WI0100106_Injection Report_20160220

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BUNNELL-LAMMONS ENGINEERING, INC.
GEOTECHNICAL,ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS
INTERIM EVALUATION REPORT --
2015 INJECTION & MONITORING
UIC PERMIT No. WI0100106
FORMER ANDREX INDUSTRIES CORP.
180 DEAVERVIEW ROAD
ASHEVILLE,NORTH CAROLINA
BROWNFIELDS PROJECT NUMBER 07022-03-11
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BLE PROJECT NUMBER J15-1022-42
IHSB ID NUMBER NONCD0001271
GROUNDWATER INCIDENT NUMBER 6586

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BUNNELL-LAMMONS ENGINEERING, INC.
GEOTECHNICAL,ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS
February 29,2016
Underground Injection Control Program
DWR-Aquifer Protection Section
1636 Mail Service Center
Raleigh,NC 27699-1636
Attention: Mr.Mike Rogers
Subject: Interim Evaluation Report—2015 Injection&Monitoring
UIC Permit No.WI0100106
Former Andrex Industries Corp.
180 Deaverview Road
Asheville,North Carolina
BLE Project Number J15-1022-42
Brownfields Project Number 07022-03-11
NCDENR Groundwater Incident Number 6586
Dear Mr.Rogers:
As authorized by Milkco, Inc.'s acceptance of our proposal number P14-0983 (dated February 5,
2015), Bunnell-Lammons Engineering, Inc. (BLE) has performed one injection event during the
2015 calendar year at the subject site. The purpose of this project was to inject 1%milk solution to
stimulate bioremediation of the chlorinated solvent contaminants in the groundwater.
The 2015 work included the installation of two(2)injection wells(IW-1 and IW-3),baseline sampling
of the wells in the IW-1 and IW-3 areas,semi-annual sampling of 2 surface water points,the performance
of one injection event, and the performance of 3 post-injection sampling (monitoring) events. This
project is compliant with the North Carolina Brownfields Program requirements to continue
groundwater remediation and monitoring at the subject site. The enclosed report describes the work
performed and presents the results obtained in accordance with the requirements of the subject UIC
permit.
Project Information: Andrex Industries Corp(Andrei) formerly owned and operated an industrial
textile production facility located at 180 Deaverview Road within the city limits of Asheville,North
Carolina (Figure 1). The company operated a knitted fabric weaving and cutting business for
women's and children's clothing at this location. In prior years,the facility was operated as a textile
finishing business that conducted cutting, dry cleaning, shrinking and packaging of fabrics. The
subject facility was in operation since the mid-1960s, although under various ownership. A two-
story light manufacturing facility with approximately 77,000 square feet of office, manufacturing,
warehouse, storage and utility space occupied the approximately nine-acre site. Two buildings were
present at the site; a split level brick building and slab-on-grade metal building.
No dry cleaning has been conducted on site since 1995. However, prior to 1995, dry cleaning
operations were prevalent on site and the use of tetrachloroethylene (a.k.a. Perchloroethylene,PCE)
was common. Virgin PCE was stored on site in a 6,000-gallon underground storage tank (UST).
6004 PONDERS COURT PHONE [phone]
GREENVILLE,SOUTH CAROLINA 29615 FAX [phone]

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Andrei Industries—2015 Interim Evaluation Report February 29,2016
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Prior to 1989,the use of the PCE UST was discontinued and the tank was filled with sand. The UST
was replaced with a 6,000-gallon AST which was used until 1995. In 1995, dry cleaning processes
and the use of PCE were discontinued.
In 1991 concentrations of PCE were detected in the groundwater above the applicable North Carolina
Title 15A Subchapter 2L (NC2L) groundwater standards' maximum level of 0.7 µg/1 and the DEQ
issued Groundwater Incident Number 6586 for the site. Concentrations of PCE were also
documented in the soil near the PCE UST and at other subsurface facility locations. The DEQ
approved a comprehensive site assessment(CSA) and corrective action plan(CAP) for the site and
remedial efforts were conducted from 1993 through 2005. Remedial efforts consisted of the
installation and operation of two groundwater pump and treat (P&T) systems and one soil vapor
extraction(SVE) system.
The SVE and both groundwater P&T systems were operated and maintained by BLE for Andrex
from May 2003 through August 2005. Treated groundwater effluent was discharged to the sanitary
sewer under a MSD permit. BLE also performed annual site-wide groundwater and surface water
sampling and analysis for Andrex to monitor the fate of the groundwater plume. BLE submitted
quarterly reports of the remedial progress through August 2005 and annual groundwater monitoring
reports through 2005 to the DEQ to document site activities.
The remediation system operations were suspended in August 2005 at the discretion of the property
owner. Annual groundwater monitoring was also suspended at the discretion of the property owner,
with the last sampling event conducted in November 2005.
In early 2005, Andrex requested that BLE evaluate feasible remedial alternatives for the site. A
preliminary review of alternate remedial technologies identified a unique opportunity to evaluate
bioremediation at the site. Food-grade lactate containing byproducts (milk solution) from the
neighboring Milkco,Inc.(Milkco)facility were being considered for use as a bio-enhancing remedial
product for the former Andrex facility. The implementation of this type of remedial action was
dependent upon the results of a feasibility study which includes bench-and field-scale testing studies
of the lactate containing byproducts.
In 2005,Andrex retained BLE to perform a pilot study of the milk solution. The study was to include
two parts. The first part was a bench test which was to be followed by a field trial. BLE completed
the bench study in early 2006. The results showed a net decrease in PCE concentration of 30%after
40 days in those microcosms containing the highest concentrations of milk solution. Significant
concentrations of PCE daughter products were also produced in the bench study indicating successful
de-chlorination of the parent product, as anticipated. The field trial portion of the pilot test was
suspended by Andrex after the bench test results were obtained.
In 2006, Milkco entered into a Brownfield's Agreement (Agreement) with the State of North
Carolina as part of a potential purchase of the Andrex property. The property was sold in 2007 and
as part of the plan (see below) for retrofit of the subject site; Milkco removed and/or demolished
selected equipment and facility infrastructure.
In August 2007, three underground storage tanks (one PCE and two heating oil)were removed and
disposed by a contractor retained by Milkco on behalf of Andrex. The results of the activities were
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documented in a report titled Report of Limited Assessment for UST Closure dated November 26,
2007 (BLE Project No. J07-1022-20).
As part of Milkco's redevelopment plans for the site, BLE issued a plan titled Work Plan for
Redevelopment of the Andrex Brownfields Site(Milkco Cooler Expansion)dated June 13,2008(BLE
Project No. J08-1022-23). The plan addressed the Brownfields Program's requirements including
excavation and disposal of contaminated soil (source area) and continued groundwater monitoring.
The Brownfields Program(Program)reviewed and approved(with modification)the plan in a letter
to BLE dated July 7,2008. The schedule for implementation of the redevelopment plan was changed
on December 11,2008 with concurrence of the Program.
hi July 2008, BLE abandoned selected groundwater monitoring and recovery wells in accordance
with the approved redevelopment plan. The results of the well abandonment activities were
documented in a report titled Report of Well Abandonment Services for the Milkco Cooler Expansion
dated January 19,2009 (BLE Project No.J08-1022-26).
From July through September 2008, contaminated soils were removed and disposed by a contractor
retained by Milkco in accordance with the approved redevelopment plan. The results of the remedial
activities were documented in a report titled Report of Hotspot Soil Removal and Disposal for the
Milkco Cooler Expansion dated June 3,2009(BLE Project No.J08-1022-25).
By December 2008, the former Andrex brick building(s) and metal building had been demolished
with only the building slabs remaining. Additionally, all groundwater and soil remediation systems
had been dismantled, removed, and stored by Milkco. All work performed by Milkco (non-
responsible party)is in compliance with the requirements of the Program and the Agreement.
In February 2008,Andrex resumed annual groundwater monitoring at the site. BLE has performed
the sampling services and prepared and submitted reports each calendar year since 2008. The
approved redevelopment plan requires the continuation of annual groundwater monitoring and remedial
activities at the site.
In June 2010, BLE submitted a permit application to the DEQ UIC program for a field-scale pilot test
for remediation of the site's groundwater using milk solution. Subsequent information was requested
by the DWQ and that information was prepared and/or collected,and submitted by BLE in August 2010
and December 2010. On December 22,2010,the DEQ issued Injection Permit WI0100106 to Milkco.
The permit required special conditions and limitations including minor modifications to the injection
monitoring plan. The permit effective dates were December 22,2010 through November 20,2013 with
a renewal option if submitted 120 days prior to expiration of the permit.
The permit was part of a green/sustainable enhanced bioremediation approach utilizing milk solution.
The injection plan included an injection schedule with semi-annual injections planned for the first two
years. BLE proposed to conduct the project in phases with the first phase including two injection events
(and monitoring)within a 12-month period(designated"Year One"in the plan). BLE was retained by
Milkco to perform the injection and monitoring services for year one in 2011.
Subsurface injections of milk solution into four former groundwater recovery wells were performed in
May/June 2011 and September/October 2011 and monitoring was conducted as planned. The results
showed that daughter products of PCE were being created as anticipated. Based on these data,injections
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during the first half of 2012 were suspended and monitoring was conducted to determine the long-term
results of the 2011 injections. Sampling was conducted at a 60-day monitoring frequency through July
2012 and site-wide annual sampling conducted in September 2012. Based on the results obtained we
recommended the performance of a third injection event in late September 2012 with a 60-day
monitoring frequency through March 2013. These modifications were documented in a letter to the UIC
Program titled Notice of Intent for Milk Solution Injection &Monitoring[3rd Injection Event and 3
Monitoring Events (2012-2013)] dated September 12, 2012 (BLE Project No. J12-1022-35). The
UIC Program approved the plan and the 3'injections were performed in September/October 2012
with subsequent monitoring conducted through March 2013.
BLE issued an interim evaluation report documenting the performance of all 3 injection events and
the 13 monitoring events performed to evaluate the results of the field-scale pilot test. The injection
events were designated Event 1, Event 2, and Event 3. The report titled Interim Evaluation Report--
Field-Scale Pilot Test UIC Permit No. W-10100106 dated July 30,2013 (BLE Project No. J12-1022-
35) concluded that the pilot project was successful and full-scale injection should be performed as a
viable groundwater remedial measure.
At the request of Milkco, BLE prepared and submitted a permit renewal application dated July 30,
2013 and addendum dated November 19, 2013. The application included a plan for injection and
monitoring over a 5 year permit term. The application et seq. and plan was approved (with
modification)by the DEQ in a letter to Milkco dated December 13, 2013.
BLE was retained by Milkco to perform the full-scale injection and monitoring services during the 2014
calendar year. The 2014 work included the installation of one injection well and one groundwater
monitoring well,the performance of 1 pre-injection sampling(baseline event),the performance of one
injection event, and performance of 3 post-injection sampling (monitoring events). The wells were
installed in April 2014 and pre-injection monitoring was performed on May 24, 2014. One injection
event was performed from May 14,2014 to June 2,2014. The injection event was designated Event 4.
Monitoring was performed from July 2, 2014 to November 18, 2014. BLE prepared a report titled
Interim Evaluation Report—2014 Injection &Monitoring UIC Permit No. WI0100106 dated March
26,2015 (BLE Project No. J14-1022-38)which documented the results.
At the request of the DEQ,BLE prepared a plan titled Injection Plan for the 2015 Calendar Year UIC
Permit No. WI0100106 dated December 22, 2014 (BLE Project No. J14-1022-38). The DEQ
subsequently approved the plan. BLE was retained by Milkco to perform the full-scale injection and
monitoring services during the 2015 calendar year. The 2015 work included the installation of two
injection wells, the performance of 1 pre-injection sampling (baseline event), the performance of one
injection event, and performance of 3 post-injection sampling (monitoring events). The wells were
installed in March 2015 and pre-injection monitoring was performed on March 27,2015. One injection
event was performed from April 6, 2015 to April 14, 2015. Post-injection monitoring was performed
from May 14,2015 to September 17,2015.
This Interim Evaluation Report documents the performance of the 2015 injection event and provides
the data from the 2015 monitoring events performed to evaluate the results of the injection. The
report also updates the status of the long-term results for the pilot injection areas(2011-2013; Events
1-3)and for the one prior full scale injection(2014;Event 4).
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Well Installation: BLE installed two (2) injection wells (1W-1 and IW-3) in March 2015 at the
locations shown on Figures 2,3,and 4. Well installations were performed and surveyed in accordance
with the approved permit. BLE prepared and submitted a GW-1 form for each well (Appendix A)to
the DEQ. BLE also prepared well construction logs for each well which are part of this report
(Appendix A).
Milk Solution Injection: One (1) milk solution injection event was performed in 2015 in
accordance with the permit. The injection event was designated 2015 (Event 5). Recall that prior
injection events conducted during the field-scale pilot test were designated 2011-1 (Event 1), 2011-2
(Event 2),and 2012-1 (Event 3). Also recall that one prior full-scale injection event has been conducted
which was designated 2014(Event 4).
Injection Event 5 was performed from April 6, 2015 to April 14, 2015. BLE provided notice to the
DEQ prior to performance of the event and an Injection Event Record was submitted to the DEQ at the
conclusion of the event as required(Appendix B).
Quality control samples of the milk solution were collected during the injection event to evaluate the
total organic carbon(TOC)content of the injectant. The samples were 3-point composites collected at
the beginning,middle,and end of a single day of injection. Three(3)composite samples were collected
during Event 2015 and were designated IC-2015-A, IC-2015-13, and IC-2015-C. The results are
summarized on Table 1 and the laboratory analytical results are included in Appendix C. The results
indicate a minimum TOC concentration of 5,900 mg/L and a maximum TOC concentration of 8,400
mg/L. An average TOC concentration of 7,033 mg/L was calculated from the results(Table 1). The
TOC historical results from the 2011-2012 field-scale pilot test injections and 2014 full scale injection
are also included on Table 1. We conclude that the TOC content of the injectant in 2015 was consistent
throughout the injection event and similar in concentration to that analyzed during the field-scale pilot.
It should be noted that the analytical method was changed from SM 5310B to EPA 9060A in 2015. It
is possible that any differences in historical results are a milk solution mixing phenomena,a sampling
artifact,a laboratory error,or due to a difference in analytical procedure.
Injections were performed into injection well AV-1 and IW-3. A groundwater elevation map (Figure
2),a plume map(Figure 3),and a hydrogeologic profile(Figure 4)are included for reference. Please
note that the data on the maps was sourced from the 2015 annual report (circa September 2015) and
that maps are not reflective of the conditions at the time of the 2015 injection event(April 2015). Milk
solution was prepared at the Milkco facility in approximate 2,000 gallon batches and delivered to the
well heads via plastic tank. The milk solution was injected via gravity flow from the tank by hose
discharging into the well heads at the ground surface. Flow rates were adjusted via valve assembly to
match the infiltration rate of the wells. The injection start date and time and end date and time were
recorded for each batch on a field log. A summary of the total volume injected is shown on Table 2.
Plots of the injection records for IW-1 and IW-3 were prepared from the field logs(Appendix B). The
plots show the actual volume injected vs.time with a graphical illustration of the target injection volume
and target injection rate. As shown on the plots, milk solution infiltration rates into both wells were
close to the target injection rates for the duration of the injection event.
During the field-scale pilot test injections we observed that injection rates slowed from Event 1 to Event
3 in each well except RW-3. Furthermore by Event 3 recovery wells RW-1 and RW-5 appeared to be
completely clogged. It is assumed that the milk solids in the injectant clogged the screen and/or filter
pack in these wells. Rehabilitation was attempted in RW-1 and RW-5 but was unsuccessful. We
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concluded that recovery wells RW-1, RW-5, and RW-7 were no longer suitable for use as injection
points but are viable monitoring points. We also concluded that RW-3 could be used as a future
injection and monitoring point but long-term hydraulic response to injection is unknown. It should be
noted that only one injection event was performed in IW-2 in 2014. It is possible that future injections
into IW-2 may clog the well's injection zone. It should also be noted that only one injection event was
performed in IW-1 and IW-3 in 2015. It is possible that future injections into IW-1 and IW-3 may also
clog the wells' injection zones.
Monitoring Results: Groundwater and surface water monitoring was performed in 2015 as
specified in the permit and injection plan as summarized on the 2015 Full-Scale Injection and Sampling
Matrix(Table 3A)and the Injection Monitoring Plan Matrix(Table 3B).
One baseline monitoring event was performed in March 2015 prior to injection Event 5. The
monitoring event included the wells in the IW-3 injection area(IW-2,RW-1,MW-6,and MW-44), in
the IW-1 injection area(RW-3, MW-5, and MW-12), and 2 surface water sampling points (BC-1 and
JW-1)as part of the semi-annual surface water monitoring program required by the permit(Table 3B).
The groundwater and surface water samples were analyzed for TOC by Method 9060A and for VOCs
by EPA Method 8260B.
A summary of the baseline TOC results are provided on Table 4. A summary of the baseline VOC
results are provided on Table 5. The laboratory data sheets are included in Appendix D. Based on
the data from baseline sampling in 2008 and 2009 it appears that the natural background TOC
concentration in groundwater at most locations is less than 10 mg/L. Baseline TOC sampling was not
performed in the surface waters. However, data from subsequent surface water monitoring events
where TOC analyses were performed indicates that natural background TOC concentration in surface
water is less than 10 mg/L.
Three(3)groundwater monitoring events and one surface water monitoring event were performed after
injection Event 2015 at approximate 30-, 90-, and 150-day milestones. The sampling events were
conducted in May 2015 (30 day),July 2015 (90 day),and September 2015 (150 day). The September
2015 event was the regularly scheduled annual monitoring event which included surface water
monitoring. The TOC results are summarized on Table 4 and the VOC results are summarized on
Tables 6, 7, & 8. The laboratory data is provided in Appendix E (May 2015), Appendix F (July
2015),and Appendix G(September 2015).
Measurements of concentration of TOC in groundwater are used as an indicator parameter for the
subsurface migration of milk solution(injection zone limits)and to assess carbon consumption as part
of biological activity. Historical plots of TOC concentrations in groundwater have been prepared for
select wells including injection wells RW-1,RW-3,RW-5,RW-6,RW-7,IW-2,and monitoring wells
MW-5, MW-6, MW-7, MW-9, MW-10, MW-1 1, MW-12, MW-13, MW-14, MW-24, and MW-44
(Appendix H). Baseline sampling event data and injection events are illustrated on each TOC plot.
Measurements of concentrations of VOCs in groundwater are used to determine if transformation of
parent product(PCE)to daughter product(TCE, Cis-DCE, and vinyl chloride) is occurring. Plots of
PCE,TCE,Cis-DCE,and vinyl chloride(VC)concentration vs.time were prepared for injection wells
RW-1,RW-3,RW-5,RW-6,RW-7,IW-2,and monitoring wells MW-5,MW-6,MW-7,MW-9,MW-
10,MW-11,MW-12,MW-13,MW-14,MW-24, and MW-44(Appendix I).
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RW-IIIW-21IW-3 Iniecdon Area Results and Conclusions
Five injection events have been performed in this area including the 3 field-scale pilot test events in
2011 to 2012(Events 1 through 3 into RW-1),a full-scale injection event in 2014(Event 4 into IW-2),
and a full-scale injection event in 2015 (Event 5 into IW-3). Monitoring in this area includes RW-1,
IW-2,MW-6, and MW-44. Monitoring well MW-9 is also monitored(on an annual frequency)but is
currently outside the injection zone.
The TOC concentrations in RW-1 spiked significantly after injection Events 1 and 2. A smaller spike
was observed after limited volumes were injected during Event 3. TOC concentrations have been on
a steady decline since 2012 as the carbon is consumed. The TOC concentration in RW-1 was not
affected by injection into IW-2 in 2014 or by injection into IW-3 in 2015. All of the PCE and TCE
contaminant mass in RW-1 has been transformed with Cis-DCE concentration below 10 µg/L and vinyl
chloride concentration below 5 µg/L remaining in RW-1 by September 2015.
The TOC concentrations in MW-6 spiked significantly after injection Events 1 through 3. However,
the carbon quickly dissipated after each event. We conclude the MW-6 is upgradient from RW-1 and
that the migration of carbon was due to the temporary hydraulic effects of injection and to a lesser
extent diffusion. The TOC concentration in MW-6 was not affected by injection into IW-2 in 2014 or
into IW-3 in 2015. A brief spike of Cis-DCE was observed in late 2012 but returned to normal historical
concentrations until late 2013 when Cis-DCE began to increase. It's possible that treated groundwater
from the RW-3 area is moving into the MW-6 area. We conclude that there was no long-term effect in
MW-6 as the result of injections into RW-1 in 2011-2012 and there was no effect in MW-6 as the result
of injection into IW-2 in 2014 or into IW-3 in 2015. It appeared that the remaining contaminants in
MW-6 may be sourced from the upper contaminated groundwater which was to be targeted in 2015
with the installation of and injection into injection well IW-3. However,the depth to rock at the IW-3
location was much deeper than anticipated and we conclude that the injections into IW-3 may have
moved below the affected groundwater in MW-6. The shallow groundwater in MW-6 will be targeted
in 2016 with the installation of injection well IW-3A.
The TOC concentrations in MW-9 do not appear to have been affected by injection Events 1 through
5. The background TOC concentration in MW-9 is highly variable and may obscure observation of
injection-sourced TOC values. The VOC concentrations observed in MW-9 appear to be similar to
historical values. However, PCE concentrations have decreased since mid-2011 and Cis-DCE
concentrations have slightly increased since late 2012. Continued monitoring may validate these
trends.
Monitoring well MW-44 was installed in 2014 and has been sampled 5 times since installation. Neither
TOC nor VOC concentrations appear to be affected by the injection events. MW-44 will continue to
be monitored as part of future injections in the RW-1/IW-2/IW-3 area after IW-3A is installed in 2016.
RW-31IW-1 Iniection Area Results and Conclusions
Four (4) injection events have been performed in this area which includes the 3 field-scale pilot test
events in 2011 to 2012(Events 1 through 3 into RW-3)and a full-scale injection event in 2015 (Event
5 into IW-1). Monitoring in this area includes RW-3, MW-5, and MW-12. Monitoring wells MW-7
and MW-24 are also monitored (on an annual frequency) but these wells are currently outside the
injection zone.
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The TOC concentrations in RW-3 spiked significantly after injection Events 1, 2, and 3 and slightly
after injection Event 5. TOC concentrations have rapidly declined after the first 3 events as the carbon
is consumed. A majority of the VOC contaminant mass in RW-3 has been completely transformed by
2013. A slight rebound of VOCs was observed in 2014 and 2015. The residual VOC concentrations
in RW-3 will be targeted by planned injections into RW-3 and IW-1 in 2016.
The time vs. TOC concentration plots for MW-5 and MW-12 (Appendix H) shows that significant
concentrations of TOC were detected in MW-12 with lesser concentrations detected in MW-5 as the
result of injection Events 1 through 3. TOC concentrations rapidly declined after in each well after
each event as the carbon is consumed. The injection into IW-1 in 2015 showed similar TOC results in
MW-12 with rapid TOC declines. Monitoring well MW-5 showed significant increases in TOC
concentration throughout 2015 with no decline as of September 2015.
The PCE concentrations in MW-12 showed a significant decrease by 2012 with a significant increase
of Cis-DCE in mid-2011 through late 2012. PCE,TCE,Cis-DCE,and vinyl chloride all reached non-
detect in MW-12 by September 2015. The PCE concentrations in MW-5 showed a significant decrease
in with contemporaneous increase in Cis-DCE immediately after injections Events 1 through 3.
However, VOC concentrations returned to historical values after the carbon was consumed. We
concluded that the contaminant mass observed in MW-5 is sourced from the upper groundwater which
was targeted in 2015 with the installation and injection into injection well IW-1. The injections into
IW-1 in 2015 resulted in a substantial decrease in PCE and TCE concentrations in MW-5. The residual
VOC concentrations in MW-5 will be targeted by planned injections into RW-3 and IW-1 in 2016.
The TOC concentrations in MW-7 and MW-24 do not appear to have been affected by injection Events
1 through 3 or by Event 5. However, increases in TOC concentrations were observed in MW-7 in
2012/2015 and in MW-24 in 2013. The observed TOC concentration increases cannot be conclusively
attributed to injection and may be an artifact of natural fluctuations. Insufficient TOC history is
available for a determination. The VOC concentrations observed in MW-7 and MW-24 appear to be
similar to historical values and not affect by the injection events.
R W-5 Iniection Area Results and Conclusions
Three injection events have been performed in this area which includes the 3 field-scale pilot test events
in 2011 to 2012(Events 1 through 3 into RW-5). Monitoring in this area includes RW-5 and MW-10.
Monitoring wells MW-13 and MW-14 and Recovery Well RW-6 are also monitored (on an annual
frequency)but these wells are currently outside the injection zone.
The TOC concentrations in RW-5 spiked significantly after injection Events 1 and 2. A smaller spike
was observed after limited volumes of milk solution was injected during Event 3(due to well clogging).
TOC concentrations declined to under 1,000 mg/L after the injection Event 2 and then slowly increased
after injection Event 3. All the carbon had been consumed by late 2014 which was confirmed in 2015.
A majority of the contaminant mass in RW-5 had been transformed by late 2011 with low
concentrations remaining until non-detect conditions were observed by 2014. Concentrations of PCE
and TCE remained at non-detect levels in 2015. Low concentrations of Cis-DCE (3.48 µg/L) were
detected in 2015. Vinyl chloride(25.10 µg/L)was detected at an all-time high in 2015
The TOC concentrations in MW-10 spiked after every injection event and was rapidly consumed. A
majority of the contaminant mass in MW-10 had been transformed by late 2012. Rebound was
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observed beginning in early 2013 and confirmed through 2015. We conclude that the contaminated
groundwater upgradient of MW-10 has migrated into the area.
The TOC and VOC concentrations in MW-13 and MW-14 appear to be unaffected by the injection into
RW-5. The TOC concentrations in RW-6 appear to be unaffected by injection into RW-5, however,
PCE concentrations have significantly declined with concentrations of Cis-DCE and VC increasing by
the end of 2014 which was confirmed in 2015. We conclude that remediated groundwater from the
RW-5 area has migrated into the RW-6 area.
RW-71Wecdon Area Results and Conclusions
Two injection events have been performed in this area which includes 2 of the field-scale pilot test
events in 2011 (Events 1 and 2). Monitoring in this area includes RW-7 and MW-11. In 2011,during
the injection events, it was discovered that the RW-7 well was clogged with tree roots and the well
screen or casing appeared to be broken at depth. The infiltration rate into RW-7 was very slow and
injection into RW-7 was discontinued during Event 2.
The TOC concentrations in RW-7 spiked significantly after injection Events 1 and 2. TOC
concentrations reached a high of 4,814 mg/L by late 2012 then declined to under 500 mg/L in late 2015
as carbon was consumed. A majority of the contaminant mass in RW-7 had been transformed by late
2012 with moderate concentrations of Cis-DCE remaining in late 2015.
The TOC concentrations in MW-I I do not appear to have been affected by injection Events 1 and 2 in
RW-7. The VOC concentrations observed in MW-11 appear to be similar to historical values. We
conclude that MW-11 is upgradient from RW-7 and that the volume of milk solution injected in RW-
7 was insufficient to affect MW-11.
Summary and Plans for Future Injection: In general the results from all injections show that
where milk solution was successfully injected into the subsurface, PCE daughter products are being
created as a result. The limiting factors for milk solution delivery into the subsurface appears to be
injection well infiltration rate, long-term well clogging issues, and the availability of milk solution.
Surface water sampling results indicate that the surface waters have been unaffected by the injection
events.
Please note that several VOCs are produced as metabolic byproducts of the groundwater
bioremediation in all injection areas. These metabolic byproducts are specified in bold text in the
footnotes on Tables 5 through 8 and are included on the laboratory results in Appendices D through
G. We anticipate that these metabolic byproducts will naturally attenuate.
Based on the preliminary evaluation of the 2015 results,BLE developed a conceptual plan for injection
and monitoring in 2016 and opened an email dialog with the DEQ to discuss those plans. The DEQ
requested that BLE prepare and submit a limited number of documents to outline plans for injection and
monitoring in 2016. The subject documents were submitted via email on December 14,2015 and were
approved by the DEQ on December 17, 2015. The plan includes installation and injection into 1 new
injection well designated IW-3A (Figure 4). Injection well IW-3A will be used to target the upper
groundwater in the MW-6/RW-1 area. Injection into IW-1 and RW-3 will be performed to address
residual contaminants present in that area. We anticipate that injection well installation and baseline
sampling will be conducted in March 2016 and that injection Event 6 will be performed in April 2016.
9

IBLE
Andrex Industries—2015 Interim Evaluation Report February 29,2016
Asheville,NC BLE Project Number J15-1022-42
Qualification of Report: The activities and evaluative approaches used in this assessment are
consistent with those normally employed in hydrogeological assessments and remediation projects of
this type. Our evaluation of site conditions has been based on our understanding of the site and project
information and the data obtained.
This report has been prepared as required by the subject permit. This report and the findings contained
herein shall not, in whole or in part,be disseminated or conveyed to any other party or used or relied
upon by any other party excluding DEQ,Milkco, and Andrex,without BLE's prior written consent.
Closing: We appreciate the opportunity to work with the DEQ on this project. Please contact us
at(864)288-1265 if you have any questions or comments regarding this report.
Sincerely,
BUNNELL-LAMMONS ENGINEERING,INC.
Andrew W.Alex der,P.G.,RSM Trevor J.Benton G.
Senior Hydrogeologist Senior Hydrogeologist
Registered,North Carolina#1475 Registered,North Carolina#2025
cc: Ms.Tracy Wahl—DWM Brownfields Program
Mr.Keith Collins—Milkco,Inc.
Mr.Andrew Moore—DWR-ARO
Mr. Stephen Gottdiener—Andrex
e:lawa projects landrex milkcolphase42 injection and monitoring 2015V 022-42 interim evaluation reportlandrex 2015 interim
evaluation report 1022-42 draft.docx
10

TABLES

Table 1
Historical Milk Solution TOC Analysis
Former Andrex Industries
Asheville,North Carolina
NCDEQ Groundwater Incident Number 6586
UIC Permit No.W10100106
BLE Project No.J15-1022-42
Pilot-Scale [3 Injection Events(2011 to 2012)]
Injection Event Number Injection Event ID Sample ID Date Result(mg/1)
IC-2011-1-A June 1, 2011 3,610
1 2011-1 IC-2011-1-13 June 7, 2011 6,940
IC-2011-1-C June 14,2011 4,970
IC-2011-1-D June 20, 2011 4,660
2 2011-2 IC-2011-2 AA September 28,2011 4,170
IC-2011-2-B October 5, 2011 3,880
3 2012 IC-2012-A September 25,2012 4,910
IC-2012-B October 4, 2012 6,470
Pilot Average All Events Not Applicable 4,951
Full-Scale [1 Injection Event(2014)]
Injection Event Number Injection Event ID Sample ID Date Result(mg/1)
IC-2014-A May 14, 2014 3,990
4 2014 IC-2014-B May 22, 2014 2,500
IC-2014-C June 2, 2014 4,100
2014 Average All Events Not Applicable 3,530
Full-Scale [1 Injection Event(2015)]
Injection Event Number Injection Event ID Sample ID Date Result(mg/1)
IC-2015-A April 6,2015 8,400
5 2015 IC-2015-B April 9,2015 5,900
IC-2015-C April 14, 2015 6,800
2015 Average All Events Not Applicable 7,033
Notes
TOC=Total Organic Carbon
Analyses by SM 5310B by Pace Analytical Services, Inc. (2011 to 2014) or EPA Method 9060A by ESC Lab Sciences(2015)
All samples are three-point composites
Injection Event 2011-1 [Start Date: May 31,2011 --End Date: June 21, 20111
Injection Event 2011-2 [Start Date: September 27, 2011 --End Date: October 10, 20111
Injection Event 2012 [Start Date: September 24,2012 --End Date: October 10,2012]
Injection Event 2014 [Start Date: May 14, 2014--End Date: June 2,2014]
Injection Event 2015 [Start Date: April 6,2015 --End Date: April 14,2015]
Prepared by:AWA
Injection TOC Results 5 Events of Tl Hist Milk Solution TOC Lab Results.xlsx Checked by:PJVH/TJB/RAD

Table 2
Milk Solution Injection Volume
Full-Scale Injection 2015
Andrex Industries
Asheville,North Carolina
NCDEQ Groundwater Incident Number 6586
BLE Project No. J15-1022-42
UIC Permit No. W10100106
o
N
4 i
O i
rl G
N
7 i
.0 .O.
IW-1 26,000 25,000
IW-3 25,496 25,000
Notes:
Injectant is a 1%milk solution via gravity feed.
Units in gallons.
Injection targets exceeded due to batching process.
Prepared by: AWA
Injection Volumes of T2 2015 Injection Volume Summary.xlsx Checked by: RAD/TJB

Table 3A
2015 Full-Scale Injection and Sampling Matrix
Andrex Industries
Asheville,North Carolina
NCDEQ Groundwater Incident Number 6586
BLE Project No.J15-1022-42
A
o �
N .�.
> o d W
O N A A N
N 7 O O r
O > V
N W ra
Neq
ti
Groundwater
MW-1 AB AB AB AB
MW-2 AB AB AB AB
MW-3 AB AB AB AB
MW-4 AB AB AB AB
MW-5 V&T V&T V&T V&T
MW-6 V&T V&T V&T V&T
MW-7 NS NS NS V&T
MW-8 AB AB AB AB
MW-8A AB AB AB AB
MW-9 NS NS NS V&T
MW-10 NS NS NS V&T
MW-11 NS NS NS V&T
MW-12 V&T V&T V&T V&T
MW-13 NS NS NS V&T
MW-14 NS NS NS V&T
MW-15 NS NS NS V
MW-16 NS NS NS V
MW-17 NS NS NS V
MW-18 NS NS NS V
MW-19 NP** NP** NP** NP**
MW-20 NS NS NS V
MW-21 NS NS NS V
MW-22 NS NS NS V
MW-23 NS NS NS V&T
MW-24 NS NS NS V&T
MW-25 NP** NP** NP** NP**
MW-26 NS NS NS V
MW-44 V&T V&T V&T V&T
IW-1 NS I NS NS NS
IW-2 V&T V&T V&T V&T
IW-3 NS I NS NS NS
RW-1 V&T V&T V&T V&T
RW-2 AB AB AB AB
RW-3 V&T V&T V&T V&T
RW-4 AB AB AB AB
RW-5 NS NS NS V&T
RW-6 NS NS NS V&T
RW-7 NS NS NS V&T
Surface Water
Smith Mill Creek 1 NS NS NS V&T
Smith Mill Creek 2 NS NS NS V&T
Smith Mill Creek 3 NS NS NS V&T
Smith Mill Creek 4 NS NS NS V&T
Smith Mill Creek 5 NS NS NS V&T
Smith Mill Creek 6 NS NS NS V&T
Bear Creek 1 V&T NS NS V&T
Bear Creek 2 NS NS NS V&T
Bear Creek 3 NS NS NS V&T
Bear Creek 4 NS NS NS V&T
Bear Creek 5 NS NS NS V&T
Jehovah Witness 1 V&T NS NS V&T
Cecil's Spring 1 NS NS NS V&T
Cecil's Spring 2 NS NS NS V&T
Notes:
V=Analyses for Volatile Organic Compounds performed by EPA 8260B
T=Analyses for Total Organic Carbon performed by EPA 9060A.
I=milk solution injected into this well.
NS=not sampled. Not on sampling matrix.
NP=not present;monitoring well was abandoned or destroyed.
AB=well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
**These wells were destroyed by grading during 2003.
Recovery/Injection well samples are grab samples collected via bailer.
Prepared by: AWA
2015 Matrix of T3A 2015 Injection and Sampling Matrix.xlsx Checked by: RAD

Table 313
Injection Monitoring Plan Matrix
Andrex Industries
Asheville,North Carolina
NCDEQ Groundwater Incident Number 6586
BLE Project No.J15-1022-42
a o
0 0 �
o
U U U
v O
W W
0 0 ° FO
b
U
O UO
y
d >
0 0 > > a cl c d
d CIO
Groundwater
RW-3 and/or*IW-1* *RW-3* X X X X
*MW-5* X X X X
*MW-12* X X X X
IW-2 and/or*IW-3* *IW-2* X X X X
*RW-1* X X X X
*MW-6* X X X X
*MW-44* X X X X
None MW-3R
IW-4 MW-7 X X X X
IW-5 MW-8R X X X X
MW-9 X X X X
IW-6 None
IW-7 RW-5 X X X X
MW-10 X X X X
MW-13 X X
MW-14 X X
IW-8 RW-6 X X X X
IW-9 RW-7 X X X X
MW-11 X X X X
IW-10 MW-23 X X
IW-11 MW-24 X X X X
IW-12 MW-25R X X X X
None MW-15 X
MW-16 X
MW-17 X
MW-18 X
MW-20 X
MW-21 X
MW-22 X
MW-26 X
Surface Water
None Smith Mill Creek 1 X
Smith Mill Creek 2 X
Smith Mill Creek 3 X
Smith Mill Creek 4 X
Smith Mill Creek 5 X
Smith Mill Creek 6 X
Bear Creek 1 X X
Bear Creek 2 X
Bear Creek 3 X
Bear Creek 4 X
Bear Creek 5 X
Jehovah Witness 1 X X
Cecil's Spring 1 X
Cecil's Spring 2 X
Notes:
Wells located outside of the Injection Zone.-
VOC analyses performed by EPA Method 8260 MSV Low Level.
TOC analyses performed by EPA Method 9060A.
It may not be possible to obtain samples at exact milestones(30,90,and 150 days,etc)
due to weekends,holidays,inclement weather,or other delays beyond our control.
Samples will be collected as near the milestone dates as the schedule allows.
*Injection/monitoring in the 2015 calendar year.*
Prepared by: AWA
Table 3B Monitoring Plan of T3B 2015 Injection Monitoring Plan Matrix.xlsx Checked by: TJB

Table 4
TOC Historical Data Summary - Groundwater & Surface Water Samples
Andrex Industries
Asheville,North Carolina
NCDEQ Groundwater Incident Number 6586
BLE Project No.J15-1022-42
i
i
W W O O W o
N S".
a$ Cd N N N N N
eq
C v O
N
vi O\ y O p 40 O O O =5 N O O oo 4
N N N ,_, 7 N N ,_, ,--i '7 N ,--� ON
0o W W W O W
N N .~-i N N
N O N
O V N v N to N c� U O N V N cd U U N N U CCJ
c� O U •^ 'O Q" Qr 70 i-4 c5� !�. c5� 7 1-O�
Groundwater
MW-1 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
MW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
MW-3 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
MW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
MW-5 2.1 1.2 18.5 5.2 2.9 ND 34.9 18.0 3.5 4.1 21.4 E 41.5 10.0 14.6 5.1 NS NS ND NS 1.2 2,800 3,600 4,740
MW-6 5.9 NS 10.6 15.6 17.8 21.9 22.5 33.1 6.4 5.7 4.6 E 7.6 5.6 32.3 8.8 6.8 6.1 2.1 2.0 2.2 ND 3.0 3.3
MW-7 ND ND NS ND ND NS 1.2 NS NS NS NS 8.0 C NS NS NS 1.2 NS NS ND NS NS NS NS 17.8
MW-8 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
MW-8A AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
MW-9 4.7 25.9 NS 4.9 4.0 NS 4.0 NS NS NS NS 9.9 C NS NS 4.7 31.2 NS NS ND NS NS NS NS 2.5
MW-10 5.8 ND 369 333 311 178 49.3 98 151 240 60 27 C 23.1 77.1 10.2 12.1 NS NS ND NS NS NS NS 2.0
MW-11 4.0 ND 3.6 4.1 3.6 4.4 3.7 4.1 4.3 NS NS E NS NS 3.4 3.5 NS NS ND NS NS NS NS 1.4
MW-12 1.3 ND 231 355 329 1,150 613 320 53 19.4 13.5 E 1,140 668 300 39.1 NS NS 3.0 NS 5.8 780 270 69.5
MW-13 3.8 ND NS 1.9 2.1 NS 2.6 NS 1.4 NS NS ND NS NS 2.2 2.7 NS NS ND NS NS NS NS ND
MW-14 2.2 ND NS 1.5 1.6 NS 1.6 NS 1.5 NS NS E NS NS 2.0 2.1 NS NS ND NS NS NS NS ND
MW-15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-17 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-19 NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP**
MW-20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS ND NS NS NS NS ND
MW-24 NS NS NS NS NS NS NS NS ND NS NS NS NS NS 1.8 2.2 NS NS ND NS NS NS NS ND
MW-25 NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP**
MW-26 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-44 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 4.8 6.3 ND ND 2.2 1.8 2.0 1.5
IW-1 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP I NS NS NS
IW-2 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 47.4 1 2,370 2,600 4,400 1,400 880 250 35.7
IW-3 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP I NS NS NS
RW-1 6.4 ND I 363 720 4,590 1 6,400 4,480 5,300 4,460 2,660 1,600 1,244 C I 2,210 1,270 738 333 667 412 190 170 71 53 37 37.5
RW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
RW-3 3.4 ND 1 320 1,400 138 I 1,970 3,960 1,190 779 296 143 93 C I 2,730 274 18.3 175 NS NS 47.0 NS 6.0 25 8.5 225
RW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
RW-5 5.4 19.2 1 438 518 462 I 3,630 268 31.8 970 263 550 292 C I 1,170 1,070 1,350 1,540 NS NS 16.0 NS NS NS NS 16.4
RW-6 4.3 13.4 NS 4.2 4.5 NS 6.0 NS 5.6 6.2 6.5 E 6.6 5.7 7.9 476 NS NS 1.0 NS NS NS NS 3.0
RW-7 4.3 13.7 i 2,560 3,520 3,010 I 4,030 4,230 3,720 3,020 NS NS 4,814 C NS NS 4,120 1,490 NS NS 730 NS NS NS NS 385
Surface Water
Smith Mill Creek 1 NS NS NS NS 2.2 NS NS NS NS NS NS 1.6 NS NS NS 1.6 NS NS 1.1 NS NS NS NS ND
Smith Mill Creek 2 NS NS NS NS 1.7 NS NS NS NS NS NS 2.0 NS NS NS 5.5 NS NS 1.1 NS NS NS NS 1.1
Smith Mill Creek 3 NS NS NS NS 1.7 NS NS NS NS NS NS 2.2 NS NS NS 1.6 NS NS 1.1 NS NS NS NS ND
Smith Mill Creek 4 NS NS NS NS 1.4 NS NS NS NS NS NS 2.5 NS NS NS 1.7 NS NS ND NS NS NS NS ND
Smith Mill Creek 5 NS NS NS NS 1.6 NS NS NS NS NS NS 2.5 NS NS NS 1.6 NS NS 1.0 NS NS NS NS ND
Smith Mill Creek 6 NS NS NS NS 1.6 NS NS NS NS NS NS 1.1 NS NS NS 1.6 NS NS 1.1 NS NS NS NS 1.0
Bear Creek 1 NS NS NS NS 1.2 NS NS NS NS NS NS ND NS NS NS 3.2 2.3 NS ND NS ND NS NS ND
Bear Creek 2 NS NS NS NS 1.5 NS NS NS NS NS NS 6.4 NS NS NS 1.8 NS NS ND NS NS NS NS ND
Bear Creek 3 NS NS NS NS 1.6 NS NS NS NS NS NS 1.7 NS NS NS 1.7 NS NS ND NS NS NS NS ND
Bear Creek 4 NS NS NS NS 1.6 NS NS NS NS NS NS 1.5 NS NS NS 2.0 NS NS ND NS NS NS NS ND
Bear Creek 5 NS NS NS NS 1.8 NS NS NS NS NS NS 1.2 NS NS NS 2.0 NS NS NS NS NS NS NS ND
Jehovah Witness 1 NS NS NS NS 8.7 NS NS NS NS NS NS 1.7 NS NS NS 2.1 2.5 NS ND NS ND NS NS ND
Cecil's Spring 1 r NS NS NS NS 3.2 NS NS NS NS NS NS 5.2 NS NS NS 1.9 NS NS 3.0 NS NS NS NS 10.9
Cecil's Spring 2 NS NS NS NS 1.6 NS NS NS NS NS NS 1.6 NS NS NS 2.4 NS NS 1.3 NS NS NS NS 6.2
Notes:
Analyses performed by SM 5310B. J-flagged(estimated)results if any are included on this table but are not identified(see the lab report).
Units in mg/l or parts per million(ppm)
I=milk solution injected into this well.
E=laboratory error due to contaminated containers,no data available.
C=data has been corrected from a labortary error,result is an estimate only.
ND=not detected at concentrations exceeding the laboratory reporting limit.
NS=not sampled. Not on sampling matrix or sampling personnel oversight or broken bottle or water level below injection stone pack.
NP=not present;monitoring well was abandoned or destroyed.
AB=well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
**These wells were destroyed by grading during 2003.
Recovery well samples are grab samples collected via bailer.
Prepared by:AWA
Table 4 TOC(2015)of T4 2015 TOC Summary.xlsx Checked by:RAD

Table 5 -- March 2015 [Baseline for Injection Event 51
Laboratory Analytical Results of Groundwater & Surface Water Samples
Selected Chlorinated VOCs Only
Andrex Industries
Asheville, North Carolina
NCDEQ Groundwater Incident Number 6586
BLE Project No. J15-1022-42
A
H
U
* H
a� W
U y z
0 0 0 0 0 o
U
NC 2L 0.7 3 70 0.03 200 0.6 7 0.4 100 70 2,000 0.6 50 6 0.2 NE
Groundwater
AB MW-1 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-3 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
3/27/2015 MW-5 1,800 120 ND 300 ND ND ND ND 13 520 ND ND ND ND ND 2,753
3/27/2015 MW-6 1,900 82 ND 13 ND ND 1.2 ND 3.2 900 ND ND ND ND ND 2,899
NS MW-7 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
AB MW-8 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-8A AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
NS MW-9 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2015 MW-12 ND ND ND ND ND ND ND ND 6.4 1.1 ND ND ND ND ND 7.5
NS MW-13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-17 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NP** MW-19 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP
NS MW-20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-24 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NP** MW-25 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP
NS MW-26 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2015 MW-44 6,100 350 ND 49 ND ND 1.0 ND 6.8 1,300 ND ND 1.6 ND 1.6 7,810
3/27/2015 IW-2 16 6.2 ND 4.0 ND ND ND ND 1.5 270 ND ND ND ND ND 298
3/27/2015 RW-1 ND 1.1 ND 230 ND ND ND ND 16 1,500 ND ND ND ND ND 1,747
AB RW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
3/27/2015 RW-3 ND ND ND 180 ND ND ND ND 23 820 ND ND ND ND ND 1,023
AB RW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
NS RW-5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS RW-6 NS NS NS NS NNSS
NS NS NS NS NS NS NS NS NS NS NS
NS RW-7 NS NS NS NSNS NS NS NS NS NS NS NS i NS i NS NS
NC 2B 0.7 2.5 NE 0.025 1 NE NE NE NE NE NE I NE I NE 488 488 1 0.17 1 NE
Surface Water
NS Smith Mill Creek 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 3 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 4 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 6 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2015 Bear Creek 1 19 1.7 ND ND ND ND ND ND ND 5.3 ND ND ND ND ND 26
NS Bear Creek 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 3 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 4 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
3/27/2015 Jehovah Witness 1 2.7 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.7
NS Cecil's Spring 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Cecil's Spring 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
Analyses performed by EPA Method 8260 MSV Low Level. J-flagged(estimated)results are included on this table but are not identified(see the lab report).
Units in µg/l or parts per billion(ppb)
Detected concentrations of petroleum hydrocarbon VOCs(if any)are NOT shown in this table(not part of the Andrex groundwater incident).
Detected concentrations of acetone,chloromethane,and methylene chloride(if any)are NOT shown in this table(probable laboratory contaminants).
Detected concentrations of 2-Butanone(MEK),Toluene,and 2-Hexanone(if any)are NOT shown in this table(metabolic products of bioremediation).
NC2L=North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1,2013.
NC2B=North Carolina Surface Water Standards[WS-Water Supply Classification]under Title 15A Subchapter 2B in µg/l dated Janaury 1,2015.
ND=not detected at concentrations exceeding the laboratory reporting limit.
NS=not sampled.
NP=not present;monitoring well was abandoned or destroyed.
AB=well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
*Compounds intermittently detected in the past.
**These wells were destroyed by grading during 2003.
Recovery&injection well samples are grab samples collected via bailer.
Prepared by:AWA
Table 5 (2015)of T5 to T8 Andrex IER 2015.xlsx Checked by:RAD

Table 6 -- May 2015 [30 Day Event]
Laboratory Analytical Results of Groundwater & Surface Water Samples
Selected Chlorinated VOCs Only
Andrex Industries
Asheville, North Carolina
NCDEQ Groundwater Incident Number 6586
BLE Project No. J15-1022-42
A
H
U
* H
a� W
U y z
0 0 0 0 0 o
U
NC 2L 0.7 3 70 0.03 200 0.6 7 0.4 100 70 2,000 0.6 50 6 0.2 NE
Groundwater
AB MW-1 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-3 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
5/14/2015 MW-5 14 9.6 ND 62 ND ND ND ND 4.0 380 ND ND ND ND ND 470
5/14/2015 MW-6 1,800 70 ND 18 ND ND ND ND 2.9 790 ND ND ND ND ND 2,681
NS MW-7 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
AB MW-8 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-8A AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
NS MW-9 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
5/14/2015 MW-12 ND ND ND 7.4 ND ND ND ND 3.2 27 ND ND ND ND ND 38
NS MW-13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-17 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NP** MW-19 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP
NS MW-20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-24 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NP** MW-25 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP
NS MW-26 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
5/14/2015 MW-44 6,900 390 ND 67 ND ND 1.4 ND 8.4 1,400 ND ND 2.0 ND 2.0 8,771
5/14/2015 IW-2 ND ND ND ND ND ND ND ND ND 210 ND ND ND ND ND 210
5/14/2015 RW-1 ND ND ND 48 ND ND ND ND 5.9 100 ND ND ND ND ND 154
AB RW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
5/14/2015 RW-3 ND ND ND 2.6 ND ND ND ND 2.2 13 ND ND ND ND ND 18
AB RW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
NS RW-5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS RW-6 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS RW-7 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NC 2B 0.7 2.5 NE 0.025 NE NE NE NE NE NE I NE I NE 488 488 1 0.17 1 NE
Surface Water
NS Smith Mill Creek 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 3 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 4 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 6 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 3 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 4 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Jehovah Witness 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Cecil's Spring 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Cecil's Spring 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
Analyses performed by EPA Method 8260 MSV Low Level. J-flagged(estimated)results are included on this table but are not identified(see the lab report).
Units in µg/l or parts per billion(ppb)
Detected concentrations of petroleum hydrocarbon VOCs(if any)are NOT shown in this table(not part of the Andrex groundwater incident).
Detected concentrations of acetone,chloromethane,and methylene chloride(if any)are NOT shown in this table(probable laboratory contaminants).
Detected concentrations of 2-Butanone(MEK),Toluene,and 2-Hexanone(if any)are NOT shown in this table(metabolic products of bioremediation).
NC2L=North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1,2013.
NC2B=North Carolina Surface Water Standards[WS-Water Supply Classification]under Title 15A Subchapter 2B in µg/l dated Janaury 1,2015.
ND=not detected at concentrations exceeding the laboratory reporting limit.
NS=not sampled.
NP=not present;monitoring well was abandoned or destroyed.
AB=well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
*Compounds intermittently detected in the past.
**These wells were destroyed by grading during 2003.
Recovery&injection well samples are grab samples collected via bailer.
Prepared by:AWA
Table 6(2015)of T5 to T8 Andrex IER 2015.xlsx Checked by:RAD

Table 7 -- July 2015 [90 Day Event]
Laboratory Analytical Results of Groundwater & Surface Water Samples
Selected Chlorinated VOCs Only
Andrex Industries
Asheville, North Carolina
NCDEQ Groundwater Incident Number 6586
BLE Project No. J15-1022-42
A
H
U
* H
a� W
y z
y N N 75 -S _0 0
C a�i b o� O O
o o o o
U
NC 2L 0.7 3 70 0.03 200 0.6 7 0.4 100 70 2,000 0.6 50 6 0.2 NE
Groundwater
AB MW-1 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-3 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
7/13/2015 MW-5 29 16 ND 33 ND ND ND ND 5.8 720 ND ND ND ND ND 804
7/13/2015 MW-6 1,900 77 ND 16 ND ND ND ND 2.9 1,000 ND ND ND ND ND 2,996
NS MW-7 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
AB MW-8 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-8A AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
NS MW-9 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
7/13/2015 MW-12 ND ND ND 11 ND ND ND ND 5.0 67 ND ND ND ND ND 83
NS MW-13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-17 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NP** MW-19 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP
NS MW-20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS MW-24 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NP** MW-25 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP
NS MW-26 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
7/13/2015 MW-44 6,700 440 ND 54 ND ND 1.4 ND 7.2 1,300 ND ND 1.7 ND 1.8 8,506
7/13/2015 IW-2 2.2 ND ND 6.0 ND ND ND ND 1.0 94 ND ND ND ND ND 103
7/13/2015 RW-1 ND ND ND 34 ND ND ND ND 6.8 86 ND ND ND ND ND 127
AB RW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
7/13/2015 RW-3 ND ND ND ND ND ND ND ND 2.9 5.0 ND ND ND ND ND 7.9
AB RW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
NS RW-5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS RW-6 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS RW-7 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NC 2B 0.7 2.5 NE 0.025 NE NE NE NE NE NE I NE I NE 488 488 1 0.17 1 NE
Surface Water
NS Smith Mill Creek 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 3 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 4 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Smith Mill Creek 6 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 3 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 4 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Bear Creek 5 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Jehovah Witness 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Cecil's Spring 1 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
NS Cecil's Spring 2 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
Analyses performed by EPA Method 8260 MSV Low Level. J-flagged(estimated)results are included on this table but are not identified(see the lab report).
Units in µg/l or parts per billion(ppb)
Detected concentrations of petroleum hydrocarbon VOCs(if any)are NOT shown in this table(not part of the Andrex groundwater incident).
Detected concentrations of acetone,chloromethane,and methylene chloride(if any)are NOT shown in this table(probable laboratory contaminants).
Detected concentrations of 2-Butanone(MEK),Toluene,and 2-Hexanone(if any)are NOT shown in this table(metabolic products of bioremediation).
NC2L=North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1,2013.
NC2B=North Carolina Surface Water Standards[WS-Water Supply Classification]under Title 15A Subchapter 2B in µg/l dated Janaury 1,2015.
ND=not detected at concentrations exceeding the laboratory reporting limit.
NS=not sampled.
NP=not present;monitoring well was abandoned or destroyed.
AB=well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
*Compounds intermittently detected in the past.
**These wells were destroyed by grading during 2003.
Recovery&injection well samples are grab samples collected via bailer.
Prepared by:AWA
Table 7(2015)of T5 to T8 Andrex IER 2015.xlsx Checked by:RAD

Table 8 -- September 2015 [150 Day & Annual Event]
Laboratory Analytical Results of Groundwater & Surface Water Samples
Selected Chlorinated VOCs Only
Andrex Industries
Asheville, North Carolina
NCDEQ Groundwater Incident Number 6586
BLE Project No. J15-1022-42
Q
w
H
U
* H
a� W
U y z
0 0 0 0 0 o
U
NC 2L 0.7 3 70 0.03 200 0.6 7 0.4 100 70 2,000 0.6 50 6 0.2 NE
Groundwater
AB MW-1 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-3 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
9/14/2015 MW-5 45.7 16.5 ND 21.1 ND ND ND ND 3.42 364 ND ND ND ND ND 451
9/14/2015 MW-6 1,600 62.9 ND 21.9 ND ND ND ND 2.93 768 ND ND ND ND ND 2,456
9/16/2015 MW-7 96.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 96
AB MW-8 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
AB MW-8A AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
9/15/2015 MW-9 1,150 89.3 ND 2.87 ND ND ND ND 1.96 504 ND ND ND ND ND 1,748
9/15/2015 MW-10 1,790 128 ND 24.1 ND ND ND ND 2.32 643 ND ND ND ND ND 2,587
9/15/2015 MW-11 433 39.5 ND ND ND ND ND ND 1.10 174 ND ND ND ND ND 648
9/14/2015 MW-12 ND ND ND ND ND ND ND ND 2.30 ND ND ND ND ND ND 2.30
9/15/2015 MW-13 598 120 ND ND ND ND ND ND 1.01 135 ND ND ND ND ND 854
9/15/2015 MW-14 519 375 ND ND ND ND 1.46 ND ND 143 ND ND ND ND ND 1,038
9/16/2015 MW-15 80.9 2.62 ND ND ND ND ND ND ND 5.62 ND ND ND ND ND 89
9/16/2015 MW-16 80.6 2.55 ND ND ND ND ND ND ND 4.49 ND ND ND ND ND 88
9/16/2015 MW-17 2.10 3.06 ND 5.29 ND ND ND ND ND 11.3 ND ND ND ND ND 22
9/16/2015 MW-18 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
NP** MW-19 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP
9/15/2015 MW-20 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/16/2015 MW-21 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/16/2015 MW-22 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/15/2015 MW-23 177 7.91 ND ND ND ND ND ND ND 17.6 ND ND ND ND ND 203
9/16/2015 MW-24 231 2.85 ND ND ND ND ND ND ND 10.6 ND ND ND ND ND 244
NP** MW-25 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP
9/16/2015 MW-26 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/14/2015 MW-44 6,550 348 ND 55.1 ND ND 1.28 ND 7.42 1,130 ND ND 1.85 ND 1.95 8,096
9/14/2015 IW-2 1.66 ND ND ND ND ND ND ND ND 1.07 ND ND ND ND ND 2.7
9/14/2015 RW-1 ND ND ND 3.97 ND ND ND ND 3.91 9.07 ND ND ND ND ND 17
AB RW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
9/14/2015 RW-3 3.56 2.03 ND 5.27 ND ND ND ND 4.65 34.1 ND ND ND ND ND 50
AB RW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB
9/15/2015 RW-5 ND ND ND 25.1 ND ND ND ND ND 3.58 ND ND ND ND ND 29
9/15/2015 RW-6 14 26.7 ND 188 ND ND 2.79 ND 4.77 527 ND ND ND ND ND 763
9/15/2015 RW-7 11.6 ND ND 8.91 ND ND ND ND I ND 570 1 ND ND ND ND I ND 591
NC 2B 0.7 2.5 NE 0.025 NE I NE I NE I NE NE NE I NE I NE 488 488 1 0.17 1 NE
Surface Water
9/17/2015 Smith Mill Creek 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/17/2015 Smith Mill Creek 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/17/2015 Smith Mill Creek 3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/17/2015 Smith Mill Creek 4 1.23 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.2
9/17/2015 Smith Mill Creek 5 1.02 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.0
9/17/2015 Smith Mill Creek 6 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/17/2015 Bear Creek 1 10.8 1.18 ND ND ND ND ND ND ND 3.56 ND ND ND ND ND 16
9/17/2015 Bear Creek 2 9.59 1.40 ND ND ND ND ND ND ND 2.88 ND ND ND ND ND 14
9/17/2015 Bear Creek 3 2.55 ND ND ND ND ND ND ND ND 1.08 ND ND ND ND ND 3.6
9/17/2015 Bear Creek 4 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/17/2015 Bear Creek 5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
9/17/2015 Jehovah Witness 1 24.3 2.46 ND ND ND ND ND ND ND 3.49 ND ND ND ND ND 30
9/17/2015 Cecil's Spring 1 9.88 2.50 ND ND ND ND ND ND ND 2.86 ND ND ND ND ND 15
9/17/2015 Cecil's Spring 2 5.83 ND ND ND ND ND ND I ND ND ND ND I ND IND IND ND 1 5.8
Notes:
Analyses performed by EPA Method 8260 MSV Low Level. J-flagged(estimated)results are included on this table but are not identified(see the lab report).
Units in µg/l or parts per billion(ppb)
Detected concentrations of petroleum hydrocarbon VOCs(if any)are NOT shown in this table(not part of the Andrex groundwater incident).
Detected concentrations of acetone,chloromethane,and methylene chloride(if any)are NOT shown in this table(probable laboratory contaminants).
Detected concentrations of 2-Butanone(MEK),Toluene,and 2-Hexanone(if any)are NOT shown in this table(metabolic products of bioremediation).
NC2L=North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1,2013.
NC2B=North Carolina Surface Water Standards[WS-Water Supply Classification]under Title 15A Subchapter 2B in µg/l dated Janaury 1,2015.
ND=not detected at concentrations exceeding the laboratory reporting limit.
NS=not sampled.
NP=not present;monitoring well was abandoned or destroyed.
AB=well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
*Compounds intermittently detected in the past.
**These wells were destroyed by grading during 2003.
Recovery&injection well samples are grab samples collected via bailer.
Prepared by:AWA
Table 8(2015)of T5 to T8 Andrex IER 2015.xlsx Checked by:RAD

FIGURES

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APPROXIMATE SCALE IN FEET ASHEVILLE AND ENKA, N.C. QUADRANGLES, 2013.
DRAWN, ACE DATE. 12-03-15 IBLEM
FIGURE
SITE LOCATION MAP
CHECKED: AWA CAD: ANDREX42-SLM ---- g W. FORMER ANDREX INDUSTRIES CORP.
6004 180 DEAVERVIEW ROAD
APPROVED. JOB NO: GREENVILLE, SOU CTM ARO�UNA 29615 ASHEVILLE, NORTH CAROLINA
J15-1022-42 PHONE' [phone] FAX. [phone]

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S = * GROUNDWATER ELEVATION IN WELL MW-14 IS TYPICALLY ARTESIAN
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QFo�Oa;.o'1���,� NP-A NOT PRESENT. WELL HAS BEEN ABANDONED.
i'#��►�e�f���N`' NP-D MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO
BE DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE.
MW-25 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO
NOTES. BE DESTROYED BY GRADING PERFORMED BY MILKO, INC.
1. THE GROUNDWATER PUMP AND TREAT SYSTEMS HAD BEEN APPROXIMATE DIRECTION OF GROUNDWATER FLOW
REMOVED AND WERE NOT IN OPERATION AT THE TIME WATER
LEVEL MEASUREMENTS WERE TAKEN. GROUNDWATER WAS NOT
BEING PUMPED FROM RW-1 THROUGH RW-7 WHILE _ �M� APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE
MEASUREMENTS WERE COLLECTED.
2. ** SKY LANES BOWLING CENTER O
NCDEH - PUBLIC WATER SYSTEM ID #10-11-025 EQUIPOTENTIAL CONTOUR LINE
WELL NAME: WELL #1
REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED
FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. "...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER." 200 100 0 200 400
APPROXIMATE SCALE IN FEET
REVISIONS DRAWN: DATE: 12-3-15 FIGURE N0.
No. DESCRIPTION BY ACE BMMLL-LAMwONS ENO UM8, NC. GROUNDWATER ELEVATION CONTOUR MAP - SEPTEMBER 14, 2015
CHECKED: CAD FILE: PONDERSCOURT ANDREX INDUSTRIES
AWA ANDREX42-WTM091415 GREENVILLE, SOUTH CAROUNA 29615 DEAVERVIEW ROAD
APPROVED: JOB NO: J15-1022-42 INC. PHONE: [phone] FAX: [phone] ASHEVILLE, NORTH CAROLINA

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RESIDENTIAL as9o�j I �� RW95 �----20 10 _-1 ---J o Mw-17
I � __ �G
MW-10 22v
® 2'588 O MW_6481 n \ I r- o RASH ROAD
W_6 \ROY D. FARMER RAR SM-3
BLOOMING
MADELINE AVENUE ARDENS / MW-13 ` 763 \ I ND- MW-21
(J i
ICE � 854 RW-7 \\�—J \� I� ND
RV � - -- — 591 � � �•�—\� MW-22
/ ORE, ** JW-1 \ ND
LAJ
' FORMER JEHOVAI..l
RESIDENTIAL i / \` SILVERS 500 --- 30 ' WITNESS PROPERTY�.`BIESTERFEDLT
X i RESIDENTI BOWLING PROPERTY _ 100 50 N OPERTY
� _ BC-2 ALLEY MWo384* ` ` XTON —19 pRFp�k
i 00000 -A TREET 14 ����gC-1 _ JUSTICE PROPERTY PROPERTdowsY PROPERTY i0 NP Sppty q/CRp SM1-2 \•.\, BAKER DRIVE
— � M �`.�•• r�—� ��.� — =:: / I� o FORMER q0 SM1.0
—••�• \ V �J WATER WELL
M RESIDENTIAL�'�� `\ SATTERFIELD __ CRYDERMAN SM-6 ''�• �•
w PROPERTY
am-goMALVERN HILLS PARK � �W BC-3 swoopQ � � �HOUSE- _ PROPERTY ND \
�/ 3.6 _J Q�PGF —= a w —ND Gunn 0
ND _ � s� — ® G °� � PEEN W RESIDENTIAL
�—� �•�•�M�• `\ � GR��NN��� MW-20 � Q
�•.-. - ..�_..� TENNIS 9 '—"—NDspop �\ ND HOE AV E ''\
Ole COURTS swoop donow � Q
ENU
Ile RUMBOUGH PLACEswoop swoop
~
_ RESIDENTIAL W
z
�'' �'•�''� j RESIDENTIAL �'•\
BC-5 /•' 100o F�. Z
W Q z
ND /•• Q pgttpN q N� RESIDENTIAL w \ '�'•�..�
MIDDL-MONT AVENUE us
NlpNw �� \•
PRINC LEGEND
ETpN aRI�E w
NOTES:
RESIDENTIAL w 1. LABORATORY ANALYSIS BY EPA METHOD 8260. Q5 APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR SHALLOW
z
2. WELLS AND SURFACE WATER WAS SAMPLED ON SEPTEMBER 14-17, 2015. BEDROCK) GROUNDWATER MONITORING WELL
J
z 3. CONCENTRATIONS OF CHLOROFORM INTERMITTENTLY DETECTED IN MW-20, MW-21 AND APPROXIMATE LOCATION OF EXISTING (TYPE III-BEDROCK)
MW-26 ARE PROBABLY RELATED TO LEAKING WATER SUPPLY LINES IN CLOSE O GROUNDWATER MONITORING WELL
PROXIMITY To THE WELLS.
4. SAMPLES FROM STREAMS DESIGNATED AS FOLLOWS: O RECOVERY WELL OR INJECTION WELL
SM = SMITH MILL CREEK TRIBUTARY
CS = CECIL'S SPRING APPROXIMATE LOCATION OF SURFACE WATER SAMPLES (SEE NOTE 4)
BC = BEAR CREEK
JW = FORMER JEHOVAH WITNESS PROPERTY (WATER SAMPLES COLLECTED 9-17-15).
5. NP = NOT PRESENT, WELL WAS NOT PRESENT AT TIME OF SAMPLING. o WATER SUPPLY WELL
6. ** SKY LANES BOWLING CENTER
NCDEH - PUBLIC WATER SYSTEM ID #10-11-025 CONCENTRATION OF TOTAL DETECTED CHLORINATED VOLATILE ORGANIC
�«►�►i�+� WELL NAME: WELL #1 162
.�•�Q�N CAR p� %� AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED COMPOUNDS IN PARTS PER BILLION (ppb).
"...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER."
BELOW GROUND STREAM SHOWING FLOW DIRECTION
S _ 7. * THE WELLS MAY INTERCEPT FRACTURE SETS OR MAY BE SCREENED AT
,475 ¢ : ELEVATIONS AT WHICH GROUNDWATER CONTAMINANT CONCENTRATIONS ARE }-••}— ABOVE GROUND STREAM SHOWING FLOW DIRECTION
f INCONSISTENT WITH THE ESTABLISHED PLUME. THE VALUES WERE IGNORED FOR
A� W` CONTOURING PURPOSES.
%yd pF0 Od�.�'�'��, -- PROPERTY LINE
'�.� 8. THE FORMER WATER SUPPLY WELL ON THE CRYDERMAN PROPERTY APPEARED
TO BE ABANDONED AND COULD NOT BE SAMPLED AS OF OCTOBER 2005. — �M, APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE
9. MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE
DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE. MW-25 WAS 100 TOTAL CHLORINATED CONCENTRATION CONTOUR IN PARTS PER BILLION
NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY
GRADING PERFORMED BY MILKO, INC. ND ESTIMATED LIMIT OF VOC'S
10. RECOVERY WELLS WERE NOT OPERATIONAL AT THE TIME OF SAMPLING.
REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA 200 loo 0 200 aoo VERY LOW CONCENTRATION AS THE RESULT OF GROUNDWATER
FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. APPROXIMATE SCALE IN FEET 11. AB = WELL ABANDONED IN 2008 PER APPROVED BROWNFIELD REDEVELOPMENT PLAN. REMEDIATION. IGNORED FOR CONTOURING PURPOSES.
REVISIONS DRAWN: DATE: 12-03-15 FIGURE No.
No. DESCRIPTION BY ACE BUNNELL-LAMMONS MONEERNO, NC. CONTOUR MAP OF TOTAL CHLORINATED VOLATILE ORGANIC COMPOUND ISOCONCENTRATIONS — SEPTEMBER 14-17, 2015
CHECKED: AWA CAD FILE: 6004 PONDERS COURT GROUNDWATER AND SURFACE WATER
ANDREX42—VOCSEPT15 GREENVILLE, SOUTH CAROLINA 29615 ANDREX INDUSTRIES Q
APPROVED: JOB NO: J15-1022-42 INC. PHONE: [phone] FAX: [phone] ASHEVILLE, NORTH CAROLINA V

2245 A A '
2245
ANDREX INDUSTRIES
2235 2235
IW-3A
2225 M W-2 IW-2 MW-6 2225
RW-3 RW-1
2215 2215
2205 2205 LEGEN D
RESIDENTIAL
2195 ECHOLS 2195
PROPERTY
AB
2185 IW-5 MW-20 2185
I MW-8R APPROXIMATE POTENTIOMETRIC SURFACE ON 9-14-2015
cf� M W-g SOUTHERN cf�
2175 \ \ RAILROAD 2175
GROUND SURFACE
~ 2165 2165 ~
17 1W-7 APPROXIMATE LOCATION OF BEDROCK ENCOUNTERED IN BORINGS RW-5
^ \ MW-10 ^
z 50 \ \, SILVERS z _
0 2155 2155
PROPERTY 0 > GROUNDWATER FLOW DIRECTION
Q2.7 MW-14 Q
2145 2145
LJJ M W-13 W 76
_ SCREENED OR OPEN BEDROCK INTERVAL WITH CONCENTRATION OF TOTAL CHLORINATED
w 2135 �� < 2135 w VOLATILE ORGANICS IN ug/I ON 9/14-17/2015
2,456
2125 1,748 2125
AB WELL WAS ABANDONED
E2,588
29
2115 2115
o VERTICAL EXAGGERATION = 1OX
NO o
2105 2105 a
SCALE 1I^ch
200 Feet
2095 2095 '
CA
2085 854 2085 INJECTION ZONE f
s
S =
2075 =7Z C 475
2075 ~5 �
�=
1,038
2065 2065 s',���►,rw'i ��``�,`,
2055 L 2055 NOTE:
INJECTION WELLS IW-4, IW-5, IW-7, AND IW-11 ARE PROPOSED FOR FUTURE INSTALLATION. ACTUAL CONSTRUCTION TO
BE DETERMINED IN THE FIELD.
0 100 200 300 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 1800
DISTANCE, FT. INJECTION WELL IW-3A IS PROPOSED FOR INSTALLATION IN 2016
GEOLOGIC PROFILE A - A '
MILKCO MW-12
MW-7
IW-11 ANDREX INDUSTRIES DEAVERVIEW ROAD
MW-24 FORMER BUILDING
2225 MW-5 2225
RW-3 1W-4 HAYNES
IW-1 CORPORATION 13 '
2215 2215
2205 2205
2195 2195
BEAR CREEK
RESIDENTIAL AREA 96 ROY D. FARMER
CITY PARK
2185 2185
2175 451 / / \ 2175 0
2165 2165
50
2155 CECIL'SRME COLLEGE
2.30 2155
(SMITH COLLEGE) i ® �
244 MW-23 n /
U� 2145 - /j / 2145 u� U 3
2135 2135
MW-15
® A
MW-16 -
2125 2125
SOUTHERN RAILROAD
O FORMER 0
2115 JEHOVAH 2115
Q WITNESS Q -
W203 CHURCH W
BIESTERFEDLT -
2105 �
W-18 / 2105
\� MW-17 PROPERTY LiJ _ -
��
SMITH MILL
2095 88
CREEK MW-21
TRIBUTARY ( IW-22 2095
89
2085 22 2085 -
2075 2075 - �
2065 NO 2065 =
B
2055 2055
NOcos
Q
2045 2045 -
NO
2035 2035
2025 2025
0 200 400 600 800 1000 1200 1400 1600 1800 2000 2200 2400 2600 2800 3000 3200 3400 3600 3800 PROFILE LOCATI ON PLAN
DISTANCE, FT.
GEOLOGIC PROFILE 13 - 13 '
REVISIONS DRAWN: DATE: 01-18-16 FIGURE NO.
No. DESCRIPTION BY ACE BUNNELL—LAMMONS ENGINEERING, INC. HYDROGEOLOGIC PROFILES OF THE AFFECTED AREA FOR THE 2015 IER
CHECKED: CAD FILE: ANDREX INDUSTRIES
AWA IER 1022-42 PROFILE ELONGATED 6004 GREENVIILLE, SOUTDHERCAROLINA 29615 DEAVERVIEW ROAD 4
APPROVED: JOB NO: J15-1022-42 INC. PHONE: [phone] FAX: [phone] ASHEVILLE, NORTH CAROLINA

APPENDICES

APPENDIX A
WELL LOGS

WELL CONSTRUCTION RECORD For Internal Use ONLY:
This form can be used for single or multiple wells
1.Well Contractor Information:
John Gorman 14.WATER ZONES
FROM TO DESCRIPTION
Well Contractor Name 50 ft' 50 ft. water-bearing fracture
3485-A ft. ft.
NC Well Contractor Certification Number 15.OUTER CASING for multi-cased wells OR LINER if a licable
FROM TO DIAMETER THICKNESS MATERL�L
Bunnell-Lammons Engineering, Inc. 0 H- 47 H- 6 in. 1 SCh40 I PVC
Company Name 16.INNER CASING OR TUBING eother at closed-loop)
U I C #W 10100106 FROM TO DIAMETER THICKNESS MATERIAL
2.Well Construction Permit#: ft. ft. in.
List all applicable well permits(i.e.Count).,State, Variance,Injection,etc.)
ft. ft. in.
3.Well Use(check well use): 17.SCREEN
Water Supply Well: FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft.❑Agricultural ❑Municipal/Public in.
❑Geothemlal eatin /Coolin Supply) ❑Residential Water Supply tt. et. in.
� g g PP Y) PP Y
❑Industrial/Commercial ❑Residential Water Supply(shared) 18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD&AMOUNT
❑hri ation 0 ft. ft
Non-Water Supply Well: 2.0 cement gravity--2 bags
❑Monitoring ❑Recovery 2 ft. 44.5 rt• bentonite gravity--25 bags
Injection Well: ft. ft.
❑Aquifer Recharge ©Groundwater Remediation 19.SAND/GRAVEL PACK if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
❑Aquifer storage and Recovery El Salinity Barrier 44.5 rt. 46.5 rf pea gravel gravity
❑Aquifer Test ❑Stormwater Drainage
❑Experimental Technology ❑Subsidence Control 46.5 ff 55 rf #3 stone gravity
20.DRILLING LOG attach additional sheets if necessary)
❑Geothermal(Closed LOOP) ❑Tracer FROM TO DESCRIPTION color,hardness,soillrock h e, rain size,etc.
❑Geothemlal(Heating/CoolingReturn) ❑Other(explain under#21 Remarks) 0 tt. 6 tt. red-brn mic f-m sandy SILT w/some clay
4.Date Well(s)Completed: Well ID#
3-16-15 IW-1 6 ft. 10 rt• red-brn mic silty f-m SAND (residuum)
10 rt• 16 rt• rock seam (PWR)
5a.Well Location:
16 rt• 32 rt. red-brn mic silty f-m SAND
Milkco, Inc. (Former Andrex) #07022-03-11
32 rt• 44 rt• brn mic silty f-m SAND w/rock fragments(PWR)
Facility/Owner Name Facility ID#(if applicable)
180 Deaverview Road, Asheville, NC 28806 44 rt• 55 bedrock
rt•
ft. ft.
Physical Address,City,and Zip
21.REMARKS
Buncombe 9667
County Parcel Identification No.(PIN)
5b.Latitude and Longitude in degrees/minutes/seconds or decimal degrees: 22.Certification:
(if well field,one lat/long is sufficient)
35.58010 N 82.61418 W ��- 3-18-15
Signature of Certified Well Contractor Date
6.Is(are)the well(s): ©Permanent or ❑Temporary By signing this form,I hereby certify that the well(s)was(were)constructed in accordance
with 15A NCAC 02C.0100 or 15A NCAC 02C.0200 Well Construction Standards and that a
7.Is this a repair to an existing well: ❑Yes or ONo copy of this record has been provided to the well owner.
If this is a repair,fill out known well construction information and explain the nature of the
repair under#21 remarks section or on the back of this form. 23.Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
8.Number of wells constructed: One construction details. You may also attach additional pages if necessary.
For multiple injection or non-water supply wells ONLY with the same construction,you can
submit one farm. SUBMITTAL INSTUCTIONS
9.Total well depth below land surface: 55 24a. For All Wells: Submit this form within 30 days of completion of well
For multiple wells list all depths ifdierent(example-3@200'and 2@100) construction to the following:
10.Static water level below top of casing: 47 (g,) Division of Water Resources,Information Processing Unit,
Ifwater level is above casing,use"+" 1617 Mail Service Center,Raleigh,NC 27699-1617
11.Borehole diameter: 10 (in.) 24b.For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well
12.Well construction method: air hammer construction to the following:
(i.e.auger,rotary,cable,direct push,etc.)
Division of Water Resources,Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center,Raleigh,NC 27699-1636
13a.Yield(gpm) Method of test: 24c.For Water Supply&Injection Wells:
Also submit one copy of this form within 30 days of completion of
13b.Disinfection type: Amount: well construction to the county health department of the county where
constructed.
Form GW-1 North Carolina Department of Environment and Natural Resources-Division of Water Resources Revised August 2013

„LIBINC. INJECTION WELL NO. IW-1
PROJECT: Former Andrex Industries PROJECT NO.: J15-1022-42
BUNNELL-LAMMONS CLIENT: Milkco START: 3-16-15 END: 3-16-15
ENGINEERING,INC. LOCATION: Asheville,North Carolina ELEVATION: 2216.43
GEOTECHNICAL AND EN VIRONMENTAL DRILLER: Landprobe,J.Gorman LOGGED BY: B.Nisbeth
CONSULTANTS DRILLING METHOD: Schramm T450WS;10-inch air hammer
DEPTH TO-WATER> INITIAL: 47 AFTER 24 HOURS:1 CAVING>777
w EZ
ELEVATION/ SOIL 0. Qp MONITOR WELL INSTALLATION
DEPTH(FT) DESCRIPTION TYPE 2 w DETAILS
y a�
3-inches of GRASS/TOPSOIL
2215 Reddish-brown, micaceous,fine to medium sandy Grout,0 to 2.0 feet
SILT with some clay
SURFACE COMPLETION
Flush-mount secured with an
8-inch diameter steel bolted
manhole cover in a X x X x 4”
5 concrete pad
0
2210 Reddish-brown, micaceous, silty, fine to medium Measuring point elev.=2,216.24
SAND feet
Ground surface elev.=2,216.43
feet
10 Latitude(North) 35.58010=
PARTIALLY WEATHERED ROCK which sampled as 0 Longitude(West)= .58010
2205 reddish-brown, micaceous, silty,fine to medium SAND
2.61418
15
0
2200 Reddish-brown, micaceous, silty,fine to medium
SAND
20 Bentonite seal,2.0 to 44.5 feet
0
2195
25
0
2190
6-inch diameter outer casing set to
47.0 feet
30
0
2185
PARTIALLY WEATHERED ROCK which sampled as
brown, micaceous, silty,fine to medium SAND
N
35
N 0
V
2180
0
z
0
w
3: INJECTION WELL NO. IW-1
z Sheet 1 of 2
w

„LMINC. INJECTION WELL NO. IW-1
PROJECT: Former Andrex Industries PROJECT NO.: J15-1022-42
BUNNELL-LAMMONS CLIENT: Milkco START: 3-16-15 END: 3-16-15
ENGINEERING,INC. LOCATION: Asheville,North Carolina ELEVATION: 2216.43
GEOTECHNICAL AND EN VIRONMENTAL DRILLER: Landprobe,J.Gorman LOGGED BY: B.Nisbeth
CONSULTANTS DRILLING METHOD: Schramm T450WS;10-inch air hammer
DEPTH TO-WATER> INITIAL: 47 AFTER 24 HOURS:1 CAVING>3m
w EZ
ELEVATION/ SOIL 0. Qp MONITOR WELL INSTALLATION
DEPTH(FT) DESCRIPTION TYPE 2 w DETAILS
(n a�
PARTIALLY WEATHERED ROCK which sampled as 0
2175 brown, micaceous, silty,fine to medium SAND Bentonite seal,2.0 to 44.5 feet
ROCK
45 0 Pea gravel,44.5 to 46.5 feet
2170
#3 Stone,46.5 to 55.0 feet
so Water bearing fracture at 50 feet 0
21s5
55
Boring terminated at 55.0 feet. Groundwater
21s0 encountered at 47.0 feet at time of drilling. Total well depth,55.0 feet
Borehole diameter,10-inches
s0
2155
s5
2150
70
2145
N
75
N
7
0 2140
0
a
J
Z
O
J
J
3 INJECTION WELL NO. IW-1
w Sheet 2 of 2

WELL CONSTRUCTION RECORD For Internal Use ONLY:
This form can be used for single or multiple wells
1.Well Contractor Information:
John Gorman 14.WATER ZONES
FROM TO DESCRIPTION
Well Contractor Name ft. ft.
3485-A ft. ft.
NC Well Contractor Certification Number 15.OUTER CASING for multi-cased wells OR LINER if a licable
FROM TO DIAMETER THICKNESS MATERL�L
Bunnell-Lammons Engineering, Inc. 0 r' 50 ft. 6 in- 1 SCh40 I PVC
Company Name 16.INNER CASING OR TUBING eother at closed-loop)
U I C #W 10100106 FROM TO DIAMETER THICKNESS MATERIAL
2.Well Construction Permit#: ft. ft. in.
List all applicable well permits(i.e.County,State, Variance,Injection,etc.)
ft. ft. in.
3.Well Use(check well use): 17.SCREEN
Water Supply Well: FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft.❑Agricultural ❑Municipal/Public in.
❑Geothenal eatin /Coolin Supply) ❑Residential Water Supply tt. et. in.
� g g PP Y) PP Y
❑Industrial/Commercial ❑Residential Water Supply(shared) 18.GROUT
FROM TO MATERIAL EMPLACEMENT METHOD&AMOUNT
❑Rri ation 0 ft. ft
Non-Water Supply Well: 3 cement gravity--3 bags
❑Monitoring ❑Recovery 3 rut. 15 ft• bentonite gravity--9 bags
Injection Well:
❑Aquifer Recharge ©Groundwater Remediation 19.SAND/GRAVEL PACK if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
❑Aquifer Storage and Recovery El Salinity Barrier 15 ft• 50 ft• pea gravel gravity
❑Aquifer Test ❑Stormwater Drainage
❑Experimental Technology ❑Subsidence Control 50 ft. �� ft. #3 stone gravity
20.DRILLING LOG attach additional sheets if necessary)
❑Geothermal(Closed Loop) ❑Tracer FROM TO DESCRIPTION color,hardness,soil/rock type, rain size,etc.
❑Geothenal(Heating/Cooling Return) ❑Other(explain under#21 Remarks) 0 ft' 10 ft red-brn mic f-m sandy SILT(fill)
4.Date Well(s)Completed: Well ID#
3-18-15 IW-3 10 ft- 25 ft• red-brn mic f-m sandy SILT(residuum)
25 ft- 38 ft• brn mic silty f-m SAND(PWR)
5a.Well Location: 38 ft 77 ft• brn mic silty f-m SAND(PWR)
Milkco, Inc. (Former Andrex) #07022-03-11
rut. 77 ft. bedrock
Facility/Owner Name Facility ID#(if applicable)
ft. ft.
180 Deaverview Road, Asheville, NC 28806
ft. ft.
Physical Address,City,and Zip
21.REMARKS
Buncombe 9667
County Parcel Identification No.(PIN)
5b.Latitude and Longitude in degrees/minutes/seconds or decimal degrees: 22.Certification:
(if well field,one lat/long is sufficient)
35.57991 N 82.61382 W az �� 3-18-15
Signature of Certified Well Contractor Date
6.Is(are)the well(s): ©Permanent or ❑Temporary By signing this form,I hereby certify that the well(s)was(were)constructed in accordance
with 15A NCAC 02C.0100 or 15A NCAC 02C.0200 Well Construction Standards and that a
7.Is this a repair to an existing well: ❑Yes or ONo copy of this record has been provided to the well owner.
If this is a repair,fill out known well construction information and explain the nature of the
repair under#21 remarks section or on the back of this form. 23.Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
8.Number of wells constructed: One construction details. You may also attach additional pages if necessary.
For multiple injection or non-water supply wells ONLY with the same construction,you can
submit one farm. SUBMITTAL INSTUCTIONS
9.Total well depth below land surface: 77 24a. For All Wells: Submit this form within 30 days of completion of well
For multiple wells list all depths ifdierent(example-3@200'and 2@100) construction to the following:
10.Static water level below top of casing: 52 (g,) Division of Water Resources,Information Processing Unit,
Ifwater level is above casing,use"+" 1617 Mail Service Center,Raleigh,NC 27699-1617
11.Borehole diameter: 10 (in.) 24b.For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well
12.Well construction method: a I r hammer construction to the following:
(i.e.auger,rotary,cable,direct push,etc.)
Division of Water Resources,Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center,Raleigh,NC 27699-1636
13a.Yield(gpm) Method of test: 24c.For Water Supply&Injection Wells:
Also submit one copy of this form within 30 days of completion of
13b.Disinfection type: Amount: well construction to the county health department of the county where
constructed.
Form GW-1 North Carolina Department of Environment and Natural Resources-Division of Water Resources Revised August 2013

„LEINC. INJECTION WELL NO. IW-3
PROJECT: Former Andrex Industries PROJECT NO.: J15-1022-42
BUNNELL-LAMMONS CLIENT: Milkco START: 3-17-15 END: 3-18-15
ENGINEERING,INC. LOCATION: Asheville,North Carolina ELEVATION: 2217.69
GEOTECHNICAL AND EN VIRONMENTAL DRILLER: Landprobe,J.Gorman LOGGED BY: B.Nisbeth
CONSULTANTS DRILLING METHOD: Schramm T450WS;10-inch air hammer
DEPTH TO-WATER> INITIAL: 50 AFTER 24 HOURS:1 CAVING>3m
w Eo
ELEVATION/ SOIL 0. Qp MONITOR WELL INSTALLATION
DEPTH(FT) DESCRIPTION TYPE 2 w DETAILS
(n a�
4-inches of GRASS/TOPSOIL
-------------
Reddish-brown, micaceous,fine to medium sandy
SILT-(fill) Grout,0 to 3.0 feet
2215
0 SURFACE COMPLETION
Flush-mount secured with an
8-inch diameter steel bolted
$ manhole cover in a X x X x 4”
concrete pad
Measuring point elev.=2,217.41
feet
2210
Ground surface elev.=2,217.69
feet
10 Latitude(North)=35.57991
Reddish-brown, micaceous,fine to medium sandy 0
SILT-(residuum) Longitude(West)=82.61382
2205
Bentonite seal,3.0 to 15.0 feet
15 0
2200
20 0 Pea gravel,15.0 to 50.0 feet
2195
25 PARTIALLY WEATHERED ROCK which sampled as 0 6-inch diameter outer casing set to
reddish-brown, micaceous, silty,fine to medium SAND 50.0feet
2190
30 0
2185
N
35 0
N
7
N
O
a 2180
PARTIALLY WEATHERED ROCK which sampled as
o brown, micaceous,fine to medium SAND
J
J
W
3 INJECTION WELL NO. IW-3
w Sheet 1 of 2

„LMINC. INJECTION WELL NO. IW-3
PROJECT: Former Andrex Industries PROJECT NO.: J15-1022-42
BUNNELL-LAMMONS CLIENT: Milkco START: 3-17-15 END: 3-18-15
ENGINEERING,INC. LOCATION: Asheville,North Carolina ELEVATION: 2217.69
GEOTECHNICAL AND EN VIRONMENTAL DRILLER: Landprobe,J.Gorman LOGGED BY: B.Nisbeth
CONSULTANTS DRILLING METHOD: Schramm T450WS;10-inch air hammer
DEPTH TO-WATER> INITIAL: 50 AFTER 24 HOURS:1 CAVING>3m
w Eo
ELEVATION/ SOIL 0. Qp MONITOR WELL INSTALLATION
DEPTH(FT) DESCRIPTION TYPE 2 w DETAILS
y a�
PARTIALLY WEATHERED ROCK which sampled as 0
brown, micaceous,fine to medium SAND
2175
Pea gravel,15.0 to 50.0 feet
45 0
2170
50 0
2165
55
2160
60 0 #3 Stone,50.0 to 77.0 feet
2155
65
2150
70 0
2145
N
75
N
7
N
N
O_
o Total well depth,77.0 feet
a 2140 Boring terminated at 77.0 feet at top of bedrock.
Z
Groundwater encountered at 50.0 feet at time of Borehole diameter,10-inches
01
drilling.
J
W
3 INJECTION WELL NO. IW-3
w Sheet 2 of 2

APPENDIX B
INJECTION EVENT RECORD&PLOT

INJECTION EVENT RECORD
North Carolina Department of Environment and Natural Resources — Division of Water Quality
Permit Number W T 0100t No
Were any wells abandoned during this injection
1 . Permit Information event?
M, lt � ❑ Yes ® No
Permittee If yes, please provide the following information :
�d ( m y Avi dve y :IA ALA � le., ( or . tau ( i Number of Monitoring Wells
Facility Name
Number of Injection Wells
I $ 0 ` )wvt�vit,,a Rol• � S�n �vi�, 1� (. Z$SO (o
Facility Address Please include two copies of the GW130 for each
well abandoned.
2 . Injection Contractor Information
4 . Injectant Information
�J uv��(. ' (,aw►w� on S �n eft n [.ryr i nab
Injection Contractor / Company Name ( b/s n* ) - ( ' %,
Injectant Type
Street Address 6OC4 ?04% r5 �jottir
Concentration �Ie
Catrc,+nyi4�- sc� 2R (� I �
City State Zip Code If the injectant is diluted please indicate the source
dilution fluid. Ir.�atcr
( (� �- ) 28 � - lZ � s
Area code — Phone number Total Volume Injected 131 , 49 (o gal [ oA5
3 . Well Information Volume Injected per well �W ' ( - Z (. 1 000 Jo, l(oow
rtW - 3 = 25 � 49c� gallons
Number of wells used for injection Z 5 . Injection History
Well names -T� W ' I S W ' 3 Injection dates) ' I S ,rw 4 . 14 • i 5
Were any new wells installed during this injection Injection number (e.g. 3 of 5) S
event?
?❑. Yes ❑ No Is this the last injection at this site?
❑ Yes ® No
If yes, please provide the following information :
Number of Monitoring Wells I DO HEREBY CERTIFY THAT ALL THE
INFORMATION ON THIS FORM IS CORRECT TO
Number of Injection Wells Z THE BEST OF MY KNOWLEDGE AND THAT THE
INJECTION WAS PERFORMED WITHIN THE
Type of Well Installed (Check applicable type) : STANDARDS LAID OUT IN THE PERMIT.
❑ Bored N Drilled ❑ Direct-Push
❑ Hand-Augured ❑ Other (specify) � +
� 154 is
S GN TfeAE OF INJECTION CONTRACTOR DATE
Please include two copies ofform GW-I b for each � 5 r ai5b
well installed. PRINT NAME OF PERSON PERFORMING THE INJECTION
Submit the original of this form to the Division of Water Quality within 30 days of injection. Form UIC-IER
Attn: UIC Program, 1636 Mail Service Center, Raleigh, NC 276994636, Phone No. 919-733 -3221 Rev. 07/09

IW-1 Injection Record for Event 2015
28,000
26,000
24,000 '
.
22,000
20,000
18,000
c ,
0
16,000 ,
t7 �
> 14,000 '
.-
M
E 12,000
Total Gallons Injected
10,000
8,000 Target Injection Rate
6,000 - . � arget Injection Volume
4,000 -
2,000 -
0
4/4/2015 4/6/2015 4/8/2015 4/10/2015 4/12/2015 4/14/2015 4/16/2015
Date

IW-3 Injection Record for Event 2015
28,000
26,000
24,000 '
.
.
22,000
20,000
18,000
c ,
0
16,000 ,
t7 �
> 14,000 '
E 12,000 '
Total Gallons Injected
10,000
8,000 00 Target Injection Rate
6,000 - � arget Injection Volume
4,000 -
2,000 -
0
4/4/2015 4/6/2015 4/8/2015 4/10/2015 4/12/2015 4/14/2015 4/16/2015
Date

APPENDIX C
LABORATORY ANALYTICAL DATA SHEETS
TOC ANALYSIS OF MILK SOLUTION
(Provided on Enclosed CD)

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Friday April 10, 2015
Report Number: L757783
Samples Received: 04/07/15
Client Project: J15-1022-42
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
Daphne Richards , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 2

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 10,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L757783-01
Date Received April 07, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IC-2015-A
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 04/06/15 10:00
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 8400000 100000 ug/l 9060A 04/09/15 100
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/10/15 16:45 Printed: 04/10/15 16:45
Page 2 of 2

9d ling lnformatlor: Anafysig/Contain er/Pregervative (Minafpustody PNe—of
Bunnell - Lammons Engineering, Inc, Project Manager
—7 -
6004 Ponders Court
G0 4 Panders Court Greenville SC 29615 _ T1 'OESC.
L'A C r-IR-N,C t-9
Report m: F•n3-1 ';a:andy@blecorp,tom 12M5 Leb.no-i Ad
Mr.Andy Alexander MUM Juliei.IN 37]22 L=t
mane:S3S-15e.5e56 .
Proj rt City/State I FNYn :BM.W.50v
1. 1 + : O
oeg[ription! Andfex Industries COlie[ted= Fw d1%JS&.59S4�r ttJJrl 7�i. 1 �!
Phone:864-2$$-1 2 65
Cilent Project# La4 Project N L IV 7 79
Fax. [phone] 114-102-2-40 EWNLAMLSSC-J14102240 S J005
Col"by Jrrint): Site/Facrlay m 4v P.o.i* ++
'V& AIAAAA- - 4 1 C 1 ASHEVIUIE, NC Atctn urn:BUN LAMGSC
Collected y(signatures: Date Results Needed -6 Temp.late:T101498
fCe�sb� I;Lab MUST 9e Natiified] �
�---- _$irnt Day .- ...............2 Prelogin; P505028
_Next Day,,,,,,,,, ,,,,, ,,,,,---1°pX Email? Na Yes
Immediately _Two Day .-.-.-.-_ ,,,,,,,,,,,,,,.,Sox — — TSR:ISO-Jimmy H u nt
O
Packed on ice N_ Y * _ThFee Day....................,,,_-.zsx FW___No —Yes
o
of +*J
ntrs Shipped Via;PedEX Ground
Sample JD Comp} rbh Matrix' bepth date Time 0
�C� oIJ ' A GUV �
/�`yy��7� Rim�{Gn[im 7ir1 iampla Y Ila},• .
Mitrlx; SS-Solt OW-Z roundwater wW-Wastewater l W-Orl nking water OT-other
J=rnarks.- pH TemA.—
Flow Other Mold p
AeNnquished by-�Si r Date; T1mf r�;[ Received by,.islp e} Sam returned pia= Q UPS Candltlon: Ilab use onI
►'� IV FedEx Courier ❑_
RkUDOlshed by:f5ignature} date= Time: Receivd by:{Sig 7a Bottles Received; dl
.;� Tefmp� °�
}xy, I
COC Seal Intact: _Y N NA
ReII+�Qui5J5ed by:{Sigu7ature) Date' Tlme; Re[xived rlab by `i ature� bate: Time; PH Checked: NCF:

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Monday April 27, 2015
Report Number: L758566
Samples Received: 04/10/15
Client Project: J14-1022-42
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
T. Alan Harvill , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 2

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 27,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L758566-01
Date Received April 10, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IC-2015-B
Project # J14-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 04/09/15 11:30
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 5900000 500000 ug/l 9060A 04/23/15 500
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/27/15 16:00 Printed: 04/27/15 16:01
Page 2 of 2

Pilling Infarmation, Aral V4i {Canta in er{Preservative Chain of Custody Pam of
Bunnell • Lammons Engineering, Inc. Project Manager
6004 Ponders Court '*ESC
6004 Ponders Court Greenville, 5C 29615
Greenville,5C 29615 I a-c P.s N.C
5
i
DA
L".365,.
Report to Emadio-indyoblerarp.corn MouraJuiiet.'rNX74Jr ❑
Mr.Andy Alexander ah�:aw-7ss-sass
Fh+fSl:9P5-757.51M
Project city/state I tax:a:s-758.5ss�
Description; Antlrex industries Collected; � t A #
7,55
Phone:[phone] Client PraJect 4 tab Projp[[A C!�
)14-10 r +' i/ OUNL-ALMGSC-JI4102240 l�
Fax! 864-M-4430 r K1 6
ro
Collected by sprint): Site{FaCIII#w 10 it P.O.11 a A€Ctnum.-BUNLAIV7C,?
ASHEVILLE, NC ,
! Template;TI01498
Cnllecte y{signature): Date Results Needled
HuSh� ILabrw4U5T9�eNutifiedJ �
Prelagin:P505026
Same Day::.:.:.:......:.:,.,:- .-Z009F
_nextovv:.:........:_..........:.:.ioo9c EmaMl� No _Yes­4 � TSR;350 JfmmYHunt
lb49
ediatelY _7wo0w ...........................::50r� No. � �
rn P6; J
Packed on Ice N Y Mree day.........................._.25x FAX?_No _Yes of N
V Shipped Via:FedEX Ground
Coro ID Sample Grab Matrix• Depth Date Tlme rtit s 0
P { i-- Rrm.fcontam,nant $e1r.uh-n1-hrA1y1
hAatOK: SS-Soil GW•Gmundwater WW-WasteWater Ow-Drinking Water 07-Other _
pH Temp
emarkw
Flow Other Hold A
Relinquished by:JSignature) Date: lime; Received by:•1Sigrr ure} sarnplesreurnedria; MUP5 Condition! (lab use
} 8 x O Courier Q . _--
Rrbture) Date: Time- Received by:{Sign Temp-�7 ec $ottles Received'7 I 1 V-
COC Seal Intact; Y _N _NA
e rrgl+eS e F
7
0

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Tuesday April 21, 2015
Report Number: L759359
Samples Received: 04/15/15
Client Project: J14-1022-42
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By: I
Jimmy Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 2

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 21,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L759359-01
Date Received April 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IC-2015-C
Project # J14-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 04/14/15 11:30
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 6800000 500000 ug/l 9060A 04/17/15 500
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/21/15 07:43 Printed: 04/21/15 07:43
Page 2 of 2

�Piling ntorm===tior. Anal!V05}Contarer}PreserybtIve ChslnofCu%Lody Page_of_
Bunnell - Lammolns Engineering, Inc. Project Manager
6Db4 Ponders Cc rt
5004 Ponders Court Grenville, SC 29615 OESC
(3reenville,SC 29615 L. a'@ 5'C'I'E'NJ E-S
I
i
f Q ork t0; F'na I-o andy@blerarP"earn •nfig-W e4 ❑� ❑
p Mouni Julie'.,TN I'M
Mr,Andy Alexander Pnaj�:615-75e-ses2
Ph&n :aaa767.5es9 l °'
Projett 0tymate FaR:fits- Eds59
. � •
pe5rriptibn; And rex InduStrieS Collected: J
Client Project M Lab Prvjer#I # {j fj
Phone.8G4 288 12b5 J14-1022 L SUNLAMGSC-J14102240 H147
Fax_ 964-288-4430
Collected tq(print): Site/Facdily I D it P.O.# ++ I
y [� ASHEVILLE NC i ACC t^Iun,:BUNLAI1f1GSC
� Temp`dte;T101498
Collects by Isignature)! 1Rush? ILab MUST Be No#ified) date Results Needed Prelog,r: P505027
.F d
Same Day,,.,.,,,,.,....,,,-,-,-..-.�CIa76 T5ft:3$-0-Jimm Ffunt
Email! No X Yee Y
ImrnediateIW _two pay ................... .......SD96 ? PB:
Packed on Ica hl Y Three Day..... "......".".....15% FAQ"—No _Ye9
Shipped Via:Fed EX Ground
Sample10 CornplGrab Matrix' Depth Date Time nrrs
V
Ri—'Cantam jar-. Sample M Oib anM
I _ _
Matrix: ss•Sail GNP-Groundwater WW-Wastewater oW-Drinkinq Water OT-Other_
Remarks: 11H Tem v p
Flour Other Holdn
Relinquished bVJSlgnat Fate: 71me: Received by'I5ig nature I Samples returned 4ia. ❑UPS Condition! (lab w9 onlyl
®FedEx O Courler ❑
Re qui9he by: Date: Time. Received by:ISignd#4r2} Tempo °C Bottles Received:
COC S-r-al Intart: _Y _N NA �
Relinquished by.rmqw
Bate: Time Rec d#nr IS�na[ } tune- pH Checked! NCF;
q(df

APPENDIX D
LABORATORY ANALYTICAL DATA SHEETS
GROUNDWATER&SURFACE WATER
MARCH 2O15 [Pre-Injection Baseline]
(Provided on Enclosed CD)

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Wednesday April 08, 2015
Report Number: L756288
Samples Received: 03/28/15
Client Project: J15-1022-42
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By: I
Jimmy Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-01
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-5
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 09:40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 1200 1000 ug/l 9060A 03/31/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 04/05/15 1
Acrolein BDL 50. ug/1 8260B 04/05/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/05/15 1
Benzene BDL 1.0 ug/1 8260B 04/05/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/05/15 1
Bromoform BDL 1.0 ug/l 8260B 04/05/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/05/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 04/05/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/05/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/05/15 1
2-Chloroethyl vinyl ether BDL 1200 ug/1 8260B 04/08/15 25
Chloroform BDL 5.0 ug/1 8260B 04/05/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/05/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/05/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/05/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/05/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/05/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/05/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/05/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 04/05/15 1
cis-1,2-Dichloroethene 520 25. ug/l 8260B 04/08/15 25
trans-1,2-Dichloroethene 13. 1.0 ug/l 8260B 04/05/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/05/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/05/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/05/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/05/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/05/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 2 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-01
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-5
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 09:40
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/05/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 04/05/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/05/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/05/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/05/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/05/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Styrene BDL 1.0 ug/1 8260B 04/05/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/05/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/05/15 1
Tetrachloroethene 1800 25. ug/1 8260B 04/08/15 25
Toluene BDL 5.0 ug/1 8260B 04/05/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/05/15 1
Trichloroethene 120 1.0 ug/1 8260B 04/05/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/05/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/05/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Vinyl chloride 300 25. ug/1 8260B 04/08/15 25
Xylenes, Total BDL 3.0 ug/l 8260B 04/05/15 1
Surrogate Recovery
Toluene-d8 107. % Rec. 8260B 04/05/15 1
Dibromofluoromethane 105. % Rec. 8260B 04/05/15 1
4-Bromofluorobenzene 98.7 % Rec. 8260B 04/05/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:01
Page 3 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-02
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-6
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 11:15
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 2200 1000 ug/l 9060A 03/31/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 04/05/15 1
Acrolein BDL 50. ug/1 8260B 04/05/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/05/15 1
Benzene BDL 1.0 ug/1 8260B 04/05/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/05/15 1
Bromoform BDL 1.0 ug/l 8260B 04/05/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/05/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Carbon tetrachloride BDL 1.0 ug/1 8260B 04/05/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/05/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/05/15 1
2-Chloroethyl vinyl ether BDL 2500 ug/1 8260B 04/08/15 50
Chloroform BDL 5.0 ug/1 8260B 04/05/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/05/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/05/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/05/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/05/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/05/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/05/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/05/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1-Dichloroethene 1.2 1.0 ug/1 8260B 04/05/15 1
cis-1,2-Dichloroethene 900 50. ug/l 8260B 04/08/15 50
trans-1,2-Dichloroethene 3.2 1.0 ug/1 8260B 04/05/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
1,1-Dichloropropene BDL 1.0 ug/1 8260B 04/05/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/05/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/05/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/05/15 1
Ethylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/05/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 4 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-02
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-6
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 11:15
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/05/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 04/05/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/05/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/05/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/05/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/05/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Styrene BDL 1.0 ug/1 8260B 04/05/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/05/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/05/15 1
Tetrachloroethene 1900 50. ug/1 8260B 04/08/15 50
Toluene BDL 5.0 ug/1 8260B 04/05/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/05/15 1
Trichloroethene 82. 1.0 ug/1 8260B 04/05/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/05/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/05/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Vinyl chloride 13. 1.0 ug/1 8260B 04/05/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 04/05/15 1
Surrogate Recovery
Toluene-d8 107. % Rec. 8260B 04/05/15 1
Dibromofluoromethane 106. % Rec. 8260B 04/05/15 1
4-Bromofluorobenzene 96.2 % Rec. 8260B 04/05/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:01
Page 5 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-03
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-12
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 11:00
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 5800 1000 ug/l 9060A 03/31/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 04/05/15 1
Acrolein BDL 50. ug/1 8260B 04/05/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/05/15 1
Benzene BDL 1.0 ug/1 8260B 04/05/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/05/15 1
Bromoform BDL 1.0 ug/l 8260B 04/05/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/05/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Carbon tetrachloride BDL 1.0 ug/1 8260B 04/05/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/05/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/05/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 04/08/15 1
Chloroform BDL 5.0 ug/1 8260B 04/05/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/05/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/05/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/05/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/05/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/05/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/05/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/05/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 04/05/15 1
cis-1,2-Dichloroethene 1.1 1.0 ug/l 8260B 04/08/15 1
trans-1,2-Dichloroethene 6.4 1.0 ug/1 8260B 04/05/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
1,1-Dichloropropene BDL 1.0 ug/1 8260B 04/05/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/05/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/05/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/05/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/05/15 1
Ethylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/05/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 6 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-03
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-12
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 11:00
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/05/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 04/05/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/05/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/05/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/05/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/05/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Styrene BDL 1.0 ug/1 8260B 04/05/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/05/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/05/15 1
Tetrachloroethene BDL 1.0 ug/1 8260B 04/08/15 1
Toluene 8.6 5.0 ug/1 8260B 04/05/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/05/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/05/15 1
Trichloroethene BDL 1.0 ug/1 8260B 04/05/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/05/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/05/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/05/15 1
Vinyl chloride BDL 1.0 ug/1 8260B 04/05/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 04/05/15 1
Surrogate Recovery
Toluene-d8 109. % Rec. 8260B 04/05/15 1
Dibromofluoromethane 109. % Rec. 8260B 04/05/15 1
4-Bromofluorobenzene 103. % Rec. 8260B 04/05/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:01
Page 7 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-04
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-44
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 12:40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 2200 1000 ug/l 9060A 03/31/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 04/03/15 1
Acrolein BDL 50. ug/1 8260B 04/03/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/03/15 1
Benzene BDL 1.0 ug/1 8260B 04/03/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/03/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/03/15 1
Bromoform BDL 1.0 ug/l 8260B 04/03/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/03/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/03/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/03/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/03/15 1
Carbon tetrachloride BDL 1.0 ug/1 8260B 04/03/15 1
Chlorobenzene 1.6 1.0 ug/1 8260B 04/03/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/03/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/03/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 04/03/15 1
Chloroform BDL 5.0 ug/1 8260B 04/03/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/03/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/03/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/03/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/03/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/03/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/03/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/03/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/03/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/03/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/03/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/03/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/03/15 1
1,1-Dichloroethene 1.0 1.0 ug/1 8260B 04/03/15 1
cis-1,2-Dichloroethene 1300 50. ug/l 8260B 04/06/15 50
trans-1,2-Dichloroethene 6.8 1.0 ug/1 8260B 04/03/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/03/15 1
1,1-Dichloropropene BDL 1.0 ug/1 8260B 04/03/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/03/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/03/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/03/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/03/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/03/15 1
Ethylbenzene BDL 1.0 ug/1 8260B 04/03/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/03/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 8 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-04
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-44
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 12:40
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/03/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/03/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 04/03/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/03/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/03/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/03/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/03/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/03/15 1
Styrene BDL 1.0 ug/1 8260B 04/03/15 1
1,1,1,2-Tetrachloroethane 1.6 1.0 ug/l 8260B 04/03/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/03/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/03/15 1
Tetrachloroethene 6100 50. ug/1 8260B 04/06/15 50
Toluene BDL 5.0 ug/1 8260B 04/03/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/03/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/03/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/03/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/03/15 1
Trichloroethene 350 50. ug/1 8260B 04/06/15 50
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/03/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/03/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/03/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/03/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/03/15 1
Vinyl chloride 49. 1.0 ug/1 8260B 04/03/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 04/03/15 1
Surrogate Recovery
Toluene-d8 95.5 % Rec. 8260B 04/03/15 1
Dibromofluoromethane 94.6 % Rec. 8260B 04/03/15 1
4-Bromofluorobenzene 94.1 % Rec. 8260B 04/03/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:01
Page 9 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-05
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 11:35
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 71000 10000 ug/l 9060A 04/03/15 10
Volatile Organics
Acetone 490 50. ug/l 8260B 04/06/15 1
Acrolein BDL 50. ug/1 8260B 04/06/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/06/15 1
Benzene BDL 1.0 ug/1 8260B 04/06/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/06/15 1
Bromoform BDL 1.0 ug/l 8260B 04/06/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/06/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Carbon tetrachloride BDL 1.0 ug/1 8260B 04/06/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/06/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/06/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 04/06/15 1
Chloroform BDL 5.0 ug/1 8260B 04/06/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/06/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/06/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/06/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/06/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/06/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/06/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/06/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/06/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 04/06/15 1
cis-1,2-Dichloroethene 1500 50. ug/l 8260B 04/08/15 50
trans-1,2-Dichloroethene 16. 1.0 ug/1 8260B 04/06/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
1,1-Dichloropropene BDL 1.0 ug/1 8260B 04/06/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/06/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/06/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/06/15 1
Ethylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/06/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 10 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-05
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 11:35
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/06/15 1
2-Butanone (MEK) 110 10. ug/l 8260B 04/06/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/06/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/06/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/06/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/06/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Styrene BDL 1.0 ug/1 8260B 04/06/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/06/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/06/15 1
Tetrachloroethene BDL 1.0 ug/1 8260B 04/06/15 1
Toluene 420 250 ug/1 8260B 04/08/15 50
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/06/15 1
Trichloroethene 1.1 1.0 ug/1 8260B 04/06/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/06/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/06/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Vinyl chloride 230 50. ug/1 8260B 04/08/15 50
Xylenes, Total BDL 3.0 ug/l 8260B 04/06/15 1
Surrogate Recovery
Toluene-d8 105. % Rec. 8260B 04/06/15 1
Dibromofluoromethane 102. % Rec. 8260B 04/06/15 1
4-Bromofluorobenzene 99.3 % Rec. 8260B 04/06/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:02
Page 11 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-06
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-3
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 09:55
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 6000 1000 ug/l 9060A 03/31/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 04/06/15 1
Acrolein BDL 50. ug/1 8260B 04/06/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/06/15 1
Benzene BDL 1.0 ug/1 8260B 04/06/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/06/15 1
Bromoform BDL 1.0 ug/l 8260B 04/06/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/06/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 04/06/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/06/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/06/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 04/06/15 1
Chloroform BDL 5.0 ug/1 8260B 04/06/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/06/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/06/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/06/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/06/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/06/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/06/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/06/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/06/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 04/06/15 1
cis-1,2-Dichloroethene 820 25. ug/l 8260B 04/08/15 25
trans-1,2-Dichloroethene 23. 1.0 ug/l 8260B 04/06/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/06/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/06/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/06/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/06/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/06/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 12 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-06
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-3
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 09:55
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/06/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 04/06/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/06/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/06/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/06/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/06/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Styrene BDL 1.0 ug/1 8260B 04/06/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/06/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/06/15 1
Tetrachloroethene BDL 1.0 ug/1 8260B 04/06/15 1
Toluene 180 5.0 ug/1 8260B 04/06/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/06/15 1
Trichloroethene BDL 1.0 ug/1 8260B 04/06/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/06/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/06/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Vinyl chloride 180 1.0 ug/1 8260B 04/06/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 04/06/15 1
Surrogate Recovery
Toluene-d8 103. % Rec. 8260B 04/06/15 1
Dibromofluoromethane 103. % Rec. 8260B 04/06/15 1
4-Bromofluorobenzene 99.1 % Rec. 8260B 04/06/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:02
Page 13 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-07
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IW-2
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 11:45
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 1400000 100000 ug/l 9060A 03/31/15 100
Volatile Organics
Acetone 120 50. ug/l 8260B 04/06/15 1
Acrolein BDL 50. ug/1 8260B 04/06/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/06/15 1
Benzene BDL 1.0 ug/1 8260B 04/06/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/06/15 1
Bromoform BDL 1.0 ug/l 8260B 04/06/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/06/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Carbon tetrachloride BDL 1.0 ug/1 8260B 04/06/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/06/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/06/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 04/06/15 1
Chloroform BDL 5.0 ug/1 8260B 04/06/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/06/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/06/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/06/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/06/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/06/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/06/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/06/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/06/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 04/06/15 1
cis-1,2-Dichloroethene 270 20. ug/l 8260B 04/08/15 20
trans-1,2-Dichloroethene 1.5 1.0 ug/1 8260B 04/06/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
1,1-Dichloropropene BDL 1.0 ug/1 8260B 04/06/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/06/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/06/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/06/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/06/15 1
Ethylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/06/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 14 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-07
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IW-2
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 11:45
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/06/15 1
2-Butanone (MEK) 46. 10. ug/l 8260B 04/06/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/06/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/06/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/06/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/06/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Styrene BDL 1.0 ug/1 8260B 04/06/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/06/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/06/15 1
Tetrachloroethene 16. 1.0 ug/1 8260B 04/06/15 1
Toluene 630 100 ug/1 8260B 04/08/15 20
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/06/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/06/15 1
Trichloroethene 6.2 1.0 ug/1 8260B 04/06/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/06/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/06/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/06/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/06/15 1
Vinyl chloride 4.0 1.0 ug/1 8260B 04/06/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 04/06/15 1
Surrogate Recovery
Toluene-d8 104. % Rec. 8260B 04/06/15 1
Dibromofluoromethane 102. % Rec. 8260B 04/06/15 1
4-Bromofluorobenzene 97.6 % Rec. 8260B 04/06/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:02
Page 15 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-08
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID BC-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 13:45
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) BDL 1000 ug/l 9060A 03/31/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 04/08/15 1
Acrolein BDL 50. ug/1 8260B 04/08/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/08/15 1
Benzene BDL 1.0 ug/1 8260B 04/08/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/08/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/08/15 1
Bromoform BDL 1.0 ug/l 8260B 04/08/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/08/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/08/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
Carbon tetrachloride BDL 1.0 ug/1 8260B 04/08/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 04/08/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/08/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/08/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 04/08/15 1
Chloroform BDL 5.0 ug/1 8260B 04/08/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/08/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/08/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/08/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/08/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/08/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/08/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/08/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/08/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/08/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/08/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/08/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/08/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 04/08/15 1
cis-1,2-Dichloroethene 5.3 1.0 ug/l 8260B 04/08/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/1 8260B 04/08/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/08/15 1
1,1-Dichloropropene BDL 1.0 ug/1 8260B 04/08/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/08/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/08/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/08/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/08/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/08/15 1
Ethylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/08/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 16 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-08
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID BC-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 13:45
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/08/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/08/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 04/08/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/08/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/08/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/08/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/08/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
Styrene BDL 1.0 ug/1 8260B 04/08/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/08/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/08/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/08/15 1
Tetrachloroethene 19. 1.0 ug/1 8260B 04/08/15 1
Toluene BDL 5.0 ug/1 8260B 04/08/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/08/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/08/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/08/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/08/15 1
Trichloroethene 1.7 1.0 ug/1 8260B 04/08/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/08/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/08/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/08/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
Vinyl chloride BDL 1.0 ug/1 8260B 04/08/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 04/08/15 1
Surrogate Recovery
Toluene-d8 110. % Rec. 8260B 04/08/15 1
Dibromofluoromethane 109. % Rec. 8260B 04/08/15 1
4-Bromofluorobenzene 101. % Rec. 8260B 04/08/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:02
Page 17 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-09
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID JW-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 14:15
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) BDL 1000 ug/l 9060A 03/31/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 04/08/15 1
Acrolein BDL 50. ug/1 8260B 04/08/15 1
Acrylonitrile BDL 10. ug/l 8260B 04/08/15 1
Benzene BDL 1.0 ug/1 8260B 04/08/15 1
Bromobenzene BDL 1.0 ug/1 8260B 04/08/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 04/08/15 1
Bromoform BDL 1.0 ug/l 8260B 04/08/15 1
Bromomethane BDL 5.0 ug/1 8260B 04/08/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 04/08/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
Carbon tetrachloride BDL 1.0 ug/1 8260B 04/08/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 04/08/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 04/08/15 1
Chloroethane BDL 5.0 ug/1 8260B 04/08/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 04/08/15 1
Chloroform BDL 5.0 ug/1 8260B 04/08/15 1
Chloromethane BDL 2.5 ug/l 8260B 04/08/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 04/08/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 04/08/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 04/08/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 04/08/15 1
Dibromomethane BDL 1.0 ug/l 8260B 04/08/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 04/08/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/08/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 04/08/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 04/08/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 04/08/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/08/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 04/08/15 1
cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/08/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/1 8260B 04/08/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 04/08/15 1
1,1-Dichloropropene BDL 1.0 ug/1 8260B 04/08/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 04/08/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/08/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 04/08/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 04/08/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 04/08/15 1
Ethylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 04/08/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 18 of 21

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander April 08,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L756288-09
Date Received March 28, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID JW-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 03/27/15 14:15
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 04/08/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 04/08/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 04/08/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 04/08/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 04/08/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/08/15 1
Naphthalene BDL 5.0 ug/1 8260B 04/08/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
Styrene BDL 1.0 ug/1 8260B 04/08/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/08/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 04/08/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/08/15 1
Tetrachloroethene 2.7 1.0 ug/1 8260B 04/08/15 1
Toluene BDL 5.0 ug/1 8260B 04/08/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/08/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 04/08/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/08/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 04/08/15 1
Trichloroethene BDL 1.0 ug/1 8260B 04/08/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 04/08/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/08/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/08/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 04/08/15 1
Vinyl chloride BDL 1.0 ug/1 8260B 04/08/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 04/08/15 1
Surrogate Recovery
Toluene-d8 109. % Rec. 8260B 04/08/15 1
Dibromofluoromethane 108. % Rec. 8260B 04/08/15 1
4-Bromofluorobenzene 102. % Rec. 8260B 04/08/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/08/15 14:01 Printed: 04/08/15 14:02
Page 19 of 21

Attachment A
List of Analytes with QC Qualifiers
Sample Work Sample Run
Number Group Type Analyte ID Qualifier
L756288-01 WG779515 SAMP n-Butylbenzene R3029010 J4
WG780646 SAMP 2-Chloroethyl vinyl ether R3029509 J4
WG779515 SAMP 2,2-Dichloropropane R3029010 J4
WG779515 SAMP 1,2,3-Trimethylbenzene R3029010 J4
L756288-02 WG779515 SAMP n-Butylbenzene R3029010 J4
WG780646 SAMP 2-Chloroethyl vinyl ether R3029509 J4
WG779515 SAMP 2,2-Dichloropropane R3029010 J4
WG779515 SAMP 1,2,3-Trimethylbenzene R3029010 J4
L756288-03 WG779515 SAMP n-Butylbenzene R3029010 J4
WG780646 SAMP 2-Chloroethyl vinyl ether R3029509 J4
WG779515 SAMP 2,2-Dichloropropane R3029010 J4
WG779515 SAMP 1,2,3-Trimethylbenzene R3029010 J4
L756288-04 WG779514 SAMP 2-Chloroethyl vinyl ether R3028770 J6
WG779514 SAMP Vinyl chloride R3028770 J6
L756288-08 WG780646 SAMP n-Butylbenzene R3029509 J4
WG780646 SAMP 2-Chloroethyl vinyl ether R3029509 J4
WG780646 SAMP 2,2-Dichloropropane R3029509 J4
L756288-09 WG780646 SAMP n-Butylbenzene R3029509 J4
WG780646 SAMP 2-Chloroethyl vinyl ether R3029509 J4
WG780646 SAMP 2,2-Dichloropropane R3029509 J4
Page 20 of 21

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J4 The associated batch QC was outside the established quality control range
for accuracy.
J6 The sample matrix interfered with the ability to make any accurate
determination; spike value is low
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected) ."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 21 of 21

Bil ling lnformatlon: ArnalySis Container Preservativu Chain aiCuitudy Page—a
Bunnell - Lammons Engineering, Inc, Project Manager
6004 Ponders Court *ESC
6004 Ponders Court Greenville, 5C 29615
L.,a-L3 s-c-,-E-rw-C E S
Greenville,SC 29615
_ ]3[65 Lebanon Rd
Report to: EmaiI TO;andy0blecorp-[om Mount Ju&LI,TN37622
Mr.Andy Alexander Phanr:�a6(067-5659
Prpjert Citylstate II /w, Far615.M-51M
pe9cription; Andrei indu Collected= '"
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APPENDIX E
LABORATORY ANALYTICAL DATA SHEETS
GROUNDWATER
MAY 2015 [30 Day]
(Provided on Enclosed CD)

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Thursday May 28, 2015
Report Number: L765479
Samples Received: 05/15/15
Client Project: J15-1022-42
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
Leslie Newton , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-01
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-5
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 10:20
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 2800000 50000 ug/l 9060A O5/21/15 50
Volatile Organics
Acetone 190 50. ug/l 8260B 05/22/15 1
Acrolein BDL 50. ug/1 8260B O5/22/15 1
Acrylonitrile BDL 10. ug/l 8260B O5/22/15 1
Benzene BDL 1.0 ug/1 8260B 05/22/15 1
Bromobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 05/22/15 1
Bromoform BDL 1.0 ug/l 8260B O5/22/15 1
Bromomethane BDL 5.0 ug/1 8260B 05/22/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 05/22/15 1
Chlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B O5/22/15 1
Chloroethane BDL 5.0 ug/1 8260B 05/22/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B O5/22/15 1
Chloroform BDL 5.0 ug/1 8260B 05/22/15 1
Chloromethane BDL 2.5 ug/l 8260B O5/22/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 05/22/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B O5/22/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 05/22/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B O5/22/15 1
Dibromomethane BDL 1.0 ug/l 8260B 05/22/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 05/22/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B O5/22/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,2-Dichloroethene 380 10. ug/l 8260B O5/26/15 10
trans-1,2-Dichloroethene 4.0 1.0 ug/l 8260B 05/22/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 05/22/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B O5/22/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 05/22/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 05/22/15 1
Ethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 05/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 2 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-01
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-5
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 10:20
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 05/22/15 1
2-Butanone (MEK) 220 10. ug/l 8260B 05/22/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 05/22/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B O5/22/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B O5/22/15 1
Naphthalene BDL 5.0 ug/1 8260B 05/22/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Styrene BDL 1.0 ug/1 8260B 05/22/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B O5/22/15 1
Tetrachloroethene 14. 1.0 ug/1 8260B 05/22/15 1
Toluene BDL 5.0 ug/1 8260B O5/22/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 05/22/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
Trichloroethene 9.6 1.0 ug/1 8260B O5/22/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 05/22/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B O5/22/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
Vinyl chloride 62. 1.0 ug/1 8260B O5/22/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 05/22/15 1
Surrogate Recovery
Toluene-d8 103. % Rec. 8260B O5/22/15 1
Dibromofluoromethane 102. % Rec. 8260B 05/22/15 1
4-Bromofluorobenzene 100. % Rec. 8260B O5/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 05/28/15 09:22 Printed: 05/28/15 09:22
Page 3 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-02
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-6
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 11:15
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) BDL 1000 ug/l 9060A O5/20/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 05/22/15 1
Acrolein BDL 50. ug/1 8260B O5/22/15 1
Acrylonitrile BDL 10. ug/l 8260B O5/22/15 1
Benzene BDL 1.0 ug/1 8260B 05/22/15 1
Bromobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 05/22/15 1
Bromoform BDL 1.0 ug/l 8260B O5/22/15 1
Bromomethane BDL 5.0 ug/1 8260B 05/22/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 05/22/15 1
Chlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B O5/22/15 1
Chloroethane BDL 5.0 ug/1 8260B 05/22/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B O5/22/15 1
Chloroform BDL 5.0 ug/1 8260B 05/22/15 1
Chloromethane BDL 2.5 ug/l 8260B O5/22/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 05/22/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B O5/22/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 05/22/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B O5/22/15 1
Dibromomethane BDL 1.0 ug/l 8260B 05/22/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 05/22/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B O5/22/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,2-Dichloroethene 790 50. ug/l 8260B O5/26/15 50
trans-1,2-Dichloroethene 2.9 1.0 ug/l 8260B 05/22/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 05/22/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B O5/22/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 05/22/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 05/22/15 1
Ethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 05/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 4 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-02
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-6
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 11:15
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 05/22/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 05/22/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 05/22/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B O5/22/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B O5/22/15 1
Naphthalene BDL 5.0 ug/1 8260B 05/22/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Styrene BDL 1.0 ug/1 8260B 05/22/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B O5/22/15 1
Tetrachloroethene 1800 50. ug/1 8260B 05/26/15 50
Toluene BDL 5.0 ug/1 8260B O5/22/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 05/22/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
Trichloroethene 70. 1.0 ug/1 8260B O5/22/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 05/22/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B O5/22/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
Vinyl chloride 18. 1.0 ug/1 8260B O5/22/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 05/22/15 1
Surrogate Recovery
Toluene-d8 103. % Rec. 8260B O5/22/15 1
Dibromofluoromethane 97.6 % Rec. 8260B 05/22/15 1
4-Bromofluorobenzene 105. % Rec. 8260B O5/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 05/28/15 09:22 Printed: 05/28/15 09:22
Page 5 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-03
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-12
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 09:45
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 780000 20000 ug/l 9060A O5/21/15 20
Volatile Organics
Acetone 90. 50. ug/l 8260B 05/22/15 1
Acrolein BDL 50. ug/1 8260B O5/22/15 1
Acrylonitrile BDL 10. ug/l 8260B O5/22/15 1
Benzene BDL 1.0 ug/1 8260B 05/22/15 1
Bromobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 05/22/15 1
Bromoform BDL 1.0 ug/l 8260B O5/22/15 1
Bromomethane BDL 5.0 ug/1 8260B 05/22/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 05/22/15 1
Chlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B O5/22/15 1
Chloroethane BDL 5.0 ug/1 8260B 05/22/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B O5/22/15 1
Chloroform BDL 5.0 ug/1 8260B 05/22/15 1
Chloromethane BDL 2.5 ug/l 8260B O5/22/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 05/22/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B O5/22/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 05/22/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B O5/22/15 1
Dibromomethane BDL 1.0 ug/l 8260B 05/22/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 05/22/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B O5/22/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,2-Dichloroethene 27. 1.0 ug/l 8260B O5/22/15 1
trans-1,2-Dichloroethene 3.2 1.0 ug/l 8260B 05/22/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 05/22/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B O5/22/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 05/22/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 05/22/15 1
Ethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 05/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 6 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-03
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-12
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 09:45
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 05/22/15 1
2-Butanone (MEK) 87. 10. ug/l 8260B 05/22/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 05/22/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B O5/22/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B O5/22/15 1
Naphthalene BDL 5.0 ug/1 8260B 05/22/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Styrene BDL 1.0 ug/1 8260B 05/22/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B O5/22/15 1
Tetrachloroethene BDL 1.0 ug/1 8260B 05/22/15 1
Toluene 2700 250 ug/1 8260B O5/26/15 50
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 05/22/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
Trichloroethene BDL 1.0 ug/1 8260B O5/22/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 05/22/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B O5/22/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
Vinyl chloride 7.4 1.0 ug/1 8260B O5/22/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 05/22/15 1
Surrogate Recovery
Toluene-d8 110. % Rec. 8260B O5/22/15 1
Dibromofluoromethane 95.8 % Rec. 8260B 05/22/15 1
4-Bromofluorobenzene 107. % Rec. 8260B O5/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 05/28/15 09:22 Printed: 05/28/15 09:22
Page 7 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-04
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-44
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 14:30
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 1800 1000 ug/l 9060A O5/20/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 05/22/15 1
Acrolein BDL 50. ug/1 8260B O5/22/15 1
Acrylonitrile BDL 10. ug/l 8260B O5/22/15 1
Benzene BDL 1.0 ug/1 8260B 05/22/15 1
Bromobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 05/22/15 1
Bromoform BDL 1.0 ug/l 8260B O5/22/15 1
Bromomethane BDL 5.0 ug/1 8260B 05/22/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 05/22/15 1
Chlorobenzene 2.0 1.0 ug/1 8260B O5/22/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B O5/22/15 1
Chloroethane BDL 5.0 ug/1 8260B 05/22/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B O5/22/15 1
Chloroform BDL 5.0 ug/1 8260B 05/22/15 1
Chloromethane BDL 2.5 ug/l 8260B O5/22/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 05/22/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B O5/22/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 05/22/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B O5/22/15 1
Dibromomethane BDL 1.0 ug/l 8260B 05/22/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 05/22/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B O5/22/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1-Dichloroethene 1.4 1.0 ug/1 8260B 05/22/15 1
cis-1,2-Dichloroethene 1400 50. ug/l 8260B O5/26/15 50
trans-1,2-Dichloroethene 8.4 1.0 ug/l 8260B 05/22/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 05/22/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B O5/22/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 05/22/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 05/22/15 1
Ethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 05/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 8 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-04
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-44
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 14:30
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 05/22/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 05/22/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 05/22/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B O5/22/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B O5/22/15 1
Naphthalene BDL 5.0 ug/1 8260B 05/22/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Styrene BDL 1.0 ug/1 8260B 05/22/15 1
1,1,1,2-Tetrachloroethane 2.0 1.0 ug/l 8260B O5/22/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B O5/22/15 1
Tetrachloroethene 6900 200 ug/1 8260B 05/28/15 200
Toluene BDL 5.0 ug/1 8260B O5/22/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 05/22/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
Trichloroethene 390 50. ug/1 8260B O5/26/15 50
Trichlorofluoromethane BDL 5.0 ug/1 8260B 05/22/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B O5/22/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
Vinyl chloride 67. 1.0 ug/1 8260B O5/22/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 05/22/15 1
Surrogate Recovery
Toluene-d8 93.0 % Rec. 8260B O5/22/15 1
Dibromofluoromethane 96.8 % Rec. 8260B 05/22/15 1
4-Bromofluorobenzene 107. % Rec. 8260B O5/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 05/28/15 09:22 Printed: 05/28/15 09:22
Page 9 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-05
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 13:30
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 53000 1000 ug/l 9060A O5/20/15 1
Volatile Organics
Acetone 64. 50. ug/l 8260B 05/22/15 1
Acrolein BDL 50. ug/1 8260B O5/22/15 1
Acrylonitrile BDL 10. ug/l 8260B O5/22/15 1
Benzene BDL 1.0 ug/1 8260B 05/22/15 1
Bromobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 05/22/15 1
Bromoform BDL 1.0 ug/l 8260B O5/22/15 1
Bromomethane BDL 5.0 ug/1 8260B 05/22/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 05/22/15 1
Chlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B O5/22/15 1
Chloroethane BDL 5.0 ug/1 8260B 05/22/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B O5/22/15 1
Chloroform BDL 5.0 ug/1 8260B 05/22/15 1
Chloromethane BDL 2.5 ug/l 8260B O5/22/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 05/22/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B O5/22/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 05/22/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B O5/22/15 1
Dibromomethane BDL 1.0 ug/l 8260B 05/22/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 05/22/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B O5/22/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,2-Dichloroethene 100 1.0 ug/l 8260B O5/22/15 1
trans-1,2-Dichloroethene 5.9 1.0 ug/l 8260B 05/22/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 05/22/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 05/22/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B O5/22/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 05/22/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B O5/22/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 05/22/15 1
Ethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 05/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 10 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-05
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 13:30
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 05/22/15 1
2-Butanone (MEK) 54. 10. ug/l 8260B 05/22/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 05/22/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B O5/22/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B O5/22/15 1
Naphthalene BDL 5.0 ug/1 8260B 05/22/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B O5/22/15 1
Styrene BDL 1.0 ug/1 8260B 05/22/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 05/22/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B O5/22/15 1
Tetrachloroethene BDL 10. ug/1 8260B 05/26/15 10
Toluene 930 50. ug/1 8260B O5/26/15 10
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 05/22/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B O5/22/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B O5/22/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 05/22/15 1
Trichloroethene BDL 1.0 ug/1 8260B O5/22/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 05/22/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B O5/22/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B O5/22/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 05/22/15 1
Vinyl chloride 48. 1.0 ug/1 8260B O5/22/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 05/22/15 1
Surrogate Recovery
Toluene-d8 108. % Rec. 8260B O5/22/15 1
Dibromofluoromethane 101. % Rec. 8260B 05/22/15 1
4-Bromofluorobenzene 105. % Rec. 8260B O5/22/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 05/28/15 09:22 Printed: 05/28/15 09:22
Page 11 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-06
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-3
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 10:45
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 25000 1000 ug/l 9060A O5/20/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 05/23/15 1
Acrolein BDL 50. ug/1 8260B O5/23/15 1
Acrylonitrile BDL 10. ug/l 8260B O5/23/15 1
Benzene BDL 1.0 ug/1 8260B 05/23/15 1
Bromobenzene BDL 1.0 ug/1 8260B O5/23/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 05/23/15 1
Bromoform BDL 1.0 ug/l 8260B O5/23/15 1
Bromomethane BDL 5.0 ug/1 8260B 05/23/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B O5/23/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 05/23/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B O5/23/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 05/23/15 1
Chlorobenzene BDL 1.0 ug/1 8260B O5/23/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B O5/23/15 1
Chloroethane BDL 5.0 ug/1 8260B 05/23/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B O5/23/15 1
Chloroform BDL 5.0 ug/1 8260B 05/23/15 1
Chloromethane BDL 2.5 ug/l 8260B O5/23/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 05/23/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B O5/23/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 05/23/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B O5/23/15 1
Dibromomethane BDL 1.0 ug/l 8260B 05/23/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B O5/23/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B O5/23/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 05/23/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B O5/23/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 05/23/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B O5/23/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 05/23/15 1
cis-1,2-Dichloroethene 13. 1.0 ug/l 8260B O5/23/15 1
trans-1,2-Dichloroethene 2.2 1.0 ug/l 8260B 05/23/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B O5/23/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 05/23/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 05/23/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B O5/23/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 05/23/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B O5/23/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 05/23/15 1
Ethylbenzene BDL 1.0 ug/l 8260B O5/23/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 05/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 12 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-06
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-3
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 10:45
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B O5/23/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 05/23/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 05/23/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 05/23/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B O5/23/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B O5/23/15 1
Naphthalene BDL 5.0 ug/1 8260B 05/23/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B O5/23/15 1
Styrene BDL 1.0 ug/1 8260B 05/23/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B O5/23/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 05/23/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B O5/23/15 1
Tetrachloroethene BDL 20. ug/1 8260B 05/27/15 20
Toluene 1400 100 ug/1 8260B O5/27/15 20
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 05/23/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B O5/23/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B O5/23/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 05/23/15 1
Trichloroethene BDL 1.0 ug/1 8260B O5/23/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 05/23/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B O5/23/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 05/23/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B O5/23/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 05/23/15 1
Vinyl chloride 2.6 1.0 ug/1 8260B O5/23/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 05/23/15 1
Surrogate Recovery
Toluene-d8 108. % Rec. 8260B O5/23/15 1
Dibromofluoromethane 101. % Rec. 8260B 05/23/15 1
4-Bromofluorobenzene 104. % Rec. 8260B O5/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 05/28/15 09:22 Printed: 05/28/15 09:22
Page 13 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-07
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IW-2
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 13:45
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 880000 20000 ug/l 9060A O5/21/15 20
Volatile Organics
Acetone BDL 1000 ug/l 8260B 05/24/15 20
Acrolein BDL 1000 ug/1 8260B O5/24/15 20
Acrylonitrile BDL 200 ug/l 8260B O5/24/15 20
Benzene BDL 20. ug/1 8260B 05/24/15 20
Bromobenzene BDL 20. ug/1 8260B O5/24/15 20
Bromodichloromethane BDL 20. ug/1 8260B 05/24/15 20
Bromoform BDL 20. ug/l 8260B O5/24/15 20
Bromomethane BDL 100 ug/1 8260B 05/24/15 20
n-Butylbenzene BDL 20. ug/l 8260B O5/24/15 20
sec-Butylbenzene BDL 20. ug/1 8260B 05/24/15 20
tert-Butylbenzene BDL 20. ug/1 8260B O5/24/15 20
Carbon tetrachloride BDL 20. ug/l 8260B 05/24/15 20
Chlorobenzene BDL 20. ug/1 8260B O5/24/15 20
Chlorodibromomethane BDL 20. ug/l 8260B O5/24/15 20
Chloroethane BDL 100 ug/1 8260B 05/24/15 20
2-Chloroethyl vinyl ether BDL 1000 ug/1 8260B O5/24/15 20
Chloroform BDL 100 ug/1 8260B 05/24/15 20
Chloromethane BDL 50. ug/l 8260B O5/24/15 20
2-Chlorotoluene BDL 20. ug/1 8260B 05/24/15 20
4-Chlorotoluene BDL 20. ug/l 8260B O5/24/15 20
1,2-Dibromo-3-Chloropropane BDL 100 ug/1 8260B 05/24/15 20
1,2-Dibromoethane BDL 20. ug/1 8260B O5/24/15 20
Dibromomethane BDL 20. ug/l 8260B 05/24/15 20
1,2-Dichlorobenzene BDL 20. ug/1 8260B O5/24/15 20
1,3-Dichlorobenzene BDL 20. ug/l 8260B O5/24/15 20
1,4-Dichlorobenzene BDL 20. ug/1 8260B 05/24/15 20
Dichlorodifluoromethane BDL 100 ug/1 8260B O5/24/15 20
1,1-Dichloroethane BDL 20. ug/1 8260B 05/24/15 20
1,2-Dichloroethane BDL 20. ug/l 8260B O5/24/15 20
1,1-Dichloroethene BDL 20. ug/1 8260B 05/24/15 20
cis-1,2-Dichloroethene 210 20. ug/l 8260B O5/24/15 20
trans-1,2-Dichloroethene BDL 20. ug/l 8260B 05/24/15 20
1,2-Dichloropropane BDL 20. ug/1 8260B O5/24/15 20
1,1-Dichloropropene BDL 20. ug/l 8260B 05/24/15 20
1,3-Dichloropropane BDL 20. ug/1 8260B 05/24/15 20
cis-1,3-Dichloropropene BDL 20. ug/1 8260B O5/24/15 20
trans-1,3-Dichloropropene BDL 20. ug/1 8260B 05/24/15 20
2,2-Dichloropropane BDL 20. ug/1 8260B O5/24/15 20
Di-isopropyl ether BDL 20. ug/1 8260B 05/24/15 20
Ethylbenzene BDL 20. ug/l 8260B O5/24/15 20
Hexachloro-1,3-butadiene BDL 20. ug/1 8260B 05/24/15 20
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 14 of 17

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander May 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L765479-07
Date Received May 15, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IW-2
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 05/14/15 13:45
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 20. ug/l 8260B O5/24/15 20
p-Isopropyltoluene BDL 20. ug/1 8260B 05/24/15 20
2-Butanone (MEK) BDL 200 ug/l 8260B 05/24/15 20
Methylene Chloride BDL 100 ug/l 8260B 05/24/15 20
4-Methyl-2-pentanone (MIBK) BDL 200 ug/1 8260B O5/24/15 20
Methyl tert-butyl ether BDL 20. ug/l 8260B O5/24/15 20
Naphthalene BDL 100 ug/1 8260B 05/24/15 20
n-Propylbenzene BDL 20. ug/1 8260B O5/24/15 20
Styrene BDL 20. ug/1 8260B 05/24/15 20
1,1,1,2-Tetrachloroethane BDL 20. ug/l 8260B O5/24/15 20
1,1,2,2-Tetrachloroethane BDL 20. ug/1 8260B 05/24/15 20
1,1,2-Trichlorotrifluoroethane BDL 20. ug/l 8260B O5/24/15 20
Tetrachloroethene BDL 20. ug/1 8260B 05/24/15 20
Toluene 4400 500 ug/1 8260B O5/26/15 100
1,2,3-Trichlorobenzene BDL 20. ug/l 8260B 05/24/15 20
1,2,4-Trichlorobenzene BDL 20. ug/1 8260B O5/24/15 20
1,1,1-Trichloroethane BDL 20. ug/l 8260B O5/24/15 20
1,1,2-Trichloroethane BDL 20. ug/1 8260B 05/24/15 20
Trichloroethene BDL 20. ug/1 8260B O5/24/15 20
Trichlorofluoromethane BDL 100 ug/1 8260B 05/24/15 20
1,2,3-Trichloropropane BDL 50. ug/l 8260B O5/24/15 20
1,2,4-Trimethylbenzene BDL 20. ug/1 8260B 05/24/15 20
1,2,3-Trimethylbenzene BDL 20. ug/l 8260B O5/24/15 20
1,3,5-Trimethylbenzene BDL 20. ug/1 8260B 05/24/15 20
Vinyl chloride BDL 20. ug/1 8260B O5/24/15 20
Xylenes, Total BDL 60. ug/l 8260B 05/24/15 20
Surrogate Recovery
Toluene-d8 107. % Rec. 8260B O5/24/15 1
Dibromofluoromethane 107. % Rec. 8260B 05/24/15 1
4-Bromofluorobenzene 103. % Rec. 8260B O5/24/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 05/28/15 09:22 Printed: 05/28/15 09:22
Page 15 of 17

Attachment A
List of Analytes with QC Qualifiers
Sample Work Sample Run
Number Group Type Analyte ID Qualifier
L765479-07 WG791140 SAMP 2-Chloroethyl vinyl ether R3038976 J3
WG791140 SAMP Naphthalene R3038976 J4
WG791140 SAMP 1,2,3-Trichlorobenzene R3038976 J4
Page 16 of 17

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J3 The associated batch QC was outside the established quality control range
for precision.
J4 The associated batch QC was outside the established quality control range
for accuracy.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected) ."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 17 of 17

SillingInformation; Analysis JContainer{Pre servatiye Chain ofcumodx Pap!_of_
Bunnell - lalmlmons Engineering, Inc. Project Manager
6004 Ponders Court
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Relinquished by:(Signaturej Gate: Time: Received for labby:Vignature Date: Time: pH Checked: NCF!

APPENDIX F
LABORATORY ANALYTICAL DATA SHEETS
GROUNDWATER
JULY 2015 [90 Day]
(Provided on Enclosed CD)

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Tuesday July 28, 2015
Report Number: L776639
Samples Received: 07/14/15
Client Project: J15-1022-42
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By: I
Jimmy Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-01
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-5
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 11:40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 3600000 100000 ug/l 9060A 07/15/15 100
Volatile Organics
Acetone 130 50. ug/l 8260B 07/18/15 1
Acrolein BDL 50. ug/1 8260B 07/18/15 1
Acrylonitrile BDL 10. ug/l 8260B 07/18/15 1
Benzene BDL 1.0 ug/1 8260B 07/18/15 1
Bromobenzene BDL 1.0 ug/1 8260B 07/18/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 07/18/15 1
Bromoform BDL 1.0 ug/l 8260B 07/18/15 1
Bromomethane BDL 5.0 ug/1 8260B 07/18/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 07/18/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 07/18/15 1
Chloroethane BDL 5.0 ug/1 8260B 07/18/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 07/18/15 1
Chloroform BDL 5.0 ug/1 8260B 07/18/15 1
Chloromethane BDL 2.5 ug/l 8260B 07/18/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 07/18/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 07/18/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 07/18/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 07/18/15 1
Dibromomethane BDL 1.0 ug/l 8260B 07/18/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 07/18/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 07/18/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 07/18/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 07/18/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 07/18/15 1
cis-1,2-Dichloroethene 720 20. ug/l 8260B 07/22/15 20
trans-1,2-Dichloroethene 5.8 1.0 ug/l 8260B 07/18/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 07/18/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 07/18/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 07/18/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/18/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/18/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 07/18/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 07/18/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 07/18/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 2 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-01
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-5
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 11:40
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 07/18/15 1
2-Butanone (MEK) 120 10. ug/l 8260B 07/18/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 07/18/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 07/18/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 07/18/15 1
Naphthalene BDL 5.0 ug/1 8260B 07/18/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
Styrene BDL 1.0 ug/1 8260B 07/18/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 07/18/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/18/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 07/18/15 1
Tetrachloroethene 29. 1.0 ug/1 8260B 07/18/15 1
Toluene 21. 5.0 ug/1 8260B 07/18/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 07/18/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 07/18/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 07/18/15 1
Trichloroethene 16. 1.0 ug/1 8260B 07/18/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 07/18/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 07/18/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
Vinyl chloride 33. 1.0 ug/1 8260B 07/18/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 07/18/15 1
Surrogate Recovery
Toluene-d8 109. % Rec. 8260B 07/18/15 1
Dibromofluoromethane 105. % Rec. 8260B 07/18/15 1
4-Bromofluorobenzene 101. % Rec. 8260B 07/18/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/22/15 16:58 Revised: 07/28/15 15:22
Page 3 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-02
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-6
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 12:30
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 3000 1000 ug/l 9060A 07/15/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 07/18/15 1
Acrolein BDL 50. ug/1 8260B 07/18/15 1
Acrylonitrile BDL 10. ug/l 8260B 07/18/15 1
Benzene BDL 1.0 ug/1 8260B 07/18/15 1
Bromobenzene BDL 1.0 ug/1 8260B 07/18/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 07/18/15 1
Bromoform BDL 1.0 ug/l 8260B 07/18/15 1
Bromomethane BDL 5.0 ug/1 8260B 07/18/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 07/18/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 07/18/15 1
Chloroethane BDL 5.0 ug/1 8260B 07/18/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 07/18/15 1
Chloroform BDL 5.0 ug/1 8260B 07/18/15 1
Chloromethane BDL 2.5 ug/l 8260B 07/18/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 07/18/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 07/18/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 07/18/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 07/18/15 1
Dibromomethane BDL 1.0 ug/l 8260B 07/18/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 07/18/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 07/18/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 07/18/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 07/18/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 07/18/15 1
cis-1,2-Dichloroethene 1000 50. ug/l 8260B 07/22/15 50
trans-1,2-Dichloroethene 2.9 1.0 ug/l 8260B 07/18/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 07/18/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 07/18/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 07/18/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/18/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/18/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 07/18/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 07/18/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 07/18/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 4 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-02
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-6
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 12:30
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 07/18/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 07/18/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 07/18/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 07/18/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 07/18/15 1
Naphthalene BDL 5.0 ug/1 8260B 07/18/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
Styrene BDL 1.0 ug/1 8260B 07/18/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 07/18/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/18/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 07/18/15 1
Tetrachloroethene 1900 50. ug/1 8260B 07/22/15 50
Toluene BDL 5.0 ug/1 8260B 07/18/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 07/18/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 07/18/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 07/18/15 1
Trichloroethene 77. 1.0 ug/1 8260B 07/18/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 07/18/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 07/18/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
Vinyl chloride 16. 1.0 ug/1 8260B 07/18/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 07/18/15 1
Surrogate Recovery
Toluene-d8 103. % Rec. 8260B 07/18/15 1
Dibromofluoromethane 105. % Rec. 8260B 07/18/15 1
4-Bromofluorobenzene 95.9 % Rec. 8260B 07/18/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/22/15 16:58 Revised: 07/28/15 15:22
Page 5 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-03
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-12
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 11:10
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 270000 10000 ug/l 9060A 07/15/15 10
Volatile Organics
Acetone 62. 50. ug/l 8260B 07/23/15 1
Acrolein BDL 50. ug/1 8260B 07/23/15 1
Acrylonitrile BDL 10. ug/l 8260B 07/23/15 1
Benzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 07/23/15 1
Bromoform BDL 1.0 ug/l 8260B 07/23/15 1
Bromomethane BDL 5.0 ug/1 8260B 07/23/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 07/23/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
Chloroethane BDL 5.0 ug/1 8260B 07/23/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 07/23/15 1
Chloroform BDL 5.0 ug/1 8260B 07/23/15 1
Chloromethane BDL 2.5 ug/l 8260B 07/23/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 07/23/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 07/23/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 07/23/15 1
Dibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,2-Dichloroethene 67. 1.0 ug/l 8260B 07/23/15 1
trans-1,2-Dichloroethene 5.0 1.0 ug/l 8260B 07/23/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 07/23/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 07/23/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 6 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-03
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-12
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 11:10
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 07/23/15 1
2-Butanone (MEK) 100 10. ug/l 8260B 07/23/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 07/23/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 07/23/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 07/23/15 1
Naphthalene BDL 5.0 ug/1 8260B 07/23/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Styrene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 07/23/15 1
Tetrachloroethene BDL 1.0 ug/1 8260B 07/23/15 1
Toluene 10000 1000 ug/1 8260B 07/22/15 200
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
Trichloroethene BDL 1.0 ug/1 8260B 07/23/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 07/23/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Vinyl chloride 11. 1.0 ug/1 8260B 07/23/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 07/23/15 1
Surrogate Recovery
Toluene-d8 119. % Rec. 8260B 07/23/15 1
Dibromofluoromethane 113. % Rec. 8260B 07/23/15 1
4-Bromofluorobenzene 102. % Rec. 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/22/15 16:58 Revised: 07/28/15 15:22
Page 7 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-04
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-44
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 14:00
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 2000 1000 ug/l 9060A 07/15/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 07/23/15 1
Acrolein BDL 50. ug/1 8260B 07/23/15 1
Acrylonitrile BDL 10. ug/l 8260B 07/23/15 1
Benzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 07/23/15 1
Bromoform BDL 1.0 ug/l 8260B 07/23/15 1
Bromomethane BDL 5.0 ug/1 8260B 07/23/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 07/23/15 1
Chlorobenzene 1.7 1.0 ug/1 8260B 07/23/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
Chloroethane BDL 5.0 ug/1 8260B 07/23/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 07/23/15 1
Chloroform BDL 5.0 ug/1 8260B 07/23/15 1
Chloromethane BDL 2.5 ug/l 8260B 07/23/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 07/23/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 07/23/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 07/23/15 1
Dibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1-Dichloroethene 1.4 1.0 ug/1 8260B 07/23/15 1
cis-1,2-Dichloroethene 1300 200 ug/l 8260B 07/22/15 200
trans-1,2-Dichloroethene 7.2 1.0 ug/l 8260B 07/23/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 07/23/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 07/23/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 8 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-04
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID MW-44
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 14:00
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 07/23/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 07/23/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 07/23/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 07/23/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 07/23/15 1
Naphthalene BDL 5.0 ug/1 8260B 07/23/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Styrene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1,2-Tetrachloroethane 1.8 1.0 ug/l 8260B 07/23/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 07/23/15 1
Tetrachloroethene 6700 200 ug/1 8260B 07/22/15 200
Toluene BDL 5.0 ug/1 8260B 07/23/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
Trichloroethene 440 1.0 ug/1 8260B 07/23/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 07/23/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Vinyl chloride 54. 1.0 ug/1 8260B 07/23/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 07/23/15 1
Surrogate Recovery
Toluene-d8 106. % Rec. 8260B 07/23/15 1
Dibromofluoromethane ill. % Rec. 8260B 07/23/15 1
4-Bromofluorobenzene 91.7 % Rec. 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/22/15 16:58 Revised: 07/28/15 15:23
Page 9 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-05
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 12:45
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 37000 10000 ug/l 9060A 07/15/15 10
Volatile Organics
Acetone BDL 50. ug/l 8260B 07/23/15 1
Acrolein BDL 50. ug/1 8260B 07/23/15 1
Acrylonitrile BDL 10. ug/l 8260B 07/23/15 1
Benzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 07/23/15 1
Bromoform BDL 1.0 ug/l 8260B 07/23/15 1
Bromomethane BDL 5.0 ug/1 8260B 07/23/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 07/23/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
Chloroethane BDL 5.0 ug/1 8260B 07/23/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 07/23/15 1
Chloroform BDL 5.0 ug/1 8260B 07/23/15 1
Chloromethane BDL 2.5 ug/l 8260B 07/23/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 07/23/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 07/23/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 07/23/15 1
Dibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,2-Dichloroethene 86. 1.0 ug/l 8260B 07/23/15 1
trans-1,2-Dichloroethene 6.8 1.0 ug/l 8260B 07/23/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 07/23/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 07/23/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 10 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-05
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-1
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 12:45
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 07/23/15 1
2-Butanone (MEK) 26. 10. ug/l 8260B 07/23/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 07/23/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 07/23/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 07/23/15 1
Naphthalene BDL 5.0 ug/1 8260B 07/23/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Styrene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 07/23/15 1
Tetrachloroethene BDL 1.0 ug/1 8260B 07/23/15 1
Toluene 1200 100 ug/1 8260B 07/22/15 20
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
Trichloroethene BDL 1.0 ug/1 8260B 07/23/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 07/23/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Vinyl chloride 34. 1.0 ug/1 8260B 07/23/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 07/23/15 1
Surrogate Recovery
Toluene-d8 105. % Rec. 8260B 07/23/15 1
Dibromofluoromethane 112. % Rec. 8260B 07/23/15 1
4-Bromofluorobenzene 100. % Rec. 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/22/15 16:58 Revised: 07/28/15 15:23
Page 11 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-06
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-3
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 12:00
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 8500 1000 ug/l 9060A 07/15/15 1
Volatile Organics
Acetone BDL 50. ug/l 8260B 07/23/15 1
Acrolein BDL 50. ug/1 8260B 07/23/15 1
Acrylonitrile BDL 10. ug/l 8260B 07/23/15 1
Benzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 07/23/15 1
Bromoform BDL 1.0 ug/l 8260B 07/23/15 1
Bromomethane BDL 5.0 ug/1 8260B 07/23/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 07/23/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
Chloroethane BDL 5.0 ug/1 8260B 07/23/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 07/23/15 1
Chloroform BDL 5.0 ug/1 8260B 07/23/15 1
Chloromethane BDL 2.5 ug/l 8260B 07/23/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 07/23/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 07/23/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 07/23/15 1
Dibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,2-Dichloroethene 5.0 1.0 ug/l 8260B 07/23/15 1
trans-1,2-Dichloroethene 2.9 1.0 ug/l 8260B 07/23/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 07/23/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 07/23/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 12 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-06
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID RW-3
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 12:00
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 07/23/15 1
2-Butanone (MEK) BDL 10. ug/l 8260B 07/23/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 07/23/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 07/23/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 07/23/15 1
Naphthalene BDL 5.0 ug/1 8260B 07/23/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Styrene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 07/23/15 1
Tetrachloroethene BDL 1.0 ug/1 8260B 07/23/15 1
Toluene 240 25. ug/1 8260B 07/22/15 5
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
Trichloroethene BDL 1.0 ug/1 8260B 07/23/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 07/23/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Vinyl chloride BDL 1.0 ug/1 8260B 07/23/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 07/23/15 1
Surrogate Recovery
Toluene-d8 109. % Rec. 8260B 07/23/15 1
Dibromofluoromethane 105. % Rec. 8260B 07/23/15 1
4-Bromofluorobenzene 103. % Rec. 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/22/15 16:58 Revised: 07/28/15 15:23
Page 13 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-07
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IW-2
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 13:00
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon) 250000 20000 ug/l 9060A 07/15/15 20
Volatile Organics
Acetone 200 50. ug/l 8260B 07/23/15 1
Acrolein BDL 50. ug/1 8260B 07/23/15 1
Acrylonitrile BDL 10. ug/l 8260B 07/23/15 1
Benzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 07/23/15 1
Bromoform BDL 1.0 ug/l 8260B 07/23/15 1
Bromomethane BDL 5.0 ug/1 8260B 07/23/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
tert-Butylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Carbon tetrachloride BDL 1.0 ug/l 8260B 07/23/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
Chloroethane BDL 5.0 ug/1 8260B 07/23/15 1
2-Chloroethyl vinyl ether BDL 50. ug/1 8260B 07/23/15 1
Chloroform BDL 5.0 ug/1 8260B 07/23/15 1
Chloromethane BDL 2.5 ug/l 8260B 07/23/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 07/23/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 07/23/15 1
1,2-Dibromoethane BDL 1.0 ug/1 8260B 07/23/15 1
Dibromomethane BDL 1.0 ug/l 8260B 07/23/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
Dichlorodifluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,2-Dichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,2-Dichloroethene 94. 1.0 ug/l 8260B 07/23/15 1
trans-1,2-Dichloroethene 1.0 1.0 ug/l 8260B 07/23/15 1
1,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 07/23/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/23/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 07/23/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 07/23/15 1
Ethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 14 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-07
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID IW-2
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 13:00
Parameter Result Det. Limit Units Method Date Dil.
Isopropylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 07/23/15 1
2-Butanone (MEK) 370 10. ug/l 8260B 07/23/15 1
Methylene Chloride BDL 5.0 ug/l 8260B 07/23/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/1 8260B 07/23/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 07/23/15 1
Naphthalene BDL 5.0 ug/1 8260B 07/23/15 1
n-Propylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Styrene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/23/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 07/23/15 1
Tetrachloroethene 2.2 1.0 ug/1 8260B 07/23/15 1
Toluene 8900 1000 ug/1 8260B 07/22/15 200
1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 07/23/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 07/23/15 1
Trichloroethene BDL 1.0 ug/1 8260B 07/23/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 07/23/15 1
1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 07/23/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 07/23/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 07/23/15 1
Vinyl chloride 6.0 1.0 ug/1 8260B 07/23/15 1
Xylenes, Total BDL 3.0 ug/l 8260B 07/23/15 1
Surrogate Recovery
Toluene-d8 ill. % Rec. 8260B 07/23/15 1
Dibromofluoromethane 121. % Rec. 8260B 07/23/15 1
4-Bromofluorobenzene 102. % Rec. 8260B 07/23/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/22/15 16:58 Revised: 07/28/15 15:23
Page 15 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-08
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID TRIP BLANK
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 00:00
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone BDL 50. ug/1 8260B 07/18/15 1
Acrolein BDL 50. ug/l 8260B 07/18/15 1
Acrylonitrile BDL 10. ug/l 8260B 07/18/15 1
Benzene BDL 1.0 ug/1 8260B 07/18/15 1
Bromobenzene BDL 1.0 ug/l 8260B 07/18/15 1
Bromodichloromethane BDL 1.0 ug/1 8260B 07/18/15 1
Bromoform BDL 1.0 ug/1 8260B 07/18/15 1
Bromomethane BDL 5.0 ug/1 8260B 07/18/15 1
n-Butylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
sec-Butylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
tert-Butylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
Carbon tetrachloride BDL 1.0 ug/1 8260B 07/18/15 1
Chlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
Chlorodibromomethane BDL 1.0 ug/l 8260B 07/18/15 1
Chloroethane BDL 5.0 ug/1 8260B 07/18/15 1
2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 07/18/15 1
Chloroform BDL 5.0 ug/1 8260B 07/18/15 1
Chloromethane BDL 2.5 ug/1 8260B 07/18/15 1
2-Chlorotoluene BDL 1.0 ug/1 8260B 07/18/15 1
4-Chlorotoluene BDL 1.0 ug/l 8260B 07/18/15 1
1,2-Dibromo-3-Chloropropane BDL 5.0 ug/1 8260B 07/18/15 1
1,2-Dibromoethane BDL 1.0 ug/l 8260B 07/18/15 1
Dibromomethane BDL 1.0 ug/1 8260B 07/18/15 1
1,2-Dichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 07/18/15 1
1,4-Dichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
Dichlorodifluoromethane BDL 5.0 ug/l 8260B 07/18/15 1
1,1-Dichloroethane BDL 1.0 ug/1 8260B 07/18/15 1
1,2-Dichloroethane BDL 1.0 ug/1 8260B 07/18/15 1
1,1-Dichloroethene BDL 1.0 ug/1 8260B 07/18/15 1
cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 07/18/15 1
trans-1,2-Dichloroethene BDL 1.0 ug/1 8260B 07/18/15 1
1,2-Dichloropropane BDL 1.0 ug/l 8260B 07/18/15 1
1,1-Dichloropropene BDL 1.0 ug/l 8260B 07/18/15 1
1,3-Dichloropropane BDL 1.0 ug/1 8260B 07/18/15 1
cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 07/18/15 1
trans-1,3-Dichloropropene BDL 1.0 ug/1 8260B 07/18/15 1
2,2-Dichloropropane BDL 1.0 ug/1 8260B 07/18/15 1
Di-isopropyl ether BDL 1.0 ug/1 8260B 07/18/15 1
Ethylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
Hexachloro-1,3-butadiene BDL 1.0 ug/1 8260B 07/18/15 1
Isopropylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
p-Isopropyltoluene BDL 1.0 ug/1 8260B 07/18/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Page 16 of 19

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Andy Alexander July 28,2015
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC Sample # L776639-08
Date Received July 14, 2015
Description Andrex Industries
Site ID ASHEVILLE, NC
Sample ID TRIP BLANK
Project # J15-1022-42
Collected By Benjamin P. Nisbeth
Collection Date 07/13/15 00:00
Parameter Result Det. Limit Units Method Date Dil.
2-Butanone (MEK) BDL 10. ug/l 8260B 07/18/15 1
Methylene Chloride BDL 5.0 ug/1 8260B 07/18/15 1
4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 07/18/15 1
Methyl tert-butyl ether BDL 1.0 ug/l 8260B 07/18/15 1
Naphthalene BDL 5.0 ug/1 8260B 07/18/15 1
n-Propylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
Styrene BDL 1.0 ug/1 8260B 07/18/15 1
1,1,1,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/18/15 1
1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 8260B 07/18/15 1
1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 07/18/15 1
Tetrachloroethene BDL 1.0 ug/1 8260B 07/18/15 1
Toluene BDL 5.0 ug/l 8260B 07/18/15 1
1,2,3-Trichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,2,4-Trichlorobenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 07/18/15 1
1,1,2-Trichloroethane BDL 1.0 ug/1 8260B 07/18/15 1
Trichloroethene BDL 1.0 ug/l 8260B 07/18/15 1
Trichlorofluoromethane BDL 5.0 ug/1 8260B 07/18/15 1
1,2,3-Trichloropropane BDL 2.5 ug/1 8260B 07/18/15 1
1,2,4-Trimethylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 07/18/15 1
1,3,5-Trimethylbenzene BDL 1.0 ug/1 8260B 07/18/15 1
Vinyl chloride BDL 1.0 ug/l 8260B 07/18/15 1
Xylenes, Total BDL 3.0 ug/1 8260B 07/18/15 1
Surrogate Recovery
Toluene-d8 106. o Rec. 8260B 07/18/15 1
Dibromofluoromethane 95.8 o Rec. 8260B 07/18/15 1
4-Bromofluorobenzene 103. o Rec. 8260B 07/18/15 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/22/15 16:58 Revised: 07/28/15 15:23
Page 17 of 19

Attachment A
List of Analytes with QC Qualifiers
Sample Work Sample Run
Number Group Type Analyte ID Qualifier
L776639-01 WG802440 SAMP 2-Chloroethyl vinyl ether R3051724 J3
L776639-02 WG802440 SAMP 2-Chloroethyl vinyl ether R3051724 J3
L776639-03 WG804487 SAMP Toluene-d8 R3052536 J1
L776639-04 WG804487 SAMP Trichloroethene R3052536 E
L776639-06 WG804487 SAMP Acetone R3052536 J3
WG804487 SAMP Acrolein R3052536 J3
WG804487 SAMP Bromodichloromethane R3052536 J5
WG804487 SAMP 2-Chloroethyl vinyl ether R3052536 J6
WG804487 SAMP 1,2-Dichloroethane R3052536 J5
WG804487 SAMP trans-1,2-Dichloroethene R3052536 J5
WG804487 SAMP Di-isopropyl ether R3052536 J5
WG804487 SAMP Methylene Chloride R3052536 J5
WG804487 SAMP 4-Methyl-2-pentanone (MIBK) R3052536 J5
WG804487 SAMP Methyl tert-butyl ether R3052536 J5J3
L776639-08 WG802440 SAMP 2-Chloroethyl vinyl ether R3051724 J3
Page 18 of 19

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
E GTL (EPA) - Greater than upper calibration limit: Actual value is known to
be greater than the upper calibration range.
J1 Surrogate recovery limits have been exceeded; values are outside upper
control limits
J3 The associated batch QC was outside the established quality control range
for precision.
J5 The sample matrix interfered with the ability to make any accurate
determination; spike value is high
J6 The sample matrix interfered with the ability to make any accurate
determination; spike value is low
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected) ."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 19 of 19

filling Information: Andly,�is f Cor.Laincr{Preserwative Chain cfCustody gage_of_
FBunnnedl # Lam mons Engineering, Inc. vmjectmanager
6004 Ponders Court *ESCI
6004 Ponders Court Greenville,SC 29615
Greenville,SC 29615
120ASLebonGhAd r2
F.mail To:andYp.
[e-mail] Mourw Juliet,1w371t2 0� � ■
!Repo it to:
Mr.Andy Alexander arm+.'we.%7-sm
aha'+e:4or1A6 -5d59
cIt istbt! + �f }/,1/ `A, F. ?S6 SH59
Project 1'7C1ltl�,( } r+�lr
Ces(.riptior: Arldrex IndUStrleS Collected- l C
L#
Client PPrnOct p Lab PFOjeCt K _
p hone:864-2$61265 J15-1022-42 BUNLAM63aSCA14102240
Fax: ,149
864-288-44 30 z
ra
Co/ii�cctedby;print]: 5ItelFacflityID40 CL U ACCtnum: BUNLAMGSC
ASHEVILLf,NC ' T mplate;T58401
Collected by(s,gna �: Rush? (Lab MU37 Be Notified) bate Results Need;;­
collected Q Prelegin:P5170Z5
�� —Same P2 y,,,,,,,,,,,,,,,,,,,,,,,�.-2{p9E E TSR:354•Jimmy Hutin
Next Day its Email? No X_Yes E in
Immediately --,,,,, ,,,,,,,,,,, C7 d o
TwaDay - FA5{�,Na Yes No. Lti0 p n;
Packed n Ice N_ Y^ —three t7ax............. ... 5% — f hl
Lo Shipped Via:FedE}( rounCJ
Sample ID Camp{brab Matrix* Dept!, Daze Time .rtrs 0 flq
Ikpm.1[ont5R7ari Sarnpltr�latt Uiily'
GUI 7.13 K 11 3 X X —---o?
w Gw I 3 x X 6YAW '
- t* - GW 1+00 3 X x Oq
- Ir Gw 3 x
r GW X °
MatYix; SS-Soil GW GFOUndwater VM-WastelJWater DIN-Drinking Water OT•Other
pH � Temp - __-
emarks:Analyre at Ur
] ! f Iow Other Hold p
Rel.inqui5hedhy-{Signat e� Date: Time- Recelved by-.(S4rl tore) Samples umedvi�; ❑UPS Co ditian: r�(�idbuse rsllyl
� } l Fed Ex ❑Courier a
• .T.r _
Re wished by;(Signature) Date: Time: Received bv:�Signatvre) Temp: "C Bottles Received! 0�
COC Seallmtact; Y •_N _NA
Relinquished by:(Signature) Date: Time: Reuei"d4pr lab by-[Signature) Date. Tlme, pm Checked. NCF-
i

APPENDIX G
LABORATORY ANALYTICAL DATA SHEETS
GROUNDWATER&SURFACE WATER
SEPTEMBER 2015 [150 Day]
(Provided on Enclosed CD)

*ESC ANALYTICAL REPORT MyESC
L-A-B S-C-I-E-N-C-E-S September 28, 2015
Bunnell - Lammons Engineering, Inc.
Sample Delivery Group: L788744
Samples Received: 09/15/2015
Project Number: J15-1022-42
Description: Andrex Industries
Site: ASHEVILLE, NC
Report To: Mr.Andy Alexander
6004 Ponders Court
Greenville, SC 29615
Entire Report Reviewed By:
Jimmy Hunt
�F Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
reproduced,except in full,without written approval of the laboratory. Where applicable,sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures:060302,060303,and 060304.
ri
r

TABLE OF CONTENTS ONE LAB.NATIONWIDE.
'Cp:Cover Page 1 Fn
2Tc:Table of Contents 2
3Ss:Sample Summary 3
4Cn:Case Narrative 5 FS
5Sr:Sample Results 6 [Cn]
RW-1 L788744-01 6
RW-3 L788744-02 8 Isr
MW-5 L788744-03 10
MW-6 L788744-04 12 RC
MW-12 L788744-05 14
R,
MW-44 L788744-06 16
IW-2 L788744-07 18 $AI
6Qc:Quality Control Summary 20
Wet Chemistry by Method 9060A 20 FSC
Volatile Organic Compounds(GC/MS) by Method 8260B 21
7GI: Glossary of Terms 30
8AI:Accreditations& Locations 31
9Sc: Chain of Custody 32
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 2 of 32

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
RW-1 L788744-01 GW Ivan Irizarry 09/14/1511:03 09/15/15 09:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time FTC
Volatile Organic Compounds(GC/MS)by Method 8260B WG816019 1 09/18/1517:36 09/18/1517:36 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG816580 20 09/21/1516:34 09/21/1516:34 KLO
Wet Chemistry by Method 9060A WG815629 20 09/17/15 23:31 09/17/15 23:31 LLS
Collected by Collected date/time Received date/time Cn
RW-3 L788744-02 GW Ivan Irizarry 09/14/1510:45 09/15/15 09:00
FSr
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260E WG816019 1 09/18/1517:55 09/18/1517:55 MCB 6QCl
Volatile Organic Compounds(GC/MS)by Method 8260E WG816580 50 09/21/1516:54 09/21/1516:54 KLO
Wet Chemistry by Method 9060A WG815629 20 09/17/15 23:43 09/17/15 23:43 LLS
�GI
Collected by Collected date/time Received date/time
MW-5 L788744-03 GW Ivan Irizarry 09/14/1510:52 09/15/15 09:00 FAI
Method Batch Dilution Preparation Analysis Analysis Analyst
FSC
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG816019 1 09/18/1518:13 09/18/1518:13 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG816580 10 09/21/1517:14 09/21/1517:14 KLO
Wet Chemistry by Method 9060A WG815629 100 09/18/15 06:21 09/18/15 06:21 LLS
Collected by Collected date/time Received date/time
MW-6 L788744-04 GW Ivan Irizarry 09/14/1510:15 09/15/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260E WG816019 1 09/18/1518:31 09/18/1518:31 MCB
Volatile Organic Compounds(GC/MS)by Method 8260E WG816580 50 09/21/1517:34 09/21/1517:34 KLO
Wet Chemistry by Method 9060A WG815629 1 09/18/15 00:18 09/18/15 00:18 LLS
Collected by Collected date/time Received date/time
MW-12 L788744-05 GW Ivan Irizarry 09/14/1511:28 09/15/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG816019 1 09/18/1518:49 09/18/1518:49 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG816806 500 09/22/1515:21 09/22/1515:21 KLO
Volatile Organic Compounds(GC/MS)by Method 8260B WG817022 1 09/23/1517:31 09/23/1517:31 KLO
Wet Chemistry by Method 9060A WG815629 20 09/18/15 00:29 09/18/15 00:29 LLS
Collected by Collected date/time Received date/time
MW-44 L788744-06 GW Ivan Irizarry 09/14/1511:30 09/15/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG816019 1 09/18/1519:08 09/18/1519:08 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG816580 200 09/21/1518:14 09/21/1518:14 KLO
Volatile Organic Compounds(GC/MS)by Method 8260B WG817022 1 09/23/15 21:53 09/23/15 21:53 KLO
Wet Chemistry by Method 9060A WG815629 1 09/18/15 00:40 09/18/15 00:40 LLS
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 3 of 32

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
IW-2 L788744-07 GW Ivan Irizarry 09/14/1510:16 09/15/1509:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time FTC
Volatile Organic Compounds(GC/MS)by Method 8260B WG816019 1 09/18/1519:26 09/18/1519:26 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG816806 1000 09/22/1515:39 09/22/1515:39 KLO
Volatile Organic Compounds(GC/MS)by Method 8260B WG817022 1 09/23/1517:52 09/23/1517:52 KLO
Wet Chemistry by Method 9060A WG815629 20 09/18/15 00:51 09/18/15 00:51 LLS
[Cn]
FSr
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 4 of 32

CASE NARRATIVE ONE LAB.NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers,with the FP1
appropriate preservatives, and within method specified holding times. All MDL(LOD)and RDL(LOQ)values reported for environmental samples have been corrected for the dilution factor used in the FTC
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my FSS
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
FSr
FC-1
�GI
Jimmy Hunt rAl
Technical Service Representative
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 5 of 32

RW-1 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 11:03 L788744
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 37500 20000 20 09/17/2015 23:31 WG815629
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/18/201517:36 WG816019
Acrolein ND 50.0 1 09/18/201517:36 WG816019
Acrylonitrile ND 10.0 1 09/18/201517:36 WG816019
Benzene ND 1.00 1 09/18/201517:36 WG816019
Bromobenzene ND 1.00 1 09/18/201517:36 WG816019 6
QC
Bromodichloromethane ND 1.00 1 09/18/201517:36 WG816019
Bromoform ND 1.00 1 09/18/201517:36 WG816019
Bromomethane ND 5.00 1 09/18/201517:36 WG816019 q
n-Butylbenzene ND 1.00 1 09/18/201517:36 WG816019
sec-Butylbenzene ND 1.00 1 09/18/201517:36 WG816019 FAI
tert-Butylbenzene ND 1.00 1 09/18/201517:36 WG816019
Carbon tetrachloride ND 1.00 1 09/18/201517:36 WG816019 FSC
Chlorobenzene ND 1.00 1 09/18/201517:36 WG816019
Chlorodibromomethane ND 1.00 1 09/18/201517:36 WG816019
Chloroethane ND 5.00 1 09/18/201517:36 WG816019
2-Chloroethyl vinyl ether ND 50.0 1 09/18/201517:36 WG816019
Chloroform ND 5.00 1 09/18/201517:36 WG816019
Chloromethane ND 2.50 1 09/18/201517:36 WG816019
2-Chlorotoluene ND 1.00 1 09/18/201517:36 WG816019
4-Chlorotoluene ND 1.00 1 09/18/201517:36 WG816019
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/18/201517:36 WG816019
1,2-Dibromoethane ND 1.00 1 09/18/201517:36 WG816019
Dibromomethane ND 1.00 1 09/18/201517:36 WG816019
1,2-Dichlo robe nzene ND 1.00 1 09/18/201517:36 WG816019
1,3-Dichlorobenzene ND 1.00 1 09/18/201517:36 WG816019
1,4-Dichlorobenzene ND 1.00 1 09/18/201517:36 WG816019
Dichlorodifluoromethane ND 5.00 1 09/18/201517:36 WG816019
1,1-Dichloroethane ND 1.00 1 09/18/201517:36 WG816019
1,2-Dichloroethane ND 1.00 1 09/18/201517:36 WG816019
1,1-Dichloroethene ND 1.00 1 09/18/201517:36 WG816019
cis-1,2-Dichloroethene 9.07 1.00 1 09/18/201517:36 WG816019
trans-1,2-Dichloroethene 3.91 1.00 1 09/18/201517:36 WG816019
1,2-Dichloropropane ND 1.00 1 09/18/201517:36 WG816019
1,1-Dichloropropene ND 1.00 1 09/18/201517:36 WG816019
1,3-Dichloropropane ND 1.00 1 09/18/201517:36 WG816019
cis-1,3-Dichloropropene ND 1.00 1 09/18/201517:36 WG816019
trans-13-Dichloropropene ND 1.00 1 09/18/201517:36 WG816019
2,2-Dichloropropane ND 1.00 1 09/18/201517:36 WG816019
Di-isopropyl ether ND 1.00 1 09/18/201517:36 WG816019
Ethylbenzene ND 1.00 1 09/18/201517:36 WG816019
Hexachloro-1,3-butadiene ND 1.00 1 09/18/201517:36 WG816019
Isopropylbenzene ND 1.00 1 09/18/201517:36 WG816019
p-Isopropyltoluene ND 1.00 1 09/18/201517:36 WG816019
2-Butanone(MEK) 24.7 10.0 1 09/18/201517:36 WG816019
Methylene Chloride ND 5.00 1 09/18/201517:36 WG816019
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/18/201517:36 WG816019
Methyl tert-butyl ether ND 1.00 1 09/18/201517:36 WG816019
Naphthalene ND 5.00 1 09/18/201517:36 WG816019
n-Propylbenzene ND 1.00 1 09/18/201517:36 WG816019
Styrene ND 1.00 1 09/18/201517:36 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 6 of 32

RW-1 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 11:03 L788744
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/18/201517:36 WG816019 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/18/201517:36 WG816019
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/18/201517:36 WG816019 F
Tetrachloroethene ND 1.00 1 09/18/201517:36 WG816019
Toluene 1130 100 20 09/21/201516:34 WG816580
1,2,3-Trichlorobenzene ND 1.00 1 09/18/201517:36 WG816019 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/18/201517:36 WG816019
1,1,1-Trichloroethane ND 1.00 1 09/18/201517:36 WG816019
1,1,2-Trichloroethane ND 1.00 1 09/18/201517:36 WG816019
Trichloroethene ND 1.00 1 09/18/201517:36 WG816019
Trichlorofluoromethane ND 5.00 1 09/18/201517:36 WG816019 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/18/201517:36 WG816019
1,2,4-Trimethylbenzene ND 1.00 1 09/18/201517:36 WG816019 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/18/201517:36 WG816019 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/18/201517:36 WG816019
Vinyl chloride 3.97 1.00 1 09/18/201517:36 WG816019 FAI
Xylenes,Total ND 3.00 1 09/18/201517:36 WG816019
(S)Toluene-d8 103 90.0-115 091181201517.36 WG816019 F
(S)Dibromofluoromethone 93.9 79.0-121 091181201517:36 WG816019
(S)4-Bromofluorobenzene 106 80.1-120 09118120151736 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 7 of 32

RW-3 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 10:45 L788744
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 225000 20000 20 09/17/2015 23:43 WG815629
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/18/201517:55 WG816019
Acrolein ND 50.0 1 09/18/201517:55 WG816019
Acrylonitrile ND 10.0 1 09/18/201517:55 WG816019
Benzene ND 1.00 1 09/18/201517:55 WG816019
Bromobenzene ND 1.00 1 09/18/201517:55 WG816019 6
QC
Bromodichloromethane ND 1.00 1 09/18/201517:55 WG816019
Bromoform ND 1.00 1 09/18/201517:55 WG816019
Bromomethane ND 5.00 1 09/18/201517:55 WG816019 q
n-Butylbenzene ND 1.00 1 09/18/201517:55 WG816019
sec-Butylbenzene ND 1.00 1 09/18/201517:55 WG816019 FAI
tert-Butylbenzene ND 1.00 1 09/18/201517:55 WG816019
Carbon tetrachloride ND 1.00 1 09/18/201517:55 WG816019 FSC
Chlorobenzene ND 1.00 1 09/18/201517:55 WG816019
Chlorodibromomethane ND 1.00 1 09/18/201517:55 WG816019
Chloroethane ND 5.00 1 09/18/201517:55 WG816019
2-Chloroethyl vinyl ether ND 50.0 1 09/18/201517:55 WG816019
Chloroform ND 5.00 1 09/18/201517:55 WG816019
Chloromethane ND 2.50 1 09/18/201517:55 WG816019
2-Chlorotoluene ND 1.00 1 09/18/201517:55 WG816019
4-Chlorotoluene ND 1.00 1 09/18/201517:55 WG816019
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/18/201517:55 WG816019
1,2-Dibromoethane ND 1.00 1 09/18/201517:55 WG816019
Dibromomethane ND 1.00 1 09/18/201517:55 WG816019
1,2-Dichlo robe nzene ND 1.00 1 09/18/201517:55 WG816019
1,3-Dichlorobenzene ND 1.00 1 09/18/201517:55 WG816019
1,4-Dichlorobenzene ND 1.00 1 09/18/201517:55 WG816019
Dichlorodifluoromethane ND 5.00 1 09/18/201517:55 WG816019
1,1-Dichloroethane ND 1.00 1 09/18/201517:55 WG816019
1,2-Dichloroethane ND 1.00 1 09/18/201517:55 WG816019
1,1-Dichloroethene ND 1.00 1 09/18/201517:55 WG816019
cis-1,2-Dichloroethene 34.1 1.00 1 09/18/201517:55 WG816019
trans-1,2-Dichloroethene 4.65 1.00 1 09/18/201517:55 WG816019
1,2-Dichloropropane ND 1.00 1 09/18/201517:55 WG816019
1,1-Dichloropropene ND 1.00 1 09/18/201517:55 WG816019
1,3-Dichloropropane ND 1.00 1 09/18/201517:55 WG816019
cis-1,3-Dichloropropene ND 1.00 1 09/18/201517:55 WG816019
trans-13-Dichloropropene ND 1.00 1 09/18/201517:55 WG816019
2,2-Dichloropropane ND 1.00 1 09/18/201517:55 WG816019
Di-isopropyl ether ND 1.00 1 09/18/201517:55 WG816019
Ethylbenzene ND 1.00 1 09/18/201517:55 WG816019
Hexachloro-1,3-butadiene ND 1.00 1 09/18/201517:55 WG816019
Isopropylbenzene ND 1.00 1 09/18/201517:55 WG816019
p-Isopropyltoluene ND 1.00 1 09/18/201517:55 WG816019
2-Butanone(MEK) 12.9 10.0 1 09/18/201517:55 WG816019
Methylene Chloride ND 5.00 1 09/18/201517:55 WG816019
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/18/201517:55 WG816019
Methyl tert-butyl ether ND 1.00 1 09/18/201517:55 WG816019
Naphthalene ND 5.00 1 09/18/201517:55 WG816019
n-Propylbenzene ND 1.00 1 09/18/201517:55 WG816019
Styrene ND 1.00 1 09/18/201517:55 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 8 of 32

RW-3 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 10:45 L788744
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/18/201517:55 WG816019 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/18/201517:55 WG816019
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/18/201517:55 WG816019 F
Tetrachloroethene 3.56 1.00 1 09/18/201517:55 WG816019
Toluene 4790 250 50 09/21/201516:54 WG816580
1,2,3-Trichlorobenzene ND 1.00 1 09/18/201517:55 WG816019 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/18/201517:55 WG816019
1,1,1-Trichloroethane ND 1.00 1 09/18/201517:55 WG816019
1,1,2-Trichloroethane ND 1.00 1 09/18/201517:55 WG816019
Trichloroethene 2.03 1.00 1 09/18/201517:55 WG816019
Trichlorofluoromethane ND 5.00 1 09/18/201517:55 WG816019 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/18/201517:55 WG816019
1,2,4-Trimethylbenzene ND 1.00 1 09/18/201517:55 WG816019 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/18/201517:55 WG816019 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/18/201517:55 WG816019
Vinyl chloride 5.27 1.00 1 09/18/201517:55 WG816019 FAI
Xylenes,Total ND 3.00 1 09/18/201517:55 WG816019
(S)Toluene-d8 105 90.0-115 091181201517:55 WG816019 F
(S)Dibromofluoromethone 94.6 79.0-121 091181201517:55 WG816019
(S)4-Bromofluorobenzene 105 80.1-120 091181201517:55 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 9 of 32

MW-5 SAMPLE RESULTS - 03 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 10:52 L788744
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/1 ug/I date/time
FTc
TOC(Total Organic Carbon) 4740000 100000 100 09/18/2015 06:21 WG815629
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone 212 50.0 1 09/18/201518:13 WG816019
Acrolein ND 50.0 1 09/18/201518:13 WG816019
Acrylonitrile ND 10.0 1 09/18/201518:13 WG816019
Benzene ND 1.00 1 09/18/201518:13 WG816019
Bromobenzene ND 1.00 1 09/18/201518:13 WG816019 6
QC
Bromodichloromethane ND 1.00 1 09/18/201518:13 WG816019
Bromoform ND 1.00 1 09/18/201518:13 WG816019
Bromomethane ND 5.00 1 09/18/201518:13 WG816019 q
n-Butylbenzene ND 1.00 1 09/18/201518:13 WG816019
sec-Butylbenzene ND 1.00 1 09/18/201518:13 WG816019 FAI
tert-Butylbenzene ND 1.00 1 09/18/201518:13 WG816019
Carbon tetrachloride ND 1.00 1 09/18/201518:13 WG816019 FSC
Chlorobenzene ND 1.00 1 09/18/201518:13 WG816019
Chlorodibromomethane ND 1.00 1 09/18/201518:13 WG816019
Chloroethane ND 5.00 1 09/18/201518:13 WG816019
2-Chloroethyl vinyl ether ND 50.0 1 09/18/201518:13 WG816019
Chloroform ND 5.00 1 09/18/201518:13 WG816019
Chloromethane ND 2.50 1 09/18/201518:13 WG816019
2-Chlorotoluene ND 1.00 1 09/18/201518:13 WG816019
4-Chlorotoluene ND 1.00 1 09/18/201518:13 WG816019
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/18/201518:13 WG816019
1,2-Dibromoethane ND 1.00 1 09/18/201518:13 WG816019
Dibromomethane ND 1.00 1 09/18/201518:13 WG816019
1,2-Dichlo robe nzene ND 1.00 1 09/18/201518:13 WG816019
1,3-Dichlorobenzene ND 1.00 1 09/18/201518:13 WG816019
1,4-Dichlorobenzene ND 1.00 1 09/18/201518:13 WG816019
Dichlorodifluoromethane ND 5.00 1 09/18/201518:13 WG816019
1,1-Dichloroethane ND 1.00 1 09/18/201518:13 WG816019
1,2-Dichloroethane ND 1.00 1 09/18/201518:13 WG816019
1,1-Dichloroethene ND 1.00 1 09/18/201518:13 WG816019
cis-1,2-Dichloroethene 364 10.0 10 09/21/201517:14 WG816580
trans-1,2-Dichloroethene 3.42 1.00 1 09/18/201518:13 WG816019
1,2-Dichloropropane ND 1.00 1 09/18/201518:13 WG816019
1,1-Dichloropropene ND 1.00 1 09/18/201518:13 WG816019
1,3-Dichloropropane ND 1.00 1 09/18/201518:13 WG816019
cis-1,3-Dichloropropene ND 1.00 1 09/18/201518:13 WG816019
trans-13-Dichloropropene ND 1.00 1 09/18/201518:13 WG816019
2,2-Dichloropropane ND 1.00 1 09/18/201518:13 WG816019
Di-isopropyl ether ND 1.00 1 09/18/201518:13 WG816019
Ethylbenzene ND 1.00 1 09/18/201518:13 WG816019
Hexachloro-1,3-butadiene ND 1.00 1 09/18/201518:13 WG816019
Isopropylbenzene ND 1.00 1 09/18/201518:13 WG816019
p-Isopropyltoluene ND 1.00 1 09/18/201518:13 WG816019
2-Butanone(MEK) 129 10.0 1 09/18/201518:13 WG816019
Methylene Chloride ND 5.00 1 09/18/201518:13 WG816019
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/18/201518:13 WG816019
Methyl tert-butyl ether ND 1.00 1 09/18/201518:13 WG816019
Naphthalene ND 5.00 1 09/18/201518:13 WG816019
n-Propylbenzene ND 1.00 1 09/18/201518:13 WG816019
Styrene ND 1.00 1 09/18/201518:13 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 10 of 32

MW-5 SAMPLE RESULTS - 03 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 10:52 L788744
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/18/201518:13 WG816019 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/18/201518:13 WG816019
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/18/201518:13 WG816019 F
Tetrachloroethene 45.7 1.00 1 09/18/201518:13 WG816019
Toluene 150 5.00 1 09/18/201518:13 WG816019
1,2,3-Trichlorobenzene ND 1.00 1 09/18/201518:13 WG816019 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/18/201518:13 WG816019
1,1,1-Trichloroethane ND 1.00 1 09/18/201518:13 WG816019
1,1,2-Trichloroethane ND 1.00 1 09/18/201518:13 WG816019
Trichloroethene 16.5 1.00 1 09/18/201518:13 WG816019
Trichlorofluoromethane ND 5.00 1 09/18/201518:13 WG816019 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/18/201518:13 WG816019
1,2,4-Trimethylbenzene ND 1.00 1 09/18/201518:13 WG816019 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/18/201518:13 WG816019 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/18/201518:13 WG816019
Vinyl chloride 21.1 1.00 1 09/18/201518:13 WG816019 FAI
Xylenes,Total ND 3.00 1 09/18/201518:13 WG816019
(S)Toluene-d8 98.9 90.0-115 091181201518:13 WG816019 FSC
(S)Dibromofluoromethone 94.0 79.0-121 091181201518:13 WG816019
(S)4-Bromofluorobenzene 106 80.1-120 091181201518:13 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 11 of 32

MW-6 SAMPLE RESULTS - 04 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 10:15 L788744
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 3250 1000 1 09/18/2015 00:18 WG815629
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/18/201518:31 WG816019
Acrolein ND 50.0 1 09/18/201518:31 WG816019
Acrylonitrile ND 10.0 1 09/18/201518:31 WG816019
Benzene ND 1.00 1 09/18/201518:31 WG816019
Bromobenzene ND 1.00 1 09/18/201518:31 WG816019 6
QC
Bromodichloromethane ND 1.00 1 09/18/201518:31 WG816019
Bromoform ND 1.00 1 09/18/201518:31 WG816019
Bromomethane ND 5.00 1 09/18/201518:31 WG816019 q
n-Butylbenzene ND 1.00 1 09/18/201518:31 WG816019
sec-Butylbenzene ND 1.00 1 09/18/201518:31 WG816019 FAI
tert-Butylbenzene ND 1.00 1 09/18/201518:31 WG816019
Carbon tetrachloride ND 1.00 1 09/18/201518:31 WG816019 FSC
Chlorobenzene ND 1.00 1 09/18/201518:31 WG816019
Chlorodibromomethane ND 1.00 1 09/18/201518:31 WG816019
Chloroethane ND 5.00 1 09/18/201518:31 WG816019
2-Chloroethyl vinyl ether ND 50.0 1 09/18/201518:31 WG816019
Chloroform ND 5.00 1 09/18/201518:31 WG816019
Chloromethane ND 2.50 1 09/18/201518:31 WG816019
2-Chlorotoluene ND 1.00 1 09/18/201518:31 WG816019
4-Chlorotoluene ND 1.00 1 09/18/201518:31 WG816019
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/18/201518:31 WG816019
1,2-Dibromoethane ND 1.00 1 09/18/201518:31 WG816019
Dibromomethane ND 1.00 1 09/18/201518:31 WG816019
1,2-Dichlo robe nzene ND 1.00 1 09/18/201518:31 WG816019
1,3-Dichlorobenzene ND 1.00 1 09/18/201518:31 WG816019
1,4-Dichlorobenzene ND 1.00 1 09/18/201518:31 WG816019
Dichlorodifluoromethane ND 5.00 1 09/18/201518:31 WG816019
1,1-Dichloroethane ND 1.00 1 09/18/201518:31 WG816019
1,2-Dichloroethane ND 1.00 1 09/18/201518:31 WG816019
1,1-Dichloroethene ND 1.00 1 09/18/201518:31 WG816019
cis-1,2-Dichloroethene 768 50.0 50 09/21/201517:34 WG816580
trans-1,2-Dichloroethene 2.93 1.00 1 09/18/201518:31 WG816019
1,2-Dichloropropane ND 1.00 1 09/18/201518:31 WG816019
1,1-Dichloropropene ND 1.00 1 09/18/201518:31 WG816019
1,3-Dichloropropane ND 1.00 1 09/18/201518:31 WG816019
cis-1,3-Dichloropropene ND 1.00 1 09/18/201518:31 WG816019
trans-13-Dichloropropene ND 1.00 1 09/18/201518:31 WG816019
2,2-Dichloropropane ND 1.00 1 09/18/201518:31 WG816019
Di-isopropyl ether ND 1.00 1 09/18/201518:31 WG816019
Ethylbenzene ND 1.00 1 09/18/201518:31 WG816019
Hexachloro-1,3-butadiene ND 1.00 1 09/18/201518:31 WG816019
Isopropylbenzene ND 1.00 1 09/18/201518:31 WG816019
p-Isopropyltoluene ND 1.00 1 09/18/201518:31 WG816019
2-Butanone(MEK) ND 10.0 1 09/18/201518:31 WG816019
Methylene Chloride ND 5.00 1 09/18/201518:31 WG816019
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/18/201518:31 WG816019
Methyl tert-butyl ether ND 1.00 1 09/18/201518:31 WG816019
Naphthalene ND 5.00 1 09/18/201518:31 WG816019
n-Propylbenzene ND 1.00 1 09/18/201518:31 WG816019
Styrene ND 1.00 1 09/18/201518:31 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 12 of 32

MW-6 SAMPLE RESULTS - 04 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 10:15 L788744
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/18/201518:31 WG816019 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/18/201518:31 WG816019
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/18/201518:31 WG816019 F
Tetrachloroethene 1600 50.0 50 09/21/201517:34 WG816580
Toluene ND 5.00 1 09/18/201518:31 WG816019
1,2,3-Trichlorobenzene ND 1.00 1 09/18/201518:31 WG816019 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/18/201518:31 WG816019
1,1,1-Trichloroethane ND 1.00 1 09/18/201518:31 WG816019
1,1,2-Trichloroethane ND 1.00 1 09/18/201518:31 WG816019
Trichloroethene 62.9 1.00 1 09/18/201518:31 WG816019
Trichlorofluoromethane ND 5.00 1 09/18/201518:31 WG816019 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/18/201518:31 WG816019
1,2,4-Trimethylbenzene ND 1.00 1 09/18/201518:31 WG816019 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/18/201518:31 WG816019 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/18/201518:31 WG816019
Vinyl chloride 21.9 1.00 1 09/18/201518:31 WG816019 FAI
Xylenes,Total ND 3.00 1 09/18/201518:31 WG816019
(S)Toluene-d8 104 90.0-115 09118120151831 WG816019 FSC
(S)Dibromofluoromethone 92.9 79.0-121 091181201518:31 WG816019
(S)4-Bromofluorobenzene 107 80.1-120 091181201518:31 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 13 of 32

MW-12 SAMPLE RESULTS - 05 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 11:28 L788744
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 69500 20000 20 09/18/2015 00:29 WG815629
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/18/201518:49 WG816019
Acrolein ND 50.0 1 09/18/201518:49 WG816019
Acrylonitrile ND 10.0 1 09/18/201518:49 WG816019
Benzene ND 1.00 1 09/18/201518:49 WG816019
Bromobenzene ND 1.00 1 09/18/201518:49 WG816019 6
QC
Bromodichloromethane ND 1.00 1 09/18/201518:49 WG816019
Bromoform ND 1.00 1 09/18/201518:49 WG816019
Bromomethane ND 5.00 1 09/18/201518:49 WG816019 q
n-Butylbenzene ND 1.00 1 09/18/201518:49 WG816019
sec-Butylbenzene ND 1.00 1 09/18/201518:49 WG816019 FAI
tert-Butylbenzene ND 1.00 1 09/18/201518:49 WG816019
Carbon tetrachloride ND 1.00 1 09/18/201518:49 WG816019 FSC
Chlorobenzene ND 1.00 1 09/18/201518:49 WG816019
Chlorodibromomethane ND 1.00 1 09/18/201518:49 WG816019
Chloroethane ND 5.00 1 09/18/201518:49 WG816019
2-Chloroethyl vinyl ether ND 50.0 1 09/18/201518:49 WG816019
Chloroform ND 5.00 1 09/18/201518:49 WG816019
Chloromethane ND 2.50 1 09/18/201518:49 WG816019
2-Chlorotoluene ND 1.00 1 09/18/201518:49 WG816019
4-Chlorotoluene ND 1.00 1 09/18/201518:49 WG816019
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/18/201518:49 WG816019
1,2-Dibromoethane ND 1.00 1 09/18/201518:49 WG816019
Dibromomethane ND 1.00 1 09/18/201518:49 WG816019
1,2-Dichlo robe nzene ND 1.00 1 09/18/201518:49 WG816019
1,3-Dichlorobenzene ND 1.00 1 09/18/201518:49 WG816019
1,4-Dichlorobenzene ND 1.00 1 09/18/201518:49 WG816019
Dichlorodifluoromethane ND 5.00 1 09/18/201518:49 WG816019
1,1-Dichloroethane ND 1.00 1 09/18/201518:49 WG816019
1,2-Dichloroethane ND 1.00 1 09/18/201518:49 WG816019
1,1-Dichloroethene ND 1.00 1 09/18/201518:49 WG816019
cis-1,2-Dichloroethene ND 1.00 1 09/23/201517:31 WG817022
trans-1,2-Dichloroethene 2.30 1.00 1 09/18/201518:49 WG816019
1,2-Dichloropropane ND 1.00 1 09/18/201518:49 WG816019
1,1-Dichloropropene ND 1.00 1 09/18/201518:49 WG816019
1,3-Dichloropropane ND 1.00 1 09/18/201518:49 WG816019
cis-1,3-Dichloropropene ND 1.00 1 09/18/201518:49 WG816019
trans-13-Dichloropropene ND 1.00 1 09/18/201518:49 WG816019
2,2-Dichloropropane ND 1.00 1 09/18/201518:49 WG816019
Di-isopropyl ether ND 1.00 1 09/18/201518:49 WG816019
Ethylbenzene ND 1.00 1 09/18/201518:49 WG816019
Hexachloro-1,3-butadiene ND 1.00 1 09/18/201518:49 WG816019
Isopropylbenzene ND 1.00 1 09/18/201518:49 WG816019
p-Isopropyltoluene ND 1.00 1 09/18/201518:49 WG816019
2-Butanone(MEK) 31.4 10.0 1 09/18/201518:49 WG816019
Methylene Chloride ND 5.00 1 09/18/201518:49 WG816019
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/18/201518:49 WG816019
Methyl tert-butyl ether ND 1.00 1 09/18/201518:49 WG816019
Naphthalene ND 5.00 1 09/18/201518:49 WG816019
n-Propylbenzene ND 1.00 1 09/18/201518:49 WG816019
Styrene ND 1.00 1 09/18/201518:49 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-12 SAMPLE RESULTS - 05 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 11:28 L788744
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/18/201518:49 WG816019 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/18/201518:49 WG816019
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/18/201518:49 WG816019 F
Tetrachloroethene ND 1.00 1 09/23/201517:31 WG817022
Toluene 20600 2500 500 09/22/201515:21 WG816806
1,2,3-Trichlorobenzene ND 1.00 1 09/18/201518:49 WG816019 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/18/201518:49 WG816019
1,1,1-Trichloroethane ND 1.00 1 09/18/201518:49 WG816019
1,1,2-Trichloroethane ND 1.00 1 09/18/201518:49 WG816019
Trichloroethene ND 1.00 1 09/18/201518:49 WG816019
Trichlorofluoromethane ND 5.00 1 09/18/201518:49 WG816019 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/18/201518:49 WG816019
1,2,4-Trimethylbenzene ND 1.00 1 09/18/201518:49 WG816019 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/18/201518:49 WG816019 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/18/201518:49 WG816019
Vinyl chloride ND 1.00 1 09/18/201518:49 WG816019 FAI
Xylenes,Total ND 3.00 1 09/18/201518:49 WG816019
(S)Toluene-d8 105 90.0-115 091181201518.49 WG816019 FSC
(S)Dibromofluoromethone 95.5 79.0-121 091181201518:49 WG816019
(S)4-Bromofluorobenzene 99.2 80.1-120 091181201518.49 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-44 SAMPLE RESULTS - 06 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 11:30 L788744
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 1470 1000 1 09/18/2015 00:40 WG815629
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/18/201519:08 WG816019
Acrolein ND 50.0 1 09/18/201519:08 WG816019
Acrylonitrile ND 10.0 1 09/18/201519:08 WG816019
Benzene ND 1.00 1 09/18/201519:08 WG816019
Bromobenzene ND 1.00 1 09/18/201519:08 WG816019 6
QC
Bromodichloromethane ND 1.00 1 09/18/201519:08 WG816019
Bromoform ND 1.00 1 09/18/201519:08 WG816019
Bromomethane ND 5.00 1 09/18/201519:08 WG816019 q
n-Butylbenzene ND 1.00 1 09/18/201519:08 WG816019
sec-Butylbenzene ND 1.00 1 09/18/201519:08 WG816019 FAI
tert-Butylbenzene ND 1.00 1 09/18/201519:08 WG816019
Carbon tetrachloride ND 1.00 1 09/18/201519:08 WG816019 FSC
Chlorobenzene 1.85 1.00 1 09/18/201519:08 WG816019
Chlorodibromomethane ND 1.00 1 09/18/201519:08 WG816019
Chloroethane ND 5.00 1 09/18/201519:08 WG816019
2-Chloroethyl vinyl ether ND 50.0 1 09/18/201519:08 WG816019
Chloroform ND 5.00 1 09/18/201519:08 WG816019
Chloromethane ND 2.50 1 09/18/201519:08 WG816019
2-Chlorotoluene ND 1.00 1 09/18/201519:08 WG816019
4-Chlorotoluene ND 1.00 1 09/18/201519:08 WG816019
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/18/201519:08 WG816019
1,2-Dibromoethane ND 1.00 1 09/18/201519:08 WG816019
Dibromomethane ND 1.00 1 09/18/201519:08 WG816019
1,2-Dichlo robe nzene ND 1.00 1 09/18/201519:08 WG816019
1,3-Dichlorobenzene ND 1.00 1 09/18/201519:08 WG816019
1,4-Dichlorobenzene ND 1.00 1 09/18/201519:08 WG816019
Dichlorodifluoromethane ND 5.00 1 09/18/201519:08 WG816019
1,1-Dichloroethane ND 1.00 1 09/18/201519:08 WG816019
1,2-Dichloroethane ND 1.00 1 09/18/201519:08 WG816019
1,1-Dichloroethene 1.28 1.00 1 09/18/201519:08 WG816019
cis-1,2-Dichloroethene 1130 1.00 200 09/21/201518:14 WG816580
trans-1,2-Dichloroethene 7.42 1.00 1 09/18/201519:08 WG816019
1,2-Dichloropropane ND 1.00 1 09/18/201519:08 WG816019
1,1-Dichloropropene ND 1.00 1 09/18/201519:08 WG816019
1,3-Dichloropropane ND 1.00 1 09/18/201519:08 WG816019
cis-1,3-Dichloropropene ND 1.00 1 09/18/201519:08 WG816019
trans-13-Dichloropropene ND 1.00 1 09/18/201519:08 WG816019
2,2-Dichloropropane ND 1.00 1 09/18/201519:08 WG816019
Di-isopropyl ether ND 1.00 1 09/18/201519:08 WG816019
Ethylbenzene ND 1.00 1 09/18/201519:08 WG816019
Hexachloro-1,3-butadiene ND 1.00 1 09/18/201519:08 WG816019
Isopropylbenzene ND 1.00 1 09/18/201519:08 WG816019
p-Isopropyltoluene ND 1.00 1 09/18/201519:08 WG816019
2-Butanone(MEK) ND 10.0 1 09/18/201519:08 WG816019
Methylene Chloride ND 5.00 1 09/18/201519:08 WG816019
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/18/201519:08 WG816019
Methyl tert-butyl ether ND 1.00 1 09/18/201519:08 WG816019
Naphthalene ND 5.00 1 09/18/201519:08 WG816019
n-Propylbenzene ND 1.00 1 09/18/201519:08 WG816019
Styrene ND 1.00 1 09/18/201519:08 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-44 SAMPLE RESULTS - 06 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 11:30 L788744
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane 1.95 1.00 1 09/18/201519:08 WG816019 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/18/201519:08 WG816019
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/18/201519:08 WG816019 F
Tetrachloroethene 6550 1.00 200 09/21/201518:14 WG816580
Toluene ND 5.00 1 09/23/2015 21:53 WG817022
1,2,3-Trichlorobenzene ND 1.00 1 09/18/201519:08 WG816019 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/18/201519:08 WG816019
1,1,1-Trichloroethane ND 1.00 1 09/18/201519:08 WG816019
1,1,2-Trichloroethane ND 1.00 1 09/18/201519:08 WG816019
Trichloroethene 348 1.00 200 09/21/201518:14 WG816580
Trichlorofluoromethane ND 5.00 1 09/18/201519:08 WG816019 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/18/201519:08 WG816019
1,2,4-Trimethylbenzene ND 1.00 1 09/18/201519:08 WG816019 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/18/201519:08 WG816019 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/18/201519:08 WG816019
Vinyl chloride 55.1 1.00 1 09/18/201519:08 WG816019 FAI
Xylenes,Total ND 3.00 1 09/18/201519:08 WG816019
(S)Toluene-d8 101 90.0-115 091181201519:08 WG816019 F
(S)Dibromofluoromethone 93.1 79.0-121 091181201519:08 WG816019
(S)4-Bromofluorobenzene 104 80.1-120 091181201519:08 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 17 of 32

IW-2 SAMPLE RESULTS - 07 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 10:16 L788744
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 35700 20000 20 09/18/2015 00:51 WG815629
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/18/201519:26 WG816019
Acrolein ND 50.0 1 09/18/201519:26 WG816019
Acrylonitrile ND 10.0 1 09/18/201519:26 WG816019
Benzene ND 1.00 1 09/18/201519:26 WG816019
Bromobenzene ND 1.00 1 09/18/201519:26 WG816019 6
QC
Bromodichloromethane ND 1.00 1 09/18/201519:26 WG816019
Bromoform ND 1.00 1 09/18/201519:26 WG816019
Bromomethane ND 5.00 1 09/18/201519:26 WG816019 q
n-Butylbenzene ND 1.00 1 09/18/201519:26 WG816019
sec-Butylbenzene ND 1.00 1 09/18/201519:26 WG816019 FAI
tert-Butylbenzene ND 1.00 1 09/18/201519:26 WG816019
Carbon tetrachloride ND 1.00 1 09/18/201519:26 WG816019 FSC
Chlorobenzene ND 1.00 1 09/18/201519:26 WG816019
Chlorodibromomethane ND 1.00 1 09/18/201519:26 WG816019
Chloroethane ND 5.00 1 09/18/201519:26 WG816019
2-Chloroethyl vinyl ether ND 50.0 1 09/18/201519:26 WG816019
Chloroform ND 5.00 1 09/18/201519:26 WG816019
Chloromethane ND 2.50 1 09/18/201519:26 WG816019
2-Chlorotoluene ND 1.00 1 09/18/201519:26 WG816019
4-Chlorotoluene ND 1.00 1 09/18/201519:26 WG816019
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/18/201519:26 WG816019
1,2-Dibromoethane ND 1.00 1 09/18/201519:26 WG816019
Dibromomethane ND 1.00 1 09/18/201519:26 WG816019
1,2-Dichlo robe nzene ND 1.00 1 09/18/201519:26 WG816019
1,3-Dichlorobenzene ND 1.00 1 09/18/201519:26 WG816019
1,4-Dichlorobenzene ND 1.00 1 09/18/201519:26 WG816019
Dichlorodifluoromethane ND 5.00 1 09/18/201519:26 WG816019
1,1-Dichloroethane ND 1.00 1 09/18/201519:26 WG816019
1,2-Dichloroethane ND 1.00 1 09/18/201519:26 WG816019
1,1-Dichloroethene ND 1.00 1 09/18/201519:26 WG816019
cis-1,2-Dichloroethene 1.07 1.00 1 09/23/201517:52 WG817022
trans-1,2-Dichloroethene ND 1.00 1 09/18/201519:26 WG816019
1,2-Dichloropropane ND 1.00 1 09/18/201519:26 WG816019
1,1-Dichloropropene ND 1.00 1 09/18/201519:26 WG816019
1,3-Dichloropropane ND 1.00 1 09/18/201519:26 WG816019
cis-1,3-Dichloropropene ND 1.00 1 09/18/201519:26 WG816019
trans-13-Dichloropropene ND 1.00 1 09/18/201519:26 WG816019
2,2-Dichloropropane ND 1.00 1 09/18/201519:26 WG816019
Di-isopropyl ether ND 1.00 1 09/18/201519:26 WG816019
Ethylbenzene ND 1.00 1 09/18/201519:26 WG816019
Hexachloro-1,3-butadiene ND 1.00 1 09/18/201519:26 WG816019
Isopropylbenzene ND 1.00 1 09/18/201519:26 WG816019
p-Isopropyltoluene ND 1.00 1 09/18/201519:26 WG816019
2-Butanone(MEK) 27.1 10.0 1 09/18/201519:26 WG816019
Methylene Chloride ND 5.00 1 09/18/201519:26 WG816019
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/18/201519:26 WG816019
Methyl tert-butyl ether ND 1.00 1 09/18/201519:26 WG816019
Naphthalene ND 5.00 1 09/18/201519:26 WG816019
n-Propylbenzene ND 1.00 1 09/18/201519:26 WG816019
Styrene ND 1.00 1 09/18/201519:26 WG816019
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 18 of 32

IW-2 SAMPLE RESULTS - 07 ONE LAB.NATIONWIDE.
Collected date/time: 09/14/15 10:16 L788744
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/18/201519:26 WG816019 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/18/201519:26 WG816019
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/18/201519:26 WG816019 F
Tetrachloroethene 1.66 1.00 1 09/23/201517:52 WG817022
Toluene 45800 5000 1000 09/22/201515:39 WG816806
1,2,3-Trichlorobenzene ND 1.00 1 09/18/201519:26 WG816019 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/18/201519:26 WG816019
1,1,1-Trichloroethane ND 1.00 1 09/18/201519:26 WG816019
1,1,2-Trichloroethane ND 1.00 1 09/18/201519:26 WG816019
Trichloroethene ND 1.00 1 09/18/201519:26 WG816019
Trichlorofluoromethane ND 5.00 1 09/18/201519:26 WG816019 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/18/201519:26 WG816019
1,2,4-Trimethylbenzene ND 1.00 1 09/18/201519:26 WG816019 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/18/201519:26 WG816019 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/18/201519:26 WG816019
Vinyl chloride ND 1.00 1 09/18/201519:26 WG816019 FAI
Xylenes,Total ND 3.00 1 09/18/201519:26 WG816019
(S)Toluene-d8 109 90.0-115 091181201519:26 WG816019 F
(S)Toluene-d8 103 90.0-115 09123120151752 WG817022
(S)Dibromof/uoromethone 97.4 79.0-121 09/23/201517.52 WG817022
(S)Dibromofluoromethone 93.4 79.0-121 091181201519:26 WG816019
(S)4-Bromof/uorobenzene 106 80.1-120 091181201519:26 WG816019
(S)4-Bromofluorobenzene 101 80.1-120 09123120151752 WG817022
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG815629 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Wet Chemistry by Method 9060A L788744-01,02,03,04,05,06,07
Method Blank (MB) FP1(MB)09/17/1517:58
MB Result MB Qualifier MB RDL
FT
Analyte mg/I mg/ICTOC ND 1.00
rsS
L788679-01 Original Sample (OS) • Duplicate (DUP)
(OS)09/17/1519:39•(DUP)09/17/15 19:51 4Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
s
Analyte mg/I mg/I % % _ Sr
TOC 3.39 3.42 1 0.881 20
L788728-07 Original Sample (OS) • Duplicate (DUP) 7
(OS)09/17/15 22:57•(DUP)09/17/15 23:09 GI
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/I mg/I % % $AI
TOC 3.95 3.94 1 0.253 20
FSC
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)09/17/1518:52•(LCSD)09/17/1519:07
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
TOC 75.0 77.4 77.3 103 103 85.0-115 0.0646 20
L788679-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)09/17/15 20:02•(MS)09/17/15 20:18•(MSD)09/17/15 20:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % %
TOC 50.0 3.49 54.4 53.2 102 99.4 1 80.0-120 2.30 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 20 of 32

WG816019 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-01,02,03,04,05,06,07
Method Blank (MB) FP1(MB)09/18/1512:20
MB Result MB Qualifier MB RDL
z
Analyte mg/I mg/I _ TC
Acetone ND 0.0500
Acrolein ND 0.0500 FSS
Acrylonitrile ND 0.0100
Benzene ND 0.00100 [Cn]
Bromobenzene ND 0.00100
Bromodichloromethane ND 0.00100
Bromoform ND 0.00100 FSr
Bromomethane ND 0.00500
n-Butylbenzene ND 0.00100
sec-Butyl benzene ND 0.00100
tert-Butyl benzene ND 0.00100
Carbon tetrachloride ND 0.00100 7G1
Chlorobenzene ND 0.00100
Chlorodibromomethane ND 0.00100
Chloroethane ND 0.00500 FAI
2-Chloroethyl vinyl ether ND 0.0500
Chloroform ND 0.00500 FSC
Chloromethane ND 0.00250
2-Chlorotoluene ND 0.00100
4-Chlorotoluene ND 0.00100
1,2-Dibromo-3-Chloropropane ND 0.00500
1,2-Dibromoethane ND 0.00100
Dibromomethane ND 0.00100
1,2-Dichlorobenzene ND 0.00100
1,3-Dichlorobenzene ND 0.00100
1,4-Dichlorobenzene ND 0.00100
Dichlorodifluoromethane ND 0.00500
1,1-Dichloroethane ND 0.00100
1,2-Dichloroethane ND 0.00100
1,1-Dichloroethene ND 0.00100
cis-1,2-Dichloroethene ND 0.00100
trans-1,2-Dichloroethene ND 0.00100
1,2-Dichloropropane ND 0.00100
1,1-Dichloropropene ND 0.00100
1,3-Dichloropropane ND 0.00100
cis-1,3-Dichloropropene ND 0.00100
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816019 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-01,02,03,04,05,06,07
Method Blank (MB) FP1(MB)09/18/1512:20
MB Result MB Qualifier MB RDL
z
Analyte mg/I mg/I _ TC
trans-1,3-Dichloropropene ND 0.00100
2,2-Dichloropropane ND 0.00100 FSS
Di-isopropyl ether ND 0.00100
Ethylbenzene ND 0.00100 [Cn]
Hexachloro-1,3-butadiene ND 0.00100
Isopropylbenzene ND 0.00100
p-Isopropyltoluene ND 0.00100 FSr
2-Butanone(MEK) ND 0.0100
Methylene Chloride ND 0.00500
4-Methyl-2-pentanone(MIBK) ND 0.0100
Methyl tert-butyl ether ND 0.00100
Naphthalene ND 0.00500 GI
n-Propylbenzene ND 0.00100
Styrene ND 0.00100 FAI
1,1,1,2-Tetrachloroethane ND 0.00100
1,1,2,2-Tetrachloroethane ND 0.00100
Tetrachloroethene ND 0.00100 FSC
Toluene ND 0.00500
1,1,2-Trichlorotrifluoroethane ND 0.00100
1,2,3-Trichlorobenzene ND 0.00100
1,2,4-Trichlorobenzene ND 0.00100
1,1,1-Trichloroethane ND 0.00100
1,1,2-Trichloroethane ND 0.00100
Trichloroethene ND 0.00100
Trichlorofluoromethane ND 0.00500
1,2,3-Trichloropropane ND 0.00250
1,2,3-Trimethylbenzene ND 0.00100
1,2,4-Trim ethyl benzene ND 0.00100
1,3,5-Trimethylbenzene ND 0.00100
Vinyl chloride ND 0.00100
Xylenes,Total ND 0.00300
(S)Toluene-d8 101 90.0-115
(S)Dibromofluoromethane 93.8 79.0-121
(S)4-Bromofluorobenzene 106 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816019 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-01,02,03,04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1
(LCS)09/18/1510:30•(LCSD)09/18/1510:49
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits FTC
Analyte mg/I mg/I mg/I % % % % %
Acetone 0.125 0.104 0.106 83.4 84.8 28.7-175 1.67 20.9
Acrolein 0.125 0.109 0.107 87.4 85.6 40.4-172 2.12 20 FSS
Acrylonitrile 0.125 0.112 0.110 89.5 88.2 58.2-145 1.45 20
Benzene 0.0250 0.0212 0.0213 84.8 85.2 73.0-122 0.580 20 [Cn]
Bromobenzene 0.0250 0.0228 0.0228 91.1 91.3 81.5-115 0.310 20
Bromodichloromethane 0.0250 0.0237 0.0233 94.6 93.2 75.5-121 1.48 20
Bromoform 0.0250 0.0248 0.0244 99.4 97.5 71.5-131 1.88 20 FSr
Bromomethane 0.0250 0.0194 0.0192 77.5 76.7 22.4-187 1.03 20
n-Butylbenzene 0.0250 0.0235 0.0234 93.9 93.8 75.9-134 0.160 20
sec-Butyl benzene 0.0250 0.0235 0.0241 94.2 96.2 80.6-126 2.14 20
tert-Butyl benzene 0.0250 0.0240 0.0244 95.8 97.4 79.3-127 1.68 20
Carbon tetrachloride 0.0250 0.0221 0.0230 88.5 92.0 70.9-129 3.85 20 7G1
Chlorobenzene 0.0250 0.0237 0.0237 94.7 94.8 79.7-122 0.110 20
Chlorodibromomethane 0.0250 0.0253 0.0250 101 100 78.2-124 1.10 20
Chloroethane 0.0250 0.0213 0.0211 85.3 84.5 41.2-153 0.920 20 FAI
2-Chloroethyl vinyl ether 0.125 0.109 0.107 87.3 85.8 23.4-162 1.72 23.5
Chloroform 0.0250 0.0222 0.0225 89.0 90.2 73.2-125 1.32 20 FSC
Chloromethane 0.0250 0.0183 0.0186 73.3 74.2 55.8-134 1.26 20
2-Chlorotoluene 0.0250 0.0232 0.0243 92.7 97.3 76.4-125 4.91 20
4-Chlorotoluene 0.0250 0.0240 0.0241 96.0 96.5 81.5-121 0.460 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0233 0.0235 93.2 94.1 64.8-131 0.920 20
1,2-Dibromoethane 0.0250 0.0231 0.0234 92.3 93.5 79.8-122 1.31 20
Dibromomethane 0.0250 0.0235 0.0227 93.9 90.7 79.5-118 3.50 20
1,2-Dichlorobenzene 0.0250 0.0237 0.0228 94.7 91.3 84.7-118 3.62 20
1,3-Dichlorobenzene 0.0250 0.0237 0.0246 94.6 98.2 77.6-127 3.73 20
1,4-Dichlorobenzene 0.0250 0.0224 0.0220 89.6 88.1 82.2-114 1.64 20
Dichlorodifluoromethane 0.0250 0.0192 0.0198 76.8 79.3 56.0-134 3.22 20
1,1-Dichloroethane 0.0250 0.0220 0.0216 87.9 86.5 71.7-127 1.62 20
1,2-Dichloroethane 0.0250 0.0215 0.0217 86.1 86.6 65.3-126 0.660 20
1,1-Dichloroethene 0.0250 0.0212 0.0212 84.7 84.9 59.9-137 0.280 20
cis-1,2-Dichloroethene 0.0250 0.0218 0.0223 87.0 89.1 77.3-122 2.32 20
trans-1,2-Dichloroethene 0.0250 0.0213 0.0218 85.3 87.2 72.6-125 2.25 20
1,2-Dichloropropane 0.0250 0.0232 0.0229 92.7 91.5 77.4-125 1.29 20
1,1-Dichloropropene 0.0250 0.0210 0.0217 84.1 86.7 72.5-127 3.04 20
1,3-Dichloropropane 0.0250 0.0226 0.0227 90.2 90.8 80.6-115 0.580 20
cis-1,3-Dichloropropene 0.0250 0.0240 0.0234 96.0 93.4 77.7-124 2.68 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816019 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-01,02,03,04,05,06,07
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1
(LCS)09/18/1510:30•(LCSD)09/18/1510:49
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z
Analyte mg/I mg/I mg/I % % % % % TC
trans-1,3-Dichloropropene 0.0250 0.0251 0.0239 100 95.6 73.5-127 4.70 20
2,2-Dichloropropane 0.0250 0.0216 0.0223 86.3 89.3 61.3-134 3.46 20 FSS
Di-isopropyl ether 0.0250 0.0225 0.0220 90.0 88.2 65.1-135 2.00 20
Ethylbenzene 0.0250 0.0235 0.0241 94.2 96.5 80.9-121 2.43 20 [Cn]
Hexachloro-1,3-butadiene 0.0250 0.0229 0.0237 91.7 94.8 73.7-133 3.27 20
Isopropylbenzene 0.0250 0.0238 0.0240 95.3 96.1 81.6-124 0.860 20
p-Isopropyltoluene 0.0250 0.0235 0.0245 94.0 98.1 77.6-129 4.35 20 FSr
2-Butanone(MEK) 0.125 0.107 0.107 85.7 86.0 46.4-155 0.360 20
Methylene Chloride 0.0250 0.0208 0.0206 83.0 82.5 69.5-120 0.670 20
4-Methyl-2-pentanone(MIBK) 0.125 0.112 0.108 89.5 86.5 63.3-138 3.33 20
Methyl tert-butyl ether 0.0250 0.0226 0.0228 90.4 91.2 70.1-125 0.860 20
Naphthalene 0.0250 0.0227 0.0227 90.9 91.0 69.7-134 0.0700 20 7G1
n-Propylbenzene 0.0250 0.0231 0.0235 92.4 94.0 81.9-122 1.69 20
Styrene 0.0250 0.0246 0.0247 98.2 98.7 79.9-124 0.470 20 FAI
1,1,1,2-Tetrachloroethane 0.0250 0.0247 0.0250 98.9 99.8 78.5-125 0.900 20
1,1,2,2-Tetrachloroethane 0.0250 0.0232 0.0228 93.0 91.1 79.3-123 2.08 20
Tetrachloroethene 0.0250 0.0234 0.0238 93.6 95.4 73.5-130 1.95 20 FSC
Toluene 0.0250 0.0229 0.0213 91.4 85.2 77.9-116 6.99 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0211 0.0227 84.6 91.0 62.0-141 7.28 20
1,2,3-Trichlorobenzene 0.0250 0.0228 0.0227 91.1 90.8 75.7-134 0.250 20
1,2,4-Trichlorobenzene 0.0250 0.0234 0.0235 93.5 94.0 76.1-136 0.450 20
1,1,1-Trichloroethane 0.0250 0.0222 0.0225 88.9 90.1 71.1-129 1.38 20
1,1,2-Trichloroethane 0.0250 0.0239 0.0241 95.6 96.3 81.6-120 0.790 20
Trichloroethene 0.0250 0.0234 0.0234 93.7 93.5 79.5-121 0.160 20
Trichlorofluoromethane 0.0250 0.0211 0.0213 84.6 85.2 49.1-157 0.770 20
1,2,3-Trichloropropane 0.0250 0.0242 0.0239 96.9 95.5 74.9-124 1.45 20
1,2,3-Trimethylbenzene 0.0250 0.0233 0.0226 93.1 90.4 79.9-118 2.94 20
1,2,4-Trim ethyl benzene 0.0250 0.0230 0.0239 92.2 95.7 79.0-122 3.68 20
1,3,5-Trimethylbenzene 0.0250 0.0238 0.0246 95.2 98.2 81.0-123 3.13 20
Vinyl chloride 0.0250 0.0203 0.0204 81.2 81.7 61.5-134 0.710 20
Xylenes,Total 0.0750 0.0711 0.0710 94.8 94.7 79.2-122 0.0800 20
(S)Toluene-d8 104 101 90.0-115
(S)Dibromofluoromethane 93.4 94.4 79.0-121
(S)4-Bromofluorobenzene 103 101 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816019 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-01,02,03,04,05,06,07
L788728-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/18/1513:57•(MS)09/18/1514:16•(MSD)09/18/1514:34
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits FTC
Analyte mg/I mg/I mg/I mg/I % % % % %
Acetone 0.125 0.000843 0.0562 0.0520 44.2 40.9 1 25.0-156 7.70 21.5
Acrolein 0.125 ND 0.132 0.136 105 109 1 34.0-194 2.90 21.5 FSS
Acrylonitrile 0.125 ND 0.129 0.123 103 98.1 1 55.9-161 5.35 20
Benzene 0.0250 ND 0.0212 0.0209 84.7 83.5 1 58.6-133 1.37 20 4
Bromobenzene 0.0250 ND 0.0231 0.0220 92.4 88.1 1 70.6-125 4.75 20 Cn
Bromodichloromethane 0.0250 ND 0.0242 0.0234 96.7 93.5 1 69.2-127 3.36 20
Bromoform 0.0250 ND 0.0261 0.0247 104 98.7 1 66.3-140 5.60 20 FSr
Bromomethane 0.0250 ND 0.0198 0.0195 79.2 78.0 1 16.6-183 1.53 20.5
n-Butylbenzene 0.0250 ND 0.0230 0.0238 91.8 95.0 1 64.8-145 3.40 20
sec-Butyl benzene 0.0250 ND 0.0245 0.0240 97.8 95.9 1 66.8-139 1.93 20
tert-Butyl benzene 0.0250 ND 0.0246 0.0241 98.5 96.4 1 67.1-138 2.17 20
Carbon tetrachloride 0.0250 ND 0.0230 0.0225 92.0 89.9 1 60.6-139 2.26 20 7G1
Chlorobenzene 0.0250 ND 0.0244 0.0230 97.8 92.2 1 70.1-130 5.89 20
Chlorodibromomethane 0.0250 ND 0.0256 0.0240 102 96.0 1 71.6-132 6.57 20
Chloroethane 0.0250 ND 0.0223 0.0212 89.4 85.0 1 33.3-155 5.03 20 FAI
2-Chloroethyl vinyl ether 0.125 ND 0.000420 0.000357 0.336 0.285 1 5.00-149 J6 J6 16.3 40
Chloroform 0.0250 ND 0.0231 0.0226 92.3 90.3 1 66.1-133 2.19 20 FSC
Chloromethane 0.0250 ND 0.0190 0.0180 75.9 72.2 1 40.7-139 5.04 20
2-Chlorotoluene 0.0250 ND 0.0238 0.0231 95.3 92.4 1 66.9-134 3.01 20
4-Chlorotoluene 0.0250 ND 0.0239 0.0232 95.8 92.8 1 66.8-134 3.13 20
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.0251 0.0257 100 103 1 63.9-142 2.20 20.2
1,2-Dibromoethane 0.0250 ND 0.0244 0.0230 97.7 91.9 1 73.8-131 6.03 20
Dibromomethane 0.0250 ND 0.0240 0.0238 95.9 95.4 1 72.8-127 0.580 20
1,2-Dichlorobenzene 0.0250 ND 0.0227 0.0235 90.9 94.0 1 77.4-127 3.44 20
1,3-Dichlorobenzene 0.0250 ND 0.0243 0.0236 97.1 94.3 1 67.9-136 2.94 20
1,4-Dichlorobenzene 0.0250 ND 0.0222 0.0215 88.9 85.9 1 74.4-123 3.38 20
Dichlorodifluoromethane 0.0250 ND 0.0215 0.0204 86.1 81.6 1 42.2-146 5.41 20
1,1-Dichloroethane 0.0250 ND 0.0231 0.0217 92.5 86.9 1 64.0-134 6.20 20
1,2-Dichloroethane 0.0250 ND 0.0226 0.0227 90.4 90.9 1 60.7-132 0.570 20
1,1-Dichloroethene 0.0250 ND 0.0219 0.0212 87.6 84.7 1 48.8-144 3.36 20
cis-1,2-Dichloroethene 0.0250 ND 0.0228 0.0226 91.3 90.2 1 60.6-136 1.17 20
trans-1,2-Dichloroethene 0.0250 ND 0.0222 0.0218 88.7 87.1 1 61.0-132 1.82 20
1,2-Dichloropropane 0.0250 ND 0.0234 0.0231 93.5 92.5 1 69.7-130 1.02 20
1,1-Dichloropropene 0.0250 ND 0.0221 0.0223 88.6 89.3 1 61.5-136 0.780 20
1,3-Dichloropropane 0.0250 ND 0.0238 0.0232 95.3 92.7 1 74.3-123 2.73 20
cis-1,3-Dichloropropene 0.0250 ND 0.0235 0.0234 94.0 93.7 1 71.1-129 0.370 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816019 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-01,02,03,04,05,06,07
L788728-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/18/1513:57•(MS)09/18/1514:16•(MSD)09/18/1514:34
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % % TC
trans-1,3-Dichloropropene 0.0250 0.000718 0.0255 0.0246 99.1 95.6 1 66.3-136 3.51 20
2,2-Dichloropropane 0.0250 ND 0.0226 0.0224 90.3 89.6 1 54.9-142 0.780 20 FSS
Di-isopropyl ether 0.0250 ND 0.0229 0.0226 91.4 90.6 1 59.9-140 0.930 20
Ethylbenzene 0.0250 ND 0.0253 0.0233 101 93.3 1 62.7-136 7.94 20 4
Hexachloro-1,3-butadiene 0.0250 ND 0.0235 0.0239 94.0 95.7 1 61.1-144 1.73 20.1 Cn
Isopropylbenzene 0.0250 ND 0.0249 0.0234 99.8 93.6 1 67.4-136 6.42 20
p-Isopropyltoluene 0.0250 ND 0.0250 0.0235 100 94.0 1 62.8-143 6.29 20 FSr
2-Butanone(MEK) 0.125 ND 0.0899 0.0883 71.9 70.6 1 45.0-156 1.85 20.8
Methylene Chloride 0.0250 0.000822 0.0214 0.0212 82.3 81.3 1 61.5-125 1.15 20
4-Methyl-2-pentanone(MIBK) 0.125 ND 0.127 0.121 101 97.0 1 60.7-150 4.41 20
Methyl tert-butyl ether 0.0250 ND 0.0241 0.0232 96.3 92.8 1 61.4-136 3.68 20
Naphthalene 0.0250 0.000432 0.0244 0.0243 96.0 95.6 1 61.8-143 0.410 20 7G1
n-Propylbenzene 0.0250 ND 0.0235 0.0225 93.8 90.0 1 63.2-139 4.14 20
Styrene 0.0250 ND 0.0251 0.0239 100 95.8 1 68.2-133 4.66 20 FAI
1,1,1,2-Tetrachloroethane 0.0250 ND 0.0254 0.0237 101 94.7 1 70.5-132 6.93 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.0254 0.0237 102 94.8 1 64.9-145 7.06 20
Tetrachloroethene 0.0250 ND 0.0232 0.0228 92.7 91.1 1 57.4-141 1.70 20 FSC
Toluene 0.0250 ND 0.0220 0.0214 88.2 85.7 1 67.8-124 2.83 20
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.0231 0.0223 92.4 89.1 1 53.7-150 3.60 20
1,2,3-Trichlorobenzene 0.0250 ND 0.0233 0.0241 93.1 96.4 1 65.7-143 3.43 20
1,2,4-Trichlorobenzene 0.0250 ND 0.0235 0.0242 93.9 96.9 1 67.0-146 3.11 20
1,1,1-Trichloroethane 0.0250 ND 0.0231 0.0223 92.3 89.2 1 58.7-134 3.48 20
1,1,2-Trichloroethane 0.0250 ND 0.0248 0.0237 99.1 94.9 1 74.1-130 4.32 20
Trichloroethene 0.0250 ND 0.0231 0.0226 92.3 90.3 1 48.9-148 2.20 20
Trichlorofluoromethane 0.0250 ND 0.0214 0.0214 85.6 85.5 1 39.9-165 0.100 20
1,2,3-Trichloropropane 0.0250 ND 0.0263 0.0249 105 99.5 1 71.5-134 5.50 20
1,2,3-Trimethylbenzene 0.0250 0.000813 0.0228 0.0224 87.8 86.4 1 62.7-133 1.51 20
1,2,4-Trim ethyl benzene 0.0250 ND 0.0238 0.0225 95.4 90.1 1 60.5-137 5.66 20
1,3,5-Trimethylbenzene 0.0250 ND 0.0239 0.0232 95.7 92.6 1 67.9-134 3.27 20
Vinyl chloride 0.0250 ND 0.0208 0.0204 83.4 81.7 1 44.3-143 1.96 20
Xylenes,Total 0.0750 ND 0.0719 0.0678 95.9 90.4 1 65.6-133 5.96 20
(S Toluene-d8 104 105 90.0-115
(S)Dibromofluoromethane 96.9 95.4 79.0-121
(S)4-Bromofluorobenzene 104 102 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816580 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-01,02,03,04,06
Method Blank (MB) FP1(MB)09/21/1513:20
MB Result MB Qualifier MB RDL
FTc
Analyte mg/I mg/I
cis-1,2-Dichloroethene ND 0.00100
Tetrachloroethene ND 0.00100 FSS
Toluene ND 0.00500
Trichloroethene ND 0.00100 [Cn]
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FSr
(LCS)09/21/15 12:21•(LCSD)09/21/15 13:41
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
cis-1,2-Dichloroethene 0.0250 0.0233 0.0229 93.0 91.4 77.3-122 1.76 20
Tetrachloroethene 0.0250 0.0235 0.0229 94.1 91.6 73.5-130 2.69 20 q
Toluene 0.0250 0.0245 0.0239 98.0 95.6 77.9-116 2.48 20
Trichloroethene 0.0250 0.0243 0.0231 97.3 92.2 79.5-121 5.33 20 rAl
L789140-19 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) [Sc
(OS)09/21/15 16:14•(MS)09/21/1514:55•(MSD)09/21/1515:15
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % %
cis-1,2-Dichloroethene 0.0250 ND 0.0201 0.0193 80.3 77.2 1 60.6-136 3.93 20
Tetrachloroethene 0.0250 ND 0.0189 0.0200 75.7 80.1 1 57.4-141 5.63 20
Toluene 0.0250 ND 0.0204 0.0206 81.8 82.6 1 67.8-124 0.980 20
Trichloroethene 0.0250 ND 0.0236 0.0238 94.5 95.1 1 48.9-148 0.580 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816806 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-05,07
Method Blank (MB) FP1(MB)09/22/1510:41
MB Result MB Qualifier MB RDL
FT
Analyte mg/I mg/ICToluene ND 0.00500
IS—S]
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)09/22/1511:09•(LCSD)09/22/1511:26 [�n]
Spike Amount LCS Result LCSD Result LCS Rec LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits —
s
Analyte mg/I mg/I mg/I % % % % % Sr
Toluene 0.0250 0.0267 0.0255 107 102 77.9-116 4.77 20
�GI
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817022 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L788744-05,06,07
Method Blank (MB) FP1(MB)09/23/15 09:20
MB Result MB Qualifier MB RDL
FTc
Analyte mg/I mg/I
cis-1,2-Dichloroethene ND 0.00100
Tetrachloroethene ND 0.00100 FSS
Toluene ND 0.00500
(S Toluene-d8 100 90.0-115 4
(S)Dibromofluoromethane 96.9 79.0-121 C n
(S)4-Bromofluorobenzene 94.8 80.1-120
FSr
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)09/23/15 07:13•(LCSD)09/23/15 07:34 M
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % % Gl
cis-1,2-Dichloroethene 0.0250 0.0248 0.0243 99.0 97.3 77.3-122 1.77 20
Tetrachloroethene 0.0250 0.0313 0.0281 125 112 73.5-130 11.0 20 FAI
Toluene 0.0250 0.0269 0.0258 108 103 77.9-116 4.24 20
(S)Toluene-d8 106 104 90.0-115
9
(S)Dibromofluoromethane 93.8 94.7 79.0-121 Sc
(S)4-Bromofluorobenzene 105 98.8 80.1-120
L789416-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)09/23/1512:13•(MS)09/23/1510:29•(MSD)09/23/15 10:50
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % %
cis-1,2-Dichloroethene 0.0250 ND 0.0264 0.0250 106 99.9 1 60.6-136 5.47 20
Tetrachloroethene 0.0250 ND 0.0306 0.0297 122 119 1 57.4-141 2.91 20
Toluene 0.0250 0.000447 0.0280 0.0267 110 105 1 67.8-124 4.78 20
(S)Toluene-d8 106 104 90.0-115
(S Dibromofluoromethane 94.8 97.4 79.0-121
(S)4-Bromofluorobenzene 101 103 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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GLOSSARY OF TERMS ONE LAB.NATIONWIDE.
Abbreviations and Definitions
SDG Sample Delivery Group. FP1
MDL Method Detection Limit.
RDL Reported Detection Limit. FTc
ND,U Not detected at the Reporting Limit(or MDL where applicable).
RPD Relative Percent Difference. FS
(dry) Results are reported based on the dry weight of the sample.[this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD) 4 n
from a quality control sample.The Original Sample may not be included within the reported SDG.
(S) Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring Sr
recovery.Surrogates are not expected to be detected in all environmental media.
Rec. Recovery. RCSDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description FAI
J6 The sample matrix interfered with the ability to make any accurate determination;spike value is FSC
low.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 30 of 32

ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE.
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other
lab is as accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry.The most significant benefit to our"one location"design is the design of our laboratory campus.The model is conducive to accelerated productivity, FP1
decreasing turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
State Accreditations ITC]
Alabama 40660 Nevada TN-03-2002-34 FSS
Alaska UST-080 New Hampshire 2975
Arizona AZ0612 New Jersey—NELAP TNO02
Arkansas 88-0469 New Mexico TN00003 4
California 01157CA New York 11742 Cn
Colorado TN00003 North Carolina Env375
Conneticut PH-0197 North Carolina DW21704 FS
Florida E87487 North Carolina 2 41
Georgia NELAP North Dakota R-140
Georgia' 923 Ohio—VAP CL0069 Rc
Idaho TN00003 Oklahoma 9915
Illinois 200008 Oregon 68-TN200002
Indiana C-TN-01 Pennsylvania 68-02979979 7G�
Iowa 364 Rhode Island 221
Kansas E-10277 South Carolina 84004
Kentucky' 90010 South Dakota n/a
Kentucky 16 Tennessee14 2006
Louisiana A130792 Texas T 104704245-07-TX FSC
Maine TN0002 Texas5 LABO152
Maryland 324 Utah 6157585858
Massachusetts M-TNO03 Vermont VT2006
Michigan 9958 Virginia 109
Minnesota 047-999-395 Washington C1915
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Nebraska NE-OS-15-05
Drinking Water z Underground Storage Tanks a Aquatic Toxicity 4.Chemical/Microbiological 5.Mold n1a Accreditation not applicable
Third Party& Federal Accreditations
A21LA—ISO 17025 1461.01 AIHA 100789
Canada 1461.01 DOD 1461.01
EPA—Crypto TN00003 USDA S-67674
Our Locations
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies.If you would like assistance from one of our support offices,please
contact our main office.ESC Lab Sciences performs all testing at our central laboratory.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L788744 09/28/1517:01 31 of 32

Bililne.Oformation: Analysls{Container/l'reSc*vative Chain ofCustody Pagr—ot_
�Innl~JI - Larrinrnons Engine Bring, Inc. Project Manager -
004 Ponders Court
isl3b Ponders Court Greenvilfe,SC 29615
Greenville,SC2961.5 L-A-e3 ESC
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m�

*ESC ANALYTICAL REPORT MyESC
L-A-B S-C-I-E-N-C-E-S October 01, 2015
Bunnell - Lammons Engineering, Inc.
Sample Delivery Group: L789514
Samples Received: 09/18/2015
Project Number: J15-1022-42
Description: Andrex Industries
Site: ASHEVILLE, NC
Report To: Mr.Andy Alexander
6004 Ponders Court
Greenville, SC 29615
Entire Report Reviewed By:
Jimmy Hunt
�F Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
reproduced,except in full,without written approval of the laboratory. Where applicable,sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures:060302,060303,and 060304.
r
_ r

TABLE OF CONTENTS ONE LAB.NATIONWIDE.
'Cp:Cover Page 1 Fn
2Tc:Table of Contents 2
3Ss:Sample Summary 3
4Cn:Case Narrative 7 FS
5Sr: Sample Results 8 [Cn]
MW-7 L789514-01 8
MW-9 L789514-02 10 FSr
MW-10 L789514-03 12
MW-11 L789514-04 14 RC
MW-13 L789514-05 16
R,
MW-14 L789514-06 18
MW-15 L789514-07 20 rAl
MW-16 L789514-08 22
MW-17 L789514-09 24 FSC
MW-18 L789514-10 26
MW-20 L789514-11 28
MW-21 L789514-12 30
MW-22 L789514-13 32
MW-23 L789514-14 34
MW-24 L789514-15 36
MW-26 L789514-16 38
RW-5 L789514-17 40
RW-6 L789514-18 42
RW-7 L789514-19 44
DUPLICATE L789514-20 46
DUPLICATE B L789514-21 48
FIELD BLANK 1 L789514-22 50
6Qc:Quality Control Summary 52
Wet Chemistry by Method 9060A 52
Volatile Organic Compounds(GC/MS) by Method 8260B 53
7GI:Glossary of Terms 67
8AI:Accreditations& Locations 68
9Sc: Chain of Custody 69
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 2 of 72

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
MW-7 L789514-01 GW Benjamin P.Nisbeth 09/16/1512:34 09/18/15 09:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time FTC
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 05:29 09/25/15 05:29 MCB
Wet Chemistry by Method 9060A WG816627 1 09/22/15 20:48 09/22/15 20:48 LLS
Collected by Collected date/time Received date/time
MW-9 L789514-02 GW Benjamin P.Nisbeth 09/15/1513:20 09/18/15 09:00 4 n
Method Batch Dilution Preparation Analysis Analysis Analyst
FSrdate/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260E WG817578 1 09/25/15 05:49 09/25/15 05:49 MCB
Volatile Organic Compounds(GC/MS)by Method 8260E WG818281 50 09/29/1514:01 09/29/1514:01 MCB 6
QC
Wet Chemistry by Method 9060A WG816627 1 09/22/15 21:00 09/22/15 21:00 LLS
Collected by Collected date/time Received date/time
MW-10 L789514-03 GW Benjamin P.Nisbeth 09/15/15 09:22 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst FAI
date/time date/time
FSC
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 06:09 09/25/15 06:09 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 50 09/29/1514:21 09/29/1514:21 MCB
Wet Chemistry by Method 9060A WG816627 1 09/22/15 22:08 09/22/15 22:08 LLS
Collected by Collected date/time Received date/time
MW-11 L789514-04 GW Benjamin P.Nisbeth 09/15/1510:13 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260E WG817578 1 09/25/15 06:29 09/25/15 06:29 MCB
Volatile Organic Compounds(GC/MS)by Method 8260E WG818281 20 09/29/1514:41 09/29/1514:41 MCB
Wet Chemistry by Method 9060A WG816627 1 09/22/15 22:22 09/22/15 22:22 LLS
Collected by Collected date/time Received date/time
MW-13 L789514-05 GW Benjamin P.Nisbeth 09/15/1511:54 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 06:49 09/25/15 06:49 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 20 09/29/1515:01 09/29/1515:01 MCB
Wet Chemistry by Method 9060A WG816627 1 09/22/15 22:36 09/22/15 22:36 LLS
Collected by Collected date/time Received date/time
MW-14 L789514-06 GW Benjamin P.Nisbeth 09/15/1511:23 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 07:09 09/25/15 07:09 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 20 09/29/1515:21 09/29/1515:21 MCB
Wet Chemistry by Method 9060A WG816627 1 09/22/15 22:48 09/22/15 22:48 LLS
Collected by Collected date/time Received date/time
MW-15 L789514-07 GW Benjamin P.Nisbeth 09/16/15 09:40 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 07:29 09/25/15 07:29 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 1 09/29/1513:41 09/29/1513:41 MCB
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 3 of 72

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
MW-16 L789514-08 GW Benjamin P.Nisbeth 09/16/15 08:30 09/18/15 09:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time FTC
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 07:49 09/25/15 07:49 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 1 09/29/1515:41 09/29/1515:41 MCB
Collected by Collected date/time Received date/time
MW-17 L789514-09 GW Benjamin P.Nisbeth 09/16/1510:35 09/18/15 09:00 4 n
Method Batch Dilution Preparation Analysis Analysis Analyst
FSrdate/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260E WG817578 1 09/25/15 08:09 09/25/15 08:09 MCB
Volatile Organic Compounds(GC/MS)by Method 8260E WG818281 1 09/29/1516:01 09/29/1516:01 MCB RC
Collected by Collected date/time Received date/time F
MW-18 L789514-10 GW Benjamin P.Nisbeth 09/16/15 08:55 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst FAI
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 08:29 09/25/15 08:29 MCB FSC
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 1 09/29/1516:21 09/29/1516:21 MCB
Collected by Collected date/time Received date/time
MW-20 L789514-11 GW Benjamin P.Nisbeth 09/15/1510:50 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 08:49 09/25/15 08:49 MCB
Collected by Collected date/time Received date/time
MW-21 L789514-12 GW Benjamin P.Nisbeth 09/16/1511:20 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 09:10 09/25/15 09:10 MCB
Collected by Collected date/time Received date/time
MW-22 L789514-13 GW Benjamin P.Nisbeth 09/16/1511:30 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 09:30 09/25/15 09:30 MCB
Collected by Collected date/time Received date/time
MW-23 L789514-14 GW Benjamin P.Nisbeth 09/15/1510:32 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/15 09:50 09/25/15 09:50 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 10 09/29/1516:41 09/29/1516:41 MCB
Wet Chemistry by Method 9060A WG816627 1 09/22/15 23:12 09/22/15 23:12 LLS
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 4 of 72

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
MW-24 L789514-15 GW Benjamin P.Nisbeth 09/16/1512:02 09/18/15 09:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time FTC
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/1510:10 09/25/1510:10 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 10 09/29/1517:02 09/29/1517:02 MCB
Wet Chemistry by Method 9060A WG816627 1 09/22/15 23:34 09/22/15 23:34 LLS
Collected by Collected date/time Received date/time Cn
MW-26 L789514-16 GW Benjamin P.Nisbeth 09/16/1510:12 09/18/15 09:00
FSr
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260E WG817578 1 09/25/1510:30 09/25/1510:30 MCB 6
QC
Volatile Organic Compounds(GC/MS)by Method 8260E WG818281 1 09/29/1517:22 09/29/1517:22 MCB
Collected by Collected date/time Received date/time
RW-5 L789514-17 GW Benjamin P.Nisbeth 09/15/1512:50 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst FAI
date/time date/time
FSC
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/1510:50 09/25/1510:50 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 10 09/29/1517:42 09/29/1517:42 MCB
Wet Chemistry by Method 9060A WG816627 1 09/22/15 23:54 09/22/15 23:54 LLS
Collected by Collected date/time Received date/time
RW-6 L789514-18 GW Benjamin P.Nisbeth 09/15/15 09:30 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260E WG817578 1 09/25/1511:10 09/25/1511:10 MCB
Volatile Organic Compounds(GC/MS)by Method 8260E WG818281 20 09/29/1518:22 09/29/1518:22 MCB
Wet Chemistry by Method 9060A WG816627 1 09/23/15 00:06 09/23/15 00:06 LLS
Collected by Collected date/time Received date/time
RW-7 L789514-19 GW Benjamin P.Nisbeth 09/15/15 09:45 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817621 1 09/26/1510:07 09/26/1510:07 KLO
Volatile Organic Compounds(GC/MS)by Method 8260B WG818034 5 09/28/1511:42 09/28/1511:42 MCB
Wet Chemistry by Method 9060A WG816627 100 09/23/15 01:47 09/23/15 01:47 LLS
Collected by Collected date/time Received date/time
DUPLICATE L789514-20 GW Benjamin P.Nisbeth 09/15/15 00:00 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/1511:30 09/25/1511:30 MCB
Volatile Organic Compounds(GC/MS)by Method 8260B WG818281 20 09/29/1518:42 09/29/1518:42 MCB
Collected by Collected date/time Received date/time
DUPLICATE B L789514-21 GW Benjamin P.Nisbeth 09/15/1500:00 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817578 1 09/25/1511:50 09/25/1511:50 MCB
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 5 of 72

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
FIELD BLANK L789514-22 GW Benjamin P.Nisbeth 09/15/1509:00 09/18/1509:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time z
Tc
Volatile Organic Compounds(GC/MS)by Method 8260B WG817621 1 09/26/1510:27 09/26/1510:27 KLO
[Cn]
FSr
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 6 of 72

CASE NARRATIVE ONE LAB.NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers,with the FP1
appropriate preservatives, and within method specified holding times. All MDL(LOD)and RDL(LOQ)values reported for environmental samples have been corrected for the dilution factor used in the FTC
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my FSS
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
FSr
FC-1
�GI
Jimmy Hunt rAl
Technical Service Representative
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 7 of 72

MW-7 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 12:34 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 17800 1000 1 09/22/2015 20:48 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/2015 05:29 WG817578
Acrolein ND 50.0 1 09/25/2015 05:29 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 05:29 WG817578
Benzene ND 1.00 1 09/25/2015 05:29 WG817578
Bromobenzene ND 1.00 1 09/25/2015 05:29 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/2015 05:29 WG817578
Bromoform ND 1.00 1 09/25/2015 05:29 WG817578 F
Bromomethane ND 5.00 1 09/25/2015 05:29 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/2015 05:29 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 05:29 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/2015 05:29 WG817578
Carbon tetrachloride ND 1.00 1 09/25/2015 05:29 WG817578 F
Chlorobenzene ND 1.00 1 09/25/2015 05:29 WG817578
Chlorodibromomethane ND 1.00 1 09/25/2015 05:29 WG817578
Chloroethane ND 5.00 1 09/25/2015 05:29 WG817578
2-Chloroethyl vinyl ether ND J3 J6 50.0 1 09/25/2015 05:29 WG817578
Chloroform ND 5.00 1 09/25/2015 05:29 WG817578
Chloromethane ND 2.50 1 09/25/2015 05:29 WG817578
2-Chlorotoluene ND 1.00 1 09/25/2015 05:29 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 05:29 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 05:29 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 05:29 WG817578
Dibromomethane ND 1.00 1 09/25/2015 05:29 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/2015 05:29 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 05:29 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 05:29 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 05:29 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 05:29 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 05:29 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 05:29 WG817578
cis-1,2-Dichloroethene ND 1.00 1 09/25/2015 05:29 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 05:29 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 05:29 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 05:29 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 05:29 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 05:29 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/2015 05:29 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 05:29 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 05:29 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 05:29 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 05:29 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 05:29 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 05:29 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 05:29 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 05:29 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 05:29 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 05:29 WG817578
Naphthalene ND 5.00 1 09/25/2015 05:29 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 05:29 WG817578
Styrene ND 1.00 1 09/25/2015 05:29 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-7 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 12:34 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 05:29 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 05:29 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 05:29 WG817578 F
Tetrachloroethene 96.2 J6 1.00 1 09/25/2015 05:29 WG817578
Toluene ND 5.00 1 09/25/2015 05:29 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 05:29 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 05:29 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 05:29 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 05:29 WG817578
Trichloroethene ND 1.00 1 09/25/2015 05:29 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 05:29 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 05:29 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 05:29 WG817578 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 05:29 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 05:29 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 05:29 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/2015 05:29 WG817578
(S)Toluene-d8 102 90.0-115 0912512015 05:29 WG817578 F
(S)Dibromofluoromethone 109 79.0-121 091251201505:29 WG817578
(S)4-Bromofluorobenzene 89.0 80.1-120 0912512015 05:29 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 9 of 72

MW-9 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 13:20 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 2490 1000 1 09/22/2015 21:00 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/2015 05:49 WG817578
Acrolein ND 50.0 1 09/25/2015 05:49 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 05:49 WG817578
Benzene ND 1.00 1 09/25/2015 05:49 WG817578
Bromobenzene ND 1.00 1 09/25/2015 05:49 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/2015 05:49 WG817578
Bromoform ND 1.00 1 09/25/2015 05:49 WG817578
Bromomethane ND 5.00 1 09/25/2015 05:49 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/2015 05:49 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 05:49 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/2015 05:49 WG817578
Carbon tetrachloride ND 1.00 1 09/25/2015 05:49 WG817578 F
Chlorobenzene ND 1.00 1 09/25/2015 05:49 WG817578
Chlorodibromomethane ND 1.00 1 09/25/2015 05:49 WG817578
Chloroethane ND 5.00 1 09/25/2015 05:49 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 05:49 WG817578
Chloroform ND 5.00 1 09/25/2015 05:49 WG817578
Chloromethane ND 2.50 1 09/25/2015 05:49 WG817578
2-Chlorotoluene ND 1.00 1 09/25/2015 05:49 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 05:49 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 05:49 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 05:49 WG817578
Dibromomethane ND 1.00 1 09/25/2015 05:49 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/2015 05:49 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 05:49 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 05:49 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 05:49 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 05:49 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 05:49 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 05:49 WG817578
cis-1,2-Dichloroethene 504 50.0 50 09/29/201514:01 WG818281
trans-1,2-Dichloroethene 1.96 1.00 1 09/25/2015 05:49 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 05:49 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 05:49 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 05:49 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 05:49 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/2015 05:49 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 05:49 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 05:49 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 05:49 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 05:49 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 05:49 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 05:49 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 05:49 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 05:49 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 05:49 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 05:49 WG817578
Naphthalene ND 5.00 1 09/25/2015 05:49 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 05:49 WG817578
Styrene ND 1.00 1 09/25/2015 05:49 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 10 of 72

MW-9 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 13:20 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 05:49 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 05:49 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 05:49 WG817578 F
Tetrachloroethene 1150 50.0 50 09/29/201514:01 WG818281
Toluene ND 5.00 1 09/25/2015 05:49 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 05:49 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 05:49 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 05:49 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 05:49 WG817578
Trichloroethene 89.3 1.00 1 09/25/2015 05:49 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 05:49 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 05:49 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 05:49 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 05:49 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 05:49 WG817578
Vinyl chloride 2.87 1.00 1 09/25/2015 05:49 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/2015 05:49 WG817578
(S)Toluene-d8 98.4 90.0-115 0912512015 05.49 WG817578 F
(S)Dibromofluoromethone 102 79.0-121 091251201505:49 WG817578
(S)4-Bromofluorobenzene 93.3 80.1-120 0912512015 05.49 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 11 of 72

MW-10 SAMPLE RESULTS - 03 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 09:22 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 1980 1000 1 09/22/2015 22:08 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/2015 06:09 WG817578
Acrolein ND 50.0 1 09/25/2015 06:09 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 06:09 WG817578
Benzene ND 1.00 1 09/25/2015 06:09 WG817578
Bromobenzene ND 1.00 1 09/25/2015 06:09 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/2015 06:09 WG817578
Bromoform ND 1.00 1 09/25/2015 06:09 WG817578 F
Bromomethane ND 5.00 1 09/25/2015 06:09 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/2015 06:09 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 06:09 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/2015 06:09 WG817578
Carbon tetrachloride ND 1.00 1 09/25/2015 06:09 WG817578 F
Chlorobenzene ND 1.00 1 09/25/2015 06:09 WG817578
Chlorodibromomethane ND 1.00 1 09/25/2015 06:09 WG817578
Chloroethane ND 5.00 1 09/25/2015 06:09 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 06:09 WG817578
Chloroform ND 5.00 1 09/25/2015 06:09 WG817578
Chloromethane ND 2.50 1 09/25/2015 06:09 WG817578
2-Chlorotoluene ND 1.00 1 09/25/2015 06:09 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 06:09 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 06:09 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 06:09 WG817578
Dibromomethane ND 1.00 1 09/25/2015 06:09 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/2015 06:09 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 06:09 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 06:09 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 06:09 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 06:09 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 06:09 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 06:09 WG817578
cis-1,2-Dichloroethene 643 50.0 50 09/29/201514:21 WG818281
trans-1,2-Dichloroethene 2.32 1.00 1 09/25/2015 06:09 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 06:09 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 06:09 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 06:09 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 06:09 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/2015 06:09 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 06:09 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 06:09 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 06:09 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 06:09 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 06:09 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 06:09 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 06:09 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 06:09 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 06:09 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 06:09 WG817578
Naphthalene ND 5.00 1 09/25/2015 06:09 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 06:09 WG817578
Styrene ND 1.00 1 09/25/2015 06:09 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 12 of 72

MW-10 SAMPLE RESULTS - 03 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 09:22 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 06:09 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 06:09 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 06:09 WG817578 F
Tetrachloroethene 1790 50.0 50 09/29/201514:21 WG818281
Toluene ND 5.00 1 09/25/2015 06:09 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 06:09 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 06:09 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 06:09 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 06:09 WG817578
Trichloroethene 128 1.00 1 09/25/2015 06:09 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 06:09 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 06:09 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 06:09 WG817578 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 06:09 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 06:09 WG817578
Vinyl chloride 24.1 1.00 1 09/25/2015 06:09 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/2015 06:09 WG817578
(S)Toluene-d8 97.8 90.0-115 0912512015 06:09 WG817578 F
(S)Dibromofluoromethone 105 79.0-121 091251201506:09 WG817578
(S)4-Bromofluorobenzene 91.0 80.1-120 0912512015 06:09 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 13 of 72

MW-11 SAMPLE RESULTS - 04 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 10:13 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 1440 1000 1 09/22/2015 22:22 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/2015 06:29 WG817578
Acrolein ND 50.0 1 09/25/2015 06:29 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 06:29 WG817578
Benzene ND 1.00 1 09/25/2015 06:29 WG817578
Bromobenzene ND 1.00 1 09/25/2015 06:29 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/2015 06:29 WG817578
Bromoform ND 1.00 1 09/25/2015 06:29 WG817578 F
Bromomethane ND 5.00 1 09/25/2015 06:29 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/2015 06:29 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 06:29 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/2015 06:29 WG817578
Carbon tetrachloride ND 1.00 1 09/25/2015 06:29 WG817578 F
Chlorobenzene ND 1.00 1 09/25/2015 06:29 WG817578
Chlorodibromomethane ND 1.00 1 09/25/2015 06:29 WG817578
Chloroethane ND 5.00 1 09/25/2015 06:29 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 06:29 WG817578
Chloroform ND 5.00 1 09/25/2015 06:29 WG817578
Chloromethane ND 2.50 1 09/25/2015 06:29 WG817578
2-Chlorotoluene ND 1.00 1 09/25/2015 06:29 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 06:29 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 06:29 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 06:29 WG817578
Dibromomethane ND 1.00 1 09/25/2015 06:29 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/2015 06:29 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 06:29 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 06:29 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 06:29 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 06:29 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 06:29 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 06:29 WG817578
cis-1,2-Dichloroethene 174 1.00 1 09/25/2015 06:29 WG817578
trans-1,2-Dichloroethene 1.10 1.00 1 09/25/2015 06:29 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 06:29 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 06:29 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 06:29 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 06:29 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/2015 06:29 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 06:29 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 06:29 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 06:29 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 06:29 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 06:29 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 06:29 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 06:29 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 06:29 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 06:29 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 06:29 WG817578
Naphthalene ND 5.00 1 09/25/2015 06:29 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 06:29 WG817578
Styrene ND 1.00 1 09/25/2015 06:29 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 14 of 72

MW-11 SAMPLE RESULTS - 04 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 10:13 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 06:29 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 06:29 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 06:29 WG817578 F
Tetrachloroethene 433 20.0 20 09/29/201514:41 WG818281
Toluene ND 5.00 1 09/25/2015 06:29 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 06:29 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 06:29 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 06:29 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 06:29 WG817578
Trichloroethene 39.5 1.00 1 09/25/2015 06:29 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 06:29 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 06:29 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 06:29 WG817578 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 06:29 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 06:29 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 06:29 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/2015 06:29 WG817578
(S)Toluene-d8 100 90.0-115 0912512015 06:29 WG817578 F
(S)Dibromofluoromethone 106 79.0-121 091251201506:29 WG817578
(S)4-Bromofluorobenzene 89.2 80.1-120 0912512015 06:29 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 15 of 72

MW-13 SAMPLE RESULTS - 05 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 11:54 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/2015 22:36 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/2015 06:49 WG817578
Acrolein ND 50.0 1 09/25/2015 06:49 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 06:49 WG817578
Benzene ND 1.00 1 09/25/2015 06:49 WG817578
Bromobenzene ND 1.00 1 09/25/2015 06:49 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/2015 06:49 WG817578
Bromoform ND 1.00 1 09/25/2015 06:49 WG817578
Bromomethane ND 5.00 1 09/25/2015 06:49 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/2015 06:49 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 06:49 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/2015 06:49 WG817578
Carbon tetrachloride ND 1.00 1 09/25/2015 06:49 WG817578 F
Chlorobenzene ND 1.00 1 09/25/2015 06:49 WG817578
Chlorodibromomethane ND 1.00 1 09/25/2015 06:49 WG817578
Chloroethane ND 5.00 1 09/25/2015 06:49 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 06:49 WG817578
Chloroform ND 5.00 1 09/25/2015 06:49 WG817578
Chloromethane ND 2.50 1 09/25/2015 06:49 WG817578
2-Chlorotoluene ND 1.00 1 09/25/2015 06:49 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 06:49 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 06:49 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 06:49 WG817578
Dibromomethane ND 1.00 1 09/25/2015 06:49 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/2015 06:49 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 06:49 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 06:49 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 06:49 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 06:49 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 06:49 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 06:49 WG817578
cis-1,2-Dichloroethene 135 1.00 1 09/25/2015 06:49 WG817578
trans-1,2-Dichloroethene 1.01 1.00 1 09/25/2015 06:49 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 06:49 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 06:49 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 06:49 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 06:49 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/2015 06:49 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 06:49 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 06:49 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 06:49 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 06:49 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 06:49 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 06:49 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 06:49 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 06:49 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 06:49 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 06:49 WG817578
Naphthalene ND 5.00 1 09/25/2015 06:49 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 06:49 WG817578
Styrene ND 1.00 1 09/25/2015 06:49 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 16 of 72

MW-13 SAMPLE RESULTS - 05 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 11:54 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 06:49 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 06:49 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 06:49 WG817578 F
Tetrachloroethene 598 20.0 20 09/29/201515:01 WG818281
Toluene ND 5.00 1 09/25/2015 06:49 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 06:49 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 06:49 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 06:49 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 06:49 WG817578
Trichloroethene 120 1.00 1 09/25/2015 06:49 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 06:49 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 06:49 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 06:49 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 06:49 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 06:49 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 06:49 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/2015 06:49 WG817578
(S)Toluene-d8 95.8 90.0-115 0912512015 06.49 WG817578 F
(S)Dibromofluoromethone 106 79.0-121 091251201506:49 WG817578
(S)4-Bromofluorobenzene 91.4 80.1-120 0912512015 06.49 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 17 of 72

MW-14 SAMPLE RESULTS - 06 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 11:23 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/2015 22:48 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/2015 07:09 WG817578
Acrolein ND 50.0 1 09/25/2015 07:09 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 07:09 WG817578
Benzene ND 1.00 1 09/25/2015 07:09 WG817578
Bromobenzene ND 1.00 1 09/25/2015 07:09 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/2015 07:09 WG817578
Bromoform ND 1.00 1 09/25/2015 07:09 WG817578 F
Bromomethane ND 5.00 1 09/25/2015 07:09 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/2015 07:09 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 07:09 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/2015 07:09 WG817578
Carbon tetrachloride ND 1.00 1 09/25/2015 07:09 WG817578 F
Chlorobenzene ND 1.00 1 09/25/2015 07:09 WG817578
Chlorodibromomethane ND 1.00 1 09/25/2015 07:09 WG817578
Chloroethane ND 5.00 1 09/25/2015 07:09 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 07:09 WG817578
Chloroform ND 5.00 1 09/25/2015 07:09 WG817578
Chloromethane ND 2.50 1 09/25/2015 07:09 WG817578
2-Chlorotoluene ND 1.00 1 09/25/2015 07:09 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 07:09 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 07:09 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 07:09 WG817578
Dibromomethane ND 1.00 1 09/25/2015 07:09 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/2015 07:09 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 07:09 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 07:09 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 07:09 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 07:09 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 07:09 WG817578
1,1-Dichloroethene 1.46 1.00 1 09/25/2015 07:09 WG817578
cis-1,2-Dichloroethene 143 1.00 1 09/25/2015 07:09 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 07:09 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 07:09 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 07:09 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 07:09 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 07:09 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/2015 07:09 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 07:09 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 07:09 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 07:09 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 07:09 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 07:09 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 07:09 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 07:09 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 07:09 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 07:09 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 07:09 WG817578
Naphthalene ND 5.00 1 09/25/2015 07:09 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 07:09 WG817578
Styrene ND 1.00 1 09/25/2015 07:09 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 18 of 72

MW-14 SAMPLE RESULTS - 06 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 11:23 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 07:09 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 07:09 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 07:09 WG817578 F
Tetrachloroethene 519 20.0 20 09/29/201515:21 WG818281
Toluene ND 5.00 1 09/25/2015 07:09 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 07:09 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 07:09 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 07:09 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 07:09 WG817578
Trichloroethene 375 20.0 20 09/29/201515:21 WG818281
Trichlorofluoromethane ND 5.00 1 09/25/2015 07:09 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 07:09 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 07:09 WG817578 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 07:09 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 07:09 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 07:09 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/2015 07:09 WG817578
(S)Toluene-d8 90.0 90.0-115 0912512015 07.-09 WG817578 F
(S)Dibromofluoromethone 105 79.0-121 091251201507-09 WG817578
(S)4-Bromofluorobenzene 89.2 80.1-120 0912512015 07.-09 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 19 of 72

MW-15 SAMPLE RESULTS - 07 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 09:40 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/2015 07:29 WG817578
Acrolein ND 50.0 1 09/25/2015 07:29 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 07:29 WG817578 F
Benzene ND 1.00 1 09/25/2015 07:29 WG817578
Bromobenzene ND 1.00 1 09/25/2015 07:29 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/2015 07:29 WG817578 Cn
Bromoform ND 1.00 1 09/25/2015 07:29 WG817578
Bromomethane ND 5.00 1 09/25/2015 07:29 WG817578
n-Butylbenzene ND 1.00 1 09/25/2015 07:29 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 07:29 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/2015 07:29 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/2015 07:29 WG817578
Chlorobenzene ND 1.00 1 09/25/2015 07:29 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/2015 07:29 WG817578
Chloroethane ND 5.00 1 09/25/2015 07:29 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 07:29 WG817578
Chloroform ND 5.00 1 09/25/2015 07:29 WG817578
Chloromethane ND 2.50 1 09/25/2015 07:29 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/2015 07:29 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 07:29 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 07:29 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 07:29 WG817578
Dibromomethane ND 1.00 1 09/25/2015 07:29 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/2015 07:29 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 07:29 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 07:29 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 07:29 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 07:29 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 07:29 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 07:29 WG817578
cis-1,2-Dichloroethene 5.62 1.00 1 09/25/2015 07:29 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 07:29 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 07:29 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 07:29 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 07:29 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 07:29 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/2015 07:29 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 07:29 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 07:29 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 07:29 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 07:29 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 07:29 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 07:29 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 07:29 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 07:29 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 07:29 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 07:29 WG817578
Naphthalene ND 5.00 1 09/25/2015 07:29 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 07:29 WG817578
Styrene ND 1.00 1 09/25/2015 07:29 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 07:29 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 07:29 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 07:29 WG817578
Tetrachloroethene 80.9 J6 1.00 1 09/29/201513:41 WG818281
Toluene ND 5.00 1 09/25/2015 07:29 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 07:29 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 20 of 72

MW-15 SAMPLE RESULTS - 07 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 09:40 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 07:29 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 07:29 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 07:29 WG817578 F
Trichloroethene 2.62 1.00 1 09/29/201513:41 WG818281
Trichlorofluoromethane ND 5.00 1 09/25/2015 07:29 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 07:29 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 07:29 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 07:29 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 07:29 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 07:29 WG817578
Xylenes,Total ND 3.00 1 09/25/2015 07:29 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 0912512015 0729 WG817578
(S)Dibromofluoromethone 103 79.0-121 0912512015 0729 WG817578 Fq
(S)4-Bromofluorobenzene 89.2 80.1-120 0912512015 0729 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 21 of 72

MW-16 SAMPLE RESULTS - 08 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 08:30 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/2015 07:49 WG817578
Acrolein ND 50.0 1 09/25/2015 07:49 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 07:49 WG817578 F
Benzene ND 1.00 1 09/25/2015 07:49 WG817578
Bromobenzene ND 1.00 1 09/25/2015 07:49 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/2015 07:49 WG817578 Cn
Bromoform ND 1.00 1 09/25/2015 07:49 WG817578
Bromomethane ND 5.00 1 09/25/2015 07:49 WG817578
n-Butylbenzene ND 1.00 1 09/25/2015 07:49 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 07:49 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/2015 07:49 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/2015 07:49 WG817578
Chlorobenzene ND 1.00 1 09/25/2015 07:49 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/2015 07:49 WG817578
Chloroethane ND 5.00 1 09/25/2015 07:49 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 07:49 WG817578
Chloroform ND 5.00 1 09/25/2015 07:49 WG817578
Chloromethane ND 2.50 1 09/25/2015 07:49 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/2015 07:49 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 07:49 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 07:49 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 07:49 WG817578
Dibromomethane ND 1.00 1 09/25/2015 07:49 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/2015 07:49 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 07:49 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 07:49 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 07:49 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 07:49 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 07:49 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 07:49 WG817578
cis-1,2-Dichloroethene 4.49 1.00 1 09/25/2015 07:49 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 07:49 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 07:49 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 07:49 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 07:49 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 07:49 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/2015 07:49 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 07:49 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 07:49 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 07:49 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 07:49 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 07:49 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 07:49 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 07:49 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 07:49 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 07:49 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 07:49 WG817578
Naphthalene ND 5.00 1 09/25/2015 07:49 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 07:49 WG817578
Styrene ND 1.00 1 09/25/2015 07:49 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 07:49 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 07:49 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 07:49 WG817578
Tetrachloroethene 80.6 1.00 1 09/29/201515:41 WG818281
Toluene ND 5.00 1 09/25/2015 07:49 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 07:49 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 22 of 72

MW-16 SAMPLE RESULTS - 08 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 08:30 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 07:49 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 07:49 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 07:49 WG817578 F
Trichloroethene 2.55 1.00 1 09/29/201515:41 WG818281
Trichlorofluoromethane ND 5.00 1 09/25/2015 07:49 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 07:49 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 07:49 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 07:49 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 07:49 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 07:49 WG817578
Xylenes,Total ND 3.00 1 09/25/2015 07:49 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 0912512015 07.49 WG817578
(S)Dibromofluoromethone 105 79.0-121 0912512015 0749 WG817578 Fq
(S)4-Bromofluorobenzene 89.8 80.1-120 0912512015 07.49 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-17 SAMPLE RESULTS - 09 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 10:35 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/2015 08:09 WG817578
Acrolein ND 50.0 1 09/25/2015 08:09 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 08:09 WG817578 F
Benzene ND 1.00 1 09/25/2015 08:09 WG817578
Bromobenzene ND 1.00 1 09/25/2015 08:09 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/2015 08:09 WG817578 Cn
Bromoform ND 1.00 1 09/25/2015 08:09 WG817578
Bromomethane ND 5.00 1 09/25/2015 08:09 WG817578
n-Butylbenzene ND 1.00 1 09/25/2015 08:09 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 08:09 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/2015 08:09 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/2015 08:09 WG817578
Chlorobenzene ND 1.00 1 09/25/2015 08:09 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/2015 08:09 WG817578
Chloroethane ND 5.00 1 09/25/2015 08:09 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 08:09 WG817578
Chloroform ND 5.00 1 09/25/2015 08:09 WG817578
Chloromethane ND 2.50 1 09/25/2015 08:09 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/2015 08:09 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 08:09 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 08:09 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 08:09 WG817578
Dibromomethane ND 1.00 1 09/25/2015 08:09 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/2015 08:09 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 08:09 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 08:09 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 08:09 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 08:09 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 08:09 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 08:09 WG817578
cis-1,2-Dichloroethene 11.3 1.00 1 09/25/2015 08:09 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 08:09 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 08:09 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 08:09 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 08:09 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 08:09 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/2015 08:09 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 08:09 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 08:09 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 08:09 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 08:09 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 08:09 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 08:09 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 08:09 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 08:09 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 08:09 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 08:09 WG817578
Naphthalene ND 5.00 1 09/25/2015 08:09 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 08:09 WG817578
Styrene ND 1.00 1 09/25/2015 08:09 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 08:09 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 08:09 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 08:09 WG817578
Tetrachloroethene 2.10 1.00 1 09/29/201516:01 WG818281
Toluene ND 5.00 1 09/25/2015 08:09 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 08:09 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 24 of 72

MW-17 SAMPLE RESULTS - 09 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 10:35 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 08:09 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 08:09 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 08:09 WG817578 F
Trichloroethene 3.06 1.00 1 09/25/2015 08:09 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 08:09 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 08:09 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 08:09 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 08:09 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 08:09 WG817578
Vinyl chloride 5.29 1.00 1 09/25/2015 08:09 WG817578
Xylenes,Total ND 3.00 1 09/25/2015 08:09 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 0912512015 08:09 WG817578
(S)Dibromofluoromethone 106 79.0-121 0912512015 08:09 WG817578 Fq
(S)4-Bromofluorobenzene 90.7 80.1-120 0912512015 08:09 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 25 of 72

MW-18 SAMPLE RESULTS - 10 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 08:55 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/2015 08:29 WG817578
Acrolein ND 50.0 1 09/25/2015 08:29 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 08:29 WG817578 F
Benzene ND 1.00 1 09/25/2015 08:29 WG817578
Bromobenzene ND 1.00 1 09/25/2015 08:29 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/2015 08:29 WG817578 Cn
Bromoform ND 1.00 1 09/25/2015 08:29 WG817578
Bromomethane ND 5.00 1 09/25/2015 08:29 WG817578
n-Butylbenzene ND 1.00 1 09/25/2015 08:29 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 08:29 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/2015 08:29 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/2015 08:29 WG817578
Chlorobenzene ND 1.00 1 09/25/2015 08:29 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/2015 08:29 WG817578
Chloroethane ND 5.00 1 09/25/2015 08:29 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 08:29 WG817578
Chloroform ND 5.00 1 09/25/2015 08:29 WG817578
Chloromethane ND 2.50 1 09/25/2015 08:29 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/2015 08:29 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 08:29 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 08:29 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 08:29 WG817578
Dibromomethane ND 1.00 1 09/25/2015 08:29 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/2015 08:29 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 08:29 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 08:29 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 08:29 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 08:29 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 08:29 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 08:29 WG817578
cis-1,2-Dichloroethene ND 1.00 1 09/25/2015 08:29 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 08:29 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 08:29 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 08:29 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 08:29 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 08:29 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/2015 08:29 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 08:29 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 08:29 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 08:29 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 08:29 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 08:29 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 08:29 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 08:29 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 08:29 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 08:29 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 08:29 WG817578
Naphthalene ND 5.00 1 09/25/2015 08:29 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 08:29 WG817578
Styrene ND 1.00 1 09/25/2015 08:29 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 08:29 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 08:29 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 08:29 WG817578
Tetrachloroethene ND 1.00 1 09/29/201516:21 WG818281
Toluene ND 5.00 1 09/25/2015 08:29 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 08:29 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-18 SAMPLE RESULTS - 10 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 08:55 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 08:29 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 08:29 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 08:29 WG817578 F
Trichloroethene ND 1.00 1 09/25/2015 08:29 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 08:29 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 08:29 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 08:29 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 08:29 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 08:29 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 08:29 WG817578
Xylenes,Total ND 3.00 1 09/25/2015 08:29 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 0912512015 08.29 WG817578
(S)Dibromofluoromethone 102 79.0-121 0912512015 08:29 WG817578 Fq
(S)4-Bromofluorobenzene 89.8 80.1-120 0912512015 08.29 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 27 of 72

MW-20 SAMPLE RESULTS - 11 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 10:50 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/2015 08:49 WG817578
Acrolein ND 50.0 1 09/25/2015 08:49 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 08:49 WG817578 F
Benzene ND 1.00 1 09/25/2015 08:49 WG817578
Bromobenzene ND 1.00 1 09/25/2015 08:49 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/2015 08:49 WG817578 Cn
Bromoform ND 1.00 1 09/25/2015 08:49 WG817578
Bromomethane ND 5.00 1 09/25/2015 08:49 WG817578
n-Butylbenzene ND 1.00 1 09/25/2015 08:49 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 08:49 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/2015 08:49 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/2015 08:49 WG817578
Chlorobenzene ND 1.00 1 09/25/2015 08:49 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/2015 08:49 WG817578
Chloroethane ND 5.00 1 09/25/2015 08:49 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 08:49 WG817578
Chloroform ND 5.00 1 09/25/2015 08:49 WG817578
Chloromethane ND 2.50 1 09/25/2015 08:49 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/2015 08:49 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 08:49 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 08:49 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 08:49 WG817578
Dibromomethane ND 1.00 1 09/25/2015 08:49 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/2015 08:49 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 08:49 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 08:49 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 08:49 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 08:49 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 08:49 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 08:49 WG817578
cis-1,2-Dichloroethene ND 1.00 1 09/25/2015 08:49 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 08:49 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 08:49 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 08:49 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 08:49 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 08:49 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/2015 08:49 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 08:49 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 08:49 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 08:49 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 08:49 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 08:49 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 08:49 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 08:49 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 08:49 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 08:49 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 08:49 WG817578
Naphthalene ND 5.00 1 09/25/2015 08:49 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 08:49 WG817578
Styrene ND 1.00 1 09/25/2015 08:49 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 08:49 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 08:49 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 08:49 WG817578
Tetrachloroethene ND 1.00 1 09/25/2015 08:49 WG817578
Toluene ND 5.00 1 09/25/2015 08:49 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 08:49 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-20 SAMPLE RESULTS - 11 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 10:50 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 08:49 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 08:49 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 08:49 WG817578 F
Trichloroethene ND 1.00 1 09/25/2015 08:49 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 08:49 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 08:49 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 08:49 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 08:49 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 08:49 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 08:49 WG817578
Xylenes,Total ND 3.00 1 09/25/2015 08:49 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 0912512015 08.49 WG817578
(S)Dibromofluoromethone 104 79.0-121 0912512015 08:49 WG817578 Fq
(S)4-Bromofluorobenzene 90.7 80.1-120 0912512015 08.49 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 29 of 72

MW-21 SAMPLE RESULTS - 12 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 11:20 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/2015 09:10 WG817578
Acrolein ND 50.0 1 09/25/2015 09:10 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 09:10 WG817578 F
Benzene ND 1.00 1 09/25/2015 09:10 WG817578
Bromobenzene ND 1.00 1 09/25/2015 09:10 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/2015 09:10 WG817578 Cn
Bromoform ND 1.00 1 09/25/2015 09:10 WG817578
Bromomethane ND 5.00 1 09/25/2015 09:10 WG817578
n-Butylbenzene ND 1.00 1 09/25/2015 09:10 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 09:10 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/2015 09:10 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/2015 09:10 WG817578
Chlorobenzene ND 1.00 1 09/25/2015 09:10 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/2015 09:10 WG817578
Chloroethane ND 5.00 1 09/25/2015 09:10 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 09:10 WG817578
Chloroform ND 5.00 1 09/25/2015 09:10 WG817578
Chloromethane ND 2.50 1 09/25/2015 09:10 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/2015 09:10 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 09:10 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 09:10 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 09:10 WG817578
Dibromomethane ND 1.00 1 09/25/2015 09:10 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/2015 09:10 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 09:10 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 09:10 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 09:10 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 09:10 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 09:10 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 09:10 WG817578
cis-1,2-Dichloroethene ND 1.00 1 09/25/2015 09:10 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 09:10 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 09:10 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 09:10 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 09:10 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 09:10 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/2015 09:10 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 09:10 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 09:10 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 09:10 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 09:10 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 09:10 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 09:10 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 09:10 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 09:10 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 09:10 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 09:10 WG817578
Naphthalene ND 5.00 1 09/25/2015 09:10 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 09:10 WG817578
Styrene ND 1.00 1 09/25/2015 09:10 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 09:10 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 09:10 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 09:10 WG817578
Tetrachloroethene ND 1.00 1 09/25/2015 09:10 WG817578
Toluene ND 5.00 1 09/25/2015 09:10 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 09:10 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-21 SAMPLE RESULTS - 12 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 11:20 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 09:10 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 09:10 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 09:10 WG817578 F
Trichloroethene ND 1.00 1 09/25/2015 09:10 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 09:10 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 09:10 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 09:10 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 09:10 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 09:10 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 09:10 WG817578
Xylenes,Total ND 3.00 1 09/25/2015 09:10 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 0912512015 09:10 WG817578
(S)Dibromofluoromethone 105 79.0-121 0912512015 09:10 WG817578 Fq
(S)4-Bromofluorobenzene 89.4 80.1-120 0912512015 09:10 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 31 of 72

MW-22 SAMPLE RESULTS - 13 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 11:30 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/2015 09:30 WG817578
Acrolein ND 50.0 1 09/25/2015 09:30 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 09:30 WG817578 F
Benzene ND 1.00 1 09/25/2015 09:30 WG817578
Bromobenzene ND 1.00 1 09/25/2015 09:30 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/2015 09:30 WG817578 Cn
Bromoform ND 1.00 1 09/25/2015 09:30 WG817578
Bromomethane ND 5.00 1 09/25/2015 09:30 WG817578
n-Butylbenzene ND 1.00 1 09/25/2015 09:30 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 09:30 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/2015 09:30 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/2015 09:30 WG817578
Chlorobenzene ND 1.00 1 09/25/2015 09:30 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/2015 09:30 WG817578
Chloroethane ND 5.00 1 09/25/2015 09:30 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 09:30 WG817578
Chloroform ND 5.00 1 09/25/2015 09:30 WG817578
Chloromethane ND 2.50 1 09/25/2015 09:30 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/2015 09:30 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 09:30 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 09:30 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 09:30 WG817578
Dibromomethane ND 1.00 1 09/25/2015 09:30 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/2015 09:30 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 09:30 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 09:30 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 09:30 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 09:30 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 09:30 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 09:30 WG817578
cis-1,2-Dichloroethene ND 1.00 1 09/25/2015 09:30 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 09:30 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 09:30 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 09:30 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 09:30 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 09:30 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/2015 09:30 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 09:30 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 09:30 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 09:30 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 09:30 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 09:30 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 09:30 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 09:30 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 09:30 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 09:30 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 09:30 WG817578
Naphthalene ND 5.00 1 09/25/2015 09:30 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 09:30 WG817578
Styrene ND 1.00 1 09/25/2015 09:30 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 09:30 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 09:30 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 09:30 WG817578
Tetrachloroethene ND 1.00 1 09/25/2015 09:30 WG817578
Toluene ND 5.00 1 09/25/2015 09:30 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 09:30 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-22 SAMPLE RESULTS - 13 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 11:30 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 09:30 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 09:30 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 09:30 WG817578 F
Trichloroethene ND 1.00 1 09/25/2015 09:30 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 09:30 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 09:30 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 09:30 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 09:30 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 09:30 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 09:30 WG817578
Xylenes,Total ND 3.00 1 09/25/2015 09:30 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 0912512015 09:30 WG817578
(S)Dibromofluoromethone 102 79.0-121 0912512015 09:30 WG817578 Fq
(S)4-Bromofluorobenzene 91.3 80.1-120 0912512015 09:30 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-23 SAMPLE RESULTS - 14 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 10:32 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/2015 23:12 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/2015 09:50 WG817578
Acrolein ND 50.0 1 09/25/2015 09:50 WG817578
Acrylonitrile ND 10.0 1 09/25/2015 09:50 WG817578
Benzene ND 1.00 1 09/25/2015 09:50 WG817578
Bromobenzene ND 1.00 1 09/25/2015 09:50 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/2015 09:50 WG817578
Bromoform ND 1.00 1 09/25/2015 09:50 WG817578 F
Bromomethane ND 5.00 1 09/25/2015 09:50 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/2015 09:50 WG817578
sec-Butylbenzene ND 1.00 1 09/25/2015 09:50 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/2015 09:50 WG817578
Carbon tetrachloride ND 1.00 1 09/25/2015 09:50 WG817578 F
Chlorobenzene ND 1.00 1 09/25/2015 09:50 WG817578
Chlorodibromomethane ND 1.00 1 09/25/2015 09:50 WG817578
Chloroethane ND 5.00 1 09/25/2015 09:50 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 09:50 WG817578
Chloroform ND 5.00 1 09/25/2015 09:50 WG817578
Chloromethane ND 2.50 1 09/25/2015 09:50 WG817578
2-Chlorotoluene ND 1.00 1 09/25/2015 09:50 WG817578
4-Chlorotoluene ND 1.00 1 09/25/2015 09:50 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 09:50 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/2015 09:50 WG817578
Dibromomethane ND 1.00 1 09/25/2015 09:50 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/2015 09:50 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 09:50 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 09:50 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/2015 09:50 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/2015 09:50 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/2015 09:50 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/2015 09:50 WG817578
cis-1,2-Dichloroethene 17.6 1.00 1 09/25/2015 09:50 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 09:50 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/2015 09:50 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/2015 09:50 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/2015 09:50 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 09:50 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/2015 09:50 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/2015 09:50 WG817578
Di-isopropyl ether ND 1.00 1 09/25/2015 09:50 WG817578
Ethylbenzene ND 1.00 1 09/25/2015 09:50 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 09:50 WG817578
Isopropylbenzene ND 1.00 1 09/25/2015 09:50 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/2015 09:50 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/2015 09:50 WG817578
Methylene Chloride ND 5.00 1 09/25/2015 09:50 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 09:50 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/2015 09:50 WG817578
Naphthalene ND 5.00 1 09/25/2015 09:50 WG817578
n-Propylbenzene ND 1.00 1 09/25/2015 09:50 WG817578
Styrene ND 1.00 1 09/25/2015 09:50 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-23 SAMPLE RESULTS - 14 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 10:32 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 09:50 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 09:50 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 09:50 WG817578 F
Tetrachloroethene 177 10.0 10 09/29/201516:41 WG818281
Toluene ND 5.00 1 09/25/2015 09:50 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 09:50 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 09:50 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 09:50 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 09:50 WG817578
Trichloroethene 7.91 1.00 1 09/25/2015 09:50 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/2015 09:50 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 09:50 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 09:50 WG817578 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 09:50 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 09:50 WG817578
Vinyl chloride ND 1.00 1 09/25/2015 09:50 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/2015 09:50 WG817578
(S)Toluene-d8 102 90.0-115 0912512015 09:50 WG817578 F
(S)Dibromofluoromethone 103 79.0-121 091251201509:50 WG817578
(S)4-Bromofluorobenzene 90.0 80.1-120 0912512015 09:50 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-24 SAMPLE RESULTS - 15 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 12:02 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/2015 23:34 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/201510:10 WG817578
Acrolein ND 50.0 1 09/25/201510:10 WG817578
Acrylonitrile ND 10.0 1 09/25/201510:10 WG817578
Benzene ND 1.00 1 09/25/201510:10 WG817578
Bromobenzene ND 1.00 1 09/25/201510:10 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/201510:10 WG817578
Bromoform ND 1.00 1 09/25/201510:10 WG817578 F
Bromomethane ND 5.00 1 09/25/201510:10 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/201510:10 WG817578
sec-Butylbenzene ND 1.00 1 09/25/201510:10 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/201510:10 WG817578
Carbon tetrachloride ND 1.00 1 09/25/201510:10 WG817578 F
Chlorobenzene ND 1.00 1 09/25/201510:10 WG817578
Chlorodibromomethane ND 1.00 1 09/25/201510:10 WG817578
Chloroethane ND 5.00 1 09/25/201510:10 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/201510:10 WG817578
Chloroform ND 5.00 1 09/25/201510:10 WG817578
Chloromethane ND 2.50 1 09/25/201510:10 WG817578
2-Chlorotoluene ND 1.00 1 09/25/201510:10 WG817578
4-Chlorotoluene ND 1.00 1 09/25/201510:10 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/201510:10 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/201510:10 WG817578
Dibromomethane ND 1.00 1 09/25/201510:10 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/201510:10 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/201510:10 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/201510:10 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/201510:10 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/201510:10 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/201510:10 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/201510:10 WG817578
cis-1,2-Dichloroethene 10.6 1.00 1 09/25/201510:10 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/201510:10 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/201510:10 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/201510:10 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/201510:10 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/201510:10 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/201510:10 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/201510:10 WG817578
Di-isopropyl ether ND 1.00 1 09/25/201510:10 WG817578
Ethylbenzene ND 1.00 1 09/25/201510:10 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/201510:10 WG817578
Isopropylbenzene ND 1.00 1 09/25/201510:10 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/201510:10 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/201510:10 WG817578
Methylene Chloride ND 5.00 1 09/25/201510:10 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/201510:10 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/201510:10 WG817578
Naphthalene ND 5.00 1 09/25/201510:10 WG817578
n-Propylbenzene ND 1.00 1 09/25/201510:10 WG817578
Styrene ND 1.00 1 09/25/201510:10 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-24 SAMPLE RESULTS - 15 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 12:02 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/201510:10 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/201510:10 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/201510:10 WG817578 F
Tetrachloroethene 231 10.0 10 09/29/201517:02 WG818281
Toluene ND 5.00 1 09/25/201510:10 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/201510:10 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/201510:10 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/201510:10 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/201510:10 WG817578
Trichloroethene 2.85 1.00 1 09/25/201510:10 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/201510:10 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/201510:10 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/201510:10 WG817578 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/201510:10 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/201510:10 WG817578
Vinyl chloride ND 1.00 1 09/25/201510:10 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/201510:10 WG817578
(S)Toluene-d8 102 90.0-115 09/25/201510.10 WG817578 F
(S)Dibromofluoromethone 105 79.0-121 091251201510.10 WG817578
(S)4-Bromofluorobenzene 88.1 80.1-120 091251201510.10 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-26 SAMPLE RESULTS - 16 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 10:12 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/201510:30 WG817578
Acrolein ND 50.0 1 09/25/201510:30 WG817578
Acrylonitrile ND 10.0 1 09/25/201510:30 WG817578 F
Benzene ND 1.00 1 09/25/201510:30 WG817578
Bromobenzene ND 1.00 1 09/25/201510:30 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/201510:30 WG817578 Cn
Bromoform ND 1.00 1 09/25/201510:30 WG817578
Bromomethane ND 5.00 1 09/25/201510:30 WG817578
n-Butylbenzene ND 1.00 1 09/25/201510:30 WG817578
sec-Butylbenzene ND 1.00 1 09/25/201510:30 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/201510:30 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/201510:30 WG817578
Chlorobenzene ND 1.00 1 09/25/201510:30 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/201510:30 WG817578
Chloroethane ND 5.00 1 09/25/201510:30 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/201510:30 WG817578
Chloroform ND 5.00 1 09/25/201510:30 WG817578
Chloromethane ND 2.50 1 09/25/201510:30 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/201510:30 WG817578
4-Chlorotoluene ND 1.00 1 09/25/201510:30 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/201510:30 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/201510:30 WG817578
Dibromomethane ND 1.00 1 09/25/201510:30 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/201510:30 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/201510:30 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/201510:30 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/201510:30 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/201510:30 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/201510:30 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/201510:30 WG817578
cis-1,2-Dichloroethene ND 1.00 1 09/25/201510:30 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/201510:30 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/201510:30 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/201510:30 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/201510:30 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/201510:30 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/201510:30 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/201510:30 WG817578
Di-isopropyl ether ND 1.00 1 09/25/201510:30 WG817578
Ethylbenzene ND 1.00 1 09/25/201510:30 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/201510:30 WG817578
Isopropylbenzene ND 1.00 1 09/25/201510:30 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/201510:30 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/201510:30 WG817578
Methylene Chloride ND 5.00 1 09/25/201510:30 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/201510:30 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/201510:30 WG817578
Naphthalene ND 5.00 1 09/25/201510:30 WG817578
n-Propylbenzene ND 1.00 1 09/25/201510:30 WG817578
Styrene ND 1.00 1 09/25/201510:30 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/201510:30 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/201510:30 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/201510:30 WG817578
Tetrachloroethene ND 1.00 1 09/29/201517:22 WG818281
Toluene ND 5.00 1 09/25/201510:30 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/201510:30 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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MW-26 SAMPLE RESULTS - 16 ONE LAB.NATIONWIDE.
Collected date/time: 09/16/15 10:12 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/201510:30 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/201510:30 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/201510:30 WG817578 F
Trichloroethene ND 1.00 1 09/25/201510:30 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/201510:30 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/201510:30 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/201510:30 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/201510:30 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/201510:30 WG817578
Vinyl chloride ND 1.00 1 09/25/201510:30 WG817578
Xylenes,Total ND 3.00 1 09/25/201510:30 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 09/25/201510:30 WG817578
(S)Dibromofluoromethone 103 79.0-121 09/25/201510:30 WG817578 Fq
(S)4-Bromofluorobenzene 90.3 80.1-120 09/25/201510:30 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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RW-5 SAMPLE RESULTS - 17 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 12:50 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 16400 1000 1 09/22/2015 23:54 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/201510:50 WG817578
Acrolein ND 50.0 1 09/25/201510:50 WG817578
Acrylonitrile ND 10.0 1 09/25/201510:50 WG817578
Benzene ND 1.00 1 09/25/201510:50 WG817578
Bromobenzene ND 1.00 1 09/25/201510:50 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/201510:50 WG817578
Bromoform ND 1.00 1 09/25/201510:50 WG817578 F
Bromomethane ND 5.00 1 09/25/201510:50 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/201510:50 WG817578
sec-Butylbenzene ND 1.00 1 09/25/201510:50 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/201510:50 WG817578
Carbon tetrachloride ND 1.00 1 09/25/201510:50 WG817578 F
Chlorobenzene ND 1.00 1 09/25/201510:50 WG817578
Chlorodibromomethane ND 1.00 1 09/25/201510:50 WG817578
Chloroethane ND 5.00 1 09/25/201510:50 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/201510:50 WG817578
Chloroform ND 5.00 1 09/25/201510:50 WG817578
Chloromethane ND 2.50 1 09/25/201510:50 WG817578
2-Chlorotoluene ND 1.00 1 09/25/201510:50 WG817578
4-Chlorotoluene ND 1.00 1 09/25/201510:50 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/201510:50 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/201510:50 WG817578
Dibromomethane ND 1.00 1 09/25/201510:50 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/201510:50 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/201510:50 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/201510:50 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/201510:50 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/201510:50 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/201510:50 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/201510:50 WG817578
cis-1,2-Dichloroethene 3.58 1.00 1 09/25/201510:50 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/201510:50 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/201510:50 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/201510:50 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/201510:50 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/201510:50 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/201510:50 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/201510:50 WG817578
Di-isopropyl ether ND 1.00 1 09/25/201510:50 WG817578
Ethylbenzene ND 1.00 1 09/25/201510:50 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/201510:50 WG817578
Isopropylbenzene ND 1.00 1 09/25/201510:50 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/201510:50 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/201510:50 WG817578
Methylene Chloride ND 5.00 1 09/25/201510:50 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/201510:50 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/201510:50 WG817578
Naphthalene ND 5.00 1 09/25/201510:50 WG817578
n-Propylbenzene ND 1.00 1 09/25/201510:50 WG817578
Styrene ND 1.00 1 09/25/201510:50 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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RW-5 SAMPLE RESULTS - 17 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 12:50 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/201510:50 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/201510:50 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/201510:50 WG817578 F
Tetrachloroethene ND 2.00 1 09/25/201510:50 WG817578
Toluene 333 50.0 10 09/29/201517:42 WG818281
1,2,3-Trichlorobenzene ND 1.00 1 09/25/201510:50 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/201510:50 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/201510:50 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/201510:50 WG817578
Trichloroethene ND 1.00 1 09/25/201510:50 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/201510:50 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/201510:50 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/201510:50 WG817578 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/201510:50 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/201510:50 WG817578
Vinyl chloride 25.1 1.00 1 09/25/201510:50 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/201510:50 WG817578
(S)Toluene-d8 103 90.0-115 09/25/201510.50 WG817578 F
(S)Dibromofluoromethone 104 79.0-121 091251201510.50 WG817578
(S)4-Bromofluorobenzene 90.3 80.1-120 091251201510.50 WG817578
Sample Narrative:
8260B L789514-17 WG817578:Tetrachloroethene RL has been elevated to 2.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 41 of 72

RW-6 SAMPLE RESULTS - 18 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 09:30 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 2980 1000 1 09/23/2015 00:06 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/25/201511:10 WG817578
Acrolein ND 50.0 1 09/25/201511:10 WG817578
Acrylonitrile ND 10.0 1 09/25/201511:10 WG817578
Benzene ND 1.00 1 09/25/201511:10 WG817578
Bromobenzene ND 1.00 1 09/25/201511:10 WG817578 6
QC
Bromodichloromethane ND 1.00 1 09/25/201511:10 WG817578
Bromoform ND 1.00 1 09/25/201511:10 WG817578 F
Bromomethane ND 5.00 1 09/25/201511:10 WG817578 q
n-Butylbenzene ND 1.00 1 09/25/201511:10 WG817578
sec-Butylbenzene ND 1.00 1 09/25/201511:10 WG817578 FAI
tert-Butylbenzene ND 1.00 1 09/25/201511:10 WG817578
Carbon tetrachloride ND 1.00 1 09/25/201511:10 WG817578 F
Chlorobenzene ND 1.00 1 09/25/201511:10 WG817578
Chlorodibromomethane ND 1.00 1 09/25/201511:10 WG817578
Chloroethane ND 5.00 1 09/25/201511:10 WG817578
2-Chloroethyl vinyl ether ND 50.0 1 09/25/201511:10 WG817578
Chloroform ND 5.00 1 09/25/201511:10 WG817578
Chloromethane ND 2.50 1 09/25/201511:10 WG817578
2-Chlorotoluene ND 1.00 1 09/25/201511:10 WG817578
4-Chlorotoluene ND 1.00 1 09/25/201511:10 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/201511:10 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/201511:10 WG817578
Dibromomethane ND 1.00 1 09/25/201511:10 WG817578
1,2-Dichlo robe nzene ND 1.00 1 09/25/201511:10 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/201511:10 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/201511:10 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/201511:10 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/201511:10 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/201511:10 WG817578
1,1-Dichloroethene 2.79 1.00 1 09/25/201511:10 WG817578
cis-1,2-Dichloroethene 527 20.0 20 09/29/201518:22 WG818281
trans-1,2-Dichloroethene 4.77 1.00 1 09/25/201511:10 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/201511:10 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/201511:10 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/201511:10 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/201511:10 WG817578
trans-13-Dichloropropene ND 1.00 1 09/25/201511:10 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/201511:10 WG817578
Di-isopropyl ether ND 1.00 1 09/25/201511:10 WG817578
Ethylbenzene ND 1.00 1 09/25/201511:10 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/201511:10 WG817578
Isopropylbenzene ND 1.00 1 09/25/201511:10 WG817578
p-Isopropyltoluene 1.41 1.00 1 09/25/201511:10 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/201511:10 WG817578
Methylene Chloride ND 5.00 1 09/25/201511:10 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/201511:10 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/201511:10 WG817578
Naphthalene ND 5.00 1 09/25/201511:10 WG817578
n-Propylbenzene ND 1.00 1 09/25/201511:10 WG817578
Styrene ND 1.00 1 09/25/201511:10 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 42 of 72

RW-6 SAMPLE RESULTS - 18 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 09:30 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/201511:10 WG817578 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/201511:10 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/201511:10 WG817578 F
Tetrachloroethene 14.0 1.00 1 09/25/201511:10 WG817578
Toluene ND 5.00 1 09/25/201511:10 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/201511:10 WG817578 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/25/201511:10 WG817578
1,1,1-Trichloroethane ND 1.00 1 09/25/201511:10 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/201511:10 WG817578
Trichloroethene 26.7 1.00 1 09/25/201511:10 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/201511:10 WG817578 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/25/201511:10 WG817578
1,2,4-Trimethylbenzene ND 1.00 1 09/25/201511:10 WG817578 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/201511:10 WG817578 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/201511:10 WG817578
Vinyl chloride 188 1.00 1 09/25/201511:10 WG817578 FAI
Xylenes,Total ND 3.00 1 09/25/201511:10 WG817578
(S)Toluene-d8 102 90.0-115 091251201511.10 WG817578 F
(S)Dibromofluoromethone 105 79.0-121 091251201511.10 WG817578
(S)4-Bromofluorobenzene 92.0 80.1-120 091251201511.10 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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RW-7 SAMPLE RESULTS - 19 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 09:45 L789514
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 385000 100000 100 09/23/2015 01:47 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone 75.0 50.0 1 09/26/201510:07 WG817621
Acrolein ND J4 50.0 1 09/26/201510:07 WG817621
Acrylonitrile ND 10.0 1 09/26/201510:07 WG817621
Benzene ND 1.00 1 09/26/201510:07 WG817621
Bromobenzene ND 1.00 1 09/26/201510:07 WG817621 6
QC
Bromodichloromethane ND 1.00 1 09/26/201510:07 WG817621
Bromoform ND 1.00 1 09/26/201510:07 WG817621
Bromomethane ND 5.00 1 09/26/201510:07 WG817621 q
n-Butylbenzene ND 1.00 1 09/26/201510:07 WG817621
sec-Butylbenzene ND 1.00 1 09/26/201510:07 WG817621 FAI
tert-Butylbenzene ND 1.00 1 09/26/201510:07 WG817621
Carbon tetrachloride ND 1.00 1 09/26/201510:07 WG817621 FSC
Chlorobenzene ND 1.00 1 09/26/201510:07 WG817621
Chlorodibromomethane ND 1.00 1 09/26/201510:07 WG817621
Chloroethane ND 5.00 1 09/26/201510:07 WG817621
2-Chloroethyl vinyl ether ND 50.0 1 09/26/201510:07 WG817621
Chloroform ND 5.00 1 09/26/201510:07 WG817621
Chloromethane ND 2.50 1 09/26/201510:07 WG817621
2-Chlorotoluene ND 1.00 1 09/26/201510:07 WG817621
4-Chlorotoluene ND 1.00 1 09/26/201510:07 WG817621
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/26/201510:07 WG817621
1,2-Dibromoethane ND 1.00 1 09/26/201510:07 WG817621
Dibromomethane ND 1.00 1 09/26/201510:07 WG817621
1,2-Dichlo robe nzene ND 1.00 1 09/26/201510:07 WG817621
1,3-Dichlorobenzene ND 1.00 1 09/26/201510:07 WG817621
1,4-Dichlorobenzene ND 1.00 1 09/26/201510:07 WG817621
Dichlorodifluoromethane ND 5.00 1 09/26/201510:07 WG817621
1,1-Dichloroethane ND 1.00 1 09/26/201510:07 WG817621
1,2-Dichloroethane ND 1.00 1 09/26/201510:07 WG817621
1,1-Dichloroethene ND 1.00 1 09/26/201510:07 WG817621
cis-1,2-Dichloroethene 570 5.00 5 09/28/201511:42 WG818034
trans-1,2-Dichloroethene NO 1.00 1 09/26/201510:07 WG817621
1,2-Dichloropropane ND 1.00 1 09/26/201510:07 WG817621
1,1-Dichloropropene ND 1.00 1 09/26/201510:07 WG817621
1,3-Dichloropropane ND 1.00 1 09/26/201510:07 WG817621
cis-1,3-Dichloropropene ND 1.00 1 09/26/201510:07 WG817621
trans-13-Dichloropropene ND 1.00 1 09/26/201510:07 WG817621
2,2-Dichloropropane ND 1.00 1 09/26/201510:07 WG817621
Di-isopropyl ether ND 1.00 1 09/26/201510:07 WG817621
Ethylbenzene ND 1.00 1 09/26/201510:07 WG817621
Hexachloro-1,3-butadiene ND 1.00 1 09/26/201510:07 WG817621
Isopropylbenzene ND 1.00 1 09/26/201510:07 WG817621
p-Isopropyltoluene ND 1.00 1 09/26/201510:07 WG817621
2-Butanone(MEK) 37.2 10.0 1 09/26/201510:07 WG817621
Methylene Chloride ND 5.00 1 09/26/201510:07 WG817621
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/26/201510:07 WG817621
Methyl tert-butyl ether ND 1.00 1 09/26/201510:07 WG817621
Naphthalene ND 5.00 1 09/26/201510:07 WG817621
n-Propylbenzene ND 1.00 1 09/26/201510:07 WG817621
Styrene ND 1.00 1 09/26/201510:07 WG817621
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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RW-7 SAMPLE RESULTS - 19 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 09:45 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/26/201510:07 WG817621 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/26/201510:07 WG817621
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/26/201510:07 WG817621 F
Tetrachloroethene 11.6 1.00 1 09/26/201510:07 WG817621
Toluene ND 5.00 1 09/26/201510:07 WG817621
1,2,3-Trichlorobenzene ND 1.00 1 09/26/201510:07 WG817621 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/26/201510:07 WG817621
1,1,1-Trichloroethane ND 1.00 1 09/26/201510:07 WG817621
1,1,2-Trichloroethane ND 1.00 1 09/26/201510:07 WG817621
Trichloroethene ND 1.00 1 09/26/201510:07 WG817621
Trichlorofluoromethane ND 5.00 1 09/26/201510:07 WG817621 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/26/201510:07 WG817621
1,2,4-Trimethylbenzene ND 1.00 1 09/26/201510:07 WG817621 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/26/201510:07 WG817621 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/26/201510:07 WG817621
Vinyl chloride 8.91 1.00 1 09/26/201510:07 WG817621 FAI
Xylenes,Total ND 3.00 1 09/26/201510:07 WG817621
(S)Toluene-d8 107 90.0-115 09/26/201510.07 WG817621 F
(S)Dibromofluoromethone 99.0 79.0-121 09/26/201510.07 WG817621
(S)4-Bromofluorobenzene 98.1 80.1-120 09/26/201510.07 WG817621
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 45 of 72

DUPLICATE SAMPLE RESULTS - 20 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 00:00 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/201511:30 WG817578
Acrolein ND 50.0 1 09/25/201511:30 WG817578
Acrylonitrile ND 10.0 1 09/25/201511:30 WG817578 F
Benzene ND 1.00 1 09/25/201511:30 WG817578
Bromobenzene ND 1.00 1 09/25/201511:30 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/201511:30 WG817578 Cn
Bromoform ND 1.00 1 09/25/201511:30 WG817578
Bromomethane ND 5.00 1 09/25/201511:30 WG817578
n-Butylbenzene ND 1.00 1 09/25/201511:30 WG817578
sec-Butylbenzene ND 1.00 1 09/25/201511:30 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/201511:30 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/201511:30 WG817578
Chlorobenzene ND 1.00 1 09/25/201511:30 WG817578 �GI
Chlorodibromomethane ND 1.00 1 09/25/201511:30 WG817578
Chloroethane ND 5.00 1 09/25/201511:30 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/201511:30 WG817578
Chloroform ND 5.00 1 09/25/201511:30 WG817578
Chloromethane ND 2.50 1 09/25/201511:30 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/201511:30 WG817578
4-Chlorotoluene ND 1.00 1 09/25/201511:30 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/201511:30 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/201511:30 WG817578
Dibromomethane ND 1.00 1 09/25/201511:30 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/201511:30 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/201511:30 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/201511:30 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/201511:30 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/201511:30 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/201511:30 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/201511:30 WG817578
cis-1,2-Dichloroethene 128 1.00 1 09/25/201511:30 WG817578
trans-1,2-Dichloroethene 2.11 1.00 1 09/25/201511:30 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/201511:30 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/201511:30 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/201511:30 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/201511:30 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/201511:30 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/201511:30 WG817578
Di-isopropyl ether ND 1.00 1 09/25/201511:30 WG817578
Ethylbenzene ND 1.00 1 09/25/201511:30 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/201511:30 WG817578
Isopropylbenzene ND 1.00 1 09/25/201511:30 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/201511:30 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/201511:30 WG817578
Methylene Chloride ND 5.00 1 09/25/201511:30 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/201511:30 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/201511:30 WG817578
Naphthalene ND 5.00 1 09/25/201511:30 WG817578
n-Propylbenzene ND 1.00 1 09/25/201511:30 WG817578
Styrene ND 1.00 1 09/25/201511:30 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/201511:30 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/201511:30 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/201511:30 WG817578
Tetrachloroethene 570 20.0 20 09/29/201518:42 WG818281
Toluene ND 5.00 1 09/25/201511:30 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/201511:30 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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DUPLICATE SAMPLE RESULTS - 20 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 00:00 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/201511:30 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/201511:30 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/201511:30 WG817578 F
Trichloroethene 116 1.00 1 09/25/201511:30 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/201511:30 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/201511:30 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/201511:30 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/201511:30 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/201511:30 WG817578
Vinyl chloride ND 1.00 1 09/25/201511:30 WG817578
Xylenes,Total ND 3.00 1 09/25/201511:30 WG817578 6
QC
(S)Toluene-d8 97.9 90.0-115 091251201511:30 WG817578
(S)Dibromofluoromethone 102 79.0-121 091251201511:30 WG817578
(S)4-Bromofluorobenzene 89.3 80.1-120 091251201511.30 WG817578 Fq
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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DUPLICATE B SAMPLE RESULTS - 21 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 00:00 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/201511:50 WG817578
Acrolein ND 50.0 1 09/25/201511:50 WG817578
Acrylonitrile ND 10.0 1 09/25/201511:50 WG817578 F
Benzene ND 1.00 1 09/25/201511:50 WG817578
Bromobenzene ND 1.00 1 09/25/201511:50 WG817578 4
Bromodichloromethane ND 1.00 1 09/25/201511:50 WG817578 Cn
Bromoform ND 1.00 1 09/25/201511:50 WG817578
Bromomethane ND 5.00 1 09/25/201511:50 WG817578
n-Butylbenzene ND 1.00 1 09/25/201511:50 WG817578
sec-Butylbenzene ND 1.00 1 09/25/201511:50 WG817578 6
tert-Butylbenzene ND 1.00 1 09/25/201511:50 WG817578 QC
Carbon tetrachloride ND 1.00 1 09/25/201511:50 WG817578
Chlorobenzene ND 1.00 1 09/25/201511:50 WG817578 7G1
Chlorodibromomethane ND 1.00 1 09/25/201511:50 WG817578
Chloroethane ND 5.00 1 09/25/201511:50 WG817578 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/201511:50 WG817578
Chloroform ND 5.00 1 09/25/201511:50 WG817578
Chloromethane ND 2.50 1 09/25/201511:50 WG817578 F
2-Chlorotoluene ND 1.00 1 09/25/201511:50 WG817578
4-Chlorotoluene ND 1.00 1 09/25/201511:50 WG817578
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/201511:50 WG817578
1,2-Dibromoethane ND 1.00 1 09/25/201511:50 WG817578
Dibromomethane ND 1.00 1 09/25/201511:50 WG817578
1,2-Dichlorobenzene ND 1.00 1 09/25/201511:50 WG817578
1,3-Dichlorobenzene ND 1.00 1 09/25/201511:50 WG817578
1,4-Dichlorobenzene ND 1.00 1 09/25/201511:50 WG817578
Dichlorodifluoromethane ND 5.00 1 09/25/201511:50 WG817578
1,1-Dichloroethane ND 1.00 1 09/25/201511:50 WG817578
1,2-Dichloroethane ND 1.00 1 09/25/201511:50 WG817578
1,1-Dichloroethene ND 1.00 1 09/25/201511:50 WG817578
cis-1,2-Dichloroethene ND 1.00 1 09/25/201511:50 WG817578
trans-1,2-Dichloroethene ND 1.00 1 09/25/201511:50 WG817578
1,2-Dichloropropane ND 1.00 1 09/25/201511:50 WG817578
1,1-Dichloropropene ND 1.00 1 09/25/201511:50 WG817578
1,3-Dichloropropane ND 1.00 1 09/25/201511:50 WG817578
cis-1,3-Dichloropropene ND 1.00 1 09/25/201511:50 WG817578
trans-1,3-Dichloropropene ND 1.00 1 09/25/201511:50 WG817578
2,2-Dichloropropane ND 1.00 1 09/25/201511:50 WG817578
Di-isopropyl ether ND 1.00 1 09/25/201511:50 WG817578
Ethylbenzene ND 1.00 1 09/25/201511:50 WG817578
Hexachloro-1,3-butadiene ND 1.00 1 09/25/201511:50 WG817578
Isopropylbenzene ND 1.00 1 09/25/201511:50 WG817578
p-Isopropyltoluene ND 1.00 1 09/25/201511:50 WG817578
2-Butanone(MEK) ND 10.0 1 09/25/201511:50 WG817578
Methylene Chloride ND 5.00 1 09/25/201511:50 WG817578
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/201511:50 WG817578
Methyl tert-butyl ether ND 1.00 1 09/25/201511:50 WG817578
Naphthalene ND 5.00 1 09/25/201511:50 WG817578
n-Propylbenzene ND 1.00 1 09/25/201511:50 WG817578
Styrene ND 1.00 1 09/25/201511:50 WG817578
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/201511:50 WG817578
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/201511:50 WG817578
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/201511:50 WG817578
Tetrachloroethene 117 1.00 1 09/25/201511:50 WG817578
Toluene ND 5.00 1 09/25/201511:50 WG817578
1,2,3-Trichlorobenzene ND 1.00 1 09/25/201511:50 WG817578
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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DUPLICATE B SAMPLE RESULTS - 21 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 00:00 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/201511:50 WG817578 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/201511:50 WG817578
1,1,2-Trichloroethane ND 1.00 1 09/25/201511:50 WG817578 F
Trichloroethene ND 1.00 1 09/25/201511:50 WG817578
Trichlorofluoromethane ND 5.00 1 09/25/201511:50 WG817578
1,2,3-Trichloropropane ND 2.50 1 09/25/201511:50 WG817578 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/201511:50 WG817578
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/201511:50 WG817578
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/201511:50 WG817578
Vinyl chloride ND 1.00 1 09/25/201511:50 WG817578
Xylenes,Total ND 3.00 1 09/25/201511:50 WG817578 6
QC
(S)Toluene-d8 102 90.0-115 091251201511.50 WG817578
(S)Dibromofluoromethone 104 79.0-121 091251201511:50 WG817578 Fq
(S)4-Bromofluorobenzene 88.2 80.1-120 091251201511.50 WG817578
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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FIELD BLANK 1 SAMPLE RESULTS - 22 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 09:00 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/26/201510:27 WG817621
Acrolein ND J4 50.0 1 09/26/201510:27 WG817621
Acrylonitrile ND 10.0 1 09/26/201510:27 WG817621 F
Benzene ND 1.00 1 09/26/201510:27 WG817621
Bromobenzene ND 1.00 1 09/26/201510:27 WG817621 4
Bromodichloromethane ND 1.00 1 09/26/201510:27 WG817621 Cn
Bromoform ND 1.00 1 09/26/201510:27 WG817621
Bromomethane ND 5.00 1 09/26/201510:27 WG817621
n-Butylbenzene ND 1.00 1 09/26/201510:27 WG817621
sec-Butylbenzene ND 1.00 1 09/26/201510:27 WG817621 Fc
tert-Butylbenzene ND 1.00 1 09/26/201510:27 WG817621
Carbon tetrachloride ND 1.00 1 09/26/201510:27 WG817621
Chlorobenzene ND 1.00 1 09/26/201510:27 WG817621 rq
Chlorodibromomethane ND 1.00 1 09/26/201510:27 WG817621
Chloroethane ND 5.00 1 09/26/201510:27 WG817621 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/26/201510:27 WG817621
Chloroform ND 5.00 1 09/26/201510:27 WG817621
Chloromethane 3.27 2.50 1 09/26/201510:27 WG817621 F
2-Chlorotoluene ND 1.00 1 09/26/201510:27 WG817621
4-Chlorotoluene ND 1.00 1 09/26/201510:27 WG817621
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/26/201510:27 WG817621
1,2-Dibromoethane ND 1.00 1 09/26/201510:27 WG817621
Dibromomethane ND 1.00 1 09/26/201510:27 WG817621
1,2-Dichlorobenzene ND 1.00 1 09/26/201510:27 WG817621
1,3-Dichlorobenzene ND 1.00 1 09/26/201510:27 WG817621
1,4-Dichlorobenzene ND 1.00 1 09/26/201510:27 WG817621
Dichlorodifluoromethane ND 5.00 1 09/26/201510:27 WG817621
1,1-Dichloroethane ND 1.00 1 09/26/201510:27 WG817621
1,2-Dichloroethane ND 1.00 1 09/26/201510:27 WG817621
1,1-Dichloroethene ND 1.00 1 09/26/201510:27 WG817621
cis-1,2-Dichloroethene ND 1.00 1 09/26/201510:27 WG817621
trans-1,2-Dichloroethene ND 1.00 1 09/26/201510:27 WG817621
1,2-Dichloropropane ND 1.00 1 09/26/201510:27 WG817621
1,1-Dichloropropene ND 1.00 1 09/26/201510:27 WG817621
1,3-Dichloropropane ND 1.00 1 09/26/201510:27 WG817621
cis-1,3-Dichloropropene ND 1.00 1 09/26/201510:27 WG817621
trans-1,3-Dichloropropene ND 1.00 1 09/26/201510:27 WG817621
2,2-Dichloropropane ND 1.00 1 09/26/201510:27 WG817621
Di-isopropyl ether ND 1.00 1 09/26/201510:27 WG817621
Ethylbenzene ND 1.00 1 09/26/201510:27 WG817621
Hexachloro-1,3-butadiene ND 1.00 1 09/26/201510:27 WG817621
Isopropylbenzene ND 1.00 1 09/26/201510:27 WG817621
p-Isopropyltoluene ND 1.00 1 09/26/201510:27 WG817621
2-Butanone(MEK) ND 10.0 1 09/26/201510:27 WG817621
Methylene Chloride ND 5.00 1 09/26/201510:27 WG817621
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/26/201510:27 WG817621
Methyl tert-butyl ether ND 1.00 1 09/26/201510:27 WG817621
Naphthalene ND 5.00 1 09/26/201510:27 WG817621
n-Propylbenzene ND 1.00 1 09/26/201510:27 WG817621
Styrene ND 1.00 1 09/26/201510:27 WG817621
1,1,1,2-Tetrachloroethane ND 1.00 1 09/26/201510:27 WG817621
1,1,2,2-Tetrachloroethane ND 1.00 1 09/26/201510:27 WG817621
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/26/201510:27 WG817621
Tetrachloroethene ND 1.00 1 09/26/201510:27 WG817621
Toluene ND 5.00 1 09/26/201510:27 WG817621
1,2,3-Trichlorobenzene ND 1.00 1 09/26/201510:27 WG817621
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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FIELD BLANK 1 SAMPLE RESULTS - 22 ONE LAB.NATIONWIDE.
Collected date/time: 09/15/15 09:00 L789514
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/26/201510:27 WG817621 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/26/201510:27 WG817621
1,1,2-Trichloroethane ND 1.00 1 09/26/201510:27 WG817621 F
Trichloroethene ND 1.00 1 09/26/201510:27 WG817621
Trichlorofluoromethane ND 5.00 1 09/26/201510:27 WG817621
1,2,3-Trichloropropane ND 2.50 1 09/26/201510:27 WG817621 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/26/201510:27 WG817621
1,2,3-Trim ethyl benzene ND 1.00 1 09/26/201510:27 WG817621
1,3,5-Trim ethyl benzene ND 1.00 1 09/26/201510:27 WG817621
Vinyl chloride ND 1.00 1 09/26/201510:27 WG817621
Xylenes,Total ND 3.00 1 09/26/201510:27 WG817621 6
QC
(S)Toluene-d8 108 90.0-115 09/26/201510.27 WG817621
(S)Dibromofluoromethone 98.5 79.0-121 09/26/201510.27 WG817621 rq
(S)4-Bromofluorobenzene 96.2 80.1-120 09/26/201510.27 WG817621
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816627 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Wet Chemistry by Method 9060A L789514-01,02,03,04,05,06,14,15,17,18,19
Method Blank (MB) FP1(MB)09/22/1515:58
MB Result MB Qualifier MB RDL
FT
Analyte mg/I mg/ICTOC ND 1.00
rsS
L789444-07 Original Sample (OS) • Duplicate (DUP)
(OS)09/22/1518:05•(DUP)09/22/15 19:29 4Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
FSr
Analyte mg/I mg/I % %
TOC 6.24 6.30 1 0.957 20
L789514-03 Original Sample (OS) • Duplicate (DUP)
(OS)09/22/15 22:08•(DUP)09/22/15 23:00 GI
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/I mg/I % % $AI
TOC 1.98 2.00 1 1.01 20
Sc
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 9
(LCS)09/22/1516:59•(LCSD)09/22/1517:16
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
TOC 75.0 73.2 73.6 97.6 98.1 85.0-115 0.559 20
L789444-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)09/22/1518:22•(MS)09/22/15 18:39•(MSD)09/22/1518:59
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % %
TOC 50.0 0.910 49.4 49.5 98.7 99.0 1 80.0-120 0.243 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817578 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789514-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21
Method Blank (MB) FP1(MB)09/25/15 03:38
MB Result MB Qualifier MB RDL
FTC
Analyte mg/I mg/I
Acetone ND 0.0500
Acrolein ND 0.0500 FSS
Acrylonitrile ND 0.0100
Benzene ND 0.00100 [Cn]
Bromobenzene ND 0.00100
Bromodichloromethane ND 0.00100
Bromoform ND 0.00100 FSr
Bromomethane ND 0.00500
n-Butylbenzene ND 0.00100
sec-Butyl benzene ND 0.00100
tert-Butyl benzene ND 0.00100
Carbon tetrachloride ND 0.00100 7G1
Chlorobenzene ND 0.00100
Chlorodibromomethane ND 0.00100
Chloroethane ND 0.00500 FAI
2-Chloroethyl vinyl ether ND 0.0500
Chloroform ND 0.00500 FSC
Chloromethane ND 0.00250
2-Chlorotoluene ND 0.00100
4-Chlorotoluene ND 0.00100
1,2-Dibromo-3-Chloropropane ND 0.00500
1,2-Dibromoethane ND 0.00100
Dibromomethane ND 0.00100
1,2-Dichlorobenzene ND 0.00100
1,3-Dichlorobenzene ND 0.00100
1,4-Dichlorobenzene ND 0.00100
Dichlorodifluoromethane ND 0.00500
1,1-Dichloroethane ND 0.00100
1,2-Dichloroethane ND 0.00100
1,1-Dichloroethene ND 0.00100
cis-1,2-Dichloroethene ND 0.00100
trans-1,2-Dichloroethene ND 0.00100
1,2-Dichloropropane ND 0.00100
1,1-Dichloropropene ND 0.00100
1,3-Dichloropropane ND 0.00100
cis-1,3-Dichloropropene ND 0.00100
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817578 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789514-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21
Method Blank (MB) FP1(MB)09/25/15 03:38
MB Result MB Qualifier MB RDL
z
Analyte mg/I mg/I TC
trans-1,3-Dichloropropene ND 0.00100
2,2-Dichloropropane ND 0.00100 FSS
Di-isopropyl ether ND 0.00100
Ethylbenzene ND 0.00100 [Cn]
Hexachloro-1,3-butadiene ND 0.00100
Isopropylbenzene ND 0.00100
p-Isopropyltoluene ND 0.00100 FSr
2-Butanone(MEK) ND 0.0100
Methylene Chloride ND 0.00500
4-Methyl-2-pentanone(MIBK) ND 0.0100
Methyl tert-butyl ether ND 0.00100
Naphthalene ND 0.00500 GI
n-Propylbenzene ND 0.00100
Styrene ND 0.00100 FAI
1,1,1,2-Tetrachloroethane ND 0.00100
1,1,2,2-Tetrachloroethane ND 0.00100
Tetrachloroethene ND 0.00100 FSC
Toluene ND 0.00500
1,1,2-Trichlorotrifluoroethane ND 0.00100
1,2,3-Trichlorobenzene ND 0.00100
1,2,4-Trichlorobenzene ND 0.00100
1,1,1-Trichloroethane ND 0.00100
1,1,2-Trichloroethane ND 0.00100
Trichloroethene ND 0.00100
Trichlorofluoromethane ND 0.00500
1,2,3-Trichloropropane ND 0.00250
1,2,3-Trimethylbenzene ND 0.00100
1,2,4-Trim ethyl benzene ND 0.00100
1,3,5-Trimethylbenzene ND 0.00100
Vinyl chloride ND 0.00100
Xylenes,Total ND 0.00300
(S)Toluene-d8 103 90.0-115
(S)Dibromofluoromethane 107 79.0-121
(S)4-Bromofluorobenzene 91.2 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817578 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789514-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1
(LCS)09/25/15 02:19•(LCSD)09/25/15 02:39
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits FTC
Analyte mg/I mg/I mg/I % % % % %
Acetone 0.125 0.215 0.193 172 155 28.7-175 10.5 20.9
Acrolein 0.125 0.198 0.181 158 145 40.4-172 8.74 20 FSS
Acrylonitrile 0.125 0.158 0.146 126 117 58.2-145 7.57 20
Benzene 0.0250 0.0275 0.0273 110 109 73.0-122 0.590 20 [Cn]
Bromobenzene 0.0250 0.0262 0.0267 105 107 81.5-115 1.65 20
Bromodichloromethane 0.0250 0.0261 0.0259 104 103 75.5-121 0.740 20
Bromoform 0.0250 0.0254 0.0257 102 103 71.5-131 1.20 20 FSr
Bromomethane 0.0250 0.0220 0.0220 88.0 87.8 22.4-187 0.160 20
n-Butylbenzene 0.0250 0.0302 0.0306 121 122 75.9-134 1.10 20
sec-Butyl benzene 0.0250 0.0266 0.0274 106 110 80.6-126 2.91 20
tert-Butyl benzene 0.0250 0.0259 0.0267 104 107 79.3-127 2.91 20
Carbon tetrachloride 0.0250 0.0294 0.0290 118 116 70.9-129 1.29 20 7G1
Chlorobenzene 0.0250 0.0252 0.0256 101 102 79.7-122 1.75 20
Chlorodibromomethane 0.0250 0.0259 0.0261 103 105 78.2-124 1.02 20
Chloroethane 0.0250 0.0269 0.0270 108 108 41.2-153 0.300 20 FAI
2-Chloroethyl vinyl ether 0.125 0.123 0.116 98.4 92.9 23.4-162 5.73 23.5
Chloroform 0.0250 0.0276 0.0276 110 110 73.2-125 0.0200 20 FSC
Chloromethane 0.0250 0.0299 0.0303 120 121 55.8-134 1.19 20
2-Chlorotoluene 0.0250 0.0243 0.0249 97.3 99.8 76.4-125 2.47 20
4-Chlorotoluene 0.0250 0.0265 0.0271 106 108 81.5-121 2.13 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0281 0.0258 112 103 64.8-131 8.19 20
1,2-Dibromoethane 0.0250 0.0262 0.0264 105 105 79.8-122 0.420 20
Dibromomethane 0.0250 0.0272 0.0267 109 107 79.5-118 1.82 20
1,2-Dichlorobenzene 0.0250 0.0283 0.0284 113 114 84.7-118 0.510 20
1,3-Dichlorobenzene 0.0250 0.0260 0.0264 104 106 77.6-127 1.55 20
1,4-Dichlorobenzene 0.0250 0.0274 0.0277 110 111 82.2-114 1.01 20
Dichlorodifluoromethane 0.0250 0.0253 0.0256 101 103 56.0-134 1.51 20
1,1-Dichloroethane 0.0250 0.0300 0.0298 120 119 71.7-127 0.590 20
1,2-Dichloroethane 0.0250 0.0289 0.0280 116 112 65.3-126 3.17 20
1,1-Dichloroethene 0.0250 0.0314 0.0315 126 126 59.9-137 0.370 20
cis-1,2-Dichloroethene 0.0250 0.0274 0.0274 110 109 77.3-122 0.180 20
trans-1,2-Dichloroethene 0.0250 0.0280 0.0276 112 110 72.6-125 1.50 20
1,2-Dichloropropane 0.0250 0.0284 0.0286 113 115 77.4-125 0.980 20
1,1-Dichloropropene 0.0250 0.0287 0.0286 115 114 72.5-127 0.320 20
1,3-Dichloropropane 0.0250 0.0264 0.0264 106 106 80.6-115 0.120 20
cis-1,3-Dichloropropene 0.0250 0.0276 0.0274 110 110 77.7-124 0.510 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817578 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789514-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1
(LCS)09/25/15 02:19•(LCSD)09/25/15 02:39
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z
Analyte mg/I mg/I mg/I % % % % % TC
trans-1,3-Dichloropropene 0.0250 0.0276 0.0268 ill 107 73.5-127 2.92 20
2,2-Dichloropropane 0.0250 0.0287 0.0293 115 117 61.3-134 1.88 20 FSS
Di-isopropyl ether 0.0250 0.0313 0.0309 125 123 65.1-135 1.51 20
Ethylbenzene 0.0250 0.0247 0.0252 98.9 101 80.9-121 1.95 20 [Cn]
Hexachloro-1,3-butadiene 0.0250 0.0286 0.0295 115 118 73.7-133 2.97 20
Isopropylbenzene 0.0250 0.0255 0.0262 102 105 81.6-124 2.94 20
p-Isopropyltoluene 0.0250 0.0266 0.0274 106 109 77.6-129 2.84 20 FSr
2-Butanone(MEK) 0.125 0.184 0.163 147 131 46.4-155 12.0 20
Methylene Chloride 0.0250 0.0267 0.0268 107 107 69.5-120 0.630 20
4-Methyl-2-pentanone(MIBK) 0.125 0.152 0.139 122 112 63.3-138 8.88 20
Methyl tert-butyl ether 0.0250 0.0287 0.0281 115 113 70.1-125 2.05 20
Naphthalene 0.0250 0.0281 0.0275 112 110 69.7-134 2.11 20 7G1
n-Propylbenzene 0.0250 0.0268 0.0274 107 110 81.9-122 2.26 20
Styrene 0.0250 0.0249 0.0256 99.7 102 79.9-124 2.69 20 FAI
1,1,1,2-Tetrachloroethane 0.0250 0.0253 0.0257 101 103 78.5-125 1.84 20
1,1,2,2-Tetrachloroethane 0.0250 0.0277 0.0269 ill 107 79.3-123 3.16 20
Tetrachloroethene 0.0250 0.0251 0.0256 100 102 73.5-130 2.12 20 FSC
Toluene 0.0250 0.0250 0.0251 100 100 77.9-116 0.160 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0294 0.0293 117 117 62.0-141 0.220 20
1,2,3-Trichlorobenzene 0.0250 0.0283 0.0282 113 113 75.7-134 0.300 20
1,2,4-Trichlorobenzene 0.0250 0.0285 0.0286 114 115 76.1-136 0.300 20
1,1,1-Trichloroethane 0.0250 0.0284 0.0287 113 115 71.1-129 1.15 20
1,1,2-Trichloroethane 0.0250 0.0252 0.0250 101 100 81.6-120 0.670 20
Trichloroethene 0.0250 0.0260 0.0260 104 104 79.5-121 0.0800 20
Trichlorofluoromethane 0.0250 0.0263 0.0265 105 106 49.1-157 0.900 20
1,2,3-Trichloropropane 0.0250 0.0279 0.0267 112 107 74.9-124 4.37 20
1,2,3-Trimethylbenzene 0.0250 0.0274 0.0277 109 ill 79.9-118 1.31 20
1,2,4-Trim ethyl benzene 0.0250 0.0252 0.0259 101 104 79.0-122 2.75 20
1,3,5-Trimethylbenzene 0.0250 0.0259 0.0265 104 106 81.0-123 2.14 20
Vinyl chloride 0.0250 0.0290 0.0290 116 116 61.5-134 0.110 20
Xylenes,Total 0.0750 0.0734 0.0753 97.9 100 79.2-122 2.51 20
(S)Toluene-d8 102 102 90.0-115
(S)Dibromofluoromethane 108 107 79.0-121
(S)4-Bromofluorobenzene 91.0 94.1 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817578 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789514-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21
L789514-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/25/15 05:29•(MS)09/25/15 04:29•(MSD)09/25/15 04:49
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits FTC
Analyte mg/I mg/I mg/I mg/I % % % % %
Acetone 0.125 0.00177 0.0963 0.0975 75.7 76.6 1 25.0-156 1.18 21.5
Acrolein 0.125 ND 0.174 0.175 139 140 1 34.0-194 0.300 21.5 FSS
Acrylonitrile 0.125 ND 0.158 0.161 126 129 1 55.9-161 1.84 20
Benzene 0.0250 ND 0.0264 0.0257 105 103 1 58.6-133 2.65 20 [Cn]
Bromobenzene 0.0250 ND 0.0254 0.0249 102 99.5 1 70.6-125 2.26 20
Bromodichloromethane 0.0250 ND 0.0252 0.0247 101 98.8 1 69.2-127 2.07 20
Bromoform 0.0250 ND 0.0252 0.0251 101 100 1 66.3-140 0.320 20 FSr
Bromomethane 0.0250 ND 0.0201 0.0198 80.4 79.3 1 16.6-183 1.42 20.5
n-Butylbenzene 0.0250 ND 0.0278 0.0277 111 111 1 64.8-145 0.370 20
sec-Butyl benzene 0.0250 ND 0.0242 0.0244 96.9 97.8 1 66.8-139 0.940 20
tert-Butyl benzene 0.0250 ND 0.0238 0.0238 95.2 95.2 1 67.1-138 0.0700 20
Carbon tetrachloride 0.0250 ND 0.0272 0.0269 109 108 1 60.6-139 0.960 20 7G1
Chlorobenzene 0.0250 ND 0.0246 0.0240 98.3 96.2 1 70.1-130 2.14 20
Chlorodibromomethane 0.0250 ND 0.0255 0.0253 102 101 1 71.6-132 0.690 20
Chloroethane 0.0250 ND 0.0250 0.0243 100 97.2 1 33.3-155 3.03 20 FAI
2-Chloroethyl vinyl ether 0.125 ND 0.00608 0.00153 4.86 1.22 1 5.00-149 J6 J3 J6 120 40
Chloroform 0.0250 ND 0.0262 0.0259 105 104 1 66.1-133 1.22 20 FSC
Chloromethane 0.0250 ND 0.0276 0.0273 110 109 1 40.7-139 0.920 20
2-Chlorotoluene 0.0250 ND 0.0226 0.0225 90.2 90.2 1 66.9-134 0.0400 20
4-Chlorotoluene 0.0250 ND 0.0251 0.0247 100 99.0 1 66.8-134 1.23 20
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.0269 0.0280 108 112 1 63.9-142 4.02 20.2
1,2-Dibromoethane 0.0250 ND 0.0261 0.0263 104 105 1 73.8-131 0.850 20
Dibromomethane 0.0250 ND 0.0271 0.0267 108 107 1 72.8-127 1.59 20
1,2-Dichlorobenzene 0.0250 ND 0.0264 0.0269 105 108 1 77.4-127 2.18 20
1,3-Dichlorobenzene 0.0250 ND 0.0243 0.0242 97.0 96.9 1 67.9-136 0.120 20
1,4-Dichlorobenzene 0.0250 ND 0.0264 0.0260 106 104 1 74.4-123 1.54 20
Dichlorodifluoromethane 0.0250 ND 0.0231 0.0231 92.4 92.2 1 42.2-146 0.180 20
1,1-Dichloroethane 0.0250 ND 0.0281 0.0278 112 111 1 64.0-134 0.980 20
1,2-Dichloroethane 0.0250 ND 0.0284 0.0280 114 112 1 60.7-132 1.50 20
1,1-Dichloroethene 0.0250 ND 0.0293 0.0287 117 115 1 48.8-144 2.16 20
cis-1,2-Dichloroethene 0.0250 ND 0.0254 0.0254 102 102 1 60.6-136 0.170 20
trans-1,2-Dichloroethene 0.0250 ND 0.0254 0.0256 102 102 1 61.0-132 0.570 20
1,2-Dichloropropane 0.0250 ND 0.0280 0.0271 112 108 1 69.7-130 3.15 20
1,1-Dichloropropene 0.0250 ND 0.0270 0.0264 108 105 1 61.5-136 2.52 20
1,3-Dichloropropane 0.0250 ND 0.0266 0.0260 106 104 1 74.3-123 2.24 20
cis-1,3-Dichloropropene 0.0250 ND 0.0270 0.0263 108 105 1 71.1-129 2.82 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817578 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789514-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,20,21
L789514-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/25/15 05:29•(MS)09/25/15 04:29•(MSD)09/25/15 04:49
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits z
Analyte mg/I mg/I mg/I mg/I % % % % % TC
trans-1,3-Dichloropropene 0.0250 ND 0.0285 0.0276 114 110 1 66.3-136 3.27 20
2,2-Dichloropropane 0.0250 ND 0.0268 0.0267 107 107 1 54.9-142 0.290 20 FSS
Di-isopropyl ether 0.0250 ND 0.0295 0.0297 118 119 1 59.9-140 0.530 20
Ethylbenzene 0.0250 ND 0.0236 0.0231 94.5 92.4 1 62.7-136 2.31 20 [Cn]
Hexachloro-1,3-butadiene 0.0250 0.000323 0.0263 0.0267 104 106 1 61.1-144 1.64 20.1
Isopropylbenzene 0.0250 ND 0.0238 0.0236 95.1 94.4 1 67.4-136 0.730 20
p-Isopropyltoluene 0.0250 ND 0.0241 0.0243 96.4 97.3 1 62.8-143 0.950 20 FSr
2-Butanone(MEK) 0.125 0.000772 0.130 0.130 103 103 1 45.0-156 0.0400 20.8
Methylene Chloride 0.0250 0.000396 0.0251 0.0256 98.7 101 1 61.5-125 2.22 20
4-Methyl-2-pentanone(MIBK) 0.125 0.000302 0.148 0.152 118 121 1 60.7-150 2.46 20
Methyl tert-butyl ether 0.0250 ND 0.0272 0.0277 109 ill 1 61.4-136 1.93 20
Naphthalene 0.0250 0.000636 0.0270 0.0283 105 ill 1 61.8-143 4.73 20 7G1
n-Propylbenzene 0.0250 ND 0.0251 0.0247 100 98.7 1 63.2-139 1.65 20
Styrene 0.0250 ND 0.0243 0.0235 97.2 94.0 1 68.2-133 3.33 20 FAI
1,1,1,2-Tetrachloroethane 0.0250 ND 0.0241 0.0244 96.3 97.4 1 70.5-132 1.11 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.0272 0.0281 109 112 1 64.9-145 3.19 20
Tetrachloroethene 0.0250 0.0962 0.112 0.104 62.9 29.9 1 57.4-141 J6 7.66 20 FSC
Toluene 0.0250 ND 0.0243 0.0233 97.2 93.2 1 67.8-124 4.17 20
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.0271 0.0265 108 106 1 53.7-150 2.17 20
1,2,3-Trichlorobenzene 0.0250 0.000560 0.0263 0.0267 103 105 1 65.7-143 1.73 20
1,2,4-Trichlorobenzene 0.0250 0.000358 0.0263 0.0268 104 106 1 67.0-146 2.05 20
1,1,1-Trichloroethane 0.0250 ND 0.0263 0.0262 105 105 1 58.7-134 0.230 20
1,1,2-Trichloroethane 0.0250 ND 0.0249 0.0253 99.7 101 1 74.1-130 1.60 20
Trichloroethene 0.0250 ND 0.0245 0.0239 98.2 95.5 1 48.9-148 2.75 20
Trichlorofluoromethane 0.0250 ND 0.0242 0.0235 96.7 94.1 1 39.9-165 2.76 20
1,2,3-Trichloropropane 0.0250 ND 0.0271 0.0280 108 112 1 71.5-134 3.09 20
1,2,3-Trimethylbenzene 0.0250 ND 0.0252 0.0254 101 102 1 62.7-133 0.810 20
1,2,4-Trim ethyl benzene 0.0250 ND 0.0231 0.0234 92.3 93.6 1 60.5-137 1.44 20
1,3,5-Trimethylbenzene 0.0250 ND 0.0238 0.0238 95.2 95.1 1 67.9-134 0.0500 20
Vinyl chloride 0.0250 ND 0.0260 0.0260 104 104 1 44.3-143 0.0600 20
Xylenes,Total 0.0750 ND 0.0700 0.0684 93.3 91.1 1 65.6-133 2.36 20
(S)Toluene-d8 102 102 90.0-115
(S)Dibromofluoromethane 105 107 79.0-121
(S)4-Bromofluorobenzene 91.5 92.0 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817621 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B 1-789514-19,22
Method Blank (MB) FP1(MB)09/26/15 07:48
MB Result MB Qualifier MB RDL
z
Analyte mg/I mg/I _ TC
Acetone ND 0.0500
Acrolein ND 0.0500 FSS
Acrylonitrile ND 0.0100
Benzene ND 0.00100 [Cn]
Bromobenzene ND 0.00100
Bromodichloromethane ND 0.00100
Bromoform ND 0.00100 FSr
Bromomethane ND 0.00500
n-Butylbenzene ND 0.00100
sec-Butyl benzene ND 0.00100
tert-Butyl benzene ND 0.00100
Carbon tetrachloride ND 0.00100 7G1
Chlorobenzene ND 0.00100
Chlorodibromomethane ND 0.00100
Chloroethane ND 0.00500 FAI
2-Chloroethyl vinyl ether ND 0.0500
Chloroform ND 0.00500 FSC
Chloromethane ND 0.00250
2-Chlorotoluene ND 0.00100
4-Chlorotoluene ND 0.00100
1,2-Dibromo-3-Chloropropane ND 0.00500
1,2-Dibromoethane ND 0.00100
Dibromomethane ND 0.00100
1,2-Dichlorobenzene ND 0.00100
1,3-Dichlorobenzene ND 0.00100
1,4-Dichlorobenzene ND 0.00100
Dichlorodifluoromethane ND 0.00500
1,1-Dichloroethane ND 0.00100
1,2-Dichloroethane ND 0.00100
1,1-Dichloroethene ND 0.00100
cis-1,2-Dichloroethene ND 0.00100
trans-1,2-Dichloroethene ND 0.00100
1,2-Dichloropropane ND 0.00100
1,1-Dichloropropene ND 0.00100
1,3-Dichloropropane ND 0.00100
cis-1,3-Dichloropropene ND 0.00100
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789514 10/01/15 09:52 59 of 72

WG817621 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B 1-789514-19,22
Method Blank (MB) FP1(MB)09/26/15 07:48
MB Result MB Qualifier MB RDL
z
Analyte mg/I mg/I TC
trans-1,3-Dichloropropene ND 0.00100
2,2-Dichloropropane ND 0.00100 FSS
Di-isopropyl ether ND 0.00100
Ethylbenzene ND 0.00100 [Cn]
Hexachloro-1,3-butadiene ND 0.00100
Isopropylbenzene ND 0.00100
p-Isopropyltoluene ND 0.00100 FSr
2-Butanone(MEK) ND 0.0100
Methylene Chloride ND 0.00500
4-Methyl-2-pentanone(MIBK) ND 0.0100
Methyl tert-butyl ether ND 0.00100
Naphthalene ND 0.00500 GI
n-Propylbenzene ND 0.00100
Styrene ND 0.00100 FAI
1,1,1,2-Tetrachloroethane ND 0.00100
1,1,2,2-Tetrachloroethane ND 0.00100
Tetrachloroethene ND 0.00100 FSC
Toluene ND 0.00500
1,1,2-Trichlorotrifluoroethane ND 0.00100
1,2,3-Trichlorobenzene ND 0.00100
1,2,4-Trichlorobenzene ND 0.00100
1,1,1-Trichloroethane ND 0.00100
1,1,2-Trichloroethane ND 0.00100
Trichloroethene ND 0.00100
Trichlorofluoromethane ND 0.00500
1,2,3-Trichloropropane ND 0.00250
1,2,3-Trimethylbenzene ND 0.00100
1,2,4-Trim ethyl benzene ND 0.00100
1,3,5-Trimethylbenzene ND 0.00100
Vinyl chloride ND 0.00100
Xylenes,Total ND 0.00300
(S)Toluene-d8 108 90.0-115
(S)Dibromofluoromethane 97.6 79.0-121
(S)4-Bromofluorobenzene 96.4 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817621 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B 1-789514-19,22
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1
(LCS)09/26/15 05:50•(LCSD)09/26/15 06:10
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits FTC
Analyte mg/I mg/I mg/I % % % % %
Acetone 0.125 0.122 0.122 97.5 97.7 28.7-175 0.240 20.9
Acrolein 0.125 0.232 0.235 186 188 40.4-172 J4 J4 1.26 20 FSS
Acrylonitrile 0.125 0.138 0.137 110 110 58.2-145 0.120 20
Benzene 0.0250 0.0226 0.0227 90.3 90.7 73.0-122 0.460 20 [Cn]
Bromobenzene 0.0250 0.0244 0.0245 97.7 97.9 81.5-115 0.220 20
Bromodichloromethane 0.0250 0.0268 0.0266 107 106 75.5-121 0.900 20
Bromoform 0.0250 0.0267 0.0266 107 106 71.5-131 0.450 20 FSr
Bromomethane 0.0250 0.0200 0.0199 79.9 79.7 22.4-187 0.250 20
n-Butylbenzene 0.0250 0.0239 0.0240 95.5 95.9 75.9-134 0.400 20
sec-Butyl benzene 0.0250 0.0247 0.0244 99.0 97.4 80.6-126 1.59 20
tert-Butyl benzene 0.0250 0.0243 0.0243 97.2 97.3 79.3-127 0.110 20
Carbon tetrachloride 0.0250 0.0216 0.0214 86.3 85.7 70.9-129 0.750 20 7G1
Chlorobenzene 0.0250 0.0229 0.0231 91.5 92.5 79.7-122 1.09 20
Chlorodibromomethane 0.0250 0.0252 0.0255 101 102 78.2-124 1.11 20
Chloroethane 0.0250 0.0203 0.0202 81.2 80.8 41.2-153 0.410 20 FAI
2-Chloroethyl vinyl ether 0.125 0.145 0.143 116 114 23.4-162 1.22 23.5
Chloroform 0.0250 0.0230 0.0231 92.1 92.5 73.2-125 0.420 20 FSC
Chloromethane 0.0250 0.0239 0.0239 95.7 95.8 55.8-134 0.100 20
2-Chlorotoluene 0.0250 0.0243 0.0243 97.1 97.1 76.4-125 0.0800 20
4-Chlorotoluene 0.0250 0.0238 0.0238 95.3 95.1 81.5-121 0.190 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0220 0.0214 88.0 85.6 64.8-131 2.79 20
1,2-Dibromoethane 0.0250 0.0241 0.0245 96.3 98.0 79.8-122 1.79 20
Dibromomethane 0.0250 0.0267 0.0262 107 105 79.5-118 1.99 20
1,2-Dichlorobenzene 0.0250 0.0246 0.0248 98.3 99.4 84.7-118 1.09 20
1,3-Dichlorobenzene 0.0250 0.0253 0.0252 101 101 77.6-127 0.300 20
1,4-Dichlorobenzene 0.0250 0.0229 0.0229 91.7 91.7 82.2-114 0.0100 20
Dichlorodifluoromethane 0.0250 0.0187 0.0191 74.9 76.5 56.0-134 2.18 20
1,1-Dichloroethane 0.0250 0.0243 0.0244 97.3 97.5 71.7-127 0.160 20
1,2-Dichloroethane 0.0250 0.0261 0.0261 104 104 65.3-126 0.170 20
1,1-Dichloroethene 0.0250 0.0233 0.0234 93.4 93.7 59.9-137 0.360 20
cis-1,2-Dichloroethene 0.0250 0.0225 0.0227 89.9 90.8 77.3-122 0.980 20
trans-1,2-Dichloroethene 0.0250 0.0220 0.0217 88.0 86.8 72.6-125 1.37 20
1,2-Dichloropropane 0.0250 0.0283 0.0284 113 113 77.4-125 0.370 20
1,1-Dichloropropene 0.0250 0.0222 0.0226 88.9 90.3 72.5-127 1.55 20
1,3-Dichloropropane 0.0250 0.0236 0.0240 94.4 96.0 80.6-115 1.73 20
cis-1,3-Dichloropropene 0.0250 0.0272 0.0272 109 109 77.7-124 0.0800 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817621 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B 1-789514-19,22
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1
(LCS)09/26/15 05:50•(LCSD)09/26/15 06:10
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z
Analyte mg/I mg/I mg/I % % % % % TC
trans-1,3-Dichloropropene 0.0250 0.0253 0.0251 101 100 73.5-127 1.06 20
2,2-Dichloropropane 0.0250 0.0218 0.0215 87.3 85.8 61.3-134 1.68 20 FSS
Di-isopropyl ether 0.0250 0.0289 0.0286 115 114 65.1-135 0.840 20
Ethylbenzene 0.0250 0.0223 0.0225 89.1 90.2 80.9-121 1.23 20 [Cn]
Hexachloro-1,3-butadiene 0.0250 0.0252 0.0251 101 100 73.7-133 0.410 20
Isopropylbenzene 0.0250 0.0230 0.0231 91.9 92.3 81.6-124 0.390 20
p-Isopropyltoluene 0.0250 0.0258 0.0255 103 102 77.6-129 0.860 20 FSr
2-Butanone(MEK) 0.125 0.132 0.130 105 104 46.4-155 1.57 20
Methylene Chloride 0.0250 0.0217 0.0218 86.8 87.3 69.5-120 0.560 20
4-Methyl-2-pentanone(MIBK) 0.125 0.151 0.146 121 117 63.3-138 3.43 20
Methyl tert-butyl ether 0.0250 0.0253 0.0247 101 98.7 70.1-125 2.37 20
Naphthalene 0.0250 0.0225 0.0228 89.9 91.2 69.7-134 1.36 20 7G1
n-Propylbenzene 0.0250 0.0237 0.0237 94.7 94.9 81.9-122 0.260 20
Styrene 0.0250 0.0245 0.0248 98.1 99.4 79.9-124 1.29 20 FAI
1,1,1,2-Tetrachloroethane 0.0250 0.0246 0.0241 98.4 96.6 78.5-125 1.85 20
1,1,2,2-Tetrachloroethane 0.0250 0.0265 0.0257 106 103 79.3-123 2.90 20
Tetrachloroethene 0.0250 0.0214 0.0217 85.6 87.0 73.5-130 1.61 20 FSC
Toluene 0.0250 0.0233 0.0233 93.0 93.1 77.9-116 0.100 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0208 0.0209 83.4 83.8 62.0-141 0.510 20
1,2,3-Trichlorobenzene 0.0250 0.0232 0.0238 92.7 95.1 75.7-134 2.57 20
1,2,4-Trichlorobenzene 0.0250 0.0240 0.0245 95.8 98.0 76.1-136 2.28 20
1,1,1-Trichloroethane 0.0250 0.0216 0.0216 86.4 86.3 71.1-129 0.100 20
1,1,2-Trichloroethane 0.0250 0.0241 0.0242 96.6 96.8 81.6-120 0.200 20
Trichloroethene 0.0250 0.0239 0.0242 95.4 96.8 79.5-121 1.48 20
Trichlorofluoromethane 0.0250 0.0202 0.0199 80.9 79.5 49.1-157 1.71 20
1,2,3-Trichloropropane 0.0250 0.0250 0.0245 100 98.1 74.9-124 1.98 20
1,2,3-Trimethylbenzene 0.0250 0.0238 0.0234 95.2 93.6 79.9-118 1.63 20
1,2,4-Trim ethyl benzene 0.0250 0.0249 0.0248 99.5 99.0 79.0-122 0.470 20
1,3,5-Trimethylbenzene 0.0250 0.0242 0.0242 96.8 96.9 81.0-123 0.0700 20
Vinyl chloride 0.0250 0.0218 0.0216 87.0 86.4 61.5-134 0.740 20
Xylenes,Total 0.0750 0.0682 0.0687 90.9 91.5 79.2-122 0.730 20
(S)Toluene-d8 109 108 90.0-115
(S)Dibromofluoromethane 97.7 978 79.0-121
(S)4-Bromofluorobenzene 99.2 99.5 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817621 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B 1-789514-19,22
L789697-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/26/15 09:47•(MS)09/26/15 08:08•(MSD)09/26/15 08:28
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % % FTCAcetone 0.125 0.00118 0.0793 0.0815 62.5 64.2 1 25.0-156 2.63 21.5
Acrolein 0.125 ND 0.539 0.550 431 440 1 34.0-194 J5 J5 1.94 21.5 FSS
Acrylonitrile 0.125 ND 0.149 0.148 119 118 1 55.9-161 0.410 20
Benzene 0.0250 ND 0.0232 0.0229 92.7 91.6 1 58.6-133 1.18 20 [Cn]
Bromobenzene 0.0250 ND 0.0244 0.0244 97.8 97.8 1 70.6-125 0.0100 20
Bromodichloromethane 0.0250 ND 0.0274 0.0267 110 107 1 69.2-127 2.52 20
Bromoform 0.0250 ND 0.0279 0.0279 112 111 1 66.3-140 0.230 20 FSr
Bromomethane 0.0250 ND 0.0201 0.0205 80.3 81.9 1 16.6-183 1.97 20.5
n-Butylbenzene 0.0250 ND 0.0247 0.0248 98.8 99.0 1 64.8-145 0.190 20
sec-Butyl benzene 0.0250 ND 0.0238 0.0242 95.2 96.8 1 66.8-139 1.65 20
tert-Butyl benzene 0.0250 ND 0.0237 0.0237 94.8 94.9 1 67.1-138 0.130 20
Carbon tetrachloride 0.0250 ND 0.0222 0.0211 88.9 84.2 1 60.6-139 5.40 20 7G1
Chlorobenzene 0.0250 ND 0.0234 0.0231 93.4 92.3 1 70.1-130 1.23 20
Chlorodibromomethane 0.0250 ND 0.0262 0.0258 105 103 1 71.6-132 1.61 20
Chloroethane 0.0250 ND 0.0203 0.0204 81.1 81.8 1 33.3-155 0.850 20 FAI
2-Chloroethyl vinyl ether 0.125 ND 0.0347 0.0176 27.8 14.1 1 5.00-149 J3 65.6 40
Chloroform 0.0250 ND 0.0238 0.0235 95.2 94.0 1 66.1-133 1.27 20 FSC
Chloromethane 0.0250 ND 0.0238 0.0236 95.4 94.3 1 40.7-139 1.16 20
2-Chlorotoluene 0.0250 ND 0.0244 0.0242 97.5 96.8 1 66.9-134 0.750 20
4-Chlorotoluene 0.0250 ND 0.0241 0.0245 96.6 97.8 1 66.8-134 1.31 20
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.0226 0.0226 90.3 90.4 1 63.9-142 0.110 20.2
1,2-Dibromoethane 0.0250 ND 0.0253 0.0251 101 100 1 73.8-131 0.840 20
Dibromomethane 0.0250 ND 0.0278 0.0274 111 109 1 72.8-127 1.45 20
1,2-Dichlorobenzene 0.0250 ND 0.0254 0.0254 101 102 1 77.4-127 0.320 20
1,3-Dichlorobenzene 0.0250 ND 0.0259 0.0261 104 104 1 67.9-136 0.760 20
1,4-Dichlorobenzene 0.0250 ND 0.0238 0.0235 95.4 94.2 1 74.4-123 1.23 20
Dichlorodifluoromethane 0.0250 ND 0.0197 0.0196 79.0 78.2 1 42.2-146 0.990 20
1,1-Dichloroethane 0.0250 ND 0.0252 0.0248 101 99.0 1 64.0-134 1.75 20
1,2-Dichloroethane 0.0250 ND 0.0272 0.0270 109 108 1 60.7-132 0.410 20
1,1-Dichloroethene 0.0250 ND 0.0242 0.0239 96.9 95.8 1 48.8-144 1.15 20
cis-1,2-Dichloroethene 0.0250 ND 0.0234 0.0229 93.7 91.7 1 60.6-136 2.21 20
trans-1,2-Dichloroethene 0.0250 ND 0.0224 0.0222 89.5 88.8 1 61.0-132 0.860 20
1,2-Dichloropropane 0.0250 ND 0.0284 0.0286 114 114 1 69.7-130 0.680 20
1,1-Dichloropropene 0.0250 ND 0.0232 0.0229 92.8 91.7 1 61.5-136 1.22 20
1,3-Dichloropropane 0.0250 ND 0.0248 0.0247 99.0 98.6 1 74.3-123 0.390 20
cis-1,3-Dichloropropene 0.0250 ND 0.0282 0.0278 113 111 1 71.1-129 1.40 20
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WG817621 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B 1-789514-19,22
L789697-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/26/15 09:47•(MS)09/26/15 08:08•(MSD)09/26/15 08:28
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % % TC
trans-1,3-Dichloropropene 0.0250 ND 0.0264 0.0257 105 103 1 66.3-136 2.34 20
2,2-Dichloropropane 0.0250 ND 0.0222 0.0215 88.7 85.9 1 54.9-142 3.27 20 FSS
Di-isopropyl ether 0.0250 ND 0.0296 0.0291 119 116 1 59.9-140 1.92 20
Ethylbenzene 0.0250 ND 0.0226 0.0223 90.5 89.4 1 62.7-136 1.31 20 [Cn]
Hexachloro-1,3-butadiene 0.0250 ND 0.0261 0.0269 104 108 1 61.1-144 3.16 20.1
Isopropylbenzene 0.0250 ND 0.0228 0.0228 91.2 91.0 1 67.4-136 0.220 20
p-Isopropyltoluene 0.0250 ND 0.0253 0.0256 101 102 1 62.8-143 1.39 20 FSr
2-Butanone(MEK) 0.125 ND 0.114 0.115 91.2 91.8 1 45.0-156 0.610 20.8
Methylene Chloride 0.0250 ND 0.0226 0.0223 90.5 89.3 1 61.5-125 1.33 20
4-Methyl-2-pentanone(MIBK) 0.125 ND 0.154 0.152 124 121 1 60.7-150 1.71 20
Methyl tert-butyl ether 0.0250 ND 0.0255 0.0253 102 101 1 61.4-136 0.420 20
Naphthalene 0.0250 ND 0.0244 0.0268 97.7 107 1 61.8-143 9.35 20 7G1
n-Propylbenzene 0.0250 ND 0.0238 0.0237 95.0 94.8 1 63.2-139 0.260 20
Styrene 0.0250 ND 0.0252 0.0248 101 99.2 1 68.2-133 1.56 20 FAI
1,1,1,2-Tetrachloroethane 0.0250 ND 0.0246 0.0239 98.2 95.5 1 70.5-132 2.76 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.0275 0.0273 110 109 1 64.9-145 0.940 20
Tetrachloroethene 0.0250 ND 0.0215 0.0213 86.2 85.2 1 57.4-141 1.06 20 FSC
Toluene 0.0250 ND 0.0239 0.0233 95.8 93.2 1 67.8-124 2.75 20
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.0208 0.0208 83.1 83.2 1 53.7-150 0.120 20
1,2,3-Trichlorobenzene 0.0250 ND 0.0264 0.0300 106 120 1 65.7-143 12.7 20
1,2,4-Trichlorobenzene 0.0250 ND 0.0278 0.0298 ill 119 1 67.0-146 6.84 20
1,1,1-Trichloroethane 0.0250 ND 0.0221 0.0213 88.6 85.0 1 58.7-134 4.08 20
1,1,2-Trichloroethane 0.0250 ND 0.0253 0.0249 101 99.8 1 74.1-130 1.35 20
Trichloroethene 0.0250 ND 0.0243 0.0238 97.3 95.2 1 48.9-148 2.17 20
Trichlorofluoromethane 0.0250 ND 0.0205 0.0202 82.0 81.0 1 39.9-165 1.33 20
1,2,3-Trichloropropane 0.0250 ND 0.0255 0.0257 102 103 1 71.5-134 0.710 20
1,2,3-Trimethylbenzene 0.0250 ND 0.0237 0.0239 94.8 95.6 1 62.7-133 0.840 20
1,2,4-Trim ethyl benzene 0.0250 ND 0.0245 0.0252 98.2 101 1 60.5-137 2.49 20
1,3,5-Trimethylbenzene 0.0250 ND 0.0241 0.0243 96.3 97.3 1 67.9-134 1.09 20
Vinyl chloride 0.0250 ND 0.0219 0.0219 87.4 87.5 1 44.3-143 0.150 20
Xylenes,Total 0.0750 ND 0.0689 0.0680 91.9 90.7 1 65.6-133 1.25 20
(S Toluene-d8 108 108 90.0-115
(S)Dibromofluoromethane 98.6 99.1 79.0-121
(S)4-Bromofluorobenzene 97.9 98.3 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG818034 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789514-19
Method Blank (MB) FP1(MB)09/28/15 10:21
MB Result MB Qualifier MB RDL
F
Analyte mg/I mg/1
cis-1,2-Dichloroethene ND 0.00100
FSS
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)09/28/15 06:40•(LCSD)09/28/15 07:00 [�n]
Spike Amount LCS Result LCSD Result LCS Rec. — LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits —
FSr
Analyte mg/I mg/I mg/I % % % % %
cis-1,2-Dichloroethene 0.0250 0.0273 0.0272 109 109 77.3-122 0.610 20
L790160-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)09/28/1514:03•(MS)09/28/15 08:13•(MSD)09/28/15 08:33 ql
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % E
cis-1,2-Dichloroethene 0.0250 ND 0.0277 0.0258 111 103 1 60.6-136 7.04 20
[Sc
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WG818281 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789514-02,03,04,05,06,07,08,09,10,14,15,16,17,18,20
Method Blank (MB) FP1(MB)09/29/1511:54
MB Result MB Qualifier MB RDL
FTc
Analyte mg/I mg/I
cis-1,2-Dichloroethene ND 0.00100
Tetrachloroethene ND 0.00100 FSS
Toluene ND 0.00500
Trichloroethene ND 0.00100 [Cn]
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FSr
(LCS)09/29/1510:28•(LCSD)09/29/15 10:48
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
cis-1,2-Dichloroethene 0.0250 0.0258 0.0250 103 100 77.3-122 3.32 20
Tetrachloroethene 0.0250 0.0266 0.0264 107 106 73.5-130 0.950 20 GI
Toluene 0.0250 0.0241 0.0242 96.2 96.9 77.9-116 0.750 20
Trichloroethene 0.0250 0.0257 0.0255 103 102 79.5-121 0.850 20 rAl
L789514-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) [Sc
(OS)09/29/1513:41•(MS)09/29/1512:40•(MSD)09/29/1513:00
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % %
cis-1,2-Dichloroethene 0.0250 0.00508 0.0306 0.0309 102 103 1 60.6-136 0.950 20
Tetrachloroethene 0.0250 0.0809 0.0823 0.0789 5.76 0.000 1 57.4-141 J6 J6 4.22 20
Toluene 0.0250 ND 0.0249 0.0248 99.5 99.1 1 67.8-124 0.430 20
Trichloroethene 0.0250 0.00262 0.0270 0.0276 97.5 100 1 48.9-148 2.24 20
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GLOSSARY OF TERMS ONE LAB.NATIONWIDE.
Abbreviations and Definitions
SDG Sample Delivery Group. FP1
MDL Method Detection Limit.
RDL Reported Detection Limit. FTc
ND,U Not detected at the Reporting Limit(or MDL where applicable).
RPD Relative Percent Difference. FS
(dry) Results are reported based on the dry weight of the sample.[this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD) 4 n
from a quality control sample.The Original Sample may not be included within the reported SDG.
(S) Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring Sr
recovery.Surrogates are not expected to be detected in all environmental media.
Rec. Recovery. RCSDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description rAl
J3 The associated batch QC was outside the established quality control range for precision. FSC
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination;spike value is
high.
J6 The sample matrix interfered with the ability to make any accurate determination;spike value is
low.
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ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE.
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other
lab is as accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry.The most significant benefit to our"one location"design is the design of our laboratory campus.The model is conducive to accelerated productivity, FP1
decreasing turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
State Accreditations ITC]
Alabama 40660 Nevada TN-03-2002-34 FSS
Alaska UST-080 New Hampshire 2975
Arizona AZ0612 New Jersey—NELAP TNO02
Arkansas 88-0469 New Mexico TN00003 4
California 01157CA New York 11742 Cn
Colorado TN00003 North Carolina Env375
Conneticut PH-0197 North Carolina DW21704 FS
Florida E87487 North Carolina 2 41
Georgia NELAP North Dakota R-140
Georgia' 923 Ohio—VAP CL0069 Rc
Idaho TN00003 Oklahoma 9915
Illinois 200008 Oregon 68-TN200002
Indiana C-TN-01 Pennsylvania 68-02979979 7G�
Iowa 364 Rhode Island 221
Kansas E-10277 South Carolina 84004
Kentucky' 90010 South Dakota n/a
Kentucky 16 Tennessee14 2006
Louisiana A130792 Texas T 104704245-07-TX FSC
Maine TN0002 Texas5 LABO152
Maryland 324 Utah 6157585858
Massachusetts M-TNO03 Vermont VT2006
Michigan 9958 Virginia 109
Minnesota 047-999-395 Washington C1915
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Nebraska NE-OS-15-05
Drinking Water z Underground Storage Tanks a Aquatic Toxicity 4.Chemical/Microbiological 5.Mold n1a Accreditation not applicable
Third Party& Federal Accreditations
A21LA—ISO 17025 1461.01 AIHA 100789
Canada 1461.01 DOD 1461.01
EPA—Crypto TN00003 USDA S-67674
Our Locations
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies.If you would like assistance from one of our support offices,please
contact our main office.ESC Lab Sciences performs all testing at our central laboratory.
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filling Infwmatlan= Analysis f Cantaini�r}Prescnrative :Ta r of Custedq Page_oi_
Bunnell - Lalmmons Engineering, Inc. Project Miinaggr 1
6004 Ponders Court
6004 Ponders Court Greenville, SC 29615
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Bunnell - iramrinons Engineering, Ire . p it li n$infbrmatior: An alysi 5{Container{Pr+'sBrvative Chain of G li#ody RagR,of
ProjBCt Manager I �
fx004 Panders Court
6Uk]A Panders Court Greenville, 5C 29615
Greenville,5C 29615 L:n:8 s-C-I-E N c s
Rc o I to: F^ 31 3ndy hlecorp.cpm 1205s:ebjiwn Rd �
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Troy Dunlap
ESC Lab Sciences
Non-Conformance Form
—[—
Login ##:789514 Client: BUNCANIGSC Late: 09/18/15 Evawated by: M. Lowe
Non-C'onfornlancc (:heck( a ]'cable itellkr
sample Ira#ewrity Chan of Custody Clarifica#[on
Paranwter{s] past hoJdi,rg
time Ln n Cladfication Noeded
Improper I(Broken Container:
tem rature Chain of custodY is incom fete
Improper container Insuffisie[rt aa lick in13 material around Container
e Please specify Metals requested, [rtsuf-Ident PaCking niaterial inside
Improper cooler
reservation please specify TCLP requested,
lm ro erhandlin b carrier edEx UPS Courie
fnsnfieients2m [evp[ume, x Received additioJtalSam p[es not IistedanCDC. ampiewas
Sample is biphasic. Sample ids on cDntainers do not match fds Oii frozen
Lac
Vials received with hea[lspace, 77[P UJank not received- Coritaiater lid not intact
Broken container x Client dirt not"XI ana]ysJs, if no Chaiat of Custo[i
Broken Container. R(1(:eA ed bv_
Chain Of Cus[od is missin
Sufficient sarnlpJe remains [ dtE Tiarre=
Tern Coact Rec 4:
Carrier
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Deceived TO for sarnple id. M -i 7, no analysis marked on Chain for Tor_
91entinFOrmed b Ca!!
TR Initials: 'eh � Entail o[re Mail
lierr[ o��tart- Bernlisbeth date: 21 15
Time- 0945
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Thfs E-mail and any-attached fifes are eunfidential,and ma} lie
eommuniratlon is StricflYprohibited, !f}+xu have reeetved this m ssAge(",error, ltd,Plea T
information'WeNed, yrfght proaected. [fy�ou Are nut the ltddressee,'n y d
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1

*ESC ANALYTICAL REPORT MyESC
L-A-B S-C-I-E-N-C-E-S September 30, 2015
Bunnell - Lammons Engineering, Inc.
Sample Delivery Group: L789444
Samples Received: 09/18/2015
Project Number: J15-1022-42
Description: Former Andrex Industries
Site: ASHEVILLE, NC
Report To: Mr.Andy Alexander
6004 Ponders Court
Greenville, SC 29615
Entire Report Reviewed By:
Jimmy Hunt
�F Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
reproduced,except in full,without written approval of the laboratory. Where applicable,sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures:060302,060303,and 060304.
ri
r

TABLE OF CONTENTS ONE LAB.NATIONWIDE.
'gin
'Cp:Cover Page 1
2Tc:Table of Contents 2
3Ss:Sample Summary 3
4Cn:Case Narrative 6 FS
5Sr:Sample Results 7 [Cn]
BC-1 L789444-01 7
BC-2 L789444-02 9 Isr
BC-3 L789444-03 11
BC-4 L789444-04 13 RC
BC-5 L789444-05 15
F,
CS-1 L789444-06 17
CS-2 L789444-07 19 FAI
SM-1 L789444-08 21
SM-2 L789444-09 23 FSC
SM-3 L789444-10 25
SM-4 L789444-11 27
SM-5 L789444-12 29
SM-6 L789444-13 31
JW-1 L789444-14 33
FIELD BLANK 2 L789444-15 35
6Qc:Quality Control Summary 37
Wet Chemistry by Method 9060A 37
Volatile Organic Compounds(GC/MS) by Method 8260B 40
7GI:Glossary of Terms 46
"Al:Accreditations& Locations 47
9Sc: Chain of Custody 48
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 2 of 50

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
BC-1 L789444-01 GW Benjamin P.Nisbeth 09/17/1510:30 09/18/15 09:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time z
TC
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/1519:07 09/24/1519:07 KLO
Wet Chemistry by Method 9060A WG816626 1 09/21/15 23:19 09/21/15 23:19 LLS
Collected by Collected date/time Received date/time
BC-2 L789444-02 GW Benjamin P.Nisbeth 09/17/1510:20 09/18/15 09:00 [Cn]
Method Batch Dilution Preparation Analysis Analysis Analyst
FSrdate/time date/time
Volatile Organic Compounds(GC/MS)by Method 82606 WG817026 1 09/24/1519:28 09/24/1519:28 KLO
Wet Chemistry by Method 9060A WG816626 1 09/21/15 23:31 09/21/15 23:31 LLS RC
Collected by Collected date/time Received date/time F
BC-3 L789444-03 GW Benjamin P.Nisbeth 09/17/1510:10 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst FAI
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/1519:50 09/24/1519:50 KLO
FSCWet Chemistry by Method 9060A WG816626 1 09/21/15 23:48 09/21/15 23:48 LLS
Collected by Collected date/time Received date/time
BC-4 L789444-04 GW Benjamin P.Nisbeth 09/17/1510:00 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 20:10 09/24/15 20:10 KLO
Wet Chemistry by Method 9060A WG816626 1 09/21/15 23:59 09/21/15 23:59 LLS
Collected by Collected date/time Received date/time
BC-5 L789444-05 GW Benjamin P.Nisbeth 09/17/15 09:50 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 20:31 09/24/15 20:31 KLO
Wet Chemistry by Method 9060A WG816626 1 09/22/15 00:11 09/22/15 00:11 LLS
Collected by Collected date/time Received date/time
CS-1 L789444-06 GW Benjamin P.Nisbeth 09/17/1511:00 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 20:53 09/24/15 20:53 KLO
Wet Chemistry by Method 9060A WG816626 1 09/22/15 00:23 09/22/15 00:23 LLS
Collected by Collected date/time Received date/time
CS-2 L789444-07 GW Benjamin P.Nisbeth 09/17/1510:50 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 21:14 09/24/15 21:14 KLO
Wet Chemistry by Method 9060A WG816627 1 09/22/1518:05 09/22/1518:05 LLS
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 3 of 50

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
SM-1 L789444-08 GW Benjamin P.Nisbeth 09/17/1512:55 09/18/15 09:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time z
TC
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 21:35 09/24/15 21:35 KLO
Wet Chemistry by Method 9060A WG816627 1 09/22/1518:22 09/22/1518:22 LLS
Collected by Collected date/time Received date/time
SM-2 L789444-09 GW Benjamin P.Nisbeth 09/17/1512:45 09/18/15 09:00 4 n
Method Batch Dilution Preparation Analysis Analysis Analyst
FSrdate/time date/time
Volatile Organic Compounds(GC/MS)by Method 82606 WG817026 1 09/24/15 21:56 09/24/15 21:56 KLO
Wet Chemistry by Method 9060A WG816627 1 09/22/1519:16 09/22/1519:16 LLS RC
Collected by Collected date/time Received date/time F
SM-3 L789444-10 GW Benjamin P.Nisbeth 09/17/1512:40 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst FAI
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 22:18 09/24/15 22:18 KLO
FSCWet Chemistry by Method 9060A WG816627 1 09/22/1519:43 09/22/1519:43 LLS
Collected by Collected date/time Received date/time
SM-4 L789444-11 GW Benjamin P.Nisbeth 09/17/1512:30 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 22:39 09/24/15 22:39 KLO
Wet Chemistry by Method 9060A WG816627 1 09/22/1519:55 09/22/1519:55 LLS
Collected by Collected date/time Received date/time
SM-5 L789444-12 GW Benjamin P.Nisbeth 09/17/1512:20 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 23:00 09/24/15 23:00 KLO
Wet Chemistry by Method 9060A WG816627 1 09/22/15 20:07 09/22/15 20:07 LLS
Collected by Collected date/time Received date/time
SM-6 L789444-13 GW Benjamin P.Nisbeth 09/17/1512:15 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 23:21 09/24/15 23:21 KLO
Wet Chemistry by Method 9060A WG816627 1 09/22/15 20:20 09/22/15 20:20 LLS
Collected by Collected date/time Received date/time
JW-1 L789444-14 GW Benjamin P.Nisbeth 09/17/1513:15 09/18/15 09:00
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/24/15 23:42 09/24/15 23:42 KLO
Wet Chemistry by Method 9060A WG816627 1 09/22/15 20:32 09/22/15 20:32 LLS
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 4 of 50

SAMPLE SUMMARY ONE LAB.NATIONWIDE.
Collected by Collected date/time Received date/time
FIELD BLANK 2 L789444-15 GW Benjamin P.Nisbeth 09/17/1509:00 09/18/1509:00 FP1
Method Batch Dilution Preparation Analysis Analysis Analyst
date/time date/time z
Tc
Volatile Organic Compounds(GC/MS)by Method 8260B WG817026 1 09/25/15 00:04 09/25/15 00:04 KLO
[Cn]
FSr
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 5 of 50

CASE NARRATIVE ONE LAB.NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers,with the FP1
appropriate preservatives, and within method specified holding times. All MDL(LOD)and RDL(LOQ)values reported for environmental samples have been corrected for the dilution factor used in the FTC
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my FSS
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
FSr
FC-1
�GI
Jimmy Hunt rAl
Technical Service Representative
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 6 of 50

BC-1 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:30 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/21/2015 23:19 WG816626
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/201519:07 WG817026
Acrolein ND 50.0 1 09/24/201519:07 WG817026
Acrylonitrile ND 10.0 1 09/24/201519:07 WG817026
Benzene ND 1.00 1 09/24/201519:07 WG817026
Bromobenzene ND 1.00 1 09/24/201519:07 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/201519:07 WG817026
Bromoform ND 1.00 1 09/24/201519:07 WG817026 F
Bromomethane ND 5.00 1 09/24/201519:07 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/201519:07 WG817026
sec-Butylbenzene ND 1.00 1 09/24/201519:07 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/201519:07 WG817026
Carbon tetrachloride ND 1.00 1 09/24/201519:07 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/201519:07 WG817026
Chlorodibromomethane ND 1.00 1 09/24/201519:07 WG817026
Chloroethane ND 5.00 1 09/24/201519:07 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/201519:07 WG817026
Chloroform ND 5.00 1 09/24/201519:07 WG817026
Chloromethane ND 2.50 1 09/24/201519:07 WG817026
2-Chlorotoluene ND 1.00 1 09/24/201519:07 WG817026
4-Chlorotoluene ND 1.00 1 09/24/201519:07 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/201519:07 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/201519:07 WG817026
Dibromomethane ND 1.00 1 09/24/201519:07 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/201519:07 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/201519:07 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/201519:07 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/201519:07 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/201519:07 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/201519:07 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/201519:07 WG817026
cis-1,2-Dichloroethene 3.56 1.00 1 09/24/201519:07 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/201519:07 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/201519:07 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/201519:07 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/201519:07 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/201519:07 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/201519:07 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/201519:07 WG817026
Di-isopropyl ether ND 1.00 1 09/24/201519:07 WG817026
Ethylbenzene ND 1.00 1 09/24/201519:07 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/201519:07 WG817026
Isopropylbenzene ND 1.00 1 09/24/201519:07 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/201519:07 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/201519:07 WG817026
Methylene Chloride ND 5.00 1 09/24/201519:07 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/201519:07 WG817026
Methyl tert-butyl ether ND 1.00 1 09/24/201519:07 WG817026
Naphthalene ND 5.00 1 09/24/201519:07 WG817026
n-Propylbenzene ND 1.00 1 09/24/201519:07 WG817026
Styrene ND 1.00 1 09/24/201519:07 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 7 of 50

BC-1 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:30 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/201519:07 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/201519:07 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/201519:07 WG817026 F
Tetrachloroethene 10.8 1.00 1 09/24/201519:07 WG817026
Toluene ND 5.00 1 09/24/201519:07 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/201519:07 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/201519:07 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/201519:07 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/201519:07 WG817026
Trichloroethene 1.18 1.00 1 09/24/201519:07 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/201519:07 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/201519:07 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/201519:07 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/201519:07 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/201519:07 WG817026
Vinyl chloride ND 1.00 1 09/24/201519:07 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/201519:07 WG817026
(S)Toluene-d8 104 90.0-115 09/24/201519.07 WG817026 F
(S)Dibromofluoromethone 99.7 79.0-121 091241201519.07 WG817026
(S)4-Bromofluorobenzene 100 80.1-120 09/24/201519.07 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 8 of 50

BC-2 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:20 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/21/2015 23:31 WG816626
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/201519:28 WG817026
Acrolein ND 50.0 1 09/24/201519:28 WG817026
Acrylonitrile ND 10.0 1 09/24/201519:28 WG817026
Benzene ND 1.00 1 09/24/201519:28 WG817026
Bromobenzene ND 1.00 1 09/24/201519:28 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/201519:28 WG817026
Bromoform ND 1.00 1 09/24/201519:28 WG817026 F
Bromomethane ND 5.00 1 09/24/201519:28 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/201519:28 WG817026
sec-Butylbenzene ND 1.00 1 09/24/201519:28 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/201519:28 WG817026
Carbon tetrachloride ND 1.00 1 09/24/201519:28 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/201519:28 WG817026
Chlorodibromomethane ND 1.00 1 09/24/201519:28 WG817026
Chloroethane ND 5.00 1 09/24/201519:28 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/201519:28 WG817026
Chloroform ND 5.00 1 09/24/201519:28 WG817026
Chloromethane ND 2.50 1 09/24/201519:28 WG817026
2-Chlorotoluene ND 1.00 1 09/24/201519:28 WG817026
4-Chlorotoluene ND 1.00 1 09/24/201519:28 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/201519:28 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/201519:28 WG817026
Dibromomethane ND 1.00 1 09/24/201519:28 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/201519:28 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/201519:28 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/201519:28 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/201519:28 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/201519:28 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/201519:28 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/201519:28 WG817026
cis-1,2-Dichloroethene 2.88 1.00 1 09/24/201519:28 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/201519:28 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/201519:28 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/201519:28 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/201519:28 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/201519:28 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/201519:28 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/201519:28 WG817026
Di-isopropyl ether ND 1.00 1 09/24/201519:28 WG817026
Ethylbenzene ND 1.00 1 09/24/201519:28 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/201519:28 WG817026
Isopropylbenzene ND 1.00 1 09/24/201519:28 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/201519:28 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/201519:28 WG817026
Methylene Chloride ND 5.00 1 09/24/201519:28 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/201519:28 WG817026
Methyl tert-butyl ether ND 1.00 1 09/24/201519:28 WG817026
Naphthalene ND 5.00 1 09/24/201519:28 WG817026
n-Propylbenzene ND 1.00 1 09/24/201519:28 WG817026
Styrene ND 1.00 1 09/24/201519:28 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 9 of 50

BC-2 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:20 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/201519:28 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/201519:28 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/201519:28 WG817026 F
Tetrachloroethene 9.59 1.00 1 09/24/201519:28 WG817026
Toluene ND 5.00 1 09/24/201519:28 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/201519:28 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/201519:28 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/201519:28 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/201519:28 WG817026
Trichloroethene 1.40 1.00 1 09/24/201519:28 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/201519:28 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/201519:28 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/201519:28 WG817026
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/201519:28 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/201519:28 WG817026
Vinyl chloride ND 1.00 1 09/24/201519:28 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/201519:28 WG817026
(S)Toluene-d8 102 90.0-115 09/24/201519.28 WG817026 F
(S)Dibromofluoromethone 97.6 79.0-121 09/24/201519.28 WG817026
(S)4-Bromofluorobenzene 98.9 80.1-120 09/24/201519.28 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 10 of 50

BC-3 SAMPLE RESULTS - 03 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:10 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/21/2015 23:48 WG816626
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/201519:50 WG817026
Acrolein ND 50.0 1 09/24/201519:50 WG817026
Acrylonitrile ND 10.0 1 09/24/201519:50 WG817026
Benzene ND 1.00 1 09/24/201519:50 WG817026
Bromobenzene ND 1.00 1 09/24/201519:50 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/201519:50 WG817026
Bromoform ND 1.00 1 09/24/201519:50 WG817026 F
Bromomethane ND 5.00 1 09/24/201519:50 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/201519:50 WG817026
sec-Butylbenzene ND 1.00 1 09/24/201519:50 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/201519:50 WG817026
Carbon tetrachloride ND 1.00 1 09/24/201519:50 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/201519:50 WG817026
Chlorodibromomethane ND 1.00 1 09/24/201519:50 WG817026
Chloroethane ND 5.00 1 09/24/201519:50 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/201519:50 WG817026
Chloroform ND 5.00 1 09/24/201519:50 WG817026
Chloromethane ND 2.50 1 09/24/201519:50 WG817026
2-Chlorotoluene ND 1.00 1 09/24/201519:50 WG817026
4-Chlorotoluene ND 1.00 1 09/24/201519:50 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/201519:50 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/201519:50 WG817026
Dibromomethane ND 1.00 1 09/24/201519:50 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/201519:50 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/201519:50 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/201519:50 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/201519:50 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/201519:50 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/201519:50 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/201519:50 WG817026
cis-1,2-Dichloroethene 1.08 1.00 1 09/24/201519:50 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/201519:50 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/201519:50 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/201519:50 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/201519:50 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/201519:50 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/201519:50 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/201519:50 WG817026
Di-isopropyl ether ND 1.00 1 09/24/201519:50 WG817026
Ethylbenzene ND 1.00 1 09/24/201519:50 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/201519:50 WG817026
Isopropylbenzene ND 1.00 1 09/24/201519:50 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/201519:50 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/201519:50 WG817026
Methylene Chloride ND 5.00 1 09/24/201519:50 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/201519:50 WG817026
Methyl tert-butyl ether ND 1.00 1 09/24/201519:50 WG817026
Naphthalene ND 5.00 1 09/24/201519:50 WG817026
n-Propylbenzene ND 1.00 1 09/24/201519:50 WG817026
Styrene ND 1.00 1 09/24/201519:50 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 11 of 50

BC-3 SAMPLE RESULTS - 03 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:10 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/201519:50 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/201519:50 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/201519:50 WG817026 F
Tetrachloroethene 2.55 1.00 1 09/24/201519:50 WG817026
Toluene ND 5.00 1 09/24/201519:50 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/201519:50 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/201519:50 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/201519:50 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/201519:50 WG817026
Trichloroethene ND 1.00 1 09/24/201519:50 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/201519:50 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/201519:50 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/201519:50 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/201519:50 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/201519:50 WG817026
Vinyl chloride ND 1.00 1 09/24/201519:50 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/201519:50 WG817026
(S)Toluene-d8 103 90.0-115 091241201519.50 WG817026 F
(S)Dibromofluoromethone 101 79.0-121 091241201519.50 WG817026
(S)4-Bromofluorobenzene 104 80.1-120 091241201519.50 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 12 of 50

BC-4 SAMPLE RESULTS - 04 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:00 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/21/2015 23:59 WG816626
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 20:10 WG817026
Acrolein ND 50.0 1 09/24/2015 20:10 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 20:10 WG817026
Benzene ND 1.00 1 09/24/2015 20:10 WG817026
Bromobenzene ND 1.00 1 09/24/2015 20:10 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 20:10 WG817026
Bromoform ND 1.00 1 09/24/2015 20:10 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 20:10 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 20:10 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 20:10 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 20:10 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 20:10 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 20:10 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 20:10 WG817026
Chloroethane ND 5.00 1 09/24/2015 20:10 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 20:10 WG817026
Chloroform ND 5.00 1 09/24/2015 20:10 WG817026
Chloromethane ND 2.50 1 09/24/2015 20:10 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 20:10 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 20:10 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 20:10 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 20:10 WG817026
Dibromomethane ND 1.00 1 09/24/2015 20:10 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 20:10 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 20:10 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 20:10 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 20:10 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 20:10 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 20:10 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 20:10 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 20:10 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 20:10 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 20:10 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 20:10 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 20:10 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 20:10 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 20:10 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 20:10 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 20:10 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 20:10 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 20:10 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 20:10 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 20:10 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 20:10 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 20:10 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 20:10 WG817026
Methyl tert-butyl ether ND 1.00 1 09/24/2015 20:10 WG817026
Naphthalene ND 5.00 1 09/24/2015 20:10 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 20:10 WG817026
Styrene ND 1.00 1 09/24/2015 20:10 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 13 of 50

BC-4 SAMPLE RESULTS - 04 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:00 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 20:10 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 20:10 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 20:10 WG817026 F
Tetrachloroethene ND 1.00 1 09/24/2015 20:10 WG817026
Toluene ND 5.00 1 09/24/2015 20:10 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 20:10 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 20:10 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 20:10 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 20:10 WG817026
Trichloroethene ND 1.00 1 09/24/2015 20:10 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 20:10 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 20:10 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 20:10 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 20:10 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 20:10 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 20:10 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 20:10 WG817026
(S)Toluene-d8 102 90.0-115 091241201520.10 WG817026 F
(S)Dibromofluoromethone 100 79.0-121 091241201520.10 WG817026
(S)4-Bromofluorobenzene 99.3 80.1-120 091241201520.10 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 14 of 50

BC-5 SAMPLE RESULTS - 05 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 09:50 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/2015 00:11 WG816626
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 20:31 WG817026
Acrolein ND 50.0 1 09/24/2015 20:31 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 20:31 WG817026
Benzene ND 1.00 1 09/24/2015 20:31 WG817026
Bromobenzene ND 1.00 1 09/24/2015 20:31 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 20:31 WG817026
Bromoform ND 1.00 1 09/24/2015 20:31 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 20:31 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 20:31 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 20:31 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 20:31 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 20:31 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 20:31 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 20:31 WG817026
Chloroethane ND 5.00 1 09/24/2015 20:31 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 20:31 WG817026
Chloroform ND 5.00 1 09/24/2015 20:31 WG817026
Chloromethane ND 2.50 1 09/24/2015 20:31 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 20:31 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 20:31 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 20:31 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 20:31 WG817026
Dibromomethane ND 1.00 1 09/24/2015 20:31 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 20:31 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 20:31 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 20:31 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 20:31 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 20:31 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 20:31 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 20:31 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 20:31 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 20:31 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 20:31 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 20:31 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 20:31 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 20:31 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 20:31 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 20:31 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 20:31 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 20:31 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 20:31 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 20:31 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 20:31 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 20:31 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 20:31 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 20:31 WG817026
Methyl tert-butyl ether ND 1.00 1 09/24/2015 20:31 WG817026
Naphthalene ND 5.00 1 09/24/2015 20:31 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 20:31 WG817026
Styrene ND 1.00 1 09/24/2015 20:31 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 15 of 50

BC-5 SAMPLE RESULTS - 05 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 09:50 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 20:31 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 20:31 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 20:31 WG817026 F
Tetrachloroethene ND 1.00 1 09/24/2015 20:31 WG817026
Toluene ND 5.00 1 09/24/2015 20:31 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 20:31 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 20:31 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 20:31 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 20:31 WG817026
Trichloroethene ND 1.00 1 09/24/2015 20:31 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 20:31 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 20:31 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 20:31 WG817026
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 20:31 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 20:31 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 20:31 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 20:31 WG817026
(S)Toluene-d8 104 90.0-115 09124120152031 WG817026 F
(S)Dibromofluoromethone 99.7 79.0-121 091241201520:31 WG817026
(S)4-Bromofluorobenzene 96.4 80.1-120 091241201520:31 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 16 of 50

CS-1 SAMPLE RESULTS - 06 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 11:00 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 10900 1000 1 09/22/2015 00:23 WG816626
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 20:53 WG817026
Acrolein ND 50.0 1 09/24/2015 20:53 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 20:53 WG817026
Benzene ND 1.00 1 09/24/2015 20:53 WG817026
Bromobenzene ND 1.00 1 09/24/2015 20:53 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 20:53 WG817026
Bromoform ND 1.00 1 09/24/2015 20:53 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 20:53 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 20:53 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 20:53 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 20:53 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 20:53 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 20:53 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 20:53 WG817026
Chloroethane ND 5.00 1 09/24/2015 20:53 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 20:53 WG817026
Chloroform ND 5.00 1 09/24/2015 20:53 WG817026
Chloromethane ND 2.50 1 09/24/2015 20:53 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 20:53 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 20:53 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 20:53 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 20:53 WG817026
Dibromomethane ND 1.00 1 09/24/2015 20:53 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 20:53 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 20:53 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 20:53 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 20:53 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 20:53 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 20:53 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 20:53 WG817026
cis-1,2-Dichloroethene 2.86 1.00 1 09/24/2015 20:53 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 20:53 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 20:53 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 20:53 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 20:53 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 20:53 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 20:53 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 20:53 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 20:53 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 20:53 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 20:53 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 20:53 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 20:53 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 20:53 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 20:53 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 20:53 WG817026
Methyl tert-butyl ether ND 1.00 1 09/24/2015 20:53 WG817026
Naphthalene ND 5.00 1 09/24/2015 20:53 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 20:53 WG817026
Styrene ND 1.00 1 09/24/2015 20:53 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 17 of 50

CS-1 SAMPLE RESULTS - 06 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 11:00 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 20:53 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 20:53 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 20:53 WG817026 F
Tetrachloroethene 9.88 1.00 1 09/24/2015 20:53 WG817026
Toluene ND 5.00 1 09/24/2015 20:53 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 20:53 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 20:53 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 20:53 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 20:53 WG817026
Trichloroethene 2.50 1.00 1 09/24/2015 20:53 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 20:53 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 20:53 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 20:53 WG817026
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 20:53 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 20:53 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 20:53 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 20:53 WG817026
(S)Toluene-d8 105 90.0-115 091241201520.53 WG817026 F
(S)Dibromofluoromethone 100 79.0-121 091241201520.53 WG817026
(S)4-Bromofluorobenzene 99.3 80.1-120 091241201520.53 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 18 of 50

CS-2 SAMPLE RESULTS - 07 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:50 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 6240 1000 1 09/22/201518:05 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 21:14 WG817026
Acrolein ND 50.0 1 09/24/2015 21:14 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 21:14 WG817026
Benzene ND 1.00 1 09/24/2015 21:14 WG817026
Bromobenzene ND 1.00 1 09/24/2015 21:14 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 21:14 WG817026
Bromoform ND 1.00 1 09/24/2015 21:14 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 21:14 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 21:14 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 21:14 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 21:14 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 21:14 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 21:14 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 21:14 WG817026
Chloroethane ND 5.00 1 09/24/2015 21:14 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 21:14 WG817026
Chloroform ND 5.00 1 09/24/2015 21:14 WG817026
Chloromethane ND 2.50 1 09/24/2015 21:14 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 21:14 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 21:14 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 21:14 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 21:14 WG817026
Dibromomethane ND 1.00 1 09/24/2015 21:14 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 21:14 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 21:14 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 21:14 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 21:14 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 21:14 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 21:14 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 21:14 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 21:14 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 21:14 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 21:14 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 21:14 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 21:14 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 21:14 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 21:14 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 21:14 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 21:14 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 21:14 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 21:14 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 21:14 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 21:14 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 21:14 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 21:14 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 21:14 WG817026
Methyl tert-butyl ether ND 1.00 1 09/24/2015 21:14 WG817026
Naphthalene ND 5.00 1 09/24/2015 21:14 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 21:14 WG817026
Styrene ND 1.00 1 09/24/2015 21:14 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 19 of 50

CS-2 SAMPLE RESULTS - 07 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 10:50 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 21:14 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 21:14 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 21:14 WG817026 F
Tetrachloroethene 5.83 1.00 1 09/24/2015 21:14 WG817026
Toluene ND 5.00 1 09/24/2015 21:14 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 21:14 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 21:14 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 21:14 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 21:14 WG817026
Trichloroethene ND 1.00 1 09/24/2015 21:14 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 21:14 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 21:14 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 21:14 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 21:14 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 21:14 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 21:14 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 21:14 WG817026
(S)Toluene-d8 102 90.0-115 091241201521.14 WG817026 F
(S)Dibromofluoromethone 97.6 79.0-121 091241201521.14 WG817026
(S)4-Bromofluorobenzene 99.7 80.1-120 091241201521.14 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 20 of 50

S M-1 SAMPLE RESULTS - 08 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:55 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/201518:22 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 21:35 WG817026
Acrolein ND 50.0 1 09/24/2015 21:35 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 21:35 WG817026
Benzene ND 1.00 1 09/24/2015 21:35 WG817026
Bromobenzene ND 1.00 1 09/24/2015 21:35 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 21:35 WG817026
Bromoform ND 1.00 1 09/24/2015 21:35 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 21:35 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 21:35 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 21:35 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 21:35 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 21:35 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 21:35 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 21:35 WG817026
Chloroethane ND 5.00 1 09/24/2015 21:35 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 21:35 WG817026
Chloroform ND 5.00 1 09/24/2015 21:35 WG817026
Chloromethane ND 2.50 1 09/24/2015 21:35 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 21:35 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 21:35 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 21:35 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 21:35 WG817026
Dibromomethane ND 1.00 1 09/24/2015 21:35 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 21:35 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 21:35 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 21:35 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 21:35 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 21:35 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 21:35 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 21:35 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 21:35 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 21:35 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 21:35 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 21:35 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 21:35 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 21:35 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 21:35 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 21:35 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 21:35 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 21:35 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 21:35 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 21:35 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 21:35 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 21:35 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 21:35 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 21:35 WG817026
Methyl tert-butyl ether 5.36 1.00 1 09/24/2015 21:35 WG817026
Naphthalene ND 5.00 1 09/24/2015 21:35 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 21:35 WG817026
Styrene ND 1.00 1 09/24/2015 21:35 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 21 of 50

S M-1 SAMPLE RESULTS - 08 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:55 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 21:35 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 21:35 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 21:35 WG817026 F
Tetrachloroethene ND 1.00 1 09/24/2015 21:35 WG817026
Toluene ND 5.00 1 09/24/2015 21:35 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 21:35 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 21:35 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 21:35 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 21:35 WG817026
Trichloroethene ND 1.00 1 09/24/2015 21:35 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 21:35 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 21:35 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 21:35 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 21:35 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 21:35 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 21:35 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 21:35 WG817026
(S)Toluene-d8 106 90.0-115 09124120152135 WG817026 F
(S)Dibromofluoromethone 101 79.0-121 091241201521.35 WG817026
(S)4-Bromofluorobenzene 100 80.1-120 091241201521.35 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 22 of 50

SM-2 SAMPLE RESULTS - 09 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:45 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 1080 1000 1 09/22/201519:16 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 21:56 WG817026
Acrolein ND 50.0 1 09/24/2015 21:56 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 21:56 WG817026
Benzene ND 1.00 1 09/24/2015 21:56 WG817026
Bromobenzene ND 1.00 1 09/24/2015 21:56 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 21:56 WG817026
Bromoform ND 1.00 1 09/24/2015 21:56 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 21:56 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 21:56 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 21:56 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 21:56 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 21:56 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 21:56 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 21:56 WG817026
Chloroethane ND 5.00 1 09/24/2015 21:56 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 21:56 WG817026
Chloroform ND 5.00 1 09/24/2015 21:56 WG817026
Chloromethane ND 2.50 1 09/24/2015 21:56 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 21:56 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 21:56 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 21:56 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 21:56 WG817026
Dibromomethane ND 1.00 1 09/24/2015 21:56 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 21:56 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 21:56 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 21:56 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 21:56 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 21:56 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 21:56 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 21:56 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 21:56 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 21:56 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 21:56 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 21:56 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 21:56 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 21:56 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 21:56 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 21:56 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 21:56 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 21:56 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 21:56 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 21:56 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 21:56 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 21:56 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 21:56 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 21:56 WG817026
Methyl tert-butyl ether 3.86 1.00 1 09/24/2015 21:56 WG817026
Naphthalene ND 5.00 1 09/24/2015 21:56 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 21:56 WG817026
Styrene ND 1.00 1 09/24/2015 21:56 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 23 of 50

SM-2 SAMPLE RESULTS - 09 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:45 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 21:56 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 21:56 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 21:56 WG817026 F
Tetrachloroethene ND 1.00 1 09/24/2015 21:56 WG817026
Toluene ND 5.00 1 09/24/2015 21:56 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 21:56 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 21:56 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 21:56 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 21:56 WG817026
Trichloroethene ND 1.00 1 09/24/2015 21:56 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 21:56 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 21:56 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 21:56 WG817026
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 21:56 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 21:56 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 21:56 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 21:56 WG817026
(S)Toluene-d8 102 90.0-115 091241201521.56 WG817026 F
(S)Dibromofluoromethone 98.1 79.0-121 091241201521.56 WG817026
(S)4-Bromofluorobenzene 97.5 80.1-120 091241201521.56 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 24 of 50

SM-3 SAMPLE RESULTS - 10 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:40 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/201519:43 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 22:18 WG817026
Acrolein ND 50.0 1 09/24/2015 22:18 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 22:18 WG817026
Benzene ND 1.00 1 09/24/2015 22:18 WG817026
Bromobenzene ND 1.00 1 09/24/2015 22:18 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 22:18 WG817026
Bromoform ND 1.00 1 09/24/2015 22:18 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 22:18 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 22:18 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 22:18 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 22:18 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 22:18 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 22:18 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 22:18 WG817026
Chloroethane ND 5.00 1 09/24/2015 22:18 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 22:18 WG817026
Chloroform ND 5.00 1 09/24/2015 22:18 WG817026
Chloromethane ND 2.50 1 09/24/2015 22:18 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 22:18 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 22:18 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 22:18 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 22:18 WG817026
Dibromomethane ND 1.00 1 09/24/2015 22:18 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 22:18 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 22:18 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 22:18 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 22:18 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 22:18 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 22:18 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 22:18 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 22:18 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 22:18 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 22:18 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 22:18 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 22:18 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 22:18 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 22:18 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 22:18 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 22:18 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 22:18 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 22:18 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 22:18 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 22:18 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 22:18 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 22:18 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 22:18 WG817026
Methyl tert-butyl ether 1.62 1.00 1 09/24/2015 22:18 WG817026
Naphthalene ND 5.00 1 09/24/2015 22:18 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 22:18 WG817026
Styrene ND 1.00 1 09/24/2015 22:18 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 25 of 50

SM-3 SAMPLE RESULTS - 10 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:40 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 22:18 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 22:18 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 22:18 WG817026 F
Tetrachloroethene ND 1.00 1 09/24/2015 22:18 WG817026
Toluene ND 5.00 1 09/24/2015 22:18 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 22:18 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 22:18 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 22:18 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 22:18 WG817026
Trichloroethene ND 1.00 1 09/24/2015 22:18 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 22:18 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 22:18 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 22:18 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 22:18 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 22:18 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 22:18 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 22:18 WG817026
(S)Toluene-d8 91.2 90.0-115 091241201522:18 WG817026 F
(S)Dibromofluoromethone 103 79.0-121 091241201522:18 WG817026
(S)4-Bromofluorobenzene 75.9 J2 80.1-120 091241201522:18 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 26 of 50

SM-4 SAMPLE RESULTS - 11 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:30 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/201519:55 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 22:39 WG817026
Acrolein ND 50.0 1 09/24/2015 22:39 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 22:39 WG817026
Benzene ND 1.00 1 09/24/2015 22:39 WG817026
Bromobenzene ND 1.00 1 09/24/2015 22:39 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 22:39 WG817026
Bromoform ND 1.00 1 09/24/2015 22:39 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 22:39 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 22:39 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 22:39 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 22:39 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 22:39 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 22:39 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 22:39 WG817026
Chloroethane ND 5.00 1 09/24/2015 22:39 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 22:39 WG817026
Chloroform ND 5.00 1 09/24/2015 22:39 WG817026
Chloromethane ND 2.50 1 09/24/2015 22:39 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 22:39 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 22:39 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 22:39 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 22:39 WG817026
Dibromomethane ND 1.00 1 09/24/2015 22:39 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 22:39 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 22:39 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 22:39 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 22:39 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 22:39 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 22:39 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 22:39 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 22:39 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 22:39 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 22:39 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 22:39 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 22:39 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 22:39 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 22:39 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 22:39 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 22:39 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 22:39 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 22:39 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 22:39 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 22:39 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 22:39 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 22:39 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 22:39 WG817026
Methyl tert-butyl ether 2.13 1.00 1 09/24/2015 22:39 WG817026
Naphthalene ND 5.00 1 09/24/2015 22:39 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 22:39 WG817026
Styrene ND 1.00 1 09/24/2015 22:39 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 27 of 50

SM-4 SAMPLE RESULTS - 11 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:30 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 22:39 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 22:39 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 22:39 WG817026 F
Tetrachloroethene 1.23 1.00 1 09/24/2015 22:39 WG817026
Toluene ND 5.00 1 09/24/2015 22:39 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 22:39 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 22:39 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 22:39 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 22:39 WG817026
Trichloroethene ND 1.00 1 09/24/2015 22:39 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 22:39 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 22:39 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 22:39 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 22:39 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 22:39 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 22:39 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 22:39 WG817026
(S)Toluene-d8 101 90.0-115 09124120152239 WG817026 F
(S)Dibromofluoromethone 99.2 79.0-121 091241201522:39 WG817026
(S)4-Bromofluorobenzene 99.5 80.1-120 091241201522:39 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 28 of 50

SM-5 SAMPLE RESULTS - 12 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:20 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/2015 20:07 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 23:00 WG817026
Acrolein ND 50.0 1 09/24/2015 23:00 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 23:00 WG817026
Benzene ND 1.00 1 09/24/2015 23:00 WG817026
Bromobenzene ND 1.00 1 09/24/2015 23:00 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 23:00 WG817026
Bromoform ND 1.00 1 09/24/2015 23:00 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 23:00 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 23:00 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 23:00 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 23:00 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 23:00 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 23:00 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 23:00 WG817026
Chloroethane ND 5.00 1 09/24/2015 23:00 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 23:00 WG817026
Chloroform ND 5.00 1 09/24/2015 23:00 WG817026
Chloromethane ND 2.50 1 09/24/2015 23:00 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 23:00 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 23:00 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 23:00 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 23:00 WG817026
Dibromomethane ND 1.00 1 09/24/2015 23:00 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 23:00 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 23:00 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 23:00 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 23:00 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 23:00 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 23:00 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 23:00 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 23:00 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 23:00 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 23:00 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 23:00 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 23:00 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 23:00 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 23:00 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 23:00 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 23:00 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 23:00 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 23:00 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 23:00 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 23:00 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 23:00 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 23:00 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 23:00 WG817026
Methyl tert-butyl ether 1.87 1.00 1 09/24/2015 23:00 WG817026
Naphthalene ND 5.00 1 09/24/2015 23:00 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 23:00 WG817026
Styrene ND 1.00 1 09/24/2015 23:00 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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SM-5 SAMPLE RESULTS - 12 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:20 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 23:00 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 23:00 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 23:00 WG817026 F
Tetrachloroethene 1.02 1.00 1 09/24/2015 23:00 WG817026
Toluene ND 5.00 1 09/24/2015 23:00 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 23:00 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 23:00 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 23:00 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 23:00 WG817026
Trichloroethene ND 1.00 1 09/24/2015 23:00 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 23:00 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 23:00 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 23:00 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 23:00 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 23:00 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 23:00 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 23:00 WG817026
(S)Toluene-d8 102 90.0-115 091241201523:00 WG817026 F
(S)Dibromofluoromethone 96.5 79.0-121 091241201523:00 WG817026
(S)4-Bromofluorobenzene 100 80.1-120 091241201523:00 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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SM-6 SAMPLE RESULTS - 13 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:15 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) 1010 1000 1 09/22/2015 20:20 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 23:21 WG817026
Acrolein ND 50.0 1 09/24/2015 23:21 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 23:21 WG817026
Benzene ND 1.00 1 09/24/2015 23:21 WG817026
Bromobenzene ND 1.00 1 09/24/2015 23:21 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 23:21 WG817026
Bromoform ND 1.00 1 09/24/2015 23:21 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 23:21 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 23:21 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 23:21 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 23:21 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 23:21 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 23:21 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 23:21 WG817026
Chloroethane ND 5.00 1 09/24/2015 23:21 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 23:21 WG817026
Chloroform ND 5.00 1 09/24/2015 23:21 WG817026
Chloromethane ND 2.50 1 09/24/2015 23:21 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 23:21 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 23:21 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 23:21 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 23:21 WG817026
Dibromomethane ND 1.00 1 09/24/2015 23:21 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 23:21 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 23:21 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 23:21 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 23:21 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 23:21 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 23:21 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 23:21 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/24/2015 23:21 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 23:21 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 23:21 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 23:21 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 23:21 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 23:21 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 23:21 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 23:21 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 23:21 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 23:21 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 23:21 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 23:21 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 23:21 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 23:21 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 23:21 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 23:21 WG817026
Methyl tert-butyl ether 1.58 1.00 1 09/24/2015 23:21 WG817026
Naphthalene ND 5.00 1 09/24/2015 23:21 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 23:21 WG817026
Styrene ND 1.00 1 09/24/2015 23:21 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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SM-6 SAMPLE RESULTS - 13 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 12:15 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 23:21 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 23:21 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 23:21 WG817026 F
Tetrachloroethene ND 1.00 1 09/24/2015 23:21 WG817026
Toluene ND 5.00 1 09/24/2015 23:21 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 23:21 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 23:21 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 23:21 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 23:21 WG817026
Trichloroethene ND 1.00 1 09/24/2015 23:21 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 23:21 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 23:21 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 23:21 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 23:21 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 23:21 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 23:21 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 23:21 WG817026
(S)Toluene-d8 100 90.0-115 091241201523:21 WG817026 F
(S)Dibromofluoromethone 101 79.0-121 091241201523:21 WG817026
(S)4-Bromofluorobenzene 103 80.1-120 091241201523:21 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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JW-1 SAMPLE RESULTS - 14 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 13:15 L789444
Wet Chemistry by Method 9060A
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
TOC(Total Organic Carbon) ND 1000 1 09/22/2015 20:32 WG816627
Volatile Organic Compounds (GC/MS) by Method 8260B FSS
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/I ug/I date/time 4Cn
Acetone ND 50.0 1 09/24/2015 23:42 WG817026
Acrolein ND 50.0 1 09/24/2015 23:42 WG817026
Acrylonitrile ND 10.0 1 09/24/2015 23:42 WG817026
Benzene ND 1.00 1 09/24/2015 23:42 WG817026
Bromobenzene ND 1.00 1 09/24/2015 23:42 WG817026 6
QC
Bromodichloromethane ND 1.00 1 09/24/2015 23:42 WG817026
Bromoform ND 1.00 1 09/24/2015 23:42 WG817026 F
Bromomethane ND 5.00 1 09/24/2015 23:42 WG817026 q
n-Butylbenzene ND 1.00 1 09/24/2015 23:42 WG817026
sec-Butylbenzene ND 1.00 1 09/24/2015 23:42 WG817026 FAI
tert-Butylbenzene ND 1.00 1 09/24/2015 23:42 WG817026
Carbon tetrachloride ND 1.00 1 09/24/2015 23:42 WG817026 FSC
Chlorobenzene ND 1.00 1 09/24/2015 23:42 WG817026
Chlorodibromomethane ND 1.00 1 09/24/2015 23:42 WG817026
Chloroethane ND 5.00 1 09/24/2015 23:42 WG817026
2-Chloroethyl vinyl ether ND 50.0 1 09/24/2015 23:42 WG817026
Chloroform ND 5.00 1 09/24/2015 23:42 WG817026
Chloromethane ND 2.50 1 09/24/2015 23:42 WG817026
2-Chlorotoluene ND 1.00 1 09/24/2015 23:42 WG817026
4-Chlorotoluene ND 1.00 1 09/24/2015 23:42 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/24/2015 23:42 WG817026
1,2-Dibromoethane ND 1.00 1 09/24/2015 23:42 WG817026
Dibromomethane ND 1.00 1 09/24/2015 23:42 WG817026
1,2-Dichlo robe nzene ND 1.00 1 09/24/2015 23:42 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/24/2015 23:42 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/24/2015 23:42 WG817026
Dichlorodifluoromethane ND 5.00 1 09/24/2015 23:42 WG817026
1,1-Dichloroethane ND 1.00 1 09/24/2015 23:42 WG817026
1,2-Dichloroethane ND 1.00 1 09/24/2015 23:42 WG817026
1,1-Dichloroethene ND 1.00 1 09/24/2015 23:42 WG817026
cis-1,2-Dichloroethene 3.49 1.00 1 09/24/2015 23:42 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/24/2015 23:42 WG817026
1,2-Dichloropropane ND 1.00 1 09/24/2015 23:42 WG817026
1,1-Dichloropropene ND 1.00 1 09/24/2015 23:42 WG817026
1,3-Dichloropropane ND 1.00 1 09/24/2015 23:42 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/24/2015 23:42 WG817026
trans-13-Dichloropropene ND 1.00 1 09/24/2015 23:42 WG817026
2,2-Dichloropropane ND 1.00 1 09/24/2015 23:42 WG817026
Di-isopropyl ether ND 1.00 1 09/24/2015 23:42 WG817026
Ethylbenzene ND 1.00 1 09/24/2015 23:42 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/24/2015 23:42 WG817026
Isopropylbenzene ND 1.00 1 09/24/2015 23:42 WG817026
p-Isopropyltoluene ND 1.00 1 09/24/2015 23:42 WG817026
2-Butanone(MEK) ND 10.0 1 09/24/2015 23:42 WG817026
Methylene Chloride ND 5.00 1 09/24/2015 23:42 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/24/2015 23:42 WG817026
Methyl tert-butyl ether ND 1.00 1 09/24/2015 23:42 WG817026
Naphthalene ND 5.00 1 09/24/2015 23:42 WG817026
n-Propylbenzene ND 1.00 1 09/24/2015 23:42 WG817026
Styrene ND 1.00 1 09/24/2015 23:42 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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JW-1 SAMPLE RESULTS - 14 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 13:15 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,1,1,2-Tetrachloroethane ND 1.00 1 09/24/2015 23:42 WG817026 Z
Tc
1,1,2,2-Tetrachloroethane ND 1.00 1 09/24/2015 23:42 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/24/2015 23:42 WG817026 F
Tetrachloroethene 24.3 1.00 1 09/24/2015 23:42 WG817026
Toluene ND 5.00 1 09/24/2015 23:42 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/24/2015 23:42 WG817026 Fn
1,2,4-Trichlorobenzene ND 1.00 1 09/24/2015 23:42 WG817026
1,1,1-Trichloroethane ND 1.00 1 09/24/2015 23:42 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/24/2015 23:42 WG817026
Trichloroethene 2.46 1.00 1 09/24/2015 23:42 WG817026
Trichlorofluoromethane ND 5.00 1 09/24/2015 23:42 WG817026 6
QC
1,2,3-Trichloropropane ND 2.50 1 09/24/2015 23:42 WG817026
1,2,4-Trimethylbenzene ND 1.00 1 09/24/2015 23:42 WG817026 F
1,2,3-Trim ethyl benzene ND 1.00 1 09/24/2015 23:42 WG817026 ql
1,3,5-Trim ethyl benzene ND 1.00 1 09/24/2015 23:42 WG817026
Vinyl chloride ND 1.00 1 09/24/2015 23:42 WG817026 FAI
Xylenes,Total ND 3.00 1 09/24/2015 23:42 WG817026
(S)Toluene-d8 101 90.0-115 091241201523:42 WG817026 F
(S)Dibromofluoromethone 101 79.0-121 091241201523:42 WG817026
(S)4-Bromofluorobenzene 102 80.1-120 091241201523.42 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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FIELD BLANK 2 SAMPLE RESULTS - 15 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 09:00 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch FP1
Analyte ug/I ug/I date/time
FTc
Acetone ND 50.0 1 09/25/2015 00:04 WG817026
Acrolein ND 50.0 1 09/25/2015 00:04 WG817026
Acrylonitrile ND 10.0 1 09/25/2015 00:04 WG817026 F
Benzene ND 1.00 1 09/25/2015 00:04 WG817026
Bromobenzene ND 1.00 1 09/25/2015 00:04 WG817026 4
Bromodichloromethane ND 1.00 1 09/25/2015 00:04 WG817026 Cn
Bromoform ND 1.00 1 09/25/2015 00:04 WG817026
Bromomethane ND 5.00 1 09/25/2015 00:04 WG817026
n-Butylbenzene ND 1.00 1 09/25/2015 00:04 WG817026
sec-Butylbenzene ND 1.00 1 09/25/2015 00:04 WG817026 Fc
tert-Butylbenzene ND 1.00 1 09/25/2015 00:04 WG817026
Carbon tetrachloride ND 1.00 1 09/25/2015 00:04 WG817026
Chlorobenzene ND 1.00 1 09/25/2015 00:04 WG817026 rq
Chlorodibromomethane ND 1.00 1 09/25/2015 00:04 WG817026
Chloroethane ND 5.00 1 09/25/2015 00:04 WG817026 FAI
2-Chloroethyl vinyl ether ND 50.0 1 09/25/2015 00:04 WG817026
Chloroform ND 5.00 1 09/25/2015 00:04 WG817026
Chloromethane ND 2.50 1 09/25/2015 00:04 WG817026 F
2-Chlorotoluene ND 1.00 1 09/25/2015 00:04 WG817026
4-Chlorotoluene ND 1.00 1 09/25/2015 00:04 WG817026
1,2-Dibromo-3-Chloropropane ND 5.00 1 09/25/2015 00:04 WG817026
1,2-Dibromoethane ND 1.00 1 09/25/2015 00:04 WG817026
Dibromomethane ND 1.00 1 09/25/2015 00:04 WG817026
1,2-Dichlorobenzene ND 1.00 1 09/25/2015 00:04 WG817026
1,3-Dichlorobenzene ND 1.00 1 09/25/2015 00:04 WG817026
1,4-Dichlorobenzene ND 1.00 1 09/25/2015 00:04 WG817026
Dichlorodifluoromethane ND 5.00 1 09/25/2015 00:04 WG817026
1,1-Dichloroethane ND 1.00 1 09/25/2015 00:04 WG817026
1,2-Dichloroethane ND 1.00 1 09/25/2015 00:04 WG817026
1,1-Dichloroethene ND 1.00 1 09/25/2015 00:04 WG817026
cis-1,2-Dichloroethene ND 1.00 1 09/25/2015 00:04 WG817026
trans-1,2-Dichloroethene ND 1.00 1 09/25/2015 00:04 WG817026
1,2-Dichloropropane ND 1.00 1 09/25/2015 00:04 WG817026
1,1-Dichloropropene ND 1.00 1 09/25/2015 00:04 WG817026
1,3-Dichloropropane ND 1.00 1 09/25/2015 00:04 WG817026
cis-1,3-Dichloropropene ND 1.00 1 09/25/2015 00:04 WG817026
trans-1,3-Dichloropropene ND 1.00 1 09/25/2015 00:04 WG817026
2,2-Dichloropropane ND 1.00 1 09/25/2015 00:04 WG817026
Di-isopropyl ether ND 1.00 1 09/25/2015 00:04 WG817026
Ethylbenzene ND 1.00 1 09/25/2015 00:04 WG817026
Hexachloro-1,3-butadiene ND 1.00 1 09/25/2015 00:04 WG817026
Isopropylbenzene ND 1.00 1 09/25/2015 00:04 WG817026
p-Isopropyltoluene ND 1.00 1 09/25/2015 00:04 WG817026
2-Butanone(MEK) ND 10.0 1 09/25/2015 00:04 WG817026
Methylene Chloride ND 5.00 1 09/25/2015 00:04 WG817026
4-Methyl-2-pentanone(MIBK) ND 10.0 1 09/25/2015 00:04 WG817026
Methyl tert-butyl ether ND 1.00 1 09/25/2015 00:04 WG817026
Naphthalene ND 5.00 1 09/25/2015 00:04 WG817026
n-Propylbenzene ND 1.00 1 09/25/2015 00:04 WG817026
Styrene ND 1.00 1 09/25/2015 00:04 WG817026
1,1,1,2-Tetrachloroethane ND 1.00 1 09/25/2015 00:04 WG817026
1,1,2,2-Tetrachloroethane ND 1.00 1 09/25/2015 00:04 WG817026
1,1,2-Trichlorotrifluoroethane ND 1.00 1 09/25/2015 00:04 WG817026
Tetrachloroethene ND 1.00 1 09/25/2015 00:04 WG817026
Toluene ND 5.00 1 09/25/2015 00:04 WG817026
1,2,3-Trichlorobenzene ND 1.00 1 09/25/2015 00:04 WG817026
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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FIELD BLANK 2 SAMPLE RESULTS - 15 ONE LAB.NATIONWIDE.
Collected date/time: 09/17/15 09:00 L789444
Volatile Organic Compounds (GC/MS) by Method 8260B
Result Qualifier RDL Dilution Analysis Batch F
Analyte ug/I ug/I date/time
1,2,4-Trichlorobenzene ND 1.00 1 09/25/2015 00:04 WG817026 Z
Tc
1,1,1-Trichloroethane ND 1.00 1 09/25/2015 00:04 WG817026
1,1,2-Trichloroethane ND 1.00 1 09/25/2015 00:04 WG817026 F
Trichloroethene ND 1.00 1 09/25/2015 00:04 WG817026
Trichlorofluoromethane ND 5.00 1 09/25/2015 00:04 WG817026
1,2,3-Trichloropropane ND 2.50 1 09/25/2015 00:04 WG817026 Fn
1,2,4-Trimethylbenzene ND 1.00 1 09/25/2015 00:04 WG817026
1,2,3-Trim ethyl benzene ND 1.00 1 09/25/2015 00:04 WG817026
1,3,5-Trim ethyl benzene ND 1.00 1 09/25/2015 00:04 WG817026
Vinyl chloride ND 1.00 1 09/25/2015 00:04 WG817026
Xylenes,Total ND 3.00 1 09/25/2015 00:04 WG817026 6
QC
(S)Toluene-d8 102 90.0-115 0912512015 00:04 WG817026
(S)Dibromofluoromethone 101 79.0-121 0912512015 00:04 WG817026 rq
(S)4-Bromofluorobenzene 94.1 80.1-120 0912512015 00:04 WG817026
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG816626 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Wet Chemistry by Method 9060A L789444-01,02,03,04,05,06
Method Blank (MB) FP1(MB)09/21/15 16:26
MB Result MB Qualifier MB RDL
FT
Analyte mg/I mg/ICTOC ND 1.00
rsS
L789224-01 Original Sample (OS) • Duplicate (DUP)
(OS)09/21/15 19:19•(DUP)09/21/1519:30 4Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
FSr
Analyte mg/I mg/I % %
TOC 2.42 2.50 1 3.25 20
L789075-05 Original Sample (OS) • Duplicate (DUP)
(OS)09/22/15 00:34•(DUP)09/22/15 00:46 GI
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/I mg/I % % $AI
TOC 3.53 3.82 1 7.89 20
Sc
L789399-02 Original Sample (OS) • Duplicate (DUP) 9
(OS)09/21/15 22:33•(DUP)09/21/15 22:45
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/I mg/I % %
TOC 3.58 3.52 1 1.69 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)09/21/15 17:20•(LCSD)09/21/1517:50
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/1 % % % % %
TOC 75.0 78.7 78.7 105 105 85.0-115 0.0762 20
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WG816626 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Wet Chemistry by Method 9060A L789444-01,02,03,04,05,06
L789224-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/21/15 19:42•(MS)09/21/1519:57•(MSD)09/21/15 20:12
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits F
Analyte mg/I mg/I mg/I mg/I % % % % %
TOC 50.0 5.19 56.6 50.9 103 91.3 1 80.0-120 10.6 20
FSS
[Cn]
FSr
�GI
FAI
[Sc
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WG816627 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Wet Chemistry by Method 9060A L789444-07,08,09,10,11,12,13,14
Method Blank (MB) FP1(MB)09/22/1515:58
MB Result MB Qualifier MB RDL
FT
Analyte mg/I mg/ICTOC ND 1.00
rsS
L789444-07 Original Sample (OS) • Duplicate (DUP)
(OS)09/22/1518:05•(DUP)09/22/15 19:29 4Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
FSr
Analyte mg/I mg/I % %
TOC 6.24 6.30 1 0.957 20
L789514-03 Original Sample (OS) • Duplicate (DUP)
(OS)09/22/15 22:08•(DUP)09/22/15 23:00 GI
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte mg/I mg/I % % $AI
TOC 1.98 2.00 1 1.01 20
Sc
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 9
(LCS)09/22/1516:59•(LCSD)09/22/1517:16
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
TOC 75.0 73.2 73.6 97.6 98.1 85.0-115 0.559 20
L789444-08 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)09/22/1518:22•(MS)09/22/15 18:39•(MSD)09/22/1518:59
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % %
TOC 50.0 0.910 49.4 49.5 98.7 99.0 1 80.0-120 0.243 20
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WG817026 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789444-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Method Blank (MB) FP1(MB)09/24/15 14:54
MB Result MB Qualifier MB RDL
FTC
Analyte mg/I mg/I
Acetone ND 0.0500
Acrolein ND 0.0500 FSS
Acrylonitrile ND 0.0100
Benzene ND 0.00100 [Cn]
Bromobenzene ND 0.00100
Bromodichloromethane ND 0.00100
Bromoform ND 0.00100 FSr
Bromomethane ND 0.00500
n-Butylbenzene ND 0.00100
sec-Butyl benzene ND 0.00100
tert-Butyl benzene ND 0.00100
Carbon tetrachloride ND 0.00100 7G1
Chlorobenzene ND 0.00100
Chlorodibromomethane ND 0.00100
Chloroethane ND 0.00500 FAI
2-Chloroethyl vinyl ether ND 0.0500
Chloroform ND 0.00500 FSC
Chloromethane ND 0.00250
2-Chlorotoluene ND 0.00100
4-Chlorotoluene ND 0.00100
1,2-Dibromo-3-Chloropropane ND 0.00500
1,2-Dibromoethane ND 0.00100
Dibromomethane ND 0.00100
1,2-Dichlorobenzene ND 0.00100
1,3-Dichlorobenzene ND 0.00100
1,4-Dichlorobenzene ND 0.00100
Dichlorodifluoromethane ND 0.00500
1,1-Dichloroethane ND 0.00100
1,2-Dichloroethane ND 0.00100
1,1-Dichloroethene ND 0.00100
cis-1,2-Dichloroethene ND 0.00100
trans-1,2-Dichloroethene ND 0.00100
1,2-Dichloropropane ND 0.00100
1,1-Dichloropropene ND 0.00100
1,3-Dichloropropane ND 0.00100
cis-1,3-Dichloropropene ND 0.00100
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WG817026 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789444-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Method Blank (MB) FP1(MB)09/24/15 14:54
MB Result MB Qualifier MB RDL
z
Analyte mg/I mg/I TC
trans-1,3-Dichloropropene ND 0.00100
2,2-Dichloropropane ND 0.00100 FSS
Di-isopropyl ether ND 0.00100
Ethylbenzene ND 0.00100 [Cn]
Hexachloro-1,3-butadiene ND 0.00100
Isopropylbenzene ND 0.00100
p-Isopropyltoluene ND 0.00100 FSr
2-Butanone(MEK) ND 0.0100
Methylene Chloride ND 0.00500
4-Methyl-2-pentanone(MIBK) ND 0.0100
Methyl tert-butyl ether ND 0.00100
Naphthalene ND 0.00500 GI
n-Propylbenzene ND 0.00100
Styrene ND 0.00100 FAI
1,1,1,2-Tetrachloroethane ND 0.00100
1,1,2,2-Tetrachloroethane ND 0.00100
Tetrachloroethene ND 0.00100 FSC
Toluene ND 0.00500
1,1,2-Trichlorotrifluoroethane ND 0.00100
1,2,3-Trichlorobenzene ND 0.00100
1,2,4-Trichlorobenzene ND 0.00100
1,1,1-Trichloroethane ND 0.00100
1,1,2-Trichloroethane ND 0.00100
Trichloroethene ND 0.00100
Trichlorofluoromethane ND 0.00500
1,2,3-Trichloropropane ND 0.00250
1,2,3-Trimethylbenzene ND 0.00100
1,2,4-Trim ethyl benzene ND 0.00100
1,3,5-Trimethylbenzene ND 0.00100
Vinyl chloride ND 0.00100
Xylenes,Total ND 0.00300
(S)Toluene-d8 103 90.0-115
(S)Dibromofluoromethane 99.4 79.0-121
(S)4-Bromofluorobenzene 103 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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WG817026 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789444-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1
(LCS)09/24/15 13:29•(LCSD)09/24/1513:50
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits FTC
Analyte mg/I mg/I mg/I % % % % %
Acetone 0.125 0.103 0.107 82.1 85.4 28.7-175 3.91 20.9
Acrolein 0.125 0.134 0.140 107 112 40.4-172 4.57 20 FSS
Acrylonitrile 0.125 0.113 0.118 90.2 94.5 58.2-145 4.64 20
Benzene 0.0250 0.0249 0.0257 99.4 103 73.0-122 3.43 20 [Cn]
Bromobenzene 0.0250 0.0269 0.0273 108 109 81.5-115 1.66 20
Bromodichloromethane 0.0250 0.0268 0.0267 107 107 75.5-121 0.290 20
Bromoform 0.0250 0.0272 0.0291 109 116 71.5-131 6.68 20 FSr
Bromomethane 0.0250 0.0274 0.0294 110 117 22.4-187 6.78 20
n-Butylbenzene 0.0250 0.0283 0.0277 113 111 75.9-134 2.12 20
sec-Butyl benzene 0.0250 0.0301 0.0300 120 120 80.6-126 0.320 20
tert-Butyl benzene 0.0250 0.0305 0.0299 122 120 79.3-127 2.16 20
Carbon tetrachloride 0.0250 0.0275 0.0288 110 115 70.9-129 4.64 20 7G1
Chlorobenzene 0.0250 0.0288 0.0290 115 116 79.7-122 0.710 20
Chlorodibromomethane 0.0250 0.0274 0.0278 110 111 78.2-124 1.40 20
Chloroethane 0.0250 0.0288 0.0297 115 119 41.2-153 3.14 20 FAI
2-Chloroethyl vinyl ether 0.125 0.0994 0.122 79.6 97.7 23.4-162 20.4 23.5
Chloroform 0.0250 0.0246 0.0256 98.2 102 73.2-125 4.13 20 FSC
Chloromethane 0.0250 0.0250 0.0265 100 106 55.8-134 5.74 20
2-Chlorotoluene 0.0250 0.0293 0.0289 117 116 76.4-125 1.28 20
4-Chlorotoluene 0.0250 0.0294 0.0285 118 114 81.5-121 3.01 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0233 0.0243 93.1 97.2 64.8-131 4.34 20
1,2-Dibromoethane 0.0250 0.0253 0.0261 101 104 79.8-122 3.15 20
Dibromomethane 0.0250 0.0254 0.0266 102 106 79.5-118 4.50 20
1,2-Dichlorobenzene 0.0250 0.0274 0.0267 109 107 84.7-118 2.42 20
1,3-Dichlorobenzene 0.0250 0.0298 0.0291 119 116 77.6-127 2.35 20
1,4-Dichlorobenzene 0.0250 0.0252 0.0248 101 99.4 82.2-114 1.33 20
Dichlorodifluoromethane 0.0250 0.0277 0.0286 111 114 56.0-134 2.92 20
1,1-Dichloroethane 0.0250 0.0250 0.0262 100 105 71.7-127 4.52 20
1,2-Dichloroethane 0.0250 0.0240 0.0243 96.0 97.0 65.3-126 1.03 20
1,1-Dichloroethene 0.0250 0.0284 0.0301 114 120 59.9-137 5.51 20
cis-1,2-Dichloroethene 0.0250 0.0253 0.0258 101 103 77.3-122 1.80 20
trans-1,2-Dichloroethene 0.0250 0.0261 0.0270 104 108 72.6-125 3.24 20
1,2-Dichloropropane 0.0250 0.0267 0.0266 107 107 77.4-125 0.260 20
1,1-Dichloropropene 0.0250 0.0255 0.0264 102 106 72.5-127 3.33 20
1,3-Dichloropropane 0.0250 0.0245 0.0243 98.1 97.2 80.6-115 0.900 20
cis-1,3-Dichloropropene 0.0250 0.0269 0.0268 107 107 77.7-124 0.460 20
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WG817026 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789444-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1
(LCS)09/24/15 13:29•(LCSD)09/24/1513:50
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z
Analyte mg/I mg/I mg/I % % % % % TC
trans-1,3-Dichloropropene 0.0250 0.0264 0.0269 105 108 73.5-127 2.15 20
2,2-Dichloropropane 0.0250 0.0261 0.0292 105 117 61.3-134 11.2 20 FSS
Di-isopropyl ether 0.0250 0.0245 0.0259 97.9 104 65.1-135 5.76 20
Ethylbenzene 0.0250 0.0285 0.0291 114 116 80.9-121 2.00 20 [Cn]
Hexachloro-1,3-butadiene 0.0250 0.0309 0.0283 124 113 73.7-133 8.60 20
Isopropylbenzene 0.0250 0.0289 0.0290 116 116 81.6-124 0.450 20
p-Isopropyltoluene 0.0250 0.0312 0.0305 125 122 77.6-129 2.02 20 FSr
2-Butanone(MEK) 0.125 0.0991 0.103 79.3 82.1 46.4-155 3.48 20
Methylene Chloride 0.0250 0.0238 0.0250 95.3 99.9 69.5-120 4.69 20
4-Methyl-2-pentanone(MIBK) 0.125 0.121 0.120 96.6 95.9 63.3-138 0.740 20
Methyl tert-butyl ether 0.0250 0.0241 0.0261 96.5 104 70.1-125 7.86 20
Naphthalene 0.0250 0.0262 0.0266 105 106 69.7-134 1.63 20 7G1
n-Propylbenzene 0.0250 0.0288 0.0283 115 113 81.9-122 1.88 20
Styrene 0.0250 0.0287 0.0286 115 114 79.9-124 0.320 20 FAI
1,1,1,2-Tetrachloroethane 0.0250 0.0284 0.0295 113 118 78.5-125 4.04 20
1,1,2,2-Tetrachloroethane 0.0250 0.0263 0.0265 105 106 79.3-123 0.940 20
Tetrachloroethene 0.0250 0.0304 0.0304 122 121 73.5-130 0.270 20 FSC
Toluene 0.0250 0.0263 0.0262 105 105 77.9-116 0.270 20
1,1,2-Trichlorotrifluoroethane 0.0250 0.0293 0.0302 117 121 62.0-141 3.01 20
1,2,3-Trichlorobenzene 0.0250 0.0280 0.0281 112 112 75.7-134 0.370 20
1,2,4-Trichlorobenzene 0.0250 0.0297 0.0304 119 122 76.1-136 2.62 20
1,1,1-Trichloroethane 0.0250 0.0271 0.0287 109 115 71.1-129 5.65 20
1,1,2-Trichloroethane 0.0250 0.0266 0.0267 106 107 81.6-120 0.530 20
Trichloroethene 0.0250 0.0282 0.0281 113 112 79.5-121 0.260 20
Trichlorofluoromethane 0.0250 0.0304 0.0319 122 128 49.1-157 4.93 20
1,2,3-Trichloropropane 0.0250 0.0261 0.0269 104 108 74.9-124 3.23 20
1,2,3-Trimethylbenzene 0.0250 0.0272 0.0267 109 107 79.9-118 1.98 20
1,2,4-Trim ethyl benzene 0.0250 0.0294 0.0287 118 115 79.0-122 2.34 20
1,3,5-Trimethylbenzene 0.0250 0.0295 0.0295 118 118 81.0-123 0.190 20
Vinyl chloride 0.0250 0.0279 0.0293 112 117 61.5-134 4.85 20
Xylenes,Total 0.0750 0.0882 0.0875 118 117 79.2-122 0.770 20
(S)Toluene-d8 104 105 90.0-115
(S)Dibromofluoromethane 94.8 95.8 79.0-121
(S)4-Bromofluorobenzene 105 104 80.1-120
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WG817026 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789444-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
L789333-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/24/15 17:21•(MS)09/24/1515:30•(MSD)09/24/15 15:52
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % % FTCAcetone 0.125 0.00196 0.109 0.0996 85.9 78.1 1 25.0-156 9.36 21.5
Acrolein 0.125 ND 0.136 0.130 108 104 1 34.0-194 4.61 21.5 FSS
Acrylonitrile 0.125 ND 0.119 0.116 94.9 92.5 1 55.9-161 2.56 20
Benzene 0.0250 ND 0.0233 0.0232 93.4 92.9 1 58.6-133 0.490 20 4
Bromobenzene 0.0250 ND 0.0252 0.0261 101 104 1 70.6-125 3.42 20 Cn
Bromodichloromethane 0.0250 ND 0.0256 0.0260 103 104 1 69.2-127 1.29 20
Bromoform 0.0250 ND 0.0279 0.0268 112 107 1 66.3-140 3.97 20 FSr
Bromomethane 0.0250 ND 0.0265 0.0251 106 100 1 16.6-183 5.44 20.5
n-Butylbenzene 0.0250 ND 0.0273 0.0276 109 110 1 64.8-145 1.09 20
sec-Butyl benzene 0.0250 ND 0.0275 0.0276 110 111 1 66.8-139 0.490 20
tert-Butyl benzene 0.0250 ND 0.0273 0.0280 109 112 1 67.1-138 2.47 20
Carbon tetrachloride 0.0250 ND 0.0266 0.0263 106 105 1 60.6-139 1.19 20 7G1
Chlorobenzene 0.0250 ND 0.0268 0.0266 107 106 1 70.1-130 0.980 20
Chlorodibromomethane 0.0250 ND 0.0269 0.0266 108 106 1 71.6-132 1.04 20
Chloroethane 0.0250 ND 0.0283 0.0276 113 110 1 33.3-155 2.62 20 FAI
2-Chloroethyl vinyl ether 0.125 ND 0.124 0.118 99.6 94.8 1 5.00-149 4.93 40
Chloroform 0.0250 ND 0.0242 0.0237 96.9 94.8 1 66.1-133 2.28 20 FSC
Chloromethane 0.0250 ND 0.0236 0.0230 94.4 92.1 1 40.7-139 2.43 20
2-Chlorotoluene 0.0250 ND 0.0268 0.0264 107 106 1 66.9-134 1.50 20
4-Chlorotoluene 0.0250 ND 0.0269 0.0271 107 108 1 66.8-134 0.960 20
1,2-Dibromo-3-Chloropropane 0.0250 ND 0.0260 0.0235 104 93.9 1 63.9-142 10.2 20.2
1,2-Dibromoethane 0.0250 ND 0.0251 0.0258 100 103 1 73.8-131 2.82 20
Dibromomethane 0.0250 ND 0.0253 0.0246 101 98.6 1 72.8-127 2.73 20
1,2-Dichlorobenzene 0.0250 ND 0.0272 0.0266 109 106 1 77.4-127 2.13 20
1,3-Dichlorobenzene 0.0250 ND 0.0285 0.0281 114 112 1 67.9-136 1.43 20
1,4-Dichlorobenzene 0.0250 ND 0.0241 0.0241 96.3 96.4 1 74.4-123 0.140 20
Dichlorodifluoromethane 0.0250 ND 0.0259 0.0253 104 101 1 42.2-146 2.41 20
1,1-Dichloroethane 0.0250 ND 0.0236 0.0237 94.4 94.7 1 64.0-134 0.360 20
1,2-Dichloroethane 0.0250 ND 0.0235 0.0230 93.9 92.0 1 60.7-132 2.00 20
1,1-Dichloroethene 0.0250 ND 0.0264 0.0261 106 104 1 48.8-144 1.39 20
cis-1,2-Dichloroethene 0.0250 ND 0.0240 0.0230 95.9 92.1 1 60.6-136 3.95 20
trans-1,2-Dichloroethene 0.0250 ND 0.0242 0.0238 96.6 95.1 1 61.0-132 1.63 20
1,2-Dichloropropane 0.0250 ND 0.0256 0.0249 103 99.7 1 69.7-130 2.81 20
1,1-Dichloropropene 0.0250 ND 0.0237 0.0240 94.8 95.9 1 61.5-136 1.20 20
1,3-Dichloropropane 0.0250 ND 0.0236 0.0237 94.3 94.9 1 74.3-123 0.600 20
cis-1,3-Dichloropropene 0.0250 ND 0.0255 0.0252 102 101 1 71.1-129 1.21 20
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WG817026 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L789444-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
L789333-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1
(OS)09/24/15 17:21•(MS)09/24/1515:30•(MSD)09/24/15 15:52
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits z
Analyte mg/I mg/I mg/I mg/I % % % % % TC
trans-1,3-Dichloropropene 0.0250 ND 0.0267 0.0263 107 105 1 66.3-136 1.59 20
2,2-Dichloropropane 0.0250 ND 0.0267 0.0260 107 104 1 54.9-142 2.73 20 FSS
Di-isopropyl ether 0.0250 ND 0.0235 0.0234 94.1 93.5 1 59.9-140 0.640 20
Ethylbenzene 0.0250 ND 0.0267 0.0265 107 106 1 62.7-136 0.640 20 4
Hexachloro-1,3-butadiene 0.0250 ND 0.0286 0.0289 114 116 1 61.1-144 1.23 20.1 Cn
Isopropylbenzene 0.0250 ND 0.0266 0.0270 106 108 1 67.4-136 1.50 20
p-Isopropyltoluene 0.0250 ND 0.0288 0.0285 115 114 1 62.8-143 1.15 20 FSr
2-Butanone(MEK) 0.125 ND 0.103 0.0982 82.1 78.5 1 45.0-156 4.45 20.8
Methylene Chloride 0.0250 0.000736 0.0234 0.0224 90.5 86.7 1 61.5-125 4.21 20
4-Methyl-2-pentanone(MIBK) 0.125 ND 0.123 0.117 98.0 93.8 1 60.7-150 4.43 20
Methyl tert-butyl ether 0.0250 ND 0.0251 0.0233 101 93.1 1 61.4-136 7.69 20
Naphthalene 0.0250 ND 0.0261 0.0253 104 101 1 61.8-143 2.89 20 7G1
n-Propylbenzene 0.0250 ND 0.0266 0.0268 107 107 1 63.2-139 0.620 20
Styrene 0.0250 ND 0.0268 0.0270 107 108 1 68.2-133 0.920 20 FAI
1,1,1,2-Tetrachloroethane 0.0250 ND 0.0274 0.0276 109 ill 1 70.5-132 1.05 20
1,1,2,2-Tetrachloroethane 0.0250 ND 0.0266 0.0256 106 103 1 64.9-145 3.69 20
Tetrachloroethene 0.0250 ND 0.0283 0.0274 113 110 1 57.4-141 3.30 20 FSC
Toluene 0.0250 ND 0.0249 0.0244 99.5 97.5 1 67.8-124 1.99 20
1,1,2-Trichlorotrifluoroethane 0.0250 ND 0.0280 0.0265 112 106 1 53.7-150 5.55 20
1,2,3-Trichlorobenzene 0.0250 ND 0.0278 0.0273 ill 109 1 65.7-143 1.83 20
1,2,4-Trichlorobenzene 0.0250 ND 0.0309 0.0292 123 117 1 67.0-146 5.42 20
1,1,1-Trichloroethane 0.0250 ND 0.0264 0.0251 105 100 1 58.7-134 4.79 20
1,1,2-Trichloroethane 0.0250 ND 0.0257 0.0255 103 102 1 74.1-130 0.880 20
Trichloroethene 0.0250 ND 0.0263 0.0258 105 103 1 48.9-148 1.74 20
Trichlorofluoromethane 0.0250 ND 0.0295 0.0295 118 118 1 39.9-165 0.200 20
1,2,3-Trichloropropane 0.0250 ND 0.0252 0.0252 101 101 1 71.5-134 0.110 20
1,2,3-Trimethylbenzene 0.0250 ND 0.0256 0.0256 102 102 1 62.7-133 0.0700 20
1,2,4-Trim ethyl benzene 0.0250 ND 0.0274 0.0275 110 110 1 60.5-137 0.200 20
1,3,5-Trimethylbenzene 0.0250 ND 0.0276 0.0271 110 108 1 67.9-134 1.56 20
Vinyl chloride 0.0250 ND 0.0264 0.0263 106 105 1 44.3-143 0.210 20
Xylenes,Total 0.0750 ND 0.0821 0.0813 109 108 1 65.6-133 0.960 20
(S)Toluene-d8 105 103 90.0-115
(S)Dibromofluoromethane 95.7 95.7 79.0-121
(S)4-Bromofluorobenzene 101 104 80.1-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Bunnell-Lammons Engineering,Inc. J15-1022-42 L789444 09/30/1510:25 45 of 50

GLOSSARY OF TERMS ONE LAB.NATIONWIDE.
Abbreviations and Definitions
SDG Sample Delivery Group. FP1
MDL Method Detection Limit.
RDL Reported Detection Limit. FTc
ND,U Not detected at the Reporting Limit(or MDL where applicable).
RPD Relative Percent Difference. FS
(dry) Results are reported based on the dry weight of the sample.[this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD) 4 n
from a quality control sample.The Original Sample may not be included within the reported SDG.
(S) Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring Sr
recovery.Surrogates are not expected to be detected in all environmental media.
Rec. Recovery. RCSDL Sample Detection Limit.
MQL Method Quantitation Limit.
Unadj. MQL Unadjusted Method Quantitation Limit.
Qualifier Description rAl
J2 Surrogate recovery limits have been exceeded;values are outside lower control limits. FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE.
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lab is as accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the
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decreasing turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
State Accreditations ITC]
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California 01157CA New York 11742 Cn
Colorado TN00003 North Carolina Env375
Conneticut PH-0197 North Carolina DW21704 FS
Florida E87487 North Carolina 2 41
Georgia NELAP North Dakota R-140
Georgia' 923 Ohio—VAP CL0069 Rc
Idaho TN00003 Oklahoma 9915
Illinois 200008 Oregon 68-TN200002
Indiana C-TN-01 Pennsylvania 68-02979979 7G�
Iowa 364 Rhode Island 221
Kansas E-10277 South Carolina 84004
Kentucky' 90010 South Dakota n/a
Kentucky 16 Tennessee14 2006
Louisiana A130792 Texas T 104704245-07-TX FSC
Maine TN0002 Texas5 LABO152
Maryland 324 Utah 6157585858
Massachusetts M-TNO03 Vermont VT2006
Michigan 9958 Virginia 109
Minnesota 047-999-395 Washington C1915
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Nebraska NE-OS-15-05
Drinking Water z Underground Storage Tanks a Aquatic Toxicity 4.Chemical/Microbiological 5.Mold n1a Accreditation not applicable
Third Party& Federal Accreditations
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Canada 1461.01 DOD 1461.01
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Our Locations
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies.If you would like assistance from one of our support offices,please
contact our main office.ESC Lab Sciences performs all testing at our central laboratory.
m
WA
ME
MT ND
OR MN
IO SO Ir NJI T NY T +
WY �I
T NE 1= PA
Gam. NV U ♦
T T COT ♦ T
T KS MT VAT
KY
i TAZ NM OIt Ali N SC
T a7 T
T !MS AL CA
TX LA T
AK T
a a FL
Q
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ego . HI 5 y
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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Billing lnrarmation- Analysis I Can#airier}PrQj vjtFie Char,of Cu�ap4�y Paige of
Bunnell - Lammons Engineering, Inc. project manager -- -
6004 Ponders Court
6004 Ponders Court Greenville,5C 29615 OESCI
Greenville,5C 29615 � i_-A C-I.E-N-C—E �
Report tc]; F..ma;I To:andy@b1K0FP,C0M 206�Lrhanon Rd Q Q
Maur;Juliet,TN 3 73 22
Mr.Andy Alexander A Phore:ais-rssssse
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Project t,r.v +r Clty/5tat I Fer 615.7sa-aesg
4eserlptian- Andrex Industries Colleted! it -,//-,7 g.q.
Phone.[phone] Client Project P Lab Project itI I C 2
JIS-1022-42 SUNLAMGSC-J141O2240 + F242
Fax_ 964-288-4430 2
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collected by(prinQ: SitejFa€ility Id 0 P.U.g b-
ASHE;III.LE,,N€ InI I
Acctnum;9UNLAMGSC
Template_T98401
CDl�ecied by(signs }: Rush? (Lab MUST Be Notified Dace Results Needed E E I
d' _Same day..."."......"."...."......"2W9G Pre login;P524318
_N c)t L°ay............................13C4f kmail? No 5f Yes O TSR: 0-lirrrr,►"d^1�F+t
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Packed on Ice N_ Y_ _1 liras Day.--... ..."....................1595 fA}(",-Np _yes II
of
V rw Shipped Via:Fed EX Standard
Sample ID Comp/Grab MatrIK Uepth Date Time ri:rs , o0
A EM)CantinN nr iAin ale M;lat oils I
C - "wGW M f TO 3 x
GW 3 X X
Gyk GWJ X X
GW 15 174, 3 X X _
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Matrix. Z•Sal GW-Groundwater WW-4Wast�Water D'JV-Orinking hater OT-Other
emarlcsAnalyte at 1x. pH Temp -
Flow .. Other — Hold R
Relinq ui shed by:(Sig re Date;f Time! Received by;ISlgn urS) Sa;ltdE);
returned "a-- G]UP5 ---" [anditi�n T� (.'ab use on�l
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e uish by: date; Tlrne; Received by;(Sig q Temp, eC 9otiles Received:
incart! `- Y N NA
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kelloqulshed'ay- date: Time: Received far lab by_(5ignature� DiNte- m pHk-necked: NCF;
µ _L

9illingInfarmatrun: Analyiil{Cantai r�"Peservrkvc Chain ofCu�tQdy Page_at�
Bunnell - LrrTmons Engineering, inc. Project Manager
6004 Panders Court
6004 Ponders Court Greenville, SC 29615
CireenvilJe,SC 29615 i*ESC�
RepQrtto; EmailTo Andy@blerarp-wm :iafi5LtbananRd 1=1
Mr.Andy Alexander Moons luliet.77137122 �
Phana 615-:56-5e49
Pfbje[t ,9e—e r, City4late Phone.C011-m m95
1 i� Fax:fiLfi-75d-5a59 IeF
Description! L4ndrele InduStrics Collected= A r�-, Lr �•
Phone:S64 288-1 65 Cllent Paojefk R Lab aroiect N C it q F�+
eax. 864-298 30 J15-1D22-4 BUNLAMGSC-JI41OZ2,40 V I _�-�—�b ff�7
Table 4 F
Collected by(printl-;y 5,[e{Faul ity it)spCL
3c .L T Lrc ASHEVILLE, NC sa j Acctnum; BUNLAMGSC
Collated by{signa#ure ;
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sh? (lab MUST Be N4[ificd} Date ResulkS Needrd I
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shipped via:Fed EX Ste Time � 0 Go e1
,a-znle a,
GW X
IY1 - ' w art GW X
rl'1 - rib GW z 3 X X _ }
CIO 'i GW ( x 3 X X
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hllr trl]C 55-$OR SW Grauncrwgker MM-W.a5leS MEF aW-C�rinkl ng water 01.Other_ —
emarks;Analyze at lx. P„ -- femp 1
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Rellnqtrlshed by:($igna Date: Time- Recelved by:;Sign ture) Samples returned".. Q UPS ConQltion:
{1�'� �� {lab u4e only}}
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R In ishkl by= r)ate Time, Received by:i5ig q Te p= IlMtles Received-,
.
L '7 +—F k:OC seal Intact: _Y _N NA
Relinquished by; Pate: Time: Rp[eived for lab by [Signatiire� date; Time; pH Checked= NCF —

Troy Dunlap
EC Lab Sciences
Nan-Conformance Form
Login#: L 889444 Client: BU LLAMGSC �ate.9/18/15 E+,+aluated by:Troy Dunlap
Non-Conformance(Lheck a p p livable iteins
Sampie Integrity Chain of Custody Clarification
Parameter(s)past holding
time X Lo in Clarification Needed if Broken COatalner.
Improper
temperature Chain of custody is incomplete Insufficient packing material around container
Improper container Pleases eci Metals re uested. insufficient packing material inside
e
i f}' cooler
Improper Ple2se specify TCLP requested_
preservation Improperhandlin b carrier FedEx UPS Course
Received additional sample sample was
not listed on coc, frozen
Insumcientsample volume.
Sample ids on containers do not match ids on
Sample is biphasic. coc Cont2aIner lid not intact
Vials received with headspace. Trip Blank not received 1f no Chain of Custody:
Broken container Client did not"X"analysis. Received by:
Broken container. Chain ofCtistodz is missing Date Time:
Sufficient sa rniple remains 'fern Cont.Rec./PH:
Carrier-
Trackin
Login ents: Did n9t received a TOC Contiainer for F AD BLANK
Client informed b = Call x I Email Voice Mail Date; 211 1! Time= 0935
T R Initials: "eh Client Contact; Ben Nisberh
Login InsUlictiolls: Field 131anh 2 should only e analyzed for V
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1

APPENDIX H
TOC
TIME VS.CONCENTRATION PLOTS

MW-5 -- Total Organic Carbon
5,000 -1-
Injection RW-1, RW-3, RW-5,& RW-7
4,500 Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
4,000 Injection IW-2
Injection IW-1& IW-3
3,500
J
to
E 3,000
c
0
2,500
4-0
w 2,000
c
0
u 1,500
1,000
500
<--- Baseline Data ---> d
�J
0 L Aff-I
O O r-I r-1 r-I r-1 T-I
N N N N N N N N N

MW-6 -- Total Organic Carbon
35
amommoInjection RW-1, RW-3, RW-5,& RW-7
30 Injection RW-1, RW-3, RW-5,& RW-7
sommisiniection RW-1, RW-3, & RW-5
Injection IW-2
25 ammmisinjection IW-1& IW-3
J
tw
E
20
C
O
i
a,
15
c
V
10
.o7
5
Se`�epa Q'aSe���
0
M O r-I N M Oct e``�e LA
0 0 0 0 0 0 has o 0 0
N N N N N N N N N

MW-7 -- Total Organic Carbon
20
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
15 Injection IW-1& IW-3
J
to
E
C
O
10
4-0
a,
U
C
V
5
<--- Baseline Data --->
0 iA
LM
N N N N N N N N 0

MW-9 -- Total Organic Carbon
40
Injection RW-1, RW-3, RW-5,& RW-7
35 Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
30 Injection IW-1& IW-3
J
dA
E 25
c
0
20
4-0
a�
c 15
0
u
10
5
F<--- Baseline Data --->
0
OO �r�-I �N-I iM-I ��-I
0
0
0
0
N N N N N

MW-10 -- Total Organic Carbon
450
Injection RW-1, RW-3, RW-5,& RW-7
400 Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
350 Injection IW-2
Injection IW-1& IW-3
J 300
to
E
c 250
4-0
200
a�
c
150
100
50
<--- Baseline Data --->
0 ``�
OaSe rqLM
N N N N N N N N N

MW-11 -- Total Organic Carbon
20
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
15 Injection IW-1& IW-3
J
to
E
C
O
10
4-0
a,
U
C
V
5
F<--- Baseline Data --->
Ao--O�
o �
0
0
0
0
N N N N N

MW-12 -- Total Organic Carbon
1,400
Injection RW-1, RW-3, RW-5,& RW-7
—Injection RW-1, RW-3, RW-5,& RW-7
1,200
Injection RW-1, RW-3, & RW-5
Injection IW-2
1,000 'Injection IW-1& IW-3
J
dA
E
C
800
O
4-0
600
c
u°
400
200
<--- Baseline Data --->
0
0 0 �
N N N N N N N N N

MW-13 -- Total Organic Carbon
20
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
15 Injection IW-1& IW-3
J
to
E
C
O
10
4-0
a,
U
C
V
5
<--- Baseline Data --->
0
o r
0
0
0
0
N N N N N

MW-14 -- Total Organic Carbon
20
Injection RW-1, RW-3, RW-5,& RW-7
� Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
15 Injection IW-1& IW-3
J
to
E
C
O
10
4-0
a,
U
C
V
5
<--- Baseline Data --->
0
o �
0
0
0
0
N N N N N

MW-24 -- Total Organic Carbon
20
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
15 Injection IW-1& IW-3
J
tw
E
C
O
10
c
a�
U
C
V
5
0100Mel
0 0 � � � RCT �
N N N N N N N N N

MW-44 -- Total Organic Carbon
20
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
15 Injection IW-1& IW-3
J
to
E
C
O
10
4-0
c `OG•
O 4�
V
5
dip
0
0
Ln
O O r-I r-I r-I r-I r-I r-I rl
0
0
0
0
N 0
N N 0

IW-2 -- Total Organic Carbon
5,000
Injection RW-1, RW-3, RW-5,& RW-7
4,500 Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
4,000 Injection IW-2
Injection IW-1& IW-3
._ 3,500
to
E 3,000
c
0
2,500
4-0
w 2,000
c
0
u 1,500
1,000
0
49
c�
500 a 4
40.
0
o r ° �
N N N N N N N N 0

RW-1 -- Total Organic Carbon
7,000
Injection RW-1, RW-3, RW-5,& RW-7
m Injection RW-1, RW-3, RW-5,& RW-7
6,000 Injection RW-1, RW-3, & RW-5
Injection IW-2
Injection IW-1& IW-3
5,000
J
dA
E
r 4,000
0
4-0
a,
3,000
U
C
0
V
2,000
BasP,'�e
1,000
<--- Baseline Data --->
�J
0
Ln
O O r-I r-I r-I r-I r-I
N N N N N N N N N

RW-3 -- Total Organic Carbon
4,500 -1-
Injection RW-1, RW-3, RW-5,& RW-7
4,000 Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
3,500 Injection IW-2
Injection IW-1& IW-3
3,000
ao
E
v
c 2,500
c 2,000
w
U
C
1,500
1,000
o �
500 a
< Baseline Data --->
v
0 J
01 O r-I N M Ln
O O O O O O O O O
N N N N N N N N N

RW-5 -- Total Organic Carbon
4,000
Injection RW-1, RW-3, RW-5,& RW-7
3,500 Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
3,000 Injection IW-1& IW-3
J
E 2,500
v
O
2,000
4-0
a�
c 1,500
u°
1,000
500
<--- Baseline Data --->
0
o � T I AM
0
0
0
0
0
0
0
N N

RW-6 -- Total Organic Carbon
20
Injection RW-1, RW-3, RW-5,& RW-7
� Injection RW-1, RW-3, RW-5,& RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
15 Injection IW-1& IW-3
J
to
E
C
O
10
4-0
a,
U
C
O
V
5
<--- Baseline Data --->
I
0
LM
O r�-I rN-I rM-I r�-I rrq
0
0
0
0
0
0
0
N 0

RW-7 -- Total Organic Carbon
6,000
Injection RW-1, RW-3, RW-5,& RW-7
4- —Injection RW-1, RW-3, RW-5,& RW-7
5,000 Injection RW-1, RW-3, & RW-5
Injection IW-2
Injection IW-1& IW-3
4,000
ao
E
v
r_
O
3,000
c
a,
U
C
u° 2.000
1,000
<--- Baseline Data --->
0
LM
N N N N N N N N N

APPENDIX I
VOC
TIME VS.CONCENTRATION PLOTS

Monitoring Well MW-5
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
9,000
-� Perchloroethene
—0 Trichloroethene
8,000 --#- cis-1,2-Dichloroethene
— —Vinyl Chloride
7,000 ♦ Injection RW-1, RW-3, RW-5, & RW-7
0 Injection IW-2
6,000 o Injection IW-1 & IW-3
0 Injection RW-1, RW-3, RW-5, & RW-7
C 5,000 0 Injection RW-1, RW-3, & RW-5
co
i
4.000
a�
U
C /110
u° 3,000
2,000
1,000 <-- Baseline Data -->
0
0) O r-I N M RZT Ln l0 n
O O O O O O O O O
N N N N N N N N N

Monitoring Well MW-6
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
4,000 - Perchloroethene
Trichloroethene
cis-1,2-Dichloroethene
3,500000� —$FVinyl Chloride
A Injection RW-1, RW-3, RW-5,& RW-7
3,000 0 Injection RW-1, RW-3,& RW-5
0 Injection IW-1& IW-3
♦ Injection RW-1, RW-3, RW-5,& RW-7
b\u0 2,500 A Injection IW-2
C
O
2,000
c
a�
c 1,500
U
1,000
<-- Baseline Data -->
500
0
01 O r-I N M RZT Ln l0 N.
O O O O O O O O O
N N N N N N N N N

Monitoring Well MW-7
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
200
180
160
140
J
120
c
0
100
Perchloroethene
C
v80 Trichloroethene
C
o cis-1,2-Dichloroethene
V i
60 — —Vinyl Chloride
< Baseline Data --> ♦ Injection RW-1, RW-3, RW-5, & RW-7
40 0 Injection IW-2
A Injection IW-1 & IW-3
20 / A Injection RW-1, RW-3, RW-5, & RW-7
A Injection RW-1, RW-3, & RW-5
0
01 O r-I N M Ln tD I.
O O O O O O O O O
N N N N N N N N N

Monitoring Well MW-9
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
6,000
--F Perchloroethene
5,000 Trichloroethene
cis-1,2-Dichloroethene
— FVinyl Chloride
4,000 0 Injection RW-1, RW-3, RW-5, & RW-7
dA 0 Injection RW-1, RW-3, & RW-5
♦ Injection RW-1, RW-3, RW-5, & RW-7
O
o Injection Iw-2
3,000
A Injection IW-1 & IW-3
C
O
U
C
u° 2.000
<-- Baseline Data -->
Ooeoor
1,000
0
01 O r-I N M Ln W N.
O O O O O O O O O
N N N N N N N N N

Monitoring Well MW-10
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
4,000
Perchloroethene
3,500 Trichloroethene
cis-1,2-Dichloroethene
3,000 — FVinyl Chloride
♦ Injection RW-1, RW-3, RW-5, & RW-7
0 Injection IW-2
txo 2,500 0 Injection IW-1 & IW-3
0 Injection RW-1, RW-3, RW-5, & RW-7
O
0 2,000 0 Injection RW-1, RW-3, & RW-5
i
C
a1
c 1,500
V
1,000 <-- Baseline Data -->
500
0
0) O r-I N M Ln lC n
O O O O O O O O O
N N N N N N N N N

Monitroing Well MW-11
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
3,000
• Perchloroethene
2,500 Trichloroethene
cis-1,2-Dichloroethene
— FVinyl Chloride
2 0 Injection RW-1, RW-3, RW-5, & RW-7
,000
0 Injection RW-1, RW-3, & RW-5
�- , Injection IW-1 & IW-3
C
p ♦ Injection RW-1, RW-3, RW-5, & RW-7
1500 A Injection IW-2
C
<- Baseline Data ->
u° 1,000
500
0
(n O N M RZT Ln 1.0 N.
O O O O O O O O O
N N N N N N N N N

Monitoring Well MW-12
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
8,000
7,000 Perchloroethene
Trichloroethene
cis-1,2-Dichloroethene
6,000 -1FVinyl Chloride
A Injection RW-1, RW-3, RW-5, & RW-7
J
5,000 AInjection RW-1, RW-3, & RW-5
0 Injection IW-1& IW-3
C
0 ♦ Injection RW-1, RW-3, RW-5, & RW-7
4,000 A Injection IW-2
C
c 3,000
U
2,000
<-- Baseline Data -->
1,000
0
01 O r-I N M Ln W N.
O O O O O O O O O
N N N N N N N N N

Monitroing Well MW-13
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
2,000
-W-Perch loroeth e ne
Trichloroethene
1,800 cis-1,2-Dichloroethene
—N—Vinyl Chloride
♦ Injection RW-1, RW-3, RW-5, & RW-7
1,600 A Injection IW-2
0 Injection IW-1 & IW-3
1,400 0 Injection RW-1, RW-3, RW-5, & RW-7
J
0 Injection RW-1, RW-3, & RW-5
1,200
c
0
1,000
c
800
c
0
U
600
400 <--- Baseline Data --->
200
0
0) O r-I N M Ln l0 N.
O O O O O O O O O
N N N N N N N N N

Monitroing Well MW-14
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
2,000
1,800 Perchloroethene
Trichloroethene
1,600 cis-1,2-Dichloroethene
--FVinyl Chloride
1,400 0 Injection RW-1, RW-3, RW-5, & RW-7
0 Injection RW-1, RW-3, & RW-5
1,200 - 0 Injection IW-1& IW-3
♦ Injection RW-1, RW-3, RW-5, & RW-7
O
1,000 <- Baseline Data -> 0 Injection IW-2
c
800
c
O
U
600
400
200
0
01 O r-I N M R* Ln l0 n
O O O O O O O O O
N N N N N N N N N

Monitroing Well MW-24
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
800
Perchloroethene
Trichloroethene
700
cis-1,2-Dichloroethene
— —Vinyl Chloride
C00 ♦ Injection RW-1, RW-3, RW-5, & RW-7
0 Injection IW-2
dA 500 � Injection IW-1 & IW-3
0 Injection RW-1, RW-3, RW-5, & RW-7
0 Injection RW-1, RW-3, & RW-5
O
400
c
c 300
O
V �
200 <- Baseline Data ->
100
0
0) O r-I N M Ln l0 N.
O O O O O O O O O
N N N N N N N N N

Monitroing Well MW-44
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
7,000
f Perchloroethene
6,000 Trichloroethene
cis-1,2-Dichloroethene
—W-Vinyl Chloride
5,000 A Injection RW-1, RW-3, RW-5, & RW-7
A Injection RW-1, RW-3, & RW-5
dA 0 Injection IW-1& IW-3
C 4,000 ♦ Injection RW-1, RW-3, RW-5, & RW-7
O
.+ A Injection IW-2
co
i
3,000
U
C
O
U
2,000
1,000
Baseline Data --->
0
M O N M RT Ln
O O O O O O O O O
N N N N N N N N N

Injection Well IW-2
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
300
Perchloroethene
250 Trichloroethene
cis-1,2-Dichloroethene
— —Vinyl Chloride
0 Injection RW-1, RW-3, RW-5, & RW-7
200 0 Injection RW-1, RW-3, & RW-5
W
Injection IW-1 & IW-3
♦ Injection RW-1, RW-3, RW-5, & RW-7
O
150 0 Injection IW-2
U
00 100 Base%he
Oats
50
0
C1 O N M RT Ln l0 N.
O O O O O O O O O
N N N N N N N N N

Recovery/Injection Well RW-1
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
25,000
Perchloroethene
Trichloroethene
20,000 cis-1,2-Dichloroethene
*-Vinyl Chloride
♦ Injection RW-1, RW-3, RW-5, & RW-7
A Injection IW-2
215,000 AM 0 Injection IW-1& IW-3
r- 0 Injection RW-1, RW-3, RW-5, & RW-7
0 Injection RW-1, RW-3, & RW-5
m
i
°;10,000
0
V i
5,000 <-- Baseline Data -->
0
01 O r-I N M Ln l0 n
O O O O O O O O O
N N N N N N N N N

Recovery/Injection Well RW-3
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
14,000
Perchloroethene
Trichloroethene
12,000
cis-1,2-Dichloroethene
—1FVinyl Chloride
10,000 Ilk 0 Injection RW-1, RW-3, RW-5, & RW-7
J A Injection RW-1, RW-3, & RW-5
ap ♦ Injection RW-1, RW-3, RW-5, & RW-7
8,000 0 Injection IW-2
0 Injection IW-1& IW-3
m
i
6,000
U
V
4,000
<-- Baseline Data -->
2,000
0
01 O r-I N M RT Ln l0 n
O O O O O O O O O
N N N N N N N N N

Recovery/Injection Well RW-5
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
5,000
4,500 Perchloroethene
Trichloroethene
4,000 cis-1,2-Dichloroethene
—1FVinyl Chloride
3,500 <-- Baseline Data --> A Injection RW-1, RW-3, RW-5, & RW-7
0 Injection RW-1, RW-3, & RW-5
3,000 0 Injection IW-1 & IW-3
♦ Injection RW-1, RW-3, RW-5,& RW-7
O
a 2,500 Injection IW-2
i
C
2,000
c
O
V
1,500
1,000
500
0
01 O ri N M Ln lC n
O r-I ri r-1 r-I r-I r-1 r-I ri
N N N N N N N N N

Recovery/Injection Well RW-6
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
2,500
Perchloroethene
Trichloroethene
2,000 cis-1,2-Dichloroethene
\IRS A—HFVinyl Chloride
Injection RW-1, RW-3, RW-5, & RW-7
A Injection RW-1, RW-3, & RW-5
1,500 ♦ Injection RW-1, RW-3, RW-5, & RW-7
0 Injection IW-2
O
0 Injection IW-1& IW-3
co
i
C
IN 1.000
c
O
U
<-- Baseline Data -->
500
9 =-7--�
0
01 O r-I N M RiT Ln W N.
O O O O O O O O O
N N N N N N N N N

Recovery/Injection Well RW-7
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
3,500
Perchloroethene
3,000 Trichloroethene
cis-1,2-Dichloroethene
— —Vinyl Chloride
2,500 0 Injection RW-1, RW-3, RW-5, & RW-7
0 Injection RW-1, RW-3, & RW-5
dA ♦ Injection RW-1, RW-3, RW-5, & RW-7
2,000 A Injection IW-2
O
, Injection IW-1 & IW-3
co
i
1,500
U
C
O
U
1,000
<--- Baseline Data --->
500
0
0) O r-I N M Ln l0 N.
O O O O O O O O O
N N N N N N N N N