WI0501062_Permit (Issuance)_20201027

October 13, 2020
North Carolina Department of Environmental and Natural Resources
Department of Water Resources
UIC Program
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
Dear Sir or Madam:
Reference No. 11219094
Re: Notification of Intent to Construct or Operate Injection Wells
Portion of Rocky Mount Fiber Dump (American Fibers and Yarns)
Atlantic Avenue, Rocky Mount, Edgecombe County, North Carolina (Site)
NCD041466525 - Docket No. 12-SF-357 (Former Docket No. 10-SF-336)
On behalf of Phillips 66 Company, GHD is submitting the enclosed Notification of Intent to Construct or
Operate Injection Wells (Notification) for the above -referenced Site. The Site is currently managed under
the Division of Waste Management, Inactive Hazardous Sites Branch, Registered Environmental
Consultant (REC) Program. On June 25, 2015, GHD submitted a certified Remedial Action Plan -
Groundwater (Groundwater RAP) for the site that proposed treatment of impacted groundwater using
chemical injection.
There are two areas of impacted groundwater at the Site and are located on separate parcels with
different owners. The first area is identified as the Dowtherm A Area and is located on the 1245 Atlantic
Avenue parcel for which a separate Notification has been provided. The second area is identified as the
Former Landfill Area and is located on the 1301 Atlantic Avenue parcel for which this Notification is being
submitted.
Groundwater in the Former Landfill Area is impacted with chlorinated volatile organic compounds,
diphenyl ether, and/or 1,1-biphenyl. The areas demonstrating the greatest concentrations of these
compounds will be addressed through the injection of an injectable liquid activated carbon (PlumeStop by
Regenesis) to adsorb contaminants and the injection of oxygen (ORC-Advanced by Regenesis) that will
be released over time to stimulate aerobic biodegradation. Both injectants have been approved by the
North Carolina Department Human and Health Services for injection into groundwater; however,
PlumeStop was approved with stipulations. As required by the stipulations, a potable well survey has been
included as Attachment D of this submittal which indicates there are no public or private water wells within
2,000 feet downgradient of the application area. Additionally, there are no designated surface water
supplies within 1,500 feet downgradient of the application area and Figure 1 included in Attachment C
provides the location of the monitoring well network present at the Site. The enclosed notification is for a
small-scale injection operation for an area less than or equal to10,000 square feet. The injection will be
performed in accordance with the rules specified in 15A NCAC 02C .0225.
GHD O 1 900
3075 Breckinridge Boulevard Suite 470 Duluth Georgia 30096 USA IS1S FERi�E$i 1
T 770 441 0027 F 770 441 2050 W www.ghd.com

If you have any questions, please contact the undersigned at [phone].
Sincerely,
GHD
John A. DiZinno, P.E.
JAD/da/2
Encl.
cc: Ed Kuhn, Phillips 66 Company
NCDE — 11219094Notifcation of Intent2

GHD I NCDE — 11219094Notification of Intent2

Attachment A
Notification of Intent (NOI)

NC Department of Environmental Quality — Division of Water Resources (DWR)
NOTIFICATION OF INTENT (NOI) TO CONSTRUCT OR OPERATE INJECTION WELLS
The following are `permitted by rule" and do not require an individual permit when constructed in accordance
with the rules of 15A NCAC 02C.0200 (NOTE: This form must be received at least 14 DAYS prior to injection)
AQUIFER TEST WELLS (15A NCAC 02C .0220)
These wells are used to inject uncontaminated fluid into an aquifer to determine aquifer hydraulic characteristics.
IN SITU REMEDIATION (15A NCAC 02C .02251 or TRACER WELLS (15A NCAC 02C .0229):
1) Passive Injection Systems - In -well delivery systems to diffuse injectants into the subsurface. Examples include
ORC socks, iSOC systems, and other gas infusion methods (Note: Injection Event Records (IER) do not need to be
submitted for replacement of each sock used in ORC systems).
2) Small -Scale Injection Operations — Injection wells located within a land surface area not to exceed 10,000
square feet for the purpose of soil or groundwater remediation or tracer tests. An individual permit shall be required
for test or treatment areas exceeding 10,000 square feet.
3) Pilot Tests - Preliminary studies conducted for the purpose of evaluating the technical feasibility of a
remediation strategy in order to develop a full scale remediation plan for future implementation, and where the
surface area of the injection zone wells is located within an area that does not exceed five percent of the land surface
above the known extent of groundwater contamination. An individual permit shall be required to conduct more
than one pilot test on any separate groundwater contaminant plume.
4) Air Injection Wells - Used to inject ambient air to enhance in -situ treatment of soil or groundwater.
5) In -Situ Thermal Wells (IST) — Used to `heat' contaminated groundwater to enhance remediation.
Print Clearly or Type Information. Illegible Submittals Will Be Returned as Incomplete.
DATE: October 12, 2020 PERMIT NO. W10501062 (to be filled in by DWR)
NOTE- If this NOI is being submitted as notification of a modification of a previously issued NOI for this site (e.g.,
different injection wells, plume, additives, etc.) and still meets the deemed permitted by rule criteria, provide the
previously assigned permit tracking number and any needed relevant information to assess and approve injection:
Permit No.
Issued Date:
A. WELL TYPE TO BE CONSTRUCTED OR OPERATED
(1)
Air Injection Well .......................................
Complete sections B through F, J, M
(2)
Aquifer Test Well .......................................
Complete sections B through F, J, M
(3)
Passive Injection System ...............................
Complete sections B through F, H-M
(4)
(XX)_Small-Scale Injection Operation ......................
Complete sections B through M
(5)
Pilot Test .................................................
Complete sections B through M
(6)
Tracer Injection Well ...................................
Complete sections B through M
(7)
In -Situ Thermal (IST) Well ...........................
Complete sections B through M
B. STATUS OF WELL OWNER: Business/Organization
Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 1

C.
D.
F.
G.
WELL OWNER(S) — State name of Business/Agency, and Name and Title of person delegated authority to
sign on behalf of the business or agency:
Name(s): Phillips 66 Company Atm. Ed Kuhn
Mailing Address: c/o GHD 222 S. Church St. Suite 400
City: Charlotte State: NC_ Zip Code: 28202 County: Mecklenberg
Day Tele No.: 980-209-6353 Cell No.: 704-975-3000
EMAIL Address: Ed. Kuhn(&contractor.p66.com Fax No.:
PROPERTY OWNER(S) (if different than well owner/applicant)
Name and Title: Charles Duckworth, Owner
Company Name Individual
Mailing Address: P.O. Box 14
City: Rocky Mount
State: NC Zip Code:27802
County: Edgecombe
Day Tele No.: 252-442-1536 Cell No.:
EMAIL Address: dfrinc2000(kaol.com Fax No.:
E. PROJECT CONTACT (Typically Environmental Consulting/Engineering Firm)
Name and Title: John DiZinno Engineer
Company Name GHD
Mailing Address: 3075 Breckinridge Blvd, Suite 470
City: Duluth State: GA Zip Code:30096 County: Gwinnett
Day Tele No.: 678-280-2121 Cell No.: 470-345-2317
EMAIL Address: john.dizinno(kghd.com Fax No.: 770-441-2050
PHYSICAL LOCATION OF WELL SITE
(1) Facility Name & Address: 1301 Atlantic Avenue
City: Rocky Mount County. Edgecombe Zip Code: 27801
(2) Geographic Coordinates: Latitude": 35 ° 57 ' 55.74 " or °
Longitude": 77
° 46 ' 42.77 " or °
Reference Datum: NAD83 (NSRS2007) Accuracy: 0.08 feet
Method of Collection: Professional Land Survey
"FOR AIR INJECTION AND AQUIFER TEST WELLS ONLY: A FACILITY SITE MAP WITH PROPERTY
BOUNDARIES MAY BE SUBMITTED IN LIEU OF GEOGRAPHIC COORDINATES.
TREATMENT AREA
Land surface area of contaminant plume: 30,000 square feet
Land surface area of inj. well network: 600 square feet (< 10,000 ft2 for small-scale injections)
Percent of contaminant plume area to be treated: —10% (must be < 5% of plume for pilot test injections)
Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 2

H. INJECTION ZONE MAPS — Attach the following to the notification.
(1) Contaminant plume map(s) with isoconcentration lines that show the horizontal extent of the
contaminant plume in soil and groundwater, existing and proposed monitoring wells, and existing and
proposed injection wells; and
(2) Cross-section(s) to the known or projected depth of contamination that show the horizontal and vertical
extent of the contaminant plume in soil and groundwater, changes in lithology, existing and proposed
monitoring wells, and existing and proposed injection wells.
(3) Potentiometric surface map(s) indicating the rate and direction of groundwater movement, plus existing
and proposed wells.
I. DESCRIPTION OF PROPOSED INJECTION ACTIVITIES AT THE SITE — Provide a brief narrative
regarding the cause of the contamination, and purpose, scope, goals of the proposed injection activity:
The purpose of the proposed injection is to treat localized areas of groundwater contaminated with 1,1-biphen 1,
and/or diphenyl ether and chlorinated VOCs. The proposed injection of ORC-Advanced and P1umeStop is
expected to stimulate aerobic biodegradation of the contaminants to concentrations below the 2L Standards.
Thirty-nine (39) Gallons of a 30% ORC Advanced® solution will be injected into the subsurface (8 to 20 feet
below grade) into each of 6 DPT boreholes and approximatelypounds of P1umeStop (552 gallons of
solution) will be injected into each of 14 DPT boreholes in the vicinity of well LF-20. The injection area near
LF-20 is 30 feet x 20 feet. The iniectants will be delivered at low pressure (less than 20 psi) and at less than 10
gpm in a single application. Quarterly post -injection groundwater monitoring will be performed on LF-20 to
assess performance.
J. WELL CONSTRUCTION DATA
(1) No. of injection wells: 20 DPT Points Proposed Existing (provide NC Well
Construction Record (GW-1) for each well)
(2) Appx. injection depths (BLS): 20 feet
(3) For Proposed wells or Existing wells not having GW-1s, provide well construction details for each
injection well in a diagram or table format. A single diagram or line in a table can be used for
multiple wells with the same construction details. Well construction details shall include the
following (indicate if construction is proposed or as -built): See Section I. Above
(a) Well type as permanent, Geoprobe/DPT, or subsurface distribution infiltration gallery
(b) Depth below land surface of casing, each grout type and depth, screen, and sand pack
(c) Well contractor name and certification number
K. INJECTION SUMMARY
NOTE: Onlv iniectants avvroved by the evidemiolo,2v section of the NC Division ofPublic Health. Devartment
of Health and Human Services can be iniected. Approved iniectants can be found online at
hiip: Hdeq.nc. gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/ground-water-
protection/ground-water-approved-injectants. All other substances must be reviewed by the DHHS prior to use.
Contact the UIC Proms for more info if you wish to approval for a different additive. However, please
note it may take 3 months or longer. If no injectants are to be used use N/A.
Injectant: ORC Advanced® by Regenesis Total Amt. to be injected (gal)/event: 234 gallons
Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 3

Injectant: PltimeSto l by Regenesis Total Amt. to be injected (gal)levent: 7,734 gallons
Injectant; Total Amt. to be injected (gal)/event:
Injectantt
Total Amt. to be injected (gal)levent:
Injectant: Total Amt. to be injected (gal)levent:
Total Amt. to be injected (gal(event):
No. of separate injection events: I Total Amt. to be injected (gal): 7,968 -allons
Source of Water (if applicable): Local Fire Hydrant _
L. MONITORING PLAN — Describe below or in separate attachment a monitoring plan to be used to determine
if violations of groundwater quality standards specified in Subchapter 02L result from the injection activity.
Groundwater monitoring of select monitoring wells will occur quarterly following the injcetion as prescribed in
the Groundwater RAP p=ared and submitted under the VoIun Cleanup Prognun by the Re istered
Environmental Consultant (REC).
M. SIGNATURE OF APPLICANT AND PROPERTY OWNER
Well OwnerlApplicant: "I hereby cert fy, under penalty of law, that I am familiar with the information
submitted in this document and all attachments thereto and that, based on my ingu;ry of those individuals
immediately responsible for obtaining said information, 1 believe that the information is true, accurate and
complete. 1 am aware that there are significant penalties, including the possibility of fines and imprisonment,
for submitting false information. I agree to construct, operate, maintain, repair, and if applicable, abandon the
injection well and al{related appurtenances in accordance with the 15A NC.4C 02C 02ij!`I Rules.
Signature of Applicant Print orType Full Name and Title
PrWerty Owner if the pLoe is not owned by the Well Owner/Applicant);
"As owner of the property on which the injection wells} are to be constructed and operated, 1 hereby consent to
allow the applcant to construct each injection well as outlined in this application and agree that it shall he the
responsibility of the applicant to ensure that the injection well(s) conform to the Well Construction Standards
(15A NCAC 02C.02001. "
"Owner" means any person who holds the fee or other property rights in the well being constructed. A well
is real property and its construction on land sha:l be deemed to vest ownership in the land owner, in the
absence of contrary agreement in writing.
Refer to Attached Access A reement Att E Charles Duckworth Owner
Signature* of Property Owner (if different Tram applicant) Print or Type Full Flame and Title
*An access agreement between the applicant and property owner may be submitted in lieu oJa signature on this form.
Please send 1 (one) hard color copy of this NOi alongwith a copy on an attached CD or Flash Drive at least
two (2) weeks prior to injection to:
DWR — UIC Program
1636 Mail Service Center
Raleigh, NC 27699-1636
Telephone: (�19) 707-9000
Deemed permitted GW Rem.-diatinn NDt Rev. 2-17-2020 Page 4

GHD I NCDE — 11219094Notification of Intent2

64 REGENESIS
Technology -Based Solutions for the Environment
1. Identification
Product identifier
Other means of identification
Recommended use
Recommended restrictions
SAFETY DATA SHEET
Oxygen Release Compound Advanced (ORC Advanced®)
None.
Soil and Groundwater Remediation.
None known.
Manufacturer/Importer/Supplier/Distributor information
Company name Regenesis
Address 1011 Calle Sombra
San Clemente, CA 92673 USA
General information 949-366-8000
E-mail [e-mail]
Emergency phone number For Hazardous Materials Incidents ONLY (spill, leak, fire, exposure or accident), call
CHEMTREC 24/7 at:
USA, Canada, Mexico (+)1-800-424-9300
International (+)1-703-527-3887
2. Hazard identification
Physical hazards Oxidising solids Category 2
Health hazards Skin corrosion/irritation Category 2
Serious eye damage/eye irritation Category 1
Specific target organ toxicity following single Category 3 respiratory tract irritation
exposure
Label elements
< > >
Signal word Danger
Hazard statement May intensify fire; oxidiser. Causes skin irritation. Causes serious eye damage. May cause
respiratory irritation.
Precautionary statement
Prevention Keep away from heat, hot surfaces, sparks, open flames and other ignition sources. No smoking.
Keep away from clothing and other combustible materials. Avoid breathing dust. Wash thoroughly
after handling. Use only outdoors or in a well -ventilated area. Wear protective gloves/protective
clothing/eye protection/face protection.
Response IF ON SKIN: Wash with plenty of water. IF INHALED: Remove person to fresh air and keep
comfortable for breathing. IF IN EYES: Rinse cautiously with water for several minutes. Remove
contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON
CENTRE/doctor. If skin irritation occurs: Get medical advice/attention. Take off contaminated
clothing and wash it before reuse. In case of fire: Use appropriate media to extinguish.
Storage Store in a well -ventilated place. Keep container tightly closed. Store locked up.
Disposal Dispose of contents/container in accordance with local/regional/national/international regulations.
Other hazards None known.
Supplemental information None.
3. Composition/information on ingredients
Mixtures
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 1/8

Chemical name Common name and CAS number %
synonyms
Calcium peroxide 1305-79-9 >_75
Calcium hydroxide 1305-62-0 <_25
Dipotassium Phosphate 7758-11-4 <5
Monopotassium Phosphate 7778-77-0 <5
Composition comments All concentrations are in percent by weight unless otherwise indicated.
4. First -aid measures
Inhalation
Remove victim to fresh air and keep at rest in a position comfortable for breathing. Call a POISON
CENTRE or doctor/physician if you feel unwell.
Skin contact
IF ON CLOTHING: rinse immediately contaminated clothing and skin with plenty of water before
removing clothes. Rinse skin with water/shower. If skin irritation occurs: Get medical
advice/attention. Wash contaminated clothing before reuse.
Eye contact
Do not rub eyes. Immediately flush eyes with plenty of water for at least 15 minutes. Remove
contact lenses, if present and easy to do. Continue rinsing. Get medical attention immediately.
Ingestion
Never give anything by mouth to a victim who is unconscious or is having convulsions. Rinse
mouth. Do not induce vomiting. If vomiting occurs, keep head low so that stomach content doesn't
get into the lungs. Get medical attention if symptoms occur.
Most important
Severe eye irritation. Symptoms may include stinging, tearing, redness, swelling, and blurred
symptoms/effects, acute and
vision. Permanent eye damage including blindness could result. Dusts may irritate the respiratory
delayed
tract, skin and eyes. Skin irritation. May cause redness and pain.
Indication of immediate
Provide general supportive measures and treat symptomatically. Keep victim under observation.
medical attention and special
Symptoms may be delayed.
treatment needed
General information
Take off all contaminated clothing immediately. Contact with combustible material may cause fire.
Ensure that medical personnel are aware of the material(s) involved, and take precautions to
protect themselves. Wash contaminated clothing before reuse.
5. Fire -fighting measures
Suitable extinguishing media
Water spray, fog (flooding amounts). Foam. Dry chemical powder. Carbon dioxide (CO2).
Unsuitable extinguishing
None known.
media
Specific hazards arising from
Greatly increases the burning rate of combustible materials. Containers may explode when
the chemical
heated. During fire, gases hazardous to health may be formed. Combustion products may include:
metal oxides.
Special protective equipment
Self-contained breathing apparatus and full protective clothing must be worn in case of fire.
and precautions for firefighters
Fire fighting
In case of fire and/or explosion do not breathe fumes. Move containers from fire area if you can do
equipment/instructions
so without risk. Use water spray to cool unopened containers.
Specific methods
Cool containers exposed to flames with water until well after the fire is out.
General fire hazards
May intensify fire; oxidiser. Contact with combustible material may cause fire.
6. Accidental release measures
Personal precautions, Keep unnecessary personnel away. Keep people away from and upwind of spill/leak. Keep away
protective equipment and from clothing and other combustible materials. Wear appropriate protective equipment and
emergency procedures clothing during clean-up. Use a NIOSH/MSHA approved respirator if there is a risk of exposure to
dust/fume at levels exceeding the exposure limits. Do not touch damaged containers or spilled
material unless wearing appropriate protective clothing. Ensure adequate ventilation. Local
authorities should be advised if significant spillages cannot be contained. For personal protection,
see section 8 of the SDS.
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 2/8

Methods and materials for Eliminate all ignition sources (no smoking, flares, sparks, or flames in immediate area). Collect
containment and cleaning up dust using a vacuum cleaner equipped with HEPA filter. Keep combustibles (wood, paper, oil etc)
away from spilled material. Ventilate the contaminated area. Stop the flow of material, if this is
without risk. Absorb in vermiculite, dry sand or earth and place into containers.
Large Spills: Sweep up or vacuum up spillage and collect in suitable container for disposal. Shovel
the material into waste container. Minimise dust generation and accumulation. Avoid the
generation of dusts during clean-up. Following product recovery, flush area with water.
Small Spills: Wipe up with absorbent material (e.g. cloth, fleece). Clean surface thoroughly to
remove residual contamination.
Never return spills to original containers for re -use. Place all material into loosely covered plastic
containers for later disposal. For waste disposal, see section 13 of the SIDS. Wear appropriate
protective equipment and clothing during clean-up.
Environmental precautions Avoid discharge into drains, water courses or onto the ground.
7. Handling and storage
Precautions for safe handling Minimise dust generation and accumulation. Routine housekeeping should be instituted to ensure
that dusts do not accumulate on surfaces. Keep away from heat. Provide appropriate exhaust
ventilation at places where dust is formed. Keep away from clothing and other combustible
materials. Take any precaution to avoid mixing with combustibles. Avoid contact with water and
moisture. Do not get this material in contact with eyes. Avoid contact with eyes, skin, and clothing.
Avoid prolonged exposure. Wear appropriate personal protective equipment. Observe good
industrial hygiene practices.
Conditions for safe storage, Keep away from heat. Store in a cool, dry place out of direct sunlight. Store in original tightly
including any incompatibilities closed container. Keep container tightly closed. Store in a well -ventilated place. Do not store near
combustible materials. Store away from incompatible materials (see Section 10 of the SDS).
8. Exposure controls/personal protection
Occupational exposure limits
US. ACGIH Threshold Limit Values
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. Alberta OELs (Occupational Health & Safety Code, Schedule 1, Table 2)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. British Columbia OELs. (Occupational Exposure Limits for Chemical Substances, Occupational Health and
Safety Regulation 296/97, as amended)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. Manitoba OELs (Reg. 217/2006, The Workplace Safety And Health Act)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. Ontario OELs. (Control of Exposure to Biological or Chemical Agents)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. Quebec OELs. (Ministry of Labor - Regulation respecting occupational health and safety)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 3/8

Canada. Saskatchewan OELs (Occupational Health and Safety Regulations, 1996, Table 21)
Components Type Value
Calcium hydroxide (CAS
15 minute 10 mg/m3
1305-62-0)
8 hour 5 mg/m3
Biological limit values
No biological exposure limits noted for the ingredient(s).
Appropriate engineering
Good general ventilation should be used. Ventilation rates should be matched to conditions. If
controls
applicable, use process enclosures, local exhaust ventilation, or other engineering controls to
maintain airborne levels below recommended exposure limits. If exposure limits have not been
established, maintain airborne levels to an acceptable level. If engineering measures are not
sufficient to maintain concentrations of dust particulates below the OEL (occupational exposure
limit), suitable respiratory protection must be worn. If material is ground, cut, or used in any
operation which may generate dusts, use appropriate local exhaust ventilation to keep exposures
below the recommended exposure limits. Eye wash facilities and emergency shower must be
available when handling this product.
Individual protection measures, such as personal protective equipment
Eye/face protection
Use dust -tight, unvented chemical safety goggles when there is potential for eye contact.
Skin protection
Hand protection
Wear appropriate chemical resistant gloves. Frequent change is advisable. Recommended gloves
include rubber, neoprene, nitrile or viton.
Other
Wear appropriate chemical resistant clothing.
Respiratory protection
If engineering controls do not maintain airborne concentrations below recommended exposure
limits (where applicable) or to an acceptable level (in countries where exposure limits have not
been established), an approved respirator must be worn. Recommended use: Wear respirator with
dust filter.
Thermal hazards
Wear appropriate thermal protective clothing, when necessary.
General hygiene
Keep from contact with clothing and other combustible materials. Remove and wash contaminated
considerations
clothing promptly. Always observe good personal hygiene measures, such as washing after
handling the material and before eating, drinking, and/or smoking. Routinely wash work clothing
and protective equipment to remove contaminants.
9. Physical and chemical
properties
Appearance
Physical state
Solid.
Form
Powder.
Colour
White to pale yellow.
Odour
Odourless.
Odour threshold
Not available.
pH 12.5 (3% suspension/water)
Melting point/freezing point Not available.
Initial boiling point and boiling Not available.
range
Flash point Not available.
Evaporation rate Not available.
Flammability (solid, gas) Oxidizer.
Upper/lower flammability or explosive limits
Flammability limit - lower Not available.
(%)
Flammability limit - upper Not available.
(%)
Explosive limit - lower (%) Not available.
Explosive limit — upper
Not available.
(%)
Vapour pressure
Not available.
Vapour density
Not available.
Relative density
Not available.
Oxygen Release Compound Advanced (ORC Advanced®) SIDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 4/8

Solubility(ies)
Solubility (water)
Slightly soluble
Partition coefficient
Not available.
(n-octanol/water)
Auto -ignition temperature
Not available.
Decomposition temperature
275 °C (527 °F)
Viscosity
Not available.
Other information
Bulk density 0.5 - 0.9 g/ml
Explosive limit Non -explosive.
10. Stability and reactivity
Reactivity Greatly increases the burning rate of combustible materials.
Chemical stability Decomposes on heating. Product may be unstable at temperatures above: 275°C/527°F.
Possibility of hazardous Reacts slowly with water.
reactions
Conditions to avoid Heat. Moisture. Avoid temperatures exceeding the decomposition temperature. Contact with
incompatible materials.
Incompatible materials Acids. Bases. Salts of heavy metals. Reducing Agents. Combustible material.
Hazardous decomposition Oxygen. Hydrogen peroxide (H2O2). Steam. Heat.
products
11. Toxicological information
Information on likely routes of exposure
Inhalation Dust may irritate respiratory system. Prolonged inhalation may be harmful.
Skin contact Causes skin irritation.
Eye contact Causes serious eye damage.
Ingestion Ingestion may cause irritation and malaise.
Symptoms related to the Severe eye irritation. Symptoms may include stinging, tearing, redness, swelling, and blurred
physical, chemical and vision. Permanent eye damage including blindness could result. Dusts may irritate the respiratory
toxicological characteristics tract, skin and eyes. Skin irritation. May cause redness and pain.
Information on toxicological effects
Acute toxicity
Components
Species Test Results
Calcium hydroxide (CAS 1305-62-0)
Acute
Oral
LD50
Rat 7340 mg/kg
Dipotassium Phosphate (CAS 7758-11-4)
Acute
Oral
LD50
Rat > 2000 mg/kg
Skin corrosion/irritation
Causes skin irritation.
Serious eye damage/eye
Causes serious eye damage.
irritation
Respiratory or skin sensitisation
Canada - Alberta OELs: Irritant
Calcium hydroxide (CAS 1305-62-0)
Irritant
Respiratory sensitisation
Not a respiratory sensitiser.
Skin sensitisation
This product is not expected to cause skin sensitisation.
Germ cell mutagenicity
No data available to indicate product or any components present at greater than 0.1 % are
mutagenic or genotoxic.
Carcinogenicity
This product is not considered to be a carcinogen by IARC, ACGIH, NTP, or OSHA.
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 5/8

Reproductive toxicity
Specific target organ toxicity -
single exposure
Specific target organ toxicity -
repeated exposure
Aspiration hazard
Chronic effects
12. Ecological information
Ecotoxicity
Components
This product is not expected to cause reproductive or developmental effects.
May cause respiratory irritation.
Not classified.
Due to the physical form of the product it is not expected to be an aspiration hazard.
Prolonged inhalation may be harmful.
The product is not classified as environmentally hazardous. However, this does not exclude the
possibility that large or frequent spills can have a harmful or damaging effect on the environment.
Species Test Results
Dipotassium Phosphate (CAS 7758-11-4)
Aquatic
Acute
Algae EC50 Pseudokirchneriella subcapitata > 100 mg/I, 72 Hours
Crustacea EC50 Daphnia magna 118.9 mg/I, 48 Hours
Fish LC50 Oryzias latipes > 100 mg/I, 96 Hours
Persistence and degradability Decomposes in the presence of water. The product contains inorganic compounds which are not
biodegradable.
Bioaccumulative potential The product does not contain any substances expected to be bioaccumulating.
Mobility in soil This substance has very low solubility in water and low mobility in the environment.
Other adverse effects None known.
13. Disposal considerations
Disposal instructions
Collect and reclaim or dispose in sealed containers at licensed waste disposal site. Dispose of
contents/container in accordance with local/regional/national/international regulations.
Local disposal regulations
Dispose in accordance with all applicable regulations.
Hazardous waste code
The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.
Waste from residues / unused
Dispose of in accordance with local regulations. Empty containers or liners may retain some
products
product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Contaminated packaging
Empty containers should be taken to an approved waste handling site for recycling or disposal.
Since emptied containers may retain product residue, follow label warnings even after container is
emptied.
14. Transport information
TDG
UN number
UN1457
UN proper shipping name
CALCIUM PEROXIDE
Transport hazard class(es)
Class
5.1
Subsidiary risk
-
Packing group
II
Environmental hazards
No
Special precautions for user Read safety instructions, SDS and emergency procedures before handling.
IATA
UN number
UN1457
UN proper shipping name
Calcium peroxide
Transport hazard class(es)
Class
5.1
Subsidiary risk
-
Packing group
II
Environmental hazards
No
ERG Code
5L
Special precautions for user Read safety instructions, SDS and emergency procedures before handling.
Oxygen Release Compound Advanced (ORC Advanced®) SIDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 6/8

IMDG
UN number
UN1457
UN proper shipping name
CALCIUM PEROXIDE
Transport hazard class(es)
Class
5.1
Subsidiary risk
-
Packing group
II
Environmental hazards
Marine pollutant
No
EmS
F-G, S-Q
Special precautions for user Read safety instructions, SDS and emergency procedures before handling.
Transport in bulk according to
Not applicable.
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
Canadian regulations
Controlled Drugs and Substances Act
Not regulated.
Export Control List (CEPA 1999, Schedule 3)
Not listed.
Greenhouse Gases
Not listed.
Precursor Control Regulations
Not regulated.
International regulations
Stockholm Convention
Not applicable.
Rotterdam Convention
Not applicable.
Kyoto Protocol
Not applicable.
Montreal Protocol
Not applicable.
Basel Convention
Calcium peroxide (CAS 1305-79-9)
International Inventories
Country(s) or region
Inventory name
On inventory (yes/no)*
Australia
Australian Inventory of Chemical Substances (AICS)
Yes
Canada
Domestic Substances List (DSL)
Yes
Canada
Non -Domestic Substances List (NDSL)
No
China
Inventory of Existing Chemical Substances in China (IECSC)
Yes
Europe
European Inventory of Existing Commercial Chemical
Yes
Substances (EINECS)
Europe
European List of Notified Chemical Substances (ELINCS)
No
Japan
Inventory of Existing and New Chemical Substances (ENCS)
Yes
Korea
Existing Chemicals List (ECL)
Yes
New Zealand
New Zealand Inventory
Yes
Philippines
Philippine Inventory of Chemicals and Chemical Substances
Yes
(PICCS)
Taiwan
Taiwan Chemical Substance Inventory (TCSI)
No
United States & Puerto Rico
Toxic Substances Control Act (TSCA) Inventory
Yes
*A "Yes" indicates this product complies
with the inventory requirements administered by the governing country(s).
A "No" indicates that one or more
components of the product are not listed or exempt from listing on the inventory administered
by the governing
country(s).
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 7/8

16. Other information
Issue date 12-October-2015
Revision date 09-January-2019
Version No. 02
Disclaimer Regenesis cannot anticipate all conditions under which this information and its product, or the
products of other manufacturers in combination with its product, may be used. It is the user's
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
Oxygen Release Compound Advanced (ORC Advanced®) SIDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 8/8

® REGENESI_ ® 1 w 1
Technology -Based solutions for the Environment
1 0-
Product identifier PlumeSTOP°
Other means of identification None.
Recommended use Soil and Groundwater Remediation.
Recommended restrictions None known.
Manufacturer/Importer/Supplier/Distributor information
Company Name Regenesis
Address 1011 Calle Sombra
San Clemente, CA 92673
Telephone [phone]
E-mail [e-mail]
Emergency phone number CHEMTREC° at 1-800-424-9300 (International)
2. Hazard(s) identification
Physical hazards
Not classified.
Health hazards
Not classified.
OSHA defined hazards
Not classified.
Label elements
Hazard symbol
None.
Signal word
None.
Hazard statement
The mixture does not meet the criteria for classification.
Precautionary statement
Prevention
Observe good industrial hygiene practices.
Response
Wash hands after handling.
Storage
Store away from incompatible materials.
Disposal
Dispose of waste and residues in accordance with local authority requirements.
Hazard(s) not otherwise
None known.
classified (HNOC)
3. Composition/information on ingredients
Mixtures
Chemical name
CAS number %
Water
7732-18-5 >75
Colloidal activated carbon s2.5
7440-44-0 <25
µm
Proprietary additives
<2
Composition comments
All concentrations are in percent by weight unless otherwise indicated.
4. First -aid measures
Inhalation Move to fresh air. Call a physician if symptoms develop or persist.
Skin contact Wash off with soap and water. Get medical attention if irritation develops and persists.
Eye contact Rinse with water. Get medical attention if irritation develops and persists.
Ingestion Rinse mouth. Get medical attention if symptoms occur.
Most important Direct contact with eyes may cause temporary irritation.
symptoms/effects, acute and
delayed
PlumeSTOPa SDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 1/6

Indication of immediate Treat symptomatically.
medical attention and special
treatment needed
General information If you feel unwell, seek medical advice (show the label where possible). Show this safety data
sheet to the doctor in attendance.
5. Fire -fighting measures
Suitable extinguishing media Carbon dioxide, alcohol -resistant foam, dry chemical, water spray, or water fog.
Unsuitable extinguishing None known.
media
Specific hazards arising from During fire, gases hazardous to health may be formed. Combustion products may include: carbon
the chemical monoxide, carbon dioxide, sodium oxides, metal oxides.
Special protective equipment Use protective equipment appropriate for surrounding materials.
and precautions for firefighters
Fire fighting Move containers from fire area if you can do so without risk.
equipmentli nstructions
Specific methods Use standard firefighting procedures and consider the hazards of other involved materials. Use
water spray to keep fire -exposed containers cool.
General fire hazards This material will not burn until the water has evaporated. Residue can burn. When dry may form
combustible dust concentrations in air.
6. Accidental release measures
Personal precautions,
Keep unnecessary personnel away. Avoid contact with spilled material. For personal protection,
protective equipment and
see section 8 of the SIDS.
emergency procedures
Methods and materials for
This product is miscible in water.
containment and cleaning up
Large Spills: Stop the flow of material, if this is without risk. Dike the spilled material, where this is
possible. Cover with plastic sheet to prevent spreading. Absorb in vermiculite, dry sand or earth
and place into containers. Following product recovery, flush area with water.
Small Spills: Wipe up with absorbent material (e.g. cloth, fleece). Clean surface thoroughly to
remove residual contamination.
Never return spills to original containers for re -use. For waste disposal, see section 13 of the SDS.
Environmental precautions Avoid discharge into drains, water courses or onto the ground.
7. Handling and storage
Precautions for safe handling Avoid contact with skin and eyes. Avoid prolonged exposure. Observe good industrial hygiene
practices. Wash thoroughly after handling. Wear appropriate personal protective equipment (See
Section 8).
Conditions for safe storage, Store in original tightly closed container. Store away from incompatible materials (see Section 10
including any incompatibilities of the SDS). Protect from freezing.
8. Exposure controls/personal protection
Occupational exposure limits
US. OSHA Table Z-3 (29 CFR
1910.1000)
Components
Type Value Form
Colloidal activated carbon
TWA 5 mg/m3 Respirable fraction.
:52.5 pm (CAS 7440-44-0)
15 mg/m3 Total dust.
US. NIOSH: Pocket Guide to Chemical Hazards
Components
Type Value Form
Colloidal activated carbon
TWA 2.5 mg/m3 Respirable.
:52.5 pm (CAS 7440-44-0)
Biological limit values
No biological exposure limits noted for the ingredient(s).
Appropriate engineering
Good general ventilation (typically 10 air changes per hour) should be used. Ventilation rates
controls
should be matched to conditions. If applicable, use process enclosures, local exhaust ventilation,
or other engineering controls to maintain airborne levels below recommended exposure limits. If
exposure limits have not been established, maintain airborne levels to an acceptable level.
PlumeSTOP°
SDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 2/6

individual protection measures, such as personal protective equipment
Eye/face protection Wear approved chemical safety goggles.
Skin protection
Hand protection Rubber, neoprene or PVC gloves are recommended. Wash hands after handling.
Other Avoid contact with the skin. Wear suitable protective clothing.
Respiratory protection Not normally needed. In case of insufficient ventilation, wear suitable respiratory equipment. If
engineering controls do not maintain airborne concentrations below recommended exposure limits
(where applicable) or to an acceptable level (in countries where exposure limits have not been
established), an approved respirator must be worn.
Thermal hazards Wear appropriate thermal protective clothing, when necessary.
General hygiene Always observe good personal hygiene measures, such as washing after handling the material
considerations and before eating, drinking, and/or smoking. Routinely wash work clothing and protective
equipment to remove contaminants.
9. Physical and chemical properties
Appearance
Physical state
Liquid.
Form
Aqueous suspension.
Color
Black.
Odor
Odorless.
Odor threshold
Not available.
pH
8-10
Melting point/freezing point
Not available.
Initial boiling point and boiling
Not available.
range
Flash point
Not flammable.
Evaporation rate
Not available.
Flammability (solid, gas)
Not applicable.
Upper/lower flammability or explosive limits
Flammability limit - lower
Not available.
N
Flammability limit - upper
Not available.
N
Explosive limit - lower (%)
Not available.
Explosive limit - upper (%)
Not available.
Vapor pressure Not available.
Vapor density Not available.
Relative density 1 - 1.2
Solubility(ies)
Solubility (water) Miscible
Partition coefficient Not available.
(n-octanol/water)
Auto -ignition temperature Not available.
Decomposition temperature Not available.
Viscosity Not available.
10. Stability and reactivity
Reactivity The product is stable and non -reactive under normal conditions of use, storage and transport.
Chemical stability Material is stable under normal conditions.
Possibility of hazardous No dangerous reaction known under conditions of normal use.
reactions
Conditions to avoid Contact with incompatible materials. Keep from freezing.
Incompatible materials Strong oxidizing agents. Water reactive materials.
PlumeSTOPI SIDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 3/6

Hazardous decomposition Combustion may produce: carbon oxides.
products
11. Toxicological information
Information on likely routes of exposure
Inhalation Prolonged inhalation may be harmful.
Skin contact Prolonged or repeated skin contact may result in minor irritation.
Eye contact Direct contact with eyes may cause temporary irritation.
Ingestion Expected to be a low ingestion hazard.
Symptoms related to the Direct contact with eyes may cause temporary irritation.
physical, chemical and
toxicological characteristics
Information on toxicological effects
Acute toxicity Not expected to be acutely toxic.
Components
Species
Colloidal activated carbon :52.5 pm (CAS 7440-44-0)
Acute
Inhalation
LC50
Oral
LD50
Skin corrosion/irritation
Serious eye damage/eye
irritation
Respiratory or skin sensitization
Respiratory sensitization
Skin sensitization
Germ cell mutagenicity
Test Results
Rat > 8500 mg/m3, air
Rat > 2000 mg/kg, (Female)
Prolonged skin contact may cause temporary irritation.
Direct contact with eyes may cause temporary irritation.
Not a respiratory sensitizer.
This product is not expected to cause skin sensitization.
No data available to indicate product or any components present at greater than 0.1% are
mutagenic or genotoxic.
Carcinogenicity This product is not considered to be a carcinogen by IARC, ACGIH, NTP, or OSHA.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
Not listed.
Reproductive toxicity
Specific target organ toxicity -
single exposure
Specific target organ toxicity -
repeated exposure
Aspiration hazard
Chronic effects
12. Ecological information
Ecotoxicity
Persistence and degradability
Bioaccumulative potential
Mobility in soil
Other adverse effects
This product is not expected to cause reproductive or developmental effects.
Not classified.
Not classified.
Not an aspiration hazard.
Prolonged inhalation may be harmful.
The product is not classified as environmentally hazardous. However, this does not exclude the
possibility that large or frequent spills can have a harmful or damaging effect on the environment.
No data is available on the degradability of this product.
No data available.
Expected to be temporarily highly mobile in soil.
None known.
13. Disposal considerations
Disposal instructions Collect and reclaim or dispose in sealed containers at licensed waste disposal site.
Local disposal regulations Dispose in accordance with all applicable regulations.
Hazardous waste code The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.
PlumeSTOP' SIDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 4/6

Waste from residues / unused Dispose of in accordance with local regulations. Empty containers or liners may retain some
products product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Contaminated packaging Empty containers should be taken to an approved waste handling site for recycling or disposal.
Since emptied containers may retain product residue, follow label warnings even after container is
emptied.
14. Transport information
DOT
Not regulated as dangerous goods.
IATA
Not regulated as dangerous goods.
IMDG
Not regulated as dangerous goods.
Transport in bulk according to Not established.
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
US federal regulations All components are listed on or exempt from the U.S. EPA TSCA Inventory List.
This product is not known to be a "Hazardous Chemical' as defined by the OSHA Hazard
Communication Standard, 29 CFR 1910.1200.
TSCA Section 12(b) Export Notification (40 CFR 707, Subpt. D)
Not regulated.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
Not listed.
CERCLA Hazardous Substance List (40 CFR 302.4)
Not listed.
Superfund Amendments and Reauthorization Act of 1986 (SARA)
Hazard categories Immediate Hazard - No
Delayed Hazard - No
Fire Hazard - No
Pressure Hazard - No
Reactivity Hazard - No
SARA 302 Extremely hazardous substance
Not listed.
SARA 311/312 Hazardous No
chemical
SARA 313 (TRI reporting)
Not regulated.
Other federal regulations
Clean Air Act (CAA) Section 112 Hazardous Air Pollutants (HAPs) List
Not regulated.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130)
Not regulated.
Safe Drinking Water Act Not regulated.
(SDWA)
US state regulations
US. Massachusetts RTK - Substance List
Not regulated.
US. New Jersey Worker and Community Right -to -Know Act
Colloidal activated carbon :52.5 pm (CAS 7440-44-0)
US. Pennsylvania Worker and Community Right -to -Know Law
Not listed.
US. Rhode Island RTK
Not regulated.
PlumeSTOP9) SIDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 5/6

US. California Proposition 65
Not Listed.
International Inventories
Country(s) or region
Inventory name
On inventory (yes/no)*
Australia
Australian Inventory of Chemical Substances (AICS)
Yes
Canada
Domestic Substances List (DSL)
Yes
Canada
Non -Domestic Substances List (NDSL)
No
China
Inventory of Existing Chemical Substances in China (IECSC)
Yes
Europe
European Inventory of Existing Commercial Chemical
No
Substances (EINECS)
Europe
European List of Notified Chemical Substances (ELINCS)
No
Japan
Inventory of Existing and New Chemical Substances (ENCS)
No
Korea
Existing Chemicals List (ECL)
Yes
New Zealand
New Zealand Inventory
Yes
Philippines
Philippine Inventory of Chemicals and Chemical Substances
Yes
(PICCS)
United States & Puerto Rico
Toxic Substances Control Act (TSCA) Inventory
Yes
*A "Yes" indicates this product complies
with the inventory requirements administered by the governing country(s).
A "No" indicates that one or more
components of the product are not listed or exempt from listing on the inventory administered
by the governing
country(s).
16. Other information, including date of preparation or last revision
Issue date 26-February-2015
Revision date -
Version # 01
Further information HMISO is a registered trade and service mark of the American Coatings Association (ACA).
HMISO ratings Health: 0
Flammability: 0
Physical hazard: 0
NFPA ratings
1 0
Disclaimer Regenesis cannot anticipate all conditions under which this information and its product, or the
products of other manufacturers in combination with its product, may be used. It is the user's
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
PlumeSTOPO SIDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 6/6

4
R EEG` E N IE Sft 11 S
Technology
-Based Solutions for the Environment
im r�',
Product identifier
PlumeSTOP° Nutrients
Other means of identification
None.
Recommended use
Soil and Groundwater Rernediation.
Recommended restrictions
None known.
Manufacturer/Importer/Supplier/Distributor information
Company Name
Regenesis
Address
1011 Calle Sombra
San Clemente, CA 92673
Telephone [phone]
E-mail [e-mail]
Emergency phone number CHEMTREC® at 1-800-424-9300 (International)
2. Hazard(s) identification
Physical hazards
Health hazards
OSHA defined hazards
Label elements
Hazard symbol
Signal word
Hazard statement
Precautionary statement
Prevention
Response
Storage
Disposal
Hazard(s) not otherwise
classified (HNOC)
Supplemental information
Not classified.
Not classified.
Not classified.
None.
None.
The mixture does not meet the criteria for classification.
Observe good industrial hygiene practices.
Wash hands after handling.
Store away from incompatible materials.
Dispose of waste and residues in accordance with local authority requirements.
None known.
None.
3. Composition/information on ingredients
Mixtures
The manufacturer lists no ingredients as hazardous according to OSHA 29 CFR 1910.1200.
4. First -aid measures
Inhalation
Skin contact
Eye contact
Ingestion
Most important
symptoms/effects, acute and
delayed
Indication of immediate
medical attention and special
treatment needed
General information
Move to fresh air. Call a physician if symptoms develop or persist.
Wash off with soap and water. Get medical attention if irritation develops and persists.
Do not rub eyes. Rinse with water. Get medical attention if irritation develops and persists.
Rinse mouth. Get medical attention if symptoms occur.
Dusts may irritate the respiratory tract, skin and eyes.
Treat symptomatically.
Ensure that medical personnel are aware of the material(s) involved, and take precautions to
protect themselves.
PlumeSTOP® Nutrients SDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 1/6

5. Fire -fighting measures
Suitable extinguishing media
Unsuitable extinguishing
media
Specific hazards arising from
the chemical
Special protective equipment
and precautions for firefighters
Fire fighting
equipment/instructions
Specific methods
General fire hazards
Water fog. Foam. Dry chemical powder. Carbon dioxide (CO2). Apply extinguishing media
carefully to avoid creating airborne dust.
None known.
During fire, gases hazardous to health may be formed.
Self-contained breathing apparatus and full protective clothing must be worn in case of fire.
Use water spray to cool unopened containers. Avoid dust formation.
Use standard firefighting procedures and consider the hazards of other involved materials.
No unusual fire or explosion hazards noted.
6. Accidental release measures
Personal precautions,
Keep unnecessary personnel away. Wear appropriate protective equipment and clothing during
protective equipment and
clean-up. Use a NIOSH/MSHA approved respirator if there is a risk of exposure to dust/fume at
emergency procedures
levels exceeding the exposure limits. For personal protection, see section 8 of the SIDS.
Methods and materials for
Avoid the generation of dusts during clean-up. Collect dust using a vacuum cleaner equipped with
containment and cleaning up
HEPA filter. This product is miscible in water. Stop the flow of material, if this is without risk.
Large Spills: Wet down with water and dike for later disposal. Shovel the material into waste
container. Following product recovery, flush area with water.
Small Spills: Sweep up or vacuum up spillage and collect in suitable container for disposal. For
waste disposal, see section 13 of the SDS.
Environmental precautions Avoid discharge into drains, water courses or onto the ground.
7. Handling and storage
Precautions for safe handling Minimize dust generation and accumulation. Provide appropriate exhaust ventilation at places
where dust is formed. Practice good housekeeping.
Conditions for safe storage, Store in original tightly closed container. Store in a well -ventilated place. Store away from
including any incompatibilities incompatible materials (see Section 10 of the SDS).
8. Exposure controls/personal protection
Occupational exposure limits
US. OSHA Table Z-1 Limits for Air Contaminants (29 CFR 1910.1000)
Components
Type
Value
Form
PlumeSTOP® Nutrients
PEL
5 mg/m3
Respirable fraction.
(as dust)
15 mg/m3
Total dust.
US. OSHA Table Z-3 (29 CFR 1910.1000)
Components
Type
Value
Form
PlumeSTOP® Nutrients
TWA
5 mg/m3
Respirable fraction.
(as dust)
15 mg/m3
Total dust.
50 mppcf
Total dust.
15 mppcf
Respirable fraction.
US. ACGIH Threshold Limit Values
Components
Type
Value
Form
PlumeSTOP® Nutrients
TWA
3 mg/m3
Respirable particles.
(as dust)
10 mg/m3
Inhalable particles.
Biological limit values No biological exposure limits noted for the ingredient(s).
Appropriate engineering Ensure adequate ventilation, especially in confined areas. Local exhaust is suggested for use,
controls where possible, in enclosed or confined spaces.
PlumeSTOP° Nutrients SDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 2/6

Individual protection measures, such as personal protective equipment
Eye/face protection Wear safety glasses with side shields (or goggles). Unvented, tight fitting goggles should be worn
in dusty areas.
Skin protection
Hand protection Wear appropriate chemical resistant gloves. Suitable gloves can be recommended by the glove
supplier.
Skin protection
Other Wear suitable protective clothing.
Respiratory protection In case of inadequate ventilation, use MSHA/NIOSH approved dust respirator.
Thermal hazards Wear appropriate thermal protective clothing, when necessary.
General hygiene Always observe good personal hygiene measures, such as washing after handling the material
considerations and before eating, drinking, and/or smoking. Routinely wash work clothing and protective
equipment to remove contaminants.
9. Physical and chemical properties
Appearance
Physical state Solid.
Form Powder.
Color White.
Odor
uaoriess.
Odor threshold
Not available.
pH
Not available.
Melting point/freezing point
Not available.
Initial boiling point and boiling
Not available.
range
Flash point
Not available.
Evaporation rate
Not available.
Flammability (solid, gas)
The product is non-combustible.
Upper/lower flammability or explosive
limits
Flammability limit - lower
Not available.
N
Flammability limit - upper
Not available.
N
Explosive limit - lower (%)
Not available.
Explosive limit - upper (%)
Not available.
Vapor pressure
Not available.
Vapor density
Not available.
Relative density
Not available.
Solubility(ies)
Solubility (water)
Completely soluble.
Partition coefficient
Not available.
(n-octanol/water)
Auto -ignition temperature
Not available.
Decomposition temperature
Not available.
Viscosity
Not available.
Other information
Explosive properties
Not explosive.
Oxidizing properties
Not oxidizing.
10. Stability and reactivity
Reactivity The product is stable and non -reactive under normal conditions of use, storage and transport.
Chemical stability Material is stable under normal conditions.
PlumeSTOP® Nutrients SIDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 3/6

Possibilitv of hazardous No danqerous reaction known under conditions of normal use. Ammonia fumes may be released
reactions upon heating.
Conditions to avoid Contact with incompatible materials. Excessive heat.
Incompatible materials Strong oxidizing agents. Bases.
Hazardous decomposition Ammonia fumes may be released upon heating.
products
Information on likely routes of exposure
Inhalation Dust may irritate respiratory system.
Skin contact Dust or powder may irritate the skin.
Eye contact Dust may irritate the eyes.
Ingestion Expected to be a low ingestion hazard.
Symptoms related to the Dusts may irritate the respiratory tract, skin and eyes.
physical, chemical and
toxicological characteristics
Information on toxicological effects
Acute toxicity Not expected to be acutely toxic.
Skin corrosion/irritation Prolonged skin contact may cause temporary irritation.
Serious eye damage/eye Direct contact with eyes may cause temporary irritation.
irritation
Respiratory or skin sensitization
Respiratory sensitization Not a respiratory sensitizer.
Skin sensitization This product is not expected to cause skin sensitization.
Germ cell mutagenicity No data available to indicate product or any components present at greater than 0.1 % are
mutagenic or genotoxic.
Carcinogenicity This product is not considered to be a carcinogen by IARC, ACGIH, NTP, or OSHA.
IARC Monographs. Overall Evaluation of Carcinogenicity
Not listed.
NTP Report on Carcinogens
Not listed.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
Not regulated.
Reproductive toxicity This product is not expected to cause reproductive or developmental effects.
Specific target organ toxicity - Not classified.
single exposure
Specific target organ toxicity - Not classified.
repeated exposure
Aspiration hazard Not an aspiration hazard.
12. Ecological information
Ecotoxicity The product is not classified as environmentally hazardous. However, this does not exclude the
possibility that large or frequent spills can have a harmful or damaging effect on the environment.
Persistence and degradability No data is available on the degradability of this product.
Bioaccumulative potential No data available.
Mobility in soil This product is completely water soluble and will disperse in soil.
Other adverse effects No other adverse environmental effects (e.g. ozone depletion, photochemical ozone creation
potential, endocrine disruption, global warming potential) are expected from this component.
13. Disposal considerations
Disposal instructions Collect and reclaim or dispose in sealed containers at licensed waste disposal site.
Local disposal regulations Dispose in accordance with all applicable regulations.
Hazardous waste code The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.
PlumeSTOP® Nutrients SIDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 4/6

Waste from residues / unused Dispose of in accordance with local regulations. Empty containers or liners may retain some
products product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Contaminated packaging Since emptied containers may retain product residue, follow label warnings even after container is
emptied. Empty containers should be taken to an approved waste handling site for recycling or
disposal.
DOT
Not regulated as dangerous goods.
IATA
Not regulated as dangerous goods.
IMDG
Not regulated as dangerous goods.
Transport in bulk according to Not applicable.
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
US federal regulations This product is not known to be a "Hazardous Chemical' as defined by the OSHA Hazard
Communication Standard, 29 CFR 1910.1200.
TSCA Section 12(b) Export Notification (40 CFR 707, Subpt. D)
Not regulated.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
Not regulated.
CERCLA Hazardous Substance List (40 CFR 302.4)
Not listed.
Superfund Amendments and Reauthorization Act of 1986 (SARA)
Hazard categories Immediate Hazard - No
Delayed Hazard - No
Fire Hazard - No
Pressure Hazard - No
Reactivity Hazard - No
SARA 302 Extremely hazardous substance
Not listed.
SARA 311/312 Hazardous No
chemical
SARA 313 (TRI reporting)
Chemical name
Ammonium sulfate
CAS number % by wt.
7783-20-2 40-50
Other federal regulations
Clean Air Act (CAA) Section 112 Hazardous Air Pollutants (HAPs) List
Not regulated.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130)
Not regulated.
Safe Drinking Water Act Not regulated.
(SDWA)
US state regulations
US. Massachusetts RTK - Substance List
Ammonium sulfate (CAS 7783-20-2)
US. New Jersey Worker and Community Right -to -Know Act
Not listed.
US. Pennsylvania Worker and Community Right -to -Know Law
Ammonium sulfate (CAS 7783-20-2)
US. Rhode Island RTK
Not regulated.
PlumeSTOP® Nutrients SIDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 5/6

US. California Proposition 65
California Safe Drinking Water and Toxic Enforcement Act of 1986 (Proposition 65): This material is not known to contain
any chemicals currently listed as carcinogens or reproductive toxins.
International Inventories
Country(s) or region
Inventory name
On inventory (yes/no)*
Australia
Australian Inventory of Chemical Substances (AICS)
No
Canada
Domestic Substances List (DSL)
No
Canada
Non -Domestic Substances List (NDSL)
No
China
Inventory of Existing Chemical Substances in China (IECSC)
No
Europe
European Inventory of Existing Commercial Chemical
No
Substances (EINECS)
Europe
European List of Notified Chemical Substances (ELINCS)
No
Japan
Inventory of Existing and New Chemical Substances (ENCS)
No
Korea
Existing Chemicals List (ECL)
No
New Zealand
New Zealand Inventory
No
Philippines
Philippine Inventory of Chemicals and Chemical Substances
No
(PICCS)
United States & Puerto Rico
Toxic Substances Control Act (TSCA) Inventory
No
*A "Yes" indicates this product complies
with the inventory requirements administered by the governing country(s).
A "No" indicates that one or more
components of the product are not listed or exempt from listing on the inventory administered by the governing
country(s).
16. Other information, including date of preparation or last revision
Issue date 07-January-2016
Revision date
Version # 01
HMISO ratings Health: 1
Flammability: 0
Physical hazard: 0
NFPA ratings
41 0
Disclaimer Regenesis cannot anticipate all conditions under which this information and its product, or the
products of other manufacturers in combination with its product, may be used. It is the user's
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
PlumeSTOP® Nutrients SIDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 6/6

GHD I NCDE — 11219094Notification of Intent2

Source: ESRI Basemap Imagery, DigitalGlobe, Vivid - USA, 2/26/2017
o zoo aoo 60o4 RE: Adapted from EarthTech figure, Base Map," dated October 2007; PHILLIPS 66 COMPANY 072847
Bartlett Engineering
& Surveying, PC figure, "MiningPermit Overall Site Drawing,"FORMER PHILLIPS FIBERS CORPORATION Oct 9, 2020
dated August 2008; and USDA 2009 NAIP Aerial Photograph.
Feet All well locations surveyed by Taylor Wiseman & Taylor, June 2012 and January 2013. ' ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
Coordinate System:
NAD 1983 UTM Zone 16N SITE PLAN - LOCATION OF RELEASE AREAS FIGURE 1
GIs File: N:\US\Baton Rouge\Projects\562\11219049\GIS\Maps\Deliverables\NCDEG2\11219094(NCDGEG2)GIS-BR001.mxd

Source: ESRI Basemap Imagery, DigitalGlobe, Vivid - USA, 2/26/2017
4 RE: Adapted from EarthTech figure, "Site Base Map," dated October 2007; PHILLIPS 66 COMPANY 072847
0 62.5 125 Bartlett Engineering & Surveying, PC figure, "Mining Permit Overall Site Drawing," FORMER PHILLIPS FIBERS CORPORATION Oct 9, 2020
dated August 2008; and USDA 2009 NAIP Aerial Photograph.
Feet All well locations surveyed by Taylor Wiseman & Taylor, June 2012 and January 2013. ' ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
Coordinate System:
NAD 1983 UTM Zone 18N LANDFILLAREA INJECTION LOCATIONS FIGURE 2
GIs File: N:\US\Baton Rouge\Projects\562\11219049\GIS\Maps\Deliverables\NCDEG2\11219094(NCDGEG2)GIS-BR002.mxd

Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community.
PHILLIPS 66 COMPANY 11219094-RM00
0 60 120ft ^ FORMER PHILLIPS FIBERS CORPORATION Oct 12, 2020
ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
North Carolina GROUNDWATER ELEVATION AND CONTOUR MAP
StatePlaneNAD83 FORMER LANDFILL AREA, JULY 2019 FIGURE 3
CAD File: N:\US\Atlanta\Projects\565\11219094\Digital_Design\ACAD 2018\Figures\NCDEQ2\11219094-RM00(NCDEQ2)GN-DE001.dwg

Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNESIAirbus IDS, USDA, USGS, AeroGRID, IGN, and the GIS User Community.
PHILLIPS 66 COMPANY 11219094-RM00
0 60 120ft RE: ADAPTED FROM EARTHTECH FIGURE, "SITE BASE MAP", DATED OCTOBER 2007; ^ FORMER PHILLIPS FIBERS CORPORATION Oct 12, 2020
BARTLETT ENGINEERING & SURVEYING, PC FIGURE, "MINING PERMIT OVERALL SITE ® ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
DRAWING", DATED AUGUST 2008; AND USDA 2009 NAIP AERIAL PHOTOGRAPH. ALL ,
WELL LOCATIONS SURVEYED BY TAYLOR WISEMAN & TAYLOR, JUNE 2012 AND FORMER LANDFILL AREA
North Carolina JANUARY2013. StatePlane NAD83 TOTAL CHLORINATED VOC CONCENTRATIONS JULY 2019 FIGURE 4
CAD File: N:\USWtlanta\Projects\565\11219094\Digital_Design\ACAD 2018\Figures\NCDEQ2\11219094-RM00(NCDEQ2)GN-DE002.dwg

Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNESIAirbus IDS, USDA, USGS, AeroGRID, IGN, and the GIS User Community.
PHILLIPS 66 COMPANY 11219094-RM00
0 60 120ft RE: ADAPTED FROM EARTHTECH FIGURE, "SITE BASE MAP", DATED OCTOBER 2007; ^ FORMER PHILLIPS FIBERS CORPORATION Oct 13, 2020
BARTLETT ENGINEERING & SURVEYING, PC FIGURE, "MINING PERMIT OVERALL SITE ® ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
DRAWING", DATED AUGUST 2008; AND USDA 2009 NAIP AERIAL PHOTOGRAPH. ALL ,
WELL LOCATIONS SURVEYED BY TAYLOR WISEMAN & TAYLOR, JUNE 2012 AND FORMER LANDFILL AREA
North Carolina JANUARY 2013.
StatePlaneNAD83 DIPHENYL ETHER CONCENTRATIONS JULY 2019 FIGURE 5
CAD File: N:\USWtlanta\Projects\565\11219094\Digital_Design\ACAD 2018\Figures\NCDEQ2\11219094-RM00(NCDEQ2)GN-DE005.dwg

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Vertical Scale ROCKY MOUNT, NORTH CAROLINA Oct 12, 2020
CROSS SECTION DEVELOPED USING INFORMATION PROVIDED BY OTHERS FORMER PHILLIPS FIBERS
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CAD File: N:\US\Atlanta\Projects\565\11219094\Digital_Design\ACAD 2018\Figures\NCDEQ2\11219094-RM00(NCDEQ2)GN-DE003.dwg

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Vertical Scale
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0 20 50ft
CROSS SECTION DEVELOPED USING INFORMATION PROVIDED BY OTHERS
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CAD File: N:\US\Atlanta\Projects\565\11219094\Digital_Design\ACAD 2018\Figures\NCDEQ2\11219094-RM00(NCDEQ2)GN-DE004.dwg

GHD I NCDE — 11219094Notification of Intent2

PHYSICAL SETTING SOURCE MAP =3215868.2s
^/ County Boundary
�/ Major Roads
N Contour Lines
Earthquake epicenter, Richter 5 or greater
® Water Wells
© Public Water Supply Wells
® Cluster of Multiple Icons
o i/4 1/2
1 Mllas
Groundwater Flow Direction
0
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cV
Groundwater Flow Varies at Location
o
Rare & Endangered Species
SITE NAME:
072847-95 -Rocky Mount, NC
CLIENT:
Conestoga -Rovers &Associates
ADDRESS:
1245 Atlantic Avenue
CONTACT:
Sean Armbrust
Rocky Mount NC 27801
INQUIRY#:
3215868.2s
LAT/LONG:
35.9659 / 77.7807
DATE:
November 30, 2011 11:26 am

GEOCHEC " = PHYSICAL SETTING SOURCE SUMMARY
DATABASE SEARCH DISTANCE (miles)
Federal USGS 1.000
Federal FRDS PWS Nearest PWS within 1 mile
State Database 1.000
FEDERAL USGS WELL INFORMATION
LOCATION
MAP ID WELL ID FROM TP
No Wells Found
FEDERAL FRDS PUBLIC WATER SUPPLY SYSTEM INFORMATION
LOCATION
MAP ID WELL ID FROM TP
No PWS System Found
Note: PWS System location is not always the same as well location.
STATE DATABASE WELL INFORMATION
LOCATION
MAP ID WELL ID FROM TP
No Wells Found
OTHER STATE DATABASE INFORMATION
NORTH CAROLINA NATURAL HERITAGE ELEMENT OCCURRENCES
ID Class
KC50015010 Invertebrate
NC50019528 Invertebrate
NC50022568 Animal
NORTH CAROLINA SIGNIFICANT NATURAL HERITAGE AREAS DATABASE:
ID Name
460003336 LOWER TAR RIVER AQUATIC HABITAT
TC3215868.2s Page A-12

GEOCHECKn- PHYSICAL SETTING SOURCE MAP FINDINGS
GIS ID:
Classification by Type:
Occurrence Status:
GIS ID:
Classification by Type:
Occurrence Status:
GIS ID:
Classification by Type:
Occurrence Status:
Site Name:
Quality:
Acres per Polygon:
NC_NHEO NC50015010
382092
Invertebrate
Extant
NC_NHEO NC50019528
13229
Invertebrate
Extant
NC_NHEO NC50022568
352081
Animal
Extant
NC_SNHA
LOWER TAR RIVER AQUATIC HABITAT
Not Reported
2082.38
NC10003336
TC3215888.2s Page A-14

GHD I NCDE — 11219094Notification of Intent2

RWR Site#: 0020
ACCESS AGREEMENT
THIS AGREEMENT is made as of April 25, 2008, by and between Charles J. Duckworth
("Grantor"), and ConocoPhillips Company ("Grantee"); Grantor and Grantee, collectively, shall
sometimes hereinafter be referred to as the "Parties".
RECITALS
WHEREAS, Charles J. Duckworth is the owner(s) in fee simple of that certain
parcel(s) of land located in 1301 Atlantic Avenue, Rocky Mount, Edgecombe County, North
Carolina, pursuant to a deed recorded with the Edgecombe County Registry of Deeds in Book
1467, Page 98;
WHEREAS, the Property may be comprised of a disposal site as the result of a
release of oil and/or hazardous material; and
WHEREAS, Grantee, in cooperation with the North Carolina Department of
Environment and Natural Resources ("NCDENR" ), now desires to enter the Property to conduct
various environmental investigation and/or remediation activities, including, but not limited to
maintenance of remediation systems, including digging and trenching; drill soil borings;
installation of monitoring wells; and periodic sampling of wells on the property (the "Work");
WHEREAS, By entering into this Agreement, neither party intends for this
Agreement to be interpreted or construed as an admission of any liability;
WHEREAS, The Parties desire to enter into this Access Agreement so that the soil
and/or groundwater can be assessed pursuant to environmental laws and regulations;
NOW THEREFORE, in consideration of the granting of the foregoing, the mutual premises,
covenants, conditions and agreements hereinafter set forth, and other good and valuable con-
sideration, the receipt and adequacy of which are acknowledged, the Parties agree as follows:
1. Grant of Access - Grantor hereby grants to Grantee, and its employees, representatives
and contractors an irrevocable, non-exclusive access and right of entry (the "Access") to enter
upon the Property from time to time to conduct the activities described in the above Recitals.
Further, Grantor shall cause any tenants or lessees of the Property, not a party hereto, to provide

RM&R Site#: 0020
Grantee, including its consultant(s), and/or contractor(s), same Access. This Access Agreement
shall commence on May 1, 2008 (Effective Date), and shall run for a period of three (3) years, or
until the Work is complete. If Grantee determines in its sole discretion that the Work is
complete, it may terminate this Agreement by providing written notice to Grantor in the
recordable form. If Grantee is required by a government agency to maintain a well or other
equipment on the Property beyond the term of this Agreement, the Grantee shall, on notice of
such requirement to Grantor, be extended until thirty (30) days after such requirement ceases.
Prior to the expiration of the Agreement, Grantee shall, at its sole cost and expense, (a) cause any
excavations to be returned to the original gradient, (b) remove all equipment placed on the
Property, (c) fill and level all ditches, ruts and depressions, if any, caused by the closure of the
Grantee's excavation operations on the Property and (d) remove all debris resulting therefrom.
2. Compliance with Laws - Grantee shall conduct all operations which are the subject of
this Agreement in compliance with all federal, state, and municipal statutes and ordinances, and
with all regulations, orders, and directives of appropriate governmental agencies, as such
statutes, ordinances, regulations, orders and directives now exist or provide.
3. Permits — Grantee shall be responsible for obtaining any and all governmental permits
and approvals which may be necessary for it to conduct any work or activities under this Access
Agreement. Grantor shall coordinate and cooperate with Grantee in Grantee's activities to obtain
all necessary government permits and permissions.
4. Liens and Claims - Grantor will not permit any mechanics', materialmen's, or similar
liens or claims to stand against the Property for labor or material furnished in connection with
any work performed by Grantee under this Agreement. Upon reasonable and timely notice of
any such lien or claim delivered to Grantee by Grantor, Grantee may bond and contest the
validity and the amount of such lien, but Grantee will immediately pay any judgment rendered,
will pay all proper costs and charges, and will have the lien or claim released at its sole expense.
5. Cooperation - Grantee agrees to coordinate its activities with Grantor to minimize any
impairment of access by customers or business invitees of Grantor to the Property and
any inconvenience to or disruption of Grantor's business on the Property.
6. Provisions to Run with the Land. This Agreement establishes certain rights, liabilities,
agreements and obligations for the Property, or any portion thereof, which shall run with
the Property or any portion thereof, for the term of this Agreement. Grantor hereby
covenants for himself and his executors, administrators, heirs, successors and assigns, to
stand seized and hold title to the Property, or any portion thereof, subject to this
Agreement. The rights granted to Grantee, its successors and assigns, do not provide,
however, that a violation of this Agreement shall result in a forfeiture, termination or
otherwise.
7. Indemni - Grantee agrees that it will indemnify and hold Licensor harmless from and
against any claims, demands, actions, suits, judgments, losses, damages, costs, or
expenses incurred as a result of personal injury, property damage, civil penalties, or fines
proximately caused by the negligent acts or omissions of Grantee or its authorized
contractors, employees and agents in conducting the Work. However, this indemnity and

AWR Site#: 0020
hold harmless obligation shall not apply to any such claims, demands, actions, suits,
judgments, losses, damages, costs, or expenses to the extent caused by the sole
negligence, gross negligence, or willful misconduct of Licensor or any third party. This
indemnity is expressly conditioned on the following:
(a) In the event Grantor shall identify any matter to which this indemnity may
apply or receive a notice or claim from any third party of such matter, it shall
immediately, and in every case within thirty (30) days of said notice or claim, notify
Grantee in writing of such matter.
(b) Grantor shall cooperate with Grantee by allowing Grantee, its agents,
representatives, contractors and consultants, prompt and ready access to the Property for
the purpose of investigating any matter to which this indemnity may apply. Grantor shall
provide Grantee with copies of all investigative reports, data or other information in any
form which Grantor, its consultants, agents or attorneys may have pertaining to any such
matter, on request of Grantee.
(c) Notwithstanding anything in this agreement to the contrary, in no event
shall either party be liable to the other party for any special, indirect, or consequential
damages including, but limited to, claims for loss of use, rents, anticipated profit or
business opportunity, or business interruption.
8. Severability - Grantor hereby agrees, in the event that a court or other tribunal
determines that any provision of this instrument is invalid or unenforceable:
(a) That any such provision shall be deemed automatically modified to
conform to the requirements for validity and enforceability as determined by such court
or tribunal; or
(b) That any such provision that, by its nature, cannot be so modified, shall
be deemed deleted from this instrument as though it had never been included.
(c) In either case, the remaining provisions of this instrument shall remain in
full force and effect.
9. Notices - Any notice provided for herein or otherwise required to be given
hereunder shall be deemed received when personally served or three (3) days after
mailing by certified or registered United States mail, return receipt requested, postage
prepaid, or by facsimile machine, with transmission and receipt confirmed, or by
nationally recognized overnight delivery service, addressed as follows:
To Grantor: Charles J. Duckworth
PO Box 143
Rocky Mount, NC 27802-0143
Phone: ( 252 ) 442-7678

RM&R Site#: 0020
To Grantee: ConocoPhillips Company
600 N. Dairy Ashford
MO 1066
Houston, TX 77079
Attn: Laura Schoenberger
Phone: [phone]
Facsimile: (281) 293- 3658
The person and the place to which notices are to be mailed may be changed by
either party by providing written notice of same to the other.
10. Entire Agreement - This License Agreement represents the full, complete and entire
agreement between the Parties with respect to the subject matter hereof, and the rights
and remedies of the Parties shall be solely and exclusively those herein contained, and in
lieu of any remedies otherwise available at law or in equity.
11. Governing Law - This Agreement shall be construed and interpreted and governed by
and in accordance with the local law of the State of North Carolina without reference to
any choice of law, rules or policies which may refer the resolution of any dispute arising
hereunder to the laws of any other jurisdiction.
THE PARTIES have executed this License Agreement by their duly authorized
representative(s).
MIXI M-0 1
Name: Charles Duckworth
Title: Owner
Date:
GRANTEE
By:
Name: Greg Cardwell
Title: Attorney in Fact
Date: .5 Z/ 3 i g

R1t1&R Site#: 0020
STATE OF Texas §
COUNTY OF Harris §
On this ) 3 - day of MMT, 2007, before me KV)St" WE E . u the
undersigned officer, personally appeared Greg Cardwell, known to me (or satisfactorily proven)
to be the person whose name is subscribed as A —t`a A to a V - ', N - �Ac-+ , of ConocoPhillips
Company and acknowledged that he/she, as such A-P-►o RNEv N- VAC —It, being authorized so to do,
executed the foregoing instrument as the act of his/her principal for the purposes therein
contained, by signing the name of the said ConocoPhillips Company by himself/herself as
4" 1I .RNEU-i'w-VAJ
My commission expires:
0 5-a(--'70) 0
State of North Carolina
County of
jlm,Itffl; 4, �qq
fliTtRY PUBLIC
Notary Public in and for Harris County, TX
� . ��e��eeee�0���e�esee�ee�semj
Ip11111ry
KRISTINE E, ®®65S
NotaryPublic, State of Texas
g 1111W" �r s
My Commission Evires 05-26-10 s
Keeeeeeeeeeeeeeeee�eeeeeeeeee
I, �)ct Ili, M 6 di k TV0 , a Notary Public for .
NA-51 F County, North Carolina, do hereby certify that Charles Duckworth
personally appeared before me this day and acknowledged the due execution of the foregoing
instrument.
Witness my hand and official seal, this the day of A)& cl , 20 &�'.
(Official Seal) ��-,�, )9 (
lOfficial Signature of Notary
�' 1. & EX Tate , Notary Public
otary's printed name
My commission expires: )UDY M. OVERTON
67 os-'261G NOTARY PUBLIC
NASH COUNTY, NC