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HomeMy WebLinkAboutNC0021156_Renewal Application_20140714NPDES DOCUWENT SCANNING COVER SHEET NPDES Permit: NC0021156 Mount Holly WWTP Document Type: Permit Issuance Wasteload Allocation Authorization to Construct (AtC) Permit Modification Complete File - Historical Engineering Alternatives (EAA) Renewal Application Instream Assessment (67b) Speculative Limits Environmental Assessment (EA) Document Date: July 24, 2014 This documeat is printed on reuse paper - igzlore any content oa the resrerse side MOUNT HOLLY ; 400 East Central Avenue Post Office Box 406 Mount Holly, NC 28120 704-827-4261 704-827-6306 Fax Website: www.ntthollv.us Thursda , July 24, 2014 NCDENR/D Attn: NPDES Unit �olt 44ewwil CITY Of MOUNT HOLLY UTILITIES DEPARTMENT 1617 Mail Service Center (� Z^�S� p'� Raleigh, NC 27699-1617 VAt1 Re: NPDES Permit 4 NCO021156 Renewal ALL lip � �� Please See Att WATER TREATMENT WAS I MA PIR TRitA I Mr,NT STORMWAIF.R GIS TECI INOLOGY achments J To whom it may concern, iV S Please accept the City of Mount Holly pen t renewal form for permit „ NC0021 156. Attached with this cover letter is the completed Form 2A NPDES with Attachments I-VII. Current) we are still testing with the second species for toxicit , attachment V contains all the toxicity test performed in the last tour and one half years. Upon completion of the uta two tests we will forward those reports to you. You will find below an outline of each section that requires effluent monitoring data and dates in which the data was pulled from. • Section A.6.b&c data was pulled front July I, 2011 —June 30, 2014 • Section A.12 data was pulled from March I,2012— March 31 2014 • Section B.6 data was pulled from March I. 2012 — March 31. 2014 and Three pollutant Scans. • Par D data was pulled from March 1.2012 — March 31. 2014 and Three pollutant Scans. If any additional data is required please let me know and I will forward it as soon as possible. Sincerely, DVny Jackson City Mana er 4L J 6OD 1�o1 RECEIVED/DENR/DWR AUG - 1 2014 Water Quality Permitting Section FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba FORM 2A NPDES APPLICATION OVERVIEW Form 2A has been developed in a modular format and consists of a 'Basic Application Information" packet and a "Supplemental Application Information" packet. The Basic Application Information packet is divided into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental Application Information packet. The following items explain which parts of Form 2A you must complete. BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B. Additional Application Information for Applicants with a Design Flow Z 0.1 mgd. All treatment works that have design flows greater than or equal to 0.1 million gallons per day must complete questions B.1 through B.6. C. Certification. All applicants must complete Part C (Certification). SUPPLEMENTAL APPLICATION INFORMATION: D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D (Expanded Effluent Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to provide the information. E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program (or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. F. Industrial User Discharges and RCRAXERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges and RCRAICERCLA Wastes). SIUs are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain exclusions); or b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant; or C. Is designated as an SIU by the control authority. G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer Systems). ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION) Page t of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Permit Renewal Catawba BASIC APPLICATION INFORMATION PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS: All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet. A.1. Facility Information. Facility Name Mount Holly W WTP Mailing Address P.O Box 406 Mount Holly, NC 28120 Contact Person Jonathan Jordan Title Wastewater Treatment Plant Superintendent Telephone Number 704 8274261 Facility Address 7 Broome St Mount Holly NC 28120 (not P.O. Box) A.2. Applicant Information. If the applicant is different from the above, provide the following: Applicant Name City of Mount Holly Mailing Address P.O Box 406 Mount Holly NC 28120 Contact Person Danny Jackson Title City Manager Telephone Number (704) 827-3931 Is the applicant the owner or operator (or both) of the treatment works? E owner E operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. ❑ facility E applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state -issued permits). NPDES N00021156 PSD uIC Other Land Application W00001863 RCRA Other Storm Water NGG110000 A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.). Name Population Served Type of Collection System Ownership City of Mount Holly 13,676 (2010 Census) Separate (sanitary) Municipal Total population served 13,676 RECEIVEDIDENRIDWR � � r Water Quality - Page 2 of 30 Permitting Section FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WVVfP, NCO021156 Renewal I Catawba A.S. Indian Country. a. Is the treatment works located in Indian Country? ❑ Yes ® No b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows through) Indian Country? ❑ Yes ® No A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 121h month of "this year' occurring no more than three months prior to this application submittal. a. Design flow rate 4.0 mgd Two Years Ago Last Year This Year b. Annual average daily flow rate 1.98 2.01 2.09 C. Maximum daily flow rate 6.15 7.90 6.16 A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent contribution (by miles) of each. ® Separate sanitary sewer 100 % ❑ Combined stone and sanitary sewer % A.B. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? ® Yes ❑ No If yes, list how many of each of the following types of discharge points the treatment works uses: I. Discharges of treated effluent ii. Discharges of untreated or partially treated effluent III. Combined sewer overflow points V. Constructed emergency overflows (prior to the headworks) V. Other b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the U.S.? ❑ Yes If yes, provide the following for each surface impoundment: Location: Annual average daily volume discharge to surface impoundment(s) Is discharge ❑ continuous or ❑ intermittent? C. Does the treatment works land -apply treated wastewater? If yes, provide the following for each land application site: Location: Number of acres: X No Yes Annual average daily volume applied to site: mgd Is land application ❑ continuous or ❑ intermittent? d. Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? ❑ Yes mgd ❑ No © No RECEIVED/DENR/DWR AUG - 1 2014 Water Quality Page 3 of 30 Permitting Section FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly VWVfP, NCO021156 Renewal Catawba If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g., tank truck, pipe). If transport is by a party other than the applicant, provide: Transporter Name Mailing Address Contact Person Title Telephone Number ( 1 For each treatment works that receives this discharge, provide the following: Name Mailing Address Contact Person Title Telephone Number ( ) If known, provide the NPDES permit number of the treatment works that receives this discharge Provide the average daily flow rate from the treatment works into the receiving facility. mgd e. Does the treatment works discharge or dispose of its wastewater in a manner not included in A.B. through A.8.d above (e.g., underground percolation, well injection): ❑ Yes ® No If yes, provide the following for each disposal method: Description of method (including location and size of site(s) if applicable): Annual daily volume disposed by this method: Is disposal through this method ❑ continuous or ❑ intermittent? RECEIVED/DENR/DWR AUG - 1 2014 Water Quality PennRtlng Section Page 4 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba WASTEWATER DISCHARGES: If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question A.8.a, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Outfall. a. Outfall number 001 It. Location Mount Holly 28120 (City or town, if applicable) (Zip Code) Gaston North Carolina (County) (State) (Latitude) C. Distance from shore (if applicable) d. Depth below surface (if applicable) e. Average daily flow rate f. Does this ouffall have either an intermittent or a periodic discharge? If yes, provide the following information: Number f times per year discharge occurs: Average duration of each discharge: Average flow per discharge: Months in which discharge occurs: g. Is oudall equipped with a diffuser? A.10. Description of Receiving Waters (Longitude) ft. ft. 2.09 mgd ❑ Yes ® No (go to A.9.g.) ❑ Yes ® No mgd a. Name of receiving water Catawba River b. Name of watershed (if known) Catawba River Basin United Slates Soil Conservation Service 14-digit watershed code (if known): C. Name of State Management/River Basin (if known): Catawba River Basinwide Mot. Plan United States Geological Survey 8-digit hydrologic cataloging unit code (if known): 03050101 d. Critical low flow of receiving stream (if applicable) acute cis chronic cis e. Total hardness of receiving stream at critical low flow (if applicable): mgll of CaCO3 AUG - 1 2014 Water P�S we 5 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba A.11. Description of Treatment a. What level of treatment are provided? Check all that apply. ❑ Primary ® Secondary ❑ Advanced ❑ Other. Describe: b. Indicate the following removal rates (as applicable): Design BOD5 removal or Design CBOD5 removal 90 % Design SS removal 90 % Design P removal % Design N removal % Other % C. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe: Choldration If disinfection is by chlorination is dechlorination used for this burial? ® Yes ❑ No Does the treatment plant have post aeration? ❑ Yes ❑ No A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows In this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart Ouffall number. 001 MAXIMUM DAILY VALUE AVERAGE DAILY VALUE PARAMETER Value Units Value Units Number of Samples pH (Minimum) 6.2 S.U. pH (Ma)imum) 7.2 S.U. Flow Rate 7.904 MGD 2.157 MGD 760 Temperature (Winter) 23 °C 14.2 °C 332 Temperature (Summer) 28 °C 23.1 °C 168 For pH please report a minimum and a maximum daily value MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Cone. Units Conc. Units Numberof METHOD Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN BOD5 33.0 m /L 4.74 1 m /L 499 SM521OB-20 2.0 DEMAND (Report one) CBOD5 FECAL COLIFORM 6000 #100mL 287.76 #100mL 500 SM 9222 D 2.0 TOTAL SUSPENDED SOLIDS (TSS) 33.0 m /L 15.55 mg/L 499 SM 2440 D 2.0 END OF PART A. REFER TO TFE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE Page 6 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba BASIC APPLICATION INFORMATION PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR EQUAL TO 0.1 MGD (100,000 gallons per day). All applicants with a design flow rate 2 0.1 mgd must answer questions 8.1 through B.6. All others go to Part C (Certification). B.I. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration. >10,000 gpd Briefly explain any steps underway or planned to minimize inflow and infiltration. We are currently are performing an Inflow and Infiltration study, at this time a report has not been generated. B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) Please See Attachment II a. The area surrounding the treatment plant, including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include ouffalls from bypass piping, if applicable. c. Each well where wastewater from the treatment plant is injected underground. d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within %mile of the property boundaries of the treatment works, and 2) listed in public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed. I. If the treatment works receives waste that is classed as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail, or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed. B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. Please See Attachment III BA. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? ❑ Yes ® No If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional pages if necessary). Name: Mailing Address: Telephone Number. ( 1 Responsibilities of Contractor: B.S. Scheduled Improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5 for each. (If none, go to question B.6.) a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule. b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies. ❑ Yes ® No Page 7 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NC0021156 Renewal Catawba C. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable). d. Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as applicable. For improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates, as applicable. Indicate dates as accurately as possible. Schedule Actual Completion Implementation Stage MM/DD/YYYY MM/DD/YYYY - Begin Construction I / I l - End Construction I I I l - Begin Discharge I l I l - Attain Operational Level / / / / e. Have appropriate permits/clearances concerning other Federal/State requirements been obtained? ❑ Yes ❑ No Describe briefly: B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY). Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combine sewer overflows in this section. All Information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QAIQC requirements of 40 CFR Part 136 and other appropriate QAIQC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be based on at least three pollutant scans and must be no more than four and on -half years old. Outfall Number: 001 MAXIMUM DAILY AVERAGE DAILY DISCHARGE DISCHARGE ANALYTICAL POLLUTANT METHOD MLIMDL Cone. Units Conc. Units Number of Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA (as N) 7.2 mg/L .397 mglL 315 350.1 0.10 CHLORINE (TOTAL 49 ug1L 26.71 ug/L 499 SM 4500 Cl G 20.0 RESIDUAL, TRC) DISSOLVED OXYGEN 10.6 mg/L 6.5 mg/L 499 SM 4500 OG mg/L TOTAL KJELDAHL NITROGEN (TKN) 24 mg/L 2.88 mg/L 109 351.2 0.60 NITRATE PLUS NITRITE 32 mg/L 16.72 mg1L 109 353.2 0.20 NITROGEN OIL and GREASE 4.9 mg/L 4.7 mglL 3 1664A 4.60 PHOSPHORUS (total) 7.8 mg/L 2.829 mg/L 109 366.1 0.10 TOTAL DISSOLVED SOLIDS (TDS) 490 mil 483.3 mg/L 3 SM 2640 C 10.0 OTHER END OF PART B. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE Page 8 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba BASIC APPLICATION INFORMATION PART C. CERTIFICATION All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: ® Basic Application Information packet Supplemental Application Inforalion packet: ® Part D (Expanded Effluent Testing Data) ® Part E (Toxicity Testing: Biomonitoring Data) ® Part F (Industrial User Discharges and RCRA/CERCLA Wastes) ❑ Part G (Combined Sewer Systems) ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name and official title Rwnv Jackson 9 CrtvAAana Signature N04v�"4 4'. taLj:C�L Telephone number 70044/)827- 9311 Date signed / - 2- L - Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. SEND COMPLETED FORMS TO: NCDENR/ DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Page 9 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly WWTP, NCO021156 PERMIT ACTION REQUESTED: Renewal RIVERBASIN: Catawba SUPPLEMENTAL APPLICATION INFORMATION PART D. EXPANDED EFFLUENT TESTING DATA Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this forth. Al a minimum, effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MLIMDL Conc. Units Mass Units Conc. Units Mass Units Number of Samples METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS. ANTIMONY 0.042 mg/L 0.034 mg/L 12 200.8 0.001 ARSENIC 0.013 mg/L 0.0011 mg/L 12 200.8 0.001 BERYLLIUM <0.0004 mg/L <0.0004 mg/L 3 200.8 0.0004 CADMIUM 0.0010 mg/L 0,0002 mg/L 12 200.8 0.0001 CHROMIUM 0.0074 mg/L 0.0056 mg/L 12 200.8 0.005 COPPER 19.0 mg/L 1.59 mg/L 12 200.8 0.001 LEAD 0.002 mg/L 0.0011 mglL 12 200.8 0.001 MERCURY 15.4 ng/L 6.84 ng/L 27 1631 E 0.600 NICKEL <0.005 mg/L <0.005 mg/L 12 200.8 0.005 SELENIUM 0.005 mg/L 0.0028 mg/L 12 200.8 0.001 SILVER <0.001 mg/L <0.001 mg/L 12 200.8 0.001 THALLIUM <0.0005 mg/L -0.0005 mg/L 3 200.8 0.0005 ZINC 66o mg/L 5.53 mg/L 12 200.8 0.01 CYANIDE <0.01 mg/L <0.01 mg/L 12 10-204-00-1-X 0.01 TOTAL PHENOLIC COMPOUNDS 0.055 mg/L 0.0226 mg/L 9 420.4 0.02 HARDNESS (as CaCO3) 50 mg/L 44.3 mg/L 3 SM 2340 C 10 Use this space (or a separate sheet) to provide information on other metals requested by the permit writer Page 10 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Number Cone. TUnits Mass Units Conc. Units Mass Units Of METHOD Samples VOLATILE ORGANIC COMPOUNDS ACROLEIN <50.0 ug/L <50.0 ug/L 3 624 50.0 ACRYLONITRILE <50.0 ug/L <50.0 ug/L 3 624 50.0 BENZENE <5.0 ug/L <5.0 ug/L 3 624 5.0 BROMOFORM 9.8 ug/L 6.6 ug/L 3 624 5.0 CARBON <5.0 ug/L <5.0 uglL 3 624 5.0 TETRACHLORIDE CHLOROBENZENE <5.0 ug/L <5.0 ug/L 3 624 5.0 CHLORODIBROMO- g uglL 6.23 ug/L 3 624 5.0 METHANE CHLOROETHANE <5.0 uglL <5.0 ug/L 3 624 5.0 2-CHLOROETHYLVINYL <10.0 ug/L <10.0 ug/L 3 624 10.0 ETHER CHLOROFORM <5.0 ug/L <5.0 ug/L 3 624 5.0 DICHLOROBROMO- <5.0 uglL <5.0 ug/L 3 624 5.0 METHANE 1,1-DICHLOROETHANE <5.0 ug/L <5.0 ug/L 3 624 5.0 1,2-DICHLOROETHANE <5.0 ug/L <5.0 uglL 3 624 5.0 TRANS-I,2-DICHLORO- <5.0 ug/L <5.0 ug/L 3 624 5.0 ETHYLENE 1,1-DICHLORO- <5.0 ug/L <5.0 ug/L 3 624 5.0 ETHYLENE 1,2-DICHLOROPROPANE <5.0 ug/L <5.0 ug/L 3 624 5.0 1,3-DICHLORO- <5.0 ug/L <5.0 ug/L 3 624 5.0 PROPYLENE ETHYLBENZENE <5.0 ug/L <5.0 ug/L 3 624 5.0 METHYLBROMIDE <5.0 ug/L <5.0 ug/L 3 624 5.0 METHYLCHLORIDE <5.0 ug/L <5.0 ug/L 3 624 5.0 METHYLENE CHLORIDE <5.0 ug/L <5.0 ug/L 3 624 5.0 1,1,2,2-TETRA- <5.0 ug/L <5.0 ug/L 3 624 5.0 CHLOROETHANE TETRACHLORO- <5.0 ug/L <5.0 ug/L 3 624 5.0 ETHYLENE TOLUENE <5.0 ug/L <5.0 ug/L 3 624 5.0 Page 11 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly WWTP, NCO021156 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) POLLUTANT MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE ANALYTICAL METHOD MLIMDL Conc. Units Mass Units Conc. Units Mass Units Number of Samples 1,1,1 TRICHLOROETHANE <5.0 ug/L <5.0 ug/L 3 624 5.0 1,1,2 TRICHLOROETHANE <5.0 ug/L <5.0 uglL 3 624 5.0 TRICHLOROETHYLENE <5.0 ug/L <5.0 ug/L 3 624 5.0 VINYL CHLORIDE <5.0 ug/L <5.0 ug/L 3 624 5.0 Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer ACID -EXTRACTABLE COMPOUNDS P-CHLORO-M-CRESOL <2.0 ug/L <2.0 ug/L 3 625 2.0 2-CHLOROPHENOL <2.0 ug/L <2.0 ug/L 3 625 2.0 2,4-DICHLOROPHENOL <2.0 ug/L <2.0 ug/L 3 625 2.0 2,4-DIMETHYLPHENOL <2.0 ug/L <2.0 ug/L 3 625 2.0 4,8-DINITRO-O-CRESOL <5.3 ug/L <5.3 ug/L 3 625 2.0 2,4-DINITROPHENOL <5.3 ug/L <5.3 ug/L 3 625 2.0 2-NITROPHENOL <4.1 ug/L <4.1 ug/L 3 625 4.1 4-NITROPHENOL <10.0 ug/L <10.0 uglL 3 625 10.0 PENfACHLOROPHENOL <10.0 ug/L <10.0 ug/L 3 625 10.0 PHENOL <2.0 ug/L <2.0 ug/L 3 625 2.0 2,4,6- TRICHLOROPHENOL <2.0 ug/L <2.0 ug/L 3 625 2.0 Use this space (or a separate sheet) to provide information on other acid -extractable compounds requested by the permit writer BASE -NEUTRAL COMPOUNDS ACENAPHTHENE <2.0 ug/L <2.0 ug/L 3 625 2.0 ACENAPHTHYLENE <2.0 ug/L <2.0 ug/L 3 625 2.0 ANTHRACENE <2.0 ug/L <2.0 ug/L 3 625 2.0 BENZIDINE <10.0 ug/L <2.0 ug/L 3 625 10.0 BENZO(A)ANTHRACENE <2.0 ug/L <2.0 ug/L 3 625 2.0 BENZO(A)PYRENE <2.0 ug/L 4 <2.0 ug/L 3 625 2.0 Page 12 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL ML/MDL Number Conc. Units Mass Units Conc. Units Mass Units of METHOD Samples 3,4 BENZO- FLUORANTHENE <2.0 ug/L <2.0 ug/L 3 625 2.0 BENZO(GHI)PERYLENE <2.0 ug/L <2.0 ug/L 3 625 2.0 BENZO(K) FLUORANTHENE <2.0 ug/L <2.0 uglL 3 625 2.0 BIS (2-CHLOROETHOXY) <2.0 ug/L <2.0 ug/L 3 625 2.0 METHANE BIS (2-CHLOROETHYL)- <2.0 ug/L <2.0 ug/L 3 625 2.0 ETHER BIS (2-CHLOROISO- c2.0 ug/L <2.0 ug/L 3 625 2.0 PROPYL)ETHER BIS (2-ETHYLHEXYL) <10.0 ug/L <10.0 ug/L 3 625 10.0 PHTHALATE 4-BROMOPHENYL <2.0 uglL c2.0 uglL 3 625 2.0 PHENYLETHER BUTYL BENZYL <10.0 ug/L <10.0 ug/L 3 625 10.0 PHTHALATE 2-CHLORO- <2.0 ug/L <2.0 ug/L 3 625 2.0 NAPHTHALENE 4-CHLORPHENYL <2.0 ug/L <2.0 ug/L 3 625 2.0 PHENYL ETHER CHRYSENE <2.0 ug/L <2.0 ug/L 3 625 2.0 DI-N-BUTYL PHTHALATE <10.0 ug/L <10.0 ug/L 3 625 10.0 DI-N-OCTYL PHTHALATE <10.0 ug/L <10.0 ug/L 3 625 10.0 DIBENZO(A,H) <2.0 ug/L <2.0 ug/L 3 625 2.0 ANTHRACENE 1,2-DICHLOROBENZENE <2.0 ug/L <2.0 ug/L 3 625 2.0 1,3-DICHLOROBENZENE <2.0 ug/L <2.0 ug/L 3 625 2.0 1,4-DICHLOROBENZENE <2.0 ug/L <2.0 ug/L 3 625 2.0 3,3-DICHLORO. <10.0 ug/L <10.0 ug/L 3 625 10.0 BENZIDINE DIETHYL PHTHALATE <10.0 ug/L <10.0 ug/L 3 625 10.0 DIMETHYL PHTHALATE <10.0 ug/L <10.0 ug/L 3 625 10.0 2,4-DINITROTOLUENE <4.1 ug/L <4.1 ug/L 3 625 4.1 2,6-DINITROTOLUENE <4.1 ug/L <4.1 ug/L 3 625 4.1 1,2-DIPHENYL- <20 ug/L <2.0 ug/L 3 625 2.0 HYDRAZINE Page 13 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba Oufall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT ANALYTICAL MLIMDL Number Cone. Units Mass Units Conc. Units Mass Units of METHOD Samples FLUORANTHENE <2.0 ug/L <2.0 ug/L 3 625 2.0 FLUORENE <2.0 ug/L <2.0 ug/L 3 625 2.0 HEXACHLOROBENZENE <2.0 ug/L <2.0 ug/L 3 625 2.0 HEXACHLORO- <2.0 ug/L <2.0 ug/L 3 625 2.0 BUTADIENE HEXACHLOROCYCLO- <10.0 ug/L <10.0 ug/L 3 625 10.0 PENTADIENE HEXACHLOROETHANE <2.0 ug/L <2.0 ug/L 3 625 2.0 INDENO(1,2,3-CD) <2,0 ug/L <2.0 ug/L 3 625 2.0 PYRENE ISOPHORONE <2.0 ug/L <2.0 ug/L 3 625 2.0 NAPHTHALENE <2.0 ug/L <2.0 ug/L 3 625 2.0 NITROBENZENE <2.0 ug/L <2.0 ug/L 3 625 2.0 N-NRROSODI-N- <2,0 ug/L <2.0 ug/L 3 625 2.0 PROPYLAMINE N-NITROSODI- <2.0 ug/L <2.0 ug/L 3 625 2.0 METHYLAMINE N-NITROSODI- <2.0 uglL <2.0 ug/L 3 625 2.0 PHENYLAMINE PHENANTHRENE <2.0 ug/L <2.0 ug/L 3 625 2.0 PYRENE <2.0 ug/L <2.0 ug/L 3 625 2.0 1,2,4- <2.0 ug/L <2.0 ug/L 3 625 2.0 TRICHLOROBENZENE Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer Use this space (or a separate sheet) to provide information on other pollutants (e.g., pesticides) requested by the permit writer END OF PART D. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE Page 14 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters. • At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate Qi requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation, if one was conducted. • If you have already submitted any of the information requested in Part E. you need not submit it again. Rather, provide the information requested in question EA for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E. If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. Please See Attachment V ® chronic ❑ acute E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one column Per test (where each species constitutes a lest). Copy this page if more than three tests are being reported. Test number. Test number: Test number: a. Test information. Test Species & lest method number Age at initiation of test Outfall number Dates sample collected Date test started Duration b. Give toxicity test methods followed. Manual title Edition number and year of publication Page number(s) c. Give the samplecollection method(s) used. For multiple grab samples, indicate the number of grab samples used. 24-Hour composite Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorinaflon Page 16 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly WWTP, NCO021156 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba Test number: Test number: Test number: e. Describe the point in the treatment process at which the sample was collected. Sample was collected: I. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static -renewal Flow -through h. Source of dilution water. If laboratory water, specify type: if receiving water, specify source. Laboratory water Receiving water I. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used. Fresh water Salt water I. Give the percentage effluent used for all concentrations in the test series. k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Salinity Temperature Ammonia Dissolved oxygen I. Test Results. Acute: Percent survival in 100% effluent 0 �0 LC50 95% C.I. % % % Control percent survival % % % Other (describe) Page 16 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly WWTP, NCO021156 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba Chronic: NOEC % % % ICu % % % Control percent survival % % % Other (describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? Was reference toxicant test within acceptable bounds? What date was reference toxicant test run (MMIDD/YYYY)? Other (describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes, describe: Ed, Summary of Submitted Biomonitoring Test Information. If you have submitted biomonitodng test information, or information regarding the cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: / / (MM/DD/YYYY) Summary of results: (see instructions) END OF PART E. REFER TO THE APPLICATION OVERVIEW IPAGE 1 TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. Page 18 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. a. Number of non -categorical SIUs. 2 b. Number of ClUs. 2 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the Information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: American and Efrd. INC Mailing Address: P.O. Box 507 Mount Holly, NC 28120 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Process Water. Wash down water. Domestic Wastewater. Boiler/Coolino tower Blowdown. Cooling/Hvac water F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s):Sewing. Embroidery Threads and Industrial yams Raw material(s): Cotton . Polyester. Nylon greige yam. Dves and auxiliary chemicals F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 53T006.8 gpd (X continuous or intermittent) b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 43,541.1 gpd (X continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 410 Textile Page 19 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly WINTP, NCO021156 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba F.B. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? ® Yes (Complete F.13 through F.15.) ❑ No F.13. Waste Origin. Describe the site and type of facility at which the CERCLAIRCRAor other remedial waste originates (or is excepted to origniate in the next five years). The Jadco-Hughes Site located at 760 Cason St Belmont NC was a former solvent reclamation and storage facility that was closed in 1975 This site is does not have a IUP but the City has an agreement that allows them to discharge a daily max of 0.075 MGD to the POTW F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) Please see attachment VI F.15. Waste Treatment a. Is this waste treated (or will be treated) prior to entering the treatment works? ® Yes ❑ No If yes, describe the treatment (provide information about the removal efficiency): The untreated ground water is aerated in a 18,700 gallon equalization and Passed through a 1900 LB activated carbon gas phase adsorber b. Is the discharge (or will the discharge be) continuous or intermittent? ® Continuous ❑ Intermittent If intermittent, describe discharge schedule. Page 20 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities? ® Yes (complete F.13 through F, 15.) ❑ No F.13. Waste Origin. Describe the site and type of facility at which the CERCLAIRCRA/or other remedial waste originates (or is excepted to ongniate in the next five years). Triangle Texaco is located at 201 N. Main St. Mount Holly NC and the site of a Environmental Remediation of a former leaking UST site. The consulting company is awaiting approval from the state to proceed at this time. The estimated time to start operation is September 2014. F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known. (Attach additional sheets if necessary.) Please see attachment VII FA 5. Waste Treatment a. Is this waste treated (or will be treated) prior to entering the treatment works? ® Yes ❑ No If yes, describe the treatment (provide information about the removal efficiency): The around water is Pumped from multiple wells and sent through a air stripper. b. Is the discharge (or will the discharge be) continuous or intermittent? ® Continuous ❑ Intermittent If intermittent, describe discharge schedule. Page 21 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly WWTP, NCO021156 GENERAL INFORMATION: PERMIT ACTION REQUESTED: RIVER BASIN: Renewal Catawba F.I. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. C. Number of non -categorical SIUs. 2 d. Number of CIUs. 2 SIGNIFICANT INDUSTRIAL USER INFORMATION: the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and the Information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Mailing Address: Mount Holly NC 28120 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Process water, wash down water, domestic and recycled wastewater cooling water, Boiledcoolino tower blowdown and HVAC water. F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Airlaid non wovens for feminine hygiene Products, speciality wipes. na kins and incontinence Products Raw material(s): Wood pulp. Biocomoonent synthetic fiber, synthetic binders F.6. Flow Rate. C. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 29,743.0 gpd (X continuous or intermittent) d. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 57.736.4 gpd (X continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? Page 22 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly WUVfP, NCO021156 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba F.S. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. Page 23 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the Information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Clariant Corporation Mailing Address: 625 E. Catawba AVE Mount Holly NC 28120 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Process water, Domestic wastewater, Boiler/Cooling tower blowdown and stormwater. F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Specialty Chemicals (200t) including surface-active agents and DEET Raw material(s): Alcohol Oils Soaps Acids F.6. Flow Rate. e. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 60.332,5 gpd (X continuous or intermittent) f. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 44.776.4 gpd (X continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 40 CFR 414 & 455 Page 24 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly VVVVTP, NCO021156 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. Page 25 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWfP, NCO021156 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following Information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Daimler Trucks North America (Mount Holly) Mailing Address: 1800 North Main St Mount Holly NC 28120 FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Process Water. Wash down water. Domestic Wastewater. Boiler/Cooling tower Blowdown. Cooling/Hvac water. HVAC Water F.S. Principal Product's) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): M2 Freightliner Trucks Raw material(s): Aluminum, steel, acids, bases, organic solvents, and organic paints F.6. Flow Rate. g. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 12,280.2 gpd (X continuous or intermittent) h. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flaw discharged into the collection system in gallons per day (gpd) and whether the discharge is continuous or intermittent. 38, 048.6 gpd (X continuous or intermittent) F.7. Pretreatment Standards. Indicate whether the SlU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards, which category and subcategory? 40 CFR 413 Page 26 of 30 FACILITY NAME AND PERMIT NUMBER: Mount Holly WWTP, NCO021156 PERMIT ACTION REQUESTED: Renewal RIVER BASIN: Catawba F.S. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g., upsets, interference) at the treatment works in the past three years? ❑ Yes ® No If yes, describe each episode. END OF PART F. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE Page 27 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART G. COMBINED SEWER SYSTEMS If the treatment works has a combined sewer system, complete Part G. GA. System Map. Provide a map indicating the following: (may be included with Basic Application Information) a. All CSO discharge points. b. Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and outstanding natural resource waters). C. Waters that support threatened and endangered species potentially affected by CSOs. G.2. System Diagram. Provide a diagram, either in the map provided in G.1 or on a separate drawing, of the combined sewer collection system that includes the following information. a. Location of major sewer trunk lines, both combined and separate sanitary. b. Locations of points where separate sanitary sewers feed into the combined sewer system. C. Locations of in -line and off-line storage structures. d. Locations of flow -regulating devices. e. Locations of pump stations. CSO OUTFALLS: Complete questions G.3 through G.6 once for each CSO discharee point. G.3. Description of Outfall. a. Outfall number b. Location (City or town, if applicable) (Zip Code) (County) (State) (Latitude) (Longitude) C. Distance from shore (if applicable) ft. d. Depth below surface (if applicable) ft. e. Which of the following were monitored during the last year for this CSO? ❑ Rainfall ❑ CSO pollutant concentrations ❑ CSO frequency ❑ CSO flow volume ❑ Receiving water quality f. How many storm events were monitored during the last year? GA. CSO Events. a. Give the number of CSO events in the last year. events (❑ actual or ❑ approx.) b. Give the average duration per CSO event. hours (❑ actual or ❑ approx.) Page 28 of 30 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Mount Holly WWTP, NCO021156 Renewal Catawba C. Give the average volume per CSO event. million gallons (❑ actual or ❑ approx.) d. Give the minimum rainfall that caused a CSO event in the last year Inches of rainfall G.S. Description of Receiving Waters. a. Name of receiving water: b. Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code (if known): C. Name of State Management/River Basin: United States Geological Survey B-digit hydrologic cataloging unit code if known): G.B. CSO Operations. Describe any known water quality impacts on the receiving water caused by this CSO (e.g., permanent or intermittent beach closings, permanent or intermittent shell fish bed closings, fish kills, fish advisories, other recreational loss, or violation of any applicable Slate water quality standard). END OF PART G. REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. Page 29 of 30 Additional information, if provided, will appear on the following pages. I NPDES FORM 2A Additional Information ATTACHMENT I Sludge Management Plan MT. HOLLY SLUDGE SLUDGE MANAGEMENT PLAN Sludge is wasted to two 750,000 gallon holding tanks that serve as storage and aeration of biosolids.These tanks are frequently decanted to remove excess water and to thicken sludge,generally to about 3% concentration. Synagro is the contracted sludge hauler that delivers the sludge to the farmers where it is land applied. The sludge is processed in the same tanks for vector reduction and pathogen destruction.The sludge will be analyzed for complete digestion and lime stabilized when needed before hauling. The city holds land application permit # WQ 0001863 which includes the approved land application sites. SITE SUMMARY City of Mt Holly Mt. Holly. NC Site ID: NC-GA-41 Owners Name: Greg Springs Address: 427 S. Main St Mt Holly NC 28120 Phone: 704-678-0000 4611 Operator: Same as above Estimated Total Applicable Fields Acres Acres Predominant Latitude & Cron(s) Slone M Soil Series Lonaitude 01 6.8 6.8 Fescue 2-8 LdB2 Lloyd 35 17 45 N 81 01 55 W 06 15.2 14.3 Fescue 2-8 I-d B2 Lloyd 351751 N 81 01 50 W 09 17.0 13.5 Fescue 2-8 Ld B2 Lloyd 35 17 39 N 81 01 53 W 10 20.7 17.5 Fescue 2-8 LdB2 Lloyd 35 17 48 N 81 01 37 W 14 12.5 9.7 Fescue 2-8 LdB2 Lloyd 35 17 42 N 1810142 W TOTALS 72.2 61.8 Notes: Date: 03/09M 2 The compliance boundary is established at either 250 feet from the residuals application area or 50 feet within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance ,boundary and the perimeter of the residuals application area. SITE SUMMARY City of Mt Holly Mt. Holly. NC Site ID: NC-GA-44 Owners Name: George Bennett Allen (Field 01) Address: 2552 Lincointon Hwy Cherryville, NC 28021 Phone: 704435-5345 (H) 704-691-9497 (cell) Operator: Same Estimated Total Applicable Fields Acres Acres R-Anell Housing Group (Fields 02 & 03) 235 Anthony Grove Rd Crouse, NC 28033 704-445-9610 George Bennett Allen Predominant Latitude & Crne(sl Slnne f%l Snil Series Lnnnihirlp 1 10.0 6.9 Fescue 6 - 15 WeD Wedowee 35 23 59 N 81 19 48 W 2 18.9 18.9 Fescue 6 -15 ApB Appling 35 23 52 N 81 19 31 W 3 40.0 37.5 Fescue 2-8 CdB2 Cecil 35 23 41 N 8119 35 W TOTALS 68.9 63.3 Notes: Date: 03/09/12 The compliance boundary is established at either 250 feet from the residuals application area or 50 feet within the property boundary, whichever is closest to the application area. The review boundary Is established midway between the compliance boundary and the perimeter of the residuals application area. Site ID: Owners Name: SITE SUMMARY NC-LT-43 Gary Duckworth City of Mt Holly Mt. Holly. NC Address: 857 S. Hwy 16 Stanley, NC 28164 Phone: 704-827-9205 (home) 704-996-0849 (cell) Operator: Total Fields Acres Same as above Estimated Applicable Acres Predominant Latitude & Crnnisl Slnne 101M Snil Series Lnnnituda 01 13.6 11.2 Fescue 2-8 CeB2 Cecil 35 25 30 N 80 59 50 W 02 22.3 21.0 Fescue 2-8 CeB2 Cecil 35 25 35 N 80 59 46 W 03 11.0 10.0 Fescue 2-8 CeB2 Cecil 35 25 47 N 80 59 56 W 04 15.0 6.0 Fescue 8 -15 PeC2 Pacolet 35 25 36 N 80 59 41 W TOTALS 61.9 48.2 Notes: Date: 03/09/12 The compliance boundary is established at either 250 feet from the residuals application area or 50 feet within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. SITE SUMMARY City of Mount Holly WQ0001863 Site ID: NC-LT-46 Owner: Tony Jones Address: 1418 Nature Preserve Rd Denver, NC 28037 Phone: 704A83-1600 Operator: Same Lincoln Co, Estimated RYE -based Predominant Latitude/ Applicable Annual PAN Soil Series Longitude Klalda Ar_rAA Crnntal 11 RIACIVRI hnan iinitl in M R1 1 11.8 Fescue ha 209 Cecil CeB2 35 24 32 N 81 02 27 W 2 45.2 Fescue (pasture) 209 Cecil CeB2 35 24 42 N 810206 W 3 9.9 Fescue ha 209 Cecil Ce82 35 24 22 N 81 02 51 4 19.4 Fescue (pasture) 209 Cecil CeB2 35 24 29 N 8102 07 W 5 7.9 Fescue ha 176 Lloyd LdC2 35 24 56 N 810152 W 6 5.4 Fescue ha 188 Pacolet PeB2 35 24 50 N 810050 W 7 7.0 Fescue ha 188 Pacolet PeB2 35 26 35 N 810029 W 8 6.6 Fescue ha 209 Cecil CeB2 35 24 21 N 8102 28 roracs 113.2 Notes: Date: 12 O113 he compliance boundary is established at either 250 feet from the residuals pplication area or 50 feet within the property boundary, whichever is closest to the pplication area. The review boundary is established midway between the ompliance boundary and the perimeter of the residuals application area. SITE SUMMARY City of Mt Holly Mt. Holly. NC Site ID: NC-MG-37 Owners Name: Dean Stewart Connell Address: 10812 Rozzelles Ferry Rd Charlotte NC 28214 Phone: 704-737-8796 Operator: Same as above Estimated Total Applicable Fields Acres Acres X�jy jy6Mj#-Sa-P 63�/ 76� '- t3� - (M*5 cow ) Predominant Latitude & Cron(s) Slone M Soil Series Lonaitude 01 37.5 20.7 Fescue 2 - 8 Ce132 Cecil 35 17 50 N 180 59 22 W TOTALS 37.5 20.7 Notes: Date: 03/09/12 The compliance boundary is established at either 250 feet from the residuals application area or 50 feet within the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. ATTACHMENT II Topographical M"Fil" 2& .�` ..a;. —� PIPELINE_ -- City of Mount Holly Mount Holly WWTP Latitude: 350 1555" N State Grid/Ouad: F 14 SE / Mt. Hoily, NC Loneitude: Sl' 00' 35" W Permitted Flow: 4.0 NIGD Receivins Stream: Catawba River Drainage Basin: Catawba Rover Basin Stream Class: M-1V C Sub -Basin: J3-09 c 7,'. j 4 4t � �F bs[a_J'1. s 'eam.5a Ye H ,27 All Se age,' pr POsa r Facility r r. m�.0 SF Location N'; not to scale ��01"tl2 NPDES Permit No. NC002115 Gaston County ATTACHMENT III Plant Flow Diagram Influent, excluding AJZF Mille X em ire o MOUNT HOLLY WASTEWATER TREATMENT PLANT line -------- L.- A-.-.-.-.L.-.- r- N co C .N •C 4 C 'N c+� m m m C O � O C O Q N Q N Q Clarifier 0.675 MG S ` Land ��K pTicailton Sites ^------------------- Sluoe - - - - - - - i Dechlorinafion - - -0 IC hIorin KSulfur Dioxide) Clarifier 0.675 MG Chlorin Contac Digester Efflue Discharge To Catawba River ATTACHMENT IV Effluent Pollutant Scan's 'Client: City of Mount Holly Laboratory ID: PG23072-001 ~` Description: EFFLUENT P Matrix: Aqueous Date Sampled:07/23/2014 0820 Date Received:07/23/2014 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 350.1 (Ammonia - N ) 350.1 1 08/01/2014 1715 BLB 08/01/2014 1038 52987 1 (Hardness (to) SM 234OC-2011 1 08/04/2014 1653 BWS 53239 1 (Nitrate-Nitr) 353.2 10 08/01/2014 1654 MJI 52990 1 (Phosphorus) 365.1 5 07/24/2014 2000 BLB 07/24/2014 1030 52255 1 (TDS) SM 254OC-2011 1 07/24/2014 0944 SDS 52244 CAS Analytical Parameter Number Method Result Q PQL Units Run Ammonia - N (phonate) 350.1 0.34 0.10 mg/L 1 Hardness (total) SM 2340C-20 36 10 mg/L 1 Nitrate -Nitrite - N 353.2 17 0.20 mg/L 1 Phosphorus TDS 7723-14-0 365.1 2.4 0.050 mg/L 1 SM 264OC-20 580 10 mg/L 1 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 07/30/20141339 DRB1 07/25/20141534 52358 CAS Analytical ammeter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug/L 1 208-96-8 625 ND 2.0 ug/L 1 ,;/Acenaphthylene Anthracene Benzidine 120-12-7 625 ND 2.0 ug/L 1 92-87-5 625 ND 10 ug/L 1 Benzo(a)anthracene Benzo(a)pyrene 56-55-3 625 ND 2.0 ug/L 1 ✓� 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene J 205-99-2 625 ND 2.0 ug/L 1 Benzo(g,h,i)perylene d/ Benzo(k)fluoranthene 191-24-2 625 ND 2.0 ug/L 1 Y 207-08-9 625 ND 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 ug/L 1 Butyl benzyl phthalate -0/4-Chloro-3-methyl 85-68-7 625 ND 10 ug/L 1 phenol 59-50-7 625 ND 2.0 ug/L 1 <r bis(2-Chloroethoxy)methane ✓ bis(2-Chloroethyl)ether 111-91-1 625 ND 2.0 tig/L 1 k✓ bis(2-Chloroisopropyl)ether 111-44-4 108-60-1 625 ND 2.0 ug/L 1 J/2-Chloronaphthalene 625 ND 2.0 ug/L 1 ✓ 2-Chlorophenol 91-58-7 625 ND 2.0 ug/L 1 95-57-8 625 ND 2.0 ug/L 1 ✓ 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug/L 1 JChrysene Dibenzo(a,h)anthracene 218-01-9 625 ND 2.0 ug/L 1 1,2-Dichlorobenzene 53-70-3 625 ND 2.0 ug/L 1 95-50-1 625 ND 2.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug/L 1 ✓ 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 ug/L 1 ve3,3'-Dichlorobenzidine 91-94-1 625 ND 10 ug/L 1 PQL = Practical quanbtation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a ' W' Shealy Environmental Services, Inc. Page: 5 Of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: PG23072-001 Description: EFFLUENT Matrix: Aqueous Date Sampled:07/23/2014 0820 Date Received:0712312014 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 07/30/20141339 DRB1 07/25/20141534 52358 CAS Analytical f Parameter Number Method Result Q - PQL Units_ Run 2,4-Dichlorophenol 120-83-2 625 NO 2.0 ug/L 1 ✓ Diethylphthalate 84-66-2 625 NO 10 ug/L 1 1 Dimethyl phthalate 131-11-3 625 NO 10 ug/L 1 2,4-Dlmethylphenol 105-67-9 625 NO 2.0 ug/L 1 v/ i-n-butyl phthalate 84-74-2 625 NO 10 ug/L 1 V 4,6-Dinitro-2-methylphenol v'2,4-Dinitrophenol 534-52-1 625 NO 10 ug/L 1 ✓2,4-Dinitrotoluene 51-28-5 625 NO 10 ug/L 1 121-14-2 625 NO 4.0 ug/L 1 .0(2,6-Dinitrotoluene 606-20-2 625 NO 4.0 ug/L 1 ✓ Di-n-octylphthalate 117-84-0 625 NO 10 ug/L 1 1,2-Dipheny[hydrazine(as azobenzene) 103-33-3 625 NO 2.0 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 NO 10 ug/L 1 I✓ Fluoranthene 206-44-0 625 NO 2.0 ug/L 1 se Fluorene 86-73-7 625 NO 2.0 ug/L 1 ✓ Hexachlorobenzene 118-74-1 625 NO 2.0 ug/L 1 ✓ Hexachlorobutadiene 87.68-3 625 NO 2.0 ug/L, 1 ✓ Hexachlorocyclopentadiene 77-47-4 625 NO 10 ug/L 1 ✓ Hexachloroethane 67-72-1 625 NO 2.0 ug/L 1 ✓ Indeno(1,2,3-c,d)pyrene 193-39-5 625 NO 2.0 ug/L 1 Isophorone 78-59-1 625 NO 2.0 ug/L 1 J Naphthalene 91-20-3 625 NO 2.0 ug/L 1 Nitrobenzene 98-95-3 625 NO 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 NO 4.0 ug/L 1 ✓ 4-Nitrophenol 100-02-7 625 NO 10 ug/L 1 N-Nitrosodimethylamine 62-75-9 625 NO 2.0 ug/L 1 .� N-Nitrosodi-n-propylamine 621-64-7 625 NO 2.0 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 NO 2.0 ug/L 1 Pentachlorophenol 87-86-5 625 NO 10 ug/L 1 ✓ Phenanthrene 85-01-8 625 NO 2.0 ug/L 1 ✓ Phenol 108-95-2 625 NO 2.0 ug/L 1 ✓ Pyrene 129-00-0 625 NO 2.0 ug/L 1 -/1,2,4-Trichlorobenzene 120-82-1 625 NO 2.0 ug/L 1 V 2.4,6-Trichlorophenol 88-06-2 625 NO 2.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Ouentitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a `W" Shealy Environmental Services, Inc. Page: 6 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: PG23072-001 Description: EFFLUENT Matrix: Aqueous Date Sampled:07/23/2014 0820 Date Received:0712312014 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 77 37-129 2-Fluorophenol 72 24-127 Nitrobenzene-d5 70 38-127 Phenol-d5 76 28-128 Terphenyl-d 14 45 10-148 2,4,6-Tdbromophenol 88 41-144 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 07/25/2014 1506 BNW 07/25/2014 0948 52343 CAS Analytical Parameter Number Method Result 0 PQL Units Run Antimony 7440-36-0 200.8 0.028 0.001 mg/L 1 Arsenic 7440.38-2 200.8 0.001 0.001 mg/L 1 Beryllium 7440-41-7 200.8 ND 0.0004 mg/L 1 Cadmium 7440-43-9 200.8 ND 0.0001 mg/L 1 Chromium 7440-47-3 200.8 0.0072 0.005 mg/L 1 Copper 7440.50-8 200.8 0.019 0.001 mg/L 1 Lead 7439-92-1 200.8 ND 0.001 mg/L 1 Nickel 11 Selenium 7440-02-0 200.8 ND 0.005 mg/L 1 7782.49-2 200.8 0.0031 0.001 mg/L 1 v/Silver 7440-22-4 200.8 ND 0.001 mg/L 1 Thallium 7440-28-0 200.8 ND 0.0005 mg/L 1 J Zinc 7440-66-6 200.8 0.035 0.01 mg/L 1 PQL = Practical quantitation limit 8 = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W" Shealy Environmental Services. Inc. Page: 7 of 9 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: PG23072-002 �.. �►: Description: EFFLUENT Matrix: Aqueous Date Sampled:07/2312014 0830 Date Received:07/2312014 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- 1 07/30/2014 1512 NCM 07/30/2014 1000 52698 1 (Phenolics) 420.4 1 07/27/2014 0213 TAF 07/26/2014 1030 52425 1 (HEM (oil and) 1664B 1 07/29/2014 1000 JDW 52595 CAS Analytical Parameter Number Method Result Q PQL Units Run Cyanide - Total 57-12-5 SM 4500-CN ND 0.010 mg/L 1 Phenolics 420.4 ND 0.020 mg/L 1 HEM (oil and grease) 1664B ND 4.0 mg/L 1 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 08/01/2014 0904 PMM2 52948 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein ./Acrylonitrile 107-02-8 624 ND 50 ug/L 1 ✓ Benzene 107-13-1 624 ND 50 ug/L 1 71-43-2 624 ND 5.0 ug/L 1 V Bromodichloromethane 75-27-4 624 ND 5.0 ug/L 1 Bromoform 75-25-2 624 5.1 5.0 ug/L 1 /✓ romomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug/L 1 Carbon tetrachloride 56-23-5 624 ND - 5.0 ug/L 1 ✓ ,Chlorobenzene 108-90-7 624 ND 5.0 ug/L 1 /� Chloroethane 75-00-3 624 ND 5.0 ug/L 1 1d 2-Chloroethylvinylether 110-75-8 624 ND 10 u9 /L 1 hloroform 2chloromethane 67-66-3 624 ND 5.0 ug/L 1 (Methyl chloride) 74-87-3 624 ND 5.0 ug/L 1 /Dibromochloromethane vf1,1-Dichloroethane 124-48-1 624 10 5.0 ug/L 1 1,2-Dichloroethane 75-34-3 624 ND 5.0 ug/L 1 107-06-2 624 ND 5.0 ug/L 1 XJ-Dichloroethene 75-35-4 624 ND 5.0 ug/L 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 ug/L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug/L 1 cls-1,3-Dichloropropene ✓trans-1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug/L 1 Ethylbenzene 10061-02-6 624 ND 5.0 ug/L 1 Methylene chloride 100-41-4 624 ND 5.0 ug/L 1 75-09-2 624 ND 5.0 ug/L 1 1,1,2,2-Tetrachloroethane Tetrachloroethene 79-34-5 624 ND 5.0 ug/L 1 ✓ Toluene 127-18-4 624 ND 5.0 ug/L 1 ✓1,1,1-Trcchooroethane 108-88-3 624 ND 5.0 ug/L 1 71-55-6 624 ND 5.0 ug/L 1 1,1,2-Trichloroethane e/Trichloroethene 79-00-5 624 ND 5.0 ug/L 1 79-01-6 624 ND 5.0 ug/L 1 FUL = Nracocal quantitatlon limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all sod sample analysis are reported on a dry weight basis unless flagged with a "W" Shealy Environmental Services, Inc. Page: 8 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: PG23072-002 Description: EFFLUENT Matrix: Aqueous Date Sampled:0712312014 0830 Date Received:07123/2014 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 08/01/2014 0904 PMM2 52948 CAS Analytical Parameter Number Method Result Q PQL Units Run Vinyl chloride 75-01-4 624 ND 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 105 70-130 Bromofluorobenzene 112 70-130 Toluene-d8 116 70-130 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitathon of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' Shealy Environmental Services, Inc. Page: 9 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Mount Holly Lot Number: OA29039 Sample Number Sample ID Matrix Date Sampled Date Received 001 EFFLUENT Aqueous 01/29/2013 0810 01/29/2013 002 EFFLUENT Aqueous 01/29/2013 0820 01/29/2013 (2 samples) Shealy Environmental Services, Inc. Page: 3 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary City of Mount Holly Lot Number: OA29039 Sample Sample ID Matrix Parameter Method Result 0 Units Page 001 EFFLUENT Aqueous Ammonia - N (phenate) 350.1 0.51 mg/L 5 001 EFFLUENT Aqueous Hardness (total) SM 2340C- 41 mg/L 5 001 EFFLUENT Aqueous Nitrate -Nitrite - N 353.2 17 mg/L 5 001 EFFLUENT Aqueous Phosphorus 365.1 2.4 S mg/L 5 001 EFFLUENT Aqueous TDS SM 2540C- 490 mg/L 5 001 EFFLUENT Aqueous TKN 351.2 1.6 mg/L 5 001 EFFLUENT Aqueous TRC SM 4500-CL 0.055 mg/L 5 001 EFFLUENT Aqueous Antimony 200.8 0.03 mg/L 7 001 EFFLUENT Aqueous Copper 200.8 0.014 mg/L 7 001 EFFLUENT Aqueous Selenium 200.8 0.0015 mg/L 7 001 EFFLUENT Aqueous Zinc 200.8 0.041 mg/L 7 (11 detections) Shealy Environmental Services, Inc. Page: 4 of 9 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: OA29039-001 Description: EFFLUENT Matrix: Aqueous Date Sampled:01/2912013 0810 Date Received:0112912013 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM4500-NH3 (Ammonia - N ) 350.1 1 02/08/2013 1247 MML 02/07/2013 1030 13542 1 (Hardness (to) SM 2340C- 1 02/05/2013 1400 KMB 13390 1 (Nitrate-Nitr) 353.2 25 02/04/2013 2055 HBB 13237 1 (Phosphorus) 365.1 10 02/05/2013 1713 MML 01/31/2013 2331 13025 1 (TDS) SM 254OC-2011 1 02/04/2013 0827 KES 13160 1 351.4 (TKN) 351.2 1 02/04/2013 1157 MML 02/01/2013 1315 13090 1 (TRC) SM 4500-CL G-2011 1 01/30/2013 1930 HBB CAS Analytical Parameter Number Method Result Q PQL Units Run Ammonia - N (phonate) 350.1 0.51 0.10 mg/L 1 Hardness (total) SM 2340C-2011 41 10 mg/L 1 Nitrate -Nitrite - N 353.2 17 0.60 mg/L 1 Phosphorus 7723-14-0 366.1 2.4 S 0.10 mg/L 1 TDS SM 254OC-2011 490 10 mg/L 1 TKN 351.2 1.6 0.50 mg/L 1 TRC SM 4500-CL G-2011 0.055 0.050 mg/L 1 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 2 02/07/20131814 RBH 01/30/20131229 12838 2 625 625 2 02/07/20131911 JRG 02/04/20131230 13178 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug/L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug/L 1 Anthracene 120-12-7 625 ND 2.0 ug/L 1 Benzidine 92-87-5 625 ND 10 ug/L 1 Benzo(a)anthracene 56-55-3 625 ND 2.0 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 2.0 ug/L 1 f Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug/L 1 Benzo(k)fluoranthene 207-08-9 625 ND 2.0 ug/L 1 .� 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 ug/L 1 Butyl benzyl phthalate 85-68-7 625 ND 10 uglL 1 -P 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 2.0 ug/L 1 -- bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 ug/L 1 -'-bis(2-Chloroisopropyl)ether 108-60-1 625 ND 2.0 ug/L 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 ug/L 1 -�- 2-Chlorophenol 95-57-8 625 ND 2.0 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug/L 1 Chrysene 218-01-9 625 ND 2.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure ND = Not detected at or above the PQL J = Estimated result < PQL and > MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a ' W' S = MS/MSD failure Shealy Environmental Services. Inc. Page: 5 of 9 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Cliont: City of Mount Holly Laboratory ID: OA29039-001 Description: EFFLUENT Matrix: Aqueous Date Sampled:01/29/2013 0810 Date Received:0112912013 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 2 02/07/20131814 RBH 01/30/20131229 12838 2 625 625 2 02/07/20131911 JRG 02/04/20131230 13178 CAS Analytical Parameter Number Method Result Q PQL Units Run Dibenzo(a,h)anthracene 53-70-3 625 ND 2.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 625 ND 2.0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 ug/L 2 2,4-Dichlorophenol 120-83-2 625 ND 2.0 ug/L 1 Diethylphthalate 84-66-2 625 ND 10 ug/L 1 Dimethyl phthalate 131-11-3 625 ND 10 ug/L 1 - f 2,4-Dimethylphenol 105-67-9 625 ND L 2.0 ug/L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug/L 1 it 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug/L 1 + 2,4-Dinitrophenol 51-28-5 625 ND 10 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.1 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.1 ug/L 1 Di-n-octylphthalate 117-84-0 625 ND 10 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 ND 10 ug/L 1 Fluoranthene 206-44-0 625 ND 2.0 ug/L 1 Fluorene 86-73-7 625 ND 2.0 ug/L 1 Hexachlorobenzene 118-74-1 625 ND 2.0 ug/L 1 Hexachlorobutadiene 87-68-3 625 ND 2.0 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 10 ug/L 1 Hexachloroethane 67-72-1 625 ND 2.0 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug/L 1 Isophorone 78-59-1 625 ND 2.0 ug/L 1 Naphthalene 91-20-3 625 ND 2.0 ug/L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 ND 4.1 ug/L 1 �- 4-Nitrophenol 100-02-7 625 ND 10 ug/L 1 + N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug/L 1 Pentachlorophenol 87-86-5 625 ND 10 ug/L 1 Phenanthrene 85-01-8 625 ND 2.0 ug/L 1 + Phenol 108-95-2 625 ND 2.0 ug/L 1 Pyrene 129-00-0 625 ND 2.0 ug/L 1 1,2,4-Tiichlorobenzene 120-82-1 625 ND 2.0 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quandtation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MSIMSD failure Shealy Environmental Services, Inc. Page: 6 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: OA29039-001 Description: EFFLUENT Matrix: Aqueous Date Sampled:01129/2013 0810 Date Received:01/2912013 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits 2,4,6-Tribromophenol 77 41-144 66 41-144 Phenol-d5 60 28-128 54 28-128 Nitrobenzene-d5 61 38-127 54 38-127 2-Fluorobiphenyl 60 37-129 53 37-129 2-Fluorophenol 58 24-127 53 24-127 Terphenyl-d14 53 10-148 29 10-148 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 02/01/2013 0349 CDF 01/31/2013 1100 12917 2 200.2 200.8 1 02/02/20131453 BNW 01/31/20131100 12917 CAS Analytical Parameter Number Method Result Q PQL Units Run Antimony 7440-36-0 200.8 0.03 0.001 mg/L 1 Arsenic 7440-38-2 200.8 ND 0.001 mg/L 2 Beryllium 7440-41-7 200.8 ND 0.0004 mg/L 1 Cadmium 7440-43-9 200.8 ND 0.0001 mg/L 1 Chromium 7440-47-3 200.8 ND 0.005 mg/L 1 Copper 7440-50-8 200.8 0.014 0.001 mg/L 1 Lead 7439-92-1 200.8 ND 0.001 mg/L 1 Nickel 7440-02-0 200.8 ND 0.005 mg/L 1 Selenium 7782-49-2 200.8 0.0016 0.001 mg/L 2 Silver 7440-22-4 200.8 ND 0.001 mg/L 1 Thallium 7440-28-0 200.8 ND 0.0005 mg/L 1 Zinc 7440-66-6 200.8 0.041 0.01 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCSILCSD failure Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MSIMSD failure Shealy Environmental Services. Inc. Page: 7 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: OA29039-002 Description: EFFLUENT Matrix: Aqueous Date Sampled:01129/2013 0820 Date Received:0112912013 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide - To) SM 4500-CN 1 02/01/2013 0110 MML 01/31/2013 1628 12991 1 (Phenolics) 420.4 1 02/07/2013 2141 HBB 02/07/2013 1330 13439 1 (HEM (oil and) 1664B 1 02/04/2013 1057 AJK 13185 CAS Analytical Parameter Number Method Result Q PQL Units Run Cyanide - Total 57-13M 4500-CN E-2011 ND 0.010 mg/L 1 Phenolics 420.4 ND 0.020 mg/L 1 HEM (oil and grease) 1664B ND 4.7 mg/L 1 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 02/05/2013 0317 JAC 13242 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug/L 1 Acrylonitrile 107-13-1 624 ND 50 ug/L 1 Benzene 71-43-2 624 ND 5.0 ug/L 1 +Bromodichioromethane 75-27-4 624 ND 5.0 ug/L 1 Bromoform 75-25-2 624 ND 5.0 ug/L 1 -� Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug/L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 ug/L 1 Chlorobenzene 108-90-7 624 ND 5.0 ug/L 1 Chloroethane 75-00-3 624 ND 5.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624 ND 10 ug/L 1 Chloroform 67-66-3 624 ND 5.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug/L 1 Dibromochloromethane 124-48-1 624 ND 5.0 ug/L 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 ug/L 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 ug/L 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 ug/L 1 trans-1,2-Dichloroethene 156-60-5 624 ND 5.0 ug/L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug/L 1 �- trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 ug/L 1 Ethylbenzene 100-41-4 624 ND 5.0 ug/L 1 Methylene chloride 75-09-2 624 ND 5.0 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug/L 1 Tetrachloroethene 127-18-4 624 ND 5.0 ug/L 1 Toluene 108-88-3 624 ND 5.0 ug/L 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug/L 1 Trichloroethene 79-01-6 624 ND 5.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCSILCSD failure Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a' W' S = MS/MSD failure Shealy Environmental Services, Inc. Page: 8 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Meat: City of Mount Holly Laboratory ID: OA29039-002 Description: EFFLUENT Matrix: Aqueous Date Sampled:01/2912013 0820 Date Received: 0 112912013 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 02/05/2013 0317 JAC 13242 CAS Analytical Parameter Number Method Result Q PQL Units Run Vinyl chloride 75-01-4 624 ND 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 90 52-138 Bromofluorobenzene 104 70-147 Toluene-d8 96 76-125 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCSILCSD failure Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure Shealy Environmental Services, Inc. Page: 9 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Mount Holly Lot Number: NF14071 Sample Number Sample ID Matrix Date Sampled Date Received 001 Effluent Aqueous 06/14/2012 0810 06/14/2012 002 Effluent Aqueous 06/14/2012 0815 06/14/2012 (2 samples) Shealy Environmental Services, Inc. Page: 3 of 9 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary City of Mount Holly Lot Number: NF14071 Sample Sample ID Matrix Parameter Method Result 0 Units Page 001 Effluent Aqueous Ammonia - N (phenate) 350.1 0.25 mg/L 5 001 Effluent Aqueous Hardness (total) SM 2340C 42 mg/L 5 001 Effluent Aqueous Nitrate -Nitrite - N 353.2 19 mg/L 5 001 Effluent Aqueous Phosphorus 365.1 3.8 mg/L 5 001 Effluent Aqueous TDS SM 2540C 490 mg/L 5 001 Effluent Aqueous TKN 351.2 2.6 mg/L 5 001 Effluent Aqueous Antimony 200.8 0.034 mg/L 7 001 Effluent Aqueous Chromium 200.8 0.0057 mg/L 7 001 Effluent Aqueous Copper 200.8 0.019 mg/L 7 001 Effluent Aqueous Selenium 200.8 0.004 mg/L 7 001 Effluent Aqueous Zinc 200.8 0.054 mg/L 7 (11 detections) Shealy Environmental Services. Inc. Page: 4 of 9 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Repon v2.1 Client: City of Mount Holly Laboratory ID: NF14071.001 % Description: Effluent Matrix: Aqueous Date Sampled:06/14/2012 0810 Date Received:06/14/2012 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM4500-NH3 (Ammonia - N ) 350.1 1 06/22/2012 1649 SMH 06/22/2012 0938 87616 1 (Hardness (to) SM 1 06/19/2012 0842 MDR 87351 1 (Nitrate-Nitr) 353.2 10 06/20/2012 1417 HBB 87459 1 (Phosphorus) 365.1 10 06/20/2012 1051 JBS 06/19/2012 1530 87369 1 (TDS) SM 2540C 1 06/18/2012 1146 LAS 87169 1 351.4 (TKN) 351.2 1 06/21/2012 1205 JBS 06/20/2012 0900 87433 CAS Analytical Parameter Number Method Result Q PQL Units Run Ammonia - N (phenate) 350.1 0.25 0.10 mg/L 1 Hardness (total) SM 2340C 42 10 mg/L 1 Nitrate -Nitrite - N 353.2 19 0.20 mg/L 1 Phosphorus 7723-14-0 365.1 3.8 0.10 mg/L 1 TDS SM 2540C 490 10 mg/L 1 TKN 351.2 2.6 0.60 mg/L 1 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 06/18/20121908 SJA 06/15/20121008 87003 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 NO 1.0 ug/L 1 Acenaphthylene 208-96-8 625 NO 1.0 ug/L 1 Anthracene 120-12-7 625 NO 1.0 ug/L 1 Benzidine 92-87-5 625 NO 5.1 ug/L 1 Benzo(a)anthracene 56-55-3 625 ND 1.0 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 1.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 1.0 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 1.0 ug/L 1 Benzo(k)fluoranthene 207-08-9 625 ND 1.0 ug/L 1 4-Bromophenyl phenyl ether -- 101-55-3 625 ND 1.0 ug/L 1 Butyl benzyl phthalate 85-68-7 625 NO 5.1 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625 NO 1.0 ug/L 1 bis (2-C hl oroeth oxy) methane 111-91-1 625 NO 1.0 ug/L 1 .ft bis(2-Chloroethyl)ether 111-44-4 625 NO 1.0 ug/L 1 bis(2-Chloroisopropyl)ether 108-60-1 625 NO 1.0 ug/L 1 2-Chloronaphthalene 91-58-7 625 NO 1.0 ug/L 1 r 2-Chlorophenol 95-57-8 625 NO 1.0 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 NO 1.0 ug/L 1 Chrysene 218-01-9 625 NO 1.0 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625 NO 1.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625 ND 1.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 NO 1.0 ug/L 1 PQL = Practical quanbtation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W • = Reportable result (only when report all runs) Shealy Environmental Services, Inc. Page: 5 of 9 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Iient:City of Mount Holly Laboratory ID: NF14071-001 Description: Effluent Matrix: Aqueous Date Sampled:06/14/2012 0810 Date Received:06114/2012 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 06/18/20121908 SJA 06/15/20121008 87003 CAS Analytical Parameter Number Method Result 0 PQL Units Run 1,4-Dichlorobenzene 106-46-7 625 NO 1.0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 NO 5.1 ug/L 1 2,4-Dichlorophenol 120-83-2 625 NO 1.0 ug/L 1 Diethylphthalate 84-66-2 625 NO 5.1 ug/L 1 Dimethyl phthalate 131-11-3 625 NO 5.1 ug/L 1 2,4-Dimethylphenol 105-67-9 625 NO 1.0 ug/L 1 Di-n-butyl phthalate 84-74-2 625 NO 5.1 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 NO 5.1 ug/L 1 2,4-Dinitrophenol 51-28-5 625 NO 5.1 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 NO 2.0 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 NO 2.0 ug/L 1 Di-n-octylphthalate 117-84-0 625 NO 5.1 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 NO 1.0 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 NO 5.1 ug/L 1 Fluoranthene 206-44-0 625 NO 1.0 ug/L 1 Fluorene 86-73-7 625 NO 1.0 ug/L 1 Hexachlorobenzene 118-74-1 625 NO 1.0 ug/L 1 Hexachlorobutadiene 87-68-3 625 NO 1.0 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625 NO 5.1 ug/L 1 Hexachloroethane 67-72-1 625 NO 1.0 ug/L 1 lndeno(1,2,3-c,d)pyrene 193-39-5 625 NO 1.0 ug/L 1 Isophorone 78-59-1 625 NO 1.0 ug/L 1 Naphthalene 91-20-3 625 NO 1.0 ug/L 1 Nitrobenzene 98-95-3 625 NO 1.0 ug/L 1 2-Nitrophenol 88-75-5 625 NO 2.0 ug/L 1 4-Nitrophenol 100-02-7 625 NO 5.1 ug/L 1 N-Nitrosodimethylamine 62-75-9 625 NO 1.0 ug/L 1 N-N itrosodi-n-propyla mine 621-64-7 625 NO 1.0 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 NO 1.0 ug/L 1 Pentachlorophenol 87-86-5 625 NO 5.1 ug/L 1 Phenanthrene 85-01-8 625 NO 1.0 ug/L 1 Phenol 108-95-2 625 NO 1.0 ug/L 1 Pyrene 129-00-0 625 NO 1.0 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625 NO 1.0 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625 NO 1.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W' • = Reportable result (only when report all runs) Shealy Environmental Services. Inc. Page: 6 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: NF14071-001 Description: Effluent Matrix: Aqueous Date Sampled:06/1412012 0810 Date Received:0611412012 Run 1 Acceptance Surrogate Q % Recovery Limits 2,4,6-Tribromophenol 70 41-144 Phenol-d5 55 28-128 Nitrobenzene-d5 56 38-127 2-Fluorobiphenyl 58 37-129 2-Fluorophenol 53 24-127 Terphenyl-d 14 23 10-148 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 06/16/2012 0033 BNW 06/14/2012 1935 86968 2 200.2 200.8 1 06/19/2012 0137 CDF 06/14/2012 1935 86968 CAS Analytical Parameter Number Method Result Q PQL Units Run Antimony 7440-36-0 200.8 0.034 0.001 mg/L 1 Arsenic 7440-38-2 200.8 ND 0.001 mg/L 1 Beryllium 7440-41-7 200.8 ND 0.0004 mg/L 1 Cadmium 7440-43-9 200.8 ND 0.0001 mg/L 1 Chromium 7440-47-3 200.8 0.0057 0.005 mg1L 1 Copper 7440-60-8 200.8 0.019 0.001 mg/L 1 Lead 7439-92-1 200.8 ND 0.001 mg/L 1 Nickel 7440-02-0 200.8 ND 0.005 mg/L 1 Selenium 7782-49-2 200.8 0.004 0.001 mg/L 2 Silver 7440-22-4 200.8 ND 0.001 mg/L 1 Thallium 7440-28-0 200.8 ND 0.0005 mg/L 1 Zinc 7440-66-6 200.8 0.054 0.01 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W ' = Reportable result (only when report all runs) Shealy Environmental Services, Inc. Page: 7 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 - Client: City of Mount Holly Laboratory ID: NF14071-002 Description: Effluent Matrix: Aqueous Date Sampled:06/1412012 0816 Date Received:06/1412012 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide - To) 10-204- 1 06/15/2012 1256 SMH 06/15/2012 0830 87036 1 (Phenolics) 420.4 1 06/21/2012 1354 HBB 06/21/2012 0919 87514 1 (HEM (oil and) 1664A 1 06/23/2012 1302 PAT 87694 CAS Analytical Parameter Number Method Result Q PQL Units Run Cyanide - Total 57-12-5 10-204-00-1-X ND 0.010 mg/L 1 Phenolics 420.4 ND 0.020 mg/L 1 HEM (oil and grease) 1664A ND 4.5 mg/L 1 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 06/26/20121826 AAC 87792 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug/L 1 Acrylonitrile 107-13-1 624 ND 50 ug/L 1 Benzene +Bromodichloromethane 71-43-2 624 NO 5.0 ug/L 1 75-27-4 624 ND 5.0 ug/L 1 Bromoform 75-25-2 624 ND 5.0 ug/L 1 JCarbBromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug/L 1 on tetrachloride 56-23-5 624 ND 5.0 ug/L 1 Chlorobenzene 108-90-7 624 ND 5.0 ug/L 1 Chloroethane 75-00-3 624 ND 5.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624 ND 10 ug/L 1 Chloroform 67-66-3 624 NO 5.0 ug/L 1 t Chioromethane (Methyl chloride) 74-87-3 624 NO 5.0 ug/L 1 Dibromochloromethane 124-48-1 624 NO 5.0 ug/L 1 1,1-Dichloroethane 75-34-3 624 NO 5.0 ug/L 1 1,2-Dichloroethane 41,1-Dichloroethene 107-06-2 624 ND 5.0 ug/L 1 75-35-4 624 NO 5.0 ug/L 1 4^trans-1,2-Dichloroethene 156-60-5 624 NO 5.0 ug/L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 624 NO 5.0 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 ug/L 1 Ethylbenzene 100-41-4 624 NO 5.0 ug/L 1 Methylene chloride 75-09-2 624 ND 5.0 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug/L 1 Tetrachloroethene 127-18-4 624 ND 5.0 ug/L 1 Toluene 108-88-3 624 ND 5.0 ug/L 1 1,1,1-Trichloroethane 71-55-6 624 ND 5.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 624 NO 5.0 ug/L 1 Trichloroethene 79-01-6 624 NO 5.0 ug/L 1 PQL = Practical quendtation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' = Reportable result (only when report all runs) Shealy Environmental Services. Inc. Page: 8 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 Client:C sty of Mount Holly Laboratory ID: NF14071-002 Description: Effluent Matrix: Aqueous Date Sampled:0611412012 0815 Date Received:0611412012 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 06/26/20121826 AAC 87792 CAS Analytical Parameter Number Method Result Q PQL Units Run Vinyl chloride 75-01-4 624 ND 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 108 52-138 Bromofluorobenzene 97 70-147 Toluene-d8 109 76-125 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time NO = Not detected at or above the PQL J = Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a ' W' • = Reportable result (only when report all runs) Shealy Environmental Services, Inc. Page: 9 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Level 1 Report v2.1 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Mount Holly Lot Number: MJ06055 Sample Number Sample ID Matrix Date Sampled Date Received 001 Effluent Aqueous 10/06/20110820 10/06/2011 002 Effluent Aqueous 10/06/20110820 10/06/2011 kc sampies) Shealy Environmental Services, Inc. Page: 3 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com v .1 Level i Report 1 s SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary City of Mount Holly Lot Number: MJ06055 Sample Sample 1D Matrix Parameter Method Result Q Units Page 001 Effluent Aqueous Ammonia - N (phenate) 350.1 0.56 mg/L 5 001 Effluent Aqueous Hardness (total) SM 2340C 50 mg/L 5 001 Effluent Aqueous TDS SM 2540C 470 mg/L 5 001 Effluent Aqueous bis(2-Ethylhexyl)p hthal ate 625 5.9 ug/L 6 001 Effluent Aqueous Antimony 200.8 0.029 mg/L 7 001 Effluent Aqueous Arsenic 200.8 0.0013 mg/L 7 001 Effluent Aqueous Chromium 200.8 0.0053 mg/L 7 001 Effluent Aqueous Copper 200.8 0.021 mg/L 7 001 Effluent Aqueous Selenium 200.8 0.0033 mg/L 7 001 Effluent Aqueous Zinc 200.8 0.057 mg/L 7 002 Effluent Aqueous Bromoform 624 9.8 ug/L 8 002 Effluent Aqueous Dibromochloromethane 624 8.7 ug/L 8 (12 detections) Shealy Environmental Services. Inc. Level t Report 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 79'!-9111 www.shealylab.com Page: 4 v 9 v2.i Client: City of Mount Holly Description: Effluent Date Sampled: 10/06/2011 0820 Date Received:10/06/2011 Inorganic non-metals Laboratory ID: MJ0605"01 Matrix: Aqueous Run Prep Method 1 Analytical Method Dilution Analysis Date Analyst Prep Date Batch SM4500-NH3 (Ammonia - N ) 350.1 2 10/12/2011 1347 SMH 10/11/2011 1154 69434 1 (Hardness (to) SM 1 10/17/2011 1419 SMH 69774 1 (TDS) SM 2540C 1 10/08/2011 1131 CMP 69330 Parameter CAS Analytical Number Method Result Q POL Units Run Ammonia - N (phenate) Hardness (total} 350.1 0.56 0.20 mg/L 1 TDS SM 2340C 50 10 mg1L 1 SM 2540C 470 10 mg/L 1 Semiyolatile Organic Compounds by GC/MS Run Prep Method 1 Analytical Method Dilution Analysts Date Analyst Prep Date Batch _ 625 625 1 10/13/20112201 WD 10/10/20110912 69337 2 625 625 1 10/18/20111420 WD 10/10/20110912 69337 Parameter CAS Analytical Acenaphthene Number Method Result Q PQL Units Run 83-32-9 625 NO 1.1 ug/L 1 AnthrAcenaphthylene 208-96-8 625 NO 1.1 uglL 1 Benzi enzidine ne 120-12-7 625 NO 1.1 ug/L 1 Benzo(a)anthracene 92-87-5 625 ND 5.3 ug/L 1 Benzo(a)pyrene 56-55-3 625 NO 1.1 ug/L 1 Benzo(b)fluoranthene 50-32-8 625 NO 1.1 ug/L 1 Benzo(g,h,i)perylene 205-99-2 625 NO 1.1 ug/L 1 Benzo(k)fluoranthene 191-24-2 625 NO 1.1 ug/L 1 4 4-Bromophenyl phenyl ether 207-08-9 625 NO 1.1 ug/L 1 � Butyl benzyl phthalate 101-55-3 625 NO 1.1 ug/L 1 - bis(2-Chloroethoxy)methane 85-68-7 625 NO 5.3 ug/L 1 -- bis(2-Chloroethyl)ether 111-91-1 625 ND 1.1 ug/L 1 bis(2-Chloroisopropyl)ether 111-44-4 625 NO 1.1 ug/L 1 4-Chloro-2-methylphenol 108-60-1 625 NO 1.1 ug/L 1 1- �!- 4-Chloro-3-methyl phenol 1570-64-5 625 NO 1.1 ug/L 2 �- 2-Chloro-5-methylphenol 59-50-7 615-74-7 625 ND 1.1 ug/L 1 2-Chloronaphthalene 625 NO 1.1 ug/L 2 -.2-Chlorophenol 91-58-7 625 ND 1.1 ug/L 1 - 3 & 4-Chlorophenol 95-57-8 625 ND 1.1 ug/L 1 4-Chlorophenyl phenyl ether 108-43-0 625 ND 2.1 ug/L 2 Chrysene 7005-72-3 625 NO 1.1 ug/L 1 Di-n-butyl phthalate 218-01-9 625 ND 1.1 ug/L 1 Di-n-octylp htha late 84-74-2 625 NO 5.3 ug/L 1 Dibenzo(a,h)anthracene 117-84-0 625 NO 5.3 ug/L 1 1,2-Dichlorobenzene 53-70-3 625 NO 1.1 ug/L 1 1,3-Dichlorobenzene 95-50-1 625 NO 1.1 ug/L 1 541-73-1 625 NO 1.1 ug/L 1 POL = Practicai quantitation limit 13 = Detected in tno method blank ND =Not detected at or above the POL E = ouantitation of compound exceedod the calibration range J = Estimated result a POL and > MDL P = The RPD between two GC columns exceeds 40916 Where applicable. all soil sample analysis are reported on a dry weight basis unless fagged with a 'W' N =Recovery is out of criteria H =Out of holding time Environmental Services. Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com LePage: 5 tv 9 Level 1 Report v2.1 Client: City of Mount Holly Laboratory ID: MJ06055-001 Description: Effluent Matrix: Aqueous Date Sampled:10/0612011 0820 Date Received.10/06/2011 Semiyolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 10/13/20112201 WD 10/10/20110912 69337 2 625 625 1 10/18/20111420 WD 10/10/20110912 69337 Parameter CAS Analytical Number Method Result Q PQL Units Run 1,4-Dichlorobenzene 106-46-7 625 ND 1.1 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 5.3 ug/L 1 2,4-Dichlorophenol 120-83-2 625 NO, 1.1 ug/L 1 -'� 2,5-Dichlorophenol 583-78-8 625 ND 2.1 ug/L 2 3,4-Dichlorophenol 95-77-2 625 ND 1.1 ug/L 2 Diethylphthalate 84-66-2 625 ND 5.3 ug/L 1 Dimethyl phthalate 131-11-3 625 ND 5.3 ug/L 1 ...3,3'-Dimethylbenzidine 119-93-7 625 ND 5.3 uglL 1 2,4-Dimethylphenol 105-67-9 625 ND 1.1 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 5.3 ug/L 1 2,4-Dinitrophenol 51-28-5 625 ND 5.3 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 ND 2.1 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 2.1 ug/L 1 1,2-Diphenyihydrazine(as azobenzene) 103-33-3 625 NO 1.1 ug/L 1 bis(2-Ethyl hexyl)phth a late 117-81-7 625 5.9 5.3 ug/L 1 Fluoranthene 206-44-0 625 ND 1.1 ug/L 1 Fluorene 86-73-7 625 ND 1.1 ug/L 1 Hexachlorobenzene 118-74-1 625 ND 1.1 ug/L 1 Hexachlorobutadiene 87-68-3 625 ND 1.1 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 5.3 ug/L 1 Hexachloroethane 67-72-1 625 ND 1.1 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 NO 1.1 ug/L 1 Isophorone 78-59-1 625 ND 1.1 ug/L 1 •4 N-Nitrosodi-n-propylamine 1• N-Nitrosodimethylamine 621-64-7 625 ND 1.1 ug/L 1 + N-Nitrosodiphenylamine (Diphenylamine) 62-75-9 625 ND 1.1 ug/L 1 Naphthalene 86-30-6 625 ND 1.1 ug/L 1 Nitrobenzene 91-20-3 625 ND 1.1 ug/L 1 1N 2-Nitrophenol 98-95-3 625 ND 1.1 ug/L 1 -� 4-Nitrophenol 88-75-5 625 NO 2.1 ug/L 1 Pentachlorophenol 100-02-7 625 NO 5.3 ug/L 1 Phenanthrene 87-86-5 625 ND 5.3 ug/L 1 Phenol 85-01-8 625 ND 1.1 ug/L 1 Pyrene 108-95-2 625 ND 1.1 ug/L 1 1,2,4-Trichlorobenzene 129-00-0 625 ND 1.1 ug/L 1 2,4,6-Trichlorophenol 120-82-1 88-06-2 625 625 ND 1.1 ug/L 1 NO 1.1 ug/L 1 PQL a Practical quantetation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND a Not detected at or above the PQL J = Estimated result < M. and 2 MDL P a The RPD between two GC columns exceeds 40% Where applicable. all soil samele analysis are-eported on a dry weight oasis unless flagged with a -W- N = Recoveryis out of critena H =Out of holding time Shealy Environmental Services. Inc. Page: 6 of106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.Shealylab.com v 9 Level 1 Report 2.1 Client: City of Mount Holly Description: Effluent Date Sampled:10/06/2011 0820 Date Received: 10108/2011 Laboratory ID: MJ06055-001 Matrix: Aqueous Surrogate 9 Q o /o Run 1 Recovery Acceptance Limits Q Run 2 Acceptance % Recovery Limits 2,4,6-Tribromophenol 60 41-144 80 41-144 Phenol-d5 52 28-128 58 28-128 Nitrobenzene-d5 48 38-127 64 38-127 2-Fluorobiphenyl 48 37-129 59 37-129 2-Fluorophenol 48 24-127 46 24-127 Terphenyl-d 14 24 10-148 31 10-148 ICP-MS Run Prep Method 1 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 200.2 200.8 1 10/11/20111847 FTS 10/10/20111854 69390 2 200.2 200.8 1 10/12/20110349 KJC 10/10/20111854 69390 Parameter CAS Analytical Number Method Result Q PQL Units Run Antimony 7440-36-0 200.8 0.029 0.001 mg/L 1 Arsenic Beryllium 7440-38-2 200.8 0.0013 0.001 mg/L 2 Cadmium 7440-41-7 200.8 ND 00004 g.m /L 1 Chromium 7440-43-9 200.8 ND 0.0001 mg/L 1 Copper 7440-47-3 200.8 0.0053 0.005 mg/L 1 Lead 7440-50-8 200.8 0.021 0.001 mg/L 1 Nickel 7439-92-1 200.8 ND 0.001 mg/L 1 Selenium 7440-02-0 200.8 ND 0.005 mg/L 1 Silver 7782-49.2 200.8 0.0033 0.001 mg/L 2 Thallium 7440-22-4 200.8 ND 0.001 mg/L 1 Zinc 7440-28-0 200.8 ND 0.0005 mg/L 1 7440-66-6 200.8 0.057 0.01 mg/L 1 PQL m Practical quantitation limit 8 = Detected in the metnod blanr. ND =Not detected at or above the PqL E =Quantization of compound exceeded rho calibration range J = Estimated result < PQL and> MDL P = The RPD between two GC columns exceeds 40% Where applicable. all soil sample analysis are reported on a dry wergnt basis unless Bagged wrtn a -1N- N aRecovery is out of criteria H a Out of holding time Shealy Environmental Services. Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.Shealylab.com Page: 7 of 9 y Laver 1 Report v2.1 Client: City of Mount Holly Laboratory ID: MJ06055-002 Description: Effluent Matrix: Aqueous Date Sampled:10/06/2011 0820 Date Received;10/06/2011 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide -To) 10-204- 1 10/13/2011 1122 DAS 10/12/2011 0939 69502 1 (Phenolics) 420.4 1 10/11/2011 1037 SMH 10/10/2011 0845 69340 1 (HEM (oil and) 1664A 1 10/17/2011 0920 AWT 69740 Parameter CAS Analytical Number Method Result Q PQL Units Run Cyanide - Total 57-12-5 10-204-00-1 A ND 0.010 mg/L 1 Phenolics 420.4 NO 0.020 mg/L 1 HEM (oil and grease) 1664A NO 4.9 mg/L 1 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 10/11/20111300 BM 69436 2 5030B 624 1 10/12/20112149 DLB 69602 Parameter CAS Analytical Number Method Result Q PQL Units Run 107-02-8 624 ND 50 ug/L 1 AcryloAcrol ni itrile 107-13-1 624 ND 50 ug/L 1 Benzene 4Benzene 71-43-2 624 ND 5.0 ug/L 1 Bromodichloromethane 75-27-4 624 NO 5.0 ug/L 1 Bromoform -t- Bromomethane (Methyl bromide) 75-25-2 624 9.8 5.0 ug/L 1 Carbon tetrachloride 74-83-9 624 NO 5.0 ug/L 1 56-23-5 624 NO 5.0 ug/L 1 Chlorobenzene 108-90-7 624 NO 5.0 ug/L 1 Chloroethane 75-00-3 624 ND 5.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624 NO 10 ug/L 1 Chloroform 67-66-3 624 NO 5.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug/L 9 2 Dibromochloromethane 124-48-1 624 8.7 5.0 ug/L 1 1,1-Dichloroethane 75-34-3 624 NO 5.0 ug/L 1 1,2-Dichloroethane 107-06-2 624 NO 5.0 ug/L 1 1,1-Dichloroethene 75-35-4 624 NO 5.0 ug/L 1 trans-l.2-Dichloroethene 156-60-5 624 ND 5.0 ug/L 1 1,2-Dichloropropene 78-87-5 624 ND 5.0 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 624 NO 5.0 ug/L 1 -w trans- 1, 3-D ichloropropene 10061-02-6 624 ND 5.0 ug/L 1 Ethylbenzene 100-41-4 624 NO 5.0 ug/L 1 Methylene chloride 75-09-2 624 ND 5.0 ug/L 1 1.1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug/L 1 Tetrachloroethene 127-18-4 624 NO 5.0 ug/L 1 Toluene 108-88-3 624 NO 5.0 ug/L 1 1. 1, 1 -Trichloroethane 71-55-6 624 ND 5.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug/L 1 POL = Prectieat quanLtation limit B - Detected to the method blank E = Quantitabon of compound exceeded the calibration range ND = Not detected at or above the POL J = Estemated result < PQL and > MDL P = The RPD between two GC columns exceeds 401b Where applicable. all soil sample analysis are reported on a dry weignt basis unless flagged with a 'W" K = Recoveryis out of criteria H s Out of holding time Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 tn+ww.shealylab.com Page: 8 of 9 Level 1 Report v2.1 . , Client: City of Mount Holly Description: Effluent Date Sampled:10106/2011 0820 Date Received:10/06/2011 Laboratory ID: MJ06055-002 Matrix: Aqueous Volatile Organic Compounds by GC/MS Run Prep Method 1 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 5030B 624 1 10/11120111300 BM 69436 2 5030B 624 1 10/12/20112149 DLB 69602 Parameter CAS Analytical Number Q POL Units Run Trichloroethene -MethodResult 79-01-6 624 ND 5.0 ug/L 1 Vinyl chloride 75-01-4 624 NO 5.0 ug/L 1 Surrogate 9 Q o Run 1 Acceptance Run 2 Acceptance /o Recovery Limits Q % Recovery Limits 1,2-Dichloroethane-d4 104 52-138 98 52-138 Bromofluorobenzene 98 70-147 101 70-147 Toluene-d8 98 76-125 99 76-125 POL - Practical guantitation limit B = Detected in the metnod blank No =Not detected at or above the POL E = t]uanittaa0n o. compound exceeded the calibration range J = Estimated result c POL and = MDL P = The RPD between two GC columns exceeds 40% Where applicable, all soi! sample analysis are reported on a dry weight basis unless flagged with a "W" N = Recovery is out of criteria h =Out or holding time Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia. SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page: 9 of 9 Level 1 Repon v2.1 ATTACHMENT V Toxicity Reports - Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:7/31/2014 Facility: Mt. Holly WWTP NPDES # NC00 21156 Laboratory: Pace Analytical - Raleigh X LM U7111% c. Signature of Laboratory Supervisor Pipe #: 001 County: Gaston [..nmmants r MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time 7/22/2014 / 16:10 Avg Wt/Surv. Control 0.421 Test Organisms % Efi. Repl. Control Surviving # Original # Wt/original (mg) C31 Surviving # Original # Wt/original (mg) 4.61 Surviving # Original # Wt/original (mg) Q Surviving # Original # Wt/original (mg) ® Surviving # Original # Wt/ariginal (mg) 121 Surviving # Original # Wt/original (mg) tter Quality Data Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin High Concentration pH (SU) Init/Fn DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (urnhos/cm) Chlorine(mg/L) Temp. at Receipt (°C) 1 9 A a 10 9 9 10 10 10 10 10 0.451 0.378 0.342 0.431 10 9 9 6 10 10 10 10 0.495 0.383 0.455 0.397 9 10 10 8 10 10 10 10 0.434 0.396 0.438 0.386 10 9 10 J10 10 10 10 110 0.464 0.454 0.444 1 0.415 10 7 10 9 10 10 10 10 0.487 0.365 0.510 0.426 7 9 9 1 8 10 10 10 10 0.415 0.466 0.397 0.393 % Survival 95.0 Avg Wt (mg) 1 0.401 % Survival 85A Avg Wt (mg) 0.433 % Survival 92.5 Avg Wt (mg) 0.414 % Survival 97.5 Avg Wt (mg) 0.444 % Survival 90.0 Avg Wt (mg) 0.447 % Survival 82.5 Avg Wt (mg) 0.418 7.6 / 8.0 7.7 / 7.5 7.8 / 7.7 7.7 / 7.9 7.7 / 7.4 7.7 / 7.6 1 U / 7.4 7.7 / 7.7 7.8 / 6.9 8.0 / 6.5 8.0 / 7.5 8.0 / 6.6 7.9 / 7.4 7.6 / 7.2 24.8 / 24.7 24.6 / 24.8 24.9 / 24.9 24.5 / 24.7 24.7 / 24.7 24.8 / 24.8 24.9 / 24.8 0 1 9 A d r, a 7.4 / 7.9 8.0 / 7.517.8 / 7.717.7 / 7.817.9 / 7.417.7 / 7.817.8 / 7.5 7.7 / 7.7 7.7 / 7.2 17.8 / 6.2 17.1 / 7.6 8.2 / 6.3 18.1 / 7.9 8.0 / 7.4 24.9 / 24.8 25.0 / 24.9 24.6 / 24.7 24.8 / 24.8 25.1 / 24.6 25.2 / 24.7 24.8 / 24.7 1 2 3 7/20/2014 7/22/2014 7/24/2014 24.00 24.00 24.00 39.00 39.60 35.60 45.00 48.00 45.80 1049 973 993 <0.1 <0.1 <0.1 0.3 1.6 2.6 Dilution H2O Hardness (mg/L) 39.00 Alkalinity (mg/L) 28.00 Conductivity (umhos/cm) 168.6 Survival Growth Normal Pip 'Ll Horn. Var. rR PU NOEC 12 12 LOEC >12 >12 ChV >12 >12 Method DunnetCs Dunnett's Cultured In -House Outside Supplier Hatch Date: Hatch Tlme:16 06 -l"a Overall Result ChV >12% Stats Survival Growth Conc. Critical Calculated Critical Calculated 3 2.41 1.211 2.41 -1.025 4.5 2.41 0.327 2.41 -0.417 6 2.41 -0.375 2.41 -1.402 9 2.41 0.594 2.41 -1.49 12 2.41 1.67 2.41 -0.553 DWQ Form AT 5 (1104) Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Facility: Mt. Holly WWTP NPDES # NC00 21156 Pipe M 001 .t .,4,.,..,�.,.... D.,.,., A...,1..a:.,.,1 0.,1.,:.,4, InAmmante, I . Responsible Charge x - 11 / __,: Signature of Laboratory Supervisor Test Initiation Date/Time % Eff. Repi. Control Surviving # Original # Wt/original (mg) oSurviving # Original # Wt/original (mg) 4.5 Surviving # Original # Wt/original (mg) © Surviving # Original # Wt/original (mg) L-=J Surviving # Original # Wt/original (mg) 12 Surviving # Original # Wt/original (mg) Water Quality Data Control pH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin High Concentration pH (SU) [nit/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg1L) Temp. at Receipt (°C) MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 8/19/2014 / 15:00 1 2 3 4 Avg Wt/Surv. Control 1 0.575 10 10 10 9 10 10 10 10 0.589 0.548 0.547 0.554 10 10 10 10 10 10 10 10 0.512 0.607 0.570 0.569 10 10 10 10 10 10 10 10 0.595 0.486 0.607 0.549 10 10 10 10 10 10 10 10 0.533 0.620 0.519 0.555 10 10 10 10 10 10 10 10 0.584 0.563 1 0.545 1 0.551 9 10 10 10 10 10 10 10 0.533 0.508 0.499 0.613 % Survival 97.5 Avg Wt (mg) 0.560 % Survival 100.0 Avg Wt (mg) 0.565 % Survival 100.0 Avg Wt (mg) 0.559 % Survivall 100.0 Avg Wt (mg) 0.557 Survival 100.0 Avg Wt (mg) 0.561 % Survivall 97.5 Avg Wt (mg) 1 0.538 Day 0 1 2 3 4 5 6 Date:8/28/2014 County: Gaston q Z Z 1 Test Organisms ff Cultured In -House f V Outside Supplier 7.8 / 7.6 7.7 / 7.6 7.7 / 7.6 7.7 I 7.6 7.8 I 7.4 7.9 I 7.8 17.9 / 7.5 7.8 / 7.6 7.9 / 7.3 7.9 / 8.1 8.5 / 7.0 8.1 / 6.8 8.0 / 7.7 18.2 / 7.6 24.9 / 24.7 25.0 / 24.9 25.0 / 24.7 24.8 / 24.8 25.0 / 24.7 24.9 / 24.7 24.8 / 24.8 0 1 2 3 4 5 6 7.8 ! 7.6 7.8 / 7.6 7.7 / 7.6 7.8 / 7.6 7.7 / 7.4 7.7 / 7.7 7.6 / 7.6 7.8 / 7.6 8.0 / 7.2 7.8 / 8.2 8.5 / 7.2 8.4 / 6.9 8.0 / 8.0 8.2 / 8.0 25.2 / 24.9 24.7 / 24.7 25.1 / 24.8 24.6 / 24.9 25.3 / 24.8 25.0 / 24.7 24.9 / 24.8 1 2 a 8/17/2014 8/19/2014 8/21/2014 24.00 24.00 24.00 35.40 36.40 37.00 51.00 52.50 51.00 978 963 945 <0.1 <0.1 <0.1 1.3 2.2 3.1 Dilution H2O Hardness (mg/L) 39.00 Alkalinity (mg/L) 28.80 Conductivity (umhos/cm) 206.3 Survival Growth Normal rl j%I Hom. Var, U-1 Irk NOEC 12 12 LOEC >12 >12 ChV >12 >12 Method Steel's Dunnett's Hatch Date: Hatch Time: ,t � ) Overall Result ChV >12% Slats Survival Growth Conc. Critical Calculated Critical Calculated 3 10 20 2.41 -0.174 4.5 10 20 2.41 0.009 6 10 20 2.41 0.096 9 10 20 2.41 -0.043 12 10 18 2.41 0.739 DWO Form AT-5 (1104) Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:4/30/2014 Facility: Mt. Holly WWTP NPDES # NC00 21156 Pipe #: 001 County: Gaston Laboratory: Pace Analytical - Raleigh Comments WO# 9219-8333 X ni Si Lure f Operat in sponsible Charge X -� Signature of Laboratory Supervisor Test Initiation Date/Time % Eff. Repl. Fco-n-tro'll Surviving # Original # Wt/original (mg) �J Surviving # Original # Wt/original (mg) 4.5 Surviving # Original # Wt/original (mg) © Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) 12 Surviving # Original # Wt/original (mg) Water Quality Data Control PH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin High Concentration PH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp. at Receipt (°C) MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh. NC 27699-1621 4/22/2014 / 4:14pm Avg Wt/Surv. Control 0.430 1 2 z A 10 10 10 9 10 10 10 10 0.430 0.391 0.435 0.418 10 10 1 10 10 10 10 1 10 10 0.414 0.369 1 0.419 0.442 10 10 10 10 10 10 10 10 0.362 0.318 0.434 0.418 10 10 10 10 10 10 10 10 0.517 0.414 0.404 0.348 9 10 10 10 10 10 10 10 0.351 0.376 0.420 0.389 10 10 10 10 10 10 10 10 0.392 0.465 0.438 0.414 % Survivall 97.5 Avg Wt (mg) 1 0.419 % Survival 100.0 Avg Wt (mg) 1 0.411 % Survival 100.0 Avg Wt (mg) 0.383 % Survivall 100.0 Avg Wt (mg) 0.421 % Survival 97.5 Avg Wt (mg) 0.384 % Survival 100.0 Avg Wt (mg) 0.427 Day 0 1 7 q e 7.9 / 7.6 7.7 / 7.7 7.6 / 7.7 7.3 / 7.6 7.6 / 7.5 7.7 / 7.3 7.6 / 7.6 8.2 / 7.6 7.9 / 7.3 8.4 / 7.7 7.5 / 7.6 7.7 / 6.5 7.8 / 6.9 7.5 / 7.2 24.7 / 24.6 24.6 / 24.8 24.9 / 24.7 24.6 / 24.6 24.8 / 24.5 24.8 / 24.7 24.7 / 24.8 0 1 9 z 7.5 / 7.5 7.7 / 7.7 7.5 / 7.6 7.3 / 7.6 7.5 / 7.4 7.4 / 7.3 17.5 / 7.6 8.0 / 7.5 7.6 / 7.4 8.3 / 7.5 7.6 / 7.6 7.5 / 6.7 7.7 / 7.3 17.6 / 7.5 24.6 / 24.7 24.7 / 24.8 24.5 / 24.6 24.9 / 24.8 24.7 / 24.6 24.8 / 24.5 24.9 / 24.9 1 2 It 4/20/2014 4/21/2014 4/24/2014 24.00 24.00 24.00 43.00 43.60 42.40 37.50 40.50 57.00 576 693 807 <0.1 <0.1 <0.1 0.3 1.1 1 0.9 Dilution H2O Hardness (mg/L) 39.60 Alkalinity (mg/L) 29.00 Conductivity (umhos/cm) 167.2 Survival Growth Normal I irl Hom. Var. ') 971 NOEC 12 12 LOEC >12 >12 ChV >12 >12 Method Steels Dunnett's Test Organisms Fw Cultured In -House i✓ Outside Supplier Hatch Date: f Hatch Time: Overall Result ChV >12% Stats Survival Growth Conc. Critical Calculated Critical Calculated 3 10 20 2.41 0.249 4.5 10 20 2.41 1.177 6 10 20 2.41 -0.075 10 18 2.41 1.144 12 10 20 -0.29 ✓Vvw I VIM ^ I-J r I/VN/ Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:2/27/2014 Facility: Mt. Holly WWTP NPDES # NC00 21156 Signature of Laboratory Supervisor MAIL ORIGINAL TO: Environmental Sciences Branch Division of Water Quality NC DENR 1621 Mail Service Center Raleigh, NC 27699-1621 Test Initiation Date/Time 2/18/2014 % Eff. Repl. Control Surviving # Original # Wt/original (mg) Surviving # Original # Wt/original (mg) 4.5 Surviving # Original # Wt/original (mg) © Surviving # Original # Wt/original (mg) ® Surviving # Original # Wt/original (mg) 12 Surviving # Original # Wt/original (mg) r Quality Data Control PH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin High Concentration PH (SU) Init/Fin DO (mg/L) Init/Fin Temp (C) Init/Fin Sample Collection Start Date Grab Composite (Duration) Hardness (mg/L) Alkalinity (mg/L) Conductivity (umhos/cm) Chlorine(mg/L) Temp, at Receipt (°C) 1 Pipe #: 001 County: Gaston Comments WO# 92189835 / 2:22pm Avg Wt/Surv. Control 0.692 2 a d 10 10 10 10 10 10 10 10 0.704 0.632 0.537 0.893 10 10 10 10 10 10 10 10 0.582 0.609 0.729 0.618 10 10 10 10 10 10 10 10 0.794 0.612 0.636 0.579 10 10 10 10 10 10 10 10 0.636 0.660 0.579 0.674 10 10 10 10 10 10 _ 10 10 0.762 0.595 0.646 0.595 10 10 1 10 10 10 10 10 10 0.687 0.740 1 0.684 0.662 % Survival 100.0 Avg Wt (mg) 0.692 % Survival 100.0 Avg Wt (mg) 0.635 % Survivall 100.0 Avg Wt (mg) 0.655 % Survivall 100.0 Avg Wt (mg) 0.637 % Survival 100.0 Avg Wt(mg)l 0.650 % Survivall 100.0 Avg Wt (mg) 1 0.693 Day 0 1 7 Z n r 8.0 I 7.6 7.6 / 7.5 7.8 / 7.7 7.7 / 7.3 7.7 / 7.5 7.7 I 7.7 7.7 / 7.4 7.9 / 6.5 7.6 / 6.9 8.0 / 6.8 7.9 / 6.0 7.5 / 6.2 7.9 / 6.4 7.2 / 6.4 24.8 / 24.9 25.2 / 25.1 24.9 / 25.0 25.1 / 25.0 25.1 / 25.0 24.7 / 24.9 25.0 / 24.9 0 1 9 a 7.8 / 7.4 7.6 / 7.4 7.6 / 7.6 7.6 / 7.117.5 / 7.4 17.6 / 7.617.7 / 7.3 8.1 / 7.2 7.2 / 6.1 7.6 / 7.0 8.1 / 6.0 17.5 / 5.3 17.3 / 6.517.5 / 6.2 24.9 / 25.0 25.1 / 25.0 24.7 / 24.8 25.0 / 24.9 25.2 / 25.1 24.8 / 24.9 25.1 / 25.0 1 2 It 2/16/2014 2/18/2014 2/20/2014 24.00 24.00 24.00 44.00 45.00 34.00 29.00 43.00 65.50 595 688 675 <0.1 <0.1 <0.1 1.2 1.0 1.4 Dilution H2O Hardness (mg/L) 43.00 Alkalinity (mg/L) 26.50 Conductivity (umhos/cm) 145.9 Survival Growth Normal r1 G,I Hom. Var. n rV I NOEC 12 12 LOEC >12 >12 ChV >12 >12 Method Steel's Dunneirs Test Organisms T' Cultured In -House 7 Outside Supplier Hatch Date: ,T Hatch Time: ib .y- (� L. Overall Result ChV >12 % Stats Survival Growth Conc. Critical Calculated Critical Calculated 3 10 18 2.41 0.93 10 18 2.41 0.591 6 10 18 2.41 0.885 10 18 2.41 0.685 12 10 18 2.41 -0.029 uvvv roan A ►-0 I 7/u4,, ATTACHMENT VI Jadco-Hughes Site Information (D-- CONES7170GA-ROVERS & ASSOCIATES January 15, 2013 Mr. Jonathan Jordan Utilities Supervisor City of Mount Holly P.O. Box 406 Mount Holly, North Carolina 28120 Dear Mr. Jordan: 4215-1 Stuart Andrew Blvd. Charlotte, North Carolina 28217 Telephone: (704) 676-0502 Facsimile: (704) 676-0704 www.CRAworld.com Re: 2013 Annual Reporting of Discharges Jadco-Hughes Site (Site), Gaston County, North Carolina Reference No. 003669-95 On behalf of the Jadco-Hughes Site Potentially Responsible Party (PRP) Group, CRA submits this annual letter report in accordance with the May 15, 2000 agreement between the PRP Group and the City of Mount Holly (City). The reporting period is for the year 2013. A total of 13,763,997 gallons of treated water were discharged to the City Publicly Owned Treatment Works (POTW) in 2013. The water was discharged at a rate not greater than 75,000 gallons per day. CRA collected composite sample of the effluent on December 19, 2013 for compliance monitoring. The total volume discharged during the 24-hour composite sampling period (from December 18 to 19, 2013) was 29,566 gallons. CRA analyzed the composite sample for metals, ammonia (NH3) and total suspended solids (TSS). CRA also collected a grab sample of the effluent on December 19, 2012 and analyzed it for volatile organic compounds (VOCs), oil and grease, polychlorinated biphenyls (PCBs), and cyanide. All parameters were within the discharge limits. CRA also collected a sample for biochemical oxygen demand (BOD); however, the laboratory incorrectly analyzed the sample for carbonaceous BOD. CRA has collected another sample for BOO analysis and will submit the data to the City when the laboratory provides the data to us. As discussed by telephone on January 14, 2014, CRA has also collect samples for the full list of metals and base/neutral/acid compounds listed in the City's letter dated October4, 2013. These parameters were listed in the original permit; however, because there were no issues with exceeding the discharge standards and based on discussions with the City and receipt of the City's approval to do so, the metals list was reduced and BNAs were no longer analyzed. As discussed, CRA will analyze for these parameters until further discussions with the City's consultant, United Water, take place. The laboratory analytical results for December 19, 2013 are summarized in Table 1. Equal Employment Opportunity Employer ISO 9001 f INIE1140 DES104 0 CONESTOGA-ROVERS & ASSOCIATES January 15, 2013 Reference No. 003669-95 -2- The next discharge monitoring event will be performed in December 2014. We will inform you of the monitoring schedule one week prior to commencing the activities. If you have any questions, please do not hesitate to contact me at (519) 884-0510. Yours truly, CONESTOGA-ROVERS & ASSOCIATES Colleen Dietrich CD/cb/2 Encl. cc: James Friday, City of Mt. Holly Ralph Douglas, City of Mt. Holly Jadco-Hughes Technical Committee Patricia Barmeyer, King & Spalding Stephen Quigley, CRA John Uteck, CRA Parameter (1) Flow (2) BOD TSS NH3 Metals TABLE 1 ANALYTICAL RESULTS FOR 2013 ANNUAL EFFLUENT MONITORING JADCO-HUGHES SUPERFUND SITE GASTON COUNTY, NORTH CAROLINA Discharge Limits 0.075 MGD 300 mg/L 350 mg/L 25 mg/L Treated Water To Sewer System SAMPLE ID: GW-3669 JU-121913-036 Lob Results 29,566 gal (6) < 5 mg/L < 0.05 mg/L Page 1 of 2 Converted Data Arsenic 0.1 mg/L < 0.005 mg/L Cadmium 0.02 mg/L < 0.005 mg/L Chromium 0.5 mg/L < 0.01 mg/L Cyanide 0.5 mg/L < 0.005 mg/L Lead 0.05 mg/L < 0.005 mg/L Nickel 0.5 mg/L < 0.005 mg/L Base Neutral Compounds (3) 1,2,4-Trichlorobenzene 0.0759 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,2-Dichlorobenzene 0.0234 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,3-Dichlorobenzene 0.0146 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,4-Dichlorobenzene 0.0651 Ibs/day < 1 µg/L 0.0000 Ibs/day Volatile Compounds (3) 1,1,1-Trichloroethane 0.0209 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,1,2,2-Tetrachloroethane 0.0001 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,1,2-Trichloroethane 0.0009 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,1-Dichloroethane 0.0004 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,1-Dichloroethylene 0.0058 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,2-Dichloroethane 0.0822 Ibs/day 5 µg/L 0.0012 Ibs/day 1,2-Dichloroethylene (total) 0.5342 Ibs/day 110 µg/L 0.0271 Ibs/day 1,2-Dichloropropane 0.0001 Ibs/day < 1 µg/L 0.0000 Ibs/day 1,3-Dichloropropylene (total) 0.2606 Ibs/day < 1 µg/L 0.0000 Ibs/day 2-butanone 23.8207 Ibs/day < 5 µg/L 0.0000 Ibs/day 2-hexanone 0.3753 Ibs/day < 5 µg/L 0.0000 Ibs/day CRA 003669-Jordan-3-Tl Parameter (1) TABLE 1 ANALYTICAL RESULTS FOR 2013 ANNUAL EFFLUENT MONITORING JADCO-HUGHES SUPERFUND SITE GASTON COUNTY, NORTH CAROLINA Discharge Limits Page 2 of 2 Treated Water To Sewer System SAMPLE ID: GW-3669 JU-121913-036 Lab Results Converted Data Acetone 11.4558 Ibs/day < 5 µg/L 0.0000 Ibs/day Benzene 0.0229 Ibs/day < 1 µg/L 0.0000 Ibs/day Bromodichloromethane 0.1835 Ibs/day < 1 µg/L 0.0000 Ibs/day Bromoform 0.1501 Ibs/day < 1 µg/L 0.0000 Ibs/day Bromomethane 1.0425 Ibs/day < 1 µg/L 0.0000 Ibs/day Carbon Tetrachloride 0.5967 Ibs/day 14 µg/L 0.0035 Ibs/day Chlorobenzene 0.0121 Ibs/day < 1 µg/L 0.0000 Ibs/day Chloroethane 0.0033 Ibs/day < 1 µg/L 0.0000 Ibs/day Chloroform 1.4249 Ibs/day 18 µg/L 0.0044 Ibs/day Dibromochloromethane 0.1334 Ibs/day < 1 µg/L 0.0000 Ibs/day Ethylbenzene 0.0938 Ibs/day < 1 µg/L 0.0000 Ibs/day Methyl Chloride 1.0425 Ibs/day < 1 µg/L 0.0000 Ibs/day Methylene Chloride 0.2189 Ibs/day < 1 µg/L 0.0000 Ibs/day Tetrachloroethene 0.00531 Ibs/day 3.9 µg/L 0.0010 Ibs/day Toluene 1.4478 Ibs/day < 1 µg/L 0.0000 Ibs/day Trichloroethylene (7) 0.0138 Ibs/day 48 µg/L 0.0118 Ibs/day Vinyl Chloride 0.4775 Ibs/day < 1 µg/L 0.0000 Ibs/day Xylene 0.1147 Ibs/day < 15 µg/L 0.0000 Ibs/day Other Parameters Polychlorinated Biphenyls (3), (4) 0.0010 Ibs/day < 0.53 µg/L 0.0000 Ibs/day Oil and Grease 100 mg/L < 4.4 mg/L pH 5 -11(5) 8.31 Notes: < Below detection limit. The quantity shown is the detection limit. (1) Discharge limit is the concentration specified in Attachment I of the October 3, 2013 City of Mount Holly letter. (2) The converted data is based on the flow rate shown. (3) The effluent limitation is the daily maximum agreed to by City of Mount Holly (letter dated July 12, 2011). (4) Detection limit for Total PCBs shown is detection limit for each of the individual PCB Aroclors. (5) Standard Units. (6) Laboratory error. CRA will resample and submit data to the City. (7) Discharge limits for tetrachloroethene and trichloroethene are based on October 3, 2013 letter from City; however, City previously agreed to limits of 0.1068 and 0.7475 Ibs/day, respectively (letter dated November 7,199 CRA 003669-Jordan-3-Ti ATTACHMENT VII Triangle Texaco Site Information lntiristi•iat L Nei Waste« otter 5urve% Pet•mit .application COVER PAGE _-- I `v.i,nC .n AuitluYltcd reprr,rttla[t►r •.:,r, r, ::•.}•.. ,n :c , - .. ,..� :..}:.l,:.. '�mn, rYa•rns�.�r . y .,:. t.•.., ".;:....ra.rti r ..c!! ;,c• cia•. tri •i;\ ti0r!i:Ita,11% �. •.•t'�j`.•'' ri l��!••: {I: C',. 'r�::{tic:. la: ('tl'1' .ti_ ��::irl'i t:itl� ':!t��,ltl`-II'1�. :CCttfa: i.CCj,If1K. and • I��it� Sc%\Cr \utnt•ri?\ and -or flic Z t: dlta m.:I,:c ; Ili i l Mark C. Boland, P.E. Patrick R. Kelly, P G. r"'` Principal Engineer ' cars '`tih'r- 16 ''tle earsmallfirm 6 Staff Geologist Phone 4(704) 394-6913 }a`"(704) 394-6965 Plo,r7041604-5223 1 Fax v (704) 394-6968 � Email Address mboland shielden ineerin .colri ' r=n"` `''°r2" pkelly@shieldengineering.com ft sicai s eet address of 1aciri,�N 201 N. Main Street Otiicsi ma{rinta addre., J J tiereni Now it saint: ' I 4301 Taggart Creek Rd t I I c"" Mount Holly "" NC ' `'" 28120 "� Charlotte "�`` NC ziP 28086 The information provided by yatt on this questionnaire serves two funetiOnS: The information is used to determine it your facility needs an Industrial User Pretreatment Permit OUP) for the discharge of wastewater to the local sewer. If an Industrial User Pretreatment Permit OUP) is required, this survey serves as the application for an Industrial User Pretreatment Permit (]UP). Requests for con; ide.ntial treattnenr of" mforination provided on this form shall be governed by procedures bpecificd in 40 CFR Paii 2. Ill accordance with Title 40 of' the Code of Federal Regulations Part 403. Section 40,.14 and the Local Sever Use Ordinance (S110). information and data provided ill this questionnaire which identifies the content. volume and frequency of discharge shall be available to the public vOthuut restricciun This ib to be signed b\. an authorized officiai of your lirin. as defines] in the vocal Se\%cr I. se Ordinance. Section 1.2, after completion of this fens I certify under penaw, of lati that this ;�ocumen: and all attachment, \+ere prepared under m� i direction \�r super-\ ision in accor•danLe with a systenl designed to asSure that qualified personnel propt:rlN ��athcr and t:\ aluate the infor•tnatiort submitted. Based upon m-, inquiry of - the person or oersons who mana`re the system. or these persons direcd% responsible for 2atherin nfi the i,rrzi.tTI011. the irlfumatrort suhmitted is, to the hr,;t of my knowledge and � belief•, true. accurate and complete ani aware that there are: siunificant penalties for E subr@i ing,•_ tal-zt information. including the pussibilin of fine andior imprisonment for ; i:no i iz \fic.fattio Signature l�- authorized Remesenrative i 4 r.-' al d'applicable, Date paueIofI Industrial User Wastewater Survev & Permit Application V PART I,! GENERAL INFORMATION: l . Provide a brief narrative description of the type of business. manufacturing processes. or service activities your firm conducts at this site. Shield Engineering, Inc. is an environmental consulting and engineering firm contracted with a responsible party who is directed by the NCDENR to abate, assess, and remediate soil and groundwater contamination resulting from a previous underground storage tank release. �. List the primary products produced at this facility: No products are produced at this site. Environmental remediation activities are anticipated to result in recovered petroleum impacted groundwater from several recovery wells. 3. List ra%k materials and process additives used: No raw materials or process additives are used. 4. Are biocides added to any water discharged to the P01"A'. if yes describe: Yes No X 5. Describe weekly production schedule. including shifts worked per day. employees per shift. and primary operation during shift. j Automated equipment will operate 24 hours a day, with periodic maintenance visits by Shield Engineering, Inc. technicians. Shield Engineering, Inc. estimates recovery of up to approximately 40,000 gallons of petroleum impacted groundwater per week. 6. Production process is: Check. if all continuous X Check. if all batch If both please enter. % continuous = % % Batch = I % Page-" of 17 Industrial User Wastewater Survey & Permit Application i PART I GENERAL INFORMATION (cont): 7. ! Does production vary significantly (-- 20 %) by season. Describe. Possibly, Production may vary due to seasionai groundwater Yes x highs and lows. No 8. Are an\ significant (-- 20 %) changes in production that will affect wastewater discharge expected in the next 5 years. If yes. please describe. Yes, groundwater remediation activities are expected to be Yes x completed within 2-4 years of remediation system operation. No 9. list all current waste haulers. Give name. address. phone numbers. volume and materials hauled off. Not applicable. 10. Attach a copy of laborator\ analyses performed in the last year on the wastewater discharge(s) from your facilities. Summarize data on the attached Data Summary Form. See Attached Attach sketch or schematic showing sampling points and all connections to the sever. See Attached 12. Complete the Wastewater Pollutants Checklist attached to this Survey. See Attached Page 3 of 17 if �es� Permit �. Jate. ,gtn!ic:uri name I Industrial User Wastewater Survey 'I & Permit Application Y PART 1,1 GENERAL INFORMATION (cont): 131 Do you have. or hake you ever applied for. been issued. or been denied an NPDES permit to discharge to the surtace waters or storm sewers of North Carolina? If yes. list all other NPDES permits. permit numbers. dates. and names used to apply for the m. or reason denied. Permit 4 Llate_ applicant name Bantam Mart, NCG510464, 10/18/11, Petroleum World, Inc. Yes x i I1 s'c Permit .. .fate appireartt name Danieltown NCG510245 Rescinded 4126/05 Petroleum World No I Inc 14.Do vuu have. or have you ever applied for or been issued an Industrial j l�se 1- Pretreatment Permit (IUP) to discharge wastewater- to the sewer collection system. It' yes. list all other IUP permits. permit numbers. dates. and names used to a I\ Im them. rt I 1'ennit �. �laie, apt�lrcant name Yes No x 1 5. Do you have. or have you ever applied for or been issued any other Fn�ironmental Permits (for example: air. RCRA. rU11-ound%\ater. € storm\�ater. general. Non -Discharge. septic tank. etc.). It' \es. list all other errrlits. Perillit numbers. dates. and names used to a Iv for them. il'�c, � Pcrmu t�t�r. = aatc. aplthc::nt n:nne Yes if�c. �Pennit tree. u. date. appltcaitt Haute I No x Itws I�'ermrt t�pc ,laic. appirrartt name 16. Is a Spill Prevention Control and Countermeasure (Sl'CC) Plan i prepared f-or this facilit\ .) It)cs. please attach a copy. i - 17. Is a Spill 'Slu- Control Plan required b\ the POTW . prepared for this 'i facility :t f Yes No x Yes No x Pace 4 of 17 Industrial User Wastewater Survev & Permit Application - Wastewater Pollutant Checklist Chemical Name EPA Check if' Check it' Check it' Check it' Concentration Storet Present at :- bsei at I , Present in :absent in in Discharge. Code Facility Facility Discharge Discharge if Known Other Inorganics Barium �, I,,, ; Chloride , (N-to x ; Cvanide (,l,i211 Fluoride ( Purgeable Volatile Organics 1.1.1-Trichloroethane 1.1.2.2-Tetrachloroethane x 1.1?-Trichloroethane x 1 1. 1 -Dichloroethane 1.1-Dichloroethvlene x x 0.045 1 ?-Dichloroethane x 1.2-Dichloro ro ane ;a;s x ?-Chloroethvl vinvl ether x Acrolein i x Acrvlonitrile T x Benzene x 4.0 Bromodichloromethane Its E Bromoform i, Bromomethane 34413 Carbon tetrachloride 1' x Ch lorobenzene ".4;01 x Chloroethane 1 , Chloroform ,' 1,16 Chloromethane �44 i w 69 cis 1.3-Dichloro ro ene wT14 x Dibromochloromethane ITF. Ethvlbenzene ti1ethv lone chloride ',4-M 2 3 x x Tetrachloroethvlene ;�i�� x-0,0207 Toluene ;4oI x trans 1.3-Dichloro ro ene 11 ;4o,4ko x trans- 1.2-DichloroetIn lene 14i4e, x Trichloroethvlene "o i'S,, x Trichlorotluoromethane ;a31s Vinvl chloride it)►75 Others 1,2,4 Trimethyl benzene 1,3,5 Trimethylbenzene x 2.680 0.806 Page 12 of 17 Industrial User Wastewater Survey & Permit Application PART I,' GENERAL INFORMATION (cont): 13.I Do you have. or have you ever applied liar. been issued. or been denied an NPDES permit to discharge to the surface waters or stony sewers of North Carolina'? If yes. list all other NPDES permits. permit numbers. A _ , , dates. anu names used to apple for them, or reason denied ll'Nes Permit . o. date. applicant name Bantam Mart, NCG510464, 10/18/11, Petroleum World, Inc. lt'yes Permit . u. date. applicant name Danieltown, NCG510245, Rescinded 4/26/05, Petroleum World, Inc Yes x No 14.' Do you have. or have you ever applied i'or or been issued an Industrial User Pretreatment Permit OUP) to discharge wastewater to the sewer collection system. If yes. list all other IUP permits. permit numbers. dates. and names used to apply for them. It yes Permit date. applicant name Yes If Lei; Permit .:,. date. applicant name No X 15. Do you have. or have you ever applied for or been issued any other Environmental Permits (for example: air. RCRA. groundwater. stormwater. general. Non -Discharge. septic tank. etc.). if yes, list all Vutcr permILS. permit numbers, dates. and names used to a lf%es. Permit 11pe. date. applicant name II'ves Permit 1%pe. a. date. applicant name If }es. Permit tNpe. ;:. date. applicant name �m. Yes No X 16.1 Is a Spill Prevention Control and Countermeasure (SPCC) Plan prepared for this facility'? If yes. please attach a copy. Yes No x 17J is a Spill /Slug Control Plan required by the POTW. prepared for this facilitv`' Yes No x Page 4 of 17 Industrial User Wastewater Survey & Permit Application PART I, GENERAL INFORMATION cont): 18. Do you have any underground storage tanks at your facility'' If yes. list contents and volume of each tank. r No underground storage tanks to be used on site. Yes No x 19. Do you have any above ()round storage tanks at your facility'' It'yes. for each tank. list the contents. volume. %\Ihetlier- the tank has any spill prevention or containment devices. such as dikes. and procedures for draining any containment devices. Yes I x I r of Tanks No tanks on site at present time. Possible 3,000 to 5,000 gallon No double -walled polytank for temporary site storage prior to discharge may be installed if needed as part of proposed ground- water recovery system. Pa,e 5 of 17 Industrial User Wastewater Survey & Permit Application PART 11, Water Supply, Use, & Disposal Worksheet: m x 9 Water Used for: Ut 11e1 : Pet 1 ul eum i mpac_t ed .1I C1111dwa t e e ? ecove i ed f I om 10111edial re ovely ..:Ils Water Sots rce(s) ^`' gal/daygal!day Max.ti C, -- `r 'l. Disposal Method(s) ^` zal/da\ Max. dal/clay L n -- - - --- Process k\ater \NZIS11down Miller Water into product Ah Qtlillitl Perrllilled lMit-, Domestic - toilets. drinking, cafe Cooling, \%atcr. Process NON-Conlad Roller i Cooling tower blowdomi Cooling %cater. I IVA('- ( (see Source List hclo%\) V (sic Disposal list bcluwl _— 3. 5,715 11,316 x 2. 5,715 11,316 x _ -- _ Totals -- 5 715 11,316 I t't`�Is S 715 11,3161 Typical Water Sources: _ 1. ('its / Public supply- -- ?. Pirate %ells. drinking 3. Cirollndwatcr renlediallon \\ells 4. Private ponds S ace eaters of . please identify 6. Include others if applicable �-Possible Water Disposal Methods I. Sanitar\ se\\er. wilt preUratnlent �.S all, l'�' tie�1 er. \\ ithout prelreatnlenl 3. Storm se\ er 4. Sul -lace \\atcrs of N(' �. F vaporation 6. Land applied 7. -1 o groundwater. R. Septic -tank 9. Waste I laulers (identify) 10. Water into Product 11. Include others. if applicable Page 6 of 17 Industrial User Wastewater Survey & Permit Application PART III, PRETREATMENT FACILITIES: Are there any pretreatment devices or processes used for treating «wastewater before being discharged to the sever? Check all that are present. and describe. No pretreatment facilities => X 1 Flow equalization Aerated equalization => NON -Aerated equalization => 0.005 MG Total volt.rr»e ofequalization (million �gral.) _> 0.005 MG 2. Activated Carbon 3. A'ctivated Sludge 4. Air Stripping 5. Centrifu_ation 6. Chemical Precipitation 7. Chlorination 8. Cyanide Destruction 9. Cyclone 10. Dissolved Air Floatation 11. Filtration 12. Flocculation 13. Grease Trap 14. Grit Removal 15. Ion Exchange 16. Neutralize. pH adjust 17. Other Biological Treatment I8. Ozonation 19. Reverse Osmosis 20. Screening 1. Sedimentation 22. Septic Tank 23. Silver Recover, 24. Solvent Separation 25. Spill protection List any others. I� Ye� Ye; Ye Ye! Ye! Ye! Yes Ye4 Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No No No No No No do No No No No Describe any. if present. Pae7of17 Industrial User Wastewater Survey & Permit Application PART IV, CATEGORICAL INFORMATION: I . When were operations started at this facilitN Facility start up date N/A The facility is anticipated to start operation in April of 2014. 2. Li'st all Standard Industrial Classification (SIC) codes for your facility. These may be found on State Unemployment forms. tax forms. accounting records. or from the Chamber of Commerce. Environmental remediation / clean-up activities at a former Leaking UST site. 3. Has this facility ever been considered a Categorical Industrial User (CIU) as described by the Code of Federal Regulations (40 CFR)? II'yes. give complete 40 CFR number => No X it 4. Are any other facilities owned and/or operated by your company permitted as Categorical Industrial Users (CIUs) as described by the Code of Federal Regulations (40 CFR)? If yes please give name(s). location. and 40 CFR number. Yes No x Page 8 of 17 Industrial User Wastewater Survey & Permit Application PART IV, CATEGORICAL INFORMATION: (continued) 5. Check any activities listed below that are performed at your facility: Check below 40 Industrial Activity it CFR# y Check 40 Industrial Activity below CFR# 467 427 461 43i 407 408 458 411 434 465 468 405 469 413 457 412 424 418 464 426 406 454 460 447 415 420 425 Alurninum Forming Asbestos Manufacturing Battery Manufacturing Builders paper & board mills Canned & preserved fruits & vea. jCanned & preserved seafood Carbon black Manufacturing ;Cement Manufacturing_ Coal Nlininu Coil Coatine ,Copper Forming 'Dairy products processing Electrical. electronic components Electroplating Explosives Manufacturing=_ Feedlots Ferro allay Nanufacturing Fertilizer Xilanufacturing Foundries. Metal Mold & Casting Glass Manufacturim, Grain mills Gum & Wood Chemicals Mt,. Hospitals Ink formulatim, Inorganic chemical Manufacturing Iron & Steel Manufacturing Leather Tanning & Finishing 432 Meat products 433 Metal finishing; 464 :Metal rttolding and castin 436 Mineral raining and processing 471 \onferrous Metal. Form & Powders 421 Nonferrous Metals Manufacturing 414 OCPSF. Organic Chemicals. Plastics. & Synthetic Fiber Manufacturina, 435 Oil & gas extraction 440 Ore mining and dressin, 446 Paint formulating 443 Paving and roofing materials Mfg. 455 Pesticide Manufacturing 419 Petroleum Refining- 439 Pharmaceutical Manufacturing 422 Phosphate 'Manufacturing 459 Photographic supplies 463 Plastics molding and forming 466 Porcelain enameling 430 Pulp. paper. and paperboard 428 Rubber Manufacturina 417 Soap & Detergent lVlanutacturinz 423 Steam Electric power Generation 409 Sugar processing 410 Textile 'dills 429 Timber products processing Others Environmental remediation of former leaking UST site. Nage 9 of 17 Industrial User Wastewater Survey & Permit Application Wastewater Pollutant Checklist Chemical Name EPA Check if Check if Check it' check if Concentration Storet Present at Absent at i Present in :'absent in in Discharge. Code Facilit% Facilitx Discharge Discharge if Kno%,*,n Acid Extractable Organics 2-Chloro henol ll»( 2.4-Dichloro henol x 2.4-Dimethvl phenol 2.4-Dinitro henol 14hIn 2-Methv1-4.6-dinitro henol 1405 4-Chloro-3-methyl henol 2-Nitrophenol 4-Nitro henol Pentachloro henol Phenol 2.4.6-Trichloro henol �-��' I Base Neutral Organics 1.2.4-Trichlorobenzene 1.2-Dichlorobenzene 1.2-Di henvllwdrazine 1.3-Dichloroben7ene 1,4-Dichlorobenzene 34; 7I 2.4-Dinitrotoluene 3-161 I 2.6-Dinitrotoluene 2-Chloronaphthalene ; x 3.3-Dichlorobenzidine sn; I x 4-Bromophem I phem I ether 4-Chlorophenyl phenyl ether x Acenaphthene x Acenaphthylene Anthracene .422() x Benzidine i x Benzo (a) anthracene r�'< Benzo (a) pyrene 14-247 I x Benzo (b) tluoranthene 34,' "+I ; x Benzo (`hi) pen lene - - I x Benzo (k) tluoranthene 3-i24' x Bis(2-ehloroethoxv ) methane 42'8 x Bis(2-chloroeth\1) ether 27 Bis(2-chloroisopropyl) ether ;-:28 Bis(2-ethvIhexv1) phthalate Butyl benzvi phthalate Chrysene ;43-10 Di-n-butyl phthalate Pane I U of 17 Data Summary Form <= Receiving POTW <= Specific Sample Location! i.c.. ( live lU Name. It ►1't!. and/or Iiil)c# I.ab - MI)l Notes , Sample Date 11). or Sample Count Collected b 7 I (1 12 etc �I�NS Max. %aloe--: Avg. (usc 112 BI)l ) = Laboratory hcrti>rming analysis Laboratory Method Detection Limits Notes Q = Flo", Notes about Sample - -- M -= Metered �- I . I :st itnatcd mgd gal/day ----- ------ --- - T ROD TSS Ammonia Conc. Results from 1.111) <? 11101 Conc. Results 11-onl 1,111) <? mgil Conc. Results From I ah <`► mgil Total numhcr ol'samhles Maximum data Value (mg/1) Avg. data value. Include 1311. values as 1/2 detection limit Page 13 of' 17 Data Summary Form <= Receiving POTW <= Specific Sample location! i.e.. (live It I Name. It IF'#. and/or pipe # Arsenic Copper Chromium Cadmium (101) a h -- MI) Notes Cone. Results from Lab <? Cone. Results from Lah <? Illl:/I Cone. Results from I.ah <? nl'I Conc. Results 11-om I.ah G? Conc. Results from I.ah <`� nl���l Cone. Result" from I.ah `� ►/ Sample II) or Count D'He Salllhle Collected �^ 7 lu 12 etc El TN S Max. Value - Avg. (use1/2 BIM) Page 14 o f 17 Data Summary Form <= Receiving 130TW <= Specific Sample Location! - i.e.. (live It I Name. It iP#, and/car pipe H Cyanide lead Xlercury Nickel Silver zinc MIX Notes Conc. Results from I -ah <? m/I Colic. Results From I .ah <? Conc. Results from I .ah <? Cone. Results from I .ah Conc. Results From I.ah <? Conc. Results From I .ah Sample W or Count Date Sample Collected -- - -- - a 7 10 1, etc - -INS Max. Value ,Avg. (usel/2 BI)I,) Page 15 o1" 17 Data Summary Form <= Receiving POTW <= Specific Sample Location! i.e.. (live It I Narne. It ►P#. and/or pipe it Other Other Other Other ---- -_-- Other MIA, Notes Conc. Results 1i•un1 I.ah <? I11/i ('unc. Results from Lab <? ('one. Results from I.ah Curie. Results li-mil I.ah <? m%I Conc. Results From I.ah <? Conc. Results Crum I ah Sample II) ot- COUM Date Sample Collected - I 1 — 9 iU — 1? etc -INS Max. Value nvo. (usel/? BDI.) Page 16 ul' 17 Industrial User Wastewater Survey & Permit Application Part V, Othe,r: Please list any significant changes to the manufacturing processor pretreatment system since the last permit application was submitted: Not Applicable Page 17 of 17 1)1 11 \1, I'T i %I.ul.l Name: i Project: I Units Air Temp. Water Temp' Stripper: Stripper Nax Flow e-mail: T, r. l,: :, 1 1.1.. 1 . Altitude: Flow: n Stripper Air Flow �!I I1 �lripl¢�I �I„del , i r•, .bcr_cc a,. F.'. i hill nut I nm' <onit r7 and prnjc•rt rn/i,rmwiun and I-lirk Sind h, burr a (Ill) "/rrurwrnt npplre Minn +pre irdi.et ronrurl I I Name - 1,11,1 Counpany -- ---- ------- Phone - Fax I'h,nlc - --- -__-- - e-mail - InbolanJvrtihlclJengincering voill Project - [ I rianulc 1 Caacn luµ, 0I'l211 1'V.c, I'll, J nw.pll I' 2 ?1)1 � I % N V4 tl TJ � O Z N � W W W Q U aN w rK Lment:txy or mount molly Description: EFFLUENT Date Sampled:10113/2016 0805 ' Date Received:1011312016 L.aooratory lu: KJ73uto-uu9 Matrix: Aqueous Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 350.1 (Ammonia - N ) 350.1 1 10/20/20161630 BWS 24823 1 (Hardness (to) SM 2340C-2011 1 10120/20161839 MJI 24842 1 (Nitrate-Nitr) 353.2 10 10120/20161910 MSG 24828 1 (Phosphorus) 365.1 10 10/20/2016 0857 KWP 10/18/2016 2330 24665 1 (TDS) SM 254OC-2011 1 10/14/20161011 CLM 24412 1 351.4 (TKN) 351.2 1 10/20/20161815 KWP 10/20120161050 24791 CAS Analytical Parameter Number Method Result Q PQL MDL Units Run Ammonia - N (gas diffusion) 350.1 ND 0.10 0.050 mg/L 1 Hardness (total) SM 234OC-20 34 10 2.0 mg/L 1 Nitrate -Nitrite - N 353.2 15 B 0.20 0.013 mg/L 1 Phosphorus 7723-14-0 365.1 3.3 B 0.10 0.016 mg/L 1 TDS SM 254OC-20 440 10 3.4 mg/L 1 TKN 351.2 2.7 1.3 0.11 mg/L 1 Semivolatile Organic Compounds by GC/MS Run ,Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 10/19/20161713 ECB 10/17/2016 0028 24491 CAS Analytical Parameter Number Method Result Q PQL MDL Units Run Acenaphthene 83-32-9 625 ND 1.6 0.11 ug/L 1 Acenaphthylene 208-96-8 625 ND 1.6 0.060 ug/L 1 Anthracene 120-12-7 625 ND 1.6 0.060 ug/L 1 Benzidine 92-87-5 625 ND 8.0 0.44 ug/L 1 Benzo(a)anthracene 56-55-3 625 ND 1.6 0.070 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 1.6 0.040 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 1.6 0.050 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 1.6 0.12 ug/L 1 Benzo(k)fluoranthene 207-08-9 625 ND 1.6 0.070 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 1.6 0.16 ug/L 1 Butyl benzyl phthalate 85-68-7 625 ND 1.6 0.15 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625 ND 1.6 0.49 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 1.6 0.40 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 1.6 0.48 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 1.6 0.50 ug/L 1 2-Chloronaphthalene 91-58-7 625 ND 1.6 0.40 ug/L 1 2-Chlorophenol 95-57-8 625 ND 1.6 0.34 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 1.6 0.21 ug/L 1 Chrysene 218-01-9 625 ND 1.6 0.050 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625 ND 1.6 0.11 ug/L 1 1,2-Dichlorobenzene 95-50-1 625 ND 1.6 0.46 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 ND 1.6 0.40 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W Shealy Environmental Services, Inc. Page: 5 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylab.com LaDoratory lu: KJ13utb-uul Matrix: Aqueous Laienutaty or mount Mony Description: EFFLUENT Date Sampled:10/1312016 0805 Date Received:10113/2016 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 10/19/20161713 ECB 10/17/2016 0028 24491 CAS Analytical Parameter Number Method Result Q PQL MDL Units Run 1,4-Dichlorobenzene 106-46-7 625 ND 1.6 0.41 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 8.0 1.6 ug/L 1 2,4-Dichlorophenol 120-83-2 625 ND 1.6 0.70 ug/L 1 Diethylphthalate 84-66-2 625 ND 1.6 0.19 ug/L 1 Dimethyl phthalate 131-11-3 625 ND 1.6 0.21 ug/L 1 2,4-Dimethylphenol 105-67-9 625 ND 1.6 0.62 ug/L 1 Di-n-butyl phthalate 84-74-2 625 ND 1.6 0.26 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 8.0 0.69 ug/L 1 2,4-Dinitrophenol 51-28-5 625 ND 8.0 0.65 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 ND 3.2 0.48 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 3.2 0.39 ug/L 1 Di-n-octylphthalate 117-84-0 625 ND 1.6 0.070 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 1.6 0.12 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 1.3 J 1.6 0.19 ug/L 1 Fluoranthene 206-44-0 625 ND 1.6 0.050 ug/L 1 Fluorene 86-73-7 625 ND 1.6 0.060 ug/L 1 Hexachlorobenzene 118-74-1 625 ND 1.6 0.39 ug/L 1 Hexachlorobutadiene 87-68-3 625 ND 1.6 0.47 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625 ND 8.0 0.14 ug/L 1 Hexachloroethane 67-72-1 625 ND 1.6 0.53 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 1.6 0.11 ug/L 1 Isophorone 78-59-1 625 ND 1.6 0.44 ug/L 1 Naphthalene 91-20-3 625 ND 1.6 0.13 ug/L 1 Nitrobenzene 98-95-3 625 ND 1.6 1.1 ug/L 1 2-Nitrophenol 88-75-5 625 ND 3.2 0.88 ug/L 1 4-Nitrophenol 100-02-7 625 ND 8.0 1.2 ug/L 1 N-Nitrosodimethylamine 62-75-9 625 ND 1.6 0.37 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 1.6 0.15 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 1.6 0.25 ug/L 1 Pentachlorophenol 87-86-5 625 ND 8.0 1.4 ug/L 1 Phenanthrene 85-01-8 625 ND 1.6 0.12 ug/L 1 Phenol 108-95-2 625 ND 1.6 0.22 ug/L 1 Pyrene 129-00-0 625 ND 1.6 0.060 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625 ND 1.6 0.57 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 1.6 0.44 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitatlon of compound exceeded the catibration range H = Out of holding time ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40°% N = Recovery Is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a W Shealy Environmental Services, Inc. Page: 6 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com t,;ilent:uity or mount noiry t-aDoratory iu: KAMID-UUI Description: EFFLUENT Matrix: Aqueous Date Sampled:10/13/2016 0805 Date Received: 1Oil 312016 Run 1 Acceptance Surrogate 0 % Recovery Limits 2-Fluorobiphenyl 78 37-129 2-Fluorophenol 36 24-127 Nitrobenzene-d5 78 38-127 Phenol-d5 50 28-128 Terphenyl-d14 66 10-148 2,4,6-Tribromophenol 81 41-144 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 10/14/2016 2154 BNW 10/14/2016 0922 24391 CAS Analytical Parameter Number Method Result 0 PQL MDL Units Run Antimony 7440-36-0 200.8 0.022 0.001 0.00017 mglL 1 Arsenic 7440-38-2 200.8 0.00037 J 0.001 0.00026 mglL 1 Beryllium 7440-41-7 200.8 ND 0.0004 0.00012 mg/L 1 Cadmium 7440-43-9 200.8 5.7E-5 J 0.0001 4.4E-5 mg/L 1 Chromium 7"0-47-3 200.8 0.0093 0.005 0.00063 mglL 1 Copper 7440-50-8 200.8 0.028 B 0.001 0.00015 mg/L 1 Lead 7439-92-1 200.8 0.001 0.001 0.00015 mg/L 1 Nickel 7440-02-0 200.8 0.003 J 0.005 0.00063 mg/L 1 Selenium 7782-49-2 200.8 ND 0.001 0.00095 mg/L 1 Silver 7440-22-4 200.8 ND 0.001 0.00017 mg/L 1 Thallium 7440-28-0 200.8 ND 0.0005 7.5E-5 mg/L 1 Zinc 7440-66-6 200.8 0.055 0.01 0.0016 mg/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W Shealy Environmental Services, Inc. Page: 7 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shestylab.com calent:uity or Mount nosy Description: EFFLUENT Date Sampled:10113/2016 0825 Date Received:10113/2016 Laaoratory III.): KJ93U/b-UUL Matrix: Aqueous Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- 1 10/20/2016 1200 KWP 10/20/20161017 24800 1 (Phenolics) 420.4 1 10/21/20161025 BWS 10/20/20161330 24810 1 (HEM (oil and)1664B 1 10/18/2016 0000 ARP 24590 CAS Analytical Parameter Number Method Result Q PQL MDL Units Run Cyanide - Total 57-12-5 SM 4500-CN 0.026 J 0.030 0.024 mg/L 1 Phenolics 420.4 0.048 0.010 0.0040 mg/L 1 HEM (oil and grease) 1664E 1.5 J 4.1 1.4 mg/L 1 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 624 624 1 10/15/2016 0108 ECP 24472 CAS Analytical Parameter Number Method Result Q PQL MDL Units Run Acrolein 107-02-8 624 ND 5.0 4.0 ug/L 1 Acrylonitrile 107-13-1 624 ND 5.0 0.80 ug/L 1 Benzene 71-43-2 624 ND 1.0 0.40 ug/L 1 Bromodichloromethane 75-27-4 624 3.8 1.0 0.40 ug/L 1 Bromoform 75-25-2 624 3.3 1.0 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 2.0 0.40 ug/L 1 Carbon tetrachloride 56-23-5 624 ND 1.0 0.40 ug/L 1 Chlorobenzene 108-90-7 624 ND 1.0 0.40 ug/L 1 Chloroethane 75-00-3 624 ND 2.0 0.40 ug/L 1 2-Chloroethylvinylether 110-75-8 624 ND 5.0 0.40 ug/L 1 Chloroform 67-66-3 624 1.1 1.0 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 2.0 0.40 ug/L 1 Dibromochloromethane 124-48-1 624 5.5 1.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 624 ND 1.0 0.40 ug/L 1 1,3-Dichlorobenzene 541-73-1 624 ND 1.0 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 624 ND 1.0 0.40 ug/L 1 Dichlorodiftuoromethane 75-71-8 624 ND 2.0 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 624 ND 1.0 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 624 ND 1.0 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 624 ND 1.0 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 624 ND 1.0 0.40 ug/L 1 trans-1,2-Dichloroethene 156-60-5 624 ND 1.0 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 624 ND 1.0 0.40 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 1.0 0.40 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 1.0 0.40 ug/L 1 Ethylbenzene 100-41-4 624 ND 1.0 0.40 ug/L 1 Methylene chloride 75-09-2 624 ND 1.0 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 1.0 0.40 ug/L 1 PQL = Practical quantitation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a -W- Shealy Environmental Services, Inc. Page: 8 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Laient:taty or mount Moiiy Description: EFFLUENT , Date Sampled:10/13/2016 0825 Date Received:1011312016 Laooratory iu: KJ1suto-uuz Matrix: Aqueous Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 624 624 1 10/15/2016 0108 ECP 24472 CAS Analytical Parameter Number Method Result Q PQL MDL Units Run Tetrachloroethene 127-18-4 624 ND 1.0 0.40 ug/L 1 Toluene 108-88-3 624 ND 1.0 0.40 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 624 ND 1.0 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 624 ND 1.0 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 624 ND 1.0 0.40 ug/L 1 Trichloroethene 79-01-6 624 ND 1.0 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 624 ND 1.0 0.40 ug/L 1 Vinyl chloride 75-01-4 624 ND 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 112 70-130 Toluene-d8 102 70-130 Bromofluorobenzene 97 70-130 PQL = Practical quantilation limit B = Detected in the method blank E = Quentitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W' Shealy Environmental Services, Inc. Page: 9 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheal&b.com t;liencLaty or mount Irtony Description: EFFLUENT Date Sampled:07/24/2015 0805 Date Received:07/24/2015 i-aDoratory lu: wuz4u5s-uui Matrix: Aqueous Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 350.1 (Ammonia - N ) 350.1 1 07/31/20151029 BWS 07/30/20151522 81127 1 (Hardness (to) SM 2340C-2011 1 07/29/2015 1714 HMA 81009 1 (Nitrate-Nitr) 353.2 15 07/30/2015 2142 ECP 81155 1 (Phosphorus) 365.1 10 07/29/20151141 BWS 07/28/20151141 80840 1 (TDS) SM 254OC-2011 1 07/27/2015 1447 BLO 80748 1 351.4 (TKN) 351.2 1 07/30/2015 1607 BWS 07/28/2015 1143 80842 CAS Analytical Parameter Number Method Result Q PQL Units Run Ammonia - N (phonate) 350.1 0.64 0.10 mg/L 1 Hardness (total) SM 234OC-20 42 10 mg/L 1 Nitrate -Nitrite - N 353.2 26 0.30 mg/L 1 Phosphorus 7723-14-0 .365.1 3.4 0.10 mg/L 1 TDS SM 2540C-20 470 10 mg/L 1 TKN 351.2 1.5 0.50 mg/L 1 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 08/12/2015 1528 DRB1 07/27/20151014 80696 CAS Analytical Parameter Number Method Result Q PQL Units Run Acenaphthene 83-32-9 625 ND 2.0 ug/L 1 Acenaphthylene 208-96-8 625 ND 2.0 ug/L 1 Anthracene 120-12-7 625 ND 2.0 ug/L 1 Benzidine 92-87-5 625 ND 10 ug/L 1 Benzo(a)anthracene 56-55-3 625 ND 2.0 ug/L 1 Benzo(a)pyrene 50-32-8 625 ND 2.0 ug/L 1 Benzo(b)fluoranthene 205-99-2 625 ND 2.0 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625 ND 2.0 ug/L 1 Benzo(k)fluoranthene 207-08-9 625 ND 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625 ND 2.0 ug/L 1 Butyl benzyl phthalate 85-68-7 625 ND 10 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625 ND 2.0 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625 ND 2.0 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625 ND 2.0 ug/L 1 bis (2-Chloro-l-methylethyl) ether 108-60-1 625 ND 2.0 ug/L 1 2-Chloronaphthalene 91-58-7 625 ND 2.0 ug/L 1 2-Chlorophenol 95-57-8 625 ND 2.0 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625 ND 2.0 ug/L 1 Chrysene 218-01-9 625 ND 2.0 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625 ND 2.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625 ND 2.0 ug/L 1 1,3-Dichlorobenzene 541-73-1 625 ND 2.0 ug/L 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W" Shealy Environmental Services, Inc. Page: 5 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylab.com t ment: t;;ity or mount molly Description: EFFLUENT Date Sampled:07/24/2015 0805 Date Received:07/24/2015 t-aDoratory tu: uuz4uas-uui - -.,,Matrix: Aqueous Semivolatile Organic Compounds by GUMS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625 625 1 08/12/2015 1528 DRB1 07/27/20151014 80696 CAS Analytical Parameter Number Method Result Q PQL Units Run 1.4-Dichlorobenzene 106-46-7 625 ND 2.0 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625 ND 10 ug/L 1 2,4-Dichlorophenol 120-83-2 625 ND 2.0 ug/L 1 Diethylphthalate 84-66-2 625 ND 10 ug/L 1 Dimethyl phthalate 131-11-3 625 ND 10 ug/L 1 2,4-Dimethylphenol 105-67-9 625 ND 2.0 ug/L 1 Di-n-butyl phthalate 84-74-2 625 ND 10 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625 ND 10 ug/L 1 2,4-Dinitrophenol 51-28-5 625 ND 10 ug/L 1 2,4-Dinitrotoluene 121-14-2 625 ND 4.0 ug/L 1 2,6-Dinitrotoluene 606-20-2 625 ND 4.0 ug/L 1 Di-n-octylphthalate 117-84-0 625 ND 10 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625 ND 2.0 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625 ND 10 ug/L 1 Fluoranthene 206-44-0 625 ND 2.0 ug/L 1 Fluorene 86-73-7 625 ND 2.0 ug/L 1 Hexachlorobenzene 118-74-1 625 ND 2.0 ug/L 1 Hexachlorobutadlene 87-68-3 625 ND 2.0 ug/L 1 Hexachlorocyclopentadiene 7747-4 625 ND 10 ug/L 1 Hexachloroethane 67-72-1 625 ND 2.0 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625 ND 2.0 ug/L 1 Isophorone 78-59-1 625 ND 2.0 ug/L 1 Naphthalene 91-20-3 625 ND 2.0 ug/L 1 Nitrobenzene 98-95-3 625 ND 2.0 ug/L 1 2-Nitrophenol 88-75-5 625 ND 4.0 ug/L 1 4-Nitrophenol 100-02-7 625 ND 10 ug/L 1 N-Nitrosodimethylamine 62-75-9 625 ND 2.0 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625 ND 2.0 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625 ND 2.0 ug/L 1 Pentachlorophenol 87-86-5 625 ND 10 ug/L 1 Phenanthrene 85-01-8 625 ND 2.0 ug/L 1 Phenol 108-95-2 625 ND 2.0 ug/L 1 Pyrene 129-00-0 625 ND 2.0 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625 ND 2.0 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625 ND 2.0 ug/L 1 PQL = Practical quantitatlon limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W Shealy Environmental Services, Inc. Page: 6 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com talent: t:iry or Mount Molry I-aDoratory IU: QU24uos-uu1 Description: EFFLUENT Matrix: Aqueous Date Sampled:07/24/2015 0805 Date Received:0712412015 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 67 37-129 2-Fluorophenol 116 24-127 Nitrobenzene-d5 74 38-127 Phenol-d5 76 28-128 Terphenyl-d 14 37 10-148 2,4,6-Tribromophenol 71 41-144 ICP-MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 200.2 200.8 1 07/28/2015 0129 CDF 07/27/2015 0935 80688 2 200.2 200.8 1 07/29/2015 0333 CDF 07/27/2015 0935 80688 CAS Analytical Parameter Number Method Result Q PQL Units Run Antimony 7440-36-0 200.8 41 1.0 ug/L 1 Arsenic 7440-38-2 200.8 2.5 1.0 ug1L 1 Beryllium 7440-41-7 200.8 ND 0.40 ug/L 2 Cadmium 7440-43-9 200.8 ND 0.10 ug/L 1 Chromium 7440-47-3 200.8 7.2 5.0 ug/L 1 Copper 7440-50-8 200.8 31 1.0 ug/L 2 Lead 7439-92-1 200.8 ND 1.0 ug/L 1 Nickel 7440-02-0 200.8 ND 5.0 ug/L 1 Selenium 7782-49-2 200.8 6.3 1.0 ug/L 1 Silver 7440-22-4 200.8 ND 1.0 ug/L 1 Thallium 7440-28-0 200.8 ND 0.50 ug/L 1 Zinc 7440-66-6 200.8 65 10 ug/L 2 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W- Shealy Environmental Services, Inc. Page: 7 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Viienutaty oT mount rtoity Description: EFFLUENT Date Sampled:07/2412015 0815 Date Received:0712412015 t-aDoratory tu: Uuzauas-uuz - ,.Matrix: Aqueous Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- 1 07/28/2015 1717 BWS 07/28/2015 1500 80848 1 (Phenolics) 420.4 1 07/30/20151123 MJI 07/30/2015 0915 81071 1 (HEM (oil and)1664B 1 07/30/2015 0953 HKB 81069 CAS Analytical Parameter Number Method Result Q PQL Units Run Cyanide - Total 57-12-5 SM 4500-CN ND 0.010 mg/L 1 Phenolics 420.4 ND 0.020 mg/L 1 HEM (oil and grease) 1664B ND 4.4 mg/L 1 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 08/03/20151546 ALL 81339 CAS Analytical Parameter Number Method Result Q PQL Units Run Acrolein 107-02-8 624 ND 50 ug/L 1 Acrylonitrile 107-13-1 624 ND 50 ug/L 1 Benzene 71-43-2 624 ND 5.0 ug/L 1 Bromodichloromethane 75-27-4 624 5.9 5.0 ug/L 1 Bromofonm 75-25-2 624 25 5.0 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 624 ND 5.0 ug/L 1 Carbon tetrachloride 56-23-5 624 ND 5.0 ug/L 1 Chlorobenzene 108-90-7 624 ND 5.0 ug/L 1 Chloroethane 75-00-3 624 ND 5.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624 ND 10 ug/L 1 Chloroform 67-66-3 624 ND 5.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624 ND 5.0 ug/L 1 Dibromochloromethane 124-48-1 624 18 5.0 ug/L 1 1,1-Dichloroethane 75-34-3 624 ND 5.0 ug/L 1 1,2-Dichloroethane 107-06-2 624 ND 5.0 ug/L 1 1,1-Dichloroethene 75-35-4 624 ND 5.0 ug/L 1 trans- l,2-Dichloroethene 156-60-5 624 ND 5.0 ug/L 1 1,2-Dichloropropane 78-87-5 624 ND 5.0 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 624 ND 5.0 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 624 ND 5.0 ug/L 1 Ethylbenzene 100-41-4 624 ND 5.0 ug/L 1 Methylene chloride 75-09-2 624 ND 5.0 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 624 ND 5.0 ug/L 1 Tetrachloroethene 127-18-4 624 ND 5.0 ug/L 1 Toluene 108-88-3 624 ND 5.0 ug/L 1 1, 1, 1 -Trichloroethane 71-55-6 624 ND 5.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 624 ND 5.0 ug/L 1 Trichloroethene 79-01-6 624 ND 5.0 ug/L 1 PQL = Practigpl quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40°% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W" Shealy Environmental Services, Inc. Page: 8 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.sheatylab.com c:Itent: t:ity or Mount holly Description: EFFLUENT - Date Sampled:07124/2015 0815 Date Received:07/2412015 L.awratory IU: QUZ4UbJ-UUZ Matrix: Aqueous Volatile Organic Compounds by GUMS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 624 1 08103/20151546 ALL 81339 CAS Analytical Parameter Number Method Result Q PQL Units Run Vinyl chloride 75-014 624 ND 5.0 ug/L 1 Surrogate Run 1 Acceptance Q % Recovery Limits 1,2-Dichloroethane-d4 90 70-130 Bromofluorobenzene 108 70-130 Toluene-d8 94 70-130 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W' Shealy Environmental Services, Inc. Page: 9 of 9 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com