WI0100106_Report_20150326

IRL13
BUNNELL-LAMMONS ENGINEERING, INC.
GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS
INTERIM EVALUATION REPORT --
2014 INJECTION & MONITORING
%k GAR
1`� O N.
1 5 Q`
LO o�
���fJ1111111j11s
UIC PERMIT No. WI0100106
FORMER ANDREX INDUSTRIES CORP.
180 DEAVERVIEW ROAD
ASHEVILLE, NORTH CAROLINA
BROWNFIELDS PROJECT NUMBER 07022-03-11
PREPARED BY:
BUNNELL-LAMMONS ENGINEERING, INC.
GREENVILLE, SOUTH CAROLINA
MARCH 26, 2015
BLE PROJECT NUMBER J14-1022-38
IHSB ID NUMBER NONCD0001271
GROUNDWATER INCIDENT NUMBER 6586

,1,A3
BUNNELL-LAMMONS ENGINEERING, INC.
GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS
March 26, 2015
Underground Injection Control Program
DWR - Aquifer Protection Section
1636 Mail Service Center
Raleigh, NC 27699-1636
Attention: Mr. Mike Rogers
Subject: Interim Evaluation Report— 2014 Injection & Monitoring
UIC Permit No. WI0100106
Former Andrex Industries Corp.
180 Deaverview Road
Asheville, North Carolina
BLE Project Number J14-1022-38
Brownfields Project Number 07022-03-11
NCDENR Groundwater Incident Number 6586
Dear Mr. Rogers:
As authorized by Milkco, Inc.'s acceptance of our proposal number P13-0454 (dated March 14,
2014), Bunnell-Lammons Engineering, Inc. (BLE) has performed one injection event during the
2014 calendar year at the subject site. The purpose of this project was to inject 1% milk solution to
stimulate bioremediation of the chlorinated solvent contaminants in the groundwater.
The 2014 work included the installation of one injection well (IW-2) and one groundwater monitoring
well (MW-44), baseline sampling of the wells in the IW-2 area, semi-annual sampling of 2 surface water
points, the performance of one injection event, and the performance of 3 post -injection sampling
(monitoring) events. This project is compliant with the North Carolina Brownfields Program
requirements to continue groundwater remediation and monitoring at the subject site. The enclosed
report describes the work performed and presents the results obtained in accordance with the
requirements of the subject UIC permit.
Project Information: Andrex Industries Corp (Andrei) formerly owned and operated an industrial
textile production facility located at 180 Deaverview Road within the city limits of Asheville, North
Carolina (Figure 1). The company operated a knitted fabric weaving and cutting business for
women's and children's clothing at this location. In prior years, the facility was operated as a textile
finishing business that conducted cutting, dry cleaning, shrinking and packaging of fabrics. The
subject facility was in operation since the mid-1960s, although under various ownership. A two-
story light manufacturing facility with approximately 77,000 square feet of office, manufacturing,
warehouse, storage and utility space occupied the approximately nine -acre site. Two buildings were
present at the site; a split level brick building and slab -on -grade metal building.
No dry cleaning has been conducted on site since 1995. However, prior to 1995, dry cleaning
operations were prevalent on site and the use of tetrachloroethylene (a.k.a. Perchloroethylene, PCE)
was common. Virgin PCE was stored on site in a 6,000-gallon underground storage tank (UST).
6004 PONDERS COURT PHONE [phone]
GREENVILLE, SOUTH CAROLINA 29615 FAX [phone]

♦ILL
Andrei Industries — 2014Interim Evaluation Report March 26, 2015
Asheville, NC BLE Project Number J14-1022-38
Prior to 1989, the use of the PCE UST was discontinued and the tank was filled with sand. The UST
was replaced with a 6,000-gallon AST which was used until 1995. In 1995, dry cleaning processes
and the use of PCE were discontinued.
In 1991 concentrations of PCE were detected in the groundwater above the applicable North Carolina
Title 15A Subchapter 2L (NC2L) groundwater standards' maximum level of 0.7 µg/l and the
NCDENR issued Groundwater Incident Number 6586 for the site. Concentrations of PCE were also
documented in the soil near the PCE UST and at other subsurface facility locations. The NCDENR
approved a comprehensive site assessment (CSA) and corrective action plan (CAP) for the site and
remedial efforts were conducted from 1993 through 2005. Remedial efforts consisted of the
installation and operation of two groundwater pump and treat (P&T) systems and one soil vapor
extraction (SVE) system.
The SVE and both groundwater P&T systems were operated and maintained by BLE for Andrex
from May 2003 through August 2005. Treated groundwater effluent was discharged to the sanitary
sewer under a MSD permit. BLE also performed annual site -wide groundwater and surface water
sampling and analysis for Andrex to monitor the fate of the groundwater plume. BLE submitted
quarterly reports of the remedial progress through August 2005 and annual groundwater monitoring
reports through 2005 to the NCDENR to document site activities.
The remediation system operations were suspended in August 2005 at the discretion of the property
owner. Annual groundwater monitoring was also suspended at the discretion of the property owner,
with the last sampling event conducted in November 2005.
In early 2005, Andrex requested that BLE evaluate feasible remedial alternatives for the site. A
preliminary review of alternate remedial technologies identified a unique opportunity to evaluate
bioremediation at the site. Food -grade lactate containing byproducts (milk solution) from the
neighboring Milkco, Inc. (Milkco) facility were being considered for use as a bio-enhancing remedial
product for the former Andrex facility. The implementation of this type of remedial action was
dependent upon the results of a feasibility study which includes bench- and field -scale testing studies
of the milk solution.
In 2005, Andrex retained BLE to perform a pilot study of the milk solution. The study was to include
two parts. The first part was a bench test which was to be followed by a field trial. BLE completed
the bench study in early 2006. The results showed a net decrease in PCE concentration of 30% after
40 days in those microcosms containing the highest concentrations of milk solution. Significant
concentrations of PCE daughter products were also produced in the bench study indicating successful
de -chlorination of the parent product, as anticipated. The field trial portion of the pilot test was
suspended by Andrex after the bench test results were obtained.
In 2006, Milkco entered into a Brownfield's Agreement (Agreement) with the State of North
Carolina as part of a potential purchase of the Andrex property. The property was sold in 2007 and
as part of the plan (see below) for retrofit of the subject site; Milkco removed and/or demolished
selected equipment and facility infrastructure.
In August 2007, three underground storage tanks (one PCE and two heating oil) were removed and
disposed by a contractor retained by Milkco on behalf of Andrex. The results of the activities were

♦ILL
Andrei Industries — 2014Interim Evaluation Report March 26, 2015
Asheville, NC BLE Project Number J14-1022-38
documented in a report titled Report of Limited Assessment for UST Closure dated November 26,
2007 (BLE Project No. J07-1022-20).
As part of Milkco's redevelopment plans for the site, BLE issued a plan titled Work Plan for
Redevelopment of the Andrex Brownfields Site (Milkco Cooler Expansion) dated June 13, 2008 (BLE
Project No. J08-1022-23). The plan addressed the Program's requirements including excavation and
disposal of contaminated soil (source area) and continued groundwater monitoring. The Program
reviewed and approved (with modification) the plan in a letter to BLE dated July 7, 2008. The
schedule for implementation of the redevelopment plan was changed on December 11, 2008 with
concurrence of the Program.
In July 2008, BLE abandoned selected groundwater monitoring and recovery wells in accordance
with the approved redevelopment plan. The results of the well abandonment activities were
documented in a report titled Report of Well Abandonment Services for the Milkco Cooler Expansion
dated January 19, 2009 (BLE Project No. J08-1022-26).
From July through September 2008, contaminated soils were removed and disposed by a contractor
retained by Milkco in accordance with the approved redevelopment plan. The results of the remedial
activities were documented in a report titled Report of Hotspot Soil Removal and Disposal for the
Milkco Cooler Expansion dated June 3, 2009 (BLE Project No. J08-1022-25).
By December 2008, the former Andrex brick building(s) and metal building had been demolished
with only the building slabs remaining. Additionally, all groundwater and soil remediation systems
had been dismantled, removed, and stored by Milkco. All work performed by Milkco (non -
responsible party) is in compliance with the requirements of the NCDENR Brownfields Program
(Program) and the Agreement.
In February 2008, Andrex resumed annual groundwater monitoring at the site. BLE has performed
the sampling services and prepared and submitted reports each calendar year since 2008. The
approved redevelopment plan requires the continuation of annual groundwater monitoring and remedial
activities at the site.
In June 2010, BLE submitted a permit application to the NCDENR UIC program for a field -scale pilot
test for remediation of the site's groundwater using milk solution. Subsequent information was
requested by the North Carolina Division of Water Quality (DWQ) [now known as the Division of Water
Resources] and that information was prepared and/or collected, and submitted by BLE in August 2010
and December 2010. On December 22, 2010, the DWQ issued Injection Permit WI0100106 to Milkco.
The permit required special conditions and limitations including minor modifications to the injection
monitoring plan. The permit effective dates were December 22, 2010 through November 20, 2013 with
a renewal option if submitted 120 days prior to expiration of the permit.
The permit was part of a green/sustainable enhanced bioremediation approach utilizing milk solution.
The injection plan included an injection schedule over 5 years with semi-annual injections planned for
the first two years. BLE proposed to conduct the project in phases with the first phase including two
injection events (and monitoring) within a 12-month period (designated "Year One" in the plan). BLE
was retained by Milkco to perform the injection and monitoring services for year one in 2011.

♦ILL
Andrei Industries — 2014 Interim Evaluation Report March 26, 2015
Asheville, NC BLE Project Number J14-1022-38
Subsurface injections of milk solution into four former groundwater recovery wells were performed in
May/June 2011 and September/October 2011 and monitoring was conducted as planned. The results
showed that daughter products of PCE were being created as anticipated. Based on these data, injections
during the first half of 2012 were suspended and monitoring was conducted to determine the long-term
results of the 2011 injections. Sampling was conducted at a 60-day monitoring frequency through July
2012 and site -wide annual sampling conducted in September 2012. Based on the results obtained we
recommended the performance of a third injection event in late September 2012 with a 60-day
monitoring frequency through March 2013. These modifications were documented in a letter to the UIC
Program titled Notice of Intent for Milk Solution Injection & Monitoring [3rd Injection Event and 3
Monitoring Events (2012-2013)] dated September 12, 2012 (BLE Project No. J12-1022-35). The
UIC approved the plan and the 3' injections were performed in September/October 2012 with
subsequent monitoring conducted through March 2013.
BLE issued an interim evaluation report documenting the performance of all 3 injection events and
the 13 monitoring events performed to evaluate the results of the field -scale pilot test. The report
titled Interim Evaluation Report -- Field -Scale Pilot Test UIC Permit No. WI0100106 dated July 30,
2013 (BLE Project No. J12-1022-35) which concluded that the pilot project was successful and full-
scale injection should be performed as a viable groundwater remedial measure.
At the request of Milkco, BLE prepared and submitted a permit renewal application dated July 30,
2013 and addendum dated November 19, 2013. The application included a plan for injection and
monitoring over a 5 year permit term. The application et seq. and plan was approved (with
modification) by the NCDENR in a letter to Milkco dated December 13, 2013. Injection and
monitoring was performed in 2014 in accordance with the permit.
This Interim Evaluation Report documents the performance of the 2014 injection event and provides
the data from the 2014 monitoring events performed to evaluate the results of the injection. The
report also updates the status of the long-term results for the 2011-2013 pilot injection areas.
Well Installation: BLE installed one injection well (IW-2) and one groundwater monitoring well
(MW-44) in April 2014 at the locations shown on Figures 2, 3, and 4. Well installations were performed
and surveyed in accordance with the approved permit. BLE prepared and submitted a GW-1 form for
each well (Appendix A) to the DENR. BLE also prepared well construction logs for each well which
are part of this report (Appendix A).
Milk Solution Injection: One (1) milk solution injection event was performed in accordance
with the permit. The injection event was designated 2014 (Event 4). Recall that prior injection events
conducted during the field -scale pilot test were designated 2011-1 (Event 1), 2011-2 (Event 2), and
2012-1 (Event 3). Injection Event 4 was performed from May 14, 2014 to June 2, 2014. BLE provided
notice to the DWR prior to performance of the event and an Injection Event Record was submitted to
the DWR at the conclusion of the event as required (Appendix B).
Quality control samples of the milk solution were collected during to evaluate the total organic carbon
(TOC) content of the injectant. The samples were 3-point composites collected at the beginning,
middle, and end of a single day of injection. Three (3) composite samples were collected during Event
2014 and were designated IC-2014-A, IC-2014-13, and IC-2014-C. The results are summarized on
Table 1 and the laboratory analytical results are included in Appendix C. The results indicate a
minimum TOC concentration of 2,500 mg/L and a maximum TOC concentration of 4,100 mg/L. An
11

♦ILL
Andrei Industries — 2014 Interim Evaluation Report March 26, 2015
Asheville, NC BLE Project Number J14-1022-38
average TOC concentration of 3,530 mg/L was calculated from the results (Table 1). The historical
results from the 2011-2012 field -scale pilot test injections are also included on Table 1. We conclude
that the TOC content of the injectant in 2014 was not consistent throughout the injection event and
lower in concentration than that analyzed during the field -scale pilot. It is possible that the results are
a milk solution mixing error, a sampling artifact, or laboratory error.
Injections were performed into injection well IW-2. A groundwater elevation map (Figure 2), a plume
map (Figure 3), and a hydrogeologic profile (Figure 4) are included for reference. Please note that the
data on the maps was sourced from the 2014 annual report and that maps are not reflective of the
conditions at the time of the 2014 injection event. Milk solution was prepared at the Milkco facility in
2,000 gallon batches and delivered to the well head via plastic tank. The milk solution was injected via
gravity flow from the tank by hose discharging into the well head at the ground surface. Flow rates
were adjusted via valve assembly to match the infiltration rate of the well. The injection start date and
time and end date and time were recorded for each batch on a field log. A summary of the total volume
injected is shown on Table 2. A plot of the injection record for IW-2 was prepared from the field log
(Appendix B). The plot shows the actual volume injected vs. time with a graphical illustration of the
target injection volume and target injection rate. As shown on the plot, milk solution infiltration rates
into IW-2 were close to target injection rate for the duration of the injection event.
During the field -scale pilot test injections we observed that injection rates slowed from Event 1 to Event
3 in each well except RW-3. Furthermore by Event 3 recovery wells RW-1 and RW-5 appeared to be
completely clogged. It is assumed that the milk solids in the injectant clogged the screen and/or filter
pack in these wells. Rehabilitation was attempted in RW-1 and RW-5 but was unsuccessful. We
concluded that recovery wells RW-1, RW-5, and RW-7 were no longer suitable for use as injection
points but are viable monitoring points. We also concluded that RW-3 could be used as a future
injection and monitoring point but long-term hydraulic response to injection is unknown. It should be
noted that only one injection event was performed in IW-2 in 2014. It is possible that future injections
into IW-2 may clog the well's injection zone.
Monitoring Results: Groundwater and surface water monitoring was performed in 2014 as
specified in the permit and injection plan as summarized on the 2014 Full -Scale Injection and Sampling
Matrix (Table 3).
One baseline monitoring event was performed in May 2014 prior to injection Event 4. The monitoring
event included the wells in the IW-2 injection area (IW-2, RW-1, MW-6, and MW-44) and 2 surface
water sampling points (BC-1 and JW-1) as part of the semi-annual surface water monitoring program
required by the permit. The groundwater and surface water samples were analyzed for TOC by SM
5310B and for VOCs by EPA Method 8260B.
A summary of the baseline TOC results are provided on Table 4. A summary of the baseline VOC
results are provided on Table 5. The laboratory data sheets are included in Appendix D. Based on
the data from baseline sampling in 2008 and 2009 it appears that the natural background TOC
concentration in groundwater at most locations is less than 10 mg/L. Baseline TOC sampling was not
performed in the surface waters. However, data from subsequent surface water monitoring events
where TOC analyses were performed indicates that natural background TOC concentration in surface
water is less than 10 mg/L.
5

♦ILL
Andrei Industries - 2014 Interim Evaluation Report March 26, 2015
Asheville, NC BLE Project Number J14-1022-38
Three (3) groundwater monitoring events and one surface water monitoring event were performed after
injection Event 2014 at approximate 30-, 90-, and 150-day milestones. The sampling events were
conducted in July (30 day), September (90 day), and November (150 day). The September 2014 event
was the regularly scheduled annual monitoring event which included surface water monitoring. The
TOC results are summarized on Table 4 and the VOC results are summarized on Tables 6, 7, & 8.
The laboratory data is provided in Appendix E (July 2014), Appendix F (September 2014), and
Appendix G (November 2014).
Measurements of concentration of TOC in groundwater are used as an indicator parameter for the
subsurface migration of milk solution (injection zone limits) and to assess carbon consumption as part
of biological activity. Historical plots of TOC concentrations in groundwater have been prepared for
select wells including injection wells RW-1, RW-3, RW-5, RW-6, RW-7, IW-2, and monitoring wells
MW-5, MW-6, MW-7, MW-9, MW-10, MW-11, MW-12, MW-13, MW-14, MW-24, and MW-44
(Appendix H). Baseline sampling event data and injection events are illustrated on each TOC plot.
Measurements of concentrations of VOCs in groundwater are used to determine if transformation of
parent product (PCE) to daughter product (TCE, Cis-DCE, and vinyl chloride) is occurring. Plots of
PCE, TCE, Cis-DCE, and vinyl chloride (VC) concentration vs. time were prepared for injection wells
RW-1, RW-3, RW-5, RW-6, RW-7, IW-2, and monitoring wells MW-5, MW-6, MW-7, MW-9, MW-
10, MW-11, MW-12, MW-13, MW-14, MW-24, and MW-44 (Appendix I).
RW-1/IW--2 Iniection Area Results and Conclusions
Four injection events have been performed in this area including the 3 field -scale pilot test events in
2011 to 2012 (Events 1 through 3 into RW-1) and the single full-scale injection event in 2014 (Event
4 into IW-2). Monitoring in this area includes RW-1, IW-2, MW-6, and MW-44. Monitoring well
MW-9 is also monitored (on an annual frequency) but is currently outside the injection zone.
The TOC concentrations in RW-1 spiked significantly after injection Events 1 and 2. A smaller spike
was observed after limited volumes were injected during Event 3. TOC concentrations have been on
a steady decline since 2012 as the carbon is consumed. The TOC concentration in RW-1 was not
affected by injection into IW-2 in 2014. A majority of the contaminant mass in RW-1 has been
transformed to Cis-DCE and reduction of PCE concentration continues to occur.
The TOC concentrations in MW-6 spiked significantly after injection Events 1 through 3. However,
the carbon quickly dissipated after each event. We conclude the MW-6 is upgradient from RW-1 and
that the migration of carbon was due to the temporary hydraulic effects of injection and to a lesser
extent diffusion. The TOC concentration in MW-6 was not affected by injection into IW-2 in 2014. A
brief spike of Cis-DCE was observed in late 2012 but returned to normal historical concentrations until
late 2014 when Cis-DCE began to increase. It's possible that treated groundwater from the RW-3 area
is moving into the MW-6 area. We conclude that there was no long-term effect in MW-6 as the result
of injections into RW-1 in 2011-2012 and there was no effect in MW-6 as the result of injection into
IW-2 in 2014. It appears that the remaining contaminants in MW-6 (and RW-1) may be sourced from
the upper contaminated groundwater which will be targeted in 2015 with the installation of and
injections into injection well lW-3.
The TOC concentrations in MW-9 do not appear to have been affected by injection Events 1 through
4. The background TOC concentration in MW-9 is highly variable and may obscure observation of
injection -sourced TOC values. The VOC concentrations observed in MW-9 appear to be similar to
0

♦ILL
Andrei Industries — 2014 Interim Evaluation Report March 26, 2015
Asheville, NC BLE Project Number J14-1022-38
historical values. However, PCE concentrations have decreased since mid-2011 and Cis-DCE
concentrations have slightly increased since late 2012. Continued monitoring may validate these
trends.
Monitoring well MW-44 was installed in 2014 and was sampled 4 times since installation. Neither
TOC nor VOC concentrations appear to be affected by the injection events. MW-44 will continue to
be monitored as part of future injections in the RW-1/IW-2 area after IW-3 is installed in 2015.
RW-3 Iniection Area Results and Conclusions
Three injection events have been performed in this area which includes the 3 field -scale pilot test events
in 2011 to 2012 (Events 1 through 3 into RW-3). Monitoring in this area includes RW-3, MW-5, and
MW-12. Monitoring wells MW-7 and MW-24 are also monitored (on an annual frequency) but these
wells are currently outside the injection zone.
The TOC concentrations in RW-3 spiked significantly after injection Events 1, 2, and 3. TOC
concentrations have rapidly declined after each event as the carbon is consumed. A majority of the
VOC contaminant mass in RW-3 has been completely transformed. A slight rebound of VOCs was
observed in late 2014.
The time vs. TOC concentration plots for MW-5 and MW-12 (Appendix H) shows that significant
concentrations of TOC were detected in MW-12 with lesser concentrations detected in MW-5. TOC
concentrations have rapidly declined after in each well after each event as the carbon is consumed. A
majority of the VOC contaminant mass in MW-12 has been completely transformed. A slight rebound
of VOCs was observed in late 2014. The PCE concentrations in MW-5 showed a significant decrease
in with contemporaneous increase in Cis-DCE immediately after each injection event. However, VOC
concentrations returned to historical values after the carbon was consumed. We conclude that the
contaminant mass observed in MW-5 is sourced from the upper groundwater which will be targeted in
2015 with the installation and injection into injection well IW-1.
The TOC concentrations in MW-7 and MW-24 do not appear to have been affected by injection Events
1 through 3. However, slight increases in TOC concentrations were observed in MW-7 in 2012 and in
MW-24 in 2013. The observed TOC concentration increases cannot be conclusively attributed to
injection and may be an artifact of natural fluctuations. Insufficient TOC history is available for a
determination. The VOC concentrations observed in MW-7 and MW-24 appear to be similar to
historical values and not affect by the injection events.
RW-5Iniecdon Area Results and Conclusions
Three injection events have been performed in this area which includes the 3 field -scale pilot test events
in 2011 to 2012 (Events 1 through 3 into RW-3). Monitoring in this area includes RW-5 and MW-10.
Monitoring wells MW-13 and MW-14 and Recovery Well RW-6 are also monitored (on an annual
frequency) but these wells are currently outside the injection zone.
The TOC concentrations in RW-5 spiked significantly after injection Events 1 and 2. A smaller spike
was observed after limited volumes of milk solution was injected during Event 3 (due to well clogging).
TOC concentrations declined to under 1,000 mg/L after the injection Event 2 and then slowly increased
after injection Event 3. All the carbon had been consumed by late 2014. A majority of the contaminant
mass in RW-5 had been transformed by late 2011 with low concentrations remaining until non -detect
conditions were observed by 2014.

♦ILL
Andrei Industries — 2014 Interim Evaluation Report March 26, 2015
Asheville, NC BLE Project Number J14-1022-38
The TOC concentrations in MW-10 spiked after every injection event and was rapidly consumed. A
majority of the contaminant mass in MW-10 had been transformed by late 2012. Rebound was
observed beginning in early 2013. We conclude that the contaminated groundwater upgradient of MW-
10 has migrated into the area.
The TOC and VOC concentrations in MW-13 and MW-14 appear to be unaffected by the injection into
RW-5. The TOC concentrations in RW-6 appear to be unaffected by injection into RW-5, however,
PCE concentrations have significantly declined with concentrations of Cis-DCE and VC increasing by
the end of 2014. We conclude that remediated groundwater from the RW-5 area has migrated into the
RW-6 area.
R W- 7 Iniection Area Results and Conclusions
Two injection events have been performed in this area which includes the 2 of the field -scale pilot test
events in 2011 (Events 1 and 2). Monitoring in this area includes RW-7 and MW-11. In 2011, during
the injection events, it was discovered that the RW-7 well was clogged with tree roots and the well
screen or casing appeared to be broken at depth. The infiltration rate into RW-7 was very slow and
injection into RW-7 was discontinued during Event 2.
The TOC concentrations in RW-7 spiked significantly after injection Events 1 and 2. TOC
concentrations reached a high of 4,814 mg/L by late 2012 then declined to under 1,000 mg/L in late
2014 as carbon was consumed. A majority of the contaminant mass in RW-7 had been transformed by
late 2012 with moderate concentrations of Cis-DCE remaining in late 2014.
The TOC concentrations in MW-11 do not appear to have been affected by injection Events 1 and 2 in
RW-7. The VOC concentrations observed in MW-11 appear to be similar to historical values. We
conclude the MW-11 is upgradient from RW-7 and that the volume of milk solution injected in RW-7
was insufficient to affect MW-11.
Summary and Plans for Future Injection: In general the results from all injections show that
where milk solution was successfully injected into the subsurface, PCE daughter products are being
created as a result. The limiting factors for milk solution delivery into the subsurface appears to be
injection well infiltration rate, long-term well clogging issues, and the availability of milk solution.
Surface water sampling results indicate that the surface waters have been unaffected by the injection
events.
Please note that several VOCs are produced as metabolic byproducts of the groundwater
bioremediation in all injection areas. These metabolic byproducts are specified in bold text in the
footnotes on Tables 5 through 8 and are included on the laboratory results in Appendices D through
G. We anticipate that these metabolic byproducts will naturally attenuate.
Based on the 2014 results described herein, BLE developed a conceptual plan for injection and
monitoring in 2015 and opened an email dialog with the DENR to discuss those plans. The DENR
requested that BLE prepare and submit a written plan for injection and monitoring in 2015. The subject
plan was submitted on December 22, 2014 and was approved by the DENR on January 9, 2015. The
plan includes installation and injection into 2 new injection wells to target the upper groundwater in the
MW-5 and MW-6/RW-1 areas. BLE has been retained my Milkco to perform the work. Injection well
11

♦ILL
Andrei Industries — 2014Interim Evaluation Report
Asheville, NC
March 26, 2015
BLE Project Number J14-1022-38
installation and baseline sampling is scheduled for completion in March 2015. Injection Event 5 is
scheduled for April 2015.
Qualification of Report: The activities and evaluative approaches used in this assessment are
consistent with those normally employed in hydrogeological assessments and remediation projects of
this type. Our evaluation of site conditions has been based on our understanding of the site and project
information and the data obtained.
This report has been prepared as required by the subject permit. This report and the findings contained
herein shall not, in whole or in part, be disseminated or conveyed to any other party or used or relied
upon by any other party excluding DENR, Milkco, and Andrex, without BLE's prior written consent.
Closing: We appreciate the opportunity to work with the DENR on this project. Please contact
us at [phone] if you have any questions or comments regarding this report.
Sincerely,
BUNNELL-LAMMONs ENGINEERING, INC.
941aL"o-t-
Andrew W. Alex der, P.G., RSM
Senior Hydrogeologist
Registered, North Carolina #1475
cc: Ms. Tracy Wahl — DWM Brownfields Program
Mr. Keith Collins — Milkco, Inc.
Mr. Andrew Moore — DWR-ARO
Mr. Stephen Gottdiener — Andrex
Trevor J. Bento G.
Senior Hydrogeo ogist
Registered, North Carolina #2025
e: lawaprojectslandrex milkcolphase38 injection & monitoring 2014U 022-38 ier 20141andrex 2014 interim evaluation report
1022-38 draft.docx
9

TABLES

Table 1
Historical Milk Solution TOC Analysis
Former Andrex Industries
Asheville, North Carolina
NCDENR Groundwater Incident Number 6586
UIC Permit No. W10100106
BLE Project No. J13-1022-38
Pilot
-Scale 3 Injection Events (2011 to 2012)
Sample ID
Date
Result (mg/1)
IC-2011-1-A
June 1, 2011
3,610
IC-2011-1-13
June 7, 2011
6,940
IC-2011-1-C
June 14, 2011
4,970
IC-2011-1-D
June 20, 2011
4,660
IC-2011-2-A
September 28, 2011
4,170
IC-2011-2-B
October 5, 2011
3,880
IC-2012-A
September 25, 2012
4,910
IC-2012-B
October 4, 2012
6,470
Pilot Average All Events
Not Applicable
4,951
Full -Scale 1 Injection Event (2014)
Sample ID
Date
Result (mg/1)
IC-2014-A
May 14, 2014
3,990
IC-2014-B
May 22, 2014
2,500
IC-2014-C
June 2, 2014
4,100
2014 Average All Events
Not Applicable
3,530
Notes
TOC = Total Organic Carbon
Analyses by SM 5310B by Pace Analytical Services, Inc.
All samples are three-point composites
Injection Event 2011-1 [Start Date: May 31, 2011 -- End Date: June 21, 20111
Injection Event 2011-2 [Start Date: September 27, 2011 -- End Date: October 10, 20111
Injection Event 2012 [Start Date: September 24, 2012 -- End Date: October 10, 2012]
Injection Event 2014 [Start Date: May 14, 2014 -- End Date: June 2, 2014]
Prepared by: AWA
Injection TOC Results 3 Events of TI Hist Milk Solution TOC Lab Results.xlsx Checked by: PJVH/TJB

Table 2
Milk Solution Injection Volume
Full -Scale Injection 2014
Andrex Industries
Asheville, North Carolina
NCDENR Groundwater Incident Number 6586
BLE Project No. J14-1022-38
UIC Permit No. W10100106
� I
o
N I
� I
N I
I
I
I
O I
� N i
4
1H I
v I
O
I
I
O
•Y
O
�
r�1N� r l
h1 l I
�
IW-2
24,000
25,000
Notes:
Injectant is a 1% milk solution via gravity feed.
Units in gallons.
Injection target not reached because of limited solution availability.
Prepared by: AWA
Injection Volumes of T2 2014 Injection Volume Summary.xlsx Checked by: TJB

Table 3
2014 Full -Scale Injection and Sampling Matrix
Andrex Industries
Asheville, North Carolina
NCDENR Groundwater Incident Number 6586
BLE Project No. J14-1022-38
>
L7
N N
>
4
Q
ti
>
O bq
U+
CIOzA�
0
v
� U
Groundwater
MW-1
AB
AB
AB
AB
MW-2
AB
AB
AB
AB
MW-3
AB
AB
AB
AB
MW-4
AB
AB
AB
AB
MW-5
NS
NS
V & T
NS
MW-6
V&T
V&T
V&T
V&T
MW-7
NS
NS
V & T
NS
MW-8
AB
AB
AB
AB
MW-8A
AB
AB
AB
AB
MW-9
NS
NS
V & T
NS
MW-10
NS
NS
V & T
NS
MW-11
NS
NS
V & T
NS
MW-12
NS
NS
V & T
NS
MW-13
NS
NS
V & T
NS
MW-14
NS
NS
V & T
NS
MW-15
NS
NS
V & T
NS
MW-16
NS
NS
V & T
NS
MW-17
NS
NS
V & T
NS
MW-18
NS
NS
V & T
NS
MW-19
NP**
NP**
NP**
NP**
MW-20
NS
NS
V & T
NS
MW-21
NS
NS
V & T
NS
MW-22
NS
NS
V & T
NS
MW-23
NS
NS
V & T
NS
MW-24
NS
NS
V & T
NS
MW-25
NP**
NP**
NP**
NP**
MW-26
NS
NS
V & T
NS
MW-44
V&T
V&T
V&T
V&T
1W-2
V&T
I
V&T
V&T
V&T
RW-1
V&T
V&T
V&T
V&T
RW-2
AB
AB
AB
AB
RW-3
NS
NS
V & T
NS
RW-4
AB
AB
AB
AB
RW-5
NS
NS
V & T
NS
RW-6
NS
NS
V & T
NS
RW-7
NS
NS
NS
NS
Surface Water
Smith Mill Creek 1
NS
NS
V & T
NS
Smith Mill Creek 2
NS
NS
V & T
NS
Smith Mill Creek 3
NS
NS
V & T
NS
Smith Mill Creek 4
NS
NS
V & T
NS
Smith Mill Creek 5
NS
NS
V & T
NS
Smith Mill Creek 6
NS
NS
V & T
NS
Bear Creek 1
V& T
NS
V& T
NS
Bear Creek 2
NS
NS
V & T
NS
Bear Creek 3
NS
NS
V & T
NS
Bear Creek 4
NS
NS
V & T
NS
Bear Creek 5
NS
NS
NS
Jehovah Witness 1
V& T
NS
V& T
NS
Cecil's Spring 1
NS
NS
V & T
NS
Cecil's Spring 2
NS
NS
V & T
NS
Notes:
V = Analyses for Volatile Organic Compounds performed by EPA 8260B
T = Analyses for Total Organic Carbon performed by SM 5310B.
V = Analyses for Volatii Organic Compounds performed by EPA 8260B.
I = milk solution injected into this well.
NS = not sampled. Not on sampling matrix or sampling personnel oversight.
NP = not present; monitoring well was abandoned or destroyed.
AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
** These wells were destroyed by grading during 2003.
Recovery/Injection well samples are grab samples collected via bailer.
Prepared by: AWA
2014 Matrix of T3 2014 Injection and Sampling Matrix.xlsx Checked by: TJB

Table 4
TOC Historical Data Summary - Groundwater & Surface Water Samples
Andrei Industries
Asheville, North Carolina
NCDENR Groundwater Incident Number 6586
BLE Project No. J14-1022-38
c
c
W
�
E
c
W
�
o
O
•a°
N
�
E
z
O
E
�
�'
s
�
a
E
•a°
E
_
�'
s
E
W
�
v
H
•a°
r
E
E
Groundwater
MW-1
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-3
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-5
2.1
1.2
18.5
5.2
2.9
ND
34.9
18.0
3.5
4.1
21.4
E
41.5
10.0
14.6
5.1
NS
NS
ND
NS
MW-6
5.9
NS
10.6
15.6
17.8
21.9
22.5
33.1
6.4
5.7
4.6
E
7.6
5.6
32.3
8.8
6.8
6.1
2.1
2.0
MW-7
ND
No
NS
ND
ND
NS
1.2
NS
NS
NS
NS
8.0 C
NS
NS
NS
1.2
NS
NS
ND
NS
MW-8
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-8A
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-9
4.7
25.9
NS
4.9
CO
NS
4.0
NS
NS
NS
NS
9.9 C
NS
NS
C7
31.2
NS
NS
ND
NS
MW-10
5.8
ND
369
333
311
178
49.3
98
151
240
60
27 C
23.1
77.1
10.2
12.1
NS
NS
ND
NS
MW-11
4.0
ND
3.6
4.1
3.6
4.4
3.7
4.1
4.3
NS
NS
E
NS
NS
3.4
3.5
NS
NS
ND
NS
MW-12
1.3
ND
231
355
329
1,150
613
320
53
19A
13.5
E
1,140
668
300
39.1
NS
NS
3.0
NS
MW-13
3.8
ND
NS
1.9
2.1
NS
2.6
NS
1.4
NS
NS
ND
NS
NS
2.2
2.7
NS
NS
NS
MW-14
2.2
ND
NS
1.5
1.6
NS
1.6
NS
1.5
NS
NS
E
NS
NS
2.0
2.1
NS
NS
NS
MW-15
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-16
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
dNP**
NS
MW-17
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-18
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-19
NP--_
NP**
Np*x
NP**
NP**
NP**
NP**
NP**
NP**
NP**
Npx.
NP**
NP**
NP**
NP**
NP**
NP**
NP**
NP**
MW-20
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-21
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-22
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-23
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
ND
NS
MW-24
NS
NS
NS
NS
NS
NS
NS
NS
ND
NS
NS
NS
NS
NS
1.8
2.2
NS
NS
ND
NS
MW-25
NP"*
NP-*
NP-
NP**
NP-
NP**
NP**
NP**
NP**
NP**
I"**
NP**
Np**
NP**
NP**
NP**
NP**
Np•*
NP**
N.P.•
MW-26
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-44
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
4.8
6.3
ND
No
IW-2
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
47.4
I
2,370
2,600
4,400
RW-1
6.4
ND
I
363
720
4,590
I
6,400
4,480
5,300
4,460
2,660
1,600
1,244 C
I
2,210
1,270
738
333
667
412
190
170
RW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
RW-3
3.4
ND
I
320
1,400
138
1
1,970
3,960
1,190
779
296
143
93 C
I
2,730
274
18.3
175
NS
NS
47.0
NS
RW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
RW
.3
268
970
263
550
292 C
I
1,170
1,540
NS
NS
16.0
NS
RW-6
4
13.4
NS
4.2
4.5
NS
6.0
NS
5.6
6.2
6.5
E
6.6
5.7
7.9
476 P
NS
NS
1.0
NS
RW-7
4.3
13.7
I
2,560
3,520
3,010
I
4,030
4,230
3,720
3,020
NS
NS
4,814 C
NS
NS
4,120
1,490
NS
NS
730
NS
Surface Water
Smith Mill Creek 1
NS
NS
NS
NS
2.2
NS
NS
NS
NS
NS
NS
1.6
NS
NS
NS
1.6
NS
NS
1.1
NS
Smith Mill Creek 2
NS
NS
NS
NS
1.7
NS
NS
NS
NSNNS
NS
2.0
NS
NS
NS
5.5
NS
NS
1.1
NS
Smith Mill Creek 3
NS
NS
NS
NS
1.7
NS
NS
NS
NS
NS
2.2
NS
NS
NS
1.6
NS
NS
1.1
NS
Smith Mill Creek 4
NS
NS
NS
NS
1A
NS
NS
NS
NS
NS
Is
NS
NS
NS
1.7
NS
NS
ND
NS
Smith Mill Creek 5
NS
NS
NS
NS
1.6
NS
NS
NS
NS
NS
2.5
NS
NS
NS
1.6
NS
NS
1.0
NS
Smith Miff Creek 6
NS
NS
NS
NS
1.6
NS
NS
NS
NS
NS
1.1
NS
NS
NS
1.6
NS
NS
1.1
NS
Bear Creek 1
NS
NS
NS
NS
1.2
NS
NS
NS
NS
NS
ND
NS
NS
NS
3.2
2.3
NS
ND
NS
Bear Creek 2
NS
NS
NS
NS
1.5
NS
NS
NS
NS
NS
6.4
NS
NS
NS
1.8
NS
NS
ND
NS
Bear Creek 3
NS
NS
NS
NS
1.6
NS
NS
NS
NS
NS
NS
1.7
NS
NS
NS
1.7
NS
NS
ND
NS
Bear Creek 4
NS
NS
NS
NS
1.6
NS
NS
NS
NS
NS
NS
1.5
NS
NS
NS
2.0
NS
NS
ND
NS
Bear Creek 5
NS
NS
NS
NS
1.8
NS
NS
NS
NS
NS
NS
1.2
NS
NS
NS
2.0
NS
NS
NS
NS
Jehovah Witness 1
NS
NS
NS
NS
8.7
NS
NS
NS
NS
NS
NS
1.7
NS
NS
NS
2.1
2.5
NS
ND
NS
Cecil's S rin 1
NS
NS
NS
NS
3.2
NS
NS
NS
NS
NS
NS
5.2
NS
NS
NS
1.9
NS
NS
3.0
NS
Cecil's Spring 2
NS
NS
NS
NS
1.6
NS
NS
NS
NS
NS
NS
1.6
NS
NS
NS
2.4
NS
NS
1.3
NS
Notes:
Analyses performed by SM 5310B. J-flagged (estimated) results if any are included on this table but are not identified (see the lab report).
Units in rn R or parts per million (ppm)
I - milk solution injected into this well.
E - laboratory error due to contaminated containers, no data available.
C = data has been corrected from a labortary error, result is an estimate only.
ND = not detected at concentrations exceeding the laboratory reporting limit.
NS = not sampled. Not on sampling matrix or sampling personnel oversight or broken bottle.
NP - not present; monitoring well was abandoned or destroyed.
AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
P = TOC concentration is the result of several dead opossums removed from the well.
** These wells were destroyed by grading during 2003.
Recovery/Injection well samples are grab samples collected via bailer.
Prepared by: AWA
Table 4 TOC (2014) of T4 2014 TOC Historical Database.xlsx Checked by: RAD/TJB

Table 5 -- May 2014 [Baseline]
Laboratory Analytical Results of Groundwater & Surface Water Samples
Selected Chlorinated VOCs Only
Andrex Industries
Asheville, North Carolina
NCDENR Groundwater Incident Number 6586
BLE Project No. J14-1022-38
v
d
Q
V1
w
a
a�
H
w
H
U
>
a
A
p
«
q
O
0
S
a�
cad
p
q
o0
°
Fi
Q
H
w
Q
W
O
NC 2L
0.7
3
70
0.03
200
0.6
7
0.4
100
1 70
2,000
0.6
1 50
1 6
0.2
NE
Groundwater
AB
MW-1
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-3
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
MW-5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
5/14/2014
MW-6
1,920
94.7
ND
ND
ND
ND
ND
ND
ND
1,000
ND
ND
ND
ND
ND
3,015
NS
MW-7
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
AB
MW-8
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-8A
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
MW-9
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-11
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-12
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-13
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-14
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-15
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-16
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-17
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-18
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NP**
MW-19
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NS
MW-20
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-21
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-22
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-23
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-24
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NP**
MW-25
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NS
MW-26
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
5/14/2014
MW-44
3,000
170
ND
23.6
ND
ND
0.85
ND
4.9
670
ND
ND
0.9
ND
0.80
3,871
5/14/2014
IW-2
70.4
19.8
ND
16.7
ND
ND
ND
0.15
5.0
198
ND
ND
0.37
ND
ND
310
5/14/2014
RW-1
225
373
ND
23.1
ND
ND
ND
ND
7.9
2,380
ND
ND
ND
ND
ND
3,009
AB
RW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
RW-3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
AB
RW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
RW-5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
RW-6
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
RW-7
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NC 2B 0.7 2.5 NE 0.025 NE NE NE NE NE NE I NE I NE 1488 1488 1 NE I NE
Surface Water
NS
Smith Mill Creek 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 4
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 6
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
5/14/2014
Bear Creek 1
59.9
7.5
ND
ND
ND
ND
ND
ND
ND
27.6
ND
ND
ND
ND
ND
95
NS
Bear Creek 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 4
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
5/14/2014
Jehovah Witness 1
2.3
ND
ND
ND
ND
ND
ND
ND
ND
0.51
ND
j ND
ND
ND
ND
2.8
NS
Cecil's Spring 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Cecil's Spring 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Notes:
Analyses performed by EPA Method 8260 MSV Low Level. J-flagged (estimated) results are included on this table but are not identified (see the lab report).
Units in µg/l or parts per billion (ppb)
Detected concentrations of petroleum hydrocarbon VOCs (if any) are NOT shown in this table (not part of the Andrex groundwater incident).
Detected concentrations of acetone, chloromethane, and methylene chloride (if any) are NOT shown in this table (probable laboratory contaminants).
Detected concentrations of 2-Butanone (MEK), Toluene, and 2-Hexanone (if any) are NOT shown in this table (metabolic products of bioremedation).
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1, 2013.
NC2B = North Carolina Surface Water Standards [WS - Water Supply Classification] under Title 15A Subchapter 2B in µg/1 dated May 1, 2007.
ND = not detected at concentrations exceeding the laboratory reporting limit.
NS = not sampled.
NP = not present; monitoring well was abandoned or destroyed.
AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
* Compounds intermittently detected in the past.
** These wells were destroyed by grading during 2003.
Recovery & injection well samples are grab samples collected via bailer.
Prepared by: AWA
Table 5 (May 2014) of T5 to T8 Andrex IER 2014.xlsx Checked by: TJB

Table 6 -- July 2014 [30 Day]
Laboratory Analytical Results of Groundwater & Surface Water Samples
Selected Chlorinated VOCs Only
Andrex Industries
Asheville, North Carolina
NCDENR Groundwater Incident Number 6586
BLE Project No. J14-1022-38
v
d
Q
V1
w
a
a�
H
w
H
U
>
a
A
p
«
q
O
0
S
a�
cad
p
q
o0
°
Fi
Q
H
w
Q
W
O
NC 2L
0.7
3
70
0.03
200
0.6
7
0.4
100
1 70
2,000
0.6
1 50
1 6
0.2
NE
Groundwater
AB
MW-1
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-3
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
MW-5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
7/2/2014
MW-6
2,110
80.6
ND
ND
ND
ND
ND
ND
ND
1,260
ND
ND
ND
ND
ND
3,451
NS
MW-7
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
AB
MW-8
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-8A
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
MW-9
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
j NS
NS
MW-10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-11
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-12
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-13
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-14
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-15
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-16
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-17
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-18
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NP**
MW-19
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NS
MW-20
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-21
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-22
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-23
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-24
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NP**
MW-25
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NS
MW-26
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
7/2/2014
MW-44
4,260
167
ND
24.2
ND
ND
ND
ND
5.5
825
ND
ND
ND
ND
1.3
5,283
7/2/2014
IW-2
ND
ND
8.2
ND
ND
ND
ND
ND
ND
25.2
ND
ND
ND
ND
ND
33
7/2/2014
RW-1
43.4
29.5
ND
43.9
ND
ND
ND
ND
ND
3,130
ND
ND
ND
ND
ND
3,247
AB
RW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
RW-3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
AB
RW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
RW-5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
RW-6
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
RW-7
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
I NS
NS
NS
NS
NC 2B 0.7 2.5 NE 0.025 NE NE NE NE NE NE I NE I NE 1488 1488 1 NE I NE
Surface Water
NS
Smith Mill Creek 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 4
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 6
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 4
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Jehovah Witness 1
NS
NS
NS
NS
NS
JNS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Cecil's Spring 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Cecil's Spring 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Notes:
Analyses performed by EPA Method 8260 MSV Low Level. J-flagged (estimated) results are included on this table but are not identified (see the lab report).
Units in µg/l or parts per billion (ppb)
Detected concentrations of petroleum hydrocarbon VOCs (if any) are NOT shown in this table (not part of the Andrex groundwater incident).
Detected concentrations of acetone, chloromethane, and methylene chloride (if any) are NOT shown in this table (probable laboratory contaminants).
Detected concentrations of 2-Butanone (MEK), Toluene, and 2-Hexanone (if any) are NOT shown in this table (metabolic products of bioremedation).
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1, 2013.
NC2B = North Carolina Surface Water Standards [WS - Water Supply Classification] under Title 15A Subchapter 2B in µg/1 dated May 1, 2007.
ND = not detected at concentrations exceeding the laboratory reporting limit.
NS = not sampled.
NP = not present; monitoring well was abandoned or destroyed.
AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
* Compounds intermittently detected in the past.
** These wells were destroyed by grading during 2003.
Recovery & injection well samples are grab samples collected via bailer.
Prepared by: AWA
Table 6 (July 2014) of T5 to T8 Andrex IER 2014.xlsx Checked by: TJB

Table 7 -- September 2014 [90 Day & Annual Event]
Laboratory Analytical Results of Groundwater & Surface Water Samples
Selected Chlorinated VOCs Only
Andrex Industries
Asheville, North Carolina
NCDENR Groundwater Incident Number 6586
BLE Project No. J14-1022-38
v
d
Q
V1
w
a
a�
H
w
H
U
>
a
A
p
«
q
O
0
S
a�
a
cad
p
q
o0
°
Fi12
Q
H
w
Q
W
O
NC 2L
0.7
3
70
0.03
200
0.6
7
0.4
100
1 70
2,000
0.6
1 50
1 6
0.2
NE
Groundwater
AB
MW-1
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-3
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
9/4/2014
MW-5
2,200
160
ND
53
ND
ND
ND
ND
5.2
350
ND
ND
ND
ND
ND
2,768
9/4/2014
MW-6
2,400
95
ND
5.5
ND
ND
1.0
ND
3.2
1,200
ND
ND
ND
ND
ND
3,705
9/4/2014
MW-7
110
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
110
AB
MW-8
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-8A
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
9/4/2014
MW-9
2,100
140
ND
16
ND
ND
ND
ND
3.0
660
ND
ND
ND
ND
ND
2,919
9/4/2014
MW-10
360
32
ND
35
ND
ND
ND
ND
1.0
110
ND
ND
ND
ND
ND
538
9/4/2014
MW-11
860
55
ND
9.9
ND
ND
ND
ND
1.3
260
ND
ND
ND
ND
ND
19186
9/4/2014
MW-12
1.6
ND
ND
9.6
ND
ND
ND
ND
10
18
ND
ND
ND
ND
ND
39
9/3/2014
MW-13
1,300
160
ND
ND
ND
ND
ND
ND
6.8
170
ND
ND
ND
ND
ND
1,637
9/3/2014
MW-14
790
350
ND
ND
ND
ND
1.0
ND
ND
140
ND
ND
ND
ND
ND
1,281
9/3/2014
MW-15
82
2.3
ND
ND
ND
ND
ND
ND
ND
4.2
ND
ND
ND
ND
ND
89
9/3/2014
MW-16
130
3.3
ND
ND
ND
ND
ND
ND
ND
6.0
ND
ND
ND
ND
ND
139
9/3/2014
MW-17
5.5
2.9
ND
4.1
ND
ND
ND
ND
ND
8.8
ND
ND
ND
ND
ND
21
9/3/2014
MW-18
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NP**
MW-19
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
9/3/2014
MW-20
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/2/2013
MW-21
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/2/2013
MW-22
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/3/2014
MW-23
110
4.2
ND
ND
ND
ND
ND
ND
ND
9.3
ND
ND
ND
ND
ND
124
9/3/2014
MW-24
270
2.0
ND
ND
ND
ND
ND
ND
ND
4.4
ND
ND
ND
ND
ND
276
NP**
MW-25
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
9/3/2014
MW-26
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/4/2014
MW-44
4,300
230
ND
36
ND
ND
ND
ND
6.7
870
ND
ND
1.2
ND
1 1.3
5,445
9/4/2014
IW-2
9.2
1.4
ND
1.9
ND
ND
ND
ND
ND
55
ND
ND
ND
ND
ND
68
9/4/2014
RW-1
12
18
ND
41
ND
ND
1.8
ND
9.2
2,800
ND
ND
ND
ND
ND
2,882
AB
RW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
9/4/2014
RW-3
1.6
ND
ND
47
ND
ND
ND
ND
5.7
170
ND
ND
ND
ND
ND
224
AB
RW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
9/4/2014
RW-5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/4/2014
RW-6
36
30
ND
120
ND
ND
2.0
ND
4.1
540
ND
ND
ND
ND
ND
732
9/4/2014
RW-7
33
36
ND
8.7
ND
ND
ND
ND
ND
620
1 ND
ND
ND
ND
ND
698
NC 2B 0.7 2.5 NE 0.025 NE NE NE NE NE NE I NE I NE 1488 1488 1 NE I NE
Surface Water
9/5/2014
Smith Mill Creek 1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/5/2014
Smith Mill Creek 2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/5/2014
Smith Mill Creek 3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/5/2014
Smith Mill Creek 4
1.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.4
9/5/2014
Smith Mill Creek 5
1.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
9/5/2014
Smith Mill Creek 6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/5/2014
Bear Creek 1
12
1.6
ND
ND
ND
ND
ND
ND
ND
5.1
ND
ND
ND
ND
ND
19
9/5/2014
Bear Creek 2
11
1.9
ND
ND
ND
ND
ND
ND
ND
4.2
ND
ND
ND
ND
ND
17
9/5/2014
Bear Creek 3
3.3
ND
ND
ND
ND
ND
ND
ND
ND
2.0
ND
ND
ND
ND
ND
5.3
9/5/2014
Bear Creek 4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/5/2014
Bear Creek 5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/5/2014
Jehovah Witness 1
4.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.4
9/5/2014
Cecil's Spring 1
8.9
ND
ND
ND
ND
ND
ND
ND
ND
2.6
ND
ND
ND
ND
ND
12
9/5/2014
Cecil's Spring 2
3.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.6
Notes:
Analyses performed by EPA Method 8260 MSV Low Level. J-flagged (estimated) results are included on this table but are not identified (see the lab report).
Units in µg/l or parts per billion (ppb)
Detected concentrations of petroleum hydrocarbon VOCs (if any) are NOT shown in this table (not part of the Andrex groundwater incident).
Detected concentrations of acetone, chloromethane, and methylene chloride (if any) are NOT shown in this table (probable laboratory contaminants).
Detected concentrations of 2-Butanone (MEK), Toluene, and 2-Hexanone (if any) are NOT shown in this table (metabolic products of bioremedation).
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1, 2013.
NC2B = North Carolina Surface Water Standards [WS - Water Supply Classification] under Title 15A Subchapter 2B in µg/1 dated May 1, 2007.
ND = not detected at concentrations exceeding the laboratory reporting limit.
NS = not sampled.
NP = not present; monitoring well was abandoned or destroyed.
AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
* Compounds intermittently detected in the past.
** These wells were destroyed by grading during 2003.
Recovery & injection well samples are grab samples collected via bailer.
Prepared by: AWA
Table 7 (Sept 2014) of T5 to T8 Andrex IER 2014.xlsx Checked by: RAD

Table 8 -- November 2014 [150 Day]
Laboratory Analytical Results of Groundwater & Surface Water Samples
Selected Chlorinated VOCs Only
Andrex Industries
Asheville, North Carolina
NCDENR Groundwater Incident Number 6586
BLE Project No. J14-1022-38
v
d
Q
V1
w
a
a�
H
w
H
U
>
a
A
p
«
q
O
0
S
a�
a
cad
p
q
o0
°
Fi12
Q
H
w
Q
W
O
NC 2L
0.7
3
70
0.03
200
0.6
7
0.4
100
1 70
2,000
0.6
1 50
1 6
0.2
NE
Groundwater
AB
MW-1
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-3
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
MW-5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
(1/18/2014
MW-6
1,400
76
ND
12
ND
ND
1.5
ND
3.8
1,300
ND
ND
ND
ND
ND
2,793
NS
MW-7
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
AB
MW-8
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
MW-8A
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
MW-9
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-11
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-12
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-13
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-14
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-15
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-16
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-17
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-18
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NP**
MW-19
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NS
MW-20
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-21
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-22
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-23
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
MW-24
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NP**
MW-25
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NP
NS
MW-26
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
11/18/2014
MW-44
5,000
180
ND
48
ND
ND
ND
ND
5.5
1,100
ND
ND
ND
ND
ND
6,334
11/18/2014
IW-2
10
2.5
ND
2.9
ND
ND
ND
ND
1.1
180
ND
ND
ND
ND
ND
197
11/18/2014
RW-1
3.5
6.7
ND
77
ND
ND
1.7
ND
12
3,300
ND
ND
ND
ND
ND
3,401
AB
RW-2
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
RW-3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
j NS
NS
AB
RW-4
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
AB
NS
RW-5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
RW-6
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
RW-7
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NC 2B 0.7 2.5 NE 0.025 1 NE NE NE NE NE NE I NE I NE 1488 1488 1 NE I NE
Surface Water
NS
Smith Mill Creek 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 4
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Smith Mill Creek 6
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 3
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 4
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Bear Creek 5
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Jehovah Witness 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Cecil's Spring 1
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Cecil's Spring 2
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
Notes:
Analyses performed by EPA Method 8260 MSV Low Level. J-flagged (estimated) results are included on this table but are not identified (see the lab report).
Units in µg/l or parts per billion (ppb)
Detected concentrations of petroleum hydrocarbon VOCs (if any) are NOT shown in this table (not part of the Andrex groundwater incident).
Detected concentrations of acetone, chloromethane, and methylene chloride (if any) are NOT shown in this table (probable laboratory contaminants).
Detected concentrations of 2-Butanone (MEK), Toluene, and 2-Hexanone (if any) are NOT shown in this table (metabolic products of bioremedation).
NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1, 2013.
NC2B = North Carolina Surface Water Standards [WS - Water Supply Classification] under Title 15A Subchapter 2B in µg/1 dated May 1, 2007.
ND = not detected at concentrations exceeding the laboratory reporting limit.
NS = not sampled.
NP = not present; monitoring well was abandoned or destroyed.
AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008.
* Compounds intermittently detected in the past.
** These wells were destroyed by grading during 2003.
Recovery & injection well samples are grab samples collected via bailer.
Prepared by: AWA
Table 8 (November 2014) of T5 to T8 Andrex IER 2014.xlsx Checked by: TJB

FIGURES

- al

0 0 0 �o
a) o ,�K �y'`
O N ti
N
CECIL'S OLLEGE 2113.356
1` ma's spFw !_
W-15
��` �'• �� 2113.54
� l
s'G MW-18
RESIDENTIAL�� 2092.65
�� RESIDENTIAL N / �� / TWENTIETH STREET
RESIDENTIAL
BEAR CREEK ROAD
RESIDENTIAL
�HAMILTON1
PROPERTY
1<0
STREET �m=�
McpADE / i •�..
r I
�•• MALVERN HILLS I POOL-�
�� � = ��•����^4-'_-•� ® PARK
TENNIS I
COURTS I
iw PLACE
RESIDENTIAL
RESIDENTIAL
REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA
FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS.
REVISIONS
No. DESCRIPTION BY
O
(1)
O
N
DRAWN:
ACE
CHECKED: AWA
APPROVED:
BLNA
®
ENS
RESIDENTIAL
RESIDENTI
coo o
N O i
N �
N o;
0 0 o j ti
o _ .�
�'pwN �2178.?0 Q 1
N N z�80 z�O 2
/ RESI NTIAL
f '/ 1 -.000
PERFEC
_NC.
5.?5
kRnW3
Ili TI M l
ink
M 91.9711 I N
§
MW-25
"1167.80
NP-D
MW-6
2165.38
—
RW-1
'
MILKCO,
I 2165.29
MW-3
�
MW-44�
M NP-A
2158.67
-2
MW-"A*
NP-A
II
NP-A
Af�DRE I
IES, INC
MW-9
I
MW-4*
2150.45
NP—A
MW-8*
GEAR, INC.
NP-A
RW-4
I NP-A
�\
RW-5
MW-10
\ II 2144.44
2143.71
RW-6
MW-11
\\
2142.77
2140.83
ICE®�� \\�
VICE
STORE_ - **
.14.
OTM O
cm
N vm
N
�:i�yil»illr_im
DATE: 03-04-15
CAD FILE: IER 1022-38 GWEM
JOB NO: J14-1022-38
MW-14* It
SILVERS 2138.90 RW-7
MW-13 2141.03
�\ PROPERTY 2136.38 PRILVERS
i ECHOLS
NG \PROPERTY\
:Y
M JUSTICE \ 'N.
i PROPERTY - \
RESIDEN�IA�
N
�O
MW-20
2145.77
Pq TT
q 14�_"pf
A
%•
C P. /
r'
�11 O
YN FE C P. 1�
\N
RESIDENTIAL
_J ®• \
® -
ROY D. ARMER-10 1
PAR •'\ L---J
MW-23-
2117.65 I MW-21 RASH ROAD
\ 1 I i 2089.59
Of mw-22
2089.94
w J \ I I •\.
� IMW-17
12090.55 Rml= \
w NpRF \ J OVAL►,
°�K
sou TNE — — WI NESS� BIESTE F DL yys�o
glLRpgD PR PERTY , PROPERTY
RMER
M 19 W ER WELL
NP-D
S N � •�''��
PROP - RYDERMA
OPERTY
SATTERFIELD \ \ �
OPERTY OUSE
jf 0 �O
O N
RESIDENTIAL 0
)► /�"y0F q �F"UF O
LLJ
rV O
RESIDENTIAL
HAINES
ors
O
NOTES:
1. THE GROUNDWATER PUMP AND TREAT SYSTEMS HAD BEEN
REMOVED AND WERE NOT IN OPERATION AT THE TIME WATER
LEVEL MEASUREMENTS WERE TAKEN. GROUNDWATER WAS NOT
BEING PUMPED FROM RW-1 THROUGH RW-7 WHILE
MEASUREMENTS WERE COLLECTED.
2. ** SKY LANES BOWLING CENTER
NCDEH - PUBLIC WATER SYSTEM ID #10-11-025
WELL NAME: WELL #1
AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED
"...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER."
BUNNELL"IIIMONB MONEERNO, NC.
NIL
6004 PONDERS COURT
INC.TH CAROLINA 2961E PHONE: (864)288 i125 FAX: [phone]
i
t�0-r'.t
1475 cr
:ap QFo�oa`�.P�a;
2090
2080
LEGEND
APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR
SHALLOW BEDROCK) GROUNDWATER MONITORING WELL ••�
O APPROXIMATE LOCATION OF EXISTING (TYPE III -BEDROCK) ••\
GROUNDWATER MONITORING WELL
RECOVERY WELL OR INJECTION WELL
O WATER SUPPLY WELL
- - �•' - BELOW GROUND STREAM SHOWING FLOW DIRECTION
a • - • • �— ABOVE GROUND STREAM SHOWING FLOW DIRECTION
- - PROPERTY LINE
2140.83 WATER LEVEL IN FEET ABOVE MEAN SEA LEVEL
* GROUNDWATER ELEVATION IN WELL MW-14 IS TYPICALLY ARTESIAN
AND REPRESENTS THE POTENTIOMETRIC SURFACE OF THE DEEPER
ROCK AQUIFER AND WAS NOT CONSIDERED FOR CONTOURING PURPOSES.
NP-A NOT PRESENT. WELL HAS BEEN ABANDONED.
NP-D MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO
BE DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE.
MW-25 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO
BE DESTROYED BY GRADING PERFORMED BY MILKO, INC.
APPROXIMATE DIRECTION OF GROUNDWATER FLOW
�MM APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE
2120 EQUIPOTENTIAL CONTOUR LINE
200 100 0 200 400
APPROXIMATE SCALE IN FEET
GROUNDWATER ELEVATION CONTOUR MAP - SEPTEMBER 2, 2014
ANDREX INDUSTRIES
DEAVERVIEW ROAD
ASHEVILLE, NORTH CAROLINA
FIGURE NO.
2

RESIDENTIAL
RESIDENTIAL
0000
_ � � � I
� HQ � MW-26
�
IND
XFER CECICS LEGE RESIDENTIAL �sill Q5
EOCS SPRING 12MW-16� MW-15*r0139 189 � SO � �
MW-18 �� / 100 \ HAYNES CORP. J�
NO '�' WLKC HAYNES CORP
TH STREET - MW-24_2
TWEN rO o 276 AB ` y
0 CPA224 4.,E
P IC SERVIC _ MW-12 ---- - - MW 1 /
CO. NC
RESIDE AL 2,685 39 AB
is IW-12 IW-2
� o���E MW056* 68 IW-1 IW-4
cR�� MW-25R MW-25 — - — .
gEP NP RW-1 \�
\ 2,882 O IW-3
M MW 3 7 YNE\ CORP. \
MILKCO, O A 1 1
�oP
MW-44 O Q N G . 5,445
- RW-2 ' M 4 SO ` �•
_ - - AB AB j
\ 8R\ ,919 MWB8 ` RESIDENTIAL
r I _
tr ' MW - - SM-1
PEREE ION GEAR, INC. 0 �jRW-4�IW-6 A F I
1----� 1 ND
'HAMILTON I AB ANDRE,- 1� L _ _ L
M _ �� s
o PROPERTY \� III— DUSTRIES, INll ,, D MW-23 SMD 2 � Z
s -
\CO
0\ I I I ND RW-5 IW-8 - - - - -124_ - ' , - I MW-17
M I �0 IW4 1 � _ _ -
Z 21
vQ RASH ROAD
-------------------- _ R O Y D. E A EN BAR I SM -3
BLOOMING - R= MW� 11�� 1 \ I ND_ MW-21
ARDENS MW 13 - , 86� -
1,637 I ND
ICE 90� RW-7 -�
+ RV ORE i , -- — 698 I J _ _•\� MW -22
1�!
w 0000
�
RESIDENTIAL i �
X 0000 IBC-2 RESIDENT]
z ��� 17
_40000� STREsommillsoll
ET
McDADE
40000
s % i •.
swoop-400150_.._
MALVERN HILLS P 113C-3 -�
5.3 _ J
131IND
v.
TENNIS AND
posp
COURTS I — � � �
_J �
/. — — — � 0000
RUMBOUGH PLACE
w
BC-5 Lj � RESIDENTIAL
INS / ' Q Li
z
Q
cn CL
Q MIDDLEM)NT AVENUE
RESIDENTIAL
JV44FORMER JEHOVA\I 1\
SILVERS 600 100 SEXT !so WITNESS PROPERTY\.`BIESTERFEDLT
E BOWLING PROPERTY M MWZ 14* RTYj 19 NORFO so — PROPERTY NP
�K pry SM 4
eE PROPERTY 10 ,�R q1.4 \:
BC-1 M I p FORMER oqo SM.0
L-
19 �� / RESIDENTIAL \ SATTERITELD _ WATER WELL
- _ _ CRYDERMAN SI
� � � �� � � � �, PRE R� _ HOUSE - - PROPERTY
of '_ �� \ a �ND� \� _
P \ �
u ftnuft �sposs. so-
Oho swoop \ P\ V)V) -
RESIDENTIAL
MW -20 r Q
GR NO a �VENHOF n
RESIDENTIAL
RESIDENTIAL
DRIVE
LEGEND
I z v NOTES: PROPOSED INJECTION WELL (IW-1 AND IW-3 THROUGH IW-12)
1. LABORATORY ANALYSIS BY EPA METHOD 8260.
z 2. WELLS AND SURFACE WATER WAS SAMPLED ON SEPTEMBER 2-5, 2014. �� PROPOSED MONITORING WELL (MW-3R, MW-8R, AND MW-25R)
3. CONCENTRATIONS DETECTED IN MW-21 ARE PRIMARILY CHLOROFORM,
PROBABLY RELATED TO LEAKING WATER SUPPLY LINES IN CLOSE APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR SHALLOW
PROXIMITY TO THE WELLS. BEDROCK) GROUNDWATER MONITORING WELL
4. SAMPLES FROM STREAMS DESIGNATED AS FOLLOWS:
SM = SMITH MILL CREEK TRIBUTARY 0 APPROXIMATE LOCATION OF EXISTING (TYPE III -BEDROCK)
CS = CECIL'S SPRING GROUNDWATER MONITORING WELL
BC = BEAR CREEK
JW = FORMER JEHOVAH WITNESS PROPERTY 0 RECOVERY WELL
5. NP = NOT PRESENT, WELL WAS NOT PRESENT AT TIME OF SAMPLING. APPROXIMATE LOCATION OF SURFACE WATER SAMPLES (SEE NOTE 4)
CAAp���:� 6. ** SKY LANES BOWLING CENTER v (WATER SAMPLES COLLECTED 9-5-14).
�• �� ENS ,� NCDEH -PUBLIC WATER SYSTEM ID #10-11-025
WELL NAME: WELL #1 O WATER SUPPLY WELL
AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED
$ = "...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER."
1475 162 CONCENTRATION OF TOTAL DETECTED CHLORINATED VOLATILE ORGANIC
G g;QWd 7. * THE WELLS MAY INTERCEPT FRACTURE SETS OR MAY BE SCREENED AT COMPOUNDS IN PARTS PER BILLION
:� FOLOa�•'�'�',� ELEVATIONS AT WHICH GROUNDWATER CONTAMINANT CONCENTRATIONS ARE
�,''�'��r/,►w'►��,`� `,``` CONTOURING
INCONSISTENT
ONSISENT WITH
PURPOSES.
ESTABLISHED PLUME. THE VALUES WERE IGNORED FOR BELOW GROUND STREAM SHOWING FLOW DIRECTION
8. THE FORMER WATER SUPPLY WELL ON THE CRYDERMAN PROPERTY APPEARED
TO BE ABANDONED AND COULD NOT BE SAMPLED AS OF OCTOBER 2005. ABOVE GROUND STREAM SHOWING FLOW DIRECTION
9. MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE PROPERTY LINE
DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE. MW-25 WAS
NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE
GRADING PERFORMED BY MILKO, INC.
10. RECOVERY WELLS WERE NOT OPERATIONAL AT THE TIME OF SAMPLING. 100 TOTAL CHLORINATED CONCENTRATION CONTOUR IN PARTS PER BILLION
REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA 200 100 0 200 400
FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. 11. AB =WELL ABANDONED IN 2008 PER APPROVED BROWNFIELD REDEVELOPMENT PLAN. — Np ESTIMATED LIMIT OF VOC'S
APPROXIMATE SCALE IN FEET
REVISIONS
No. DESCRIPTION BY
DRAWN:
ACE
CHECKED: AWA
APPROVED:
DATE: 03-04-15
CAD FILE:
IER 1022-38 PLUME
JOB NO: J14-1022-38
BUNNELL-LAMMONS ENGINEERING, INC.
NIL
6004 PONDERS COURT
INC. PHONE: (64I)288 1 65 FAX: [phone]
CONTOUR MAP OF TOTAL CHLORINATED VOLATILE ORGANIC COMPOUND ISOCONCENTRATIONS - SEPTEMBER 2-5, 2014
WITH PROPOSED INJECTION WELL PLAN FOR 2015
ANDREX INDUSTRIES
ASHEVILLE, NORTH CAROLINA
FIGURE NO.
3

2245 -
2235
2225 -
2215
2205 -
2195
2185 -
J
Cf�
2175
~ 2165 -
LL
Z 2155
2145 -
W
w 2135
2125 -
2115
2105 -
2095
2085 -
2075
2065 -
2055 -
2225 -
2215
2205 -
2195
2185 -
2175
2165 -
2155
C%) 2145 -
2135
z 2125 -
0
~ 2115
Q
W
2105 -
W
2095
2085 -
2075
2065 -
2055
2045 -
2035
2025 -
MW
AB
ml
nji
II I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I r-7-7-7 I I
0 200 400 600 800 1000 1200 1400 1600 1800
DISTANCE, FT.
GEOLOGIC PROFILE A -A'
1 SOUT
2245
2235
2225
2215
2205
2195
2185
C/)
2175
2165 ~
LL
2155 z
0
2145
W
2135 LLJ
2125
2115
2105
2095
2085
2075
2065
2055
LEGEND
APPROXIMATE POTENTIOMETRIC SURFACE ON 9-2-2014
GROUND SURFACE
APPROXIMATE LOCATION OF BEDROCK ENCOUNTERED IN BORINGS
GROUNDWATER FLOW DIRECTION
76 SCREENED OR OPEN BEDROCK INTERVAL WITH CONCENTRATION OF TOTAL CHLORINATED
VOLATILE ORGANICS IN ug/I ON 9/2-4/2014
AB WELL WAS ABANDONED
0
_ VERTICAL EXAGGERATION = 1OX
N
SCALE 11nch
200 Feet
INJECTION ZONE
CAA
S
1475 NOTE:
INJECTION WELLS IW-1, IW-3, IW-4, IW-5, IW-7, AND IW-11 ARE PROPOSED. ACTUAL CONSTRUCTION TO
;y4 C'ttOL056G;•'.�►� BE DETERMINED IN THE FIELD.
INJECTION WELLS IW-1 AND IW-3 ARE PROPOSED FOR INSTALLATION IN 2015
2225
2215
2205
2195
2185
2175
- 2165
2155
- 2145 C�
2135
Li
- 2125 Z
O
2115 ~
Q
I
- 2105
W
2095
2085
2075
2065
2055
- 2045
2035
2025
0
0 200 400 600 800 1000 1200 1400 1600 1800 2000 2200 2400 2600 2800 3000 3200 3400 3600 3800 PROFILE LOCATI ON PLAN
DISTANCE, FT.
GEOLOGIC PROFILE 13-13'
REVISIONS DRAWN: DATE: 03-04-15 FIGURE NO.
No. DESCRIPTION BY ACE BUNNELL—LAMMONS ENGINEERING, INC. HYDROGEOLOGIC PROFILES OF THE AFFECTED AREA FOR THE 2014 IER
CHECKED: CAD FILE: PONDERS6004 ANDREX INDUSTRIES
AWA IER 1022-38 PROFILE GREENVILLE, SOUTHAROLINA 29615 DEAVERVIEW ROAD 4
APPROVED: JOB NO: IRLIEINC. PHONE: [phone] FAX: [phone] ASHEVILLE, NORTH CAROLINA
J14-1022-38

APPENDICES

APPENDIX A
WELL LOGS

WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
For Internal Use ONLY:
1. Well Contractor Information:
Brunson L. King
Well Contractor Name
3290-A
NC Well Contractor Certification Number
Landprobe, LLC
Company Name
2. Well Construction Permit #: U I C #W 10100106
List all applicable well permits (i.e. County, State, Variance, Injection, etc)
3. Well Use (check well use):
Water Supply Well:
❑Agricultural
❑Geothermal (Heating/Cooling Supply)
❑ Industrial/Commercial
❑ Irrigation
Non -Water Supply Well:
El Aquifer Recharge
El Aquifer Storage and Recovery
El Aquifer Test
❑Experimental Technology
El Geothermal (Closed Loop)
El Geothermal (Heating/Cooling
❑Municipal/Public
❑Residential Water Supply (single)
❑Residential Water Supply (shared)
©Groundwater Remediation
El Salinity Barrier
❑ Stormwater Drainage
El Subsidence Control
❑Tracer
El Other (explain under #21 1
4. Date Well(s) Completed: 4-9-14 Well ID# IW-2
5a. Well Location:
Milkco, Inc. (Former Andrex) #07022-03-11
Facility/Owner Name Facility ID# (if applicable)
180 Deaverview Road, Asheville, NC 28806
Physical Address, City, and Zip
Buncombe 9667
County Parcel Identification No. (PIN)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
35.57990 N 82.61396 W
6. Is (are) the well(s): ❑+Permanent or ❑Temporary
7. Is this a repair to an existing well: ❑Yes or E]No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: One
For multiple injection or non -water supply wells ONLY with the same construction, you can
submit one form.
9. Total well depth below land surface: 84 (ft.)
For multiple wells list all depths if different (example- 3@200' and 2@100')
10. Static water level below top of casing: 56 (ft.)
If water level is above casing, use "+ "
11. Borehole diameter: 10 (in.)
12. Well construction method: air hammer
(i.e. auger, rotary, cable, direct push, etc.)
14. WATER ZONES
FROM
TO
DESCRIPTION
70 rt.
73 rt.
water bearing fractures
rt.
rt.
15. OUTER CASING for multi -cased wells OR LINER if a licable
FROM
TO
DIAMETER
THICKNESS
MATERIAL
0 ft-
64 ft.
6 in
Sch 40
PVC
16. INNER CASING OR TUBING(geothermal closed -loop)
FROM
TO
DIAMETER
THICKNESS
MATERIAL
ft.
ft.
in.
rL
rt
in.
17. SCREEN
FROM
TO
DIAMETER
SLOT SIZE
THICKNESS
MATERIAL
rt
ft.
in.
ft.
ft,
in.
18. GROUT
FROM
TO
MATERIAL
EMPLACEMENT METHOD & AMOUNT
0 rt.
2 rt.
cement
gravity -- 1 bag
2 ft.
64 ft.
bentonite
gravity -- 13 bags
rt.
rt.
19. SAND/GRAVEL PACK (if applicable)
FROM
TO
MATERIAL
EMPLACEMENT METHOD
64 fL
84 ft
#3 stone
gravity
rt.
rt.
20. DRILLING LOG attach additional sheets if necessary)
FROM
TO
DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
0 rL
25 ft.
red-brn f-m sandy SILT (fill)
25 rL
35 rt.
red-brn silty f-m SAND (residuum)
35 ft.
64 ft.
brown silty f-m SAND (PWR)
64 ft
84 rt.
gray-brn f-m SAND (bedrock)
rt.
ft.
ft.
ft.
rL
ft.
21. REMARKS
Well construction per UIC permit
22. Certification:
4�3167
Signature of Certified Well Contractor
5-8-14
UULU
By signing this form, I hereby certify that the wells) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Iniection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636
13a. Yield m Method of test: 24c. For Water Supply & Injection Wells:
(gP ) Also submit one copy of this form within 30 days of completion of
13b. Disinfection type: Amount: well construction to the county health department of the countywhere
constructed.
Form GW-1 North Carolina Department of Environment and Natural Resources - Division of Water Resources Revised August 2013

WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
For Internal Use ONLY:
1. Well Contractor Information:
Brunson L. King
Well Contractor Name
3290-A
NC Well Contractor Certification Number
Landprobe, LLC
Company Name
2. Well Construction Permit #: U I C #W 10100106
List all applicable well permits (i.e. County, State, Variance, Injection, etc)
3. Well Use (check well use):
Water Supply Well:
❑Agricultural
❑Geothermal (Heating/Cooling Supply)
❑ Industrial/Commercial
❑ Irrigation
Non -Water Supply Well:
El Aquifer Recharge
El Aquifer Storage and Recovery
El Aquifer Test
❑Experimental Technology
El Geothermal (Closed Loop)
El Geothermal (Heating/Cooling
❑Municipal/Public
❑Residential Water Supply (single)
❑Residential Water Supply (shared)
❑Groundwater Remediation
El Salinity Barrier
❑ Stormwater Drainage
El Subsidence Control
❑Tracer
El Other (explain under #21 1
4. Date Well(s) Completed: 4-9-14 Well ID# MW-44
5a. Well Location:
Milkco, Inc. #07022-03-11
Facility/Owner Name Facility ID# (if applicable)
220 Deaverview Road, Asheville, NC 28806
Physical Address, City, and Zip
Buncombe 2678
County Parcel Identification No. (PIN)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
35.57961 N 82.61351 W
6. Is (are) the well(s): ❑+Permanent or ❑Temporary
7. Is this a repair to an existing well: ❑Yes or E]No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: One
For multiple injection or non -water supply wells ONLY with the same construction, you can
submit one form.
9. Total well depth below land surface: 81 (ft.)
For multiple wells list all depths if different (example- 3@200' and 2@100')
10. Static water level below top of casing: 59.7 (ft.)
If water level is above casing, use "+ "
11. Borehole diameter: 6 (in.)
12. Well construction method: air hammer
(i.e. auger, rotary, cable, direct push, etc.)
14. WATER ZONES
FROM
TO
DESCRIPTION
59.7 rt.
81 rt.
saprolite and PWR
rt.
rt.
15. OUTER CASING for multi -cased wells OR LINER if a licable
FROM
TO
DIAMETER
THICKNESS
MATERIAL
ft.
ft.
in.
16. INNER CASING OR TUBING(geothermal closed -loop)
FROM
TO
DIAMETER
THICKNESS
MATERIAL
ft.
ft.
in.
rL
rt
in.
17. SCREEN
FROM
TO
DIAMETER
SLOT SIZE
THICKNESS
MATERIAL
65 ft'
80 ft'
2 in.
0.0101,
Sch 40
PVC
ft.
ft.
in.
18. GROUT
FROM
TO
MATERIAL
EMPLACEMENT METHOD & AMOUNT
0 ft.
57 rt.
cement
gravity -- 17 bags
57 ft.
62 ft.
bentonite
gravity -- 1 bag
rt.
rt.
19. SAND/GRAVEL PACK (if applicable)
FROM
TO
MATERIAL
EMPLACEMENT METHOD
62 ft•
81 ft•
#2 sand
gravity -- 6.5 bags
rt.
rt.
20. DRILLING LOG attach additional sheets if necessary)
FROM
TO
DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
0 IL
25 ft.
brown f-m sandy SILT (fill)
25 rL
70 ft.
brown silty f-m SAND (residuum)
70 ft.
81 ft.
brown silty f-m SAND (PWR)
rt.
81 rt.
bedrock
rL
ft.
ft.
ft.
rL
ft.
21. REMARKS
22. Certification:
4�3167
Signature of Certified Well Contractor
5-8-14
UULU
By signing this form, I hereby certify that the wells) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Iniection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636
13a. Yield m Method of test: 24c. For Water Supply & Injection Wells:
(gP ) Also submit one copy of this form within 30 days of completion of
13b. Disinfection type: Amount: well construction to the county health department of the countywhere
constructed.
Form GW-1 North Carolina Department of Environment and Natural Resources - Division of Water Resources Revised August 2013

KEY TO SOIL CLASSIFICATIONS AND CONSISTENCY DESCRIPTIONS
BUNNELL-LAMMONS ENGINEERING, INC.
GREENVILLE, SOUTH CAROLINA
Penetration Resistance*
Relative
Particle Size Identification
Blows per Foot
Density
SANDS
Boulder: Greater than 300 mm
Cobble: 75 to 300 mm
0 to 4
Very Loose
Gravel:
5 to 10
Loose
Coarse - 19 to 75 mm
11 to 20
Firm
Fine - 4.75 to 19 mm
21 to 30
Very Firm
Sand:
31 to 50
Dense
Coarse - 2 to 4.75 mm
over 50
Very Dense
Medium - 0.425 to 2 mm
Fine - 0.075 to 0.425 mm
Silt & Clay: Less than 0.075 mm
Penetration Resistance*
Consistency
Blows per Foot
SILTS and CLAYS
0 to 2
Very Soft
3 to 4
Soft
5 to 8
Firm
9 to 15
Stiff
16 to 30
Very Stiff
31 to 50
Hard
over 50
Very Hard
*ASTM D 1586
KEY TO DRILLING SYMBOLS
® Grab Sample
NR = No reaction to HCL Groundwater Table at Time of Drilling
® Split Spoon Sample NA = Not applicable
INS = No sample .
Undisturbed Sample Groundwater Table 24 Hours after Completion of Drilling
KEY TO SOIL CLASSIFICATIONS
F
Well-graded Gravel Low Plasticity Clay Clayey Silt Silty Sand
O
GW CL MH fig SM
EjPoorly -graded Gravel Sandy Clay Sandy Silt '- • '-% Topsoil
GP CLS MILS r;:.;\T.: TOPSOIL
Partially Weathered Rock Silty Clay Sand Liquid Sludge
BLDRCBBL CL-ML SW SLUDGE
High Plasticity Clay Silt Clayey Sand Fill
CH MIL SC FILL
.....
• • •
Poorly Graded Sand Bedrock 10 • • • 01 Waste
SP BEDROCK . � � � � WOOD

,RLIHINC.
INJECTION WELL NO. IW-2
PROJECT: Former Andrex Industries PROJECT NO.: J14-1022-38
CLIENT: Milkco START: 4-9-14 END: 4-9-14
BUNNELL-LAMNIMS
ENGINEERING, INC.
LOCATION: Asheville, North Carolina ELEVATION: 2221.78
DRILLER: Landprobe, M. King LOGGED BY: B. Nisbeth
GEOTECHNICALAND ENVROIINENTAL
CONSULTANTS
DRILLING METHOD: Schramm T450WS; 10-inch air hammer
DEPTH TO - WATER> INITIAL: AFTER 24 HOURS: 1 56.0 CAVING>337
w Z E
ELEVATION/
DESCRIPTION
SOIL
a Qp
MONITOR WELL INSTALLATION
DEPTH (FT)
TYPE
w
DETAILS
y L
2-inches of GRASS/TOPSOIL
Grout, 0 to 2.0 feet
Reddish -brown, micaceous, fine to medium sandy
2220
SILT - (fill)
SURFACE COMPLETION
Flush -mount secured with an
8-inch diameter steel bolted
manhole cover in a Tx Tx 4"
concrete pad
5
Measuring point elev. = 2,221.59
2215
feet
Ground surface elev. = 2,221.78
feet
10
Latitude (North) = 35.579900
0.0
Longitude (West) = 82.613960
2210
15
2205
20
0.0
Bentonite seal, 2.0 to 64.0 feet
Brown, slightly micaceous, fine to medium sandy
SILT
2200
25
Reddish -brown, slightly micaceous, silty, fine to
medium SAND - (residuum)
2195
30
0.0
2190
35
Light brown, slightly micaceous, silty, fine to
medium SAND
2185
INJECTION WELL NO. IW-2
Sheet 1 of 3

,RLIHINC.
INJECTION WELL NO. IW-2
PROJECT: Former Andrex Industries PROJECT NO.: J14-1022-38
CLIENT: Milkco START: 4-9-14 END: 4-9-14
BUNNELL-LAMNIMS
ENGINEERING, INC.
LOCATION: Asheville, North Carolina ELEVATION: 2221.78
GEOTECHNICALAND ENVROIINENTAL
DRILLER: Landprobe, M. King LOGGED BY: B. Nisbeth
CONSULTANTS
DRILLING METHOD: Schramm T450WS; 10-inch air hammer
DEPTH TO - WATER> INITIAL: AFTER 24 HOURS: 1 56.0 CAVING>337
w
Z £
ELEVATION/
DESCRIPTION
SOIL i
Qp
MONITOR WELL INSTALLATION
DEPTH (FT)
TYPE 2
DETAILS
y
iQ
a�
Light brown, slightly micaceous, silty, fine to
0.0
medium SAND
218o
PARTIALLY WEATHERED ROCK which sampled as
light brown, slightly micaceous, silty, fine to medium
SAND
45
2175
50
0.0
2170
55
IF
PARTIALLY WEATHERED ROCK which sampled as
2165
dark brown, slightly micaceous, silty, fine to medium
SAND
Bentonite seal, 2.0 to 64.0 feet
60
0.0
2160
#3 Stone, 64.0 to 84.0 feet
ROCK with sampled as grayish -brown, slightly
65
micaceous, silty, fine to medium SAND
2155
7o
0.0
ROCK which sampled as brown, slightly micaceous,
silty, fine to medium SAND - (fracture zone)
2150
ROCK which sampled as grayish -brown, slightly
micaceous, silty, fine to medium SAND
75
2145
INJECTION WELL NO. IW-2
Sheet 2 of 3

,RLIHINC.
INJECTION WELL NO. IW-2
PROJECT: Former Andrex Industries PROJECT NO.: J14-1022-38
CLIENT: Milkco START: 4-9-14 END: 4-9-14
BUNNELL-LAMNIMS
ENGINEERING, INC.
LOCATION: Asheville, North Carolina ELEVATION: 2221.78
DRILLER: Landprobe, M. King LOGGED BY: B. Nisbeth
GEOTECHNICALAND ENVROIINENTAL
CONSULTANTS
DRILLING METHOD: Schramm T450WS; 10-inch air hammer
DEPTH TO - WATER> INITIAL: AFTER 24 HOURS: 1 56.0 CAVING>337
w Z E
ELEVATION/
DESCRIPTION
SOIL
a Qp
MONITOR WELL INSTALLATION
DEPTH (FT)
TYPE
w
DETAILS
y L=
ROCK which sampled as grayish -brown, slightly
0.0
micaceous, silty, fine to medium SAND
2140
Total borehole depth, 84.0 feet
85
Boring terminated at 84.0 feet. Groundwater
encountered at 56.0 feet after 24 hours.
Borehole diameter, 10-inches
2135
90
2130
95
2125
100
2120
105
2115
110
2110
115
2105
INJECTION WELL NO. IW-2
Sheet 3 of 3

,RLIHINC.
GROUNDWATER MONITORING WELL NO. MW-44
PROJECT: Former Andrex Industries PROJECT NO.: J14-1022-38
CLIENT: Milkco START: 4-8-14 END: 4-9-14
BUNNELL-LAMNIMS
ENGINEERING, INC.
LOCATION: Asheville, North Carolina ELEVATION: 2219.46
DRILLER: Landprobe, M. King LOGGED BY: B. Nisbeth
GEOTECHNICALAND ENVROIINENTAL
CONSULTANTS
DRILLING METHOD: Schramm T450WS; 6-inch air hammer
DEPTH TO - WATER> INITIAL: 64.0 AFTER 24 HOURS: 1 59.7 CAVING>337
w
Z E
ELEVATION/
DESCRIPTION
SOIL
a
Qp
MONITOR WELL INSTALLATION
DEPTH (FT)
TYPE
w
DETAILS
y
L
2-inches of GRASS/TOPSOIL
SURFACE COMPLETION
Flush - secured With an
8-inch diameter steel bolted
diameter
Reddish -brown micaceous fine to medium sand
> > y
SILT - (fill)
manhole cover in a Tx Tx 4"
concrete pad
Measuring point elev. = 2,219.15
2215
feet
5
Ground surface elev. = 2,219.46
Latitude (North) = 35.579610
Longitude (West) = 82.613510
2210
10
0.0
2205
15
Wood debris
2200
20
0.0
Grout, 0 to 57.0 feet
2195
25
Brown, slightly micaceous, silty, fine to medium
SAND - (residuum)
2190
30
0.0
2185
35
2180
GROUNDWATER MONITORING WELL NO. MW-44
Sheet 1 of 3

,RLIHINC.
GROUNDWATER MONITORING WELL NO. MW-44
PROJECT: Former Andrex Industries PROJECT NO.: J14-1022-38
CLIENT: Milkco START: 4-8-14 END: 4-9-14
BUNNELL-LAMNIMS
ENGINEERING, INC.
LOCATION: Asheville, North Carolina ELEVATION: 2219.46
GEOTECHNICALAND ENVROIINENTAL
DRILLER: Landprobe, M. King LOGGED BY: B. Nisbeth
CONSULTANTS
DRILLING METHOD: Schramm T450WS; 6-inch air hammer
DEPTH TO - WATER> INITIAL: 64.0 AFTER 24 HOURS: 1 59.7 CAVING>337
w
Z E
ELEVATION/
DESCRIPTION
SOIL
a
Qp
MONITOR WELL INSTALLATION
DEPTH (FT)
TYPE
Q
DETAILS
y
L i
Brown, slightly micaceous, silty, fine to medium
0.0
SAND - (residuum)
f.
2175
45
Grout, 0 to 57.0 feet
2170
50
0.0
Light brown, moist, slightly micaceous, silty, fine to
medium SAND
2165
55
Bentonite seal, 57.0 to 62.0 feet
2160
60
0.0
Filter pack #z sand, 62.0 to 81.0
Brown, slightly micaceous, silty, fine to medium
SAND
feet
2155
65
2150
7o
0.0
PARTIALLY WEATHRERED ROCK which sampled as
light brown, slightly micaceous, silty, fine to medium
SAND
2-inch diameter, 0.010-inch slotted
Schedule 40 PVC well screen, 65.0
2145
to 80.0 feet
75
Brown, slightly micaceous, silty, fine to medium
SAND (soil seam)
2140
GROUNDWATER MONITORING WELL NO. MW-44
Sheet 2 of 3

,RLIHINC.
GROUNDWATER MONITORING WELL NO. MW-44
PROJECT: Former Andrex Industries PROJECT NO.: J14-1022-38
CLIENT: Milkco START: 4-8-14 END: 4-9-14
BUNNELL-LAMNIMS
ENGINEERING, INC.
LOCATION: Asheville, North Carolina ELEVATION: 2219.46
DRILLER: Landprobe, M. King LOGGED BY: B. Nisbeth
GEOTECHNICALAND ENVROIINENTAL
CONSULTANTS
DRILLING METHOD: Schramm T450WS; 6-inch air hammer
DEPTH TO - WATER> INITIAL: 64.0 AFTER 24 HOURS: 1 59.7 CAVING>337
w
Z E
ELEVATION/
DESCRIPTION
SOIL
a
Qp
MONITOR WELL INSTALLATION
DEPTH (FT)
TYPE
Q
DETAILS
y
=
Li
ROCK which sampled as gray, slightly micaceous,
0.0
Pipe cap
silty, fine to medium SAND
Total Well depth, 80.10 feet
Boring terminated at 81.0 feet. Groundwater
encountered at 64.0 feet at time of drilling and at 59.7
Total borehole depth, 81.0 feet
feet after 24 hours.
Borehole diameter, 6-inches
2135
85
2130
90
2125
95
2120
100
2115
105
2110
110
2105
115
2100
GROUNDWATER MONITORING WELL NO. MW-44
Sheet 3 of 3

APPENDIX B
INJECTION EVENT RECORD & PLOT

INJECTION EVENT RECORD
North Carolina Department of Environment and Natural Resources —Division of Water Resources
Permit Number t,J= 0 t Oo 1b(o
1. Permit Information
2.
N G.
Permittee
Facility Name
Facility Address
Injection Contractor Information
Injection Contractor / Comp'Xny N
Street Address (p0p4 �ondt�S �u�%
CaYu.,n.y►u.2 SC, 2ge15
City State Zip Code
Area code — Phone number
3. Well Information
Number of wells used for injection
Well names
Were any new wells installed during this injection
event?
[X Yes ❑ No
If yes, please provide the following information:
Number of Monitoring Wells
Number of Injection Wells
Type of Well Installed (Check applicable type):
❑ Bored ©Drilled ❑Direct -Push
❑ Hand -Augured ❑ Other (specify)
Please include a copy of the GW4form for each
well installed.
`Catu-Irms wUt SwbMi}itcl prio< injcviio
Were any wells abandoned during this injection
event?
❑ Yes No
If yes, please provide the following
information:
g
Number of MonitorinWells
Number of Injection Wells
Please inclarde a copy of the GW-30 for each tivell
abandoned
4. Injectant Information
Ito 011 k 4341
Injectant Type
0
Concentration a
If the Injectant is diluted please indicate the source
dilution fluid. W—MI 2r
Total Volume Injected 2�� 000 qa� ons
Volume Injected per well 24 000_
5. Injection History
Injection dates) 'J * 1� • Znhl• •-r'4�rti �o • OZ • Z01'�'
Injection number (e.g. 3 of 5) q'
Is this the last injection at this site?
❑ Yes �, No
I DO HEREBY CERTIFY THAT ALL THE
INFORMATION ON THIS FORM IS CORRECT TO
THE BEST OF MY KNOWLEDGE AND THAT THE
INJECTION WAS PERFORMED WITHIN THE
STANDARDS LAID OUT IN THE PERMIT,
OF
PRINT NriME OF PERSON
CONTRACTOR DATE
THE INJECTION
Submit the original of this form to the Division of Water Resources within 30 days of injection. Form UIC-IER
Attn: UIC Program, 1636 Mail Service Center, Raleigh, NC 27699-1636, Phone No. 919-807-6464 Rev. 8/5/2013

28,000
26,000
24,000
22,000
20,000
18,000
0
16,000
C7
> 14,000
c�
12,000
u 10,000
8,000
6,000
4,000
2000,
0
5/11/2014
i
IW-2 Injection Record for Event 2014
5/16/2014
5/21/2014 5/26/2014 5/31/2014 6/5/2014
Date

APPENDIX C
LABORATORY ANALYTICAL DATA SHEETS
TOC ANALYSIS OF MILK SOLUTION
(Provided on Enclosed CD)

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
May 22, 2014
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
RE: Project: FORMERANDREX IND J14-1022-38
Pace Project No.: 92201330
Dear Mr. Alexander:
Enclosed are the analytical results for sample(s) received by the laboratory on May 14, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201330
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

aceAnalytical
—pacelabsxom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201330
Lab ID Sample ID
92201330001 IC-2014-A
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 05/14/1414:45 05/14/1416:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201330
Lab ID Sample ID
92201330001 IC-2014-A
SAMPLE ANALYTE COUNT
Method
SM 5310B
REPORT OF LABORATORY ANALYSIS
Analytes
Analysts Reported
SAE
Laboratory
PAS I -A
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201330
Sample: IC-2014-A Lab ID: 92201330001 Collected: 05/14/14 14:45 Received: 05/14/14 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 3990 mg/L 100 100 100 05/22/14 11:07 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2014 01:57 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201330
QC Batch: WETA/19054
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92201330001
METHOD BLANK: 1203097
Matrix: Water
Associated Lab Samples: 92201330001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
05/21/14 17:51
LABORATORY CONTROL SAMPLE: 1203098
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 23.8
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1203099 1203100
MS MSD
92201069001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 12.4
25 25 33.4
32.9 84 82 75-125 1 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1203101 1203102
MS MSD
92201026011 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 1.9 25 25 27.4 27.1 102 101 75-125 1 20
Date: 05/22/2014 01:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201330
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2014 01:57 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201330
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92201330001 IC-2014-A SM 5310B WETA/19054
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/22/2014 01:57 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 10

aceAnalytical e'
Document Name: Sample Condition Upon
Receipt (SCUR)
Document Revised: April 9, 2014
Page 1 of 2
/// --- www.paco/aUs.com
I
Document No.:
Issuing Authorities:
F-ASV-CS-003-rev.13
Pace Asheville Quality Office
Client Name:
Courier (Circle): Fed Ex UPS USPS Client - a Commercial Pace Other
Custody Seal on Cooler/Box Present: [� yes Sno Seals intact: yes F] no
Packing Material: Bubble Wrap Bubble Bags 0 None Other
Thermometer Used: Gun#3 -, 2659�3 Type of Ice:( Wo'', Blue None Samples on ice, cooling process has begun
O er:
Temp Correction Factor: Add / Subtract 0. 0 C
Corrected Cooler Temp.: C
Biological Tissue is Frozen: Yes No N/A
Date and Initills of erson examining
contents: (�� I
i
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
Yes
❑No
❑N/A
1.
Chain of Custody Filled Out:
2<
ONo
❑N/A
2.
Chain of Custody Relinquished:
Ye
ON
❑N/A
3.
Sampler Name & Signature on COC:
dYep,
❑No
❑N/A
4.
Samples Arrived within Hold Time:
Yes
❑No
El N/A
5.
Short Hold Time Analysis (<72hr):
❑Yes
No
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
o
❑N/A
7.
Sufficient Volume:
a
ON.
❑N/A
8.
Correct Containers Used:
Yes
❑No
❑N/A
9.
-Pace Containers Used:
@fYe
❑No
❑N/A
Containers Intact:
Yes
❑No
❑NIA
10.
Filtered volume received for Dissolved tests
❑Yes
No
/A
11.
Sample Labels match COC:
es
❑No
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
�
All containers needing preservation have been checked.
Yes
[:]No
❑N/A
13.
All containers needing preservation are found to be in
"LJYes
❑No
❑NIA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
❑Yes
LJNo
Samples checked for dechlorination:
❑Yes
❑No
N/A
14.
Headspace in VOA Vials (>6mm):
❑Yes
No
❑N/A
15.
Trip Blank Present:
❑Yes
❑No
/A
6.
Trip Blank Custody Seals Present
❑Yes
❑No
/A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
Date/Time:
SRF Review: `/ 141 JDate: 5/ 5
Note: Whenever 6A is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y / N
Place label here
1) 2 "7-0,/33O OR
Handwrite project number
(if no label available)
Page 9 of 10

PaceAnalytical'
mm.pacelatis.com
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Page: of
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information:
Company. Report To: Attention:
Address: Qj
Copy To:
Company Name:
`c+Ylul�+{rs
REGULATORY AGENCY
Y I5
Address:
NPDES GROUND WATER DRINKINGWATER
-
Email To:
irL100A
Purchase Order No.-
Pace Quote
'
P n 2g$ �S 450
Project Name:
Reference:
Paca Project
UST RCRA OTHER
D
TOG< tCYkQ�
taanager.
Site Location
Requested Due DatefrAT:.
Project Number:
Pace P:^;iite #
fleA
l�- t�22 - 3
STATE:
Requested
Analysis
Filtered
{YIN)
Section D Matrix Codes
z
Required Client lnfortnailan raarf:a r cooe
-
COLLECTED
Preservatives
Drinking Water DW
t0,
Water WT
U
O
Waste Water WW
P
coaa>os€.
COMPOSITE
�-
to
Product P
¢
Cr0
srnxT
END�Fu+e
Z
SoiVSolid SL
SAMPLE ID ail OL
o
••►
cr>
}
WipeWP
"
H
W
N
C
(A-Z. 0-9 t :) Air AR
Sample IDS MUST BE UNIQUE Tissue TS
Lu
p
a
a
Lu
m
Other OT
U
N
H
f
w
z
Z
c3
w
F-
°0
o
m
O
=
O
C6
-
~
N
O
?
=
OI2
DATE
TIME
DATE
TIME
5
2
`L
O
y1!-4
,.z
Pace Project No./ Lab 1
is
2
3
4
E
6
i
7
a
i
9
i
,012
k
i
i
ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME
ACCEPTED BY 1 AFFILIATION
DATE
SAMPLE
CONDfT1DNS
I&L��-i
f
8
�14114
fTIME��{
t6j7?�`P
i
1
t
�
l i
SAMPLER NAME AND SIGNATURE
-
.'z...
E
c
— f
PRINT Name of SAMPLER: •t _ _ 1.I. I
-
SIGNATURE of SAMPLER:
ATE Signedof
'Imponant'rote 6y signing this fcrm you are accaatine Face's A:=-V,nav r>,.-.,......r...... ........
_-__:_ _ ..:_._ ... _.. ...._ r
N
tT
N
d
-• . _. = P� +y rtxs r : p K; p ,r!!'l,.A; 43, F-ALL-0-020rev.07. , 5-k9ay-2007

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
June 04, 2014
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
RE: Project: FORMERANDREX IND. J14-1022-38
Pace Project No.: 92202615
Dear Mr. Alexander:
Enclosed are the analytical results for sample(s) received by the laboratory on May 23, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND. J14-1022-38
Pace Project No.: 92202615
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

aceAnalytical
—pacelabsxom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND. J14-1022-38
Pace Project No.: 92202615
Lab ID Sample ID
92202615001 IC-2014-B
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 05/22/14 09:30 05/23/14 08:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND. J14-1022-38
Pace Project No.: 92202615
Lab ID Sample ID
92202615001 IC-2014-B
SAMPLE ANALYTE COUNT
Method
SM 5310B
REPORT OF LABORATORY ANALYSIS
Analytes
Analysts Reported
SAE
Laboratory
PAS I -A
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND. J14-1022-38
Pace Project No.: 92202615
Sample: IC-2014-B Lab ID: 92202615001 Collected: 05/22/14 09:30 Received: 05/23/14 08:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 2500 mg/L 50.0 50.0 50 06/03/14 18:12 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2014 06:01 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND. J14-1022-38
Pace Project No.: 92202615
QC Batch: WETA/19160
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92202615001
METHOD BLANK: 1210852
Matrix: Water
Associated Lab Samples: 92202615001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
06/03/14 14:28
LABORATORY CONTROL SAMPLE: 1210853
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 25.1
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1210854 1210855
MS MSD
92202261003
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 8.8
25 25 31.8
31.6 92 91 75-125 0 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1210856 1210857
MS MSD
92202542001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 2.0 25 25 26.9 26.8 99 99 75-125 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2014 06:01 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: FORMER ANDREX IND. J14-1022-38
Pace Project No.: 92202615
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2014 06:01 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FORMER ANDREX IND. J14-1022-38
Pace Project No.: 92202615
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92202615001 IC-2014-B SM 5310E WETA/19160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2014 06:01 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 10

Document Name: Sample Condition Upon
Document Revised: April 9, 2014
Wacq!eAnalytical-Recei
t SCUR
Pa e 1 of 2
p... lab..com
Document No.:
Issuing Authorities:
F-ASV-CS-003-rev.13
Pace Asheville Quality Office
Client Name:�,,,���� .��,�F, I,
Courier (Circle): Fed Ex UPS USPS gin'o
Commercial
Custody Seal on Cooler/Box Present: yes Seals intact:
Packing Material: Z�bble Bags None Other,
Thermometer Used: Type of Ice. We Blue
Other:
Temp Correction Factor: Add / Subtract C
Pace Other
yes p no
None 24arriples on ice, cooling process has begun
Corrected Cooler Temp.: I , I C
Biological Tissue is Frozen: Yes No N/A
Date and IniWls of person examining
Temp should be above freezing to ti°C
Comments:
contents: &S ' I23 t`t
Chain of Custody Present:
U4,13No
❑N/A
1.
Chain of Custody Filled Out:
es ❑No
❑N/A
2.
Chain of Custody Relinquished:
2reVON.
❑WA
3.
Sampler Name & Signature on COC:
Yes No
❑N/A
4.
Samples Arrived within Hold Time:
es [:]No
N/A
5.
Short Hold Time Analysis (<72hr):
Dyes No
❑N/A
6.
Rush Turn Around Time Requested:
es No
El N/A
7.
Sufficient Volume:
es No
❑N/A
8.
Correct Containers Used:
ee, El No
El N/A
9.
-Pace Containers Used:
L'Yes No
❑N/A
Containers Intact:
OAK. ❑No
0 N/A
40.
Filtered volume received for Dissolved tests
❑Ye ❑No
N/A
11.
Sample Labels match COC:
Yes ❑No
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
es ❑No
❑N/A
13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
7es No
❑N/A
exceptions: VOA, colifor , TOC, &G, WI-DRO (water)
2 es ONo
Samples checked for dechlorination:
Dyes ❑No
RrN/A
14.
Headspace in VOA Vials (>6mm):
Dyes No
/A
15.
Trip Blank Present:
Dyes No
N/A
16.
Trip Blank Custody Seals Present
❑Yes o
Ell/A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
Date/Time:
SRF Review: ✓ � �� Date:
Note: Wheneve ere is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y / N
Place label here
cam/ 2
.2 62�0 OR
Handwrite project number
(if no label available)
Page 9 of 10

PakeAnalydical A
w".oacelaba.com
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
A Section B Section C
Page: ofL
{Section
Required Client Information: Required Project Information: Invoice Information:
Company: Report To: Attention:178
sss
f
Address: {j ' -a Copy
Y n9w`
To:
Company Name: CJApr r
REGULATORY AGENCY
wG
SL i5
Address:
Sa„t�
NPDES GROUND WATER DRINKING WATER.
UST RCRA j OTHER
Email To: Purchase
Order No.:
Pace Quote
M
Reference:
F -�p pQ Project
Name:
folw„�,
Pace Projecttip
LOCatiOned
Mon
o
{ �,,,{rt
y,,
".anager:Site
STATE:
e
Due DaterTAT: Proiecl
Nurnber.T`,4. 14u- st
i++
Pace Profile r:
Requested
Analysis
Filtered
(YIN)
Section D Mairix Codes
_
2
Required Glint lnforma14on MATRIX i CODE
-
c.
COLLECTED
Preservatives
>
Drinking Water DVY
a
O
U
Water 4YT
3
1
p
Waste Water Yilb'V
COMPOSITE
con:aaS:-e
Product P
-
<
START
enc•GRAS
I
?
SoitlSofid SL
?-
SAMPLE ID oil OL
U7
Wdpe WP
(A-Z. 0-91:) Air AR
u
'-
Lu
Sample IDS MUST BE UNIOUE Tissue TS
O
a
w
Z
Other OT
X
Y
Lu
a
L
a
O
U
N
O
@
tT3
a
0 �a `(�
I��Al.tni
F
G
�¢
O
n
�.
UZ
U
cUaR
—
u%
DATE
TIME
GATE
TIME
T—
S
S
Z
Z
O
,,,p
^—'
Pace Project NO.I I.II.
Tc, -U V4-15
wlc
41
Sis
5-U
130
!
3
1
X
2
3
3
A
5
j
i
1
6
i
i
7
8
9
10
1
tt
1
12
!
ADDITIONAL COMMENTS
RELINQUISHED BY l AFFILIATION
I DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
I TIME
SAMPLE CONDITIONS
t
SAMPLER NAME AND SIGNATURE
-. GINA ..
_
2
c
PRINT Name of SAMPLER: 'at t$$[_
SIGNATURE of SAMPLER:
DATE Signed
(MMIDD,, M: OS� 2
Cr
I'lam"m Note. By S; n 0 M. Fenn lmi am aece%"q Pace's NET 30 day eaymew leans and ag oewlg to late charges of 1.5' c fx;r �6nlpja!any ices rm pale •xrl+in 30 days. i F-ALL-0-020ray.07. 75-May-2007

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
June 11, 2014
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
RE: Project: FORMERANDREX IND
Pace Project No.: 92203645
Dear Mr. Alexander:
Enclosed are the analytical results for sample(s) received by the laboratory on June 03, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND
Pace Project No.: 92203645
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 10

aceAnalytical
—pacelabsxom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND
Pace Project No.: 92203645
Lab ID Sample ID
92203645001 IC-2014-C
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 06/02/14 13:00 06/03/14 08:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND
Pace Project No.: 92203645
Lab ID Sample ID
92203645001 IC-2014-C
SAMPLE ANALYTE COUNT
Method
SM 5310B
REPORT OF LABORATORY ANALYSIS
Analytes
Analysts Reported
SAE
Laboratory
PAS I -A
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND
Pace Project No.: 92203645
Sample: IC-2014-C Lab ID: 92203645001 Collected: 06/02/14 13:00 Received: 06/03/14 08:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon 4100 mg/L 100 100 100 06/11/14 11:36 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/11/2014 06:09 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND
Pace Project No.: 92203645
QC Batch: WETA/19263
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92203645001
METHOD BLANK: 1217267
Matrix: Water
Associated Lab Samples: 92203645001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
06/10/14 19:16
LABORATORY CONTROL SAMPLE: 1217268
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 24.7
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1217269 1217270
MS MSD
92204278010
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 7.6
25 25 31.1
31.1 94 94 75-125 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/11/2014 06:09 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: FORMER ANDREX IND
Pace Project No.: 92203645
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/11/2014 06:09 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 10

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FORMER ANDREX IND
Pace Project No.: 92203645
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92203645001 IC-2014-C SM 5310E WETA/19263
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/11/2014 06:09 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 10

�� yP
Document Name: Sample Condition Upon
Document Revised: April 9, 2014
Analytical-
Recei t SCUR
Page 1 of 2
Document No.:
Issuin Authorities:
9
F-ASV-CS-003-rev.13
Pace Asheville Quality Office
Client Name: Nmtt I crm,)Ms Eff
Courier (Circle): Fed Ex UPS USPS Clien Commercial Pace Other
Custody Seal on CoolerlBox Present: [] yes no eals intact: 0 yes ❑ no
Packing Material: ❑ Bu ,ape, `B�ubble Bags None Other
Thermometer Used: Gun#3-130265 CD Type of Ice: 0 Blue None Samples on ice, cooling process has begun
Other:
r_-....a,r
n.a a i Ci h4ron? /1 i l r`
,
,....r.,...,...,.,.._...----- ------ ----...--
Corrected Cooler Temp" C Biological Tissue is Frozen: Yes No N/A Date and Initials of pecontents:_({rs n�lamexamining
__(�'_
Temp should be above freezing to 6°C Comments: �( (�
Chain of Custody Present: Yes No ❑N/A 1.
Chain of Custody Filled Out: es ❑No ❑NIA 2.
Chain of Custody Relinquished: es ❑No ❑NIA 3.
Sampler Name & Signature on COC: V'Yey ❑No ❑N/A 4.
Samples Arrived within Hold Time: Yes ONo N/A 5.
Short Hold Time Analysis (<72hr): ❑Yes No N/A 6.
Rush Turn Around Time Requested: ❑Ye No El N/A 7.
Sufficient Volume: Yes ONO ❑N/A 8.
Correct Containers Used: Yeses ❑No ❑N/A 9.
-Pace Containers Used: LdYes ❑No ❑N/A
Containers Intact: Yes ❑No ❑N 10.
Filtered volume received for Dissolved tests ❑Ye ❑No N/A 11.
Sample Labels match COC: Yes ❑No ❑NIA 12.
-Includes date/tirne/ID/Anal sis Matrix: lX"
All containers needing preservation have been checked. 7.713o ❑N/A 13.
All containers needing preservation are found to be in VIC. ❑No El N/A
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water) ❑Yes 6.
Samples checked for dechlorination: ❑Yes CJNo /A 14.
Headspace in VOA Vials ( >6mm): ❑Yes ❑No NIA 16,
Trip Blank Present: ❑Yes ❑No /ry 16.
Trip Blank Custody Seals Present ❑Yes ❑No CAN//A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
Date/Time:
SRF Review: `� V\,i 1 Date: L
Note: Whenever there is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office (Le out of hold, incorrect
preservative, out of ternp, incorrect containers)
Field Data Required? Y / N
Place label here
OR
Handwrite project number
(if no label available)
5
Page 9 of 10
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
Date/Time:
SRF Review: `� V\,i 1 Date: L
Note: Whenever there is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office (Le out of hold, incorrect
preservative, out of ternp, incorrect containers)
Field Data Required? Y / N
Place label here
OR
Handwrite project number
(if no label available)
5
Page 9 of 10

0
. PaceAnalytical
www.pacelabs.coni
Section A
Required Client Information:
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Section C
Required Proiect Information:
Page: � of
Company: -
Art
Report To:
Attention:
&
f � ' -7 ' +v,
`•..3 i U,
Address:
Copy To:
Company Name: ,..
REGULATORY AGENCY
Y y
Address: l Sc,NPDES
GROUND WATER DRINKING WATER
UST RCRA OTHER
Email To:
VKiGO
Purchase Order No.:
Pace quote
Relerence:
Project Name: ./
Pace Project
Site Location
STATE:
�q(
Requested Due Date/TAT:
Project Number:
TZ 3�
P.- ProiEe #�
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
-w
z
RequiredCliem lnrormaror, NIATRIX ; CODE.
—
°-
COLLECTED
Preservatives
>-
Drinkinq Water DV,'
C
z
E
1Naier WTI
J
O
Waste Water WW
Coat?OSr=
COMapsrE
l—
PfoduCt P
SoliiSolid SL
_
rrj�
�: kti'r
atiD; r�PJ+FS
W
O
Z
>
SAMPLE ID al oL
T
_.-.._
.,ripe A
(A-Z. 0-9 r .-) Air AR R
Lu
C W
Sample IDS MUST 6E UNIQUE Tissue 7S
O
O
a}
w
v
y
'
0
Other OT
— Z
Z
w
a
U-
Q,
p'
0
cl
c
!
m`�
�
—
z
<
0�+
Z
Z
y
i
DATE
DATE
`W
Z)
2
2
2
.�
O
C
Pace Project No.� b I.D.
X
'Qtia' T
�TIIME
Va t7
-a
'TIIME
tl cu
J
y
JL
2
3
4
I
5
6
7
I
I
I
(
I
i
I
J
121
ADDITIONAL COIMEN'a S f RELINQUISHED BY f AFFILIATION
DATE 1 TIME
AC EPTED GAY (AFFILIATION
DATE
TIME
SAMPLE CONDITIONS I
E
�
I
�
I I
SA,i iPLER I A."%E ANC SIG .."'ATU
^- NT
15
DATE S ti
0
0
N
to
N
d

APPENDIX D
LABORATORY ANALYTICAL DATA SHEETS
GROUNDWATER & SURFACE WATER
May 2014 [Pre -Injection Baseline]
(Provided on Enclosed CD)

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
May 28, 2014
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
RE: Project: FORMERANDREX IND J14-1022-38
Pace Project No.: 92201331
Dear Mr. Alexander:
Enclosed are the analytical results for sample(s) received by the laboratory on May 14, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 23

aceAnalytical
—pacelabsxom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE SUMMARY
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92201331001
92201331002
MW-6
RW-1
Water
Water
05/14/14 09:25
05/14/1410:00
05/14/14 16:30
05/14/1416:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
FORMER ANDREX IND J14-1022-38
92201331
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92201331001
MW-6
EPA 8260
MCK
63
PASI-C
SM 5310B
SAE
1
PASI-A
92201331002
RW-1
EPA 8260
GAW
63
PASI-C
SM 5310B
SAE
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
Sample: MW-6 Lab ID: 92201331001 Collected: 05/14/14 09:25 Received: 05/14/14 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
250
100
10
05/27/14 23:32
67-64-1
Benzene
ND ug/L
10.0
2.5
10
05/27/14 23:32
71-43-2
Bromobenzene
ND ug/L
10.0
3.0
10
05/27/14 23:32
108-86-1
Bromochloromethane
ND ug/L
10.0
1.7
10
05/27/14 23:32
74-97-5
Bromodichloromethane
ND ug/L
10.0
1.8
10
05/27/14 23:32
75-27-4
Bromoform
ND ug/L
10.0
2.6
10
05/27/14 23:32
75-25-2
Bromomethane
ND ug/L
20.0
2.9
10
05/27/14 23:32
74-83-9
2-Butanone (MEK)
ND ug/L
50.0
9.6
10
05/27/14 23:32
78-93-3
Carbon tetrachloride
ND ug/L
10.0
2.5
10
05/27/14 23:32
56-23-5
Chlorobenzene
ND ug/L
10.0
2.3
10
05/27/14 23:32
108-90-7
Chloroethane
ND ug/L
10.0
5.4
10
05/27/14 23:32
75-00-3
Chloroform
ND ug/L
10.0
1.4
10
05/27/14 23:32
67-66-3
Chloromethane
ND ug/L
10.0
1.1
10
05/27/14 23:32
74-87-3
2-Chlorotoluene
ND ug/L
10.0
3.5
10
05/27/14 23:32
95-49-8
4-Chlorotoluene
ND ug/L
10.0
3.1
10
05/27/14 23:32
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
50.0
25.2
10
05/27/14 23:32
96-12-8
Dibromochloromethane
ND ug/L
10.0
2.1
10
05/27/14 23:32
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
10.0
2.7
10
05/27/14 23:32
106-93-4
Dibromomethane
ND ug/L
10.0
2.1
10
05/27/14 23:32
74-95-3
1,2-Dichlorobenzene
ND ug/L
10.0
3.0
10
05/27/14 23:32
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
2.4
10
05/27/14 23:32
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
3.3
10
05/27/14 23:32
106-46-7
Dichlorodifluoromethane
ND ug/L
10.0
2.1
10
05/27/14 23:32
75-71-8
1,1-Dichloroethane
ND ug/L
10.0
3.2
10
05/27/14 23:32
75-34-3
1,2-Dichloroethane
ND ug/L
10.0
1.2
10
05/27/14 23:32
107-06-2
1,1-Dichloroethene
ND ug/L
10.0
5.6
10
05/27/14 23:32
75-35-4
cis-1,2-Dichloroethene
1000 ug/L
10.0
1.9
10
05/27/14 23:32
156-59-2
trans-1,2-Dichloroethene
ND ug/L
10.0
4.9
10
05/27/14 23:32
156-60-5
1,2-Dichloropropane
ND ug/L
10.0
2.7
10
05/27/14 23:32
78-87-5
1,3-Dichloropropane
ND ug/L
10.0
2.8
10
05/27/14 23:32
142-28-9
2,2-Dichloropropane
ND ug/L
10.0
1.3
10
05/27/14 23:32
594-20-7
1,1-Dichloropropene
ND ug/L
10.0
4.9
10
05/27/14 23:32
563-58-6
cis-1,3-Dichloropropene
ND ug/L
10.0
1.3
10
05/27/14 23:32
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
10.0
2.6
10
05/27/14 23:32
10061-02-6
Diisopropyl ether
ND ug/L
10.0
1.2
10
05/27/14 23:32
108-20-3
Ethylbenzene
ND ug/L
10.0
3.0
10
05/27/14 23:32
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
10.0
7.1
10
05/27/14 23:32
87-68-3
2-Hexanone
ND ug/L
50.0
4.6
10
05/27/14 23:32
591-78-6
p-Isopropyltoluene
ND ug/L
10.0
3.1
10
05/27/14 23:32
99-87-6
Methylene Chloride
57.1 ug/L
20.0
9.7
10
05/27/14 23:32
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
50.0
3.3
10
05/27/14 23:32
108-10-1
Methyl-tert-butyl ether
ND ug/L
10.0
2.1
10
05/27/14 23:32
1634-04-4
Naphthalene
ND ug/L
10.0
2.4
10
05/27/14 23:32
91-20-3
Styrene
ND ug/L
10.0
2.6
10
05/27/14 23:32
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
10.0
3.3
10
05/27/14 23:32
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
10.0
4.0
10
05/27/14 23:32
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
Sample: MW-6
Lab ID: 92201331001
Collected:
05/14/14 09:25
Received: 05/14/14 16:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
1920 ug/L
10.0
4.6
10
05/27/14 23:32
127-18-4
Toluene
ND ug/L
10.0
2.6
10
05/27/14 23:32
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
10.0
3.3
10
05/27/14 23:32
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
10.0
3.5
10
05/27/14 23:32
120-82-1
1,1,1-Trichloroethane
ND ug/L
10.0
4.8
10
05/27/14 23:32
71-55-6
1,1,2-Trichloroethane
ND ug/L
10.0
2.9
10
05/27/14 23:32
79-00-5
Trichloroethene
94.7 ug/L
10.0
4.7
10
05/27/14 23:32
79-01-6
Trichlorofluoromethane
ND ug/L
10.0
2.0
10
05/27/14 23:32
75-69-4
1,2,3-Trichloropropane
ND ug/L
10.0
4.1
10
05/27/14 23:32
96-18-4
Vinyl acetate
ND ug/L
20.0
3.5
10
05/27/14 23:32
108-05-4
Vinyl chloride
ND ug/L
10.0
6.2
10
05/27/14 23:32
75-01-4
Xylene (Total)
ND ug/L
20.0
6.6
10
05/27/14 23:32
1330-20-7
m&p-Xylene
ND ug/L
20.0
6.6
10
05/27/14 23:32
179601-23-1
o-Xylene
ND ug/L
10.0
2.3
10
05/27/14 23:32
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
10
05/27/14 23:32
460-00-4
1,2-Dichloroethane-d4 (S)
96 %
70-130
10
05/27/14 23:32
17060-07-0
Toluene-d8 (S)
98 %
70-130
10
05/27/14 23:32
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 6.8 mg/L 1.0 1.0 1 05/21/14 23:15 7440-44-0
Date: 05/28/2014 04:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
Sample: RW-1 Lab ID: 92201331002 Collected: 05/14/14 10:00 Received: 05/14/14 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
359 ug/L
250
100
10
05/22/14 07:13
67-64-1
Benzene
5.3J ug/L
10.0
2.5
10
05/22/14 07:13
71-43-2
Bromobenzene
ND ug/L
10.0
3.0
10
05/22/14 07:13
108-86-1
Bromochloromethane
ND ug/L
10.0
1.7
10
05/22/14 07:13
74-97-5
Bromodichloromethane
ND ug/L
10.0
1.8
10
05/22/14 07:13
75-27-4
Bromoform
ND ug/L
10.0
2.6
10
05/22/14 07:13
75-25-2
Bromomethane
ND ug/L
20.0
2.9
10
05/22/14 07:13
74-83-9
2-Butanone (MEK)
324 ug/L
50.0
9.6
10
05/22/14 07:13
78-93-3
Carbon tetrachloride
ND ug/L
10.0
2.5
10
05/22/14 07:13
56-23-5
Chlorobenzene
ND ug/L
10.0
2.3
10
05/22/14 07:13
108-90-7
Chloroethane
ND ug/L
10.0
5.4
10
05/22/14 07:13
75-00-3
Chloroform
ND ug/L
10.0
1.4
10
05/22/14 07:13
67-66-3
Chloromethane
ND ug/L
10.0
1.1
10
05/22/14 07:13
74-87-3
2-Chlorotoluene
ND ug/L
10.0
3.5
10
05/22/14 07:13
95-49-8
4-Chlorotoluene
ND ug/L
10.0
3.1
10
05/22/14 07:13
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
50.0
25.2
10
05/22/14 07:13
96-12-8
Dibromochloromethane
ND ug/L
10.0
2.1
10
05/22/14 07:13
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
10.0
2.7
10
05/22/14 07:13
106-93-4
Dibromomethane
ND ug/L
10.0
2.1
10
05/22/14 07:13
74-95-3
1,2-Dichlorobenzene
ND ug/L
10.0
3.0
10
05/22/14 07:13
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
2.4
10
05/22/14 07:13
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
3.3
10
05/22/14 07:13
106-46-7
Dichlorodifluoromethane
ND ug/L
10.0
2.1
10
05/22/14 07:13
75-71-8
1,1-Dichloroethane
ND ug/L
10.0
3.2
10
05/22/14 07:13
75-34-3
1,2-Dichloroethane
ND ug/L
10.0
1.2
10
05/22/14 07:13
107-06-2
1,1-Dichloroethene
ND ug/L
10.0
5.6
10
05/22/14 07:13
75-35-4
cis-1,2-Dichloroethene
2380 ug/L
25.0
4.8
25
05/22/14 14:27
156-59-2
trans-1,2-Dichloroethene
7.9J ug/L
10.0
4.9
10
05/22/14 07:13
156-60-5
1,2-Dichloropropane
ND ug/L
10.0
2.7
10
05/22/14 07:13
78-87-5
1,3-Dichloropropane
ND ug/L
10.0
2.8
10
05/22/14 07:13
142-28-9
2,2-Dichloropropane
ND ug/L
10.0
1.3
10
05/22/14 07:13
594-20-7
1,1-Dichloropropene
ND ug/L
10.0
4.9
10
05/22/14 07:13
563-58-6
cis-1,3-Dichloropropene
ND ug/L
10.0
1.3
10
05/22/14 07:13
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
10.0
2.6
10
05/22/14 07:13
10061-02-6
Diisopropyl ether
ND ug/L
10.0
1.2
10
05/22/14 07:13
108-20-3
Ethylbenzene
6.4J ug/L
10.0
3.0
10
05/22/14 07:13
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
10.0
7.1
10
05/22/14 07:13
87-68-3
2-Hexanone
6.9J ug/L
50.0
4.6
10
05/22/14 07:13
591-78-6
p-Isopropyltoluene
ND ug/L
10.0
3.1
10
05/22/14 07:13
99-87-6
Methylene Chloride
40.7 ug/L
20.0
9.7
10
05/22/14 07:13
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
50.0
3.3
10
05/22/14 07:13
108-10-1
Methyl-tert-butyl ether
ND ug/L
10.0
2.1
10
05/22/14 07:13
1634-04-4
Naphthalene
ND ug/L
10.0
2.4
10
05/22/14 07:13
91-20-3
Styrene
ND ug/L
10.0
2.6
10
05/22/14 07:13
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
10.0
3.3
10
05/22/14 07:13
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
10.0
4.0
10
05/22/14 07:13
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
Sample: RW-1
Lab ID: 92201331002
Collected:
05/14/14 10:00
Received: 05/14/14 16:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
225 ug/L
10.0
4.6
10
05/22/14 07:13
127-18-4
Toluene
123 ug/L
10.0
2.6
10
05/22/14 07:13
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
10.0
3.3
10
05/22/14 07:13
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
10.0
3.5
10
05/22/14 07:13
120-82-1
1,1,1-Trichloroethane
ND ug/L
10.0
4.8
10
05/22/14 07:13
71-55-6
1,1,2-Trichloroethane
ND ug/L
10.0
2.9
10
05/22/14 07:13
79-00-5
Trichloroethene
373 ug/L
10.0
4.7
10
05/22/14 07:13
79-01-6
Trichlorofluoromethane
ND ug/L
10.0
2.0
10
05/22/14 07:13
75-69-4
1,2,3-Trichloropropane
ND ug/L
10.0
4.1
10
05/22/14 07:13
96-18-4
Vinyl acetate
ND ug/L
20.0
3.5
10
05/22/14 07:13
108-05-4
Vinyl chloride
23.1 ug/L
10.0
6.2
10
05/22/14 07:13
75-01-4
Xylene (Total)
22.4 ug/L
20.0
6.6
10
05/22/14 07:13
1330-20-7
m&p-Xylene
22.4 ug/L
20.0
6.6
10
05/22/14 07:13
179601-23-1
o-Xylene
7.8J ug/L
10.0
2.3
10
05/22/14 07:13
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
10
05/22/14 07:13
460-00-4
1,2-Dichloroethane-d4 (S)
101 %
70-130
10
05/22/14 07:13
17060-07-0
Toluene-d8 (S)
97 %
70-130
10
05/22/14 07:13
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 667 mg/L 20.0 20.0 20 05/22/14 11:19 7440-44-0
Date: 05/28/2014 04:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
QC Batch: MSV/26908 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92201331002
METHOD BLANK: 1203923
Associated Lab Samples: 92201331002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,1-Trichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,2-Trichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
1,2,3-Trichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2,3-Trichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,2,4-Trichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
05/21/14 22:11
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,3-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,3-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,4-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
2,2-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
2-Butanone (MEK)
ug/L
ND
5.0
05/21/14 22:11
2-Chlorotoluene
ug/L
ND
1.0
05/21/14 22:11
2-Hexanone
ug/L
ND
5.0
05/21/14 22:11
4-Chlorotoluene
ug/L
ND
1.0
05/21/14 22:11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
05/21/14 22:11
Acetone
ug/L
ND
25.0
05/21/14 22:11
Benzene
ug/L
ND
1.0
05/21/14 22:11
Bromobenzene
ug/L
ND
1.0
05/21/14 22:11
Bromochloromethane
ug/L
ND
1.0
05/21/14 22:11
Bromodichloromethane
ug/L
ND
1.0
05/21/14 22:11
Bromoform
ug/L
ND
1.0
05/21/14 22:11
Bromomethane
ug/L
ND
2.0
05/21/14 22:11
Carbon tetrachloride
ug/L
ND
1.0
05/21/14 22:11
Chlorobenzene
ug/L
ND
1.0
05/21/14 22:11
Chloroethane
ug/L
ND
1.0
05/21/14 22:11
Chloroform
ug/L
ND
1.0
05/21/14 22:11
Chloromethane
ug/L
ND
1.0
05/21/14 22:11
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
Dibromochloromethane
ug/L
ND
1.0
05/21/14 22:11
Dibromomethane
ug/L
ND
1.0
05/21/14 22:11
Dichlorodifluoromethane
ug/L
ND
1.0
05/21/14 22:11
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
METHOD BLANK: 1203923
Associated Lab Samples: 92201331002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
05/21/14 22:11
Ethylbenzene
ug/L
ND
1.0
05/21/14 22:11
Hexachloro-1,3-butadiene
ug/L
ND
1.0
05/21/14 22:11
m&p-Xylene
ug/L
ND
2.0
05/21/14 22:11
Methyl-tert-butyl ether
ug/L
ND
1.0
05/21/14 22:11
Methylene Chloride
ug/L
ND
2.0
05/21/14 22:11
Naphthalene
ug/L
ND
1.0
05/21/14 22:11
o-Xylene
ug/L
ND
1.0
05/21/14 22:11
p-Isopropyltoluene
ug/L
ND
1.0
05/21/14 22:11
Styrene
ug/L
ND
1.0
05/21/14 22:11
Tetrachloroethene
ug/L
ND
1.0
05/21/14 22:11
Toluene
ug/L
ND
1.0
05/21/14 22:11
trans-1,2-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
trans- 1,3-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
Trichloroethene
ug/L
ND
1.0
05/21/14 22:11
Trichlorofluoromethane
ug/L
ND
1.0
05/21/14 22:11
Vinyl acetate
ug/L
ND
2.0
05/21/14 22:11
Vinyl chloride
ug/L
ND
1.0
05/21/14 22:11
Xylene (Total)
ug/L
ND
2.0
05/21/14 22:11
1,2-Dichloroethane-d4 (S)
%
102
70-130
05/21/14 22:11
4-Bromofluorobenzene (S)
%
98
70-130
05/21/14 22:11
Toluene-d8 (S)
%
97
70-130
05/21/14 22:11
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1203924
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
56.1
112
70-130
1,1,1-Trichloroethane
ug/L
50
54.0
108
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
55.8
112
70-130
1,1,2-Trichloroethane
ug/L
50
56.6
113
70-130
1,1-Dichloroethane
ug/L
50
52.1
104
70-130
1,1-Dichloroethene
ug/L
50
51.7
103
70-132
1,1-Dichloropropene
ug/L
50
56.0
112
70-130
1,2,3-Trichlorobenzene
ug/L
50
54.5
109
70-135
1,2,3-Trichloropropane
ug/L
50
53.2
106
70-130
1,2,4-Trichlorobenzene
ug/L
50
54.1
108
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
47.0
94
70-130
1,2-Dibromoethane (EDB)
ug/L
50
53.9
108
70-130
1,2-Dichlorobenzene
ug/L
50
55.2
110
70-130
1,2-Dichloroethane
ug/L
50
55.6
111
70-130
1,2-Dichloropropane
ug/L
50
54.7
109
70-130
1,3-Dichlorobenzene
ug/L
50
53.6
107
70-130
1,3-Dichloropropane
ug/L
50
53.9
108
70-130
1,4-Dichlorobenzene
ug/L
50
54.1
108
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
LABORATORY CONTROL SAMPLE:
Parameter
1203924
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
49.9
100
58-145
2-Butanone (MEK)
ug/L
100
98.7
99
70-145
2-Chlorotoluene
ug/L
50
54.1
108
70-130
2-Hexanone
ug/L
100
106
106
70-144
4-Chlorotoluene
ug/L
50
52.4
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
108
108
70-140
Acetone
ug/L
100
101
101
50-175
Benzene
ug/L
50
58.0
116
70-130
Bromobenzene
ug/L
50
54.4
109
70-130
Bromochloromethane
ug/L
50
53.5
107
70-130
Bromodichloromethane
ug/L
50
54.9
110
70-130
Bromoform
ug/L
50
45.8
92
70-130
Bromomethane
ug/L
50
47.8
96
54-130
Carbon tetrachloride
ug/L
50
53.7
107
70-132
Chlorobenzene
ug/L
50
51.4
103
70-130
Chloroethane
ug/L
50
46.7
93
64-134
Chloroform
ug/L
50
52.9
106
70-130
Chloromethane
ug/L
50
44.9
90
64-130
cis-1,2-Dichloroethene
ug/L
50
53.6
107
70-131
cis-1,3-Dichloropropene
ug/L
50
56.2
112
70-130
Dibromochloromethane
ug/L
50
47.1
94
70-130
Dibromomethane
ug/L
50
54.1
108
70-131
Dichlorodifluoromethane
ug/L
50
59.2
118
56-130
Diisopropyl ether
ug/L
50
57.1
114
70-130
Ethylbenzene
ug/L
50
51.0
102
70-130
Hexachloro-1,3-butadiene
ug/L
50
51.4
103
70-130
m&p-Xylene
ug/L
100
103
103
70-130
Methyl-tert-butyl ether
ug/L
50
56.1
112
70-130
Methylene Chloride
ug/L
50
57.7
115
63-130
Naphthalene
ug/L
50
54.4
109
70-138
o-Xylene
ug/L
50
53.1
106
70-130
p-Isopropyltoluene
ug/L
50
53.9
108
70-130
Styrene
ug/L
50
54.8
110
70-130
Tetrachloroethene
ug/L
50
54.5
109
70-130
Toluene
ug/L
50
53.7
107
70-130
trans-1,2-Dichloroethene
ug/L
50
53.3
107
70-130
trans- 1,3-Dichloropropene
ug/L
50
55.2
110
70-132
Trichloroethene
ug/L
50
56.8
114
70-130
Trichlorofluoromethane
ug/L
50
49.7
99
62-133
Vinyl acetate
ug/L
100
117
117
66-157
Vinyl chloride
ug/L
50
62.3
125
69-130
Xylene (Total)
ug/L
150
157
104
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8(S)
%
101
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
MATRIX SPIKE SAMPLE: 1204539
92202095007 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
50
63.5
127
70-130
1,1,1-Trichloroethane
ug/L
ND
50
63.3
127
70-130
1,1,2,2-Tetrachloroethane
ug/L
ND
50
61.4
123
70-130
1,1,2-Trichloroethane
ug/L
ND
50
62.0
124
70-130
1,1-Dichloroethane
ug/L
ND
50
59.9
120
70-130
1,1-Dichloroethene
ug/L
ND
50
60.3
121
70-166
1,1-Dichloropropene
ug/L
ND
50
66.3
133
70-130 MO
1,2,3-Trichlorobenzene
ug/L
ND
50
57.9
116
70-130
1,2,3-Trichloropropane
ug/L
ND
50
58.8
118
70-130
1,2,4-Trichlorobenzene
ug/L
ND
50
57.7
115
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
50
50.3
101
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
50
60.5
121
70-130
1,2-Dichlorobenzene
ug/L
ND
50
60.5
121
70-130
1,2-Dichloroethane
ug/L
ND
50
63.7
127
70-130
1,2-Dichloropropane
ug/L
ND
50
60.6
121
70-130
1,3-Dichlorobenzene
ug/L
ND
50
58.0
116
70-130
1,3-Dichloropropane
ug/L
ND
50
60.3
121
70-130
1,4-Dichlorobenzene
ug/L
ND
50
59.7
119
70-130
2,2-Dichloropropane
ug/L
ND
50
63.0
126
70-130
2-Butanone (MEK)
ug/L
ND
100
113
113
70-130
2-Chlorotoluene
ug/L
ND
50
58.8
118
70-130
2-Hexanone
ug/L
ND
100
118
118
70-130
4-Chlorotoluene
ug/L
ND
50
56.9
114
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
120
120
70-130
Acetone
ug/L
ND
100
117
110
70-130
Benzene
ug/L
ND
50
65.4
131
70-148
Bromobenzene
ug/L
ND
50
58.9
118
70-130
Bromochloromethane
ug/L
ND
50
58.2
116
70-130
Bromodichloromethane
ug/L
ND
50
62.0
124
70-130
Bromoform
ug/L
ND
50
50.2
100
70-130
Bromomethane
ug/L
ND
50
59.3
119
70-130
Carbon tetrachloride
ug/L
ND
50
63.9
128
70-130
Chlorobenzene
ug/L
ND
50
58.1
116
70-146
Chloroethane
ug/L
ND
50
42.6
85
70-130
Chloroform
ug/L
1.4
50
63.5
124
70-130
Chloromethane
ug/L
ND
50
55.4
111
70-130
cis-1,2-Dichloroethene
ug/L
ND
50
60.8
122
70-130
cis-1,3-Dichloropropene
ug/L
ND
50
62.3
125
70-130
Dibromochloromethane
ug/L
ND
50
51.9
104
70-130
Dibromomethane
ug/L
ND
50
60.1
120
70-130
Dichlorodifluoromethane
ug/L
ND
50
66.0
132
70-130
Diisopropyl ether
ug/L
ND
50
64.7
129
70-130
Ethylbenzene
ug/L
ND
50
57.5
115
70-130
Hexachloro-1,3-butadiene
ug/L
ND
50
59.3
119
70-130
m&p-Xylene
ug/L
ND
100
116
116
70-130
Methyl-tert-butyl ether
ug/L
ND
50
62.3
125
70-130
Methylene Chloride
ug/L
ND
50
62.1
124
70-130
Results presented on this page are in the units indicated
by the "Units" column
except where an
alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
MATRIX SPIKE SAMPLE:
Parameter
1204539
Units
92202095007
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Naphthalene
ug/L
ND
50
57.9
116
70-130
o-Xylene
ug/L
ND
50
59.5
119
70-130
p-Isopropyltoluene
ug/L
ND
50
59.7
119
70-130
Styrene
ug/L
ND
50
62.0
124
70-130
Tetrachloroethene
ug/L
ND
50
62.9
126
70-130
Toluene
ug/L
ND
50
61.0
122
70-155
trans-1,2-Dichloroethene
ug/L
ND
50
59.0
118
70-130
trans- 1,3-Dichloropropene
ug/L
ND
50
61.0
122
70-130
Trichloroethene
ug/L
ND
50
65.3
131
69-151
Trichlorofluoromethane
ug/L
ND
50
58.5
117
70-130
Vinyl acetate
ug/L
ND
100
128
128
70-130
Vinyl chloride
ug/L
ND
50
72.0
144
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 1204540
Parameter
Units
92202095008
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,1-Dichloropropene
ug/L
ND
ND
30
1,2,3-Trichlorobenzene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2,4-Trichlorobenzene
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,3-Dichlorobenzene
ug/L
ND
ND
30
1,3-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
2,2-Dichloropropane
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Chlorotoluene
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Chlorotoluene
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
SAMPLE DUPLICATE: 1204540
Parameter
Units
92202095008
Result
Dup
Result
Bromobenzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
8.3
8.6
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
26.8
27.3
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Dichlorodifluoromethane
ug/L
ND
ND
Diisopropyl ether
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methyl-tert-butyl ether
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
p-Isopropyltoluene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
49.7
51.1
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
12.6
12.8
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
100
101
4-Bromofluorobenzene (S)
%
98
98
Toluene-d8 (S)
%
97
97
Max
RPD RPD
4
2
3
2
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
QC Batch: MSV/26961 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92201331001
METHOD BLANK: 1207085
Associated Lab Samples: 92201331001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1,1-Trichloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1,2-Trichloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1-Dichloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1-Dichloroethene
ug/L
ND
1.0
05/27/14 14:44
1,1-Dichloropropene
ug/L
ND
1.0
05/27/14 14:44
1,2,3-Trichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
1,2,3-Trichloropropane
ug/L
ND
1.0
05/27/14 14:44
1,2,4-Trichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
05/27/14 14:44
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/27/14 14:44
1,2-Dichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
1,2-Dichloroethane
ug/L
ND
1.0
05/27/14 14:44
1,2-Dichloropropane
ug/L
ND
1.0
05/27/14 14:44
1,3-Dichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
1,3-Dichloropropane
ug/L
ND
1.0
05/27/14 14:44
1,4-Dichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
2,2-Dichloropropane
ug/L
ND
1.0
05/27/14 14:44
2-Butanone (MEK)
ug/L
ND
5.0
05/27/14 14:44
2-Chlorotoluene
ug/L
ND
1.0
05/27/14 14:44
2-Hexanone
ug/L
ND
5.0
05/27/14 14:44
4-Chlorotoluene
ug/L
ND
1.0
05/27/14 14:44
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
05/27/14 14:44
Acetone
ug/L
ND
25.0
05/27/14 14:44
Benzene
ug/L
ND
1.0
05/27/14 14:44
Bromobenzene
ug/L
ND
1.0
05/27/14 14:44
Bromochloromethane
ug/L
ND
1.0
05/27/14 14:44
Bromodichloromethane
ug/L
ND
1.0
05/27/14 14:44
Bromoform
ug/L
ND
1.0
05/27/14 14:44
Bromomethane
ug/L
ND
2.0
05/27/14 14:44
Carbon tetrachloride
ug/L
ND
1.0
05/27/14 14:44
Chlorobenzene
ug/L
ND
1.0
05/27/14 14:44
Chloroethane
ug/L
ND
1.0
05/27/14 14:44
Chloroform
ug/L
ND
1.0
05/27/14 14:44
Chloromethane
ug/L
ND
1.0
05/27/14 14:44
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/27/14 14:44
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/27/14 14:44
Dibromochloromethane
ug/L
ND
1.0
05/27/14 14:44
Dibromomethane
ug/L
ND
1.0
05/27/14 14:44
Dichlorodifluoromethane
ug/L
ND
1.0
05/27/14 14:44
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
METHOD BLANK: 1207085
Associated Lab Samples: 92201331001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
05/27/14 14:44
Ethylbenzene
ug/L
ND
1.0
05/27/14 14:44
Hexachloro-1,3-butadiene
ug/L
ND
1.0
05/27/14 14:44
m&p-Xylene
ug/L
ND
2.0
05/27/14 14:44
Methyl-tert-butyl ether
ug/L
ND
1.0
05/27/14 14:44
Methylene Chloride
ug/L
ND
2.0
05/27/14 14:44
Naphthalene
ug/L
ND
1.0
05/27/14 14:44
o-Xylene
ug/L
ND
1.0
05/27/14 14:44
p-Isopropyltoluene
ug/L
ND
1.0
05/27/14 14:44
Styrene
ug/L
ND
1.0
05/27/14 14:44
Tetrachloroethene
ug/L
ND
1.0
05/27/14 14:44
Toluene
ug/L
ND
1.0
05/27/14 14:44
trans-1,2-Dichloroethene
ug/L
ND
1.0
05/27/14 14:44
trans- 1,3-Dichloropropene
ug/L
ND
1.0
05/27/14 14:44
Trichloroethene
ug/L
ND
1.0
05/27/14 14:44
Trichlorofluoromethane
ug/L
ND
1.0
05/27/14 14:44
Vinyl acetate
ug/L
ND
2.0
05/27/14 14:44
Vinyl chloride
ug/L
ND
1.0
05/27/14 14:44
Xylene (Total)
ug/L
ND
2.0
05/27/14 14:44
1,2-Dichloroethane-d4 (S)
%
93
70-130
05/27/14 14:44
4-Bromofluorobenzene (S)
%
95
70-130
05/27/14 14:44
Toluene-d8 (S)
%
98
70-130
05/27/14 14:44
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1207086
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
57.1
114
70-130
1,1,1-Trichloroethane
ug/L
50
52.5
105
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
58.1
116
70-130
1,1,2-Trichloroethane
ug/L
50
55.4
111
70-130
1,1-Dichloroethane
ug/L
50
51.8
104
70-130
1,1-Dichloroethene
ug/L
50
53.3
107
70-132
1,1-Dichloropropene
ug/L
50
56.6
113
70-130
1,2,3-Trichlorobenzene
ug/L
50
56.2
112
70-135
1,2,3-Trichloropropane
ug/L
50
54.5
109
70-130
1,2,4-Trichlorobenzene
ug/L
50
58.0
116
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
54.2
108
70-130
1,2-Dibromoethane (EDB)
ug/L
50
54.6
109
70-130
1,2-Dichlorobenzene
ug/L
50
55.8
112
70-130
1,2-Dichloroethane
ug/L
50
53.3
107
70-130
1,2-Dichloropropane
ug/L
50
54.6
109
70-130
1,3-Dichlorobenzene
ug/L
50
54.0
108
70-130
1,3-Dichloropropane
ug/L
50
56.1
112
70-130
1,4-Dichlorobenzene
ug/L
50
54.5
109
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 23

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
LABORATORY CONTROL SAMPLE:
Parameter
1207086
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
55.0
110
58-145
2-Butanone (MEK)
ug/L
100
104
104
70-145
2-Chlorotoluene
ug/L
50
54.0
108
70-130
2-Hexanone
ug/L
100
112
112
70-144
4-Chlorotoluene
ug/L
50
54.0
108
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
105
105
70-140
Acetone
ug/L
100
106
106
50-175
Benzene
ug/L
50
58.8
118
70-130
Bromobenzene
ug/L
50
55.7
111
70-130
Bromochloromethane
ug/L
50
53.8
108
70-130
Bromodichloromethane
ug/L
50
52.9
106
70-130
Bromoform
ug/L
50
57.0
114
70-130
Bromomethane
ug/L
50
32.5
65
54-130
Carbon tetrachloride
ug/L
50
52.0
104
70-132
Chlorobenzene
ug/L
50
52.9
106
70-130
Chloroethane
ug/L
50
46.4
93
64-134
Chloroform
ug/L
50
52.6
105
70-130
Chloromethane
ug/L
50
39.7
79
64-130
cis-1,2-Dichloroethene
ug/L
50
52.1
104
70-131
cis-1,3-Dichloropropene
ug/L
50
56.4
113
70-130
Dibromochloromethane
ug/L
50
54.4
109
70-130
Dibromomethane
ug/L
50
52.5
105
70-131
Dichlorodifluoromethane
ug/L
50
57.4
115
56-130
Diisopropyl ether
ug/L
50
52.5
105
70-130
Ethylbenzene
ug/L
50
52.9
106
70-130
Hexachloro-1,3-butadiene
ug/L
50
46.1
92
70-130
m&p-Xylene
ug/L
100
108
108
70-130
Methyl-tert-butyl ether
ug/L
50
54.2
108
70-130
Methylene Chloride
ug/L
50
60.6
121
63-130
Naphthalene
ug/L
50
62.8
126
70-138
o-Xylene
ug/L
50
54.6
109
70-130
p-Isopropyltoluene
ug/L
50
54.0
108
70-130
Styrene
ug/L
50
58.0
116
70-130
Tetrachloroethene
ug/L
50
54.8
110
70-130
Toluene
ug/L
50
54.4
109
70-130
trans-1,2-Dichloroethene
ug/L
50
52.7
105
70-130
trans- 1,3-Dichloropropene
ug/L
50
54.3
109
70-132
Trichloroethene
ug/L
50
56.9
114
70-130
Trichlorofluoromethane
ug/L
50
49.3
99
62-133
Vinyl acetate
ug/L
100
114
114
66-157
Vinyl chloride
ug/L
50
63.3
127
69-130
Xylene (Total)
ug/L
150
162
108
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1207719
1207720
MS
MSD
92202617035
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,1-Dichloroethene
ug/L
ND
50
50
53.6
50.4
107
101
70-166
6
30
Benzene
ug/L
ND
50
50
61.7
57.3
123
115
70-148
8
30
Chlorobenzene
ug/L
ND
50
50
55.2
52.1
110
104
70-146
6
30
Toluene
ug/L
ND
50
50
53.9
49.7
108
99
70-155
8
30
Trichloroethene
ug/L
ND
50
50
60.8
57.0
122
114
69-151
6
30
1,2-Dichloroethane-d4(S)
%
88
89
70-130
4-Bromofluorobenzene (S)
%
95
97
70-130
Toluene-d8(S)
%
98
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 18 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
QC Batch: WETA/19054
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92201331001, 92201331002
METHOD BLANK: 1203097
Matrix: Water
Associated Lab Samples: 92201331001, 92201331002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
05/21/14 17:51
LABORATORY CONTROL SAMPLE: 1203098
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 23.8
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1203099 1203100
MS MSD
92201069001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 12.4
25 25 33.4
32.9 84 82 75-125 1 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1203101 1203102
MS MSD
92201026011 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 1.9 25 25 27.4 27.1 102 101 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 19 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201331
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92201331001
MW-6
EPA 8260
MSV/26961
92201331002
RW-1
EPA 8260
MSV/26908
92201331001
MW-6
SM 5310B
WETA/19054
92201331002
RW-1
SM 5310B
WETA/19054
Date: 05/28/2014 04:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 21 of 23

Document Name: Sample Condition Upon
aceAnalytical" Recei t scull)
www.pocolabs.com
Document No.:
F-ASV-CS-003-rev.13
Client Name: 121 1 —
Document Revised: April 9, 2014
Page 1 of 2
Issuing Authorities:
Pace Asheville Qualitv Office
Courier (Circle): Fed Ex UPS USPS CI e Commercial Pace Other
Custody Seal on Cooler/Box Present: yes no Seals intact: yes [] no
Packing Material: 0 Bubble Wrap ZBubble Bags 1� None Other
6 5963
Thermometer Used: Gun#3 -jfType of Ice: W ' Blue None Samples on ice, cooling process has begun
O er• "
Temp Correction Factor, Add / Subtract . ® C
Corrected
Corrected Cooler Temp.: C
Biological Tissue is Frozen: Yes No N/A Date and In of person
Temp should be above freezing to 6°C
Comments: contents: o CS ILA N
Chain of Custody Present:
EKes
❑No
❑N/A
1.
Chain of Custody Filled Out:
e
El No
El NIA
2.
Chain of Custody Relinquished:
Ye
ONO
❑N/A
3.
Sampler Name & Signature on COC:
Ye
ONO
❑N/A
4.
Samples Arrived within Hold Time:
Zryes
❑No
❑N/A
5.
Short Hold Time Analysis (<72hr):
Dyes
No
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
No
❑N/A
7.
Sufficient Volume:
a
ONO
❑N/A
8.
Correct Containers Used:
Yes ONO
❑N/A
9.
-Pace Containers Used:
C Ye
❑No
❑N/A
Containers Intact:
Yes
❑No
❑N/A
10.
Filtered volume received for Dissolved tests
❑Yes
No
C94A
11.
Sample Labels match COC:
19K.
ONO
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
wl�:
All containers needing preservation have been checked.
Yes
ONO
❑N/A
13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
lJYes
ONO
El N/A
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
❑Yes
eN.
Samples checked for dechlorination:
❑Yes
ONO,.,
N/A
14.
Headspace in VOA Vials (>6mm):
❑Yes
No
❑N/A
15.
Trip Blank Present:
❑Yes
ONO
/A
16.
Trip Blank Custody Seals Present
❑Yes
ONO
/A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
Date/Time:
SRF Review: / 4f) Date: sle l t1
Note: Whenev r ere is a discrepancy affecting North Carolina
compliance san1ples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y / N
Place label here
1 '2 z.6,,/33 / OR
Handwrite project number
(if no label available)
Page 22 of 23

FaeeAnalytical
w .pacelahs.cem
Section A
Required Client information:
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section S Section C
Required Project Information: Invoice Information:
Page: ! of
Company:
Lft
Report To:A;Z
' ` 7
Address:
hjCnl�idin ` _
Copy To:
Company Name:
REGULATORY AGENCY
,r w(
??
Address: -
NPDES GROUND WATER
- UST RCRA
;- DRINKING WATER
OTHER
Email To: le LL`_ �
C°
Purchase Order No.:
Paco O;:ote
63�'it.of . to �+'�
Rer:•.�nce
F rne- „ i A Fes' t_�, 'r� ��y
-(A0, t7*, C%� 'i'�iR3
Project Name:
�Ot t/ -��a
Pace Pro;ec±
r+ara0er:
Site Location
STATE:
Requested Due Date/TAT: car +
0.
Project Number: - lou -
Pace Prone P:
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
-
--
y
Z
Required Chen; ir.'ormaticn hdATRiX i
COCE
-
COLLECT=D
Preservatives
>
I
Drink i
U
z
Wate
VVT
-s
-
f
Waste Wafer
4^,nld
•- M sTe
ro rw^,ire
t
i
t
Product
P
=
<
>Tu.T
c�.G+GRAa
j
z
SoiliSclid
SAMPLE ID Oil
SL
OL
M
;
,a,
y
I
(A-Z, 0-9 i .-) Air AR
p
m
a.
Fa)
I
o
��
Sample !Ds MUST BE UNIQUE Tissue
TS
O
u
rn
v'a
44•
i
'"
Other
OT
O
=
tjj
a
to
F
`t
<
G
C
a
Z
C.i
cS
r5
=
Q
o
n
-
a
DATE
TIME
DATE
TIME
_
z
z
�
O
y
f -
I
�
�
Pace Project NoJ Lao E.D.
1
y�
MW—co
'�•1�`t4
t25-
G�
1
2
itlf
b 1'E
ko
{p
X
3
4
I
f
J
I
7
8
g
)
i
{
I
I
I
10
I
I
11
EI
1z
I
I
ADDITIONAL COMMENTS
RELINQUISHED BY J AFFILIATION
DATE
TIME
ACCEPTED BY f AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
5�
�GD3a
{ 21
fEie�j�
lei
IA
I
I
i
i
I
i
i
E
I
SAMPLER NAME AND SIGNATURE
-
`P
GI �AL.
PRINT Name of SAMPLER:
SIGNATURE of a'A<v1PLER:
DATE Signed
�7/it
i&iAl1DD.YYI:
ti ; 2007

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
May 27, 2014
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
RE: Project: FORMERANDREX IND J14-1022-38
Pace Project No.: 92201335
Dear Mr. Alexander:
Enclosed are the analytical results for sample(s) received by the laboratory on May 14, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 17

aceAnalytical
—pacelabsxom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
Lab ID Sample ID
92201335001 MW-44
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 05/14/1412:00 05/14/1416:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92201335001 MW-44 EPA 8260 GAW 63 PASI-C
SM 5310B SAE 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
Sample: MW-44 Lab ID: 92201335001 Collected: 05/14/14 12:00 Received: 05/14/14 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
10.0
1
05/22/14 07:46
67-64-1
Benzene
ND ug/L
1.0
0.25
1
05/22/14 07:46
71-43-2
Bromobenzene
ND ug/L
1.0
0.30
1
05/22/14 07:46
108-86-1
Bromochloromethane
ND ug/L
1.0
0.17
1
05/22/14 07:46
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.18
1
05/22/14 07:46
75-27-4
Bromoform
ND ug/L
1.0
0.26
1
05/22/14 07:46
75-25-2
Bromomethane
ND ug/L
2.0
0.29
1
05/22/14 07:46
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
0.96
1
05/22/14 07:46
78-93-3
Carbon tetrachloride
ND ug/L
1.0
0.25
1
05/22/14 07:46
56-23-5
Chlorobenzene
0.90J ug/L
1.0
0.23
1
05/22/14 07:46
108-90-7
Chloroethane
ND ug/L
1.0
0.54
1
05/22/14 07:46
75-00-3
Chloroform
ND ug/L
1.0
0.14
1
05/22/14 07:46
67-66-3
Chloromethane
ND ug/L
1.0
0.11
1
05/22/14 07:46
74-87-3
2-Chlorotoluene
ND ug/L
1.0
0.35
1
05/22/14 07:46
95-49-8
4-Chlorotoluene
ND ug/L
1.0
0.31
1
05/22/14 07:46
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
2.5
1
05/22/14 07:46
96-12-8
Dibromochloromethane
ND ug/L
1.0
0.21
1
05/22/14 07:46
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
0.27
1
05/22/14 07:46
106-93-4
Dibromomethane
ND ug/L
1.0
0.21
1
05/22/14 07:46
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
0.30
1
05/22/14 07:46
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
0.24
1
05/22/14 07:46
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
0.33
1
05/22/14 07:46
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
0.21
1
05/22/14 07:46
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
0.32
1
05/22/14 07:46
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
0.12
1
05/22/14 07:46
107-06-2
1,1-Dichloroethene
0.85J ug/L
1.0
0.56
1
05/22/14 07:46
75-35-4
cis-1,2-Dichloroethene
670 ug/L
20.0
3.8
20
05/22/14 14:43
156-59-2
trans-1,2-Dichloroethene
4.9 ug/L
1.0
0.49
1
05/22/14 07:46
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
0.27
1
05/22/14 07:46
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
0.28
1
05/22/14 07:46
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
0.13
1
05/22/14 07:46
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
0.49
1
05/22/14 07:46
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
0.13
1
05/22/14 07:46
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
0.26
1
05/22/14 07:46
10061-02-6
Diisopropyl ether
ND ug/L
1.0
0.12
1
05/22/14 07:46
108-20-3
Ethylbenzene
ND ug/L
1.0
0.30
1
05/22/14 07:46
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
0.71
1
05/22/14 07:46
87-68-3
2-Hexanone
ND ug/L
5.0
0.46
1
05/22/14 07:46
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
0.31
1
05/22/14 07:46
99-87-6
Methylene Chloride
ND ug/L
2.0
0.97
1
05/22/14 07:46
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
0.33
1
05/22/14 07:46
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
0.21
1
05/22/14 07:46
1634-04-4
Naphthalene
ND ug/L
1.0
0.24
1
05/22/14 07:46
91-20-3
Styrene
ND ug/L
1.0
0.26
1
05/22/14 07:46
100-42-5
1,1,1,2-Tetrachloroethane
0.80J ug/L
1.0
0.33
1
05/22/14 07:46
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
0.40
1
05/22/14 07:46
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
Sample: MW-44
Lab ID: 92201335001
Collected:
05/14/14 12:00
Received: 05/14/14 16:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
3000 ug/L
20.0
9.2
20
05/22/14 14:43
127-18-4
Toluene
ND ug/L
1.0
0.26
1
05/22/14 07:46
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
0.33
1
05/22/14 07:46
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
0.35
1
05/22/14 07:46
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
0.48
1
05/22/14 07:46
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
0.29
1
05/22/14 07:46
79-00-5
Trichloroethene
170 ug/L
20.0
9.4
20
05/22/14 14:43
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
0.20
1
05/22/14 07:46
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
0.41
1
05/22/14 07:46
96-18-4
Vinyl acetate
ND ug/L
2.0
0.35
1
05/22/14 07:46
108-05-4
Vinyl chloride
23.6 ug/L
1.0
0.62
1
05/22/14 07:46
75-01-4
Xylene (Total)
ND ug/L
2.0
0.66
1
05/22/14 07:46
1330-20-7
m&p-Xylene
ND ug/L
2.0
0.66
1
05/22/14 07:46
179601-23-1
o-Xylene
ND ug/L
1.0
0.23
1
05/22/14 07:46
95-47-6
Surrogates
4-Bromofluorobenzene (S)
90 %
70-130
1
05/22/14 07:46
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
05/22/14 07:46
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
05/22/14 07:46
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 4.8 mg/L 1.0 1.0 1 05/22/14 20:48 7440-44-0
Date: 05/27/2014 01:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
QC Batch: MSV/26908 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92201335001
METHOD BLANK: 1203923
Associated Lab Samples: 92201335001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,1-Trichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,2-Trichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
1,2,3-Trichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2,3-Trichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,2,4-Trichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
05/21/14 22:11
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,3-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,3-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,4-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
2,2-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
2-Butanone (MEK)
ug/L
ND
5.0
05/21/14 22:11
2-Chlorotoluene
ug/L
ND
1.0
05/21/14 22:11
2-Hexanone
ug/L
ND
5.0
05/21/14 22:11
4-Chlorotoluene
ug/L
ND
1.0
05/21/14 22:11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
05/21/14 22:11
Acetone
ug/L
ND
25.0
05/21/14 22:11
Benzene
ug/L
ND
1.0
05/21/14 22:11
Bromobenzene
ug/L
ND
1.0
05/21/14 22:11
Bromochloromethane
ug/L
ND
1.0
05/21/14 22:11
Bromodichloromethane
ug/L
ND
1.0
05/21/14 22:11
Bromoform
ug/L
ND
1.0
05/21/14 22:11
Bromomethane
ug/L
ND
2.0
05/21/14 22:11
Carbon tetrachloride
ug/L
ND
1.0
05/21/14 22:11
Chlorobenzene
ug/L
ND
1.0
05/21/14 22:11
Chloroethane
ug/L
ND
1.0
05/21/14 22:11
Chloroform
ug/L
ND
1.0
05/21/14 22:11
Chloromethane
ug/L
ND
1.0
05/21/14 22:11
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
Dibromochloromethane
ug/L
ND
1.0
05/21/14 22:11
Dibromomethane
ug/L
ND
1.0
05/21/14 22:11
Dichlorodifluoromethane
ug/L
ND
1.0
05/21/14 22:11
Diisopropyl ether
ug/L
ND
1.0
05/21/14 22:11
Ethylbenzene
ug/L
ND
1.0
05/21/14 22:11
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
METHOD BLANK: 1203923
Associated Lab Samples: 92201335001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
1.0
05/21/14 22:11
m&p-Xylene
ug/L
ND
2.0
05/21/14 22:11
Methyl-tert-butyl ether
ug/L
ND
1.0
05/21/14 22:11
Methylene Chloride
ug/L
ND
2.0
05/21/14 22:11
Naphthalene
ug/L
ND
1.0
05/21/14 22:11
o-Xylene
ug/L
ND
1.0
05/21/14 22:11
p-Isopropyltoluene
ug/L
ND
1.0
05/21/14 22:11
Styrene
ug/L
ND
1.0
05/21/14 22:11
Tetrachloroethene
ug/L
ND
1.0
05/21/14 22:11
Toluene
ug/L
ND
1.0
05/21/14 22:11
trans-1,2-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
trans- 1,3-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
Trichloroethene
ug/L
ND
1.0
05/21/14 22:11
Trichlorofluoromethane
ug/L
ND
1.0
05/21/14 22:11
Vinyl acetate
ug/L
ND
2.0
05/21/14 22:11
Vinyl chloride
ug/L
ND
1.0
05/21/14 22:11
Xylene (Total)
ug/L
ND
2.0
05/21/14 22:11
1,2-Dichloroethane-d4 (S)
%
102
70-130
05/21/14 22:11
4-Bromofluorobenzene (S)
%
98
70-130
05/21/14 22:11
Toluene-d8 (S)
%
97
70-130
05/21/14 22:11
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1203924
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
56.1
112
70-130
1,1,1-Trichloroethane
ug/L
50
54.0
108
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
55.8
112
70-130
1,1,2-Trichloroethane
ug/L
50
56.6
113
70-130
1,1-Dichloroethane
ug/L
50
52.1
104
70-130
1,1-Dichloroethene
ug/L
50
51.7
103
70-132
1,1-Dichloropropene
ug/L
50
56.0
112
70-130
1,2,3-Trichlorobenzene
ug/L
50
54.5
109
70-135
1,2,3-Trichloropropane
ug/L
50
53.2
106
70-130
1,2,4-Trichlorobenzene
ug/L
50
54.1
108
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
47.0
94
70-130
1,2-Dibromoethane (EDB)
ug/L
50
53.9
108
70-130
1,2-Dichlorobenzene
ug/L
50
55.2
110
70-130
1,2-Dichloroethane
ug/L
50
55.6
111
70-130
1,2-Dichloropropane
ug/L
50
54.7
109
70-130
1,3-Dichlorobenzene
ug/L
50
53.6
107
70-130
1,3-Dichloropropane
ug/L
50
53.9
108
70-130
1,4-Dichlorobenzene
ug/L
50
54.1
108
70-130
2,2-Dichloropropane
ug/L
50
49.9
100
58-145
2-Butanone (MEK)
ug/L
100
98.7
99
70-145
2-Chlorotoluene
ug/L
50
54.1
108
70-130
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
LABORATORY CONTROL SAMPLE:
Parameter
1203924
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2-Hexanone
ug/L
100
106
106
70-144
4-Chlorotoluene
ug/L
50
52.4
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
108
108
70-140
Acetone
ug/L
100
101
101
50-175
Benzene
ug/L
50
58.0
116
70-130
Bromobenzene
ug/L
50
54.4
109
70-130
Bromochloromethane
ug/L
50
53.5
107
70-130
Bromodichloromethane
ug/L
50
54.9
110
70-130
Bromoform
ug/L
50
45.8
92
70-130
Bromomethane
ug/L
50
47.8
96
54-130
Carbon tetrachloride
ug/L
50
53.7
107
70-132
Chlorobenzene
ug/L
50
51.4
103
70-130
Chloroethane
ug/L
50
46.7
93
64-134
Chloroform
ug/L
50
52.9
106
70-130
Chloromethane
ug/L
50
44.9
90
64-130
cis-1,2-Dichloroethene
ug/L
50
53.6
107
70-131
cis-1,3-Dichloropropene
ug/L
50
56.2
112
70-130
Dibromochloromethane
ug/L
50
47.1
94
70-130
Dibromomethane
ug/L
50
54.1
108
70-131
Dichlorodifluoromethane
ug/L
50
59.2
118
56-130
Diisopropyl ether
ug/L
50
57.1
114
70-130
Ethylbenzene
ug/L
50
51.0
102
70-130
Hexachloro-1,3-butadiene
ug/L
50
51.4
103
70-130
m&p-Xylene
ug/L
100
103
103
70-130
Methyl-tert-butyl ether
ug/L
50
56.1
112
70-130
Methylene Chloride
ug/L
50
57.7
115
63-130
Naphthalene
ug/L
50
54.4
109
70-138
o-Xylene
ug/L
50
53.1
106
70-130
p-Isopropyltoluene
ug/L
50
53.9
108
70-130
Styrene
ug/L
50
54.8
110
70-130
Tetrachloroethene
ug/L
50
54.5
109
70-130
Toluene
ug/L
50
53.7
107
70-130
trans-1,2-Dichloroethene
ug/L
50
53.3
107
70-130
trans- 1,3-Dichloropropene
ug/L
50
55.2
110
70-132
Trichloroethene
ug/L
50
56.8
114
70-130
Trichlorofluoromethane
ug/L
50
49.7
99
62-133
Vinyl acetate
ug/L
100
117
117
66-157
Vinyl chloride
ug/L
50
62.3
125
69-130
Xylene (Total)
ug/L
150
157
104
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE SAMPLE:
Parameter
1,1,1,2-Tetrachloroethane
Date: 05/27/2014 01:38 PM
1204539
ug/L
92202095007 Spike
Units Result Conc.
ND 50
MS
Result
63.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
MS % Rec
% Rec Limits Qualifiers
127 70-130
Page 9 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
MATRIX SPIKE SAMPLE: 1204539
92202095007 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane
ug/L
ND
50
63.3
127
70-130
1,1,2,2-Tetrachloroethane
ug/L
ND
50
61.4
123
70-130
1,1,2-Trichloroethane
ug/L
ND
50
62.0
124
70-130
1,1-Dichloroethane
ug/L
ND
50
59.9
120
70-130
1,1-Dichloroethene
ug/L
ND
50
60.3
121
70-166
1,1-Dichloropropene
ug/L
ND
50
66.3
133
70-130 MO
1,2,3-Trichlorobenzene
ug/L
ND
50
57.9
116
70-130
1,2,3-Trichloropropane
ug/L
ND
50
58.8
118
70-130
1,2,4-Trichlorobenzene
ug/L
ND
50
57.7
115
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
50
50.3
101
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
50
60.5
121
70-130
1,2-Dichlorobenzene
ug/L
ND
50
60.5
121
70-130
1,2-Dichloroethane
ug/L
ND
50
63.7
127
70-130
1,2-Dichloropropane
ug/L
ND
50
60.6
121
70-130
1,3-Dichlorobenzene
ug/L
ND
50
58.0
116
70-130
1,3-Dichloropropane
ug/L
ND
50
60.3
121
70-130
1,4-Dichlorobenzene
ug/L
ND
50
59.7
119
70-130
2,2-Dichloropropane
ug/L
ND
50
63.0
126
70-130
2-Butanone (MEK)
ug/L
ND
100
113
113
70-130
2-Chlorotoluene
ug/L
ND
50
58.8
118
70-130
2-Hexanone
ug/L
ND
100
118
118
70-130
4-Chlorotoluene
ug/L
ND
50
56.9
114
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
120
120
70-130
Acetone
ug/L
ND
100
117
110
70-130
Benzene
ug/L
ND
50
65.4
131
70-148
Bromobenzene
ug/L
ND
50
58.9
118
70-130
Bromochloromethane
ug/L
ND
50
58.2
116
70-130
Bromodichloromethane
ug/L
ND
50
62.0
124
70-130
Bromoform
ug/L
ND
50
50.2
100
70-130
Bromomethane
ug/L
ND
50
59.3
119
70-130
Carbon tetrachloride
ug/L
ND
50
63.9
128
70-130
Chlorobenzene
ug/L
ND
50
58.1
116
70-146
Chloroethane
ug/L
ND
50
42.6
85
70-130
Chloroform
ug/L
1.4
50
63.5
124
70-130
Chloromethane
ug/L
ND
50
55.4
111
70-130
cis-1,2-Dichloroethene
ug/L
ND
50
60.8
122
70-130
cis-1,3-Dichloropropene
ug/L
ND
50
62.3
125
70-130
Dibromochloromethane
ug/L
ND
50
51.9
104
70-130
Dibromomethane
ug/L
ND
50
60.1
120
70-130
Dichlorodifluoromethane
ug/L
ND
50
66.0
132
70-130
Diisopropyl ether
ug/L
ND
50
64.7
129
70-130
Ethylbenzene
ug/L
ND
50
57.5
115
70-130
Hexachloro-1,3-butadiene
ug/L
ND
50
59.3
119
70-130
m&p-Xylene
ug/L
ND
100
116
116
70-130
Methyl-tert-butyl ether
ug/L
ND
50
62.3
125
70-130
Methylene Chloride
ug/L
ND
50
62.1
124
70-130
Naphthalene
ug/L
ND
50
57.9
116
70-130
o-Xylene
ug/L
ND
50
59.5
119
70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
MATRIX SPIKE SAMPLE:
Parameter
1204539
Units
92202095007
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
p-Isopropyltoluene
ug/L
ND
50
59.7
119
70-130
Styrene
ug/L
ND
50
62.0
124
70-130
Tetrachloroethene
ug/L
ND
50
62.9
126
70-130
Toluene
ug/L
ND
50
61.0
122
70-155
trans-1,2-Dichloroethene
ug/L
ND
50
59.0
118
70-130
trans- 1,3-Dichloropropene
ug/L
ND
50
61.0
122
70-130
Trichloroethene
ug/L
ND
50
65.3
131
69-151
Trichlorofluoromethane
ug/L
ND
50
58.5
117
70-130
Vinyl acetate
ug/L
ND
100
128
128
70-130
Vinyl chloride
ug/L
ND
50
72.0
144
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 1204540
Parameter
Units
92202095008
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,1-Dichloropropene
ug/L
ND
ND
30
1,2,3-Trichlorobenzene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2,4-Trichlorobenzene
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,3-Dichlorobenzene
ug/L
ND
ND
30
1,3-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
2,2-Dichloropropane
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Chlorotoluene
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Chlorotoluene
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromobenzene
ug/L
ND
ND
30
Bromochloromethane
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 11 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
SAMPLE DUPLICATE: 1204540
Parameter
Units
92202095008
Result
Dup
Result
Bromomethane
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
8.3
8.6
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
26.8
27.3
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Dichlorodifluoromethane
ug/L
ND
ND
Diisopropyl ether
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methyl-tert-butyl ether
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
p-Isopropyltoluene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
49.7
51.1
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
12.6
12.8
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
100
101
4-Bromofluorobenzene (S)
%
98
98
Toluene-d8 (S)
%
97
97
Date: 05/27/2014 01:38 PM
Max
RPD RPD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
4
2
3
2
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Qualifiers
Page 12 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
QC Batch: WETA/19083
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92201335001
METHOD BLANK: 1204906
Matrix: Water
Associated Lab Samples: 92201335001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
05/22/14 20:16
LABORATORY CONTROL SAMPLE: 1204907
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 24.1
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1204908 1204909
MS MSD
92201335001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 4.8
25 25 27.8
27.9 92 93 75-125 0 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1204910 1204911
MS MSD
92201952001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 5.8 25 25 27.2 27.3 86 86 75-125 0 20
Date: 05/27/2014 01:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201335
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92201335001
92201335001
MW-44
MW-44
EPA 8260
SM 5310B
MSV/26908
WETA/19083
Date: 05/27/2014 01:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 15 of 17

Document Name: Sample Condition Upon
( waceAnalytical'
I Document No.:
F-ASV-CS-003-rev 13
Client Name:
Fm-
7—
Document Revised: April 9, 2014
Page 1 of 2
Issuing Authorities:
Pace Asheville Qualitv Office
Courier (Circle): Fed Ex UPS USPS Client t Commercial Pace Other
Custody Seal on Cooler/Box Present: yes no Seals intact: [] yes R no
Packing Material: f—] Bubble Wrap 2 Bubble Bags E] None Other
Thermometer Used: Gun#3,a`i6265i83 Type of Ice: W '• Blue None Samples on ice, cooling process has begun
O er• �..�
Temp Correction Factor: Add / Subtract 0. () C
Corrected Cooler Temp.: 5= U C
Biological Tissue is Frozen: Yes No N/A Date and Initi Is of erson xamning
I
9
Temp should be above freezing to 6°C
contents: I 1 �(
Comments:
Chain of of Custody Present:
es
❑No
❑N/A
1.
Chain of Custody Filled Out:
e
❑No
❑N/A
2.
Chain of Custody Relinquished:
Ye
❑No
❑N/A
3.
Sampler Name & Signature on COC:
dYeg,
❑No
❑N/A
4.
Samples Arrived within Hold Time:
Yes
❑No
❑N/A
5.
Short Hold Time Analysis (<72hr):
Dyes
No
❑N/A
6.
Rush Turn Around Time Requested:
Oyes
o
❑N/A
7.
Sufficient Volume:
e
❑No
❑N/A
8.
Correct Containers Used:
Oyes ❑No
❑N/A
9.
-Pace Containers Used:
Ea1Ye
❑No
❑N/A
Containers Intact:
Z 2Y"es
❑No
❑N/A
10.
Filtered volume received for Dissolved tests
Dye s
No
/A
11.
Sample Labels match COC:
es
ON.
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
Li�f
All containers needing preservation have been checked.
Yes
ONo
❑N/A
13.
All containers needing preservation are found to be in
'LJYes
compliance with EPA recommendation.
❑No
❑N/A
exceptions: VOA, coliform, TOC, 0&G, WI-DRO (water)
Dyes
ZNo
01
Samples checked for dechlorination:
❑Yes
❑No
N/A
14.
Headspace in VOA Vials (>6mm):
Dyes
No
❑N/A
ol 5.
Trip Blank Present:
Dyes
❑No
12NNA
6.
Trip Blank Custody Seals Present
Dyes
❑No
/A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
Date/Time:
SRF Review: / `Date: IZZLIY
Note: WheneverWere is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y / N
Place label here
:330' OR
Handwrite project number
(if no label available)
Page 16 of 17

CHAIN -OF -CUSTODY / Analytical Request Document
Pke /€na yfica /'
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
w .pacelabs_com
Section A
Section B
Page:
Section C
iPage: of
Required Client Information:
Required Client Information:
Required Project Information:
Required Project Information:
Invoice
Invoice Informations
Company:
-
Report To:
Attention:
,<.
Address: j .tJM p 0M
(1T'f'
Copy -o:
Company Name:
REGULATORY AGENCY
;.
t
(JftAAp
Address: `
? a wLt.
NPDES GROUND'A'ATER
; DRINKINGLVATER
Email To:
Purchase Order
No.:
Pace Cuotz
l� M
P n � W4,5 • u
('�D
Project Name:
j
OdMB.f Wee
-�"
•ems
Reference:
Part Project
UST RCRA
Site Location
- OTHER
Requested Due DaterrAT:
Project Number
_Lys
manager:
Paoe Prof. 7
t
5
STATE:
Requested
Analysis
Filtered
(YIN)
i
Section Q Matrix Codes
-,
�"
I
Required Client lrrformatlon
MATRIX !
CGDE
x
C
COLLECTED
Preservatives
Drinking 'rVater DVt'
r
O
Water
lVT
3
0
Waste Water
VV:N
co�+Posr_
caMrosire
�-
Product
SoillSolid
P
SL
-
¢
L
vo;cr
}
SAMPLE ID
Oil
OL
a
(A-Z. 0-9 i .-)ipe .-".R
o!
E
Z
d
I
r
.`
Sample IDs MUST BE UNIQUE
Tissue
Other
TS
OT
p
O
}
<
Z
O
e
I
t
to
�agUJ
V3
I
Lve
If`/ �
ry
J�
�
J
n
to
2
p
?
m
W
~
a
m
I
0
O
Z
,
Q
yy� -
DATE
TIhViE
DATE
TfhtE
'n
S
S
Z
Z
TL
O
I
i
I Iz
Pace Project Nod Lab €w
I�r�t
I fa
(
5•s�•-
tZao
�
�I
X
I
I
ADDITIONAL COMMENTS I RELINQUISHED aY / AFFILIATION DATE I T€ME
I <-'I�L LeL Ir_
SAMPLER NAME AND SIGNATURE
IN '
_-.. PRINT Name of SAMPLER:
SIGNATURE of SAMPLER:
aC _ _ m.� s 4 - oe. e-i , :err e .:
ACCEPTED BY I AFFILIATION
DATE TIME SAMPLE CONDITIONS
0
I`
N
rn
t6
d

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
May 27, 2014
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
RE: Project: FORMERANDREX IND J14-1022-38
Pace Project No.: 92201336
Dear Mr. Alexander:
Enclosed are the analytical results for sample(s) received by the laboratory on May 14, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 17

aceAnalytical
—pacelabsxom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
Lab ID Sample ID
92201336001 IW-2
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 05/14/14 09:00 05/14/14 16:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92201336001 IW-2 EPA 8260 GAW 63 PASI-C
SM 5310B SAE 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
Sample: IW-2 Lab ID: 92201336001 Collected: 05/14/14 09:00 Received: 05/14/14 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
10.0
1
05/22/14 07:30
67-64-1
Benzene
ND ug/L
1.0
0.25
1
05/22/14 07:30
71-43-2
Bromobenzene
ND ug/L
1.0
0.30
1
05/22/14 07:30
108-86-1
Bromochloromethane
ND ug/L
1.0
0.17
1
05/22/14 07:30
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.18
1
05/22/14 07:30
75-27-4
Bromoform
ND ug/L
1.0
0.26
1
05/22/14 07:30
75-25-2
Bromomethane
ND ug/L
2.0
0.29
1
05/22/14 07:30
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
0.96
1
05/22/14 07:30
78-93-3
Carbon tetrachloride
ND ug/L
1.0
0.25
1
05/22/14 07:30
56-23-5
Chlorobenzene
0.37J ug/L
1.0
0.23
1
05/22/14 07:30
108-90-7
Chloroethane
ND ug/L
1.0
0.54
1
05/22/14 07:30
75-00-3
Chloroform
ND ug/L
1.0
0.14
1
05/22/14 07:30
67-66-3
Chloromethane
ND ug/L
1.0
0.11
1
05/22/14 07:30
74-87-3
2-Chlorotoluene
ND ug/L
1.0
0.35
1
05/22/14 07:30
95-49-8
4-Chlorotoluene
ND ug/L
1.0
0.31
1
05/22/14 07:30
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
2.5
1
05/22/14 07:30
96-12-8
Dibromochloromethane
ND ug/L
1.0
0.21
1
05/22/14 07:30
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
0.27
1
05/22/14 07:30
106-93-4
Dibromomethane
ND ug/L
1.0
0.21
1
05/22/14 07:30
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
0.30
1
05/22/14 07:30
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
0.24
1
05/22/14 07:30
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
0.33
1
05/22/14 07:30
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
0.21
1
05/22/14 07:30
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
0.32
1
05/22/14 07:30
75-34-3
1,2-Dichloroethane
0.15J ug/L
1.0
0.12
1
05/22/14 07:30
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
0.56
1
05/22/14 07:30
75-35-4
cis-1,2-Dichloroethene
198 ug/L
1.0
0.19
1
05/22/14 07:30
156-59-2
trans-1,2-Dichloroethene
5.0 ug/L
1.0
0.49
1
05/22/14 07:30
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
0.27
1
05/22/14 07:30
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
0.28
1
05/22/14 07:30
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
0.13
1
05/22/14 07:30
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
0.49
1
05/22/14 07:30
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
0.13
1
05/22/14 07:30
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
0.26
1
05/22/14 07:30
10061-02-6
Diisopropyl ether
ND ug/L
1.0
0.12
1
05/22/14 07:30
108-20-3
Ethylbenzene
ND ug/L
1.0
0.30
1
05/22/14 07:30
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
0.71
1
05/22/14 07:30
87-68-3
2-Hexanone
ND ug/L
5.0
0.46
1
05/22/14 07:30
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
0.31
1
05/22/14 07:30
99-87-6
Methylene Chloride
ND ug/L
2.0
0.97
1
05/22/14 07:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
0.33
1
05/22/14 07:30
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
0.21
1
05/22/14 07:30
1634-04-4
Naphthalene
ND ug/L
1.0
0.24
1
05/22/14 07:30
91-20-3
Styrene
ND ug/L
1.0
0.26
1
05/22/14 07:30
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
0.33
1
05/22/14 07:30
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
0.40
1
05/22/14 07:30
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
Sample: IW-2
Lab ID: 92201336001
Collected:
05/14/14 09:00
Received: 05/14/14 16:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
70.4 ug/L
1.0
0.46
1
05/22/14 07:30
127-18-4
Toluene
0.89J ug/L
1.0
0.26
1
05/22/14 07:30
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
0.33
1
05/22/14 07:30
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
0.35
1
05/22/14 07:30
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
0.48
1
05/22/14 07:30
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
0.29
1
05/22/14 07:30
79-00-5
Trichloroethene
19.8 ug/L
1.0
0.47
1
05/22/14 07:30
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
0.20
1
05/22/14 07:30
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
0.41
1
05/22/14 07:30
96-18-4
Vinyl acetate
ND ug/L
2.0
0.35
1
05/22/14 07:30
108-05-4
Vinyl chloride
16.7 ug/L
1.0
0.62
1
05/22/14 07:30
75-01-4
Xylene (Total)
ND ug/L
2.0
0.66
1
05/22/14 07:30
1330-20-7
m&p-Xylene
ND ug/L
2.0
0.66
1
05/22/14 07:30
179601-23-1
o-Xylene
ND ug/L
1.0
0.23
1
05/22/14 07:30
95-47-6
Surrogates
4-Bromofluorobenzene (S)
89 %
70-130
1
05/22/14 07:30
460-00-4
1,2-Dichloroethane-d4 (S)
100 %
70-130
1
05/22/14 07:30
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
05/22/14 07:30
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 47.4 mg/L 1.0 1.0 1 05/22/14 21:15 7440-44-0
Date: 05/27/2014 01:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
QC Batch: MSV/26908 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92201336001
METHOD BLANK: 1203923
Associated Lab Samples: 92201336001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,1-Trichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1,2-Trichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
1,1-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
1,2,3-Trichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2,3-Trichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,2,4-Trichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
05/21/14 22:11
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichloroethane
ug/L
ND
1.0
05/21/14 22:11
1,2-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,3-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
1,3-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
1,4-Dichlorobenzene
ug/L
ND
1.0
05/21/14 22:11
2,2-Dichloropropane
ug/L
ND
1.0
05/21/14 22:11
2-Butanone (MEK)
ug/L
ND
5.0
05/21/14 22:11
2-Chlorotoluene
ug/L
ND
1.0
05/21/14 22:11
2-Hexanone
ug/L
ND
5.0
05/21/14 22:11
4-Chlorotoluene
ug/L
ND
1.0
05/21/14 22:11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
05/21/14 22:11
Acetone
ug/L
ND
25.0
05/21/14 22:11
Benzene
ug/L
ND
1.0
05/21/14 22:11
Bromobenzene
ug/L
ND
1.0
05/21/14 22:11
Bromochloromethane
ug/L
ND
1.0
05/21/14 22:11
Bromodichloromethane
ug/L
ND
1.0
05/21/14 22:11
Bromoform
ug/L
ND
1.0
05/21/14 22:11
Bromomethane
ug/L
ND
2.0
05/21/14 22:11
Carbon tetrachloride
ug/L
ND
1.0
05/21/14 22:11
Chlorobenzene
ug/L
ND
1.0
05/21/14 22:11
Chloroethane
ug/L
ND
1.0
05/21/14 22:11
Chloroform
ug/L
ND
1.0
05/21/14 22:11
Chloromethane
ug/L
ND
1.0
05/21/14 22:11
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
Dibromochloromethane
ug/L
ND
1.0
05/21/14 22:11
Dibromomethane
ug/L
ND
1.0
05/21/14 22:11
Dichlorodifluoromethane
ug/L
ND
1.0
05/21/14 22:11
Diisopropyl ether
ug/L
ND
1.0
05/21/14 22:11
Ethylbenzene
ug/L
ND
1.0
05/21/14 22:11
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
METHOD BLANK: 1203923
Associated Lab Samples: 92201336001
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
1.0
05/21/14 22:11
m&p-Xylene
ug/L
ND
2.0
05/21/14 22:11
Methyl-tert-butyl ether
ug/L
ND
1.0
05/21/14 22:11
Methylene Chloride
ug/L
ND
2.0
05/21/14 22:11
Naphthalene
ug/L
ND
1.0
05/21/14 22:11
o-Xylene
ug/L
ND
1.0
05/21/14 22:11
p-Isopropyltoluene
ug/L
ND
1.0
05/21/14 22:11
Styrene
ug/L
ND
1.0
05/21/14 22:11
Tetrachloroethene
ug/L
ND
1.0
05/21/14 22:11
Toluene
ug/L
ND
1.0
05/21/14 22:11
trans-1,2-Dichloroethene
ug/L
ND
1.0
05/21/14 22:11
trans- 1,3-Dichloropropene
ug/L
ND
1.0
05/21/14 22:11
Trichloroethene
ug/L
ND
1.0
05/21/14 22:11
Trichlorofluoromethane
ug/L
ND
1.0
05/21/14 22:11
Vinyl acetate
ug/L
ND
2.0
05/21/14 22:11
Vinyl chloride
ug/L
ND
1.0
05/21/14 22:11
Xylene (Total)
ug/L
ND
2.0
05/21/14 22:11
1,2-Dichloroethane-d4 (S)
%
102
70-130
05/21/14 22:11
4-Bromofluorobenzene (S)
%
98
70-130
05/21/14 22:11
Toluene-d8 (S)
%
97
70-130
05/21/14 22:11
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1203924
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
56.1
112
70-130
1,1,1-Trichloroethane
ug/L
50
54.0
108
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
55.8
112
70-130
1,1,2-Trichloroethane
ug/L
50
56.6
113
70-130
1,1-Dichloroethane
ug/L
50
52.1
104
70-130
1,1-Dichloroethene
ug/L
50
51.7
103
70-132
1,1-Dichloropropene
ug/L
50
56.0
112
70-130
1,2,3-Trichlorobenzene
ug/L
50
54.5
109
70-135
1,2,3-Trichloropropane
ug/L
50
53.2
106
70-130
1,2,4-Trichlorobenzene
ug/L
50
54.1
108
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
47.0
94
70-130
1,2-Dibromoethane (EDB)
ug/L
50
53.9
108
70-130
1,2-Dichlorobenzene
ug/L
50
55.2
110
70-130
1,2-Dichloroethane
ug/L
50
55.6
111
70-130
1,2-Dichloropropane
ug/L
50
54.7
109
70-130
1,3-Dichlorobenzene
ug/L
50
53.6
107
70-130
1,3-Dichloropropane
ug/L
50
53.9
108
70-130
1,4-Dichlorobenzene
ug/L
50
54.1
108
70-130
2,2-Dichloropropane
ug/L
50
49.9
100
58-145
2-Butanone (MEK)
ug/L
100
98.7
99
70-145
2-Chlorotoluene
ug/L
50
54.1
108
70-130
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
LABORATORY CONTROL SAMPLE:
Parameter
1203924
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2-Hexanone
ug/L
100
106
106
70-144
4-Chlorotoluene
ug/L
50
52.4
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
108
108
70-140
Acetone
ug/L
100
101
101
50-175
Benzene
ug/L
50
58.0
116
70-130
Bromobenzene
ug/L
50
54.4
109
70-130
Bromochloromethane
ug/L
50
53.5
107
70-130
Bromodichloromethane
ug/L
50
54.9
110
70-130
Bromoform
ug/L
50
45.8
92
70-130
Bromomethane
ug/L
50
47.8
96
54-130
Carbon tetrachloride
ug/L
50
53.7
107
70-132
Chlorobenzene
ug/L
50
51.4
103
70-130
Chloroethane
ug/L
50
46.7
93
64-134
Chloroform
ug/L
50
52.9
106
70-130
Chloromethane
ug/L
50
44.9
90
64-130
cis-1,2-Dichloroethene
ug/L
50
53.6
107
70-131
cis-1,3-Dichloropropene
ug/L
50
56.2
112
70-130
Dibromochloromethane
ug/L
50
47.1
94
70-130
Dibromomethane
ug/L
50
54.1
108
70-131
Dichlorodifluoromethane
ug/L
50
59.2
118
56-130
Diisopropyl ether
ug/L
50
57.1
114
70-130
Ethylbenzene
ug/L
50
51.0
102
70-130
Hexachloro-1,3-butadiene
ug/L
50
51.4
103
70-130
m&p-Xylene
ug/L
100
103
103
70-130
Methyl-tert-butyl ether
ug/L
50
56.1
112
70-130
Methylene Chloride
ug/L
50
57.7
115
63-130
Naphthalene
ug/L
50
54.4
109
70-138
o-Xylene
ug/L
50
53.1
106
70-130
p-Isopropyltoluene
ug/L
50
53.9
108
70-130
Styrene
ug/L
50
54.8
110
70-130
Tetrachloroethene
ug/L
50
54.5
109
70-130
Toluene
ug/L
50
53.7
107
70-130
trans-1,2-Dichloroethene
ug/L
50
53.3
107
70-130
trans- 1,3-Dichloropropene
ug/L
50
55.2
110
70-132
Trichloroethene
ug/L
50
56.8
114
70-130
Trichlorofluoromethane
ug/L
50
49.7
99
62-133
Vinyl acetate
ug/L
100
117
117
66-157
Vinyl chloride
ug/L
50
62.3
125
69-130
Xylene (Total)
ug/L
150
157
104
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE SAMPLE:
Parameter
1,1,1,2-Tetrachloroethane
Date: 05/27/2014 01:38 PM
1204539
ug/L
92202095007 Spike
Units Result Conc.
ND 50
MS
Result
63.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
MS % Rec
% Rec Limits Qualifiers
127 70-130
Page 9 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
MATRIX SPIKE SAMPLE: 1204539
92202095007 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
1,1,1-Trichloroethane
ug/L
ND
50
63.3
127
70-130
1,1,2,2-Tetrachloroethane
ug/L
ND
50
61.4
123
70-130
1,1,2-Trichloroethane
ug/L
ND
50
62.0
124
70-130
1,1-Dichloroethane
ug/L
ND
50
59.9
120
70-130
1,1-Dichloroethene
ug/L
ND
50
60.3
121
70-166
1,1-Dichloropropene
ug/L
ND
50
66.3
133
70-130 MO
1,2,3-Trichlorobenzene
ug/L
ND
50
57.9
116
70-130
1,2,3-Trichloropropane
ug/L
ND
50
58.8
118
70-130
1,2,4-Trichlorobenzene
ug/L
ND
50
57.7
115
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
50
50.3
101
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
50
60.5
121
70-130
1,2-Dichlorobenzene
ug/L
ND
50
60.5
121
70-130
1,2-Dichloroethane
ug/L
ND
50
63.7
127
70-130
1,2-Dichloropropane
ug/L
ND
50
60.6
121
70-130
1,3-Dichlorobenzene
ug/L
ND
50
58.0
116
70-130
1,3-Dichloropropane
ug/L
ND
50
60.3
121
70-130
1,4-Dichlorobenzene
ug/L
ND
50
59.7
119
70-130
2,2-Dichloropropane
ug/L
ND
50
63.0
126
70-130
2-Butanone (MEK)
ug/L
ND
100
113
113
70-130
2-Chlorotoluene
ug/L
ND
50
58.8
118
70-130
2-Hexanone
ug/L
ND
100
118
118
70-130
4-Chlorotoluene
ug/L
ND
50
56.9
114
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
120
120
70-130
Acetone
ug/L
ND
100
117
110
70-130
Benzene
ug/L
ND
50
65.4
131
70-148
Bromobenzene
ug/L
ND
50
58.9
118
70-130
Bromochloromethane
ug/L
ND
50
58.2
116
70-130
Bromodichloromethane
ug/L
ND
50
62.0
124
70-130
Bromoform
ug/L
ND
50
50.2
100
70-130
Bromomethane
ug/L
ND
50
59.3
119
70-130
Carbon tetrachloride
ug/L
ND
50
63.9
128
70-130
Chlorobenzene
ug/L
ND
50
58.1
116
70-146
Chloroethane
ug/L
ND
50
42.6
85
70-130
Chloroform
ug/L
1.4
50
63.5
124
70-130
Chloromethane
ug/L
ND
50
55.4
111
70-130
cis-1,2-Dichloroethene
ug/L
ND
50
60.8
122
70-130
cis-1,3-Dichloropropene
ug/L
ND
50
62.3
125
70-130
Dibromochloromethane
ug/L
ND
50
51.9
104
70-130
Dibromomethane
ug/L
ND
50
60.1
120
70-130
Dichlorodifluoromethane
ug/L
ND
50
66.0
132
70-130
Diisopropyl ether
ug/L
ND
50
64.7
129
70-130
Ethylbenzene
ug/L
ND
50
57.5
115
70-130
Hexachloro-1,3-butadiene
ug/L
ND
50
59.3
119
70-130
m&p-Xylene
ug/L
ND
100
116
116
70-130
Methyl-tert-butyl ether
ug/L
ND
50
62.3
125
70-130
Methylene Chloride
ug/L
ND
50
62.1
124
70-130
Naphthalene
ug/L
ND
50
57.9
116
70-130
o-Xylene
ug/L
ND
50
59.5
119
70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
MATRIX SPIKE SAMPLE:
Parameter
1204539
Units
92202095007
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
p-Isopropyltoluene
ug/L
ND
50
59.7
119
70-130
Styrene
ug/L
ND
50
62.0
124
70-130
Tetrachloroethene
ug/L
ND
50
62.9
126
70-130
Toluene
ug/L
ND
50
61.0
122
70-155
trans-1,2-Dichloroethene
ug/L
ND
50
59.0
118
70-130
trans- 1,3-Dichloropropene
ug/L
ND
50
61.0
122
70-130
Trichloroethene
ug/L
ND
50
65.3
131
69-151
Trichlorofluoromethane
ug/L
ND
50
58.5
117
70-130
Vinyl acetate
ug/L
ND
100
128
128
70-130
Vinyl chloride
ug/L
ND
50
72.0
144
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 1204540
Parameter
Units
92202095008
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,1-Dichloropropene
ug/L
ND
ND
30
1,2,3-Trichlorobenzene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2,4-Trichlorobenzene
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,3-Dichlorobenzene
ug/L
ND
ND
30
1,3-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
2,2-Dichloropropane
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Chlorotoluene
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Chlorotoluene
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromobenzene
ug/L
ND
ND
30
Bromochloromethane
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 11 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
SAMPLE DUPLICATE: 1204540
Parameter
Units
92202095008
Result
Dup
Result
Bromomethane
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
8.3
8.6
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
26.8
27.3
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Dichlorodifluoromethane
ug/L
ND
ND
Diisopropyl ether
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methyl-tert-butyl ether
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
p-Isopropyltoluene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
49.7
51.1
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
12.6
12.8
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
100
101
4-Bromofluorobenzene (S)
%
98
98
Toluene-d8 (S)
%
97
97
Date: 05/27/2014 01:38 PM
Max
RPD RPD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
4
2
3
2
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Qualifiers
Page 12 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
QC Batch: WETA/19083
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92201336001
METHOD BLANK: 1204906
Matrix: Water
Associated Lab Samples: 92201336001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
05/22/14 20:16
LABORATORY CONTROL SAMPLE: 1204907
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 24.1
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1204908 1204909
MS MSD
92201335001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 4.8
25 25 27.8
27.9 92 93 75-125 0 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1204910 1204911
MS MSD
92201952001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 5.8 25 25 27.2 27.3 86 86 75-125 0 20
Date: 05/27/2014 01:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/27/2014 01:38 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201336
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92201336001
92201336001
IW-2
IW-2
EPA 8260
SM 5310B
MSV/26908
WETA/19083
Date: 05/27/2014 01:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 15 of 17

Document Name: Sample Condition Upon Document Revised: April 9, 2014
�2'eAnalytical' Receipt SOUR) Page 1 of 2
www.paco/.vbs.com
Document No.: Issuing Authorities:
F-ASV-CS-003-rev.13 Pace Asheville Quality Office
Client Name:%
Courier (Circle): Fed Ex UPS USPS Client Commercial Pace Other
Custody Seal on Cooler/Box Present: es no Seals intact: [� yes (] no
Packing Material: Bubble Wrap Bubble Bags Q None Other
Thermometer Used: Gun#3 ��J63 Type of Ice:( We#', Blue None Z Samples on ice, cooling process has begun
Other: �J
Temp Correction Factor: Add / Subtract C; . 0 C
Corrected Cooler Temp.: C
Temp should be above freezing to 6°C
Biological Tissue is Frozen: Yes No N/A Date and Initi Is oof�erson e lam
contents:
Comments:
�g
Chain of Custody Present:
Yes
❑No
❑N/A
1.
Chain of Custody Filled Out:
es,
❑No
❑N/A
2.
Chain of Custody Relinquished:
Ye
❑No
❑N/A
3.
Sampler Name & Signature on COC:
Ye
❑No
❑N/A
14.
Samples Arrived within Hold Time;
ZYes
❑No
❑N/A
5.
Short Hold Time Analysis (<72hr):
❑Yes
No
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
o
❑N/A
7.
Sufficient Volume:
CA
ElNo
❑N/A
8.
Correct Containers Used:
-Pace Containers Used:
Yes ❑No
L'lYe ❑No
❑N/A
El N/A
9.
Containers Intact:
Yes
❑No
❑N/A
10.
Filtered volume received for Dissolved tests
❑Yes
No
134A
11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
es
W�:
❑No
❑N/A
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
Yes
1 Yes
❑Yes
❑No
❑No
E No
El NIA
❑N/A
13.
Samples checked for dechlorination:
❑Yes
❑No
N/A
14,
Headspace in VOA Vials (>6mm):
❑Yes
No
❑N/A
5.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased):
❑Yes
❑Yes
❑No
❑No
N/A
/A
46.
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
Date/Time:
SRF Review: v %� _Date: 5��5 ly
Note: WheneveRiKere Is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y / N
Place label here
`? 2.2&133�- OR
Handwrite project number
(if no label available)
Page 16 of 17

CHAIN -OF -CUSTODY / Analytical Request Document
F8C2�iI7a/ICaI The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.cc
enlahc.enm d
Page: I of
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information:
Company: Repo&OWArt To: Attention:
AvuL
Address: Copy
To:
Company Name:
REGULATORY AGENCY
t 5� vito"5
Address:
NPDES GROUNDWATER 3 DRINKING WATER
-
UST RCRA OTHER
Email To: Purchase
Order No.:
Pace Quote
C ^�
Reference:
P one.'_ Fix: Project
Name:
Pace Project
Site Location
Manage::
STATE:
�L
Requested Due DatetTAT: Project
2641V
Number. •�^ — ?
`J d
Pace P.file 4:
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
~
Z
RegetrodClient Information MATRIX.?CODE
z
-
2
COLLECTED
Preservatives
}
Drink ng Water DIN
g
C)
o
water wT
8,
i
Waste Water WVV
s
n
COMPOs1TE
COMPOs.Te
0
I
_
Product P
'aSTART
ErtD:GR1tS
W
i
z
Soil(SG6d SL
SAMPLE ID Oic OL
n
ca
o
UJ
(A, ! , } Air AR
p
�
rl
-0E-
Sample tDs MUSS UNIQUET BUNIQUETissue TS
O
a
g
Q
d
y
V.0
4;b)
Other OT
V
Z
Z
c
J
J
0
m
O
p
=
O
Q
c
ti
r
ul
<
N
LL
O
n
O
Z
=
J
.Z
i DATE
TIME
DATE
TIME
_
=
T-
Z
O
00
Pace Project No./ Lab I.D.
Tw- Z
I
I
1XI
I
x
X
2
I
I
3
4
5
6
7
f
S
f
t0
i
tt
12
ADDITIONAL COMMENTS
RELINQUISHED BY t AFFILIATION
t
DATE
TIME
ACCEPTED BY f AFFILIATION
DATE
I TIME
SAMPLE CONDITIONS
k
E
E
1
i
SAMPLER NAME AND SIGNATURE
i
ORIGINAL
PRINT Name of SAMPLER:
DATE Signed
SIGNATURE of SAMPLER:
OS
E
}-
E -'
-
�% a
E
(MMtDDFYY): $ ,¢,
;n
m,corzan; Noce: �y sing tars Corm ym are accepting, epting Paca s NcT 31 day ;;ay:ne•n len ., and a;feeir:g :o izte charges o` ; 5:e Cer rnN,'—'�ny i.'tUos , Gi paid vatHn 30 darn i --ALL-0-020, ' O%, hAPy-2itG7

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
May 28, 2014
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
RE: Project: FORMERANDREX IND J14-1022-38
Pace Project No.: 92201332
Dear Mr. Alexander:
Enclosed are the analytical results for sample(s) received by the laboratory on May 14, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 17

aceAnalytical
—pacelabsxom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE SUMMARY
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92201332001
92201332002
BC-1
JW-1
Water
Water
05/14/1413:35
05/14/1414:20
05/14/1416:30
05/14/1416:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
FORMER ANDREX IND J14-1022-38
92201332
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92201332001
BC-1
EPA 8260
MCK
63
PASI-C
SM 5310B
SAE
1
PASI-A
92201332002
JW-1
EPA 8260
MCK
63
PASI-C
SM 5310B
SAE
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
Sample: BC-1 Lab ID: 92201332001 Collected: 05/14/14 13:35 Received: 05/14/14 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
10.0
1
05/27/14 23:16
67-64-1
Benzene
ND ug/L
1.0
0.25
1
05/27/14 23:16
71-43-2
Bromobenzene
ND ug/L
1.0
0.30
1
05/27/14 23:16
108-86-1
Bromochloromethane
ND ug/L
1.0
0.17
1
05/27/14 23:16
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.18
1
05/27/14 23:16
75-27-4
Bromoform
ND ug/L
1.0
0.26
1
05/27/14 23:16
75-25-2
Bromomethane
ND ug/L
2.0
0.29
1
05/27/14 23:16
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
0.96
1
05/27/14 23:16
78-93-3
Carbon tetrachloride
ND ug/L
1.0
0.25
1
05/27/14 23:16
56-23-5
Chlorobenzene
ND ug/L
1.0
0.23
1
05/27/14 23:16
108-90-7
Chloroethane
ND ug/L
1.0
0.54
1
05/27/14 23:16
75-00-3
Chloroform
ND ug/L
1.0
0.14
1
05/27/14 23:16
67-66-3
Chloromethane
ND ug/L
1.0
0.11
1
05/27/14 23:16
74-87-3
2-Chlorotoluene
ND ug/L
1.0
0.35
1
05/27/14 23:16
95-49-8
4-Chlorotoluene
ND ug/L
1.0
0.31
1
05/27/14 23:16
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
2.5
1
05/27/14 23:16
96-12-8
Dibromochloromethane
ND ug/L
1.0
0.21
1
05/27/14 23:16
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
0.27
1
05/27/14 23:16
106-93-4
Dibromomethane
ND ug/L
1.0
0.21
1
05/27/14 23:16
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
0.30
1
05/27/14 23:16
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
0.24
1
05/27/14 23:16
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
0.33
1
05/27/14 23:16
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
0.21
1
05/27/14 23:16
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
0.32
1
05/27/14 23:16
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
0.12
1
05/27/14 23:16
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
0.56
1
05/27/14 23:16
75-35-4
cis-1,2-Dichloroethene
27.6 ug/L
1.0
0.19
1
05/27/14 23:16
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
0.49
1
05/27/14 23:16
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
0.27
1
05/27/14 23:16
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
0.28
1
05/27/14 23:16
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
0.13
1
05/27/14 23:16
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
0.49
1
05/27/14 23:16
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
0.13
1
05/27/14 23:16
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
0.26
1
05/27/14 23:16
10061-02-6
Diisopropyl ether
0.57J ug/L
1.0
0.12
1
05/27/14 23:16
108-20-3
Ethylbenzene
ND ug/L
1.0
0.30
1
05/27/14 23:16
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
0.71
1
05/27/14 23:16
87-68-3
2-Hexanone
ND ug/L
5.0
0.46
1
05/27/14 23:16
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
0.31
1
05/27/14 23:16
99-87-6
Methylene Chloride
ND ug/L
2.0
0.97
1
05/27/14 23:16
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
0.33
1
05/27/14 23:16
108-10-1
Methyl-tert-butyl ether
4.3 ug/L
1.0
0.21
1
05/27/14 23:16
1634-04-4
Naphthalene
ND ug/L
1.0
0.24
1
05/27/14 23:16
91-20-3
Styrene
ND ug/L
1.0
0.26
1
05/27/14 23:16
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
0.33
1
05/27/14 23:16
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
0.40
1
05/27/14 23:16
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
Sample: BC-1
Lab ID: 92201332001
Collected:
05/14/14 13:35
Received: 05/14/14 16:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
59.9 ug/L
1.0
0.46
1
05/27/14 23:16
127-18-4
Toluene
ND ug/L
1.0
0.26
1
05/27/14 23:16
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
0.33
1
05/27/14 23:16
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
0.35
1
05/27/14 23:16
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
0.48
1
05/27/14 23:16
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
0.29
1
05/27/14 23:16
79-00-5
Trichloroethene
7.5 ug/L
1.0
0.47
1
05/27/14 23:16
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
0.20
1
05/27/14 23:16
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
0.41
1
05/27/14 23:16
96-18-4
Vinyl acetate
ND ug/L
2.0
0.35
1
05/27/14 23:16
108-05-4
Vinyl chloride
ND ug/L
1.0
0.62
1
05/27/14 23:16
75-01-4
Xylene (Total)
ND ug/L
2.0
0.66
1
05/27/14 23:16
1330-20-7
m&p-Xylene
ND ug/L
2.0
0.66
1
05/27/14 23:16
179601-23-1
o-Xylene
ND ug/L
1.0
0.23
1
05/27/14 23:16
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
1
05/27/14 23:16
460-00-4
1,2-Dichloroethane-d4 (S)
96 %
70-130
1
05/27/14 23:16
17060-07-0
Toluene-d8 (S)
97 %
70-130
1
05/27/14 23:16
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 2.3 mg/L 1.0 1.0 1 05/21/14 23:42 7440-44-0
Date: 05/28/2014 04:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
Sample: JW-1 Lab ID: 92201332002 Collected: 05/14/14 14:20 Received: 05/14/14 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
25.0
10.0
1
05/27/14 23:49
67-64-1
Benzene
ND ug/L
1.0
0.25
1
05/27/14 23:49
71-43-2
Bromobenzene
ND ug/L
1.0
0.30
1
05/27/14 23:49
108-86-1
Bromochloromethane
ND ug/L
1.0
0.17
1
05/27/14 23:49
74-97-5
Bromodichloromethane
ND ug/L
1.0
0.18
1
05/27/14 23:49
75-27-4
Bromoform
ND ug/L
1.0
0.26
1
05/27/14 23:49
75-25-2
Bromomethane
ND ug/L
2.0
0.29
1
05/27/14 23:49
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
0.96
1
05/27/14 23:49
78-93-3
Carbon tetrachloride
ND ug/L
1.0
0.25
1
05/27/14 23:49
56-23-5
Chlorobenzene
ND ug/L
1.0
0.23
1
05/27/14 23:49
108-90-7
Chloroethane
ND ug/L
1.0
0.54
1
05/27/14 23:49
75-00-3
Chloroform
ND ug/L
1.0
0.14
1
05/27/14 23:49
67-66-3
Chloromethane
ND ug/L
1.0
0.11
1
05/27/14 23:49
74-87-3
2-Chlorotoluene
ND ug/L
1.0
0.35
1
05/27/14 23:49
95-49-8
4-Chlorotoluene
ND ug/L
1.0
0.31
1
05/27/14 23:49
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
2.5
1
05/27/14 23:49
96-12-8
Dibromochloromethane
ND ug/L
1.0
0.21
1
05/27/14 23:49
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
0.27
1
05/27/14 23:49
106-93-4
Dibromomethane
ND ug/L
1.0
0.21
1
05/27/14 23:49
74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
0.30
1
05/27/14 23:49
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
0.24
1
05/27/14 23:49
541-73-1
1,4-Dichlorobenzene
ND ug/L
1.0
0.33
1
05/27/14 23:49
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
0.21
1
05/27/14 23:49
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
0.32
1
05/27/14 23:49
75-34-3
1,2-Dichloroethane
ND ug/L
1.0
0.12
1
05/27/14 23:49
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
0.56
1
05/27/14 23:49
75-35-4
cis-1,2-Dichloroethene
0.51J ug/L
1.0
0.19
1
05/27/14 23:49
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
0.49
1
05/27/14 23:49
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
0.27
1
05/27/14 23:49
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
0.28
1
05/27/14 23:49
142-28-9
2,2-Dichloropropane
ND ug/L
1.0
0.13
1
05/27/14 23:49
594-20-7
1,1-Dichloropropene
ND ug/L
1.0
0.49
1
05/27/14 23:49
563-58-6
cis-1,3-Dichloropropene
ND ug/L
1.0
0.13
1
05/27/14 23:49
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
1.0
0.26
1
05/27/14 23:49
10061-02-6
Diisopropyl ether
ND ug/L
1.0
0.12
1
05/27/14 23:49
108-20-3
Ethylbenzene
ND ug/L
1.0
0.30
1
05/27/14 23:49
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
1.0
0.71
1
05/27/14 23:49
87-68-3
2-Hexanone
ND ug/L
5.0
0.46
1
05/27/14 23:49
591-78-6
p-Isopropyltoluene
ND ug/L
1.0
0.31
1
05/27/14 23:49
99-87-6
Methylene Chloride
ND ug/L
2.0
0.97
1
05/27/14 23:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
0.33
1
05/27/14 23:49
108-10-1
Methyl-tert-butyl ether
ND ug/L
1.0
0.21
1
05/27/14 23:49
1634-04-4
Naphthalene
ND ug/L
1.0
0.24
1
05/27/14 23:49
91-20-3
Styrene
ND ug/L
1.0
0.26
1
05/27/14 23:49
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
1.0
0.33
1
05/27/14 23:49
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
0.40
1
05/27/14 23:49
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
Sample: JW-1
Lab ID: 92201332002
Collected:
05/14/14 14:20
Received: 05/14/14 16:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
2.3 ug/L
1.0
0.46
1
05/27/14 23:49
127-18-4
Toluene
ND ug/L
1.0
0.26
1
05/27/14 23:49
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
1.0
0.33
1
05/27/14 23:49
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
1.0
0.35
1
05/27/14 23:49
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
0.48
1
05/27/14 23:49
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
0.29
1
05/27/14 23:49
79-00-5
Trichloroethene
ND ug/L
1.0
0.47
1
05/27/14 23:49
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
0.20
1
05/27/14 23:49
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
0.41
1
05/27/14 23:49
96-18-4
Vinyl acetate
ND ug/L
2.0
0.35
1
05/27/14 23:49
108-05-4
Vinyl chloride
ND ug/L
1.0
0.62
1
05/27/14 23:49
75-01-4
Xylene (Total)
ND ug/L
2.0
0.66
1
05/27/14 23:49
1330-20-7
m&p-Xylene
ND ug/L
2.0
0.66
1
05/27/14 23:49
179601-23-1
o-Xylene
ND ug/L
1.0
0.23
1
05/27/14 23:49
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
1
05/27/14 23:49
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
05/27/14 23:49
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
05/27/14 23:49
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 2.5 mg/L 1.0 1.0 1 05/21/14 23:55 7440-44-0
Date: 05/28/2014 04:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
QC Batch: MSV/26961 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92201332001, 92201332002
METHOD BLANK: 1207085
Associated Lab Samples: 92201332001, 92201332002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1,1-Trichloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1,2-Trichloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1-Dichloroethane
ug/L
ND
1.0
05/27/14 14:44
1,1-Dichloroethene
ug/L
ND
1.0
05/27/14 14:44
1,1-Dichloropropene
ug/L
ND
1.0
05/27/14 14:44
1,2,3-Trichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
1,2,3-Trichloropropane
ug/L
ND
1.0
05/27/14 14:44
1,2,4-Trichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
05/27/14 14:44
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/27/14 14:44
1,2-Dichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
1,2-Dichloroethane
ug/L
ND
1.0
05/27/14 14:44
1,2-Dichloropropane
ug/L
ND
1.0
05/27/14 14:44
1,3-Dichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
1,3-Dichloropropane
ug/L
ND
1.0
05/27/14 14:44
1,4-Dichlorobenzene
ug/L
ND
1.0
05/27/14 14:44
2,2-Dichloropropane
ug/L
ND
1.0
05/27/14 14:44
2-Butanone (MEK)
ug/L
ND
5.0
05/27/14 14:44
2-Chlorotoluene
ug/L
ND
1.0
05/27/14 14:44
2-Hexanone
ug/L
ND
5.0
05/27/14 14:44
4-Chlorotoluene
ug/L
ND
1.0
05/27/14 14:44
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
05/27/14 14:44
Acetone
ug/L
ND
25.0
05/27/14 14:44
Benzene
ug/L
ND
1.0
05/27/14 14:44
Bromobenzene
ug/L
ND
1.0
05/27/14 14:44
Bromochloromethane
ug/L
ND
1.0
05/27/14 14:44
Bromodichloromethane
ug/L
ND
1.0
05/27/14 14:44
Bromoform
ug/L
ND
1.0
05/27/14 14:44
Bromomethane
ug/L
ND
2.0
05/27/14 14:44
Carbon tetrachloride
ug/L
ND
1.0
05/27/14 14:44
Chlorobenzene
ug/L
ND
1.0
05/27/14 14:44
Chloroethane
ug/L
ND
1.0
05/27/14 14:44
Chloroform
ug/L
ND
1.0
05/27/14 14:44
Chloromethane
ug/L
ND
1.0
05/27/14 14:44
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/27/14 14:44
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/27/14 14:44
Dibromochloromethane
ug/L
ND
1.0
05/27/14 14:44
Dibromomethane
ug/L
ND
1.0
05/27/14 14:44
Dichlorodifluoromethane
ug/L
ND
1.0
05/27/14 14:44
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
METHOD BLANK: 1207085
Associated Lab Samples: 92201332001, 92201332002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
05/27/14 14:44
Ethylbenzene
ug/L
ND
1.0
05/27/14 14:44
Hexachloro-1,3-butadiene
ug/L
ND
1.0
05/27/14 14:44
m&p-Xylene
ug/L
ND
2.0
05/27/14 14:44
Methyl-tert-butyl ether
ug/L
ND
1.0
05/27/14 14:44
Methylene Chloride
ug/L
ND
2.0
05/27/14 14:44
Naphthalene
ug/L
ND
1.0
05/27/14 14:44
o-Xylene
ug/L
ND
1.0
05/27/14 14:44
p-Isopropyltoluene
ug/L
ND
1.0
05/27/14 14:44
Styrene
ug/L
ND
1.0
05/27/14 14:44
Tetrachloroethene
ug/L
ND
1.0
05/27/14 14:44
Toluene
ug/L
ND
1.0
05/27/14 14:44
trans-1,2-Dichloroethene
ug/L
ND
1.0
05/27/14 14:44
trans- 1,3-Dichloropropene
ug/L
ND
1.0
05/27/14 14:44
Trichloroethene
ug/L
ND
1.0
05/27/14 14:44
Trichlorofluoromethane
ug/L
ND
1.0
05/27/14 14:44
Vinyl acetate
ug/L
ND
2.0
05/27/14 14:44
Vinyl chloride
ug/L
ND
1.0
05/27/14 14:44
Xylene (Total)
ug/L
ND
2.0
05/27/14 14:44
1,2-Dichloroethane-d4 (S)
%
93
70-130
05/27/14 14:44
4-Bromofluorobenzene (S)
%
95
70-130
05/27/14 14:44
Toluene-d8 (S)
%
98
70-130
05/27/14 14:44
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1207086
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
57.1
114
70-130
1,1,1-Trichloroethane
ug/L
50
52.5
105
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
58.1
116
70-130
1,1,2-Trichloroethane
ug/L
50
55.4
111
70-130
1,1-Dichloroethane
ug/L
50
51.8
104
70-130
1,1-Dichloroethene
ug/L
50
53.3
107
70-132
1,1-Dichloropropene
ug/L
50
56.6
113
70-130
1,2,3-Trichlorobenzene
ug/L
50
56.2
112
70-135
1,2,3-Trichloropropane
ug/L
50
54.5
109
70-130
1,2,4-Trichlorobenzene
ug/L
50
58.0
116
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
54.2
108
70-130
1,2-Dibromoethane (EDB)
ug/L
50
54.6
109
70-130
1,2-Dichlorobenzene
ug/L
50
55.8
112
70-130
1,2-Dichloroethane
ug/L
50
53.3
107
70-130
1,2-Dichloropropane
ug/L
50
54.6
109
70-130
1,3-Dichlorobenzene
ug/L
50
54.0
108
70-130
1,3-Dichloropropane
ug/L
50
56.1
112
70-130
1,4-Dichlorobenzene
ug/L
50
54.5
109
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 17

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
LABORATORY CONTROL SAMPLE:
Parameter
1207086
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
55.0
110
58-145
2-Butanone (MEK)
ug/L
100
104
104
70-145
2-Chlorotoluene
ug/L
50
54.0
108
70-130
2-Hexanone
ug/L
100
112
112
70-144
4-Chlorotoluene
ug/L
50
54.0
108
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
105
105
70-140
Acetone
ug/L
100
106
106
50-175
Benzene
ug/L
50
58.8
118
70-130
Bromobenzene
ug/L
50
55.7
111
70-130
Bromochloromethane
ug/L
50
53.8
108
70-130
Bromodichloromethane
ug/L
50
52.9
106
70-130
Bromoform
ug/L
50
57.0
114
70-130
Bromomethane
ug/L
50
32.5
65
54-130
Carbon tetrachloride
ug/L
50
52.0
104
70-132
Chlorobenzene
ug/L
50
52.9
106
70-130
Chloroethane
ug/L
50
46.4
93
64-134
Chloroform
ug/L
50
52.6
105
70-130
Chloromethane
ug/L
50
39.7
79
64-130
cis-1,2-Dichloroethene
ug/L
50
52.1
104
70-131
cis-1,3-Dichloropropene
ug/L
50
56.4
113
70-130
Dibromochloromethane
ug/L
50
54.4
109
70-130
Dibromomethane
ug/L
50
52.5
105
70-131
Dichlorodifluoromethane
ug/L
50
57.4
115
56-130
Diisopropyl ether
ug/L
50
52.5
105
70-130
Ethylbenzene
ug/L
50
52.9
106
70-130
Hexachloro-1,3-butadiene
ug/L
50
46.1
92
70-130
m&p-Xylene
ug/L
100
108
108
70-130
Methyl-tert-butyl ether
ug/L
50
54.2
108
70-130
Methylene Chloride
ug/L
50
60.6
121
63-130
Naphthalene
ug/L
50
62.8
126
70-138
o-Xylene
ug/L
50
54.6
109
70-130
p-Isopropyltoluene
ug/L
50
54.0
108
70-130
Styrene
ug/L
50
58.0
116
70-130
Tetrachloroethene
ug/L
50
54.8
110
70-130
Toluene
ug/L
50
54.4
109
70-130
trans-1,2-Dichloroethene
ug/L
50
52.7
105
70-130
trans- 1,3-Dichloropropene
ug/L
50
54.3
109
70-132
Trichloroethene
ug/L
50
56.9
114
70-130
Trichlorofluoromethane
ug/L
50
49.3
99
62-133
Vinyl acetate
ug/L
100
114
114
66-157
Vinyl chloride
ug/L
50
63.3
127
69-130
Xylene (Total)
ug/L
150
162
108
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1207719
1207720
MS
MSD
92202617035
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,1-Dichloroethene
ug/L
ND
50
50
53.6
50.4
107
101
70-166
6
30
Benzene
ug/L
ND
50
50
61.7
57.3
123
115
70-148
8
30
Chlorobenzene
ug/L
ND
50
50
55.2
52.1
110
104
70-146
6
30
Toluene
ug/L
ND
50
50
53.9
49.7
108
99
70-155
8
30
Trichloroethene
ug/L
ND
50
50
60.8
57.0
122
114
69-151
6
30
1,2-Dichloroethane-d4(S)
%
88
89
70-130
4-Bromofluorobenzene (S)
%
95
97
70-130
Toluene-d8(S)
%
98
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
QC Batch: WETA/19054
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92201332001, 92201332002
METHOD BLANK: 1203097
Matrix: Water
Associated Lab Samples: 92201332001, 92201332002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
05/21/14 17:51
LABORATORY CONTROL SAMPLE: 1203098
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 23.8
95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1203099 1203100
MS MSD
92201069001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 12.4
25 25 33.4
32.9 84 82 75-125 1 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1203101 1203102
MS MSD
92201026011 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 1.9 25 25 27.4 27.1 102 101 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2014 04:19 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 17

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FORMER ANDREX IND J14-1022-38
Pace Project No.: 92201332
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92201332001
BC-1
EPA 8260
MSV/26961
92201332002
JW-1
EPA 8260
MSV/26961
92201332001
BC-1
SM 5310E
WETA/19054
92201332002
JW-1
SM 5310B
WETA/19054
Date: 05/28/2014 04:19 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 15 of 17

m
Document Name: Sample Condition Upon
Document Revised: April 9, 2014
11�aceAnalyticalSJ
Recei t SCUR)
Page 1 of 2
Document No.:
Issuing Authorities:
F-ASV-CS-003-rev.13
Pace Asheville Quality Office
Client Name:
Courier (Circle): Fed Ex UPS USPS client Commercial Pace Other
Custody Seal on Cooler/Box Present: yes Sno Seals intact: yes R no
Packing Material: 0 Bubble Wrap � Bubble Bags F None 171 Other
Thermometer Used: Gun#3;a'36265 63 Type of Ice:( Wet', Blue None Samples on ice, cooling process has begun
O er:
Temp Correction Factor: Add / Subtract 0.0 C
Corrected Cooler Temp.: 5 = L� C
Biological Tissue is Frozen: Yes No N/A Date and Init/i�is of erson xam'ning
Tempshould be above freezing to 6°C
g
contents: t�� d I
Comments:
d �{
Chain of Custody Present:
E4.ZEIN.
❑N/A
1.
Chain of Custody Filled Out:
e
❑No
❑N/A
2.
Chain of Custody Relinquished:
Ye
ON.
❑N/A
3.
Sampler Name & Signature on COC:
Ye
❑No
❑N/A
14.
Samples Arrived within Hold Time:
Yes
❑No
❑N/A
5.
Short Hold Time Analysis (<72hr):
Dyes
ZNo,
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
o
❑N/A
7.
Sufficient Volume:
a
ON.
❑N/A
8.
Correct Containers Used:
Yes ❑No
❑N/A
9.
-Pace Containers Used:
@ .
❑No
❑N/A
Containers Intact:
Yes
❑No
El N/A,
10.
Filtered volume received for Dissolved tests
❑Yes
No
514A
11.
Sample Labels match COC:
ZKe.
❑No
❑N/A
12,
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
Yes
ONo
❑N/A
13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
'Kes
❑No
❑N/A
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
Dyes
IJNo
Samples checked for dechlorination:
❑Yes
❑No
N/A
14.
Headspace in VOA Vials (>6mm):
❑Yes
ON.
❑N/A
15.
Trip Blank Present:
Dyes
❑No
25NMA
6.
Trip Blank Custody Seals Present
Dyes
❑No
/A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
SCURF Review:
Date:
SRF Review-T -0 (Date:
Date/Time:
Note: Wheneve�re is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office ( i.e out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y / N
Place label here
OR
Handwrite project number
(if no label available)
Page 16 of 17

-P 'a ceAnalyfical'
—M.pacelabsxom
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completec accurately.
Section A Section B Section C
Page: of
Required Client information: Required Project Information invoice Information
Company: - Report To Alenlco,:
1'r
Address:
Copy To: J
'Eompany Name:
REGULATORY AGENCY
�c
Address:
NPDES GRCUND VVATER DRINKING WATER
EmailTO:
@-
Purchase )rder No.:
LIST RCRA OTHER
ptw� M vi-k I F &OU 4+3o
Project Name:
AndygyPace
Pmea
�Y-
Site Locationj
Requested Due Date/TAT: 154...
Project Number.
ST
Requested
Analysis
Filtered
(Y[N)
Section D Matrix Codes
RequiredCl�
. -nt lnfonnation 1VATRN I CODE
E
COLLECTED
Preservatives
Drinking Water D10,1
.1
1 Q
I
Water WT
'S
Waste Walter 111"Al
e,
COt,'POSITE
COMPOSITE
Product P
=
<
SoiSolid SL
SAMPLE ID oil OL
1.
—
.1
0 u3
Arlpe VVP
Lu
q�a
(A-Z- 0-91.-) Aii AR
LU
Sam -pie I Ds MUST BE UNIOUE Issue TS
0
a -
tn
Other
z
e
Z
-F
x
Lu
0
C)
Q
(D
cy
<
0
<
<
c
z
DATE
T*,(.E
DATE
TIME
M
z
z
:E
0
Pace Project No./ L—#,b,)-
ZT0
L'TG
i
5 tt
i42v
(
i X
x
3
4
5
6
7
8
12
ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE TIMEACCEPTED
BY! AFFILIATION
DATE,
TIME
SAMPLE CONDITIONS
14-- if
h
-j—
SAMPLER NAME AND SIGNATURE
z
z
PRINT Name of SAMPLER:
E
SIGNATURE of SAMPLER: DATESigned
af
F
(MM,'DD, 1:
F-ALL-0-020re-,07' 15 Mlay 2007

APPENDIX E
LABORATORY ANALYTICAL DATA SHEETS
GROUNDWATER
JULY 2014 [30 Day]
(Provided on Enclosed CD)

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
July 11, 2014
Mr. Andy Alexander
Bunnell-Lammons Engineering
6004 Ponders Court
Greenville, SC 29615
RE: Project: FORMERANDREX INDUSTRIES
Pace Project No.: 92207829
Dear Mr. Alexander:
Enclosed are the analytical results for sample(s) received by the laboratory on July 03, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 20

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 20

aceAnalytical
—pacelabsxom
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE SUMMARY
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92207829001
MW-6
Water
07/02/14 10:45
07/03/14 08:05
92207829002
MW-44
Water
07/02/14 09:50
07/03/14 08:05
92207829003
RW-1
Water
07/02/14 10:15
07/03/14 08:05
92207829004
IW-2
Water
07/02/14 11:05
07/03/14 08:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 20

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
FORMER ANDREX INDUSTRIES
92207829
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92207829001
MW-6
EPA 8260
GAW
63
PASI-C
SM 5310B
SAE
1
PASI-A
92207829002
MW-44
EPA 8260
GAW
63
PASI-C
SM 5310B
SAE
1
PASI-A
92207829003
RW-1
EPA 8260
GAW
63
PASI-C
SM 5310B
SAE
1
PASI-A
92207829004
IW-2
EPA 8260
GAW
63
PASI-C
SM 5310B
SAE
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Sample: MW-6 Lab ID: 92207829001 Collected: 07/02/14 10:45 Received: 07/03/14 08:05 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
824 ug/L
250
100
10
07/08/14 22:21
67-64-1
Benzene
ND ug/L
10.0
2.5
10
07/08/14 22:21
71-43-2
Bromobenzene
ND ug/L
10.0
3.0
10
07/08/14 22:21
108-86-1
Bromochloromethane
ND ug/L
10.0
1.7
10
07/08/14 22:21
74-97-5
Bromodichloromethane
ND ug/L
10.0
1.8
10
07/08/14 22:21
75-27-4
Bromoform
ND ug/L
10.0
2.6
10
07/08/14 22:21
75-25-2
Bromomethane
ND ug/L
20.0
2.9
10
07/08/14 22:21
74-83-9
2-Butanone (MEK)
ND ug/L
50.0
9.6
10
07/08/14 22:21
78-93-3
Carbon tetrachloride
ND ug/L
10.0
2.5
10
07/08/14 22:21
56-23-5
Chlorobenzene
ND ug/L
10.0
2.3
10
07/08/14 22:21
108-90-7
Chloroethane
ND ug/L
10.0
5.4
10
07/08/14 22:21
75-00-3
Chloroform
ND ug/L
10.0
1.4
10
07/08/14 22:21
67-66-3
Chloromethane
ND ug/L
10.0
1.1
10
07/08/14 22:21
74-87-3
2-Chlorotoluene
ND ug/L
10.0
3.5
10
07/08/14 22:21
95-49-8
4-Chlorotoluene
ND ug/L
10.0
3.1
10
07/08/14 22:21
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
20.0
20.0
10
07/08/14 22:21
96-12-8
Dibromochloromethane
ND ug/L
10.0
2.1
10
07/08/14 22:21
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
10.0
2.7
10
07/08/14 22:21
106-93-4
Dibromomethane
ND ug/L
10.0
2.1
10
07/08/14 22:21
74-95-3
1,2-Dichlorobenzene
ND ug/L
10.0
3.0
10
07/08/14 22:21
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
2.4
10
07/08/14 22:21
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
3.3
10
07/08/14 22:21
106-46-7
Dichlorodifluoromethane
ND ug/L
10.0
2.1
10
07/08/14 22:21
75-71-8
1,1-Dichloroethane
ND ug/L
10.0
3.2
10
07/08/14 22:21
75-34-3
1,2-Dichloroethane
ND ug/L
10.0
1.2
10
07/08/14 22:21
107-06-2
1,1-Dichloroethene
ND ug/L
10.0
5.6
10
07/08/14 22:21
75-35-4
cis-1,2-Dichloroethene
1260 ug/L
10.0
1.9
10
07/08/14 22:21
156-59-2
trans-1,2-Dichloroethene
ND ug/L
10.0
4.9
10
07/08/14 22:21
156-60-5
1,2-Dichloropropane
ND ug/L
10.0
2.7
10
07/08/14 22:21
78-87-5
1,3-Dichloropropane
ND ug/L
10.0
2.8
10
07/08/14 22:21
142-28-9
2,2-Dichloropropane
ND ug/L
10.0
1.3
10
07/08/14 22:21
594-20-7
1,1-Dichloropropene
ND ug/L
10.0
4.9
10
07/08/14 22:21
563-58-6
cis-1,3-Dichloropropene
ND ug/L
10.0
1.3
10
07/08/14 22:21
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
10.0
2.6
10
07/08/14 22:21
10061-02-6
Diisopropyl ether
ND ug/L
10.0
1.2
10
07/08/14 22:21
108-20-3
Ethylbenzene
ND ug/L
10.0
3.0
10
07/08/14 22:21
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
10.0
7.1
10
07/08/14 22:21
87-68-3
2-Hexanone
ND ug/L
50.0
4.6
10
07/08/14 22:21
591-78-6
p-Isopropyltoluene
ND ug/L
10.0
3.1
10
07/08/14 22:21
99-87-6
Methylene Chloride
12.OJ ug/L
20.0
9.7
10
07/08/14 22:21
75-09-2
4-Methyl-2-pentanone (MIBK)
5.6J ug/L
50.0
3.3
10
07/08/14 22:21
108-10-1
Methyl-tert-butyl ether
ND ug/L
10.0
2.1
10
07/08/14 22:21
1634-04-4
Naphthalene
ND ug/L
10.0
2.4
10
07/08/14 22:21
91-20-3
Styrene
ND ug/L
10.0
2.6
10
07/08/14 22:21
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
10.0
3.3
10
07/08/14 22:21
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
10.0
4.0
10
07/08/14 22:21
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/11/2014 03:43 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Sample: MW-6
Lab ID: 92207829001
Collected:
07/02/14 10:45
Received: 07/03/14 08:05 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
2110 ug/L
25.0
11.5
25
07/09/14 11:19
127-18-4
Toluene
9.7J ug/L
10.0
2.6
10
07/08/14 22:21
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
10.0
3.3
10
07/08/14 22:21
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
10.0
3.5
10
07/08/14 22:21
120-82-1
1,1,1-Trichloroethane
ND ug/L
10.0
4.8
10
07/08/14 22:21
71-55-6
1,1,2-Trichloroethane
ND ug/L
10.0
2.9
10
07/08/14 22:21
79-00-5
Trichloroethene
80.6 ug/L
10.0
4.7
10
07/08/14 22:21
79-01-6
Trichlorofluoromethane
ND ug/L
10.0
2.0
10
07/08/14 22:21
75-69-4
1,2,3-Trichloropropane
ND ug/L
10.0
4.1
10
07/08/14 22:21
96-18-4
Vinyl acetate
ND ug/L
20.0
3.5
10
07/08/14 22:21
108-05-4
Vinyl chloride
ND ug/L
10.0
6.2
10
07/08/14 22:21
75-01-4
Xylene (Total)
ND ug/L
20.0
6.6
10
07/08/14 22:21
1330-20-7
m&p-Xylene
ND ug/L
20.0
6.6
10
07/08/14 22:21
179601-23-1
o-Xylene
ND ug/L
10.0
2.3
10
07/08/14 22:21
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
10
07/08/14 22:21
460-00-4
1,2-Dichloroethane-d4 (S)
101 %
70-130
10
07/08/14 22:21
17060-07-0
Toluene-d8 (S)
101 %
70-130
10
07/08/14 22:21
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 6.1 mg/L 1.0 1.0 1 07/10/14 22:37 7440-44-0
Date: 07/11/2014 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Sample: MW-44 Lab ID: 92207829002 Collected: 07/02/14 09:50 Received: 07/03/14 08:05 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
ND ug/L
250
100
10
07/08/14 22:37
67-64-1
Benzene
ND ug/L
10.0
2.5
10
07/08/14 22:37
71-43-2
Bromobenzene
ND ug/L
10.0
3.0
10
07/08/14 22:37
108-86-1
Bromochloromethane
ND ug/L
10.0
1.7
10
07/08/14 22:37
74-97-5
Bromodichloromethane
ND ug/L
10.0
1.8
10
07/08/14 22:37
75-27-4
Bromoform
ND ug/L
10.0
2.6
10
07/08/14 22:37
75-25-2
Bromomethane
ND ug/L
20.0
2.9
10
07/08/14 22:37
74-83-9
2-Butanone (MEK)
ND ug/L
50.0
9.6
10
07/08/14 22:37
78-93-3
Carbon tetrachloride
ND ug/L
10.0
2.5
10
07/08/14 22:37
56-23-5
Chlorobenzene
ND ug/L
10.0
2.3
10
07/08/14 22:37
108-90-7
Chloroethane
ND ug/L
10.0
5.4
10
07/08/14 22:37
75-00-3
Chloroform
ND ug/L
10.0
1.4
10
07/08/14 22:37
67-66-3
Chloromethane
ND ug/L
10.0
1.1
10
07/08/14 22:37
74-87-3
2-Chlorotoluene
ND ug/L
10.0
3.5
10
07/08/14 22:37
95-49-8
4-Chlorotoluene
ND ug/L
10.0
3.1
10
07/08/14 22:37
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
20.0
20.0
10
07/08/14 22:37
96-12-8
Dibromochloromethane
ND ug/L
10.0
2.1
10
07/08/14 22:37
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
10.0
2.7
10
07/08/14 22:37
106-93-4
Dibromomethane
ND ug/L
10.0
2.1
10
07/08/14 22:37
74-95-3
1,2-Dichlorobenzene
ND ug/L
10.0
3.0
10
07/08/14 22:37
95-50-1
1,3-Dichlorobenzene
ND ug/L
10.0
2.4
10
07/08/14 22:37
541-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
3.3
10
07/08/14 22:37
106-46-7
Dichlorodifluoromethane
ND ug/L
10.0
2.1
10
07/08/14 22:37
75-71-8
1,1-Dichloroethane
ND ug/L
10.0
3.2
10
07/08/14 22:37
75-34-3
1,2-Dichloroethane
ND ug/L
10.0
1.2
10
07/08/14 22:37
107-06-2
1,1-Dichloroethene
ND ug/L
10.0
5.6
10
07/08/14 22:37
75-35-4
cis-1,2-Dichloroethene
825 ug/L
10.0
1.9
10
07/08/14 22:37
156-59-2
trans-1,2-Dichloroethene
5.5J ug/L
10.0
4.9
10
07/08/14 22:37
156-60-5
1,2-Dichloropropane
ND ug/L
10.0
2.7
10
07/08/14 22:37
78-87-5
1,3-Dichloropropane
ND ug/L
10.0
2.8
10
07/08/14 22:37
142-28-9
2,2-Dichloropropane
ND ug/L
10.0
1.3
10
07/08/14 22:37
594-20-7
1,1-Dichloropropene
ND ug/L
10.0
4.9
10
07/08/14 22:37
563-58-6
cis-1,3-Dichloropropene
ND ug/L
10.0
1.3
10
07/08/14 22:37
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
10.0
2.6
10
07/08/14 22:37
10061-02-6
Diisopropyl ether
ND ug/L
10.0
1.2
10
07/08/14 22:37
108-20-3
Ethylbenzene
ND ug/L
10.0
3.0
10
07/08/14 22:37
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
10.0
7.1
10
07/08/14 22:37
87-68-3
2-Hexanone
ND ug/L
50.0
4.6
10
07/08/14 22:37
591-78-6
p-Isopropyltoluene
ND ug/L
10.0
3.1
10
07/08/14 22:37
99-87-6
Methylene Chloride
17.6J ug/L
20.0
9.7
10
07/08/14 22:37
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
50.0
3.3
10
07/08/14 22:37
108-10-1
Methyl-tert-butyl ether
ND ug/L
10.0
2.1
10
07/08/14 22:37
1634-04-4
Naphthalene
ND ug/L
10.0
2.4
10
07/08/14 22:37
91-20-3
Styrene
ND ug/L
10.0
2.6
10
07/08/14 22:37
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
10.0
3.3
10
07/08/14 22:37
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
10.0
4.0
10
07/08/14 22:37
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/11/2014 03:43 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Sample: MW-44
Lab ID: 92207829002
Collected:
07/02/14 09:50
Received: 07/03/14 08:05 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
4260 ug/L
50.0
23.0
50
07/09/14 11:35
127-18-4
Toluene
11.9 ug/L
10.0
2.6
10
07/08/14 22:37
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
10.0
3.3
10
07/08/14 22:37
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
10.0
3.5
10
07/08/14 22:37
120-82-1
1,1,1-Trichloroethane
ND ug/L
10.0
4.8
10
07/08/14 22:37
71-55-6
1,1,2-Trichloroethane
ND ug/L
10.0
2.9
10
07/08/14 22:37
79-00-5
Trichloroethene
167 ug/L
10.0
4.7
10
07/08/14 22:37
79-01-6
Trichlorofluoromethane
ND ug/L
10.0
2.0
10
07/08/14 22:37
75-69-4
1,2,3-Trichloropropane
ND ug/L
10.0
4.1
10
07/08/14 22:37
96-18-4
Vinyl acetate
ND ug/L
20.0
3.5
10
07/08/14 22:37
108-05-4
Vinyl chloride
24.2 ug/L
10.0
6.2
10
07/08/14 22:37
75-01-4
Xylene (Total)
ND ug/L
20.0
6.6
10
07/08/14 22:37
1330-20-7
m&p-Xylene
ND ug/L
20.0
6.6
10
07/08/14 22:37
179601-23-1
o-Xylene
ND ug/L
10.0
2.3
10
07/08/14 22:37
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
10
07/08/14 22:37
460-00-4
1,2-Dichloroethane-d4 (S)
103 %
70-130
10
07/08/14 22:37
17060-07-0
Toluene-d8 (S)
99 %
70-130
10
07/08/14 22:37
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 6.3 mg/L 1.0 1.0 1 07/10/14 22:47 7440-44-0
Date: 07/11/2014 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Sample: RW-1 Lab ID: 92207829003 Collected: 07/02/14 10:15 Received: 07/03/14 08:05 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Analytical Method: EPA 8260
Acetone
317J ug/L
625
250
25
07/08/14 22:54
67-64-1
Benzene
7.1J ug/L
25.0
6.2
25
07/08/14 22:54
71-43-2
Bromobenzene
ND ug/L
25.0
7.5
25
07/08/14 22:54
108-86-1
Bromochloromethane
ND ug/L
25.0
4.2
25
07/08/14 22:54
74-97-5
Bromodichloromethane
ND ug/L
25.0
4.5
25
07/08/14 22:54
75-27-4
Bromoform
ND ug/L
25.0
6.5
25
07/08/14 22:54
75-25-2
Bromomethane
ND ug/L
50.0
7.2
25
07/08/14 22:54
74-83-9
2-Butanone (MEK)
299 ug/L
125
24.0
25
07/08/14 22:54
78-93-3
Carbon tetrachloride
ND ug/L
25.0
6.2
25
07/08/14 22:54
56-23-5
Chlorobenzene
ND ug/L
25.0
5.8
25
07/08/14 22:54
108-90-7
Chloroethane
ND ug/L
25.0
13.5
25
07/08/14 22:54
75-00-3
Chloroform
ND ug/L
25.0
3.5
25
07/08/14 22:54
67-66-3
Chloromethane
ND ug/L
25.0
2.8
25
07/08/14 22:54
74-87-3
2-Chlorotoluene
ND ug/L
25.0
8.8
25
07/08/14 22:54
95-49-8
4-Chlorotoluene
ND ug/L
25.0
7.8
25
07/08/14 22:54
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
50.0
50.0
25
07/08/14 22:54
96-12-8
Dibromochloromethane
ND ug/L
25.0
5.2
25
07/08/14 22:54
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
25.0
6.8
25
07/08/14 22:54
106-93-4
Dibromomethane
ND ug/L
25.0
5.2
25
07/08/14 22:54
74-95-3
1,2-Dichlorobenzene
ND ug/L
25.0
7.5
25
07/08/14 22:54
95-50-1
1,3-Dichlorobenzene
ND ug/L
25.0
6.0
25
07/08/14 22:54
541-73-1
1,4-Dichlorobenzene
ND ug/L
25.0
8.2
25
07/08/14 22:54
106-46-7
Dichlorodifluoromethane
ND ug/L
25.0
5.2
25
07/08/14 22:54
75-71-8
1,1-Dichloroethane
ND ug/L
25.0
8.0
25
07/08/14 22:54
75-34-3
1,2-Dichloroethane
ND ug/L
25.0
3.0
25
07/08/14 22:54
107-06-2
1,1-Dichloroethene
ND ug/L
25.0
14.0
25
07/08/14 22:54
75-35-4
cis-1,2-Dichloroethene
3130 ug/L
25.0
4.8
25
07/08/14 22:54
156-59-2
trans-1,2-Dichloroethene
ND ug/L
25.0
12.2
25
07/08/14 22:54
156-60-5
1,2-Dichloropropane
ND ug/L
25.0
6.8
25
07/08/14 22:54
78-87-5
1,3-Dichloropropane
ND ug/L
25.0
7.0
25
07/08/14 22:54
142-28-9
2,2-Dichloropropane
ND ug/L
25.0
3.2
25
07/08/14 22:54
594-20-7
1,1-Dichloropropene
ND ug/L
25.0
12.2
25
07/08/14 22:54
563-58-6
cis-1,3-Dichloropropene
ND ug/L
25.0
3.2
25
07/08/14 22:54
10061-01-5
trans- 1,3-Dichloropropene
ND ug/L
25.0
6.5
25
07/08/14 22:54
10061-02-6
Diisopropyl ether
ND ug/L
25.0
3.0
25
07/08/14 22:54
108-20-3
Ethylbenzene
ND ug/L
25.0
7.5
25
07/08/14 22:54
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
25.0
17.8
25
07/08/14 22:54
87-68-3
2-Hexanone
ND ug/L
125
11.5
25
07/08/14 22:54
591-78-6
p-Isopropyltoluene
ND ug/L
25.0
7.8
25
07/08/14 22:54
99-87-6
Methylene Chloride
38.9J ug/L
50.0
24.2
25
07/08/14 22:54
75-09-2
4-Methyl-2-pentanone (MIBK)
ND ug/L
125
8.2
25
07/08/14 22:54
108-10-1
Methyl-tert-butyl ether
ND ug/L
25.0
5.2
25
07/08/14 22:54
1634-04-4
Naphthalene
ND ug/L
25.0
6.0
25
07/08/14 22:54
91-20-3
Styrene
ND ug/L
25.0
6.5
25
07/08/14 22:54
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
25.0
8.2
25
07/08/14 22:54
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
25.0
10.0
25
07/08/14 22:54
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/11/2014 03:43 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Sample: RW-1
Lab ID: 92207829003
Collected:
07/02/14 10:15
Received: 07/03/14 08:05 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
43.4 ug/L
25.0
11.5
25
07/08/14 22:54
127-18-4
Toluene
39.8 ug/L
25.0
6.5
25
07/08/14 22:54
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
25.0
8.2
25
07/08/14 22:54
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
25.0
8.8
25
07/08/14 22:54
120-82-1
1,1,1-Trichloroethane
ND ug/L
25.0
12.0
25
07/08/14 22:54
71-55-6
1,1,2-Trichloroethane
ND ug/L
25.0
7.2
25
07/08/14 22:54
79-00-5
Trichloroethene
29.5 ug/L
25.0
11.8
25
07/08/14 22:54
79-01-6
Trichlorofluoromethane
ND ug/L
25.0
5.0
25
07/08/14 22:54
75-69-4
1,2,3-Trichloropropane
ND ug/L
25.0
10.2
25
07/08/14 22:54
96-18-4
Vinyl acetate
ND ug/L
50.0
8.8
25
07/08/14 22:54
108-05-4
Vinyl chloride
43.9 ug/L
25.0
15.5
25
07/08/14 22:54
75-01-4
Xylene (Total)
ND ug/L
50.0
16.5
25
07/08/14 22:54
1330-20-7
m&p-Xylene
ND ug/L
50.0
16.5
25
07/08/14 22:54
179601-23-1
o-Xylene
ND ug/L
25.0
5.8
25
07/08/14 22:54
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95 %
70-130
25
07/08/14 22:54
460-00-4
1,2-Dichloroethane-d4 (S)
106 %
70-130
25
07/08/14 22:54
17060-07-0
Toluene-d8 (S)
105 %
70-130
25
07/08/14 22:54
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 412 mg/L 100 100 100 07/10/14 22:58 7440-44-0
Date: 07/11/2014 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Sample: IW-2 Lab ID: 92207829004 Collected: 07/02/14 11:05 Received: 07/03/14 08:05 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Date: 07/11/2014 03:43 PM
Analytical Method: EPA 8260
ND ug/L
625
250
25
07/08/14 23:10
67-64-1 D3
8.1J ug/L
25.0
6.2
25
07/08/14 23:10
71-43-2
ND ug/L
25.0
7.5
25
07/08/14 23:10
108-86-1
ND ug/L
25.0
4.2
25
07/08/14 23:10
74-97-5
ND ug/L
25.0
4.5
25
07/08/14 23:10
75-27-4
ND ug/L
25.0
6.5
25
07/08/14 23:10
75-25-2
ND ug/L
50.0
7.2
25
07/08/14 23:10
74-83-9
ND ug/L
125
24.0
25
07/08/14 23:10
78-93-3
ND ug/L
25.0
6.2
25
07/08/14 23:10
56-23-5
ND ug/L
25.0
5.8
25
07/08/14 23:10
108-90-7
ND ug/L
25.0
13.5
25
07/08/14 23:10
75-00-3
8.2J ug/L
25.0
3.5
25
07/08/14 23:10
67-66-3
ND ug/L
25.0
2.8
25
07/08/14 23:10
74-87-3
ND ug/L
25.0
8.8
25
07/08/14 23:10
95-49-8
ND ug/L
25.0
7.8
25
07/08/14 23:10
106-43-4
ND ug/L
50.0
50.0
25
07/08/14 23:10
96-12-8
ND ug/L
25.0
5.2
25
07/08/14 23:10
124-48-1
ND ug/L
25.0
6.8
25
07/08/14 23:10
106-93-4
ND ug/L
25.0
5.2
25
07/08/14 23:10
74-95-3
ND ug/L
25.0
7.5
25
07/08/14 23:10
95-50-1
ND ug/L
25.0
6.0
25
07/08/14 23:10
541-73-1
ND ug/L
25.0
8.2
25
07/08/14 23:10
106-46-7
ND ug/L
25.0
5.2
25
07/08/14 23:10
75-71-8
ND ug/L
25.0
8.0
25
07/08/14 23:10
75-34-3
ND ug/L
25.0
3.0
25
07/08/14 23:10
107-06-2
ND ug/L
25.0
14.0
25
07/08/14 23:10
75-35-4
25.2 ug/L
25.0
4.8
25
07/08/14 23:10
156-59-2
ND ug/L
25.0
12.2
25
07/08/14 23:10
156-60-5
ND ug/L
25.0
6.8
25
07/08/14 23:10
78-87-5
ND ug/L
25.0
7.0
25
07/08/14 23:10
142-28-9
ND ug/L
25.0
3.2
25
07/08/14 23:10
594-20-7
ND ug/L
25.0
12.2
25
07/08/14 23:10
563-58-6
ND ug/L
25.0
3.2
25
07/08/14 23:10
10061-01-5
ND ug/L
25.0
6.5
25
07/08/14 23:10
10061-02-6
ND ug/L
25.0
3.0
25
07/08/14 23:10
108-20-3
ND ug/L
25.0
7.5
25
07/08/14 23:10
100-41-4
ND ug/L
25.0
17.8
25
07/08/14 23:10
87-68-3
ND ug/L
125
11.5
25
07/08/14 23:10
591-78-6
ND ug/L
25.0
7.8
25
07/08/14 23:10
99-87-6
44.3J ug/L
50.0
24.2
25
07/08/14 23:10
75-09-2
ND ug/L
125
8.2
25
07/08/14 23:10
108-10-1
ND ug/L
25.0
5.2
25
07/08/14 23:10
1634-04-4
ND ug/L
25.0
6.0
25
07/08/14 23:10
91-20-3
ND ug/L
25.0
6.5
25
07/08/14 23:10
100-42-5
ND ug/L
25.0
8.2
25
07/08/14 23:10
630-20-6
ND ug/L
25.0
10.0
25
07/08/14 23:10
79-34-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 20

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Sample: IW-2
Lab ID: 92207829004
Collected:
07/02/14 11:05
Received: 07/03/14 08:05 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Tetrachloroethene
ND ug/L
25.0
11.5
25
07/08/14 23:10
127-18-4
Toluene
38.1 ug/L
25.0
6.5
25
07/08/14 23:10
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
25.0
8.2
25
07/08/14 23:10
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
25.0
8.8
25
07/08/14 23:10
120-82-1
1,1,1-Trichloroethane
ND ug/L
25.0
12.0
25
07/08/14 23:10
71-55-6
1,1,2-Trichloroethane
ND ug/L
25.0
7.2
25
07/08/14 23:10
79-00-5
Trichloroethene
ND ug/L
25.0
11.8
25
07/08/14 23:10
79-01-6
Trichlorofluoromethane
ND ug/L
25.0
5.0
25
07/08/14 23:10
75-69-4
1,2,3-Trichloropropane
ND ug/L
25.0
10.2
25
07/08/14 23:10
96-18-4
Vinyl acetate
ND ug/L
50.0
8.8
25
07/08/14 23:10
108-05-4
Vinyl chloride
ND ug/L
25.0
15.5
25
07/08/14 23:10
75-01-4
Xylene (Total)
ND ug/L
50.0
16.5
25
07/08/14 23:10
1330-20-7
m&p-Xylene
ND ug/L
50.0
16.5
25
07/08/14 23:10
179601-23-1
o-Xylene
ND ug/L
25.0
5.8
25
07/08/14 23:10
95-47-6
Surrogates
4-Bromofluorobenzene (S)
93 %
70-130
25
07/08/14 23:10
460-00-4
1,2-Dichloroethane-d4 (S)
107 %
70-130
25
07/08/14 23:10
17060-07-0
Toluene-d8 (S)
105 %
70-130
25
07/08/14 23:10
2037-26-5
5310E TOC Analytical Method: SM 5310B
Total Organic Carbon 2370 mg/L 100 100 100 07/11/14 11:49 7440-44-0 M6
Date: 07/11/2014 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
QC Batch: MSV/27512 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92207829001, 92207829002, 92207829003, 92207829004
METHOD BLANK: 1237546 Matrix: Water
Associated Lab Samples: 92207829001, 92207829002, 92207829003, 92207829004
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
07/08/14 19:02
1,1,1-Trichloroethane
ug/L
ND
1.0
07/08/14 19:02
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
07/08/14 19:02
1,1,2-Trichloroethane
ug/L
ND
1.0
07/08/14 19:02
1,1-Dichloroethane
ug/L
ND
1.0
07/08/14 19:02
1,1-Dichloroethene
ug/L
ND
1.0
07/08/14 19:02
1,1-Dichloropropene
ug/L
ND
1.0
07/08/14 19:02
1,2,3-Trichlorobenzene
ug/L
ND
1.0
07/08/14 19:02
1,2,3-Trichloropropane
ug/L
ND
1.0
07/08/14 19:02
1,2,4-Trichlorobenzene
ug/L
ND
1.0
07/08/14 19:02
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
07/08/14 19:02
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
07/08/14 19:02
1,2-Dichlorobenzene
ug/L
ND
1.0
07/08/14 19:02
1,2-Dichloroethane
ug/L
ND
1.0
07/08/14 19:02
1,2-Dichloropropane
ug/L
ND
1.0
07/08/14 19:02
1,3-Dichlorobenzene
ug/L
ND
1.0
07/08/14 19:02
1,3-Dichloropropane
ug/L
ND
1.0
07/08/14 19:02
1,4-Dichlorobenzene
ug/L
ND
1.0
07/08/14 19:02
2,2-Dichloropropane
ug/L
ND
1.0
07/08/14 19:02
2-Butanone (MEK)
ug/L
ND
5.0
07/08/14 19:02
2-Chlorotoluene
ug/L
ND
1.0
07/08/14 19:02
2-Hexanone
ug/L
ND
5.0
07/08/14 19:02
4-Chlorotoluene
ug/L
ND
1.0
07/08/14 19:02
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
07/08/14 19:02
Acetone
ug/L
ND
25.0
07/08/14 19:02
Benzene
ug/L
ND
1.0
07/08/14 19:02
Bromobenzene
ug/L
ND
1.0
07/08/14 19:02
Bromochloromethane
ug/L
ND
1.0
07/08/14 19:02
Bromodichloromethane
ug/L
ND
1.0
07/08/14 19:02
Bromoform
ug/L
ND
1.0
07/08/14 19:02
Bromomethane
ug/L
ND
2.0
07/08/14 19:02
Carbon tetrachloride
ug/L
ND
1.0
07/08/14 19:02
Chlorobenzene
ug/L
ND
1.0
07/08/14 19:02
Chloroethane
ug/L
ND
1.0
07/08/14 19:02
Chloroform
ug/L
ND
1.0
07/08/14 19:02
Chloromethane
ug/L
ND
1.0
07/08/14 19:02
cis-1,2-Dichloroethene
ug/L
ND
1.0
07/08/14 19:02
cis-1,3-Dichloropropene
ug/L
ND
1.0
07/08/14 19:02
Dibromochloromethane
ug/L
ND
1.0
07/08/14 19:02
Dibromomethane
ug/L
ND
1.0
07/08/14 19:02
Dichlorodifluoromethane
ug/L
ND
1.0
07/08/14 19:02
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/11/2014 03:43 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
METHOD BLANK: 1237546 Matrix: Water
Associated Lab Samples: 92207829001, 92207829002, 92207829003, 92207829004
Blank Reporting
Parameter Units Result Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
07/08/14 19:02
Ethylbenzene
ug/L
ND
1.0
07/08/14 19:02
Hexachloro-1,3-butadiene
ug/L
ND
1.0
07/08/14 19:02
m&p-Xylene
ug/L
ND
2.0
07/08/14 19:02
Methyl-tert-butyl ether
ug/L
ND
1.0
07/08/14 19:02
Methylene Chloride
ug/L
ND
2.0
07/08/14 19:02
Naphthalene
ug/L
ND
1.0
07/08/14 19:02
o-Xylene
ug/L
ND
1.0
07/08/14 19:02
p-Isopropyltoluene
ug/L
ND
1.0
07/08/14 19:02
Styrene
ug/L
ND
1.0
07/08/14 19:02
Tetrachloroethene
ug/L
ND
1.0
07/08/14 19:02
Toluene
ug/L
ND
1.0
07/08/14 19:02
trans-1,2-Dichloroethene
ug/L
ND
1.0
07/08/14 19:02
trans- 1,3-Dichloropropene
ug/L
ND
1.0
07/08/14 19:02
Trichloroethene
ug/L
ND
1.0
07/08/14 19:02
Trichlorofluoromethane
ug/L
ND
1.0
07/08/14 19:02
Vinyl acetate
ug/L
ND
2.0
07/08/14 19:02
Vinyl chloride
ug/L
ND
1.0
07/08/14 19:02
Xylene (Total)
ug/L
ND
2.0
07/08/14 19:02
1,2-Dichloroethane-d4 (S)
%
104
70-130
07/08/14 19:02
4-Bromofluorobenzene (S)
%
95
70-130
07/08/14 19:02
Toluene-d8 (S)
%
103
70-130
07/08/14 19:02
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1237547
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
46.5
93
70-130
1,1,1-Trichloroethane
ug/L
50
52.1
104
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.3
105
70-130
1,1,2-Trichloroethane
ug/L
50
52.0
104
70-130
1,1-Dichloroethane
ug/L
50
50.9
102
70-130
1,1-Dichloroethene
ug/L
50
54.6
109
70-132
1,1-Dichloropropene
ug/L
50
55.0
110
70-130
1,2,3-Trichlorobenzene
ug/L
50
56.3
113
70-135
1,2,3-Trichloropropane
ug/L
50
52.2
104
70-130
1,2,4-Trichlorobenzene
ug/L
50
56.8
114
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
51.5
103
70-130
1,2-Dibromoethane (EDB)
ug/L
50
56.9
114
70-130
1,2-Dichlorobenzene
ug/L
50
53.1
106
70-130
1,2-Dichloroethane
ug/L
50
50.4
101
70-130
1,2-Dichloropropane
ug/L
50
51.4
103
70-130
1,3-Dichlorobenzene
ug/L
50
50.6
101
70-130
1,3-Dichloropropane
ug/L
50
54.7
109
70-130
1,4-Dichlorobenzene
ug/L
50
50.1
100
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/11/2014 03:43 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 20

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
LABORATORY CONTROL SAMPLE:
Parameter
1237547
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
53.5
107
58-145
2-Butanone (MEK)
ug/L
100
106
106
70-145
2-Chlorotoluene
ug/L
50
47.8
96
70-130
2-Hexanone
ug/L
100
108
108
70-144
4-Chlorotoluene
ug/L
50
50.8
102
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
103
103
70-140
Acetone
ug/L
100
107
107
50-175
Benzene
ug/L
50
51.6
103
70-130
Bromobenzene
ug/L
50
51.3
103
70-130
Bromochloromethane
ug/L
50
54.1
108
70-130
Bromodichloromethane
ug/L
50
50.7
101
70-130
Bromoform
ug/L
50
42.2
84
70-130
Bromomethane
ug/L
50
42.0
84
54-130
Carbon tetrachloride
ug/L
50
46.9
94
70-132
Chlorobenzene
ug/L
50
49.7
99
70-130
Chloroethane
ug/L
50
34.4
69
64-134
Chloroform
ug/L
50
49.2
98
70-130
Chloromethane
ug/L
50
49.0
98
64-130
cis-1,2-Dichloroethene
ug/L
50
50.0
100
70-131
cis-1,3-Dichloropropene
ug/L
50
49.1
98
70-130
Dibromochloromethane
ug/L
50
45.5
91
70-130
Dibromomethane
ug/L
50
47.4
95
70-131
Dichlorodifluoromethane
ug/L
50
41.5
83
56-130
Diisopropyl ether
ug/L
50
51.8
104
70-130
Ethylbenzene
ug/L
50
51.1
102
70-130
Hexachloro-1,3-butadiene
ug/L
50
56.1
112
70-130
m&p-Xylene
ug/L
100
104
104
70-130
Methyl-tert-butyl ether
ug/L
50
51.6
103
70-130
Methylene Chloride
ug/L
50
55.7
111
63-130
Naphthalene
ug/L
50
57.5
115
70-138
o-Xylene
ug/L
50
52.0
104
70-130
p-Isopropyltoluene
ug/L
50
55.4
111
70-130
Styrene
ug/L
50
54.7
109
70-130
Tetrachloroethene
ug/L
50
55.3
111
70-130
Toluene
ug/L
50
49.8
100
70-130
trans-1,2-Dichloroethene
ug/L
50
52.1
104
70-130
trans- 1,3-Dichloropropene
ug/L
50
53.8
108
70-132
Trichloroethene
ug/L
50
52.0
104
70-130
Trichlorofluoromethane
ug/L
50
48.4
97
62-133
Vinyl acetate
ug/L
100
110
110
66-157
Vinyl chloride
ug/L
50
48.9
98
50-150
Xylene (Total)
ug/L
150
156
104
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
97
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/11/2014 03:43 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 20

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
QC Batch: WETA/19522
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92207829001, 92207829002,
92207829003, 92207829004
METHOD BLANK: 1237405
Matrix: Water
Associated Lab Samples: 92207829001, 92207829002,
92207829003, 92207829004
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0
07/10/14 20:08
LABORATORY CONTROL SAMPLE: 1237406
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25 24.0
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1237407 1237408
MS MSD
92207053003
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 5.5
25 25 30.7
30.4 101 100 75-125 1 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1237409 1237410
MS MSD
92207829004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Total Organic Carbon mg/L 2370 25 25 2280 2260 -332 -412 75-125 1 20 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/11/2014 03:43 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 20

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LOD - Limit of Detection.
LOQ - Limit of Quantitation.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/11/2014 03:43 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 20

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: FORMER ANDREX INDUSTRIES
Pace Project No.: 92207829
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92207829001
MW-6
EPA 8260
MSV/27512
92207829002
MW-44
EPA 8260
MSV/27512
92207829003
RW-1
EPA 8260
MSV/27512
92207829004
IW-2
EPA 8260
MSV/27512
92207829001
MW-6
SM
5310B
WETA/19522
92207829002
MW-44
SM
5310B
WETA/19522
92207829003
RW-1
SM
5310B
WETA/19522
92207829004
IW-2
SM
5310B
WETA/19522
Date: 07/11/2014 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 18 of 20

l Document Name: ;ample Condition Upon Document Revised: June 10, 2014
Plc Anal yt1C3/ Receipt (SGUFt) Page 1 of 2
Document No.: Issuing Authorities:
t. {� i
F-ASV-CS-003-rev.j14 Pace Asheville Quality Office
Client ��v1rne: �),,,v�1_', '
Courier (Circle): Fed Ex UPS US;(e<slrL�
C'IiGrt Commercial Pace Other___
Custody Seal on Cooler/Box Present: ED no Seals intact: [] yes (] no
Packing Material: L_� Bubble Wrap J_ Bubble Bags ❑ None Other, `
Thermorneter Used: IR Gun#3-130265963 Type of Ice: Blue None Samples on ice, cooling process has begun
IR ran 14 SM-140290365 Other: _
Temp Correction Factor: Add / Subtract , C
Corrected Cooler Temp.:t. Zi C
Biological Tissue is Frozen: Yes No IA
pate and inittr I o person erfarnining
contents: % 5`
Temp should be above freezing to 61C
/�`
Comments:
Chain of Custody Present:
No
11N/A
1.
Chain of Custody Filled Out:
es Ne
❑wA
2.
Chain of Custody Relinquished:
G4e,,- Na
❑NIA
3.
Sampler Name & Signature an COC:
1/4❑No
LdN/A
4.
Samples Arrived within Hold Time:
O/Yes ❑No
1JN/A
5.
Short Hold Time Analysis (<72hr):
❑Ye Nu
❑N/A
6.
Rush Turn Around Time Requested:
e L-1No
❑N/A
7. vie —�k
Sufficient Volume:
Yes . No
❑N/A
8.
Correct Containers Used:
.1-1 Ye -.)No
El N/A
9.
-Pace Containers Used:
2ysl_ No
ON/A
Containers Intact:
UYes ❑No
LOINIA,
G.
Filtered volume received for Dissolved tests
❑Ye�o
/A
11,
Sample labels match COC:
Yes ❑No
_
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.F)I
les No
❑NIA
13.
All containers needing preservation are found to be in
Yes ❑ o
❑NIA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
- Yes _ No
Samples checked for dechlorination:
es o
. N/A
14.
Headspace in VOA Vials ( =6mm):
❑Yes �No--E]N/A
15.
Trip Blank Present:
❑Yes VNo
❑N/A
ht5-
Trip Blank Custody Seals Present
❑Yes ❑No
_ N/A
Pace Trip Blank Lot it (if purchased):__
Client Notification/ Resolution:
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:l !/ �� DDate:
SRF Review:w jDato:
Note: Whenever re is a discrepancy affecting North Carolina
compliance samples, a copy of this form will be sent to the North
Carolina DEHNR Certification Office (Le out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y / N
Place label here
C� aw79 2- - (DR
Handwrite project number
(if no label available)
Page 19 of 20

0.0
PaceAnalytical
www.0acetabs.cam
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately -
Section A Section B Section C
Page: / of l
( f
Required Client Information: Required Project Information: Invoice Information:
Company: Report To: Attention:
z t
_
Address: Copy
To:
Company Name:
REGULATORY AGENCY
-r
i
Address:---
NPDES GROUND WATER DRINKING VJATEP,
-
UST RCRA OTHER
Email To: Purchase
Order No.:
Pace a -ate
tM
References
P one' �S� F Project
Name:
1
al e�,e ti ri/t i*^
Pace Pro eel P
1,4 � er: r,-
n
SLi
Site
STATE:
14 G
Requested Due DateRAT: d Project
Number. �L
e1 (
Pace Pronie 4:
Requested
Analysis
Filtered
(YIN}
Section D Matrix Codes
-
a
Z
Required Client lnfom:aeicn MATRx ; CODE
-
COLLECTED
Preservatives
i-
Drinking ;relater DW
O
O
Water WT
$
O
I
waste Water "VW
COMPOSITE
COP'aOSiT'
Product P
-
�
START
-r+nrO�aa
O
z
SoiUSOlid SL
o
Q
IL
SAl1 PLE ID oil
t?
U
�
I
e
(A-2. 0-9 ?:) Air AR
LU
a
L,
Z
I
N
FIV
I
c
Sample IDS MUST BE UNIQUE Tissue TS
O
0.
H
0
y
I
C:
Other OT
U
x
u
w
z
O.
'N
V
�
�
O
p
O
tn"
L�
r�
0
�
n
G
�
r
O
1
DATE
TIME
, DATE
TIME
N
2
2
T
Z
Z
O
.,�
tr
Pace Project No.! a I.D.
1
AU) �O
I •t32•i
Q+
i
2
MLO -*+
1
r,I
'G2•
O
(0
11
4
wr
ot- 14,
Ito 5
�4
I
5
6
7
8
9
j
I
10
11
i
12
ADDITIONAL COMMENTS
RELINQUISHED BY! AFFILIATION
DATE
TIME
EPTED BY 1 AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
I
i
I
�
E
i
SAMPLER NAME AND SIGNATURE
PRINT Name of SAMPLER
SIGNATURE Of SAMPLER:
DATE Signed
e ., - I are a« 1:,:g I'. -a NET ;g day p<-atr-art i -r s ald a9reei p :c ate d qe: of i..i., per eD; paid wrtim i6 days ` :ALL-0-020rev.07. 15-M iy-2007

APPENDIX F
LABORATORY ANALYTICAL DATA SHEETS
GROUNDWATER & SURFACE WATER
SEPTEMBER 2014 [90 Day]
(Provided on Enclosed CD)

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Tuesday September 16, 2014
Report Number: L720290
Samples Received: 09/06/14
Client Project: J14-1022-40
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
Jimmy Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-3
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 11:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-01
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
47000
Volatile Organics
Acetone
160
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
170
trans-1,2-Dichloroethene
5.7
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
10000 ug/l 9060A 09/12/14 10
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 2 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-3
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 11:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-01
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
17.
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
1.6
1.0
ug/1
8260B
09/09/14
Toluene
730
120
ug/1
8260B
09/15/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
47.
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.9
% Rec.
8260B
09/09/14
Dibromofluoromethane
94.8
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
100.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 3 of 63
1
1
1
1
1
1
1
1
1
1
1
1
1
25
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-5
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 10:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-02
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
350
trans-1,2-Dichloroethene
5.2
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14 1
50.
ug/l
8260B
09/10/14
1
50.
ug/1
8260B
09/10/14
1
10.
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
50.
ug/1
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
2.5
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
100
ug/l
8260B
09/11/14
100
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
Page 4 of 63

12065
Lebanon Rd.
Mt. Juliet,
TN 37122
(615)
758-5858
1-800-767-5859
Fax (615)
758-5859
Tax I.D.
62-0814289
Est.
1970
REPORT
OF ANALYSIS
Mr. Andy Alexander
September
16,2014
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC
Sample #
L720290-02
Date Received September 06, 2014
Description Andrex Industries
Site
ID
ASHEVILLE, NC
Sample ID MW-5
Project
#
J14-1022-40
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 10:00
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/10/14
1
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/10/14
1
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/10/14
1
Methylene Chloride
BDL
5.0
ug/l
8260B
09/10/14
1
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/10/14
1
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/10/14
1
Naphthalene
BDL
5.0
ug/1
8260B
09/10/14
1
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/10/14
1
Styrene
BDL
1.0
ug/1
8260B
09/10/14
1
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/10/14
1
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/10/14
1
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/10/14
1
Tetrachloroethene
2200
100
ug/1
8260B
09/11/14
100
Toluene
BDL
5.0
ug/1
8260B
09/10/14
1
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/10/14
1
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/10/14
1
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/10/14
1
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/10/14
1
Trichloroethene
160
1.0
ug/1
8260B
09/10/14
1
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/10/14
1
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/10/14
1
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
1
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/10/14
1
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
1
Vinyl chloride
53.
1.0
ug/1
8260B
09/10/14
1
Xylenes, Total
BDL
3.0
ug/l
8260B
09/10/14
1
Surrogate Recovery
Toluene-d8
98.7
% Rec.
8260B
09/10/14
1
Dibromofluoromethane
101.
% Rec.
8260B
09/10/14
1
4-Bromofluorobenzene
87.9
% Rec.
8260B
09/10/14
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 5 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-12
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 09:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-03
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
3000
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
18.
trans-1,2-Dichloroethene
10.
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 6 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-12
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 09:30
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-03
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
1.6
1.0
ug/1
8260B
09/09/14
Toluene
240
50.
ug/1
8260B
09/11/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
9.6
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
98.8
% Rec.
8260B
09/09/14
Dibromofluoromethane
101.
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
98.5
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 7 of 63
1
1
1
1
1
1
1
1
1
1
1
1
1
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID IW-2
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 11:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-04
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
2600000
Volatile Organics
Acetone
180
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
55.
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
100000 ug/l 9060A
09/12/14 100
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 8 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID IW-2
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 11:30
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-04
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
530
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
9.2
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
1.4
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
1.9
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
96.4
% Rec.
8260B
09/09/14
Dibromofluoromethane
92.4
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
105.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 9 of 63
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-1
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 11:15
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-05
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
190000
Volatile Organics
Acetone
170
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
1.8
cis-1,2-Dichloroethene
2800
trans-1,2-Dichloroethene
9.2
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
10000 ug/l 9060A 09/12/14 10
50.
ug/l
8260B
09/09/14
1
50.
ug/1
8260B
09/09/14
1
10.
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
50.
ug/1
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
2.5
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
50.
ug/l
8260B
09/11/14
50
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
Page 10 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-1
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 11:15
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-05
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
250
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
12.
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/15/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
18.
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
41.
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.7
% Rec.
8260B
09/09/14
Dibromofluoromethane
97.0
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
100.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 11 of 63
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-6
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 10:35
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-06
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
2100
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
1.0
cis-1,2-Dichloroethene
1200
trans-1,2-Dichloroethene
3.2
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14 1
50.
ug/l
8260B
09/09/14
1
50.
ug/1
8260B
09/09/14
1
10.
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
50.
ug/1
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
2.5
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
50.
ug/l
8260B
09/11/14
50
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
Page 12 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-6
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 10:35
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-06
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
2400
50.
ug/1
8260B
09/11/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
95.
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
5.5
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
97.5
% Rec.
8260B
09/09/14
Dibromofluoromethane
87.1
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
112.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 13 of 63
1
1
1
1
1
1
1
1
1
1
1
1
50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-44
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 10:13
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-07
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
1.2
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
870
trans-1,2-Dichloroethene
6.7
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14 1
50.
ug/l
8260B
09/09/14
1
50.
ug/1
8260B
09/09/14
1
10.
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
50.
ug/1
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
2.5
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
100
ug/l
8260B
09/11/14
100
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
Page 14 of 63

12065
Lebanon Rd.
Mt. Juliet,
TN 37122
(615)
758-5858
1-800-767-5859
Fax (615)
758-5859
Tax I.D.
62-0814289
Est.
1970
REPORT
OF ANALYSIS
Mr. Andy Alexander
September
16,2014
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC
Sample #
L720290-07
Date Received September 06, 2014
Description Andrex Industries
Site
ID
ASHEVILLE, NC
Sample ID MW-44
Project
#
J14-1022-40
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 10:13
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
1
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
1
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
1
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
1
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
1
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
1
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1
1,1,1,2-Tetrachloroethane
1.3
1.0
ug/l
8260B
09/09/14
1
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
1
Tetrachloroethene
4300
100
ug/1
8260B
09/11/14
100
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
1
Trichloroethene
230
100
ug/1
8260B
09/11/14
100
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1
Vinyl chloride
36.
1.0
ug/1
8260B
09/09/14
1
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
1
Surrogate Recovery
Toluene-d8
97.4
% Rec.
8260B
09/09/14
1
Dibromofluoromethane
98.4
% Rec.
8260B
09/09/14
1
4-Bromofluorobenzene
118.
% Rec.
8260B
09/09/14
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 15 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-7
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 09:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-08
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/11/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 16 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-7
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 09:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-08
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
110
1.0
ug/1
8260B
09/11/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/11/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.1
% Rec.
8260B
09/09/14
Dibromofluoromethane
96.8
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
101.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 17 of 63
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-9
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 13:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-09
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
660
trans-1,2-Dichloroethene
3.0
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14 1
50.
ug/l
8260B
09/09/14
1
50.
ug/1
8260B
09/09/14
1
10.
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
50.
ug/1
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
2.5
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
5.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
50.
ug/l
8260B
09/11/14
50
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
1.0
ug/l
8260B
09/09/14
1
1.0
ug/1
8260B
09/09/14
1
Page 18 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-9
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 13:30
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-09
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
2100
50.
ug/1
8260B
09/11/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
140
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
16.
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
96.5
% Rec.
8260B
09/09/14
Dibromofluoromethane
97.7
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
109.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 19 of 63
1
1
1
1
1
1
1
1
1
1
1
1
50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-5
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 15:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-10
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
16000
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/15/14
50.
ug/1
8260B
09/15/14
10.
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
5.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
5.0
ug/1
8260B
09/15/14
50.
ug/1
8260B
09/15/14
5.0
ug/1
8260B
09/15/14
2.5
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
5.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
5.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/16/14
1.0
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
1.0
ug/l
8260B
09/15/14
1.0
ug/1
8260B
09/15/14
Page 20 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-5
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 15:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-10
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/15/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/15/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/15/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/15/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/15/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/15/14
Naphthalene
BDL
5.0
ug/1
8260B
09/15/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/15/14
Styrene
BDL
1.0
ug/1
8260B
09/15/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/15/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/15/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/15/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/15/14
Toluene
1500
50.
ug/1
8260B
09/11/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/15/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/15/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/15/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/15/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/15/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/15/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/15/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/15/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/15/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/15/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/15/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/15/14
Surrogate Recovery
Toluene-d8
103.
% Rec.
8260B
09/15/14
Dibromofluoromethane
97.7
% Rec.
8260B
09/15/14
4-Bromofluorobenzene
102.
% Rec.
8260B
09/15/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:28
Page 21 of 63
1
1
1
1
1
1
1
1
1
1
1
1
1
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-10
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 14:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-11
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
110
trans-1,2-Dichloroethene
1.0
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 22 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-10
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 14:30
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-11
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
360
5.0
ug/1
8260B
09/11/14
Toluene
BDL
5.0
ug/1
8260B
09/15/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
32.
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
35.
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
98.2
% Rec.
8260B
09/09/14
Dibromofluoromethane
96.1
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
100.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 23 of 63
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-13
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 14:15
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-12
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
170
trans-1,2-Dichloroethene
6.8
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 24 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-13
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 14:15
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-12
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
1300
50.
ug/1
8260B
09/11/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
160
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
97.1
% Rec.
8260B
09/09/14
Dibromofluoromethane
96.1
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
105.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 25 of 63
1
1
1
1
1
1
1
1
1
1
1
1
50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-14
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 16:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-13
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
1.0
cis-1,2-Dichloroethene
140
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 26 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-14
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 16:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-13
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
790
20.
ug/1
8260B
09/11/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
350
20.
ug/1
8260B
09/11/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
95.2
% Rec.
8260B
09/09/14
Dibromofluoromethane
93.1
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
105.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 27 of 63
1
1
1
1
1
1
1
1
1
1
1
1
20
1
1
1
1
1
20
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-6
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 15:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-14
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
1000
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
2.0
cis-1,2-Dichloroethene
540
trans-1,2-Dichloroethene
4.1
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14 1
50.
ug/l
8260B
09/09/14 1
50.
ug/1
8260B
09/09/14 1
10.
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
5.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
5.0
ug/1
8260B
09/09/14 1
50.
ug/1
8260B
09/09/14 1
5.0
ug/1
8260B
09/09/14 1
2.5
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
5.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
5.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
10.
ug/l
8260B
09/11/14 10
1.0
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
1.0
ug/l
8260B
09/09/14 1
1.0
ug/1
8260B
09/09/14 1
Page 28 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-6
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 15:30
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-14
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
36.
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
30.
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
120
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
98.1
% Rec.
8260B
09/09/14
Dibromofluoromethane
90.0
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
100.
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 29 of 63
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-7
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 14:55
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-15
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
730000
Volatile Organics
Acetone
87.
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
620
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
100000
ug/l
9060A
09/12/14
100
50.
ug/l
8260B
09/15/14
1
50.
ug/1
8260B
09/15/14
1
10.
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
5.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
5.0
ug/1
8260B
09/15/14
1
50.
ug/1
8260B
09/15/14
1
5.0
ug/1
8260B
09/15/14
1
2.5
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
5.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
5.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
10.
ug/l
8260B
09/10/14
10
1.0
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
1.0
ug/l
8260B
09/15/14
1
1.0
ug/1
8260B
09/15/14
1
Page 30 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID RW-7
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 14:55
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-15
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/15/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/15/14
2-Butanone (MEK)
21.
10.
ug/l
8260B
09/15/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/15/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/15/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/15/14
Naphthalene
BDL
5.0
ug/1
8260B
09/15/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/15/14
Styrene
BDL
1.0
ug/1
8260B
09/15/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/15/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/15/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/15/14
Tetrachloroethene
33.
1.0
ug/1
8260B
09/15/14
Toluene
BDL
5.0
ug/1
8260B
09/15/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/15/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/15/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/15/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/15/14
Trichloroethene
36.
1.0
ug/1
8260B
09/15/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/15/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/15/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/15/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/15/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/15/14
Vinyl chloride
8.7
1.0
ug/1
8260B
09/15/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/15/14
Surrogate Recovery
Toluene-d8
98.0
% Rec.
8260B
09/15/14
Dibromofluoromethane
95.2
% Rec.
8260B
09/15/14
4-Bromofluorobenzene
106.
% Rec.
8260B
09/15/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 31 of 63
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-11
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 14:29
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-16
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
260
trans-1,2-Dichloroethene
1.3
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14 1
50.
ug/l
8260B
09/10/14
1
50.
ug/1
8260B
09/10/14
1
10.
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
50.
ug/1
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
2.5
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
5.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
25.
ug/l
8260B
09/11/14
25
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
1.0
ug/l
8260B
09/10/14
1
1.0
ug/1
8260B
09/10/14
1
Page 32 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-11
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 14:29
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-16
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/10/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/10/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/10/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/10/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/10/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/10/14
Naphthalene
BDL
5.0
ug/1
8260B
09/10/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/10/14
Styrene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/10/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/10/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/10/14
Tetrachloroethene
860
25.
ug/1
8260B
09/11/14
Toluene
BDL
5.0
ug/1
8260B
09/10/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/10/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/10/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/10/14
Trichloroethene
55.
1.0
ug/1
8260B
09/10/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/10/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/10/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/10/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
Vinyl chloride
9.9
1.0
ug/1
8260B
09/10/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/10/14
Surrogate Recovery
Toluene-d8
100.
% Rec.
8260B
09/10/14
Dibromofluoromethane
104.
% Rec.
8260B
09/10/14
4-Bromofluorobenzene
89.6
% Rec.
8260B
09/10/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 33 of 63
1
1
1
1
1
1
1
1
1
1
1
1
25
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-23
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 11:20
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-17
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
9.3
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/10/14
50.
ug/1
8260B
09/10/14
10.
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
50.
ug/1
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
2.5
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
Page 34 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-23
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 11:20
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-17
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/10/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/10/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/10/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/10/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/10/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/10/14
Naphthalene
BDL
5.0
ug/1
8260B
09/10/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/10/14
Styrene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/10/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/10/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/10/14
Tetrachloroethene
110
1.0
ug/1
8260B
09/10/14
Toluene
BDL
5.0
ug/1
8260B
09/10/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/10/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/10/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/10/14
Trichloroethene
4.2
1.0
ug/1
8260B
09/10/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/10/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/10/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/10/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/10/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/10/14
Surrogate Recovery
Toluene-d8
102.
% Rec.
8260B
09/10/14
Dibromofluoromethane
106.
% Rec.
8260B
09/10/14
4-Bromofluorobenzene
92.2
% Rec.
8260B
09/10/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 35 of 63
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-24
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 10:29
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-18
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
4.4
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/10/14
50.
ug/1
8260B
09/10/14
10.
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
50.
ug/1
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
2.5
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
Page 36 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-24
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 10:29
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-18
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/10/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/10/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/10/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/10/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/10/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/10/14
Naphthalene
BDL
5.0
ug/1
8260B
09/10/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/10/14
Styrene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/10/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/10/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/10/14
Tetrachloroethene
270
10.
ug/1
8260B
09/11/14
Toluene
BDL
5.0
ug/1
8260B
09/10/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/10/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/10/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/10/14
Trichloroethene
2.0
1.0
ug/1
8260B
09/10/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/10/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/10/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/10/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/10/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/10/14
Surrogate Recovery
Toluene-d8
101.
% Rec.
8260B
09/10/14
Dibromofluoromethane
103.
% Rec.
8260B
09/10/14
4-Bromofluorobenzene
90.3
% Rec.
8260B
09/10/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 37 of 63
1
1
1
1
1
1
1
1
1
1
1
1
10
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-15
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 12:05
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-19
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
4.2
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/10/14
50.
ug/l
8260B
09/10/14
10.
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
50.
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
2.5
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
5.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
Page 38 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-15
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 12:05
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-19
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/10/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/10/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/10/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/10/14
Naphthalene
BDL
5.0
ug/1
8260B
09/10/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/10/14
Styrene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/10/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/10/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/10/14
Tetrachloroethene
82.
1.0
ug/1
8260B
09/10/14
Toluene
BDL
5.0
ug/l
8260B
09/10/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/10/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/10/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/10/14
Trichloroethene
2.3
1.0
ug/l
8260B
09/10/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/10/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/10/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/10/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/10/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/10/14
Surrogate Recovery
Toluene-d8
102.
o Rec.
8260B
09/10/14
Dibromofluoromethane
103.
o Rec.
8260B
09/10/14
4-Bromofluorobenzene
90.8
o Rec.
8260B
09/10/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 39 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-16
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 12:20
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-20
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
6.0
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/10/14
50.
ug/l
8260B
09/10/14
10.
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
50.
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
2.5
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
5.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
5.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
1.0
ug/l
8260B
09/10/14
1.0
ug/1
8260B
09/10/14
Page 40 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-16
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 12:20
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-20
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/10/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/10/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/10/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/10/14
Naphthalene
BDL
5.0
ug/1
8260B
09/10/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/10/14
Styrene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/10/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/10/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/10/14
Tetrachloroethene
130
1.0
ug/1
8260B
09/10/14
Toluene
BDL
5.0
ug/l
8260B
09/10/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/10/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/10/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/10/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/10/14
Trichloroethene
3.3
1.0
ug/l
8260B
09/10/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/10/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/10/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/10/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/10/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/10/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/10/14
Surrogate Recovery
Toluene-d8
100.
o Rec.
8260B
09/10/14
Dibromofluoromethane
103.
o Rec.
8260B
09/10/14
4-Bromofluorobenzene
94.3
o Rec.
8260B
09/10/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 41 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-17
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 10:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-21
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
8.8
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 42 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-17
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 10:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-21
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
5.5
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
2.9
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
4.1
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
97.5
o Rec.
8260B
09/09/14
Dibromofluoromethane
97.1
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
99.9
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 43 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-18
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 13:15
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-22
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 44 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-18
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 13:15
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-22
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
97.3
o Rec.
8260B
09/09/14
Dibromofluoromethane
106.
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
94.9
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 45 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-20
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 09:50
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-23
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 46 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-20
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 09:50
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-23
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.5
o Rec.
8260B
09/09/14
Dibromofluoromethane
101.
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
98.7
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 47 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-21
Collected By Benjamin P. Nisbeth
Collection Date 09/02/14 15:50
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-24
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 48 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-21
Collected By Benjamin P. Nisbeth
Collection Date 09/02/14 15:50
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-24
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
100.
o Rec.
8260B
09/09/14
Dibromofluoromethane
95.5
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
95.1
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 49 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-22
Collected By Benjamin P. Nisbeth
Collection Date 09/02/14 14:55
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-25
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 50 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-22
Collected By Benjamin P. Nisbeth
Collection Date 09/02/14 14:55
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-25
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.3
o Rec.
8260B
09/09/14
Dibromofluoromethane
115.
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
99.2
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 51 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-26
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 09:20
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-26
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 52 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID MW-26
Collected By Benjamin P. Nisbeth
Collection Date 09/03/14 09:20
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-26
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.2
o Rec.
8260B
09/09/14
Dibromofluoromethane
94.3
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
95.3
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 53 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID FIELD BLANK
Collected By Benjamin P. Nisbeth
Collection Date 09/02/14 15:15
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-27
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 54 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID FIELD BLANK
Collected By Benjamin P. Nisbeth
Collection Date 09/02/14 15:15
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-27
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.0
o Rec.
8260B
09/09/14
Dibromofluoromethane
104.
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
94.9
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 55 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID FIELD BLANK
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-28
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 56 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID FIELD BLANK
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-28
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
98.8
o Rec.
8260B
09/09/14
Dibromofluoromethane
96.1
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
96.3
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 57 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID DUPLICATE
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 00:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-29
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
130
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 58 of 63

12065
Lebanon Rd.
Mt. Juliet,
TN 37122
(615)
758-5858
1-800-767-5859
Fax (615)
758-5859
Tax I.D.
62-0814289
Est.
1970
REPORT
OF ANALYSIS
Mr. Andy Alexander
September
16,2014
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC
Sample #
L720290-29
Date Received September 06, 2014
Description Andrex Industries
Site
ID
ASHEVILLE, NC
Sample ID DUPLICATE
Project
#
J14-1022-40
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 00:00
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
1
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
1
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
1
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
1
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
1
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
1
Tetrachloroethene
1000
20.
ug/1
8260B
09/12/14
20
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
1
Trichloroethene
400
20.
ug/l
8260B
09/12/14
20
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
1
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
1
Surrogate Recovery
Toluene-d8
96.6
o Rec.
8260B
09/09/14
1
Dibromofluoromethane
96.0
o Rec.
8260B
09/09/14
1
4-Bromofluorobenzene
104.
o Rec.
8260B
09/09/14
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 59 of 63

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID TRIP BLANK
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 00:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-30
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 60 of 63

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID TRIP BLANK
Collected By Benjamin P. Nisbeth
Collection Date 09/04/14 00:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 16,2014
ESC Sample # : L720290-30
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/l
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/09/14
Surrogate Recovery
Toluene-d8
98.3
o Rec.
8260B
09/09/14
Dibromofluoromethane
94.7
o Rec.
8260B
09/09/14
4-Bromofluorobenzene
98.6
o Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 16:53 Revised: 09/16/14 14:29
Page 61 of 63

Attachment A
List of Analytes with QC Qualifiers
Sample
Work
Sample
Run
Number
Group
Type
Analyte
ID
Qualifier
L720290-01
WG741510
SAMP
2-Chloroethyl vinyl ether
R2987334
J6J3
L720290-10
WG742349
SAMP
Toluene
R2988398
V
L720290-21
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-22
WG741511
SAMP
2-Chloroethyl vinyl ether
R2987892
J6J3
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-23
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-24
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-25
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-26
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-27
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-28
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-29
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720290-30
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
Page 62 of 63

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J3 The associated batch QC was outside the established quality control range
for precision.
J4 The associated batch QC was outside the established quality control range
for accuracy.
J6 The sample matrix interfered with the ability to make any accurate
determination; spike value is low
V (ESC) - Additional QC Info: The sample concentration is too high to
evaluate accurate spike recoveries.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 63 of 63

willing lnmrrnaimn: Analysis fCo ntainer } Pre9erwative Chain of Custody pose —L of
Bunnell - Lammolns Engineering, Inc. Project Manager
6004 Ponders Court
6004 Panders Court Greenville, SC 29615 :OESC
Greenville, SC29515 L-k-o s c- I-£-N-c-e-$
] 2UdS Ll6al-1oR Ikd
ReDort t,3. EmailTo! pndyblaorlp.rortr O
AiouM Mist, TN �7] 22
Mr- Andy Alexander alh�:
PFmrre: b06767s859
pro)act City{SWtie a�}_ Fu:6i9.xse-sera q
E7ascripticn Andrex Industries Collected; [%] L
Client Prpjpt Lab Project p
FaL #
one:864-2881 J14-1022-40 9UNLAM65C414102240 u "—
Fax! 864-ASS-4430 Fi206
fa �
C411ertedby{print]' SlteJf26litylDiF P.O.# C T Acrtnum BIJNLAItijICiSC
i45HEVILLE, NCGn
Templake:T9fi49
I
Collected by (signature ' Rush? ?Lab. MUST Be Notified date Results Needed 0
- Pre login; P480308
Same Dory,,,,,,,,,,,,,,,,,,,,,,,,,,,ZOC% I Q
Emall7 No X Yes E I TSR:35 Jimmy urst
J el'dia _Twflext0Day ............................:.M
Packed on lee N Y- I/ _ Three DaY ,-,-, .............25% FAX? No Yes H o' Ln O p PB: �
of
u N r%y Shipped Via-F dEX Ground
Sam pie ID Comp/Grab Matfix• Depth Date Time ntrs 0 N M
> &x P3r k{Iab only)
MW-5 6 GW Of Iloco 3 X X — �
MW-I +raLo GW ' D+- l r 3 X X — 03
I-2 av G, Gw C}'- 3 3 X X — L)q
RW-1 c L GW 111 3 X X
MW-G r W 103 3 X X r. ¢
MW-44 L, G W 1013 3 X X
MW-T s.:�, G W 100 3 X X -off
MW-9 (av�. GW D+. 1 3 3 X X
RW-5 G W X X
61 r"4 11-o4-14 15bo
Matrix; SS - Soll Gw - Groundwater Vim - wasteWater dW - DFla,king Water OT - other _
CIRafICS: ph Temp —..
Flow _ Other
Holdl!
Relinquished by; (Si nature) DM-, Time: Received by: {5iBn4!ure) Sa2dE
eturnedyia; 0 UPS Condition- ( at) use only)
�J ex ❑ Courier ❑
e Inquished by : (Signatures Oats- Time-, Received bY: (Signature) Ternp- 'C Bottles Rerelved-
COC Seal Intact: �Y iN NA
Ftellnqulshedby. Cate; Time: ReCe�vedfor Iabby; (5ignature) Date; Time: pH Check NCF;
a - o f--6 44-

Billing information-
Bunnell - Lalmmons Engineering, Inc.
Project Manager
6004 Panders Court
6004 Ponders Court
Greenville, SC 29615
Greenville, SC 29615
BeADrt to: Emdil To: [e-mail]
Mr. Andy Alexander '4
Projem Clky}5ta[e y�y{r�57 i�
Description. And rex Industries Collected: 11 j ,{ A ram+
Phone: [phone] Client Project # Lab Project p
Fax: 864-2I;&4430 J14-1022-40 BUNLAMGSC-J14102240 U
Collected
by (Print): Site/Facility ID R P-0, {!
�N -1;A 45 ASHEVILLE. INC Oar
in I
Collected by [sig �� Rush? (LabAUST Be Notified] E
�'Dare Results N-eeded
Newt Rav ,,. ,-,.,_.-.-.- tCQ% €mai 12 No �C_Yes
ediateiy Two oay......................._.....50% Na. O
Packed on toe N Y Threr ae FAX? No Y Ln
Y ..... .................._25i6 — es r
of N �
U �
"�mRie IQ Camp/Grab hAatrlrl • Depth date time �rltrs 0
f--1
jMW-16 w" GW 9 • • t+ )430 3 X
M -13 GcmGW D3-1# I 3 k'
MW-14 6ml6GW 1.03 I { c)o 3
RW-6 r GWIf 10 3 X x
RW-7 rs� GW I ' 3
MW-11 GW 1f 11111 3 X x
M -23 {,s GW 03 • (4- 1 Zp 3 X X
NSW-24 a GW 9.03-4 Iml 3 X x
MW-16 ja GW 1 1.03 • t Lo) 2 X
M-16 ? G1N
Matrix: SS - 5uil GW • Groundwater U1 w - wastewater OW • Drinking Wat#r Qt- Uther — -
trainer (Preservative
Chain pf Custody Page '
OESC
k
22ass I ebaron Rd Q �j
Mmn9 iullet.TN 37122 Lf
Phan*:615-75&-s656
Phan*. 80o-767-Ses9
Pax! 5lis-M-5s59
LFr L_7 o -�o
Table #
Acctnum. 6UNL4MGSC
Template:T96493
PrOogin! P480308
TER' 351)Ilmmy punt
pla - q 16J &)It (L - ml�'J
Via:
R*en.KmLVnlnanl
iampla A fob ony]
_c3.
�q
.;" "" ^''
pH
Temp
HOW
OLher
RefinglFished by-{5i�n *2}
Dice/{;y�
Time-
xed by (Sgnature)
5arnp�l s returned,+la; ❑ URS
Fte IfWulshed by; ($ignaturej
Date-
Time;
Pd by: j5ignaturej
Temp: ..
eC Bottles R.re,"cr;
fR4�mailrvy,'.d
tf+
�.
Relinquished by. rel
Date:
Time:
forlabby:jSignature)
Date;
Time:
Haid #
Conditipn. {leh use only]
COC Seat intact: _ Y N t N.A
pH Chet NCF-

BilLft tnformatlon_
Bunnell - Lam mons Engineering, Inc. project manager
6004 Ponders Court
6004 Ponders Court Greenville. 5C 29615
Greenville, SC. 29615
R,�p"rt ko-
Mlr. Andy Alexander
Project
Description: Andrex Industries
P hone. 864-288-1265
Fax: [phone]
Gvlllllectk by WirQ::
D
Collected by Wgnatur
immediately
Packed an toe
Sample to
anopbleaarpxom
Client Project #
114-1022-40
5i1eyFacilikq tD it
ASHE ILLE, NC
R,Sh? (Lab MUST" Notifledi
—
me Daw ............. .......... -10Y4
.... NeN DW ............. .......I lb%
—Two Day ,,,,,,,,,,,,,,,,,,,,,,,,,,--Scs
Three Day ....... .....................
Comip{Grab Matrix* Depth
GW
M -17
*410
MW-18
G
�
MW-20
fk-
G
M11'11-21
G
MW-22
GW
MW-26
[ �,�
GIN
FIELD BLANK
FIELD BLANK
[v7
GV
DUPLICATE
, j
GW
ITRIP BLANK
GW
Matrix; SS Sall Gw - Groundwater WW - Wastewater uw - ur
Relinquished bY', , t pate;
Re n uished by . i5lgnature� Date:
cotat2
llecB IB
r_ouected:
Lab Project a
BUfI LAmi G$C-1141kG2240
P.4,#
Email? —NO Yes
FAX? `NO _Yes
Date iim�
°( -03 M¢
L
dime:
pate; Time.
by ; l5ignaturei
I
13105
fro
r�vkoo
No
2
2
N
v
X
x
x
x
Container I Pres2rWative
[TalnaFCustody Page'7at-.?--
*ESC
L-4 a 3'G-1',L-N-'--'E-S
] 7Cd5 LebAnon Rd Q
MOW Juliet. TN 37122
ph.:615-75e-595a
khonr.S6O-M 5959
Fa... 515-75a-56S9
?table #
Amn"L 6UNLANIGSC
Temptate:T96493
PrelDgin; MOM
TSR: 3SG1f-Jlmmy-Hunt
5hlppeld vFa_ F dE Ground
pem.jccr.14.winari Sample x i'3 a on77
t S
Z�
Y
�1
pH temp— _.
Flow
Hold #
le[eived by: (Stgndture) Samp returned via; ❑ l}PS
Condition, (I ab use only]
fedEx ❑ COUrier 13-
deceived hY� (Sigr78tur2) T R' T Battles Recelved_ 17
x4 c COC Seal Intact; _Y ___N _NA
F:
nature) Date' V Time- pH Checked: NC
ReCe'rred for lab by: (5�6 .,

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Friday September 12, 2014
Report Number: L720293
Samples Received: 09/06/14
Client Project: J14-1022-40
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
Jimmy Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 33

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 1
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 11:20
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-01
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
1100
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 2 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 1
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 11:20
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-01
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
9.3
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/12/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/12/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.1
% Rec.
8260B
09/09/14
Dibromofluoromethane
102.
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
97.5
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 3 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 2
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 11:10
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-02
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
1100
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 4 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 2
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 11:10
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-02
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
6.9
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/12/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
97.8
% Rec.
8260B
09/09/14
Dibromofluoromethane
92.8
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
97.3
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 5 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 3
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 11:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-03
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
1100
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 6 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 3
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 11:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-03
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
7.6
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
98.2
% Rec.
8260B
09/09/14
Dibromofluoromethane
102.
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
93.5
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 7 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 4
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:50
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-04
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 8 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 4
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:50
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-04
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
6.0
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
1.4
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.1
% Rec.
8260B
09/09/14
Dibromofluoromethane
104.
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
94.3
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 9 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 5
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:40
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-05
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
1000
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 10 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 5
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:40
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-05
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
4.8
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
1.0
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
96.5
% Rec.
8260B
09/09/14
Dibromofluoromethane
92.2
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
96.8
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 11 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 6
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-06
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
1100
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 12 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID SMITH MILL CREEK 6
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:30
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-06
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
4.2
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
98.7
% Rec.
8260B
09/09/14
Dibromofluoromethane
93.0
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
95.1
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 13 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 1
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:45
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-07
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
5.1
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 14 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 1
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:45
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-07
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
12.
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
1.6
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.5
% Rec.
8260B
09/09/14
Dibromofluoromethane
98.6
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
98.1
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 15 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 2
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:35
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-08
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
4.2
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 16 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 2
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:35
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-08
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
11.
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
1.9
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
100.
% Rec.
8260B
09/09/14
Dibromofluoromethane
100.
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
96.2
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 17 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 3
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:25
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-09
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
2.0
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 18 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 3
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:25
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-09
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
3.3
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
96.6
% Rec.
8260B
09/09/14
Dibromofluoromethane
104.
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
96.8
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 19 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 4
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:15
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-10
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/09/14
50.
ug/1
8260B
09/09/14
10.
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
50.
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
2.5
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
5.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
1.0
ug/l
8260B
09/09/14
1.0
ug/1
8260B
09/09/14
Page 20 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 4
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:15
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-10
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/09/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/09/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/09/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/09/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/09/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/09/14
Naphthalene
BDL
5.0
ug/1
8260B
09/09/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Styrene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/09/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/09/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/09/14
Toluene
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/09/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/09/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/09/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/09/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/09/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/09/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/09/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/09/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/09/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/09/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/09/14
Surrogate Recovery
Toluene-d8
99.1
% Rec.
8260B
09/09/14
Dibromofluoromethane
93.5
% Rec.
8260B
09/09/14
4-Bromofluorobenzene
98.0
% Rec.
8260B
09/09/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 21 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 5
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:05
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-11
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/08/14
50.
ug/l
8260B
09/08/14
10.
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
50.
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
2.5
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
5.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
Page 22 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID BEAR CREEK 5
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 09:05
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-11
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/08/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/08/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/08/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/08/14
Naphthalene
BDL
5.0
ug/1
8260B
09/08/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/08/14
Styrene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/08/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/08/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/08/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/12/14
Toluene
BDL
5.0
ug/l
8260B
09/08/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/08/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/08/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/08/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/08/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/08/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/08/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/08/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/08/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/08/14
Surrogate Recovery
Toluene-d8
101.
o Rec.
8260B
09/08/14
Dibromofluoromethane
113.
o Rec.
8260B
09/08/14
4-Bromofluorobenzene
93.1
o Rec.
8260B
09/08/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 23 of 33

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID JEHOVAH WITNESS 1
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 11:35
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-12
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/08/14
50.
ug/1
8260B
09/08/14
10.
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
50.
ug/1
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
2.5
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
Page 24 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID JEHOVAH WITNESS 1
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 11:35
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-12
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/08/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/08/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/08/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/08/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/08/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/08/14
Naphthalene
BDL
5.0
ug/1
8260B
09/08/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/08/14
Styrene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/08/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/08/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/08/14
Tetrachloroethene
4.4
1.0
ug/1
8260B
09/12/14
Toluene
BDL
5.0
ug/1
8260B
09/08/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/08/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/08/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/08/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/08/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/08/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/08/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/08/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/08/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/08/14
Surrogate Recovery
Toluene-d8
98.9
% Rec.
8260B
09/08/14
Dibromofluoromethane
103.
% Rec.
8260B
09/08/14
4-Bromofluorobenzene
97.8
% Rec.
8260B
09/08/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 25 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID CECIL'S SPRING 1
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:15
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-13
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
3000
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
2.6
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/08/14
50.
ug/1
8260B
09/08/14
10.
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
50.
ug/1
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
2.5
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
Page 26 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID CECIL'S SPRING 1
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:15
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-13
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/08/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/08/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/08/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/08/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/08/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/08/14
Naphthalene
BDL
5.0
ug/1
8260B
09/08/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/08/14
Styrene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/08/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/08/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/08/14
Tetrachloroethene
8.9
1.0
ug/1
8260B
09/12/14
Toluene
BDL
5.0
ug/1
8260B
09/08/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/08/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/08/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/08/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/08/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/08/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/08/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/08/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/08/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/08/14
Surrogate Recovery
Toluene-d8
98.0
% Rec.
8260B
09/08/14
Dibromofluoromethane
96.5
% Rec.
8260B
09/08/14
4-Bromofluorobenzene
96.9
% Rec.
8260B
09/08/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 27 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID CECIL'S SPRING 2
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:05
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-14
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
1300
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 09/12/14
50.
ug/l
8260B
09/08/14
50.
ug/1
8260B
09/08/14
10.
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
50.
ug/1
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
2.5
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
Page 28 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID CECIL'S SPRING 2
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 10:05
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-14
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
09/08/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
09/08/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/08/14
Methylene Chloride
BDL
5.0
ug/l
8260B
09/08/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
09/08/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/08/14
Naphthalene
BDL
5.0
ug/1
8260B
09/08/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
09/08/14
Styrene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
09/08/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/08/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/08/14
Tetrachloroethene
3.6
1.0
ug/1
8260B
09/12/14
Toluene
BDL
5.0
ug/1
8260B
09/08/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
09/08/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/08/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/08/14
Trichloroethene
BDL
1.0
ug/1
8260B
09/08/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/08/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
09/08/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/08/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
Vinyl chloride
BDL
1.0
ug/1
8260B
09/08/14
Xylenes, Total
BDL
3.0
ug/l
8260B
09/08/14
Surrogate Recovery
Toluene-d8
100.
% Rec.
8260B
09/08/14
Dibromofluoromethane
108.
% Rec.
8260B
09/08/14
4-Bromofluorobenzene
94.9
% Rec.
8260B
09/08/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 29 of 33
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID TRIP BLANK
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 00:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-15
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
09/08/14
50.
ug/l
8260B
09/08/14
10.
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
50.
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
2.5
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
5.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
5.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
1.0
ug/l
8260B
09/08/14
1.0
ug/1
8260B
09/08/14
Page 30 of 33

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received September 06, 2014
Description Andrex Industries
Sample ID TRIP BLANK
Collected By Benjamin P. Nisbeth
Collection Date 09/05/14 00:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
September 12,2014
ESC Sample # : L720293-15
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
09/08/14
Methylene Chloride
BDL
5.0
ug/1
8260B
09/08/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
09/08/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
09/08/14
Naphthalene
BDL
5.0
ug/1
8260B
09/08/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
09/08/14
Styrene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/08/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
09/08/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
09/08/14
Tetrachloroethene
BDL
1.0
ug/1
8260B
09/08/14
Toluene
BDL
5.0
ug/l
8260B
09/08/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/08/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
09/08/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
09/08/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
09/08/14
Trichloroethene
BDL
1.0
ug/l
8260B
09/08/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
09/08/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
09/08/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
09/08/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
09/08/14
Vinyl chloride
BDL
1.0
ug/l
8260B
09/08/14
Xylenes, Total
BDL
3.0
ug/1
8260B
09/08/14
Surrogate Recovery
Toluene-d8
99.7
o Rec.
8260B
09/08/14
Dibromofluoromethane
91.5
o Rec.
8260B
09/08/14
4-Bromofluorobenzene
95.7
o Rec.
8260B
09/08/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 09/12/14 17:39 Printed: 09/12/14 17:40
Page 31 of 33

Attachment A
List of Analytes with QC Qualifiers
Sample
Work
Sample
Run
Number
Group
Type
Analyte
ID
Qualifier
L720293-01
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-02
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-03
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-04
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-05
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-06
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-07
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-08
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-09
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
L720293-10
WG741511
SAMP
1,1,1-Trichloroethane
R2987892
J4
WG741511
SAMP
1,2,3-Trichloropropane
R2987892
J4
Page 32 of 33

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J4 The associated batch QC was outside the established quality control range
for accuracy.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 33 of 33

9illirg Infor•natian:
Analysis
f
Container
% Preservative
Ch*In-ofCuavdy Pace J-of
Bunnell - Lammons Engineering, Inc.
Project Manager
6004 Panders Court
OESC
6004 Panders Court
Greenville, SC 29615
Greenvill Ie,SC29615
L-"-B 5-C•I-E-#Q-- `.-F-5
I12C65ttb4r
11Rd
Mfluns 1 37112
Report to:
ErnailTo:andy@blerarp.€om
Mr.AndyAlexander
'Y
615-7515c8.SA5R
rr�nt: A4476�5859
F., 615-759-5959
PrOACt
_
Citymate
Collected: 4'm'
Description; Andrex Industries
p 77 1 3
FL
CIien1 Proiett P
La# Project
Phonr;864- 88-1 65
Fax: 864-288-A 3
J14-1OZZ-40
BUNLAMGSC-J14102240
U
I
H2O5
ra
=
m
=
J
Acttnum: BUNLAMGSC
Collected by (print):
�+
Site}Fa€il1ty ID A
ASHEVILLE, NC
P.O. 9
i_ ►+s�
is
Ed
E
E
Template!T965il
prelogin: P480314
Col lected tpy (signature
Alt#✓'1 (La bl�ll►5T9eN4tified}
date Results Needed
swc Day .......... 203%
RemOaY .............................li 4
1_
im
TSR= 3 D -1✓ m my Bunt
Email? Na ]i Yes
mmediat1Iy
Packed on Ice N — Y _
_ Two Oay ,,,,, ,,,,,,,,,,,,,,,,,,, ,,,SOK
_ Thfcr Day - ...........................25%
FAX? _No _Yes
f
in
fN in
U
i o
iN
w
o
fN
go
p�' .
5hippe is,F$ EX Ground
Sample ID
Comp/Grab
Matrix
Depth
Date
Time
ntrS
}
h—jCnrdx -nant sample R (lab �hrl
SMITH MILL CREEK 1
r. r
GW
p
��
a
X
X
—
SMITH MILLCREEK 2
�
GW
`p
� tic)
3
X
X
02
SMITH MILL CREEK 3
ex 6
Gw
05' (f
100
3
X
X
— 0
SMITH MILL CREEK 4
GW
_p
3
X
X
o`{
SMITH MILL CREEK 5
"6
G*
`fi 0541'
I
3
X
X
SMITH MILL CREEK 6
&ro;.
GW
1-C -W
11W0
3
X
X
6
BEAR CREEK 1
GW
61 -05, jf
q
3
X
X
t D-)
BEAR CREEK 2
GW?
-(
'i
3
X
X
e
BEAR CREEK 3 GW 3 X X o Q
BEAR CREEK 4 Gw 0•( 3 X X I I
hAatrlx: SS- Sail GW - Groundwater WW - YJasteWater OW - Drinkln Water OT - ORher
�rJ l pH TemP
Remarks, � C' - Sc�4t�I1eS
..r I L J�
5'1'� 1 C �1t { {,J� I - 50 t}J Flour other - _ Hold 9
Relirtgwshed by: (Sigri atuptl
Date:
Tlrne;
ReceInmd by; (54, oelr
Sam.-,pp�Fes returned vla; ❑ UPS
Conditioa! Ilab use only)
� •
�
L� FedEK � CouKier ❑
C-
q (Sign ature�
pate:
Time:
Received by. (SignaWFL.
Temp; eC 6ottles Received:
CDC Seal Intact: �'/Y —N NA
Relinquished by : f5ignaLurc
ate:
Time:
Received far lab by: (5'gna.ure)
TlFne;
pH Che€ked:
NCF:
'_ZZ
/Date=

ySunnell - Lamlmons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report to:
Mr. Andy Alexander
Project
Description- Andrex Industrie9
Phone! $64-288-1265
Fax- 864-288-4410
Collected by (print]!
Collerte�dbyIsign atu }_
limeTtely
Packed an Ice N Y
Sample ID
BEAR CREEK 5
JEHOVAH WITNESS 1
CECIL'S SPRING 1
CEC112S SPRING 2
TRIP BLANK
BilFrlg In'or n7t r.n.
Project Manager
6004 Ponders Court
Greenville, 5C 29615
cmailTa:
Client Project N
114-1022-40
Site/Facility ID #
ASHEVIL.LE, NC
Rush? (lab MUST Be Natlfmd)
Sarno W y------- .:......... —.200%
Next day ............... .......... -.100%
Two l)&V......................::.:.:..50%
mrw Uaw----------- :.:.:.:........... 25%
Comp{Crrab Matrix • depth
GW
! G
G
rw G W
GW
;pm
CO/State f
falllleeked: A4vo l/
L,b Project a
BUNLAIVIGSC4141102240
Date Results Needed
Email?
—No X_Ves
FAX? !No
_Yes
date
lime
q
i 0
C
rod
-0j-
i - 05.
bo)5
14
Jr
4
a
E
u-I
fN
=
_
N o .
U
�
rq
7yy
rw
}
A
3
X
X
3
3
X
X
X
Preservative I'ha1n of [U5" Page',or
OESC
I
Ib965teb• bnRd
WLwrL1LAm,TN37L22 '
�h= 615-759-5M
►hie: 09-767-5659
FAx:[phone]A59
A � 7 204Zq3
Table 0
A€itnum: BUNLAMGSC
1
TemInlate;T96511
Prelagin. P480314
T5kq; M- lmmy P unt.,
FIR;
Shipped Via: F dEX Ground
K. m +Cogkam lank Sample P Ilab a":
rrf
_IL
�l
Matrix! SS - Soil SW - Groundwater WW - WastaWater DW - OrFnking Water GT - Other
Q
Remarks-
� 1.kO N
p
emp
W
Floor
Other
Hold #
Relinquished by ; (Si atu
lake-
Time:
Received by' (Sipiw re)
$iimple$ returned via! ❑ UPS
Cond;tior.
+Iah use only)
130
L7FedEx
[]Courier ❑_.-_
li is>tied bye: 3$ignature]
Date:
Time:
Received by: (Signature)
Temp:
'C Battles Received:
4
c
},
COC Seal Intact; _
__�YY _N _NA
Relrn,Quished by: (Slgrr3kurt ti
Date:
Time!
Received for lab by; (Signature)
Date:
Time:
pHIChetk &
NCF:
r
��
'r--
a.

APPENDIX G
LABORATORY ANALYTICAL DATA SHEETS
GROUNDWATER
NOVEMBER 2014 [150 Day]
(Provided on Enclosed CD)

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Report Summary
Thursday December 04, 2014
Report Number: L734762
Samples Received: 11/20/14
Client Project: J14-1022-40
Description: Andrex Industries
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
Jimmy Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 11

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received November 20, 2014
Description Andrex Industries
Sample ID IW-2
Collected By Benjamin P. Nisbeth
Collection Date 11/18/14 12:15
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 04,2014
ESC Sample # : L734762-01
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
4400000
Volatile Organics
Acetone
170
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
180
trans-1,2-Dichloroethene
1.1
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
100000 ug/l 9060A
11/26/14 100
50.
ug/l
8260B
11/26/14
50.
ug/1
8260B
11/26/14
10.
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
5.0
ug/1
8260B
11/28/14
1.0
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
5.0
ug/1
8260B
11/26/14
50.
ug/1
8260B
11/26/14
5.0
ug/1
8260B
11/26/14
2.5
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
5.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
5.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
1.0
ug/l
8260B
11/26/14
1.0
ug/1
8260B
11/26/14
Page 2 of 11

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received November 20, 2014
Description Andrex Industries
Sample ID IW-2
Collected By Benjamin P. Nisbeth
Collection Date 11/18/14 12:15
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 04,2014
ESC Sample # : L734762-01
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
11/26/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
11/26/14
2-Butanone (MEK)
310
10.
ug/l
8260B
11/26/14
Methylene Chloride
BDL
5.0
ug/l
8260B
11/26/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
11/26/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
11/26/14
Naphthalene
BDL
5.0
ug/1
8260B
11/26/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
11/26/14
Styrene
BDL
1.0
ug/1
8260B
11/26/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
11/26/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
11/26/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
11/26/14
Tetrachloroethene
10.
1.0
ug/1
8260B
11/26/14
Toluene
8.6
5.0
ug/1
8260B
11/26/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
11/26/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
11/26/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
11/26/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
11/26/14
Trichloroethene
2.5
1.0
ug/1
8260B
11/26/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
11/26/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
11/26/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
11/26/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
11/26/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
11/26/14
Vinyl chloride
2.9
1.0
ug/1
8260B
11/26/14
Xylenes, Total
BDL
3.0
ug/l
8260B
11/26/14
Surrogate Recovery
Toluene-d8
102.
% Rec.
8260B
11/26/14
Dibromofluoromethane
91.4
% Rec.
8260B
11/26/14
4-Bromofluorobenzene
108.
% Rec.
8260B
11/26/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 12/01/14 19:30 Revised: 12/04/14 08:51
Page 3 of 11
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received November 20, 2014
Description Andrex Industries
Sample ID RW-1
Collected By Benjamin P. Nisbeth
Collection Date 11/18/14 12:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 04,2014
ESC Sample # : L734762-02
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
170000
Volatile Organics
Acetone
160
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
1.7
cis-1,2-Dichloroethene
3300
trans-1,2-Dichloroethene
12.
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
100000
ug/l
9060A
11/26/14
100
50.
ug/l
8260B
12/03/14
1
50.
ug/1
8260B
12/03/14
1
10.
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
50.
ug/1
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
2.5
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
100
ug/l
8260B
11/28/14
100
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
Page 4 of 11

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received November 20, 2014
Description Andrex Industries
Sample ID RW-1
Collected By Benjamin P. Nisbeth
Collection Date 11/18/14 12:00
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 04,2014
ESC Sample # : L734762-02
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
12/03/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
12/03/14
2-Butanone (MEK)
140
10.
ug/l
8260B
12/03/14
Methylene Chloride
BDL
5.0
ug/l
8260B
12/03/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
12/03/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
12/03/14
Naphthalene
BDL
5.0
ug/1
8260B
12/03/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
12/03/14
Styrene
BDL
1.0
ug/1
8260B
12/03/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
12/03/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
12/03/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
12/03/14
Tetrachloroethene
3.5
1.0
ug/1
8260B
12/03/14
Toluene
13.
5.0
ug/1
8260B
12/03/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
12/03/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
12/03/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
12/03/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
12/03/14
Trichloroethene
6.7
1.0
ug/1
8260B
12/03/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
12/03/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
12/03/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
12/03/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
12/03/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
12/03/14
Vinyl chloride
77.
1.0
ug/1
8260B
12/03/14
Xylenes, Total
BDL
3.0
ug/l
8260B
12/03/14
Surrogate Recovery
Toluene-d8
103.
% Rec.
8260B
12/03/14
Dibromofluoromethane
ill.
% Rec.
8260B
12/03/14
4-Bromofluorobenzene
101.
% Rec.
8260B
12/03/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 12/01/14 19:30 Revised: 12/04/14 08:51
Page 5 of 11
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received November 20, 2014
Description Andrex Industries
Sample ID MW-6
Collected By Benjamin P. Nisbeth
Collection Date 11/18/14 11:20
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 04,2014
ESC Sample # : L734762-03
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
2000
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
1.5
cis-1,2-Dichloroethene
1300
trans-1,2-Dichloroethene
3.8
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 11/26/14 1
50.
ug/l
8260B
12/03/14
1
50.
ug/1
8260B
12/03/14
1
10.
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
50.
ug/1
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
2.5
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
5.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
50.
ug/l
8260B
11/28/14
50
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
1.0
ug/l
8260B
12/03/14
1
1.0
ug/1
8260B
12/03/14
1
Page 6 of 11

Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received November 20, 2014
Description Andrex Industries
Sample ID MW-6
Collected By Benjamin P. Nisbeth
Collection Date 11/18/14 11:20
Parameter
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 04,2014
ESC Sample # : L734762-03
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Result Det. Limit Units Method Date Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
12/03/14
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
12/03/14
2-Butanone (MEK)
BDL
10.
ug/l
8260B
12/03/14
Methylene Chloride
BDL
5.0
ug/l
8260B
12/03/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
12/03/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
12/03/14
Naphthalene
BDL
5.0
ug/1
8260B
12/03/14
n-Propylbenzene
BDL
1.0
ug/1
8260B
12/03/14
Styrene
BDL
1.0
ug/1
8260B
12/03/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
12/03/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
12/03/14
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
12/03/14
Tetrachloroethene
1400
50.
ug/1
8260B
11/28/14
Toluene
BDL
5.0
ug/1
8260B
12/03/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
12/03/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
12/03/14
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
12/03/14
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
12/03/14
Trichloroethene
76.
1.0
ug/1
8260B
12/03/14
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
12/03/14
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
12/03/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
12/03/14
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
12/03/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
12/03/14
Vinyl chloride
12.
1.0
ug/1
8260B
12/03/14
Xylenes, Total
BDL
3.0
ug/l
8260B
12/03/14
Surrogate Recovery
Toluene-d8
98.5
% Rec.
8260B
12/03/14
Dibromofluoromethane
107.
% Rec.
8260B
12/03/14
4-Bromofluorobenzene
99.7
% Rec.
8260B
12/03/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 12/01/14 19:30 Revised: 12/04/14 08:51
Page 7 of 11
1
1
1
1
1
1
1
1
1
1
1
1
50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1

REPORT OF ANALYSIS
Mr. Andy Alexander
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
Date Received November 20, 2014
Description Andrex Industries
Sample ID MW-44
Collected By Benjamin P. Nisbeth
Collection Date 11/18/14 11:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 04,2014
ESC Sample # : L734762-04
Site ID : ASHEVILLE, NC
Project # J14-1022-40
Parameter Result Det. Limit Units Method Date Dil.
TOC (Total Organic Carbon)
BDL
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
1100
trans-1,2-Dichloroethene
5.5
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
1000 ug/l 9060A 11/26/14 1
50.
ug/l
8260B
12/03/14 1
50.
ug/1
8260B
12/03/14 1
10.
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
5.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
5.0
ug/1
8260B
12/03/14 1
50.
ug/1
8260B
12/03/14 1
5.0
ug/1
8260B
12/03/14 1
2.5
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
5.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
5.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
10.
ug/l
8260B
11/29/14 10
1.0
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
1.0
ug/l
8260B
12/03/14 1
1.0
ug/1
8260B
12/03/14 1
Page 8 of 11

12065
Lebanon Rd.
Mt. Juliet,
TN 37122
(615)
758-5858
1-800-767-5859
Fax (615)
758-5859
Tax I.D.
62-0814289
Est.
1970
REPORT
OF ANALYSIS
Mr. Andy Alexander
December
04,2014
Bunnell - Lammons Engineering, Inc.
6004 Ponders Court
Greenville, SC 29615
ESC
Sample #
L734762-04
Date Received November 20, 2014
Description Andrex Industries
Site
ID
ASHEVILLE, NC
Sample ID MW-44
Project
#
J14-1022-40
Collected By Benjamin P. Nisbeth
Collection Date 11/18/14 11:00
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
Isopropylbenzene
BDL
1.0
ug/l
8260B
12/03/14
1
p-Isopropyltoluene
BDL
1.0
ug/1
8260B
12/03/14
1
2-Butanone (MEK)
BDL
10.
ug/l
8260B
12/03/14
1
Methylene Chloride
BDL
5.0
ug/l
8260B
12/03/14
1
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
8260B
12/03/14
1
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
12/03/14
1
Naphthalene
BDL
5.0
ug/1
8260B
12/03/14
1
n-Propylbenzene
BDL
1.0
ug/1
8260B
12/03/14
1
Styrene
BDL
1.0
ug/1
8260B
12/03/14
1
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
12/03/14
1
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
12/03/14
1
1,1,2-Trichlorotrifluoroethane
BDL
1.0
ug/l
8260B
12/03/14
1
Tetrachloroethene
5000
100
ug/1
8260B
11/26/14
100
Toluene
BDL
5.0
ug/1
8260B
12/03/14
1
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
12/03/14
1
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
12/03/14
1
1,1,1-Trichloroethane
BDL
1.0
ug/l
8260B
12/03/14
1
1,1,2-Trichloroethane
BDL
1.0
ug/1
8260B
12/03/14
1
Trichloroethene
180
1.0
ug/1
8260B
12/03/14
1
Trichlorofluoromethane
BDL
5.0
ug/1
8260B
12/03/14
1
1,2,3-Trichloropropane
BDL
2.5
ug/l
8260B
12/03/14
1
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
8260B
12/03/14
1
1,2,3-Trimethylbenzene
BDL
1.0
ug/l
8260B
12/03/14
1
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
12/03/14
1
Vinyl chloride
48.
1.0
ug/1
8260B
12/03/14
1
Xylenes, Total
BDL
3.0
ug/l
8260B
12/03/14
1
Surrogate Recovery
Toluene-d8
99.1
% Rec.
8260B
12/03/14
1
Dibromofluoromethane
102.
% Rec.
8260B
12/03/14
1
4-Bromofluorobenzene
96.9
% Rec.
8260B
12/03/14
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 12/01/14 19:30 Revised: 12/04/14 08:51
Page 9 of 11

Sample
Number
L734762-01
Attachment A
List of Analytes with QC Qualifiers
Work
Sample
Group
Type
Analyte
WG756003
SAMP
Chloroethane
WG756003
SAMP
1,2-Dibromo-3-Chloropropane
WG756003
SAMP
cis-1,2-Dichloroethene
WG756003
SAMP
Naphthalene
Run
ID Qualifier
R3006754 J4
R3006754 J5
R3006754 V
R3006754 J4J5
Page 10 of 11

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J4 The associated batch QC was outside the established quality control range
for accuracy.
J5 The sample matrix interfered with the ability to make any accurate
determination; spike value is high
V (ESC) - Additional QC Info: The sample concentration is too high to
evaluate accurate spike recoveries.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 11 of 11

6llling Info !rnd#ian:
Analysis f Cantairter/ Preservative
I chain DrCas#odx Page —af
Bunnell - Lammons Engineering, Inc. P roie ct man age r
1*ESC
6004 Ponders Court
'
6004 Ponders Court
Greenville, SC 29615
1 n- B s -C - i - E - W. c - E. s
Greenville, 5C 29615
�
RE port to'
Email To-_ andy@ blerorp-ram
#nouns lulie9. TM 37i22 yti rf
.Phara:6k5-756-5as9 I
Mr. Andy Alexander
Phorx: d00-367-Sa59
Fak:6L575A-SA51 �
Prolert
Ci#yf5tME
CalletLed:
f
y
Description: And rex in dustrles
Client Proj@& # Lab Projed A
Phone:[phone]
JS4-1022-40 OUNLAMGSC-J14102240
�
J076
Fax: [phone]
_
---
ColLeC#edby(printj,
Site/FariMYID41 P.0 p
AottnuY BUNLAhAGSC
.��
ASHEVILLE, NC
Template:T984f?1
'WAdate
Caller#ed by (Signtlr�
Results Needed
J4dsb? (Lab MUST Be Notlfled)
�
E
�
Prelogin' P48948�
Same bay ,,.-..,.,�,-.�_.-,.,,,, 20056
—
E
TSR: 350 - JI mrny Bunt
Email?
_No il_Yes
a
PB: - r
Immediately
Patked on Ice N Y
—Two Day -,-,.,,.,.,- �,-,-,-,-,.,,50�6 FAX?
Three Day ............................. SSW
No Yes No
pi
Ln
�
Via' Fed EX 6raund
Sample ID
CUm{�,rab lyldkrixr Depth Date
ntr5
Time
L.)Shipped
00
14xm1CnnurniraqL Sd'p!#ilahnnlyl
G I`
k l -1
X
X
IIN-Z
R-1
G't
1ao 3
x
x
M -6
Gw , '
l{,�, 3
X
X
r3w
3
X
X_
MBIrIX! S5-5ail GN1 Gmurtdwmter AW- Wastewater DYP- drinkingWater OT - Other
pH � Temp
-
emarks-
Flow Other
Hald $1
by:�$i to
Date: TllMe!
ReCeisred by, ISlgnatu--el
Sample return advla: r3 UPS
Conclition: Ilabuse only)
5
ed
01iuishtd
uls 2dby :
date; I Time:
Re[eNed by (SiB�a#urej
Temp Battles Rceed'
ITO
r-oc Seal Intact: /Y _N `NA
Relinquished by' ti
Date: Time-
Receiv tar lab by_J.Signaturej
pate: Time:
pH fICF=

APPENDIX H
TOC
TIME VS. CONCENTRATION PLOTS

7,000
6,000
5,000
J
tw
E
C 4,000
0
c�
3,000
U
C
0
V
2,000
1,000
0
RW-1-- Total Organic Carbon
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
BdTe/I-
<--- Baseline
a
Data --->
O O O O O O O O
N N N N N N N N

4,500
4,000
3,500
3,000
as
E
c 2,500
c�
2,000
a,
U
C
°
V 1,500
1,000
500
❑c
RW-3 -- Total Organic Carbon
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
<--- Baseline Data --->
N N N N N N N N

4,000
3,500
3,000
J
2,500
0
2,000
a,
= 1,500
0
V
1,000
500
11
RW-5 -- Total Organic Carbon
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
I
<--- Baseline Data --->
01 O r-1 N M Ln lD
O O O O O O O O
N N N N N N N N

20 -
15
11
RW-6 -- Total Organic Carbon
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
I <--- Baseline Data ---> I
O 0 r-I
O O O
N N N
N M RT Ln lD
O O O O O
N N N N N

6,000
5,000
4,000
wo
rR
1,000
11
RW-7 -- Total Organic Carbon
O r-I N M Ln lD
O O O O O O O
N N N N N N N

5,000
4,500
►A
3,500
J
3,000
c
0
2,500
c
2,000
c
0
V
1,500
1,000
500
0
IW-2 -- Total Organic Carbon
N N N N N N N N

45
35
J 30
as
E
c 25
0
c�
20
a,
U
C
u° 15
10
5
MW-5--Total Organic Carbon
0 rl 0 � rq � � � rq
N N N N N N N N

35
30
25
10
11
MW-6 -- Total Organic Carbon
M O %_4 N M Ln lD
O O O O O O O O
N N N N N N N N

20 -
15
11
MW-7 -- Total Organic Carbon
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
<--- Baseline Data --->
01 O r-1
O r-I r-I
O O O
N N N
N M 111, Lin lD
O O O O O
N N N N N

MW-9 -- Total Organic Carbon
W111111111111111
Injection RW-1, RW-3, RW-5, & RW-7
35 — Injection RW-1, RW-3, RW-5, & RW-7 —
�Injection RW-1, RW-3, & RW-5
30
J
E
25
0
20
a,
= 15
0
V
10
5
11
Injection IW-2
I <--- Baseline Data ---> I
O 0 r-I
O O O
N N N
N M RT Ln lD
O O O O O
N N N N N

450
gel
350
J 300
wo
0
250
= 200
a,
U
i
150
100
6111
11
MW-10 -- Total Organic Carbon
N N N N N N N N

20
15
11
MW-11-- Total Organic Carbon
ON �%_4-I rN-I �M-I ��-I �Ln-I
N N N N N N N N

1,400
1,200
1,000
J
= 000
0
600
U
i
0
V
m
200
MW-12 -- Total Organic Carbon
ON �V-1-I rN-I �M-I r�-I �Ln-I
N N N N N N N N

20
15
11
MW-13 -- Total Organic Carbon
O0 �%_4-I rN-I �M-I ��-I �Ln-I
N N N N N N N N

20
15
11
MW-14 -- Total Organic Carbon
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
<--- Baseline Data --->
O0 �V-4-I rN-I �M-I rRT-I �Ln-I �ko-I
N N N N N N N N

20
15
11
MW-24 -- Total Organic Carbon
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, RW-5, & RW-7
Injection RW-1, RW-3, & RW-5
Injection IW-2
ON �V-4-I rN-I �M-I �RCT-I �Ln-I �ko-I
N N N N N N N N

20
15
11
MW-44 -- Total Organic Carbon
M O %_4 N M Ln lD
O O O O O O O O
N N N N N N N N

APPENDIX I
VOC
TIME VS. CONCENTRATION PLOTS

25,000
20,000
°;10,000
0
V
5,000
C
Recovery/Injection Well RW-1
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
N N N N N N N N

Recovery/Injection Well RW-3
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
14,000
12,000
10,000
J
tw
= 8,000
O
a-+
6,000
U
i
O
V
4,000
2,000
C
RW-5, & RW-7
& RW-5
RW-5, & RW-7

5,000
4,500
4,000
3,500
J
3,000
c
0
2,500
L
v 2,000
c
O
V
1,500
1,000
500
0
Recovery/Injection Well RW-5
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
01 O r-1 N M R* Ln w
O O O O O O O O
N N N N N N N N

2,500
2,000
°; 1,000
O
V
1 1X
0
Recovery/Injection Well RW-6
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
O0 �T-4-I rN-I �M-I rq:T-I
N N N N N N
e
RW-5, & RW-7
& RW-5
RW-5, & RW-7
Ln 9.0
r-I r-I
N N

Recovery/Injection Well RW-7
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
3,500
Perchloroethene
31000 Trichloroethene
cis- 1,2-DichIoroethene
—FVinyl Chloride
21500 A Injection RW-1, RW-3, RW-5, & RW-7
—J A Injection RW-1, RW-3, & RW-5
txO ♦ Injection RW-1, RW-3, RW-5, & RW-7
= 2,000 A Injection IW-2
O
t�
a-+
1,500
U
_
0 <--- Baseline Data --->
V
1,000
500
0
N
N
N
N
N
N
N
N

Injection Well IW-2
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
250
Perchloroethene
Trichloroethene
200
cis-1,2-Dichloroethene
—HFVinyl Chloride
0 Injection RW-1, RW-3, RW-5, & RW-7
—J
A Injection RW-1, RW-3, & RW-5
txO 150
A Injection RW-1, RW-3, RW-5, & RW-7
.�
_
A Injection IW-2
O
t�
a-+
°; 100
O
V
50
A
8asez
data
N N N

9,000
8,000 -
7,000 -
6,000
aA
c 5,000
= 4,000
a,
U
i
u° 3,000
2,000
1,000
0
Monitoring Well MW-5
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
<--- Baseline Data ---> I-

4,000
3,500
3,000
J
2,500
0
2,000
a,
c 1,500
V
1,000
500
C
Monitoring Well MW-6
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
N N N N N N N N

200
. R
MOIC
140
tw
120
0
100
80
0
V
60
af,
0
Monitoring Well MW-7
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
01 O r-I N M q:T Ln to
O r-I r-I r-I r-I r-I r-I r-I
N N N N N N N N

Monitoring Well MW-9
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
f Perchloroethene
Trichloroethene
5,000 cis-1,2-Dichloroethene
—FVinyl Chloride
A Injection RW-1, RW-3, RW-5, & RW-7
4,000 0 Injection RW-1, RW-3, & RW-5
txO ♦ Injection RW-1, RW-3, RW-5, & RW-7
= 0 Injection IW-2
O
3,000
U
<--- Baseline Data --->
_
u° 2,000
1,000
0
N
-
o
N
N
N
N
N
N
N

4,000
3,500
3,000
J
2,500
c
0
2,000
L
c 1,500
u
1,000
500
0
Monitoring Well MW-10
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
01 O r-I N M R* Ln w
O O O O O O O O
N N N N N N N N

3,000
2,500
2,000
t]A
FAR
C
Monitroing Well MW-11
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
RW-5, & RW-7
& RW-5
RW-5, & RW-7
N N N N N N N

7,000 -
6,000
J
5,000
_
O
4,000
a,
c 3,000
V
2,000
1,000
C
Monitoring Well MW-12
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
Perchloroethene
Trichloroethene
cis-1,2-Dichloroethene
Vinyl Chloride
• Injection RW-1, RW-3, RW-5, & RW-7
0 Injection RW-1, RW-3, & RW-5
♦ Injection RW-1, RW-3, RW-5, & RW-7
• Injection IW-2

1,600
1,400
1,200
J
tw 1,000
rR
800
a-+
c 600
V
Monitroing Well MW-13
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
Oz
Perchloroethene
Trichloroethene
cis-1,2-Dichloroethene
—W-Vinyl Chloride
♦ Injection RW-1, RW-3, RW-5, & RW-7
A Injection IW-2
400 - Baseline Data ---> A Injection RW-1, RW-3, RW-5, & RW-7
A Injection RW-1, RW-3, & RW-5
200
0
O0 �T-1-I rN-I �M-I rq:T-I �Ln-I �9.0-I
N N N N N N N N

2,000
1,800
1,600
1,400
tw
1,200
0
1,000
800
0
V
600
e ff
200
0
Monitroing Well MW-14
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
N N N N N N N N

e
FAR
400
aA
rR
u° 200
MOR
0
Monitroing Well MW-24
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
N N N N N N N N

Monitroing Well MW-44
PCE, TCE, cis-1,2 DCE, & Vinyl Chloride
Perchloroethene
Trichloroethene
5,000 - cis-1,2-Dichloroethene
—FVinyl Chloride
4,000
tw
_
O
3,000
a,
U
_
u° 2,000
1,000
C
A Injection RW-1, RW-3, RW-5, & RW-7
A Injection RW-1, RW-3, & RW-5
♦ Injection RW-1, RW-3, RW-5, & RW-7
A Injection IW-2
Baseline Data --->
AIL AIL
N N N N N N N N