NCS000551_Permit Application_20110531

Please print or type in the unshaded areas only.
Az-,5v, ')D: �cv�,e
LS C) C) C) 5 3 Form Approved. OMB No. 2040-0086.
FORM
U.S. ENVIRONMENTAL PROTECTION AGENCY
1. EPA I.D. NUMBER
sINCDO47372503
TIA C
d% ZoEPA GENERAL INFORMATION
F
Consolidated Permits Program
D
GENERAL
(Read the "General Instructions - bqfoi-e starling')
2 13 14 15
LABEL ITEMS
GENERAL INSTRUCTIONS
If a preprinted label has been provided, affix it in the
designated space. Review the information carefully; if any of it
is incorrect, cross through it and enter the correct data in the
1. EPA I.D. NUMBER
appropriate fill-in area below. Also, if any of the preprinted data
is absent (the area to the left of the label space lists the
Ill. FACILITY NAME
PLEASE PLACE LABEL IN THIS
SPACE
information that should appear), please provide it in the proper
fill-in area(s) below. If the label is complete and correct, you
need not complete Items 1, Ill, V, and VI (except VI-8 which
V. FACILITY MAILING
ADDRESS
must be completed regardless). Complete all items if no label
has been provided. Refer to the instructions for detailed item
descriptions and for the legal authorizations under which this
VI. FACILITY LOCATION
data is collected.
IL POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer "yes" to any questions, you must
submit this form and the supplemental form listed in the parenthesis following the question. Mark "X" in the box in the third column if the supplemental form is attached. If
you answer "no" to each question, you need not submit any of these forms. You may answer "no" if your activity is excluded from permit requirements; see Section C of the
instructions. See also, Section D of the instructions for definitions of bold-faced terms.
Mark
W
Mark 'X"
YES
NO
FORM
ATTACHED
YES
NO
FORM
ATTACHED
SPECIFIC QUESTIONS
SPECIFIC QUESTIONS
A. Is this facility a publicly owned treatment works which
B. Does or will this facility (either existing or proposed)
results in a discharge to waters of the U.S.? (FORM 2A)
X
include a concentrated animal feeding operation or
X
aquatic animal production facility which results in a
16
17
18
19
20
21
discharge to waters of the U.S.? (FORM 2B)
C. Is this a facility which currently results in discharges to
X
X
D. Is this a proposed facility (other than those described in A
X
waters of the U.S. other than those described in A or B
or B above) which will result in a discharge to waters of
above? (FORM 2C)
22
23
24
the U.S.? (FORM 2D)
25
26
27
E. Does or will this facility treat, store, or dispose of
F. Do you or will you inject at this facility industrial or
hazardous wastes? (FORM 3)
X
municipal effluent below the lowermost stratum
X
containing, within one quarter mile of the well bore,
28
29
30
underground sources of drinking water? (FORM 4)
31
32
33
G. Do you or will you inject at this facility any produced water
H. Do you or will you inject at this facility fluids for special
or other fluids which are brought to the surface in
processes such as mining of sulfur by the Frasch process,
connection with conventional oil or natural gas production,
X
solution mining of minerals, in situ combustion of fossil
X
inject fluids used for enhanced recovery of oil or natural
fuel, or recovery of geothermal energy? (FORM 4)
gas, or inject fluids for storage of liquid hydrocarbons?
(FORM 4)
34
35
36
37
38
39
L Is this facility a proposed stationary source which is one
J. Is this facility a proposed stationary source which is
of the 28 industrial categories listed in the instructions and
X
NOT one of the 28 industrial categories listed in the
X
which will potentially emit 100 tons per year of any air
instructions and which will potentially emit 250 tons per
pollutant regulated under the Clean Air Act and may affect
year of any air pollutant regulated under the Clean Air Act
0
4,
42
43
44
45
or be located in an attainment area? (FORM 5)
and may affect or be located in an attainment area?
(FORM 5)
111. NAME OF FACILITY
SKIP I JI I I I I I I I I I I I I I I F I
BRENN'TAG SOUTHEAST, INC.
I I I I I I I I I I I I I I I I I I I
30
69
IV, FACILITY CONTACT
A. NAME & TITLE (lost, first, & title)
B. PHONE (area code & no.)
c
I I I I I I I I I I I I I I I I I I I I I I I I I I I I I
BIEHL, BRUCE—DIRECTOR OF ENGINEERING&REGULATORY AFFAIRS
I I I I I I I 1 1
[phone]
,2
16
45
46 48T49 51TI2- 55
V. FACILTY MAILING ADDRESS
A. STREET OR P.O. BOX
c 31 2000 EAST PETTIGREW STREET
16
45
B. CITY OR TOWN
C. STATE D. ZIP CODE
DURHAM
NC
27703
15
16
40
41 42 47 51
VI. FACILITY LOCATION
A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
c 151 2000 EAST PETTIGREW STREET
16
45
B. COUNTY NAME
DURHAM
46
70
C. CITY OR TOWN
D. STATE
E. ZIP CODE
F. COUNTY CODE (iftnown)
l�isc16
DURHAM
I
1
NC
I I I I
27703
40
41 42
47 51
52
EPA Form 3510-1 (8-90)
CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
1
VII. SIC CODES 4-di it, in order ofpriority)
A. FIRST B. SECOND
516 9
(specify) 7
(specify)
15 116
191
CHEMICAL PACKAGING AND DISTRIBUTION
15
116 19
NA
C. THIRD D. FOURTH
c
(specify) c
(specify)
15
16 19
NA �
15
16 19
NA
VIII. OPERATOR INFORMATION
A. NAME
B.Is the name listed in Item
also the owner?
1VIII-A
8
BRENNTAG SOUTHEAST, INC.
EI YES ❑ NO
15
16
55 66
C. STATUS OF OPERATOR (Enter the appropriate letter into the anslver box: if "Other, "specify.) D.
PHONE (area code & no.)
F =FEDERAL M = PUBLIC (otherthan federal or state)
S=STATE
P
(specify)
CHEMICAL DISTRIBUTION A
[phone]
O=OTHER (specify)
P = PRIVATE
15
%
6 18 119 21 22 26
E. STREET OR P.O. BOX
2000 EAST PETTIGREW STREET
26 55
F. CITY OR TOWN
G. STATE
I H. ZIP CODE
IX. INDIAN LAND
Is the facility located on Indian lands?
Ic
S
DURHAM
NC
27703
J
❑ YES 17 NO
52
18 40
�1
4] - 51
X. EXISTING ENVIRONMENTAL PERMITS
A. NPDES (Dischar es to Sin ace Water)
D. PSD (Air Emissions roT2r osedSources)
c
r
c
I r
g
N
NA
g
P
�18
NA
15
i6
1]
18 39
15
18
1]
30
B. U I C (Under oundlnjectlono Fluids)
E. OTHER (s eci )
C
I T
I I
I I I I I I I I I I
NA
C
T
(specify)
9jul
9
15
i6
it
18 30
15
1fi
1] 18
39
C. RCRA (Hazardous Wastes)
E. OTHER s eci )
C
T
NA
C T I I T I I I (Spec)
9
R
9
15 i6 17 18 38
XI. MAP
15 1 16 1 17 18 30
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the
location of each of its existing and proposed intake and discharge structures, each of its hazardous waste treatment, storage, or disposal facilities, and each well where it
injects fluids underground. Include all springs, rivers, and other surface water bodies in the map area. See instructions for precise requirements.
XII. NATURE OF BUSINESS (provide a brief description)
BRENNTAG SOUTHEAST, INC. IS A CHEMICAL DISTRIBUTOR WHICH HANDLES SEVERAL HUNDERED DIFFERENT CHEMICAL PRODUCTS.
THE CHEMICAL PRODUCTS RECEIVED IN BULI: QUANTITES ARE REPACRAGED INTO SMALLER CONTAINERS FOR SALE.
All. CERTIFICATION (see instructions)
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my
inquiry of those persons immediately responsible for obtaining the information contained in the application, 1 believe that the information is true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment.
A. NAME & OFFICIAL TITLE (type orprint)
BRUCE BIEHL
B. SIGNATURE
C. DATE IGNE
DIRECTOR OF ENGINEERING AND REGULATORY
l%
AFFAIRS
�%
COMMENTS FOR OFFICIAL USE ONLY
C
15
16 55
EPA Form 3510-1 (8-90)

EPA ID Number (copy from Item 1 of Form 1) Form Approved. OMB No. 2040-0086
Please print or type in the unshaded areas only. NCD047372503 Approval expires 5-31-92
FORM
2F
NPDES
U.S. Environmental Protection Agency
SWEPA pp Washington, DC
Application for Permit to Discharge Storm Water
Discharges Associated with Industrial Activity
Paperwork Reduction Act Notice
Public reporting burden for this application is estimated to average 28.6 hours per application, including time for reviewing instructions, searching existing data sources,
gathering and maintaining the data needed, and completing and reviewing the collection of information. Send comments regarding the burden estimate, any other aspect
of this collection of information, or suggestions for improving this form, including suggestions which may increase or reduce this burden to: Chief, Information Policy
Branch, PM-223, U.S. Environmental Protection Agency, 1200 Pennsylvania Avenue, NW, Washington, DC 20460, or Director, Office of Information and Regulatory
Affairs, Office of Management and Budget, Washington, DC 20503.
I. Outfall Location
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. Outfall Number
(list)
B. Latitude
C. Longitude
D. Receiving Water
(name)
1
35
58
45
78
53
00
Unnamed Tributary to Third Fork Creek
2
35
58
45
78
53
00
Unnamed Tributary to Third Fork Creek
3
35
58
45
78
53
n0
Unnamed Tributary to Third Fork Creek
II. Improvements
A. Are you now required by any Federal, State, or local authority to meet any implementation schedule for the construction, upgrading or operation of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited
to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
1. Identification of Conditions,
Agreements, Etc.
2. Affected Outfalis
3. Brief Description of Project
4. Final
Compliance Date
number
source of discharge
a. req.
b. proj.
NOT APPLICABLE
B: You may attach additional sheets describing any additional water pollution (or other environmental projects which may affect your discharges) you now have under
way or which you plan. Indicate whether each program is now under way or planned, and indicate your actual or planned schedules for construction.
III. Site Drainage Map
Attach a site map showing topography (or indicating the outline of drainage areas served by the outfalls(s) covered in the application if a topographic map is unavailable)
depicting the facility including: each of its intake and discharge structures; the drainage area of each storm water outfall; paved areas and buildings within the drainage
area of each storm water outfall, each known past or present areas used for outdoor storage of disposal of significant materials, each existing structural control measure
to reduce pollutants in storm water runoff, materials loading and access areas, areas where pesticides, herbicides, soil conditioners and fertilizers are applied; each of
its hazardous waste treatment, storage or disposal units (including each area not required to have a RCRA permit which is used for accumulating hazardous waste
under 40 CFR 262.34); each well where fluids from the facility are injected underground; springs, and other surface water bodies which received storm water discharges
from the facility.
EPA Form 3510-2F (1-92) Page 1 of 3 Continue on Page 2

1
rI
Continued from the Front
IV. Narrative Description of Pollutant Sources
A. For each outfall, provide an estimate of the area (include units) of imperious surfaces (including paved areas and building roofs) drained to the outfall, and an estimate of the total surface area
drained by the outfall.
Outfall
Area of Impervious Surface
Total Area Drained
Outfall
Area of Impervious Surface
Total Area Drained
Number
(provide units)
(provide units)
Number
(provide units)
(provide units)
7-777,777
square feet (.sq ft)
217,165 sq ft
4774sq ft
49,958 sq ft
2
150,082 sq ft
142,577 sq ft
B. Provide a narrative description of significant materials that are currently or in the past three years have been treated, stored or disposed in a manner to allow exposure
to storm water; method of treatment, storage, or disposal; past and present materials management practices employed to minimize contact by these materials with
storm water runoff; materials loading and access areas, and the location, manner, and frequency in which pesticides, herbicides, soil conditioners, and fertilizers are
applied.
See Attached Sheet
C. For each outfall, provide the location and a description of existing structural and nonstructural control measures to reduce pollutants in storm water runoff; and a
description of the treatment the storm water receives, including the schedule and type of maintenance for control and treatment measures and the ultimate disposal
of any solid or fluid wastes other than by discharge.
Outfall
List Codes from
Number
Treatment
Table 2F-1
1 Containment Basins (4) with a valve plus employee training and visual inspections. NA
2 Visual inspections only. NA
3 Visual inspections only. NA
V. Nonstormwater Discharges
A. I certify under penalty of law hat the outfall(s) covered by this application have been tested or evaluated for the presence of nonstormwater discharges, and that all
nonstormwater discharged from these outfall(s) are identified in either an accompanying Form 2C or From 2E application for the outfall.
Name and Official Title (type or print)
Signature
Date Sig d
BRUCE BIEHL
DIRECTOR OF ENGINEERING AND
REGULATORY AFFAIRS
r�
t
B. Provide a description of the method used, the date of any testing, and the onsite drainage points that were directly observed during a test.
A visual inspection of the stormwater systems is conducted on a weekly basis. All three outfalls in addition to the catch
basins for the various systems are visually inspected.
VI. Significant Leaks or Spills
Provide existing information regarding the history of significant leaks or spills of toxic or hazardous pollutants at the facility in the last three years, including the
approximate date and location of the spill or leak, and the type and amount of material released.
No significant leaks or spills are known to have occurred in the past three years.
EPA Form 3510-21' (1-92) Page 2 of 3 Continue on Page 3

1
1
EPA250 umber (copy from 1 ofForm 1)
Continued from Page 2 INCDO4737
VII. Discharge Information
A, B, C, & D: See instructions before proceeding. Complete one set of tables for each outfall. Annotate the outfall number in the space provided.
Table VII-A, VII-B, VII-C are included on separate sheets numbers VII-1 and VII-2.
E. Potential discharges not covered by analysis - is any toxic pollutant listed in table 2F-2, 2F-3, or 2F-4, a substance or a component of a substance which you
currently use or manufacture as an intermediate or final product or byproduct?
✓❑ Yes (list all such pollutants below) ❑ No (go to Section 1X)
See Attached Sheet
Vill. Biological Toxicity Testing Data
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
❑ Yes (list all such pollutants below) ✓❑ No (go to Section IX)
IX. Contract Analysis Information
Were any of the analyses reported in Item VII performed by a contract laboratory or consulting firm?
❑✓ Yes (list the name, address, and telephone number of, and pollutants
❑ No (go to Section X)
analyzed by, each such laboratory or firm below)
A. Name
B. Address
C. Area Code & Phone No.
D. Pollutants Analyzed
Test America
5102 LaRoche Avenue
912-354-7858
Ammonia, PP Metals plus Hg,
Savannah, Georgia 31404
pH,. conductivity, Oil and
Grease, BNA Priority
Pollutants, Pureable
Organics, Total Suspended
Solids, Total BOD, Total
COD/TKN, Dissolved COD,
Total Organic Carbon,
Dissolved Organic Carbon
X. Certification
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
A. Name & Official Title (Type Or Print)
B. Area Code and Phone No.
BRUCE BIEHL DIRECTOR OF ENGINEERING AND REGULATORY AFFAIRS
9 1C1
1�
C. Signature
D. Date Signed
J
EPA Form 3510-21' (1-92) Page 3 of 3

1
EPA ID Number (copy from Item 1 of Form 1) Form Approved. OMB No. 2040-0086
NCD047372503 I Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F) OUTFALL #1
Part A — You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
< 5.0 mg/L
NIA
1
Runoff from onsite production area
Biological Oxygen
Demand (BODS)
4.3 mg/L
Not Applicable
1
Same
Chemical Oxygen
Demand (COD)
26 mg/L
Not Applicable
1
Same
Total Suspended
Solids (TSS)
9.5 mg/L
Not Applicable
1
Same
Total Nitrogen
3.4 mg/L
Not Applicable
1
Same
Total Phosphorus
Not Applicable
Not Applicable
1
Same
pH
Minimum 9.2s
Maximum
Minimum
Maximum
1
Same
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
NOT APPLICABLE
EPA Form 3510-2F (1-92)
Page VII-1
Continue on Reverse

I
Continued from the Front
Part C - List each pollutant shown in Table 2F-2, 2F-3, and 2F-4 that you know or have reason to believe is present. See the instructions for additional details and
requirements. Complete one table for each outfall.
Maximum Values Average Values
(include units) (include units) Number
Pollutant Grab Sample Grab Sample of
and Taken During Taken During Storm
CAS Number First 20 Flow -Weighted First 20 Flow -Weighted Events
(if available) Minutes Composite Minutes Composite Sampled Sources of Pollutants
See Apoenxic 1 for attachpi analvtical repo t from TestA erica for monitori a event cond cted on 3/1/2011
Part D - Provide data for the storm event(s) which resulted in the maximum values for the flow weighted composite sample
4.
5.
1.
2.
3.
Number of hours between
Maximum flow rate during
6.
Date of
Duration
Total rainfall
beginning of storm measured
rain event
Total flow from
Storm
of Storm Event
during storm event
and end of previous
(gallons/minute or
rain event
Event
(in minutes)
(in inches)
measurable rain event
specify units)
(gallons or specify units)
2/28/2011
180
0.79
560 hours
Not Applicable -
101,592 gallons
Water is retained in
retention basin and
discharged in batch
volumes.
1 7. Provide a description of the method of flow measurement or estimate.
(Rainfall event of 0.79 inches on 2/28/2011 over 206,306 square feet of impervious drainage area.
EPA Form 3510-21' (1-92)
Page VII-2

1
EPA ID Number (copy from Item i of Form 1) Form Approved. OMB No. 2040-0086
gCID047372503 I Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F) OUTFALL #2
Part A — You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
NOT APPLICABLE
N/A
Biological Oxygen
Demand (BOD5)
NOT APPLICABLE
Not Applicable
Chemical Oxygen
Demand (COD)
NOT APPLICABLE
Not Applicable
Total Suspended
Solids (TSS)
NOT APPLICABLE
Not Applicable
Total Nitrogen
NOT APPLICABLE
Not Applicable
Total Phosphorus
NOT APPLICABLE
Not Applicable
pH
Minimum
Maximum
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Not Applicable
EPA Form 3510-2F (1-92)
Page VII-1
Continue on Reverse

Continued from the Front
Part C - List each pollutant shown in Table 2F-2, 2F-3, and 2F-4 that you know or have reason to believe is present. See the instructions for additional details and
requirements. Complete one table for each outfall.
Pollutant
and
CAS Number
(ifavailable)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Not Applic-ble
Part D — Provide data for the storm event(s) which resulted in the maximum values for the flow weighted composite sample.
1.
Date of
Storm
Event
2.
Duration
of Storm Event
(in minutes)
3.
Total rainfall
during storm event
(in inches)
4.
Number of hours between
beginning of storm measured
and end of previous
measurable rain event
5.
Maximum flow rate during
rain event
(gallonslminute or
specify units)
6.
Total flow from
rain event
(gallons or specify units)
NA
NA
NA
NA
NA
NA
7. Provide a description of the method of flow measurement or estimate.
NA
EPA Form 3510-21' (1-92)
Page VII-2

1
EPA ID Number (copy from Item 1 of Form 1) Form Approved. OMB No. 2040-0086
QCD047372503 I Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F) OUTFALL #3
Part A — You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
NOT APPLICABLE
N/A
Biological Oxygen
Demand (BOD5)
NOT APPLICABLE
Not Applicable
Chemical Oxygen
Demand (COD)
NOT APPLICABLE
Not Applicable
Total Suspended
Solids (TSS)
NOT APPLICABLE
Not Applicable
Total Nitrogen
NOT APPLICABLE
Not Applicable
Total Phosphorus
NOT APPLICABLE
Not Applicable
pH
Minimum
Maximum
I Minimum
Maximum
Part B— List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Not Applicable
EPA Form 3510-2F (1-92)
Page VII-1
Continue on Reverse

Continued from the Front
Part C - List each pollutant shown in Table 2F-2, 2F-3, and 2F-4 that you know or have reason to believe is present. See the instructions for additional details and
requirements. Complete one table for each outfall.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Not ApplicEble
Part D — Provide data for the storm event(s) which resulted in the maximum values for the flow weighted composite sample.
1.
Date of
Storm
Event
2.
Duration
of Storm Event
(in minutes)
3.
Total rainfall
during storm event
(in inches)
4.
Number of hours between
beginning of storm measured
and end of previous
measurable rain event
5.
Maximum flow rate during
rain event
(gallons/minute or
specify units)
6.
Total flow from
rain event
(gallons or specify units)
NA
NA
NA
NA
NA
NA
7. Provide a description of the method of flow measurement or estimate.
NA
EPA Form 3510-2F (1-92) Page VII-2

Attachment to Item IV.B.
Brenntag, Inc. (Brenntag) is a chemical distributor, which handles several hundred different
chemical products. Brenntag takes great care in handling of materials; however, small amount of
these products may have been inadvertently and accidentally released to the ground through
drippage from repackaging, unloading, loading and transferring operations located throughout the
facility.
In order to prevent this situation, Brenntag has installed several secondary and tertiary containment
areas including its storage tanks and drum storage areas which are required to be diked under
OSHA. Tertiary containment is comprised of valved containment areas at the outflow of storm
drains from these areas.
Waste materials from alkali and acid repackaging operations are sent to an elementary
neutralization system. They are neutralized, stored and sent out for disposal as non -hazardous
waste. We currently have installed a waste water evaporator unit and are in the process of
refining it to allow for efficient evaporation rates.
All waste generated from the solvent side are either sold to customers who can use it as is or sent
out for proper hazardous and non -hazardous waste disposal.
Oil from our oil repackaging operation is sent out for disposal through an oil disposal
service.
As a hazardous waste generator, we are required to follow the North Carolina Hazardous Waste
Rules for Generators. In addition, Brenntag does broker some hazardous waste for its customers.
These wastes are typically streams from the use of our virgin materials. The waste can be held
at Brenntag for 10 days as a transporter and are then shipped out to qualified disposal facilities.
Brenntag does not handle pesticides of any type except for one, Sodium Hypochlorite
Bleach.
No materials have been treated, or disposed of in a manner that would expose any of Brenntag's
raw material, hazardous and non -hazardous waste products to the storm system.

M.
ry-..tIN
�
7
Ri
i I �,L� "� ►fib IN;r :� Ali AIM'
COS
1. Stormwater discharges to the unnamed tributary to Third Fork Creek
class WS-IV waters, in the Cape Fear River Basin.
801
00 orate Center Drive,
-
Raleigh, NC ARCADIS 1,-8.4-1282
..
G&M of North Carolina, Inc.
DRAWING®
5/18/11
��� -•�•
FORMERCLIENT: SITE LOCATION MAP -im
BRENNTAG SOUTHEAST, INC.
•
• . . • . PROJECT

TestAmerica
itIE LEADER IN ENVIRONNIEN"TAL TESTING
Job Number: 680-66071-1
Job Description: Brenntag/Durham Stormwater
For:
ARCADIS U.S., Inc.
801 Corporate Center Drive
Suite 300
Raleigh, NC 27607-5073
Attention: Mr. Jim Shilliday
TI
Kathryn Smith
Project Manager I
[e-mail]
03/16/2011
Approved for release.
Kathryn Smith
Project Manager I
3/1612011 3:28 PM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www.testamericainc.com
,N o09Oa
ye
U
Page 1 of 36
_

Job Narrative
680-66071-1
Comments
No additional comments.
Receipt
All samples were received in good condition within temperature requirements.
GC/MS VOA
No analytical or quality issues were noted.
GC/MS Semi VOA
No analytical or quality issues were noted.
Metals
No analytical or quality issues were noted.
General Chemistry
Method(s) 150.1, SM 4500 H+ B: This analysis is normally performed in the field and has a method -defined holding time of 15 minutes.
The following sample(s) has been qualified with the "HF" flag to indicate analysis was performed in the laboratory outside the 15 minute
timeframe: SW (3-1-11) (680-66071-1)
No other analytical or quality issues were noted.
Page 2 of 36
)
w

METHOD SUMMARY
Client: ARCADIS U.S., Inc. Job Number: 680-66071-1
Description
Lab Location
Method
Preparation Method
Matrix Water
Volatile Organic Compounds (GC/MS)
TAL SAV
40CFR136A 624
Semivolatile Organic Compounds (GC/MS)
TAL SAV
40CFR136A 625
Liquid -Liquid Extraction
TAL SAV
40CFR136A 625
Metals (ICP/MS)
TAL SAV
EPA 200.8
Preparation, Total Recoverable Metals
TAL SAV
EPA 200.8
Mercury (CVAA)
TAL SAV
EPA 245.1
Preparation, Mercury
TAL SAV
EPA 245.1
Conductivity, Specific Conductance
TAIL SAV
MCAWW 120.1
pH (Electrometric)
TAL SAV
MCAWW 150.1
HEM and SGT-HEM
TAL SAV
1664A 1664A
HEM and SGT-HEM (Aqueous)
TAL SAV
1664A 1664A
Nitrogen, Ammonia
TAL SAV
MCAWW 350.1
Nitrogen, Total Kjeldahl
TAL SAV
MCAWW 351.2
Nitrogen, Total Kjeldahl
TAL SAV
MCAWW 351.2
Nitrogen, Nitrate -Nitrite
TAL SAV
MCAWW 353.2
Nitrogen, Nitrite
TAL SAV
MCAWW 353.2
BOD, 5-Day
TAL SAV
MCAWW 405.1
BOD, 5-Day
TAL SAV
MCAWW 405.1
Sample Filtration
IAL SAV
FILTRATION
COD
TAL SAV
MCAWW 410.4
COD
TAL SAV
MCAWW 410.4
Sample Filtration
TAL SAV
FILTRATION
DOC
TAL SAV
MCAWW 415.1
Sample Filtration, Field
FIELD FLTRD
TOC
TAL SAV
MCAWW 415.1
Solids, Total Suspended (TSS)
TAIL SAV
SM SM 2540D
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
1664A = EPA-821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A,
October 26, 1984 and subsequent revisions.
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater',
TestAmerica Savannah Page 3 of 36

METHOD / ANALYST SUMMARY
Client: ARCADIS U.S., Inc. Job Number: 680-66071-1
Method
Analyst
Analyst ID
40CFR136A 624
Cowart, Judson
WJC
40CFR136A 625
Hao, Lili
LH
EPA 200.8
Boyuk, Brian
BB
EPA 245.1
Vasquez,Juana
JV
MCAWW 120.1
Robinson, Tiffany
TR
MCAWW 150.1
Jackson, Michelle S
MSJ
1664A 1664A
Samuel, Sarita
SS
MCAWW 350.1
Ross, Jon
JR
MCAWW 351.2
Ross, Jon
JR
MCAWW 353.2
Ross, Jon
JR
MCAWW 405.1
Jackson, Michelle S
MSJ
MCAWW 410.4
McDonald, Debbie
DAM
MCAWW 415.1
Blackshear, Kim
KB
SM SM 2540D
Robinson, Tiffany
TR
TestAmerica Savannah
Page 4 of 36

SAMPLE SUMMARY
Client: ARCADIS U.S., Inc. Job Number: 680-66071-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-66071-1 SW (3-1-11) Water 03/01/2011 0900 03/02/2011 0927
TestAmerica Savannah
Page 5 of 36

Client: ARCADIS U.S.. Inc.
Client Sample ID: SW (3-1-11)
Lab Sample ID: 680-66071-1
Client Matrix: Water
Analytical Data
Job Number: 680-66071-1
Date Sampled: 03/01/2011 0900
Date Received: 03/02/2011 0927
624 Volatile Organic Compounds (GC/MS)
Method:
624
Analysis Batch: 680-196105 Instrument ID:
MSB
Preparation:
N/A
Lab File ID:
b157.d
Dilution:
1.0
Initial Weight/Volume:
5 mL
Date Analyzed:
03/04/2011 2330
Final Weight/Volume:
5 mL
Date Prepared:
Analyte
Result (ug/L)
Qualifier
RL
Acetone
190
25
Benzene
1.0
U
1.0
Bromodichloromethane
1.0
U
1.0
Bromoform
1.0
U
1.0
Bromomethane
1.0
U
1.0
Carbon tetrachloride
1.0
U
1.0
Chlorobenzene
1.0
U
1.0
Chloroethane
1.0
U
1.0
Chloroform
1_1
1.0
Chloromethane
1.0
U
1.0
Dibromochloromethane
1.0
U
1.0
1,1-Dichloroethane
2.4
1.0
1,2-Dichloroethane
1.0
U
1.0
1,1-Dichloroethene
1.0
U
1.0
1,2-Dichloropropane
1.0
U
1.0
1,3-Dichloropropene, Total
2.0
U
2.0
Ethylbenzene
1.0
U
1.0
Methylene Chloride
5.0
U
5.0
1,1,2,2-Tetr2chloroethene
1.0
U
1.0
Tetrachloroethene
1.0
U
1.0
Toluene
2.5
1.0
trans-1,2-Dichloroethene
1.0
U
1.0
1,1,1-Trichloroethane
3.8
1.0
1,1,2-Trichloroethane
1.0
U
1.0
Trichloroethene
1.0
U
1.0
Vinyl chloride
1.0
U
1.0
Surrogate
%Rec
Qualifier
Acceptance Limits
4-Bromofluorobenzene
98
71 - 121
Dibromofluoromethane
105
77 - 129
Toluene-d8 (Sun•)
93
79 - 119
TestAmerica Savannah Page 6 of 36

Analytical Data
Client: ARCADIS U.S., Inc. Job Number: 680-66071-1
Client Sample ID: SW (3-1-11)
Lab Sample ID: 680-66071-1 Date Sampled: 03/01/2011 0900
Client Matrix: Water Date Received: 03/02/2011 0927
625 Semivolatile Organic Compounds (GC/MS)
Method: 625
Analysis Batch: 680-196311
Instrument ID:
MST
Preparation: 625
Prep Batch: 680-195844
Lab File ID:
t2572.d
Dilution: 1.0
Initial Weight/Volume:
963.3 mL
Date Analyzed: 03/08/2011 0810
Final Weight/Volume:
1 mL
Date Prepared: 03/03/2011 1032
Injection Volume:
1 uL
Analyte
Result (ug/L)
Qualifier
RL
_.... ..... ,.._,,,,.
2,4,6 Trichlorophenol
_
10
U
.... , ,,._.,...
10
2,4-Dichlorophenol
10
U
10
2,4-Dimethylphenol
10
U *
10
2,4-Dinitrophenol
52
U
52
2-Nitrophenol
10
U
10
4,6-Dinitro-2-methylphenol
52
U
52
4-Chloro-3-methylphenol
10
U
10
4-Nitrophenol
52
U
52
Pentachlorophenol
52
U
52
Phenol
10
U
10
2-Chlorophenol
10
U
10
Surrogate __.,.,__ ..
_, .._.,... ,_,
%Rec
Qualifier Acceptance Limits
.,__.....__.. _.... . ........... . ..,.,,_
2,4,6-Tribromophenol
__ .,.,._-.
63
34 132
_,...
2-Fluorophenol
44
35 - 110
Phenol-d5
41
27 - 119
TestAmerica Savannah Page 7 of 36

Analytical Data
Client: ARCADIS U.S., Inc. Job Number: 680-66071-1
Client Sample ID: SW (3-1-11)
Lab Sample ID: 680-66071-1
Client Matrix: Water
Date Sampled: 03/01/2011 0900
Date Received: 03/02/2011 0927
625 Semivolatile Organic Compounds (GC/MS)
Method: 625
Analysis Batch: 680-196470
Instrument ID:
MSG
Preparation: 625
Prep Batch: 680-195844
Lab File ID:
g5979.d
Dilution: 1.0
Initial Weight/Volume:
963.3 mL
Date Analyzed: 03/08/2011 2113
Final Weight/Volume:
1 mL
Date Prepared: 03/03/2011 1032
Injection Volume:
1 uL
Analyte
Result (ug/L)
Qualifier
RL
Tnchlorobenzene
10
U
10
1,2-Dichlorobenzene
10
U
10
1,2-Diphenylhydrazine
10
U
10
1,3-Dichlorobenzene
10
U
10
1,4-Dichlorobenzene
10
U
10
2-Chloronaphthalene
10
U
10
2,6-Dinitrotoluene
10
U
10
2,4-Dinitrotoluene
10
U
10
3,3'-Dichlorobenzidine
62
U
62
4-Bromophenyl phenyl ether
10
U
10
4-Chlorophenyl phenyl ether
10
U
10
Acenaphthene
10
U
10
Acenaphthylene
10
U
10
Anthracene
10
U
10
Benzidine
83
U
83
Benzo[a]anthracene
10
U
10
Benzo[a]pyrene
10
U
10
Benzo[b]fluoranthene
10
U
10
Benzo[g,h,i]perylene
10
U
10
Benzo[k]fluoranthene
10
U
10
Bis(2-chloroethoxy)methane
10
U
10
Bis(2-chloroethyl)ether
10
U
10
Bis(2-ethylhexyl) phthalate
10
U
10
Butyl benzyl phthalate
10
U
10
Chrysene
10
U
10
Di-n-butyl phthalate
10
U
10
Di-n-octyl phthalate
10
U
10
Dibenz(a,h)anthracene
10
U
10
Diethyl phthalate
10
U
10
Dimethyl phthalate
10
U
10
Fluoranthene
10
U
10
Fluorene
10
U
10
Hexachlorobenzene
10
U
10
Hexachlorobutadiene
10
U
10
Hexachlorocyclopentadiene
21
U
21
Hexachloroethane
10
U
10
Indeno[1,2,3-cd]pyrene
10
U
10
Isophorone
10
U
10
N-Nitrosodi-n-propylamine
10
U
10
N-Nltrosodlmethylamine
21
U
21
N-Nitrosodiphenylamine
10
U
10
Naphthalene
10
U
10
Nitrobenzene
10
U
10
Phenanthrene
10
U
10
Pyrene
10
U
10
2,4-Dimethylphenol
10
U
10
TestAmerica Savannah Page 8 of 36

Client: ARCADIS U.S., Inc.
Client Sample ID: SW (3-1-11)
Lab Sample ID: 680-66071-1
Client Matrix: Water
Analytical Data
Job Number: 680-66071-1
Date Sampled: 03/01/2011 0900
Date Received: 03/02/2011 0927
625 Semivolatile Organic Compounds (GC/MS)
Method:
625
Analysis Batch: 680-196470
Instrument ID:
MSG
Preparation:
625
Prep Batch: 680-195844
Lab File ID:
g5979.d
Dilution:
1.0
Initial Weight/Volume:
963.3 mL
Date Analyzed:
03/08/2011 2113
Final Weight/Volume:
1 mL
Date Prepared:
03/03/2011 1032
Injection Volume:
1 uL
Analyte
Result (ug/L)
Qualifier
RL
bis(chloroisopropyl) ether ...
10 ......,..
U ....
.. . ......�0
Surrogate _.__
'i-" ,_-
%Rec
Qualifier Acceptance Limits
2Fluorobiphenyl..
51
_.. _ _ 12
38 - 1
... _.: �....,..
Nitrobenzene-d5
52
44 - 119
Terphenyl-d14
40
10 - 165
TestAmerica Savannah Page 9 of 36

Client: ARCADIS U.S.. Inc.
Client Sample ID: SW (3-1-11)
Lab Sample ID: 680-66071-1
Client Matrix: Water
Method:
200.8
Preparation:
200.8
Dilution:
1.0
Date Analyzed:
03/10/2011 0042
Date Prepared:
03/04/2011 1120
Analyte
Antimony
Arsenic
Beryllium
Cadmium
Chromium.
Copper
Lead
Nickel
Selenium
Silver
Thallium
Zinc
Analytical Data
Job Number: 680-66071-1
Date Sampled: 03/01/2011 0900
Date Received: 03/02/2011 0927
200.8 Metals (ICP/MS)-Total Recoverable
Analysis Batch: 680-196661 Instrument ID: ICPMSC
Prep Batch: 680-196026 Lab File ID: 196SMPL.D
Initial Weight/Volume: 50 mL
Final Weight/Volume: 250 mL
Result (ug/L)
Qualifier
RL
5.0
U
.. .... .... _....
5.0
2.5
U
2.5
0.50
U
0.50
0.50
U
0.50
5.0
U
5.0
11
5.0
4.3
1.5
8.4
5.0
2.5
U
2.5
1.0
U
1.0
1.0
U
1.0
160
20
245.1 Mercury (CVAA)
Method:
245.1
Analysis Batch: 680-196504
Preparation:
245.1
Prep Batch: 680-196183
Dilution:
1.0
Date Analyzed:
03/08/2011 1910
Date Prepared:
03/07/2011 1240
Analyte Result (ug/L)
Qualifier
Instrument ID:
LEEMAN1
Lab File ID:
030811.chr
Initial Weight/Volume:
50 mL
Final Weight/Volume:
50 mL
0.20 U k0.20
12 n_y11L o, o i 2�tr�y� L
TestAmerica Savannah Page 10 of 36

Analytical Data
Client: ARCADIS U.S., Inc. Job Number: 680-66071-1
General Chemistry
Client Sample ID: SW (3-1-11)
Lab Sample ID: 680-66071-1
Client Matrix: Water
Date Sampled: 03/01/2011 0900
Date Received: 03/02/2011 0927
Analyte Result
Qual Units
RL
Dil
Method
HEM (Oil & Grease) 5.0
U mg/L
5.0
1.0
1664A
Analysis Batch: 680-196638
Date Analyzed: 03/10/2011 1315
Prep Batch: 680-196533
Date Prepared: 03/09/2011 1720
Ammonia 0.24
mg/L
0.050
1.0
350.1
Analysis Batch: 680-196814
Date Analyzed: 03/10/2011 1309
Nitrogen, Kjeldahl 1.5
mg/L
0.20
1.0
351.2
Analysis Batch: 680-197150
Date Analyzed: 03/14/2011 1442
Prep Batch: 680-197005
Date Prepared: 03/12/2011 1430
Nitrite as N 0.050
U mg/L
0.050
1.0
353.2
Analysis Batch: 680-196072
Date Analyzed: 03/02/2011 1655
Nitrate as N 0.44
mg/L
0.050
1.0
353.2
Analysis Batch: 680-195898
Date Analyzed: 03/02/2011 1655
Chemical Oxygen Demand 51
mg/L
20
1.0
410.4
Analysis Batch: 680-196298
Date Analyzed: 03/08/2011 0900
Chemical Oxygen 20
U mg/L
20
1.0
410.4
Demand -Dissolved Analysis Batch: 680-196301
Date Analyzed: 03/08/2011 0900
Dissolved Organic Carbon -Dissolved 11
mg/L
1.0
1.0
415.1
Analysis Batch: 680-196545
Date Analyzed: 03/08/2011 2228
Total Organic Carbon 11
mg/L
1.0
1.0
415.1
Analysis Batch: 680-196538
Date Analyzed: 03/08/2011 1852
Analyte Result
Qual Units
Dil
Method
pH 7.00
HF SU
1.0
150.1
Analysis Batch: 680-195951
Date Analyzed: 03/03/2011 1227
Analyte Result
Qual Units
RL
Dil
Method
9 ..-_ ,._ .._:.�_ .::,_..�...._........_.
Specific Conductance 5.0
U umhos/cm
5.0
_...
1.0
. ..,......., ._.
120.1
Analysis Batch: 680-195821
Date Analyzed: 03/02/2011 1855
Biochemical Oxygen Demand 25
mg/L
2.0
1.0
405.1
Analysis Batch: 680-195785
Date Analyzed: 03/02/2011 1445
Biochemical Oxygen 18
mg/L
2.0
1.0
405.1
Demand -Dissolved Analysis Batch: 680-195785
Date Analyzed: 03/02/2011 1445
Total Suspended Solids 45
mg/L
10
1.0
SM 2540D
Analysis Batch: 680-195968
Date Analyzed: 03/03/2011 1953
TestAmerica Savannah Page 11 of 36

DATA REPORTING QUALIFIERS
Client: ARCADIS U.S., Inc.
Lab Section Qualifier Description
GC/MS VOA
GC/MS Semi VOA
Metals
General Chemistry
TestAmerica Savannah
Job Number: 680-66071-1
U Indicates the analyte was analyzed for but not detected.
U Indicates the analyte was analyzed for but not detected.
LCS or LCSD exceeds the control limits
U Indicates the analyte was analyzed for but not detected.
HF Field parameter with a holding time of 15 minutes
U Indicates the analyte was analyzed for but not detected.
Page 12 of 36

Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 680-66071-1
Method Blank - Batch: 680-196105
Method: 624
Preparation: NIA
Lab Sample ID: MB 680-196105/9
Analysis Batch: 680-196105
Instrument ID: MSB
Client Matrix: Water
Prep Batch: N/A
Lab File ID: bg097.d
Dilution: 1.0
Units: ug/L
Initial Weight/Volume: 5
mL
Date Analyzed: 03/04/2011 1843
Final Weight/Volume: 5
mL
Date Prepared: N/A
Analyte
Result
Qua[
RL
Acetone
25
U.,ti
25
Benzene
1.0
U
1.0
Bromodichloromethane
1.0
U
1.0
Bromoform
1.0
U
1.0
Bromomethane
1.0
U
1.0
Carbon tetrachloride
1.0
U
1.0
Chlorobenzene
1.0
U
1.0
Chloroethane
1.0
U
1.0
Chloroform
1.0
U
1.0
Chloromethane
1.0
U
1.0
Dibromochloromethane
1.0
U
1.0
1,1-Dichloroethane
1.0
U
1.0
1,2-Dichloroethane
1.0
U
1.0
1,1-Dichloroethene
1.0
U
1.0
1,2-Dichloropropane
1.0
U
1.0
1,3-Dichloropropene, Total
2.0
U
2.0
Ethylbenzene
1.0
U
1.0
Methylene Chloride
5.0
U
5.0
1,1,2,2-Tetrachloroethane
1.0
U
1.0
Tetrachloroethene
1.0
U
1.0
Toluene
1.0
U
1.0
trans-1,2-Dichloroethene
1.0
U
1.0
1,1,1-Trichloroethane
1.0
U
1.0
1,1,2-Trichloroethane
1.0
U
1.0
Trichloroethene
1.0
U
1.0
Vinyl chloride
1.0
U
1.0
Surrogate
% Rec
Acceptance Limits
4-Bromofluorobenzene
99
71 - 121
Dibromofluoromethane
104
77 - 129
Toluene-d8 (Surr)
93
79 - 119
TestAmerica Savannah Page 13 of 36

Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 680-66071-1
Lab Control Sample/
Method: 624
Lab Control Sample Duplicate Recovery Report
- Batch: 680-196105
Preparation: N/A
LCS Lab Sample ID: LCS 680-196105/7
Analysis Batch:
680-196105
Instrument ID: MSB
Client Matrix: Water
Prep Batch: N/A
Lab File ID: bg094.d
Dilution: 1.0
Units: ug/L
Initial Weight/Volume: 5 mL
Date Analyzed: 03/04/2011 1725
Final Weight/Volume: 5 mL
Date Prepared: N/A
LCSD Lab Sample ID: LCSD 680-196105/8
Analysis Batch:
680-196105
Instrument ID: MSB
Client Matrix: Water
Prep Batch: N/A
Lab File ID: bg095.d
Dilution: 1.0
Units: ug/L
Initial Weight/Volume: 5 mL
Date Analyzed: 03/04/2011 1751
Final Weight/Volume: 5 mL
Date Prepared: N/A
% Rec.
Analyte
LCS LCSD
Limit
RPD
RPD Limit LCS Qual LCSD Qual
Acetone
116 111
20 - 183
5
50
Benzene
104 106
37-151
2
30
Bromodichloromethane
93 95
35 - 155
2
30
Bromoform
112 111
45 - 169
1
30
Bromomethane
152 144
1 - 242
5
100
Carbon tetrachloride
94 92
70 - 140
1
30
Chlorobenzene
113 111
37 - 160
1
30
Chloroethane
109 105
14 - 230
4
50
Chloroform
98 95
51 - 138
3
30
Chloromethane
116 109
1 - 273
6
50
Dibromochloromethane
97 95
53 - 149
2
30
1,1-Dichloroethane
113 108
59 - 155
5
30
1,2-Dichloroethane
98 104
49 - 155
6
30
1,1-Dichloroethene
105 100
1 -234
5
30
1,2-Dichloropropane
102 104
1 -210
2
30
1,3-Dichloropropene, Total
100 104
17 - 183
4
30
Ethylbenzene
116 114
37 - 162
1
30
Methylene Chloride
110 103
1 - 221
7
30
1,1,2,2-Tetrachloroethane
112 112
46 - 157
0
30
Tetra chloroethene
121 121
64 - 148
0
30
Toluene
106 108
47 - 150
2
30
trans-1,2-Dichloroethene
115 108
54-156
6
30
1,1,1-Trichloroethane
108 112
52-162
3
30
1,1,2-Trichloroethane
104 107
52-150
2
30
Trichloroethene
105 107
71 - 157
2
30
Vinyl chloride
89 80
1 - 251
10
50
Surrogate
LCS % Rec
I CSD %
Rec
Acceptance I imits
4-Bromofluorobenzene
105
105
71 -121
Dibromofluoromethane
105
103
77 - 129
Toluene-d8 (Surr)
98
99
79 - 119
TestAmerica Savannah Page 14 of 36

Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 680-66071-1
Method Blank - Batch: 680-195844
Method: 625
Preparation: 625
Lab Sample ID: MB 680-195844/8-A
Analysis Batch: 680-196311
Instrument ID: MST
Client Matrix: Water
Prep Batch: 680-195844
Lab File ID: t2569.d
Dilution: 1.0
Units: ug/L
Initial Weight/Volume: 1000 mL
Date Analyzed: 03/08/2011 0158
Final Weight/Volume: 1 mL
Date Prepared: 03/03/2011 1032
Injection Volume: 1 uL
Analyte
Result
Qual
RL
2,4,6-Trichlorophenol
10
U
10
2,4-Dichlorophenol
10
U
10
2,4-Dinitrophenol
50
U
50
2-Nitrophenol
10
U
10
4,6-Dinitro-2-methylphenol
50
U
50
4-Chloro-3-methylphenol
10
U
10
4-Nitrophenol
50
U
50
Pentachlorophenol
50
U
50
Phenol
10
U
10
2-Chlorophenol
10
U
10
2,4-Dimethylphenol
10
U
10
Surrogate
% Rec
Acceptance Limits
2,4,6-Tribromophenol
70
34 - 132
2-Fluorophenol
75
35 - 110
Phenol-d5
61
27 - 119
TestAmerica Savannah Page 15 of 36

Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 680-66071-1
Method Blank - Batch: 680-195844
Method: 625
Preparation: 625
Lab Sample ID: MB 680-195844/8-A
Analysis Batch: 680-196470
Instrument ID: MSG
Client Matrix: Water
Prep Batch: 680-195844
Lab File ID: g5976.d
Dilution: 1.0
Units: ug/L
Initial Weight/Volume:
1000 mL
Date Analyzed: 03/08/2011 1949
Final Weight/Volume:
1 mL
Date Prepared: 03/03/2011 1032
Injection Volume:
1 uL
Analyte
Result
Qual
RL
1,2,4-Trichlorobenzene
10
U
10
1,2-Dichlorobenzene
10
U
10
1,2-Diphenylhydrazine
10
U
10
1,3-Dichlorobenzene
10
U
10
1,4-Dichlorobe nzene
10
U
10
2-Chloronaphthalene
10
U
10
2,6-Dinitrotoluene
10
U
10
2,4-Dinitrotoluene
10
U
10
3,3'-Dichlorobenzidine
60
U
60
4-Bromophenyl phenyl ether
10
U
10
4-Chlorophenyl phenyl ether
10
U
10
Acenaphthene
10
U
10
Acenaphthylene
10
U
10
Anthracene
10
U
10
Benzidine
80
U
80
Benzo[a]anthracene
10
U
10
Benzo[a]pyrene
10
U
10
Benzo[b]fluoranthene
10
U
10
Benzo[g,h,i]perylene
10
U
10
Benzo[k]fluoranthene
10
U
10
Bis(2-chloroethoxy)methane
10
U
10
Bis(2-chloroethyl)ether
10
U
10
Bis(2-ethylhexyl) phthalate
10
U
10
Butyl benzyl phthalate
10
U
10
Chrysene
10
U
10
Di-n-butyl phthalate
10
U
10
Di-n-octyl phthalate
10
U
10
Dibenz(a,h)anthracene
10
U
10
Diethyl phthalate
10
U
10
Dimethyl phthalate
10
U
10
Fluoranthene
10
U
10
Fluorene
10
U
10
Hexachlorobenzene
10
U
10
Hexachlorobutadiene
10
U
10
Hexachlorocyclopentadiene
20
U
20
Hexachloroethane
10
U
10
Indeno[1,2,3-cdjpyrene
10
U
10
Isophorone
10
U
10
N-Nitrosodi-n-propylamine
10
U
10
N-Nitrosodimethylamine
20
U
20
N-Nitrosodiphenylamine
10
U
10
Naphthalene
10
U
10
Nitrobenzene
10
U
10
TestAmerica Savannah Page 16 of 36

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-195844
Lab Sample ID: MB 680-195844/8-A
Analysis Batch: 680-196470
Client Matrix: Water
Prep Batch: 680-195844
Dilution: 1.0
Units: ug/L
Date Analyzed: 03/08/2011 1949
Date Prepared: 03/03/2011 1032
Analyte
Result
Qual
Phenanthrene _.,.,. - �...._... ._. ..�
.w..w._...-.... w.10
U_.._
Pyrene
10
U
2,4-Dimethyl phenol
10
U
bis(chloroisopropyl) ether
10
U
Surrogate
% Rec
2-Fluorobiphenyl
77
Nitrobenzene-d5
67
Terphenyl-d14
91
Quality Control Results
Job Number: 680-66071-1
Method: 625
Preparation: 625
Instrument ID: MSG
Lab File ID: g5976.d
Initial Weight/Volume: 1000 mL
Final Weight/Volume: 1 mL
Injection Volume: 1 uL
Acceptance Limits
38 - 121
44 - 119
10-165
71
10
10
10
10
TestAmerica Savannah Page 17 of 36

Quality Control Results
I
Client: ARCADIS U.S., Inc.
Job Number: 680-66071-1
..,1
Lab Control Sample - Batch: 680-195844
Method: 625
Preparation: 625
Lab Sample ID: LCS 680-195844/9-A
Analysis Batch:
680-196470
Instrument ID: MSG
Client Matrix: Water
Prep Batch: 680-195844
Lab File ID: g5977.d
Dilution: 1.0
Units: ug/L
Initial Weight/Volume: 1000 mL
Date Analyzed: 03/08/2011 2017
Final Weight/Volume: 1 mL
Date Prepared: 03/03/2011 1032
Injection Volume: 1 uL
Analyte
Spike Amount
Result
% Rec.
Limit Qual
1,2,4-Trichlorobenzene
100
78.5
78
44 - 142
1,2-Dichlorobenzene
100
76.0
76
32 - 129
1,2-Diphenylhydrazine
100
88.7
89
30 - 130
1,3-Dichlorobenzene
100
73.7
74
1 - 172
1,4-Dichlorobenzene
100
74.2
74
20 - 124
2-Chloronaphthalene
100
86.4
86
60 - 118
g
2,6-Dinitrotoluene
100
99.1
99
50 - 158
i
2,4-Dinitrotoluene
100
97.4
97
39 - 139
3,3'-Dichlorobenzidine
100
97.6
98
1 - 262
4-Bromophenyl phenyl ether
100
103
103
53 - 127
4-Chlorophenyl phenyl ether
100
93.8
94
25 - 158
Acenaphthene
100
90.9
91
47 - 145
Acenaphthylene
100
94.4
94
33 - 145
Anthracene
100
94.1
94
27 - 133
Benzidine
100
81.0
81
1 - 200
Benzo[a]anthracene
100
100
100
33 - 143
Benzo[a]pyrene
100
110
110
17 - 163
Benzo[b]fluoranthene
100
92.9
93
24 - 159
Benzo[g,h,i]perylene
100
85.8
86
1 - 219
-A
Benzo[k]fluoranthene
100
94.9
95
11 - 162
Bis(2-chloroethoxy)methane
100
90.8
91
33 - 184
Bis(2-chloroethyl)ether
100
80.4
80
12 - 158
Bis(2-ethylhexyl) phthalate
100
112
112
8 - 158
Butyl benzyl phthalate
100
101
101
1 - 152
Chrysene
100
99.4
99
17 - 168
Di-n-butyl phthalate
100
89.2
89
1 - 118
Di-n-octyl phthalate
100
112
112
4 - 146
Dibenz(a,h)anthracene
100
90.1
90
1 - 227
Diethyl phthalate
100
54.8
55
1 - 114
Dimethyl phthalate
100
26.7
27
1 - 112
Fluoranthene
100
92.1
92
26 - 137
Fluorene
100
94.2
94
59 - 121
Hexachlorobenzene
100
95.3
95
1 - 152
Hexachlorobutadiene
100
83.5
84
24 - 116
Hexachlorocyclopentadiene
100
20
19
1 - 200 U
Hexachloroethane
100
69.2
69
40 - 113
Indr;no[1,2,3-cd]pyrene
100
83.5
84
1 - 171
]
Isophorone
100
85.0
85
21 - 196
_ J
N-Nitrosodi-n-propy[amine
100
87.9
88
1 - 230
N-Nitrosodimethylamine
100
70.5
71
10 - 150
N-Nitrosodiphenylamine
100
101
101
10 - 150
Naphthalene
100
84.3
84
21 - 133
j
Nitrobenzene
100
81.6
82
35 - 180
TestAmerica Savannah
Page
18 of 36

Client: ARCADIS U.S., Inc.
Lab Control Sample - Batch: 680-195844
Lab Sample ID:
LCS 680-195844/9-A
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
03/08/2011 2017
Date Prepared:
03/03/2011 1032
Analyte
Phenanthrene
Pyrene
2,4-Dimethylphenol
bis(chloroisopropyl) ether
Lab Control Sample - Batch: 680-195844
Analysis Batch: 680-196470
Prep Batch: 680-195844
Units: ug/L
Quality Control Results
Job Number: 680-66071-1
Method: 625
Preparation: 625
Instrument ID: MSG
Lab File ID: g5977.d
Initial Weight/Volume: 1000 mL
Final Weight/Volume: 1 mL
Injection Volume: 1 uL
Spike Amount
Result
% Rec.
Limit
100
97.5
98
54 - 120
100
105
105
52-115
100
52.8
53
32 - 119
100
80.6
81
36 - 166
Method: 625
Preparation: 625
Qual
Lab Sample ID: LCS 680-195844/9-A
Analysis Batch: 680-196462
Instrument ID: MSN
Client Matrix: Water
Prep Batch: 680-195844
Lab File ID: n1429.d
Dilution: 1.0
Units: ug/L
Initial Weight/Volume: 1000 mL
Date Analyzed: 03/08/2011 2021
Final Weight/Volume: 1 mL
Date Prepared: 03/03/2011 1032
Injection Volume: 1 uL
Analyte
Spike Amount
Result
% Rec.
Limit Qua]
2,4,6 Trichlorophenol
100
86.8
87
37 - 144
2,4-Dichlorophenol
100
81.9
82
39 - 135
2,4-Dinitrophenol
100
93.7
94
1 - 191
2-Nitrophenol
100
76.2
76
29 - 182
4,6-Dinitro-2-methylphenol
100
91.1
91
1 - 181
4-Chloro-3-methylphenol
100
50.5
51
22 - 147
4-Nitrophenol
100
76.8
77
1 - 132
Pentachlorophenol
100
97.0
97
14 - 176
Phenol
100
73.9
74
5 - 112
2-Chlorophenol
100
81.5
82
23 - 134
2,4-Dimethylphenol
100
10
7
32 - 119 U
Surrogate
% Rec
Acceptance Limits
2-Fluorophenol
77
35 - 110
TestAmerica Savannah Page 19 of 36

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-196026
Lab Sample ID:
MB 680-196026/1-A
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
03/10/2011 0027
Date Prepared:
03/04/2011 1120
Analysis Batch: 680-196661
Prep Batch: 680-196026
Units: ug/L
Quality Control Results
Job Number: 680-66071-1
Method: 200.8
Preparation: 200.8
Total Recoverable
Instrument ID: ICPMSC
Lab File ID: 192SMPL.D
Initial Weight/Volume: 50 mL
Final Weight/Volume: 250 mL
Analyte
Result
Qua]
RL
Antimony
5.0
U
5.0
Arsenic
2.5
U
2.5
Beryllium
0.50
U
0.50
Cadmium
0.50
U
0.50
Chromium
5.0
U
5.0
Copper
5.0
U
5.0
Lead
1.5
U
1.5
Nickel
5.0
U
5.0
Selenium
2.5
U
2.5
Silver
1.0
U
1.0
Thallium
1.0
U
1.0
Zinc
20
U
20
Lab Control Sample - Batch: 680-196026
Method: 200.8
Preparation: 200.8
Total Recoverable
Lab Sample ID:
LCS 680-196026/2-A
Analysis Batch: 680-196661
Instrument ID: ICPMSC
Client Matrix:
Water
Prep Batch: 680-196026
Lab File ID: 193SMPL.D
Dilution:
1.0
Units:
ug/L
Initial Weight/Volume:
50 mL
Date Analyzed:
03/10/2011 0031
Final Weight/Volume:
250 mL
Date Prepared:
03/04/2011 1120
Analyte
Spike Amount
Result
% Rec.
Limit
Antimony
50.0
55.8
112
85 - 115
Arsenic
100
98.3
98
85 - 115
Beryllium
50.0
48.0
96
85 - 115
Cadmium
50.0
50.8
102
85 - 115
Chromium
100
99.3
99
85 - 115
Copper
100
103
103
85 - 115
Lead
50.0
49.8
100
85 - 115
Nickel
100
102
102
85 - 115
Selenium
100
102
102
85 - 115
Silver
50.0
49.6
99
85 - 115
Thallium
40.0
40.8
102
85 - 115
Zinc
100
102
102
85 - 115
Qual
TestAmerica Savannah Page 20 of 36

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-196183
Lab Sample ID:
MB 680-196183/10-A
Analysis Batch: 680-196504
Client Matrix:
Water
Prep Batch: 680-196183
Dilution:
1.0
Units: ug/L
Date Analyzed:
03/08/2011 1719
Date Prepared:
03/07/2011 1237
Analyte
Result Qual
Mercury
0.20 U
Lab Control Sample - Batch: 680-196183
Lab Sample ID:
LCS 680-196183/11-A
Analysis Batch: 680-196504
Client Matrix:
Water
Prep Batch: 680-196183
Dilution:
1.0
Units: ug/L
Date Analyzed:
03/08/2011 1722
Date Prepared:
03/07/2011 1237
Quality Control Results
Job Number: 680-66071-1
Method: 245.1
Preparation: 245.1
Instrument ID: LEEMAN1
Lab File ID: 030811.chr
Initial Weight/Volume: 50 mL
Final Weight/Volume: 50 mL
RL
0.20
Method: 245.1
Preparation: 245.1
Instrument ID: LEEMAN1
Lab File ID: 030811.chr
Initial Weight/Volume: 50 mL
Final Weight[Volume: 50 mL
Analyte Spike Amount Result % Rec. Limit
Mercury 2.50 2.52 101 85 115
Qua]
TestAmerica Savannah Page 21 of 36

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-195821
Lab Sample ID:
MB 680-195821/5
Analysis Batch: 680-195821
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: umhos/cm
Date Analyzed:
03/02/2011 1633
Date Prepared:
N/A
Analyte
Result Qua]
Specific Conductance
5.0 U
Lab Control Sample - Batch: 680-195821
Lab Sample ID:
LCS 680-195821/8
Analysis Batch: 680-195821
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: umhos/cm
Date Analyzed:
03/02/2011 1640
Date Prepared:
N/A
Quality Control Results
Job Number: 680-66071-1
Method: 120.1
Preparation: N/A
Instrument ID: MANTECH
Lab File ID: sc030211.TXT
Initial Weight/Volume:
Final Weight/Volume: 1.0 mL
RL
5.0
Method: 120.1
Preparation: N/A
Instrument ID: MANTECH
Lab File ID: sc030211.TXT
Initial Weight/Volume:
Final Weight/Volume: 1.0 mL
Analyte Spike Amount Result % Rec. Limit
Specific Conductance 1000 1020 102 90 - 110
Qual
TestAmerica Savannah Page 22 of 36

Client: ARCADIS U.S.. Inc.
Lab Control Sample - Batch: 680-195951
Lab Sample ID:
LCS 680-195951/7
Analysis Batch: 680-195951
Client Matrix:
Water
Prep Batch: N/A
Dilution:
1.0
Units: SU
Date Analyzed:
03/03/2011 1212
Date Prepared:
N/A
Analyte
Spike Amount Result
pH
7.00 7.010
Quality Control Results
Job Number: 680-66071-1
Method: 150.1
Preparation: N/A
Instrument ID: MANTECH
Lab File ID: 030311 ph.TXT
Initial Weight/Volume:
Final Weight/Volume: 1.0 mL
% Rec. Limit
100 63-158
Qua[
TestAmerica Savannah Page 23 of 36
j

Client: ARCADIS U.S.. Inc.
Method Blank -Batch: 680-196533
Quality Control Results
Job Number: 680-66071-1
Method: 1664A
Preparation: 1664A
Lab Sample ID: MB 680-196533/21-A
Analysis Batch: 680-196638
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: 680-196533
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 500 mL
Date Analyzed: 03/10/2011 1315
Final Weight/Volume: 500 mL
Date Prepared: 03/09/2011 1720
Analyte
Result
Qual RL
._..M.5.0
.HEM (Oil & Grease)
u..,.,.y-5.0�-
Lab Control Sample/
Method: 1664A
Lab Control Sample Duplicate Recovery Report - Batch: 680-196533
Preparation: 1664A
LCS Lab Sample ID: LCS 680-196533/22-A
Analysis Batch: 680-196638
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: 680-196533
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight[Volume: 500 mL
Date Analyzed: 03/10/2011 1315
Final Weight/Volume: 500 mL
Date Prepared: 03/09/2011 1720
LCSD Lab Sample ID: LCSD 680-196533123-A
Analysis Batch: 680-196638
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: 680-196533
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: b00 mL
Date Analyzed: 03/10/2011 1315
Final Weight/Volume: 500 mL
Date Prepared: 03/09/2011 1720
% Rec.
Analyte
LCS LCSD Limit
RPD RPD Limit LCS Qual LCSD Qua]
HEM (Oil & Grease)
98 97 78 - 114
2 18
TestAmerica Savannah Page 24 of 36

Quality Control Results
Client: ARCADIS U.S., Inc. Job Number: 680-66071-1
Method Blank - Batch: 680-196814
Method: 350.1
Preparation: N/A
Lab Sample ID:
MB 680-196814/1
Analysis Batch: 680-196814
Instrument ID: KONELAB1
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: KONE11103101NH3A.xls
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 2 mL
Date Analyzed:
03/10/2011 1300
Final Weight/Volume: 2 mL
Date Prepared:
NIA
Analyte
Result
Qual RL
Ammonia
0.050
U 0.050
Lab Control Sample - Batch: 680-196814
Method: 350.1
Preparation: NIA
Lab Sample ID:
LCS 680-196814/2
Analysis Batch: 680-196814
Instrument ID: KONELAB1
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: KONE11103101NH3A.xis
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 2 mL
Date Analyzed:
03/10/2011 1300
Final WeighWolume: 2 mL
Date Prepared:
N/A
Analyte
Spike Amount Result
% Rec. Limit Qual
Ammonia
1.00 1.06
106 90 - 110
TestAmerica Savannah Page 25 of 36

Quality Control Results
Client: ARCADIS U.S., Inc. Job Number: 680-66071-1
Method Blank - Batch: 680-197005 Method: 351.2
Preparation: 351.2
Lab Sample ID: MB 680-197005/1-A Analysis Batch: 680-197150 Instrument ID: KONELAB1
Client Matrix: Water Prep Batch: 680-197005 Lab File ID: KONE11103141TKNA.xls
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 40 mL
Date Analyzed: 03/14/2011 1433 Final Weight/Volume: 40 mL
Date Prepared: 03/12/2011 1430
Analyte Result Qual RL
Nitrogen, K'eldahl 0.20 U 0.20
Lab Control Sample - Batch: 680-197005 Method: 351.2
Preparation: 351.2
Lab Sample ID: LCS 680-197005/2-A Analysis Batch: 680-197150 Instrument ID: KONELAB1
Client Matrix: Water Prep Batch: 680-197005 Lab File ID: KONE11103141TKNA.xls
Dilution: 1.0 Units: mg/L Initial Weight/Volume: 40 mL
Date Analyzed: 03/14/2011 1433 Final Weight/Volume: 40 mL
Date Prepared: 03/12/2011 1430
Analyte Spike Amount Result % Rec. Limit Qual
Nitrogen, Kjoldahl 1.00 1.03 103 75 - 125
TestAmerica Savannah Page 26 of 36

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-195898
Lab Sample ID:
MB 680-195898/1
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
03/02/2011 1645
Date Prepared:
N/A
Analyte
Nitrite as N
Nitrate as N
Nitrate Nitrite as N
Lab Control Sample - Batch: 680-195898
Lab Sample ID:
LCS 680-195898/2
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
03/02/2011 1646
Date Prepared:
N/A
Analysis Batch: 680-195898
Prep Batch: N/A
Units: mg/L
Quality Control Results
Job Number: 680-66071-1
Method: 353.2
Preparation: N/A
Instrument ID: LACHAT2
Lab File ID: OM 3-2-2011 16-16-39,OMN
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
Result
Qual
RL
0.050
U
0.050
0.050
U
0.050
0.050
U
0.050
Analysis Batch: 680-195898
Prep Batch: N/A
Units: mg/L
Method: 353.2
Preparation: N/A
Instrument ID: LACHAT2
Lab File ID: OM-3-2-2011-16-16-39.OMN
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
Analyto
Spike Amount
Result
% Rec. Limit
Nitrite as N
0.500
0.488
98 90-110
Nitrate as N
0.500
0.515
103
Nitrate Nitrite as N
1.00
1.00
100 90-110
Qual
TestAmerica Savannah
Page 27 of 36

Quality Control Results
Client: ARCADIS U.S., Inc.
Job Number: 680-66071-1
Method Blank - Batch: 680-196072
Method: 353.2
Preparation: N/A
Lab Sample ID:
MB 680-196072/1
Analysis Batch: 680-196072
Instrument ID: LACHAT2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 2
mL
Date Analyzed:
03/02/2011 1644
Final Weight/Volume: 2
mL
Date Prepared:
N/A
Analyte
Result
Qual
RL
Nitrite as N
0.050
U
0.050
Lab Control Sample - Batch: 680-196072
Method: 353.2
Preparation: N/A
Lab Sample ID:
LCS 680-196072/2
Analysis Batch: 680-196072
Instrument ID: LACHAT2
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Units: mg/L
Initial Weight/Volume: 2
mL
Date Analyzed:
03/02/2011 1646
Final Weight/Volume: 2
mL
Date Prepared:
N/A
Analyte
Spike Amount Result
% Rec. Limit
Qual
Nitritp as N
0.500 0488
----------
98 qO - 110
TestAmerica Savannah Page 28 of 36

Client: ARCADIS U.S., Inc.
Unseeded Control Blank - Batch: 680-195785
Quality Control Results
Job Number: 680-66071-1
Method: 405.1
Preparation: N/A
Lab Sample ID: USB 680-195785/1
Analysis Batch: 680-195785
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 1.0 mL
Date Analyzed: 03/02/2011 1445
Final Weight/Volume: 1.0 mL
Date Prepared: N/A
Analyte
Result
Qual RL
Biochemical Oxygen Demand
2.0
U 2.0
Lab Control Sample/
Method: 405.1
Lab Control Sample Duplicate Recovery Report
- Batch: 680-195785
Preparation: N/A
LCS Lab Sample ID: LCS 680-195785/2
Analysis Batch: 680-195785
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume: 1.0 mL
Date Analyzed: 03/02/2011 1445
Final Weight/Volume: 1.0 mL
Date Prepared: N/A
LCSD Lab Sample ID: LCSD 680-195785/3
Analysis Batch: 680-195785
Instrument ID: No Equipment Assigned
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dlluflon: 1.0
Units: mg/L
Initial Weight/Volume: 1.0 mL
Date Analyzed: 03/02/2011 1445
Final Weight/Volume: 1.0 mL
Date Prepared: N/A
% Rec.
Analyte
LCS LCSD Limit
RPD RPD Limit LCS Qual LCSD Qual
_. .,».,..,_.,..,..,. ...,._.._..
Biochemical Oxygen Demand
, ....,...._...,,.._......... ....
100 97 85 - 115
_ .._»,...._......_. _ ... _._. _,...,_....,.,_.,
3 30
TestAmerica Savannah Page 29 of 36

Client: ARCADIS U.S., Inc.
Quality Control Results
Job Number: 680-66071-1
Method Blank -Batch: 680-196298
Method: 410.4
Preparation: N/A
Lab Sample ID: MB 680-196298/3
Analysis Batch: 680-196298
Instrument ID: SPC1
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume:
2 mL
Date Analyzed: 03/08/2011 0900
Final Weight/Volume:
2 mL
Date Prepared: N/A
Analyte
Result
Qual
RL
Chemical Oxygen Demand
20
L1
20
Lab Control Sample - Batch: 680-196298
Method: 410.4
Preparation: N/A
Lab Sample ID: LCS 680-196298/4
Analysis Batch: 680-196298
Instrument ID: SPC1
Client Matrix: Water
Prep Batch: N/A
Lab File ID: N/A
Dilution: 1.0
Units: mg/L
Initial Weight/Volume:
2 mL
Date Analyzed: 03/08/2011 0900
Final Weight/Volume:
2 mL
Date Prepared: N/A
Analyte
Spike Amount Result
% Rec. Limit
Chemical Oxygen Demand
100 95.6
96 90-110
Qual
TestAmerica Savannah
Page 30 of 36

Client: ARCADIS U.S., Inc.
Method Blank -Batch: 680-196301
Lab Sample ID:
MB 680-196300/1-A
Client Matrix:
Water
Dilution:
1.0
Date Analyzed:
03/08/2011 0900
Date Prepared:
N/A
Analyte
Chemical Oxygen Demand -Dissolved
Analysis Batch: 680-196301
Prep Batch: N/A
Units: mg/L
Result
20
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-196301
Quality Control Results
Job Number: 680-66071-1
Method: 410.4
Preparation: N/A
Instrument ID: SPC1
Lab File ID: N/A
Initial Weight/Volume: 2 mL
Final Weight/Volume: 2 mL
Qual RL
U 20
Method: 410.4
Preparation: N/A
MS Lab Sample ID:
680-66071-1
Analysis Batch: 680-196301
Instrument ID: SPC1
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Initial Weight/Volume:
10 mL
Date Analyzed:
03/08/2011 0900
Final Weight/Volume:
10 mL
Date Prepared:
N/A
MSD Lab Sample ID:
680-66071-1
Analysis Batch: 680-196301
Instrument ID: SPC1
Client Matrix:
Water
Prep Batch: N/A
Lab File ID: N/A
Dilution:
1.0
Initial Weight/Volume:
10 mL
Date Analyzed:
03/08/2011 0900
Final Weight/Volume:
10 mL
Date Prepared:
N/A
Analyte
Chemical Oxygen Demand -Dissolved
% Rec.
MS MSD Limit
109 109 90 - 110
RPD RPD Limit MS Qual MSD Qual
0 30
TestAmerica Savannah Page 31 of 36

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Login Sample Receipt Checklist
Client: ARCADIS U.S., Inc.
Login Number: 66071
List Number: 1
Creator: Conner, Keaton
Question
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
I Sample bottles are completely filled.
Sample Preservation Verified
There is sufficient vol. foi all requested analyses, Incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Answer Comment
N/A
True
True
True
True
True
True
True
True
N/A
True
True
True
True
True
True
True
True
True
True
True
N/A
N/A
Job Number: 680-66071-1
List Source: TestAmerica Savannah
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1 TestAmerica Savannah Page 36 of 36