WI0300160_Monitoring (Report)_20110809

License No. C-0281
CIVIL/SANITARY/ENVIRONMENTAL ENGINEERS
Municipal
Services
SITE PLANNING/SUBDIVISIONS
Mr. Thomas Slusser, P.G.
Aquifer Protection Section — UIC Staff
DENR — Division of Water Quality
1636 Mail Service Center
Raleigh, NC 27699-1636
Re: Monitoring Event Report
Alexander County Landfill
SWS Permit #02-01
UIC Permit No. WI0300160
SOLID WASTE MANAGEMENT
Engineering
Company, P.A.
OF -
SUBSURFACE UTILITY ENGINEERING (SUE)
August 8, 2011
RECEIVED / DENR / DWQ
Aquifer Protection Section
AUG 0 9 2011
Dear Mr. Slusser:
�e9
U
,C unicipal Engineering Services Company, PA (MESCO) instituted quarterly monitoring for the MW-26 area of concern.
Sampling was conducted in conjunction with the semi-annual and MNA monitoring procedures from June 28 to July 1,
2011. The scope -of -work for this sampling event was outlined in the Injection Well Permit Application and Well Permit
o. �141 ,�9�). Monitoring wells MW-3, MW-11, MW-26, MW-27 and MW-3Iwere sampled for Appendix I
metals by EPA Test Method 6010, Appendix I VOCs by EPA Test Method 8260, Sulfate by EPA Test Method 300.0,
Chloride by Test Method SM 4500-C1-E, Alkalinity by Test Method SM232013, Total Organic Carbon (TOC) by Test
Method SM 5310B and BOD by Test Method SM 5210B. Field parameters are reported on Table 1.
The laboratory analysis was provided by Pace Analytical, report copies are included. Due to this quarterly event occurring
in conjunction with the semi-annual and MNA sampling additional parameters not specified in the permit are included.
MW-3 was not analyzed for alkalinity due to a sampling oversight; it will be included in the next event, scheduled for
September 2011. Future quarterly sampling results and additional injection reports will be submitted to both the Raleigh
and Mooresville offices in accordance with the permit requirements.
The injection of Bac-9 was performed on February 17, 2011. The bacteria should have had ample time to migrate through
the bedrock fractures to avoid being accidentally removed in the sampling process by the collection date. The flow rate in
the vicinity of MW-26 is approximately 55 feet per year. Considering the injection well is roughly 50 feet up -gradient of
MW-26 we should begin to see evidence of the injection around the March 2012 quarterly sampling event.
Please contact us at [phone] or m erman ,mesco.com with questions or comments.
Respectfully submitted,
MUNICIPAL ENGINEERING SERVICES COMPANY, P.A.
i+ �jfUJ' I
Madeline German, PG
Geologist
Enclosure
CC: Josh Mitchell, Alexander County
Jaclynne Drummond, SWS-Compliance Branch
DENR-DWQ Mooresville Regional Office
PO Box 97, Garner, North Carolina 27529 [phone]
PO Box 349, Boone, NC 28607 [phone]

Table 1
Field Parameter Data Summary
June 28-July 1, 2011
j
WLR
Water
TOC
Specific
Parameter
i
(BTOC)*
Elevation
Elevation
Temp.
ORP
DO
pH
Conductance
TDS
Turbidity
Units
ft
ft (amsl)
ft (amsl)
C
mV
mg/L
SU
umhos/cm
mg/L
Visual or NTU
MW-3
25.78
998.95
1024.73
16.4
-32
0.1
5.81
301
150
Clear
MW-11
41.58
970.38
1011.96
17.0
14
1.2
6.02
396
198
Clear
MW-26
27.05
963.64
990.69
16.3
37
1.8
5.84
323
162
Clear
-, MW-27
20.92
971.27
992.19
15.9
-7
3.7
6.68
468
234
Clear
MW-31
22.86
962.56
985.42
15.4
527
1.1
5.36
110
55
16.3
Minimum
20.92
962.56
985.42
15.4
-32
0.1
5.36
110
55
16.3
Maximum
41.58
998.95
1024.73
17
527
3.7
6.68
468
234
16
Average
27.64
973.36
1001
16.2
108
1.6
5.94
320
160
16
WLR recorded 6/28/11
Alexander County Quarterly Injection Monitoring Report

�;a'ceAnalyfical'
% www.pacelabs.com
July 20, 2011
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
RE: Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on July 01, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
cam— '�J",� -
:t371MI • enk i1
[e-mail]
Project Manager
Enclosures
cc: Ms. Maggie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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/�aceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
CERTIFICATIONS
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Connecticut Certification #: PH-0104
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DHH Drinking Water # LA 100031
South Carolina Certification #: 99006001
West Virginia Certification #: 357
South Carolina Drinking Water Cert. #: 99006003
Virginia/VELAP Certification #: 460144
Virginia Drinking Water Certification #: 00213
m
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
Virgina/VELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 18

1�5WAMIXical"
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�I
l�
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project:
ALEXANDER MSWLF-MW-3
Pace Project No.:
9297450
Lab ID
Sample ID
9297450001
MW-3
9297450002
MW-3
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Water
06/30/1109:00
07/01/1114:10
Water
07/01/1111:20
07/01/1114:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 18

aWnaljdkal
f www.pacetabs.corti.
t
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
Project:
ALEXANDER MSWLF-MW-3
Pace Project No.:
9297450
Lab ID
Sample ID
9297450001
MW-3
9297450002 MW-3
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Method
Analysts
Analytes
Reported
Laboratory
EPA6010
JMW, SHB
16
PASI-A
EPA 8270
PPM
4
PASI-C
EPA 8260
MCK
54
PASI-C
EPA 300.0
EWS
1
PASI-A
SM 4500-CI-E
JDA
1
PASI-A
SM 5310B
EWS
1
PASI-A
SM 5210B
SAJ
1
PASI-A
REPORT OF LABORATORY ANALYSIS Page 4 of 18
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® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
1�5a'xAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr.
wmpacelabs.wm Eden, NC 27288 Asheville, NC 28804
j [phone] [phone]
ANALYTICAL RESULTS
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-3 Lab ID: 9297450001 Collected: 06/30/11 09:00 Received: 07/01/11 14:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 ICP Groundwater
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Thallium
Tin
Vanadium
Zinc
8270 MSSV Semivolatile Organic
2,4-Dimethylphenol
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans- l,4-Di chloro-2-butene
1,1-Dichloroethane
Analytical Method: EPA 6010 Preparation Method: EPA 3010
ND ug/L
6.0
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-36-0
ND ug/L
10.0
5.0
1
07/09/11 14:30
07/14/11 15:42
7440-38-2
47.5J ug/L
100
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-39-3
ND ug/L
1.0
1.0
1
07/09/11 14:30
07/13/11 21:51
7440-41-7
ND ug/L
1.0
1.0
1
07/09/11 14:30
07/13/11 21:51
7440-43-9
SAJ ug/L
10.0
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-47-3
13.1 ug/L
10.0
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-48-4
ND ug/L
10.0
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-50-8
ND ug/L
10.0
5.0
1
07/09/11 14:30
07/13/11 21:51
7439-92-1
29.5J ug/L
50.0
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-02-0
ND ug/L
10.0
10.0
1
07/09/11 14:30
07/13/11 21:51
7782-49-2
ND ug/L
10.0
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-22-4
ND ug/L
5.5
5.4
1
07/09/11 14:30
07/13/11 21:51
7440-28-0
ND ug/L
100
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-31-5
ND ug/L
25.0
5.0
1
07/09/11 14:30
07/13/11 21:51
7440-62-2
12.1 ug/L
10.0
10.0
1
07/06/11 14:30
07/13/11 21:51
7440-66-6
Analytical Method: EPA
8270 Preparation Method: EPA 3510
ND ug/L
10.0
1.2
1
07/08/11 15:00
07/11/11 18:38
105-67-9
24 %
10-110
1
07/08/11 15:00
07/11/11 18:38
13127-88-3
41 %
12-110
1
07/08/11 15:00
07/11/11 18:38
367-12-4
87 %
27-110
1
07/08/11 15:00
07/11/11 18:38
118-79-6
Analytical Method: EPA 8260
5.3J ug/L
100
2.2
1
07/07/11 19:58
67-64-1
ND ug/L
200
1.9
1
07/07/11 19:58
107-13-1
6.1 ug/L
1.0
0.25
1
07/07/11 19:58
71-43-2
ND ug/L
3.0
0.17
1
07/07/11 19:58
74-97-5
ND ug/L
1.0
0.18
1
07/07/11 19:58
75-27-4
ND ug/L
3.0
0.26
1
07/07/11 19:58
75-25-2
ND ug/L
10.0
0.29
1
07/07/11 19:58
74-83-9
ND ug/L
100
0.96
1
07/07/11 19:58
78-93-3
6.8J ug/L
100
1.2
1
07/07/11 19:58
75-15-0
ND ug/L
1.0
0.25
1
07/07/11 19:58
56-23-5
0.93J ug/L
3.0
0.23
1
07/07/11 19:58
108-90-7
1.3J ug/L
10.0
0.54
1
07/07/11 19:58
75-00-3
ND ug/L
5.0
0.14
1
07/07/11 19:58
67-66-3
ND ug/L
1.0
0.11
1
07/07/11 19:58
74-87-3
ND ug/L
13.0
2.5
1
07/07/11 19:58
96-12-8
ND ug/L
3.0
0.21
1
07/07/11 19:58
124-48-1
ND ug/L
1.0
0.27
1
07/07/11 19:58
106-93-4
ND ug/L
10.0
0.21
1 _
07/07/11 19:58
74-95-3
0.47J ug/L
5.0
0.30
1
07/07/11 19:58
95-50-1
5.5 ug/L
1.0
0.33
1
07/07/11 19:58
106-46-7
ND ug/L
100
1.0
1
07/07/11 19:58
110-57-6
2.OJ ug/L
5.0
0.32
1
07/07/11 19:58
75-34-3
1g
Date: 07/20/2011 04:36 PM REPORT OF LABORATORY ANALYSIS Page 5 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

1�5a'xAnalytical
www.pacelabsxom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-3
Parameters
Lab ID: 9297450001
Results Units
Collected:
Report
Limit
06/30/11 09:00
MDL DF
Received: 07/01/11 14:10 Matrix: Water
Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
1,2-Dichloroethane
0.31J ug/L
1.0
0.12
1
07/07/11 19:58
107-06-2
1,1-Dichloroethene
ND ug/L
5.0
0.56
1
07/07/11 19:58
75-35-4
cis-1,2-Dichloroethene
9.8 ug/L
5.0
0.19
1
07/07/11 19:58
156-59-2
trans- l,2-Dichloroethene
ND ug/L
5.0
0.49
1
07/07/11 19:58
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
0.27
1
07/07/11 19:58
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
0.28
1
07/07/11 19:58
142-28-9
cis- 1,3-Dichloropropene
ND ug/L
1.0
0.13
1
07/07/11 19:58
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
1.0
0.26
1
07/07/11 19:58
10061-02-6
Ethylbenzene
1.7 ug/L
1.0
0.30
1
07/07/11 19:58
100-41-4
2-Hexanone
ND ug/L
50.0
0.46
1
07/07/11 19:58
591-78-6
lodomethane
ND ug/L
10.0
0.32
1
07/07/11 19:58
74-88-4
Methylene Chloride
ND ug/L
1.0
0.97
1
07/07/11 19:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
100
0.33
1
07/07/11 19:58
108-10-1
Naphthalene
4.8J ug/L
10.0
0.24
1
07/07/11 19:58
91-20-3
Styrene
ND ug/L
1.0
0.26
1
07/07/11 19:58
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
5.0
0.33
1
07/07/11 19:58
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
3.0
0.40
1
07/07/11 19:58
79-34-5
Tetrachloroethene
ND ug/L
1.0
0.46
1
07/07/11 19:58
127-18-4
Toluene
0.86J ug/L
1.0
0.26
1
07/07/11 19:58
108-88-3
1,2,4-Trichlorobenzene
ND ug/L
10.0
0.35
1
07/07/11 19:58
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
0.48
1
07/07/11 19:58
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
0.29
1
07/07/11 19:58
79-00-5
Trichloroethene
1.2 ug/L
1.0
0.47
1
07/07/11 19:58
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
0.20
1
07/07/11 19:58
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
0.41
1
07/07/11 19:58
96-18-4
Vinyl acetate
ND ug/L
50.0
0.35
1
07/07/11 19:58
108-05-4
Vinyl chloride
0.87J ug/L
1.0
0.62
1
07/07/11 19:58
75-01-4
Xylene (Total)
7.6 ug/L
5.0
0.66
1
07/07/11 19:58
1330-20-7
4-13romofluorobenzene _(S)
95 %
70-130
1
07/07/11 19:58
460-00-4
Dibromofluoromethane (S)
118 %
70-130
1
07/07/11 19:58
1868-53-7
1,2-Dichloroethane-d4 (S)
116 %
70-130
1
07/07/11 19:58
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
07/07/11 19:58
2037-26-5
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate 1960J ug/L 250000 1 07/14/11 04:57 14808-79-8
4500 Chloride Analytical Method: SM 4500-CI-E
Chloride 18800 ug/L 5000 5000 1 07/15/11 14:14 16887-00-6
5310E TOC Analytical Method: SM 531013
Total Organic Carbon 13400 ug/L 1000 1000 1 07/19/11 22:17 7440-44-0
Date: 07/20/2011 04:36 PM REPORT OF LABORATORY ANALYSIS Page 6 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aoAnalylical
— www.pacdabs.com
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
Sample: MW-3
Parameters
5210B BOD, 5 day
BOD, 5 day
I
Date: 07/20/2011 04:36 PM
1
i
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 9297450002 Collected: 07/01/11 11:20 Received: 07/01/11 14:10 Matrix: Water
Report
Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Analytical Method: SM 521013
ND ug/L 2000 2000 1 07/02/11 11:30 07/07/11 11:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 18

/5a'ceAnalXical'
www.pacelabs.com
r
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/8694 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET NC Groundwater
Associated Lab Samples: 9297450001
METHOD BLANK: 631117
Associated Lab Samples:
9297450001
Parameter
Units
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Lead
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Thallium
ug/L
Tin
ug/L
Vanadium
ug/L
Zinc
ug/L
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed
ND
6.0
07/13/1120:19
ND
10.0
07/13/1120:19
ND
100
07/13/1120:19
NO
1.0
07/13/1120:19
NO
1.0
07/13/1120:19
ND
10.0
07/13/1120:19
ND
10.0
07/13/1120:19
ND
10.0
07/13/1120:19
ND
10.0
07/13/1120:19
ND
50.0
07/13/1120:19
ND
10.0
07/13/1120:19
ND
10.0
07/13/1120:19
ND
5.5
07/13/1120:19
ND
100
07/13/1120:19
ND
25.0
07/13/1120:19
ND
10.0
07/13/1120:19
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
631118
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
499
100
80-120
Arsenic
ug/L
500
501
100
80-120
Barium
ug/L
500
508
102
80-120
Beryllium
ug/L
500
504
101
80-120
Cadmium
ug/L
500
498
100
80-120
Chromium
ug/L
500
498
100
80-120
Cobalt
ug/L
500
504
101
80-120
Copper
ug/L
500
504
101
80-120
Lead
ug/L
500
504
101
80-120
Nickel
ug/L
500
502
100
80-120
Selenium
ug/L
500
503
101
80-120
Silver
ug/L
250
248
99
80-120
Thallium
ug/L
500
496
99
80-120
Tin
ug/L
500
510
102
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
519
104
80-120
Date: 07/20/2011 04:36 PM REPORT OF LABORATORY ANALYSIS Page 8 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

I
aceAnalytical
www.pacelabs.com
1
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 631119
9297382003
Parameter Units Result
MS
Spike
Conc.
Antimony
ug/L
ND
500
Arsenic
ug/L
ND
500
Barium
ug/L
41.2J
500
Beryllium
ug/L
ND
500
Cadmium
ug/L
ND
500
Chromium
ug/L
ND
500
Cobalt
ug/L
ND
500
Copper
ug/L
ND
500
Lead
ug/L
ND
500
Nickel
ug/L
ND
500
Selenium
ug/L
ND
500
Silver
ug/L
ND
250
Thallium
ug/L
ND
500
Tin
ug/L
ND
500
Vanadium
ug/L
ND
500
Zinc
ug/L
ND
500
Date: 07/20/2011 04:36 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
631120
MSD
Spike
MS
MSD
MS
MSD
% Rec
Max
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
500
506
494
101
99
75-125
2
25
500
516
502
103
100
75-125
3
25
500
555
541
103
100
75-125
3
25
500
514
501
103
100
75-125
3
25
500
506
493
101
99
75-125
3
25
500
502
492
100
98
75-125
2
25
500
500
487
100
97
75-125
3
25
500
506
494
101
99
75-125
2
25
500
497
487
99
97
75-125
2
25
500
497
485
99
97
75-125
2
25
500
513
499
103
100
75-125
3
25
250
253
246
101
98
75-125
3
25
500
486
474
97
95
75-125
2
25
500
513
501
103
100
75-125
2
25
500
508
496
101
99
75-125
2
25
500
520
512
103
101
75-125
2
25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 18

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aXAnalylical 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.pacelabs.com. Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
QC Batch: OEXT/14166 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: 82.70 Water MSSV
Associated Lab Samples: 9297450001
METHOD BLANK: 631462
Associated Lab Samples: 9297450001
Parameter Units
2,4-Dimethylphenol ug/L
2,4,6-Tribromophenol (S) %
2-Fluorophenol (S) %
Phenol-d6 (S) %
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
10.0
07111/1118:10
67
27-110
07/11/1118:10
43
12-110
07/11/1118:10
27
10-110
07/11/1118:10
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 631463
631464
Spike LCS LCSD LCS
LCSD
% Rec Max
Parameter
Units
Conc. Result Result % Rec
% Rec
Limits RPD RPD Qualifiers
2,4-Dimethylphenol
ug/L
50 30.9 17.1 62
34
15-109 57 30
2,4,6-Tribromophenol (S)
%
84
53
27-110
2-Fluorophenol (S)
%
49
23
12-110
Phenol-d6 (S)
%
31
16
10-110
Date: 07/20/2011 04:36 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 18

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acoAnaljltical 205 East Meadow Road - Suite A 2225 Riverside Dr.
wwrw.pacelabs.com Eden, NC 27288 Asheville, NC 28804
( [phone] [phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
QC Batch: MSV/15933 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 9297450001
METHOD BLANK: 630602
Associated Lab Samples: 9297450001
Parameter
Matrix: Water
Blank Reporting
Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
5.0
07/07/11 11:02
1,1,1-Trichloroethane
ug/L
ND
1.0
07/07/11 11:02
1,1,2,2-Tetrachloroethane
ug/L
ND
3.0
07/07/11 11:02
1,1,2-Trichloroethane
ug/L
ND
1.0
07/07/11 11:02
1,1-Dichloroethane
ug/L
ND
5.0
07/07/11 11:02
1,1-Dichloroethene
ug/L
ND
5.0
07/07/11 11:02
1,2,3-Trichloropropane
ug/L
ND
1.0
07107/1111:02
1,2,4-Trichlorobenzene
ug/L
ND
10.0
07/07/11 11:02
1,2-Dibromo-3-chloropropane
ug/L
ND
13.0
07/07/11 11:02
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
07/07/11 11:02
1,2-Dichlorobenzene
ug/L
ND
5.0
07/07/11 11:02
1,2-Dichloroethane
ug/L
ND
1.0
07/07/11 11:02
1,2-Dichloropropane
ug/L
ND
1.0
07/07/11 11:02
1,3-Dichloropropane
ug/L
ND
1.0
07/07/11 11:02
1,4-Dichlorobenzene
ug/L
ND
1.0
07/07/11 11:02
2-Butanone (MEK)
ug/L
ND
100
07/07/11 11:02
2-Hexanone
ug/L
ND
50.0
07/07/11 11:02
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
07/07/11 11:02
Acetone
ug/L
2.9J
100
07/07/11 11:02
Acrylonitrile
ug/L
ND
200
07/07/11 11:02
Benzene
ug/L
ND
1.0
07/07/11 11:02
Bromochloromethane
ug/L
ND
3.0
07/07/11 11:02
Bromodichloromethane
ug/L
ND
1.0
07/07/11 11:02
Bromoform
ug/L
ND
3.0
07/07/11 11:02
Bromomethane
ug/L
ND
10.0
07/07/11 11:02
Carbon disulfide
ug/L
ND
100
07/07/11 11:02
Carbon tetrachloride
ug/L
ND
1.0
07/07/11 11:02
Chlorobenzene
ug/L
ND
3.0
07/07/11 11:02
Chloroethane
ug/L
ND
10.0
07/07/11 11:02
Chloroform
ug/L
0.14J
5.0
07/0711111:02
Chloromethane
ug/L
ND
1.0
07/07/11 11:02
cis- 1,2-Dichloroethene
ug/L
ND
5.0
07/07/11 11:02
cis- 1,3-Dichloropropene
ug/L
ND
1.0
07107/1111:02
Dibromochloromethane
ug/L
ND
3.0
07/07/11 11:02
Dibromomethane
ug/L
ND
10.0
07/07/11 11:02
Ethylbenzene
ug/L
ND
1.0
07107/1111:02
lodomethane
ug/L
ND
10.0
07/07/11 11:02
Methylene Chloride
ug/L
ND
1.0
07/07/11 11:02
Naphthalene
ug/L
ND
10.0
07/07/11 11:02
Styrene
ug/L
ND
1.0
07/07/11 11:02
Tetrachloroethene
ug/L
ND
1.0
07/07/11 11:02
Toluene
ug/L
ND
1.0
07/07/11 11:02
trans-1,2-Dichloroethene
ug/L
ND
5.0
07/07/11 11:02
Date: 07/20/2011 04:36 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be
reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 18

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Analytical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
wmpacetab&com
Eden, NC 27288
Asheville, NC
28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
METHOD BLANK: 630602
Matrix:
Water
Associated Lab Samples: 9297450001
Blank
Reporting
Parameter
Units Result
Limit
Analyzed
Qualifiers
trans-1,3-Dichloropropene
ug/L
ND
1.0
07/07/11 11:02
trans-1,4-Dichloro-2-butene
ug/L
ND
100
07/07/11 11:02
Trchloroethene
ug/L
ND
1.0
07/07/11 11:02
Trichlorofluoromethane
ug/L
ND
1.0
07/07/11 11:02
Vinyl acetate
ug/L
ND
50.0
07/07/11 11:02
Vinyl chloride
ug/L
ND
1.0
07/07/11 11:02
Xylene (Total)
ug/L
ND
5.0
07/07/11 11:02
1,2-Dichloroethane-d4 (S)
%
113
70-130
07/07/11 11:02
4-Bromofluorobenzene IS)
%
94
70-130
07/07/11 11:02
Dibromofluoromethane (S)
%
118
70-130
07/07/11 11:02
Toluene-d8IS)
%
97
70-130
07/07/11 11:02
LABORATORY CONTROL SAMPLE:
630603
Spike
LCS
LCS %
Rec
Parameter
Units Conc. Result
% Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.9
102
70-130
1,1,1-Trichloroethane
ug/L
50
51.0
102
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
32.1
64
70-130 LO
1,1,2-Trichloroethane
ug/L
50
50.8
102
70-130
1,1-Dichloroethane
ug/L
50
51.4
103
70-130
1,1-Dichloroethene
ug/L
50
49.5
99
70-132
1,2,3-Tdchloropropane
ug/L
50
48.0
96
70-130
1,2,4-Trichlorobenzene
ug/L
50
51.6
103
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
46.6
93
70-130
1,2-Dibromoethane (EDB)
ug/L
50
48.9
98
70-130
1,2-Dichlorobenzene
ug/L
50
50.8
102
70-130
1,2-Dichloroethane
ug/L
50
51.2
102
70-130
1,2-Dichloropropane
ug/L
50
48.9
98
70-130
1,3-Dichloropropane
ug/L
50
50.2
100
70-130
1,4-Dichlorobenzene
ug/L
50
48.5
97
70-130
2-Butanone (MEK)
ug/L
100
94.8J
95
70-145
2-Hexanone
ug/L
100
92.2
92
70-144
4-Methyl-2-pentanone (MIBK)
ug/L
100
90.91
91
70-140
Acetone
ug/L
100
99.2J
99
50-175
Acrylonitrile
ug/L
250
268
107
70-143
Benzene
ug/L
50
46.5
93
70-130
Bromochloromethane
ug/L
50
50.3
101
70-130
Bromodichloromethane
ug/L
50
49.8
100
70-130
Bromoform
ug/L
50
49.5
99
70-130
Bromomethane
ug/L
50
63.5
127
54-130
Carbon disulfide
ug/L
50
53.7J
107
70-131
Carbon tetrachloride
ug/L
50
49.5
99
70-132
Chlorobenzene
ug/L
50
49.6
99
70-130
Chloroethane
ug/L
50
53.9
108
64-134
Chloroform
ug/L
50
52.2
104
70-130
Date: 07/20/2011 04:36 PM
REPORT OF LABORATORY ANALYSIS
Page 12 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
5aceAnaljftal 205 East Meadow Road - Suite A 2225 Riverside Dr.
lwwwpacelabs.com. Eden, NC 27288 Asheville, NC 28804
!r [phone] [phone]
f
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 630603
Spike
LCS
LCS
% Rec
Parameter
Units Cone.
Result
% Rec
Limits
Qualifiers
Chloromethane
ug/L
50
43.3
87
64-130
cis-1,2-Dichloroethene
ug/L
50
50.2
100
70-131
cis- 1,3-Dichloropropene
ug/L
50
56.5
113
70-130
Dibromochloromethane
ug/L
50
47.5
95
70-130
Dibromomethane
ug/L
50
49.0
98
70-131
Ethylbenzene
ug/L
50
50.1
100
70-130
lodomethane
ug/L
100
121
121
49-180
Methylene Chloride
ug/L
50
50.6
101
63-130
Naphthalene
ug/L
50
48.0
96
70-138
Styrene
ug/L
50
55.1
110
70-130
Tetrachloroethene
ug/L
50
47.7
95
70-130
Toluene
ug/L
50
48.3
97
70-130
trans-1,2-Dichloroethene
ug/L
50
49.5
99
70-130
trans-1,3-Dichloropropene
ug/L
50
54.2
108
70-132
trans-1,4-Dichloro-2-butene
ug/L
50
50.8J
102
70-141
Trichloroethene
ug/L
50
59.0
118
70-130
Trichlorofluoromethane
ug/L
50
50.6
101
62-133
Vinyl acetate
ug/L
100
105
105
66-157
Vinyl chloride
ug/L
50
48.8
98
69-130
Xylene (Total)
ug/L
150
161
107
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Dibromofluoromethane (S)
%
104
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
I
630604
630605
,
MS
MSD
9297234026 Spike
Spike MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result Cone.
Cone. Result
Result
% Rec % Rec
Limits
RPD RPD Qual
1,1-Dichloroethene .
ug/L
ND 50
50 48.3
53.1
97
106
70-166
9 30
Benzene
ug/L
ND 50
50 43.6
48.8
87
98
70-148
11 30
Chlorobenzene
ug/L
ND 50
50 44.1
49.4
88
99
70-146
11 30
Toluene
ug/L
ND 50
50 44.5
49.3
89
99
70-155
10 30
Trichloroethene
ug/L
ND 50
50 42.2
46.8
84
93
69-151
10 30
1,2-Dichloroethane-d4 (S)
%
116
113
70-130
4-Bromofluorobenzene (S)
%
93
94
70-130
Dibromofluoromethane (S)
%
118
115
70-130
Toluene-d8 (S)
I I
%
94
95
70-130
Date: 07/20/2011 04:36 PM
REPORT OF LABORATORY ANALYSIS
Page 13 of 18
This report shall
not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr.
wmpacelabs.com Eden, NC 27288 Asheville, NC 28804
f
j [phone] [phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
QC Batch: WET/17021 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 9297450002
METHOD BLANK: 629470
Associated Lab Samples: 9297450002
Parameter
Units
BOD, 5 day
ug/L
LABORATORY CONTROL SAMPLE:
629471
Parameter
Units
BOD, 5 day
ug/L
SAMPLE DUPLICATE: 629472
Parameter
Units
BOD, 5 day
ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2000 07/07/1111:36
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198000 200000 101 84-115
9297153005 Dup Max
Result Result RPD RPD Qualifiers
13.7 mg/L 12200 12 20
Date: 07/20/2011 04:36 PM REPORT OF LABORATORY ANALYSIS Page 14 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnaljftal
- !! www.pac0abs.com
I S
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
i QUALITY CONTROL DATA
I
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
QC Batch: WETA/10086
QC Batch Method: EPA 300.0
Associated Lab Samples: 9297450001
METHOD BLANK: 632809
Associated Lab Samples: 9297450001
Parameter Units
Sulfate ug/L
LABORATORY CONTROL SAMPLE:
632810
Parameter
Units
Sulfate
ug/L
MATRIX SPIKE SAMPLE:
632811
Parameter
Units
Sulfate
ug/L
MATRIX SPIKE SAMPLE:
632813
Parameter
I_
Units
Sulfate
ug/L
SAMPLE DUPLICATE: 632812
Parameter
Sulfate
SAMPLE DUPLICATE: 632814
Parameter
Sulfate
I
Date: 07/20/2011 04:36 PM
I
Analysis Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
0.01 250000 07/14/1101:06
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
20000 190001 95 90-110
9297410001 Spike MS MS % Rec
Result Cone. Result % Rec Limits Qualifiers
ND 20000 20000J 89 90-110 M1
9297410002 Spike MS MS % Rec
Result Cone. Result % Rec Limits Qualifiers
45.6 mg/L 20000 61200J 78 90-110 M1
9297410001 Dup
Units Result Result RPD
ug/L ND 2170J
Max
RPD Qualifiers
20
9297410002 Dup Max
Units Result Result RPD RPD Qualifiers
ug/L 45.6 mg/L 46100J 1 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 18

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/�aceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr.
wwv pacelab&com Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
QC Batch: WETA/10107
QC Batch Method: SM 4500-CI-E
Associated Lab Samples: 9297450001
METHOD BLANK: 634467
Associated Lab Samples: 9297450001
Parameter Units
Chloride ug/L
LABORATORY CONTROL SAMPLE: 634468
Parameter Units
Chloride ug/L
MATRIX SPIKE SAMPLE: 634469
Parameter Units
Chloride ug/L
Analysis Method: SM 4500-CI-E
Analysis Description: 4500 Chloride
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5000 07/15/1113:59
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20000 20200 101 90-110
9297593002 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
2790 mg/L 5000000 3810000 20 75-125 MO
SAMPLE DUPLICATE: 634470
9297594001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Chloride ug/L 6440 mg/L 6600000 3 20
Date: 07/20/2011 04:36 PM REPORT OF LABORATORY ANALYSIS Page 16 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aXAnalj6cal
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
- www.pacelabscom
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
j
[phone] [phone]
[phone]
-
i�
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
QC Batch: WETA/10087
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310B TOC
- Associated Lab Samples: 9297450001
METHOD BLANK: 632815
Matrix: Water
Associated Lab Samples: 9297450001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Organic Carbon
ug/L
ND 1000 07/19/11 21:17
LABORATORY CONTROL SAMPLE:
632816
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Organic Carbon
ug/L
25000 24600 98 90-110
MATRIX SPIKE SAMPLE:
632817
f _
9297645001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Total Organic Carbon
i
ug/L
3.6 mg/L 25000 26700 92
75-125
MATRIX SPIKE SAMPLE:
632819
9297319002 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Total Organic Carbon
ug/L
8800 25000 32300 94
75-125
SAMPLE DUPLICATE: 632818
9297450001 Dup Max
Parameter
Units
Result Result RPD RPD
Qualifiers
Total Organic Carbon
ug/L
13400 13400 0 20
SAMPLE DUPLICATE: 632820
9297319003 Dup Max
Parameter
Units
Result Result RPD RPD
Qualifiers
Total Organic Carbon
ug/L
10800 10700 1 20
I
Date: 07/20/2011 04:36 PM
REPORT OF LABORATORY ANALYSIS
Page 17 of 18
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-
I
1
without the written consent of Pace Analytical Services, Inc..

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aceAnalytical
205 East Meadow Road - Suite
2225 Riverside Dr.
9800 KinceyAve. Suite 100
www.pacelabs.cortr.
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
3
[phone]
[phone]
[phone]
QUALIFIERS
Project: ALEXANDER MSWLF-MW-3
Pace Project No.: 9297450
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
1g Re -extraction conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Date: 07/20/2011 04:36 PM REPORT OF LABORATORY ANALYSIS Page 18 of 18
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CHAIN -OF -CUSTODY / Analytical Request Document
aceAnalJ/•�/Cial ® The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. RQ Ct/
www.pacelab3.com
Section A Section B Section C
Page: ( of
Required Client Information: Required Project Information: Invoice Information:
Compan : Report To: Attention:
1166519
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Copy To:
CCwI
Company Name:
REGtJLATQRYAGENCY'
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r NPDES r GROUND WATER j- DRINKING WATER
(r UST (` RCRA OTHER
Email To:
Purchase Order No.:
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Reference:
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(r
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Manager. \ �
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Requested Due DaterTAT: 1
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Section D Matrix Codes
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Required Client Information MATRIX I CODE
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COLLECTED
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ADDITIONAL COMMENTS
RELINQ
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rp
DATE+TIjWE
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SAMPLE CONDITIONS
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SIGNATURE of SAMPLER: DATE Signed
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Sample Condition Upon Receipt
-.-AaceAnalyt/cal Client Name: Project #
Where Received: P—Huntersville ❑ Asheville ❑ Eden
Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ Commercial J6\ Pace Other O tidrla
Custody Seal on Cooler/Box Present: ❑ yes no Seals intact: ❑ yes ❑ no w
Packing Material: ❑ Bubble Wrap Kubble Bags ❑ None ❑Other
Thermometer Used: IR Gun: T1102 Type of Ice: Wet Blue None Samples on ice, cooling process has begun
CIIIt.1 Vv�lcVuv... a........ ..�.-. �___. ___
Corrected Cooler Temp.: � ` C
_ _ /���
Biological Tissue is Frozen: Ye�
Date and I ' ' Is oape o n xamining
content • � l
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
Yes
❑No
❑NIA
1.
Chain of Custody Filled Out:
Yes
❑No
❑N/A
2.
Chain of Custody Relinquished:
Yes
❑No
❑N/A
3.
Sampler Name & Signature on COC:
ZYes
❑No
❑N/A
4.
Samples Arrived within Hold Time:
Yes
❑No
❑N/A
5.
Short Hold Time Analysis (<72hr):
Yes
DNo
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
PIN.
❑N/A
7.
Sufficient Volume:
VYes
❑No
❑N/A
8.
Correct Containers Used:
'Yes
❑No
❑N/A
9.
-Pace Containers Used:
Yes
❑No
❑N/A
Containers Intact:
Yes
❑No
❑N/A
10.
Filtered volume received for Dissolved tests
❑Yes
❑No
N/A
11.
Sample Labels match COC:
Dyes
6&o
❑N/A
12. u t, —TY
-Includes date/time/ID/Analysis Matrix:
�—
e•�e��
All containers needing preservation have been checked.
es
❑No
❑N/A
13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
Yes
❑No
❑N/A
exceptions: VOA, coliform, TOC. O&G, WI-DRO (water)
Dyes
❑No
Initial when completed
Samples checked for dechlorination:
Vfy.s
❑No
❑N/A
14.
Headspace in VOA Vials ( >6mm):
❑Yes
No
❑N/A
15.
Trip Blank Present:
❑Yes
❑No
N/A
16.
Trip Blank Custody Seals Present
❑Yes
❑No
NIA
Pace TriD Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
Date/Time:
Field Data Required? Y / N
SCURF Review: I Date: ��1 SRF Review: 1 t�� (Date: � — (% [ (_j�"
Note: Whenever t is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North `Carolilina D�EHNNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)
F-CHR-CS-003-rev.04 27Jun2011

aceAnalXical.
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden. NC 27288
[phone]
July 21, 2011
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
RE: Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between June 30, 2011
and July 05, 2011. The results relate only to the samples included in this report. Results reported
herein conform to the most current TNI standards, where applicable, unless otherwise narrated in
the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��-
Kevin Godwin
[e-mail]
Project Manager
Enclosures
cc: Ms. Maggie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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xnvw.pacefabs,odm.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
CERTIFICATIONS
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Arizona Certification #: AZ0735
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH 0216
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: LA090012
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL1264
Massachusetts Certification #: M-FL1264
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Virginia Drinking Water Certification M 00213
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Montana Certification #: Cert 0074
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification M FL765
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Pennsylvania Certification #: 68-547
Puerto Rico Certification #: FLO1264
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
Virginia Certification #: 00432
Wyoming Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460144
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
VirginaNELAP Certification #: 460147
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 43

i
® Pace Analytical Services, Inc.
-- aceAnaljftal
205 East Meadow Road -Suite A
www.pacetabsxvrn Eden, NC 27288
I
/ [phone]
Project:
ALEXANDER MSWLF - SWS +UIC
Pace Project No.:
9297319
Lab ID
Sample ID
9297319001
MW-31
9297319002
MW-11
— 9297319003
MW-26
9297319004
MW-27
9297319005
MW-26
- 9297319006
MW-27
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Water
06/29/1114:35
06/30/1111:45
Water
06/30/1117:30
07/01/1114:10
Water
06/30/1116:30
07/01/1114:10
Water
06/30/1115:35
07/01/1114:10
Water
06/30/1116:30
07/05/1112:30
Water
06/30/1115:35
07/05/1112:30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
REPORT OF LABORATORY ANALYSIS Page 3 of 43
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® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acemalytiml 205 East Meadow Road - Suite A 2225 Riverside Dr.
wmpacelabs.com Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
SAMPLE ANALYTE COUNT
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Lab ID Sample ID
9297319001 MW-31
9297319002 MW-11
9297319003 MW-26
9297319004 MW-27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Method
Analysts
Analytes
Reported
Laboratory
EPA 6010
JMW, SHB
16
PASI-A
EPA7470
JMW
1
PASI-A
EPA8260
MCK
52
PASI-C
SM 2320B
AES
1
PASI-A
SM 4500-S21D
AES
1
PASI-A
SM 5210B
SDH
1
PASI-A
EPA 300.0
EWS
1
PASI-A
EPA353.2
DMN
1
PASI-A
SM 4500-CI-E
JDA
1
PASI-A
SM 5220D
SDH
1
PASI-A
SM 53106
EWS
1
PASI-A
EPA6010
SHB
16
PASI-A
EPA7470
JMW
1
PASI-A
EPA 8260
MCK
5
PASI-C
SM 2320B
AES
1
PASI-A
SM 4500-S2D
AES
1
PASI-A
SM 5210B
SAJ
1
PASI-A
EPA 300.0
EWS
1
PASI-A
EPA353.2
DMN
1
PASI-A
SM 4500-CI-E
JDA
1
PASI-A
SM 5220D
SDH
1
PASI-A
SM 5310B
EWS
1
PASI-A
EPA 8260
MCK
52
PASI-C
SM 2320B
AES
1
PASI-A
SM 4500-S2D
AES
1
PASI-A
SM 5210E
SAJ
1
PASI-A
EPA 300.0
EWS
1
PASI-A
EPA353.2
DMN
1
PASI-A
SM 4500-CI-E
JDA
1
PASI-A
SM 5220D
SDH
1
PASI-A
SM 5310B
EWS
1
PASI-A
EPA8151
LJM
2
PASI-O
EPA 8260
MCK
52
PASI-C
SM 2320B
AES
1
PASI-A
SM 5210B
SAJ
1
PASI-A
EPA 300.0
EWS
1
PASI-A
EPA353.2
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acemalytical 205 East Meadow Road - Suite 2225 Riverside Dr. 9800 KinceyAve. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
Project: ALEXANDER MSWLF - SWS +UIC
_ Pace Project No.: 9297319
I
I
Lab ID Sample ID
1
9297319005 MW-26
I �
I
9297319006 MW-27
i
I
SAMPLE ANALYTE COUNT
Method
SM 4500-CI-E
SM 5310B
EPA 6010
EPA 7470
EPA 6010
EPA 7470
Analytes
Analysts
Reported
Laboratory
JDA
1
PASI-A
EWS
1
PASI-A
SHB
16
PASI-A
JMW
1
PASI-A
SHB
15
PASI-A
JMW
1
PASI-A
REPORT OF LABORATORY ANALYSIS Page 5 of 43
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® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnaljftal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
/ www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
I
ANALYTICAL RESULTS
Project: ALEXANDER MSWLF - SWS +UIC ` -
Pace Project No.: 9297319
Sample: MW-31 Lab ID: 9297319001 Collected: 06/29/11 14:35 Received: 06/30/11 11:45 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
i
6010 ICP Groundwater Analytical Method: EPA 6010 Preparation Method: EPA 3010
Antimony ND ug/L 6.0 5.0 1 07/09/11 12:15 07/13/11 18:59 7440-36-0
Arsenic ND ug/L 10.0 5.0 1 07/09/11 12:15 07/14/11 15:32 7440-38-2
Barium 97.9.1 ug/L 100 5.0 1 07/09/11 12:15 07/13/11 18:59 7440-39-3
Beryllium ND ug/L 1.0 1.0 1 07/09/11 12:15 07/13/11 18:59 7440-41-7
Cadmium ND ug/L 1.0 1.0 1 07/09/11 12:15 07/13/11 18:59 7440-43-9
Chromium ND ug/L 10.0 5.0 1 07/09/11 12:15 07/13/11 18:59 7440-47-3
Cobalt ND ug/L 10.0 5.0 1 07/09/11 12:15 07/13/11 18:59 7440-48-4
Copper ND ug/L 10.0 5.0 1 07/09/11 12:15 07/13/11 18:59 7440-50-8
Iron 1790 ug/L 300 50.0 1 07/09/11 12:15 07/13/11 18:59 7439-89-6
Lead ND ug/L 10.0 5.0 1 07/09/11 12:15 07/13/11 18:59 7439-92-1
Nickel ND ug/L 50.0 5.0 1 07/09/11 12:15 07/13/11 18:59 7440-02-0
Selenium ND ug/L 10.0 10.0 1 07/09/11 12:15 07/13/11 18:59 7782-49-2
Silver ND ug/L 10.0 5.0 1 07/09/11 12:15 07/13/11 18:59 7440-22-4
Thallium ND ug/L 5.5 5.4 1 07/09/11 12:15 07/13/11 18:59 7440-28-0
Vanadium ND ug/L 25.0 5.0 1 07/09/11 12:15 07/13/11 18:59 7440-62-2
Zinc 12.3 ug/L 10.0 10.0 1 07/09/11 12:15 07/13/11 18:59 7440-66-6
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
I
Mercury ND ug/L 0.20 0.10 1 07/11/11 14:15 07/12/11 13:04 7439-97-6
8260 MSV Low Level Landfill Analytical Method: EPA 8260
Acetone ND ug/L 100 2.2 1 07/01/11 23:45 67-64-1
Acrylonitrile ND ug/L 200 1.9 1 07/01/11 23:45 107-13-1
Benzene 0.30J ug/L 1.0 0.25 1 07/01/11 23:45 71-43-2
Bromochloromethane ND ug/L 3.0 0.17 1 07/01/11 23:45 74-97-5
Bromodichloromethane ND ug/L 1.0 0.18 1 07/01/11 23:45 75-27-4 j
Bromoform ND ug/L 3.0 0.26 1 07/01/11 23:45 75-25-2
Bromomethane ND ug/L 10.0 0.29 1 07/01/11 23:45 74-83-9
2-Butanone (MEI) ND ug/L 100 0.96 1 07/01/11 23:45 78-93-3
Carbon disulfide ND ug/L 100 1.2 1 07/01/11 23:45. 75-15-0
Carbon tetrachloride ND ug/L 1.0 0.25 1 07/01/11 23:45 56-23-5 - =
Chlorobenzene ND ug/L 3.0 0.23 1 07/01/11 23:45 108-90-7
Chloroethane ND ug/L 10.0 0.54 1 07/01/11 23:45 75-00-3
Chloroform ND ug/L 5.0 0.14 1 07/01/11 23:45 67-66-3
i
Chloromethane ND ug/L 1.0 0.11 1 07/01/11 23:45 74-87-3 -
1,2-Dibromo-3-chloropropane ND ug/L 13.0 2.5 1 07/01/11 23:45 96-12-8
Dibromochloromethane ND ug/L 3.0 0.21 1 07/01/11 23:45 124-48-1
1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 07/01/11 23:45 106-93-4
Dibromomethane ND ug/L 10.0 0.21 1 07/01/11 23:45 74-95-3 -
1,2-Dichlorobenzene ND ug/L 5.0 0.30 1 07/01/11 23:45 95-50-1
1,4-Dichlorobenzene 0.89J ug/L 1.0 0.33 1 07/01/11 23:45 106-46-7
trans-1,4-Dichloro-2-butene ND ug/L 100 1.0 1 07/01/11 23:45 110-57-6
1,1-Dichloroethane 0.66J ug/L 5.0 0.32 1 07/01/11 23:45 75-34-3
1,2-Dichloroethane ND ug/L 1.0 0.12 1 07/01/11 23:45 107-06-2
1,1-Dichloroethene ND ug/L 5.0 0.56 1 07/01/11 23:45 75-35-4
cis-1,2-Dichloroethene 3.0.1 ug/L 5.0 0.19 1 07/01/11 23:45 156-59-2
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 6 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. - -

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Sample: MW-31
Parameters
8260 MSV Low Level Landfill
trans-1,2-Dichloroethene
1,2-Dichloropropane
I
1,3-Dichloropropane
cis-1, 3-Dichloropropene
tra ns-1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBI)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trchloroethene
Trichlorofluoromethane
1,2,3-Tdchloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane IS)
1,2-Dichloroethane-d4 IS)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
4500S2D Sulfide Water
Sulfide
5210B BOD, 5 day
BOD, 5 day
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
Date: 07/21/2011 03:58 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 9297319001 Collected:
06/29/11 14:35
Received: 06/30/11 11:45 Matrix: Water
Report
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No.
Analytical Method: EPA 8260
ND ug/L 5.0
0.49
1
07/01/11 23:45
156-60-5
ND ug/L 1.0
0.27
1
07/01/11 23:45
78-87-5
ND ug/L 1.0
0.28
1
07/01/11 23:45
142-28-9
ND ug/L 1.0
0.13
1
07/01/11 23:45
10061-01-5
ND ug/L 1.0
0.26
1
07/01/11 23:45
10061-02-6
ND ug/L 1.0
0.30
1
07/01/11 23:45
100-41-4
ND ug/L 50.0
0.46
1
07/01/11 23:45
591-78-6
ND ug/L 10.0
0.32
1
07/01/11 23:45
74-88-4
ND ug/L 1.0
0.97
1
07/01/11 23:45
75-09-2
ND ug/L 100
0.33
1
07/01/11 23:45
108-10-1
ND ug/L 1.0
0.26
1
07/01/11 23:45
100-42-5
ND ug/L 5.0
0.33
1
07/01/11 23:45
630-20-6
ND ug/L 3.0
0.40
1
07/01/11 23:45
79-34-5
ND ug/L 1.0
0.46
1
07/01/11 23:45
127-18-4
ND ug/L 1.0
0.26
1
07/01/11 23:45
108-88-3
ND ug/L 1.0
0.48
1
07/01/11 23:45
71-55-6
ND ug/L 1.0
0.29
1
07/01/11 23:45
79-00-5
ND ug/L 1.0
0.47
1
07/01/11 23:45
79-01-6
ND ug/L 1.0
0.20
1
07/01/11 23:45
75-69-4
ND ug/L 1.0
0.41
1
07/01/11 23:45
96-18-4
ND ug/L 50.0
0.35
1
07/01/11 23:45
108-05-4
ND ug/L 1.0
0.62
1
07/01/11 23:45
75-01-4
ND ug/L 5.0
0.66
1
07/01/11 23:45
1330-20-7
93 % 70-130
1
07/01/11 23:45
460-00-4
113 % 70-130
1
07/01/11 23:45
1868-53-7
110 % 70-130
1
07/01/11 23:45
17060-07-0
97 % 70-130
1
07/01/11 23:45
2037-26-5
Analytical Method: SM 2320B
36600 ug/L 5000
5000
1
07/12/11 14:00
Analytical Method: SM 4500-S2D
ND ug/L 1000
100
1
07/06/11 16:30
18496-25-8
Analytical Method: SM 5210B
ND ug/L 2000
2000
1
07/01/11 11:44 07/06/11 09:07
Analytical Method: EPA 300.0
1640J ug/L 250000
1
07/13/11 22:23
14808-79-8
Analytical Method: EPA 353.2
474J ug/L 10000
200
1
06/30/11 21:58
Analytical Method: SM 4500-CI-E
Qual
10100 ug/L 5000 5000 1 07/15/11 14:09 16887-00-6
REPORT OF LABORATORY ANALYSIS Page 7 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
xwvw.pacelabs.com
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-31
Lab ID: 9297319001 Collected:
06/29/11 14:35
Received: 06/30/11 11:45 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
6220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND ug/L 25000
25000 1
07/18/11 13:57
531013 TOC
Analytical Method: SM 5310B
Total Organic Carbon
8850 ug/L 1000
1000 1
07/01/11 20:31 7440-44-0
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 8 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceMalXical
www.pamlabs.com
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-11 Lab ID: 9297319002 Collected: 06/30/11 17:30 Received: 07/01/11 14:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 ICP Groundwater
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Nickel
Selenium
Silver
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
8260 MSV Low Level Landfill
1,2,4-Trichlorobenzene
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
4500S2D Sulfide Water
Sulfide
5210E BOD, 5 day
BOD, 5 day
300.0 IC Anions 28 Days
Sulfate
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
Analytical Method: EPA 6010. Preparation Method: EPA 3010
ND ug/L 6.0
5.0
1
07/18/11 10:15
07/18/11 23:46
7440-36-0
ND ug/L 10.0
5.0
1
07/18/11 10:15
07/18/11 23:46
7440-38-2
197 ug/L 100
5.0
1
07/18/11 10:15
07/18/11 23:46
7440-39-3
ND ug/L 1.0
1.0
1
07/18/11 10:15
07/18/11 23:46
7440-41-7
ND ug/L 1.0
1.0
1
07/18/11 10:15
07/18/11 23:46
7440-43-9
36.3 ug/L 10.0
5.0
1
07/18/11 10:15
07/18/11 23:46
7440-47-3
127 ug/L 10.0
5.0
1
07/18/11 10:15
07/18/11 23:46
7440-48-4
18.6 ug/L 10.0
5.0
1
07/18/11 10:15
07/19/11 12:05
7440-50-8
45300 ug/L 300
50.0
1
07/18/11 10:15
07/18/11 23:46
7439-89-6
8.0.1 ug/L 10.0
5.0
1
07/18/11 10:15
07/18/11 23:46
7439-92-1
30.5J ug/L 50.0
5.0
1
07/18/11 10:15
07/18/11 23:46
7440-02-0
ND ug/L 10.0
10.0
1
07/18/11 10:15
07/19/11 12:05
7782-49-2
ND ug/L 10.0
5.0
1
07/18/11 10:15
07/18/11 23:46
7440-22-4
ND ug/L 5.5
5.4
1
07/18/11 10:15
07/19/11 12:05
7440-28-0
18.2J ug/L 25.0
5.0
1
07/18/11 10:15
07/18/11 23:46
7440-62-2
198 ug/L 10.0
10.0
1
07/18/11 10:15
07/18/11 23:46
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20
0.10
1
07/12/11 15:05
07/13/11 13:41
7439-97-6
Analytical Method: EPA 8260
0.68.1 ug/L 10.0
0.35
1
07/07/11 18:16
120-82-1
96 % 70-130
1
07/07/11 18:16
460-00-4
118 % 70-130
1
07/07/11 18:16
1868-53-7
114 % 70-130
1
07/07/11 18:16
17060-07-0
100 % 70-130
1
07/07/11 18:16
2037-26-5
Analytical Method: SM 2320B
239000 ug/L 5000
5000
1
07/14/11 13:50
Analytical Method: SM 4500-S2D
ND ug/L 1000
100
1
07/06/11 16:30
18496-25-8
Analytical Method: SM 5210B
ND ug/L 2000
2000
1
07/02/11 11:30
07/07/11 11:36
Analytical Method: EPA 300.0
2720J ug/L 250000
1
07/14/1105:11
14808-79-8
Analytical Method: EPA 353.2
ND ug/L 10000
200
1
07/01/11 21:13
Analytical Method: SM 4500-CI-E
22600 ug/L 5000
5000
1
07/15/11 14:15
16887-00-6
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 9 of 43
This report shall not be reproduced, except in full,
withoutthe written consent of Pace Analytical Services, Inc..

aceAnaliftal
wr W.Pacelabs.com.
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-11
Lab ID: 9297319002 Collected:
06/30/11 17:30
Received: 07/01/11 14:10 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
30000 ug/L 25000
25000 1
07/18/11 13:57
5310E TOC
Analytical Method: SM 5310B
Total Organic Carbon
8800 ug/L 1000
1000 1
07/20/11 12:59 7440-44-0
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 10 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

neiAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-26 Lab ID: 9297319003 Collected: 06/30/11 16:30 Received: 07/01/11 14:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 NISV Low Level Landfill
Analytical Method: EPA 8260
Acetone
2.5.1 ug/L
100
2.2
1
07/07/11 18:42
67-64-1
Acrylonitrile
ND ug/L
200
1.9
1
07/07/11 18:42
107-13-1
Benzene
2.9 ug/L
1.0
0.25
1
07/07/11 18:42
71-43-2
-- Bromochloromethane
ND ug/L
3.0
0.17
1
07/07/11 18:42
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.18
1
07/07/11 18:42
75-27-4
Bromoform
ND ug/L
3.0
0.26
1
07/07/11 18:42
75-25-2
Bromomethane
ND ug/L
10.0
0.29
1
07/07/11 18:42
74-83-9
2-Butanone (MEK)
ND ug/L
100
0.96
1
07/07/11 18:42
78-93-3
Carbon disulfide
ND ug/L
100
1.2
1
07/07/11 18:42
75-15-0
Carbon tetrachloride
ND ug/L
1.0
0.25
1
07/07/11 18:42
56-23-5
Chlorobenzene
1.8J ug/L
3.0
0.23
1
07/07/11 18:42
108-90-7
Chloroethane
1.1J ug/L
10.0
0.54
1
07/07/11 18:42
75-00-3
Chloroform
ND ug/L
5.0
0.14
1
07/07/11 18:42
67-66-3
Chloromethane
ND ug/L
1.0
0.11
1
07/07/11 18:42
74-87-3
1,2-Dibromo-3-chloropropane
ND ug/L
13.0
2.5
1
07/07/11 18:42
96-12-8
Dibromochloromethane
ND ug/L
3.0
0.21
1
07/07/11 18:42
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
0.27
1
07/07/11 18:42
106-93-4
Dibromomethane
ND ug/L
10.0
0.21
1
07/07/11 18:42
74-95-3
1,2-Dichlorobenzene
ND ug/L
5.0
0.30
1
07/07/11 18:42
95-50-1
1,4-Dichlorobenzene
6.7 ug/L
1.0
0.33
1
07/07/11 18:42
106-46-7
trans-1,4-Dichloro-2-butene
ND ug/L
100
1.0
1
07/07/11 18:42
110-57-6
1,1-Dichloroethane
1.OJ ug/L
5.0
0.32
1
07/07/11 18:42
75-34-3
1,2-Dichloroethane
0.119.1 ug/L
1.0
0.12
1
07/07/11 18:42
107-06-2
1,1-Dichloroethene
ND ug/L
5.0
0.56
1
07/07/11 18:42
75-35-4
cis-1,2-Dichloroethene
30.5 ug/L
5.0
0.19
1
07/07/11 18:42
156-59-2
trans-1,2-Dichloroethene
ND ug/L
5.0
0.49
1
07/07/11 18:42
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
0.27
1
07/07/11 18:42
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
0.28
1
07/07/11 18:42
142-28-9
cis-1,3-Dichloropropene
ND ug/L
1.0
0.13
1
07/07/11 18:42
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
1.0
0.26
1
07/07/11 18:42
10061-02-6
Ethylbenzene
ND ug/L
1.0
0.30
1
07/07/11 18:42
100-41-4
2-Hexanone
ND ug/L
50.0
0.46
1
07/07/11 18:42
591-78-6
lodomethane
ND ug/L
10.0
0.32
1
07/07/11 18:42
74-88-4
Methylene Chloride
ND ug/L
1.0
0.97
1
07/07/11 18:42
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
100
0.33
1
07/07/11 18:42
108-10-1
Styrene
ND ug/L
1.0
0.26
1
07/07/11 18:42
100-42-5
- 1,1,1,2-Tetrachloroethane
ND ug/L
5.0
0.33
1
07/07/11 18:42
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
3.0
0.40
1
07/07/11 18:42
79-34-5
Tetrachloroethene
ND ug/L
1.0
0.46
1
07/07/11 18:42
127-18-4
Toluene
ND ug/L
1.0
0.26
1
07/07/11 18:42
108-88-3
1,1,1-Trichloroethane
ND ug/L
1.0
0.48
1
07/07/11 18:42
71-55-6
1,12-Trichloroethane
ND ug/L
1.0
0.29
1
07/07/11 18:42
79-00-5
Trichloroethene
ND ug/L
1.0
0.47
1
07/07/11 18:42
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
0.20
1
07/07/11 18:42
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
0.41
1
07/07/11 18:42
96-18-4
Vinyl acetate
ND ug/L
50.0
0.35
1
07/07/11 18:42
108-05-4
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 11 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceiAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wmpawlabs.com. Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
ANALYTICAL RESULTS
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Sample: MW-26 Lab ID: 9297319003 Collected: 06/30/11 16:30 Received: 07/01/11 14:10 Matrix: Water
Parameters
8260 MSV Low Level Landfill
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
4500S2D Sulfide Water
Sulfide
5210B BOD, 5 day
BOD, 5 day
300.0 IC Anions 28 Days
Sulfate
363.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
5310B TOC
Total Organic Carbon
Report
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: EPA 8260
ND ug/L 1.0
0.62
1
07/07/11 18:42
75-01-4
ND ug/L 5.0
0.66
1
07/07/11 18:42
1330-20-7
96 % 70-130
1
07/07/11 18:42
460-00-4
119 % 70-130
1
07/07/11 18:42
1868-53-7
116 % 70-130
1
07/07/11 18:42
17060-07-0
99 % 70-130
1
07/07/11 18:42
2037-26-5
Analytical Method: SM 2320B
183000 ug/L 5000
5000
1
07/14/11 13:50
Analytical Method: SM 4500-S2D
ND ug/L 1000
100
1
07/06/11 16:30
18496-25-8
Analytical Method: SM 5210B
ND ug/L 2000
2000
1
07/02/11 11:30 07/07/11 11:36
Analytical Method: EPA 300.0
4020J ug/L 250000
1
07/14/11 05:24
14808-79-8
Analytical Method: EPA 353.2
ND ug/L . 10000
200
1
07/01/11 21:11
Analytical Method: SM 4500-CI-E
14400 ug/L 5000
5000
1
07/15/11 14:15
16887-00-6
Analytical Method: SM 5220D
ND ug/L 25000
25000
1
07/18/11 13:57
Analytical Method: SM 5310B
10800 ug/L 1000
1000
1
07/19/11 22:58
7440-44-0
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 12 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-27
Parameters
Lab ID: 9297319004
Results Units
Collected:
Report
Limit
06/30/11 15:35 Received: 07/01/11 14:10 Matrix: Water
MDL DF Prepared Analyzed CAS No. Qual
8151 Chlorinated Herbicides
Analytical Method: EPA8151
Dinoseb
ND ug/L
1.0
0.057
1 07/06/11 13:30
07/07/11 09:36
88-85-7
2,4-DCPA (S)
88 %
65.5-
1 07/06/11 13:30
07/07/11 09:36
19719-28-9
125.7
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
Acetone
3.1J ug/L
100
2.2
1
07/07/11 19:07
67-64-1
Acrylonitrile
ND ug/L
200
1.9
1
07/07/11 19:07
107-13-1
Benzene
ND ug/L
1.0
0.25
1
07/07/11 19:07
71-43-2
Bromochloromethane
ND ug/L
3.0
0.17
1
07/07/11 19:07
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.18
1
07/07/11 19:07
75-27-4
Bromoform
ND ug/L
3.0
0.26
1
07/07/11 19:07
75-25-2
Bromomethane
ND ug/L
10.0
0.29
1
07/07/11 19:07
74-83-9
2-Butanone (MEK)
ND ug/L
100
0.96
1
07/07/11 19:07
78-93-3
Carbon disulfide
ND ug/L
100
1.2
1
07/07/11 19:07
75-15-0
Carbon tetrachloride
ND ug/L
1.0
0.25
1
07/07/11 19:07
56-23-5
Chlorobenzene
ND ug/L
3.0
0.23
1
07/07/11 19:07
108-90-7
Chloroethane
ND ug/L
10.0
0.54
1
07/07/11 19:07
75-00-3
Chloroform
ND ug/L
5.0
0.14
1
07/07/11 19:07
67-66-3
Chloromethane
ND ug/L
1.0
0.11
1
07/07/11 19:07
74-87-3
1,2-Dibromo-3-chloropropane
ND ug/L
13.0
2.5
1
07/07/11 19:07
96-12-8
Dibromochloromethane
ND ug/L
3.0
0.21
1
07/07/11 19:07
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
0.27
1
07/07/11 19:07
106-93-4
Dibromomethane
ND ug/L
10.0
0.21
1
07/07/11 19:07
74-95-3
1,2-Dichlorobenzene
ND ug/L
5.0
0.30
1
07/07/11 19:07
95-50-1
1,4-Dichlorobenzene
ND ug/L
1.0
0.33
1
07/07/11 19:07
106-46-7
trans-1,4-Dichloro-2-butene
ND ug/L
100
1.0
1
07/07/11 19:07
110-57-6
1,1-Dichloroethane
0.76J ug/L
5.0
0.32
1
07/07/11 19:07
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
0.12
1
07/07/11 19:07
107-06-2
1,1-Dichloroethene
ND ug/L
5.0
0.56
1
07/07/11 19:07
75-35-4
cis-1,2-Dichloroethene
22.6 ug/L
5.0
0.19
1
07/07/11 19:07
156-59-2
trans-1,2-Dichloroethene
ND ug/L
5.0
0.49
1
07/07/11 19:07
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
0.27
1
07/07/11 19:07
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
0.28
1
07/07/11 19:07
142-28-9
cis-1,3-Dichloropropene
ND ug/L
1.0
0.13
1
07/07/11 19:07
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
1.0
0.26
1
07/07/11 19:07
10061-02-6
Ethylbenzene
ND ug/L
1.0
0.30
1
07/07/11 19:07
100-41-4
2-Hexanone
ND ug/L
50.0
0.46
1
07/07/11 19:07
591-78-6
lodomethane
ND ug/L
10.0
0.32
1
07/07/11 19:07
74-88-4
Methylene Chloride
ND ug/L
1.0
0.97
1
07/07/11 19:07
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
100
0.33
1
07/07/11 19:07
108-10-1
Styrene
ND ug/L
1.0
0.26
1
07/07/11 19:07
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
5.0
0.33
1
07/07/11 19:07
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
3.0
0.40
1
07/07/11 19:07
79-34-5
Tetrachloroethene
ND ug/L
1.0
0.46
1
07/07/11 19:07
127-18-4
Toluene
ND ug/L
1.0
0.26
1
07/07/11 19:07
108-88-3
1,1,1-Trichloroethane
ND ug/L
1.0
0.48
1
07/07/11 19:07
71-55-6
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
Page 13 of 43
This report shall not be reproduced,
except in full,
without the written
consent of Pace Analytical Services, Inc..

aceAnaiXical
` www.pacelabs.com
i
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Sample: MW-27 Lab ID: 9297319004 Collected: 06/30/11 15:35 Received: 07/01/11 14:10 Matrix: Water
Parameters
8260 MSV Low Level Landfill
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
5210B BOD, 5 day
BOD, 5 day
300.0 IC Anions 28 Days
Sulfate
363.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
5310E TOC
Total Organic Carbon
Report
Results Units Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: EPA 8260
ND ug/L 1.0
0.29
1
07/07/11 19:07
79-00-5
ND ug/L 1.0
0.47
1
07/07/11 19:07
79-01-6
ND ug/L 1.0
0.20
1
07/07/11 19:07
75-69-4
ND ug/L 1.0
0.41
1
07/07/11 19:07
96-18-4
ND ug/L 50.0
0.35
1
07/07/11 19:07
108-05-4
ND ug/L 1.0
0.62
1
07/07/11 19:07
75-01-4
ND ug/L 5.0
0.66
1
07/07/11 19:07
1330-20-7
97 % 70-130
1
07/07/11 19:07
460-00-4
120 % 70-130
1
07/07/11 19:07
1868-53-7
115 % 70-130
1
07/07/11 19:07
17060-07-0
99 % 70-130
1
07/07/11 19:07
2037-26-5
Analytical Method: SM 2320B
265000 ug/L 5000
5000
1
07/14/11 13:50
Analytical Method: SM 5210B
ND ug/L 2000
2000
1
07/02/11 11:30 07/07/11 11:36
Analytical Method: EPA 300.0
26100J ug/L 250000
1
07/14/11 05:38
14808-79-8
Analytical Method: EPA 353.2
ND ug/L 10000
200
1
07/01/11 21:07
Analytical Method: SM 4500-CI-E
13200 ug/L 5000
5000
1
07/15/11 14:16
16887-00-6
Analytical Method: SM 5310B
3610 ug/L 1000
1000
1
07/20/11 09:14
7440-44-0
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 14 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

®
Pace Analytical Services, Inc.
Pace Analytical
Services, Inc. Pace Analytical Services, Inc.
acemalidical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pacelabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
j
[phone]
[phone]
[phone]
ANALYTICAL
RESULTS
Project: ALEXANDER
MSWLF - SWS +UIC
Pace Project No.: 9297319
Sample: MW-26
Lab ID: 9297319006 Collected:
06/30/11 16:30
Received: 07/05/11 12:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 ICP Groundwater
Analytical Method:
EPA 6010 Preparation
Method: EPA 3010
Antimony
ND ug/L
6.0
5.0
1
07/18/11 10:15
07/19/11 00:07
7440-36-0
Arsenic
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:07
7440-38-2
Barium
8.4J ug/L
100
5.0
1
07/18/11 10:15
07/19/11 00:07
7440-39-3
Beryllium
ND ug/L
1.0
1.0
1
07/18/11 10:15
07/19/11 00:07
7440-41-7
Cadmium
ND ug/L
1.0
1.0
1
07/18/11 10:15
07/19/11 00:07
7440-43-9
Chromium
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:07
7440-47-3
Cobalt
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:07
7440-48-4
Copper
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 12:09
7440-50-8
Iron
62.4J ug/L
300
50.0
1
07/18/11 10:15
07/19/11 00:07
7439-89-6
Lead
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:07
7439-92-1
Nickel
ND ug/L
50.0
5.0
1
07/18/11 10:15
07/19/11 00:07
7440-02-0
Selenium
ND ug/L
10.0
10.0
1
07/18/11 10:15
07/19/11 12:09
7782-49-2
Silver
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:07
7440-22-4
Thallium
ND ug/L
5.5
5.4
1
07/18/11 10:15
07/19/11 12:09
7440-28-0
Vanadium
ND ug/L
25.0
5.0
1
07/18/11 10:15
07/19/11 00:07
7440-62-2
Zinc
ND ug/L
10.0
10.0
1
07/18/11 10:15
07/19/11 00:07
7440-66-6
7470 Mercury
Analytical Method:
EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
0.10
1
07/12/11 15:05
07/13/11 13:52
7439-97-6
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 15 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
1�5aceAnalXicale 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.pacelabs.c= Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
ANALYTICAL RESULTS
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-27
Lab ID: 9297319006
Collected:
06/30/11 15:35
Received: 07/05/11 12:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
60101CP Groundwater
Analytical Method: EPA6010 Preparation Method: EPA3010
Antimony
ND ug/L
6.0
5.0
1
07/18/11 10:15
07/19/11 00:14
7440-36-0
Arsenic
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:14
7440-38-2
Barium
12.3.1 ug/L
100
5.0
1
07/18/11 10:15
07/19/11 00:14
7440-39-3
Beryllium
ND ug/L
1.0
1.0
1
07/18/11 10:15
07/19/11 00:14
7440-41-7
Cadmium
ND ug/L
1.0
1.0
1
07/18/11 10:15
07/19/11 00:14
7440-43-9
Chromium
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:14
7440-47-3
Cobalt
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:14
7440-48-4
Copper
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 12:12
7440-50-8
Lead
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:14
7439-92-1
Nickel
ND ug/L
50.0
5.0
1
07/18/11 10:15
07/19/11 00:14
7440-02-0
Selenium
ND ug/L
10.0
10.0
1
07/18/11 10:15
07/19/11 12:12
7782-49-2
Silver
ND ug/L
10.0
5.0
1
07/18/11 10:15
07/19/11 00:14
7440-22-4
Thallium
ND ug/L
5.5
5.4
1
07/18/11 10:15
07/19/11 12:12
7440-28-0
Vanadium
ND ug/L
25.0
5.0
1
07/18/11 10:15
07/19/11 00:14
7440-62-2
Zinc
ND ug/L
10.0
10.0
1
07/18/11 10:15
07/19/11 00:14
7440-66-6
7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 0.20 0.10 1 07/12/11 15:05 07/13/11 13:55 7439-97-6
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 16 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc.
aW nalytical 205 East Meadow Road - Suite A
www.pacetabsx= Eden, NC 27288
l [phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: GCSV/5095
Analysis Method: EPA 8151
QC Batch Method: EPA 8151
Analysis Description: 8151A GCS Herbicides
- Associated Lab Samples: 9297319004
METHOD BLANK: 220073
Matrix: Water
Associated Lab Samples: 9297319004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
- Dinoseb ug/L
ND 1.0
07107/1107:13
2,4-DCPA (S) %
92 65.5-125.7
07/07/11 07:13
LABORATORY CONTROL SAMPLE: 220074
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Dinoseb ug/L
1.2 0.97J
80 44-111.8
2,4-DCPA (S) %
94 65.5-125.7
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 220202
220203
MS MSD
9297234018
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Cone. Result
Result % Rec % Rec Limits RPD RPD Qual
Dinoseb ug/L ND
2.4 2.4 2.0
1.8J 85 77 44-111.8 10 40
2,4-DCPA (S) %
96 86 65.5-125
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 43

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: MPRP/8693
QC Batch Method: EPA 3010 '
Associated Lab Samples: 9297319001
METHOD BLANK: 631113
Associated Lab Samples: 9297319001
Parameter Units
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Iron
ug/L
Lead
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Thallium
ug/L
Vanadium
ug/L
Zinc
ug/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Water
EPA 6010
6010 MET NC Groundwater
Blank
Result
Reporting
Limit
Analyzed
ND
6.0
07/13/1118:53
ND
10.0
07/13/1118:53
ND
100
07/13/1118:53
ND
1.0
07/13/1118:53
ND
1.0
07/13/1118:53
ND
10.0
07/13/1118:53
ND
10.0
07/13/1118:53
ND
10.0
07/13/1118:53
ND
300
07/13/1118:53
ND
10.0
07/13/1118:53
ND
50.0
07113/1118:53
ND
10.0
07/13/1118:53
ND
10.0
07/13/1118:53
ND
5.5
07113/1118:53
ND
25.0
07/13/1118:53
ND
10.0
07/13/1118:53
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
631114
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
506
101
80-120
Arsenic
ug/L
500
506
101
80-120
Barium
ug/L
500
515
103
80-120
Beryllium
ug/L
500
515
103
80-120
Cadmium
ug/L
500
508
102
80-120
Chromium
ug/L
500
511
102
80-120
Cobalt
ug/L
500
514
103
80-120
Copper
ug/L
500
514
103
80-120
Iron
ug/L
5000
5080
102
80-120
Lead
ug/L
500
515
103
80-120
Nickel
ug/L
500
513
103
80-120
Selenium
ug/L
500
507
101
80-120
Silver
ug/L
250
254
102
80-120
Thallium
ug/L
500
509
102
80-120
Vanadium
ug/L
500
507
101
80-120
Zinc
ug/L
500
521
104
80-120
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 18 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

l
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
46maixical" 205 East Meadow Road - Suite A 2225 Riverside Dr.
-- / www.pacelab&com Eden, NC 27288 Asheville, NC 28804
+ [phone] [phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
MATRIX SPIKE SAMPLE: 631115
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
9297319001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Antimony
ug/L
ND
500
493
99
75-125
Arsenic
ug/L
ND
500
501
99
75-125
Barium
ug/L
97.9J
500
602
101
75-125
Beryllium
ug/L
ND
500
506
101
75-125
Cadmium
ug/L
ND
500
498
100
75-125
Chromium
ug/L
ND
500
508
101
75-125
Cobalt
ug/L
ND
500
503
100
75-125
Copper
ug/L
ND
500
503
101
75-125
Iron
ug/L
1790
5000
6830
101
75-125
Lead
ug/L
ND
500
503
100
75-125
Nickel
ug/L
ND
500
505
100
75-125
j Selenium
ug/L
ND
500
502
100
75-125
' Silver
ug/L
ND
250
249
100
75-125
Thallium,
ug/L
ND
500
492
98
75-125
Vanadium
ug/L
ND
500
504
100
75-125
Zinc
I
ug/L
12.3
500
519
101
75-125
SAMPLE DUPLICATE: 631116
j
9297234005
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Antimony
ug/L
ND
ND
25
Arsenic
ug/L
ND
ND
25
Barium
ug/L
30.7J
30.2J
1
25
Beryllium
ug/L
ND
ND
25
Cadmium
ug/L
ND
ND
25
Chromium
ug/L
ND
ND
25
Cobalt
ug/L
ND
ND
25
Copper
ug/L
ND
ND
25
Iron
ug/L
5720
5680
1
25
Lead
ug/L
ND
ND
25
Nickel
ug/L
ND
ND
25
Selenium
ug/L
ND
ND
25
Silver
ug/L
ND
ND
25
Thallium
ug/L
ND
ND
25
Vanadium
ug/L
ND
ND
25
Zinc
ug/L
ND
ND
25
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 43

®
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Analytical
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
wwwpacelab.to=
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
!�
t
[phone]
[phone]
[phone] r
QUALITY CONTROL
DATA
-
Project: ALEXANDER MSWLF -
SWS +UIC
—
Pace Project No.: 9297319
QC Batch: MPRP/8751
Analysis Method:
EPA6010
QC Batch Method: EPA 3010
Analysis Description:
6010 MET NC Groundwater
Associated Lab Samples: 9297319002, 9297319005, 9297319006
METHOD BLANK: 635078
Matrix: Water
Associated Lab Samples: 9297319002, 9297319005, 9297319006
Blank Reporting
Parameter
Units Result Limit
Analyzed Qualifiers
Antimony
ug/L
ND
6.0 07/18/1123:39
i l
Arsenic
ug/L
ND
10.0 07/18/1123:39
Barium
ug/L
ND
100 07/18/1123:39
Beryllium
ug/L
ND
1.0 07118/1123:39
'
Cadmium
ug/L
ND
1.0 07/18/1123:39
Chromium
ug/L
ND
10.0 07/18/1123:39
Cobalt
ug/L
ND
10.0 07/18/1123:39
Copper
ug/L
ND
10.0 07/18/1123:39
Iron
ug/L
ND
300 07/18/1123:39
Lead
ug/L
ND
10.0 07/18/1123:39
Nickel
ug/L
ND
50.0 07/18/1123:39
Selenium
ug/L
ND
10.0 07/18/1123:39
Silver
ug/L
ND
10.0 07/1811123:39
Thallium
ug/L
ND
5.5 07118/1123:39
--
Vanadium
ug/L
ND
25.0 07118/1123:39
Zinc
ug/L
ND
10.0 07/1811123:39
LABORATORY CONTROL SAMPLE:
635079
+
Spike LCS
LCS % Rec
Parameter
Units Conc. Result
% Rec Limits Qualifiers
Antimony
ug/L
500 443
89 80-120
Arsenic
ug/L
500 446
89 80-120
Barium
ug/L
500 453
91 80-120
Beryllium
ug/L
500 457
91 80-120
Cadmium
ug/L
500 461
92 80-120
Chromium
ug/L
500 469
94 80-120
j
Cobalt
ug/L
500 460
92 80-120
Copper
ug/L
500 444
89 80-120
Iron
ug/L
5000 4620
92 80-120
1
Lead
ug/L
500 456
91 80-120
Nickel
ug/L
500 464
93 80-120
Selenium
ug/L
500 435
87 80-120
Silver
ug/L
250 235
94 J 80-120
Thallium
ug/L
500 435
87 80-120
Vanadium
ug/L
500 452
90 80-120
Zinc
ug/L
500 463
93 80-120
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
Page 20 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/5aceMaliftal 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.pamlabs.com Eden, NC 27288 Asheville, NC 28804
1 [phone] [phone]
QUALITY CONTROL DATA
I
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
635080
9297319002
Spike
MS _
MS
% Rec
_ Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Antimony
ug/L
ND
500
446
89
75-125
Arsenic
ug/L
ND
500
459
91
75-125
Barium
ug/L
197
500
653
91
75-125
Beryllium
ug/L
ND
500
469
94
75-125
j Cadmium
ug/L
ND
500
465
93
75-125
Chromium
ug/L
36.3
500
512
95
75-125
Cobalt
ug/L
127
500
583
91
75-125
Copper
ug/L
18.6
500
479
92
75-125
Iron
ug/L
45300
5000
49600
87
75-125
Lead
ug/L
8.OJ
500
463
91
75-125
Nickel
ug/L
30.5J
500
494
93
75-125
-' Selenium
ug%L
ND
500
451
89
75-125
Silver
ug/L
ND
250
239
96
75-125
Thallium
ug/L
ND
500
435
86
75-125
Vanadium
ug/L
18.2J
500
483
93
75-125
Zinc
ug/L
198
500
677
96
75-125
SAMPLE DUPLICATE: 635081
9297319005
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Antimony
ug/L
ND
ND
25
Arsenic
ug/L
ND
ND
25
Barium
ug/L
8AJ
8.3J
1
25
Beryllium
ug/L
ND
ND
25
Cadmium
ug/L
ND
ND
25
Chromium
ug/L
ND
ND
25
Cobalt
ug/L
ND
ND
25
Copper
ug/L
ND
ND
25
Iron
ug/L
62AJ
ND
25
Lead
ug/L
ND
ND
25
Nickel
ug/L
ND
ND
25
Selenium
ug/L
ND
ND
25
Silver
ug/L
ND
ND
25
Thallium
ug/L
ND
ND
25
Vanadium
ug/L
ND
ND
25
Zinc
ug/L
ND
ND
25
I
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 43

aceAnalytical
wwwpacelabs,com.
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: MERP/3604
QC Batch Method: EPA 7470
Associated Lab Samples: 9297319001
METHOD BLANK: 632070
Associated Lab Samples: 9297319001
Parameter Units
Mercury ug/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7470
Analysis Description: 7470 Mercury
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 0.20 07/12/1113:41
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 632071
Spike
LCS
LCS
% Rec
Parameter Units
Cone.
Result
% Rec
Limits
Qualifiers
Mercury ug/L
2.5
2.4
97
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 632072
632073
MS
MSD
9297084001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Mercury ug/L ND
2.5
2.5
1.7
1.7
69
70
75-125
1 25 MO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 632074
632075
MS
MSD
9297084002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD . RPD Qual
Mercury ug/L ND
2.5
2.5
1.6
2.1
63
85
75-125
30 25 M0,R1
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 22 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc.
aW nalytical 205 East Meadow Road - Suite A
- www.pacelabs.00m Eden, NC 27288
j [phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: MERP/3605 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 9297319002, 9297319005, 9297319006
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
METHOD BLANK: 632262 Matrix: Water
Associated Lab Samples: 9297319002, 9297319006, 9297319006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 07/13/1112:46
LABORATORY CONTROL SAMPLE: 632263
Parameter Units
Mercury ug/L
Spike LCS
Conc. Result
2.5 2.3
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
91 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 632264
632265
MS
MSD
9297391006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Mercury ug/L ND
2.5
2.5
2.2
2.3
86
91
75-125
5 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 632266
632267
MS
MSD
9297391007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Mercury ug/L ND
2.5
2.5
2.3
2.6
94
104
75-125
10 25
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 23 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

1
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
0
acemal 4 cal 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.parelabs.com. Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: MSV/15871 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 9297319001
METHOD BLANK: 628900
Associated Lab Samples: 9297319001
Parameter
Matrix: Water
Blank Reporting
Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
5.0
07101/1115:15
1,1,1-Trichloroethane
ug/L
ND
1.0
07/01/11 15:15
1,1,2,2-Tetrachloroethane
ug/L
ND
3.0
07/01/11 15:15
1,12-Trichloroethane
ug/L
ND
1.0
07101/1115:15
1,1-Dichloroethane
ug/L
ND
5.0
07/01/11 15:15
1,1-Diehl oroethene
ug/L
ND
5.0
07/01/11 15:15
1,2,3-Trichloropropane
ug/L
ND
1.0
07/01/11 15:15
1,2-Dibromo-3-chloropropane
ug/L
ND
13.0
07/01/11 15:15
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
07/01/11 15:15
1,2-Dichlorobenzene
ug/L
ND
5.0
07/01/11 15:15
1,2-Dichloroethane
ug/L
ND
1.0
07/01/11 15:15
1,2-Dichloropropane
ug/L
ND
1.0
07/01/11 15:15
1,3-Dichloropropane
ug/L
ND
1.0
07/01/11 15:15
1,4-Dichlorobenzene
ug/L
ND
1.0
07/01/11 15:15
2-Butanone (MEK)
ug/L
ND
100
07/01/11 15:15
2-Hexanone
ug/L
ND
50.0
07/01/11 15:15
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
07/01/11 15:15
Acetone
ug/L
ND
100
07/01/11 15:15
Acrylonitrile
ug/L
ND
200
07/01/11 15:15
Benzene
ug/L
ND
1.0
07/01/11 15:15
Bromochloromethane
ug/L
ND
3.0
07/01/11 15:15
Bromodichloromethane
ug/L
ND
1.0
07/01/11 15:15
Bromoform
ug/L
ND
3.0
07/0111115:15
Bromomethane
ug/L
ND
10.0
07/01/11 15:15
Carbon disulfide
ug/L
ND
100
07/01/11 15:15
Carbon tetrachloride
ug/L
ND
1.0
07/01/11 15:15
Chlorobenzene
ug/L
0.23J
3.0
07/01/11 15:15
Chloroethane
ug/L
ND
10.0
07/01/11 15:15
Chloroform
ug/L
ND
5.0
07/01/11 15:15
Chloromethane
ug/L
ND
1.0
07/01/11 15:15
cis- 1,2-Dichloroethene
ug/L
ND
5.0
07/01/11 15:15
cis-1,3-Dichloropropene
ug/L
ND
1.0
07/01/11 15:15
Dibromochloromethane
ug/L
ND
3.0
07/01/11 15:15
Dibromomethane
ug/L
ND
10.0
07/01/11 15:15
Ethylbenzene
ug/L
ND
1.0
07/01/11 15:15
lodomethane
ug/L
ND
10.0
07/0111115:15
Methylene Chloride
ug/L
ND
1.0
07/01/11 15:15
Styrene
ug/L
ND
1.0
07/01/11 15:15
Tetrachloroethene
ug/L
ND
1.0
07/01/11 15:15
Toluene
ug/L
ND
1.0
07/01/11 15:15
trans-1,2-Dichloroethene
ug/L
ND
5.0
07/01/11 15:15
trans- 1,3-Dichloropropene
ug/L
ND
1.0
07/01/11 15:15
trans-1,4-Dichloro-2-butene
ug/L
ND
100
07/01/11 15:15
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be
reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
�r
Page 24 of 43

aceAnalytical
twww.pacelabs.com.
7
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
METHOD BLANK: 628900
Matrix: Water
Associated Lab Samples:
9297319001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Trchloroethene
ug/L
ND
1.0
07/01/11 15:15
Trichlorofluoromethane
ug/L
ND
1.0
07/01/11 15:15
Vinyl acetate
ug/L
ND
50.0
07/01/11 15:15
Vinyl chloride
ug/L
ND
1.0
07/01/11 15:15
Xylene (Total)
ug/L
ND
5.0
07/01/11 15:15
1,2-Dichloroethane-d4 (S)
%
102
70-130
07/01/11 15:15
4-Bromofluorobenzene (S)
%
93
70-130
07/01/11 15:15
Dibromofluoromethane (S)
%
106
70-130
07/01/11 15:15
Toluene-d8 (S)
%
99
70-130
07/01/11 15:15
LABORATORY CONTROL SAMPLE:
Parameter
628901
Spike
Units Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
47.8
96
70-130
1,1,1-Trichloroethane
ug/L
50
45.0
90
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.5
101
70-130
1,1,2-Trichloroethane
ug/L
50
50.1
100
70-130
1,1-Dichloroethane
ug/L
50
49.1
98
70-130
1,1-Dichloroethene
ug/L
50
46.8
94
70-132
1,2,3-Trichloropropane
ug/L
50
48.4
97
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
49.9
100
70-130
1,2-Dibromoethane (EDB)
ug/L
50
48.5
97
70-130
1,2-Dichlorobenzene
ug/L
50
50.3
101
70-130
1,2-Dichloroethane
ug/L
50
46.0
92
70-130
1,2-Dichloropropane
ug/L
50
49.6
99
70-130
1,3-Dichloropropane
ug/L
50
49.4
99
70-130
1,4-Dichlorobenzene
ug/L
50
47.4
95
70-130
2-Butanone (MEK)
ug/L
100
101
101
70-145
2-Hexanone
ug/L
100
96.5
96
70-144
4-Methyl-2-pentanone (MIBK)
ug/L
100
93.5J
93
70-140
Acetone
ug/L
100
97.3J
97
50-175
Acrylonitrile
ug/L
250
286
115
70-143
Benzene
ug/L
50
46.1
92
70-130
Bromochloromethane
ug/L
50
46.5
93
70-130
Bromodichloromethane
ug/L
50
45.0
90
70-130
Bromoform
ug/L
50
50.1
100
70-130
Bromomethane
ug/L
50
48.9
98
54-130
Carbon disulfide
ug/L
50
53.8J
108
70-131
Carbon tetrachloride
ug/L
50
43.5
87
70-132
Chlorobenzene
ug/L
50
48.9
98
70-130
Chloroethane
ug/L
50
63.9
108
64-134
Chloroform
ug/L
50
47.8
96
70-130
Chloromethane
ug/L
50
43.6
87
64-130
cis- 1,2-Dichloroethene
ug/L
50
47.1
94
70-131
cis-1,3-Dichloropropene
ug/L
50
52.3
105
70-130
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 25 of 43

aceAnaiytical
mvwpacefa6s.wrp
1
)
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
LABORATORY CONTROL SAMPLE: 628901
Parameter
Units
Dibromochloromethane
ug/L
Dibromomethane
ug/L
Ethylbenzene
ug/L
lodomethane
ug/L
Methylene Chloride
ug/L
Styrene
ug/L
Tetrachloroethene
ug/L
Toluene
ug/L
trans-1,2-Dichloroethene
ug/L
trans- 1,3-Dichloropropene
ug/L
trans-1,4-Dichloro-2-butene
ug/L
Trichloroethene
ug/L
Trichlorofluoromethane
ug/L
Vinyl acetate
ug/L
Vinyl chloride
ug/L
Xylene (Total)
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Dibromofluoromethane (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
50
45.7
91
70-130
50
47.5
95
70-131
50
48.2
96
70-130
100
117
117
49-180
50
49.1
98
63-130
50
52.6
105
70-130
50
46.7
93
70-130
50
46.6
93
70-130
50
47.6
95
70-130
50
50.5
101
70-132
50
57.3.1
115
70-141
50
48.8
98
70-130
50
45.5
91
62-133
100
108
108
66-157
50
53.0
106
69-130
150
150
100
70-130
93
70-130
98
70-130
99
70-130
101
70-130
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
628902
628903
MS
MSD
9297234017
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,1-Dichloroethene
ug/L
ND
50
50
46.8
51.2
94
102
70-166
9
30
Benzene
ug/L
6.7
50
50
57.6
60.7
102
108
70-148
5
30
Chlorobenzene
ug/L
2.3J
50
50
51.7
56.5
99
108
70-146
9
30
Toluene
ug/L
ND
50
50
49.7
53.2
99
106
70-155
7
30
Trichloroethene
ug/L
2.4
50
50
50.5
53.5
96
102
69-151
6
30
1,2-Dichloroethane-d4 (S)
%
97
99
70-130
4-Bromofluorobenzene (S)
%
92
94
70-130
Dibromofluoromethane (S)
%
104
106
70-130
Toluene-d8 (S)
%
96
96
70-130
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 26 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalyiical®
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MSV/15933 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 9297319002, 9297319003, 9297319004
METHOD BLANK: 630602
Associated Lab Samples:
Parameter
Matrix: Water
9297319002,9297319003,9297319004
Blank Reporting
Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1;1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichloropropane
1,4-Dichlorobenzene
2-butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis- 1,3-Dichloropropene
Dibromoch lodomethane
Dibromomethane
Ethylbenzene
lodomethane
Methylene Chloride
Styrene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans- 1,3-Dichloropropene
Date: 07/21/2011 03:58 PM
ug/L
ND
5.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
3.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
5.0
07/07/1111:02
ug/L
ND
5.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
10.0
07/07/1111:02
ug/L
ND
13.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
5.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
100
07107/1111:02
ug/L
ND
50.0
07/07/1111:02
ug/L
ND
100
07/07/1111:02
ug/L
2.9J
100
07/07/1111:02
ug/L
ND
200
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
3.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
3.0
07/07/1111:02
ug/L
ND
10.0
07/07/1111:02
ug/L
ND
100
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
3.0
07/07/1111:02
ug/L
ND
10.0
07/07/1111:02
ug/L
0.14J
5.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
5.0
07/07/1111:02
ug/L
ND
1.0
07/0711111:02
ug/L
ND
3.0
07107/1111:02
ug/L
ND
10.0
07/0711111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
10.0
07/07/1111:02
ug/L
ND
1.0
07107/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
ug/L
ND
5.0
07/07/1111:02
ug/L
ND
1.0
07/07/1111:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 43

j�,, ® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aciei U alXical 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
METHOD BLANK: 630602
Associated Lab Samples:
Parameter
Matrix: Water
9297319002, 9297319003, 9297319004
Blank Reporting
Units Result Limit
Analyzed Qualifiers
trans-1,4-Dichloro-2-butene
ug/L
ND
100
07/07/11 11:02
Trichloroethene
ug/L
ND
1.0
07/07/11 11:02
Trichlorofluoromethane
ug/L
ND
1.0
07/07/11 11:02
Vinyl acetate
ug/L
ND
50.0
07/07/11 11:02
Vinyl chloride
ug/L
ND
1.0
07/07/11 11:02
Xylene (Total)
ug/L
ND
5.0
07/07/11 11:02
1,2-Dichloroethane-d4 (S)
%
113
70-130
07/07/11 11:02
4-Bromofluorobenzene (S)
%
94
70-130
07/07/11 11:02
Dibromofluoromethane IS)
%
118
70-130
07/07/11 11:02
Toluene-d8 (S)
%
97
70-130
07/07/11 11:02
LABORATORY CONTROL SAMPLE: 630603
Parameter
1,1,1,2-Tetrachloroethane
ug/L
1,1,1-Trichloroethane
ug/L
1,1,2,2-Tetrachloroethane
ug/L
1,1,2-Trichloroethane
ug/L
1,1-Dichloroethane
ug/L
1,1-Dichloroethene
ug/L
1,2,3-Trichloropropane
ug/L
1,2,4-Trichlorobenzene
ug/L
1,2-Dibromo-3-chloropropane
ug/L
1,2-Dibromoethane (EDB)
ug/L
1,2-Dichlorobenzene
ug/L
1,2-Dichloroethane
ug/L
1,2-Dichloropropane
ug/L
1,3-Dichloropropane
ug/L
1,4-Dichlorobenzene
ug/L
2-Butanone (MEK)
ug/L
2-Hexanone
ug/L
4-Methyl-2-pentanone (MIBK)
ug/L
Acetone
ug/L
Acrylonitrile
ug/L
Benzene
ug/L
Bromochloromethane
ug/L
Bromodichloromethane
ug/L
Bromoform
ug/L
Bromomethane
ug/L
Carbon disulfide
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroethane
ug/L
Chloroform
ug/L
Chloromethane
ug/L
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike
Units Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
50
50.9
102
70-130
50
51.0
102
70-130
50
32.1
64
70-130 LO
50
50.8
102
70-130
50
51.4
103
70-130
50
49.5
99
70-132
50
48.0
96
70-130
50
51.6
103
70-134
50
46.6
93
70-130
50
48.9
98
70-130
50
50.8
102
70-130
50
51.2
102
70-130
50
48.9
98
70-130
50
50.2
100
70-130
50
48.5
97
70-130
100
94.8J
95
70-145
100
92.2
92
70-144
100
90.91
91
70-140
100
99.2J
99
50-175
250
268
107
70-143
50
46.5
93
70-130
50
50.3
101
70-130
50
49.8
100
70-130
50
49.5
99
70-130
50
63.5
127
54-130
50
53.7J
107
70-131
50
49.5
99
70-132
50
49.6
99
70-130
50
53.9
108
64-134
50
52.2
104
70-130
50
43.3
87
64-130
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 28 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
J

j�
i
axAnalYdical
J www.pacelabs.com,
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
LABORATORY CONTROL SAMPLE:
630603
_ Parameter
Units
cis-1,2-Dichloroethene
ug/L
cis- 1,3-Dichloropropene
ug/L
Dibromochloromethane
ug/L
j— Dibromomethane
ug/L
Ethylbenzene
ug/L
— lodomethane
ug/L
Methylene Chloride
ug/L
Styrene
ug/L
Tetrachloroethene
ug/L
Toluene
ug/L
trans-1,2-Dichloroethene
ug/L
trans-1,3-Dichloropropene
ug/L
trans-1,4-Dichloro-2-butene
ug/L
Trichloroethene
ug/L
Trichlorofluoromethane
ug/L
Vinyl acetate
ug/L
Vinyl chloride
ug/L
Xylene (Total)
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Dibromofluoromethane (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
50
50.2
100
70-131
50
56.5
113
70-130
50
47.5
95
70-130
50
49.0
98
70-131
50
50.1
100
70-130
100
121
121
49-180
50
50.6
101
63-130
50
55.1
110
70-130
50
47.7
95
70-130
50
48.3
97
70-130
50
49.5
99
70-130
50
54.2
108
70-132
50
50.8J
102
70-141
50
59.0
118
70-130
50
50.6
101
62-133
100
105
105
66-157
50
48.8
98
69-130
150
161
107
70-130
101
70-130
99
70-130
104
70-130
101
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 630604
9297234026
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
630605
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
Max
RPD RPD Qua[
1,1-Dichloroethene
ug/L
ND
50
50
48.3
53.1
97
106
70-166
9
30
Benzene
ug/L
ND
50
50
43.6
48.8
87
98
70-148
11
30
Chlorobenzene
ug/L
ND
50
50
44.1
49.4
88
99
70-146
11
30
Toluene
ug/L
ND
50
50
44.5
49.3
89
99
70-155
10
30
Trichloroethene
ug/L
ND
50
50
42.2
46.8
84
93
69-151
10
30
1,2-Dichloroethane-d4 (S)
%
116
113
70-130
4-Bromofluorobenzene (S)
%
93
94
70-130
Dibromofluoromethane (S)
IN,
118
115
70-130
Toluene-d8 (S)
%
94
95
70-130
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 29 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
'®
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA --
NDER MSWLF - SWS +UIC
�
319
T/17103
Analysis Method: SM 2320B i
2320E
Analysis Description: 2320B Alkalinity
9297319001
37
Matrix: Water
9297319001
Blank Reporting —
Units
Result Limit Analyzed Qualifiers
ug/L
ND 5000 07/12/1114:00 -1
SAMPLE: 632238
Spike LCS LCS % Rec
Units
Conc. Result % Rec Limits Qualifiers
ug/L
50000 51200 102 90-110
632239
9297589001 Dup Max
Units
Result Result RPD RPD Qualifiers
ug/L
30.2 mg/L 29100 4 20
aceAnalytica
wwwpacelabs.cc
1
Project: ALEXA
Pace Project No.: 9297
QC Batch: WE
QC Batch Method: SM
Associated Lab Samples:
METHOD BLANK: 6322
Atssociated Lab Samples:
Parameter
Alkalinity, Total as CaCO3
LABORATORY CONTROL
Parameter
Alkalinity, Total as CaCO3
SAMPLE DUPLICATE:
Parameter
Alkalinity, Total as CaCO3
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
I �!
Page 30 of 43
_I
I

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
a205 East Meadow Road - Suite A 2225 Riverside Dr.
ceAnalytical
w,vw.pacela6s.corn Eden, NC 27288 Asheville, NC 28804
_
r
[phone] [phone]
QUALITY CONTROL DATA
-' Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WET/17121 Analysis Method: SM 2320B
QC Batch Method: SM 2320B Analysis Description: 2320B Alkalinity
Associated Lab Samples: 9297319002, 9297319003, 9297319004
METHOD BLANK: 632752 Matrix: Water
Associated Lab Samples: 9297319002, 9297319003, 9297319004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Alkalinity, Total as CaCO3 ug/L ND 5000 07/14/11 13:50
! LABORATORY CONTROL SAMPLE: 632753
Spike LCS LCS
i
Parameter Units Conc. Result % Rec
Alkalinity, Total as CaCO3 ug/L 50000 50800 102
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
90-110
SAMPLE DUPLICATE: 632754
9297234007 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Alkalinity, Total as CaCO3 ug/L 43800 41700 5 20
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 31 of 43

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
�®
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
11
[phone] [phone]
[phone]
QUALITY CONTROL DATA
-
ANDER MSWLF - SWS +UIC
319
T/17048
Analysis Method: SM 4500-S2D
4500-S2D
Analysis Description: 450OS2D Sulfide Water
� I
9297319001,9297319002,9297319003
16
Matrix: Water
9297319001,9297319002,9297319003
Blank Reporting
Units Result Limit Analyzed Qualifiers
ug/L ND 1000 07106/1116:30
SAMPLE:
630317
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
i
ug/L 500 509J 102 90-110
630318
9297185002 Spike MS MS
% Rec I
Units Result Conc. Result % Rec
Limits Qualifiers
ug/L ND 500 ND 6
75-125 MO
acmnalj4b
J www.pacelabs.com
Project: ALE)
Pace Project No.: 9297
QC Batch: WE
QC Batch Method: SM
Associated Lab Samples:
METHOD BLANK: 6303
Associated Lab Samples:
Parameter
Sulfide
LABORATORY CONTROL
Parameter
Sulfide
MATRIX SPIKE SAMPLE:
Parameter
Sulfide
SAMPLE DUPLICATE:
Parameter
Sulfide
Date: 07/21/2011 03:58 PM
6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 32 of 43

aceAnalytical
2 5ace East Meadow Ro dAnalycal'ces- Suite A
wrw.pacelabs.com Eden, NC 27288
- r
[phone]
— Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WET/16998
QC Batch Method: SM 5210B
Associated Lab Samples: 9297319001
J METHOD BLANK: 628803
Associated Lab Samples: 9297319001
Parameter Units
BOD, 5 day ug/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 5210B BOD, 5 day
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2000 07/06/1109:07
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 628804
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
i BOD, 5 day ug/L 198000 193000 97 84-115
SAMPLE DUPLICATE: 628805
9297319001 Dup
Parameter Units Result Result
BOD, 5 day ug/L ND ND
i
Date: 07/21/2011 03:58 PM
Max
RPD RPD Qualifiers
20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 33 of 43

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
f
�j /�+�
ll fGi� iG"d'
x
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100 -
www.paoMa6s.cdrrr.
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
(
J
[phone] [phone]
[phone]
i
QUALITY CONTROL DATA
—,
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WET/17021
Analysis Method: SM 5210B
QC Batch Method: SM 5210B
Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 9297319002, 9297319003, 9297319004
METHOD BLANK: 629470
Matrix: Water
Associated Lab Samples: 9297319002, 9297319003, 9297319004
Blank Reporting
-
Parameter
Units Result Limit Analyzed Qualifiers
BOD, 5 day
ug/L ND 2000 07/07/11 11:36
LABORATORY CONTROL SAMPLE:
629471
Spike LCS LCS % Rec
Parameter
Units Conc. Result % Rec Limits Qualifiers
BOD, 5 day
ug/L 198000 200000 101 84-115
SAMPLE DUPLICATE: 629472
9297153005 Dup Max
Parameter
Units Result Result RPD RPD
Qualifiers
BOD, 5 day
ug/L 13.7 mg/L 12200 12 20
—i
I I
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
' I
1
�J
Page 34 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

-I
®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
/+aa/� ��77 /
aG'1� A11a��L'a'
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Wmpacelabs.00m
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
j
[phone] [phone]
[phone]
i
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WETA/10085
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 9297319001
METHOD BLANK: 632799
Matrix: Water
Associated Lab Samples: 9297319001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Sulfate
ug/L
0.01 250000 07/13/1117:52
LABORATORY CONTROL SAMPLE:
632800
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Sulfate
ug/L
20000 19500J 97 90-110
MATRIX SPIKE SAMPLE:
632801
9297093002 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Sulfate
ug/L
8.8 mg/L 20000 28300J 97
90-110
MATRIX SPIKE SAMPLE:
632803
9297093003 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Sulfate
ug/L
10.8 mg/L 20000 30000J 96
90-110
SAMPLE DUPLICATE: 632802
9297093002 Dup Max
- Parameter
Units
Result Result RPD RPD
Qualifiers
Sulfate
ug/L
8.8 mg/L 8870J 1 20
Parameter
Sulfate
Date: 07/21/2011 03:58 PM
I
9297093003 Dup Max
Units Result Result RPD RPD Qualifiers
ug/L 10.8 mg/L 10700J 0 20
REPORT OF LABORATORY ANALYSIS
This haport shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 35 of 43

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
y
mai(Xical'
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pac0abs.com
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
j
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF - SWS +UIC
II,
Pace Project No.: 9297319
QC Batch: WETA/10086
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 9297319002, 9297319003, 9297319004
METHOD BLANK: 632809
Matrix: Water
Associated Lab Samples: 9297319002, 9297319003, 9297319004
Blank Reporting
Parameter
Units Result Limit Analyzed Qualifiers
Sulfate
ug/L 0.01 250000 07/14/1101:06
LABORATORY CONTROL SAMPLE:
632810
Spike LCS LCS % Rec
Parameter
Units Conc. Result % Rec Limits
Qualifiers
Sulfate
ug/L 20000 190001 95 90-110
MATRIX SPIKE SAMPLE:
632811
9297410001 Spike MS MS
% Rec
Parameter
Units Result Conc. Result % Rec
Limits Qualifiers
Sulfate
,
ug/L ND 20000 20000J
89 90-110 M1
� I
MATRIX SPIKE SAMPLE:
632813
9297410002 Spike MS MS
% Rec
Parameter
Units Result Conc. Result % Rec
Limits Qualifiers
Sulfate
ug/L 45.6 mg/L 20000 61200J
78 90-110 M1
SAMPLE DUPLICATE: 632812
9297410001 Dup Max
Parameter
Units Result Result RPD RPD
Qualifiers
Sulfate
ug/L ND 2170J
20
SAMPLE DUPLICATE: 632814
I
9297410002 Dup Max
j
Parameter
Units Result Result RPD RPD
Qualifiers -'
Sulfate
ug/L 45.6 mg/L 46100J 1
20
F
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
Page 36 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
_
i
ace

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aceftljftal
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pacelabs.com
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
i
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
-- Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WETA/10021
Analysis Method:
EPA 353.2
- QC Batch Method: EPA 353.2
Analysis Description:
353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 9297319001
METHOD BLANK: 628790
Matrix: Water
Associated Lab Samples: 9297319001
-
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
ug/L
ND 10000 06/30/11 21:38
LABORATORY CONTROL SAMPLE:
628791
Spike LCS
LCS % Rec
-- Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
ug/L
5000 5080J
102 90-110
MATRIX SPIKE SAMPLE:
628792
9297183001 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
- Nitrogen, Nitrate
ug/L
2.6 mg/L 5000
7870J 105
90-110
MATRIX SPIKE SAMPLE:
628794
-
9297212001 Spike
MS MS
%Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Nitrogen, Nitrate
ug/L
7.0 mg/L 5000
12800J 115
90-110 M1
Parameter
Nitrogen, Nitrate
SAMPLE DUPLICATE: 628795
Parameter
Nitrogen, Nitrate
Date: 07/21/2011 03:58 PM
9297183001
Dup
Max
Units Result
Result
RPD RPD Qualifiers
ug/L 2.6 mg/L
2640J
0 20
9297212001
Dup
Max
Units Result
Result
RPD RPD Qualifiers
ug/L 7.0 mg/L
7050J
0 20
REPORT OF LABORATORY ANALYSIS Page 37 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
1�5acemalXical 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.pacelabs.com. Eden, NC 27288 Asheville, NC 28804
j' [phone] [phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WETA/10033 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 9297319002, 9297319003, 9297319004
METHOD BLANK: 629444 Matrix: Water
Associated Lab Samples: 9297319002, 9297319003, 9297319004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate ug/L ND 10000 07/01/11 21:03
LABORATORY CONTROL SAMPLE: 629445
Parameter Units
Nitrogen, Nitrate ug/L
MATRIX SPIKE SAMPLE: 629446
Parameter Units
Nitrogen, Nitrate ug/L
SAMPLE DUPLICATE: 629447
Parameter
Nitrogen, Nitrate
Date: 07/21/2011 03:58 PM
9297319004 Dup
Units Result Result
ug/L ND ND
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
�I
i
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
5000 4930J 99 90-110
9297319004 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 5000 4990J 98 90-110
I I
t
I i
Page 38 of 43
'J
i I
f
Max
RPD RPD Qualifiers
20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
1�5aceAnaljdical 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804
j [phone] [phone]
i
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WETA/10107 Analysis Method: SM 4500-CI-E
QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride
Associated Lab Samples: 9297319001, 9297319002, 9297319003, 9297319004
METHOD BLANK: 634467 Matrix: Water
Associated Lab Samples: 9297319001, 9297319002, 9297319003, 9297319004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride ug/L ND 5000 07/15/1113:59
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
634468
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Chloride
ug/L
20000 20200
101
90-110
MATRIX SPIKE SAMPLE:
634469
9297593002 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Chloride
ug/L
2790 mg/L 5000000
3810000
20
75-125 MO
SAMPLE DUPLICATE: 634470
Parameter
Chloride
Date: 07/21/2011 03:58 PM
I
9297594001 Dup Max
Units Result Result RPD RPD Qualifiers
ug/L 6440 mg/L 6600000 3 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
withoutthe written consent of Pace Analytical Services, Inc..
Page 39 of 43

racil
®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Analytical
205 East Meadow Road - Suite A 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
www.pacelabs.com
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
[phone] [phone]
[phone]
QUALITY CONTROL DATA
r
i
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
_
QC Batch: WETA/10113
Analysis Method: SM 5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 9297319001, 9297319002, 9297319003
METHOD BLANK: 634928
Matrix: Water
Associated Lab Samples: 9297319001, 9297319002, 9297319003
Blank Reporting
Parameter
Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand
ug/L ND 25000 07/18/11 13:57
LABORATORY CONTROL SAMPLE:
634929
Spike LCS LCS % Rec
Parameter
Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand
ug/L 750000 728000 97 90-110
MATRIX SPIKE SAMPLE:
634930
9297305002 Spike MS MS
% Rec
Parameter
Units Result Cone. Result % Rec
Limits Qualifiers
Chemical Oxygen Demand
ug/L 719 mg/L 750000 1450000 98
75-125
MATRIX SPIKE SAMPLE:
634932
9297319001 Spike MS MS
% Rec
Parameter
Units Result Cone. Result % Rec
Limits Qualifiers I
Chemical Oxygen Demand
ug/L ND 750000 733000 98
75-125
SAMPLE DUPLICATE: 634931
9297305002 Dup Max
Parameter
Units Result Result RPD RPD
Qualifiers
Chemical Oxygen Demand
ug/L 719 mg/L 782000 8 20
SAMPLE DUPLICATE: 634933
9297319001 Dup Max
Parameter
Units Result Result RPD RPD
Qualifiers
Chemical Oxygen Demand
ug/L ND ND 20
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
Page 40 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

®
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acema,(Xical
205 East Meadow Road - Suite 2225 Riverside Dr.
9800 Kincey Ave. Suite 100
wmpacelabscorri
Eden, NC 27288 Asheville, NG 28804
Huntersville, NC 28078
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WETA/10028
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 9297319001
METHOD BLANK: 628908
Matrix: Water
Associated Lab Samples: 9297319001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Organic Carbon
ug/L
ND 1000 07/01/11 16:30
LABORATORY CONTROL SAMPLE:
628909
Spike LCS LCS % Rec
- Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Organic Carbon
ug/L
25000 24500 98 90-110
MATRIX SPIKE SAMPLE:
628912
9297084014 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Total Organic Carbon
ug/L
8.4 mg/L 25000 27300 76
75-125
MATRIX SPIKE SAMPLE:
628913
9297084001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
Total Organic Carbon
ug/L
14.0 mg/L 25000 29100 60
75-125 M1
SAMPLE DUPLICATE: 628910
9297385001 Dup Max
Parameter
Units
Result Result RPD RPD
Qualifiers
Total Organic Carbon
ug/L
2.6 mg/L 2610 1 20
SAMPLE DUPLICATE: 628911
9297385002 Dup Max
Parameter
Units
Result Result RPD RPD
Qualifiers
Total Organic Carbon
ug/L
21.5 mg/L 21400 0 20
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
Page 41 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

Services, Inc.
aceAnalytical
® 205 ace East Meadocal w Road 'ces- Suite A Pace Analyt2225 Riverside Dr.
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804
f [phone] [phone]
I
I -I
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
-,
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
QC Batch: WETA110087
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310B TOC
-
Associated Lab Samples: 9297319002, 9297319003, 9297319004
METHOD BLANK: 632815
Matrix: Water
Associated Lab Samples: 9297319002, 9297319003, 9297319004
Blank Reporting
Parameter
Units Result Limit Analyzed
Qualifiers
Total Organic Carbon
ug/L ND 1000 07/19/11 21:17
LABORATORY CONTROL SAMPLE:
632816
Spike LCS LCS
% Rec
Parameter
Units Conc. Result % Rec
Limits
Qualifiers
Total Organic Carbon
ug/L 25000 24600 98
90-110
MATRIX SPIKE SAMPLE:
632817
-
9297645001 Spike MS
MS
% Rec
Parameter
Units Result Conc. Result
% Rec
Limits Qualifiers
Total Organic Carbon
ug/L 3.6 mg/L 25000 26700
92
75-125
MATRIX SPIKE SAMPLE:
632819
9297319002 Spike MS
MS
% Rec
Parameter
Units Result Conc. Result
% Rec
Limits Qualifiers
Total Organic Carbon
ug/L 8800 25000 32300
94
75-125
SAMPLE DUPLICATE: 632818
9297450001 Dup
Max
Parameter
Units Result Result RPD
RPD
Qualifiers
Total Organic Carbon
ug/L 13400 13400 0
20
SAMPLE DUPLICATE: 632820
9297319003 Dup
Max
Parameter
Units Result Result RPD
RPD
Qualifiers
Total Organic Carbon
ug/L 10800 10700 1
20
I
Date: 07/21/2011 03:58 PM
REPORT OF LABORATORY ANALYSIS
Page 42 of 43
This report shall not be reproduced, except in full,
withoutthe written consent of Pace Analytical Services, Inc..
_I

I
aceAnalXical
wwvrpacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Project: ALEXANDER MSWLF - SWS +UIC
Pace Project No.: 9297319
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
Date: 07/21/2011 03:58 PM REPORT OF LABORATORY ANALYSIS Page 43 of 43
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

--- - I - ---� — - --- —' --�—-- - --' ----TJ
Qa►+'gl ��61�:��1
CHAIN -OF -CUSTODY / Analytical Request Document 'sw lea to
The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately, a off/
aceAnalytical ° � ll !�� � cr+
Section A Section B Section C Page: of
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Required Client Information: Required Project Information: Invoice Information:
Company: Report To: 4 Attention: 147
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0 ,�► +rtnwt Q jMef(o. Cp jrtl REGULATORY AGENCY
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-Imponent Note: tfy signing mis form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month fir ally Iftolces not paid withln 30 days. F-ALL-Q-020rev.07. 15-May-ZUU7

Sample Condition Upon
0 PAW,
Client Name: Project # g Z g-7 3l
Where Received: L" Huntersville ❑ Asheville ❑ Eden
"ourier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ Commercial 9 Pace Other
.fl''tioria _. ` �s -11
ustody Seal on Cooler/Box Present:
❑ yes [E no Seals intact: El yes
❑ no
P o� ` e�`Qa � ;
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Packing Material: ❑ Bubble Wrap
[bubble Bags ❑ None El Other
hermorneter Used: IR Gun: T1102
Type of Ice: Wet Blue None
Samples on ice, cooling process has begun
Temp Correction Factor: Add / Subtract 0 'C
orrected Cooler Temp.: a IS
C Biological Tissue is Frozen: Yes No
Date and Initials of person examining
contents: 3—M. 6-3c)
amp should be above freezing to 6°C
Comments:
^hain of Custody Present:
P'res— ONO ❑N/A
1.
:hain of Custody Filled Out:
2 r s ONO ❑N/A
2.
Chain of Custody Relinquished:
21e"s ❑No ❑N/A
3.
ampler Name & Signature on COC:
Samples Arrived within Hold Time:
ihort Hold Time Analysis (<72hr):
Lush Turn Around Time Requested:
Sufficient Volume:
;orrect Containers Used:
-Pace Containers Used:
ontainers Intact:
riltered volume received for Dissolved tests
-,ample Labels match COC:
-Includes date/time/ID/Analysis Matri
All containers needing preservation have been ched
B'q'e ❑No ❑N/A
4.
L-9,'ess ONO ❑N/A
5.
t1res ONO ❑N/A
6.
❑Yes O;Ko- ❑N/A
7,
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8.
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II containers needing preservation are found to be in ❑Yes ONO ❑N/A
)mpliance with EPA recommendation.
I-Yceptions: VOA, coliform, TOC, O&G, WI-DRO (water) ❑Yes ONO initial when completed
samples checked for dechlorination: (< ONO ❑N/A 14.
Headspace in VOA Vials ( >6mm): ❑Yes &Ko- ❑N/A 15.
rip Blank Present: Ores ONO 13INVA 16.
II rip Blank Custody Seals Present ❑Yes ONO N/A
-'ace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y I N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review Ia Date: I �O3d / SRF Review: t Date: (
Jote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy is form Wil be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)
F-CHR-CS-003-rev.04 27Jun2011

/ 2.hnalvtical
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
- - WWW.pacelabs.com
Page: ` . of 1
Section A Section El Section C.
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Required Client Information: Required Project Information: Invoice Information:
C mpany: Repo pp Attention:
A.
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Sample Condition UponReceipt
i
- 6kWcaf Client Name: /"V;�w pl Project #
fhere Received: Huntersville ❑ Asheville ❑ Eden
ourier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ Commercial K Pace Other
ustody Seal on Cooler/Box Present: ❑ yes 01 no Seals intact: ❑ yes ❑ no
O
acking Material: ❑ Bubble Wrap ]Bubble Bags ❑ None El Other
hermometer Used: IR Gun: T1102 Type of Ice: Wet Blue None [samples on ice, cooling process has begun
Fer•fnr• OrM / Sutftrar_t 0 'C
r j(
orrected Cooler Temp.:_�- 1 C
Biological Tissue is Frozen: Yes No
Date and I ' ' Is o pe on xa 'ning
contents: � e 6
I emp should be above freezing to 6'C
Comments:
hain of Custody Present:
es ONO
❑N/A
1.
hain of Custody Filled Out:
Yes ONO
❑N/A
2.
Chain of Custody Relinquished:
Yes ONO
❑N/A
3.
ampler Name $ Signature on COC:
I OYes ONO
❑N/A
4.
Samples Arrived within Hold Time:
OYes ONO
❑N/A
5.
hort Hold Time Analysis (<72hr):
Yes [iNo
❑NIA
6.
mush Turn Around Time Requested:
Dyes VNo
❑N/A
7.
"ufficientVolume:
o
❑N/A
a.'
orrect Containers Used:
Yes ONO
❑N/A
J, Fcs—
-Pace Containers Used:
Yes ONO
❑N/A
ontainers Intact:
OYes ONO
❑N/A
10.
Filtered volume received for Dissolved tests
Dyes ONO
N/A
11.
ample Labels match COC:
Yes No
❑N/A
12. tZ d�J-- °� t"�' A,
-Includes date/time/ID/Analysis Matrix:
vT ` s 6W C'
13.
All containers needing preservation have been checked. (J�Yes ONO
❑WA
II containers needing preservation are found to be in
ampliance with EPA recommendation.
I(�Yes ONO
I
❑NIA
:ceptions: VOA, colifonm, TOC, O&G, WI-DRO (water)
Dyes ONO
Initial when completed
amples checked for dechlorination:
OYes ONO
❑N/A
14.
Headspace in VOA Vials (>6mm),
rip Blank Present:
Dyes No
Dyes ❑No
❑NIA
�N/A
((((�N/A
15.
16.
(Trip Blank Custody Seals Present
Dyes ON.
. i _a �t /•s .. ..&. ..A�.
lace I np alarm Lui tt kn pi auaacu .
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: _ j o,� �� ka k-. Date/Time:/ 7 i I
Comments/ Resolution: s st - /c C
)CURF Review:/.., LIDate:1. 7/ l SRF Review: Date: `(_ ( J
Jote: Whenever t e 1s a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)
F-CHR-CS-003-rev.04 27Jun2011

CHAIN -OF -CUSTODY 1 Analytical Request Document
aceAnalytical ® The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
/ www.oseelebIt.eom
Section A Section B Section C
Page: of I
Required Client Information: Required Project Information: Invoice Information:
Company: Report TO:
�C � \ �
147436 8
1 A. tS, IL
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Address: Copy
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To:
Company Name:
TORYAGEfVCY
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Address:
r NPDES` r GROUND WATER r DRINKING WATER
UST RCRA /
Email To: Purchase
Order No.:
r A
Pace Quoteeb
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OTHER
Phone: i
-f313
Fax: Project
Name:
N}�
Pace Protect
SIt9 LOCati011
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Manager.
Requested a Date AT: Project
Number.
Pace Profile #:
s
Reque'stec�,Anatys(s'Ftltered(Y%N)
- .
Section D Matrix Codes
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Required Client Information 'MATRIX 1 CODE
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COLLECTED
Preservatives
tt;'
Drinking Water DIN
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Water WT
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Waste Water WIN
Product P
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START
COMPOSITE
END/GRAB
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SAMPLE ID Oil OL
Wipe WP
¢
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Sample IDS MUST BE UNIQUE Tissue TS
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SAMPLER NAME`AND
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(MMIDD/YY):
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Sample Condition Upon Receipt
-FaceAr*Vcal Client Name: Moa f IQCA Enm. Project # 1? 2�7V�
Where Received: Huntersville ❑ Asheville ❑ Eden
wrier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ Commercial Pace Other lona�
p-o�'���`�ate��.
Custody Seal on Cooler/Box Present: ❑ yes ❑ o Seals intact: ❑ yes ❑ no pplarne
icking Material: ❑ Bubble Wrap ❑Bubble Bags ['bone ❑Other
Thermometer Used: IR Gun: T1102
Type of Ice: Wet lue None
;mp Correction Factor: Add / Subtract
0 'C
,,orrected Cooler Temp.:
C Biological Tissue is Frozen: Yes No
Temp should be above freezing to 6'C
Comments:
lain of Custody Present:
BI;s ❑No ❑N/A
1.
Chain of Custod Filled Out:
Bl'e7 ❑No ❑N/A
2.
pain of Custody Relinquished:
res ❑No ❑N/A
3.
oampler Name & Si nature on COC:
amples Arrived within Hold Time:
hort Hold Time Analysis (<72hr):
Rush Turn Around Time Requested:
ufficient Volume:
(Correct Containers Used:
-Pace Containers Used:
containers Intact:
Piltered volume received for Dissolved tests
ample Labels match COC:
-Includes date/time/ID/Analysis Matr
I containers needing preservation have been chec
r,d containers needing preservation are found to be in
(compliance with EPA recommendation.
31es El No ❑N/A
es ❑No ❑N/A
4,
5.
❑Yes Litro— ❑N/A
6.
❑Yes B<o ❑N/A
7.
Yes ❑No El N/A
$,
es ❑No ❑N/A
es ❑No ❑N/A
9.
E!lVe—s ❑No ❑N/A
10.
❑Yes ❑No X/A
11.
❑Yes 9No ❑NIA I12. nn "�lMe_ ©C
EYes ❑No ❑N/A 13.
es ❑No ❑N/A
Samples on ice, cooling process has begun
Date and Initials of
mac\ C VA \e lGI•e1 z•-
;eptions: VOA, coliform, TOC, O&G, WI-DRO (water) ❑Yes ❑No Initial when completed
Samples checked for dechlorination: []Yes ❑No /A 14.
eadspace in VOA Vials ( >6mm): ❑Yes ❑No ETNJA 15.
rip Blank Present: ❑Yes ❑No N/A 16.
Trip Blank Custody Seals Present ❑Yes ❑No /A
,ace Trip Blank Lot # (if purchased):
client Notification/ Resolution: Field Data Required? Y I N
Person Contacted: Date/Time:
Comments/ Resolution:
;CURF Review: Date: '7 / SRF Review��Date: %/S /
Note: Whenever t is a discrepancy affecting North Carolina compliance samples, a cop this form will be sent to the North Carolina DEHNR
certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers)
F-CHR-CS-003-rev.04 27Jun2011