.23 1 01/19/20 00:15 75-71-8 ND ug/L 1.0 0.27 1 01/19/20 00:15 75-34-3 ND ug/L 1.0 0.34 1 01/19/20 00:15 107-06-2 ND ug/L 1.0 0.24 1 01/19/20 00:15 75-35-4 ND ug/L 1.0 0.29 1 01/19/20 00:15 156-59-2 ND ug/L 1.0 0.25 1 01/19/20 00:15 156-60-5 ND ug/L 1.0 0.19 1 01/19/20 00:15 78-87-5 ND ug/L 1.0 0.16 1 01/19/20 00:15 142-28-9 ND ug/L 1.0 0.27 1 01/19/20 00:15 594-20-7 ND ug/L 1.0 0.21 1 01/19/20 00:15 563-58-6 ND ug/L 1.0 0.30 1 01/19/20 00:15 10061-01-5 ND ug/L 1.0 0.31 1 01/19/20 00:15 10061-02-6 ND ug/L 1.0 0.22 1 01/19/20 00:15 108-20-3 ND ug/L 1.0 0.26 1 01/19/20 00:15 100-41-4 ND ug/L 1.0 0.44 1 01/19/20 00:15 87-68-3 ND ug/L 5.0 0.57 1 01/19/20 00:15 591-78-6 ND ug/L 1.0 0.21 1 01/19/20 00:15 99-87-6 ND ug/L 5.0 3.7 1 01/19/20 00:15 75-09-2 ND ug/L 5.0 4.5 1 01/19/20 00:15 108-10-1 ND ug/L 1.0 0.28 1 01/19/20 00:15 1634-04-4 ND ug/L 1.0 0.35 1 01/19/20 00:15 91-20-3 ND ug/L 1.0 0.27 1 01/19/20 00:15 100-42-5 ND ug/L 1.0 0.34 1 01/19/20 00:15 630-20-6 ND ug/L 1.0 0.22 1 01/19/20 00:15 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 115 v2 v2 Page 68 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Trex-Charlotte GW Pace Project No.: 92461009 Sample: Trip Blank 4 Lab ID: 92461009031 Collected: 01/15/20 17:10 Received: 01/16/20 09:47 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Tetrachloroethene ND ug/L 1.0 0.16 1 01/19/20 00:15 127-18-4 Toluene ND ug/L 1.0 0.24 1 01/19/20 00:15 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.34 1 01/19/20 00:15 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.22 1 01/19/20 00:15 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.18 1 01/19/20 00:15 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.24 1 01/19/20 00:15 79-00-5 Trichloroethene ND ug/L 1.0 0.22 1 01/19/20 00:15 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.31 1 01/19/20 00:15 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 01/19/20 00:15 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 01/19/20 00:15 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 01/19/20 00:15 75-01-4 Xylene (Total) ND ug/L 1.0 0.63 1 01/19/20 00:15 1330-20-7 m&p-Xylene ND ug/L 2.0 0.41 1 01/19/20 00:15 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 01/19/20 00:15 95-47-6 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 01/19/20 00:15 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 01/19/20 00:15 17060-07-0 Toluene-d8 (S) 106 % 70-130 1 01/19/20 00:15 2037-26-5 Date: 01/23/2020 03:52 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 69 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 1413908 Analysis Method: RSK-175 QC Batch Method: RSK175 Analysis Description: VOA (GC) RSK175 Associated Lab Samples: 92461009001, 92461009002, 92461009003, 92461009004, 92461009005, 92461009006, 92461009007, 92461009008,92461009009,92461009010,92461009011,92461009012 METHOD BLANK: R3492339-1 Matrix: Water Associated Lab Samples: 92461009001, 92461009002, 92461009003, 92461009004, 92461009005, 92461009006, 92461009007, 92461009008,92461009009,92461009010,92461009011,92461009012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Ethene ug/L ND 13.0 4.26 01/20/2014:08 LABORATORY CONTROL SAMPLE & LCSD: R3492339-4 R3492339-5 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Ethene ug/L 127 119 117 93.7 92.1 85.0-115 1.69 20 SAMPLE DUPLICATE: R3492339-2 92461009001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Ethene ug/L ND ND 0.00 20 SAMPLE DUPLICATE: R3492339-3 92461009011 Dup Max Parameter Units Result Result RPD RPD Qualifiers Ethene ug/L ND ND 0.00 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 70 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 1414316 Analysis Method: RSK-175 QC Batch Method: RSK175 Analysis Description: VOA (GC) RSK175 Associated Lab Samples: 92461009013, 92461009014, 92461009015, 92461009016, 92461009017, 92461009018, 92461009019, 92461009020,92461009021,92461009022 METHOD BLANK: R3492685-1 Matrix: Water Associated Lab Samples: 92461009013, 92461009014, 92461009015, 92461009016, 92461009017, 92461009018, 92461009019, 92461009020,92461009021,92461009022 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Ethene ug/L ND 13.0 4.26 01/21/2011:54 LABORATORY CONTROL SAMPLE & LCSD: R3492685-6 R3492685-7 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Ethene ug/L 127 108 117 85.0 92.1 85.0-115 8.00 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3492685-4 R3492685-5 MS MSD L1180405-09 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Ethene ug/L ND 127 127 59.1 70.7 46.5 55.7 85.0-115 17.9 20 ML SAMPLE DUPLICATE: R3492685-2 L1180404-01 Dup Max Parameter Units Result Result RPD RPD Qualifiers Ethene ug/L ND ND 0.00 20 SAMPLE DUPLICATE: R3492685-3 92461009017 Dup Max Parameter Units Result Result RPD RPD Qualifiers Ethene ug/L ND ND 0.00 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 71 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 519857 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92461009001, 92461009002, 92461009003, 92461009004, 92461009005, 92461009006, 92461009007, 92461009008,92461009009,92461009010,92461009011,92461009012,92461009013,92461009014, 92461009015 METHOD BLANK: 2782192 Matrix: Water Associated Lab Samples: 92461009001, 92461009002, 92461009003, 92461009004, 92461009005, 92461009006, 92461009007, 92461009008,92461009009,92461009010,92461009011,92461009012,92461009013,92461009014, 92461009015 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Iron ug/L ND 50.0 19.5 01/17/20 22:13 LABORATORY CONTROL SAMPLE: 2782193 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Iron ug/L 5000 4910 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2782194 2782195 MS MSD 92460779001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Iron ug/L 407000 5000 5000 341000 293000 -1330 -2280 75-125 15 20 M6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 72 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 520385 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92461009016,92461009017,92461009018,92461009019,92461009020,92461009021,92461009022 METHOD BLANK: 2784754 Matrix: Water Associated Lab Samples: 92461009016,92461009017,92461009018,92461009019,92461009020,92461009021,92461009022 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Iron ug/L ND 50.0 19.5 01/22/20 04:25 LABORATORY CONTROL SAMPLE: 2784755 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Iron ug/L 5000 5170 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2784756 2784757 MS MSD 92460845001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Iron ug/L 64900 5000 5000 68600 67000 75 42 75-125 2 20 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 73 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 520137 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Associated Lab Samples: 92461009008,92461009011,92461009013,92461009024,92461009025,92461009026,92461009027, 92461009028,92461009029,92461009030,92461009031 METHOD BLANK: 2783485 Matrix: Water Associated Lab Samples: 92461009008,92461009011,92461009013,92461009024,92461009025,92461009026,92461009027, 92461009028,92461009029,92461009030,92461009031 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 01/18/20 22:10 1,1,1-Trichloroethane ug/L ND 1.0 0.18 01/18/20 22:10 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 01/18/20 22:10 1,1,2-Trichloroethane ug/L ND 1.0 0.24 01/18/20 22:10 1,1-Dichloroethane ug/L ND 1.0 0.27 01/18/20 22:10 1,1-Dichloroethene ug/L ND 1.0 0.24 01/18/20 22:10 1,1-Dichloropropene ug/L ND 1.0 0.21 01/18/20 22:10 1,2,3-Trichlorobenzene ug/L ND 1.0 0.34 01/18/20 22:10 1,2,3-Trichloropropane ug/L ND 1.0 0.35 01/18/20 22:10 1,2,4-Trichlorobenzene ug/L ND 1.0 0.22 01/18/20 22:10 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 01/18/20 22:10 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 01/18/20 22:10 1,2-Dichlorobenzene ug/L ND 1.0 0.29 01/18/20 22:10 1,2-Dichloroethane ug/L ND 1.0 0.34 01/18/20 22:10 1,2-Dichloropropane ug/L ND 1.0 0.19 01/18/20 22:10 1,3-Dichlorobenzene ug/L ND 1.0 0.22 01/18/20 22:10 1,3-Dichloropropane ug/L ND 1.0 0.16 01/18/20 22:10 1,4-Dichlorobenzene ug/L ND 1.0 0.26 01/18/20 22:10 2,2-Dichloropropane ug/L ND 1.0 0.27 01/18/20 22:10 2-Butanone (MEK) ug/L ND 5.0 3.3 01/18/20 22:10 2-Chlorotoluene ug/L ND 1.0 0.20 01/18/20 22:10 2-Hexanone ug/L ND 5.0 0.57 01/18/20 22:10 4-Chlorotoluene ug/L ND 1.0 0.20 01/18/20 22:10 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 01/18/20 22:10 Acetone ug/L ND 25.0 6.2 01/18/20 22:10 Benzene ug/L ND 1.0 0.15 01/18/20 22:10 Bromobenzene ug/L ND 1.0 0.22 01/18/20 22:10 Bromochloromethane ug/L ND 1.0 0.34 01/18/20 22:10 Bromodichloromethane ug/L ND 1.0 0.26 01/18/20 22:10 Bromoform ug/L ND 1.0 0.62 01/18/20 22:10 Bromomethane ug/L ND 2.0 0.62 01/18/20 22:10 Carbon tetrachloride ug/L ND 1.0 0.22 01/18/20 22:10 Chlorobenzene ug/L ND 1.0 0.23 01/18/20 22:10 Chloroethane ug/L ND 1.0 0.49 01/18/20 22:10 Chloroform ug/L ND 5.0 2.3 01/18/20 22:10 Chloromethane ug/L ND 1.0 0.39 01/18/20 22:10 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 01/18/20 22:10 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 01/18/20 22:10 Dibromochloromethane ug/L ND 1.0 0.41 01/18/20 22:10 Dibromomethane ug/L ND 1.0 0.46 01/18/20 22:10 L v2 v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 74 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 METHOD BLANK: 2783485 Matrix: Water Associated Lab Samples: 92461009008,92461009011,92461009013,92461009024,92461009025,92461009026,92461009027, 92461009028,92461009029,92461009030,92461009031 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Dichlorodifluoromethane ug/L ND 1.0 0.23 01/18/20 22:10 Diisopropyl ether ug/L ND 1.0 0.22 01/18/20 22:10 Ethylbenzene ug/L ND 1.0 0.26 01/18/20 22:10 Hexachloro-1,3-butadiene ug/L ND 1.0 0.44 01/18/20 22:10 m&p-Xylene ug/L ND 2.0 0.41 01/18/20 22:10 Methyl-tert-butyl ether ug/L ND 1.0 0.28 01/18/20 22:10 Methylene Chloride ug/L ND 5.0 3.7 01/18/20 22:10 Naphthalene ug/L ND 1.0 0.35 01/18/20 22:10 o-Xylene ug/L ND 1.0 0.22 01/18/20 22:10 p-Isopropyltoluene ug/L ND 1.0 0.21 01/18/20 22:10 Styrene ug/L ND 1.0 0.27 01/18/20 22:10 Tetrachloroethene ug/L ND 1.0 0.16 01/18/20 22:10 Toluene ug/L ND 1.0 0.24 01/18/20 22:10 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 01/18/20 22:10 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 01/18/20 22:10 Trichloroethene ug/L ND 1.0 0.22 01/18/20 22:10 Trichlorofluoromethane ug/L ND 1.0 0.31 01/18/20 22:10 Vinyl acetate ug/L ND 2.0 1.4 01/18/20 22:10 IK Vinyl chloride ug/L ND 1.0 0.24 01/18/20 22:10 Xylene (Total) ug/L ND 1.0 0.63 01/18/20 22:10 1,2-Dichloroethane-d4 (S) % 89 70-130 01/18/20 22:10 4-Bromofluorobenzene (S) % 98 70-130 01/18/20 22:10 Toluene-d8 (S) % 105 70-130 01/18/20 22:10 LABORATORY CONTROL SAMPLE: 2783486 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 54.3 109 70-130 1,1,1-Trichloroethane ug/L 50 49.1 98 70-130 1,1,2,2-Tetrachloroethane ug/L 50 50.6 101 70-130 1,1,2-Trichloroethane ug/L 50 53.0 106 70-130 1,1-Dichloroethane ug/L 50 46.2 92 70-130 1,1-Dichloroethene ug/L 50 46.1 92 70-130 1,1-Dichloropropene ug/L 50 54.7 109 70-130 1,2,3-Trichlorobenzene ug/L 50 56.5 113 70-130 1,2,3-Trichloropropane ug/L 50 49.6 99 70-130 1,2,4-Trichlorobenzene ug/L 50 54.9 110 70-130 1,2-Dibromo-3-chloropropane ug/L 50 53.1 106 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.3 109 70-130 1,2-Dichlorobenzene ug/L 50 53.1 106 70-130 1,2-Dichloroethane ug/L 50 46.3 93 70-130 1,2-Dichloropropane ug/L 50 51.6 103 70-130 1,3-Dichlorobenzene ug/L 50 51.9 104 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 75 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 LABORATORY CONTROL SAMPLE: Parameter 2783486 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,3-Dichloropropane ug/L 50 54.7 109 70-131 1,4-Dichlorobenzene ug/L 50 52.7 105 70-130 2,2-Dichloropropane ug/L 50 46.8 94 69-130 2-Butanone (MEK) ug/L 100 94.9 95 64-135 2-Chlorotoluene ug/L 50 50.4 101 70-130 2-Hexanone ug/L 100 101 101 66-135 4-Chlorotoluene ug/L 50 49.7 99 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 101 101 70-130 Acetone ug/L 100 111 111 61-157 Benzene ug/L 50 51.1 102 70-130 Bromobenzene ug/L 50 54.1 108 70-130 Bromochloromethane ug/L 50 50.3 101 70-130 Bromodichloromethane ug/L 50 48.7 97 70-130 Bromoform ug/L 50 52.1 104 70-130 Bromomethane ug/L 50 45.7 91 38-130IK Carbon tetrachloride ug/L 50 51.3 103 70-130 Chlorobenzene ug/L 50 50.7 101 70-130 Chloroethane ug/L 50 32.2 64 37-142 v3 Chloroform ug/L 50 48.4 97 70-130 Chloromethane ug/L 50 34.3 69 48-130 v3 cis-1,2-Dichloroethene ug/L 50 46.0 92 70-130 cis-1,3-Dichloropropene ug/L 50 53.4 107 70-130 Dibromochloromethane ug/L 50 52.6 105 70-130 Dibromomethane ug/L 50 53.1 106 70-130 Dichlorodifluoromethane ug/L 50 40.2 80 53-134 Diisopropyl ether ug/L 50 49.6 99 70-135 Ethylbenzene ug/L 50 49.1 98 70-130 Hexachloro-1,3-butadiene ug/L 50 53.8 108 68-132 m&p-Xylene ug/L 100 97.9 98 70-130 Methyl-tert-butyl ether ug/L 50 53.4 107 70-130 Methylene Chloride ug/L 50 44.8 90 67-132 Naphthalene ug/L 50 51.9 104 70-130 o-Xylene ug/L 50 49.7 99 70-131 p-Isopropyltoluene ug/L 50 51.2 102 70-130 Styrene ug/L 50 50.2 100 70-130 Tetrachloroethene ug/L 50 52.9 106 69-130 Toluene ug/L 50 48.3 97 70-130 trans-1,2-Dichloroethene ug/L 50 46.7 93 70-130 trans- 1,3-Dichloropropene ug/L 50 51.7 103 70-130 Trichloroethene ug/L 50 56.0 112 70-130 Trichlorofluoromethane ug/L 50 44.3 89 63-130 Vinyl acetate ug/L 100 93.6 94 55-143 IK Vinyl chloride ug/L 50 40.6 81 70-131 Xylene (Total) ug/L 150 148 98 70-130 1,2-Dichloroethane-d4 (S) % 88 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8 (S) % 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 76 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2783487 MS 92461009008 Spike Parameter Units Result Conc. 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1, 2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2-Dibromo-3- chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2783488 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD ug/L ND 10000 10000 10600 10700 106 107 73-134 2 ug/L 820 10000 10000 12000 12000 112 112 82-143 0 ug/L ND 10000 10000 9920 10100 99 101 70-136 1 ug/L ND 10000 10000 10900 11100 109 111 70-135 2 ug/L ND 10000 10000 10600 10600 106 106 70-139 1 ug/L ND 10000 10000 10900 10900 109 109 70-154 0 ug/L ND 10000 10000 12000 12100 120 121 70-149 1 ug/L ND 10000 10000 11300 11400 113 114 70-135 0 ug/L ND 10000 10000 9580 9350 96 94 71-137 2 ug/L ND 10000 10000 11000 11200 110 112 73-140 1 ug/L ND 10000 10000 9640 9410 96 94 65-134 3 Max RPD Qual 30 30 30 30 30 30 30 30 30 30 30 ug/L ND 10000 10000 10800 10800 108 108 70-137 0 30 ug/L ND 10000 10000 10900 11100 109 111 70-133 2 30 ug/L ND 10000 10000 10200 10100 102 101 70-137 1 30 ug/L ND 10000 10000 11300 11200 113 112 70-140 1 30 ug/L ND 10000 10000 10700 10900 107 109 70-135 2 30 ug/L ND 10000 10000 11300 11100 113 111 70-143 2 30 ug/L ND 10000 10000 11000 11100 110 111 70-133 0 30 ug/L ND 10000 10000 7950 7910 80 79 61-148 0 30 ug/L ND 20000 20000 17300 16800 87 84 60-139 3 30 ug/L ND 10000 10000 10600 10700 106 107 70-144 0 30 ug/L ND 20000 20000 19000 18600 95 93 65-138 2 30 ug/L ND 10000 10000 10600 10500 106 105 70-137 0 30 ug/L ND 20000 20000 19200 19300 96 97 65-135 1 30 ug/L ND 20000 20000 21800 20400 109 102 60-148 7 30 ug/L ND 10000 10000 11400 11500 114 115 70-151 1 30 ug/L ND 10000 10000 11300 11500 113 115 70-136 2 30 ug/L ND 10000 10000 11100 10900 111 109 70-141 1 30 ug/L ND 10000 10000 10500 10600 105 106 70-138 1 30 ug/L ND 10000 10000 9750 9680 98 97 63-130 1 30 ug/L ND 10000 10000 8530 11600 85 116 15-152 30 30 IK ug/L ND 10000 10000 11500 11800 115 118 70-143 3 30 ug/L ND 10000 10000 11000 11100 110 111 70-138 1 30 ug/L ND 10000 10000 8280 8800 83 88 52-163 6 30 v3 ug/L ND 10000 10000 11000 10800 110 108 70-139 2 30 ug/L ND 10000 10000 7640 8130 76 81 41-139 6 30 v3 ug/L 2610 10000 10000 12900 13000 103 104 70-141 0 30 ug/L ND 10000 10000 10500 10500 105 105 70-137 0 30 ug/L ND 10000 10000 10300 10300 103 103 70-134 0 30 ug/L ND 10000 10000 11600 11600 116 116 70-138 0 30 ug/L ND 10000 10000 8950 9840 89 98 47-155 9 30 ug/L ND 10000 10000 9920 10000 99 100 63-144 1 30 ug/L ND 10000 10000 10900 11100 109 111 66-153 2 30 ug/L ND 10000 10000 10700 11300 107 113 65-149 6 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 77 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2783487 2783488 MS MSD 92461009008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual m&p-Xylene ug/L ND 20000 20000 21700 22000 109 110 69-152 1 30 Methyl-tert-butyl ether ug/L ND 10000 10000 10800 10800 108 108 54-156 0 30 Methylene Chloride ug/L ND 10000 10000 10300 10400 103 104 42-159 1 30 Naphthalene ug/L ND 10000 10000 10000 10300 100 103 61-148 3 30 o-Xylene ug/L ND 10000 10000 11000 11000 110 110 70-148 1 30 p-Isopropyltoluene ug/L ND 10000 10000 10800 10900 108 109 70-146 1 30 Styrene ug/L ND 10000 10000 10800 10800 108 108 70-135 0 30 Tetrachloroethene ug/L 29900 10000 10000 42100 42000 121 120 59-143 0 30 Toluene ug/L ND 10000 10000 10700 10900 107 109 59-148 2 30 trans-1,2-Dichloroethene ug/L 398J 10000 10000 11200 11200 108 108 70-146 0 30 trans-1,3-Dichloropropene ug/L ND 10000 10000 9780 9810 98 98 70-135 0 30 Trichloroethene ug/L 49700 10000 10000 67300 66400 176 166 70-147 1 30 M1 Trichlorofluoromethane ug/L ND 10000 10000 10700 11000 107 110 70-148 3 30 Vinyl acetate ug/L ND 20000 20000 18600 18700 93 94 49-151 0 30 IK Vinyl chloride ug/L ND 10000 10000 9290 9620 93 96 70-156 3 30 Xylene (Total) ug/L ND 30000 30000 32700 33100 109 110 63-158 1 30 1,2-Dichloroethane-d4 (S) % 98 98 70-130 4-Bromofluorobenzene (S) % 97 97 70-130 Toluene-d8 (S) % 97 97 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 78 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 520138 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Associated Lab Samples: 92461009003, 92461009004, 92461009012 METHOD BLANK: 2783489 Matrix: Associated Lab Samples: 92461009003, 92461009004, 92461009012 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 01/18/20 22:28 1,1,1-Trichloroethane ug/L ND 1.0 0.18 01/18/20 22:28 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 01/18/20 22:28 1,1,2-Trichloroethane ug/L ND 1.0 0.24 01/18/20 22:28 1,1-Dichloroethane ug/L ND 1.0 0.27 01/18/20 22:28 1,1-Dichloroethene ug/L ND 1.0 0.24 01/18/20 22:28 1,1-Dichloropropene ug/L ND 1.0 0.21 01/18/20 22:28 1,2,3-Trichlorobenzene ug/L ND 1.0 0.34 01/18/20 22:28 1,2,3-Trichloropropane ug/L ND 1.0 0.35 01/18/20 22:28 1,2,4-Trichlorobenzene ug/L ND 1.0 0.22 01/18/20 22:28 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 01/18/20 22:28 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 01/18/20 22:28 1,2-Dichlorobenzene ug/L ND 1.0 0.29 01/18/20 22:28 1,2-Dichloroethane ug/L ND 1.0 0.34 01/18/20 22:28 1,2-Dichloropropane ug/L ND 1.0 0.19 01/18/20 22:28 1,3-Dichlorobenzene ug/L ND 1.0 0.22 01/18/20 22:28 1,3-Dichloropropane ug/L ND 1.0 0.16 01/18/20 22:28 1,4-Dichlorobenzene ug/L ND 1.0 0.26 01/18/20 22:28 2,2-Dichloropropane ug/L ND 1.0 0.27 01/18/20 22:28 2-Butanone (MEK) ug/L ND 5.0 3.3 01/18/20 22:28 2-Chlorotoluene ug/L ND 1.0 0.20 01/18/20 22:28 2-Hexanone ug/L ND 5.0 0.57 01/18/20 22:28 4-Chlorotoluene ug/L ND 1.0 0.20 01/18/20 22:28 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 01/18/20 22:28 Acetone ug/L ND 25.0 6.2 01/18/20 22:28 Benzene ug/L ND 1.0 0.15 01/18/20 22:28 Bromobenzene ug/L ND 1.0 0.22 01/18/20 22:28 Bromochloromethane ug/L ND 1.0 0.34 01/18/20 22:28 Bromodichloromethane ug/L ND 1.0 0.26 01/18/20 22:28 Bromoform ug/L ND 1.0 0.62 01/18/20 22:28 Bromomethane ug/L ND 2.0 0.62 01/18/20 22:28 Carbon tetrachloride ug/L ND 1.0 0.22 01/18/20 22:28 Chlorobenzene ug/L ND 1.0 0.23 01/18/20 22:28 Chloroethane ug/L ND 1.0 0.49 01/18/20 22:28 Chloroform ug/L ND 5.0 2.3 01/18/20 22:28 Chloromethane ug/L ND 1.0 0.39 01/18/20 22:28 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 01/18/20 22:28 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 01/18/20 22:28 Dibromochloromethane ug/L ND 1.0 0.41 01/18/20 22:28 Dibromomethane ug/L ND 1.0 0.46 01/18/20 22:28 Dichlorodifluoromethane ug/L ND 1.0 0.23 01/18/20 22:28 IK v2 v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 79 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 METHOD BLANK: 2783489 Matrix: Associated Lab Samples: 92461009003, 92461009004, 92461009012 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Diisopropyl ether ug/L ND 1.0 0.22 01/18/20 22:28 Ethylbenzene ug/L ND 1.0 0.26 01/18/20 22:28 Hexachloro-1,3-butadiene ug/L ND 1.0 0.44 01/18/20 22:28 m&p-Xylene ug/L ND 2.0 0.41 01/18/20 22:28 Methyl-tert-butyl ether ug/L ND 1.0 0.28 01/18/20 22:28 Methylene Chloride ug/L ND 5.0 3.7 01/18/20 22:28 Naphthalene ug/L ND 1.0 0.35 01/18/20 22:28 o-Xylene ug/L ND 1.0 0.22 01/18/20 22:28 p-Isopropyltoluene ug/L ND 1.0 0.21 01/18/20 22:28 Styrene ug/L ND 1.0 0.27 01/18/20 22:28 Tetrachloroethene ug/L ND 1.0 0.16 01/18/20 22:28 Toluene ug/L ND 1.0 0.24 01/18/20 22:28 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 01/18/20 22:28 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 01/18/20 22:28 Trichloroethene ug/L ND 1.0 0.22 01/18/20 22:28 Trichlorofluoromethane ug/L ND 1.0 0.31 01/18/20 22:28 Vinyl acetate ug/L ND 2.0 1.4 01/18/20 22:28 Vinyl chloride ug/L ND 1.0 0.24 01/18/20 22:28 Xylene (Total) ug/L ND 1.0 0.63 01/18/20 22:28 1,2-Dichloroethane-d4 (S) % 88 70-130 01/18/20 22:28 4-Bromofluorobenzene (S) % 98 70-130 01/18/20 22:28 Toluene-d8 (S) % 105 70-130 01/18/20 22:28 LABORATORY CONTROL SAMPLE: Parameter 2783490 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 54.3 109 70-130 1,1,1-Trichloroethane ug/L 50 49.1 98 70-130 1,1,2,2-Tetrachloroethane ug/L 50 50.6 101 70-130 1,1,2-Trichloroethane ug/L 50 53.0 106 70-130 1,1-Dichloroethane ug/L 50 46.2 92 70-130 1,1-Dichloroethene ug/L 50 46.1 92 70-130 1,1-Dichloropropene ug/L 50 54.7 109 70-130 1,2,3-Trichlorobenzene ug/L 50 56.5 113 70-130 1,2,3-Trichloropropane ug/L 50 49.6 99 70-130 1,2,4-Trichlorobenzene ug/L 50 54.9 110 70-130 1,2-Dibromo-3-chloropropane ug/L 50 53.1 106 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.3 109 70-130 1,2-Dichlorobenzene ug/L 50 53.1 106 70-130 1,2-Dichloroethane ug/L 50 46.3 93 70-130 1,2-Dichloropropane ug/L 50 51.6 103 70-130 1,3-Dichlorobenzene ug/L 50 51.9 104 70-130 1,3-Dichloropropane ug/L 50 54.7 109 70-131 1,4-Dichlorobenzene ug/L 50 52.7 105 70-130 Qualifiers I:/ Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 80 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 LABORATORY CONTROL SAMPLE: Parameter 2783490 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,2-Dichloropropane ug/L 50 46.8 94 69-130 2-Butanone (MEK) ug/L 100 94.9 95 64-135 2-Chlorotoluene ug/L 50 50.4 101 70-130 2-Hexanone ug/L 100 101 101 66-135 4-Chlorotoluene ug/L 50 49.7 99 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 101 101 70-130 Acetone ug/L 100 111 111 61-157 Benzene ug/L 50 51.1 102 70-130 Bromobenzene ug/L 50 54.1 108 70-130 Bromochloromethane ug/L 50 50.3 101 70-130 Bromodichloromethane ug/L 50 48.7 97 70-130 Bromoform ug/L 50 52.1 104 70-130 Bromomethane ug/L 50 45.7 91 38-130IK Carbon tetrachloride ug/L 50 51.3 103 70-130 Chlorobenzene ug/L 50 50.7 101 70-130 Chloroethane ug/L 50 32.2 64 37-142 v3 Chloroform ug/L 50 48.4 97 70-130 Chloromethane ug/L 50 34.3 69 48-130 v3 cis-1,2-Dichloroethene ug/L 50 46.0 92 70-130 cis-1,3-Dichloropropene ug/L 50 53.4 107 70-130 Dibromochloromethane ug/L 50 52.6 105 70-130 Dibromomethane ug/L 50 53.1 106 70-130 Dichlorodifluoromethane ug/L 50 40.2 80 53-134 Diisopropyl ether ug/L 50 49.6 99 70-135 Ethylbenzene ug/L 50 49.1 98 70-130 Hexachloro-1,3-butadiene ug/L 50 53.8 108 68-132 m&p-Xylene ug/L 100 97.9 98 70-130 Methyl-tert-butyl ether ug/L 50 53.4 107 70-130 Methylene Chloride ug/L 50 44.8 90 67-132 Naphthalene ug/L 50 51.9 104 70-130 o-Xylene ug/L 50 49.7 99 70-131 p-Isopropyltoluene ug/L 50 51.2 102 70-130 Styrene ug/L 50 50.2 100 70-130 Tetrachloroethene ug/L 50 52.9 106 69-130 Toluene ug/L 50 48.3 97 70-130 trans-1,2-Dichloroethene ug/L 50 46.7 93 70-130 trans- 1,3-Dichloropropene ug/L 50 51.7 103 70-130 Trichloroethene ug/L 50 56.0 112 70-130 Trichlorofluoromethane ug/L 50 44.3 89 63-130 Vinyl acetate ug/L 100 93.6 94 55-143 IK Vinyl chloride ug/L 50 40.6 81 70-131 Xylene (Total) ug/L 150 148 98 70-130 1,2-Dichloroethane-d4 (S) % 88 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8 (S) % 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 81 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2783863 MS 92461009003 Spike Parameter Units Result Conc. 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1, 2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2-Dibromo-3- chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2783864 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits ug/L ND 200 200 217 211 109 106 73-134 ug/L ND 200 200 226 215 113 107 82-143 ug/L ND 200 200 200 200 100 100 70-136 ug/L ND 200 200 218 210 109 105 70-135 ug/L ND 200 200 211 198 105 99 70-139 ug/L ND 200 200 217 206 109 103 70-154 ug/L ND 200 200 239 227 120 114 70-149 ug/L ND 200 200 227 221 113 110 70-135 ug/L ND 200 200 195 196 98 98 71-137 ug/L ND 200 200 224 220 112 110 73-140 ug/L ND 200 200 193 193 96 97 65-134 Max RPD RPD Qual 3 30 5 30 0 30 4 30 6 30 5 30 5 30 3 30 0 30 2 30 0 30 ug/L ND 200 200 216 215 108 107 70-137 0 30 ug/L ND 200 200 223 217 112 108 70-133 3 30 ug/L ND 200 200 198 194 99 97 70-137 2 30 ug/L ND 200 200 224 213 112 107 70-140 5 30 ug/L ND 200 200 220 212 110 106 70-135 4 30 ug/L ND 200 200 221 220 110 110 70-143 0 30 ug/L ND 200 200 226 221 113 111 70-133 2 30 ug/L ND 200 200 209 197 104 99 61-148 6 30 ug/L ND 400 400 331 344 83 86 60-139 4 30 ug/L ND 200 200 213 209 106 105 70-144 2 30 ug/L ND 400 400 366 380 91 95 65-138 4 30 ug/L ND 200 200 213 207 107 103 70-137 3 30 ug/L ND 400 400 374 385 93 96 65-135 3 30 ug/L ND 400 400 544 554 136 138 60-148 2 30 ug/L ND 200 200 227 216 113 108 70-151 5 30 ug/L ND 200 200 230 217 115 109 70-136 6 30 ug/L ND 200 200 216 206 108 103 70-141 5 30 ug/L ND 200 200 207 199 103 99 70-138 4 30 ug/L ND 200 200 193 193 97 96 63-130 0 30 ug/L ND 200 200 254 235 127 117 15-152 8 30 IK ug/L ND 200 200 232 220 116 110 70-143 5 30 ug/L ND 200 200 224 217 112 108 70-138 3 30 ug/L ND 200 200 166 156 83 78 52-163 6 30 v3 ug/L ND 200 200 217 207 109 104 70-139 5 30 ug/L ND 200 200 152 147 76 74 41-139 3 30 v3 ug/L 94.2 200 200 294 276 100 91 70-141 6 30 ug/L ND 200 200 214 207 107 104 70-137 3 30 ug/L ND 200 200 206 202 103 101 70-134 2 30 ug/L ND 200 200 229 221 114 110 70-138 4 30 ug/L ND 200 200 190 181 95 90 47-155 5 30 ug/L ND 200 200 195 192 98 96 63-144 1 30 ug/L ND 200 200 220 215 110 108 66-153 2 30 ug/L ND 200 200 226 212 113 106 65-149 7 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 82 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2783863 2783864 MS MSD 92461009003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual m&p-Xylene ug/L ND 400 400 445 428 111 107 69-152 4 30 Methyl-tert-butyl ether ug/L ND 200 200 213 209 107 105 54-156 2 30 Methylene Chloride ug/L ND 200 200 200 191 100 95 42-159 5 30 Naphthalene ug/L ND 200 200 207 204 104 102 61-148 2 30 o-Xylene ug/L ND 200 200 222 216 111 108 70-148 3 30 p-Isopropyltoluene ug/L ND 200 200 220 212 110 106 70-146 4 30 Styrene ug/L ND 200 200 215 212 108 106 70-135 1 30 Tetrachloroethene ug/L 1120 200 200 1340 1280 110 79 59-143 5 30 Toluene ug/L ND 200 200 216 208 108 104 59-148 4 30 trans-1,2-Dichloroethene ug/L ND 200 200 212 203 106 102 70-146 4 30 trans-1,3-Dichloropropene ug/L ND 200 200 208 197 104 99 70-135 5 30 Trichloroethene ug/L 133 200 200 398 378 132 122 70-147 5 30 Trichlorofluoromethane ug/L ND 200 200 214 205 107 102 70-148 5 30 Vinyl acetate ug/L ND 400 400 373 367 93 92 49-151 2 30 IK Vinyl chloride ug/L ND 200 200 182 173 91 87 70-156 5 30 v3 Xylene (Total) ug/L ND 600 600 666 644 111 107 63-158 3 30 1,2-Dichloroethane-d4 (S) % 96 95 70-130 4-Bromofluorobenzene (S) % 96 98 70-130 Toluene-d8 (S) % 96 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 83 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 520139 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Associated Lab Samples: 92461009002, 92461009015, 92461009016, 92461009017, 92461009023 METHOD BLANK: 2783502 Matrix: Water Associated Lab Samples: 92461009002, 92461009015, 92461009016, 92461009017, 92461009023 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 01/18/20 22:54 1,1,1-Trichloroethane ug/L ND 1.0 0.18 01/18/20 22:54 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 01/18/20 22:54 1,1,2-Trichloroethane ug/L ND 1.0 0.24 01/18/20 22:54 1,1-Dichloroethane ug/L ND 1.0 0.27 01/18/20 22:54 1,1-Dichloroethene ug/L ND 1.0 0.24 01/18/20 22:54 1,1-Dichloropropene ug/L ND 1.0 0.21 01/18/20 22:54 1,2,3-Trichlorobenzene ug/L ND 1.0 0.34 01/18/20 22:54 1,2,3-Trichloropropane ug/L ND 1.0 0.35 01/18/20 22:54 1,2,4-Trichlorobenzene ug/L ND 1.0 0.22 01/18/20 22:54 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 01/18/20 22:54 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 01/18/20 22:54 1,2-Dichlorobenzene ug/L ND 1.0 0.29 01/18/20 22:54 1,2-Dichloroethane ug/L ND 1.0 0.34 01/18/20 22:54 1,2-Dichloropropane ug/L ND 1.0 0.19 01/18/20 22:54 1,3-Dichlorobenzene ug/L ND 1.0 0.22 01/18/20 22:54 1,3-Dichloropropane ug/L ND 1.0 0.16 01/18/20 22:54 1,4-Dichlorobenzene ug/L ND 1.0 0.26 01/18/20 22:54 2,2-Dichloropropane ug/L ND 1.0 0.27 01/18/20 22:54 2-Butanone (MEK) ug/L ND 5.0 3.3 01/18/20 22:54 2-Chlorotoluene ug/L ND 1.0 0.20 01/18/20 22:54 2-Hexanone ug/L ND 5.0 0.57 01/18/20 22:54 4-Chlorotoluene ug/L ND 1.0 0.20 01/18/20 22:54 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 01/18/20 22:54 Acetone ug/L ND 25.0 6.2 01/18/20 22:54 Benzene ug/L ND 1.0 0.15 01/18/20 22:54 Bromobenzene ug/L ND 1.0 0.22 01/18/20 22:54 Bromochloromethane ug/L ND 1.0 0.34 01/18/20 22:54 Bromodichloromethane ug/L ND 1.0 0.26 01/18/20 22:54 Bromoform ug/L ND 1.0 0.62 01/18/20 22:54 Bromomethane ug/L ND 2.0 0.62 01/18/20 22:54 Carbon tetrachloride ug/L ND 1.0 0.22 01/18/20 22:54 Chlorobenzene ug/L ND 1.0 0.23 01/18/20 22:54 Chloroethane ug/L ND 1.0 0.49 01/18/20 22:54 Chloroform ug/L ND 5.0 2.3 01/18/20 22:54 Chloromethane ug/L ND 1.0 0.39 01/18/20 22:54 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 01/18/20 22:54 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 01/18/20 22:54 Dibromochloromethane ug/L ND 1.0 0.41 01/18/20 22:54 Dibromomethane ug/L ND 1.0 0.46 01/18/20 22:54 Dichlorodifluoromethane ug/L ND 1.0 0.23 01/18/20 22:54 v2 IL v2 v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 84 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 METHOD BLANK: 2783502 Matrix: Water Associated Lab Samples: 92461009002, 92461009015, 92461009016, 92461009017, 92461009023 Blank Reporting Parameter Units Result Limit MDL Analyzed Diisopropyl ether ug/L ND 1.0 0.22 01/18/20 22:54 Ethylbenzene ug/L ND 1.0 0.26 01/18/20 22:54 Hexachloro-1,3-butadiene ug/L ND 1.0 0.44 01/18/20 22:54 m&p-Xylene ug/L ND 2.0 0.41 01/18/20 22:54 Methyl-tert-butyl ether ug/L ND 1.0 0.28 01/18/20 22:54 Methylene Chloride ug/L ND 5.0 3.7 01/18/20 22:54 Naphthalene ug/L ND 1.0 0.35 01/18/20 22:54 o-Xylene ug/L ND 1.0 0.22 01/18/20 22:54 p-Isopropyltoluene ug/L ND 1.0 0.21 01/18/20 22:54 Styrene ug/L ND 1.0 0.27 01/18/20 22:54 Tetrachloroethene ug/L ND 1.0 0.16 01/18/20 22:54 Toluene ug/L ND 1.0 0.24 01/18/20 22:54 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 01/18/20 22:54 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 01/18/20 22:54 Trichloroethene ug/L ND 1.0 0.22 01/18/20 22:54 Trichlorofluoromethane ug/L ND 1.0 0.31 01/18/20 22:54 Vinyl acetate ug/L ND 2.0 1.4 01/18/20 22:54 Vinyl chloride ug/L ND 1.0 0.24 01/18/20 22:54 Xylene (Total) ug/L ND 1.0 0.63 01/18/20 22:54 1,2-Dichloroethane-d4 (S) % 97 70-130 01/18/20 22:54 4-Bromofluorobenzene (S) % 103 70-130 01/18/20 22:54 Toluene-d8 (S) % 103 70-130 01/18/20 22:54 LABORATORY CONTROL SAMPLE: Parameter 2783503 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 54.5 109 70-130 1,1,1-Trichloroethane ug/L 50 50.6 101 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.0 106 70-130 1,1,2-Trichloroethane ug/L 50 54.0 108 70-130 1,1-Dichloroethane ug/L 50 53.2 106 70-130 1,1-Dichloroethene ug/L 50 51.9 104 70-130 1,1-Dichloropropene ug/L 50 55.3 111 70-130 1,2,3-Trichlorobenzene ug/L 50 54.8 110 70-130 1,2,3-Trichloropropane ug/L 50 51.7 103 70-130 1,2,4-Trichlorobenzene ug/L 50 53.7 107 70-130 1,2-Dibromo-3-chloropropane ug/L 50 57.0 114 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.1 108 70-130 1,2-Dichlorobenzene ug/L 50 52.6 105 70-130 1,2-Dichloroethane ug/L 50 49.2 98 70-130 1,2-Dichloropropane ug/L 50 53.9 108 70-130 1,3-Dichlorobenzene ug/L 50 52.1 104 70-130 1,3-Dichloropropane ug/L 50 55.0 110 70-131 1,4-Dichlorobenzene ug/L 50 51.9 104 70-130 Qualifiers IK v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 85 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 LABORATORY CONTROL SAMPLE: Parameter 2783503 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,2-Dichloropropane ug/L 50 57.0 114 69-130 2-Butanone (MEK) ug/L 100 108 108 64-135 2-Chlorotoluene ug/L 50 52.9 106 70-130 2-Hexanone ug/L 100 99.6 100 66-135 4-Chlorotoluene ug/L 50 53.1 106 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 100 100 70-130 Acetone ug/L 100 122 122 61-157 Benzene ug/L 50 53.2 106 70-130 Bromobenzene ug/L 50 54.0 108 70-130 Bromochloromethane ug/L 50 55.8 112 70-130 Bromodichloromethane ug/L 50 53.4 107 70-130 Bromoform ug/L 50 54.5 109 70-130 Bromomethane ug/L 50 29.1 58 38-130 v2 Carbon tetrachloride ug/L 50 50.2 100 70-130 Chlorobenzene ug/L 50 51.4 103 70-130 Chloroethane ug/L 50 35.1 70 37-142 IL Chloroform ug/L 50 51.7 103 70-130 Chloromethane ug/L 50 37.7 75 48-130 v2 cis-1,2-Dichloroethene ug/L 50 51.8 104 70-130 cis-1,3-Dichloropropene ug/L 50 58.0 116 70-130 Dibromochloromethane ug/L 50 54.9 110 70-130 Dibromomethane ug/L 50 52.5 105 70-130 Dichlorodifluoromethane ug/L 50 36.1 72 53-134 v2 Diisopropyl ether ug/L 50 55.6 111 70-135 Ethylbenzene ug/L 50 50.4 101 70-130 Hexachloro-1,3-butadiene ug/L 50 53.8 108 68-132 m&p-Xylene ug/L 100 101 101 70-130 Methyl-tert-butyl ether ug/L 50 54.7 109 70-130 Methylene Chloride ug/L 50 51.5 103 67-132 Naphthalene ug/L 50 53.6 107 70-130 o-Xylene ug/L 50 50.9 102 70-131 p-Isopropyltoluene ug/L 50 52.3 105 70-130 Styrene ug/L 50 51.8 104 70-130 Tetrachloroethene ug/L 50 50.2 100 69-130 Toluene ug/L 50 51.0 102 70-130 trans-1,2-Dichloroethene ug/L 50 52.5 105 70-130 trans- 1,3-Dichloropropene ug/L 50 57.3 115 70-130 Trichloroethene ug/L 50 49.6 99 70-130 Trichlorofluoromethane ug/L 50 44.7 89 63-130 Vinyl acetate ug/L 100 103 103 55-143 IK Vinyl chloride ug/L 50 44.1 88 70-131 v2 Xylene (Total) ug/L 150 152 102 70-130 1,2-Dichloroethane-d4 (S) % 99 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 86 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2783504 MS 92461115016 Spike Parameter Units Result Conc. 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1, 2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2-Dibromo-3- chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2783505 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits ug/L ND 20 20 21.4 22.5 107 112 73-134 ug/L ND 20 20 22.0 22.7 110 113 82-143 ug/L ND 20 20 20.7 21.3 104 106 70-136 ug/L ND 20 20 21.4 21.1 107 106 70-135 ug/L ND 20 20 21.2 22.6 106 113 70-139 ug/L ND 20 20 21.4 22.2 107 111 70-154 ug/L ND 20 20 22.7 23.5 113 118 70-149 ug/L ND 20 20 21.1 21.1 106 106 70-135 ug/L ND 20 20 21.0 21.5 105 107 71-137 ug/L ND 20 20 21.4 20.2 107 101 73-140 ug/L ND 20 20 21.4 21.2 107 106 65-134 Max RPD RPD Qual 5 30 3 30 3 30 1 30 6 30 4 30 4 30 0 30 2 30 6 30 1 30 ug/L ND 20 20 20.9 21.9 105 109 70-137 4 30 ug/L ND 20 20 20.0 20.8 100 104 70-133 4 30 ug/L ND 20 20 20.8 21.7 104 109 70-137 4 30 ug/L ND 20 20 21.2 21.8 106 109 70-140 3 30 ug/L ND 20 20 19.9 20.0 99 100 70-135 1 30 ug/L ND 20 20 21.1 21.9 105 110 70-143 4 30 ug/L ND 20 20 19.9 20.6 100 103 70-133 3 30 ug/L ND 20 20 22.1 23.1 111 115 61-148 4 30 ug/L ND 40 40 43.3 43.7 108 109 60-139 1 30 ug/L ND 20 20 21.1 21.5 105 107 70-144 2 30 ug/L ND 40 40 41.5 42.1 104 105 65-138 1 30 ug/L ND 20 20 20.6 21.3 103 106 70-137 3 30 ug/L ND 40 40 40.0 41.1 100 103 65-135 3 30 ug/L ND 40 40 44.6 47.0 112 117 60-148 5 30 ug/L ND 20 20 21.6 22.3 108 112 70-151 3 30 ug/L ND 20 20 20.6 21.6 103 108 70-136 5 30 ug/L ND 20 20 21.6 22.7 108 114 70-141 5 30 ug/L ND 20 20 20.9 21.3 104 106 70-138 2 30 ug/L ND 20 20 19.5 20.4 97 102 63-130 4 30 ug/L ND 20 20 24.4 27.6 122 138 15-152 12 30 ug/L ND 20 20 22.1 22.5 110 112 70-143 2 30 ug/L ND 20 20 20.8 22.0 104 110 70-138 5 30 ug/L ND 20 20 18.5 19.3 92 97 52-163 4 30 ug/L ND 20 20 22.4 22.3 112 111 70-139 0 30 ug/L ND 20 20 18.4 19.1 92 95 41-139 4 30 ug/L ND 20 20 21.2 22.3 106 111 70-141 5 30 ug/L ND 20 20 21.2 22.0 106 110 70-137 4 30 ug/L ND 20 20 21.3 21.4 107 107 70-134 0 30 ug/L ND 20 20 21.2 21.1 106 105 70-138 1 30 ug/L ND 20 20 17.6 18.4 88 92 47-155 4 30 ug/L ND 20 20 21.6 22.2 108 111 63-144 3 30 ug/L ND 20 20 21.2 22.2 106 111 66-153 5 30 ug/L ND 20 20 22.0 21.2 110 106 65-149 4 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 87 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2783504 2783505 MS MSD 92461115016 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual m&p-Xylene ug/L ND 40 40 42.6 44.8 106 112 69-152 5 30 Methyl-tert-butyl ether ug/L ND 20 20 21.8 22.5 109 113 54-156 3 30 Methylene Chloride ug/L ND 20 20 21.4 22.1 107 110 42-159 3 30 Naphthalene ug/L ND 20 20 20.8 19.9 104 100 61-148 4 30 o-Xylene ug/L ND 20 20 20.3 21.5 101 107 70-148 6 30 p-Isopropyltoluene ug/L ND 20 20 20.8 21.3 104 106 70-146 2 30 Styrene ug/L ND 20 20 19.7 20.9 98 104 70-135 6 30 Tetrachloroethene ug/L ND 20 20 20.7 20.8 103 104 59-143 1 30 Toluene ug/L ND 20 20 21.2 22.0 106 110 59-148 4 30 trans-1,2-Dichloroethene ug/L ND 20 20 21.5 22.1 108 111 70-146 3 30 trans-1,3-Dichloropropene ug/L ND 20 20 21.4 22.3 107 111 70-135 4 30 Trichloroethene ug/L ND 20 20 21.2 22.1 106 110 70-147 4 30 Trichlorofluoromethane ug/L ND 20 20 20.4 21.8 102 109 70-148 7 30 Vinyl acetate ug/L ND 40 40 41.7 43.1 104 108 49-151 3 30 Vinyl chloride ug/L ND 20 20 20.6 21.0 103 105 70-156 2 30 Xylene (Total) ug/L ND 60 60 62.9 66.3 105 111 63-158 5 30 1,2-Dichloroethane-d4 (S) % 108 108 70-130 4-Bromofluorobenzene (S) % 99 100 70-130 Toluene-d8 (S) % 102 101 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 88 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 520274 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Associated Lab Samples: 92461009001, 92461009005, 92461009006, 92461009007, 92461009009, 92461009010, 92461009014, 92461009018,92461009019,92461009020,92461009022 METHOD BLANK: 2783999 Matrix: Water Associated Lab Samples: 92461009001, 92461009005, 92461009006, 92461009007, 92461009009, 92461009010, 92461009014, 92461009018,92461009019,92461009020,92461009022 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 01/20/20 11:45 1,1,1-Trichloroethane ug/L ND 1.0 0.18 01/20/20 11:45 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 01/20/20 11:45 1,1,2-Trichloroethane ug/L ND 1.0 0.24 01/20/20 11:45 1,1-Dichloroethane ug/L ND 1.0 0.27 01/20/20 11:45 1,1-Dichloroethene ug/L ND 1.0 0.24 01/20/20 11:45 1,1-Dichloropropene ug/L ND 1.0 0.21 01/20/20 11:45 1,2,3-Trichlorobenzene ug/L ND 1.0 0.34 01/20/20 11:45 1,2,3-Trichloropropane ug/L ND 1.0 0.35 01/20/20 11:45 1,2,4-Trichlorobenzene ug/L ND 1.0 0.22 01/20/20 11:45 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 01/20/20 11:45 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 01/20/20 11:45 1,2-Dichlorobenzene ug/L ND 1.0 0.29 01/20/20 11:45 1,2-Dichloroethane ug/L ND 1.0 0.34 01/20/20 11:45 1,2-Dichloropropane ug/L ND 1.0 0.19 01/20/20 11:45 1,3-Dichlorobenzene ug/L ND 1.0 0.22 01/20/20 11:45 1,3-Dichloropropane ug/L ND 1.0 0.16 01/20/20 11:45 1,4-Dichlorobenzene ug/L ND 1.0 0.26 01/20/20 11:45 2,2-Dichloropropane ug/L ND 1.0 0.27 01/20/20 11:45 2-Butanone (MEK) ug/L ND 5.0 3.3 01/20/20 11:45 2-Chlorotoluene ug/L ND 1.0 0.20 01/20/20 11:45 2-Hexanone ug/L ND 5.0 0.57 01/20/20 11:45 4-Chlorotoluene ug/L ND 1.0 0.20 01/20/20 11:45 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 01/20/20 11:45 Acetone ug/L ND 25.0 6.2 01/20/20 11:45 Benzene ug/L ND 1.0 0.15 01/20/20 11:45 Bromobenzene ug/L ND 1.0 0.22 01/20/20 11:45 Bromochloromethane ug/L ND 1.0 0.34 01/20/20 11:45 Bromodichloromethane ug/L ND 1.0 0.26 01/20/20 11:45 Bromoform ug/L ND 1.0 0.62 01/20/20 11:45 Bromomethane ug/L ND 2.0 0.62 01/20/20 11:45 Carbon tetrachloride ug/L ND 1.0 0.22 01/20/20 11:45 Chlorobenzene ug/L ND 1.0 0.23 01/20/20 11:45 Chloroethane ug/L ND 1.0 0.49 01/20/20 11:45 Chloroform ug/L ND 5.0 2.3 01/20/20 11:45 Chloromethane ug/L ND 1.0 0.39 01/20/20 11:45 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 01/20/20 11:45 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 01/20/20 11:45 Dibromochloromethane ug/L ND 1.0 0.41 01/20/20 11:45 Dibromomethane ug/L ND 1.0 0.46 01/20/20 11:45 L v2 v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 89 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 METHOD BLANK: 2783999 Matrix: Water Associated Lab Samples: 92461009001, 92461009005, 92461009006, 92461009007, 92461009009, 92461009010, 92461009014, 92461009018,92461009019,92461009020,92461009022 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Dichlorodifluoromethane ug/L ND 1.0 0.23 01/20/20 11:45 Diisopropyl ether ug/L ND 1.0 0.22 01/20/20 11:45 Ethylbenzene ug/L ND 1.0 0.26 01/20/20 11:45 Hexachloro-1,3-butadiene ug/L ND 1.0 0.44 01/20/20 11:45 m&p-Xylene ug/L ND 2.0 0.41 01/20/20 11:45 Methyl-tert-butyl ether ug/L ND 1.0 0.28 01/20/20 11:45 Methylene Chloride ug/L ND 5.0 3.7 01/20/20 11:45 Naphthalene ug/L ND 1.0 0.35 01/20/20 11:45 o-Xylene ug/L ND 1.0 0.22 01/20/20 11:45 p-Isopropyltoluene ug/L ND 1.0 0.21 01/20/20 11:45 Styrene ug/L ND 1.0 0.27 01/20/20 11:45 Tetrachloroethene ug/L ND 1.0 0.16 01/20/20 11:45 Toluene ug/L ND 1.0 0.24 01/20/20 11:45 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 01/20/20 11:45 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 01/20/20 11:45 Trichloroethene ug/L ND 1.0 0.22 01/20/20 11:45 Trichlorofluoromethane ug/L ND 1.0 0.31 01/20/20 11:45 Vinyl acetate ug/L ND 2.0 1.4 01/20/20 11:45 IK Vinyl chloride ug/L ND 1.0 0.24 01/20/20 11:45 Xylene (Total) ug/L ND 1.0 0.63 01/20/20 11:45 1,2-Dichloroethane-d4 (S) % 93 70-130 01/20/20 11:45 4-Bromofluorobenzene (S) % 98 70-130 01/20/20 11:45 Toluene-d8(S) % 104 70-130 01/20/20 11:45 LABORATORY CONTROL SAMPLE: 2784000 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 52.1 104 70-130 1,1,1-Trichloroethane ug/L 50 48.7 97 70-130 1,1,2,2-Tetrachloroethane ug/L 50 48.8 98 70-130 1,1,2-Trichloroethane ug/L 50 51.5 103 70-130 1,1-Dichloroethane ug/L 50 46.5 93 70-130 1,1-Dichloroethene ug/L 50 46.7 93 70-130 1,1-Dichloropropene ug/L 50 53.9 108 70-130 1,2,3-Trichlorobenzene ug/L 50 52.8 106 70-130 1,2,3-Trichloropropane ug/L 50 48.6 97 70-130 1,2,4-Trichlorobenzene ug/L 50 52.6 105 70-130 1,2-Dibromo-3-chloropropane ug/L 50 49.6 99 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.2 104 70-130 1,2-Dichlorobenzene ug/L 50 50.3 101 70-130 1,2-Dichloroethane ug/L 50 46.5 93 70-130 1,2-Dichloropropane ug/L 50 50.0 100 70-130 1,3-Dichlorobenzene ug/L 50 49.5 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 90 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 LABORATORY CONTROL SAMPLE: Parameter 2784000 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,3-Dichloropropane ug/L 50 53.1 106 70-131 1,4-Dichlorobenzene ug/L 50 50.8 102 70-130 2,2-Dichloropropane ug/L 50 47.4 95 69-130 2-Butanone (MEK) ug/L 100 90.7 91 64-135 2-Chlorotoluene ug/L 50 48.8 98 70-130 2-Hexanone ug/L 100 94.0 94 66-135 4-Chlorotoluene ug/L 50 48.0 96 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 93.3 93 70-130 Acetone ug/L 100 109 109 61-157 Benzene ug/L 50 50.2 100 70-130 Bromobenzene ug/L 50 51.5 103 70-130 Bromochloromethane ug/L 50 49.7 99 70-130 Bromodichloromethane ug/L 50 48.3 97 70-130 Bromoform ug/L 50 51.7 103 70-130 Bromomethane ug/L 50 40.6 81 38-130IK Carbon tetrachloride ug/L 50 50.5 101 70-130 Chlorobenzene ug/L 50 49.0 98 70-130 Chloroethane ug/L 50 33.3 67 37-142 v3 Chloroform ug/L 50 48.1 96 70-130 Chloromethane ug/L 50 34.0 68 48-130 v3 cis-1,2-Dichloroethene ug/L 50 45.8 92 70-130 cis-1,3-Dichloropropene ug/L 50 52.4 105 70-130 Dibromochloromethane ug/L 50 51.6 103 70-130 Dibromomethane ug/L 50 50.8 102 70-130 Dichlorodifluoromethane ug/L 50 42.1 84 53-134 Diisopropyl ether ug/L 50 49.3 99 70-135 Ethylbenzene ug/L 50 47.8 96 70-130 Hexachloro-1,3-butadiene ug/L 50 51.4 103 68-132 m&p-Xylene ug/L 100 95.9 96 70-130 Methyl-tert-butyl ether ug/L 50 52.6 105 70-130 Methylene Chloride ug/L 50 44.9 90 67-132 Naphthalene ug/L 50 48.7 97 70-130 o-Xylene ug/L 50 48.1 96 70-131 p-Isopropyltoluene ug/L 50 49.4 99 70-130 Styrene ug/L 50 48.6 97 70-130 Tetrachloroethene ug/L 50 51.5 103 69-130 Toluene ug/L 50 46.8 94 70-130 trans-1,2-Dichloroethene ug/L 50 47.5 95 70-130 trans- 1,3-Dichloropropene ug/L 50 50.7 101 70-130 Trichloroethene ug/L 50 54.3 109 70-130 Trichlorofluoromethane ug/L 50 44.2 88 63-130 Vinyl acetate ug/L 100 91.5 91 55-143 IK Vinyl chloride ug/L 50 41.0 82 70-131 Xylene (Total) ug/L 150 144 96 70-130 1,2-Dichloroethane-d4 (S) % 92 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8 (S) % 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 91 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2784001 MS 92461009019 Spike Parameter Units Result Conc. 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1, 2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2-Dibromo-3- chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2784002 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits ug/L ND 200 200 205 212 102 106 73-134 ug/L 5.8J 200 200 224 231 109 113 82-143 ug/L ND 200 200 200 200 100 100 70-136 ug/L ND 200 200 215 219 108 109 70-135 ug/L 4.OJ 200 200 211 215 104 106 70-139 ug/L 12.2 200 200 225 230 107 109 70-154 ug/L ND 200 200 238 241 119 120 70-149 ug/L ND 200 200 217 227 108 114 70-135 ug/L ND 200 200 184 189 92 94 71-137 ug/L ND 200 200 214 224 107 112 73-140 ug/L ND 200 200 194 196 97 98 65-134 Max RPD RPD Qual 4 30 3 30 0 30 2 30 2 30 2 30 1 30 5 30 2 30 5 30 1 30 ug/L ND 200 200 209 213 105 106 70-137 2 30 ug/L ND 200 200 218 221 109 110 70-133 1 30 ug/L ND 200 200 203 204 101 102 70-137 1 30 ug/L ND 200 200 220 229 110 115 70-140 4 30 ug/L ND 200 200 220 221 110 111 70-135 1 30 ug/L ND 200 200 216 223 108 112 70-143 3 30 ug/L ND 200 200 211 225 105 113 70-133 7 30 ug/L ND 200 200 196 197 98 99 61-148 1 30 ug/L ND 400 400 353 338 88 85 60-139 4 30 ug/L ND 200 200 207 216 103 108 70-144 4 30 ug/L ND 400 400 383 377 96 94 65-138 2 30 ug/L ND 200 200 206 216 103 108 70-137 5 30 ug/L ND 400 400 391 388 98 97 65-135 1 30 ug/L 161J 400 400 605 576 111 104 60-148 5 30 ug/L N D 200 200 224 233 112 117 70-151 4 30 ug/L N D 200 200 222 229 111 114 70-136 3 30 ug/L N D 200 200 215 219 108 109 70-141 2 30 ug/L N D 200 200 210 213 105 107 70-138 2 30 ug/L ND 200 200 185 190 92 95 63-130 3 30 ug/L ND 200 200 106 132 53 66 15-152 22 30 IK ug/L N D 200 200 230 237 115 119 70-143 3 30 ug/L N D 200 200 216 225 108 112 70-138 4 30 ug/L N D 200 200 161 171 81 86 52-163 6 30 v3 ug/L N D 200 200 213 219 106 109 70-139 3 30 ug/L N D 200 200 150 149 75 75 41-139 0 30 v3 ug/L 59.0 200 200 261 270 101 105 70-141 3 30 ug/L N D 200 200 211 217 105 109 70-137 3 30 ug/L N D 200 200 200 206 100 103 70-134 3 30 ug/L N D 200 200 225 234 112 117 70-138 4 30 ug/L ND 200 200 152 158 76 79 47-155 4 30 ug/L ND 200 200 194 194 97 97 63-144 0 30 ug/L N D 200 200 214 223 107 111 66-153 4 30 ug/L ND 200 200 215 222 108 111 65-149 3 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 92 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2784001 2784002 MS MSD 92461009019 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual m&p-Xylene ug/L ND 400 400 430 452 108 113 69-152 5 30 Methyl-tert-butyl ether ug/L ND 200 200 214 211 107 106 54-156 1 30 Methylene Chloride ug/L ND 200 200 204 205 102 103 42-159 0 30 Naphthalene ug/L ND 200 200 199 206 99 103 61-148 4 30 o-Xylene ug/L ND 200 200 216 223 108 111 70-148 3 30 p-Isopropyltoluene ug/L ND 200 200 212 222 106 111 70-146 5 30 Styrene ug/L ND 200 200 207 215 104 107 70-135 4 30 Tetrachloroethene ug/L 124 200 200 358 372 117 124 59-143 4 30 Toluene ug/L ND 200 200 216 220 108 110 59-148 2 30 trans-1,2-Dichloroethene ug/L ND 200 200 212 218 106 109 70-146 3 30 trans-1,3-Dichloropropene ug/L ND 200 200 201 204 100 102 70-135 2 30 Trichloroethene ug/L 1170 200 200 1510 1580 168 205 70-147 5 30 M1 Trichlorofluoromethane ug/L ND 200 200 205 211 103 106 70-148 3 30 Vinyl acetate ug/L ND 400 400 375 375 94 94 49-151 0 30 IK Vinyl chloride ug/L ND 200 200 178 182 89 91 70-156 2 30 Xylene (Total) ug/L ND 600 600 646 675 108 112 63-158 4 30 1,2-Dichloroethane-d4 (S) % 98 97 70-130 4-Bromofluorobenzene (S) % 98 97 70-130 Toluene-d8 (S) % 97 97 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 93 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 520868 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Associated Lab Samples: 92461009021 METHOD BLANK: 2787015 Associated Lab Samples: 92461009021 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 01/22/20 16:01 1,1,1-Trichloroethane ug/L ND 1.0 0.18 01/22/20 16:01 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 01/22/20 16:01 1,1,2-Trichloroethane ug/L ND 1.0 0.24 01/22/20 16:01 1,1-Dichloroethane ug/L ND 1.0 0.27 01/22/20 16:01 1,1-Dichloroethene ug/L ND 1.0 0.24 01/22/20 16:01 1,1-Dichloropropene ug/L ND 1.0 0.21 01/22/20 16:01 1,2,3-Trichlorobenzene ug/L ND 1.0 0.34 01/22/20 16:01 1,2,3-Trichloropropane ug/L ND 1.0 0.35 01/22/20 16:01 1,2,4-Trichlorobenzene ug/L ND 1.0 0.22 01/22/20 16:01 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 01/22/20 16:01 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 01/22/20 16:01 1,2-Dichlorobenzene ug/L ND 1.0 0.29 01/22/20 16:01 1,2-Dichloroethane ug/L ND 1.0 0.34 01/22/20 16:01 1,2-Dichloropropane ug/L ND 1.0 0.19 01/22/20 16:01 1,3-Dichlorobenzene ug/L ND 1.0 0.22 01/22/20 16:01 1,3-Dichloropropane ug/L ND 1.0 0.16 01/22/20 16:01 1,4-Dichlorobenzene ug/L ND 1.0 0.26 01/22/20 16:01 2,2-Dichloropropane ug/L ND 1.0 0.27 01/22/20 16:01 2-Butanone (MEK) ug/L ND 5.0 3.3 01/22/20 16:01 2-Chlorotoluene ug/L ND 1.0 0.20 01/22/20 16:01 2-Hexanone ug/L ND 5.0 0.57 01/22/20 16:01 4-Chlorotoluene ug/L ND 1.0 0.20 01/22/20 16:01 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 01/22/20 16:01 Acetone ug/L ND 25.0 6.2 01/22/20 16:01 Benzene ug/L ND 1.0 0.15 01/22/20 16:01 Bromobenzene ug/L ND 1.0 0.22 01/22/20 16:01 Bromochloromethane ug/L ND 1.0 0.34 01/22/20 16:01 Bromodichloromethane ug/L ND 1.0 0.26 01/22/20 16:01 Bromoform ug/L ND 1.0 0.62 01/22/20 16:01 Bromomethane ug/L ND 2.0 0.62 01/22/20 16:01 IH,IK,v1 Carbon tetrachloride ug/L ND 1.0 0.22 01/22/20 16:01 Chlorobenzene ug/L ND 1.0 0.23 01/22/20 16:01 Chloroethane ug/L ND 1.0 0.49 01/22/20 16:01 Chloroform ug/L ND 5.0 2.3 01/22/20 16:01 Chloromethane ug/L ND 1.0 0.39 01/22/20 16:01 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 01/22/20 16:01 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 01/22/20 16:01 Dibromochloromethane ug/L ND 1.0 0.41 01/22/20 16:01 Dibromomethane ug/L ND 1.0 0.46 01/22/20 16:01 Dichlorodifluoromethane ug/L ND 1.0 0.23 01/22/20 16:01 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 94 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 METHOD BLANK: 2787015 Associated Lab Samples: 92461009021 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Diisopropyl ether ug/L ND 1.0 0.22 01/22/20 16:01 Ethylbenzene ug/L ND 1.0 0.26 01/22/20 16:01 Hexachloro-1,3-butadiene ug/L 0.991 1.0 0.44 01/22/20 16:01 m&p-Xylene ug/L ND 2.0 0.41 01/22/20 16:01 Methyl-tert-butyl ether ug/L ND 1.0 0.28 01/22/20 16:01 Methylene Chloride ug/L ND 5.0 3.7 01/22/20 16:01 Naphthalene ug/L ND 1.0 0.35 01/22/20 16:01 o-Xylene ug/L ND 1.0 0.22 01/22/20 16:01 p-Isopropyltoluene ug/L ND 1.0 0.21 01/22/20 16:01 Styrene ug/L ND 1.0 0.27 01/22/20 16:01 Tetrachloroethene ug/L ND 1.0 0.16 01/22/20 16:01 Toluene ug/L ND 1.0 0.24 01/22/20 16:01 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 01/22/20 16:01 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 01/22/20 16:01 Trichloroethene ug/L ND 1.0 0.22 01/22/20 16:01 Trichlorofluoromethane ug/L ND 1.0 0.31 01/22/20 16:01 Vinyl acetate ug/L ND 2.0 1.4 01/22/20 16:01 Vinyl chloride ug/L ND 1.0 0.24 01/22/20 16:01 Xylene (Total) ug/L ND 1.0 0.63 01/22/20 16:01 1,2-Dichloroethane-d4 (S) % 100 70-130 01/22/20 16:01 4-Bromofluorobenzene (S) % 102 70-130 01/22/20 16:01 Toluene-d8 (S) % 99 70-130 01/22/20 16:01 LABORATORY CONTROL SAMPLE: Parameter 2787016 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 56.4 113 70-130 1,1,1-Trichloroethane ug/L 50 53.2 106 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.5 107 70-130 1,1,2-Trichloroethane ug/L 50 55.3 111 70-130 1,1-Dichloroethane ug/L 50 51.2 102 70-130 1,1-Dichloroethene ug/L 50 51.4 103 70-130 1,1-Dichloropropene ug/L 50 53.3 107 70-130 1,2,3-Trichlorobenzene ug/L 50 57.5 115 70-130 1,2,3-Trichloropropane ug/L 50 52.1 104 70-130 1,2,4-Trichlorobenzene ug/L 50 57.0 114 70-130 1,2-Dibromo-3-chloropropane ug/L 50 58.7 117 70-130 1,2-Dibromoethane (EDB) ug/L 50 56.1 112 70-130 1,2-Dichlorobenzene ug/L 50 53.1 106 70-130 1,2-Dichloroethane ug/L 50 49.2 98 70-130 1,2-Dichloropropane ug/L 50 52.2 104 70-130 1,3-Dichlorobenzene ug/L 50 53.2 106 70-130 1,3-Dichloropropane ug/L 50 53.5 107 70-131 1,4-Dichlorobenzene ug/L 50 52.6 105 70-130 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 95 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 LABORATORY CONTROL SAMPLE: Parameter 2787016 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,2-Dichloropropane ug/L 50 51.9 104 69-130 2-Butanone (MEK) ug/L 100 108 108 64-135 2-Chlorotoluene ug/L 50 53.2 106 70-130 2-Hexanone ug/L 100 107 107 66-135 4-Chlorotoluene ug/L 50 52.9 106 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 108 108 70-130 Acetone ug/L 100 119 119 61-157 Benzene ug/L 50 52.7 105 70-130 Bromobenzene ug/L 50 54.8 110 70-130 Bromochloromethane ug/L 50 53.3 107 70-130 Bromodichloromethane ug/L 50 51.9 104 70-130 Bromoform ug/L 50 53.5 107 70-130 Bromomethane ug/L 50 66.1 132 38-1301H,IK,L1,v1 Carbon tetrachloride ug/L 50 53.9 108 70-130 Chlorobenzene ug/L 50 52.9 106 70-130 Chloroethane ug/L 50 50.7 101 37-142 Chloroform ug/L 50 51.1 102 70-130 Chloromethane ug/L 50 47.0 94 48-130 cis-1,2-Dichloroethene ug/L 50 51.1 102 70-130 cis-1,3-Dichloropropene ug/L 50 54.1 108 70-130 Dibromochloromethane ug/L 50 55.3 111 70-130 Dibromomethane ug/L 50 53.2 106 70-130 Dichlorodifluoromethane ug/L 50 53.3 107 53-134 Diisopropyl ether ug/L 50 52.3 105 70-135 Ethylbenzene ug/L 50 51.5 103 70-130 Hexachloro-1,3-butadiene ug/L 50 58.3 117 68-132 m&p-Xylene ug/L 100 103 103 70-130 Methyl-tert-butyl ether ug/L 50 52.2 104 70-130 Methylene Chloride ug/L 50 50.8 102 67-132 Naphthalene ug/L 50 57.3 115 70-130 o-Xylene ug/L 50 52.0 104 70-131 p-Isopropyltoluene ug/L 50 53.3 107 70-130 Styrene ug/L 50 53.0 106 70-130 Tetrachloroethene ug/L 50 54.2 108 69-130 Toluene ug/L 50 50.9 102 70-130 trans-1,2-Dichloroethene ug/L 50 51.6 103 70-130 trans- 1,3-Dichloropropene ug/L 50 54.0 108 70-130 Trichloroethene ug/L 50 54.3 109 70-130 Trichlorofluoromethane ug/L 50 48.8 98 63-130 Vinyl acetate ug/L 100 113 113 55-143 Vinyl chloride ug/L 50 59.0 118 70-131 Xylene (Total) ug/L 150 155 103 70-130 1,2-Dichloroethane-d4 (S) % 98 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 100 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 96 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2787017 MS 92461009021 Spike Parameter Units Result Conc. MSD Spike Conc. 2787018 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 5000 5000 5920 5810 118 116 73-134 2 30 1,1,1-Trichloroethane ug/L 430 5000 5000 6610 6390 124 119 82-143 3 30 1,1,2,2-Tetrachloroethane ug/L ND 5000 5000 5640 5670 113 113 70-136 1 30 1,1,2-Trichloroethane ug/L ND 5000 5000 5860 5760 117 115 70-135 2 30 1,1-Dichloroethane ug/L 86AJ 5000 5000 5900 5890 116 116 70-139 0 30 1,1-Dichloroethene ug/L 422 5000 5000 6530 6340 122 118 70-154 3 30 1,1-Dichloropropene ug/L ND 5000 5000 6230 6240 125 125 70-149 0 30 1,2,3-Trichlorobenzene ug/L ND 5000 5000 5360 5850 107 117 70-135 9 30 1,2,3-Trichloropropane ug/L ND 5000 5000 5620 5580 112 112 71-137 1 30 1,2,4-Trichlorobenzene ug/L ND 5000 5000 5470 5680 109 114 73-140 4 30 1,2-Dibromo-3- ug/L ND 5000 5000 5620 5780 112 116 65-134 3 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 5000 5000 5790 5710 116 114 70-137 1 30 1,2-Dichlorobenzene ug/L ND 5000 5000 5670 5610 113 112 70-133 1 30 1,2-Dichloroethane ug/L ND 5000 5000 5620 5580 112 112 70-137 1 30 1,2-Dichloropropane ug/L ND 5000 5000 5780 5700 116 114 70-140 1 30 1,3-Dichlorobenzene ug/L ND 5000 5000 5590 5610 112 112 70-135 0 30 1,3-Dichloropropane ug/L ND 5000 5000 5810 5670 116 113 70-143 2 30 1,4-Dichlorobenzene ug/L ND 5000 5000 5630 5570 113 111 70-133 1 30 2,2-Dichloropropane ug/L ND 5000 5000 5850 5750 117 115 61-148 2 30 2-Butanone (MEK) ug/L ND 10000 10000 11000 11400 110 114 60-139 3 30 2-Chlorotoluene ug/L ND 5000 5000 5700 5670 114 113 70-144 0 30 2-Hexanone ug/L ND 10000 10000 10800 10900 108 109 65-138 0 30 4-Chlorotoluene ug/L ND 5000 5000 5760 5780 115 116 70-137 0 30 4-Methyl-2-pentanone ug/L ND 10000 10000 10700 11100 107 111 65-135 4 30 (MIBK) Acetone ug/L ND 10000 10000 11400 11900 114 119 60-148 4 30 Benzene ug/L ND 5000 5000 5900 5860 118 117 70-151 1 30 Bromobenzene ug/L ND 5000 5000 5720 5720 114 114 70-136 0 30 Bromochloromethane ug/L ND 5000 5000 6000 5960 120 119 70-141 1 30 Bromodichloromethane ug/L ND 5000 5000 5450 5480 109 110 70-138 0 30 Bromoform ug/L ND 5000 5000 5240 5220 105 104 63-130 0 30 Bromomethane ug/L ND 5000 5000 7120 7510 142 150 15-152 5 30 IH,IK, v1 Carbon tetrachloride ug/L ND 5000 5000 6040 5950 121 119 70-143 1 30 Chlorobenzene ug/L ND 5000 5000 5760 5650 115 113 70-138 2 30 Chloroethane ug/L ND 5000 5000 6380 6280 128 126 52-163 2 30 Chloroform ug/L ND 5000 5000 5830 5900 117 118 70-139 1 30 Chloromethane ug/L ND 5000 5000 5510 5400 110 108 41-139 2 30 cis-1,2-Dichloroethene ug/L 1770 5000 5000 7560 7550 116 116 70-141 0 30 cis-1,3-Dichloropropene ug/L ND 5000 5000 5640 5620 113 112 70-137 0 30 Dibromochloromethane ug/L ND 5000 5000 5680 5600 114 112 70-134 1 30 Dibromomethane ug/L ND 5000 5000 5710 5690 114 114 70-138 0 30 Dichlorodifluoromethane ug/L ND 5000 5000 6140 6010 123 120 47-155 2 30 Diisopropyl ether ug/L ND 5000 5000 5700 5760 114 115 63-144 1 30 Ethylbenzene ug/L ND 5000 5000 5740 5610 115 112 66-153 2 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 97 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2787017 2787018 MS MSD 92461009021 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Hexachloro-1,3-butadiene ug/L ND 5000 5000 5320 5600 106 112 65-149 5 30 m&p-Xylene ug/L ND 10000 10000 11600 11400 116 114 69-152 2 30 Methyl-tert-butyl ether ug/L ND 5000 5000 5620 5550 112 111 54-156 1 30 Methylene Chloride ug/L ND 5000 5000 5820 5800 116 116 42-159 0 30 Naphthalene ug/L ND 5000 5000 5170 5740 103 115 61-148 10 30 o-Xylene ug/L ND 5000 5000 5690 5540 114 111 70-148 3 30 p-Isopropyltoluene ug/L ND 5000 5000 5780 5690 116 114 70-146 2 30 Styrene ug/L ND 5000 5000 5810 5670 116 113 70-135 2 30 Tetrachloroethene ug/L 7380 5000 5000 13600 13300 124 119 59-143 2 30 Toluene ug/L ND 5000 5000 5610 5480 112 110 59-148 2 30 trans-1,2-Dichloroethene ug/L ND 5000 5000 6150 6010 123 120 70-146 2 30 trans-1,3-Dichloropropene ug/L ND 5000 5000 5550 5550 111 111 70-135 0 30 Trichloroethene ug/L 41100 5000 5000 46900 46600 115 110 70-147 1 30 Trichlorofluoromethane ug/L ND 5000 5000 5970 5890 119 118 70-148 1 30 Vinyl acetate ug/L ND 10000 10000 12100 12300 121 123 49-151 2 30 Vinyl chloride ug/L ND 5000 5000 6920 6830 138 137 70-156 1 30 Xylene (Total) ug/L ND 15000 15000 17300 17000 115 113 63-158 2 30 1,2-Dichloroethane-d4 (S) % 103 102 70-130 4-Bromofluorobenzene (S) % 102 100 70-130 Toluene-d8 (S) % 98 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 98 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 519870 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92461009001, 92461009002, 92461009003, 92461009004, 92461009005, 92461009006, 92461009007, 92461009008,92461009009 METHOD BLANK: 2782227 Matrix: Water Associated Lab Samples: 92461009001, 92461009002, 92461009003, 92461009004, 92461009005, 92461009006, 92461009007, 92461009008,92461009009 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride mg/L ND 1.0 0.60 01/17/20 22:17 Sulfate mg/L ND 1.0 0.50 01/17/20 22:17 LABORATORY CONTROL SAMPLE: 2782228 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 50 51.7 103 90-110 Sulfate mg/L 50 50.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2782229 2782230 MS MSD 92460490070 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride mg/L 6.5 50 50 65.9 66.4 119 120 90-110 1 10 M1 Sulfate mg/L 0.61J 50 50 58.9 59.4 117 118 90-110 1 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2782231 2782232 MS MSD 92461004002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride mg/L 12.3 50 50 71.8 72.3 119 120 90-110 1 10 M1 Sulfate mg/L 10.0 50 50 68.9 69.4 118 119 90-110 1 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 99 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 519871 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92461009010, 92461009011, 92461009012, 92461009013, 92461009014, 92461009015, 92461009016, 92461009017,92461009018,92461009019,92461009020,92461009021,92461009022 METHOD BLANK: 2782233 Matrix: Water Associated Lab Samples: 92461009010, 92461009011, 92461009012, 92461009013, 92461009014, 92461009015, 92461009016, 92461009017,92461009018,92461009019,92461009020,92461009021,92461009022 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride mg/L ND 1.0 0.60 01/18/20 05:44 Sulfate mg/L ND 1.0 0.50 01/18/20 05:44 LABORATORY CONTROL SAMPLE: 2782234 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 50 52.1 104 90-110 Sulfate mg/L 50 51.0 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2782235 2782236 MS MSD 92461009010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride mg/L 3.0 50 50 63.5 63.6 121 121 90-110 0 10 M1 Sulfate mg/L 5.8 50 50 65.8 65.6 120 120 90-110 0 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2782237 2782238 MS MSD 92461009020 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride mg/L 13.2 50 50 74.0 74.1 122 122 90-110 0 10 M1 Sulfate mg/L 15.4 50 50 75.7 76.2 121 122 90-110 1 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 100 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 520064 Analysis Method: SM 531 OB-2011 QC Batch Method: SM 531 OB-2011 Analysis Description: 5310E TOC Associated Lab Samples: 92461009001, 92461009002, 92461009003, 92461009004, 92461009005, 92461009006, 92461009007, 92461009008,92461009009,92461009010,92461009011,92461009012,92461009013,92461009014, 92461009015,92461009016,92461009017,92461009018,92461009019,92461009020 METHOD BLANK: 2783248 Matrix: Water Associated Lab Samples: 92461009001, 92461009002, 92461009003, 92461009004, 92461009005, 92461009006, 92461009007, 92461009008,92461009009,92461009010,92461009011,92461009012,92461009013,92461009014, 92461009015,92461009016,92461009017,92461009018,92461009019,92461009020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 0.50 01/20/20 21:48 LABORATORY CONTROL SAMPLE: 2783249 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.2 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2783250 2783251 MS MSD 92461009001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 10.9 25 25 35.3 35.3 97 98 90-110 0 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2783252 2783253 MS MSD 92461009011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L ND 25 25 24.7 24.6 98 98 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 101 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Trex-Charlotte GW Pace Project No.: 92461009 QC Batch: 520472 Analysis Method: SM 531 OB-2011 QC Batch Method: SM 531 OB-2011 Analysis Description: 5310E TOC Associated Lab Samples: 92461009021, 92461009022 METHOD BLANK: 2784937 Matrix: Water Associated Lab Samples: 92461009021, 92461009022 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 0.50 01/21/20 15:27 LABORATORY CONTROL SAMPLE: 2784938 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.7 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2784939 2784940 MS MSD 92461009021 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 2.0 25 25 25.4 25.2 94 93 90-110 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2784941 2784942 MS MSD 92461146004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 0.59J 25 25 23.7 23.7 92 92 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 102 of 114 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Trex-Charlotte GW Pace Project No.: 92461009 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PAN Pace Analytical National PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. ML Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased low. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 103 of 114 Pace Analytical Services, LLC ceAnalyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Trex-Charlotte GW Pace Project No.: 92461009 ANALYTE QUALIFIERS v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 104 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Trex-Charlotte GW Pace Project No.: 92461009 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92461009001 PMW-1A RSK175 1413908 RSK-175 1413908 92461009002 PMW-1 B RSK175 1413908 RSK-175 1413908 92461009003 PMW-2A RSK175 1413908 RSK-175 1413908 92461009004 PMW-2B RSK175 1413908 RSK-175 1413908 92461009005 PMW-3A RSK175 1413908 RSK-175 1413908 92461009006 PMW-4A RSK175 1413908 RSK-175 1413908 92461009007 PMW-5A RSK175 1413908 RSK-175 1413908 92461009008 PMW-6A RSK175 1413908 RSK-175 1413908 92461009009 PMW-7A RSK175 1413908 RSK-175 1413908 92461009010 PMW-7B RSK175 1413908 RSK-175 1413908 92461009011 PMW-8A RSK175 1413908 RSK-175 1413908 92461009012 PMW-8B RSK175 1413908 RSK-175 1413908 92461009013 PMW-9A RSK175 1414316 RSK-175 1414316 92461009014 PMW-9B RSK175 1414316 RSK-175 1414316 92461009015 PMW-9C RSK175 1414316 RSK-175 1414316 92461009016 PMW-10A RSK175 1414316 RSK-175 1414316 92461009017 PMW-10B RSK175 1414316 RSK-175 1414316 92461009018 PMW-11A RSK175 1414316 RSK-175 1414316 92461009019 PMW-11B RSK175 1414316 RSK-175 1414316 92461009020 PMW-13B RSK175 1414316 RSK-175 1414316 92461009021 PMW-DUP1 RSK175 1414316 RSK-175 1414316 92461009022 PMW-DUP2 RSK175 1414316 RSK-175 1414316 92461009001 PMW-1A EPA 3010A 519857 EPA 6010D 519877 92461009002 PMW-1 B EPA 3010A 519857 EPA 6010D 519877 92461009003 PMW-2A EPA 3010A 519857 EPA 6010D 519877 92461009004 PMW-2B EPA 3010A 519857 EPA 6010D 519877 92461009005 PMW-3A EPA 3010A 519857 EPA 6010D 519877 92461009006 PMW-4A EPA 3010A 519857 EPA 6010D 519877 92461009007 PMW-5A EPA 3010A 519857 EPA 6010D 519877 92461009008 PMW-6A EPA 3010A 519857 EPA 6010D 519877 92461009009 PMW-7A EPA 3010A 519857 EPA 6010D 519877 92461009010 PMW-7B EPA 3010A 519857 EPA 6010D 519877 92461009011 PMW-8A EPA 3010A 519857 EPA 6010D 519877 92461009012 PMW-8B EPA 3010A 519857 EPA 6010D 519877 92461009013 PMW-9A EPA 3010A 519857 EPA 6010D 519877 92461009014 PMW-9B EPA 3010A 519857 EPA 6010D 519877 92461009015 PMW-9C EPA 3010A 519857 EPA 6010D 519877 92461009016 PMW-10A EPA 3010A 520385 EPA 6010D 520403 92461009017 PMW-10B EPA 3010A 520385 EPA 6010D 520403 92461009018 PMW-11A EPA 3010A 520385 EPA 6010D 520403 92461009019 PMW-11 B EPA 3010A 520385 EPA 6010D 520403 92461009020 PMW-13B EPA 3010A 520385 EPA 6010D 520403 92461009021 PMW-DUP1 EPA 3010A 520385 EPA 6010D 520403 92461009022 PMW-DUP2 EPA 3010A 520385 EPA 6010D 520403 92461009001 PMW-1A EPA8260D 520274 92461009002 PMW-1 B EPA 8260D 520139 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 105 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Trex-Charlotte GW Pace Project No.: 92461009 Lab ID Sample ID QC Batch Method QC Batch 92461009003 PMW-2A EPA 8260D 520138 92461009004 PMW-2B EPA 8260D 520138 92461009005 PMW-3A EPA 8260D 520274 92461009006 PMW-4A EPA 8260D 520274 92461009007 PMW-5A EPA 8260D 520274 92461009008 PMW-6A EPA 8260D 520137 92461009009 PMW-7A EPA 8260D 520274 92461009010 PMW-7B EPA 8260D 520274 92461009011 PMW-8A EPA 8260D 520137 92461009012 PMW-8B EPA 8260D 520138 92461009013 PMW-9A EPA 8260D 520137 92461009014 PMW-9B EPA 8260D 520274 92461009015 PMW-9C EPA 8260D 520139 92461009016 PMW-10A EPA 8260D 520139 92461009017 PMW-10B EPA 8260D 520139 92461009018 PMW-11A EPA 8260D 520274 92461009019 PMW-11 B EPA 8260D 520274 92461009020 PMW-13B EPA 8260D 520274 92461009021 PMW-DUP1 EPA 8260D 520868 92461009022 PMW-DUP2 EPA 8260D 520274 92461009023 SW-1 EPA 8260D 520139 92461009024 SW-2 EPA 8260D 520137 92461009025 SW-3 EPA 8260D 520137 92461009026 EB-1 EPA 8260D 520137 92461009027 EB-2 EPA 8260D 520137 92461009028 Trip Blank 1 EPA 8260D 520137 92461009029 Trip Blank 2 EPA 8260D 520137 92461009030 Trip Blank 3 EPA 8260D 520137 92461009031 Trip Blank 4 EPA 8260D 520137 92461009001 PMW-1A EPA 300.0 Rev 2.1 1993 519870 92461009002 PMW-1 B EPA 300.0 Rev 2.1 1993 519870 92461009003 PMW-2A EPA 300.0 Rev 2.1 1993 519870 92461009004 PMW-2B EPA 300.0 Rev 2.1 1993 519870 92461009005 PMW-3A EPA 300.0 Rev 2.1 1993 519870 92461009006 PMW-4A EPA 300.0 Rev 2.1 1993 519870 92461009007 PMW-5A EPA 300.0 Rev 2.1 1993 519870 92461009008 PMW-6A EPA 300.0 Rev 2.1 1993 519870 92461009009 PMW-7A EPA 300.0 Rev 2.1 1993 519870 92461009010 PMW-7B EPA 300.0 Rev 2.1 1993 519871 92461009011 PMW-8A EPA 300.0 Rev 2.1 1993 519871 92461009012 PMW-8B EPA 300.0 Rev 2.1 1993 519871 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch Page 106 of 114 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Trex-Charlotte GW Pace Project No.: 92461009 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92461009013 PMW-9A EPA 300.0 Rev 2.1 1993 519871 92461009014 PMW-9B EPA 300.0 Rev 2.1 1993 519871 92461009015 PMW-9C EPA 300.0 Rev 2.1 1993 519871 92461009016 PMW-10A EPA 300.0 Rev 2.1 1993 519871 92461009017 PMW-10B EPA 300.0 Rev 2.1 1993 519871 92461009018 PMW-11A EPA 300.0 Rev 2.1 1993 519871 92461009019 PMW-11 B EPA 300.0 Rev 2.1 1993 519871 92461009020 PMW-13B EPA 300.0 Rev 2.1 1993 519871 92461009021 PMW-DUP1 EPA 300.0 Rev 2.1 1993 519871 92461009022 PMW-DUP2 EPA 300.0 Rev 2.1 1993 519871 92461009001 PMW-1A SM 5310E-2011 520064 92461009002 PMW-1 B SM 5310B-2011 520064 92461009003 PMW-2A SM 5310E-2011 520064 92461009004 PMW-2B SM 5310E-2011 520064 92461009005 PMW-3A SM 5310E-2011 520064 92461009006 PMW-4A SM 5310E-2011 520064 92461009007 PMW-5A SM 5310E-2011 520064 92461009008 PMW-6A SM 5310E-2011 520064 92461009009 PMW-7A SM 5310E-2011 520064 92461009010 PMW-7B SM 5310E-2011 520064 92461009011 PMW-8A SM 5310E-2011 520064 92461009012 PMW-8B SM 5310E-2011 520064 92461009013 PMW-9A SM 5310E-2011 520064 92461009014 PMW-9B SM 5310E-2011 520064 92461009015 PMW-9C SM 5310E-2011 520064 92461009016 PMW-10A SM 5310B-2011 520064 92461009017 PMW-10B SM 5310B-2011 520064 92461009018 PMW-11A SM 5310B-2011 520064 92461009019 PMW-11 B SM 5310B-2011 520064 92461009020 PMW-13B SM 5310B-2011 520064 92461009021 PMW-DUP1 SM 5310B-2011 520472 92461009022 PMW-DUP2 SM 5310B-2011 520472 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /23/2020 03:52 PM without the written consent of Pace Analytical Services, LLC. Page 107 of 114 Document Name: Document Revised: February 7, 2018 m IeAnalyfidat Sample Condition U on Receipt(SCUR) Page I of 2 Document No.: Issuing Authority: j F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: i Asheville ❑ Eden[] Greenwood ❑ Huntersville E] Raleigh❑ Mechanicsville❑ ConditionSample client Name: W®# : 92461®Q9 Upon Receipt ••r Project ii: Courier: OF€dEx OUPS ❑LISPS ❑Client ❑ Commercial []Pace ❑Other; 924B1A>j9 1 Custody Seal Present? ❑Yes []No seals IntaO ❑Yes []No yr. Packing Material: ❑Bubble Wrap ❑Bubble Bags []None ❑ Other Thermometey: 92T058 Type of Ira: wet [:]Blue❑IR Gun ID: 71 i Cooler Temp ('C): correction Factorr�:JAdd/Subtract ('C) O°C Cooler Temp Corrected(' USDA Regulated Soil ([� N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? n>rPs nN„ Oete/Initials Person Examining ContenWs —t'J—� -/ e'-7-Q,/ Bloingical Tissue Fro2en? ❑Nave ❑Yes ❑No [TN/A Temp should be above freezing to 6'C []Samples out of temp criteria. Samples on ice, cooling process hasbegvn Did samples originate from a forelrn source (internationally, Includine Hawail and Puerto Riroll f lYes FlNo Comments/DLcre anc : Chain of Custody Present? ❑res ❑Na ❑NIA 1. 2. Samples Arrived within Hold Time? ❑Yes ❑No _ , ❑N/A Short Hold Time Analysis 1<72 hr.)? ❑Yes Q No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes ❑No []N/A Al. Sufficient Volume? ❑Yes ❑Na L]N/A 5. Correct Containers Used? -Pace Containers Used? ❑Yes ❑yes ❑No -❑No []N/A []N/A 6. Containers Intact? , Yes ❑No ❑N/A Z. Dissolved analysis: Samples Field Filtered? [:]Yes []No ❑fV A 8. Sample Labels Match CCIC? -Includes Date/Time/IO/analysis Matrix: 0<es w ❑No ❑N/A 9. j Headspace in VOA Vials (?5-6mm)? Ely,. ---No ❑N/A 10. Trip Blar,k Present? Trip Sian l CustodySeals Present? Yes Yes ❑No Na ❑N/A [:]N/A 11. COMMENTS/SAMPLE DISCREPANCY Field Data Reclutred? ❑Yes ❑No Lot ID of split Containers: CLIENT NOTIFICATION/RESOLUTION 'erson contacted: Date/Time: l Project Manager SCURF Review: Date: Zp Project Manager SRF Review: Date: VZO Page 108 of 114 Document Name: Document Revised: February 7, 2018 =Analyfieal Sam le Condition Upon Recel tiSCURi Page 1 of 2 Document No.: Issuing Authority: ( F-CAR•CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, Toc, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle _ Project A WO# : 92461409 Pm: PTE Due Date: 01/23/20 CLIENT: 92-EnviroAna _ z " U 4 ,; Q n Z 2 2 Z`t 2 iJ N N O 1p Z C✓1 ryry rl v a C z Z d 2 -O Oi �' Jv v 2 v Z a 2 m v x v °� a�i { v 2 N v x d x z 4 Z = ? S a Z Z a Q Z in 2 N. c c a N Z¢D -yam.. In y 2 J e$c c a a a m N a a ry j a a a E ¢ E Q 6 v E E Q o rev ¢ O Q p > a O > O 7 a u J ^ a G J u A E E in N E O 1n E O C5 d Y .- — E in N J E O In E rn N E �n N :c. J E C N Q `u J E o L9 J E y E C) E E N �O =° } E In N J E G J E S ei E O N E q V rl a N a Vl n ."1 a �..� N Z a T +a.V '+ ri rn 7 7 M ' FtE m a 7 m m m m m m ca m rt a a a a a a C a } 0 7 AA H m a o \\V7 3 L 7 4 -- ` } Tl _ b ? r r -, 10 y J J } 1 1 l 1 I I pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot tl 1 Note: Whenever there is a discrepancy anecting Nortn Carolina compliance samples, a copy or tnrs Form wiu oe sent io the rvann "rouna utnnn i eftmcanon Vince ti.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 109 of 114 Document Name: Document Revised: February 7, 2018 s, Sample Condition Upon Recei t(SCUR) Page 1 of 2 aceAnalytrr,�! Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quall Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions! VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle �)Z Project It Wp# : 92461009 Due Date: 01/23/20 92-EnviroAna pN: PTE CLIENT: zt z -° a y u m FL J E „N 'r J v C. m z 8i a 7 u_ }� d a J E N ' ref a m 4 8 u r7 a J E, CD V�5 J N e, m z c n u G a ••1 ? rr M m N v N N V N H IL 0 fV v 2 4 ro n E N x eq 6 m z ea z N a J E -i N V 4 m ry ri n O Z a J E ,N-I V a m ai a C � ' ° E v Vr z v c a E Q er .+ C7 a v u E Q v S rl r7 a 2 E d r a N 7 m l7 a N v a E Q ,, r%1 rl l7 a ry y x `� x E ¢ J E U1 e�'] W a -7 v x z E Q o N r�l U' a Z Q E 1 C1 C7 a ¢ ? O rNj z Q O 7 E d1 17 a a C n a O E V C7 [7 p rY5 x, 4 O �! E i 6 QI t7 a> ? v '11 + " v M w Y Q t] ? ♦+ R a i r a J 9 - Y ti > d Z 4 m N J E Ny F 1A 6 1 a . z a yN d yr E N r N a w, M C1 as S Z « rL J E a 4" 6 m '8 =� ° 7 s E a J E 7 O l7 a V o J EEE N 3 (t�� r7r 5 0 y CL C m E J V QI V' a 2 - 7 3 fi i l 1 7 l 9 10I ( ) 1 11 I � 1 N 1 \1 12 NNN) � 1* 1 I N pH Adjustment Log for Preserved Samples Sample ID Type of preservative pH ua»n receipt Date preservation adjusted Time preservation adjusted Amount of Preservative addec Rot d Note: whenevertnere is a rllscrepancy affecting Nortn Carolina compliance samples, a copy orLn15 form Wln uesent to tneNortn t,arollna UCnlvrt c.erttncatrun Vance tl.e Out of hold, incorrect preservative, out of temp, incorrect containers. Page 110 of 114 Document Name: Document Revised: February 7, 2019 Sample Condition Upon Recelpt(SOUR) Page 1 of 2 ace Analytical Document No.: issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle p3 Project # WO# : 92461009 PM: PTE Due Date: 01/23/20 CLIENT: 92—EnviraAna E +� 3 W Wlu n c u v a E rl a a m 4l c c u ; a E o N ran a Go W N C u , a ^� E y'�y ' r4 a Co Z 32yr Y/ 7 +• 2 1 �, i rl I a m V V .5 N Ydi n. E 0 rNF ,� 0 N V Q, Z 4 ro n E Nryy 4 m x Z rt• 4 a N m a J E Ln v d CO ryry ri a 2 p 2 A a 1 E Ln a a � TO E v " � Z i- d 0. 7 a E a « rs .�, l7 a Y n Z a E a y e� ._. C7 Q as v�i n ? E a o �, N M C7 Q ry V C O N E a '.� C7 4 i V A Q = E a J E ,�, r i M l7 Q u U Z L E a a rev � � _a ril [7 a _ a z d 0 E o 1 a �ry C Z N C C } q rn ''r lT}> _ a ? a a E io I a', 0 = ? v d ¢ b _ E o q 06, y LM m a Lf$Z * w y " a ? lE 2 a y 9 .fir lY7 i }i w a N J E Ln 'I r ? V •+ a a cn E 0 N _ 0;'D Qy to N n s U a J E N d vai P. c E E S ri Z c 'e c vU E a N ? d tv d a E o V } 4 2 3 l 4 ) I d - 5 1 7 FT— 8 9 Il 12 N\ i pH Adjustment Log for Preserved Samples Sample ID Type of Preservatly pH upon receipt Date preservation adjusted Time preservation adjusted .Amount of preservative added Lot h Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy ar EMS form vvul oe sent to the Norm c aronna uetirvn c.ertuicauon VrriCe ii.e. put of hold, incorrect preservative, out of temp, incorrect containers. Page 141 of 114 p i y m ;a C d z D X m m 0 o A N cn z Q 4 n rn m 'i I I TEMP in C t Received on Ice (YIN) uslo y Sealed Cooler YIN Samples matt lYfN) N o m co V m (Aa w N ITEM # Z m n 3 p n m m= w m �. a. 2 g a 03 3 3 3 D- 0 o m m m m D 9 m V D D b Y D ca D y O 3 _� a o < m n c N o o g a m n N D ❑ a n u 3 m v O.0 °5 r M M v oc n O O a q x8 rn 3 3P�Owvehn o e8w_F� N y S O O C O tD Ip f9 [n�:09 �"2 "Imoa A 2i N 3 0 p v W R � MATRIX CODE (sse valid codes to leA) o it a _ SAMPLETYPE (O-GRAB C=COMP) '1 ° � x O rn rn j m A 5 m O z r m h m m a n v r m T C 0 zz r � o m r z Q - In - SAMPLE TEMP AT COLLECTION — # OF CONTAINERS X `—1 1 lS. unpreservad H2SO4 X yC ;X �. < HNO3 - X X �. -X HCI NaOH o e Na2.S203 11 Methanol r� }t %< ;x. Other o Analyses Test ` < X x x x x x 1>9 VOC by 8260 < x x x x X I X X TOCby5310 < x X x x x x x Sulfate, Chloride by 300 < x x x x x x X Iron by 6010 c x X x x x x x Elhene by RSK Trip BLANK 01 Waler Residual Chlorine (YIN) 0 3 n al 7 Z c -n Vl O 0 m d v n p D N C N N = n m d o MID gc m v m p > rr- ca f° N 0 � Qa C nn G1 o` m �C $ ry N < (D o = C 3 R! n N N 1"f Cv C sa p 0 m C n a (A rD r- � rt CL tv n E3 Z � rn y) M w TD c � m 7 D LD o � a tJ n A o -n 4W Page 112 of 114 X v m rn D n aJ u A w N CDa oo Vi m A w ITEM # O 'm N C' cm m n 3a a 2 to cn ro ro v v ro v ro ro v En r_ v C:w m D w D C� m Y y 0 v o m 3 N ° y o niF n n - N o m m u » N�� �00 rn �C O C g �, m a x % o w 3 ❑ N 0 O m 4 MATRIX CODE (see valid cedes to left) o cG 44 # SAMPLE TYPE (G=GRAB G=COMP) v v m fDn Cn a F £ I(yr > O 'D Ln z R D 0 m = p n c m v 3 n re F; m m m O D n y .. i!, m v v - - �- -C- C-- A A Z O m SAMPLE TEMP AT COLLECTION C m mmnn O OF CONTAINERS o _D n s 0 o 'n v �' A a 3° u m o 4 °. m y Unpreserved \j11{1I m ° ° N , �4 �. y H2SO4 m � ii ro ' z n a H N 03 m m HCI m .rk' ?< Y 2 NaOH m N 0 Na2S203 no K m N o Methanol .n ((' m CD < Other ?4 7t i4 > 'n a ° N Analyses Test YIN x x x x x X x X X X x x vac by 8260 z x x x x x x x x x x TOC by 5310 m p x x x x x x x x x x Sulfate, Chloride by 300 L� x x X X x X x x x x Iron by6010 Q n x x X x x x x x x x Ethene by RSK Trip BLANK E H H DI Water n° m m �t = � z 3 m � v TEMP in C m 9 w Residual Chlorine (Y!N} _ La y m � 0 o I t m ° Received on Ice ^ r; 9 D N (Y1N) 007i'1 o Custody Sealed Cooler o o O Y!N y Samples C- Intact r w (YIN) m /Z1 < m m (p a (/I 3 cr n n v CD m a m ''* a w n C m m Page 113 of 114 w w w as w w w N N N -4 N Iv ITEM # c C 0 2, m a 3 �' rn (A A w AN O W CC 0 (h m= w Nw 0 m o o 7 a y m m T 9? w W nr m v m m iv NO b O N d j [ S- 3 V/ m ro C N N p O o �J m 2 0 0 a � rn s y H n r- i M >n w ;r 0 n .:.'9 o' a C 7 C v o 3 0 a z � 3 �2EFo�SmS�� m � n @ C O �0a���90 » m C a C m # Z m a O- a C a N O 0 @ MATRIX CODE (sea valid codas to left) C # C n C SAMPLE TYPE (G=GRAB C=COMP) x m D \� m ❑ � m mm Q1 v o � £ 7 D T � D A m G) 3 O 1 a , z m n - y A m 3 n 3 m C• 6 N C, e-. C G V F? rn m O _ _ p Y Z, r rn r rn Z n �.' SAMPLE TEl COLLECTION m ry (ai_s. # OF CONTAINERS v v m a o Y Unpresarved M a o -00 a, a N m `� o n' o m as H2SO4 n � m n $ HNO3 m m HCI o C. m / NaOH in N Na2S203 N m Methanol m w o m Other M Analyses Test YIN ( r T N x x x VOC by all n s o TOG by 5310 3 M N m Sulfate, Chloride by 300 iQ c N Iron by 6010 a a Ethel by RSK _ 1 x x x Trip BLANK fillx N p DI Water _ m C a IF ! m m La r _1 TEMP in C ; (' i `D Residual Chlorine (Y!N) j n m o to iu Recelvad an Ice 9 D w (YIN) x _% o a n Custody Sealed ❑ } vlj O Cooler 1 ° - 11 Y1N Z N a Samples Intact w (YIN) 3 rD 2 n D Z . �rO N O 0 C N L/ ❑f M p O � O D C m, Z 'y, 0 v w m C CD m Nrt �v O m 0 n = a CD ID � m a, !v C w CD � Page 114 of 114 EnviraAnalytics Group APPENDIX D GRAPHS OF CONTAMINANT CONCENTRATIONS VERSUS TIME TRENDS 2500 2000 1500 1000 500 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-1A 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane f 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene tTrichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-1B 350 300 250 200 150 100 50 0 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene --40---Trichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) 1400 1200 ............ 1000 800 600 400 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-2A 200 0 • • 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene tTrichloroethene t Vinyl chloride •••••• Linear(1,1,1-Trichloroethane) •••••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) Bann 400 200 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-2B G i � 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene tTrichloroethene --*—Vinyl chloride •••••• Linear(1,1,1-Trichloroethane) •••••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) 25000 20000 15000 10000 5000 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-3A ................ 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene --6—Tetrachloroethene tTrichloroethene t Vinyl chloride •••••• Linear(1,1,1-Trichloroethane) •••••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) 700 600 500 400 300 200 100 0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-4A ............. .......................... ........... 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane + 1,1-Dichloroethene cis-1,2-Dichloroethene --*—Tetrachloroethene tTrichloroethene tVinyl chloride •••••• Linear(1,1,1-Trichloroethane) •••••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-5A 120,000 100,000 80,000 60,000 40,000 20,000 ......... .... 0 i 222 - 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene tTetrachloroethene tTrichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) 100,000 90,000 80,000 70,000 60,000 50,000 40,000 30,000 20,000 10,000 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-6A ..................... �= — — 0 = r 11/27/2018 2/20/2019 7/24/2019 1/15/2020 • — - 1,1,1-Trichloroethane + 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene tTrichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-7A 3000 2500 2000..................................................... 1500 1000 500 0 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane t 1,1-Dichloroethene t cis-1,2-Dichloroethene --*—Tetrachloroethene --*—Trichloroethene Vinyl chloride •••••• Linear(1,1,1-Trichloroethane) •••••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-7B 9000 8000 7000 6000 5000 4000 3000 2000 1000 0 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene tTrichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-8A 700.0 600.0 500.0 400.0 300.0 200.0 "j 1,1,1-Trichloroethane 100.0 0.0 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1-Dichloroethene t cis-1,2-Dichloroethene tTetra chloroethene tTrichloroethene tVinyl chloride •••••• Linear(1,1,1-Trichloroethane) •••••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-8B 1200 1000 800 600 400 200 0 i 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene tTrichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) 600 500 400 300 200 100 0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-9A 11/27/2018 2/20/2019 7/24/2019 1/15/2020 —1,1,1-Trichloroethane — 1,1-Dichloroethene — cis-1,2-Dichloroethene --*—Tetra ch lo roethe ne —Trichloroethene —Vinyl chloride •••••• Linear(1,1,1-Trichloroethane) •••••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-9B 2000 1800 1600 1400 1200 1000 800 600 400 200 --------------- 0 i 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane 1,1-Dichloroethene --6— cis-1,2-Dichloroethene �Tetrachloroethene --40---Trichloroethene t Vinyl chloride •••••• Linear(1,1,1-Trichloroethane) ••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) 60,000.0 50,000.0 40,000.0 30,000.0 20,000.0 10,000.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-9C 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene tTetrachloroethene tTrichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-10A 70,000 60,000 50,000 40,000 30,000 20,000 10,000 — 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t 1,1,1-Trichloroethane f 1,1-Dichloroethene t cis-1,2-Dichloroethene tTetrachloroethene tTrichloroethene --*--Vinyl chloride ...... Linear (1,1,1-Trichloroethane) ...... Linear (1,1-Dichloroethene) ..... • Linear (cis-1,2-Dichloroethene) ------ Linear (Tetra ch lo roethe ne) ------ Linear(Trichloroethene) ...... Linear (Vinyl chloride) 60000 50000 40000 30000 20000 10000 0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-10B 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane f 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene tTrichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) 2,500.0 2,000.0 1,500.0 1,000.0 500.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-11A 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene tTrichloroethene --*—Vinyl chloride •••••• Linear(1,1,1-Trichloroethane) •••••• Linear(1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) • • • • • • Linear (Vinyl chloride) 2500 2000 1500 1000 500 0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-11B 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene --o—Trichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) 45,000.0 40,000.0 35,000.0 30,000.0 25,000.0 20,000.0 15,000.0 10,000.0 5,000.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - PMW-13B 11/27/2018 2/20/2019 7/24/2019 1/15/2020 1,1,1-Trichloroethane 1,1-Dichloroethene t cis-1,2-Dichloroethene t Tetrachloroethene — Trichloroethene t Vinyl chloride • • • • • • Linear (1,1,1-Trichloroethane) • • • • • • Linear (1,1-Dichloroethene) • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) • • • • • • Linear (Vinyl chloride) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - SW-1 80.0 70.0 60.0 50.0 40.0 30.0 20.0 10.0 0.0 • • • 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t cis-1,2-Dichloroethene tTetrachloroethene 0 -Trichloroethene • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) • • • • • • Linear (Trichloroethene) 160.0 140.0 120.0 100.0 80.0 60.0 40.0 20.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - SW-2 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t cis-1,2-Dichloroethene +Tetrachloroethene tTrichloroethene • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear (Tetra ch lo roethe ne) •••••• Linear(Trichloroethene) 120.0 100.0 80.0 60.0 40.0 20.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC VOC CONCENTRATIONS (ug/L) VS TIME - SW-3 11/27/2018 2/20/2019 7/24/2019 1/15/2020 f cis-1,2-Dichloroethene --0—Tetrachloroethene f Trichloroethene • • • • • • Linear (cis-1,2-Dichloroethene) •••••• Linear(Tetrachloroethene) •••••• Linear(Trichloroethene) 2500.0 2000.0 1500.0 1000.0 500.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - 1,1 Dichloroethene (Shallow Wells) 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-1A PMW-2A PMW-4A PMW-5A t PMW-8A PMW-9A PMW-10A t PMW-11A • • • • • • Linear (PMW-1A) • • • • • • Linear (PMW-2A) • • • • • • Linear (PMW-4A) • • • • • • Linear (PMW-5A) •••••• Linear(PMW-10A) 3000 2500 2000 1500 1000 500 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - 1,1 Dichloroethene (Deep Wells) 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-8B t PMW-9B PMW-9c PMW-10B PMW-13B • • • • • • Linear (PMW-9Q • • • • • • Linear (PMW-10B) 8000 7000 6000 5000 4000 3000 2000 1000 0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - 1,1,1 Trichloroethane 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-1A PMW-2A PMW-4A t PMW-5A PMW-10A t PMW-10B t PMW-11A • • • • • • Linear (PMW-1A) • • • • • • Linear (PMW-2A) • • • • • • Linear (PMW-4A) • • • • • • Linear (PMW-5A) • • • • • • Linear (PMW-10A) • • • • • • Linear (PMW-10B) 45000.0 40000.0 35000.0 30000.0 25000.0 20000.0 15000.0 10000.0 5000.0 0.0 ........... 11/27/2018 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - Tetrachloroethene (Shallow Wells) 2/20/2019 ............ 7/24/2019 1/15/2020 t PMW-1A PMW-2A PMW-3A PMW-4A PMW-5A PMW-6A PMW-7A t PMW-8A t PMW-9A PMW-10A PMW-11A • • • • • • Linear (PMW-1A) • • • • • • Linear (PMW-2A) • • • • • • Linear (PMW-3A) • • • • • • Linear (PMW-4A) • • • • • • Linear (PMW-5A) • • • • • • Linear (PMW-6A) • • • • • • Linear (PMW-10A) 25000 20000 15000 10000 5000 0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - Tetrachloroethene (Deep Wells) 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-1B PMW-2B PMW-7B t PMW-8B PMW-9B t PMW-9c t PMW-10B t PMW-11B PMW-13B • • • • • • Linear (PMW-1B) • • • • • • Linear (PMW-2B) • • • • • • Linear (PMW-7B) • • • • • • Linear (PMW-8B) • • • • • • Linear (PMW-9B) • • • • • • Linear (PMW-9Q • • • • • • Linear (PMW-10B) • • • • • • Linear (PMW-13B) 120,000 100,000 80,000 60,000 40,000 20,000 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME -Trichlorethene (Shallow Wells) L ...... Nsl� .... 0 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t PMW-IA t PMW-2A PMW-3A PMW-4A PMW-5A PMW-6A PMW-7A PMW-8A t PMW-9A t PMW-10A PMW-11A • • • • • • Linear (PMW-1A) • • • • • • Linear (PMW-2A) • • • • • • Linear (PMW-3A) • • • • • • Linear (PMW-4A) • • • • • • Linear (PMW-5A) • • • • • • Linear (PMW-6A) • • • • • • Linear (PMW-10A) 60000 50000 40000 30000 20000 10000 0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - Trichlorethene (Deep Wells) 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-1B PMW-2B PMW-7B t PMW-8B t PMW-9B PMW-9c PMW-10B t PMW-11B PMW-13B • • • • • • Linear (PMW-1B) • • • • • • Linear (PMW-2B) • • • • • • Linear (PMW-7B) • • • • • • Linear (PMW-8B) • • • • • • Linear (PMW-9B) • • • • • • Linear (PMW-9Q • • • • • • Linear (PMW-10B) • • • • • • Linear (PMW-13B) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - Cis 1,2 Dichloroethene (Shallow Wells) 6,000 5,000 4,000 3,000 2,000 1101010101 1,000 0 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t PMW-IA t PMW-2A t PMW-3A t PMW-4A t PMW-5A PMW-6A PMW-7A PMW-8A t PMW-9A PMW-10A PMW-11A • • • • • • Linear (PMW-1A) • • • • • • Linear (PMW-2A) • • • • • • Linear (PMW-3A) • • • • • • Linear (PMW-4A) • • • • • • Linear (PMW-5A) • • • • • • Linear (PMW-6A) •••••• Linear(PMW-10A) 2,500 2,000 1,500 1,000 500 0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - Cis 1,2 Dichloroethene (Deep Wells) 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-1B f PMW-2B PMW-7B PMW-8B PMW-9B PMW-9C PMW-10B PMW-11B PMW-13B • • • • • • Linear (PMW-1B) • • • • • • Linear (PMW-2B) • • • • • • Linear (PMW-7B) • • • • • • Linear (PMW-8B) • • • • • • Linear (PMW-9B) • • • • • • Linear (PMW-9C) • • • • • • Linear (PMW-10B) • • • • • • Linear (PMW-13B) 250 200 150 100 50 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC CONCENTRATIONS (ug/L) VS TIME - Vinyl Chloride 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t PMW-1A PMW-9A --0-- PMW-9B •••••• Linear (P MW-1A) Linear (PMW-9A) • • • • • • Linear (PMW-9B) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-1A & PMW-1B 14000 12000 10000 8000 6000 4000 t PMW-1A PMW-1B • • • • • • Linear (PMW-lA) • • • • • • Linear (PMW-lB) 2000 — 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 6000.0 5000.0 4000.0 3000.0 2000.0 1000.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-2A & MW-26 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t PMW-2A t PMW-2B • • • • • • Linear (PMW-2A) • • • • • • Linear (PMW-2B) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-3A & MW-4A 60000.0 50000.0 40000.0 30000.0 20000.0 10000.0 0.0 y 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t PMW-3A t PMW-4A • • • • • • Linear (PMW-3A) • • • • • • Linear (PMW-4A) 250000.0 200000.0 150000.0 100000.0 50000.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-5A & MW-6A 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-5A --H PMW-6A • • • • • • Linear (PMW-5A) • • • • • • Linear (PMW-6A) APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-7A & MW-76 35000.0 30000.0 25000.0 20000.0 15000.0 10000.0 5000.0 0.0 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 t PMW-7A PMW-7B • • • • • Linear (PMW-7B) 2000.0 1800.0 1600.0 1400.0 1200.0 1000.0 800.0 600.0 400.0 200.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-8A & MW-813 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-8A PMW-8B • • • • • • Linear (PMW-8B) 140000.0 120000.0 100000.0 80000.0 60000.0 40000.0 20000.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-9A, 9B & MW-9C 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-9A PMW-9B PMW-9C • • • • • • Linear (PMW-9A) • • • • • • Linear (PMW-9B) • • • • • • Linear (PMW-9C) 250000.0 — 200000.0 150000.0 100000.0 50000.0 0.0 9/26/2012 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-10A & MW-1013 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-10A t PMW-10B • • • • • • Linear (PMW-10A) • • • • • • Linear (PMW-10B) 25000.0 20000.0 15000.0 10000.0 5000.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-11A & MW-1113 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 --S-PMW-11A --*--PMW-11B 90000.0 80000.0 70000.0 60000.0 50000.0 40000.0 30000.0 20000.0 10000.0 0.0 APPENDIX D CONCENTRATION VERSUS TIME GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC TOTAL VOC CONCENTRATIONS (ug/L) VS TIME - PMW-13B 9/26/2012 9/23/2015 11/27/2018 2/20/2019 7/24/2019 1/15/2020 PMW-13B • • • • • • Linear (PMW-13B) EnviroAnafytics Group APPENDIX E IET 360-DAY DATA EVALUATION Innovative Environmental TWinologies, Inc. February 19th, 2020 Matthew Dostal Trex Properties, LLC Re: 360-Day Data Evaluation for 3114-3124 Cullman Ave. Site in Charlotte, NC Dear Mr. Dostal: Innovative Environmental Technologies, Inc. (IET) is pleased to provide an evaluation of the groundwater data collected at the Cullman Ave. site in Charlotte, NC. The sampling is being done to monitor the remedial injections that were completed from 1/7/2019- 1/17/2019. The injection plan included the direct injection of ferric iron activated persulfate at 20 permanent injection wells. One well (IW-16) was unable to be installed and three others (IW-1, IW-2 and IW-13) did not accept the proposed amount of reagent. In these instances field modifications were required in order to apply all the proposed reagent to the subsurface. In total IET injected 158,858 pounds of sodium persulfate, 13,826 pounds of ferric oxide powder in approximately 69,536 gallons of reagent across the site. The figure pictured below identifies the monitoring locations that are installed within the injection area and over the targeted injection zones. Each of these monitoring locations is evaluated below. Innovative Eniironmental Rchnoloor, Inc. ' PMW-10A PMW- 1A 1 (v4, — s� - did I P` A _ / fr-1 20) # PitIW-21 Y®— PM-2 to 1 PMW-6A ` a 1 ' 1 1 1 PMW-SA ilk'J W� 6O11RCE ARBOR coMAMIN[1noN ` Z iCCJ! uw-Sti7 vow-)x a o a6 40 �2a p DPT Locations PMW-1A PMW-3A f Figure 1. Monitoring Well Locations Innovative Emvmmnental T6bnoWws, Inc. PMW-1A This monitoring location is located south of the building and is screened at the shallower depth of 7-12' bgs. Injection wells 1 and 2 were installed in this area but daylighting from both wells occurred and a change in the application method of the reagent was applied. DPT locations were installed south of the building in order to apply the remaining reagent in this area. PMW-lA was sampled during the 30,120 and 360-day monitoring events and appears to have been impacted by the injection event, increases in sulfate, a drop in pH and increase in ORP confirm that the injected reagent was successfully applied to this area. The geochemical and analytical parameters have been included in the table below along with further discussion on the collected data. PMW-1A (7-12') Geochemical Parameters 11/27/2018 2/20/2019 7/24/2019 1/15/2020 Depth to Water ft. 5.42 7.08 5.03 H SU 6.25 3.06 4.88 5.58 Specific Conductance uMhos/cm) 367,000 2,100,000 1,010,000 1,270,000 Temperature C de 14.3 12.46 23.20 19.05 Dissolved Oxygen m /L 0.98 0.32 0.00 0.00 ORP my -64 411.7 123.0 130 Iron otal u /L 7,750 5,710 22,200 5,060 Sulfate u /L 20,000 1,380,000 414,000 634,000 I VOC's (u /L) 1,1,1 Trichloroethane <4.8 276 <3.5 16.3 1,1,2,2 Tetrachloroethane <4.0 78.6 22 <1.1 1,1,2 Trichloroethane <2.9 5.6 <4.7 <1.2 1,1 Dichloroethane <3.2 19 18 5.8 1,1 Dichloroethene <5.6 2J 13.4 <1.2 Chloromethane <1.1 13.1 <7.8 <1.9 Trans 1,2 Dichloroethene <4.9 13.9 <5.1 <1.3 cis-1,2-Dichloroethene 1,170 206 1,280 5 88 Methylene chloride 114J <25 <74 <18.4 Tetrachloroethene <4.6 181 282 71.7 Trichloroethene <4.7 480 2,180 218 Vin 1 Chloride 1 226 1 10.7 r 75.6 19 The proliferation of sulfate seen during the 30-day sampling event has since decreased along with the ORP value in the 360-day sampling event. This is likely a result of mineral formation of iron sulfates, as the concentration of iron increased during the 120-day event, but has since decreased to below it's baseline levels during the 360 day sampling event. pH is beginning to rebound, but remains below 6 which is just out of optimal range for enhanced attenuation via biological mechanisms. The ORP has remained slightly elevated at +132mV which is also out of the optimal range for facultative biological attenuation (typically -100mV to +100 mV). The total HVOC concentrations have decreased by 29% since the baseline sampling event and 74% since the 120-day rebound. Assuming the shallower soil's buffering capacity can increase the pH back to it's baseline level of 6.25, further decreases in these concentrations are expected in the next sampling events at PMW- lA as sulfate and iron concentrations have remained available. Innovative Emironmental T6bnoWws, Inc. PMW-3A This monitoring location is located south of the building and is screened at 15-25' bgs. Injection wells 1 and 2 were installed in this area but daylighting from both wells occurred and a change in the application method of the reagent was applied. DPT locations were installed south of the building in order to apply the remaining reagent in this area. PMW- 3A was sampled during the 30, 120 and 360-day monitoring events and appears to have been impacted by the injection event, increases in sulfate, a drop in pH and increase in ORP confirm that the injected reagent was successfully applied to this area. The geochemical and analytical parameters have been included in the table below along with further discussion on the collected data. PMW-3A (15-25') Geochemical Parameters 11/24/2018 2/20/2019 7/24/2019 1/15/2020 Depth to Water ft. 5.58 7.26 6.01 H U 5.61 4.18 4.25 5.16 Specific Conductance uMhos/cm) 155,000 4,480,000 4,250,000 764,000 Temperature C de 16.5 15.26 22.30 19.93 Dissolved Oxygen (m /L) 0.60 0.18 0.00 4.14 ORP(my) 191 300.1 471.0 450 Iron (Total)(ug/L 1,720 1,300 1,520 2,010 Sulfate /L 10,100 458,000 505,000 232,000 HVOC's /L 1,1,2,2 Tetrachloroed=c <50.0 <100.0 25.4 <11.1 1,1,2 Trichloroethane <36.2 <100 3.81 <11.8 Acetone <1250 <2500 343 953 Cis 1,2 Dichloroethane 1,030 243 48 845 Trans 1,2 Dichloroerhane <61.2 <100 73J 110 Terrachloroethene 20,600 7,610 1,500 3,870 Trichloroerhene 1,860 494 49 363 The proliferation of sulfate in PMW-3A continued through the 120-day sampling event, but has since decreased to 232,000 ug/L in the 360-day sampling period. The ORP has remained highly oxidizing at +450 mV, which indicates that the chemical oxidation via production of sulfate free radicals is continuing to occur. pH remains depressed as a result of generation/exhaustion of the sulfate free radicals causing temporarily acidic conditions. The HVOC concentrations have decreased in the 360-day sampling event by approximately 74%, when compared to they're baseline levels. Given PMW-3A's location on the upgradient edge of the plume and it's screened interval along the deeper zone of the targeted treatment area, fluctuations in HVOC concentrations seem to correlate with groundwater level. When groundwater is high, untreated water from under the building seems to migrate within this well screen, when groundwater is low during the summer months, concentrations decrease. So long as the well remains highly oxidizing overall degradation will occur, although at a slower rate than during the 120-day post injection period. For biological attenuation to occur at an enhanced rate the pH would need to return to neutral which depends on the bicarbonate alkalinity and buffering capacity of the groundwater is this area. Noting that baseline pH values were around 5.6 in PMW-3A. Innovative Emironmental'li'chnoMor, Inc. This monitoring location is located northeast of the building and is screened at 30-40' bgs. Injection wells 4 and 7 were installed and completed as proposed in this area. Daylighting from IW-7 was observed and thus was completed using a lower injection pressure. PMW- 5A was sampled during the 30, 120 and 360-day monitoring events and appears to have been impacted by the injection event, increases in sulfate, a drop in pH and increase in ORP confirm that the injected reagent was successfully applied to this area. The geochemical and analytical parameters have been included in the table below along with further discussion on the collected data. PMW-SA (30-40') Geochemical Parameters 11/26/2018 2/19/2019 7/24/2019 1/14/2020 Depth to Water ft. 3.97 5.42 3.96 H (SU) 6.6 5.34 5.55 5.15 Specific Conductance uMhos/cm) 243 4,078 2,050 1860 Temperature (C de) 19.2 16.02 23.11 19.45 Dissolved Oxygen m /L 0.30 0.34 0.00 0.00 ORP (mv) 10.2 359.8 237.0 366 Iron otal u /L 6,330 387 F 215 449 Sulfate /L 12,200 576,000 F 410,000 527,000 HVOC's (u /L) 1,1,1 Trichloroethane 1,630 <500 <87.5 6,710 1,1 Dichloroethene 1,900 <500 <122 <245 Acetone <5,000 <12,500 <3,080 19,600 Cis-1,2 Dichloroethene 3,530 2,300 1,990 1,400 Tetrachloroethene 15,000 10,800 13,300 1Q 900 Trichloroethene 75,900 1 50,500 r 98,900 r 93,600 The proliferation of sulfate in PMW-5A occurred during the 30-day sampling event and has remained elevated during the 360-day sampling event. ORP values have remained elevated during the 360-day sampling event, sustaining at +366mV. The HVOC concentrations decreased in the 30-day sampling event, but PCE and TCE have since rebounded to at or above they're baseline levels. This is likely a result of desorption of the more hydrophobic compounds having occurred due to the increase in groundwater temperature from 16.02' in February 2019 to 23.11 ° in July 2019, along with downgradient migration of more heavily impacted groundwater. The rate of chemical degradation has slowed in PMW-5A based of concentrations of chloride having remained in the 67,000 mg/L range during the 360-day sampling event. Chloride is the end product of TCE having been completely oxidized by a sulfate free radical. TCE + SO4 - --), CO2 + Cl- Innovative Environmental Technologies, Inc. Sulfate reduction of HVOCs has not been enhanced as of the 360-day sampling event, due to the remaining high ORP and depressed pH at PMW-5A. Wu \L�Q11 This monitoring location is located north of the building and south of Cullman Ave. it is screened at 28-38' bgs. Injection wells 5 and 8 were installed and completed as proposed in this area. PMW-6A was sampled during the 30,120 and 360-day monitoring events and appears to have been impacted by the injection event, increases in sulfate, a drop in pH and increase in ORP confirm that the injected reagent was successfully applied to this area. The geochemical and analytical parameters have been included in the table below along with further discussion on the collected data. PMW-6A (28-38') Geochemical Parameters 11/27/2018 2/19/2019 7/24/2019 1/14/2020 Depth to Water (ft.) 4.87 6.07 4.74 H SU 6.1 3.86 4.56 4.75 Specific Conductance uMhos/cm 255 11,250 4,730 2,020 Temperature C de 18.5 16.23 23.21 20.43 Dissolved Oxygen m /L 0.75 0.24 0.00 0.00 ORP my -21.7 431.3 453.0 491 Iron otal /L 9,940 3,290 7,090 663 Sulfate /L 21,500 817,000 622,000 541,000 Chloride /L 30,400 69,500 r 67,900 58,700 Total Organic Carbon (u /L) 3,600 9,300 r 7,400 8,200 HVOC's ( /L) 1,1,1 Trichloroethane <240 823 <87.5 820 1,1 Dichloroethene 3,330 <500 <122 <122 Cis-1,2 Dichloroethene 5,350 2,330 2,710 2,610 Tetrachloroethene 41,200 26,800 34,000 29,900 Trans-1,2 Dichloroethene <245 349J 1 419 398 Trichloroethene 86,000 48,400 57,400 49,700 Trichloroflouromethane 290J 1 SOJ 197J <156 The proliferation of sulfate in PMW-6A occurred during the 30-day sampling event and has decreased during the 120 and 360-day sampling events. This is likely a result of the formation of iron sulfate minerals. ORP values initially increased to +431.3 in PMW-6A and have remained elevated at +491.0 during the 360-day sampling event. This indicates that the chemical oxidation via production of sulfate free radicals and hydroxyl radicals is continuing to occur. pH remains depressed as a result of generation/exhaustion of the sulfate free radicals causing temporarily acidic conditions. The HVOC concentrations decreased by approximately 39% in the 360-day sampling event, but concentrations of PCE and TCE have remained elevated in the 360-day sampling event. This is likely a result of an initial desorption of the more hydrophobic compounds having occurred due to the increase in groundwater temperature from 16.23 ° in February 2019 to 23.21 ° in July 2019, along with an exhaustion of chemical oxidants. An increase in TOC concentrations indicate that the background SCOD of this area may have been underestimated. PMW- Innovative Emironmenral la&n&Oes, In. 6A should continue to be monitored as the oxidation event expires ORP values are expected to decrease and biological attenuation via sulfate reduction expected to occur in the next 6 to 8 months, however pH in this area may need to be adjusted manually if the aquifer's buffering capacity isn't able to neutralize the pH naturally. PMW-10A This monitoring location is located at the northern end of the plume and is screened at 53- 63' bgs. Injection well 19 was installed and completed as proposed in this area, however IW-16 was proposed immediately upgradient and was unable to be installed. PMW-10A was sampled during the 30, 120 and 360-day monitoring events and appears to have been impacted by the injection event, increases in sulfate, a drop in pH and increase in ORP confirm that the injected reagent was successfully applied to this area. The geochemical and analytical parameters have been included in the table below along with further discussion on the collected data. PMW-10A (53-63') Geochemical Parameters 11/27/2018 2/19/2019 7/23/2019 1/15/2020 Depth to Water (ft.) 6.97 7.92 H SU 6.6 5.4 6.19 .2 61 Specific Conductance uMhos/cm 261 6,733 1,300 753 Temperature C de 17.1 15.53 21.50 17.78 Dissolved Oxygen m /L 1.00 0.018 0.00 0.00 ORP my 9.8 359.2 289.0 323 Iron (To /L) <25 7,710 66.3 45 Sulfate /L 15,500 344,000 120,000 99,200 Chloride ( /L) 19,800 1 55,700 r 32,000 r 25,200 Total Organic Carbon ( /L) 1 1,500 1 5,600 r 3,200 r 2,100 HVOC's u /L 1,1,1 Trichloroethane 653 499 <43.8 <43.8 1,1 DicMoroethene 2,110 <200 <61.2 454 Cis-1,2 Dichloroethene 3,260 879 1,400 1,690 TetracHoroethene 11,400 4,060 6,870 6,880 Trans-1,2 DicHoroethene <245 143J 187J <63.5 Trichloroethene 66,100 1 23,600 r 38,100 r 37,900 The proliferation of sulfate in PMW-l0A occurred during the 30-day sampling event and has decreased during the 120 and 360-day sampling events. This is likely a result of the formation of iron sulfate minerals. ORP values initially increased to +359.2 in PMW-l0A and have since remained elevated at +323 during the 360-day sampling event. The HVOC concentrations decreased by approximately 44% in the 360-day sampling event, but PCE and WE have have remained elevated in the 360-day sampling event. This is likely a result untreated groundwater from upgradient migrating into PMW-l0A's well screen. Sulfate concentrations have depleted to below 100 ppm and iron concentrations have depleted to 45 ppb. The pH has started to rebound in this monitoring well location, however it is unlikely that the remaining HVOC concentration will be attenuated via Innovative Emimmental Tkhnolo es, Ina biological processes due to the lowered concentrations of electron donor present in the form of sulfate and ferrous iron. PMW-1OB This monitoring location is located at the northern end of the plume and is screened at 68- 73' bgs. Injection well 19 was installed and completed as proposed in this area, however IW-16 was proposed immediately upgradient and was unable to be installed. PMW-IOB was sampled during the 30, 120 and 360-day monitoring events and appears to have been impacted by the injection event, increases in sulfate, a drop in pH and increase in ORP confirm that the injected reagent was successfully applied to this area. The geochemical and analytical parameters have been included in the table below along with further discussion on the collected data. PMW-1OB (68-73') Geochemical Parameters 11/27/2018 2/19/2019 7/23/2019 1/15/2020 Depth to Water (ft.) 6.58 7.92 7.93 H (SU) 6.7 5.72 6.13 6.15 Specific Conductance uMhos/cm) 244 901 112 724 Temperature C de 15.5 15.2 1 20.77 17.91 Dissolved Oxygen m /L 0.75 2.68 0.70 0.00 ORP (mv) -24 243.5 280.0 224 Iron otal u /L 154 62 176 128 Sulfate /L 15,800 84,700 91,700 88,600 Chloride /L 17,800 48'800 26,000 23,000 Total Organic Carbon /L 1,200 4,400 2,500 1,700 HVOC's (u /L) 1,1,1 Trichloroefl=e <192 211 <43.8 <43.8 1,1 Dichloroethane <128 40.9j <67 <67 1,1 Dichloroethene 1,380 <50.1 <61.2 209 Cis-1,2 Dichloroethene 2,300 222 1,140 1,330 Tetrachloroethene 6,370 1,150 5,720 5,030 Trans-1,2 Dichloroethene <196 32.6 <63.5 <63.5 Trichloroethene 48,900 7,110 27,300 r 26,800 A slight proliferation of sulfate in PMW-IOB occurred during the 30-day sampling event and has remained slightly elevated during the 360-day sampling event at 88,600 ug/L. ORP values initially increased to +243.5 in PMW-lOB and have remained elevated at +224.0 during the 360-day sampling event. The HVOC concentrations decreased by approximately 43% in the 360-day sampling event, but PCE and TCE have remained elevated. This is likely a result of the migration of untreated groundwater from upgradient having impacted PMW-lOB as the depth to water has decreased, noting that IW-16 was not installed. It is expected that the deeper groundwater at the site will equilibriate and further reductions of PCE and TCE are expected to occur as the site transitions to a reducing environment, however complete biological degradation of these compounds is unlikely due to the lower concentrations of bio-available sulfate and iron in PMW-1 OB. Innovative Emironmental T6bnoWk s, Inc. PMW-11A This monitoring location is located at the northeastern end of the plume and is screened at 53-63' bgs. Injection wells 14 and 18 were installed and completed as proposed in this area. PMW-11A was sampled during the 30, 120 and 360-day monitoring events and appears to have been slightly impacted by the injection event, increases in sulfate, a drop in pH and increase in ORP confirm that the injected reagent was successfully applied within or immediately upgradient of this area. The geochemical and analytical parameters have been included in the table below along with further discussion on the collected data. PMW-11A (53-63') Geochemical Parameters 11/27/2018 2/20/2019 7/23/2019 1/14/2020 Depth to Water ft. 6.69 8.00 8.01 H SU 6.7 6.93 6.20 6.06 Specific Conductance uMhos/cm) 194 80 r 841 r 939 Temperature C de 15.0 15.69 19.17 17.80 Dissolved Oxygen m /L 1.62 2.89 1.35 0.97 ORP my 29.3 136.4 230.0 447 Iron (Total)(u /L) 481 10,200 227 309 Sulfate ( /L) 15,800 3,300 57,700 85,900 Chloride (u /L) 4,800 1,600 7,700 6,300 Total Or ark Carbon ( /L) 1,200 1 9,200 820J r 2,400 HVOC's (u /L) 1,1,1 Trichloroethane <9.6 3.8 <0.7 15.9 1,1 Dichloroethane <6.4 <5.0 7.1 3.9 1,1 Dichloroethene 39 7.3 <0.98 <0.24 Cis-1,2 Dichloroethene 168 76 36 4.4 Methylene Chloride 30.8 <25 <14.8 <3.7 Tetrachloroediene 346 1 91.3 r 200 r 31 Trichloroethene 2,060 1 494 r 660 r 68 A slight proliferation of sulfate in PMW-IOB continues to occur during the 360-day sampling event. ORP values initially increased to +136mV, and have continued to increase, having been measured at +447mV during the 360-day sampling event. This indicates that the injections that occurred upgradient are beginning to impact this area. The HVOC concentrations decreased by approximately 95% in the 360-day sampling event. The water entering this location seems to be indicative of the fringe area of injection, likely from IW-14, and it's possible that injection into IW-18 migrated west rather than towards this monitoring location. As reducing conditions are enhanced further degradation of the HVOCs in the area around this monitoring location are expected in the next few sampling events. Innovative Environmental TbchnoMor, Inc. Other On -site monitoring locations Several other wells have been sampled, but fall either outside of the treatment area or are screened outside of the injection interval, these include (PMW-4A, PMW-lB, PMW-2A, PMW-213, PMW-8A, PMW-813, PMW-I IB, PMW-13B, PMW-9A, PMW-913, and PMW- 9C). Generally, these wells were unimpacted by the injection event. Sight increases in sulfate were noted in PMW-IB, PMW-4A and PMW-9C, and hits of persulfate at PMW- 1113 and PMW-13B. Substantial increases in HVOC concentrations were observed in PMW-13B and PMW-9C. In the case of 9C, this well is installed within the treatment zone and downgradient of the treatment area so migration of PCE and TCE maybe occurring from the IW-13, IW-9 area. PMW-13B is screened from 98-103' bgs, approximately 25' deeper than the deepest injection well, although within the treatment area. PCE and TCE could be migrating down a compromised grout seal at PMW-13B, but more likely the groundwater from the highly impacted area around PMW-5A has migrated down vertical fractures into this deeper well screen. Geochemical parameters of the groundwater don't match that of the PMW-5A area but HVOC concentration and chloride/sulfate/iron concentrations are similar and appear to correlate with the groundwater collected in that area. Conclusion and Recommendations Chemical oxidation via production of sulfate free radicals appears to have run it's course across the treatment area, overall degradation of total HVOCs has been observed, however elevated concentrations of HVOCs remain in most wells. Site wide sulfate concentrations remain elevated and pH levels remain slightly acidic, in order to gain degradation of HVOC via sulfate reduction a pH buffer is recommended to be applied in these areas, specifically the PMW-5a and PMW-6a area. In addition, the installation of more injection wells should be considered, specifically between IW-15 and IW-17, where IW-16 was originally proposed, another injection well should be considered between IW-13 and IW-17 to catch some of the migrating HVOC impacted grounwater in that area. Monitoring wells are recommended to be installed both inside the building and west of PMW-5a to further delineate the plume both vertically and horizontally, based on this data additional injection wells may be recommended to be both installed and injected. Deeper injection wells are likely necessary to address the HVOC concentrations in PMW-13B. If a follow up injection event is designed an additional oxidation event would also be recommended while the work within the new injection wells and the pH buffer is being applied. Please let me know if you have any questions or comments. Sincerely, Ian H. Connor, Vice President of Operations ianconnor@iet-inc.net Innovative Environmental lbdmoWk s, Inc. Innovative Environmental Technologies, Inc. 6071 Easton Rd. Pipersville, PA 18947 www.iet-inc.net (888) 721-8283 EnviroAnafytics Group APPENDIX F SVE SYSTEM GRAPHS 18 I6 I4 12 10 8 fi 9 2 0 APPENDIX F SVE SYSTEM GRAPHS TREX PROPERTIES, LLC CHARLOTTE, NC PID Readings in ppm for SVE Wells in 3124 Cullman Avenue PID Readings in ppm for SVE Wells in 3114 Cullman Avenue