WI0501061_Permit (Issuance)_20201027

October 12, 2020
North Carolina Department of Environmental and Natural Resources
Department of Water Resources
UIC Program
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
Dear Sir or Madam:
Reference No. 11219094
Re: Notification of Intent to Construct or Operate Injection Wells
Portion of Rocky Mount Fiber Dump (American Fibers and Yarns)
Atlantic Avenue, Rocky Mount, Edgecombe County, North Carolina (Site)
NCD041466525 - Docket No. 12-SF-357 (Former Docket No. 10-SF-336
On behalf of Phillips 66 Company, GHD is submitting the enclosed Notification of Intent to Construct or
Operate Injection Wells (Notification) for the above -referenced Site. The Site is currently managed under
the Division of Waste Management, Inactive Hazardous Sites Branch, Registered Environmental
Consultant (REC) Program. On June 25, 2015, GHD submitted a certified Remedial Action Plan -
Groundwater (Groundwater RAP) for the site that proposed treatment of impacted groundwater using
chemical injection.
There are two areas of impacted groundwater at the Site and are located on separate parcels with
different owners. The first area is identified as the Dowtherm A Area and is located on the 1245 Atlantic
Avenue parcel for which this Notification is being submitted. The second area is identified as the Former
Landfill Area and is located on the 1301 Atlantic Avenue parcel for which a separate Notification has been
provided.
Groundwater in the Dowtherm A Area is impacted with diphenyl ether and/or 1,1-biphenyl. The areas
demonstrating the greatest concentrations of these compounds will be addressed through the injection of
an injectable liquid activated carbon (PlumeStop by Regenesis) to adsorb contaminants and the injection
of oxygen (ORC-Advanced by Regenesis) that will be released over time to stimulate aerobic
biodegradation. Both injectants have been approved by the North Carolina Department Human and Health
Services for injection into groundwater; however, PlumeStop was approved with stipulations. As required
by the stipulations, a potable well survey has been included as Attachment D of this submittal which
indicates there are no public or private water wells within 2,000 feet downgradient of the application area.
Additionally, there are no designated surface water supplies within 1,500 feet downgradient of the
application area and Figure 1 included in Attachment C provides the location of the monitoring well
network present at the Site. The enclosed notification and attachments are for small-scale injections
operations for an area less than 10,000 square feet. The injection will be performed in accordance with
the rules specified in 15A NCAC 02C .0225.
GHD D 1 900
3075 Breckinridge Boulevard Suite 470 Duluth Georgia 30096 USA IS1S FERi0[5 1
T 770 441 0027 F 770 441 2050 W www.ghd.com

If you have any questions, please contact the undersigned at [phone].
Sincerely,
GHD
John A. DiZinno, P.E.
JAD/da/1
Encl.
cc: Ed Kuhn, Phillips 66 Company
NCDE — 072847Notification of Intend

GHD I NCDE — 072847Notificafion of Intend

GHD I NCDE — 072847Notificafion of Intend

NC Department of Environmental Quality — Division of Water Resources (DWR)
NOTIFICATION OF INTENT (NOI) TO CONSTRUCT OR OPERATE INJECTION WELLS
The following are `permitted by rule" and do not require an individual permit when constructed in accordance
with the rules of 15A NCAC 02C.0200 (NOTE: This form must be received at least 14 DAYS prior to injection)
AQUIFER TEST WELLS (15A NCAC 02C .0220)
These wells are used to inject uncontaminated fluid into an aquifer to determine aquifer hydraulic characteristics.
IN SITU REMEDIATION (15A NCAC 02C .02251 or TRACER WELLS (15A NCAC 02C .0229):
1) Passive Injection Systems - In -well delivery systems to diffuse injectants into the subsurface. Examples include
ORC socks, iSOC systems, and other gas infusion methods (Note: Injection Event Records (IER) do not need to be
submitted for replacement of each sock used in ORC systems).
2) Small -Scale Injection Operations — Injection wells located within a land surface area not to exceed 10,000
square feet for the purpose of soil or groundwater remediation or tracer tests. An individual permit shall be required
for test or treatment areas exceeding 10,000 square feet.
3) Pilot Tests - Preliminary studies conducted for the purpose of evaluating the technical feasibility of a
remediation strategy in order to develop a full scale remediation plan for future implementation, and where the
surface area of the injection zone wells is located within an area that does not exceed five percent of the land surface
above the known extent of groundwater contamination. An individual permit shall be required to conduct more
than one pilot test on any separate groundwater contaminant plume.
4) Air Injection Wells - Used to inject ambient air to enhance in -situ treatment of soil or groundwater.
5) In -Situ Thermal Wells (IST) — Used to `heat' contaminated groundwater to enhance remediation.
Print Clearly or Type Information. Illegible Submittals Will Be Returned as Incomplete.
DATE: October 12, 2020 PERMIT NO. W10501061 (to be filled in by DWR)
NOTE- If this NOI is being submitted as notification of a modification of a previously issued NOI for this site (e.g.,
different injection wells, plume, additives, etc.) and still meets the deemed permitted by rule criteria, provide the
previously assigned permit tracking number and any needed relevant information to assess and approve injection:
Permit No.
Issued Date:
A. WELL TYPE TO BE CONSTRUCTED OR OPERATED
(1)
Air Injection Well .......................................
Complete sections B through F, J, M
(2)
Aquifer Test Well .......................................
Complete sections B through F, J, M
(3)
Passive Injection System ...............................
Complete sections B through F, H-M
(4)
(XX)_Small-Scale Injection Operation ......................
Complete sections B through M
(5)
Pilot Test .................................................
Complete sections B through M
(6)
Tracer Injection Well ...................................
Complete sections B through M
(7)
In -Situ Thermal (IST) Well ...........................
Complete sections B through M
B. STATUS OF WELL OWNER: Business/Organization
Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 1

C.
D.
F.
G.
WELL OWNER(S) — State name of Business/Agency, and Name and Title of person delegated authority to
sign on behalf of the business or agency:
Name(s): Phillips 66 Company Atm. Ed Kuhn
Mailing Address: c/o GHD 222 S. Church St. Suite 400
City: Charlotte State: NC_ Zip Code: 28202 County: Mecklenberg
Day Tele No.: 980-209-6353 Cell No.: 704-975-3000
EMAIL Address: Ed. Kuhn(&contractor.p66.com Fax No.:
PROPERTY OWNER(S) (if different than well owner/applicant)
Name and Title: Bill Whitford Site Manager
Company Name SePro Development Company
Mailing Address: 16013 Watson Seed Farm Road
City:
Whitakers
State: NC Zip Code:27801
County: Nash
Day Tele No.: 252-391-8373 Cell No.:
EMAIL Address: billw(ksepro.com Fax No.:
E. PROJECT CONTACT (Typically Environmental Consulting/Engineering Firm)
Name and Title: John DiZinno Engineer
Company Name GHD
Mailing Address: 3075 Breckinridge Blvd, Suite 470
City: Duluth State: GA Zip Code:30096 County: Gwinnett
Day Tele No.: 678-280-2121 Cell No.: 470-345-2317
EMAIL Address: john.dizinno(kghd.com Fax No.: 770-441-2050
PHYSICAL LOCATION OF WELL SITE
(1) Facility Name & Address: 1245 Atlantic Avenue
City: Rocky Mount County. Edgecombe Zip Code: 27801
(2) Geographic Coordinates: Latitude": 35 ° 57 ' 47.29 " or °
Longitude": 77
° 46 ' 54.75 "or °
Reference Datum: NAD83 (NSRS2007) Accuracy: 0.08 feet
Method of Collection: Professional Land Survey
"FOR AIR INJECTION AND AQUIFER TEST WELLS ONLY: A FACILITY SITE MAP WITH PROPERTY
BOUNDARIES MAY BE SUBMITTED IN LIEU OF GEOGRAPHIC COORDINATES.
TREATMENT AREA
Land surface area of contaminant plume: 2,500 square feet
Land surface area of inj. well network: 2,500 square feet (< 10,000 ft2 for small-scale injections)
Percent of contaminant plume area to be treated: —100% (must be < 5% of plume for pilot test injections)
Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 2

H. INJECTION ZONE MAPS — Attach the following to the notification.
(1) Contaminant plume map(s) with isoconcentration lines that show the horizontal extent of the
contaminant plume in soil and groundwater, existing and proposed monitoring wells, and existing and
proposed injection wells; and
(2) Cross-section(s) to the known or projected depth of contamination that show the horizontal and vertical
extent of the contaminant plume in soil and groundwater, changes in lithology, existing and proposed
monitoring wells, and existing and proposed injection wells.
(3) Potentiometric surface map(s) indicating the rate and direction of groundwater movement, plus existing
and proposed wells.
I. DESCRIPTION OF PROPOSED INJECTION ACTIVITIES AT THE SITE — Provide a brief narrative
regarding the cause of the contamination, and purpose, scope, goals of the proposed injection activity:
The purpose of the proposed injection is to treat localized areas of groundwater contaminated with 1, 1 -biphenyl,
and/or diphenyl ether. The proposed injection of ORC-Advanced and P1umeStop is expected to stimulate aerobic
biodegradation of the contaminants to concentrations below the 2L Standards. Twenty-two (22) Gallons of a
30% ORC Advanced® solution will be injected into the subsurface (8 to 15 feet below grade) into each of 6 DPT
boreholes and approximately 200 pounds of P1umeStop (295 ,gallons of solution) will be injected into each of 14
DPT boreholes in the vicinity of well MW-20. The injection area near MW-20 is 30 feet x 20 feet. The injectants
will be delivered at low pressure (less than 20 psi) and at less than 10 gpm in a single application. Quarterly
post -injection groundwater monitoring will be performed on MW-20 to assess performance.
J. WELL CONSTRUCTION DATA
(1) No. of injection wells: 20 DPT Points Proposed Existing (provide NC Well
Construction Record (GW-1) for each well)
(2) Appx. injection depths (BLS): 15 feet
(3) For Proposed wells or Existing wells not having GW-1s, provide well construction details for each
injection well in a diagram or table format. A single diagram or line in a table can be used for
multiple wells with the same construction details. Well construction details shall include the
following (indicate if construction is proposed or as -built): See Section I. Above
(a) Well type as permanent, Geoprobe/DPT, or subsurface distribution infiltration gallery
(b) Depth below land surface of casing, each grout type and depth, screen, and sand pack
(c) Well contractor name and certification number
K. INJECTION SUMMARY
NOTE: Onlv iniectants annroved by the enidemioloev section ofthe NC Division ofPublic Health. Department
of Health and Human Services can be injected. Approved injectants can be found online at
hlt 2:Hdeg.nc.jzov/about/divisions/water-resources/water-resources-permits/wastewater-branch/ground-watgr-
protection/ground-water-approved-injectants. All other substances must be reviewed by the DHHSprior to use.
Contact the UIC Program for more info if you wish to get approval for a different additive. However, please
note it may take 3 months or lonzer. If no injectants are to be used use N/A.
Injectant: ORC Advanced® by Re_e� nesis Total Amt. to be injected (gal)/event: 130 gallons
Injectant: P1umeStop® by Regenesis Total Amt. to be injected (gal)/event: 4,130 gallons
Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 3

Inj ectant:
Inj
Inj
Total Amt. to be injected (gal/event):
Total Amt. to be injected (gal)/event_
Total Amt. to be injected (gal
Total Amt. to be injected (gal)/event:
No. of separate injection events: 1 Total Amt. to be injected (gal): 4,260 11allons
Source of Water (if applicable): Local Fire Hydrant
L. MONITORING PLAN — Describe below or in separate attachment a monitoring plan to be used to determine
if violations of groundwater quality standards specified in Subchapter 02L result from the injection activity.
Groundwater monitoring of select monitoring wells will occur quarterly followingthe he injection as prescribed in
the Groundwater RAP prepared and submitted under the Voluntary Cleanup Programy the Re isg tered
Environmental Consultant (REC).
M. SIGNATURE OF APPLICANT AND PROPERTY OWNER
Well Owner/Applicant: `I hereby certify, under penalty of law, that I am familiar with the information
submitted in this document and all attachments thereto and that, based on my inquiry of those individuals
immediately responsible for obtaining said information, I believe that the information is true, accurate and
complete. I am aware that there are significant penalties, including the possibility of fines and imprisonment,
for submitting false information. I agree to construct, operate, maintain, repair, and if applicable, abandon the
injection well and all related appurtenances in accordance with the 1 SA NCAC 02C 0200 Rules. "
Ed Kuhn, Phillips 66 Contract Program Manager
Signature of Applicant Print or Type Full Name and Title
Property Owner (if the property is not owned by the Well Owner/Applicant):
"As owner of the property on which the injection well(s) are to be constructed and operated, I hereby consent to
allow the applicant to construct each injection well as outlined in this application and agree that it shall be the
responsibility of the applicant to ensure that the injection wells) conform to the Well Construction Standards
(1 SA NCAC 02C . 0200). "
"Owner" means any person who holds the fee or other property rights in the well being constructed. A well
is real property and its construction on land shall be deemed to vest ownership in the land owner, in the
absence of contrary agreement in writing.
Refer to Access Agreement (Att E) Bill Whitworth, Director of Manufacturing
Signature* of Property Owner (if different from applicant) Print or Type Full Name and Title
*An access agreement between the applicant and property owner may be submitted in lieu of a signature on this form.
Please send 1 (one) hard color copy of this NOI along with a copy on an attached CD or Flash Drive at least
two (2) weeks prior to injection to:
DWR — UIC Program
1636 Mail Service Center
Raleigh, NC 27699-1636
Telephone: [phone]
Deemed Permitted GW Remediation NOI Rev. 2-17-2020 Page 4

GHD I NCDE — 072847Notificafion of Intend

64 REGENESIS
Technology -Based Solutions for the Environment
1. Identification
Product identifier
Other means of identification
Recommended use
Recommended restrictions
SAFETY DATA SHEET
Oxygen Release Compound Advanced (ORC Advanced®)
None.
Soil and Groundwater Remediation.
None known.
Manufacturer/Importer/Supplier/Distributor information
Company name Regenesis
Address 1011 Calle Sombra
San Clemente, CA 92673 USA
General information 949-366-8000
E-mail [e-mail]
Emergency phone number For Hazardous Materials Incidents ONLY (spill, leak, fire, exposure or accident), call
CHEMTREC 24/7 at:
USA, Canada, Mexico (+)1-800-424-9300
International (+)1-703-527-3887
2. Hazard identification
Physical hazards Oxidising solids Category 2
Health hazards Skin corrosion/irritation Category 2
Serious eye damage/eye irritation Category 1
Specific target organ toxicity following single Category 3 respiratory tract irritation
exposure
Label elements
< > >
Signal word Danger
Hazard statement May intensify fire; oxidiser. Causes skin irritation. Causes serious eye damage. May cause
respiratory irritation.
Precautionary statement
Prevention Keep away from heat, hot surfaces, sparks, open flames and other ignition sources. No smoking.
Keep away from clothing and other combustible materials. Avoid breathing dust. Wash thoroughly
after handling. Use only outdoors or in a well -ventilated area. Wear protective gloves/protective
clothing/eye protection/face protection.
Response IF ON SKIN: Wash with plenty of water. IF INHALED: Remove person to fresh air and keep
comfortable for breathing. IF IN EYES: Rinse cautiously with water for several minutes. Remove
contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON
CENTRE/doctor. If skin irritation occurs: Get medical advice/attention. Take off contaminated
clothing and wash it before reuse. In case of fire: Use appropriate media to extinguish.
Storage Store in a well -ventilated place. Keep container tightly closed. Store locked up.
Disposal Dispose of contents/container in accordance with local/regional/national/international regulations.
Other hazards None known.
Supplemental information None.
3. Composition/information on ingredients
Mixtures
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 1/8

Chemical name Common name and CAS number %
synonyms
Calcium peroxide 1305-79-9 >_75
Calcium hydroxide 1305-62-0 <_25
Dipotassium Phosphate 7758-11-4 <5
Monopotassium Phosphate 7778-77-0 <5
Composition comments All concentrations are in percent by weight unless otherwise indicated.
4. First -aid measures
Inhalation
Remove victim to fresh air and keep at rest in a position comfortable for breathing. Call a POISON
CENTRE or doctor/physician if you feel unwell.
Skin contact
IF ON CLOTHING: rinse immediately contaminated clothing and skin with plenty of water before
removing clothes. Rinse skin with water/shower. If skin irritation occurs: Get medical
advice/attention. Wash contaminated clothing before reuse.
Eye contact
Do not rub eyes. Immediately flush eyes with plenty of water for at least 15 minutes. Remove
contact lenses, if present and easy to do. Continue rinsing. Get medical attention immediately.
Ingestion
Never give anything by mouth to a victim who is unconscious or is having convulsions. Rinse
mouth. Do not induce vomiting. If vomiting occurs, keep head low so that stomach content doesn't
get into the lungs. Get medical attention if symptoms occur.
Most important
Severe eye irritation. Symptoms may include stinging, tearing, redness, swelling, and blurred
symptoms/effects, acute and
vision. Permanent eye damage including blindness could result. Dusts may irritate the respiratory
delayed
tract, skin and eyes. Skin irritation. May cause redness and pain.
Indication of immediate
Provide general supportive measures and treat symptomatically. Keep victim under observation.
medical attention and special
Symptoms may be delayed.
treatment needed
General information
Take off all contaminated clothing immediately. Contact with combustible material may cause fire.
Ensure that medical personnel are aware of the material(s) involved, and take precautions to
protect themselves. Wash contaminated clothing before reuse.
5. Fire -fighting measures
Suitable extinguishing media
Water spray, fog (flooding amounts). Foam. Dry chemical powder. Carbon dioxide (CO2).
Unsuitable extinguishing
None known.
media
Specific hazards arising from
Greatly increases the burning rate of combustible materials. Containers may explode when
the chemical
heated. During fire, gases hazardous to health may be formed. Combustion products may include:
metal oxides.
Special protective equipment
Self-contained breathing apparatus and full protective clothing must be worn in case of fire.
and precautions for firefighters
Fire fighting
In case of fire and/or explosion do not breathe fumes. Move containers from fire area if you can do
equipment/instructions
so without risk. Use water spray to cool unopened containers.
Specific methods
Cool containers exposed to flames with water until well after the fire is out.
General fire hazards
May intensify fire; oxidiser. Contact with combustible material may cause fire.
6. Accidental release measures
Personal precautions, Keep unnecessary personnel away. Keep people away from and upwind of spill/leak. Keep away
protective equipment and from clothing and other combustible materials. Wear appropriate protective equipment and
emergency procedures clothing during clean-up. Use a NIOSH/MSHA approved respirator if there is a risk of exposure to
dust/fume at levels exceeding the exposure limits. Do not touch damaged containers or spilled
material unless wearing appropriate protective clothing. Ensure adequate ventilation. Local
authorities should be advised if significant spillages cannot be contained. For personal protection,
see section 8 of the SDS.
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 2/8

Methods and materials for Eliminate all ignition sources (no smoking, flares, sparks, or flames in immediate area). Collect
containment and cleaning up dust using a vacuum cleaner equipped with HEPA filter. Keep combustibles (wood, paper, oil etc)
away from spilled material. Ventilate the contaminated area. Stop the flow of material, if this is
without risk. Absorb in vermiculite, dry sand or earth and place into containers.
Large Spills: Sweep up or vacuum up spillage and collect in suitable container for disposal. Shovel
the material into waste container. Minimise dust generation and accumulation. Avoid the
generation of dusts during clean-up. Following product recovery, flush area with water.
Small Spills: Wipe up with absorbent material (e.g. cloth, fleece). Clean surface thoroughly to
remove residual contamination.
Never return spills to original containers for re -use. Place all material into loosely covered plastic
containers for later disposal. For waste disposal, see section 13 of the SIDS. Wear appropriate
protective equipment and clothing during clean-up.
Environmental precautions Avoid discharge into drains, water courses or onto the ground.
7. Handling and storage
Precautions for safe handling Minimise dust generation and accumulation. Routine housekeeping should be instituted to ensure
that dusts do not accumulate on surfaces. Keep away from heat. Provide appropriate exhaust
ventilation at places where dust is formed. Keep away from clothing and other combustible
materials. Take any precaution to avoid mixing with combustibles. Avoid contact with water and
moisture. Do not get this material in contact with eyes. Avoid contact with eyes, skin, and clothing.
Avoid prolonged exposure. Wear appropriate personal protective equipment. Observe good
industrial hygiene practices.
Conditions for safe storage, Keep away from heat. Store in a cool, dry place out of direct sunlight. Store in original tightly
including any incompatibilities closed container. Keep container tightly closed. Store in a well -ventilated place. Do not store near
combustible materials. Store away from incompatible materials (see Section 10 of the SDS).
8. Exposure controls/personal protection
Occupational exposure limits
US. ACGIH Threshold Limit Values
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. Alberta OELs (Occupational Health & Safety Code, Schedule 1, Table 2)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. British Columbia OELs. (Occupational Exposure Limits for Chemical Substances, Occupational Health and
Safety Regulation 296/97, as amended)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. Manitoba OELs (Reg. 217/2006, The Workplace Safety And Health Act)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. Ontario OELs. (Control of Exposure to Biological or Chemical Agents)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Canada. Quebec OELs. (Ministry of Labor - Regulation respecting occupational health and safety)
Components Type Value
Calcium hydroxide (CAS TWA 5 mg/m3
1305-62-0)
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 3/8

Canada. Saskatchewan OELs (Occupational Health and Safety Regulations, 1996, Table 21)
Components Type Value
Calcium hydroxide (CAS
15 minute 10 mg/m3
1305-62-0)
8 hour 5 mg/m3
Biological limit values
No biological exposure limits noted for the ingredient(s).
Appropriate engineering
Good general ventilation should be used. Ventilation rates should be matched to conditions. If
controls
applicable, use process enclosures, local exhaust ventilation, or other engineering controls to
maintain airborne levels below recommended exposure limits. If exposure limits have not been
established, maintain airborne levels to an acceptable level. If engineering measures are not
sufficient to maintain concentrations of dust particulates below the OEL (occupational exposure
limit), suitable respiratory protection must be worn. If material is ground, cut, or used in any
operation which may generate dusts, use appropriate local exhaust ventilation to keep exposures
below the recommended exposure limits. Eye wash facilities and emergency shower must be
available when handling this product.
Individual protection measures, such as personal protective equipment
Eye/face protection
Use dust -tight, unvented chemical safety goggles when there is potential for eye contact.
Skin protection
Hand protection
Wear appropriate chemical resistant gloves. Frequent change is advisable. Recommended gloves
include rubber, neoprene, nitrile or viton.
Other
Wear appropriate chemical resistant clothing.
Respiratory protection
If engineering controls do not maintain airborne concentrations below recommended exposure
limits (where applicable) or to an acceptable level (in countries where exposure limits have not
been established), an approved respirator must be worn. Recommended use: Wear respirator with
dust filter.
Thermal hazards
Wear appropriate thermal protective clothing, when necessary.
General hygiene
Keep from contact with clothing and other combustible materials. Remove and wash contaminated
considerations
clothing promptly. Always observe good personal hygiene measures, such as washing after
handling the material and before eating, drinking, and/or smoking. Routinely wash work clothing
and protective equipment to remove contaminants.
9. Physical and chemical
properties
Appearance
Physical state
Solid.
Form
Powder.
Colour
White to pale yellow.
Odour
Odourless.
Odour threshold
Not available.
pH 12.5 (3% suspension/water)
Melting point/freezing point Not available.
Initial boiling point and boiling Not available.
range
Flash point Not available.
Evaporation rate Not available.
Flammability (solid, gas) Oxidizer.
Upper/lower flammability or explosive limits
Flammability limit - lower Not available.
(%)
Flammability limit - upper Not available.
(%)
Explosive limit - lower (%) Not available.
Explosive limit — upper
Not available.
(%)
Vapour pressure
Not available.
Vapour density
Not available.
Relative density
Not available.
Oxygen Release Compound Advanced (ORC Advanced®) SIDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 4/8

Solubility(ies)
Solubility (water)
Slightly soluble
Partition coefficient
Not available.
(n-octanol/water)
Auto -ignition temperature
Not available.
Decomposition temperature
275 °C (527 °F)
Viscosity
Not available.
Other information
Bulk density 0.5 - 0.9 g/ml
Explosive limit Non -explosive.
10. Stability and reactivity
Reactivity Greatly increases the burning rate of combustible materials.
Chemical stability Decomposes on heating. Product may be unstable at temperatures above: 275°C/527°F.
Possibility of hazardous Reacts slowly with water.
reactions
Conditions to avoid Heat. Moisture. Avoid temperatures exceeding the decomposition temperature. Contact with
incompatible materials.
Incompatible materials Acids. Bases. Salts of heavy metals. Reducing Agents. Combustible material.
Hazardous decomposition Oxygen. Hydrogen peroxide (H2O2). Steam. Heat.
products
11. Toxicological information
Information on likely routes of exposure
Inhalation Dust may irritate respiratory system. Prolonged inhalation may be harmful.
Skin contact Causes skin irritation.
Eye contact Causes serious eye damage.
Ingestion Ingestion may cause irritation and malaise.
Symptoms related to the Severe eye irritation. Symptoms may include stinging, tearing, redness, swelling, and blurred
physical, chemical and vision. Permanent eye damage including blindness could result. Dusts may irritate the respiratory
toxicological characteristics tract, skin and eyes. Skin irritation. May cause redness and pain.
Information on toxicological effects
Acute toxicity
Components
Species Test Results
Calcium hydroxide (CAS 1305-62-0)
Acute
Oral
LD50
Rat 7340 mg/kg
Dipotassium Phosphate (CAS 7758-11-4)
Acute
Oral
LD50
Rat > 2000 mg/kg
Skin corrosion/irritation
Causes skin irritation.
Serious eye damage/eye
Causes serious eye damage.
irritation
Respiratory or skin sensitisation
Canada - Alberta OELs: Irritant
Calcium hydroxide (CAS 1305-62-0)
Irritant
Respiratory sensitisation
Not a respiratory sensitiser.
Skin sensitisation
This product is not expected to cause skin sensitisation.
Germ cell mutagenicity
No data available to indicate product or any components present at greater than 0.1 % are
mutagenic or genotoxic.
Carcinogenicity
This product is not considered to be a carcinogen by IARC, ACGIH, NTP, or OSHA.
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 5/8

Reproductive toxicity
Specific target organ toxicity -
single exposure
Specific target organ toxicity -
repeated exposure
Aspiration hazard
Chronic effects
12. Ecological information
Ecotoxicity
Components
This product is not expected to cause reproductive or developmental effects.
May cause respiratory irritation.
Not classified.
Due to the physical form of the product it is not expected to be an aspiration hazard.
Prolonged inhalation may be harmful.
The product is not classified as environmentally hazardous. However, this does not exclude the
possibility that large or frequent spills can have a harmful or damaging effect on the environment.
Species Test Results
Dipotassium Phosphate (CAS 7758-11-4)
Aquatic
Acute
Algae EC50 Pseudokirchneriella subcapitata > 100 mg/I, 72 Hours
Crustacea EC50 Daphnia magna 118.9 mg/I, 48 Hours
Fish LC50 Oryzias latipes > 100 mg/I, 96 Hours
Persistence and degradability Decomposes in the presence of water. The product contains inorganic compounds which are not
biodegradable.
Bioaccumulative potential The product does not contain any substances expected to be bioaccumulating.
Mobility in soil This substance has very low solubility in water and low mobility in the environment.
Other adverse effects None known.
13. Disposal considerations
Disposal instructions
Collect and reclaim or dispose in sealed containers at licensed waste disposal site. Dispose of
contents/container in accordance with local/regional/national/international regulations.
Local disposal regulations
Dispose in accordance with all applicable regulations.
Hazardous waste code
The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.
Waste from residues / unused
Dispose of in accordance with local regulations. Empty containers or liners may retain some
products
product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Contaminated packaging
Empty containers should be taken to an approved waste handling site for recycling or disposal.
Since emptied containers may retain product residue, follow label warnings even after container is
emptied.
14. Transport information
TDG
UN number
UN1457
UN proper shipping name
CALCIUM PEROXIDE
Transport hazard class(es)
Class
5.1
Subsidiary risk
-
Packing group
II
Environmental hazards
No
Special precautions for user Read safety instructions, SDS and emergency procedures before handling.
IATA
UN number
UN1457
UN proper shipping name
Calcium peroxide
Transport hazard class(es)
Class
5.1
Subsidiary risk
-
Packing group
II
Environmental hazards
No
ERG Code
5L
Special precautions for user Read safety instructions, SDS and emergency procedures before handling.
Oxygen Release Compound Advanced (ORC Advanced®) SIDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 6/8

IMDG
UN number
UN1457
UN proper shipping name
CALCIUM PEROXIDE
Transport hazard class(es)
Class
5.1
Subsidiary risk
-
Packing group
II
Environmental hazards
Marine pollutant
No
EmS
F-G, S-Q
Special precautions for user Read safety instructions, SDS and emergency procedures before handling.
Transport in bulk according to
Not applicable.
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
Canadian regulations
Controlled Drugs and Substances Act
Not regulated.
Export Control List (CEPA 1999, Schedule 3)
Not listed.
Greenhouse Gases
Not listed.
Precursor Control Regulations
Not regulated.
International regulations
Stockholm Convention
Not applicable.
Rotterdam Convention
Not applicable.
Kyoto Protocol
Not applicable.
Montreal Protocol
Not applicable.
Basel Convention
Calcium peroxide (CAS 1305-79-9)
International Inventories
Country(s) or region
Inventory name
On inventory (yes/no)*
Australia
Australian Inventory of Chemical Substances (AICS)
Yes
Canada
Domestic Substances List (DSL)
Yes
Canada
Non -Domestic Substances List (NDSL)
No
China
Inventory of Existing Chemical Substances in China (IECSC)
Yes
Europe
European Inventory of Existing Commercial Chemical
Yes
Substances (EINECS)
Europe
European List of Notified Chemical Substances (ELINCS)
No
Japan
Inventory of Existing and New Chemical Substances (ENCS)
Yes
Korea
Existing Chemicals List (ECL)
Yes
New Zealand
New Zealand Inventory
Yes
Philippines
Philippine Inventory of Chemicals and Chemical Substances
Yes
(PICCS)
Taiwan
Taiwan Chemical Substance Inventory (TCSI)
No
United States & Puerto Rico
Toxic Substances Control Act (TSCA) Inventory
Yes
*A "Yes" indicates this product complies
with the inventory requirements administered by the governing country(s).
A "No" indicates that one or more
components of the product are not listed or exempt from listing on the inventory administered
by the governing
country(s).
Oxygen Release Compound Advanced (ORC Advanced®) SDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 7/8

16. Other information
Issue date 12-October-2015
Revision date 09-January-2019
Version No. 02
Disclaimer Regenesis cannot anticipate all conditions under which this information and its product, or the
products of other manufacturers in combination with its product, may be used. It is the user's
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
Oxygen Release Compound Advanced (ORC Advanced®) SIDS
930769 Version #: 02 Revision date: 09-January-2019 Issue date: 12-October-2015 8/8

® REGENESI_ ® 1 w 1
Technology -Based solutions for the Environment
1 0-
Product identifier PlumeSTOP°
Other means of identification None.
Recommended use Soil and Groundwater Remediation.
Recommended restrictions None known.
Manufacturer/Importer/Supplier/Distributor information
Company Name Regenesis
Address 1011 Calle Sombra
San Clemente, CA 92673
Telephone [phone]
E-mail [e-mail]
Emergency phone number CHEMTREC° at 1-800-424-9300 (International)
2. Hazard(s) identification
Physical hazards
Not classified.
Health hazards
Not classified.
OSHA defined hazards
Not classified.
Label elements
Hazard symbol
None.
Signal word
None.
Hazard statement
The mixture does not meet the criteria for classification.
Precautionary statement
Prevention
Observe good industrial hygiene practices.
Response
Wash hands after handling.
Storage
Store away from incompatible materials.
Disposal
Dispose of waste and residues in accordance with local authority requirements.
Hazard(s) not otherwise
None known.
classified (HNOC)
3. Composition/information on ingredients
Mixtures
Chemical name
CAS number %
Water
7732-18-5 >75
Colloidal activated carbon s2.5
7440-44-0 <25
µm
Proprietary additives
<2
Composition comments
All concentrations are in percent by weight unless otherwise indicated.
4. First -aid measures
Inhalation Move to fresh air. Call a physician if symptoms develop or persist.
Skin contact Wash off with soap and water. Get medical attention if irritation develops and persists.
Eye contact Rinse with water. Get medical attention if irritation develops and persists.
Ingestion Rinse mouth. Get medical attention if symptoms occur.
Most important Direct contact with eyes may cause temporary irritation.
symptoms/effects, acute and
delayed
PlumeSTOPa SDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 1/6

Indication of immediate Treat symptomatically.
medical attention and special
treatment needed
General information If you feel unwell, seek medical advice (show the label where possible). Show this safety data
sheet to the doctor in attendance.
5. Fire -fighting measures
Suitable extinguishing media Carbon dioxide, alcohol -resistant foam, dry chemical, water spray, or water fog.
Unsuitable extinguishing None known.
media
Specific hazards arising from During fire, gases hazardous to health may be formed. Combustion products may include: carbon
the chemical monoxide, carbon dioxide, sodium oxides, metal oxides.
Special protective equipment Use protective equipment appropriate for surrounding materials.
and precautions for firefighters
Fire fighting Move containers from fire area if you can do so without risk.
equipmentli nstructions
Specific methods Use standard firefighting procedures and consider the hazards of other involved materials. Use
water spray to keep fire -exposed containers cool.
General fire hazards This material will not burn until the water has evaporated. Residue can burn. When dry may form
combustible dust concentrations in air.
6. Accidental release measures
Personal precautions,
Keep unnecessary personnel away. Avoid contact with spilled material. For personal protection,
protective equipment and
see section 8 of the SIDS.
emergency procedures
Methods and materials for
This product is miscible in water.
containment and cleaning up
Large Spills: Stop the flow of material, if this is without risk. Dike the spilled material, where this is
possible. Cover with plastic sheet to prevent spreading. Absorb in vermiculite, dry sand or earth
and place into containers. Following product recovery, flush area with water.
Small Spills: Wipe up with absorbent material (e.g. cloth, fleece). Clean surface thoroughly to
remove residual contamination.
Never return spills to original containers for re -use. For waste disposal, see section 13 of the SDS.
Environmental precautions Avoid discharge into drains, water courses or onto the ground.
7. Handling and storage
Precautions for safe handling Avoid contact with skin and eyes. Avoid prolonged exposure. Observe good industrial hygiene
practices. Wash thoroughly after handling. Wear appropriate personal protective equipment (See
Section 8).
Conditions for safe storage, Store in original tightly closed container. Store away from incompatible materials (see Section 10
including any incompatibilities of the SDS). Protect from freezing.
8. Exposure controls/personal protection
Occupational exposure limits
US. OSHA Table Z-3 (29 CFR
1910.1000)
Components
Type Value Form
Colloidal activated carbon
TWA 5 mg/m3 Respirable fraction.
:52.5 pm (CAS 7440-44-0)
15 mg/m3 Total dust.
US. NIOSH: Pocket Guide to Chemical Hazards
Components
Type Value Form
Colloidal activated carbon
TWA 2.5 mg/m3 Respirable.
:52.5 pm (CAS 7440-44-0)
Biological limit values
No biological exposure limits noted for the ingredient(s).
Appropriate engineering
Good general ventilation (typically 10 air changes per hour) should be used. Ventilation rates
controls
should be matched to conditions. If applicable, use process enclosures, local exhaust ventilation,
or other engineering controls to maintain airborne levels below recommended exposure limits. If
exposure limits have not been established, maintain airborne levels to an acceptable level.
PlumeSTOP°
SDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 2/6

individual protection measures, such as personal protective equipment
Eye/face protection Wear approved chemical safety goggles.
Skin protection
Hand protection Rubber, neoprene or PVC gloves are recommended. Wash hands after handling.
Other Avoid contact with the skin. Wear suitable protective clothing.
Respiratory protection Not normally needed. In case of insufficient ventilation, wear suitable respiratory equipment. If
engineering controls do not maintain airborne concentrations below recommended exposure limits
(where applicable) or to an acceptable level (in countries where exposure limits have not been
established), an approved respirator must be worn.
Thermal hazards Wear appropriate thermal protective clothing, when necessary.
General hygiene Always observe good personal hygiene measures, such as washing after handling the material
considerations and before eating, drinking, and/or smoking. Routinely wash work clothing and protective
equipment to remove contaminants.
9. Physical and chemical properties
Appearance
Physical state
Liquid.
Form
Aqueous suspension.
Color
Black.
Odor
Odorless.
Odor threshold
Not available.
pH
8-10
Melting point/freezing point
Not available.
Initial boiling point and boiling
Not available.
range
Flash point
Not flammable.
Evaporation rate
Not available.
Flammability (solid, gas)
Not applicable.
Upper/lower flammability or explosive limits
Flammability limit - lower
Not available.
N
Flammability limit - upper
Not available.
N
Explosive limit - lower (%)
Not available.
Explosive limit - upper (%)
Not available.
Vapor pressure Not available.
Vapor density Not available.
Relative density 1 - 1.2
Solubility(ies)
Solubility (water) Miscible
Partition coefficient Not available.
(n-octanol/water)
Auto -ignition temperature Not available.
Decomposition temperature Not available.
Viscosity Not available.
10. Stability and reactivity
Reactivity The product is stable and non -reactive under normal conditions of use, storage and transport.
Chemical stability Material is stable under normal conditions.
Possibility of hazardous No dangerous reaction known under conditions of normal use.
reactions
Conditions to avoid Contact with incompatible materials. Keep from freezing.
Incompatible materials Strong oxidizing agents. Water reactive materials.
PlumeSTOPI SIDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 3/6

Hazardous decomposition Combustion may produce: carbon oxides.
products
11. Toxicological information
Information on likely routes of exposure
Inhalation Prolonged inhalation may be harmful.
Skin contact Prolonged or repeated skin contact may result in minor irritation.
Eye contact Direct contact with eyes may cause temporary irritation.
Ingestion Expected to be a low ingestion hazard.
Symptoms related to the Direct contact with eyes may cause temporary irritation.
physical, chemical and
toxicological characteristics
Information on toxicological effects
Acute toxicity Not expected to be acutely toxic.
Components
Species
Colloidal activated carbon :52.5 pm (CAS 7440-44-0)
Acute
Inhalation
LC50
Oral
LD50
Skin corrosion/irritation
Serious eye damage/eye
irritation
Respiratory or skin sensitization
Respiratory sensitization
Skin sensitization
Germ cell mutagenicity
Test Results
Rat > 8500 mg/m3, air
Rat > 2000 mg/kg, (Female)
Prolonged skin contact may cause temporary irritation.
Direct contact with eyes may cause temporary irritation.
Not a respiratory sensitizer.
This product is not expected to cause skin sensitization.
No data available to indicate product or any components present at greater than 0.1% are
mutagenic or genotoxic.
Carcinogenicity This product is not considered to be a carcinogen by IARC, ACGIH, NTP, or OSHA.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
Not listed.
Reproductive toxicity
Specific target organ toxicity -
single exposure
Specific target organ toxicity -
repeated exposure
Aspiration hazard
Chronic effects
12. Ecological information
Ecotoxicity
Persistence and degradability
Bioaccumulative potential
Mobility in soil
Other adverse effects
This product is not expected to cause reproductive or developmental effects.
Not classified.
Not classified.
Not an aspiration hazard.
Prolonged inhalation may be harmful.
The product is not classified as environmentally hazardous. However, this does not exclude the
possibility that large or frequent spills can have a harmful or damaging effect on the environment.
No data is available on the degradability of this product.
No data available.
Expected to be temporarily highly mobile in soil.
None known.
13. Disposal considerations
Disposal instructions Collect and reclaim or dispose in sealed containers at licensed waste disposal site.
Local disposal regulations Dispose in accordance with all applicable regulations.
Hazardous waste code The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.
PlumeSTOP' SIDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 4/6

Waste from residues / unused Dispose of in accordance with local regulations. Empty containers or liners may retain some
products product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Contaminated packaging Empty containers should be taken to an approved waste handling site for recycling or disposal.
Since emptied containers may retain product residue, follow label warnings even after container is
emptied.
14. Transport information
DOT
Not regulated as dangerous goods.
IATA
Not regulated as dangerous goods.
IMDG
Not regulated as dangerous goods.
Transport in bulk according to Not established.
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
US federal regulations All components are listed on or exempt from the U.S. EPA TSCA Inventory List.
This product is not known to be a "Hazardous Chemical' as defined by the OSHA Hazard
Communication Standard, 29 CFR 1910.1200.
TSCA Section 12(b) Export Notification (40 CFR 707, Subpt. D)
Not regulated.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
Not listed.
CERCLA Hazardous Substance List (40 CFR 302.4)
Not listed.
Superfund Amendments and Reauthorization Act of 1986 (SARA)
Hazard categories Immediate Hazard - No
Delayed Hazard - No
Fire Hazard - No
Pressure Hazard - No
Reactivity Hazard - No
SARA 302 Extremely hazardous substance
Not listed.
SARA 311/312 Hazardous No
chemical
SARA 313 (TRI reporting)
Not regulated.
Other federal regulations
Clean Air Act (CAA) Section 112 Hazardous Air Pollutants (HAPs) List
Not regulated.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130)
Not regulated.
Safe Drinking Water Act Not regulated.
(SDWA)
US state regulations
US. Massachusetts RTK - Substance List
Not regulated.
US. New Jersey Worker and Community Right -to -Know Act
Colloidal activated carbon :52.5 pm (CAS 7440-44-0)
US. Pennsylvania Worker and Community Right -to -Know Law
Not listed.
US. Rhode Island RTK
Not regulated.
PlumeSTOP9) SIDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 5/6

US. California Proposition 65
Not Listed.
International Inventories
Country(s) or region
Inventory name
On inventory (yes/no)*
Australia
Australian Inventory of Chemical Substances (AICS)
Yes
Canada
Domestic Substances List (DSL)
Yes
Canada
Non -Domestic Substances List (NDSL)
No
China
Inventory of Existing Chemical Substances in China (IECSC)
Yes
Europe
European Inventory of Existing Commercial Chemical
No
Substances (EINECS)
Europe
European List of Notified Chemical Substances (ELINCS)
No
Japan
Inventory of Existing and New Chemical Substances (ENCS)
No
Korea
Existing Chemicals List (ECL)
Yes
New Zealand
New Zealand Inventory
Yes
Philippines
Philippine Inventory of Chemicals and Chemical Substances
Yes
(PICCS)
United States & Puerto Rico
Toxic Substances Control Act (TSCA) Inventory
Yes
*A "Yes" indicates this product complies
with the inventory requirements administered by the governing country(s).
A "No" indicates that one or more
components of the product are not listed or exempt from listing on the inventory administered
by the governing
country(s).
16. Other information, including date of preparation or last revision
Issue date 26-February-2015
Revision date -
Version # 01
Further information HMISO is a registered trade and service mark of the American Coatings Association (ACA).
HMISO ratings Health: 0
Flammability: 0
Physical hazard: 0
NFPA ratings
1 0
Disclaimer Regenesis cannot anticipate all conditions under which this information and its product, or the
products of other manufacturers in combination with its product, may be used. It is the user's
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
PlumeSTOPO SIDS US
923801 Version #: 01 Revision date: - Issue date: 26-February-2015 6/6

4
R EEG` E N IE Sft 11 S
Technology
-Based Solutions for the Environment
im r�',
Product identifier
PlumeSTOP° Nutrients
Other means of identification
None.
Recommended use
Soil and Groundwater Rernediation.
Recommended restrictions
None known.
Manufacturer/Importer/Supplier/Distributor information
Company Name
Regenesis
Address
1011 Calle Sombra
San Clemente, CA 92673
Telephone [phone]
E-mail [e-mail]
Emergency phone number CHEMTREC® at 1-800-424-9300 (International)
2. Hazard(s) identification
Physical hazards
Health hazards
OSHA defined hazards
Label elements
Hazard symbol
Signal word
Hazard statement
Precautionary statement
Prevention
Response
Storage
Disposal
Hazard(s) not otherwise
classified (HNOC)
Supplemental information
Not classified.
Not classified.
Not classified.
None.
None.
The mixture does not meet the criteria for classification.
Observe good industrial hygiene practices.
Wash hands after handling.
Store away from incompatible materials.
Dispose of waste and residues in accordance with local authority requirements.
None known.
None.
3. Composition/information on ingredients
Mixtures
The manufacturer lists no ingredients as hazardous according to OSHA 29 CFR 1910.1200.
4. First -aid measures
Inhalation
Skin contact
Eye contact
Ingestion
Most important
symptoms/effects, acute and
delayed
Indication of immediate
medical attention and special
treatment needed
General information
Move to fresh air. Call a physician if symptoms develop or persist.
Wash off with soap and water. Get medical attention if irritation develops and persists.
Do not rub eyes. Rinse with water. Get medical attention if irritation develops and persists.
Rinse mouth. Get medical attention if symptoms occur.
Dusts may irritate the respiratory tract, skin and eyes.
Treat symptomatically.
Ensure that medical personnel are aware of the material(s) involved, and take precautions to
protect themselves.
PlumeSTOP® Nutrients SDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 1/6

5. Fire -fighting measures
Suitable extinguishing media
Unsuitable extinguishing
media
Specific hazards arising from
the chemical
Special protective equipment
and precautions for firefighters
Fire fighting
equipment/instructions
Specific methods
General fire hazards
Water fog. Foam. Dry chemical powder. Carbon dioxide (CO2). Apply extinguishing media
carefully to avoid creating airborne dust.
None known.
During fire, gases hazardous to health may be formed.
Self-contained breathing apparatus and full protective clothing must be worn in case of fire.
Use water spray to cool unopened containers. Avoid dust formation.
Use standard firefighting procedures and consider the hazards of other involved materials.
No unusual fire or explosion hazards noted.
6. Accidental release measures
Personal precautions,
Keep unnecessary personnel away. Wear appropriate protective equipment and clothing during
protective equipment and
clean-up. Use a NIOSH/MSHA approved respirator if there is a risk of exposure to dust/fume at
emergency procedures
levels exceeding the exposure limits. For personal protection, see section 8 of the SIDS.
Methods and materials for
Avoid the generation of dusts during clean-up. Collect dust using a vacuum cleaner equipped with
containment and cleaning up
HEPA filter. This product is miscible in water. Stop the flow of material, if this is without risk.
Large Spills: Wet down with water and dike for later disposal. Shovel the material into waste
container. Following product recovery, flush area with water.
Small Spills: Sweep up or vacuum up spillage and collect in suitable container for disposal. For
waste disposal, see section 13 of the SDS.
Environmental precautions Avoid discharge into drains, water courses or onto the ground.
7. Handling and storage
Precautions for safe handling Minimize dust generation and accumulation. Provide appropriate exhaust ventilation at places
where dust is formed. Practice good housekeeping.
Conditions for safe storage, Store in original tightly closed container. Store in a well -ventilated place. Store away from
including any incompatibilities incompatible materials (see Section 10 of the SDS).
8. Exposure controls/personal protection
Occupational exposure limits
US. OSHA Table Z-1 Limits for Air Contaminants (29 CFR 1910.1000)
Components
Type
Value
Form
PlumeSTOP® Nutrients
PEL
5 mg/m3
Respirable fraction.
(as dust)
15 mg/m3
Total dust.
US. OSHA Table Z-3 (29 CFR 1910.1000)
Components
Type
Value
Form
PlumeSTOP® Nutrients
TWA
5 mg/m3
Respirable fraction.
(as dust)
15 mg/m3
Total dust.
50 mppcf
Total dust.
15 mppcf
Respirable fraction.
US. ACGIH Threshold Limit Values
Components
Type
Value
Form
PlumeSTOP® Nutrients
TWA
3 mg/m3
Respirable particles.
(as dust)
10 mg/m3
Inhalable particles.
Biological limit values No biological exposure limits noted for the ingredient(s).
Appropriate engineering Ensure adequate ventilation, especially in confined areas. Local exhaust is suggested for use,
controls where possible, in enclosed or confined spaces.
PlumeSTOP° Nutrients SDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 2/6

Individual protection measures, such as personal protective equipment
Eye/face protection Wear safety glasses with side shields (or goggles). Unvented, tight fitting goggles should be worn
in dusty areas.
Skin protection
Hand protection Wear appropriate chemical resistant gloves. Suitable gloves can be recommended by the glove
supplier.
Skin protection
Other Wear suitable protective clothing.
Respiratory protection In case of inadequate ventilation, use MSHA/NIOSH approved dust respirator.
Thermal hazards Wear appropriate thermal protective clothing, when necessary.
General hygiene Always observe good personal hygiene measures, such as washing after handling the material
considerations and before eating, drinking, and/or smoking. Routinely wash work clothing and protective
equipment to remove contaminants.
9. Physical and chemical properties
Appearance
Physical state Solid.
Form Powder.
Color White.
Odor
uaoriess.
Odor threshold
Not available.
pH
Not available.
Melting point/freezing point
Not available.
Initial boiling point and boiling
Not available.
range
Flash point
Not available.
Evaporation rate
Not available.
Flammability (solid, gas)
The product is non-combustible.
Upper/lower flammability or explosive
limits
Flammability limit - lower
Not available.
N
Flammability limit - upper
Not available.
N
Explosive limit - lower (%)
Not available.
Explosive limit - upper (%)
Not available.
Vapor pressure
Not available.
Vapor density
Not available.
Relative density
Not available.
Solubility(ies)
Solubility (water)
Completely soluble.
Partition coefficient
Not available.
(n-octanol/water)
Auto -ignition temperature
Not available.
Decomposition temperature
Not available.
Viscosity
Not available.
Other information
Explosive properties
Not explosive.
Oxidizing properties
Not oxidizing.
10. Stability and reactivity
Reactivity The product is stable and non -reactive under normal conditions of use, storage and transport.
Chemical stability Material is stable under normal conditions.
PlumeSTOP® Nutrients SIDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 3/6

Possibilitv of hazardous No danqerous reaction known under conditions of normal use. Ammonia fumes may be released
reactions upon heating.
Conditions to avoid Contact with incompatible materials. Excessive heat.
Incompatible materials Strong oxidizing agents. Bases.
Hazardous decomposition Ammonia fumes may be released upon heating.
products
Information on likely routes of exposure
Inhalation Dust may irritate respiratory system.
Skin contact Dust or powder may irritate the skin.
Eye contact Dust may irritate the eyes.
Ingestion Expected to be a low ingestion hazard.
Symptoms related to the Dusts may irritate the respiratory tract, skin and eyes.
physical, chemical and
toxicological characteristics
Information on toxicological effects
Acute toxicity Not expected to be acutely toxic.
Skin corrosion/irritation Prolonged skin contact may cause temporary irritation.
Serious eye damage/eye Direct contact with eyes may cause temporary irritation.
irritation
Respiratory or skin sensitization
Respiratory sensitization Not a respiratory sensitizer.
Skin sensitization This product is not expected to cause skin sensitization.
Germ cell mutagenicity No data available to indicate product or any components present at greater than 0.1 % are
mutagenic or genotoxic.
Carcinogenicity This product is not considered to be a carcinogen by IARC, ACGIH, NTP, or OSHA.
IARC Monographs. Overall Evaluation of Carcinogenicity
Not listed.
NTP Report on Carcinogens
Not listed.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
Not regulated.
Reproductive toxicity This product is not expected to cause reproductive or developmental effects.
Specific target organ toxicity - Not classified.
single exposure
Specific target organ toxicity - Not classified.
repeated exposure
Aspiration hazard Not an aspiration hazard.
12. Ecological information
Ecotoxicity The product is not classified as environmentally hazardous. However, this does not exclude the
possibility that large or frequent spills can have a harmful or damaging effect on the environment.
Persistence and degradability No data is available on the degradability of this product.
Bioaccumulative potential No data available.
Mobility in soil This product is completely water soluble and will disperse in soil.
Other adverse effects No other adverse environmental effects (e.g. ozone depletion, photochemical ozone creation
potential, endocrine disruption, global warming potential) are expected from this component.
13. Disposal considerations
Disposal instructions Collect and reclaim or dispose in sealed containers at licensed waste disposal site.
Local disposal regulations Dispose in accordance with all applicable regulations.
Hazardous waste code The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.
PlumeSTOP® Nutrients SIDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 4/6

Waste from residues / unused Dispose of in accordance with local regulations. Empty containers or liners may retain some
products product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Contaminated packaging Since emptied containers may retain product residue, follow label warnings even after container is
emptied. Empty containers should be taken to an approved waste handling site for recycling or
disposal.
DOT
Not regulated as dangerous goods.
IATA
Not regulated as dangerous goods.
IMDG
Not regulated as dangerous goods.
Transport in bulk according to Not applicable.
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
US federal regulations This product is not known to be a "Hazardous Chemical' as defined by the OSHA Hazard
Communication Standard, 29 CFR 1910.1200.
TSCA Section 12(b) Export Notification (40 CFR 707, Subpt. D)
Not regulated.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
Not regulated.
CERCLA Hazardous Substance List (40 CFR 302.4)
Not listed.
Superfund Amendments and Reauthorization Act of 1986 (SARA)
Hazard categories Immediate Hazard - No
Delayed Hazard - No
Fire Hazard - No
Pressure Hazard - No
Reactivity Hazard - No
SARA 302 Extremely hazardous substance
Not listed.
SARA 311/312 Hazardous No
chemical
SARA 313 (TRI reporting)
Chemical name
Ammonium sulfate
CAS number % by wt.
7783-20-2 40-50
Other federal regulations
Clean Air Act (CAA) Section 112 Hazardous Air Pollutants (HAPs) List
Not regulated.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130)
Not regulated.
Safe Drinking Water Act Not regulated.
(SDWA)
US state regulations
US. Massachusetts RTK - Substance List
Ammonium sulfate (CAS 7783-20-2)
US. New Jersey Worker and Community Right -to -Know Act
Not listed.
US. Pennsylvania Worker and Community Right -to -Know Law
Ammonium sulfate (CAS 7783-20-2)
US. Rhode Island RTK
Not regulated.
PlumeSTOP® Nutrients SIDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 5/6

US. California Proposition 65
California Safe Drinking Water and Toxic Enforcement Act of 1986 (Proposition 65): This material is not known to contain
any chemicals currently listed as carcinogens or reproductive toxins.
International Inventories
Country(s) or region
Inventory name
On inventory (yes/no)*
Australia
Australian Inventory of Chemical Substances (AICS)
No
Canada
Domestic Substances List (DSL)
No
Canada
Non -Domestic Substances List (NDSL)
No
China
Inventory of Existing Chemical Substances in China (IECSC)
No
Europe
European Inventory of Existing Commercial Chemical
No
Substances (EINECS)
Europe
European List of Notified Chemical Substances (ELINCS)
No
Japan
Inventory of Existing and New Chemical Substances (ENCS)
No
Korea
Existing Chemicals List (ECL)
No
New Zealand
New Zealand Inventory
No
Philippines
Philippine Inventory of Chemicals and Chemical Substances
No
(PICCS)
United States & Puerto Rico
Toxic Substances Control Act (TSCA) Inventory
No
*A "Yes" indicates this product complies
with the inventory requirements administered by the governing country(s).
A "No" indicates that one or more
components of the product are not listed or exempt from listing on the inventory administered by the governing
country(s).
16. Other information, including date of preparation or last revision
Issue date 07-January-2016
Revision date
Version # 01
HMISO ratings Health: 1
Flammability: 0
Physical hazard: 0
NFPA ratings
41 0
Disclaimer Regenesis cannot anticipate all conditions under which this information and its product, or the
products of other manufacturers in combination with its product, may be used. It is the user's
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
PlumeSTOP® Nutrients SIDS US
931709 Version #: 01 Revision date: - Issue date: 07-January-2016 6/6

GHD I NCDE — 072847Notificafion of Intend

Source: ESRI Basemap Imagery, DigitalGlobe, Vivid - USA, 2/26/2017
200 400 600
Feet
Coordinate System:
NAD 1983 UTM Zone 16N
RE: Adapted from EarthTech figure, "Site Base Map," dated October 2007;
Bartlett Engineering & Surveying, PC figure, "Mining Permit Overall Site Drawing,"
dated August 2008; and USDA 2009 NAIP Aerial Photograph.
All well locations surveyed by Taylor Wiseman & Taylor, June 2012 and January 2013
PHILLIPS 66 COMPANY
FORMER PHILLIPS FIBERS CORPORATION
ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
SITE PLAN - LOCATION OF RELEASE AREAS
072847
Oct 9, 2020
FIGURE 1
GIs File: N:\US\Baton Rouge\Projects\562\11219049\GIS\Maps\Deliverables\NCDEQ1\11219094(NCDEGi)GIS-BR001.mxd

Source: ESRI Basemap Imagery, DigitalGlobe, Vivid - USA, 2/26/2017
4 RE: Adapted from EarthTech figure, "Site Base Map," dated October 2007; PHILLIPS 66 COMPANY 072847
0 62.5 125 Bartlett Engineering & Surveying, PC figure, "Mining Permit Overall Site Drawing," FORMER PHILLIPS FIBERS CORPORATION Oct 9, 2020
dated August 2008; and USDA 2009 NAIP Aerial Photograph.
Feet All well locations surveyed by Taylor Wiseman & Taylor, June 2012 and January 2013. ' ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
Coordinate System:
NAD 1983 UTM Zone 18N DOWTHERM AAREA INJECTION LOCATIONS FIGURE 2
GIs File: N:\US\Baton Rouge\Projects\562\11219049\GIS\Maps\Deliverables\NCDEQ1\11219094(NCDEGi)GIS-BR002.mxd

Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNESIAirbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community.
PHILLIPS 66 COMPANY 11219094-RM00
0 75 150ft ^ FORMER PHILLIPS FIBERS CORPORATION Oct 12, 2020
ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
North Carolina GROUNDWATER ELEVATION AND CONTOUR MAP
StatePlaneNAD83 DOWTHERM A AREA, JULY 2019 FIGURE 3
CAD File: N:\US\Atlanta\Projects\565\11219094\Digital_Design\ACAD 2018\Figures\NCDEQ1\11219094-RM00(NCDEQI)GN-DE001.dwg

Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNESIAirbus IDS, USDA, USGS, AeroGRID, IGN, and the GIS User Community.
PHILLIPS 66 COMPANY 11219094-RM00
0 75 150ft RE: ADAPTED FROM EARTHTECH FIGURE, "SITE BASE MAP", DATED OCTOBER 2007; ^ FORMER PHILLIPS FIBERS CORPORATION Oct 12, 2020
BARTLETT ENGINEERING & SURVEYING, PC FIGURE, "MINING PERMIT OVERALL SITE ® ATLANTIC AVENUE (NC HWY 97), ROCKY MOUNT, NORTH CAROLINA
DRAWING", DATED AUGUST 2008; AND USDA 2009 NAIP AERIAL PHOTOGRAPH. ALL ,
WELL LOCATIONS SURVEYED BY TAYLOR WISEMAN & TAYLOR, JUNE 2012 AND DOWTH E RM A AREA
North Carolina JANUARY 2013.
StatePlaneNAD83 DIPHENYL ETHER CONCENTRATIONS JULY 2019 FIGURE 4
CAD File: N:\USWtlanta\Projects\565\11219094\Digital_Design\ACAD 2018\Figures\NCDEQ1\11219094-RM00(NCDEQI)GN-DE003.dwg

A
90
85
00
o
0
80
m
Q
Z
I--- 75
Z
O
70
W
J 65
Lu
60
55
50
BH-17•
A BH-18
MW-5• BH-16
•
MW-�
BH-15
MW-21 B
MW-4
• BH-19
• BH-13
•
4 BH-12
BH-11
MW-1
DW-3
MW-20 BH-10
B H-9•
BH-6
• BH-20
• MW-14
PLAN VIEW
A'
90
0
N 85
m 2 m m o o w N 80
• BH-5D
0 50 150ft
• BH-8
• BH-70 MW-8
MW-7
• BH-25
BH-4D
BH-24
MWMW-200
A'
• BH-23
•
MW-13D
MW-12
75
LEGEND
70 1 APPROXIMATE GROUNDWATER ELEVATION
WELL SCREEN
65 SANDY CLAY
SAND
CLAY
60
WEATHERED ROCK
,OQ _ APPROXIMATE EXTENT OF DIPHENYL ETHER IMPACTED
55 GROUNDWATER, ug/L
PROPOSED INJECTION ZONE
50
0 5 loft PHILLIPS 66 COMPANY 111219094-RM00
NOTE: �
Vertical Scale ROCKY MOUNT, NORTH CAROLINA Oct 12, 2020
THE GROUND ELEVATION FOR BH-18 IS APPROXIMATED. FORMER PHILLIPS FIBERS
0 50 100ft
Horizontal Scale GEOLOGIC CROSS SECTION A - A' FIGURE 5
CAD File: N:\US\Atlanta\Projects\565\11219094\Digital_Design\ACAD 2018\Figures\NCDEQI\11219094-RM00(NCDEQI)GN-DE002.dwg

GHD I NCDE — 072847Notificafion of Intend

PHYSICAL SETTING SOURCE MAP =3215868.2s
^/ County Boundary
�/ Major Roads
N Contour Lines
Earthquake epicenter, Richter 5 or greater
® Water Wells
© Public Water Supply Wells
® Cluster of Multiple Icons
o i/4 1/2
1 Mllas
Groundwater Flow Direction
0
Wildlife Areas
c I
Indeterminate Groundwater Flow at Location
0
Natural Areas
cV
Groundwater Flow Varies at Location
o
Rare & Endangered Species
SITE NAME:
072847-95 -Rocky Mount, NC
CLIENT:
Conestoga -Rovers &Associates
ADDRESS:
1245 Atlantic Avenue
CONTACT:
Sean Armbrust
Rocky Mount NC 27801
INQUIRY#:
3215868.2s
LAT/LONG:
35.9659 / 77.7807
DATE:
November 30, 2011 11:26 am

GEOCHEC " = PHYSICAL SETTING SOURCE SUMMARY
DATABASE SEARCH DISTANCE (miles)
Federal USGS 1.000
Federal FRDS PWS Nearest PWS within 1 mile
State Database 1.000
FEDERAL USGS WELL INFORMATION
LOCATION
MAP ID WELL ID FROM TP
No Wells Found
FEDERAL FRDS PUBLIC WATER SUPPLY SYSTEM INFORMATION
LOCATION
MAP ID WELL ID FROM TP
No PWS System Found
Note: PWS System location is not always the same as well location.
STATE DATABASE WELL INFORMATION
LOCATION
MAP ID WELL ID FROM TP
No Wells Found
OTHER STATE DATABASE INFORMATION
NORTH CAROLINA NATURAL HERITAGE ELEMENT OCCURRENCES
ID Class
KC50015010 Invertebrate
NC50019528 Invertebrate
NC50022568 Animal
NORTH CAROLINA SIGNIFICANT NATURAL HERITAGE AREAS DATABASE:
ID Name
460003336 LOWER TAR RIVER AQUATIC HABITAT
TC3215868.2s Page A-12

GEOCHECKn- PHYSICAL SETTING SOURCE MAP FINDINGS
GIS ID:
Classification by Type:
Occurrence Status:
GIS ID:
Classification by Type:
Occurrence Status:
GIS ID:
Classification by Type:
Occurrence Status:
Site Name:
Quality:
Acres per Polygon:
NC_NHEO NC50015010
382092
Invertebrate
Extant
NC_NHEO NC50019528
13229
Invertebrate
Extant
NC_NHEO NC50022568
352081
Animal
Extant
NC_SNHA
LOWER TAR RIVER AQUATIC HABITAT
Not Reported
2082.38
NC10003336
TC3215888.2s Page A-14

GHD I NCDE — 072847Notificafion of Intend

AOC Site #: 0020
Acquisition #: 0020
LICENSE AGREEMENT
THIS LICENSE AGREEMENT (the "Agreement") is made as of March 28, 2014, by and
between SEPRO DEVELOPMENT COMPANY IV, LLC ("Licensor") and PHILLIPS 66
COMPANY ("Licensee"); Licensor and Licensee, together, shall sometimes hereinafter be
referred to as the "Parties."
RECITALS
A. Licensor is the legal and rightful owner of a certain parcel of real property located
at 1245 Atlantic Avenue, Rocky Mount, North Carolina, further identified by the Edgecombe
County Assessor as Parcel No. 3860-08-8196 and 3860-08-8740 (the "Property"), and also referred
to as the former Phillips Fibers Corporation facility portion of the Site located at 1245 & 1301
Atlantic Avenue, Rocky Mount, North Carolina (the "Site");
B. Licensee, in cooperation with the North Carolina Department of Environment and
Natural Resources ("NCDENR"), now desires to enter the Property to continue its various
environmental investigation and/or remediation activities, including, but not limited to, the
following; as may be shown on the Site Location Map labeled as Exhibit "A," attached hereto and
incorporated herein (the "Work");
1. Continued periodic monitoring, sampling, and maintenance of
eight (8) previously installed groundwater monitoring wells,
"MW-1, MW-4, MW-9, MW-10, MW-181 LF-6, LF-71), and LF-
18;"
2. Soil removal, and other remediation activities, as may be
required; and
3. Eventual proper well abandonment in accordance with state
and/or municipal protocols.
C. The Patties desire to enter into this Agreement so that the soil and/or groundwater
can continue to be assessed and/or remediated pursuant to environmental laws and regulations;
NOW THEREFORE, in consideration of the granting of the foregoing, the mutual premises,
covenants, conditions and agreements hereinafter set forth, and other good and valuable
consideration, the receipt and adequacy of which are acknowledged, the Parties hereby agree as
follows:
1. Grant of License - Licensor hereby grants to Licensee, and its employees, representatives
and/or contractors a non-exclusive license (the "License") to enter upon the Property from time to
time in accordance with Paragraph 2 below to conduct the activities described in Recitals
Paragraph B and C above. Further, Licensor shall cause any lessees of the Property, not a party
hereto, to provide Licensee, including its consultant(s), and/or contractor(s), same License. This
License shall commence on March 28, 2014 (Effective Date), and shall end on March 28, 2024,
unless the Parties agree in writing to extend the term of the License. Notwithstanding the foregoing
sentence, Licensor may terminate this License at any time by providing Licensee with at least sixty
(60) days written notice of Licensor's intent to terminate. The Licensee and its employees,
Page 1 of 5
License Agreement PTRRC12v.1

AOC Site #: 0020
Acquisition #: 0020
representatives and/or contractors shall enter the Property at their own risk accepting the Property
"as is" without limitation. The Licensee shall also take all reasonable steps to minimize
disturbance to the Property while performing the Work and, at no cost or expense to Licensor, will
promptly restore the Property as nearly as reasonably possible to its prior condition following any
excavating or other activity affecting the topography, and will promptly remove from the Property
any waste materials generated by the Work. In any event, prior to the expiration or termination of
this License, Licensee shall, at no cost or expense to Licensor, (a) cause any excavations to be
returned to the original gradient, (b) remove all equipment placed on the Property (except for any
permanent monitoring wells still being used for data collection at the direction of the NCDENR, or
its successor in function), (c) fill and level all ditches, ruts and depressions, if any, caused by the
closure of the Licensee's excavation operations on the Property and (d) remove all debris resulting
therefrom.
2. Access to Property — Licensee shall provide Licensor with at least forty-eight (48) hours
advance notice prior to entering the Property by notifying by telephone or email either Bill
Whitford (252-391-8373; [e-mail]) or John Gardner (252-406-5954; johng@sese rn o.com),
or such substitute person as Licensor may identify by providing written notice to Licensee.
Licensee shall inform Licensor of the nature of the Work to be performed and shall coordinate its
activities with Licensor in accordance with Paragraph 6 below. Licensor's consent to allow
Licensee's requested access to the Property during normal business days/hours (Monday through
Friday, 8:00 a.m. until 5:00 p.m.) will not be unreasonably withheld; provided, however, Licensee
acknowledges and agrees that Licensor shall have no obligation to provide Licensee with access to
the Property on weekends, federal holidays, from December 23 through January 1, or on a normal
business day at a time other than between 8:00 a.m. and 5:00 p.m. (weekends, federal holidays etc.
hereinafter collectively "Business Closure Time"). If Licensee's access to the Property includes
access during any Business Closure Time, then Licensee shall promptly pay Licensor the sum of
Five Hundred Dollars ($500.00) for each day, or part of a day, of access during Business Closure
Time.
3. Compliance with Laws - Licensee shall conduct all operations which are the subject of
this License in compliance with all federal, state, and municipal statutes and ordinances, and with
all regulations, orders, and directives of appropriate governmental agencies, as such statutes,
ordinances, regulations, orders and directives now exist or provide.
4. Permits - Licensee, at no cost or expense to Licensor, shall be responsible for obtaining
any and all governmental permits and approvals which may be necessary for it to conduct any
work or activities under this Agreement. Licensor, at no cost or expense to itself, shall coordinate
and cooperate with Licensee in Licensee's activities to obtain all necessary government permits
and permissions to perform the Work.
5. Liens and Claims - Licensee will not permit any mechanics', materialmen's, or similar
liens or claims to stand against the Property for labor or material furnished in connection with any
work performed by Licensee under this Agreement. Upon reasonable and timely notice of any
such lien or claim delivered to Licensee, Licensee may bond and contest the validity and the
amount of such lien, but in all cases Licensee will immediately pay any judgment rendered, will
pay all proper costs and charges, and will have the lien or claim released at its sole expense.
Page 2 of 5
License Agreement PTRRC12v.I

AOC Site #: 0020
Acquisition #: 0020
6. Cooperation - Licensee agrees to coordinate its activities with Licensor to minimize any
impairment of access by customers or business invitees of Licensor, or of any lessee, to the
Property and any inconvenience to or disruption of Licensor's, or of any lessee's, business on the
Property.
7. Indemnity - Licensee agrees that it will indemnify and hold Licensor harmless from and
against any claims, demands, actions, suits, judgments, losses, damages, costs, or expenses
incurred as a result of personal injury, property damage, civil penalties, or fines to the extent
proximately caused in whole or in part by the negligent acts or omissions of Licensee or its
authorized contractors and employees in conducting the Work. However, this indemnity and hold
harmless obligation shall not apply to any such claims, demands, actions, suits, judgments, losses,
damages, costs, or expenses to the extent caused by the sole negligence, gross negligence, or
willful misconduct of Licensor. This indemnity, which shall survive the expiration or termination
of this License, is expressly conditioned on the following:
(a) In the event Licensor shall identify any matter to which this indemnity may apply or
receive a written notice or claim from any third party of such matter, it shall promptly, and in
every case within thirty (30) days of said written notice or claim, notify Licensee in writing of such
matter.
(b) Licensor shall cooperate with Licensee by allowing Licensee, its agents, -
representatives, contractors and consultants prompt and reasonable access to the Property for the
purpose of investigating any matter to which this indemnity may apply.
Severabilitv - In case any one or more of the provisions contained in this Agreement shall
be invalid, illegal or unenforceable in any respect, the validity, legality, and enforceability of the
remaining provisions contained herein shall not in any way be affected or impaired thereby.
8. Notices — Except with regard to the notice to be provided by Licensee in accordance with
Paragraph 2 above, any notice provided for herein or otherwise required to be given hereunder
shall be deemed received when personally served or three (3) days after mailing by certified or
registered United States mail, return receipt requested, postage prepaid, or by facsimile machine,
with transmission and receipt confirmed, or by nationally recognized overnight delivery service,
addressed as follows:
To Licensor: Sepro Development Company IV, LLC
16013 Watson Seed Farm Road
Whitakers, NC 27891
Attention: Bill Whitford
Telephone: [phone]
Facsimile:
Page 3 of S
License Agreement PTRRC12v.1

AOC Sile #: 0020
Acquislllon #: 0020
To Licensee: Phillips 66 Company
1232 Park Sheet, Suite #300
Paso Robles, CA 93446
Attention: Colleen S. Hagemann
Telephone: [phone]
Facsimile: [phone]
With Copies to: Phillips 66 Company
900 S. Central Avenue
Roxana,IL 62084
Attention: Eric S. Petersen, Program Manager
Telephone: [phone]
Facsimile: [phone]
The person and the place to which notices are to be mailed may be changed by either party
by providing written notice of same to the other.
9. Assignment - This Agreement may not be assigned by any Party without the prior written
consent of the non -assigning Party, which consent shall not be unreasonably withheld, provided,
however:
(a) Licensee may assign or transfer this Agreement to a successor in interest
("Assignee") which assumes the responsibility of conducting the Work, without consent of
Licensor. Automatically upon such assignment or transfer, Licensee shall be released from all
obligations and liabilities hereunder accruing after the effective date of such assignment or
transfer, provided that, Assignee assumes all of the obligations and liabilities hereunder accruing
after the effective date of such assignment or transfer.
(b) Licensor understands and acknowledges that should Licensor assign this Agreement,
to an assignee ("Licensor's Assignee") without the prior written consent of Licensee, acceptance
of this Agreement by Licensor's Assignee is with recourse to Licensor, and failure of Licensor's
Assignee to fulfill its obligations under this Agreement will constitute a material breach of this
Agreement by Licensor and Licensor's Assignee.
10. Change in Ownership - Licensor shall notify Licensee of any change in Property
ownership within ten (10) days of the close of Property's escrow or the recordation of a deed
indicating Licensor has transferred the Property to another person(s) or entity(ies) by providing
Licensee at a minimum, the new Property owner's name and contact information. Should Licensor
fail to notify Licensee of Licensor's transfer of the Property, Licensor agrees to indemnify
Licensee for any cause of action asserted against Licensee for trespass to the Property.
11. Governing Law - This Agreement shall be construed and interpreted and governed by and
in accordance with the local law of the State of North Carolina reference to any choice of law,
rules or policies which may refer the resolution of any dispute arising hereunder to the laws of any
other jurisdiction.
12. Entire Agreement — Except as expressly provided herein to the contrary, this Agreement
represents the full, complete and entire agreement between the Parties with respect to the subject
Page 4 of 5
License Agreement PTRRC12v.1

AOCSite #: 0020
Acquisition #: 0020
matter hereof, and the rights and remedies of the Parties shall be solely and exclusively those
herein contained, and in lieu of any remedies otherwise available at law or in equity.
13. Execution of Agreement - Each of the undersigned hereby represents and warrants that
they are authorized to execute this Agreement on behalf of the respective Parties to the Agreement,
and that this Agreement, when executed by those Parties, shall become a valid and binding
obligation, enforceable in accordance with its terms. Upon execution, this Agreement shall be
binding as to the Parties' respective parent companies, subsidiaries, affiliates, successors, heirs and
assigns.
14. Counterparts,- This Agreement may be executed in one or more counterparts, each of
which shall be deemed an original, and all of which, taken together, shall constitute one and the
same Agreement.
THE PARTIES have executed this Agreement in two (2) duplicate originals on the dates
set forth below.
LICENSOR
SEPRO DEVELOPMENT
COMPANY IV, LLC
By:
Name:
Title:
Date: /t-le� U , 20 l l
LICENSEE
PHILLIPS 66 COMPANY
Name: Bill A. Hallett
Title: Attorney -in -Fact
Date:
Page 5 of 5
License Agreement PTRRC12v.1

co
D
a